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Sample records for spectrometry x-ray emission

  1. X-ray emission spectroscopy. X-ray fluorescence

    International Nuclear Information System (INIS)

    Despujols, J.

    1992-01-01

    Principles of X-ray emission spectrometry are first recalled, then wave-length dispersive and energy dispersive X-ray fluorescence spectrometer are described. They are essentially designed for qualitative and quantitative analysis of elements (Z>10). Sample preparation, calibration, corrections, interferences, accuracy are reviewed. Examples of use in different industries are given. (71 refs.)

  2. X-ray spectrometry with synchrotron radiation; Roentgenspektrometrie mit Synchrotronstrahlung

    Energy Technology Data Exchange (ETDEWEB)

    Mueller, Matthias [Physikalisch-Technische Bundesanstalt (PTB), Berlin (Germany). Arbeitsgruppe ' Roentgen- und IR-Spektrometrie' ; Gerlach, Martin; Holfelder, Ina; Hoenicke, Philipp; Lubeck, Janin; Nutsch, Andreas; Pollakowski, Beatrix; Streeck, Cornelia; Unterumsberger, Rainer; Weser, Jan; Beckhoff, Burkhard

    2014-12-15

    The X-ray spectrometry of the PTB at the BESSY II storage ring with radiation in the range from 78 eV to 10.5 keV is described. After a description of the instrumentation development reference-sample free X-ray fluorescence analysis, the determination of fundamental atomic parameters, X-ray fluorescence analysis under glance-angle incidence, highly-resolving absorption spectrometry, and emission spectrometry are considered. Finally liquid cells and in-situ measurement techniques are described. (HSI)

  3. Application of X-ray emission techniques for monitoring environmental pollution

    International Nuclear Information System (INIS)

    Bernasconi, G.; Danesi, P.R.; Dargie, M.; Haselberger, N.; Markowicz, A.; Tajani, A.

    1997-01-01

    X-ray emission techniques are versatile and powerful methods used for multielement non-destructive analysis. They include X-ray fluorescence (XRF), particle induced X-ray emission (PIXE), scanning electron microscopy combined with X-ray spectrometry and electron probe microanalysis (EPMA). Since many years the IAEA has utilised and promoted these techniques for the analysis of environmental, biological and geological samples. In this paper recent progress at our laboratory in selected aspects related to the application of X-ray emission techniques is briefly overviewed. (authors)

  4. X-ray fluorescence analysis and optical emission spectrometry of an roman mirror from Tomis, Romania

    International Nuclear Information System (INIS)

    Belc, M.; Bogoi, M.; Ionescu, D.; Guita, D.; Caiteanu, S.; Caiteanu, D.

    2000-01-01

    The miscellaneous population of Roman Empire, their diverse cultural tradition, their ability to assimilate the roman civilization spirits, had determined a permanent reassessment superimposed upon the roman contribution. Analysis was undertaken using optical emission spectrometry and non-destructive X-ray fluorescence. X-ray fluorescence analysis is a well-established method and is often used in archaeometry and other work dealing with valuable objects pertaining to the history of art and civilization. Roman mirror analysed has been found not to be made of speculum (a high tin bronze). (authors)

  5. The Determination of Composite Elements in Zircaloy-2 by X-Ray Fluorescence and Emission Spectrometry Method

    International Nuclear Information System (INIS)

    Dian Anggraini; Rosika Kriswarini; Yusuf N

    2007-01-01

    Analysis of composing elements in zircaloy-2 has been done by Emission Spectrometry method and X-Ray Fluorescence (XRF). The aim of the analysis is to verify conformity between composing elements in zircaloy-2 and the material certificate. Spectrometry Emission method has higher sensitivity in element determination of a material than that of XRF method, so can be estimated that emission spectrometry method has higher accuracy than that of XRF method. The result of qualitative analysis by Emission Spectrometry indicate that the composing elements in zircaloy-2 were Sn, Cr and Ni. However, the qualitative analysis result by XRF method indicated that the composing elements in zircaloy 2 were Sn, Cr, Ni and Fe. Fe element can not be analysed by Emission Spectrometry method because Emission Spectrometer did not equipped with Fe detector. The quantitative analysis result of the composing elements in the material with both methods showed that Sn, Cr and Ni concentration of zircaloy 2 existed in concentration ranges of the material certificate. Result of statistical test (F and t-test) of analysis result of both methods can be used for analyzing composing elements in zircaloy 2. Emission Spectrometry method was more sensitive and accurate for determining Cr and Ni element in zircaloy 2 than that of emission Spectrometry method but both methods had same accuracy. The precision of measurement of Sn, Cr and Ni element using XRF method was better than that of Emission spectrometry method. (author)

  6. Target characterization by PIXE, alpha spectrometry and X-ray absorption

    International Nuclear Information System (INIS)

    Kheswa, N.Y.; Papka, P.; Pineda-Vargas, C.A.; Newman, R.T.

    2011-01-01

    We report on the thickness and homogeneity characterization of thin metallic targets of Zr-96 by means of alpha absorption spectrometry, Particle Induced X-ray Emission (PIXE) and X-ray absorption. The target thicknesses determined by means of the above mentioned methods are critically compared. The thicknesses were determined before and after irradiation with a 70 MeV beam of 14 N ions.

  7. High-Resolution X-ray Emission and X-ray Absorption Spectroscopy

    NARCIS (Netherlands)

    Groot, F.M.F. de

    2000-01-01

    In this review, high-resolution X-ray emission and X-ray absorption spectroscopy will be discussed. The focus is on the 3d transition-metal systems. To understand high-resolution X-ray emission and reso-nant X-ray emission, it is first necessary to spend some time discussing the X-ray absorption

  8. Physical methods for studying minerals and solid materials: X-ray, electron and neutron diffraction; scanning and transmission electron microscopy; X-ray, electron and ion spectrometry

    International Nuclear Information System (INIS)

    Eberhart, J.-P.

    1976-01-01

    The following topics are discussed: theoretical aspects of radiation-matter interactions; production and measurement of radiations (X rays, electrons, neutrons); applications of radiation interactions to the study of crystalline materials. The following techniques are presented: X-ray and neutron diffraction, electron microscopy, electron diffraction, X-ray fluorescence analysis, electron probe microanalysis, surface analysis by electron emission spectrometry (ESCA and Auger electrons), scanning electron microscopy, secondary ion emission analysis [fr

  9. X-ray hot plasma diagnostics

    International Nuclear Information System (INIS)

    Cojocaru, E.

    1984-11-01

    X-ray plasma emission study is powerful diagnostic tool of hot plasmas. In this review article the main techniques of X-ray plasma emission measurement are shortly presented: X-ray spectrometry using absorbent filters, crystal and grating spectrometers, imaging techniques using pinhole cameras, X-ray microscopes and Fresnel zone plate cameras, X-ray plasma emission calorimetry. Advances in these techniques with examples for different hot plasma devices are also presentes. (author)

  10. X-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Ray, N.B.

    1977-01-01

    The principle, instrument and procedure of X-ray fluorescence spectrometry are described. It is a rapid, simple and sensitive method for the trace analysis of elements from sodium to uranium in powder, liquid or metal samples. (M.G.B.)

  11. Assembly of positioner of automated two-dimensional scan coupled to X-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Silva, Leonardo Santiago Melgaço

    2011-01-01

    This work describes the design and assembling of a prototype automated positioner two-dimensional scanning coupled to X-ray fluorescence spectrometry. The work aims to achieve a portable and easy to use, device of broad utility in the analysis of samples by X-ray fluorescence area of expertise and research. The two-dimensional scanning of the positioner is by means of two stepper motors controlled by a microcontroller PIC 16F877A, encoder and optical sensors. The user interacts with the XY table through an interface program for the Windows operating system, which communicates with the microcontroller through the serial port. The system of Fluorescence Spectroscopy incorporated into the positioner consists of a system commercially available system from the company AMPTEK, where the primary source of excitation of the sample was a source of 241 Am of 59.5 KeV emissions. Resolution and accuracy of tests were performed in the XY scanning process and reproducibility of the same kit with the fluorescence spectrometry X-ray. Qualitative tests by X-ray fluorescence spectrometry in samples were performed to demonstrate the applicability and versatility of the project. It follows that the prototype illustrates a possible adequately to portable device for X-ray spectrometry of two-dimensional. (author)

  12. X-ray Emission from Solar Flares

    Indian Academy of Sciences (India)

    2016-01-27

    Jan 27, 2016 ... Solar flares; X-ray detectors; X-ray line emission and continuum; break energy; microflares. Abstract. Solar X-ray Spectrometer (SOXS), the first space-borne solar astronomy experiment of India was designed to improve our current understanding of X-ray emission from the Sun in general and solar flares in ...

  13. X-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Vries, J.L. de.

    1976-01-01

    The seventh edition of Philips' Review of Literature on x-ray fluorescence spectrometry starts with a list of conference proceedings on the subject, organised by the Philips organisation at regular intervals in various European countries. It is followed by a list of bulletins. The bibliography is subdivided according to spectra, equipment, applications and absorption analysis

  14. X-ray spectrometry induced by electron and proton bombardment: Two complementary techniques for the micro-characterization of mineral materials

    International Nuclear Information System (INIS)

    Remond, G.; Gilles, C.; Isabelle, D.; Choi, C.G.; Rouer, O.; Cesbron, F.; Yang, C.

    1994-01-01

    Spatially resolved quantitative analysis by means of the Electron Probe Micro Analyser (EPMA) is now well established as a routine analytical method for point chemical analysis of a variety of mineral materials. Modern computer controlled EPMA are most often equipped with wavelength dispersive spectro- meters (WDS). Quantitative analyses are generally carried out according to a standard based approach, i. e, the x-ray intensities measured at the surface of the unknowns are normalized to those measured at the surface of reference specimens. By the use of energy dispersive spectrometry (EDS) a standardless quantitative based method is preferred when the incident beam current is not accurately known as for the case of EDS analysis coupled to Scanning Electron Microscopy (SEM). The accuracy of point analysis by means of electron beam induced x-ray spectrometry is discussed emphasizing the x-ray photon interactions respectively.The continuous x-ray emission is the physical limit of detection. The excitation conditions must be optimised in order to obtain the higher peak to continuous emission intensity ratios for each element within the matrix. Proton Induced X-ray Emission (PIXE) complements this electron induced x-ray emission for the localization of elements present at trace levels. The experimental procedure used for quantitative analysis by means of PIXE is illustrated emphasizing the use of a limited number of reference materials for deriving quantitative data from the raw PIXE spectra. The complementarity of EMPA/SEM and PIXE techniques is illustrated for the case of rare-earth elements (REE) bearing natural and synthetic doped zircon crystals (Si Zr O sub 4). For such compounds x-ray spectra are very complex because of the existence of severe peak overlaps between the L x-ray emission spectra of the REE. It is shown that cathodoluminescence (EPLA:SEM) and ionoluminescence (PIXE) may be an original alternative approach to x-ray spectrometry for studying REE

  15. X-Ray Emission Properties of Supernova Remnants

    NARCIS (Netherlands)

    Vink, J.; Alsabti, A.W.; Murdin, P.

    2016-01-01

    X-ray emission from supernova remnants can be broadly divided into thermal X-ray emission from the shock-heated plasmas and in nonthermal (synchrotron) emission caused by very high-energy (10–100 TeV) electrons moving in the magnetic fields of the hot plasmas. The thermal X-ray emission of young

  16. Diagnostic X-ray spectrometry using a commercial CdZnTe detector

    International Nuclear Information System (INIS)

    Becker, P.H.B.

    1998-01-01

    X ray spectrometry using Ge or Si detectors is an established tool to measure characterization parameters of X-ray beams. This work describes how a commercial CdZnTe was used to perform diagnostic X-ray spectrometry. Spectra were measured for two X-ray machines and compared with similar data found in the literature with an agreement of 2% rms

  17. X-ray spectrometry for preventive conservation of cultural heritage

    Indian Academy of Sciences (India)

    Analytical chemistry does play a key role in the chemical characterization of the environment and it appears that X-ray spectrometry, in its many forms, is one of the most relevant analytical techniques in preventive conservation, as it is in cultural heritage research in general. X-ray spectrometry has indeed been the method ...

  18. X-ray emission from comets

    International Nuclear Information System (INIS)

    Dennerl, Konrad

    1999-01-01

    When comet Hyakutake (C/1996 B2) encountered Earth in March 1996 at a minimum distance of only 15 million kilometers (40 times the distance of the moon), x-ray and extreme ultraviolet emission was discovered for the first time from a comet. The observations were performed with the astronomy satellites ROSAT and EUVE. A systematic search for x-rays from comets in archival data, obtained during the ROSAT all-sky survey in 1990/91, resulted in the discovery of x-ray emission from four additional comets. They were detected at seven occasions in total, when they were optically 300 to 30 000 times fainter than Hyakutake. These findings indicated that comets represent a new class of celestial x-ray sources. Subsequent detections of x-ray emission from additional comets with the satellites ROSAT, EUVE, and BeppoSAX confirmed this conclusion. The x-ray observations have obviously revealed the presence of a process in comets which had escaped attention until recently. This process is most likely charge exchange between highly charged heavy ions in the solar wind and cometary neutrals. The solar wind, a stream of particles continuously emitted from the sun with ≅ 400 km s -1 , consists predominantly of protons, electrons, and alpha particles, but contains also a small fraction (≅0.1%) of highly charged heavier ions, such as C 6+ ,O 6+ ,Ne 8+ ,Si 9+ ,Fe 11+ . When these ions capture electrons from the cometary gas, they attain highly excited states and radiate a large fraction of their excitation energy in the extreme ultraviolet and x-ray part of the spectrum. Charge exchange reproduces the intensity, the morphology and the spectrum of the observed x-ray emission from comets very well

  19. Efficient high-resolution X-ray emission spectrometry using synchrotron radiation

    International Nuclear Information System (INIS)

    Unterumsberger, Rainer

    2015-01-01

    The aim of the present work is to get access to high-resolution X-Ray Emission Spectrometry (XES) at nanoscaled materials, consisting of light elements and transition metals, by the increase of the sensitivity of a Wavelength-Dispersive Spectrometer (WDS) in the soft X-Ray range. The increase of the sensitivity was achieved by a refocusing of the incident radiation. With the increased sensitivity of the WDS, it was possible to determine the chemical species of different, nominal 100 nm thin titanium oxides. The combination of the refocusing optic and calibrated spectrometer enabled the detection and deconvolution of the L-fluorescence radiation of these nanoscaled titanium oxides. Due to the calibration of the spectrometer, a reliable determination of the transition probabilities of the titanium La- and Ll-fluorescence lines as a function of the chemical state is possible. To the best of my knowledge, the determination of the transition probabilities as a function of the chemical state in the soft X-Ray range has not been investigated yet. The quality of the refocusing was characterized using different diagnostic tools. Vertical full width at half maximum (FWHM) values of the focused beam between 10 μm to 20 μm and horizontal FWHM values between 12 μm and 25 μm could be achieved over an energy range of 180 eV to 1310 eV. Using calibrated photodiodes, it was possible to determine the absolute transmission of the used single bounce monocapillary as well as to monitor the absolute photon flux. By means of the refocusing, it was possible to increase the photon flux by a factor of 4.9 experimentally. The increase of the photon flux enables the analysis of nanoscaled materials with the used spectrometer. This could be shown based on the determination of the lower limit of detection of boron Ka and titanium La. In both cases, the lower limit of detection of 0.4 nm equivalent layer thickness was achieved (about 1.10 -7 g/cm 2 to 2.10 -7 g/cm 2 or 3.10 15 atoms/cm 2 to

  20. Theory of X-ray absorption and emission spectra

    International Nuclear Information System (INIS)

    Mukoyama, Takeshi

    2004-01-01

    Theoretical studies on X-ray absorption and emission spectroscopy are discussed. Simple expressions for X-ray emission rate and X-ray absorption cross section are presented in the dipole approximation. Various atomic models to obtain realistic wave functions and theoretical calculations for X-ray absorption cross sections and X-ray emission rates are described. In the case of molecules and solids, molecular orbital methods for electronic structures and molecular wave functions are discussed. The emphasis is on the procedures to obtain the excited-state and continuum wave functions for molecules and to calculate the multi-center dipole matrix elements. The examples of the calculated X-ray absorption and emission spectra are shown and compared with the experimental results

  1. X-ray and extreme ultraviolet emission from comets

    Science.gov (United States)

    Lisse, C. M.; Cravens, T. E.; Dennerl, K.

    The discovery of high energy X-ray emission in 1996 from C/1996 B2 (Hyakutake) has created a surprising new class of X-ray emitting objects. The original discovery (Lisse et al., 1996) and subsequent detection of X-rays from 17 other comets (Table 1) have shown that the very soft (E < 1 keV) emission is due to an interaction between the solar wind and the comet's atmosphere, and that X-ray emission is a fundamental property of comets. Theoretical and observational work has demonstrated that charge exchange collisions of highly charged solar wind ions with cometary neutral species is the best explanation for the emission. Now a rapidly changing and expanding field, the study of cometary X-ray emission appears to be able to lead us to a better understanding of a number of physical phenomena: the nature of the cometary coma, other sources of X-ray emission in the solar system, the structure of the solar wind in the heliosphere, and the source of the local soft X-ray background.

  2. Major constituent quantitative determination in uranium alloys by coupled plasma atomic emission spectrometry and X ray fluorescence wavelength dispersive spectrometry

    International Nuclear Information System (INIS)

    Oliveira, Luis Claudio de; Silva, Adriana Mascarenhas Martins da; Gomide, Ricardo Goncalves; Silva, Ieda de Souza

    2013-01-01

    A wavelength-dispersive X-ray fluorescence (WD-XRF) spectrometric method for determination of major constituents elements (Zr, Nb, Mo) in Uranium/Zirconium/Niobium and Uranium/Molybdenum alloy samples were developed. The methods use samples taken in the form of chips that were dissolved in hot nitric acid and precipitate particles melted with lithium tetraborate and dissolved in hot nitric acid and finally analyzed as a solution. Studies on the determination by inductively coupled plasma optic emission spectrometry (ICP OES) using matched matrix in calibration curve were developed. The same samples solution were analyzed in both methods. The limits of detection (LOD), linearity of the calibrations curves, recovery study, accuracy and precision of the both techniques were carried out. The results were compared. (author)

  3. Soft x-ray emission from gamma-ray bursts observed with ginga

    International Nuclear Information System (INIS)

    Yoshida, Atsumasa; Murakami, Toshio; Itoh, Masayuki

    1989-01-01

    The soft X-ray emission of gamma-ray bursts below 10 keV provides information about size, location, and emission mechanism. The Gamma-ray Burst Detector (GBD) on board Ginga, which consists of a proportional counter and a scintillation detector, covers an energy range down to 1.5 keV with 63 cm 2 effective area. In several of the observed gamma-ray bursts, the intensity of the soft X-ray emission showed a longer decay time of 50 to 100s after the higher energy gamma-ray emission had ended. Although we cannot rule out other models, such as bremsstrahlung and thermal cyclotron types, due to poor statistics, the soft X-ray spectra are consistent with a blackbody of 1 to 2 keV in the late phase of the gamma-ray bursts. This enables us to estimate the size of the blackbody responsible for the X-ray emission. (author)

  4. SphinX MEASUREMENTS OF THE 2009 SOLAR MINIMUM X-RAY EMISSION

    International Nuclear Information System (INIS)

    Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Bakała, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B.; Kuzin, S.; Farnik, F.; Reale, F.; Phillips, K. J. H.

    2012-01-01

    The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 × 10 47 cm –3 and 1.1 × 10 48 cm –3 . Comparing SphinX emission with that from the Hinode X-ray Telescope, we deduce that most of the emission is from general coronal structures rather than confined features like bright points. For one of 27 intervals of exceptionally low activity identified in the SphinX data, the Sun's X-ray luminosity in an energy range roughly extrapolated to that of ROSAT (0.1-2.4 keV) was less than most nearby K and M dwarfs.

  5. SphinX Measurements of the 2009 Solar Minimum X-Ray Emission

    Science.gov (United States)

    Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Kuzin, S.; Farnik, F.; Reale, F.; Phillips, K. J. H.; Bakała, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B.

    2012-06-01

    The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 × 1047 cm-3 and 1.1 × 1048 cm-3. Comparing SphinX emission with that from the Hinode X-ray Telescope, we deduce that most of the emission is from general coronal structures rather than confined features like bright points. For one of 27 intervals of exceptionally low activity identified in the SphinX data, the Sun's X-ray luminosity in an energy range roughly extrapolated to that of ROSAT (0.1-2.4 keV) was less than most nearby K and M dwarfs.

  6. SphinX MEASUREMENTS OF THE 2009 SOLAR MINIMUM X-RAY EMISSION

    Energy Technology Data Exchange (ETDEWEB)

    Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Bakala, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B. [Space Research Centre, Polish Academy of Sciences, 51-622, Kopernika 11, Wroclaw (Poland); Kuzin, S. [P. N. Lebedev Physical Institute (FIAN), Russian Academy of Sciences, Leninsky Prospect 53, Moscow 119991 (Russian Federation); Farnik, F. [Astronomical Institute, Ondrejov Observatory (Czech Republic); Reale, F. [Dipartimento di Fisica, Universita di Palermo, Palermo, Italy, and INAF, Osservatorio Astronomico di Palermo, Palermo (Italy); Phillips, K. J. H., E-mail: js@cbk.pan.wroc.pl [Mullard Space Science Laboratory, University College London, Holmbury St. Mary, Dorking, Surrey RH5 6NT (United Kingdom)

    2012-06-01

    The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 Multiplication-Sign 10{sup 47} cm{sup -3} and 1.1 Multiplication-Sign 10{sup 48} cm{sup -3}. Comparing SphinX emission with that from the Hinode X-ray Telescope, we deduce that most of the emission is from general coronal structures rather than confined features like bright points. For one of 27 intervals of exceptionally low activity identified in the SphinX data, the Sun's X-ray luminosity in an energy range roughly extrapolated to that of ROSAT (0.1-2.4 keV) was less than most nearby K and M dwarfs.

  7. SphinX MEASUREMENTS OF THE 2009 SOLAR MINIMUM X-RAY EMISSION

    OpenAIRE

    Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Kuzin, S.; Farnik, F.; Reale, F.; Phillips, K. J. H.; Bakala, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B.

    2012-01-01

    The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 x 10^47 cm^-3 and 1.1 x 10^48 cm^-3. Comparing Sph...

  8. Cu,Cr and As determination in preserved woods (Eucalyptus ssp.) by X-ray fluorescence spectrometries

    International Nuclear Information System (INIS)

    Pereira Junior, Sergio Matias

    2014-01-01

    Brazil produces around 2.2 millions of cubic meters of treated wood to meet the annual demand of railway, electric, rural and construction sectors. The most used wood species are eucalyptus (Eucalyptus ssp.) and pine (Pinus ssp.).The treated woods used for poles, sleepers, fence posts and plywoods should be according to Brazilian norms requirements. The most usual wood preservative products used in Brazil are CCA (chromated copper arsenate) and CCB (copper chromium and boron salt). The analytical methods, such as flame atomic absorption spectrometry (FAAS), plasma inductively coupled optical emission spectrometry (ICPOES) and X-ray fluorescence spectrometry (XRFS) have been used for the analytical control of those treatment processes. In this work, the eucalyptus trees (Eucalyptus ssp) samples was obtained from Minas Gerais State, Brazil, cut plantation areas. Under pressure, eucalyptus wood samples were submitted to different concentration of CCA solution reaching 3.9, 6.7, 9.1, 12.4 and 14.0 kg of CCA by m-³ sapwood retentions. Samples in cylinders and sawdust forms were obtained from treated wood samples. Copper, chromium and arsenic determination was performed using the energy dispersive X-ray fluorescence spectrometry (EDXRFS), portable X-ray fluorescence spectrometry (PXRFS), flame atomic absorption spectrometry (FAAS) and instrumental neutron activation analysis. In this work, the method of analysis, sensitivity, precision and accuracy performances of the related techniques were outlined. (author)

  9. Proton induced X-ray emission analysis

    International Nuclear Information System (INIS)

    Khan, Rashiduzzman

    1976-09-01

    The developments in proton induced X-ray emission analysis are reviewed. Techniques for analyzing thick and thin samples of different origin are described. Discussions on the application of proton induced X-ray emission analysis in different fields, comparison of the sensitivity of this method with other analytical techniques, its limitations and possible improvements are presented

  10. X-ray fluorescence imaging with polycapillary X-ray optics

    International Nuclear Information System (INIS)

    Yonehara, Tasuku; Yamaguchi, Makoto; Tsuji, Kouichi

    2010-01-01

    X-ray fluorescence spectrometry imaging is a powerful tool to provide information about the chemical composition and elemental distribution of a specimen. X-ray fluorescence spectrometry images were conventionally obtained by using a μ-X-ray fluorescence spectrometry spectrometer, which requires scanning a sample. Faster X-ray fluorescence spectrometry imaging would be achieved by eliminating the process of sample scanning. Thus, we developed an X-ray fluorescence spectrometry imaging instrument without sample scanning by using polycapillary X-ray optics, which had energy filter characteristics caused by the energy dependence of the total reflection phenomenon. In the present paper, we show that two independent straight polycapillary X-ray optics could be used as an energy filter of X-rays for X-ray fluorescence. Only low energy X-rays were detected when the angle between the two optical axes was increased slightly. Energy-selective X-ray fluorescence spectrometry images with projection mode were taken by using an X-ray CCD camera equipped with two polycapillary optics. It was shown that Fe Kα (6.40 keV) and Cu Kα (8.04 keV) could be discriminated for Fe and Cu foils.

  11. Handbook of X-Ray Data

    CERN Document Server

    Zschornack, Günter

    2007-01-01

    This sourcebook is intended as an X-ray data reference for scientists and engineers working in the field of energy or wavelength dispersive X-ray spectrometry and related fields of basic and applied research, technology, or process and quality controlling. In a concise and informative manner, the most important data connected with the emission of characteristic X-ray lines are tabulated for all elements up to Z = 95 (Americium). This includes X-ray energies, emission rates and widths as well as level characteristics such as binding energies, fluorescence yields, level widths and absorption edges. The tabulated data are characterized and, in most cases, evaluated. Furthermore, all important processes and phenomena connected with the production, emission and detection of characteristic X-rays are discussed. This reference book addresses all researchers and practitioners working with X-ray radiation and fills a gap in the available literature.

  12. Chemical effects in x-ray emission spectra

    International Nuclear Information System (INIS)

    Fernandes, N.G.

    1982-01-01

    The chemical bond influence in X-ray emission spectra of hafnium, iodine, iron, sulphur, aluminium and magnesium is detected. The position of one X-ray emission line is determined by three methods: parabolic profile; Gaussian distribution and extra-heavy maximum. (author)

  13. Use of X-Ray Fluorescence Spectrometry to Determine Trace ...

    African Journals Online (AJOL)

    This paper deals with application of X-ray fluorescence spectrometry for the detection of trace elements in graphic. An X-ray spectrometer was constructed and used to carry out measurements on graphite spheres impregnated with different chemical elements. The intensities of the lines of these trace elements, as function of ...

  14. X-ray Emission Line Spectroscopy of Nearby Galaxies

    Science.gov (United States)

    Wang, Daniel

    What are the origins of the diffuse soft X-ray emission from non-AGN galaxies? Preliminary analysis of XMM-Newton RGS spectra shows that a substantial fraction of the emission cannot arise from optically-thin thermal plasma, as commonly assumed, and may originate in charge exchange at the interface with neutral gas. We request the support for a comprehensive observing, data analysis, and modeling program to spectroscopically determine the origins of the emission. First, we will use our scheduled XMM-Newton AO-10 368 ks observations of the nearest compact elliptical galaxy M32 to obtain the first spectroscopic calibration of the cumulative soft X-ray emission from the old stellar population and will develop a spectral model for the charge exchange, as well as analysis tools to measure the spatial and kinematic properties of the X-ray line- emitting plasma. Second, we will characterize the truly diffuse emission from the hot plasma and/or its interplay with the neutral gas in a sample of galactic spheroids and active star forming/starburst regions in nearby galaxies observed by XMM-Newton. In particular, we will map out the spatial distributions of key emission lines and measure (or tightly constrain) the kinematics of hot plasma outflows for a few X-ray-emitting regions with high-quality RGS data. For galaxies with insufficient counting statistics in individual emission lines, we will conduct a spectral stacking analysis to constrain the average properties of the X-ray-emitting plasma. We will use the results of these X-ray spectroscopic analyses, together with complementary X-ray CCD imaging/spectral data and observations in other wavelength bands, to test the models of the emission. In addition to the charge exchange, alternative scenarios such as resonance scattering and relic AGN photo-ionization will also be examined for suitable regions. These studies are important to the understanding of the relationship between the diffuse soft X-ray emission and various

  15. X-Ray-Driven Gamma Emission

    International Nuclear Information System (INIS)

    Carroll, J. J.; Karamian, S. A.; Rivlin, L. A.; Zadernovsky, A. A.

    2001-01-01

    X-ray-driven gamma emission describes processes that may release nuclear energy in a 'clean' way, as bursts of incoherent or coherent gamma rays without the production of radioactive by-products. Over the past decade, studies in this area, as a part of the larger field of quantum nucleonics, have gained tremendous momentum. Since 1987 it has been established that photons could trigger gamma emission from a long-lived metastable nuclear excited state of one nuclide and it appears likely that triggering in other isotopes will be demonstrated conclusively in the near future. With these experimental results have come new proposals for the creation of collective and avalanche-like incoherent gamma-ray bursts and even for the ultimate light source, a gamma-ray laser. Obviously, many applications would benefit from controlled bursts of gamma radiation, whether coherent or not. This paper reviews the experimental results and concepts for the production of gamma rays, driven by externally produced X-rays

  16. X-ray Emission from the Guitar Nebula

    OpenAIRE

    Romani, Roger W.; Cordes, James M.; Yadigaroglu, I. -A.

    1997-01-01

    We have detected weak soft X-ray emission from the Pulsar Wind Nebula trailing the high velocity star PSR 2224+65 (the `Guitar Nebula'). This X-ray flux gives evidence of \\gamma~10^7 eV particles in the pulsar wind and constrains the properties of the post-shock flow. The X-ray emission is most easily understood if the shocked pulsar wind is partly confined in the nebula and if magnetic fields in this zone can grow to near equipartition values.

  17. X-Ray Emission from the Guitar Nebula

    Science.gov (United States)

    Romani, Roger W.; Cordes, James M.; Yadigaroglu, I.-A.

    1997-01-01

    We have detected weak soft X-ray emission from the pulsar wind nebula trailing the high-velocity star PSR 2224+65 (the "Guitar Nebula"). This X-ray flux gives evidence of gamma approximately 10(exp 7) eV particles in the pulsar wind and constrains the properties of the postshock flow. The X-ray emission is most easily understood if the shocked pulsar wind is partly confined in the nebula and if magnetic fields in this zone can grow to near-equipartition values.

  18. Radio and X-ray emission from supernova remnants

    International Nuclear Information System (INIS)

    Asvarova, A.I.; Novruzova, H.I.; Ahmedova, S.I.

    2010-01-01

    In this paper it was studied the statistical correlation between radio and X-ray emissions from shell-type supernova remnants (SNR). The primary aim of this study is to test the model of radio emission of shell-type SNRs presented by one of the authors. Based on this model of radio emission, by using the Monte Carlo techniques we have simulated statistical relations radio - X-ray luminosities (not surface brightnesses) which then were compared with the observations. X-ray emission is assumed to be thermal. To have a uniform statistical material it was used observational data on the SNRs in Magellanic Clouds

  19. Development of a portable system of X-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Mantuano, Andrea; Crisostomo, Jose V.V.; Barros, Mariana J.; Oliveira, Luis F.; Barroso, Regina C.

    2009-01-01

    This paper develops a compact and portable spectrometry system that will be used at the Laboratory of Applied Physics to the Biomedical and Environmental Sciences of the Institute of Physics/UERJ, Rio de Janeiro, Brazil. The laboratory both prepares the samples and develops the X-ray spectrometry techniques. The techniques of X-ray diffraction and fluorescence on various samples (biological, industrial and environmental) are used, attending to pos-graduation and graduation students, with multidisciplinary characteristics. The Mini-X system consists of X-ray mini tube MINI-X from Amptek with tungsten (W) target, and a compact spectrometer X123, also from Amptek that includes a detector, pre-amplifier, digital pulse processor, and multichannel. All the system is controlled by dedicated microprocessor. This work will present both a methodology for alignment and calibration of the system as far the first measurements performed using the X-ray fluorescence technique on standard samples. The multi elementary analysis by X-ray fluorescence (XRF) is based on the measurements of the characteristic X-ray intensity emitted by the chemical elements components of the samples when excited. Therefore, from the development of this compact and versatile system it will be possible to obtain the fluorescent intensities of the analysed samples at the Laboratory, not only at the research area but at the teaching area. Besides, new laboratory practices are being developed for the discipline of medical physics

  20. X-ray spectrometry

    International Nuclear Information System (INIS)

    Markowicz, A.A.; Van Grieken, R.E.

    1986-01-01

    In the period under review, i.e, through 1984 and 1985, some 600 articles on XRS (X-ray spectrometry) were published; most of these have been scanned and the most fundamental ones are discussed. All references will refer to English-language articles, unless states otherwise. Also general books have appeared on quantitative EPXMA (electron-probe X-ray microanalysis) and analytical electron microscopy (AEM) as well as an extensive review on the application of XRS to trace analysis of environmental samples. In the period under review no radically new developments have been seen in XRS. However, significant improvements have been made. Gain in intensities has been achieved by more efficient excitation, higher reflectivity of dispersing media, and better geometry. Better understanding of the physical process of photon- and electron-specimen interactions led to complex but more accurate equations for correction of various interelement effects. Extensive use of micro- and minicomputers now enables fully automatic operation, including qualitative analysis. However, sample preparation and presentation still put a limit to further progress. Although some authors find XRS in the phase of stabilization or even stagnation, further gradual developments are expected, particularly toward more dedicated equipment, advanced automation, and image analysis systems. Ways are outlined in which XRS has been improved in the 2 last years by excitation, detection, instrumental, methodological, and theoretical advances. 340 references

  1. Proton Induced X-Rays Emission (PIXE) and Atomic Absorption Spectrometry (AAS) applied in the environmental sample analysis

    International Nuclear Information System (INIS)

    Popescu, Ion V.; Iordan, M.; Stihi, C.; Bancuta, A.; Dima, G.; Busuioc, G.; Ciupina, V.; Belc, M.; Badica, T.

    2003-01-01

    The aim of this work is to determine the elemental composition of tree leaves using Proton-Induced X-Rays Emission (PIXE) and Atomic Absorption Spectrophotometry (AAS) methods. By PIXE Spectrometry we identified and determined the concentration of S, Cl, K, Ca, Ti, Cr, Mn, Fe, Co, Ni, Cu Zn, As, Br, Sr and by AAS method the concentration of elements: Cr, Mn, Fe, Co, Cu, Zn, Se, Cd. Pb was identified in only 2 samples from 29. For tree leave samples collected at a large distance to the polluting source the Sr concentration decreased and the Mg, Ca, Se, Zn and Fe concentrations increased. Also, we can observe a small affinity of these leaves for the environmental Pb which was detected for two samples at a small distance to polluting source. (authors)

  2. Determination of rare-earth elements in rocks by isotope-excited X-ray fluorescence spectrometry

    DEFF Research Database (Denmark)

    Kunzendorf, Helmar; Wollenberg, H.A.

    1970-01-01

    Isotope-excited X-ray fluorescence spectrometry furnishes a rapid determination of rare-earth elements in unprepared rock samples. The samples are excited by 241Am γ-rays, generating X-ray spectra on a multichannel pulse-height analyser. Gaussian peaks of the Kα and Kβ X-ray energies are treated ......-ray spectrometric scan of a longitudinally sliced drill core showed a close correlation between rare-earth abundances and appropriate minerals.......Isotope-excited X-ray fluorescence spectrometry furnishes a rapid determination of rare-earth elements in unprepared rock samples. The samples are excited by 241Am γ-rays, generating X-ray spectra on a multichannel pulse-height analyser. Gaussian peaks of the Kα and Kβ X-ray energies are treated...

  3. use of x-ray fluorescence spectrometry to determine trace elements ...

    African Journals Online (AJOL)

    NIJOTECH

    Abstract. This paper deals with application of X-ray fluorescence spectrometry for the detection of trace elements in graphic. An X-ray spectrometer was constructed and used to carry out measurements on graphite spheres impregnated with different chemical elements. The intensities of the lines of these trace elements, ...

  4. X-ray fluorescence spectrometry - an introduction course

    International Nuclear Information System (INIS)

    Salvador, V.L.R.

    1989-01-01

    The theoretical and experimental principles of the X-ray fluorescence spectrometry, is presented the text is a synthesis of the most important literature in this area. The authors included are: E.P. Bertin, R. Jenkins, J.L. Devries, R. Muller, R. Tertian, F. Claisse e K.L. Willians. (author)

  5. The application of X-ray fluorescence spectrometry to prospecting potential gold deposits

    International Nuclear Information System (INIS)

    Shang Fengjun; Wang Haixia; Zhou Rongsheng

    2001-01-01

    The fieldwork high-sensitivity X-ray fluorescence analysis (FXFA) adopting miniaturized X-ray tube, Si-PIN detector with peltier cooler and notebook PC spectrometry is presented. Using this system, the authors carried out a preliminary research of its application to some gold mine in Sichuan. According to the close relationship between the high-grade element arsenic and gold in ore-forming components, X-ray fluorescence spectrometry can be used to reveal the existence of potential gold mineralization in fields rapidly. This is of great significance in guiding the field geological collection

  6. Observational Trends of Cometary X-ray Emission

    Science.gov (United States)

    Lisse, C. M.

    2001-05-01

    The unexpected discovery of x-ray emission from Comet Hyakutake in March 1996 (Lisse et al. 1996) has produced a number of questions about the physical mechanism producing the radiation. The original detection and subsequent observations (Dennerl et al. 1997, Mumma et al. 1997, Krasnopolsky et al. 1998, Owens et al. 1998, Lisse et al. 1999, Lisse et a. 2001, Dennerl et al. 2001) have shown that the very soft (best fit thermal bremsstrahlung model kT = 0.23 keV) emission is due to an interaction between the solar wind and the comet's atmosphere. Using the results from the more than 15 comets detected to date in x-rays, we report on the latest results on cometary x-ray emission. Our emphasis will be on understanding the physical mechanism producing the emission, and using this to determine the nature of the cometary coma and solar wind flux. As-observed morphologies, spectra, and light curves will be discussed. We also report on the status of current cometary observations using the new powerful x-ray observatories Chandra and XMM. This work has been graciously supported by grants from the NASA Planetary Astronomy and Astrophysical Data Programs.

  7. Compilation of monographs on α-, β-, γ- and X-ray spectrometry

    International Nuclear Information System (INIS)

    Debertin, K.

    1977-11-01

    The working group 'α-, β-, γ-Ray Spectrometry' of the International Committee for Radionuclide Metrology (ICRM) compiled about 35 monographs on α-, β-, γ- and X-ray spectrometry which were published in the years 1970 to 1976. Support was obtained by the Zentralstelle fuer Atomkernenergie-Dokumentation (ZAED) in Karlsruhe. (orig.) [de

  8. Certification of reference materials by energy-dispersive x-ray fluorescence spectrometry?

    DEFF Research Database (Denmark)

    Christensen, Leif Højslet; Heydorn, Kaj

    1985-01-01

    This paper studies the precision and accuracy that can be achieved using energy-dispersive x-ray fluorescence spectrometry for the determination of total sulphur content in BCR 38 Fly Ash issued by the European Community Bureau of Reference.......This paper studies the precision and accuracy that can be achieved using energy-dispersive x-ray fluorescence spectrometry for the determination of total sulphur content in BCR 38 Fly Ash issued by the European Community Bureau of Reference....

  9. Scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX) and aerosol time-of-flight mass spectrometry (ATOFMS) single particle analysis of metallurgy plant emissions.

    Science.gov (United States)

    Arndt, J; Deboudt, K; Anderson, A; Blondel, A; Eliet, S; Flament, P; Fourmentin, M; Healy, R M; Savary, V; Setyan, A; Wenger, J C

    2016-03-01

    The chemical composition of single particles deposited on industrial filters located in three different chimneys of an iron-manganese (Fe-Mn) alloy manufacturing plant have been compared using aerosol time-of-flight mass spectrometry (ATOFMS) and scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX). Very similar types of particles were observed using both analytical techniques. Calcium-containing particles dominated in the firing area of the sintering unit, Mn and/or Al-bearing particles were observed at the cooling area of the sintering unit, while Mn-containing particles were dominant at the smelting unit. SEM-EDX analysis of particles collected downstream of the industrial filters showed that the composition of the particles emitted from the chimneys is very similar to those collected on the filters. ATOFMS analysis of ore samples was also performed to identify particulate emissions that could be generated by wind erosion and manual activities. Specific particle types have been identified for each emission source (chimneys and ore piles) and can be used as tracers for source apportionment of ambient PM measured in the vicinity of the industrial site. Copyright © 2015 Elsevier Ltd. All rights reserved.

  10. Neutron and X-ray emission studies in a low energy plasma focus

    Energy Technology Data Exchange (ETDEWEB)

    Zakaullah, M. [Quaid-i-Azam Univ., Islamabad (Pakistan). Dept. of Physics; Murtaza, G. [Quaid-i-Azam Univ., Islamabad (Pakistan). Dept. of Physics; Qamar, S. [Quaid-i-Azam Univ., Islamabad (Pakistan). Dept. of Physics; Ahmad, I. [Quaid-i-Azam Univ., Islamabad (Pakistan). Dept. of Physics; Beg, M.M. [Quaid-i-Azam Univ., Islamabad (Pakistan). Dept. of Physics

    1996-03-01

    In a low energy Mather-type plasma focus energized by a single 32 {mu}F capacitor, the X-ray and neutron emission is investigated using time-integrated and time-resolved detectors. The X-ray emission profile has a width (FWHM) of 40-50 ns. The neutron emission profile is broader compared to the X-ray emission profile and also delayed by 30-40 ns. To identify different regimes of X-ray emission, an X-ray pin-hole camera along with different absorption filters is employed. While the X-ray emission is high within a narrow pressure range of 2.0-2.5 mbar, the neutron emission is intense for a wider range of 1.0-4.5 mbar. The intense X-ray emission seems to originate from the axially moving shock wave. These results also indicate rather different production mechanisms for X-ray and neutron emission. Also on comparing the X-ray images with Al(2 {mu}m), Al(5 {mu}m), Al(9 {mu}m) filters, we find that the bulk of X-rays from the focus filament have energies less than 2 keV. (orig.).

  11. THERMAL X-RAY EMISSION FROM THE SHOCKED STELLAR WIND OF PULSAR GAMMA-RAY BINARIES

    Energy Technology Data Exchange (ETDEWEB)

    Zabalza, V.; Paredes, J. M. [Departament d' Astronomia i Meteorologia, Institut de Ciencies del Cosmos (ICC), Universitat de Barcelona (IEEC-UB), Marti i Franques 1, E08028 Barcelona (Spain); Bosch-Ramon, V., E-mail: vzabalza@am.ub.es [Dublin Institute for Advanced Studies, 31 Fitzwilliam Place, Dublin 2 (Ireland)

    2011-12-10

    Gamma-ray-loud X-ray binaries are binary systems that show non-thermal broadband emission from radio to gamma rays. If the system comprises a massive star and a young non-accreting pulsar, their winds will collide producing broadband non-thermal emission, most likely originated in the shocked pulsar wind. Thermal X-ray emission is expected from the shocked stellar wind, but until now it has neither been detected nor studied in the context of gamma-ray binaries. We present a semi-analytic model of the thermal X-ray emission from the shocked stellar wind in pulsar gamma-ray binaries, and find that the thermal X-ray emission increases monotonically with the pulsar spin-down luminosity, reaching luminosities of the order of 10{sup 33} erg s{sup -1}. The lack of thermal features in the X-ray spectrum of gamma-ray binaries can then be used to constrain the properties of the pulsar and stellar winds. By fitting the observed X-ray spectra of gamma-ray binaries with a source model composed of an absorbed non-thermal power law and the computed thermal X-ray emission, we are able to derive upper limits on the spin-down luminosity of the putative pulsar. We applied this method to LS 5039, the only gamma-ray binary with a radial, powerful wind, and obtain an upper limit on the pulsar spin-down luminosity of {approx}6 Multiplication-Sign 10{sup 36} erg s{sup -1}. Given the energetic constraints from its high-energy gamma-ray emission, a non-thermal to spin-down luminosity ratio very close to unity may be required.

  12. Determination of impurities in silicon nitride by particle induced x-ray emission analysis

    International Nuclear Information System (INIS)

    Miyagawa, Yoshiko; Saito, Kazuo; Niwa, Hiroaki; Ishizuka, Toshio; Miyagawa, Soji

    1985-01-01

    A method is presented for quantitative particle induced X-ray emission (PIXE) analysis of impurities in the thick samples of silicon nitride. In the analysis of ceramic materials such as silicon nitride, chemical treatments are required to prepare thin enough samples. However, the chemical treatments are undesirable for the PIXE analysis, because another complications are brought about. Our method does not need any chemical treatments and thick samples can be subjected to the measurements. The determination of impurities were made by on-line use of a personal computer in which standard X-ray intensity data were stored. The method and procedures are as follows: After subtracting a buckground spectrum from an observed PIXE spectrum, the resultant peaks are assigned to individual elements. Then, in order to determine the contents of the impurities, the intensity of each peak is compared with a Gaussian curve which is generated from the standard X-ray intensity data. The latter data were determined theoretically. The results were in satisfactory agreement with those obtained by ICP emission spectrometry. (author)

  13. Determination of chlorine in coal by X-ray fluorescence spectrometry method

    Energy Technology Data Exchange (ETDEWEB)

    Marek, S.; Bojarska, K. [Central Mining Institute, Katowice (Poland). Dept. of Environmental Monitoring

    1997-12-31

    Determination of chlorine contents in coal is essential for both environmental protection and its technological use. The existing method of chlorine determination in coal are titration methods which have considerable errors particularly in the low concentration range. The elaborated method with the use of X-ray fluorescence spectrometry in a comparison to the other methods is much faster and has better precision and accuracy. The principle of the method lies in the measurement of X-ray fluorescence radiation intensity which is emitted by chlorine in a sample and its comparison with standards. The calibration of the elaborated XRF method is based on natural coals having various concentrations of chlorine within the whole range of its occurrence in Polish coals. Concentrations for the calibration purpose were obtained by the determination of chlorine contents in selected coals by atomic absorption spectrometry method. The procedure of sample preparation for direct X-ray measurements, instrumental measuring conditions and the way of calibration curve preparation are described in the paper. All X-ray measurements were done with a Phillips sequential X-ray fluorescence spectrometer. A double anode Cr-Au X-ray tube with maximum power 3000 MW was used as the excitation source. 5 figs., 4 tabs.

  14. Correlation between X-ray and high energy gamma-ray emission form Cygnus X-3

    International Nuclear Information System (INIS)

    Weekes, T.C.; Danaher, S.; Fegan, D.J.; Porter, N.A.

    1981-01-01

    In May-June 1980, the 4.8 hour modulated X-ray flux from Cygnus X-3 underwent a significant change in the shape of the light curve; this change correlates with the peak in the high-energy (E > 2 x 10 12 eV) gamma ray emission at the same epoch. (orig.)

  15. Observations of EUV and X-ray Emission from Comets

    Science.gov (United States)

    Lisse, C.

    The unexpected discovery of x-ray emission from Comet Hyakutake in March 1996 (Lisse et al. 1996) produced a number of questions about the physical mechanism producing the radiation. The original detection and subsequent observations have shown that the very soft (best fit thermal bremsstrahlung model kT0.2 keV) emission is due to an interaction between the solar wind and the comet's atmosphere. Using the results from the more than 15 comets detected to date in x-rays, I report here on the latest results on cometary x-ray emission, including new results from Chandra, and show that charge exchange between highly ionized minor ions in the solar wind and neutral gases in the cometary coma is the most likely operative mechanism. I then use this result to study a number of problems of astrophysical interest: the nature of the cometary coma, other possible sources of x-ray emission in the solar system, the structure of the solar wind in the heliosphere, and the source of the local x-ray background.

  16. Discovery of Diffuse Hard X-ray Emission associated with Jupiter

    Science.gov (United States)

    Ezoe, Y.; Miyoshi, Y.; Ishikawa, K.; Ohashi, T.; Terada, N.; Uchiyama, Y.; Negoro, H.

    2009-12-01

    Our discovery of diffuse hard (1-5 keV) X-ray emission around Jupiter is reported. Recent Chandra and XMM-Newton observations revealed several types of X-rays in the vicinity of Jupiter such as auroral and disk emission from Jupiter and faint diffuse X-rays from the Io Plasma Torus (see Bhardwaj et al. 2007 for review). To investigate possible diffuse hard X-ray emission around Jupiter with the highest sensitivity, we conducted data analysis of Suzaku XIS observations of Jupiter on Feb 2006. After removing satellite and planetary orbital motions, we detected a significant diffuse X-ray emission extending to ~6 x 3 arcmin with the 1-5 keV X-ray luminosity of ~3e15 erg/s. The emitting region very well coincided with the Jupiter's radiation belts. The 1-5 keV X-ray spectrum was represented by a simple power law model with a photon index of 1.4. Such a flat continuum strongly suggests non-thermal origin. Although such an emission can be originated from multiple background point sources, its possibility is quite low. We hence examined three mechanisms, assuming that the emission is truly diffuse: bremsstrahlung by keV electrons, synchrotron emission by TeV electrons, and inverse Compton scattering of solar photons by MeV electrons. The former two can be rejected because of the X-ray spectral shape and implausible existence of TeV electrons around Jupiter, respectively. The last possibility was found to be possible because tens MeV electrons, which have been confirmed in inner radiation belts (Bolton et al. 2002), can kick solar photons to the keV energy range and provide a simple power-law continuum. We estimated an average electron density from the X-ray luminosity assuming the oblate spheroid shaped emitting region with 8 x 8 x 4 Jovian radii. The necessary density was 0.02 1/cm3 for 50 MeV electrons. Hence, our results may suggest a new particle acceleration phenomenon around Jupiter.

  17. Observing Solvation Dynamics with Simultaneous Femtosecond X-ray Emission Spectroscopy and X-ray Scattering

    DEFF Research Database (Denmark)

    Haldrup, Kristoffer; Gawelda, Wojciech; Abela, Rafael

    2016-01-01

    and structural changes, and local solvent structural changes are desired. We have studied the intra- and intermolecular dynamics of a model chromophore, aqueous [Fe(bpy)3]2+, with complementary X-ray tools in a single experiment exploiting intense XFEL radiation as a probe. We monitored the ultrafast structural...... rearrangement of the solute with X-ray emission spectroscopy, thus establishing time zero for the ensuing X-ray diffuse scattering analysis. The simultaneously recorded X-ray diffuse scattering atterns reveal slower subpicosecond dynamics triggered by the intramolecular structural dynamics of the photoexcited...

  18. Metrology and X-rays emissions

    International Nuclear Information System (INIS)

    Chancel, C.; Schirmann, D.

    1993-01-01

    This scientific journal explains different technologies used to study X-rays emissions hot dense plasmas created by laser at the Dam center of Limeil-Valenton (CEL-V) or created by nuclear fire in the Pacific

  19. Stimulated X-Ray Emission Spectroscopy in Transition Metal Complexes

    Science.gov (United States)

    Kroll, Thomas; Weninger, Clemens; Alonso-Mori, Roberto; Sokaras, Dimosthenis; Zhu, Diling; Mercadier, Laurent; Majety, Vinay P.; Marinelli, Agostino; Lutman, Alberto; Guetg, Marc W.; Decker, Franz-Josef; Boutet, Sébastien; Aquila, Andy; Koglin, Jason; Koralek, Jake; DePonte, Daniel P.; Kern, Jan; Fuller, Franklin D.; Pastor, Ernest; Fransson, Thomas; Zhang, Yu; Yano, Junko; Yachandra, Vittal K.; Rohringer, Nina; Bergmann, Uwe

    2018-03-01

    We report the observation and analysis of the gain curve of amplified K α x-ray emission from solutions of Mn(II) and Mn(VII) complexes using an x-ray free electron laser to create the 1 s core-hole population inversion. We find spectra at amplification levels extending over 4 orders of magnitude until saturation. We observe bandwidths below the Mn 1 s core-hole lifetime broadening in the onset of the stimulated emission. In the exponential amplification regime the resolution corrected spectral width of ˜1.7 eV FWHM is constant over 3 orders of magnitude, pointing to the buildup of transform limited pulses of ˜1 fs duration. Driving the amplification into saturation leads to broadening and a shift of the line. Importantly, the chemical sensitivity of the stimulated x-ray emission to the Mn oxidation state is preserved at power densities of ˜1020 W /cm2 for the incoming x-ray pulses. Differences in signal sensitivity and spectral information compared to conventional (spontaneous) x-ray emission spectroscopy are discussed. Our findings build a baseline for nonlinear x-ray spectroscopy for a wide range of transition metal complexes in inorganic chemistry, catalysis, and materials science.

  20. Development of multilayer optics for X-ray broadband spectrometry of plasma emission

    International Nuclear Information System (INIS)

    Emprin, Benoit

    2014-01-01

    Within the framework of the research on inertial confinement fusion, the 'Commissariat a l'energie atomique et aux energies alternatives' has studied and implemented an absolute calibrated time-Resolved broadband soft x-Ray spectrometer, called 'Diagnostic de Mesure du rayonnement X'. This diagnostic, composed of 20 measurement channels, measures the emitted radiant power from a laser created plasma in the range from 50 eV to 20 keV. We have developed additional measurement channels to obtain redundancy and an improvement in measurement accuracy. The principle of these new channels is based on an original concept to obtain spectral bounded flat-Responses. Two channels have been developed for the 2 - 4 keV and 4 - 6 keV spectral ranges, using aperiodic multilayer mirrors made at the 'Laboratoire Charles Fabry' with Cr/Sc and Ni/W/SiC/W layers respectively. These mirrors were characterized at synchrotron radiation facilities and integrated into the spectrometer. The two new channels were used during laser-Plasma experimental campaigns at the OMEGA laser facility in Rochester (USA). This allowed us to determine directly the radiant power with only one measurement within a certain spectral band, and with a better precision when compared with using standard channels. The results, in good agreement with the standard measurement channels, allowed us to validate the use of aperiodic multilayer mirrors for X-Ray broadband spectrometry. (author) [fr

  1. Analysis of eight argonne premium coal samples by X-ray fluorescence spectrometry

    Science.gov (United States)

    Evans, J.R.; Sellers, G.A.; Johnson, R.G.; Vivit, D.V.; Kent, J.

    1990-01-01

    X-ray fluorescence spectrometric methods were used in the analysis of eight Argonne Premium Coal Samples. Trace elements (Cr, Ni, Cu, Zn, Rb, Sr, Y, Zr, Nb, Ba, La, and Ce) in coal ash were determined by energy-dispersive X-ray fluorescence spectrometry; major elements (Na, Mg, Al, Si, P, S, K, Ca, Ti, Mn, and Fe) in coal ash and trace elements (Cl and P) in whole coal were determined by wavelength-dispersive X-ray fluorescence spectrometry. The results of this study will be used in a geochemical database compiled for these materials from various analytical techniques. The experimental XRF methods and procedures used to determine these major and trace elements are described.

  2. Assembly of positioner of automated two-dimensional scan coupled to X-ray fluorescence spectrometry; Montagem de posicionador de varredura bidimensional automatizada acoplado a espectrometria de fluorescência de raios-X

    Energy Technology Data Exchange (ETDEWEB)

    Silva, Leonardo Santiago Melgaço

    2011-07-01

    This work describes the design and assembling of a prototype automated positioner two-dimensional scanning coupled to X-ray fluorescence spectrometry. The work aims to achieve a portable and easy to use, device of broad utility in the analysis of samples by X-ray fluorescence area of expertise and research. The two-dimensional scanning of the positioner is by means of two stepper motors controlled by a microcontroller PIC 16F877A, encoder and optical sensors. The user interacts with the XY table through an interface program for the Windows operating system, which communicates with the microcontroller through the serial port. The system of Fluorescence Spectroscopy incorporated into the positioner consists of a system commercially available system from the company AMPTEK, where the primary source of excitation of the sample was a source of {sup 241}Am of 59.5 KeV emissions. Resolution and accuracy of tests were performed in the XY scanning process and reproducibility of the same kit with the fluorescence spectrometry X-ray. Qualitative tests by X-ray fluorescence spectrometry in samples were performed to demonstrate the applicability and versatility of the project. It follows that the prototype illustrates a possible adequately to portable device for X-ray spectrometry of two-dimensional. (author)

  3. Comparison of a portable micro-X-ray fluorescence spectrometry with inductively coupled plasma atomic emission spectrometry for the ancient ceramics analysis

    International Nuclear Information System (INIS)

    Papadopoulou, D.N.; Zachariadis, G.A.; Anthemidis, A.N.; Tsirliganis, N.C.; Stratis, J.A.

    2004-01-01

    Two multielement instrumental methods of analysis, micro X-ray fluorescence spectrometry (micro-XRF) and inductively coupled plasma atomic emission spectrometry (ICP-AES) were applied for the analysis of 7th and 5th century B.C. ancient ceramic sherds in order to evaluate the above two methods and to assess the potential to use the current compact and portable micro-XRF instrument for the in situ analysis of ancient ceramics. The distinguishing factor of interest is that micro-XRF spectrometry offers the possibility of a nondestructive analysis, an aspect of primary importance in the compositional analysis of cultural objects. Micro-XRF measurements were performed firstly directly on the ceramic sherds with no special pretreatment apart from surface cleaning (micro-XRF on sherds) and secondly on pressed pellet disks which were prepared for each ceramic sherd (micro-XRF on pellet). For the ICP-AES determination of elements, test solutions were prepared by the application of a microwave-assisted decomposition procedure in closed high-pressure PFA vessels. Also, the standard reference material SARM 69 was used for the efficiency calibration of the micro-XRF instrument and was analysed by both methods. In order to verify the calibration, the standard reference materials NCS DC 73332 and SRM620 as well as the reference materials AWI-1 and PRI-1 were analysed by micro-XRF. Elemental concentrations determined by the three analytical procedures (ICP-AES, micro-XRF on sherds and micro-XRF on pellets) were statistically treated by correlation analysis and Student's t-test (at the 95% confidence level)

  4. Comparison of a portable micro-X-ray fluorescence spectrometry with inductively coupled plasma atomic emission spectrometry for the ancient ceramics analysis

    Energy Technology Data Exchange (ETDEWEB)

    Papadopoulou, D.N. [Laboratory of Analytical Chemistry, Faculty of Chemistry, Aristotle University, GR-54124, Thessaloniki (Greece); Zachariadis, G.A. [Laboratory of Analytical Chemistry, Faculty of Chemistry, Aristotle University, GR-54124, Thessaloniki (Greece); Anthemidis, A.N. [Laboratory of Analytical Chemistry, Faculty of Chemistry, Aristotle University, GR-54124, Thessaloniki (Greece); Tsirliganis, N.C. [Archaeometry Laboratory, Cultural and Educational Technology Institute, Tsimiski 58, GR-67100, Xanthi (Greece); Stratis, J.A. [Laboratory of Analytical Chemistry, Faculty of Chemistry, Aristotle University, GR-54124, Thessaloniki (Greece)]. E-mail: jstratis@chem.auth.gr

    2004-12-01

    Two multielement instrumental methods of analysis, micro X-ray fluorescence spectrometry (micro-XRF) and inductively coupled plasma atomic emission spectrometry (ICP-AES) were applied for the analysis of 7th and 5th century B.C. ancient ceramic sherds in order to evaluate the above two methods and to assess the potential to use the current compact and portable micro-XRF instrument for the in situ analysis of ancient ceramics. The distinguishing factor of interest is that micro-XRF spectrometry offers the possibility of a nondestructive analysis, an aspect of primary importance in the compositional analysis of cultural objects. Micro-XRF measurements were performed firstly directly on the ceramic sherds with no special pretreatment apart from surface cleaning (micro-XRF on sherds) and secondly on pressed pellet disks which were prepared for each ceramic sherd (micro-XRF on pellet). For the ICP-AES determination of elements, test solutions were prepared by the application of a microwave-assisted decomposition procedure in closed high-pressure PFA vessels. Also, the standard reference material SARM 69 was used for the efficiency calibration of the micro-XRF instrument and was analysed by both methods. In order to verify the calibration, the standard reference materials NCS DC 73332 and SRM620 as well as the reference materials AWI-1 and PRI-1 were analysed by micro-XRF. Elemental concentrations determined by the three analytical procedures (ICP-AES, micro-XRF on sherds and micro-XRF on pellets) were statistically treated by correlation analysis and Student's t-test (at the 95% confidence level)

  5. Ion induced x-ray emission

    International Nuclear Information System (INIS)

    Cohen, D.D.; Clayton, E.

    1989-01-01

    This paper discusses particle induced x-ray emission (PIXE). Its use as a tool for multi-element non-destructive trace element analysis of small samples is addressed. Concepts and details needed for the construction of a PIXE system are offered

  6. X-Ray and Near-Infrared Spectroscopy of Dim X-Ray Point Sources Constituting the Galactic Ridge X-Ray Emission

    Directory of Open Access Journals (Sweden)

    Kumiko Morihana

    2014-12-01

    Full Text Available We present the results of X-ray and Near-Infrared observations of the Galactic Ridge X-ray Emission (GRXE. We extracted 2,002 X-ray point sources in the Chandra Bulge Field (l =0°.113, b = 1°.424 down to ~10-14.8 ergscm-2s-1 in 2-8 keV band with the longest observation (900 ks of the GRXE. Based on X-ray brightness and hardness, we classied the X-ray point sources into three groups: A (hard, B (soft and broad spectrum, and C (soft and peaked spectrum. In order to know populations of the X-ray point sources, we carried out NIR imaging and spectroscopy observation. We identied 11% of X-ray point sources with NIR and extracted NIR spectra for some of them. Based on X-ray and NIR properties, we concluded that non-thermal sources in the group A are mostly active galactic nuclei and the thermal sources are mostly white dwarf binaries such as cataclysmic variables (CVs and Pre-CVs. We concluded that the group B and C sources are X-ray active stars in flare and quiescence, respectively.

  7. Method for detecting binding events using micro-X-ray fluorescence spectrometry

    Science.gov (United States)

    Warner, Benjamin P.; Havrilla, George J.; Mann, Grace

    2010-12-28

    Method for detecting binding events using micro-X-ray fluorescence spectrometry. Receptors are exposed to at least one potential binder and arrayed on a substrate support. Each member of the array is exposed to X-ray radiation. The magnitude of a detectable X-ray fluorescence signal for at least one element can be used to determine whether a binding event between a binder and a receptor has occurred, and can provide information related to the extent of binding between the binder and receptor.

  8. Installation for β- and X-ray spectrometry

    International Nuclear Information System (INIS)

    Sokolov, A.D.; Pchelintsev, A.B.; Lupilov, A.V.; Zalinkevich, V.A.; Lapenas, A.

    2002-01-01

    Paper presents design and parameters of an installation for spectrometry of β- particles and conversion electrons within 15-3000 keV energy range and for X-ray radiation within 2-60 keV range. Si(Li) detector with 500 mm 2 area and 4.5 mm sensitive range thickness is used to record radiation. Energy resolution for 624 keV energy conversion electrons constitutes [ru

  9. L X-ray emission induced by heavy ions

    Energy Technology Data Exchange (ETDEWEB)

    Pajek, M. [Institute of Physics, Jan Kochanowski University, 25-406 Kielce (Poland); Banaś, D., E-mail: d.banas@ujk.edu.pl [Institute of Physics, Jan Kochanowski University, 25-406 Kielce (Poland); Braziewicz, J.; Majewska, U.; Semaniak, J. [Institute of Physics, Jan Kochanowski University, 25-406 Kielce (Poland); Fijał-Kirejczyk, I. [The Institute of Atomic Energy, 05-400 Otwock-Świerk (Poland); Jaskóła, M.; Czarnacki, W.; Korman, A. [The National Centre for Nuclear Research, 05-400 Otwock-Świerk (Poland); Kretschmer, W. [Physikalisches Institut, Universität Erlangen-Nürnberg, D-91058 Erlangen (Germany); Mukoyama, T. [Institute for Nuclear Research, Hungarian Academy of Sciences (ATOMKI), H-4026 Debrecen (Hungary); Trautmann, D. [Institut für Physik, Universität Basel, Basel (Switzerland)

    2015-11-15

    Particle-induced X-ray emission (PIXE) technique is usually applied using typically 1 MeV to 3 MeV protons or helium ions, for which the ion-atom interaction is dominated by the single ionization process. For heavier ions the multiple ionization plays an increasingly important role and this process can influence substantially both the X-ray spectra and atomic decay rates. Additionally, the subshell coupling effects are important for the L- and M-shells ionized by heavy ions. Here we discuss the main features of the X-ray emission induced by heavy ions which are important for PIXE applications, namely, the effects of X-ray line shifts and broadening, vacancy rearrangement and change of the fluorescence and Coster–Kronig yields in multiple ionized atoms. These effects are illustrated here by the results of the measurements of L X-ray emission from heavy atoms bombarded by 6 MeV to 36 MeV Si ions, which were reported earlier. The strong L-subshell coupling effects are observed, in particular L{sub 2}-subshell, which can be accounted for within the coupling subshell model (CSM) developed within the semiclassical approximation. Finally, the prospects to use heavy ions in PIXE analysis are discussed.

  10. Determination of 239Pu and 240Pu isotope ratio for a nuclear bomb particle using X-ray spectrometry in conjunction with γ-ray spectrometry and non-destructive α-particle spectrometry

    International Nuclear Information System (INIS)

    Poellaenen, R.; Ruotsalainen, K.; Toivonen, H.

    2009-01-01

    A nuclear bomb particle from Thule containing Pu and U was analyzed using X-ray spectrometry in combination with γ-ray spectrometry and non-destructive α-spectrometry. The main objective was to investigate the possibility to determine the 239 Pu and 240 Pu isotope ratios. Previously, X-ray spectrometry together with the above-mentioned methods has been successfully applied for radiochemically processed samples, but not for individual particles. In the present paper we demonstrate the power of non-destructive analysis. The 239 Pu/( 239 Pu+ 240 Pu) atom ratio for the Thule particle was determined, using two different approaches, to be 0.93±0.07 and 0.91±0.05. These results are consistent with weapons-grade material and the results obtained by other investigators.

  11. Weak hard X-ray emission from broad absorption line quasars: evidence for intrinsic X-ray weakness

    International Nuclear Information System (INIS)

    Luo, B.; Brandt, W. N.; Scott, A. E.; Alexander, D. M.; Gandhi, P.; Stern, D.; Teng, S. H.; Arévalo, P.; Bauer, F. E.; Boggs, S. E.; Craig, W. W.; Christensen, F. E.; Comastri, A.; Farrah, D.; Hailey, C. J.; Harrison, F. A.; Koss, M.; Ogle, P.; Puccetti, S.; Saez, C.

    2014-01-01

    We report NuSTAR observations of a sample of six X-ray weak broad absorption line (BAL) quasars. These targets, at z = 0.148-1.223, are among the optically brightest and most luminous BAL quasars known at z < 1.3. However, their rest-frame ≈2 keV luminosities are 14 to >330 times weaker than expected for typical quasars. Our results from a pilot NuSTAR study of two low-redshift BAL quasars, a Chandra stacking analysis of a sample of high-redshift BAL quasars, and a NuSTAR spectral analysis of the local BAL quasar Mrk 231 have already suggested the existence of intrinsically X-ray weak BAL quasars, i.e., quasars not emitting X-rays at the level expected from their optical/UV emission. The aim of the current program is to extend the search for such extraordinary objects. Three of the six new targets are weakly detected by NuSTAR with ≲ 45 counts in the 3-24 keV band, and the other three are not detected. The hard X-ray (8-24 keV) weakness observed by NuSTAR requires Compton-thick absorption if these objects have nominal underlying X-ray emission. However, a soft stacked effective photon index (Γ eff ≈ 1.8) for this sample disfavors Compton-thick absorption in general. The uniform hard X-ray weakness observed by NuSTAR for this and the pilot samples selected with <10 keV weakness also suggests that the X-ray weakness is intrinsic in at least some of the targets. We conclude that the NuSTAR observations have likely discovered a significant population (≳ 33%) of intrinsically X-ray weak objects among the BAL quasars with significantly weak <10 keV emission. We suggest that intrinsically X-ray weak quasars might be preferentially observed as BAL quasars.

  12. X-ray emission as a diagnostic from pseudospark-sourced electron beams

    Energy Technology Data Exchange (ETDEWEB)

    Bowes, D., E-mail: david.bowes@strath.ac.uk [Department of Physics, SUPA, University of Strathclyde, Glasgow G4 0NG (United Kingdom); Yin, H.; He, W.; Zhang, L.; Cross, A.W.; Ronald, K.; Phelps, A.D.R. [Department of Physics, SUPA, University of Strathclyde, Glasgow G4 0NG (United Kingdom); Chen, D.; Zhang, P. [Computed Tomography Lab, School of Mathematical Sciences, Capital Normal University, Beijing 100048 (China); Chen, X.; Li, D. [Department of Electronic Engineering, Queen Mary University of London, London E1 4NS (United Kingdom)

    2014-09-15

    X-ray emission has been achieved using an electron beam generated by a pseudospark low-pressure discharge and utilised as a diagnostic for beam detection. A 300 A, 34 kV PS-sourced electron beam pulse of 3 mm diameter impacting on a 0.1 mm-thick molybdenum target generated X-rays which were detected via the use of a small, portable X-ray detector. Clear X-ray images of a micro-sized object were captured using an X-ray photodetector. This demonstrates the inducement of proton induced X-ray emission (PIXE) not only as an indicator of beam presence but also as a future X-ray source for small-spot X-ray imaging of materials.

  13. X-ray emission from National Ignition Facility indirect drive targets

    International Nuclear Information System (INIS)

    Anderson, A.T.; Managan, R.A.; Tobin, M.T.; Peterson, P.F.

    1996-01-01

    We have performed a series of 1-D numerical simulations of the x-ray emission from National Ignition Facility (NIF) targets. Results are presented in terms of total x-ray energy, pulse length, and spectrum. Scaling of x-ray emissions is presented for variations in both target yield and hohlraum thickness. Experiments conducted on the Nova facility provide some validation of the computational tools and methods

  14. Is X-ray emissivity constant on magnetic flux surfaces?

    International Nuclear Information System (INIS)

    Granetz, R.S.; Borras, M.C.

    1997-01-01

    Knowledge of the elongations and shifts of internal magnetic flux surfaces can be used to determine the q profile in elongated tokamak plasmas. X-ray tomography is thought to be a reasonable technique for independently measuring internal flux surface shapes, because it is widely believed that X-ray emissivity should be constant on a magnetic flux surface. In the Alcator C-Mod tokamak, the X-ray tomography diagnostic system consists of four arrays of 38 chords each. A comparison of reconstructed X-ray contours with magnetic flux surfaces shows a small but consistent discrepancy in the radial profile of elongation. Numerous computational tests have been performed to verify these findings, including tests of the sensitivity to calibration and viewing geometry errors, the accuracy of the tomography reconstruction algorithms, and other subtler effects. We conclude that the discrepancy between the X-ray contours and the magnetic flux surfaces is real, leading to the conclusion that X-ray emissivity is not exactly constant on a flux surface. (orig.)

  15. Discovery of Hard Nonthermal Pulsed X-Ray Emission from the Anomalous X-Ray Pulsar 1E 1841-045

    NARCIS (Netherlands)

    Kuiper, L.; Hermsen, W.; Méndez, R.M.

    2004-01-01

    We report the discovery of nonthermal pulsed X-ray/soft gamma-ray emission up to ~150 keV from the anomalous 11.8 s X-ray pulsar AXP 1E 1841-045 located near the center of supernova remnant Kes 73 using Rossi X-Ray Timing Explorer (RXTE) Proportional Counter Array and High Energy X-Ray Timing

  16. X-ray fluorescence spectrometry applied to soil analysis

    International Nuclear Information System (INIS)

    Salvador, Vera Lucia Ribeiro; Sato, Ivone Mulako; Scapin Junior, Wilson Santo; Scapin, Marcos Antonio; Imakima, Kengo

    1997-01-01

    This paper studies the X-ray fluorescence spectrometry applied to the soil analysis. A comparative study of the WD-XRFS and ED-XRFS techniques was carried out by using the following soil samples: SL-1, SOIL-7 and marine sediment SD-M-2/TM, from IAEA, and clay, JG-1a from Geological Survey of Japan (GSJ)

  17. Particle induced x-ray emission (PIXE) measurement of the Cd content in animal tissues

    International Nuclear Information System (INIS)

    Le Huong Quynh; Demeter, I.; Hollos-Nagy, K.; Szoekefalvi-Nagy, Z.

    1989-12-01

    Particle induced x-ray emission (PIXE) measurements were performed on thin samples prepared from different rabbit tissues, using 3 MeV proton beam for inducing x-rays from the animal tissues. This method is very sensitive and very small amounts of trace elements can be detected. Cadmium, one of the most toxic elements which can be concentrated in animal and human tissues due to environmental pollution, was detected with a limit of 0.7 ppm. The trace element concentrations obtained by PIXE were compared to those measured by atomic absorption spectrometry. PIXE method is proposed for routine analysis at the Veterinary and Food Investigating Service, Budapest, Hungary. (D.Gy.) 6 refs.; 3 figs

  18. A PILOT DEEP SURVEY FOR X-RAY EMISSION FROM fuvAGB STARS

    Energy Technology Data Exchange (ETDEWEB)

    Sahai, R. [Jet Propulsion Laboratory, MS 183-900, California Institute of Technology, Pasadena, CA 91109 (United States); Sanz-Forcada, J.; Sánchez Contreras, C. [Astrobiology Center (CSIC-INTA), ESAC campus, E-28691 Villanueva de la Canada, Madrid (Spain); Stute, M. [Institute for Astronomy and Astrophysics, Eberhard Karls Universität Tübingen, Auf der Morgenstelle 10, D-72076, Tübingen (Germany)

    2015-09-01

    We report the results of a pilot survey for X-ray emission from a newly discovered class of AGB stars with far-ultraviolet excesses (fuvAGB stars) using XMM-Newton and Chandra. We detected X-ray emission in three of six fuvAGB stars observed—the X-ray fluxes are found to vary in a stochastic or quasi-periodic manner on roughly hour-long timescales, and simultaneous UV observations using the Optical Monitor on XMM for these sources show similar variations in the UV flux. These data, together with previous studies, show that X-ray emission is found only in fuvAGB stars. From modeling the spectra, we find that the observed X-ray luminosities are ∼(0.002–0.2) L{sub ⊙} and the X-ray-emitting plasma temperatures are ∼(35–160) × 10{sup 6} K. The high X-ray temperatures argue against the emission arising in stellar coronae, or directly in an accretion shock, unless it occurs on a WD companion. However, none of the detected objects is a known WD-symbiotic star, suggesting that if WD companions are present, they are relatively cool (<20,000 K). In addition, the high X-ray luminosities specifically argue against emission originating in the coronae of main-sequence companions. We discuss several models for the X-ray emission and its variability and find that the most likely scenario for the origin of the X-ray (and FUV) emission involves accretion activity around a companion star, with confinement by strong magnetic fields associated with the companion and/or an accretion disk around it.

  19. X-ray/UV variability and the origin of soft X-ray excess emission from II Zw 177

    Science.gov (United States)

    Pal, Main

    We study a detailed broad-band X-ray/UV emission from the narrow line Seyfert 1 galaxy II Zw 177 based on two XMM-Newton and single Swift/XRT observations. Both XMM-Newton observations show the soft X-ray excess emission below 2 keV when the best-fit 2 - 10 keV power law is extrapolated down to 0.3 keV. We find the blurred reflection from an ionized accretion disc and Comptonized disc emission both describe the observed soft excess well. We find a remarkable trend of decreasing UV flux with increasing soft X-ray excess and power law emission. We suggest that this could be due to that the external edge of corona hide a fraction of accretion disk. Co-Author: Prof. Gulab C. Dewangan (IUCAA), Prof. Ranjeev Misra (IUCAA), Pramod Kumar (Nanded university)

  20. A Non-thermal Pulsed X-Ray Emission of AR Scorpii

    Science.gov (United States)

    Takata, J.; Hu, C.-P.; Lin, L. C. C.; Tam, P. H. T.; Pal, P. S.; Hui, C. Y.; Kong, A. K. H.; Cheng, K. S.

    2018-02-01

    We report the analysis result of UV/X-ray emission from AR Scorpii, which is an intermediate polar (IP) composed of a magnetic white dwarf and an M-type star, with the XMM-Newton data. The X-ray/UV emission clearly shows a large variation over the orbit, and their intensity maximum (or minimum) is located at the superior conjunction (or inferior conjunction) of the M star orbit. The hardness ratio of the X-ray emission shows a small variation over the orbital phase and shows no indication of the absorption by an accretion column. These properties are naturally explained by the emission from the M star surface rather than that from the accretion column on the white dwarf’s (WD) star, which is similar to usual IPs. Additionally, the observed X-ray emission also modulates with the WD’s spin with a pulse fraction of ∼14%. The peak position is aligned in the optical/UV/X-ray band. This supports the hypothesis that the electrons in AR Scorpii are accelerated to a relativistic speed and emit non-thermal photons via the synchrotron radiation. In the X-ray bands, evidence of the power-law spectrum is found in the pulsed component, although the observed emission is dominated by the optically thin thermal plasma emissions with several different temperatures. It is considered that the magnetic dissipation/reconnection process on the M star surface heats up the plasma to a temperature of several keV and also accelerates the electrons to the relativistic speed. The relativistic electrons are trapped in the WD’s closed magnetic field lines by the magnetic mirror effect. In this model, the observed pulsed component is explained by the emissions from the first magnetic mirror point.

  1. X-ray absorption and X-ray emission spectroscopy theory and applications

    CERN Document Server

    Lamberti, Carlo

    2016-01-01

    During the last two decades, remarkable and often spectacular progress has been made in the methodological and instrumental aspects of x–ray absorption and emission spectroscopy. This progress includes considerable technological improvements in the design and production of detectors especially with the development and expansion of large-scale synchrotron reactors All this has resulted in improved analytical performance and new applications, as well as in the perspective of a dramatic enhancement in the potential of x–ray based analysis techniques for the near future. This comprehensive two-volume treatise features articles that explain the phenomena and describe examples of X–ray absorption and emission applications in several fields, including chemistry, biochemistry, catalysis, amorphous and liquid systems, synchrotron radiation, and surface phenomena. Contributors explain the underlying theory, how to set up X–ray absorption experiments, and how to analyze the details of the resulting spectra. X-R...

  2. On the Absence of Non-thermal X-Ray Emission around Runaway O Stars

    Energy Technology Data Exchange (ETDEWEB)

    Toalá, J. A. [Institute of Astronomy and Astrophysics, Academia Sinica (ASIAA), Taipei 10617, Taiwan (China); Oskinova, L. M. [Institute for Physics and Astronomy, University of Potsdam, D-14476 Potsdam (Germany); Ignace, R. [Department of Physics and Astronomy, East Tennessee State University, Johnson City, TN 37614 (United States)

    2017-04-01

    Theoretical models predict that the compressed interstellar medium around runaway O stars can produce high-energy non-thermal diffuse emission, in particular, non-thermal X-ray and γ -ray emission. So far, detection of non-thermal X-ray emission was claimed for only one runaway star, AE Aur. We present a search for non-thermal diffuse X-ray emission from bow shocks using archived XMM-Newton observations for a clean sample of six well-determined runaway O stars. We find that none of these objects present diffuse X-ray emission associated with their bow shocks, similarly to previous X-ray studies toward ζ Oph and BD+43°3654. We carefully investigated multi-wavelength observations of AE Aur and could not confirm previous findings of non-thermal X-rays. We conclude that so far there is no clear evidence of non-thermal extended emission in bow shocks around runaway O stars.

  3. Soft X ray spectrometry at high count rates

    International Nuclear Information System (INIS)

    Blanc, P.; Brouquet, P.; Uhre, N.

    1978-06-01

    Two modifications of the classical method of X-ray spectrometry by a semi-conductor diode permit a count rate of 10 5 c/s with an energy resolution of 350 eV. With a specially constructed pulse height analyzer, this detector can measure four spectra of 5 ms each, in the range of 1-30 keV, during a plasma shot

  4. Composition of Renaissance paint layers: simultaneous particle induced X-ray emission and backscattering spectrometry.

    Science.gov (United States)

    de Viguerie, L; Beck, L; Salomon, J; Pichon, L; Walter, Ph

    2009-10-01

    Particle induced X-ray emission spectroscopy (PIXE) is now routinely used in the field of cultural heritage. Various setups have been developed to investigate the elemental composition of wood/canvas paintings or of cross-section samples. However, it is not possible to obtain information concerning the quantity of organic binder. Backscattering spectrometry (BS) can be a useful complementary method to overcome this limitation. In the case of paint layers, PIXE brings the elemental composition (major elements to traces) and the BS spectrum can give access to the proportion of pigment and binder. With the use of 3 MeV protons for PIXE and BS simultaneously, it was possible to perform quantitative analysis including C and O for which the non-Rutherford cross sections are intense. Furthermore, with the use of the same conditions for PIXE and BS, the experiment time and the potential damage by the ion beam were reduced. The results obtained with the external beam of the Accélérateur Grand Louvre pour l'Analyse Elementaire (AGLAE) facility on various test painting samples and on cross sections from Italian Renaissance masterpieces are shown. Simultaneous combination of PIXE and BS leads to a complete characterization of the paint layers: elemental composition and proportion of the organic binder have been determined and thus provide useful information about ancient oil painting recipes.

  5. Relative probabilities of the uranium isotopes for thorium x-ray emission and fluorescence of uranium x-rays

    International Nuclear Information System (INIS)

    Parker, J.L.

    1991-01-01

    Both thorium x-rays from decaying uranium isotopes and self-fluoresced uranium x-rays are prominent in high-resolution gamma-ray spectra of uranium-bearing materials. Useful application of the information carried by those x-rays has been curtailed because the probabilities of the uranium isotopes for thorium x-ray emission and for uranium x-ray fluorescence have not been known. By analyzing enrichment-meter geometry spectra from uranium oxide standards whose enrichments ranged from 0.7% to 91%, relative values, primarily, have been obtained for the probabilities of both processes. Thorium x-ray emission is very heavily dominated by 235 U. In all ordinarily occurring uranium isotopic distributions, thorium x-rays may be used as a valid 235 U signature. The probability for a thorium K α1 x-ray to be emitted in the decay of a 235 U atom is 0.048 ±0.002. In infinitely thick uranium oxide materials, the relative ratios of effectiveness for self-fluorescence, on a per unit mass basis, are approximately 234 U : 235 U : 236 U : 238 U = 1.13 : 1.00 : 0.52 : 0.028. on a per decay basis, the approximate ratios are 0.00039 : 1.00 : 0.017 : 0.18. These results imply that, contrary to what has often been stated, gamma rays are far more important than alpha particles in the self-fluorescence of uranium. Because of the importance of gamma-ray self-fluorescence, the uranium x-ray yield will be somewhat influenced by the size, shape, and composition of the materials. 4 refs., 1 fig

  6. Determination of rare-earth elements in rocks by isotope-excited X-ray fluorescence spectrometry

    DEFF Research Database (Denmark)

    Kunzendorf, Helmar; Wollenberg, H.A.

    1970-01-01

    Isotope-excited X-ray fluorescence spectrometry furnishes a rapid determination of rare-earth elements in unprepared rock samples. The samples are excited by 241Am γ-rays, generating X-ray spectra on a multichannel pulse-height analyser. Gaussian peaks of the Kα and Kβ X-ray energies are treated......-ray spectrometric scan of a longitudinally sliced drill core showed a close correlation between rare-earth abundances and appropriate minerals....

  7. Applications of particle induced X-ray emission

    International Nuclear Information System (INIS)

    Akselsson, K. R.

    1978-01-01

    In Particle Induced X-ray Emission (PIXE) analysis samples are bombarded by protons or α-particles of a few MeV/u. The induced characteristic x-rays are detected with a x-ray detector e.g. a Si(Li)-detector. The energies of the x-ray peaks are characteristic for the elements in the samples and the intensities of the x-ray transitions are proportional to the abundances of the elements. The research area which first attracted those of us working with PIXE was the study of sources, transport and deposition of airborne particulates. Sources, transport, wet deposition, other applications where PIXE is already known to be competitive are trace elemental analysis of water below the ppb-level and analyses requiring a space resolution of 1-10μ. However, there is still much to do for physicists in developing the full potential of low-energy accelerators as analytical tools in multidisciplinary teams. (JIW)

  8. X-Ray Fluorescence Spectrometry. II. Determination of Uranium in ores

    International Nuclear Information System (INIS)

    Bermudez Polonio, J.; Crus Castillo, F. de la; Fernandez Cellini, R.

    1961-01-01

    A method of analysis of uranium in ores by X-ray spectrometry was developed, using the internal standard technique. Strontium was found to be the most suitable internal standard for general use. A Norelco Philips X-ray fluorescent spectrometer was used in this work, equipped with a lithium fluoride crystal acting as a diffraction grating analyzer. The intensity of the uranium-L α 1 spectral line is calculated and related to corresponding strontium-K α spectral line, both detected with a Scintillation Counter. (Author) 31 refs

  9. Application of total reflection X-ray fluorescence spectrometry for ...

    Indian Academy of Sciences (India)

    Applicability of total reflection X-ray fluorescence (TXRF) spectrometry for trace elemental analysis of rainwater samples was studied. The study was used to develop these samples as rainwater standards by the National University of Singapore (NUS). Our laboratory was one of the participants to use TXRF for this study.

  10. DISCOVERY OF X-RAY EMISSION FROM YOUNG SUNS IN THE SMALL MAGELLANIC CLOUD

    International Nuclear Information System (INIS)

    Oskinova, L. M.; Hainich, R.; Sun, W.; Chen, Y.; Evans, C. J.; Hénault-Brunet, V.; Chu, Y.-H.; Gruendl, R. A.; Gallagher, J. S. III; Guerrero, M. A.; Güdel, M.; Silich, S.; Nazé, Y.; Reyes-Iturbide, J.

    2013-01-01

    We report the discovery of extended X-ray emission within the young star cluster NGC 602a in the Wing of the Small Magellanic Cloud (SMC) based on observations obtained with the Chandra X-Ray Observatory. X-ray emission is detected from the cluster core area with the highest stellar density and from a dusty ridge surrounding the H II region. We use a census of massive stars in the cluster to demonstrate that a cluster wind or wind-blown bubble is unlikely to provide a significant contribution to the X-ray emission detected from the central area of the cluster. We therefore suggest that X-ray emission at the cluster core originates from an ensemble of low- and solar-mass pre-main-sequence (PMS) stars, each of which would be too weak in X-rays to be detected individually. We attribute the X-ray emission from the dusty ridge to the embedded tight cluster of the newborn stars known in this area from infrared studies. Assuming that the levels of X-ray activity in young stars in the low-metallicity environment of NGC 602a are comparable to their Galactic counterparts, then the detected spatial distribution, spectral properties, and level of X-ray emission are largely consistent with those expected from low- and solar-mass PMS stars and young stellar objects (YSOs). This is the first discovery of X-ray emission attributable to PMS stars and YSOs in the SMC, which suggests that the accretion and dynamo processes in young, low-mass objects in the SMC resemble those in the Galaxy.

  11. Characterization of X-ray emission from laser generated plasma

    Science.gov (United States)

    Cannavò, Antonino; Torrisi, Lorenzo; Ceccio, Giovanni; Cutroneo, Mariapompea; Calcagno, Lucia; Sciuto, Antonella; Mazzillo, Massimo

    2018-01-01

    X-ray emission from laser generated plasma was studied at low (1010 W/cm2) and high (1018 W/cm2) intensity using ns and fs laser, respectively. Plasma characteristics were controlled trough the laser parameters, the irradiation conditions and the target properties. The X-ray spectra were acquired using fast detection technique based on SiC diodes with different active regions. The X-ray yield increases with the atomic number of the target, both at low and high intensity, and a similar empirical law has been obtained. The X-ray emission mechanisms from plasma are correlated to the plasma temperature and density and to the Coulomb charge particle acceleration, due to the charge separation effects produced in the non-equilibrium plasma. Functional dependences, theoretical approaches and interpretation of possible mechanism will be presented and discussed.

  12. Characterization of X-ray emission from laser generated plasma

    Directory of Open Access Journals (Sweden)

    Cannavò Antonino

    2018-01-01

    Full Text Available X-ray emission from laser generated plasma was studied at low (1010 W/cm2 and high (1018 W/cm2 intensity using ns and fs laser, respectively. Plasma characteristics were controlled trough the laser parameters, the irradiation conditions and the target properties. The X-ray spectra were acquired using fast detection technique based on SiC diodes with different active regions. The X-ray yield increases with the atomic number of the target, both at low and high intensity, and a similar empirical law has been obtained. The X-ray emission mechanisms from plasma are correlated to the plasma temperature and density and to the Coulomb charge particle acceleration, due to the charge separation effects produced in the non-equilibrium plasma. Functional dependences, theoretical approaches and interpretation of possible mechanism will be presented and discussed.

  13. Luminosity dependence in the ratio of X-ray to infrared emission of QSOs

    International Nuclear Information System (INIS)

    Worrall, D.M.

    1987-01-01

    The correlation of X-ray and near-infrared luminosity is studied for a sample of radio-quiet QSOs. The X-ray to infrared ratio is found to decrease as the infrared luminosity increases. No preference is found between the correlations of X-ray luminosity with optical or infrared luminosity. This implies that optical and infrared emission are equally good predictors of X-ray emission. Source models which directly link infrared and X-ray emission are discussed, and a preference is found for a specific synchrotron self-Compton model. This model predicts the correct luminosity dependence of the X-ray to infrared ratio if certain conditions apply. 55 references

  14. Automatic sample changer system for a chain of X-Ray Spectrometry

    International Nuclear Information System (INIS)

    Kall, B.

    2004-01-01

    Nowadays, the science evolves and the used techniques become more pointed. At the same time, instruments are more powerful. This rule also applies in the domain of the nuclear science. The object of these works goes in this sense and touch the branch of the X-Ray spectrometry and that brings back himself to the conception and the realization of an automatic sample changer system for the chain of X-Ray Spectrometry. Baptized KEN-001 , it is an instrument of sample changer ordered from certain distance. Indeed, the sample carriers are placed of advance in compartments on its tray and by a control, KEN-001 put one by one those reflectors in the carries reflective for analysis. Once the analysis is finished, the system is in charge of taking and replacing the reflector in its compartment of origin. Of this way, one wins in time and therefore in number of analysis to do in an interval of time given. This instrument of precision contributes to the improvement of the analysis and the evolution of the technique of the X-Ray fluorescence [fr

  15. X-Rays from NGC 3256: High-Energy Emission in Starburst Galaxies and Their Contribution to the Cosmic X-Ray Background

    International Nuclear Information System (INIS)

    Moran, Edward C.; Lehnert, Matthew D.; Helfand, David J.

    1999-01-01

    The infrared-luminous galaxy NGC 3256 is a classic example of a merger-induced nuclear starburst system. We find here that it is the most X-ray-luminous star-forming galaxy yet detected (L 0.5-10keV =1.6x10 42 ergs s-1). Long-slit optical spectroscopy and a deep, high-resolution ROSAT X-ray image show that the starburst is driving a ''superwind'' which accounts for ∼20% of the observed soft X-ray emission. Analysis of X-ray spectral data from ASCA indicates this gas has a characteristic temperature of kT≅0.3 keV. Our model for the broadband X-ray emission of NGC 3256 contains two additional components: a warm thermal plasma (kT≅0.8 keV) associated with the central starburst, and a hard power-law component with an energy index of α X ≅0.7. We discuss the energy budget for the two thermal plasmas and find that the input of mechanical energy from the starburst is more than sufficient to sustain the observed level of emission. We also examine possible origins for the power-law component, concluding that neither a buried AGN nor the expected population of high-mass X-ray binaries can account for this emission. Inverse Compton scattering, involving the galaxy's copious flux of infrared photons and the relativistic electrons produced by supernovae, is likely to make a substantial contribution to the hard X-ray flux. Such a model is consistent with the observed radio and IR fluxes and the radio and X-ray spectral indices. We explore the role of X-ray-luminous starbursts in the production of the cosmic X-ray background radiation. The number counts and spectral index distribution of the faint radio source population, thought to be dominated by star-forming galaxies, suggest that a significant fraction of the hard X-ray background could arise from starbursts at moderate redshift. (c) (c) 1999. The American Astronomical Society

  16. News on the X-ray emission from hot subdwarf stars

    Directory of Open Access Journals (Sweden)

    Palombara Nicola La

    2017-12-01

    Full Text Available In latest years, the high sensitivity of the instruments on-board the XMM-Newton and Chandra satellites allowed us to explore the properties of the X-ray emission from hot subdwarf stars. The small but growing sample of X-ray detected hot subdwarfs includes binary systems, in which the X-ray emission is due to wind accretion onto a compact companion (white dwarf or neutron star, as well as isolated sdO stars, in which X-rays are probably due to shock instabilities in the wind. X-ray observations of these low-mass stars provide information which can be useful for our understanding of the weak winds of this type of stars and can lead to the discovery of particularly interesting binary systems. Here we report the most recent results we have recently obtained in this research area.

  17. Modeling of X-ray emissions produced by stepping lightning leaders

    OpenAIRE

    Xu , Wei; Celestin , Sebastien; Pasko , Victor P.

    2014-01-01

    International audience; Intense and brief bursts of X-ray emissions have been measured during the stepping processof both natural cloud-to-ground (CG) and rocket-triggered lightning flashes. In this paper, we investigatetheoretically the energy spectra of X-rays produced by the bremsstrahlung emission of thermal runawayelectrons accelerated in the inhomogeneous electric field produced around lightning leader tips. The X-rayenergy spectrum depends on the physical properties of the associated l...

  18. The Sun's X-ray Emission During the Recent Solar Minimum

    Science.gov (United States)

    Sylwester, Janusz; Kowalinski, Mirek; Gburek, Szymon; Siarkowski, Marek; Kuzin, Sergey; Farnik, Frantisek; Reale, Fabio; Phillips, Kenneth J. H.

    2010-02-01

    The Sun recently underwent a period of a remarkable lack of major activity such as large flares and sunspots, without equal since the advent of the space age a half century ago. A widely used measure of solar activity is the amount of solar soft X-ray emission, but until recently this has been below the threshold of the X-ray-monitoring Geostationary Operational Environmental Satellites (GOES). There is thus an urgent need for more sensitive instrumentation to record solar X-ray emission in this range. Anticipating this need, a highly sensitive spectrophotometer called Solar Photometer in X-rays (SphinX) was included in the solar telescope/spectrometer TESIS instrument package on the third spacecraft in Russia's Complex Orbital Observations Near-Earth of Activity of the Sun (CORONAS-PHOTON) program, launched 30 January 2009 into a near-polar orbit. SphinX measures X-rays in a band similar to the GOES longer-wavelength channel.

  19. The X-ray spectrometry Si(Li) system and it's application in quantitative analysis of rare-earth elements

    International Nuclear Information System (INIS)

    Barbosa, J.B.S.

    1985-11-01

    The basic principles involved in Si(Li) system used in X-ray spectrometry is described. It also demonstrates its application in the energy range where the resolution is better than that characteristic of conventional spectrometers. The theoretical principles underlying the interaction between the electromagnetic radiation and matter, and a review on semiconductors are presented at first. It emphasizes the fluorescence phenomenon and the process of photon detection by semiconductor crystals whose properties and characteristics allow, in the specific case of Si-crystal, the confection of detectors with large sensitivity volume useful for X-ray spectrometry. In addition, the components of the Si(Li) system are described individually, with special attention to the operating aspects, and to the parameters affecting the quality of pulse height spectrum. Finally, the spectrometer performance is experimentally evaluated though the quantitative analyses of rare-earth element oxides (La, Ce, Pr, Nd). It should be stressed that this research indicates that the X-ray emission-transmission analysis is the most adequate method under the activation conditions provided by the spectrometer, where Am 241 emissor UPSILON of 60KeV is the photon source for the fluorescence. Therefore, the experimental work was extended in order to include all the necessary treatment. (Author) [pt

  20. X-Ray Spectrometry for Preventive Conservation Research

    International Nuclear Information System (INIS)

    Grieken, V. R.

    2008-01-01

    Preventive conservation studies the influence of environmental conditions on the durability of works of art. X-ray spectrometry (XRS), in its many forms, is one of the main physical analysis techniques used in the context of cultural heritage in view of its non-destructive nature; it is also highly indicated for studying the composition of e.g. harmful atmospheric particles in e.g. museums. A short literature overview will be to illustrate the important role of XRS in conservation. Then some of our own applications of XRS (especially automated electron probe X-ray microanalysis for individual atmospheric particles) will be shown. These include studies in the Wawel Castle in Cracow, Poland (where outdoor soot nanoparticles and deicing salts brought in by visitors were most threatening for the wall tapestry collections) and the Metropolitan Museum in New York, USA (where sodium nitrate particles from the reaction of sea spray with car exhaust gases were predominant in some rooms)

  1. X-ray emission lines from photoionized plasmas

    International Nuclear Information System (INIS)

    Liedahl, D.A.

    1992-11-01

    Plasma emission codes have become a standard tool for the analysis of spectroscopic data from cosmic X-ray sources. However, the assumption of collisional equilibrium, typically invoked in these codes, renders them inapplicable to many important astrophysical situations, particularly those involving X-ray photoionized nebulae, which are likely to exist in the circumsource environments of compact X-ray sources. X-ray line production in a photoionized plasma is primarily the result of radiative cascades following recombination. Through the development of atomic models of several highly-charged ions, this work extends the range of applicability of discrete spectral models to plasmas dominated by recombination. Assuming that ambient plasma conditions lie in the temperature range 10 5 --10 6 K and the density range 10 11 --10 16 cm -3 , X-ray line spectra are calculated over the wavelength range 5--45 angstrom using the HULLAC atomic physics package. Most of the work focuses on the Fe L-shell ions. Line ratios of the form (3s-2p)/(3d-2p) are shown to characterize the principal mode of line excitation, thereby providing a simple signature of photoionization. At electron densities exceeding 10 12 cm -3 , metastable state populations in the ground configurations approach their LTE value, resulting in the enrichment of the Fe L-shell recombination spectrum and a set of density-sensitive X-ray line ratios. Radiative recombination continua and emission lines produced selectively by Δn = 0 dielectronic recombination are shown to provide two classes of temperature diagnostics. Because of the extreme overionization, the recombination continua are expected to be narrow (ΔE/E much-lt 1), with ΔE = kT. Dielectronic recombination selectively drives radiative transitions that originate on states with vacancies in the 2s subshell, states that are inaccessible under pure RR population kinetics

  2. Spectrum unfolding in X-ray spectrometry using the maximum entropy method

    International Nuclear Information System (INIS)

    Fernandez, Jorge E.; Scot, Viviana; Di Giulio, Eugenio

    2014-01-01

    The solution of the unfolding problem is an ever-present issue in X-ray spectrometry. The maximum entropy technique solves this problem by taking advantage of some known a priori physical information and by ensuring an outcome with only positive values. This method is implemented in MAXED (MAXimum Entropy Deconvolution), a software code contained in the package UMG (Unfolding with MAXED and GRAVEL) developed at PTB and distributed by NEA Data Bank. This package contains also the code GRAVEL (used to estimate the precision of the solution). This article introduces the new code UMESTRAT (Unfolding Maximum Entropy STRATegy) which applies a semi-automatic strategy to solve the unfolding problem by using a suitable combination of MAXED and GRAVEL for applications in X-ray spectrometry. Some examples of the use of UMESTRAT are shown, demonstrating its capability to remove detector artifacts from the measured spectrum consistently with the model used for the detector response function (DRF). - Highlights: ► A new strategy to solve the unfolding problem in X-ray spectrometry is presented. ► The presented strategy uses a suitable combination of the codes MAXED and GRAVEL. ► The applied strategy provides additional information on the Detector Response Function. ► The code UMESTRAT is developed to apply this new strategy in a semi-automatic mode

  3. The Relationship Between Solar Radio and Hard X-Ray Emission

    Science.gov (United States)

    White, S. M.; Benz, A. O.; Christe, S.; Farnik, F.; Kundu, M. R.; Mann, G.; Ning, Z.; Raulin, J.-P.; Silva-Valio, A. V. R.; Saint-Hilaire, P.; hide

    2011-01-01

    This review discusses the complementary relationship between radio and hard Xray observations of the Sun using primarily results from the era of the Reuven Ramaty High Energy Solar Spectroscopic Imager satellite. A primary focus of joint radio and hard X-ray studies of solar flares uses observations of nonthermal gyrosynchrotron emission at radio wavelengths and bremsstrahlung hard X-rays to study the properties of electrons accelerated in the main flare site, since it is well established that these two emissions show very similar temporal behavior. A quantitative prescription is given for comparing the electron energy distributions derived separately from the two wavelength ranges: this is an important application with the potential for measuring the magnetic field strength in the flaring region, and reveals significant differences between the electrons in different energy ranges. Examples of the use of simultaneous data from the two wavelength ranges to derive physical conditions are then discussed, including the case of microflares, and the comparison of images at radio and hard X-ray wavelengths is presented. There have been puzzling results obtained from observations of solar flares at millimeter and submillimeter wavelengths, and the comparison of these results with corresponding hard X-ray data is presented. Finally, the review discusses the association of hard X-ray releases with radio emission at decimeter and meter wavelengths, which is dominated by plasma emission (at lower frequencies) and electron cyclotron maser emission (at higher frequencies), both coherent emission mechanisms that require small numbers of energetic electrons. These comparisons show broad general associations but detailed correspondence remains more elusive.

  4. Hard X-ray Emission and Efficient Particle Acceleration by Supernova Remnants

    International Nuclear Information System (INIS)

    Vink, Jacco

    2009-01-01

    I discuss the non-thermal X-ray emission from young supernova remnants. Over the last decade it has become clear from both X-ray and γ-ray observations that young supernovae accelerate particles up to 100 TeV. In soft X-rays the accelerated >10 TeV electrons produce synchrotron radiation, coming from narrow filaments located at the shock fronts. The width of these filaments shows that the magnetic fields are relatively high, thus providing evidence for magnetic field amplification.The synchrotron radiation of several remnants is known to extend into the hard X-ray regime. In particular Cas A, has a spectrum that appears as a power law up to almost 100 TeV. This is very surprising, as a steepening is expected going from the soft to the hard X-ray band. The spectrum is likely a result of many superimposed individual spectra, each steepening at different energies. This implies considerable spatial variation in hard X-rays, an obvious target for Simbol-X. The variations will be important to infer local shock acceleration properties, but also magnetic field fluctuations may cause spatial and temporal variations.Finally, I draw the attention to super bubbles and supernovae as sources of cosmic rays. As such they may be sources of hard X-ray emission. In particular, supernovae exploding inside the dense red supergiants winds of their progenitors ares promising candidates for hard X-ray emission.

  5. Hard X-ray Emission and Efficient Particle Acceleration by Supernova Remnants

    Science.gov (United States)

    Vink, Jacco

    2009-05-01

    I discuss the non-thermal X-ray emission from young supernova remnants. Over the last decade it has become clear from both X-ray and γ-ray observations that young supernovae accelerate particles up to 100 TeV. In soft X-rays the accelerated >10 TeV electrons produce synchrotron radiation, coming from narrow filaments located at the shock fronts. The width of these filaments shows that the magnetic fields are relatively high, thus providing evidence for magnetic field amplification. The synchrotron radiation of several remnants is known to extend into the hard X-ray regime. In particular Cas A, has a spectrum that appears as a power law up to almost 100 TeV. This is very surprising, as a steepening is expected going from the soft to the hard X-ray band. The spectrum is likely a result of many superimposed individual spectra, each steepening at different energies. This implies considerable spatial variation in hard X-rays, an obvious target for Simbol-X. The variations will be important to infer local shock acceleration properties, but also magnetic field fluctuations may cause spatial and temporal variations. Finally, I draw the attention to super bubbles and supernovae as sources of cosmic rays. As such they may be sources of hard X-ray emission. In particular, supernovae exploding inside the dense red supergiants winds of their progenitors ares promising candidates for hard X-ray emission.

  6. Synchrotron-Radiation Induced X-Ray Emission (SRIXE)

    Energy Technology Data Exchange (ETDEWEB)

    Jones, Keith W.

    1999-09-01

    Elemental analysis using emission of characteristic x rays is a well-established scientific method. The success of this analytical method is highly dependent on the properties of the source used to produce the x rays. X-ray tubes have long existed as a principal excitation source, but electron and proton beams have also been employed extensively. The development of the synchrotron radiation x-ray source that has taken place during the past 40 years has had a major impact on the general field of x-ray analysis. Even tier 40 years, science of x-ray analysis with synchrotron x-ray beams is by no means mature. Improvements being made to existing synchrotron facilities and the design and construction of new facilities promise to accelerate the development of the general scientific use of synchrotron x-ray sources for at least the next ten years. The effective use of the synchrotron source technology depends heavily on the use of high-performance computers for analysis and theoretical interpretation of the experimental data. Fortunately, computer technology has advanced at least as rapidly as the x-ray technology during the past 40 years and should continue to do so during the next decade. The combination of these technologies should bring about dramatic advances in many fields where synchrotron x-ray science is applied. It is interesting also to compare the growth and rate of acceptance of this particular research endeavor to the rates for other technological endeavors. Griibler [1997] cataloged the time required for introduction, diffusion,and acceptance of technological, economic, and social change and found mean values of 40 to 50 years. The introduction of the synchrotron source depends on both technical and non-technical factors, and the time scale at which this seems to be occurring is quite compatible with what is seen for other major innovations such as the railroad or the telegraph. It will be interesting to see how long the present rate of technological change

  7. Synchrotron-Radiation Induced X-Ray Emission (SRIXE)

    International Nuclear Information System (INIS)

    Jones, Keith W.

    1999-01-01

    Elemental analysis using emission of characteristic x rays is a well-established scientific method. The success of this analytical method is highly dependent on the properties of the source used to produce the x rays. X-ray tubes have long existed as a principal excitation source, but electron and proton beams have also been employed extensively. The development of the synchrotron radiation x-ray source that has taken place during the past 40 years has had a major impact on the general field of x-ray analysis. Even tier 40 years, science of x-ray analysis with synchrotron x-ray beams is by no means mature. Improvements being made to existing synchrotron facilities and the design and construction of new facilities promise to accelerate the development of the general scientific use of synchrotron x-ray sources for at least the next ten years. The effective use of the synchrotron source technology depends heavily on the use of high-performance computers for analysis and theoretical interpretation of the experimental data. Fortunately, computer technology has advanced at least as rapidly as the x-ray technology during the past 40 years and should continue to do so during the next decade. The combination of these technologies should bring about dramatic advances in many fields where synchrotron x-ray science is applied. It is interesting also to compare the growth and rate of acceptance of this particular research endeavor to the rates for other technological endeavors. Griibler [1997] cataloged the time required for introduction, diffusion,and acceptance of technological, economic, and social change and found mean values of 40 to 50 years. The introduction of the synchrotron source depends on both technical and non-technical factors, and the time scale at which this seems to be occurring is quite compatible with what is seen for other major innovations such as the railroad or the telegraph. It will be interesting to see how long the present rate of technological change

  8. X-ray emission from the Pleiades cluster

    Science.gov (United States)

    Agrawal, P. C.; Singh, K. P.; Riegler, G. R.

    1983-01-01

    The detection and identification of H0344+24, a new X-ray source located in the Pleiades cluster, is reported, based on observations made with HEAO A-2 low-energy detector 1 in the 0.15-3.0-keV energy band in August, 1977. The 90-percent-confidence error box for the new source is centered at 03 h 44.1 min right ascension (1950), near the center star of the 500-star Pleiades cluster, 25-eta-Tau. Since no likely galactic or extragalactic source of X-rays was found in a catalog search of the error-box region, identification of the source with the Pleiades cluster is considered secure. X-ray luminosity of the source is calculated to be about 10 to the 32nd ergs/sec, based on a distance of 125 pc. The X-ray characteristics of the Pleiades stars are discussed, and it is concluded that H0344+24 can best be explained as the integrated X-ray emission of all the B and F stars in the cluster.

  9. Ultrafast secondary emission x-ray imaging detectors

    International Nuclear Information System (INIS)

    Akkerman, A.; Gibrekhterman, A.; Majewski, S.

    1991-07-01

    Fast high accuracy, x-ray imaging at high photon flux can be achieved when coupling thin solid convertors to gaseous electron multipliers, operating at low gas pressures. Secondary electron emitted from the convertor foil are multiplied in several successive amplification elements. The obvious advantage of solid x-ray detectors, as compared to gaseous conversion, are the production of parallax-free images and the fast (subnanoseconds) response. These x-ray detectors have many potential applications in basic and applied research. Of particular interest is the possibility of an efficient and ultrafast high resolution imaging of transition radiation,with a reduced dE/dx background. We present experimental results on the operation of the secondary emission x-ray (SEX) detectors, their detection efficiency, localization and time resolution. The experimental work is accompanied by mathematical modelling and computer simulation of transition radiation detectors based on CsI transition radiation convertors. (author)

  10. Circumstellar X-ray Emission from SN1978K

    Science.gov (United States)

    Schlegel, Eric M.; Colbert, E.; Petre, R.

    1995-02-01

    We present the X-ray light curve in the 0.2 2.4 keV band based on fiveROSAT observations of SN1978K in NGC 1313. The X-ray emission is believed to arise from the interaction of the reverse shock and the expanding debris from the supernova. The reverse shock becomes established after the outgoing shock runs into circumstellar matter.

  11. A giant radio flare from Cygnus X-3 with associated γ-ray emission

    Science.gov (United States)

    Corbel, S.; Dubus, G.; Tomsick, J. A.; Szostek, A.; Corbet, R. H. D.; Miller-Jones, J. C. A.; Richards, J. L.; Pooley, G.; Trushkin, S.; Dubois, R.; Hill, A. B.; Kerr, M.; Max-Moerbeck, W.; Readhead, A. C. S.; Bodaghee, A.; Tudose, V.; Parent, D.; Wilms, J.; Pottschmidt, K.

    2012-04-01

    With frequent flaring activity of its relativistic jets, Cygnus X-3 (Cyg X-3) is one of the most active microquasars and is the only Galactic black hole candidate with confirmed high-energy γ-ray emission, thanks to detections by Fermi Large Area Telescope (Fermi/LAT) and AGILE. In 2011, Cyg X-3 was observed to transit to a soft X-ray state, which is known to be associated with high-energy γ-ray emission. We present the results of a multiwavelength campaign covering a quenched state, when radio emission from Cyg X-3 is at its weakest and the X-ray spectrum is very soft. A giant (˜20 Jy) optically thin radio flare marks the end of the quenched state, accompanied by rising non-thermal hard X-rays. Fermi/LAT observations (E≥ 100 MeV) reveal renewed γ-ray activity associated with this giant radio flare, suggesting a common origin for all non-thermal components. In addition, current observations unambiguously show that the γ-ray emission is not exclusively related to the rare giant radio flares. A three-week period of γ-ray emission is also detected when Cyg X-3 was weakly flaring in radio, right before transition to the radio quenched state. No γ-rays are observed during the ˜1-month long quenched state, when the radio flux is weakest. Our results suggest transitions into and out of the ultrasoft X-ray (radio-quenched) state trigger γ-ray emission, implying a connection to the accretion process, and also that the γ-ray activity is related to the level of radio flux (and possibly shock formation), strengthening the connection to the relativistic jets.

  12. NuSTAR HARD X-RAY SURVEY OF THE GALACTIC CENTER REGION. I. HARD X-RAY MORPHOLOGY AND SPECTROSCOPY OF THE DIFFUSE EMISSION

    Energy Technology Data Exchange (ETDEWEB)

    Mori, Kaya; Hailey, Charles J.; Perez, Kerstin; Nynka, Melania; Zhang, Shuo; Canipe, Alicia M. [Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Krivonos, Roman; Tomsick, John A.; Barrière, Nicolas; Boggs, Steven E.; Craig, William W. [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Hong, Jaesub [Harvard-Smithsonian Center for Astrophysics, Cambridge, MA 02138 (United States); Ponti, Gabriele [Max-Planck-Institut f. extraterrestrische Physik, HEG, Garching (Germany); Bauer, Franz [Instituto de Astrofísica, Facultad de Física, Pontificia Universidad Católica de Chile, 306, Santiago 22 (Chile); Alexander, David M. [Department of Physics, Durham University, Durham DH1 3LE (United Kingdom); Baganoff, Frederick K. [Kavli Institute for Astrophysics and Space Research, Massachusets Institute of Technology, Cambridge, MA 02139 (United States); Barret, Didier [Université de Toulouse, UPS-OMP, IRAP, Toulouse (France); Christensen, Finn E. [DTU Space—National Space Institute, Technical University of Denmark, Elektrovej 327, DK-2800 Lyngby (Denmark); Forster, Karl [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, Pasadena, CA 91125 (United States); Giommi, Paolo, E-mail: kaya@astro.columbia.edu [ASI Science Data Center, Via del Politecnico snc I-00133, Roma (Italy); and others

    2015-12-01

    We present the first sub-arcminute images of the Galactic Center above 10 keV, obtained with NuSTAR. NuSTAR resolves the hard X-ray source IGR J17456–2901 into non-thermal X-ray filaments, molecular clouds, point sources, and a previously unknown central component of hard X-ray emission (CHXE). NuSTAR detects four non-thermal X-ray filaments, extending the detection of their power-law spectra with Γ ∼ 1.3–2.3 up to ∼50 keV. A morphological and spectral study of the filaments suggests that their origin may be heterogeneous, where previous studies suggested a common origin in young pulsar wind nebulae (PWNe). NuSTAR detects non-thermal X-ray continuum emission spatially correlated with the 6.4 keV Fe Kα fluorescence line emission associated with two Sgr A molecular clouds: MC1 and the Bridge. Broadband X-ray spectral analysis with a Monte-Carlo based X-ray reflection model self-consistently determined their intrinsic column density (∼10{sup 23} cm{sup −2}), primary X-ray spectra (power-laws with Γ ∼ 2) and set a lower limit of the X-ray luminosity of Sgr A* flare illuminating the Sgr A clouds to L{sub X} ≳ 10{sup 38} erg s{sup −1}. Above ∼20 keV, hard X-ray emission in the central 10 pc region around Sgr A* consists of the candidate PWN G359.95–0.04 and the CHXE, possibly resulting from an unresolved population of massive CVs with white dwarf masses M{sub WD} ∼ 0.9 M{sub ⊙}. Spectral energy distribution analysis suggests that G359.95–0.04 is likely the hard X-ray counterpart of the ultra-high gamma-ray source HESS J1745–290, strongly favoring a leptonic origin of the GC TeV emission.

  13. Soft X-ray-induced decomposition of amino acids: An XPS, mass spectrometry, and NEXAFS study

    International Nuclear Information System (INIS)

    Zubavichus, Yan; Fuchs, Oliver; Weinhardt, Lothar; Heske, Clemens; Umbach, Eberhard; Denlinger, Jonathan D.; Grunze, Michael

    2003-01-01

    Decomposition of five amino acids, alanine, serine, cysteine, aspartic acid, and asparagine, under irradiation with soft X-rays (magnesium Ka X-ray source) in ultra-high vacuum was studied by means of X-ray photoelectron spectrometry (XPS) and mass spectrometry. A comparative analysis of changes in XPS line shapes, stoichiometry and residual gas composition indicates that the molecules decompose by several pathways. Dehydration, decarboxylation, decarbonylation,deamination and desulfurization of pristine molecules accompanied by desorption of H2, H2O, CO2, CO, NH3and H2S are observed with rates depending on the specific amino acid. NEXAFS spectra of cysteine at the carbon, oxygen and nitrogen K-shell and sulfur L2,3 edges complement the XPS and mass spectrometry data and show that the exposure of the sample to an intense soft X-ray synchrotron beam results in the formation of C-C and C-N double and triple bonds. Qualitatively, the amino acids studied can be arranged in the following ascending order of radiation stability:serine< alanine< aspartic acid< cysteine< asparagine

  14. X-ray emission and the winds of cataclysmic variables

    International Nuclear Information System (INIS)

    Cordova, F.A.

    1985-01-01

    X-ray and ultraviolet observations of cataclysmic variable stars reveal a variety of exotic behavior - pulsations, winds, and episodic outbursts - are these related, what do they tell us about the nature of the outburst, about the environment of the accreting white dwarf. The author summarizes the observed changes in the x-ray and uv continuum and spectral features through the outbursts of the dwarf novae. The author then discusses how the modeling of these data have refined our ideas about the location and nature of the emissions, and the source of the outbursts. The author shows how comparisons of the x-ray and uv properties of cataclysmic variables with similar phenomena in other astronomical systems - the solar corona, OB stars, and Be stars - suggest ways in which the x-ray and uv emissions in CVs may be related, and point to further, specific observations that would elucidate our understanding of the behavior and role of the white dwarf in the outburst. 26 references

  15. Soft X-ray Emission from Large-Scale Galactic Outflows in Seyfert Galaxies

    Science.gov (United States)

    Colbert, E. J. M.; Baum, S.; O'Dea, C.; Veilleux, S.

    1998-01-01

    Kiloparsec-scale soft X-ray nebulae extend along the galaxy minor axes in several Seyfert galaxies, including NGC 2992, NGC 4388 and NGC 5506. In these three galaxies, the extended X-ray emission observed in ROSAT HRI images has 0.2-2.4 keV X-ray luminosities of 0.4-3.5 x 10(40) erg s(-1) . The X-ray nebulae are roughly co-spatial with the large-scale radio emission, suggesting that both are produced by large-scale galactic outflows. Assuming pressure balance between the radio and X-ray plasmas, the X-ray filling factor is >~ 10(4) times as large as the radio plasma filling factor, suggesting that large-scale outflows in Seyfert galaxies are predominantly winds of thermal X-ray emitting gas. We favor an interpretation in which large-scale outflows originate as AGN-driven jets that entrain and heat gas on kpc scales as they make their way out of the galaxy. AGN- and starburst-driven winds are also possible explanations if the winds are oriented along the rotation axis of the galaxy disk. Since large-scale outflows are present in at least 50 percent of Seyfert galaxies, the soft X-ray emission from the outflowing gas may, in many cases, explain the ``soft excess" X-ray feature observed below 2 keV in X-ray spectra of many Seyfert 2 galaxies.

  16. Sample analysis using gamma ray induced fluorescent X-ray emission

    Energy Technology Data Exchange (ETDEWEB)

    Sood, B S; Allawadhi, K L; Gandhi, R; Batra, O P; Singh, N [Punjabi Univ., Patiala (India). Nuclear Science Labs.

    1983-01-01

    A non-destructive method for the analysis of materials using gamma ray-induced fluorescent x-ray emission has been developed. In this method, special preparation of very thin samples in which the absorption of the incident gamma rays and the emitted fluorescent x-rays is negligible, is not needed, and the absorption correction is determined experimentally. A suitable choice of the incident gamma ray energies is made to minimise enhancement effects through selective photoionization of the elements in the sample. The method is applied to the analysis of a typical sample of the soldering material using 279 keV and 59.5 keV gamma rays from /sup 203/Hg and /sup 241/Am radioactive sources respectively. The results of the analysis are found to agree well with those obtained from the chemical analysis.

  17. Design of a tritium gas cell for beta-ray induced X-ray spectrometry using Monte Carlo simulation

    Energy Technology Data Exchange (ETDEWEB)

    Hara, Masanori, E-mail: masahara@ctg.u-toyama.ac.jp [Hydrogen Isotope Research Center, Organization for Promotion of Research, University of Toyama, 3190 Gofuku, Toyama City, Toyama 930-8555 (Japan); Abe, Shinsuke; Matsuyama, Masao [Hydrogen Isotope Research Center, Organization for Promotion of Research, University of Toyama, 3190 Gofuku, Toyama City, Toyama 930-8555 (Japan); Aso, Tsukasa [Electronics and Computer Engineering, National Institute of Technology, Toyama College, 1-2 Ebie-neriya, Imizu City, Toyama 933-0293 (Japan); Tatenuma, Katsuyoshi; Kawakami, Tomohiko; Ito, Takeshi [KAKEN Company Limited, 1044 Horimachi, Mito City, Ibaraki 310-0903 (Japan)

    2017-06-15

    Highlights: • Beta-ray induced X-ray spectrometry (BIXS) is a method for tritium gas analysis. • Gas cell for BIXS was designed by Monte Carlo simulations. • The optimum thickness of the gold layer on a beryllium window was around 150 nm. • This simulation model considered the self-absorption with increasing the cell length. - Abstract: One of the methods used for tritium gas analysis is beta-ray induced X-ray spectrometry (BIXS). Gas cell design is important in this method. The structure of the gas cell for BIXS was optimized by Monte Carlo simulation of beta-ray induced X-ray spectra in various window geometries using the Geant4 tool kit (version 10.01.p02). The simulated spectrum from tritium decay fitted the observed one, and the simulation model was used to obtain the cell parameters for BIXS. The optimum thickness of the gold layer on a beryllium window was around 150 nm. This simulation model also considered the relationship between self-absorption by hydrogen gas and the cell length. Self-absorption increased with increasing cell length and the relationship between the sample pressure and cell length was formulated.

  18. Scaling of x-ray emission and ion velocity in laser produced Cu ...

    Indian Academy of Sciences (India)

    Laser plasma; x-ray emission; conversion efficiency; ion velocities. ... fits from this kind of optimization studies are in the fields of x-ray lithography, x-ray lasers etc. .... formula between the x-ray conversion rate versus different parameters of the ...

  19. A giant radio flare from Cygnus X-3 with associated γ-ray emission: The 2011 radio and γ-ray flare of Cyg X-3

    International Nuclear Information System (INIS)

    Corbel, S.; Dubus, G.; Tomsick, J. A.; Szostek, A.

    2012-01-01

    With frequent flaring activity of its relativistic jets, Cygnus X-3 (Cyg X-3) is one of the most active microquasars and is the only Galactic black hole candidate with confirmed high-energy γ-ray emission, thanks to detections by Fermi Large Area Telescope (Fermi/LAT) and AGILE. In 2011, we observed Cyg X-3 in order to transit to a soft X-ray state, which is known to be associated with high-energy γ-ray emission. We present the results of a multiwavelength campaign covering a quenched state, when radio emission from Cyg X-3 is at its weakest and the X-ray spectrum is very soft. A giant (~20 Jy) optically thin radio flare marks the end of the quenched state, accompanied by rising non-thermal hard X-rays. Fermi/LAT observations (E≥ 100 MeV) reveal renewed γ-ray activity associated with this giant radio flare, suggesting a common origin for all non-thermal components. In addition, current observations unambiguously show that the γ-ray emission is not exclusively related to the rare giant radio flares. A three-week period of γ-ray emission is also detected when Cyg X-3 was weakly flaring in radio, right before transition to the radio quenched state. There were no γ-rays observed during the ~1-month long quenched state, when the radio flux is weakest. These results suggest transitions into and out of the ultrasoft X-ray (radio-quenched) state trigger γ-ray emission, implying a connection to the accretion process, and also that the γ-ray activity is related to the level of radio flux (and possibly shock formation), strengthening the connection to the relativistic jets.

  20. Case Studies on Facility Characterization with X-Ray Fluorescence Spectrometry

    International Nuclear Information System (INIS)

    Kirk, K.T.; Brooksbank, R.D.; Meszaros, J.M.; Towery, W.E.

    2008-01-01

    A hand-held x-ray fluorescence (XRF) analyzer is being used to characterize facilities in support of demolition activities at the East Tennessee Technology Park (ETTP) in Oak Ridge, Tennessee. Approximately 500 facilities at the U.S. Department of Energy site are being demolished under the ETTP Decontamination and Decommissioning (D and D) project. Facility characterization is being conducted to provide data for waste profiling and identify hazards to demolition workers. XRF spectrometry is a non-destructive analytical technique used to identify and quantify the elemental composition of a substance based on the intensity of its characteristic X-ray emission wavelength or energy. The Innov-X Systems R Model XT-245S XRF analyzer used at ETTP is equipped with a silver anode x-ray tube and a Si PIN diode detector. X-rays are generated by electrical current, eliminating the need for radioactive isotopes. Electronic components can be powered by either a lithium-ion battery or an A/C adapter, and the instrument is controlled by an iPAQ R pocket personal computer. The unit has two primary operating modes. Alloy analysis mode measures percent levels of elements in metals such as a pipes, valves, equipment, or construction materials. Soil mode provides parts-per-million (ppm) quantities in bulk solids like concrete dust, residue, paint chips, or soil. The hand-held unit can analyze material in place, or it can analyze samples in a test stand by remote operation. This paper present some case studies demonstrating a variety of XRF applications for facility characterization: Metal Materials Characterization, Lead Paint Identification, Hot Spot Delineation, Bulk Solids Testing. XRF has been the analytical technique of choice for identifying metal alloy components and has also been useful in analyzing bulk materials. Limitations of XRF testing include the inability to directly analyze elements with low atomic weights. Light elements such as beryllium and aluminum do not emit

  1. Observation of hard X-rays line emission from Her X-1

    Energy Technology Data Exchange (ETDEWEB)

    Polcaro, V.F.; Bazzano, A.; la Padula, C.; Ubertini, P.; Vialetto, G.; Manchanda, R.K.; Damle, S.V.

    1982-04-01

    We present the results of a hard X-ray measurement of the binary source Her X-1, carried out with a balloon borne X-ray telescope consisting of two Multiwire Proportional Counters, having 900 cm/sup 2/ sensitive area each and spectral resolution of 15% and 24% FWHM respectively at 60 keV. The source was observed during the 'Mid-on' state. Our data confirm the previously reported high energy emission line overimposed on the low energy thermal spectrum.

  2. Signatures of Synchrotron: Low-cutoff X-ray emission and the hard X-ray spectrum of Cas A

    Science.gov (United States)

    Stage, Michael D.; Fedor, Emily Elizabeth; Martina-Hood, Hyourin

    2018-06-01

    In soft X-rays, bright, young Galactic remnants (Cas A, Kepler, Tycho, etc.) present thermal line emission and bremsstrahlung from ejecta, and synchrotron radiation from the shocks. Their hard X-ray spectra tend to be dominated by power-law sources. However, it can be non-trivial to discriminate between contributions from processes such as synchrotron and bremsstrahlung from nonthermally accelerated electrons, even though the energies of the electrons producing this radiation may be very different. Spatially-resolved spectroscopic analysis of 0.5-10 keV observations with, e.g., Chandracan provide leverage in identifying the processes and their locations. Previously, Stage & Allen (2006), Allen & Stage (2007) and Stage & Allen (2011) identified regions characterized by high-cutoff synchrotron radiation. Extrapolating synchrotron model fits to the emission in the Chandra band, they estimated the synchrotron contribution to the hard X-ray spectrum at about one-third the observed flux, fitting the balance with nonthermal bremsstrahlung emission produced by nonthermal electrons in the ejecta. Although it is unlikely this analysis missed regions of the highest-cutoff synchrotron emission, which supplies the bulk of the synchrotron above 15 keV, it may have missed regions of lower-cutoff emission, especially if they are near bright ejecta and the reverse shock. These regions cannot explain the emission at the highest energies (~50 keV), but may make significant contributions to the hard spectrum at lower energies (~10 keV). Using the technique described in Fedor, Martina-Hood & Stage (this meeting), we revisit the analysis to include regions that may be dominated by low-cutoff synchrotron, located in the interior of the remnant, and/or correlated with the reverse shock. Identifying X-ray emission from accelerated electrons associated with the reverse-shock would have important implications for synchrotron and non-thermal bremsstrahlung radiation above the 10 keV.

  3. Hard X-ray emission spectroscopy with pink beam

    Energy Technology Data Exchange (ETDEWEB)

    Kvashnina, Kristina O.; Rossberg, Andre; Exner, Joerg; Scheinost, Andreas C. [Helmholtz-Zentrum Dresden-Rossendorf e.V., Dresden (Germany). Molecular Structures

    2017-06-01

    Valence-band X-ray emission spectroscopy (XES) with a ''pink beam'', i.e. a beam with large energy bandwidth produced by a double-multilayer monochromator, is introduced here to overcome the weak count rate of monochromatic beams produced by conventional double-crystal monochromators. Our results demonstrate that - in spite of the large bandwidth in the order of 100 eV - the high spectral resolution of the Johann-type spectrometer is maintained, while the two orders of magnitude higher flux greatly reduces the required counting time. The short working distance Johann-type X-ray emission spectrometer and multilayer monochromator is available at ROBL.

  4. Scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX) and aerosol time-of-flight mass spectrometry (ATOFMS) single particle analysis of metallurgy plant emissions

    International Nuclear Information System (INIS)

    Arndt, J.; Deboudt, K.; Anderson, A.; Blondel, A.; Eliet, S.; Flament, P.; Fourmentin, M.; Healy, R.M.; Savary, V.; Setyan, A.; Wenger, J.C.

    2016-01-01

    The chemical composition of single particles deposited on industrial filters located in three different chimneys of an iron-manganese (Fe–Mn) alloy manufacturing plant have been compared using aerosol time-of-flight mass spectrometry (ATOFMS) and scanning electron microscopy–energy dispersive X-ray spectrometry (SEM-EDX). Very similar types of particles were observed using both analytical techniques. Calcium-containing particles dominated in the firing area of the sintering unit, Mn and/or Al-bearing particles were observed at the cooling area of the sintering unit, while Mn-containing particles were dominant at the smelting unit. SEM-EDX analysis of particles collected downstream of the industrial filters showed that the composition of the particles emitted from the chimneys is very similar to those collected on the filters. ATOFMS analysis of ore samples was also performed to identify particulate emissions that could be generated by wind erosion and manual activities. Specific particle types have been identified for each emission source (chimneys and ore piles) and can be used as tracers for source apportionment of ambient PM measured in the vicinity of the industrial site. - Highlights: • Similar composition for emitted particles as those collected on the chimney filters. • Emitted particles dominated by Ca-, Mn and/or Al-containing particles. • Identification of specific particle types emitted by the different process units. - The particles emitted by metallurgy activities are fully described by ATOFMS and SEM-EDX, enabling the identification of specific particle types from the different units of the process.

  5. Resonant X-ray emission spectroscopy in Dy compounds

    International Nuclear Information System (INIS)

    Tanaka, Satoshi; Okada, Kozo; Kotani, Akio.

    1994-01-01

    The excitation spectrum of the L 3 -M 5 X-ray emission of Dy compounds in the pre-edge region of Dy L 3 X-ray absorption near edge structure (L 3 -XANES) is theoretically investigated based upon the coherent second order optical formula with multiplet coupling effects. The spectral broadening of the excitation spectrum is determined by the M 5 core hole lifetime, being free from the L 3 core hole lifetime. The fine pre-edge structure of the L 3 edge due to the 2p→4f quadrupole transition can be seen in the excitation spectrum, while this structure is invisible in the conventional XANES, in agreement with the recent experimental results. We clarify the conditions for the excitation spectrum to be regarded as the absorption spectrum with a smaller width. The resonant X-ray emission spectra for various incident photon energies around the L 3 edge are also calculated. (author)

  6. Laboratory simulation of charge exchange-produced X-ray emission from comets.

    Science.gov (United States)

    Beiersdorfer, P; Boyce, K R; Brown, G V; Chen, H; Kahn, S M; Kelley, R L; May, M; Olson, R E; Porter, F S; Stahle, C K; Tillotson, W A

    2003-06-06

    In laboratory experiments using the engineering spare microcalorimeter detector from the ASTRO-E satellite mission, we recorded the x-ray emission of highly charged ions of carbon, nitrogen, and oxygen, which simulates charge exchange reactions between heavy ions in the solar wind and neutral gases in cometary comae. The spectra are complex and do not readily match predictions. We developed a charge exchange emission model that successfully reproduces the soft x-ray spectrum of comet Linear C/1999 S4, observed with the Chandra X-ray Observatory.

  7. X-ray emission from stainless steel foils irradiated by femtosecond petawatt laser pulses

    Science.gov (United States)

    Alkhimova, M. A.; Faenov, A. Ya; Pikuz, T. A.; Skobelev, I. Yu; Pikuz, S. A.; Nishiuchi, M.; Sakaki, H.; Pirozhkov, A. S.; Sagisaka, S.; Dover, N. P.; Kondo, Ko; Ogura, K.; Fukuda, Y.; Kiriyama, H.; Esirkepov, T.; Bulanov, S. V.; Andreev, A.; Kando, M.; Zhidkov, A.; Nishitani, K.; Miyahara, T.; Watanabe, Y.; Kodama, R.; Kondo, K.

    2018-01-01

    We report about nonlinear growth of x-ray emission intensity emitted from plasma generated by femtosecond petawatt laser pulses irradiating stainless steel foils. X-ray emission intensity increases as ˜ I 4.5 with laser intensity I on a target. High spectrally resolved x-ray emission from front and rear surfaces of 5 μm thickness stainless steel targets were obtained at the wavelength range 1.7-2.1 Å, for the first time in experiments at femtosecond petawatt laser facility J-KAREN-P. Total intensity of front x-ray spectra three times dominates to rear side spectra for maximum laser intensity I ≈ 3.2×1021 W/cm2. Growth of x-ray emission is mostly determined by contribution of bremsstrahlung radiation that allowed estimating bulk electron plasma temperature for various magnitude of laser intensity on target.

  8. The Elusive Soft Emission from Hard X-ray Symbiotic System RT Cru

    Science.gov (United States)

    Karovska, Margarita

    2014-09-01

    RT Cru is a fascinating member of a new class of hard X-ray emitting symbiotic binaries showing X-ray emission extending to over 50keV. While its hard X-ray emission has been studied in detail, the soft component of the spectrum, including flares, remains elusive, since previous observations have focused on the high-energy regime. We propose Chandra HRC-S/LETG observations to determine the spatial, spectral, and temporal characteristics of the source of the soft X-ray emission with a goal to establish the origin of the soft component, and determine whether and how it is tied to the hard component. Determining the origin of the soft emission is a crucial piece of the puzzle to understanding the geometry, energetics, and the environment of WD accretion in this class of symbiotic systems.

  9. Chandra Observations of Extended X-Ray Emission in ARP 220

    Science.gov (United States)

    McDowell, J. C.; Clements, D. L.; Lamb, S. A.; Shaked, S.; Hearn, N. C.; Colina, L.; Mundell, C.; Borne, K.; Baker, A. C.; Arribas, S.

    2003-01-01

    We resolve the extended X-ray emission from the prototypical ultraluminous infrared galaxy Arp 220. Extended, faint, edge-brightened, soft X-ray lobes outside the optical galaxy are observed to a distance of 1CL 15 kpc on each side of the nuclear region. Bright plumes inside the optical isophotes coincide with the optical line emission and extend 1 1 kpc from end to end across the nucleus. The data for the plumes cannot be fitted by a single-temperature plasma and display a range of temperatures from 0.2 to 1 keV. The plumes emerge from bright, diffuse circumnuclear emission in the inner 3 kpc centered on the Ha peak, which is displaced from the radio nuclei. There is a close morphological correspondence between the Ha and soft X-ray emission on all spatial scales. We interpret the plumes as a starburst-driven superwind and discuss two interpretations of the emission from the lobes in the context of simulations of the merger dynamics of Arp 220.

  10. X-ray emission from hot plasma

    International Nuclear Information System (INIS)

    Hayakawa, Satio; Kato, Takako.

    1979-01-01

    X-ray emission from hot plasmas is discussed with a critical review of different theories. The results given in the present paper are complementary to those given by Kato in the sense that the present paper is introductory to the paper by Kato. The contents of the present paper are; 1. Introduction 2. Ionization and Recombination Rate Coefficients 3. Relative Abundances of Ions 4. Intensity and Spectra of Radiation 5. Comparison with Earlier Results 6. Emission and Absorption Lines (author)

  11. Combined X-ray CT and mass spectrometry for biomedical imaging applications

    Science.gov (United States)

    Schioppa, E., Jr.; Ellis, S.; Bruinen, A. L.; Visser, J.; Heeren, R. M. A.; Uher, J.; Koffeman, E.

    2014-04-01

    Imaging technologies play a key role in many branches of science, especially in biology and medicine. They provide an invaluable insight into both internal structure and processes within a broad range of samples. There are many techniques that allow one to obtain images of an object. Different techniques are based on the analysis of a particular sample property by means of a dedicated imaging system, and as such, each imaging modality provides the researcher with different information. The use of multimodal imaging (imaging with several different techniques) can provide additional and complementary information that is not possible when employing a single imaging technique alone. In this study, we present for the first time a multi-modal imaging technique where X-ray computerized tomography (CT) is combined with mass spectrometry imaging (MSI). While X-ray CT provides 3-dimensional information regarding the internal structure of the sample based on X-ray absorption coefficients, MSI of thin sections acquired from the same sample allows the spatial distribution of many elements/molecules, each distinguished by its unique mass-to-charge ratio (m/z), to be determined within a single measurement and with a spatial resolution as low as 1 μm or even less. The aim of the work is to demonstrate how molecular information from MSI can be spatially correlated with 3D structural information acquired from X-ray CT. In these experiments, frozen samples are imaged in an X-ray CT setup using Medipix based detectors equipped with a CO2 cooled sample holder. Single projections are pre-processed before tomographic reconstruction using a signal-to-thickness calibration. In the second step, the object is sliced into thin sections (circa 20 μm) that are then imaged using both matrix-assisted laser desorption/ionization mass spectrometry (MALDI-MS) and secondary ion (SIMS) mass spectrometry, where the spatial distribution of specific molecules within the sample is determined. The

  12. Spectral analysis of K-shell X-ray emission of magnesium plasma

    Indian Academy of Sciences (India)

    2014-02-06

    Feb 6, 2014 ... Spectral analysis of K-shell X-ray emission of magnesium plasma, produced by laser pulses of 45 fs duration, focussed up to an intensity of ∼1018 W cm-2, is carried out. The plasma conditions prevalent during the emission of X-ray spectrum were identified by comparing the experimental spectra with the ...

  13. K and L X-ray emission intensities of some radionuclides

    Energy Technology Data Exchange (ETDEWEB)

    Verma, H R; Pal, D [Punjabi Univ., Patiala (India). Dept. of Physics

    1985-01-01

    The K and L x-ray emission intensities per 100 disintegrations have been calculated for some radionuclides using the latest adopted data for gamma-ray intensities, electron capture and internal conversion coefficients for the parent nuclides, fluorescence yield values, Coster-Kronig transition probabilities, average total number of primary L shell vacancies produced in the decay of K shell vacancies and emission rates for various shells and subshells for the daughter nuclei. The results are in good agreement with theoretical and experimental values for the K x-ray intensities. There are no experimental results available to compare with the present calculations for the L x-ray intensities; however, there is a marked discrepancy in the L..cap alpha.. and L..beta.. intensities available on the basis of theoretical estimates.

  14. Particle induced X-ray emission

    International Nuclear Information System (INIS)

    Cohen, D.D.

    1991-08-01

    The accelerator based ion beam technique of Particle Induced X-ray Emission (PIXE) is discussed in some detail. This report pulls together all major reviews and references over the last ten years and reports on PIXE in vacuum and using external beams. The advantages, limitations, costs and types of studies that may be undertaken using an accelerator based ion beam technique such as PIXE, are also discussed. 25 refs., 7 tabs., 40 figs

  15. Chandra X-ray Observations of Jovian Low-latitude Emissions: Morphological, Temporal, and Spectral Characteristics

    Science.gov (United States)

    Bhardwaj, Anil; Elsner, Ronald F.; Gladstone, G. Randall; Cravens, Thomas E.; Waiate J. Hunter, Jr.; Branduardi-Raymont, Graziella; Ford, Peter

    2004-01-01

    Chandra observed X-rays from Jupiter during 24-26 February 2003 for about 40 hours with the ACIS-S and HRC-I instruments. The analysis of Jovian low-latitude "disk" Xray emissions are presented and compared with the high-latitude "auroral" emissions. We report the first Chandra ACIS-S measured X-ray spectrum (0.3-2 keV) of Jupiter's low-latitude disk The disk X-ray emission is harder and extends to higher energies than the auroral spectrum. The temporal variation in the Jovian disk X-rays is on an average consistent with those in the solar X-rays observed by GOES, and TIMED/SSE. Contrary to the auroral X-rays, the disk emissions are uniformly distributed over Jupiter; no indication of longitudinal dependence or correlation with surface magneh field strength is visible. Also, unlike the approx. 40 +/- 20 min periodic oscillations seen in the auroral X-ray emissions, the disk emissions do not show any periodic oscillations. The disk spectrum seems to be consistent with resonant and fluorescent scattering of solar X-rays by the Jovian upper atmosphere. Jupiter's disk is found to be about 50% dimmer in soft X-rays in February 2003 compared that in December 2000, which is consistent with the decrease in solar activity. No evidence of lightning-induced X-rays is seen in the Chandra X-ray data. The Jovian disk spectra observed with Chandra-ACIS is stronger than that observed with XMM-Newton two months later during April 28-29, 2003. The XMM-Newton Xray image of Jupiter shows evidence of limb darkening on the anti-sunward side as seen from Earth, as well as an asymmetry with respect to the subsolar point: suggesting a solar driven process.

  16. X-RAY EMISSION FROM THE WOLF-RAYET BUBBLE S 308

    International Nuclear Information System (INIS)

    Toalá, J. A.; Guerrero, M. A.; Chu, Y.-H.; Gruendl, R. A.; Arthur, S. J.; Smith, R. C.; Snowden, S. L.

    2012-01-01

    The Wolf-Rayet (WR) bubble S 308 around the WR star HD 50896 is one of the only two WR bubbles known to possess X-ray emission. We present XMM-Newton observations of three fields of this WR bubble that, in conjunction with an existing observation of its northwest quadrant, map most of the nebula. The X-ray emission from S 308 displays a limb-brightened morphology, with a central cavity ∼22' in size and a shell thickness of ∼8'. This X-ray shell is confined by the optical shell of ionized material. The spectrum is dominated by the He-like triplets of N VI at 0.43 keV and O VII at 0.57 keV, and declines toward high energies, with a faint tail up to 1 keV. This spectrum can be described by a two-temperature optically thin plasma emission model (T 1 ∼ 1.1 × 10 6 K, T 2 ∼ 13 × 10 6 K), with a total X-ray luminosity ∼2 × 10 33 erg s –1 at the assumed distance of 1.5 kpc.

  17. X-RAY EMISSION FROM THE WOLF-RAYET BUBBLE S 308

    Energy Technology Data Exchange (ETDEWEB)

    Toala, J. A.; Guerrero, M. A. [Instituto de Astrofisica de Andalucia, IAA-CSIC, Glorieta de la Astronomia s/n, 18008 Granada (Spain); Chu, Y.-H.; Gruendl, R. A. [Department of Astronomy, University of Illinois, 1002 West Green Street, Urbana, IL 61801 (United States); Arthur, S. J. [Centro de Radioastronomia y Astrofisica, Universidad Nacional Autonoma de Mexico, Campus Morelia, Apartado Postal 3-72, 58090, Morelia, Michoacan (Mexico); Smith, R. C. [NOAO/CTIO, 950 N. Cherry Avenue, Tucson, AZ 85719 (United States); Snowden, S. L., E-mail: toala@iaa.es [NASA Goddard Space Flight Center, Code 662, Greenbelt, MD 20771 (United States)

    2012-08-10

    The Wolf-Rayet (WR) bubble S 308 around the WR star HD 50896 is one of the only two WR bubbles known to possess X-ray emission. We present XMM-Newton observations of three fields of this WR bubble that, in conjunction with an existing observation of its northwest quadrant, map most of the nebula. The X-ray emission from S 308 displays a limb-brightened morphology, with a central cavity {approx}22' in size and a shell thickness of {approx}8'. This X-ray shell is confined by the optical shell of ionized material. The spectrum is dominated by the He-like triplets of N VI at 0.43 keV and O VII at 0.57 keV, and declines toward high energies, with a faint tail up to 1 keV. This spectrum can be described by a two-temperature optically thin plasma emission model (T{sub 1} {approx} 1.1 Multiplication-Sign 10{sup 6} K, T{sub 2} {approx} 13 Multiplication-Sign 10{sup 6} K), with a total X-ray luminosity {approx}2 Multiplication-Sign 10{sup 33} erg s{sup -1} at the assumed distance of 1.5 kpc.

  18. Space- and time-resolved diagnostics of soft x-ray emission from laser plasmas

    International Nuclear Information System (INIS)

    Richardson, M.C.; Jaanimagi, P.A.; Chen, H.

    1988-01-01

    The analysis of soft x-ray emission from plasmas created by intense short-wavelength laser radiation can provide much useful information on the density, temperature and ionization distribution of the plasma. Until recently, limitations of sensitivity and the availability of suitable x-ray optical elements have restricted studies of soft x-ray emission from laser plasmas. In this paper, the authors describe novel instrumentation which provides high sensitivity in the soft x-ray spectrum with spatial and temporal resolution in the micron and picosecond ranges respectively. These systems exploit advances made in soft x-ray optic and electro-optic technology. Their application in current studies of laser fusion, x-ray lasers, and high density atomic physics are discussed

  19. Low-energy X-ray and gamma spectrometry using silicon photodiodes

    International Nuclear Information System (INIS)

    Silva, Iran Jose Oliveira da

    2000-08-01

    The use of semiconductor detectors for radiation detection has increased in recent years due to advantages they present in comparison to other types of detectors. As the working principle of commercially available photodiodes is similar to the semiconductor detector, this study was carried out to evaluate the use of Si photodiodes for low energy x-ray and gamma spectrometry. The photodiodes investigated were SFH-205, SFH-206, BPW-34 and XRA-50 which have the following characteristics: active area of 0,07 cm 2 and 0,25 cm 2 , thickness of the depletion ranging from 100 to 200 μm and junction capacitance of 72 pF. The photodiode was polarized with a reverse bias and connected to a charge sensitive pre-amplifier, followed by a amplifier and multichannel pulse analyzer. Standard radiation source used in this experiment were 241 Am, 109 Cd, 57 Co and 133 Ba. The X-ray fluorescence of lead and silver were also measured through K- and L-lines. All the measurements were made with the photodiodes at room temperature.The results show that the responses of the photodiodes very linear by the x-ray energy and that the energy resolution in FWHM varied between 1.9 keV and 4.4 keV for peaks corresponding to 11.9 keV to 59 keV. The BPW-34 showed the best energy resolution and the lower dark current. The full-energy peak efficiency was also determined and it was observed that the peak efficiency decreases rapidly above 50 keV. The resolution and efficiency are similar to the values obtained with other semiconductor detectors, evidencing that the photodiodes used in that study can be used as a good performance detector for low energy X-ray and gamma spectrometry. (author)

  20. A laboratory-based hard x-ray monochromator for high-resolution x-ray emission spectroscopy and x-ray absorption near edge structure measurements

    Energy Technology Data Exchange (ETDEWEB)

    Seidler, G. T., E-mail: seidler@uw.edu; Mortensen, D. R.; Remesnik, A. J.; Pacold, J. I.; Ball, N. A.; Barry, N.; Styczinski, M.; Hoidn, O. R. [Physics Department, University of Washington, Seattle, Washington 98195-1560 (United States)

    2014-11-15

    We report the development of a laboratory-based Rowland-circle monochromator that incorporates a low power x-ray (bremsstrahlung) tube source, a spherically bent crystal analyzer, and an energy-resolving solid-state detector. This relatively inexpensive, introductory level instrument achieves 1-eV energy resolution for photon energies of ∼5 keV to ∼10 keV while also demonstrating a net efficiency previously seen only in laboratory monochromators having much coarser energy resolution. Despite the use of only a compact, air-cooled 10 W x-ray tube, we find count rates for nonresonant x-ray emission spectroscopy comparable to those achieved at monochromatized spectroscopy beamlines at synchrotron light sources. For x-ray absorption near edge structure, the monochromatized flux is small (due to the use of a low-powered x-ray generator) but still useful for routine transmission-mode studies of concentrated samples. These results indicate that upgrading to a standard commercial high-power line-focused x-ray tube or rotating anode x-ray generator would result in monochromatized fluxes of order 10{sup 6}–10{sup 7} photons/s with no loss in energy resolution. This work establishes core technical capabilities for a rejuvenation of laboratory-based hard x-ray spectroscopies that could have special relevance for contemporary research on catalytic or electrical energy storage systems using transition-metal, lanthanide, or noble-metal active species.

  1. Studies of the Hard X-ray Emission from the Filippov Type Plasma Focus Device, Dena

    Science.gov (United States)

    Tafreshi, M. A.; Saeedzadeh, E.

    2006-12-01

    This article is about the characteristics of the hard X-ray (HXR) emission from the Filippov type plasma focus (PF) device, Dena. The article begins with a brief presentation of Dena, and the mechanism of the HXR production in PF devices. Then using the differential absorption spectrometry, the energy resolved spectrum of the HXR emission from a 37 kJ discharge in Dena, is estimated. The energy flux density and the energy fluence of this emission have also been calculated to be 1.9 kJ cm-2 s-1 and 9.4 × 10-5 J cm-2. In the end, after presentation of radiography of sheep bones and calf ribs, the medical application of the PF devices has been discussed.

  2. X-ray-based attenuation correction for positron emission tomography/computed tomography scanners.

    Science.gov (United States)

    Kinahan, Paul E; Hasegawa, Bruce H; Beyer, Thomas

    2003-07-01

    A synergy of positron emission tomography (PET)/computed tomography (CT) scanners is the use of the CT data for x-ray-based attenuation correction of the PET emission data. Current methods of measuring transmission use positron sources, gamma-ray sources, or x-ray sources. Each of the types of transmission scans involves different trade-offs of noise versus bias, with positron transmission scans having the highest noise but lowest bias, whereas x-ray scans have negligible noise but the potential for increased quantitative errors. The use of x-ray-based attenuation correction, however, has other advantages, including a lack of bias introduced from post-injection transmission scanning, which is an important practical consideration for clinical scanners, as well as reduced scan times. The sensitivity of x-ray-based attenuation correction to artifacts and quantitative errors depends on the method of translating the CT image from the effective x-ray energy of approximately 70 keV to attenuation coefficients at the PET energy of 511 keV. These translation methods are usually based on segmentation and/or scaling techniques. Errors in the PET emission image arise from positional mismatches caused by patient motion or respiration differences between the PET and CT scans; incorrect calculation of attenuation coefficients for CT contrast agents or metallic implants; or keeping the patient's arms in the field of view, which leads to truncation and/or beam-hardening (or x-ray scatter) artifacts. Proper interpretation of PET emission images corrected for attenuation by using the CT image relies on an understanding of the potential artifacts. In cases where an artifact or bias is suspected, careful inspection of all three available images (CT and PET emission with and without attenuation correction) is recommended. Copyright 2003 Elsevier Inc. All rights reserved.

  3. Cometary X-ray Emission: the View After the First Chandra Observations

    Science.gov (United States)

    Lisse, C. M.

    2002-01-01

    The unexpected discovery of x-ray emission from Comet Hyakutake in March 1996 (Lisse et al. 1996) has produced a number of questions about the physical mechanism producing the radiation. The original detection and subsequent observations (Dennerl et al. 1997, Mumma et al. 1997, Krasnopolsky et al. 1998, Owens et al. 1998, Lisse et al. 1999) have shown that the very soft (best fit thermal bremsstrahlung model kT ~ 0.2 keV) emission is due to an interaction between the solar wind and the comet's atmosphere. Using the results from the 15 comets detected to date in x-rays, we report on the latest results on cometary x-ray emission, including new results from Chandra and XMM. As-observed morphologies, spectra, and light curves will be discussed. Our emphasis will be on understanding the physical mechanism producing the emission, and using this to determine the nature of the cometary coma, the structure of the solar wind in the heliosphere, and the source of the local soft x-ray background. This work has been graciously supported by grants from the NASA Planetary Astronomy and Astrophysical Data Programs.

  4. THERMAL EMISSION IN THE EARLY X-RAY AFTERGLOWS OF GAMMA-RAY BURSTS: FOLLOWING THE PROMPT PHASE TO LATE TIMES

    Energy Technology Data Exchange (ETDEWEB)

    Friis, Mette [Centre for Astrophysics and Cosmology, Science Institute, University of Iceland, Dunhagi 5, 107 Reykjavik (Iceland); Watson, Darach, E-mail: mef4@hi.is, E-mail: darach@dark-cosmology.dk [Dark Cosmology Centre, Niels Bohr Institute, University of Copenhagen, Juliane Maries Vej 30, DK-2100 Copenhagen O (Denmark)

    2013-07-01

    Thermal radiation, peaking in soft X-rays, has now been detected in a handful of gamma-ray burst (GRB) afterglows and has to date been interpreted as shock break-out of the GRB's progenitor star. We present a search for thermal emission in the early X-ray afterglows of a sample of Swift bursts selected by their brightness in X-rays at early times. We identify a clear thermal component in eight GRBs and track the evolution. We show that at least some of the emission must come from highly relativistic material since two show an apparent super-luminal expansion of the thermal component. Furthermore, we determine very large luminosities and high temperatures for many of the components-too high to originate in a supernova shock break-out. Instead, we suggest that the component may be modeled as late photospheric emission from the jet, linking it to the apparently thermal component observed in the prompt emission of some GRBs at gamma-ray and hard X-ray energies. By comparing the parameters from the prompt emission and the early afterglow emission, we find that the results are compatible with the interpretation that we are observing the prompt quasi-thermal emission component in soft X-rays at a later point in its evolution.

  5. Lifetime-vibrational interference effects in resonantly excited x-ray emission spectra of CO

    Energy Technology Data Exchange (ETDEWEB)

    Skytt, P.; Glans, P.; Gunnelin, K. [Uppsala Univ. (Sweden)] [and others

    1997-04-01

    The parity selection rule for resonant X-ray emission as demonstrated for O{sub 2} and N{sub 2} can be seen as an effect of interference between coherently excited degenerate localized core states. One system where the core state degeneracy is not exact but somewhat lifted was previously studied at ALS, namely the resonant X-ray emission of amino-substituted benzene (aniline). It was shown that the X-ray fluorescence spectrum resulting from excitation of the C1s at the site of the {open_quotes}aminocarbon{close_quotes} could be described in a picture separating the excitation and the emission processes, whereas the spectrum corresponding to the quasi-degenerate carbons could not. Thus, in this case it was necessary to take interference effects between the quasi-degenerate intermediate core excited states into account in order to obtain agreement between calculations and experiment. The different vibrational levels of core excited states in molecules have energy splittings which are of the same order of magnitude as the natural lifetime broadening of core excitations in the soft X-ray range. Therefore, lifetime-vibrational interference effects are likely to appear and influence the band shapes in resonant X-ray emission spectra. Lifetime-vibrational interference has been studied in non-resonant X-ray emission, and in Auger spectra. In this report the authors discuss results of selectively excited soft X-ray fluorescence spectra of molecules, where they focus on lifetime-interference effects appearing in the band shapes.

  6. Hard X-ray Emission from Galaxy Clusters Observed with INTEGRAL and Prospects for Simbol-X

    Science.gov (United States)

    Eckert, D.; Paltani, S.; Courvoisier, T. J.-L.

    2009-05-01

    Some galaxy clusters are known to contain a large population of relativistic electrons, which produce radio emission through synchrotron radiation. Therefore, it is expected that inverse-Compton scattering of the relativistic electrons with the CMB produce non-thermal emission which should be observable in the hard X-ray domain. Here we focus on the recent results by INTEGRAL, which shed a new light on the non-thermal emission thanks to its angular resolution and sensitivity in the hard X-ray range. We also present the exciting prospects in this field for Simbol-X, which will allow us to detect the non-thermal emission in a number of clusters and map the magnetic field throughout the intra-cluster medium.

  7. INTEGRAL hard X-ray spectra of the cosmic X-ray background and Galactic ridge emission

    Science.gov (United States)

    Türler, M.; Chernyakova, M.; Courvoisier, T. J.-L.; Lubiński, P.; Neronov, A.; Produit, N.; Walter, R.

    2010-03-01

    Aims: We derive the spectra of the cosmic X-ray background (CXB) and of the Galactic ridge X-ray emission (GRXE) in the ~20-200 keV range from the data of the IBIS instrument aboard the INTEGRAL satellite obtained during the four dedicated Earth-occultation observations in early 2006. Methods: We analyze the modulation of the IBIS/ISGRI detector counts induced by the passage of the Earth through the field of view of the instrument. Unlike previous studies, we do not fix the spectral shape of the various contributions, but model instead their spatial distribution and derive for each of them the expected modulation of the detector counts. The spectra of the diffuse emission components are obtained by fitting the normalizations of the model lightcurves to the observed modulation in different energy bins. Because of degeneracy, we guide the fits with a realistic choice of the input parameters and a constraint for spectral smoothness. Results: The obtained CXB spectrum is consistent with the historic HEAO-1 results and falls slightly below the spectrum derived with Swift/BAT. A 10% higher normalization of the CXB cannot be completely excluded, but it would imply an unrealistically high albedo of the Earth. The derived spectrum of the GRXE confirms the presence of a minimum around 80 keV with improved statistics and yields an estimate of ~0.6 M⊙ for the average mass of white dwarfs in the Galaxy. The analysis also provides updated normalizations for the spectra of the Earth's albedo and the cosmic-ray induced atmospheric emission. Conclusions: This study demonstrates the potential of INTEGRAL Earth-occultation observations to derive the hard X-ray spectra of three fundamental components: the CXB, the GRXE and the Earth emission. Further observations would be extremely valuable to confirm our results with improved statistics.

  8. Characterizing X-Ray and Radio Emission in the Black Hole X-Ray Binary V404 Cygni During Quiescence

    Science.gov (United States)

    Rana, Vikram; Loh, Alan; Corbel, Stephane; Tomsick, John A.; Chakrabarty, Deepto; Walton, Dominic J.; Barret, Didier; Boggs, Steven E.; Christensen, Finn E.; Craig, William; hide

    2016-01-01

    We present results from multi-wavelength simultaneous X-ray and radio observations of the black hole X-ray binary V404 Cyg in quiescence. Our coverage with NuSTAR provides the very first opportunity to study the X-ray spectrum of V404 Cyg at energies above 10 keV. The unabsorbed broadband (0.3-30 keV) quiescent luminosity of the source is 8.9 x 10(exp 32) erg per sec for a distance of 2.4 kpc. The source shows clear variability on short timescales (an hour to a couple of hours) in the radio, soft X-ray, and hard X-ray bands in the form of multiple flares. The broadband X-ray spectra obtained from XMM-Newton and NuSTAR can be characterized with a power-law model having a photon index of gamma = 2.12 +/- 0.07 (90% confidence errors); however, residuals at high energies indicate spectral curvature significant at a 3 sigma confidence level with the e-folding energy of the cutoff as 20(sub -7)(sup +20) keV. Such curvature can be explained using synchrotron emission from the base of a jet outflow. Radio observations using the VLA reveal that the spectral index evolves on very fast timescales (as short as 10 minutes), switching between optically thick and thin synchrotron emission, possibly due to instabilities in the compact jet or stochastic instabilities in the accretion rate. We explore different scenarios to explain this very fast variability.

  9. Non-thermal Hard X-Ray Emission from Coma and Several Abell Clusters

    International Nuclear Information System (INIS)

    Correa, C

    2004-01-01

    We report results of hard X-Ray observations of the clusters Coma, Abell 496, Abell754, Abell 1060, Abell 1367, Abell2256 and Abell3558 using RXTE data from the NASA HEASARC public archive. Specifically we searched for clusters with hard x-ray emission that can be fitted by a power law because this would indicate that the cluster is a source of non-thermal emission. We are assuming the emission mechanism proposed by Vahk Petrosian where the inter cluster space contains clouds of relativistic electrons that by themselves create a magnetic field and emit radio synchrotron radiation. These relativistic electrons Inverse-Compton scatter Microwave Background photons up to hard x-ray energies. The clusters that were found to be sources of non-thermal hard x-rays are Coma, Abell496, Abell754 and Abell 1060

  10. Cu,Cr and As determination in preserved woods (Eucalyptus ssp.) by X-ray fluorescence spectrometries; Determinacao de cobre, cromo e arsenio em madeira preservada (Eucalyptus sp.) pelas espectrometrias de fluorescencia de raios X

    Energy Technology Data Exchange (ETDEWEB)

    Pereira Junior, Sergio Matias

    2014-07-01

    Brazil produces around 2.2 millions of cubic meters of treated wood to meet the annual demand of railway, electric, rural and construction sectors. The most used wood species are eucalyptus (Eucalyptus ssp.) and pine (Pinus ssp.).The treated woods used for poles, sleepers, fence posts and plywoods should be according to Brazilian norms requirements. The most usual wood preservative products used in Brazil are CCA (chromated copper arsenate) and CCB (copper chromium and boron salt). The analytical methods, such as flame atomic absorption spectrometry (FAAS), plasma inductively coupled optical emission spectrometry (ICPOES) and X-ray fluorescence spectrometry (XRFS) have been used for the analytical control of those treatment processes. In this work, the eucalyptus trees (Eucalyptus ssp) samples was obtained from Minas Gerais State, Brazil, cut plantation areas. Under pressure, eucalyptus wood samples were submitted to different concentration of CCA solution reaching 3.9, 6.7, 9.1, 12.4 and 14.0 kg of CCA by m-³ sapwood retentions. Samples in cylinders and sawdust forms were obtained from treated wood samples. Copper, chromium and arsenic determination was performed using the energy dispersive X-ray fluorescence spectrometry (EDXRFS), portable X-ray fluorescence spectrometry (PXRFS), flame atomic absorption spectrometry (FAAS) and instrumental neutron activation analysis. In this work, the method of analysis, sensitivity, precision and accuracy performances of the related techniques were outlined. (author)

  11. Disentangling the gamma-ray emission towards Cygnus X: Sh2-104

    Science.gov (United States)

    Gotthelf, Eric

    2015-09-01

    We have just discovered distinct X-ray emission coincident with VER J2018+363, a TeV source recently resolved from the giant gamma-ray complex MGRO J2019+37 in the Cygnus region. NuSTAR reveals a hard point source and a diffuse nebula adjacent to and possibly part of Sh2-104, a compact HII region containing several young massive stellar clusters. There is reasonable evidence that these X-rays probe the origin of the gamma-ray flux, however, unrelated extragalactic sources need to be excluded. We propose a short Chandra observation to localize the X-ray emission to identify a putative pulsar or stellar counterpart(s). This is an important step to fully understand the energetics of the MGRO J2019+37 complex and the production of gamma-rays in star formation regions, in general.

  12. High resolution krypton M/sub 4,5/ x-ray emission spectra

    International Nuclear Information System (INIS)

    Perera, R.C.C.; Hettrick, M.C.; Lindle, D.W.

    1987-10-01

    High resolution M/sub 4,5/ (3d → 4p) x-ray emission spectra from a krypton plasma were measured using a recently developed grazing-incidence reflection-grating monochromator/spectrometer with very high flux rates at extreme ultraviolet and soft x-ray wave lengths. The nominal resolving power of the instrument, E/ΔE, is about 300 in this energy range (∼80 eV). Three dipole-allowed 3d → 4p emission lines were observed at 80.98 eV, 80.35 eV and 79.73 eV. A broad peak at about 82.3 eV is tentatively assigned to transitions resulting from Kr 2+ , and effects of excitation energy on M/sub 4,5/ x-ray emission were observed. 9 refs., 3 figs., 1 tab

  13. A ROTSE-I/ROSAT Survey of X-ray Emission from Contact Binary Stars

    Science.gov (United States)

    Geske, M.; McKay, T.

    2005-05-01

    Using public data from the ROSAT All Sky Survey (RASS) and the ROTSE-I Sky Patrols, the incidence of strong x-ray emissions from contact binary systems was examined. The RASS data was matched to an expanded catalog of contact binary systems from the ROTSE-I data, using a 35 arc second radius. X-ray luminosities for matching objects were then determined. This information was then used to evaluate the total x-ray emissions from all such objects, in order to determine their contribution to the galactic x-ray background.

  14. Working gas effects on the X-ray emission of a plasma focus device

    Energy Technology Data Exchange (ETDEWEB)

    Cengher, M; Presura, R; Zoita, V [Inst. of Physics and Technology of Radiation Devices, Bucharest (Romania)

    1997-12-31

    Experiments on the plasma focus device IPF-2/20 operating with argon, neon and mixtures of argon with deuterium were performed and some X-ray emission parameters measured. The time evolution of the X-ray emission and dependence of the X-ray yield on the working gas composition was analyzed. The softer X radiation was measured with time resolution in the energy bands from 4 to 40 keV, and the hard X-rays for energies above 200 keV. In deuterium-argon mixtures the soft X-ray yield increases both with pressure (for the same ratio of argon) and with the quantity of argon added to deuterium at the same total pressure. For argon or neon the hard X-ray yield is lower than for deuterium-heavy gas mixtures. The softer X-ray yield decreases with pressure both for neon and for argon. (author). 4 figs., 5 refs.

  15. Simple procedure for nutrient analysis of coffee plant with energy dispersive X-ray fluorescence spectrometry (EDXRF)

    Energy Technology Data Exchange (ETDEWEB)

    Tezotto, Tiago; Favarin, Jose Laercio; Neto, Ana Paula; Azevedo, Ricardo Antunes, E-mail: tiago.tezotto@usp.br [Escola Superior de Agricultura Luiz de Queiroz (ESALQ/USP), Piracicaba, SP (Brazil); Gratao, Priscila Lupino [Universidade Estadual Paulista Julio de Mesquita Filho (UNESP/ FCAV), Jaboticabal, SP (Brazil). Dept. de Biologia Aplicada a Agropecuaria; Mazzafera, Paulo [Universidade Estadual de Campinas (UNICAMP/IB), SP (Brazil). Dept. Biologia Vegetal

    2013-07-15

    Nutrient analysis is used to estimate nutrient content of crop plants to manage fertilizer application for sustained crop production. Direct solid analysis of agricultural and environmental samples by energy dispersive X-ray fluorescence spectrometry (EDXRF) was chosen as alternative technique to evaluate the simultaneous multielemental quantification of the most important essential elements in coffee (Coffea arabica L.) plants. Inductively coupled plasma atomic emission spectrometry and certified reference materials made from leaves were used to calibrate and check the trueness of EDXRF method for the determination of the concentration of several nutrients in coffee leaves and branches. Fluorescence spectrometry proved to be advantageous and presented low cost as loose powder samples could be used. Samples collected from a field experiment where coffee plants were treated with excess of Ni and Zn were used to verify the practical application of the method. Good relationships were achieved between certified values and data obtained by EDXRF, with recoveries ranging from 82 to 117 %.(author)

  16. X-Ray Emission from Active Galactic Nuclei with Intermediate-Mass Black Holes

    Science.gov (United States)

    Dewangan, G. C.; Mathur, S.; Griffiths, R. E.; Rao, A. R.

    2008-12-01

    We present a systematic X-ray study of eight active galactic nuclei (AGNs) with intermediate-mass black holes (MBH ~ 8-95 × 104 M⊙) based on 12 XMM-Newton observations. The sample includes the two prototype AGNs in this class—NGC 4395 and POX 52 and six other AGNs discovered with the Sloan Digitized Sky Survey. These AGNs show some of the strongest X-ray variability, with the normalized excess variances being the largest and the power density break timescales being the shortest observed among radio-quiet AGNs. The excess-variance-luminosity correlation appears to depend on both the BH mass and the Eddington luminosity ratio. The break timescale-black hole mass relations for AGN with IMBHs are consistent with that observed for massive AGNs. We find that the FWHM of the Hβ/Hα line is uncorrelated with the BH mass, but shows strong anticorrelation with the Eddington luminosity ratio. Four AGNs show clear evidence for soft X-ray excess emission (kTin ~ 150-200 eV). X-ray spectra of three other AGNs are consistent with the presence of the soft excess emission. NGC 4395 with lowest L/LEdd lacks the soft excess emission. Evidently small black mass is not the primary driver of strong soft X-ray excess emission from AGNs. The X-ray spectral properties and optical-to-X-ray spectral energy distributions of these AGNs are similar to those of Seyfert 1 galaxies. The observed X-ray/UV properties of AGNs with IMBHs are consistent with these AGNs being low-mass extensions of more massive AGNs, those with high Eddington luminosity ratio looking more like narrow-line Seyfert 1 s and those with low L/LEdd looking more like broad-line Seyfert 1 galaxies.

  17. Chemical analysis by X-ray fluorescence, of niobium in high-strength plate steels

    International Nuclear Information System (INIS)

    Iozzi, F.B.; Dias, M.J.P.

    1981-01-01

    The use of X-ray fluorescence spectrometry in quantitative analysis of niobium in steels, as an alternative solution for optical emission spectrometry, in the rapid chemical control of steel fabrication by LD type converters, is presented. (M.C.K.) [pt

  18. X-ray sky

    International Nuclear Information System (INIS)

    Gruen, M.; Koubsky, P.

    1977-01-01

    The history is described of the discoveries of X-ray sources in the sky. The individual X-ray detectors are described in more detail, i.e., gas counters, scintillation detectors, semiconductor detectors, and the principles of X-ray spectrometry and of radiation collimation aimed at increased resolution are discussed. Currently, over 200 celestial X-ray sources are known. Some were identified as nebulae, in some pulsations were found or the source was identified as a binary star. X-ray bursts of novae were also observed. The X-ray radiation is briefly mentioned of spherical star clusters and of extragalactic X-ray sources. (Oy)

  19. Standard test methods for chemical analysis of ceramic whiteware materials using wavelength dispersive X-Ray fluorescence spectrometry

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2004-01-01

    1.1 These test methods cover the determination of ten major elements (SiO2, Al2O3, Fe2O3, MgO, CaO, Na2O, K2O, TiO2, P2O5, MnO, and LOI in ceramic whitewares clays and minerals using wavelength dispersive X-ray fluorescence spectrometry (WDXRF). The sample is first ignited, then fused with lithium tetraborate and the resultant glass disc is introduced into a wavelength dispersive X-ray spectrometer. The disc is irradiated with X-rays from an X-ray tube. X-ray photons emitted by the elements in the samples are counted and concentrations determined using previously prepared calibration standards. (1) In addition to 10 major elements, the method provides a gravimetric loss-on-ignition. Note 1—Much of the text of this test method is derived directly from Major element analysis by wavelength dispersive X-ray fluorescence spectrometry, included in Ref (1). 1.2 Interferences, with analysis by WDXRF, may result from mineralogical or other structural effects, line overlaps, and matrix effects. The structure of the...

  20. The Multi-component X-ray Emission of 3C 273

    Science.gov (United States)

    Soldi, S.; Türler, M.; Paltani, S.; Courvoisier, T. J.-L.

    2009-05-01

    3C 273 is the brightest quasar in the sky and among the most extensively observed and studied AGN, therefore one of the most suitable targets for a long-term, multi-frequency study. The superposition of a thermal Comptonisation component, similar to that observed in Seyfert galaxies, and of a non-thermal component, related to the jet emission, seems to explain some of the spectral and timing properties of the X-ray emission of 3C 273. Yet, during some observations this dichotomy has not been observed and the variability properties could also be consistent with a single-component scenario, characterised by two parameters varying independently. In order to understand the nature of the X-ray emission in 3C 273, a series of observations up to 80-100 keV, possibly catching the source in different flux states, are essential. Simbol-X will be able to study the emission of 3C 273 in the broad 0.5-80 keV band with high sensitivity, allowing us to disentangle the emission from different spectral components, with 20-30 ks long observations. In addition, the shape and the origin of the high-energy emission of this quasar will be further constrained thanks to the AGILE and Fermi satellites, monitoring the γ-ray sky in the MeV-GeV energy domain.

  1. Proton induced X-ray emission (PIXE) analysis at Lucas Heights

    International Nuclear Information System (INIS)

    Cohen, D.; Duerden, P.

    1979-02-01

    The state of the proton induced X-ray emission (PIXE) work at Lucas Heights is reported together with a full description of the experimental arrangement and its use for analysis of trace elements (Z >or= 14). The fundamentals of PIXE are examined in detail with a view to understanding not only the background continuum but also the X-ray production mechanisms. Quantitative predictions for the number of X-rays detected after proton bombardment of the target have been made and these compare well with experiments

  2. THE SPECTACULAR RADIO-NEAR-IR-X-RAY JET OF 3C 111: THE X-RAY EMISSION MECHANISM AND JET KINEMATICS

    Energy Technology Data Exchange (ETDEWEB)

    Clautice, Devon; Perlman, Eric S. [Department of Physics and Space Sciences, Florida Institute of Technology, 150 W. University Boulevard, Melbourne, FL 32901 (United States); Georganopoulos, Markos [Department of Physics, University of Maryland—Baltimore County, 1000 Hilltop Circle, Baltimore, MD 21250 (United States); Lister, Matthew L.; Hogan, Brandon [Department of Physics and Astronomy, Purdue University, 525 Northwestern Avenue, West Lafayette, IN 47907 (United States); Tombesi, Francesco [Department of Astronomy, University of Maryland, College Park, MD 20742-2421 (United States); Cara, Mihai [Space Telescope Science Institute, 3700 San Martin Drive, Baltimore, MD 21218 (United States); Marshall, Herman L. [Kavli Institute for Astrophysics and Space Research, Massachusetts Institute of Technology, Cambridge, MA 02139 (United States); Kazanas, Demos [NASA’s Goddard Space Flight Center, Astrophysics Science Division, Code 663, Greenbelt, MD 20771 (United States)

    2016-08-01

    Relativistic jets are the most energetic manifestation of the active galactic nucleus (AGN) phenomenon. AGN jets are observed from the radio through gamma-rays and carry copious amounts of matter and energy from the sub-parsec central regions out to the kiloparsec and often megaparsec scale galaxy and cluster environs. While most spatially resolved jets are seen in the radio, an increasing number have been discovered to emit in the optical/near-IR and/or X-ray bands. Here we discuss a spectacular example of this class, the 3C 111 jet, housed in one of the nearest, double-lobed FR II radio galaxies known. We discuss new, deep Chandra and Hubble Space Telescope ( HST ) observations that reveal both near-IR and X-ray emission from several components of the 3C 111 jet, as well as both the northern and southern hotspots. Important differences are seen between the morphologies in the radio, X-ray, and near-IR bands. The long (over 100 kpc on each side), straight nature of this jet makes it an excellent prototype for future, deep observations, as it is one of the longest such features seen in the radio, near-IR/optical, and X-ray bands. Several independent lines of evidence, including the X-ray and broadband spectral shape as well as the implied velocity of the approaching hotspot, lead us to strongly disfavor the EC/CMB model and instead favor a two-component synchrotron model to explain the observed X-ray emission for several jet components. Future observations with NuSTAR , HST , and Chandra will allow us to further constrain the emission mechanisms.

  3. Exploring the Hard and Soft X-ray Emission of Magnetic Cataclysmic Variables

    Science.gov (United States)

    de Martino, D.; Anzolin, G.; Bonnet-Bidaud, J.-M.; Falanga, M.; Matt, G.; Mouchet, M.; Mukai, K.; Masetti, N.

    2009-05-01

    A non-negligible fraction of galactic hard (>20 keV) X-ray sources were identified as CVs of the magnetic Intermediate Polar type in INTEGRAL, SWIFT and RXTE surveys, that suggests a still hidden but potentially important population of faint hard X-ray sources. Simbol-X has the unique potential to simultaneously characterize their variable and complex soft and hard X-ray emission thus allowing to understand their putative role in galactic populations of X-ray sources.

  4. Forensic analysis of tempered sheet glass by particle induced X-ray emission (PIXE)

    Energy Technology Data Exchange (ETDEWEB)

    Jisonna, L.J. [Department of Chemistry and Department of Physics, Hope College, Holland, MI 49422-9000 (United States); DeYoung, P.A., E-mail: deyoung@hope.ed [Department of Chemistry and Department of Physics, Hope College, Holland, MI 49422-9000 (United States); Ferens, J.; Hall, C.; Lunderberg, J.M.; Mears, P. [Department of Chemistry and Department of Physics, Hope College, Holland, MI 49422-9000 (United States); Padilla, D. [Department of Physics, San Diego State University, San Diego, CA 92182-1233 (United States); Peaslee, G.F. [Department of Chemistry and Department of Physics, Hope College, Holland, MI 49422-9000 (United States); Sampson, R. [Department of Physics, Columbia University, New York, NY 10027 (United States)

    2011-05-15

    Highlights: {yields} PIXE was found to give the same results for trace elements in glass as ICP. {yields} PIXE can non-destructively determine trace element concentrations in auto glass. {yields} Measured Ca, Fe, Ti, Mn, and Sr in auto glass with PIXE. -- Abstract: The elemental concentrations of five trace elements in tempered sheet glass fragments were determined using particle-induced X-ray emission (PIXE) spectrometry. The trace element concentrations for calcium, iron, manganese, strontium, and titanium are compared to those obtained by inductively-coupled plasma-atomic emission spectrometry (ICP-AES) following complete digestion by hydrofluoric acid. For these five elements, the absolute concentrations obtained by both methods are shown to agree well over a wide range of concentrations. The limits of detection for trace elements are typically lower for the ICP-AES method. However, we show that the concentrations of these five elements can be accurately measured by the PIXE method. Since PIXE is an entirely non-destructive method, there exists a niche for this technique to be used as a complement to the more sensitive ICP-AES technique in the forensic analysis of sheet glass.

  5. Quantitative analysis of phosphosilicate glass films on silicon wafers for calibration of x-ray fluorescence spectrometry standards

    International Nuclear Information System (INIS)

    Weissman, S.H.

    1983-01-01

    The phosphorus and silicon contents of phosphosilicate glass films deposited by chemical vapor deposition (CVD) on silicon wafers were determined. These films were prepared for use as x-ray fluorescence (XRF) spectrometry standards. The thin films were removed from the wafer by etching with dilute hydrofluoric acid, and the P and Si concentrations in solution were determined by inductively coupled plasma atomic emission spectroscopy (ICP). The calculated phosphorus concentration ranged from 2.2 to 12 wt %, with an uncertainty of 2.73 to 10.1 relative percent. Variation between the calculated weight loss (summation of P 2 O 5 and SiO 2 amounts as determined by ICP) and the measured weight loss (determined gravimetrically) averaged 4.9%. Results from the ICP method, Fourier transform-infrared spectroscopy (FT-IR), dispersive infrared spectroscopy, electron microprobe, and x-ray fluorescence spectroscopy for the same samples are compared

  6. Heavy metal determination by X-rays spectrometry for superficial sediments at Guantanamo bay

    International Nuclear Information System (INIS)

    Gelen, A.; Izquierdo; Corrales, W. Y.; Lopez, N.; Casanova, A. O.; Diaz, O.; Manso, M.V.; D Alessandro, K.; Reyes, E.; Toledo, C.; Ruiz, F.; Ramirez, M.; Beltran, J.; Martin, A.

    2007-01-01

    Twelve surface samples of the Guantanamo Bay (Cuba) were collected and analysed by X-Rays Spectrometry. Twenty one elements (Si, Ca, K, Na, P, S, Cl, Al, Fe, Mg, Ti, Mn, C, O, Cr, Cu, Ni, Co, Pb, V and Zn) have been determined. The distribution of the metals is associated with the wastewater from anthropogenic origin that receives the bay, mainly by fluvial currents. Multivariate statistical were used for the analysis of the results. Finally the results analysed were compared with the analysis performed by Engineering Centre for Environmental Management of Bays and Coasts (Cimab) using Inductively Coupled Plasma Emission (ICP) for some elements such as: Cr, Cu, Fe, Ni, Pb, V and Zn. The results show the Guantanamo Bay is less polluted than others Cuban Bays. (Author)

  7. X-RAY EMISSION FROM SN 2004dj: A TALE OF TWO SHOCKS

    Energy Technology Data Exchange (ETDEWEB)

    Chakraborti, Sayan; Yadav, Naveen; Ray, Alak [Tata Institute of Fundamental Research, 1 Homi Bhabha Road, Colaba, Mumbai 400 005 (India); Smith, Randall [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States); Chandra, Poonam [Department of Physics, Royal Military College of Canada, Kingston, ON K7K 7B4 (Canada); Pooley, David, E-mail: schakraborti@fas.harvard.edu [Department of Physics, Sam Houston State University, Huntsville, TX (United States)

    2012-12-20

    Type IIP (Plateau) supernovae are the most commonly observed variety of core-collapse events. They have been detected in a wide range of wavelengths from radio, through optical to X-rays. The standard picture of a Type IIP supernova has the blastwave interacting with the progenitor's circumstellar matter to produce a hot region bounded by a forward and a reverse shock. This region is thought to be responsible for most of the X-ray and radio emission from these objects. Yet the origin of X-rays from these supernovae is not well understood quantitatively. The relative contributions of particle acceleration and magnetic field amplification in generating the X-ray and radio emission need to be determined. In this work, we analyze archival Chandra observations of SN 2004dj, one of the nearest supernovae since SN 1987A, along with published radio and optical information. We determine the pre-explosion mass-loss rate, blastwave velocity, electron acceleration, and magnetic field amplification efficiencies. We find that a greater fraction of the thermal energy goes into accelerating electrons than into amplifying magnetic fields. We conclude that the X-ray emission arises out of a combination of inverse Compton scattering by non-thermal electrons accelerated in the forward shock and thermal emission from supernova ejecta heated by the reverse shock.

  8. Chemical analysis of zinc electroplating solutions by x-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Jung, Sung-Mo; Cho, Young-Mo; Na, Han-Gil

    2007-01-01

    A quantitative analysis method used to analyze chlorine, iron and zinc in electroplating solutions, using X-ray spectrometry in atmospheric He mode, is proposed. The present research concerns the replacement of the conventional analyses of electroplating solutions with rapid and reproducible quantification using X-ray fluorescence spectrometer. An in-depth investigation conducted in the present study identifies the species present in the real electroplating solutions. XRD patterns and semi-quantitative results for the electroplating solutions show synthetic standards based on the compositional range of solutions by analyzing the electroplating solutions obtained in real processes. 28 calibration standard solutions are prepared by diluting liquid standard solutions certified by titration and ICP-OES analyses used to construct the XRF calibration curves for Cl, Fe and Zn. The suggested method showed satisfactory precision and accuracy in the analysis of electroplating solutions. The present study provides evidences that the proposed XRF spectrometry could be an alternative analytical method to replace the conventional techniques by comparing the uncertainties estimated for each method. (author)

  9. Is scanning electron microscopy/energy dispersive X-ray spectrometry (SEM/EDS) quantitative?

    Science.gov (United States)

    Newbury, Dale E; Ritchie, Nicholas W M

    2013-01-01

    Scanning electron microscopy/energy dispersive X-ray spectrometry (SEM/EDS) is a widely applied elemental microanalysis method capable of identifying and quantifying all elements in the periodic table except H, He, and Li. By following the "k-ratio" (unknown/standard) measurement protocol development for electron-excited wavelength dispersive spectrometry (WDS), SEM/EDS can achieve accuracy and precision equivalent to WDS and at substantially lower electron dose, even when severe X-ray peak overlaps occur, provided sufficient counts are recorded. Achieving this level of performance is now much more practical with the advent of the high-throughput silicon drift detector energy dispersive X-ray spectrometer (SDD-EDS). However, three measurement issues continue to diminish the impact of SEM/EDS: (1) In the qualitative analysis (i.e., element identification) that must precede quantitative analysis, at least some current and many legacy software systems are vulnerable to occasional misidentification of major constituent peaks, with the frequency of misidentifications rising significantly for minor and trace constituents. (2) The use of standardless analysis, which is subject to much broader systematic errors, leads to quantitative results that, while useful, do not have sufficient accuracy to solve critical problems, e.g. determining the formula of a compound. (3) EDS spectrometers have such a large volume of acceptance that apparently credible spectra can be obtained from specimens with complex topography that introduce uncontrolled geometric factors that modify X-ray generation and propagation, resulting in very large systematic errors, often a factor of ten or more. © Wiley Periodicals, Inc.

  10. Solar Coronal Events with Extended Hard X-ray and Gamma-ray Emission

    Science.gov (United States)

    Hudson, H. S.

    2017-12-01

    A characteristic pattern of solar hard X-ray emission, first identified in SOL1969-03-31 by Frost & Dennis (1971) now has been linked to prolonged high-energy gamma-ray emission detected by the Fermi/LAT experiment, for example in SOL2014-09-01. The distinctive features of these events include flat hard X-ray spectra extending well above 100 keV, a characteristic pattern of time development, low-frequency gyrosynchrotron peaks, CME association, and gamma-rays identifiable with pion decay originating in GeV ions. The identification of these events with otherwise known solar structures nevertheless remains elusive, in spite of the wealth of imagery available from AIA. The quandary is that these events have a clear association with CMEs in the high corona, and yet the gamma-ray production implicates the photosphere itself. The vanishingly small loss cone in the nominal acceleration region makes this extremely difficult. I propose direct inward advection of a part of the SEP particle population, as created on closed field structures, as a possible resolution of this puzzle, and note that this requires retracting magnetic structures on long time scales following the flare itself.

  11. Analyais of solar X-ray emission line profiles

    International Nuclear Information System (INIS)

    Burek, A.J.; Marrus, D.M.; Blake, R.L.; Fenimore, E.E.

    1981-01-01

    We report results of the analysis of the X-ray emission line profiles for the Ne X La and Fe XVII 4d 1 P 1 lines produced in an active region that was undergoing a radio and X-ray gradual rise and fall (GRF) in intensity. The spectra were obtained with collimated Bragg spectrometers launched on a rocket from White Sands Missile Range on 1976 March 26. Using a crystal of ammonium acid phthalate, we have fully resolved the Ne X La and Fe XVII 4d 1 P 1 lines, permitting an accurate determinination of the Ne X La intensity and allowing Doppler broadened profiles for lines formed from ions having greatly different atomic mass and charge to be measured. An isothermal model derived from the Ne IX/Ne X resonance line intensity ratio gives an electron temperature of 3.4 x 10 6 K. An isothermal model, however, fails to account for the intensities of all lines and continuum observed. All multitemperature models that do reproduce the observed relative line intensities require the presence of a hot plasma component with an electron temperature in excess of 5 x 10 6 K. The presence of a high temperature component is also suggested by the measured line to continuum ratio of 3.6 in the 12--15 A wavelength interval. Interpretation of the line profiles in terms of a multitemperature model requires an rms turbulence velocity of 48 +- 15 km s -1 for Fe XVII 1 P 1 and 74 +- 54 km s - 2exclamation for Ne X La at the 95% confidence level. Collimated scans across the active region show the presence of a compact source of intense X-ray emission close to the magnetic neutral line, which is very probably the GRF plasma

  12. Energy dispersive x-ray spectrometry by microcalorimetry for the SEM

    CERN Document Server

    Newbury, D; Sae Woo Nam; Hilton, G; Irwin, K; Small, J; Martinis, J

    2002-01-01

    Analytical x-ray spectrometry for electron beam instruments has advanced significantly with the development of the microcalorimeter energy dispersive x-ray spectrometer (mu cal EDS). The mu cal EDS operates by measuring the temperature rise when a single photon is absorbed in a metal target. A cryoelectronic circuit with electrothermal feedback and a superconducting transition edge sensor serves as the thermometer. Spectral resolution approaching 4.5 eV for high energy photons (6000 eV) and 2 eV for low energy photons below 2000 eV has been demonstrated in energy dispersive operation across a photon energy range from 250 eV to 8 keV. Spectra of a variety of materials demonstrate the power of the mu cal EDS to solve practical problems while operating on a scanning electron microscope platform. (author)

  13. NuSTAR Hard X-ray Survey of the Galactic Center Region. I. Hard X-ray Morphology and Spectroscopy of the Diffuse Emission

    DEFF Research Database (Denmark)

    Mori, Kaya; Hailey, Charles J.; Krivonos, Roman

    2015-01-01

    We present the first sub-arcminute images of the Galactic Center above 10 keV, obtained with NuSTAR. NuSTAR resolves the hard X-ray source IGR J17456-2901 into non-thermal X-ray filaments, molecular clouds, point sources, and a previously unknown central component of hard X-ray emission (CHXE). Nu...

  14. Dissecting Diffuse X-ray Emission in 30 Doradus with T-ReX

    Science.gov (United States)

    Townsley, Leisa K.; Broos, Patrick

    2017-08-01

    30 Doradus (the Tarantula Nebula) offers us a microscope on starburst astrophysics, having endured 25 Myrs of the birth and death of the most massive stars known. Across 30 Dor's 250-pc extent, stellar winds and supernovae have carved its ISM into an amazing display of arcs, pillars, and bubbles. For over 40 years, we have also known that 30 Dor is a bright X-ray emitter, so its familiar stars and cold ISM structures suffer irradiation by multi-million-degree plasmas. The 2-Ms Chandra X-ray Visionary Project ``The Tarantula -- Revealed by X-rays'' (T-ReX) exploits Chandra's fine spatial resolution and the ACIS-I field of view to study ISM interfaces on 1--10 pc scales across the entire 30 Dor complex. Here we give preliminary results from ongoing analyses of these data, focusing on the diffuse X-ray emission. Massive star winds and cavity supernovae over the millenia have contributed to a broad mix of X-ray-emitting plasmas and absorbing columns, showing that 30 Dor's hot ISM is just as complex and confusing as that seen at colder temperatures.

  15. Hard x ray imaging and the relative contribution of thermal and nonthermal emission in flares

    International Nuclear Information System (INIS)

    Holman, G.D.

    1986-01-01

    The question of whether the impulsive 25 to 100 keV x ray emission from solar flares is thermal or nonthermal has been a long-standing controversy. Both thermal and nonthermal (beam) models have been developed and applied to the hard x ray data. It now seems likely that both thermal and nonthermal emission have been observed at hard x ray energies. The Hinotori classification scheme, for example, is an attempt to associate the thermal-nonthermal characteristics of flare hard x ray emission with other flare properties. From a theoretical point of view, it is difficult to generate energetic, nonthermal electrons without dumping an equal or greater amount of energy into plasma heating. On the other hand, any impulsive heating process will invariably generate at least some nonthermal particles. Hence, strictly speaking, although thermal or nonthermal emission may dominate the hard x ray emission in a given energy range for a given flare, there is no such thing as a purely thermal or nonthermal flare mechanism

  16. Extracting chemical information from high-resolution Kβ X-ray emission spectroscopy

    Science.gov (United States)

    Limandri, S.; Robledo, J.; Tirao, G.

    2018-06-01

    High-resolution X-ray emission spectroscopy allows studying the chemical environment of a wide variety of materials. Chemical information can be obtained by fitting the X-ray spectra and observing the behavior of some spectral features. Spectral changes can also be quantified by means of statistical parameters calculated by considering the spectrum as a probability distribution. Another possibility is to perform statistical multivariate analysis, such as principal component analysis. In this work the performance of these procedures for extracting chemical information in X-ray emission spectroscopy spectra for mixtures of Mn2+ and Mn4+ oxides are studied. A detail analysis of the parameters obtained, as well as the associated uncertainties is shown. The methodologies are also applied for Mn oxidation state characterization of double perovskite oxides Ba1+xLa1-xMnSbO6 (with 0 ≤ x ≤ 0.7). The results show that statistical parameters and multivariate analysis are the most suitable for the analysis of this kind of spectra.

  17. The Origin of the Extra-nuclear X-ray Emission in the Seyfert Galaxy NGC 2992

    Science.gov (United States)

    Colbert, E. J. M.; Strickland, D. K.; Veilleux, S.; Weaver, K. A.

    2004-12-01

    We present an analysis of a Chandra ACIS observation of the edge-on Seyfert galaxy NGC 2992. We find extended X-ray emission with Lx(total) in excess of 10**40 erg/s. The brightest nebula is positioned a few 100 pc from the X-ray core, and is spatially coincident with optical line and radio emission. This emission nebula may be energized by the AGN, as opposed to a nuclear starburst. The expected kpc-scale X-ray emission due to a starburst-driven wind is larger than a few 10**39 erg/s, and we present large-scale X-ray emission that may be associated with such an outflow. The extra-nuclear emission has a very soft spectrum. Chandra and XMM spectra of the total nuclear region show a very prominent ``soft excess'' below 2-3 keV. We shall discuss the spectral properties of this soft excess, and will compare with the results from the spatial analysis, and with AGN and starburst models for extranuclear X-ray nebulae.

  18. Hard X-ray emission from accretion shocks around galaxy clusters

    Science.gov (United States)

    Kushnir, Doron; Waxman, Eli

    2010-02-01

    We show that the hard X-ray (HXR) emission observed from several galaxy clusters is consistent with a simple model, in which the nonthermal emission is produced by inverse Compton scattering of cosmic microwave background photons by electrons accelerated in cluster accretion shocks: The dependence of HXR surface brightness on cluster temperature is consistent with that predicted by the model, and the observed HXR luminosity is consistent with the fraction of shock thermal energy deposited in relativistic electrons being lesssim0.1. Alternative models, where the HXR emission is predicted to be correlated with the cluster thermal emission, are disfavored by the data. The implications of our predictions to future HXR observations (e.g. by NuStar, Simbol-X) and to (space/ground based) γ-ray observations (e.g. by Fermi, HESS, MAGIC, VERITAS) are discussed.

  19. Hard X-ray emission from accretion shocks around galaxy clusters

    Energy Technology Data Exchange (ETDEWEB)

    Kushnir, Doron; Waxman, Eli, E-mail: doron.kushnir@weizmann.ac.il, E-mail: eli.waxman@weizmann.ac.il [Physics Faculty, Weizmann Institute of Science, PO Box 26, Rehovot (Israel)

    2010-02-01

    We show that the hard X-ray (HXR) emission observed from several galaxy clusters is consistent with a simple model, in which the nonthermal emission is produced by inverse Compton scattering of cosmic microwave background photons by electrons accelerated in cluster accretion shocks: The dependence of HXR surface brightness on cluster temperature is consistent with that predicted by the model, and the observed HXR luminosity is consistent with the fraction of shock thermal energy deposited in relativistic electrons being ∼<0.1. Alternative models, where the HXR emission is predicted to be correlated with the cluster thermal emission, are disfavored by the data. The implications of our predictions to future HXR observations (e.g. by NuStar, Simbol-X) and to (space/ground based) γ-ray observations (e.g. by Fermi, HESS, MAGIC, VERITAS) are discussed.

  20. Hard X-ray emission from accretion shocks around galaxy clusters

    International Nuclear Information System (INIS)

    Kushnir, Doron; Waxman, Eli

    2010-01-01

    We show that the hard X-ray (HXR) emission observed from several galaxy clusters is consistent with a simple model, in which the nonthermal emission is produced by inverse Compton scattering of cosmic microwave background photons by electrons accelerated in cluster accretion shocks: The dependence of HXR surface brightness on cluster temperature is consistent with that predicted by the model, and the observed HXR luminosity is consistent with the fraction of shock thermal energy deposited in relativistic electrons being ∼<0.1. Alternative models, where the HXR emission is predicted to be correlated with the cluster thermal emission, are disfavored by the data. The implications of our predictions to future HXR observations (e.g. by NuStar, Simbol-X) and to (space/ground based) γ-ray observations (e.g. by Fermi, HESS, MAGIC, VERITAS) are discussed

  1. X-ray fluorescence spectrometry and related techniques an introduction

    CERN Document Server

    Margui, Eva

    2013-01-01

    X-ray fluorescence spectrometry (XRF) is a well-established analytical technique for qualitative and quantitative elemental analysis of a wide variety of routine quality control and research samples. Among its many desirable features, it delivers true multi-element character analysis, acceptable speed and economy, easy of automation, and the capacity to analyze solid samples. This remarkable contribution to this field provides a comprehensive and up-to-date account of basic principles, recent developments, instrumentation, sample preparation procedures, and applications of XRF analysis. If you are a professional in materials science, analytic chemistry, or physics, you will benefit from not only the review of basics, but also the newly developed technologies with XRF. Those recent technological advances, including the design of low-power micro- focus tubes and novel X-ray optics and detectors, have made it possible to extend XRF to the analysis of low-Z elements and to obtain 2D or 3D information on a microme...

  2. The determination of light elements in heavy matrix using proton induced X-ray emission

    International Nuclear Information System (INIS)

    Levenets, V.V.; Omel'nik, A.P.; Shchur, A.A.; Chernov, A.E.; Usikov, N.P.; Zats, A.V.

    2007-01-01

    In this report the possibility of determination of light impurities in heavy matrixes is studied using proton induced X-Ray emission. The wide-band X-ray emission filter made from pyrolytic graphite was used in spectrometric scheme of experiment. The results of studying of filter features in energy range of X-ray emission from 4 to 12 keV were presented. The possibilities were examined of application of pyrolytic graphite filter to modify the X-rays spectrum for determination of iron, using characteristic emission of K-series, and hafnium, using L-series, in substances on base of zirconium (glasses, alloys etc.). It was shown, that the using of similar filter allows to reach the significant improving of metrological characteristics of analysis of mentioned impurities: the limits of detection of iron and hafnium were lowered single-order of magnitude. (authors)

  3. X-ray emission from open star clusters with Spectrum-Rontgen-Gamma

    DEFF Research Database (Denmark)

    Singh, K.P.; Ojha, D.K.; Schnopper, H.W.

    1998-01-01

    The study of X-ray emission from co-evolving populations of stars in open dusters is extremely important for understanding the dynamo activity among the stars. With this objective, we propose to observe a number of open clusters in the X-ray and UV bands using SPECTRUM-Rontgen-Gamma. The high...... throughput of SPECTRUM-Rontgen-Gamma will help detect main sequence stars like Sun in middle-aged and old clusters. We will study the relationships between various parameters - age, rotation, abundance, UBV colors, X-ray luminosity, coronal temperature etc. X-ray spectra of younger and brighter populations...

  4. Magnetar-like X-Ray Bursts Suppress Pulsar Radio Emission

    Energy Technology Data Exchange (ETDEWEB)

    Archibald, R. F.; Lyutikov, M.; Kaspi, V. M.; Tendulkar, S. P. [Department of Physics and McGill Space Institute, McGill University, 3600 University Street, Montreal, QC H3A 2T8 (Canada); Burgay, M.; Possenti, A. [INAF–Osservatorio Astronomico di Cagliari, Via della Scienza 5, I-09047 Selargius (Italy); Esposito, P.; Rea, N. [Anton Pannekoek Institute for Astronomy, University of Amsterdam, Postbus 94249, 1090 GE Amsterdam (Netherlands); Israel, G. [INAF–Osservatorio Astronomico di Roma, via Frascati 33, I-00040 Monteporzio Catone, Roma (Italy); Kerr, M. [Space Science Division, Naval Research Laboratory, Washington, DC 20375-5352 (United States); Sarkissian, J. [CSIRO Astronomy and Space Science, Parkes Observatory, P.O. Box 276, Parkes, NSW 2870 (Australia); Scholz, P., E-mail: archibald@astro.utoronto.ca [National Research Council of Canada, Herzberg Astronomy and Astrophysics, Dominion Radio Astrophysical Observatory, P.O. Box 248, Penticton, BC V2A 6J9 (Canada)

    2017-11-10

    Rotation-powered pulsars and magnetars are two different observational manifestations of neutron stars: rotation-powered pulsars are rapidly spinning objects that are mostly observed as pulsating radio sources, while magnetars, neutron stars with the highest known magnetic fields, often emit short-duration X-ray bursts. Here, we report simultaneous observations of the high-magnetic-field radio pulsar PSR J1119−6127 at X-ray, with XMM-Newton and NuSTAR , and at radio energies with the Parkes radio telescope, during a period of magnetar-like bursts. The rotationally powered radio emission shuts off coincident with the occurrence of multiple X-ray bursts and recovers on a timescale of ∼70 s. These observations of related radio and X-ray phenomena further solidify the connection between radio pulsars and magnetars and suggest that the pair plasma produced in bursts can disrupt the acceleration mechanism of radio-emitting particles.

  5. Quantifying the Exospheric Component of Soft X-ray Emission

    Science.gov (United States)

    Kuntz, Kip; Collier, Michael R.; Snowden, Steven L.; Robertson, Ina; Hansen, Kenneth; Cravens, Thomas

    2007-01-01

    High charge state heavy ions in the solar wind exchange charge with ambient neutral gas. This process creates a product ion in an excited state. During the radiative cascade process, EUV and X-ray photons are emitted with energies in the range of about 100 eV to 1 keV. Because the terrestrial exospheric density at the nominal magnetopause location is relatively high, approx. 10 cu cm, solar wind charge exchange, or SWCX, can be observed by Earth-orbiting soft X-ray instruments such as the ROSAT Position Sensitive Proportional Counters (PSPC). In this presentation, we will compare simulated and observed soft Xray emission during an event on August 18-19, 1991 and discuss the role of exospheric SWCX emission for this and other events.

  6. Electron and photon emissions from gold nanoparticles irradiated by X-ray photons

    Energy Technology Data Exchange (ETDEWEB)

    Casta, R., E-mail: castaromain@gmail.com, E-mail: romain.casta@irsamc.ups-tlse.fr; Champeaux, J.-P.; Moretto-Capelle, P.; Sence, M.; Cafarelli, P. [Université de Toulouse, UPS, Laboratoire Collisions Agrégats Réactivité, IRSAMC, CNRS, UMR 5589 (France)

    2015-01-15

    In this paper, we develop a totally new probabilistic model for the electron and photon emission of gold nanoparticles irradiated by X-ray photons. This model allows direct applications to recent researches about the radiotherapy enhancement by gold nanoparticles in the context of cancer treatment. Our model uses, in a complete original way, simulated Auger cascade and stopping power to compute electron emission spectra, photon emission spectra and released energy inside the material of gold nanoparticles. It allows us to present new results about the electron and photon emission of gold nanoparticle irradiated by hard X-rays.

  7. Application of high resolution x-ray spectrometry preceded by neutron activation for elemental analysis of soil samples

    International Nuclear Information System (INIS)

    Hernandez Rivero, A.; Capote Rodriguez, G.; Herrera Peraza, E.

    1996-01-01

    Utilization of High Resolution X-Ray Spectrometry preceded by activation of the samples by irradiation with neutron fluxes (NAA R X) is a relatively modern trend in application of nuclear techniques. This method may complement advantageously the usual Neutron Activation Analysis by means of Gamma Spectrometry (NAA-G) In this work results obtained by the application of NAA-RX for non-destructive analysis of Cuban soil samples are discussed. The samples were irradiated with reactor neutron fluxes and the induced characteristic X-rays were measured by using Si(li)-detector. Concentrations of Fe, Zn and Eu as determined by NAA-RX are compared with both NAA-G and XRF data. For the elaboration of X-ray and Gamma Spectra the computer programs AXIL and ACTAN were used respectively

  8. Forensic application of total reflection X-ray fluorescence spectrometry for elemental characterization of ink samples

    International Nuclear Information System (INIS)

    Dhara, Sangita; Misra, N.L.; Maind, S.D.; Kumar, Sanjukta A.; Chattopadhyay, N.; Aggarwal, S.K.

    2010-01-01

    The possibility of applying Total Reflection X-ray Fluorescence for qualitative and quantitative differentiation of documents printed with rare earth tagged and untagged inks has been explored in this paper. For qualitative differentiation, a very small amount of ink was loosened from the printed documents by smoothly rubbing with a new clean blade without destroying the manuscript. 50 μL of Milli-Q water was put on this loose powder, on the manuscript, and was agitated by sucking and releasing the suspension two to three times with the help of a micropipette. The resultant dispersion was deposited on quartz sample support for Total Reflection X-ray Fluorescence measurements. The Total Reflection X-ray Fluorescence spectrum of tagged and untagged inks could be clearly differentiated. In order to see the applicability of Total Reflection X-ray Fluorescence for quantitative determinations of rare earths and also to countercheck such determinations in ink samples, the amounts of rare earth in painted papers with single rare earth tagged inks were determined by digesting the painted paper in HNO 3 /HClO 4 , mixing this solution with the internal standard and recording their Total Reflection X-ray Fluorescence spectra after calibration of the instrument. The results thus obtained were compared with those obtained by Inductively Coupled Plasma Mass Spectrometry and were found in good agreement. The average precision of the Total Reflection X-ray Fluorescence determinations was 5.5% (1σ) and the average deviation of Total Reflection X-ray Fluorescence determined values with that of Inductively Coupled Plasma Mass Spectrometry was 7.3%. These studies have shown that Total Reflection X-ray Fluorescence offers a promising and potential application in forensic work of this nature.

  9. Forensic application of total reflection X-ray fluorescence spectrometry for elemental characterization of ink samples

    Energy Technology Data Exchange (ETDEWEB)

    Dhara, Sangita [Fuel Chemistry Division, Bhabha Atomic Research Centre, Mumbai 400 085 (India); Misra, N.L., E-mail: nlmisra@barc.gov.i [Fuel Chemistry Division, Bhabha Atomic Research Centre, Mumbai 400 085 (India); Maind, S.D. [NAA Unit of Central Forensic Science Laboratory Hyderabad at Analytical Chemistry Division, Bhabha Atomic Research Centre, Mumbai 400 085 (India); Kumar, Sanjukta A. [Analytical Chemistry Division, Bhabha Atomic Research Centre, Mumbai 400 085 (India); Chattopadhyay, N. [NAA Unit of Central Forensic Science Laboratory Hyderabad at Analytical Chemistry Division, Bhabha Atomic Research Centre, Mumbai 400 085 (India); Aggarwal, S.K. [Fuel Chemistry Division, Bhabha Atomic Research Centre, Mumbai 400 085 (India)

    2010-02-15

    The possibility of applying Total Reflection X-ray Fluorescence for qualitative and quantitative differentiation of documents printed with rare earth tagged and untagged inks has been explored in this paper. For qualitative differentiation, a very small amount of ink was loosened from the printed documents by smoothly rubbing with a new clean blade without destroying the manuscript. 50 muL of Milli-Q water was put on this loose powder, on the manuscript, and was agitated by sucking and releasing the suspension two to three times with the help of a micropipette. The resultant dispersion was deposited on quartz sample support for Total Reflection X-ray Fluorescence measurements. The Total Reflection X-ray Fluorescence spectrum of tagged and untagged inks could be clearly differentiated. In order to see the applicability of Total Reflection X-ray Fluorescence for quantitative determinations of rare earths and also to countercheck such determinations in ink samples, the amounts of rare earth in painted papers with single rare earth tagged inks were determined by digesting the painted paper in HNO{sub 3}/HClO{sub 4}, mixing this solution with the internal standard and recording their Total Reflection X-ray Fluorescence spectra after calibration of the instrument. The results thus obtained were compared with those obtained by Inductively Coupled Plasma Mass Spectrometry and were found in good agreement. The average precision of the Total Reflection X-ray Fluorescence determinations was 5.5% (1sigma) and the average deviation of Total Reflection X-ray Fluorescence determined values with that of Inductively Coupled Plasma Mass Spectrometry was 7.3%. These studies have shown that Total Reflection X-ray Fluorescence offers a promising and potential application in forensic work of this nature.

  10. Elemental analysis of air particulate samples in Jakarta area by x-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Yumiarti; Yusuf, M.; Mellawati, June; Menry, Yulizon; Surtipanti S

    1998-01-01

    Determination of elements in air particulate samples collected from Jakarta, especially from industrial area Pulo Gadung, also from residence, office, and recreation sites had been carried out. The samples collected periodically from August through December 1996. The elements were analyzed by X-ray fluorescence spectrometry method. Quantitative and qualitative analyses were done using QXAS AXIL (Quantitative X-ray Analysis System of x-ray Spectra by Iterative Least squares fitting) and QAES (Quantitative Analyses of Environmental Samples) package program. Results of the analyses showed that the content of heavy metal elements in air particulate samples from all areas studied were still below the maximum permissible concentration. (authors)

  11. Gravitational Waves versus X and Gamma Ray Emission in a Short Gamma-Ray Burst

    OpenAIRE

    Oliveira, F. G.; Rueda, Jorge A.; Ruffini, Remo

    2012-01-01

    The recent progress in the understanding the physical nature of neutron star equilibrium configurations and the first observational evidence of a genuinely short gamma-ray burst, GRB 090227B, allows to give an estimate of the gravitational waves versus the X and Gamma-ray emission in a short gamma-ray burst.

  12. Modelling of X-ray emission supernova remnants observed by the European satellite XMM-Newton

    International Nuclear Information System (INIS)

    Cassam-Chenai, G.

    2004-01-01

    This thesis deals with the X-ray emission of supernova remnants (SNRs) observed by the European satellite XMM-Newton. In SNRs, the matter heated to millions of degrees shines brightly in X-rays. This emission depends on the hydrodynamical evolution of the SNR, on the chemical composition of the ejected matter and on the ambient medium. Moreover, the blast-wave is considered to be the prime site of the production and the acceleration of cosmic-rays in our Galaxy. XMM-Newton is one of the first to allow the investigation of these different aspects thanks to its spatially-resolved spectroscopy and its very good sensitivity. l first studied Kepler's SNR (SN 1604) whose X-ray emission is dominated by the ejecta. Its observation has allowed to obtain information on the nucleosynthesis products, on their spatial distribution and on the temperature structure in the shocked ejecta. This gives strong constraints on the physics of the explosion and on the progenitor's type. l have shown also that the X-ray emission at the shock is likely to be non-thermal. Then, l studied the SNR G347.3-0.5 whose X-ray emission is entirely due to the synchrotron radiation of relativistic (TeV) electrons accelerated at the shock. From five pointing, l made a full mapping of the X-ray emission characteristics (brightness, absorption and spectral index) at small scale. Combined to radio observations, these results have indicated a clear interaction between the SNR and molecular clouds located at 1 kpc and not at 6 kpc as previously estimated. Lastly, in the framework of a self-similar hydrodynamical model coupled with non-linear particle acceleration, l have obtained the synchrotron emission profile in SNRs, including the adiabatic and radiative losses of the accelerated electrons. (author) [fr

  13. Study of X-ray emission in aluminium z-pinches

    International Nuclear Information System (INIS)

    Rosch, R.

    1999-01-01

    Previous experiments, at 0.1. TX level, have shown that stability and x-ray emission of fast Z-pinches, could be strongly increased by imploding an aluminium vapor jet onto a very thin coaxial wire. We present here first results of an aluminium Z-pinch, using a similar liner, but at mega-ampere level. The pinch is driven by AMBIORIX high-power facility, a 2 TW, 0.5 Ω, 2 MA, 50 ns pulse-line generator. We study the effect of an aluminium wire and its diameter (20-50 μm) on the implosion dynamics, on x-ray yield on MHD stability of the column at stagnation. Analysis of A1 jet on A1 wire shots demonstrates that x-ray yield due to emission processes in the H- and He- like ionization stages (i.e. the K-shell) is significantly enhanced, relative to that of A1 jet only ones. The wire also leads to better symmetry of the implosion, and to better reproducibility of shots. X-ray signals exhibit two similar pulses, 10 ns in width, 15 ns spaced. To discern spectral origin of both pulses, experiments are realized with stainless steel wire (25 μm in diameter). Results show that liner and wire radial simultaneously and contribute to both pulses. Analysis of a typical A1 jet on A1 wire shot, using detailed collisional-radiative equilibrium (CRE) model is also given in this thesis. View o the pinch at stagnation as a cola-dense core surrounded by a hot-low density corona reproduces all features of the X-ray data. (author)

  14. Extended hard-X-ray emission in the inner few parsecs of the Galaxy

    DEFF Research Database (Denmark)

    Perez, Kerstin; Hailey, Charles J.; Bauer, Franz E.

    2015-01-01

    of objects emitting soft X-rays (less than 10 kiloelectronvolts) within the surrounding hundreds of parsecs, as well as the population responsible for unresolved X-ray emission extending along the Galactic plane, is dominated by accreting white dwarf systems. Observations of diffuse hard-X-ray (more than 10...... kiloelectronvolts) emission in the inner 10 parsecs, however, have been hampered by the limited spatial resolution of previous instruments. Here we report the presence of a distinct hard-X-ray component within the central 4 × 8 parsecs, as revealed by subarcminute-resolution images in the 20-40 kiloelectronvolt...... outflows interacting with the surrounding radiation field, dense molecular material or magnetic fields. However, all these interpretations pose significant challenges to our understanding of stellar evolution, binary formation, and cosmic-ray production in the Galactic Centre....

  15. Resonant x-ray emission from gas-phase TiCl4

    International Nuclear Information System (INIS)

    Hague, C.F.; Tronc, M.; De Groot, F.

    1997-01-01

    Resonant x-ray emission spectroscopy (RXES) has proved to be a powerful tool for studying the electronic structure of condensed matter. Over the past few years it has been used mainly for studying the valence bands of solids and condensed molecules. Very recently the advent of high brightness photon beams provided by third generation synchrotron radiation source undulators, associated with efficient x-ray emission spectrometers has made it possible to perform experiments on free diatomic molecular systems. RXE spectra of free molecules are of prime importance to gain insight into their electronic structure and bonding as they reflect the symmetry of orbitals engaged in the two-electron, two-step process with the l = 0, ±2 parity-conserving selection rule, and are free from solid state effects which can introduce difficulties in the interpretation. They provide information (more so than XAS) on the core excited states, and, when performed at fixed incident photon energy as a function of the emitted photon energy, on the electronic excitation (charge transfer, multiplet states). Moreover the anisotropy of the angular distribution of resonant x-ray emission affects the relative intensity of the emission peaks and provides information concerning the symmetries of final states. This is a preliminary report on what are the first RXE spectra of a 3d transition metal complex in the gas phase. The experiment concerns the Ti 3d →2p emission spectrum of TiCl 4 over the 450 to 470 eV region

  16. The X-ray emission spectrum of gaseous acetylene

    International Nuclear Information System (INIS)

    Brammer, R.; Rubensson, J.E.; Wassdahl, N.; Nordgren, J.

    1987-01-01

    The X-ray emission spectrum of acetylene in the gas phase has been recorded using a 10 m grazing incidence spectrometer. Analysis of the spectrum is made based on calculations of total energies, potential curves and Franck-Condon vibrational intensities. Four emission bands are seen with the 1 π u band exhibiting vibrational structure. Analysis of the vibrations gives the CIs ionization energy. High energy satellite structure is observed and interpreted. (orig.)

  17. Optimization of neon soft X-ray emission from 200 J plasma focus device for application in soft X-ray lithography

    International Nuclear Information System (INIS)

    Kalaiselvi, S.M. P.; Tan, T.L.; Talebitaher, A.; Lee, Paul; Rawat, R.S.

    2014-01-01

    The Fast Miniature Plasma Focus (FMPF) device is basically made up of coaxial electrodes with centrally placed anode and six cathode rods surrounding them concentrically. They are enclosed in a vacuum chamber, filled with low pressure operating gas. However, in our experiments, these cathode rods were removed to investigate the influence of them on neon soft X-ray (SXR) and hard X-ray (HXR) emission from the device. On removal of cathode rods, the cathode base plate serves as cathode and the plasma sheath is formed between the anode and the base plate of cathode. Neon was used as the operating gas for our experiments and the FMPF device used is of 235 J energy capacities. The experimental results showed that the FMPF device was able to focus better and the SXR emission efficiency was five times higher without cathode rods than with cathode rods. On the contrary, HXR emission did not vary with and without cathode rods. This observed phenomenon was further cross-checked through imaging of plasma dynamics, with and without cathode rods. FMPF device consists of 4 Pseudo Spark Gap (PSG) switches, which need to operate synchronously to deliver high voltage from capacitors to the anode. It was also seen that, the presence or absence of cathode rods also influence the synchronous operation of PSG switches. It also implies that this is one definite way to optimize the SXR emission from the FMPF device. This study reveals an important finding that, cathode rods play a vital role in the formation of plasma sheath with consequential influence on the radiation emission from plasma focus devices. Enhancement of the X-ray emission from this device is definitely a stepping stone in the realization of this device for industrial applications such as X-ray lithography for semiconductor industries. (author)

  18. Intense Non-Linear Soft X-Ray Emission from a Hydride Target during Pulsed D Bombardment

    Science.gov (United States)

    Miley, George H.; Yang, Yang; Lipson, Andrei; Haque, Munima; Percel, Ian; Romer, Michael

    Radiation emission from low-energy nuclear radiation (LENR) electrodes (both charged-particle and X-rays) represents an important feature of LENR in general. Here, calibration, measurement techniques, and soft X-ray emission results from deuterium bombardment of a Pd target (cathode) placed in a pulsed deuterium glow discharge (PGD) are described. An X-ray intensity of 13.4 mW/cm2 and a dose of 3.3 μJ/cm2 were calculated over a 0.5 ms pulse time from AXUV photodiode radiation detector measurements. A most striking feature is that X-ray energies >600 V are observed with a discharge voltage only about half of that value. To further investigate this phenomenon, emission during room temperature D-desorption from electrolytically loaded Pd:Dx cathodes was also studied. The X-ray emission energy observed was quite similar to the PGD case. However, the intensity in this case was almost 13 orders of magnitude lower due to the much lower deuterium fluxes involved.

  19. Intense non-linear soft X-ray emission from a hydride target during pulsed D bombardment

    International Nuclear Information System (INIS)

    Miley, George H.; Yang, Yang; Lipson, Andrei; Haque, Munima; Percel, Ian; Romer, Michael

    2006-01-01

    Radiation emission from low-energy nuclear radiation (LENR) electrodes (both charged-particle and X-rays) represents an important feature of LENR in general. Here, calibration, measurement techniques, and soft X-ray emission results from deuterium bombardment of a Pd target (cathode) placed in a pulsed deuterium glow discharge (PGD) are described. An X-ray intensity of 13.4 mW/cm 2 and a dose of 3.3 μJ/cm 2 were calculated over a 0.5 ms pulse time from AXUV photodiode radiation detector measurements. A most striking feature is that X-ray energies >600 V are observed with a discharge voltage only about half of that value. To further investigate this phenomenon, emission during room temperature D-desorption from electrolytically loaded Pd:Dx cathodes was also studied. The X-ray emission energy observed was quite similar to the PGD case. However, the intensity in this case was almost 13 orders of magnitude lower due to the much lower deuterium fluxes involved. (author)

  20. X-ray fluorescence and gamma-ray spectrometry combined with multivariate analysis for topographic studies in agricultural soil

    International Nuclear Information System (INIS)

    Castilhos, Natara D.B. de; Melquiades, Fábio L.; Thomaz, Edivaldo L.; Bastos, Rodrigo Oliveira

    2015-01-01

    Physical and chemical properties of soils play a major role in the evaluation of different geochemical signature, soil quality, discrimination of land use type, soil provenance and soil degradation. The objectives of the present study are the soil elemental characterization and soil differentiation in topographic sequence and depth, using Energy Dispersive X-Ray Fluorescence (EDXRF) as well as gamma-ray spectrometry data combined with Principal Component Analysis (PCA). The study area is an agricultural region of Boa Vista catchment which is located at Guamiranga municipality, Brazil. PCA analysis was performed with four different data sets: spectral data from EDXRF, spectral data from gamma-ray spectrometry, concentration values from EDXRF measurements and concentration values from gamma-ray spectrometry. All PCAs showed similar results, confirmed by hierarchical cluster analysis, allowing the data grouping into top, bottom and riparian zone samples, i.e. the samples were separated due to its landscape position. The two hillslopes present the same behavior independent of the land use history. There are distinctive and characteristic patterns in the analyzed soil. The methodologies presented are promising and could be used to infer significant information about the region to be studied. - Highlights: • Characterization of topographic sequence of two hillslopes from agricultural soil. • Employment of EDXRF and gamma-ray spectrometry data combined with PCA. • The combination of green analytical methodologies with chemometric studies allowed soil differentiation. • The innovative methodology is promising for direct characterization of agricultural catchments

  1. X-ray emission in heavy-ion collisions. Progress report, April 1, 1979-March 31, 1980

    International Nuclear Information System (INIS)

    Watson, R.L.

    1980-04-01

    Recent research in the cyclotron institute and department of chemistry at Texas A and M University on the x-ray emission in heavy-ion collisions is described. Areas covered include: spectra of Ka x-rays from 64 MeV sulfur ions traveling in solids; foil-excited Ka x-ray transitions in few-electron sulfur ions; high-resolution study of the target thickness dependence of x-ray emission from 65 MeV sulfur ions; dynamic screening of highly stripped sulfur ions in solids; Mg Ka x-ray satellites excited by ion bombardment, multiplet structure and dependence on projectile and chemical environment; angular distributions of beam and target Ka x-rays; chemical effects on K x-ray satellites of fluorine compounds; and a non-linear least-squares peak-fitting program employing Voight functions

  2. Modulated High-Energy Gamma-Ray Emission from the Micro-quasar Cygnus X-3

    International Nuclear Information System (INIS)

    Abdo, A.A.; Cheung, C.C.; Dermer, C.D.; Grove, J.E.; Johnson, W.N.; Lovellette, M.N.; Makeev, A.; Ray, P.S.; Strickman, M.S.; Wood, K.S.; Abdo, A.A.; Cheung, C.C.; Ackermann, M.; Ajello, M.; Bechtol, K.; Berenji, B.; Blandford, R.D.; Bloom, E.D.; Borgland, A.W.; Cameron, R.A.; Chiang, J.; Claus, R.; Digel, S.W.; Silva, E.D.E.; Drell, P.S.; Dubois, R.; Focke, W.B.; Glanzman, T.; Godfrey, G.; Hayashida, M.; Johannesson, G.; Johnson, A.S.; Kamae, T.; Kocian, M.L.; Lande, J.; Madejski, G.M.; Michelson, P.F.; Mitthumsiri, W.; Monzani, M.E.; Moskalenko, I.V.; Murgia, S.; Nolan, P.L.; Paneque, D.; Reimer, A.; Reimer, O.; Rochester, L.S.; Romani, R.W.; Tanaka, T.; Thayer, J.B.; Tramacere, A.; Uchiyama, Y.; Usher, T.L.; Waite, A.P.; Wang, P.; Ackermann, M.; Ajello, M.; Bechtol, K.; Berenji, B.; Blandford, R.D.; Bloom, E.D.; Borgland, A.W.; Cameron, R.A.; Chiang, J.; Claus, R.; Digel, S.W.; Silva, E.D.E.; Drell, P.S.; Dubois, R.; Focke, W.B.; Glanzman, T.; Godfrey, G.; Hayashida, M.; Johannesson, G.; Johnson, A.S.; Kamae, T.; Kocian, M.L.; Lande, J.; Madejski, G.M.; Michelson, P.F.; Mitthumsiri, W.; Monzani, M.E.; Moskalenko, I.V.; Murgia, S.; Nolan, P.L.; Paneque, D.; Reimer, A.; Reimer, O.; Rochester, L.S.; Romani, R.W.; Tanaka, T.; Thayer, J.B.; Tramacere, A.; Uchiyama, Y.; Usher, T.L.; Waite, A.P.; Wang, P.; Axelsson, M.; Hjalmarsdotter, L.; Axelsson, M.; Conrad, J.; Hjalmarsdotter, L.; Jackson, M.S.; Meurer, C.; Ryde, F.; Ylinen, T.; Baldini, L.; Bellazzini, R.; Brez, A.; Kuss, M.; Latronico, L.; Omodei, N.; Pesce-Rollins, M.; Razzano, M.; Sgro, C.; Ballet, J.; Casandjian, J.M.; Chaty, S.; Corbel, S.; Grenier, I.A.; Koerding, E.; Rodriguez, J.; Starck, J.L.; Tibaldo, L.

    2009-01-01

    Micro-quasars are accreting black holes or neutron stars in binary systems with associated relativistic jets. Despite their frequent outburst activity, they have never been unambiguously detected emitting high-energy gamma rays. The Fermi Large Area Telescope (LAT) has detected a variable high-energy source coinciding with the position of the x-ray binary and micro-quasar Cygnus X-3. Its identification with Cygnus X-3 is secured by the detection of its orbital period in gamma rays, as well as the correlation of the LAT flux with radio emission from the relativistic jets of Cygnus X-3. The gamma-ray emission probably originates from within the binary system, opening new areas in which to study the formation of relativistic jets. (authors)

  3. X-RAY EMISSION FROM YOUNG STARS IN THE MASSIVE STAR-FORMING REGION IRAS 20126+4104

    International Nuclear Information System (INIS)

    Anderson, C. N.; Hofner, P.; Creech-Eakman, M.; Shepherd, D.

    2011-01-01

    We present a 40 ks Chandra observation of the IRAS 20126+4104 core region. In the inner 6'' two X-ray sources were detected, which are coincident with the radio jet source I20S and the variable radio source I20Var. No X-ray emission was detected from the nearby massive protostar I20N. The spectra of both detected sources are hard and highly absorbed, with no emission below 3 keV. For I20S, the measured 0.5-8 keV count rate was 4.3 counts ks -1 . The X-ray spectrum was fitted with an absorbed 1T APEC model with an energy of kT =10 keV and an absorbing column of N H = 1.2 x 10 23 cm -2 . An unabsorbed X-ray luminosity of about 1.4 x 10 32 erg s -1 was estimated. The spectrum shows broad line emission between 6.4 and 6.7 keV, indicative of emission from both neutral and highly ionized iron. The X-ray light curve indicates that I20S is marginally variable; however, no flare emission was observed. The variable radio source I20Var was detected with a count rate of 0.9 counts ks -1 but there was no evidence of X-ray variability. The best-fit spectral model is a 1T APEC model with an absorbing hydrogen column of N H = 1.1 x 10 23 cm -2 and a plasma energy of kT = 6.0 keV. The unabsorbed X-ray luminosity is about 3 x 10 31 erg s -1 .

  4. MODELING THE THERMAL DIFFUSE SOFT AND HARD X-RAY EMISSION IN M17

    International Nuclear Information System (INIS)

    Velázquez, P. F.; Rodríguez-González, A.; Esquivel, A.; Rosado, M.; Reyes-Iturbide, J.

    2013-01-01

    We present numerical models of very young wind driven superbubbles. The parameters chosen for the simulations correspond to the particular case of the M17 nebula, but are appropriate for any young superbubble in which the wind sources have not completely dispersed their parental cloud. From the simulations, we computed the diffuse emission in the soft ([0.5-1.5] keV) and hard ([1.5-5] keV) X-ray bands. The total luminosity in our simulations agrees with the observations of Hyodo et al., about two orders of magnitude below the prediction of the standard model of Weaver et al.. The difference with respect to the standard (adiabatic) model is the inclusion of radiative cooling, which is still important in such young bubbles. We show that for this type of object the diffuse hard X-ray luminosity is significant compared to that of soft X-rays, contributing as much as 10% of the total luminosity, in contrast with more evolved bubbles where the hard X-ray emission is indeed negligible, being at least four orders of magnitude lower than the soft X-ray emission.

  5. Spectral properties of X-ray selected narrow emission line galaxies

    Science.gov (United States)

    Romero-Colmenero, E.

    1998-03-01

    This thesis reports a study of the X-ray and optical properties of two samples of X-ray selected Narrow Emission Line Galaxies (NELGs), and their comparison with the properties of broad line Active Galactic Nuclei (AGN). One sample (18 NELGs) is drawn from the ROSAT International X-ray Optical Survey (RIXOS), the other (19 NELGs and 33 AGN) from the ROSAT UK Deep Survey. ROSAT multi-channel X-ray spectra have been extracted and fitted with power-law, bremsstrahlung and black body models for the brighter RIXOS sources. In most cases, power-law and bremsstrahlung models provide the best results. The average spectral energy index, alpha, of the RIXOS NELGs is 0.96 +/- 0.07, similar to that of AGN (alpha~1). For the fainter RIXOS NELGs, as well as for all the UK Deep Survey sources, counts in three spectral bands have been extracted and fitted with a power-law model, assuming the Galactic value for N_H. The brighter RIXOS sources demonstrated that the results obtained by these two different extraction and fitting procedures provide consistent results. Two average X-ray spectra, one for the NELGs and another for the AGN, were created from the UK Deep Survey sources. The power-law slope of the average NELG is alpha = 0.45 +/- 0.09, whilst that of the AGN is alpha = 0.96 +/- 0.03. ROSAT X-ray surveys have shown that the fractional surface density of NELGs increases with respect to AGN at faint fluxes (case for NELGs to be major contributors to the XRB at the fainter fluxes. The analysis of optical spectroscopy, obtained on La Palma and Hawaii, shows that NELGs form a very heterogeneous group, made up of a mixture of Seyfert 2, LINER and HII-region like galaxies. Seyfert 2 galaxies are found to possess in general the steepest X-ray slopes. Ways to explain this in the context of the unified model of AGN are discussed. The FWHM of some emission lines (Halpha, Hbeta, [NII]) in the NELGs appears to increase with steepening X-ray spectral slope. In the case of the Balmer lines

  6. Weak Hard X-Ray Emission from Two Broad Absorption Line Quasars Observed with NuStar: Compton-Thick Absorption or Intrinsic X-Ray Weakness?

    Science.gov (United States)

    Luo, B.; Brandt, W. N.; Alexander, D. M.; Harrison, F. A.; Stern, D.; Bauer, F. E.; Boggs, S. E.; Christensen, F. E.; Comastri, A.; Craig, W. W..; hide

    2013-01-01

    We present Nuclear Spectroscopic Telescope Array (NuSTAR) hard X-ray observations of two X-ray weak broad absorption line (BAL) quasars, PG 1004+130 (radio loud) and PG 1700+518 (radio quiet). Many BAL quasars appear X-ray weak, probably due to absorption by the shielding gas between the nucleus and the accretion-disk wind. The two targets are among the optically brightest BAL quasars, yet they are known to be significantly X-ray weak at rest-frame 2-10 keV (16-120 times fainter than typical quasars). We would expect to obtain approx. or equal to 400-600 hard X-ray (is greater than or equal to 10 keV) photons with NuSTAR, provided that these photons are not significantly absorbed N(sub H) is less than or equal to 10(exp24) cm(exp-2). However, both BAL quasars are only detected in the softer NuSTAR bands (e.g., 4-20 keV) but not in its harder bands (e.g., 20-30 keV), suggesting that either the shielding gas is highly Compton-thick or the two targets are intrinsically X-ray weak. We constrain the column densities for both to be N(sub H) 7 × 10(exp 24) cm(exp-2) if the weak hard X-ray emission is caused by obscuration from the shielding gas. We discuss a few possibilities for how PG 1004+130 could have Compton-thick shielding gas without strong Fe Ka line emission; dilution from jet-linked X-ray emission is one likely explanation. We also discuss the intrinsic X-ray weakness scenario based on a coronal-quenching model relevant to the shielding gas and disk wind of BAL quasars. Motivated by our NuSTAR results, we perform a Chandra stacking analysis with the Large Bright Quasar Survey BAL quasar sample and place statistical constraints upon the fraction of intrinsically X-ray weak BAL quasars; this fraction is likely 17%-40%.

  7. WEAK HARD X-RAY EMISSION FROM TWO BROAD ABSORPTION LINE QUASARS OBSERVED WITH NuSTAR: COMPTON-THICK ABSORPTION OR INTRINSIC X-RAY WEAKNESS?

    Energy Technology Data Exchange (ETDEWEB)

    Luo, B.; Brandt, W. N. [Department of Astronomy and Astrophysics, 525 Davey Lab, The Pennsylvania State University, University Park, PA 16802 (United States); Alexander, D. M.; Hickox, R. [Department of Physics, Durham University, South Road, Durham DH1 3LE (United Kingdom); Harrison, F. A.; Fuerst, F.; Grefenstette, B. W.; Madsen, K. K. [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, Pasadena, CA 91125 (United States); Stern, D. [Jet Propulsion Laboratory, California Institute of Technology, Pasadena, CA 91109 (United States); Bauer, F. E. [Departamento de Astronomia y Astrofisica, Pontificia Universidad Catolica de Chile, Casilla 306, Santiago 22 (Chile); Boggs, S. E.; Craig, W. W. [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Christensen, F. E. [DTU Space-National Space Institute, Technical University of Denmark, Elektrovej 327, DK-2800 Lyngby (Denmark); Comastri, A. [INAF-Osservatorio Astronomico di Bologna, Via Ranzani 1, I-40127 Bologna (Italy); Fabian, A. C. [Institute of Astronomy, Madingley Road, Cambridge CB3 0HA (United Kingdom); Farrah, D. [Department of Physics, Virginia Tech, Blacksburg, VA 24061 (United States); Fiore, F. [Osservatorio Astronomico di Roma, via Frascati 33, I-00040 Monteporzio Catone (Italy); Hailey, C. J. [Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Matt, G. [Dipartimento di Matematica e Fisica, Universita degli Studi Roma Tre, via della Vasca Navale 84, I-00146 Roma (Italy); Ogle, P. [IPAC, California Institute of Technology, Mail Code 220-6, Pasadena, CA 91125 (United States); and others

    2013-08-01

    We present Nuclear Spectroscopic Telescope Array (NuSTAR) hard X-ray observations of two X-ray weak broad absorption line (BAL) quasars, PG 1004+130 (radio loud) and PG 1700+518 (radio quiet). Many BAL quasars appear X-ray weak, probably due to absorption by the shielding gas between the nucleus and the accretion-disk wind. The two targets are among the optically brightest BAL quasars, yet they are known to be significantly X-ray weak at rest-frame 2-10 keV (16-120 times fainter than typical quasars). We would expect to obtain Almost-Equal-To 400-600 hard X-ray ({approx}> 10 keV) photons with NuSTAR, provided that these photons are not significantly absorbed (N{sub H} {approx}< 10{sup 24} cm{sup -2}). However, both BAL quasars are only detected in the softer NuSTAR bands (e.g., 4-20 keV) but not in its harder bands (e.g., 20-30 keV), suggesting that either the shielding gas is highly Compton-thick or the two targets are intrinsically X-ray weak. We constrain the column densities for both to be N{sub H} Almost-Equal-To 7 Multiplication-Sign 10{sup 24} cm{sup -2} if the weak hard X-ray emission is caused by obscuration from the shielding gas. We discuss a few possibilities for how PG 1004+130 could have Compton-thick shielding gas without strong Fe K{alpha} line emission; dilution from jet-linked X-ray emission is one likely explanation. We also discuss the intrinsic X-ray weakness scenario based on a coronal-quenching model relevant to the shielding gas and disk wind of BAL quasars. Motivated by our NuSTAR results, we perform a Chandra stacking analysis with the Large Bright Quasar Survey BAL quasar sample and place statistical constraints upon the fraction of intrinsically X-ray weak BAL quasars; this fraction is likely 17%-40%.

  8. Evaluation of an automated assay system to measure soil radionuclides by L x-ray and gamma-ray spectrometry

    International Nuclear Information System (INIS)

    Nyhan, J.W.; Drennon, B.J.; Crowell, J.M.

    1982-08-01

    An automated radionuclide assay system for conducting soil radioassays using L x-ray and gamma-ray spectrometry was evaluated. Wet chemistry assay procedures were shown to be considerably more time consuming than similar analyses of soil on this radionuclide assay system. The detection limits of 241 Am and plutonium were determined, as well as the reproducibility of radionuclide assay results. The L x-ray spectrometric measurements were compared with radiochemical analyses on several tuff samples. The assay system's intrinsic germanium detector was found to respond linearly to varying low concentrations of 241 Am and plutonium, both of which were easily detected in the presence of elevated concentrations of 137 Cs

  9. Application of high resolution x-ray spectrometry preceded by neutron activation for elemental analysis of soil samples

    International Nuclear Information System (INIS)

    Hernandez Rivero, A.; Capote Rodriguez, G.; Padilla Alvarez, R.; Herrera Peraza, E.

    1997-01-01

    Utilization of High Resolution X-Ray Spectrometry preceded by activation of the samples by irradiation with neutron fluxes (NAA-RX) is a relatively modern trend in application of nuclear techniques. This method may complement advantageously the usual Neutron Activation Analysis by means of Gamma Spectrometry (NAA-G). In this work results obtained by the application of NAA-RX for non-destructive analysis of Cuban soil samples are discussed. The samples were irradiated with reactor neutron fluxes and the induced characteristic X-rays were measured by using Si(Li)-detector. Concentrations of Fe, Zn and Eu as determined by NAA-RX are compared with both NAA-G and XRF data. For the elaboration of X-Ray and Gamma Spectra the computer programs AXIL and ACTAN were used respectively. (author) [es

  10. Ultrafast atomic process in X-ray emission by using inner-shell ionization method for sodium and carbon atoms

    Energy Technology Data Exchange (ETDEWEB)

    Moribayashi, Kengo; Sasaki, Akira; Tajima, Toshiki [Japan Atomic Energy Research Inst., Neyagawa, Osaka (Japan). Kansai Research Establishment

    1998-07-01

    An ultrafast inner-shell ionization process with X-ray emission stimulated by high-intensity short-pulse X-ray is studied. Carbon and sodium atoms are treated as target matter. It is shown that atomic processes of the target determine the necessary X-ray intensity for X-ray laser emission as well as the features of X-ray laser such as wavelength and duration time. The intensity also depends on the density of initial atoms. Furthermore, we show that as the intensity of X-ray source becomes high, the multi-inner-shell ionization predominates, leading to the formation of hollow atoms. As the density of hollow atoms is increased by the pumping X-ray power, the emission of X-rays is not only of significance for high brightness X-ray measurement but also is good for X-ray lasing. New classes of experiments of pump X-ray probe and X-ray laser are suggested. (author)

  11. X-ray emission in collisions of highly charged I, Pr, Ho, and Bi ions with a W surface

    International Nuclear Information System (INIS)

    Watanabe, H.; Tona, M.; Ohtani, S.; Sun, J.; Nakamura, N.; Yamada, C.; Yoshiyasu, N.; Sakurai, M.

    2007-01-01

    X-ray emission yields, which are defined as the total number of emitted x-ray photons per incident ion, and dissipated fractions of potential energies through x-ray emission have been measured for slow highly charged ions of I, Pr, Ho, and Bi colliding with a W surface. A larger amount of potential energy was consumed for the x-ray emission with increasing the atomic number and the charge state. The present measurements show that x-ray emission is one of the main decay channels of hollow atoms produced in collisions of very highly charged ions of heavy elements

  12. Applications of the Basic programming language in X-ray spectrometry

    International Nuclear Information System (INIS)

    Diaz-Guerra, J.P.; Roca, M.

    1981-01-01

    An assembly of programs written in ''Basic'' language and related with the calculation needs at the X-ray spectrometry laboratory of the Spanish J.E.N. has been developed. The principal problems considered, concerning the X-ray fluorescence technique, are the following: selection of the instrumental parameters; correction of the effects due to the dead time, background and spectral interferences; fitting of polynomial functions, which relate the variables intensity-concentration; application of some empirical-mathematical methods (Lucas-Tooth, Beattie and Brissey and Tertian procedures) to the correction of the inter-element effects; addition method, and statistical treatment of the results (correlation coefficient and ''F'' and ''t'' tests). Likewise, programs for the computation of spacings from powder diffraction patterns (Debye-Scherrer and counter diffractometer procedures) have been written. The proposed programs run following conversational patterns, in which different possibilities and incidences have been foreseen. (author)

  13. The Chandra planetary nebula survey (CHANPLANS). II. X-ray emission from compact planetary nebulae

    Energy Technology Data Exchange (ETDEWEB)

    Freeman, M.; Kastner, J. H. [Center for Imaging Science and Laboratory for Multiwavelength Astrophysics, Rochester Institute of Technology, 54 Lomb Memorial Drive, Rochester, NY 14623 (United States); Montez, R. Jr. [Department of Physics and Astronomy, Vanderbilt University, Nashville, TN (United States); Balick, B. [Department of Astronomy, University of Washington, Seattle, WA (United States); Frew, D. J.; De Marco, O.; Parker, Q. A. [Department of Physics and Astronomy and Macquarie Research Centre for Astronomy, Astrophysics and Astrophotonics, Macquarie University, Sydney, NSW 2109 (Australia); Jones, D. [Departamento de Física, Universidad de Atacama, Copayapu 485, Copiapó (Chile); Miszalski, B. [South African Astronomical Observatory, P.O. Box 9, Observatory, 7935 (South Africa); Sahai, R. [Jet Propulsion Laboratory, MS 183-900, California Institute of Technology, Pasadena, CA 91109 (United States); Blackman, E.; Frank, A. [Department of Physics and Astronomy, University of Rochester, Rochester, NY (United States); Chu, Y.-H. [Department of Astronomy, University of Illinois at Urbana-Champaign, Urbana, IL (United States); Guerrero, M. A. [Instituto de Astrofísica de Andalucía, IAA-CSIC, Glorieta de la Astronomía s/n, Granada, E-18008 (Spain); Lopez, J. A. [Instituto de Astronomía, Universidad Nacional Autonoma de Mexico, Campus Ensenada, Apdo. Postal 22860, Ensenada, B. C. (Mexico); Zijlstra, A. [School of Physics and Astronomy, University of Manchester, Manchester M13 9PL (United Kingdom); Bujarrabal, V. [Instituto de Astrofísica de Canarias, E-38200 La Laguna, Tenerife (Spain); Corradi, R. L. M. [Departamento de Astrofísica, Universidad de La Laguna, E-38206 La Laguna, Tenerife (Spain); Nordhaus, J. [NSF Astronomy and Astrophysics Fellow, Center for Computational Relativity and Gravitation, Rochester Institute of Technology, Rochester, NY 14623 (United States); and others

    2014-10-20

    We present results from the most recent set of observations obtained as part of the Chandra X-ray observatory Planetary Nebula Survey (CHANPLANS), the first comprehensive X-ray survey of planetary nebulae (PNe) in the solar neighborhood (i.e., within ∼1.5 kpc of the Sun). The survey is designed to place constraints on the frequency of appearance and range of X-ray spectral characteristics of X-ray-emitting PN central stars and the evolutionary timescales of wind-shock-heated bubbles within PNe. CHANPLANS began with a combined Cycle 12 and archive Chandra survey of 35 PNe. CHANPLANS continued via a Chandra Cycle 14 Large Program which targeted all (24) remaining known compact (R {sub neb} ≲ 0.4 pc), young PNe that lie within ∼1.5 kpc. Results from these Cycle 14 observations include first-time X-ray detections of hot bubbles within NGC 1501, 3918, 6153, and 6369, and point sources in HbDs 1, NGC 6337, and Sp 1. The addition of the Cycle 14 results brings the overall CHANPLANS diffuse X-ray detection rate to ∼27% and the point source detection rate to ∼36%. It has become clearer that diffuse X-ray emission is associated with young (≲ 5 × 10{sup 3} yr), and likewise compact (R {sub neb} ≲ 0.15 pc), PNe with closed structures and high central electron densities (n{sub e} ≳ 1000 cm{sup –3}), and is rarely associated with PNe that show H{sub 2} emission and/or pronounced butterfly structures. Hb 5 is one such exception of a PN with a butterfly structure that hosts diffuse X-ray emission. Additionally, two of the five new diffuse X-ray detections (NGC 1501 and NGC 6369) host [WR]-type central stars, supporting the hypothesis that PNe with central stars of [WR]-type are likely to display diffuse X-ray emission.

  14. CHANDRA DETECTION OF X-RAY EMISSION FROM ULTRACOMPACT DWARF GALAXIES AND EXTENDED STAR CLUSTERS

    International Nuclear Information System (INIS)

    Hou, Meicun; Li, Zhiyuan

    2016-01-01

    We have conducted a systematic study of X-ray emission from ultracompact dwarf (UCD) galaxies and extended star clusters (ESCs), based on archival Chandra observations. Among a sample of 511 UCDs and ESCs complied from the literature, 17 X-ray counterparts with 0.5–8 keV luminosities above ∼5 × 10 36 erg s −1 are identified, which are distributed in eight early-type host galaxies. To facilitate comparison, we also identify X-ray counterparts of 360 globular clusters (GCs) distributed in four of the eight galaxies. The X-ray properties of the UCDs and ESCs are found to be broadly similar to those of the GCs. The incidence rate of X-ray-detected UCDs and ESCs, 3.3% ± 0.8%, while lower than that of the X-ray-detected GCs (7.0% ± 0.4%), is substantially higher than expected from the field populations of external galaxies. A stacking analysis of the individually undetected UCDs/ESCs further reveals significant X-ray signals, which corresponds to an equivalent 0.5–8 keV luminosity of ∼4 × 10 35 erg s −1 per source. Taken together, these provide strong evidence that the X-ray emission from UCDs and ESCs is dominated by low-mass X-ray binaries having formed from stellar dynamical interactions, consistent with the stellar populations in these dense systems being predominantly old. For the most massive UCDs, there remains the possibility that a putative central massive black hole gives rise to the observed X-ray emission

  15. CHANDRA DETECTION OF X-RAY EMISSION FROM ULTRACOMPACT DWARF GALAXIES AND EXTENDED STAR CLUSTERS

    Energy Technology Data Exchange (ETDEWEB)

    Hou, Meicun; Li, Zhiyuan, E-mail: lizy@nju.edu.cn [School of Astronomy and Space Science, Nanjing University, Nanjing 210046 (China)

    2016-03-10

    We have conducted a systematic study of X-ray emission from ultracompact dwarf (UCD) galaxies and extended star clusters (ESCs), based on archival Chandra observations. Among a sample of 511 UCDs and ESCs complied from the literature, 17 X-ray counterparts with 0.5–8 keV luminosities above ∼5 × 10{sup 36} erg s{sup −1} are identified, which are distributed in eight early-type host galaxies. To facilitate comparison, we also identify X-ray counterparts of 360 globular clusters (GCs) distributed in four of the eight galaxies. The X-ray properties of the UCDs and ESCs are found to be broadly similar to those of the GCs. The incidence rate of X-ray-detected UCDs and ESCs, 3.3% ± 0.8%, while lower than that of the X-ray-detected GCs (7.0% ± 0.4%), is substantially higher than expected from the field populations of external galaxies. A stacking analysis of the individually undetected UCDs/ESCs further reveals significant X-ray signals, which corresponds to an equivalent 0.5–8 keV luminosity of ∼4 × 10{sup 35} erg s{sup −1} per source. Taken together, these provide strong evidence that the X-ray emission from UCDs and ESCs is dominated by low-mass X-ray binaries having formed from stellar dynamical interactions, consistent with the stellar populations in these dense systems being predominantly old. For the most massive UCDs, there remains the possibility that a putative central massive black hole gives rise to the observed X-ray emission.

  16. Optimization of measure parameters for an X- and gamma-ray spectrometry portable system

    International Nuclear Information System (INIS)

    Fernandes, Jaquiel S.; Appoloni, Carlos R.

    2008-01-01

    In order to optimize the use of a system for in situ gamma (γ)- and X-ray spectrometry composed of a 3x3x1 mm 3 Cadmium Telluride (CdTe) detector with respect to the detection of low-activity radioactive sources, a two level factorial planning was accomplished, involving three factors that could modify the system response. This planning was made with a 137 Cs punctual source, analyzing the X-ray energy line of 32 keV from 137m Ba. It was concluded that, for the system optimization, the best configuration for the involved parameters was to work with the detector at temperature of -22 o C, shaping time of 3 μs and rise time discrimination (RTD) with value 3

  17. X-ray Imaging and preliminary studies of the X-ray self-emission from an innovative plasma-trap based on the Bernstein waves heating mechanism

    Science.gov (United States)

    Caliri, C.; Romano, F. P.; Mascali, D.; Gammino, S.; Musumarra, A.; Castro, G.; Celona, L.; Neri, L.; Altana, C.

    2013-10-01

    Electron Cyclotron Resonance Ion Sources (ECRIS) are based on ECR heated plasmas emitting high fluxes of X-rays. Here we illustrate a pilot study of the X-ray emission from a compact plasma-trap in which an off-resonance microwave-plasma interaction has been attempted, highlighting a possible Bernstein-Waves based heating mechanism. EBWs-heating is obtained via the inner plasma EM-to-ES wave conversion and enables to reach densities much larger than the cut-off ones. At LNS-INFN, an innovative diagnostic technique based on the design of a Pinhole Camera (PHC) coupled to a CCD device for X-ray Imaging of the plasma (XRI) has been developed, in order to integrate X-ray traditional diagnostics (XRS). The complementary use of electrostatic probes measurements and X-ray diagnostics enabled us to gain knowledge about the high energy electrons density and temperature and about the spatial structure of the source. The combination of the experimental data with appropriate modeling of the plasma-source allowed to estimate the X-ray emission intensity in different energy domains (ranging from EUV up to Hard X-rays). The use of ECRIS as X-ray source for multidisciplinary applications, is now a concrete perspective due to the intense fluxes produced by the new plasma heating mechanism.

  18. DETECTION OF HIGH-ENERGY GAMMA-RAY EMISSION DURING THE X-RAY FLARING ACTIVITY IN GRB 100728A

    International Nuclear Information System (INIS)

    Abdo, A. A.; Ackermann, M.; Ajello, M.; Bechtol, K.; Berenji, B.; Blandford, R. D.; Borgland, A. W.; Baldini, L.; Bellazzini, R.; Bregeon, J.; Ballet, J.; Barbiellini, G.; Baring, M. G.; Bastieri, D.; Bhat, P. N.; Bissaldi, E.; Bonamente, E.; Bonnell, J.; Bouvier, A.; Brigida, M.

    2011-01-01

    We present the simultaneous Swift and Fermi observations of the bright GRB 100728A and its afterglow. The early X-ray emission is dominated by a vigorous flaring activity continuing until 1 ks after the burst. In the same time interval, high-energy emission is significantly detected by the Fermi/Large Area Telescope. Marginal evidence of GeV emission is observed up to later times. We discuss the broadband properties of this burst within both the internal and external shock scenarios, with a particular emphasis on the relation between X-ray flares, the GeV emission, and a continued long-duration central engine activity as their power source.

  19. Elemental analysis of coal by proton-induced x-ray emission analysis

    International Nuclear Information System (INIS)

    Cronch, S.M.; Ehmann, W.D.; Laumer, H.W.; Gabbard, F.

    1976-01-01

    Proton-induced x-ray emission was used to determine elemental concentrations in solid coal samples. The coal samples were irradiated with 2.5 to 5.5 MeV protons. Concentrations were determined from characteristic x-ray yields taking into account matrix absorption. The precision is shown by replicate analysis and the accuracy by comparison with results obtained by other laboratories using different techniques

  20. Colliding Stellar Winds Structure and X-ray Emission

    Science.gov (United States)

    Pittard, J. M.; Dawson, B.

    2018-04-01

    We investigate the structure and X-ray emission from the colliding stellar winds in massive star binaries. We find that the opening angle of the contact discontinuity (CD) is overestimated by several formulae in the literature at very small values of the wind momentum ratio, η. We find also that the shocks in the primary (dominant) and secondary winds flare by ≈20° compared to the CD, and that the entire secondary wind is shocked when η ≲ 0.02. Analytical expressions for the opening angles of the shocks, and the fraction of each wind that is shocked, are provided. We find that the X-ray luminosity Lx∝η, and that the spectrum softens slightly as η decreases.

  1. High-resolution X-ray emission spectroscopy with transition-edge sensors: present performance and future potential

    Energy Technology Data Exchange (ETDEWEB)

    Uhlig, J.; Doriese, W. B.; Fowler, J. W.; Swetz, D. S.; Jaye, C.; Fischer, D. A.; Reintsema, C. D.; Bennett, D. A.; Vale, L. R.; Mandal, U.; O' Neil, G. C.; Miaja-Avila, L.; Joe, Y. I.; El Nahhas, A.; Fullagar, W.; Parnefjord Gustafsson, F.; Sundström, V.; Kurunthu, D.; Hilton, G. C.; Schmidt, D. R.; Ullom, J. N.

    2015-04-21

    X-ray emission spectroscopy (XES) is a powerful element-selective tool to analyze the oxidation states of atoms in complex compounds, determine their electronic configuration, and identify unknown compounds in challenging environments. Until now the low efficiency of wavelength-dispersive X-ray spectrometer technology has limited the use of XES, especially in combination with weaker laboratory X-ray sources. More efficient energy-dispersive detectors have either insufficient energy resolution because of the statistical limits described by Fano or too low counting rates to be of practical use. This paper updates an approach to high-resolution X-ray emission spectroscopy that uses a microcalorimeter detector array of superconducting transition-edge sensors (TESs). TES arrays are discussed and compared with conventional methods, and shown under which circumstances they are superior. It is also shown that a TES array can be integrated into a table-top time-resolved X-ray source and a soft X-ray synchrotron beamline to perform emission spectroscopy with good chemical sensitivity over a very wide range of energies.

  2. Nondestructive analysis of silver in gold foil using synchrotron radiation X-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Kasamatsu, Masaaki; Suzuki, Yasuhiro; Suzuki, Shinichi; Nakanishi, Toshio; Shimoda, Osamu; Nishiwaki, Yoshinori; Miyamoto, Naoki

    2005-01-01

    Small particles of gold foil detached from an indoor decoration might be important evidence to associate a suspect with a crime scene. We have investigated the application of elemental analysis using synchrotron radiation X-ray fluorescence spectrometry to discriminate small particles of gold foil. Eight kinds of gold foil samples collected in Japan were used in the experiments. As a result of synchrotron radiation X-ray fluorescence spectrometry, only two elements, gold and silver, were detected from all gold foil samples. The intensity ratios of AgK α /AuL α showed good correlation with the content ratios of Ag/Au. The variation of intensity ratio within a same sample was sufficiently small compared with those of different samples. Therefore the comparison of this intensity ratio can be an effective method to discriminate small particles originating from different types of gold foil. (author)

  3. Simultaneous emissions of X-rays and microwaves from long laboratory sparks and downward lightning leaders

    Science.gov (United States)

    Montanya, J.; Oscar, V. D. V.; Tapia, F. F.

    2017-12-01

    Since the discovery of the Terrestrial Gamma-ray Flashes more than 20 years ago, investigations on high energy emissions from natural lightning and high voltage laboratory sparks gained significant interest. X-ray emissions from lightning as well from high voltage laboratory sparks have in common the role played by negative leaders/streamers. On the other hand, negative leaders are well known to produce much more VHF and microwave radiation than positive leaders. Moreover, in previous works, microwave emissions from lightning leaders have been attributed to Bremsstrahlung process. The object of this work is to investigate if X-rays and RF microwave emissions share the same origin. We present simultaneous measurements of X-rays and microwaves in high voltage sparks and natural lightning. The instrumentation consists on a NaI(Tl) and LaBr3 scintillation detectors and two different receivers. One is fix tuned at 2.4 GHz with a bandwidth of 5.5 MHz. The second can be tuned at any frequency up to 18 GHz with different selectable bandwidths of 10 MHz, 40 MHz and 100 MHz. In the laboratory, results have shown that all the sparks presented microwave radiation before the breakdown of the gap, either X-rays were detected or not. In the cases where X-rays were identified, microwave emissions peaked at the same time (in the microsecond scale). We found that the power amplitudes of the microwave emissions are related to the applied voltage to the gap. In the same configuration, those cases where X-rays were detected microwave emissions presented higher power levels. The results suggest that in some part of the discharge electrons are very fast accelerated allowing, in some cases, to reach enought energy to produce X-rays. In the field, we have found similar results. On 13th of June of 2015 a bipolar cloud-to-ground flash struck 200 m close to the Eagle Nest instrumented tower (Spanish Pyrenees, 2536 m ASL). The flash presented four strokes and, in all of them, microwave

  4. Utilization of synchrotron radiation in analytical chemistry. Soft X-ray emission and absorption spectroscopy

    International Nuclear Information System (INIS)

    Muramatsu, Yasuji

    2015-01-01

    Synchrotron soft X-ray spectroscopy includes three major types of spectroscopy such as X-ray absorption spectroscopy (XAS), X-ray emission spectroscopy (XES), and X-ray photoelectron spectroscopy (XPS). This paper takes up XAS and XES of soft X-rays, and briefly describes the principle. XAS is roughly classified into XANES (X-ray absorption near-edge structure) and EXAFS (extended X-ray absorption fine structure), and XANES is mainly used in the analysis based on XAS of soft X-rays. As the examples of the latest soft X-ray analyses, the following are introduced: (1) bandgap of boron implantation diamond and the local structure of boron, (2) catalytic sites in solid fuel cell carbon electrode, and (3) soft X-ray analysis under atmospheric pressure. (A.O.)

  5. Measurement of X-ray emission efficiency for K-lines.

    Science.gov (United States)

    Procop, M

    2004-08-01

    Results for the X-ray emission efficiency (counts per C per sr) of K-lines for selected elements (C, Al, Si, Ti, Cu, Ge) and for the first time also for compounds and alloys (SiC, GaP, AlCu, TiAlC) are presented. An energy dispersive X-ray spectrometer (EDS) of known detection efficiency (counts per photon) has been used to record the spectra at a takeoff angle of 25 degrees determined by the geometry of the secondary electron microscope's specimen chamber. Overall uncertainty in measurement could be reduced to 5 to 10% in dependence on the line intensity and energy. Measured emission efficiencies have been compared with calculated efficiencies based on models applied in standardless analysis. The widespread XPP and PROZA models give somewhat too low emission efficiencies. The best agreement between measured and calculated efficiencies could be achieved by replacing in the modular PROZA96 model the original expression for the ionization cross section by the formula given by Casnati et al. (1982) A discrepancy remains for carbon, probably due to the high overvoltage ratio.

  6. X-ray astronomy

    International Nuclear Information System (INIS)

    Giacconi, R.; Gursky, H.

    1974-01-01

    This text contains ten chapters and three appendices. Following an introduction, chapters two through five deal with observational techniques, mechanisms for the production of x rays in a cosmic setting, the x-ray sky and solar x-ray emission. Chapters six through ten include compact x-ray sources, supernova remnants, the interstellar medium, extragalactic x-ray sources and the cosmic x-ray background. Interactions of x rays with matter, units and conversion factors and a catalog of x-ray sources comprise the three appendices. (U.S.)

  7. Application of particle-induced X-ray emission, backscattering spectrometry and scanning electron microscopy in the evaluation of orthodontic materials

    International Nuclear Information System (INIS)

    Gihwala, D.; Mars, J.A.; Pineda-Vargas, C.

    2013-01-01

    The focus of this investigation was on orthodontic materials used in the manufacture of dental brackets. The properties of these dental materials are subjected to various physical parameters such as elongation, yield strength and elasticity that justify their application. In turn, these parameters depend on the quantitative elemental concentration distribution (QECD) in the materials used in the manufacture. For compositional analysis, proton-induced X-ray emission (PIXE), backscatter spectrometry (BS) and scanning electron microscopy (SEM) were applied. QECD analysis was performed to correlate the physical parameters with the composition and to quantify imperfections in the materials. PIXE and BS analyses were performed simultaneously with a 3 MeV proton beam while electrons accelerated at 25 keV were used for the SEM analysis. From the QECDs it was observed that: (1) the major elements Cr, Fe and Ni were homogeneously distributed in the orthodontic plate; (2) the distribution of Mo and O correlated with one another; (3) there was a spread of Cr around regions of high C concentration; and, (4) areas of high concentrations of Mo and O corresponded to a decrease in C concentrations. Elemental concentration correlations are shown to indicate the similarities and differences in the ease of formation of phases, based on the tangent of linearity. (author)

  8. X-RAY AND RADIO EMISSION FROM TYPE IIn SUPERNOVA SN 2010jl

    Energy Technology Data Exchange (ETDEWEB)

    Chandra, Poonam [National Centre for Radio Astrophysics, Tata Institute of Fundamental Research, Pune University Campus, Pune 411 007 (India); Chevalier, Roger A. [Department of Astronomy, University of Virginia, P.O. Box 400325, Charlottesville, VA 22904-4325 (United States); Chugai, Nikolai [Institute of Astronomy of Russian Academy of Sciences, Pyatnitskaya St. 48, 109017 Moscow (Russian Federation); Fransson, Claes [Oskar Klein Centre, Department of Astronomy, Stockholm University, AlbaNova, SE-106 91 Stockholm (Sweden); Soderberg, Alicia M., E-mail: poonam@ncra.tifr.res.in [Smithsonian Astrophysical Observatory, 60 Garden St., MS-20, Cambridge, MA 02138 (United States)

    2015-09-01

    We present all X-ray and radio observations of the Type IIn supernova SN 2010jl. The X-ray observations cover a period up to day 1500 with Chandra, XMM-Newton, NuSTAR, and Swift-X-ray Telescope (XRT). The Chandra observations after 2012 June, the XMM-Newton observation in 2013 November, and most of the Swift-XRT observations until 2014 December are presented for the first time. All the spectra can be fitted by an absorbed hot thermal model except for Chandra spectra on 2011 October and 2012 June when an additional component is needed. Although the origin of this component is uncertain, it is spatially coincident with the supernova and occurs when there are changes to the supernova spectrum in the energy range close to that of the extra component, indicating that the emission is related to the supernova. The X-ray light curve shows an initial plateau followed by a steep drop starting at day ∼300. We attribute the drop to a decrease in the circumstellar density. The column density to the X-ray emission drops rapidly with time, showing that the absorption is in the vicinity of the supernova. We also present Very Large Array radio observations of SN 2010jl. Radio emission was detected from SN 2010jl from day 570 onwards. The radio light curves and spectra suggest that the radio luminosity was close to its maximum at the first detection. The velocity of the shocked ejecta derived assuming synchrotron self-absorption is much less than that estimated from the optical and X-ray observations, suggesting that free–free absorption dominates.

  9. Globular clusters as a source of X-ray emission from the neighbourhood of M87

    International Nuclear Information System (INIS)

    Fabian, A.C.; Pringle, J.E.; Rees, M.J.

    1976-01-01

    It is stated that the X-ray emission from globular clusters may be attributable to accretion on to compact objects, the accreting material being supplied from binary companions, or gas trapped in the potential well of the cluster. Counts of objects in the vicinity of the M87 have revealed that it has an extensive halo of globular clusters, the number of which may exceed 10,000 within a radius of 23 arc min. Most of these clusters may be explicable as a population effect, and the similarity of their optical properties to those of cluster in our own Galaxy suggests that they may also contain X-ray sources. The brighter globular clusters in M87 may, however, be substantially more X-ray luminous, and there may be proportionally more gas available in globular clusters in M87 compared with our Galaxy. The average X-ray luminosity of individual globular clusters may be of the order of 10 38 erg/sec., which raises the possibility that the integrated globular cluster emission may account for a substantial fraction of the X-ray emission observed from the region of M87. In support of this it is noted that the extended X-ray emission from the Virgo cluster is centered on M87, which lies approximately 45 arc min from the cluster centroid, and it is expected that the general X-ray emission from the globular cluster will appear to be smoothly and symmetrically distributed about M87 at moderate spatial resolution. A similar situation may apply to the elliptical galaxy NGC 3311 in Abell 1060 which, as a cluster, has been suggested as the identification for the X-ray source 3 U 1044-40, and it seems possible that that galaxy is surrounded by a similar globular cluster population to that of M87. (U.K.)

  10. X-Ray Emission from a Merger Remnant, NGC 7252 (the ``Atoms-for-Peace'' Galaxy)

    Science.gov (United States)

    Awaki, Hisamitsu; Matsumoto, Hironori; Tomida, Hiroshi

    2002-03-01

    We observed a nearby merger remnant NGC 7252 with the X-ray satellite ASCA and detected X-ray emission with the X-ray flux of (1.8+/-0.3)×10-13 ergs s-1 cm-2 in the 0.5-10 keV band. This corresponds to the X-ray luminosity of 8.1×1040 ergs s-1. The X-ray emission is well described with a two-component model: a soft component with kT=0.72+/-0.13 keV and a hard component with kT>5.1 keV. Although NGC 7252 is referred to as a dynamically young protoelliptical, the 0.5-4 keV luminosity of the soft component is about 2×1040 ergs s-1, which is low for an early-type galaxy. The ratio of LX/LFIR suggests that the soft component originated from the hot gas due to star formation. Its low luminosity can be explained by the gas ejection from the galaxy as galaxy winds. Our observation reveals the existence of hard X-ray emission with the 2-10 keV luminosity of 5.6×1040 ergs s-1. This may indicate the existence of nuclear activity or an intermediate-mass black hole in NGC 7252.

  11. Polarized Gamma-Ray Emission from the Galactic Black Hole Cygnus X-1

    Science.gov (United States)

    Laurent, P.; Rodriquez, J.; Wilms, J.; Bel, M. Cadolle; Pottschmidt, K.; Grinberg, V.

    2011-01-01

    Because of their inherently high flux allowing the detection of clear signals, black hole X-ray binaries are interesting candidates for polarization studies, even if no polarization signals have been observed from them before. Such measurements would provide further detailed insight into these sources' emission mechanisms. We measured the polarization of the gamma-ray emission from the black hole binary system Cygnus X-I with the INTEGRAL/IBIS telescope. Spectral modeling ofthe data reveals two emission mechanisms: The 250-400 keY data are consistent with emission dominated by Compton scattering on thermal electrons and are weakly polarized. The second spectral component seen in the 400keV-2MeV band is by contrast strongly polarized, revealing that the MeV emission is probably related to the jet first detected in the radio band.

  12. Characterizing the X-ray Emission in Small Magellanic Cloud Supernova Remnants

    Science.gov (United States)

    Man, Nicole; Auchettl, Katie; Lopez, Laura

    2018-01-01

    The Small Magellanic Cloud is a close, metal-poor galaxy with active star formation, and it has a diverse population of 24 supernova remnants (SNRs) that have been identified at several wavelengths. Past work has characterized the X-ray emission in these sources separately and aimed to constrain their explosive origins from observations with Chandra and XMM-Newton. Three SNRs have possible evidence for Type Ia explosions based on strong Fe-L emission in their X-ray spectra, although the environments and intermediate-mass element abundances are more consistent with those of core-collapse SNe. In this poster, we analyze the archival Chandra and XMM-Newton observations of the SMC SNR sample, and we model the sources' X-ray spectra in a systematic way to derive the plasma properties and to constrain the nature of the explosions. In one SNR, we note the presence of an X-ray binary near the source's geometric center, suggesting the compact object was produced in the SN explosion. As one of only three SNRs known in the Local Group to host a binary system, this source is worthy of follow-up investigations to probe explosions of massive stars in binary systems.

  13. Weak Hard X-Ray Emission from Broad Absorption Line Quasars: Evidence for Intrinsic X-Ray Weakness

    DEFF Research Database (Denmark)

    Luo, B.; Brandt, W. N.; Alexander, D. M.

    2014-01-01

    We report NuSTAR observations of a sample of six X-ray weak broad absorption line (BAL) quasars. These targets, at z = 0.148-1.223, are among the optically brightest and most luminous BAL quasars known at z 330 times weaker than...... expected for typical quasars. Our results from a pilot NuSTAR study of two low-redshift BAL quasars, a Chandra stacking analysis of a sample of high-redshift BAL quasars, and a NuSTAR spectral analysis of the local BAL quasar Mrk 231 have already suggested the existence of intrinsically X-ray weak BAL...... quasars, i.e., quasars not emitting X-rays at the level expected from their optical/UV emission. The aim of the current program is to extend the search for such extraordinary objects. Three of the six new targets are weakly detected by NuSTAR with ≲ 45 counts in the 3-24 keV band, and the other three...

  14. X-RAY AND MULTIWAVELENGTH INSIGHTS INTO THE NATURE OF WEAK EMISSION-LINE QUASARS AT LOW REDSHIFT

    Energy Technology Data Exchange (ETDEWEB)

    Wu Jianfeng; Brandt, W. N.; Schneider, Donald P. [Department of Astronomy and Astrophysics, Pennsylvania State University, 525 Davey Lab, University Park, PA 16802 (United States); Anderson, Scott F. [Department of Astronomy, University of Washington, Box 351580, Seattle, WA 98195 (United States); Diamond-Stanic, Aleksandar M. [Center for Astrophysics and Space Sciences, University of California, San Diego, La Jolla, CA 92903 (United States); Hall, Patrick B. [Department of Physics and Astronomy, York University, 4700 Keele Street, Toronto, ON M3J 1P3 (Canada); Plotkin, Richard M. [Astronomical Institute ' Anton Pannekoek' , University of Amsterdam, Science Park 904, 1098 XH Amsterdam (Netherlands); Shemmer, Ohad, E-mail: jfwu@astro.psu.edu [Department of Physics, University of North Texas, Denton, TX 76203 (United States)

    2012-03-01

    We report on the X-ray and multiwavelength properties of 11 radio-quiet quasars with weak or no emission lines identified by the Sloan Digital Sky Survey (SDSS) with redshift z = 0.4-2.5. Our sample was selected from the Plotkin et al. catalog of radio-quiet, weak-featured active galactic nuclei (AGNs). The distribution of relative X-ray brightness for our low-redshift weak-line quasar (WLQ) candidates is significantly different from that of typical radio-quiet quasars, having an excess of X-ray weak sources, but it is consistent with that of high-redshift WLQs. Over half of the low-redshift WLQ candidates are X-ray weak by a factor of {approx}> 5, compared to a typical SDSS quasar with similar UV/optical luminosity. These X-ray weak sources generally show similar UV emission-line properties to those of the X-ray weak quasar PHL 1811 (weak and blueshifted high-ionization lines, weak semiforbidden lines, and strong UV Fe emission); they may belong to the notable class of PHL 1811 analogs. The average X-ray spectrum of these sources is somewhat harder than that of typical radio-quiet quasars. Several other low-redshift WLQ candidates have normal ratios of X-ray-to-optical/UV flux, and their average X-ray spectral properties are also similar to those of typical radio-quiet quasars. The X-ray weak and X-ray normal WLQ candidates may belong to the same subset of quasars having high-ionization 'shielding gas' covering most of the wind-dominated broad emission-line region, but be viewed at different inclinations. The mid-infrared-to-X-ray spectral energy distributions (SEDs) of these sources are generally consistent with those of typical SDSS quasars, showing that they are not likely to be BL Lac objects with relativistically boosted continua and diluted emission lines. The mid-infrared-to-UV SEDs of most radio-quiet weak-featured AGNs without sensitive X-ray coverage (34 objects) are also consistent with those of typical SDSS quasars. However, one source in our

  15. X-RAY AND MULTIWAVELENGTH INSIGHTS INTO THE NATURE OF WEAK EMISSION-LINE QUASARS AT LOW REDSHIFT

    International Nuclear Information System (INIS)

    Wu Jianfeng; Brandt, W. N.; Schneider, Donald P.; Anderson, Scott F.; Diamond-Stanic, Aleksandar M.; Hall, Patrick B.; Plotkin, Richard M.; Shemmer, Ohad

    2012-01-01

    We report on the X-ray and multiwavelength properties of 11 radio-quiet quasars with weak or no emission lines identified by the Sloan Digital Sky Survey (SDSS) with redshift z = 0.4-2.5. Our sample was selected from the Plotkin et al. catalog of radio-quiet, weak-featured active galactic nuclei (AGNs). The distribution of relative X-ray brightness for our low-redshift weak-line quasar (WLQ) candidates is significantly different from that of typical radio-quiet quasars, having an excess of X-ray weak sources, but it is consistent with that of high-redshift WLQs. Over half of the low-redshift WLQ candidates are X-ray weak by a factor of ∼> 5, compared to a typical SDSS quasar with similar UV/optical luminosity. These X-ray weak sources generally show similar UV emission-line properties to those of the X-ray weak quasar PHL 1811 (weak and blueshifted high-ionization lines, weak semiforbidden lines, and strong UV Fe emission); they may belong to the notable class of PHL 1811 analogs. The average X-ray spectrum of these sources is somewhat harder than that of typical radio-quiet quasars. Several other low-redshift WLQ candidates have normal ratios of X-ray-to-optical/UV flux, and their average X-ray spectral properties are also similar to those of typical radio-quiet quasars. The X-ray weak and X-ray normal WLQ candidates may belong to the same subset of quasars having high-ionization 'shielding gas' covering most of the wind-dominated broad emission-line region, but be viewed at different inclinations. The mid-infrared-to-X-ray spectral energy distributions (SEDs) of these sources are generally consistent with those of typical SDSS quasars, showing that they are not likely to be BL Lac objects with relativistically boosted continua and diluted emission lines. The mid-infrared-to-UV SEDs of most radio-quiet weak-featured AGNs without sensitive X-ray coverage (34 objects) are also consistent with those of typical SDSS quasars. However, one source in our X-ray

  16. X-ray continuum and iron K emission line from the radio galaxy 3C 390.3

    Science.gov (United States)

    Inda, M.; Makishima, K.; Kohmura, Y.; Tashiro, M.; Ohashi, T.; Barr, P.; Hayashida, K.; Palumbo, G. G. C.; Trinchieri, G.; Elvis, M.

    1994-01-01

    X-ray properties of the radio galaxy 3C 390.3 were investigated using the European X-ray Observatory Satellite (EXOSAT) and Ginga satellites. Long-term, large-amplitude X-ray intensity changes were detected over a period extending from 1984 through 1991, and high-quality X-ray spectra were obtained especially with Ginga. The X-ray continuum spectra were described with power-law model with photon slope in the range 1.5-1.8, and the slope flattened as the 2-20 keV luminosity decreased by 40%. There was a first detection of the iron emission line from this source at the 90% confidence level. An upper limit was derived on the thermal X-ray component. X-ray emission mechanisms and possible origins of the long-term variation are discussed.

  17. X-ray emission in slow highly charged ion-surface collisions

    International Nuclear Information System (INIS)

    Watanabe, H; Abe, T; Fujita, Y; Sun, J; Takahashi, S; Tona, M; Yoshiyasu, N; Nakamura, N; Sakurai, M; Yamada, C; Ohtani, S

    2007-01-01

    X-rays emitted in the collisions of highly charged ions with a surface have been measured to investigate dissipation schemes of their potential energies. While 8.1% of the potential energy was dissipated in the collisions of He-like I ions with a W surface, 29.1% has been dissipated in the case of He-like Bi ions. The x-ray emissions play significant roles in the dissipation of the potential energies in the interaction of highly charged heavy ions with the surface

  18. Experimental study of X-ray emission in laser-cluster interaction; Etude experimentale de l'emission X issue de l'interaction laser-agregats

    Energy Technology Data Exchange (ETDEWEB)

    Caillaud, T

    2004-09-01

    Rare gas cluster jets are an intermediate medium between solid and gas targets. Laser-cluster jets interaction may generate a great number of energetic particles as X-rays, UV, high harmonics, ions, electrons and neutrons. To understand all the mechanisms involved in such an interaction we need to make a complete study of individual cluster response to an ultra-short laser pulse. We studied the laser interaction with our argon cluster gas jet, which is well characterized in cluster size and density, to enlarge the knowledge of this interaction. We measured absorption, heating and X-ray emission spectra versus laser parameters and clusters size ({approx} 15-30 nm). We show that there is a strong refraction effect on laser propagation due to the residual gas density. This effect was confirmed by laser propagation simulation with a cylindrical 2-dimensional particle code WAKE. The role played by refraction was to limit maximum laser intensity on the focal spot and to increase interaction volume. By this way, X-ray emission was observed with laser intensity not so far from the ionization threshold (few 10{sup 14} W.cm{sup -2}). We also studied plasma expansion both at cluster scale and focal volume scale and deduced the deposited energy distribution as a function of time. Thanks to a simple hydrodynamic model, we used these results to study cluster expansion. X-ray emission is then simulated by TRANSPEC code in order to reproduce X-ray spectra and duration. Those results revealed an extremely brief X-ray emission consistent with a preliminary measure by streak camera (on ps scale). (author)

  19. X-ray emission from a high-atomic-number z-pinch plasma created from compact wire arrays

    International Nuclear Information System (INIS)

    Sanford, T.W.L.; Mosher, D.; De Groot, J.S.

    1996-01-01

    Thermal and nonthermal x-ray emission from the implosion of compact tungsten wire arrays in 5-MA Saturn discharges is reported. The timing of multiple implosions and the thermal x-ray spectra (1 to 10 keV) agree with 2D radiation-hydrocode simulations. Nonthermal x-ray emission (10 to 100 keV) correlates with pinch spots distributed along the z-axis. The similarities of the measured nonthermal spectrum, yield, and pinch-spot emission with those of 0.8-MA, single-exploded-wire discharges on Gamble-II suggest a common nonthermal-production mechanism. Nonthermal x-ray yields are lower than expected from current scaling of Gamble II results, suggesting that implosion geometries are not as efficient as single-wire geometries for nonthermal x-ray production. The instabilities, azimuthal asymmetries, and inferred multiple implosions that accompany the implosion geometry lead to larger, more irregular pinch spots, a likely reason for reduced nonthermal efficiency. A model for nonthermal-electron acceleration across magnetic fields in highly-collisional, high-atomic-number plasmas combined with 1D hydrocode simulations of Saturn compact loads predicts weak nonthermal x-ray emission. (author). 3 figs., 10 refs

  20. X-ray emission from a high-atomic-number z-pinch plasma created from compact wire arrays

    International Nuclear Information System (INIS)

    Sanford, T.W.L.; Mosher, D.; De Groot, J.S.

    1996-01-01

    Thermal and nonthermal x-ray emission from the implosion of compact tungsten wire arrays in 5-MA Saturn discharges is reported. The timing of multiple implosions and the thermal x-ray spectra (1 to 10 keV) agree with 2D radiation-hydrocode simulations. Nonthermal x-ray emission (10 to 100 keV) correlates with pinch spots distributed along the z-axis. The similarities of the measured nonthermal spectrum, yield, and pinch-spot emission with those of 0.8-MA, single- exploded-wire discharges on Gamble-II suggest a common nonthermal- production mechanism. Nonthermal x-ray yields are lower than expected from current scaling of Gamble II results, suggesting that implosion geometries are not as efficient as single-wire geometries for nonthermal x-ray production. The instabilities, azimuthal asymmetries, and inferred multiple implosions that accompany the implosion geometry lead to larger, more irregular pinch spots, a likely reason for reduced nonthermal efficiency. A model for nonthermal-electron acceleration across magnetic fields in highly- collisional, high-atomic-number plasmas combined with 1D hydrocode simulations of Saturn compact loads predicts weak nonthermal x-ray emission

  1. Thin coating thickness determination using radioisotope-excited x-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Del Castillo, Lorena A.; Calix, Virginia S.

    2001-01-01

    Three different approaches on thin coating thickness determination using a radioisotope-excited x-ray fluorescence spectrometry were demonstrated and results were compared. A standard of thin layer of gold (Au) on a nickel (Ni) substrate from the US National Bureau of Standards (with a nominal thickness of 0.300505 microns of at least 99.9% Au electrodeposited over 2 nils of Ni) on low carbon steel (1010) was analyzed using a Cd 109-excited XRF system. Au thickness computations were done using the (a) thin standard approach, (b) thick standard approach, and (c) x-ray absorption method (ASTM A754-79 1982). These three methods yielded results within the limit set by the American Society for Testing Materials (ASTM), which is +/-3%. Of the three methods, the thick standard yielded the best result with 0.124% error. (Author)

  2. Resonant x-ray emission from gas-phase TiCl{sub 4}

    Energy Technology Data Exchange (ETDEWEB)

    Hague, C.F.; Tronc, M. [Universite Pierre et Marie Curie, Paris (France); De Groot, F. [Univ. of Groningen (Netherlands)] [and others

    1997-04-01

    Resonant x-ray emission spectroscopy (RXES) has proved to be a powerful tool for studying the electronic structure of condensed matter. Over the past few years it has been used mainly for studying the valence bands of solids and condensed molecules. Very recently the advent of high brightness photon beams provided by third generation synchrotron radiation source undulators, associated with efficient x-ray emission spectrometers has made it possible to perform experiments on free diatomic molecular systems. RXE spectra of free molecules are of prime importance to gain insight into their electronic structure and bonding as they reflect the symmetry of orbitals engaged in the two-electron, two-step process with the l = 0, {+-}2 parity-conserving selection rule, and are free from solid state effects which can introduce difficulties in the interpretation. They provide information (more so than XAS) on the core excited states, and, when performed at fixed incident photon energy as a function of the emitted photon energy, on the electronic excitation (charge transfer, multiplet states). Moreover the anisotropy of the angular distribution of resonant x-ray emission affects the relative intensity of the emission peaks and provides information concerning the symmetries of final states. This is a preliminary report on what are the first RXE spectra of a 3d transition metal complex in the gas phase. The experiment concerns the Ti 3d {yields}2p emission spectrum of TiCl{sub 4} over the 450 to 470 eV region.

  3. Analysis of selected elements in tobacco by wavelength dispersive X-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Martin, J.M.

    1988-01-01

    A rapid method for the determination of 16 elements in tobacco by wavelength dispersive X-ray fluorescence spectrometry has been developed. The method is accurate and precise, and requires only 9 min per sample for quantitation. Sample preparation consists of placing a portion of dried, ground tobacco in a sample cup, and pressing at 25 tons pressure to make a compressed pellet. This pellet is then automatically analyzed by X-ray fluorescence for 16 elements. The results are stored on a computer disk for future recall and report generation. The elements are: Al, Br, Ca, Cl, Cu, Fe, K, Mg, Mn, Na, P, S, Si, Sr, Ti and Zn

  4. X-ray emission, ablation pressure, and preheating for foils irradiated at 0. 26. mu. m wavelength

    Energy Technology Data Exchange (ETDEWEB)

    Pepin, H.; Fabbro, R.; Faral, B.; Amiranoff, F.; Virmont, J.; Cottet, F.; Romain, J.P.

    1985-11-01

    The x-ray emission, ablation pressure, and preheating for foils irradiated with a 0.26 ..mu..m laser at intensities approx.10/sup 15/ W cm/sup -2/ are studied. The foils are Al with various thicknesses, coated or uncoated with CH or Au. The x-ray emission and conversion efficiency are obtained with a multichannel x-ray diode spectrometer, the ablation pressures are deduced from shock transit times, and the rear temperatures are inferred from x-ray pyrometry. For thin foils (<<12 ..mu..m), the rear temperatures can be predicted reasonably well with the use of the front x-ray spectra. For thick foils shock preheating is dominant.

  5. X-ray emission, ablation pressure, and preheating for foils irradiated at 0.26 μm wavelength

    International Nuclear Information System (INIS)

    Pepin, H.; Fabbro, R.; Faral, B.; Amiranoff, F.; Virmont, J.; Cottet, F.; Romain, J.P.

    1985-01-01

    The x-ray emission, ablation pressure, and preheating for foils irradiated with a 0.26 μm laser at intensities approx.10 15 W cm -2 are studied. The foils are Al with various thicknesses, coated or uncoated with CH or Au. The x-ray emission and conversion efficiency are obtained with a multichannel x-ray diode spectrometer, the ablation pressures are deduced from shock transit times, and the rear temperatures are inferred from x-ray pyrometry. For thin foils (<<12 μm), the rear temperatures can be predicted reasonably well with the use of the front x-ray spectra. For thick foils shock preheating is dominant

  6. Radio emission from the X-ray pulsar Her X-1: a jet launched by a strong magnetic field neutron star?

    Science.gov (United States)

    van den Eijnden, J.; Degenaar, N.; Russell, T. D.; Miller-Jones, J. C. A.; Wijnands, R.; Miller, J. M.; King, A. L.; Rupen, M. P.

    2018-01-01

    Her X-1 is an accreting neutron star (NS) in an intermediate-mass X-ray binary. Like low-mass X-ray binaries (LMXBs), it accretes via Roche lobe overflow, but similar to many high-mass X-ray binaries containing a NS; Her X-1 has a strong magnetic field and slow spin. Here, we present the discovery of radio emission from Her X-1 with the Very Large Array. During the radio observation, the central X-ray source was partially obscured by a warped disc. We measure a radio flux density of 38.7 ± 4.8 μJy at 9 GHz but cannot constrain the spectral shape. We discuss possible origins of the radio emission, and conclude that coherent emission, a stellar wind, shocks and a propeller outflow are all unlikely explanations. A jet, as seen in LMXBs, is consistent with the observed radio properties. We consider the implications of the presence of a jet in Her X-1 on jet formation mechanisms and on the launching of jets by NSs with strong magnetic fields.

  7. X-ray emission from hot subdwarfs with compact companions

    Directory of Open Access Journals (Sweden)

    Esposito P.

    2013-03-01

    Full Text Available We review the X-ray observations of hot subdwarf stars. While no X-ray emission has been detected yet from binaries containing B-type subdwarfs, interesting results have been obtained in the case of the two luminous O-type subdwarfs HD 49798 and BD + 37° 442. Both of them are members of binary systems in which the X-ray luminosity is powered by accretion onto a compact object: a rapidly spinning (13.2 s and massive (1.28  M⊙ white dwarf in the case of HD 49798 and most likely a neutron star, spinning at 19.2 s, in the case of BD + 37° 442. Their study can shed light on the poorly known processes taking place during common envelope evolutionary phases and on the properties of wind mass loss from hot subdwarfs.

  8. An optimised set-up for total reflection particle induced X-ray emission

    International Nuclear Information System (INIS)

    Kan, J.A. van; Vis, R.D.

    1997-01-01

    MeV proton beams at small angles of incidence (0-35 mrad) are used to analyse trace elements on flat surfaces such as Si wafers or quartz substrates. In these experiments, the particle induced X-ray emission (PIXE) signal is used in a new optimized set-up. This set-up is constructed in such a way that the X-ray detector can reach very large solid angles, larger than 1 sr. Use of these large detector solid angles, combined with the reduction of bremsstrahlung background, affords limits of detection (LOD) of the order of 10 10 at cm -2 using total reflection particle induced X-ray emission (TPIXE). The LODs from earlier TPIXE measurements in a non-optimized set-up are used to estimate LODs in the new TPIXE set-up. Si wafers with low surface concentrations of V, Ni, Cu and Ag are used as standards to calibrate the LODs found with this set-up. The metal concentrations are determined by total reflection X-ray fluorescence (TXRF). The TPIXE measurements are compared with TXRF measurements on the same wafers. (Author)

  9. C IV EMISSION AND THE ULTRAVIOLET THROUGH X-RAY SPECTRAL ENERGY DISTRIBUTION OF RADIO-QUIET QUASARS

    International Nuclear Information System (INIS)

    Kruczek, Nicholas E.; Richards, Gordon T.; Deo, Rajesh P.; Krawczyk, Coleman M.; Gallagher, S. C.; Hall, Patrick B.; Hewett, Paul C.; Leighly, Karen M.; Proga, Daniel

    2011-01-01

    In the rest-frame ultraviolet (UV), two of the parameters that best characterize the range of emission-line properties in quasar broad emission-line regions are the equivalent width and the blueshift of the C IV λ1549 line relative to the quasar rest frame. We explore the connection between these emission-line properties and the UV through X-ray spectral energy distribution (SED) for radio-quiet (RQ) quasars. Our sample consists of a heterogeneous compilation of 406 quasars from the Sloan Digital Sky Survey (at z > 1.54) and Palomar-Green survey (at z < 0.4) that have well-measured C IV emission-line and X-ray properties (including 164 objects with measured Γ). We find that RQ quasars with both strong C IV emission and small C IV blueshifts can be classified as 'hard-spectrum' sources that are (relatively) strong in the X-ray as compared to the UV. On the other hand, RQ quasars with both weak C IV emission and large C IV blueshifts are instead 'soft-spectrum' sources that are (relatively) weak in the X-ray as compared to the UV. This work helps to further bridge optical/soft X-ray 'eigenvector 1' relationships to the UV and hard X-ray. Based on these findings, we argue that future work should consider systematic errors in bolometric corrections (and thus accretion rates) that are derived from a single mean SED. Detailed analysis of the C IV emission line may allow for SED-dependent corrections to these quantities.

  10. Electron emission regulator for an x-ray tube filament

    International Nuclear Information System (INIS)

    Daniels, H.E.; Randall, H.G.

    1982-01-01

    An x-ray tube ma regulator has an scr phase shift voltage regulator supplying the primary winding of a transformer whose secondary is coupled to the x-ray tube filament. Prior to initiation of an x-ray exposure, the filament is preheated to a temperature corresponding substantially to the electron emissivity needed for obtaining the desired tube ma during an exposure. During the preexposure interval, the phase shift regulator is controlled by a signal corresponding to the sum of signals representative of the voltage applied to the filament transformer, the desired filament voltage and the space charge compensation needed for the selected x-ray tube anode to cathode voltage. When an exposure is initiated, control of the voltage regulator is switched to a circuit that responds to the tube current by controlling the amount of phase shift and, hence, the voltage supplied to the transformer. Transformer leakage current compensation is provided during the exposure interval with a circuit that includes an element whose impedance is varied in accordance with the anode-to-cathode voltage setting so the element drains off tube current as required to cancel the effect of leakage current variations

  11. Analysis of metal-laden water via portable X-ray fluorescence spectrometry

    Science.gov (United States)

    Pearson, Delaina; Weindorf, David C.; Chakraborty, Somsubhra; Li, Bin; Koch, Jaco; Van Deventer, Piet; de Wet, Jandre; Kusi, Nana Yaw

    2018-06-01

    A rapid method for in-situ elemental composition analysis of metal-laden water would be indispensable for studying polluted water. Current analytical lab methods to determine water quality include flame atomic absorption spectrometry (FAAS), atomic absorption spectrophotometry (AAS), electrothermal atomic absorption spectrometry (EAAS), and inductively coupled plasma (ICP) spectroscopy. However only two field methods, colorimetry and absorptiometry, exist for elemental analysis of water. Portable X-ray fluorescence (PXRF) spectrometry is an effective method for elemental analysis of soil, sediment, and other matrices. However, the accuracy of PXRF is known to be affected while scanning moisture-laden soil samples. This study sought to statistically establish PXRF's predictive ability for various elements in water at different concentrations relative to inductively coupled plasma atomic emission spectroscopy (ICP-AES). A total of 390 metal-laden water samples collected from leaching columns of mine tailings in South Africa were analyzed via PXRF and ICP-AES. The PXRF showed differential effectiveness in elemental quantification. For the collected water samples, the best relationships between ICP and PXRF elemental data were obtained for K and Cu (R2 = 0.92). However, when scanning ICP calibration solutions with elements in isolation, PXRF results indicated near perfect agreement; Ca, K, Fe, Cu and Pb produced an R2 of 0.99 while Zn and Mn produced an R2 of 1.00. The utilization of multiple PXRF (stacked) beams produced stronger correlation to ICP relative to the use of a single beam in isolation. The results of this study demonstrated the PXRF's ability to satisfactorily predict the composition of metal-laden water as reported by ICP for several elements. Additionally this study indicated the need for a "Water Mode" calibration for the PXRF and demonstrates the potential of PXRF for future study of polluted or contaminated waters.

  12. Anatomy of the AGN in NGC 5548. IX. Photoionized emission features in the soft X-ray spectra

    Science.gov (United States)

    Mao, Junjie; Kaastra, J. S.; Mehdipour, M.; Gu, Liyi; Costantini, E.; Kriss, G. A.; Bianchi, S.; Branduardi-Raymont, G.; Behar, E.; Di Gesu, L.; Ponti, G.; Petrucci, P.-O.; Ebrero, J.

    2018-04-01

    The X-ray narrow emission line region (NELR) of the archetypal Seyfert 1 galaxy NGC 5548 has been interpreted as a single-phase photoionized plasma that is absorbed by some of the warm absorber components. This scenario requires those overlaying warm absorber components to have larger distance (to the central engine) than the X-ray NELR, which is not fully consistent with the distance estimates found in the literature. Therefore, we reanalyze the high-resolution spectra obtained in 2013-2014 with the Reflection Grating Spectrometer (RGS) aboard XMM-Newton to provide an alternative interpretation of the X-ray narrow emission features. We find that the X-ray narrow emission features in NGC 5548 can be described by a two-phase photoionized plasma with different ionization parameters (logξ = 1.3 and 0.1) and kinematics (vout = -50 and -400 km s-1), and no further absorption by the warm absorber components. The X-ray and optical NELR might be the same multi-phase photoionized plasma. Both X-ray and optical NELR have comparable distances, asymmetric line profiles, and the underlying photoionized plasma is turbulent and compact in size. The X-ray NELR is not the counterpart of the UV/X-ray absorber outside the line of sight because their distances and kinematics are not consistent. In addition, X-ray broad emission features that we find in the spectrum can be accounted for by a third photoionized emission component. The RGS spectrum obtained in 2016 is analyzed as well, where the luminosity of most prominent emission lines (the O VII forbidden line and O VIII Lyα line) are the same (at a 1σ confidence level) as in 2013-2014.

  13. X-ray Spectrometry: Basic principles

    International Nuclear Information System (INIS)

    Carvalho, R.M.; Teixeira, G.J.; Cardoso, R.S.; Peixoto, J.G.P.

    2017-01-01

    The application of X rays requires a study of its spectrum. Intrinsic difficulties of the own method and of all the instrumentation necessary for the accomplishment of this practice were related. The objective was to demonstrate the use of a commercial spectrometer using at room temperature and compare it with spectra theoretically obtained by simulation. As an initial result was that both instrumentation is compatible to be used in an X-ray beam, with and without scattering material and its theoretical data were obtained. (author)

  14. Rare earth aerosol analysis by x-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Citron, I.M.; Mausner, L.F.

    1982-01-01

    An analytical method for the determination of four lanthanides in air filter samples is described. The method involves simultaneous quantitative determinations of La, Ce, Pr, and Nd at the microgram level by x-ray fluorescence spectrometry without chemical separation of these rare earths and without serious interferences from the dust matrices on the filters. The method has been used successfully to analyze some air filter samples collected at a rare earth processing refinery in Illinois. A description of the development of the method is given as well as the results obtained by using this method on the air filter samples. The reproducibility of the results was generally +-5%

  15. Single-Shot Spectrometry for X-Ray Free-Electron Lasers

    International Nuclear Information System (INIS)

    Yabashi, Makina; Ishikawa, Tetsuya; Hastings, Jerome B.; Zolotorev, Max S.; Mimura, Hidekazu; Yumoto, Hirokatsu; Matsuyama, Satoshi; Yamauchi, Kazuto

    2006-01-01

    An experimental scheme to realize single-shot spectrometry for the diagnostics of x-ray free-electron lasers (XFELs) is presented. The combination of an ultraprecisely figured mirror and a perfect crystal form a simple, high-precision spectrometer that can cover an energy range from a few eV to a hundred eV with high resolution. The application of the spectrometer to determine XFEL pulse widths was investigated theoretically and experimentally. It has been shown that the present system can determine pulse widths from sub-fs to ps in a single shot even for spontaneous radiation. The system can be easily extended to even shorter pulses

  16. X-ray Emission Spectrum of Liquid Ethanol: Origin of Split Peaks.

    Science.gov (United States)

    Takahashi, Osamu; Ljungberg, Mathias P; Pettersson, Lars G M

    2017-12-14

    The X-ray emission spectrum of liquid ethanol was calculated using density functional theory and a semiclassical approximation to the Kramers-Heisenberg formula including core-hole-induced dynamics. Our spectrum agrees well with the experimental spectrum. We found that the intensity ratio between the two peaks at 526 and 527 eV assigned as 10a' and 3a″ depends not only on the hydrogen bonding network around the target molecule but also on the intramolecular conformation. This effect is absent in liquid methanol and demonstrates the high sensitivity of X-ray emission to molecular structure. The dependence of spectral features on hydrogen-bonding as well as on dynamical effects following core excitation are also discussed.

  17. X-ray emission from supernova remnants with particular reference to the Cygnus Loop

    International Nuclear Information System (INIS)

    Gronenschild, E.H.B.M.

    1979-01-01

    Observational or theoretical results related to the study of supernova remnants (SNRs) are described. Some background information is given by reviewing the present status of our knowledge of supernovae and supernova remnants, both from theory and observations. Also the distribution of all known radio, optical, and X-ray SNRs in the Galaxy is shown and a comparison is made. The X-ray observations of the well-known X-ray SNR the Cygnus Loop are discussed in detail and the discovery of a new X-ray emitting SNR W44 is described. Other radio sources are investigated, and the observed X-ray emission of SNRs are analysed using thermal spectra like exponential or bremsstrahlung spectra. The X-ray line spectrum that emerges from SNRs is described in detail. (Auth.)

  18. Sample positioning effects in x-ray spectrometry

    International Nuclear Information System (INIS)

    Carpenter, D.

    Instrument error due to variation in sample position in a crystal x-ray spectrometer can easily exceed the total instrumental error. Lack of reproducibility in sample position in the x-ray optics is the single largest source of system error. The factors that account for sample positioning error are described, and many of the details of flat crystal x-ray optics are discussed

  19. Multichannel, sequential or combined X-ray spectrometry

    International Nuclear Information System (INIS)

    Florestan, J.

    1979-01-01

    X-ray spectrometer qualities and defects are evaluated for sequential and multichannel categories. Multichannel X-ray spectrometer has time-coherency advantage and its results could be more reproducible; on the other hand some spatial incoherency limits low percentage and traces applications, specially when backgrounds are very variable. In this last case, sequential X-ray spectrometer would find again great usefulness [fr

  20. Microwave and X-Ray emission during a isentropic expansion and its application to solar bursts

    International Nuclear Information System (INIS)

    Piazza, L.R.

    1983-01-01

    The gyro-synchrotron emission in microwaves and the free-free emission in X-rays of a plasma enclosed in a cylinder coincident with a magnetic force tube were calculated for an isentropic self-similar expansion, with plane and cylindrical symmetries. This expansion model was applied to a region of the low solar corona, and the results were compared to the emission observed in some simple solar events of low intensity. The calculations show satisfactory coincidence with the events in X-rays for energies around 10 29 ergs. The solar events analyzed in microwaves, which are not the same that were studied in X-rays, in general do not fit the theoretical results. The origin of the discrepancy is probably the formulation of the processes of emission applied to the expansion. (Author) [pt

  1. X-ray and neutron emission studies in a new Filippov type plasma focus

    Energy Technology Data Exchange (ETDEWEB)

    Babazadeh, A.R.; Banoushi, A. [Technical University of Amirkabir, Tehran (Iran, Islamic Republic of). Dept. of Physics; Roshan, M.V.; Habibi, H.; Nasiry, A.; Memarzadeh, M.; Lamehi, M.; Kiai, S.M. Sadat [Atomic Energy Organization of Iran (AEOI), Tehran (Iran, Islamic Republic of). Nuclear Fusion Research Center

    2002-03-01

    We have performed experimental comparative studies of the X-ray and neutron emission generated by the new Filippov-type plasma focus 'Dena', (90 kJ, 25 kV, 288{mu}F) in the pressure range of 0.6-1 torr. Time-integrated and time-resolved detectors, together with an X-ray pin-hole camera, along with a Be filter of 10{mu}m thickness have been used. For a working gas of neon and a at insert anode, the maximum soft and hard X-rays (SXR-HXR) yield obtained was 16 V and 1.5 V/shot over a 4{pi} solid angle, respectively, for a charging voltage range of 16-20 kV. As for the argon gas, the similar results such as 3.5 and 2 V/shot have been found, leading to a total conversion efficiency of X-ray emission of 0.09 % (for neon) and 0.03 % (for argon) of the stored energy. These efficiencies have been improved by the employment of a conic insert anode up to 0.4% and 0.1%. With deuterium puffing gas and a at insert anode, the maximum emission yield has been found to be 2.5 V for SXR and 1 V for HXR/shot which produce an ultimate emission profile width (FWHM) of 70-90 ns for X-rays and neutrons, giving rise to a maximum neutron yield of 1.2 x 10{sup 9}. Nevertheless, the maximum yield has been increased up to 5.5 times with the conic insert anode. In order to increase the neutron yield, we have introduced a krypton admixture to the deuterium filling gas and found that, for a krypton pressure of about 0.1 torr, the neutron yield increases by a factor of 3.5 for the flat insert and 1.5 for the conic insert anodes. (author)

  2. X-ray emission of the hot gas and of accelerated particles in supernova remnants

    International Nuclear Information System (INIS)

    Acero, F.

    2008-09-01

    The current observations seem to support the theory that the shock wave of supernova remnants accelerate electrons (representing about 1% of cosmic rays) of the interstellar medium up to energies of about 10 15 eV. However there is still no solid evidence that supernova remnants also accelerate protons (major component of cosmic rays). The X-ray observations of those supernova remnants with the satellite XMM-Newton can provide crucial information on the acceleration mechanisms and on this population of accelerated particles. This thesis presents the X-ray analysis of the supernova remnants RX J1713.7-3946 and SN 1006 for which it has been shown that they accelerate electrons efficiently. As a result, these objects are very good targets to compare the theoretical models of acceleration to the observation. For the first object, I constructed through new XMM-Newton observations, the first high-angular resolution mosaic of the entire supernova remnant. I then compared the X- and gamma-ray emission of this object in order to understand the nature of the gamma-ray emission. This spectral and morphological comparison allowed me to discuss the two possible origins of the gamma-ray radiation (issued by electrons or by protons). For SN 1006, I studied the density of the ambient medium in which the shock wave propagates. This density is a key parameter for the hydrodynamical evolution of the remnant and for studying a future gamma-ray emission. The study of X-ray emission of the gas heated by the shock wave allowed me to better estimate of the value of the density so far poorly constrained for this object. (author)

  3. Streaked spectrometry using multilayer x-ray-interference mirrors to investigate energy transport in laser-plasma applications

    International Nuclear Information System (INIS)

    Stradling, G.L.; Barbee, T.W. Jr.; Henke, B.L.; Campbell, E.M.; Mead, W.C.

    1981-08-01

    Transport of energy in laser-produced plasmas is scrutinized by devising spectrally and temporally identifiable characteristics in the x-ray emission history which identify the heat-front position at various times in the heating process. Measurements of the relative turn-on times of these characteristics show the rate of energy transport between various points. These measurements can in turn constrain models of energy transport phenomena. We are time-resolving spectrally distinguishable subkilovolt x-ray emissions from different layers of a disk target to examine the transport rate of energy into the target. A similar technique is used to measure the lateral expansion rate of the plasma spot. A soft x-ray streak camera with 15-psec temporal resolution is used to make the temporal measurements. Spectral discrimination of the incident signal is provided by multilayer x-ray interference mirrors

  4. Repeated pulsed x-ray emission equipment

    International Nuclear Information System (INIS)

    Terauchi, Hikaru; Iida, Satoshi

    1982-01-01

    X-ray diffraction technique has been applied to determine the spatial positions of atoms which compose a material, and it is needless to say that the technique is a fundamental means regardless of the fields of research. However, the application of X-ray diffraction to the research on physical properties has been so far limited to know the spatial positions of atoms or molecules under thermal equilibrium condition. The addition of time element to the conventional technique, that is, the analysis of material structure including the time-varying processes under non-equilibrium conditions, is considered to approach the elucidation of the essence of materials. The authors call this dynamic structural analysis. The authors have planned to analyze X-ray diffraction intensity which has the resolution of about 10 -8 s in the real time which is conjugate with energy. However, present pulsed X-ray sources are not suitable for diffraction experiment because the pulse width is too long or X-ray wavelength is too short. Accordingly, the authors have made for trial a pulsed X-ray source for diffraction experiment. Its specifications are: diode voltage (X-ray tube voltage) from 200 to 300 kV, diode current from 2 to 5 kA, pulse width of about 30ns, maximum repetition frequency 10 pps, and X-ray focus size of 2 mm diameter. One of the features of this source is the repeated generation of pulsed X-ray. This is the first trial in the world, and is indispensable to the dynamic structural analysis described above. The quality of the emitted X-ray is also written. (Wakatsuki, Y.)

  5. Symbiotic Stars in X-rays

    Science.gov (United States)

    Luna, G. J. M.; Sokoloski, J. L.; Mukai, K.; Nelson, T.

    2014-01-01

    Until recently, symbiotic binary systems in which a white dwarf accretes from a red giant were thought to be mainly a soft X-ray population. Here we describe the detection with the X-ray Telescope (XRT) on the Swift satellite of 9 white dwarf symbiotics that were not previously known to be X-ray sources and one that was previously detected as a supersoft X-ray source. The 9 new X-ray detections were the result of a survey of 41 symbiotic stars, and they increase the number of symbiotic stars known to be X-ray sources by approximately 30%. Swift/XRT detected all of the new X-ray sources at energies greater than 2 keV. Their X-ray spectra are consistent with thermal emission and fall naturally into three distinct groups. The first group contains those sources with a single, highly absorbed hard component, which we identify as probably coming from an accretion-disk boundary layer. The second group is composed of those sources with a single, soft X-ray spectral component, which likely arises in a region where low-velocity shocks produce X-ray emission, i.e. a colliding-wind region. The third group consists of those sources with both hard and soft X-ray spectral components. We also find that unlike in the optical, where rapid, stochastic brightness variations from the accretion disk typically are not seen, detectable UV flickering is a common property of symbiotic stars. Supporting our physical interpretation of the two X-ray spectral components, simultaneous Swift UV photometry shows that symbiotic stars with harder X-ray emission tend to have stronger UV flickering, which is usually associated with accretion through a disk. To place these new observations in the context of previous work on X-ray emission from symbiotic stars, we modified and extended the alpha/beta/gamma classification scheme for symbiotic-star X-ray spectra that was introduced by Muerset et al. based upon observations with the ROSAT satellite, to include a new sigma classification for sources with

  6. Commercial Applications of X Ray Spectrometric Techniques

    Energy Technology Data Exchange (ETDEWEB)

    Wegrzynek, D., E-mail: D.Wedgrznek@iaea.org [International Atomic Energy Agency, The IAEA Laboratories, Seibersdorf, Vienna (Austria)

    2013-07-15

    In the 21st century, the X-ray fluorescence (XRF) technique is widely used in process control, industrial applications and for routine elemental analysis. The technique has a multielement capability capable of detecting elements with Z {>=} 10, with a few instruments capable of detecting also elements with Z {>=} 5. It is characterized by a non-destructive analysis process and relatively good detection limits, typically one part per million, for a wide range of elements. The first commercial XRF instruments were introduced to the market about 50 years ago. They were the wavelength dispersive X ray fluorescence (WDXRF) spectrometers utilizing Bragg's law and reflection on crystal lattices for sequential elemental analysis of sample composition. The advances made in radiation detector technology, especially the introduction of semiconductor detectors, improvements in signal processing electronics, availability and exponential growth of personal computer market led to invention of energy dispersive X ray fluorescence (EDXRF) technique. The EDXRF is more cost effective as compared to WDXRF. It also allows for designing compact instruments. Such instruments can be easily tailored to the needs of different customers, integrated with industrial installations, and also miniaturized for the purpose of in-situ applications. The versatility of the technique has been confirmed in a spectacular way by using the XRF and X-ray spectrometric techniques, among few others, during the NASA and ESA missions in search for the evidence of life and presence of water on the surface of Mars. The XRF technique has achieved its strong position within the atomic spectroscopy group of analytical techniques not only due to its versatility but also due to relatively low running costs, as compared to the commonly used methods, e.g., atomic absorption spectrometry (AAS) or inductively coupled plasma atomic emission/mass spectrometry (ICP-AES/MS). Presently, the XRF technique together with X ray

  7. A Multiwavelength Exploration of the Grand Design Spiral M83: Diffuse X-ray Emission

    Science.gov (United States)

    Kuntz, K. D.; Long, K. S.; Blair, W. P.; Plucinsky, P. P.; Soria, R.; Winkler, P. F.

    2013-01-01

    We have obtained a series of deep X-ray images of the nearby galaxy M83, with a total exposure 729 ksec with the Chandra ACIS-S array. Since the bulk of the X-ray emitting disk falls within the BI chip, these observations allow a detailed study of the soft diffuse emission in the disk. Most of the diffuse emission is related to star-formation regions and must be powered by supernovae and stellar winds, though the amount of emission due to identifiable SNR is only a few percent. The relation between the spectral shape and surface brightness that was seen in M101 suggests that the properties of the X-ray emission in spiral disks are shaped by the local hot gas production rate (traced by the local star-formation rate) or the disk mid-plane pressure, but it is unclear which physical mechanism dominates. To illuminate this problem, we will compare M83 with the previous Chandra studies of M101 and M33.

  8. Discovery of the double Doppler-shifted emission-line systems in the X-ray spectrum of SS 433

    Science.gov (United States)

    Kotani, Taro; Kawai, Nobuyuki; Aoki, Takashi; Doty, John; Matsuoka, Masaru; Mitsuda, Kazuhisa; Nagase, Fumiaki; Ricker, George; White, Nick E.

    1994-01-01

    We have used the CCD X-ray spectrometers on ASCA and resolved the X-ray emission line from the jet of SS 433 both into Doppler-shifted components with two distinct velocities, and into emission from different ionization states of iron, i.e., Fe XXV and Fe XXVI. This is the first direct detection of the two Doppler shifted beams in the X-ray spectra of SS 433 and allows the radial velocity of the jet along the line of sight to be determined with an accuracy comparable to the optical spectroscopy. We also found pairs of emission lines from other atomic species, such as ionized silicon and sulfur, with the Doppler shifts consistent with each other. This confirms the origin of the X-ray emission in the high temperature plasma in the jets.

  9. X-ray emission characteristics of foam target plasmas

    International Nuclear Information System (INIS)

    Fronya, A.A.; Borisenko, N.G.; Chernodub, M.L.; Merkuliev, Yu.A.; Osipov, M.V.; Puzyrev, V.N.; Sahakyan, A.T.; Starodub, A.N.; Vasin, B.L.; Yakushev, O.F.

    2010-01-01

    Complete text of publication follows. Experimental results of laser radiation interaction with a foam targets are presented. The spatial, temporal and energy characteristics of x-ray plasma radiation have been investigated. The pinhole-camera and Schwarzschild objective have been used for the plasma image formation in different spectral ranges. The plasma image is registered by the Schwarzschild objective in a narrow spectral range 180 - 200 A. Spectral characteristics of x-ray radiation registered by pinhole-camera have been defined by means outer filters. The use of the filters with different transmission curves allowed one the determine the localization of x-ray radiation with fixed wavelength. Spatial resolution accounts 16 μm in the pinhole-camera diagnostic channel and 2.5 μm in the Schwarzschild objective diagnostic channel. The plasma images in the intrinsic x-ray radiation show that the emission area in the transverse direction with respect to the direction of the propagating heating radiation exceeds the focal spot size. This fact indicates that the target heating in the transverse direction is due to internal energy of the created plasma. The average value of plasma electron temperature is ∼ 0.4 - 1.4 keV. Acknowledgements. The work is partly supported by the Russian Foundation for Basic Researches, grant no. 10-02-00113 and by Federal Target Program 'Research and scientific-pedagogical cadres of Innovative Russia' (grant 2009-1.1-122-052-025).

  10. Applied gamma-ray spectrometry

    CERN Document Server

    Dams, R; Crouthamel, Carl E

    1970-01-01

    Applied Gamma-Ray Spectrometry covers real life application of the gamma-ray and the devices used in their experimental studies. This book is organized into 9 chapters, and starts with discussions of the various decay processes, the possible interaction mechanisms of gamma radiation with matter, and the intrinsic and extrinsic variables, which affect the observed gamma-ray and X-ray spectra. The subsequent chapters deal with the properties and fabrication of scintillation detectors, semiconductor detectors, and proportional gas counters. These chapters present some of the most widely utilized

  11. Massive stars, x-ray ridge, and galactic 26Al gamma-ray line emission

    International Nuclear Information System (INIS)

    Montmerle, T.

    1986-07-01

    Massive stars interact with their parent molecular cloud by means of their ionizing flux and strong winds, thereby creating giant, hollow HII regions. To account for the observed structure of these HII regions, it appears necessary that all the wind energy be dissipated. Dorland and Montmerle have recently proposed a new dissipation mechanism, in the process, diffuse hard X-rays are emitted. If the observed galactic X-ray ''ridge'' results from this process on a galactic scale, it can be accounted for by the interaction of ∼3000 Wolf-Rayet stars (mostly within a ∼6.5 kpc ring) with their surrounding interstellar gas. This result is essentially consistent with the suggestion by Prantzos and Casse that the galactic 26 Al γ-ray line emission originates in Wolf-Rayet stars

  12. Ultra fast atomic process in X-ray emission by inner-shell ionization

    Energy Technology Data Exchange (ETDEWEB)

    Moribayashi, Kengo; Sasaki, Akira [Japan Atomic Energy Research Inst., Neyagawa, Osaka (Japan). Kansai Research Establishment; Tajima, T

    1998-03-01

    An ultra-fast atomic process together with X-ray emission by inner-shell ionization using high intensity (10{sup 18} W/cm{sup 2}) short pulse (20fs) X-ray is studied. A new class of experiment is proposed and a useful pumping source is suggested. In this method, it is found that the gain value of X-ray laser amounts to larger than 1000(1/cm) with use of the density of 10{sup 22}/cm{sup 3} of carbon atom. Electron impact ionization effect and initial density effect as well as intensity of pumping source effect are also discussed. (author)

  13. Relations Between FUV Excess and Coronal Soft X-Ray Emission Among Dwarf Stars

    Science.gov (United States)

    Smith, Graeme H.; Hargrave, Mason; Eckholm, Elliot

    2017-11-01

    The far-ultraviolet magnitudes of late-F, G and early-K dwarfs with (B - V) ⩾ 0.50 as measured by the GALEX satellite are shown to correlate with soft X-ray luminosity. This result indicates that line and continuum emission from stellar active regions make significant contributions to the flux in the GALEX FUV band for late-F, G and K dwarfs. By contrast, detection of a correlation between FUV brightness and soft X-ray luminosity among early-F dwarfs requires subtraction of the photospheric component from the FUV flux. The range in (B - V) among F and G dwarfs over which a correlation between uncorrected FUV magnitude and X-ray luminosity is detected coincides with the range in colour over which coronal and chromospheric emission correlates with stellar rotation.

  14. Design and characterization for absolute x-ray spectrometry in the 100-10,000 eV region

    International Nuclear Information System (INIS)

    Henke, B.L.

    1986-08-01

    Reviewed here are the design and characterization procedures used in our program for developing absolute x-ray spectrometry in the 100 to 10,000 eV region. Described are the selection and experimental calibration of the x-ray filters, mirror momochromators, crystal/multilayer analyzers, and the photographic (time integrating) and photoelectric (time resolving) position-sensitive detectors. Analytical response functions have been derived that characterize the energy dependence of the mirror and crystal/multilayer reflectivities and of the photographic film and photocathode sensitivities. These response functions permit rapid, small-computer reduction of the experimental spectra to absolute spectra (measured in photons per stearadian from the source for radiative transitions at indicated photon energies). Our x-ray spectrographic systems are being applied to the diagnostics of pulsed, high temperature plasma sources in laser fusion and x-ray laser research. 15 refs., 27 figs

  15. Electron-electron correlation, resonant photoemission and X-ray emission spectra

    International Nuclear Information System (INIS)

    Parlebas, J.C.; Kotani, Akio; Tanaka, Satoshi.

    1991-01-01

    In this short review paper we essentially focus on the high energy spectroscopies which involve second order quantum processes, i.e., resonance photoemission, Auger and X-ray emission spectroscopies, denoted respectively by RXPS, AES and XES. First, we summarize the main 3p-RXPS and AES results obtained in Cu and Ni metals; especially we recall that the satellite near the 3p-threshold in the spectra, which arises from a d-hole pair bound state, needs a careful treatment of the electron-electron correlation. Then we analyze the RXPS spectra in a few Ce compounds (CeO 2 , Ce 2 O 3 and CeF 3 ) involving 3d or 4d core levels and we interpret the spectra consistently with the other spectroscopies, such as core XPS and XAS which are first order quantum processes. Finally within the same one-impurity model and basically with the same sets of parameters, we review a theory for the Ce 5p→3d XES, as well as for the corresponding RXES, where (1) the incident X-ray is tuned to resonate with the 3d→4f transition and (2) the X-ray emission due to the 5p→3d transition is actually observed. The paper ends with a general discussion. (author) 77 refs

  16. Trends in grazing emission x-ray analysis techniques

    International Nuclear Information System (INIS)

    Grieken, R. van; Tsuji, K.; Injuk, J.

    2000-01-01

    In grazing-emission x-ray fluorescence (GEXRF) spectrometry, XRF is made surface-sensitive, not by grazing incidence of the exciting radiation as in total reflection XRF (TXRF), but by detecting only that part of fluorescence radiation that is emitted at grazing angles above a polished sample carrier or above a flat wafer. In case of GEXRF, and contrary to TXRF, wavelength-dispersive (WD) detection can be used. Applications are, in principle, similar to those of (variable angle) TXRF. At the laboratory scale, only prototype instruments are available, and the GEXRF unit can be an accessory to a commercial WD-XRF instrument. The detection limits of GEXRF are in the higher pg range, corresponding to a concentration of between 0.4-3 μg/l, if a sample volume of 100 μl is examined. Because of the WD detection, GEXRF also lends itself for the analysis of low-Z elements, from Z > 5; this is an advantage over conventional TXRF (but similar to TXRF using a thin-window energy-dispersive detector). Since the GEXRF prototype is a sequential rather than a simultaneous instrument, the analysis time is long when many elements have to be determined. Moreover, because the soft characteristic radiation is more strongly absorbed in its longer path through the matrix than in TXRF, the linear response for trace analysis using GEXRF is limited; this was proven by calculating the fluorescence intensities as a function of layer thickness and composition. The specimens are very limited in thickness. The sample preparation procedure for liquid or other samples to be analyzed with the GEXRF unit is thus very problematic. Results for water samples, bio-materials and pigment and aerosol samples have indeed shown that the quantitative nature of GEXRF for trace analysis is poor. The most promising features of GEXRF are in the field of surface and thin-layer analysis. Trace contaminations on silicon wafers can be determined and depth profiling can characterize stratified near-surface layers. But

  17. A SEARCH FOR X-RAY EMISSION FROM COLLIDING MAGNETOSPHERES IN YOUNG ECCENTRIC STELLAR BINARIES

    Energy Technology Data Exchange (ETDEWEB)

    Getman, Konstantin V.; Broos, Patrick S. [Department of Astronomy and Astrophysics, 525 Davey Laboratory, Pennsylvania State University, University Park, PA 16802 (United States); Kóspál, Ágnes [Konkoly Observatory, Research Center for Astronomy and Earth Sciences, Hungarian Academy of Sciences, P.O. Box 67, 1525 Budapest (Hungary); Salter, Demerese M. [Department of Astronomy and Laboratory for Millimeter-Wave Astronomy, University of Maryland, College Park, MD 20742 (United States); Garmire, Gordon P. [Huntingdon Institute for X-ray Astronomy, LLC, 10677 Franks Road, Huntingdon, PA 16652 (United States)

    2016-12-01

    Among young binary stars whose magnetospheres are expected to collide, only two systems have been observed near periastron in the X-ray band: the low-mass DQ Tau and the older and more massive HD 152404. Both exhibit elevated levels of X-ray emission at periastron. Our goal is to determine whether colliding magnetospheres in young high-eccentricity binaries commonly produce elevated average levels of X-ray activity. This work is based on Chandra snapshots of multiple periastron and non-periastron passages in four nearby young eccentric binaries (Parenago 523, RX J1622.7-2325 Nw, UZ Tau E, and HD 152404). We find that for the merged sample of all four binaries the current X-ray data show an increasing average X-ray flux near periastron (at a ∼2.5-sigma level). Further comparison of these data with the X-ray properties of hundreds of young stars in the Orion Nebula Cluster, produced by the Chandra Orion Ultradeep Project (COUP), indicates that the X-ray emission from the merged sample of our binaries cannot be explained within the framework of the COUP-like X-ray activity. However, due to the inhomogeneities of the merged binary sample and the relatively low statistical significance of the detected flux increase, these findings are regarded as tentative only. More data are needed to prove that the flux increase is real and is related to the processes of colliding magnetospheres.

  18. Analysis of borophosphosilicate glass layers on silicon wafers by X-ray emission from photon and electron excitation

    International Nuclear Information System (INIS)

    Elgersma, O.; Borstrok, J.J.M.

    1989-01-01

    Phosphorus and oxygen concentrations in the homogeneous layer of borosilicate glass (BPSG) deposited on Si-integrated circuits are determined by X-ray fluorescence from photon excitation. The X-ray emission from electron excitation in an open X-ray tube instrument yields a sufficiently precise determination of the boron content. The thickness of the layer can be derived from silicon Kα-fluorescence. A calibration model is proposed for photon as well as for electron excitation. The experimentally determined parameters in this model well agree with those derived from fundamental parameters for X-ray absorption and emission. The chemical surrounding of silicon affects strongly the peak profile of the silicon Kβ-emission. This enables to distinguish emission from the silicon atoms in the wafer and from the silicon atoms in the silicon oxide complexes of the BPSG-layer. (author)

  19. Observation of soft X-ray spectra from a Seyfert 1 and a narrow emission-line galaxy

    International Nuclear Information System (INIS)

    Singh, K.P.; Garmire, G.P.; Nousek, J.

    1985-01-01

    The 0.2-40 keV X-ray spectra of the Seyfert 1 galaxy Mrk 509 and the narrow emission-line galaxy NGC 2992 are analyzed. The results suggest the presence of a steep soft X-ray component in Mrk 509 in addition to the well-known Gamma = 1.7 component found in other active galactic nuclei in the 2-40 keV energy range. The soft X-ray component is interpreted as due to thermal emission from a hot gas, probably associated with the highly ionized gas observed to be outflowing from the galaxy. The X-ray spectrum of NGC 2992 does not show any steepening in the soft X-ray band and is consistent with a single power law (Gamma = 1.78) with very low absorbing column density of 4 x 10 to the 21st/sq cm. A model with partial covering of the nuclear X-ray source is preferred, however, to a simple model with a single power law and absorption. 34 references

  20. Calculation of X-ray emission produced by a quasi-monoenergetic electron distribution

    International Nuclear Information System (INIS)

    Fanaei, M.; Sadighi-Bonabi, R.

    2010-01-01

    Complete text of publication follows. By using an intense ultrafast laser interaction with plasma, generation of accelerated relativistic electrons with quasi monoenergetic spectrum has been possible. Analytic expressions for spectra and emission efficiencies of x-rays bremsstrahlung and characteristic line emission produced by a quasi-monoenergetic electron distribution from several targets are investigated. In this work, a Gaussian profile is assumed for the quasi-monoenergetic electron spectrum. The produced x-ray radiations are compared with the previous achieved results for a Maxwellian electron profile. These results and achievements are discussed in detail. Also, the outcomes can be evaluated with the experimental and simulated results.

  1. X-ray emission spectroscopic determination of iron in a polyurethane encapsulant curing agent

    International Nuclear Information System (INIS)

    Carter, J.M.; Kling, E.N.

    1979-01-01

    Presented is a procedure for determining the iron content in a polyurethane encapsulant curing agent by x-ray emission spectroscopy. Standards were prepared by adding ferric acetyl acetonate to a curing agent of identical composition to that being analyzed, but containing no iron. Results show that x-ray emission spectroscopy is feasible for determination of iron in the 30 to 50 ppM range. This range could probably be extended by the preparation of additional standards. Precision of the method is approximately 1.2 ppM at the 99 percent confidence level

  2. Radio search for pulsed emission from X-ray pulsars

    Energy Technology Data Exchange (ETDEWEB)

    delli Santi, F S; Delpino, F [Bologna Univ. (Italy). Ist. di Astronomia; Inzani, P; Sironi, G [Consiglio Nazionale delle Ricerche, Milan (Italy). Lab. di Fisica Cosmica e Tecnologie Relative; Mandolesi, N; Morigi, G [Consiglio Nazionale delle Ricerche, Bologna (Italy). Lab. TESRE

    1981-05-01

    An experiment has been performed at 325 MHz, with a 10 m tracking dish, for the search of pulsed radio emission associated with X-ray pulsars. No evidence of radio pulses has been found in the four sources investigated, although the radio pulsar PSR 0329 + 54, used a testing object, has been detected successfully.

  3. Detection of halogenated flame retardants in polyurethane foam by particle induced X-ray emission

    International Nuclear Information System (INIS)

    Maley, Adam M.; Falk, Kyle A.; Hoover, Luke; Earlywine, Elly B.; Seymour, Michael D.; DeYoung, Paul A.; Blum, Arlene; Stapleton, Heather M.; Peaslee, Graham F.

    2015-01-01

    A novel application of particle-induced X-ray emission (PIXE) has been developed to detect the presence of chlorinated and brominated flame retardant chemicals in polyurethane foams. Traditional Gas Chromatography–Mass Spectrometry (GC–MS) methods for the detection and identification of halogenated flame retardants in foams require extensive sample preparation and data acquisition time. The elemental analysis of the halogens in polyurethane foam performed by PIXE offers the opportunity to identify the presence of halogenated flame retardants in a fraction of the time and sample preparation cost. Through comparative GC–MS and PIXE analysis of 215 foam samples, excellent agreement between the two methods was obtained. These results suggest that PIXE could be an ideal rapid screening method for the presence of chlorinated and brominated flame retardants in polyurethane foams

  4. Detection of halogenated flame retardants in polyurethane foam by particle induced X-ray emission

    Energy Technology Data Exchange (ETDEWEB)

    Maley, Adam M.; Falk, Kyle A.; Hoover, Luke; Earlywine, Elly B.; Seymour, Michael D. [Department of Chemistry, Hope College, 35 E. 12th Street, Holland, MI 49423 (United States); DeYoung, Paul A. [Department of Physics, Hope College, 27 Graves Place, Holland, MI 49423 (United States); Blum, Arlene [Green Science Policy Institute, Box 5455, Berkeley, CA 94705 (United States); Stapleton, Heather M. [Nicholas School of the Environment, Duke University, LSRC Box 90328, Durham, NC 27708 (United States); Peaslee, Graham F., E-mail: peaslee@hope.edu [Department of Chemistry, Hope College, 35 E. 12th Street, Holland, MI 49423 (United States)

    2015-09-01

    A novel application of particle-induced X-ray emission (PIXE) has been developed to detect the presence of chlorinated and brominated flame retardant chemicals in polyurethane foams. Traditional Gas Chromatography–Mass Spectrometry (GC–MS) methods for the detection and identification of halogenated flame retardants in foams require extensive sample preparation and data acquisition time. The elemental analysis of the halogens in polyurethane foam performed by PIXE offers the opportunity to identify the presence of halogenated flame retardants in a fraction of the time and sample preparation cost. Through comparative GC–MS and PIXE analysis of 215 foam samples, excellent agreement between the two methods was obtained. These results suggest that PIXE could be an ideal rapid screening method for the presence of chlorinated and brominated flame retardants in polyurethane foams.

  5. X-RAY EMISSION FROM J1446–4701, J1311–3430, AND OTHER BLACK WIDOW PULSARS

    Energy Technology Data Exchange (ETDEWEB)

    Arumugasamy, Prakash; Pavlov, George G. [Department of Astronomy and Astrophysics, 525 Davey Lab, The Pennsylvania State University, University Park, PA 16802 (United States); Garmire, Gordon P., E-mail: pxa151@ucs.psu.edu [Huntingdon Institute for X-ray Astronomy, LLC, 10677 Franks Road, Huntingdon, PA 16652 (United States)

    2015-12-01

    We present the results of detailed X-ray analysis of two black-widow pulsars (BWPs), J1446–4701 and J1311–3430. PSR J1446–4701 is a BWP with orbital parameters near the median values of the sample of known BWPs. Its X-ray emission that was detected by XMM-Newton is well characterized by a soft power-law (PL) spectrum (photon index Γ ≈ 3), and it shows no significant orbital modulations. In view of a lack of radio eclipses and an optical non-detection, the system most likely has a low orbital inclination. PSR J1311–3430 is an extreme BWP with a very compact orbit and the lowest minimum mass companion. Our Chandra data confirm the hard Γ ≈ 1.3 emission seen in previous observations. Through phase-restricted spectral analysis, we found a hint (∼2.6σ) of spectral hardening around pulsar inferior conjunction. We also provide a uniform analysis of the 12 BWPs observed with Chandra and compare their X-ray properties. Pulsars with soft, Γ > 2.5 emission seem to have lower than average X-ray and γ-ray luminosities. We do not, however, see any other prominent correlation between the pulsar’s X-ray emission characteristics and any of its other properties. The contribution of the intra-binary shock to the total X-ray emission, if any, is not discernible in this sample of pulsars with shallow observations.

  6. Multiwavelength Photometric Imaging of X-Ray and EUV Emission from Comet P/Tempel-Tuttle 1998

    Science.gov (United States)

    Lisse, Carey M.

    2004-01-01

    The unexpected discovery of x-ray emission from Comet Hyakutake in March 1996 (Lisse et ai. 1996) has produced a number of questions about the physical mechanism producing the radiation. The original detection and subsequent observations (Dennerl et ai. 1997, Mumma et al. 1997, Krasnopolsky et al. 1998, Owens et al. 1998. Lisse et al. 1999) have shown that the very soft (best fit thermal bremsstrahlung model kT approx. 0.2 keV) emission is due to an interaction between the solar wind and the comet's atmosphere. Using the results fiom the 15 comets detected to date in x-rays, we report on the latest results on cometary x-ray emission, including new results from Chandra and XMM. As-observed morphologies, spectra, and light curves will be discussed. Our emphasis will be on understanding the physical mechanism producing the emission, and using this to determine the nature of the cometary coma, the structure of the solar wind in the heliosphere, and the source of the local soft x-ray background. This work has been graciously supported by grants from the NASA Planetary Astronomy and Astrophysical Data Programs.

  7. Ferro-metry and X-ray fluorescence to measure wear

    International Nuclear Information System (INIS)

    Catherin, J.Y.

    1997-01-01

    The determination of wear of metallic structures is carried out by measuring metallic particles in the lubricating oil. This method is routinely used by SNCF, the French railroad company to control the motors of the high speed trains (TGV). Four methods, plasma emission spectrometry, X-ray fluorescence analysis, ferro-metry and magnetometry are used. The field of application and advantage of each method is described. (C.B.)

  8. Some implications of excess soft X-ray emission from Seyfert 1 galaxies

    International Nuclear Information System (INIS)

    Fabian, A.C.; Guilbert, P.W.; Arnaud, K.A.; Shafer, R.A.; Tennant, A.F.; Ward, M.J.

    1986-01-01

    The X-ray spectrum of Seyfert 1 galaxies is characterized by a hard power-law spectrum. It is often postulated that this maintains a Compton-heated two-phase Broad-Line Region (BLR) around the central source. It is shown here that the strong excess soft X-ray emission observed in MKN 841 and other Seyfert galaxies invalidates this model if the BLR is spherically symmetric. Alternatives are proposed. (author)

  9. X ray spectra of X Per. [oso-8 observations

    Science.gov (United States)

    Becker, R. H.; Boldt, E. A.; Holt, S. S.; Pravdo, S. H.; Robinson-Saba, J.; Serlemitsos, P. J.; Swank, J. H.

    1978-01-01

    The cosmic X-ray spectroscopy experiment on OSO-8 observed X Per for twenty days during two observations in Feb. 1976 and Feb. 1977. The spectrum of X Per varies in phase with its 13.9 min period, hardening significantly at X-ray minimum. Unlike other X-ray binary pulsar spectra, X Per's spectra do not exhibit iron line emission or strong absorption features. The data show no evidence for a 22 hour periodicity in the X-ray intensity of X Per. These results indicate that the X-ray emission from X Per may be originating from a neutron star in a low density region far from the optically identified Be star.

  10. A strategy for vitrification product assurance and control with X-ray fluorescence spectrometry (PACX)

    International Nuclear Information System (INIS)

    Resce, J.L.

    1995-01-01

    A product control strategy is proposed for the vitrification of low-level and/or mixed waste. This strategy is called Product Assurance and Control with X-ray fluorescence spectrometry (PACX). The strategy utilizes sequential wavelength dispersive x-ray fluorescence spectrometry and standardless fundamental parameters calculations to analyze both the melter feed and the glassy products. The melter feed is sampled prior to addition to the melt tank and then melted and cast into samples which should closely resemble the product from the vitrification process itself. The resulting sample disks are then analyzed by x-ray fluorescence spectrometry. All elements with atomic numbers down to sodium can be determined directly and then either boron or lithium can be determined by difference from the mass balance. The XRF intensities are converted into oxide compositions with the use of a novel standardless fundamental parameters program. Previous work has shown that there is an excellent correlation between the XRF results and the results from conventional wet chemical analyses, but the XRF results can be obtained within two to three hours of sampling. If compositional control limits for durability are available, the product acceptability can be determined prior to the batch being introduced into the melter. The durability could also be estimated from a model, if available, which predicts product durability from composition. If the predicted durability is estimated to be too low, the model can then be used to determine additives which will raise the durability of the final product to within acceptable limits. The additives can then be incorporated into the batch prior to addition into the melter. A similar XRF analysis can be carried out on the glass product from the melter which can then be used to predict and thus assure product acceptance

  11. Balloon observation of the binary X-ray source Her X-1 1.24 sec pulsation and cyclotron line emission

    International Nuclear Information System (INIS)

    Pietsch, W.; Reppin, C.; Truemper, J.; Voges, W.; Kendziorra, E.; Staubert, R.; Tuebingen Univ.

    1978-01-01

    During a balloon observation from Palestine, Texas, the authors detected for the first time the 1.24 sec pulsation of Hercules X-1 in the hard X-ray range up to 70 keV and discovered strong line emission in its spectrum at 58 keV. They estimated a line flux of 3x10 -3 photons cm -2 sec -1 and a line width of less than 12 keV. The phenomenon is interpreted as electron cyclotron emission at the basic frequency emitted by the hot polar plasma of the rotating neutron star. The line measured leads to a magnetic field strength of 5.3x10 12 gauss. In further observations during a balloon campaign in Sept./Oct. 1977 the authors confirmed the existence of the line emission and for the first time found pulsed X-ray emission above 15 keV during the 'short on' - and 'off'-state of the Her X-1 35 day cycle. The pulse to interpulse ratio seems to vary with the 35 day phase

  12. X-ray clusters of galaxies

    International Nuclear Information System (INIS)

    McKee, J.D.

    1980-01-01

    This work is in three chapters, of which the first is an introduction to clusters of galaxies. The second chapter describes the HEAO A-2 Survey of Abell Clusters. The 225 clusters of galaxies listed in Abell's (1958) catalog which are of distance class four or less, were surveyed for 2 to 10 keV x-ray emission. Thirty-two identifications of x-ray sources with the clusters were made, fluxes and error boxes were determined for these sources; twelve of the identifications are new. The x-ray luminosity function has been derived and analytical fits have been made, the best fit is f(L) = 26.9 x 10 -8 exp( - L 44 /1.7) per Mpc per 10 44 erg s -1 per 2 to 10 keV band pass. The relationship between x-ray luminosity, Bautz-Morgan type, Rood-Sastry type, and richness has also been examined. The contribution of clusters to the x-ray background has been calculated from the luminosity function and has been found to be 3.5%, and with 90% certainty, less than 8% in the 2 to 10 keV band pass, assuming that clusters were not brighter in the past than they are at present. If they were bright enough in the past to account for the x-ray background, the evolution must have scaled more rapidly than (1 + z) 7 if clusters formed at z = 3, or (1 + z) 5 if clusters formed at z = 10. Chapter Three examines x-ray emission from poor clusters of galaxies. Burns and Owens' (1979) sample of 25 4C radio sources which coincide with Zwicky clusters of galaxies has been searched for x-ray emission in the HEAO A-2 data base. X-ray emission was detected from five sources at the 3sigma level, two exceeded 5 sigma. The search for x-ray emission was prompted by the knowledge of the existence of distorted radio sources in the clusters. The distortion implies the presence of a relatively dense intracluster medium which is expected to produce thermal bremsstrahlung x-ray emission

  13. Einstein Observatory survey of X-ray emission from solar-type stars - the late F and G dwarf stars

    Energy Technology Data Exchange (ETDEWEB)

    Maggio, A.; Sciortino, S.; Vaiana, G.S.; Majer, P.; Bookbinder, J.

    1987-04-01

    Results of a volume-limited X-ray survey of stars of luminosity classes IV and V in the spectral range F7-G9 observed with the Einstein Observatory are presented. Using survival analysis techniques, the stellar X-ray luminosity function in the 0.15-4.0 keV energy band for both single and multiple sources. It is shown that the difference in X-ray luminosity between these two classes of sources is consistent with the superposition of individual components in multiple-component systems, whose X-ray properties are similar to those of the single-component sources. The X-ray emission of the stars in our sample is well correlated with their chromospheric CA II H-K line emission and with their projected equatorial rotational velocity. Comparison of the X-ray luminosity function constructed for the sample of the dG stars of the local population with the corresponding functions derived elsewhere for the Hyades, the Pleiades, and the Orion Ic open cluster confirms that the level of X-ray emission decreases with stellar age. 62 references.

  14. Einstein Observatory survey of X-ray emission from solar-type stars - The late F and G dwarf stars

    Science.gov (United States)

    Maggio, A.; Sciortino, S.; Vaiana, G. S.; Majer, P.; Bookbinder, J.

    1987-01-01

    Results of a volume-limited X-ray survey of stars of luminosity classes IV and V in the spectral range F7-G9 observed with the Einstein Observatory are presented. Using survival analysis techniques, the stellar X-ray luminosity function in the 0.15-4.0 keV energy band for both single and multiple sources. It is shown that the difference in X-ray luminosity between these two classes of sources is consistent with the superposition of individual components in multiple-component systems, whose X-ray properties are similar to those of the single-component sources. The X-ray emission of the stars in our sample is well correlated with their chromospheric CA II H-K line emission and with their projected equatorial rotational velocity. Comparison of the X-ray luminosity function constructed for the sample of the dG stars of the local population with the corresponding functions derived elsewhere for the Hyades, the Pleiades, and the Orion Ic open cluster confirms that the level of X-ray emission decreases with stellar age.

  15. A study of x-ray emission from the anode region in a plasma focus device

    International Nuclear Information System (INIS)

    Jia Wang; Tsinchi Yang

    1988-01-01

    The physical process of x-ray emission from the anode region in a plasma focus device due to the interaction of a powerful electron beam with the metal anode and with ionised metallic vapour from the anode is investigated. The influence of the magnetic field of the beam is taken into consideration. A MC-PIC model (Monte Carlo-particle in cell) is proposed for the process, in which an electron-photon collision cascade is simulated by the MC approach and the time-dependent state of metallic vapour is determined by PIC computation. The time-resolved energy spectra and angular distributions of x-ray emission from the extending anode region are calculated. The time-integrated characteristics of the x-ray emission can be compared with the results of experiments as far as they are available. (author)

  16. Theoretical estimation of proton induced X-ray emission yield of the trace elements present in the lung and breast cancer

    International Nuclear Information System (INIS)

    Manjunatha, H.C.; Sowmya, N.

    2013-01-01

    X-rays may be produced following the excitation of target atoms induced by an energetic incident ion beam of protons. Proton induced X-ray emission (PIXE) analysis has been used for many years for the determination of elemental composition of materials using X-rays. Recent interest in the proton induced X-ray emission cross section has arisen due to their importance in the rapidly expanding field of PIXE analysis. One of the steps in the analysis is to fit the measured X-ray spectrum with theoretical spectrum. The theoretical cross section and yields are essential for the evaluation of spectrum. We have theoretically evaluated the PIXE cross sections for trace elements in the lung and breast cancer tissues such as Cl, K, Ca,Ti, Cr, Mn, Fe, Ni, Cu, Zn, As, Se, Br, Rb, P, S, Sr, Hg and Pb. The estimated cross section is used in the evaluation of Proton induced X-ray emission spectrum for the given trace elements.We have also evaluated the Proton induced X-ray emission yields in the thin and thick target of the given trace elements. The evaluated Proton induced X-ray emission cross-section, spectrum and yields are graphically represented. Some of these values are also tabulated. Proton induced X-ray emission cross sections and a yield for the given trace elements varies with the energy. PIXE yield depends on a real density and does not on thickness of the target. (author)

  17. A double cell for X-ray absorption spectrometry of atomic Zn

    CERN Document Server

    Mihelic, A; Arcon, I; Padeznik-Gomilsek, J; Borowski, M

    2002-01-01

    A high-temperature cell with a double wall design has been constructed for X-ray absorption spectrometry of metal vapors. The inner cell, assembled from a corundum tube and thin plates without welding or reshaping, serves as a container of the vapor sample. It is not vacuum tight: instead, the outer tube provides inert atmosphere. Several spectra of K-edge atomic absorption of Zn were obtained in the stationary working regime below the Zn boiling point. The K-edge profile shows an extremely strong resonance and, above the continuum threshold, coexcitations of the outer electrons.

  18. X-ray tube target

    International Nuclear Information System (INIS)

    Weber, R.G.

    1980-01-01

    A target with an improved heat emissive surface for use in a rotating anode type x-ray tube is described. The target consists of a body having a first surface portion made of x-ray emissive material and a second surface portion made of a heat emissive material comprising at least one of hafnium boride, hafnium oxide, hafnium nitride, hafnium silicide, and hafnium aluminide. (U.K.)

  19. Steep Hard-X-ray Spectra Indicate Extremely High Accretion Rates in Weak Emission-Line Quasars

    Science.gov (United States)

    Marlar, Andrea; Shemmer, Ohad; Anderson, Scott F.; Brandt, W. Niel; Diamond-Stanic, Aleksandar M.; Fan, Xiaohui; Luo, Bin; Plotkin, Richard; Richards, Gordon T.; Schneider, Donald P.; Wu, Jianfeng

    2018-06-01

    We present XMM-Newton imaging spectroscopy of ten weak emission-line quasars (WLQs) at 0.928 ≤ z ≤ 3.767, six of which are radio quiet and four which are radio intermediate. The new X-ray data enabled us to measure the hard-X-ray power-law photon index (Γ) in each source with relatively high accuracy. These measurements allowed us to confirm previous reports that WLQs have steeper X-ray spectra, therefore indicating higher accretion rates with respect to "typical" quasars. A comparison between the Γ values of our radio-quiet WLQs and those of a carefully-selected, uniform sample of 84 quasars shows that the first are significantly higher, at the ≥ 3σ level. Collectively, the four radio-intermediate WLQs have lower Γ values with respect to the six radio-quiet WLQs, as may be expected if the spectra of the first group are contaminated by X-ray emission from a jet. These results suggest that, in the absence of significant jet emission along our line of sight, WLQs constitute the extreme high end of the accretion rate distribution in quasars. We detect soft excess emission in our lowest-redshift radio-quiet WLQ, in agreement with previous findings suggesting that the prominence of this feature is associated with a high accretion rate. We have not detected signatures of Compton reflection, Fe Kα lines, or strong variability between two X-ray epochs in any of our WLQs.

  20. A new generation of x-ray spectrometry UHV instruments at the SR facilities BESSY II, ELETTRA and SOLEIL

    Energy Technology Data Exchange (ETDEWEB)

    Lubeck, J., E-mail: janin.lubeck@ptb.de; Fliegauf, R.; Holfelder, I.; Hönicke, P.; Müller, M.; Pollakowski, B.; Ulm, G.; Weser, J.; Beckhoff, B. [Physikalisch-Technische Bundesanstalt (PTB), Abbestr. 2-12, 10587 Berlin (Germany); Bogovac, M.; Kaiser, R. B.; Karydas, A. G.; Leani, J. J.; Migliori, A.; Sghaier, H. [Nuclear Science and Instrumentation Laboratory, IAEA Laboratories, A-2444, Seibersdorf (Austria); Boyer, B.; Lépy, M. C.; Ménesguen, Y. [CEA, LIST, Laboratoire National Henri Becquerel, Bât. 602 PC 111, CEA-Saclay 91191 Gif-sur-Yvette c. (France); Detlefs, B. [CEA-LETI, Minatec Campus, 17 rue des Martyrs, 38054 Grenoble (France); Eichert, D. [Elettra - Sincrotrone Trieste (EST) S.C.p.A., 34149 Basovizza, Trieste (Italy); and others

    2016-07-27

    A novel type of ultra-high vacuum instrument for X-ray reflectometry and spectrometry-related techniques for nanoanalytics by means of synchrotron radiation (SR) has been constructed and commissioned at BESSY II. This versa-tile instrument was developed by the PTB, Germany’s national metrology institute, and includes a 9-axis manipulator that allows for an independent alignment of the samples with respect to all degrees of freedom. In addition, it integrates a rotational and translational movement of several photodiodes as well as a translational movement of a beam-geometry-defining aperture system. Thus, the new instrument enables various analytical techniques based on energy dispersive X-ray detectors such as reference-free X-Ray Fluorescence (XRF) analysis, total-reflection XRF, grazing-incidence XRF, in addition to optional X-Ray Reflectometry (XRR) measurements or polarization-dependent X-ray absorption fine structure analyses (XAFS). Samples having a size of up to (100 × 100) mm{sup 2}; can be analyzed with respect to their mass deposition, elemental, spatial or species composition. Surface contamination, nanolayer composition and thickness, depth pro-file of matrix elements or implants, nanoparticles or buried interfaces as well as molecular orientation of bonds can be accessed. Three technology transfer projects of adapted instruments have enhanced X-Ray Spectrometry (XRS) research activities within Europe at the synchrotron radiation facilities ELETTRA (IAEA) and SOLEIL (CEA/LNE-LNHB) as well as at the X-ray innovation laboratory BLiX (TU Berlin) where different laboratory sources are used. Here, smaller chamber requirements led PTB in cooperation with TU Berlin to develop a modified instrument equipped with a 7-axis manipulator: reduced freedom in the choice of experimental geometry modifications (absence of out-of-SR-plane and reference-free XRS options) has been compensated by encoder-enhanced angular accuracy for GIXRF and XRR.

  1. Application of delayed X-ray spectrometry to the analysis of some rare earth elements

    International Nuclear Information System (INIS)

    Pillay, A.E.; Mboweni, R.C.M.

    1991-01-01

    The capabilities of delayed x-ray spectrometry preceded by isotope-source thermal neutron activation for the specific determination of some rare earth elements (Sm, Eu, Dy, Ho) in small powdered samples was evaluated. The feasibility study relied heavily on the low-energy sensitivity of the detector used. Detection of the delayed x-rays was achieved with a 100-mm 2 Ge detector with the ability to produce optimum photopeak-to-noise ratios. The rare earth elements were chosen on the basis of their inherent favourable nuclear properties for producing a practicable x-ray yield and on the demand for their analysis. Analytical results are presented over a range of concentrations for the elements of interest and the potential of the technique for application to their general routine analysis is discussed. Interferences from the sample matrix can be suppressed to an extent that makes the method almost independent of the matrix. This and other features make the technique a strong rival to conventional activation analysis. (author)

  2. 0.5 to 6 MeV Ar ion induced X-ray emission in view to analytical application

    International Nuclear Information System (INIS)

    Tenorio Castilleros, M.D.

    1979-01-01

    A study of the X-ray emission induced by 0.5 to 6 MeV Ar ions has been realized in view of multielemental analytical applications. The historical development of the use of heavy ion induced X-ray emission in analysis and the theoretical background of inner-shell ionization in heavy ion-atom collisions are described. The emission of non characteristic X-rays and the effects related to the penetration of heavy ions in matter are also related. The experimental part contains a description of the experimental devices and of the X-ray spectra fitting method. Thick target yields as a function of the target Z and the Ar ion energy are reported. The analytical possibilities are examined and an application to the analysis of Si and Cl in cadmium telluride crystals is given [fr

  3. X-ray Lβ215 emission spectrum of Ru in Ru(NH3)6Cl3

    International Nuclear Information System (INIS)

    Perera, R.C.C.; Barth, J.; LaVilla, R.E.; Nordling, C.

    1984-07-01

    One of the broader applications of synchrotron radiation has been to EXAFS studies for material structure determination, i.e., for an analysis of x-ray absorption over an extended energy region beyond a core ionization limit. Studies of the near edge structure (XANES) give a different type of information, characteristic of the local symmetry and electronic configuration of the absorbing atom. This type of information is reflected also in the x-ray emission spectra, in particular for transitions involving the valence levels. Examination of the near edge absorption or the emission spectrum does not require an instrument capable of scanning a wide energy range with high counting statistics, as does EXAFS; the needs are rather for good resolution and a reliable calibration of the energy scale. Some of the problems of near edge spectra were particularly evident in our investigation of Ru-Lβ 2 15 emission from Ru(NH 3 ) 6 Cl 3 . The Ru-Lβ 2 15 emission was measured with a laboratory Rowland circle x-ray spectrometer with a curved quartz (1010) crystal (radius = 22 inches) in a fixed position appropriate to the energy range, and a position sensitive detector which can be positioned along the Rowland circle. The Ru spectrum was excited mainly by Sn-L/sub α/ primary radiation from a Sn anode in a demountable x-ray tube operating at 13 kV and 120 mA. The resolution of the instrument in this region is 1.5 eV. An accurate calibration of the energy scale was conveniently obtained by measuring a reference x-ray emission line in the same instrumental configuration. In the present case the Pd-L/sub α/ emission line at 2838 eV was used to establish the energy scale. The energy dispersion of the instrument was determined from the Cl-K/sub β/ emission spectrum of CH 3 Cl between 2810 eV and 2830 eV and Pd-Lα 1 2 and extrapolated to the energy region of the recorded emission spectrum. 6 references, 1 figure

  4. Discovery of X-Ray Emission from the Galactic Supernova Remnant G32.8-0.1 with Suzaku

    Science.gov (United States)

    Bamba, Aya; Terada, Yukikatsu; Hewitt, John; Petre, Robert; Angelini, Lorella; Safi-Harb, Samar; Zhou, Ping; Bocchino, Fabrizio; Sawada, Makoto

    2016-01-01

    We present the first dedicated X-ray study of the supernova remnant (SNR) G32.8-0.1 (Kes 78) with Suzaku. X-ray emission from the whole SNR shell has been detected for the first time. The X-ray morphology is well correlated with the emission from the radio shell, while anti-correlated with the molecular cloud found in the SNR field. The X-ray spectrum shows not only conventional low-temperature (kT approximately 0.6 kiloelectronvolts) thermal emission in a nonequilibrium ionization state, but also a very high-temperature (approximately 3.4 kiloelectronvolts) component with a very low ionization timescale (approximately 2.7 times 10 (sup 9) per cubic centimeter per second), or a hard nonthermal component with a photon index Gamma approximately equal to 2.3. The average density of the low-temperature plasma is rather low, of the order of 10 (sup -3) - 10 (sup -2) per cubic centimeter, implying that this SNR is expanding into a low-density cavity. We discuss the X-ray emission of the SNR, also detected in teraelectronvolts with H.E.S.S. (High Energy Stereoscopic System), together with multi-wavelength studies of the remnant and other gamma-ray emitting SNRs, such as W28 and RCW 86. Analysis of a time-variable source, 2XMM J185114.3-000004, found in the northern part of the SNR, is also reported for the first time. Rapid time variability and a heavily absorbed hard-X-ray spectrum suggest that this source could be a new supergiant fast X-ray transient.

  5. Highly ionized copper contribution to the soft X-ray emission in a plasma focus device

    Energy Technology Data Exchange (ETDEWEB)

    Zoita, V; Patran, A [Inst. of Physics and Technology of Radiation Devices, Bucharest (Romania); Larour, J [Ecole Polytechnique, Palaiseau (France). Lab. de Physique des Milieux Ionises

    1997-12-31

    In order to discriminate between the contributions of the gas plasma and of the anode (solid or plasma) to the soft X-ray emission in a plasma focus device, a series of experiments was carried out using the following combinations of experimental conditions: various gases, different absorption filters and viewing different regions in front of the centre electrode. The experiments were performed on the IPF-2/20 plasma focus device using the following working gases: helium, neon and helium-argon mixtures. The diagnostics used: magnetic probe for current derivative, PIN diode for the minimum pinch radius detection, PIN diodes for the soft X-ray emission, scintillator-photomultiplier detector for the hard X-ray emission. From the analysis of the various diagnostics data recorded with very good time correlation, it followed that the soft K-ray signals had a strong contribution from optical transitions of the highly ionised Cu (Cu XX to XXII) emitting in the range 0.8-1.3 nm. (author). 7 figs., 9 refs.

  6. Assessment of coal and ash environmental impact with the use of gamma- and X-ray spectrometry

    International Nuclear Information System (INIS)

    Kierzek, J.; Malozewska-Bucko, B.; Bukowski, P.; Parus, J.L.; Ciurapisnki, A.; Zaras, S.; Kunach, B.; Wiland, K.

    1999-01-01

    Gamma-ray spectrometry (GS), energy dispersive X-ray fluorescence (EDXRF) analysis methods and wavelength dispersive X-ray fluorescence (WDXRF) were applied for the studies of some coal components, e.g., sulphur, light and heavy metal element concentrations and naturally occurring radioactive isotope contents. Hundred fifty coal samples originating mostly from eight different coal mines from Upper Silesian Coal Basin and 150 samples of ash obtained from these coal samples in laboratory by total combustion at final temperature of 820 deg C, were analyzed. Such comparative analyses can be helpful in selection of most suitable kind of coal for burning in electrical power and heat plants to minimize the environmental pollution. (author)

  7. Time Variabilities of Solar Wind Ion Fluxes and of X-ray and EUV Emissions from Comet Hyakutake

    Science.gov (United States)

    Neugebauer, M.; Cravens, T.; Lisse, C.; Ipavich, F.; von Steiger, R.; Shah, P.; Armstrong, T.

    1999-01-01

    Observations of X-ray and extreme ultraviolet (EUV) emissions from comet C/Hyakutake 1996 B2 made by the Rontgen X-ray satellite (ROSAT) and the Extreme Ultraviolet Explorer (EUVE) revealed a total X-ray luminosity of about 500 MW.

  8. Proton-induced X-ray emission analysis of Jordanian cigarettes

    International Nuclear Information System (INIS)

    Hallak, A.B.

    1981-01-01

    Proton-induced X-ray emission spectroscopy was applied to determine the concentration of 11 elements in cigaretta tobacco of four brands commercially made in Jordan, and one foreign brand. The results are expressed in absolute amount per cigarette. Cigarette wrapping paper and cigarette smoke were also anlayzed. The significance of some of the elements found in the samples are discussed. (author)

  9. Determination of U, Th and K in bricks by gamma -ray spectrometry, X-ray fluorescence analysis and neutron activation analysis

    Czech Academy of Sciences Publication Activity Database

    Bártová, H.; Kučera, Jan; Musílek, L.; Trojek, T.; Gregorová, E.

    2017-01-01

    Roč. 140, NOV (2017), s. 161-166 ISSN 0969-806X R&D Projects: GA MŠk LM2015056 Institutional support: RVO:61389005 Keywords : Gamma-ray spectrometry * neutron activation analysis * environmental dosimetry Subject RIV: CB - Analytical Chemistry , Separation OBOR OECD: Analytical chemistry Impact factor: 1.315, year: 2016

  10. Commercial Applications of X Ray Spectrometric Techniques

    International Nuclear Information System (INIS)

    Wegrzynek, D.

    2013-01-01

    In the 21st century, the X-ray fluorescence (XRF) technique is widely used in process control, industrial applications and for routine elemental analysis. The technique has a multielement capability capable of detecting elements with Z ≥ 10, with a few instruments capable of detecting also elements with Z ≥ 5. It is characterized by a non-destructive analysis process and relatively good detection limits, typically one part per million, for a wide range of elements. The first commercial XRF instruments were introduced to the market about 50 years ago. They were the wavelength dispersive X ray fluorescence (WDXRF) spectrometers utilizing Bragg’s law and reflection on crystal lattices for sequential elemental analysis of sample composition. The advances made in radiation detector technology, especially the introduction of semiconductor detectors, improvements in signal processing electronics, availability and exponential growth of personal computer market led to invention of energy dispersive X ray fluorescence (EDXRF) technique. The EDXRF is more cost effective as compared to WDXRF. It also allows for designing compact instruments. Such instruments can be easily tailored to the needs of different customers, integrated with industrial installations, and also miniaturized for the purpose of in-situ applications. The versatility of the technique has been confirmed in a spectacular way by using the XRF and X-ray spectrometric techniques, among few others, during the NASA and ESA missions in search for the evidence of life and presence of water on the surface of Mars. The XRF technique has achieved its strong position within the atomic spectroscopy group of analytical techniques not only due to its versatility but also due to relatively low running costs, as compared to the commonly used methods, e.g., atomic absorption spectrometry (AAS) or inductively coupled plasma atomic emission/mass spectrometry (ICP-AES/MS). Presently, the XRF technique together with X ray

  11. Electron and X-ray emission in collisions of multiply charged ions and atoms

    International Nuclear Information System (INIS)

    Woerlee, P.H.

    1979-01-01

    The author presents experimental results of electron and X-ray emission following slow collisions of multiply charged ions and atoms. The aim of the investigation was to study the mechanisms which are responsible for the emission. (G.T.H.)

  12. Trace analysis in cadmium telluride by heavy ion induced X-ray emission and by SIMS

    International Nuclear Information System (INIS)

    Scharager, C.; Stuck, R.; Siffert, P.; Cailleret, J.; Heitz, Ch.; Lagarde, G.; Tenorio, D.

    1979-01-01

    The possibilities of using both selective heavy ion induced X-ray emission and secondary ion mass spectroscopy (SIMS), for the identification of impurities present at low concentrations in cadmium telluride are examined. The relative concentrations of the impurities along CdTe crystals have been determined by exciting the X-ray emission of the elements in several slices with Ar and Kr ions and by comparing the relative characteristic X-ray emission yields. As a consequence of the quasimolecular inner shell ionization mechanism in heavy ion-atom collisions, Ar and Kr ions allow a strong excitation of the main impurities seen by SIMS namely Si, Cl and Ge, As, with only a minor contribution of Cd and Te. From the changes of the concentrations of the various impurities along the crystal, informations about segregation coefficients and compensation can be obtained

  13. First hard X-ray detection of the non-thermal emission around the Arches cluster: morphology and spectral studies with NuSTAR

    DEFF Research Database (Denmark)

    Krivonos, Roman A.; Tomsick, John A.; Bauer, Franz E.

    2014-01-01

    The Arches cluster is a young, densely packed massive star cluster in our Galaxy that shows a high level of star formation activity. The nature of the extended non-thermal X-ray emission around the cluster remains unclear. The observed bright Fe Ku line emission at 6.4 keV from material that is n......The Arches cluster is a young, densely packed massive star cluster in our Galaxy that shows a high level of star formation activity. The nature of the extended non-thermal X-ray emission around the cluster remains unclear. The observed bright Fe Ku line emission at 6.4 keV from material...... and spectrum. The spatial distribution of the hard X-ray emission is found to be consistent with the broad region around the cluster where the 6.4 keV line is observed. The interpretation of the hard X-ray emission within the context of the X-ray reflection model puts a strong constraint on the luminosity...... of the possible illuminating hard X-ray source. The properties of the observed emission are also in broad agreement with the low-energy cosmic-ray proton excitation scenario....

  14. Study of x-ray emission enhancement via high contrast femtosecond laser interacting with solid foil

    International Nuclear Information System (INIS)

    Chen, Liming; Kando, Masaki; Bulanov, S.V.; Koga, James K.; Tajima, Toshiki; Xu M.H.; Yuan X.H.; Li Y.T.; Dong Q.L.; Zhang J.

    2007-01-01

    We studied the hard x-ray emission and the Kα x-ray conversion efficiency (η K ) produced by 60 fs high contrast frequency doubled Ti: sapphire laser pulse focused on Cu foil target. Cu Kα photon emission obtained with second harmonic laser pulse is more intense than the case of fundamental laser pulse. The Cu η K shows strong dependence on laser nonlinearly skewed pulse shape and reaches the maximum value 4x10 -4 with 100 fs negatively skewed pulse. It shows the electron spectrum shaping contribute to the increase of η K . (author)

  15. Obtaining attosecond x-ray pulses using a self-amplified spontaneous emission free electron laser

    Directory of Open Access Journals (Sweden)

    A. A. Zholents

    2005-05-01

    Full Text Available We describe a technique for the generation of a solitary attosecond x-ray pulse in a free-electron laser (FEL, via a process of self-amplified spontaneous emission. In this method, electrons experience an energy modulation upon interacting with laser pulses having a duration of a few cycles within single-period wiggler magnets. Two consecutive modulation sections, followed by compression in a dispersive section, are used to obtain a single, subfemtosecond spike in the electron peak current. This region of the electron beam experiences an enhanced growth rate for FEL amplification. After propagation through a long undulator, this current spike emits a ∼250   attosecond x-ray pulse whose intensity dominates the x-ray emission from the rest of the electron bunch.

  16. Spectral analysis of K-shell X-ray emission of magnesium plasma ...

    Indian Academy of Sciences (India)

    2014-02-06

    Feb 6, 2014 ... the experimental spectra with the synthetic spectra generated using .... user to specify the time duration over which the ionic populations ... ied the dependence of X-ray emission spectrum as a function of laser intensity in the.

  17. X ray emission: a tool and a probe for laser - clusters interaction

    International Nuclear Information System (INIS)

    Prigent, Ch.

    2004-12-01

    In intense laser-cluster interaction, the experimental results show a strong energetic coupling between radiation and matter. We have measured absolute X-ray yields and charge state distributions under well control conditions as a function of physical parameters governing the interaction; namely laser intensity, pulse duration, wavelength or polarization state of the laser light, the size and the species of the clusters (Ar, Kr, Xe). We have highlighted, for the first time, an intensity threshold in the X-ray production very low (∼ 2.10 14 W/cm 2 for a pulse duration of 300 fs) which can results from an effect of the dynamical polarisation of clusters in an intense electric field. A weak dependence with the wavelength (400 nm / 800 nm) on the absolute X-ray yields has been found. Moreover, we have observed a saturation of the X-ray emission probability below a critical cluster size. (author)

  18. Recent measurements of soft X-ray emission from the DPF-1000U facility

    Directory of Open Access Journals (Sweden)

    Surała Władysław

    2015-06-01

    Full Text Available Soft X-ray imaging is a very useful diagnostic technique in plasma-focus (PF experiments. This paper reports results of four experimental sessions which were carried out at the DPF-1000U plasma-focus facility in 2013 and 2014. Over 200 discharges were performed at various experimental conditions. Measurements were taken using two X-ray pinhole cameras with a line of sight perpendicular to the z-axis, at different azimuthal angles (about 20° and 200°, and looking towards the centre of the PF-pinch column. They were equipped with diaphragms 1000 μm or 200–300 μm in diameter and coated with filters of 500 μm Al foil and 10 μm Be foil, respectively. Data on the neutron emission were collected with silver activation counters. For time-resolved measurements the use was made of four PIN diodes equipped with various filters and oriented towards the centre of the PF-column, in the direction perpendicular to the electrode axis. The recorded X-ray images revealed that when the additional gas-puff system is activated during the discharge, the stability of the discharge is improved. The data collected in these experiments confirmed the appearance of a filamentary fine structure in the PF discharges. In the past years the formation of such filaments was observed in many Z-pinch type experiments. Some of the recorded X-ray images have also revealed the appearance of the so-called hot-spots, i.e. small plasma regions of a very intense X-ray emission. Such a phenomenon was observed before in many PF experiments, e.g. in the MAJA-PF device, but it has not been investigated so far in a large facility such as the DPF-1000U. The time-resolved measurements provided the evidence of a time lapse between the X-ray emission from plasma regions located at different distance from the anode surface. The formation of distinct ‘hot-spots’ in different instants of the DPF-1000U discharge was also observed.

  19. X-rays from comets - a surprising discovery

    CERN Document Server

    CERN. Geneva

    2000-01-01

    Comets are kilometre-size aggregates of ice and dust, which remained from the formation of the solar system. It was not obvious to expect X-ray emission from such objects. Nevertheless, when comet Hyakutake (C/1996 B2) was observed with the ROSAT X-ray satellite during its close approach to Earth in March 1996, bright X-ray emission from this comet was discovered. This finding triggered a search in archival ROSAT data for comets, which might have accidentally crossed the field of view during observations of unrelated targets. To increase the surprise even more, X-ray emission was detected from four additional comets, which were optically 300 to 30 000 times fainter than Hyakutake. For one of them, comet Arai (C/1991 A2), X-ray emission was even found in data which were taken six weeks before the comet was optically discovered. These findings showed that comets represent a new class of celestial X-ray sources. The subsequent detection of X-ray emission from several other comets in dedicated observations confir...

  20. DISCOVERY OF X-RAY EMISSION FROM THE GALACTIC SUPERNOVA REMNANT G32.8-0.1 WITH SUZAKU

    Energy Technology Data Exchange (ETDEWEB)

    Bamba, Aya; Sawada, Makoto [Department of Physics and Mathematics, Aoyama Gakuin University 5-10-1 Fuchinobe Chuo-ku, Sagamihara, Kanagawa 252-5258 (Japan); Terada, Yukikatsu [Department of Physics, Science, Saitama University, Sakura, Saitama 338-8570 (Japan); Hewitt, John; Petre, Robert; Angelini, Lorella [NASA Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Safi-Harb, Samar [Department of Physics and Astronomy, University of Manitoba, Winnipeg MB R3T 2N2 (Canada); Zhou, Ping [Department of Astronomy, Nanjing University, Nanjing 210093 (China); Bocchino, Fabrizio [INAF—Osservatorio Astronomico di Palermo, Piazza del Parlamento 1, I-90134, Palermo (Italy)

    2016-02-10

    We present the first dedicated X-ray study of the supernova remnant (SNR) G32.8−0.1 (Kes 78) with Suzaku. X-ray emission from the whole SNR shell has been detected for the first time. The X-ray morphology is well correlated with the emission from the radio shell, while anti-correlated with the molecular cloud found in the SNR field. The X-ray spectrum shows not only conventional low-temperature (kT ∼ 0.6 keV) thermal emission in a non-equilibrium ionization state, but also a very high-temperature (kT ∼ 3.4 keV) component with a very low ionization timescale (∼2.7 × 10{sup 9} cm{sup −3} s), or a hard nonthermal component with a photon index Γ ∼ 2.3. The average density of the low-temperature plasma is rather low, of the order of 10{sup −3}–10{sup −2} cm{sup −3}, implying that this SNR is expanding into a low-density cavity. We discuss the X-ray emission of the SNR, also detected in TeV with H.E.S.S., together with multi-wavelength studies of the remnant and other gamma-ray emitting SNRs, such as W28 and RCW 86. Analysis of a time-variable source, 2XMM J185114.3−000004, found in the northern part of the SNR, is also reported for the first time. Rapid time variability and a heavily absorbed hard-X-ray spectrum suggest that this source could be a new supergiant fast X-ray transient.

  1. LabVIEW interface with Tango control system for a multi-technique X-ray spectrometry IAEA beamline end-station at Elettra Sincrotrone Trieste

    Energy Technology Data Exchange (ETDEWEB)

    Wrobel, P.M. [Physics Section, Nuclear Science and Instrumentation Laboratory (NSIL), IAEA Laboratories, A-2444 Seibersdorf (Austria); AGH University of Science and Technology, Faculty of Physics and Applied Computer Science, al. A. Mickiewicza 30, 30-059 Krakow (Poland); Bogovac, M. [Physics Section, Nuclear Science and Instrumentation Laboratory (NSIL), IAEA Laboratories, A-2444 Seibersdorf (Austria); Sghaier, H. [Physics Section, Nuclear Science and Instrumentation Laboratory (NSIL), IAEA Laboratories, A-2444 Seibersdorf (Austria); Institut Superieur d’Informatique et de Mathematiques de Monastir (ISIMM), Departement de technologie, 5000 Monastir (Tunisia); Leani, J.J. [Physics Section, Nuclear Science and Instrumentation Laboratory (NSIL), IAEA Laboratories, A-2444 Seibersdorf (Austria); IFEG – CONICET, Facultad de Matematica Astronomia y Fisica, Universidad Nacional de Cordoba, 5000 Cordoba (Argentina); Migliori, A.; Padilla-Alvarez, R. [Physics Section, Nuclear Science and Instrumentation Laboratory (NSIL), IAEA Laboratories, A-2444 Seibersdorf (Austria); Czyzycki, M. [Physics Section, Nuclear Science and Instrumentation Laboratory (NSIL), IAEA Laboratories, A-2444 Seibersdorf (Austria); AGH University of Science and Technology, Faculty of Physics and Applied Computer Science, al. A. Mickiewicza 30, 30-059 Krakow (Poland); Osan, J. [Physics Section, Nuclear Science and Instrumentation Laboratory (NSIL), IAEA Laboratories, A-2444 Seibersdorf (Austria); Environmental Physics Department, Hungarian Academy of Sciences Centre for Energy Research, Konkoly-Thege M. út 29-33., H-1121 Budapest (Hungary); Kaiser, R.B. [Physics Section, Nuclear Science and Instrumentation Laboratory (NSIL), IAEA Laboratories, A-2444 Seibersdorf (Austria); and others

    2016-10-11

    A new synchrotron beamline end-station for multipurpose X-ray spectrometry applications has been recently commissioned and it is currently accessible by end-users at the XRF beamline of Elettra Sincrotrone Trieste. The end-station consists of an ultra-high vacuum chamber that includes as main instrument a seven-axis motorized manipulator for sample and detectors positioning, different kinds of X-ray detectors and optical cameras. The beamline end-station allows performing measurements in different X-ray spectrometry techniques such as Microscopic X-Ray Fluorescence analysis (µXRF), Total Reflection X-Ray Fluorescence analysis (TXRF), Grazing Incidence/Exit X-Ray Fluorescence analysis (GI-XRF/GE-XRF), X-Ray Reflectometry (XRR), and X-Ray Absorption Spectroscopy (XAS). A LabVIEW Graphical User Interface (GUI) bound with Tango control system consisted of many custom made software modules is utilized as a user-friendly tool for control of the entire end-station hardware components. The present work describes this advanced Tango and LabVIEW software platform that utilizes in an optimal synergistic manner the merits and functionality of these well-established programming and equipment control tools. - Highlights: • A new methodology for control of a synchrotron beamline end-station is shown. • The new control system comprises a novel binding of Tango control system with LabVIEW interface. • The reliability of the control system is demonstrated by examples of analytical applications.

  2. Soft X-ray emission from the radio pulsar PSR 0656 + 14

    Science.gov (United States)

    Cordova, F. A.; Middleditch, J.; Hjellming, R. M.; Mason, K. O.

    1989-01-01

    A radio source with a flux density of a few mJy was found in the error region of the soft X-ray source E0656 + 14, and identified as the radio pulsar PSR 0656 + 14. The radio source has a steep, nonthermal spectrum and a high degree of linear (62 percent) and circular (19 percent) polarization. The X-ray spectrum of the pulsar is among the softest sources observed with the Einstein Observatory. The X-ray data taken with the Einstein imaging proportional counter (IPC) permit a range of blackbody temperatures of 3-6 x 10 to the 5th K, and an equivalent column density of hydrogen smaller than 4 x 10 to the 20th/sq cm. If the assumption is made that the X-ray flux is thermal radiation from surface of the neutron star, then the pulsar must be at a distance smaller than 550 pc, consistent with the low dispersion measure of PSR 0656 + 14. The X-ray timing data suggest that the X-ray emission is modulated at the pulsar's 0.385-s spin period with an amplitude of 18 percent + or - 6 percent, and that there is a 0.0002 probability that this is spurious. It was noted that PSR 0656 + 14 is close to the geometric center of a 20-deg diameter soft X-ray emitting ring called the Gemini-Monoceros enhancement. The close distance of the pulsar, together with its relatively young age of 1.1 x 10 to the 5th yr, makes it possible that the ring is a supernova remnant from the explosion of the pulsar's progenitor. A radio source extending over a region 1.2 to 3.3 arcmin south of the pulsar is a candidate for association with the pulsar.

  3. Soft X-ray emission from the radio pulsar PSR 0656 + 14

    International Nuclear Information System (INIS)

    Cordova, F.A.; Middleditch, J.; Hjellming, R.M.; Mason, K.O.

    1989-01-01

    A radio source with a flux density of a few mJy was found in the error region of the soft X-ray source E0656 + 14, and identified as the radio pulsar PSR 0656 + 14. The radio source has a steep, nonthermal spectrum and a high degree of linear (62%) and circular (19%) polarization. The X-ray spectrum of the pulsar is among the softest sources observed with the Einstein Observatory. The X-ray data taken with the Einstein imaging proportional counter (IPC) permit a range of blackbody temperatures of 3-6 x 10 to the 5th K, and an equivalent column density of hydrogen smaller than 4 x 10 to the 20th/sq cm. If the assumption is made that the X-ray flux is thermal radiation from surface of the neutron star, then the pulsar must be at a distance smaller than 550 pc, consistent with the low dispersion measure of PSR 0656 + 14. The X-ray timing data suggest that the X-ray emission is modulated at the pulsar's 0.385-s spin period with an amplitude of 18% + or - 6%, and that there is a 0.0002 probability that this is spurious. It was noted that PSR 0656 + 14 is close to the geometric center of a 20-deg diameter soft X-ray emitting ring called the Gemini-Monoceros enhancement. The close distance of the pulsar, together with its relatively young age of 1.1 x 10 to the 5th yr, makes it possible that the ring is a supernova remnant from the explosion of the pulsar's progenitor. A radio source extending over a region 1.2 to 3.3 arcmin south of the pulsar is a candidate for association with the pulsar. 46 refs

  4. Proton-Induced X-Ray Emission Analysis of Crematorium Emissions

    Science.gov (United States)

    Ali, Salina; Nadareski, Benjamin; Yoskowitz, Joshua; Labrake, Scott; Vineyard, Michael

    2014-09-01

    There has been considerable debate in recent years about possible mercury emissions from crematoria due to amalgam tooth restorations. We have performed a proton-induced X-ray emission (PIXE) analysis of aerosol and soil samples taken near the Vale Cemetery Crematorium in Schenectady, NY, to address this concern. The aerosol samples were collected on the roof of the crematorium using a nine-stage, cascade impactor that separates the particulate matter by aerodynamic diameter and deposits it onto thin Kapton foils. The soil samples were collected at several different distances from the crematorium and compressed into pellets with a hydraulic press. The Kapton foils containing the aerosol samples and the soil pellets were bombarded with 2.2-MeV protons from the 1.1-MV tandem Pelletron accelerator in the Union College Ion-Beam Analysis Laboratory. We measured significant concentrations of sulfur, phosphorus, potassium, calcium, and iron, but essentially no mercury in the aerosol samples. The lower limit of detection for airborne mercury in this experiment was approximately 0.2 ng / m3. The PIXE analysis of the soil samples showed the presence of elements commonly found in soil (Si, K, Ca, Ti, Mn, Fe), but no trace of mercury. There has been considerable debate in recent years about possible mercury emissions from crematoria due to amalgam tooth restorations. We have performed a proton-induced X-ray emission (PIXE) analysis of aerosol and soil samples taken near the Vale Cemetery Crematorium in Schenectady, NY, to address this concern. The aerosol samples were collected on the roof of the crematorium using a nine-stage, cascade impactor that separates the particulate matter by aerodynamic diameter and deposits it onto thin Kapton foils. The soil samples were collected at several different distances from the crematorium and compressed into pellets with a hydraulic press. The Kapton foils containing the aerosol samples and the soil pellets were bombarded with 2.2-Me

  5. Radioactive implant induced x-ray emission technique for noninvasive determination of iodine content in thyroid: experimental study

    Energy Technology Data Exchange (ETDEWEB)

    Amano, R; Ando, A; Hiraki, T [Kanazawa Univ. (Japan). School of Allied Medical Professions; Tonami, N; Hisada, K [Kanazawa Univ. (Japan). School of Medicine

    1984-02-01

    A new technique, radioactive implant x-ray emission spectrometry to determine the in vivo iodine content of the human thyroid is proposed. The variations of counting rate and effective excitation efficiencies of I Ksub(..cap alpha..) (28.6 keV) with iodine content, thyroid volume and skin-thyroid distance were studied for the /sup 201/Tl source to examine the properties of excitation and photon attenuation. As a result, the gland depth and volume could be estimated from the peak ratios of 30.7 keV/167.6 keV and 28.6 keV/167.6 keV. Using a 1 MBq /sup 201/Tl implant source, the detectable minimum iodine concentration found was approximately 70 ..mu..g/g for 2000 s measuring time in the phantom experiment. The effectiveness of the RIXE technique is discussed. It was concluded that the /sup 201/Tl RIXE spectrometry might serve to determine the in vivo iodine content of the human thyroid.

  6. Radioactive implant induced x-ray emission technique for noninvasive determination of iodine content in thyroid: experimental study

    Energy Technology Data Exchange (ETDEWEB)

    Amano, R; Tonami, N; Ando, A; Hiraki, T; Hisada, K

    1984-02-01

    A new technique, radioactive implant x-ray emission spectrometry to determine the in vivo iodine content of the human thyroid is proposed. The variations of counting rate and effective excitation efficiencies of I K alpha (28.6 keV) with iodine content, thyroid volume and skin-thyroid distance were studied for the /sup 201/Tl source to examine the properties of excitation and photon attenuation. As a result, the gland depth and volume could be estimated from the peak ratios of 30.7 keV/167.6 keV and 28.6 keV/167.6 keV. Using a 1 MBq /sup 201/Tl implant source, the detectable minimum iodine concentration found was approximately 70 micrograms/g for 2000 s measuring time in the phantom experiment. The effectiveness of the RIXE technique is discussed. It was concluded that the /sup 201/Tl RIXE spectrometry might serve to determine the in vivo iodine content of the human thyroid.

  7. Combined analysis of 1,3-benzodioxoles by crystalline sponge X-ray crystallography and laser desorption ionization mass spectrometry.

    Science.gov (United States)

    Hayashi, Yukako; Ohara, Kazuaki; Taki, Rika; Saeki, Tomomi; Yamaguchi, Kentaro

    2018-03-12

    The crystalline sponge (CS) method, which employs single-crystal X-ray diffraction to determine the structure of an analyte present as a liquid or an oil and having a low melting point, was used in combination with laser desorption ionization mass spectrometry (LDI-MS). 1,3-Benzodioxole derivatives were encapsulated in CS and their structures were determined by combining X-ray crystallography and MS. After the X-ray analysis, the CS was subjected to imaging mass spectrometry (IMS) with an LDI spiral-time-of-flight mass spectrometer (TOF-MS). The ion detection area matched the microscopic image of the encapsulated CS. In addition, the accumulated 1D mass spectra showed that fragmentation of the guest molecule (hereafter, guest) can be easily visualized without any interference from the fragment ions of CS except for two strong ion peaks derived from the tridentate ligand TPT (2,4,6-tris(4-pyridyl)-1,3,5-triazine) of the CS and its fragment. X-ray analysis clearly showed the presence of the guest as well as the π-π, CH-halogen, and CH-O interactions between the guest and the CS framework. However, some guests remained randomly diffused in the nanopores of CS. In addition, the detection limit was less than sub-pmol order based on the weight and density of CS determined by X-ray analysis. Spectroscopic data, such as UV-vis and NMR, also supported the encapsulation of the guest through the interaction between the guest and CS components. The results denote that the CS-LDI-MS method, which combines CS, X-ray analysis and LDI-MS, is effective for structure determination.

  8. Optical and X-ray studies of Compact X-ray Binaries in NGC 5904

    Science.gov (United States)

    Bhalotia, Vanshree; Beck-Winchatz, Bernhard

    2018-06-01

    Due to their high stellar densities, globular cluster systems trigger various dynamical interactions, such as the formation of compact X-ray binaries. Stellar collisional frequencies have been correlated to the number of X-ray sources detected in various clusters and we hope to measure this correlation for NGC 5904. Optical fluxes of sources from archival HST images of NGC 5904 have been measured using a DOLPHOT PSF photometry in the UV, optical and near-infrared. We developed a data analysis pipeline to process the fluxes of tens of thousands of objects using awk, python and DOLPHOT. We plot color magnitude diagrams in different photometric bands in order to identify outliers that could be X-ray binaries, since they do not evolve the same way as singular stars. Aligning previously measured astrometric data for X-ray sources in NGC 5904 from Chandra with archival astrometric data from HST will filter out the outlier objects that are not X-ray producing, and provide a sample of compact binary systems that are responsible for X-ray emission in NGC 5904. Furthermore, previously measured X-ray fluxes of NGC 5904 from Chandra have also been used to measure the X-ray to optical flux ratio and identify the types of compact X-ray binaries responsible for the X-ray emissions in NGC 5904. We gratefully acknowledge the support from the Illinois Space Grant Consortium.

  9. Recent trends in total reflection X-ray fluorescence spectrometry for biological applications

    International Nuclear Information System (INIS)

    Szoboszlai, Norbert; Polgari, Zsofia; Mihucz, Victor G.; Zaray, Gyula

    2009-01-01

    This review is focused on the application of total reflection X-ray fluorescence (TXRF) spectrometry in the field of biological research. In the last decade, most papers were published by authors who applied laboratory-scale TXRF equipments. The application of synchrotron radiation as excitation source (SR-TXRF) shows a slowly increasing tendency. In the cited papers the micro-, trace and multielement capability of these TXRF techniques was demonstrated in the clinical and medical laboratory practice, as well as in various plant physiological studies. For speciation of elements in biological matrices, the TXRF was used as element specific detector following an off-line separation step (e.g., thin layer chromatography, high performance liquid chromatography), however, these off-line methods are not competitive with the on-line coupled HPLC-inductively coupled plasma mass spectrometry

  10. Search for very high-energy gamma-ray emission from the microquasar Cygnus X-1 with the MAGIC telescopes

    Science.gov (United States)

    Ahnen, M. L.; Ansoldi, S.; Antonelli, L. A.; Arcaro, C.; Babić, A.; Banerjee, B.; Bangale, P.; Barres de Almeida, U.; Barrio, J. A.; Becerra González, J.; Bednarek, W.; Bernardini, E.; Berti, A.; Bhattacharyya, W.; Biasuzzi, B.; Biland, A.; Blanch, O.; Bonnefoy, S.; Bonnoli, G.; Carosi, R.; Carosi, A.; Chatterjee, A.; Colin, P.; Colombo, E.; Contreras, J. L.; Cortina, J.; Covino, S.; Cumani, P.; da Vela, P.; Dazzi, F.; de Angelis, A.; de Lotto, B.; de Oña Wilhelmi, E.; di Pierro, F.; Doert, M.; Domínguez, A.; Dominis Prester, D.; Dorner, D.; Doro, M.; Einecke, S.; Eisenacher Glawion, D.; Elsaesser, D.; Engelkemeier, M.; Fallah Ramazani, V.; Fernández-Barral, A.; Fidalgo, D.; Fonseca, M. V.; Font, L.; Fruck, C.; Galindo, D.; García López, R. J.; Garczarczyk, M.; Gaug, M.; Giammaria, P.; Godinović, N.; Gora, D.; Guberman, D.; Hadasch, D.; Hahn, A.; Hassan, T.; Hayashida, M.; Herrera, J.; Hose, J.; Hrupec, D.; Ishio, K.; Konno, Y.; Kubo, H.; Kushida, J.; Kuveždić, D.; Lelas, D.; Lindfors, E.; Lombardi, S.; Longo, F.; López, M.; Maggio, C.; Majumdar, P.; Makariev, M.; Maneva, G.; Manganaro, M.; Mannheim, K.; Maraschi, L.; Mariotti, M.; Martínez, M.; Mazin, D.; Menzel, U.; Minev, M.; Mirzoyan, R.; Moralejo, A.; Moreno, V.; Moretti, E.; Neustroev, V.; Niedzwiecki, A.; Nievas Rosillo, M.; Nilsson, K.; Ninci, D.; Nishijima, K.; Noda, K.; Nogués, L.; Paiano, S.; Palacio, J.; Paneque, D.; Paoletti, R.; Paredes, J. M.; Paredes-Fortuny, X.; Pedaletti, G.; Peresano, M.; Perri, L.; Persic, M.; Prada Moroni, P. G.; Prandini, E.; Puljak, I.; Garcia, J. R.; Reichardt, I.; Rhode, W.; Ribó, M.; Rico, J.; Righi, C.; Saito, T.; Satalecka, K.; Schroeder, S.; Schweizer, T.; Sitarek, J.; Šnidarić, I.; Sobczynska, D.; Stamerra, A.; Strzys, M.; Surić, T.; Takalo, L.; Tavecchio, F.; Temnikov, P.; Terzić, T.; Tescaro, D.; Teshima, M.; Torres, D. F.; Torres-Albà, N.; Treves, A.; Vanzo, G.; Vazquez Acosta, M.; Vovk, I.; Ward, J. E.; Will, M.; Zarić, D.; MAGIC Collaboration; Bosch-Ramon, V.; Pooley, G. G.; Trushkin, S. A.; Zanin, R.

    2017-12-01

    The microquasar Cygnus X-1 displays the two typical soft and hard X-ray states of a black hole transient. During the latter, Cygnus X-1 shows a one-sided relativistic radio-jet. Recent detection of the system in the high energy (HE; E ≳ 60 MeV) gamma-ray range with Fermi-LAT associates this emission with the outflow. Former MAGIC observations revealed a hint of flaring activity in the very high-energy (VHE; E ≳ 100 GeV) regime during this X-ray state. We analyse ∼97 h of Cygnus X-1 data taken with the MAGIC telescopes between July 2007 and October 2014. To shed light on the correlation between hard X-ray and VHE gamma rays as previously suggested, we study each main X-ray state separately. We perform an orbital phase-folded analysis to look for variability in the VHE band. Additionally, to place this variability behaviour in a multiwavelength context, we compare our results with Fermi-LAT, AGILE, Swift-BAT, MAXI, RXTE-ASM, AMI and RATAN-600 data. We do not detect Cygnus X-1 in the VHE regime. We establish upper limits for each X-ray state, assuming a power-law distribution with photon index Γ = 3.2. For steady emission in the hard and soft X-ray states, we set integral upper limits at 95 per cent confidence level for energies above 200 GeV at 2.6 × 10-12 photons cm-2 s-1 and 1.0 × 10-11 photons cm-2 s-1, respectively. We rule out steady VHE gamma-ray emission above this energy range, at the level of the MAGIC sensitivity, originating in the interaction between the relativistic jet and the surrounding medium, while the emission above this flux level produced inside the binary still remains a valid possibility.

  11. Trace element analysis in liquids by proton induced x-ray emission

    International Nuclear Information System (INIS)

    Deconninck, G.

    Proton induced x-ray emission (PIXE) from liquid has been developed for quantitative and simultaneous analysis of trace elements. Liquid drops and trickles are bombarded at atmospheric pressure, x-rays are detected in a non dispersive Si(Li) solid state detector. Absolute determinations are made by comparison with standard solutions. Detection limits in a 5 minutes run are in the ppm range for a single drop (0.05 ml). The application of this technique to the determination of trace elements in biological liquids is investigated (Cr, Mn, Fe, Co, Ni, Cu, Zn, in plant extracts, haemocyanine, albumins...). (author)

  12. Single particle transfer for quantitative analysis with total-reflection X-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Esaka, Fumitaka; Esaka, Konomi T.; Magara, Masaaki; Sakurai, Satoshi; Usuda, Shigekazu; Watanabe, Kazuo

    2006-01-01

    The technique of single particle transfer was applied to quantitative analysis with total-reflection X-ray fluorescence (TXRF) spectrometry. The technique was evaluated by performing quantitative analysis of individual Cu particles with diameters between 3.9 and 13.2 μm. The direct quantitative analysis of the Cu particle transferred onto a Si carrier gave a discrepancy between measured and calculated Cu amounts due to the absorption effects of incident and fluorescent X-rays within the particle. By the correction for the absorption effects, the Cu amounts in individual particles could be determined with the deviation within 10.5%. When the Cu particles were dissolved with HNO 3 solution prior to the TXRF analysis, the deviation was improved to be within 3.8%. In this case, no correction for the absorption effects was needed for quantification

  13. Periodicities in the X-ray Emission from the Solar Corona: SphinX and SOXS Observations

    Science.gov (United States)

    Steślicki, M.; Awasthi, A. K.; Gryciuk, M.; Jain, R.

    The structure and evolution of the solar magnetic field is driven by a magnetohydrodynamic dynamo operating in the solar interior, which induces various solar activities that exhibit periodic variations on different timescales. Therefore, probing the periodic nature of emission originating from the solar corona may provide insights of the convection-zone-photosphere-corona coupling processes. We present the study of the mid-range periodicities, between rotation period (˜27 days) and the Schwabe cycle period (˜11 yr), in the solar soft X-ray emission, based on the data obtained by two instruments: SphinX and SOXS in various energy bands.

  14. Angle-resolved X-ray fluorescence spectrometry using synchrotron radiation at ELSA

    International Nuclear Information System (INIS)

    Schmitt, W.; Rothe, J.; Hormes, J.; Gries, W.H.

    1994-01-01

    Measurements on the centroid depth of ion-implanted phosphorus-in-silicon specimen by the method of angle-resolved, self-ratio X-ray fluorescence spectrometry (AR/SR/XFS) have been carried out using 'white' synchrotron radiation (SR). The measurements were performed using a modified wavelength-dispersive fluorescence spectrometer. Problems due to the use of SR, like carbonaceous specimen contamination and sample heating were overcome by flooding the specimen chamber with helium and by pre-absorbing the non-exciting parts of the incident SR with suitable filters, respectively. The decaying primary intensity was monitored by measuring the compensation current of the photoelectrons emitted from a tungsten wire stretched across the primary beam. Results have been obtained for specimen with dose density levels of 10 16 cm -2 and 3x10 15 cm -2 . (orig.)

  15. X-ray emission as a potential hazard during ultrashort pulse laser material processing

    Science.gov (United States)

    Legall, Herbert; Schwanke, Christoph; Pentzien, Simone; Dittmar, Günter; Bonse, Jörn; Krüger, Jörg

    2018-06-01

    In laser machining with ultrashort laser pulses unwanted X-ray radiation in the keV range can be generated when a critical laser intensity is exceeded. Even if the emitted X-ray dose per pulse is low, high laser repetition rates can lead to an accumulation of X-ray doses beyond exposure safety limits. For 925 fs pulse duration at a center wavelength of 1030 nm, the X-ray emission was investigated up to an intensity of 2.6 × 1014 W/cm2. The experiments were performed in air with a thin disk laser at a repetition rate of 400 kHz. X-ray spectra and doses were measured for various planar target materials covering a wide range of the periodic table from aluminum to tungsten. Without radiation shielding, the measured radiation doses at this high repetition rate clearly exceed the regulatory limits. Estimations for an adequate radiation shielding are provided.

  16. X-ray emission from a nanosecond-pulse discharge in an inhomogeneous electric field at atmospheric pressure

    International Nuclear Information System (INIS)

    Zhang Cheng; Shao Tao; Ren Chengyan; Zhang Dongdong; Tarasenko, Victor; Kostyrya, Igor D.; Ma Hao; Yan Ping

    2012-01-01

    This paper describes experimental studies of the dependence of the X-ray intensity on the anode material in nanosecond high-voltage discharges. The discharges were generated by two nanosecond-pulse generators in atmospheric air with a highly inhomogeneous electric field by a tube-plate gap. The output pulse of the first generator (repetitive pulse generator) has a rise time of about 15 ns and a full width at half maximum of 30–40 ns. The output of the second generator (single pulse generator) has a rise time of about 0.3 ns and a full width at half maximum of 1 ns. The electrical characteristics and the X-ray emission of nanosecond-pulse discharge in atmospheric air are studied by the measurement of voltage-current waveforms, discharge images, X-ray count and dose. Our experimental results showed that the anode material rarely affects electrical characteristics, but it can significantly affect the X-ray density. Comparing the density of X-rays, it was shown that the highest x-rays density occurred in the diffuse discharge in repetitive pulse mode, then the spark discharge with a small air gap, and then the corona discharge with a large air gap, in which the X-ray density was the lowest. Therefore, it could be confirmed that the bremsstrahlung at the anode contributes to the X-ray emission from nanosecond-pulse discharges.

  17. X-ray emission from reverse-shocked ejecta in supernova remnants

    Science.gov (United States)

    Cioffi, Denis F.; Mckee, Christopher F.

    1990-01-01

    A simple physical model of the dynamics of a young supernova remnant is used to derive a straightforward kinematical description of the reverse shock. With suitable approximations, formulae can then be developed to give the X-ray emission of the reverse-shocked ejecta. The results are found to agree favorably with observations of SN1006.

  18. Miniature x-ray point source for alignment and calibration of x-ray optics

    International Nuclear Information System (INIS)

    Price, R.H.; Boyle, M.J.; Glaros, S.S.

    1977-01-01

    A miniature x-ray point source of high brightness similar to that of Rovinsky, et al. is described. One version of the x-ray source is used to align the x-ray optics on the Argus and Shiva laser systems. A second version is used to determine the spatial and spectral transmission functions of the x-ray optics. The spatial and spectral characteristics of the x-ray emission from the x-ray point source are described. The physical constraints including size, intensity and thermal limitations, and useful lifetime are discussed. The alignment and calibration techniques for various x-ray optics and detector combinations are described

  19. Measurement of anisotropic soft X-ray emission during radio-frequency current drive in the JFT-2M tokamak

    International Nuclear Information System (INIS)

    Kawashima, Hisato; Matoba, Tohru; Hoshino, Katsumichi; Kawakami, Tomohide; Yamamoto, Takumi; Hasegawa, Mitsuru; Fuchs, Gerhard; Uesugi, Yoshihiko.

    1994-01-01

    A new vertical soft X-ray pulse height analyzer (PHA) system and a tangential PHA system were used to measure the anisotropy of soft X-ray emission during lower-hybrid current drive (LHCD) and also during current drive by the combination of LHCD and electron cyclotron resonance heating (ECRH) in the JFT-2M tokamak. The strong soft X-ray emission was measured in the parallel forward direction during LHCD. When ECRH was applied during LHCD, the perpendicular emission was enhanced. The high-energy electron velocity distribution was evaluated by comparing the measured and calculated X-ray spectra. The distribution form was consistent with the theoretical prediction based on the electron Landau damping of lower-hybrid waves and the electron cyclotron damping of electron cyclotron waves for reasonable energy ranges. (author)

  20. Is low-energy-ion bombardment generated X-ray emission a secondary mutational source to ion-beam-induced genetic mutation?

    Energy Technology Data Exchange (ETDEWEB)

    Thongkumkoon, P. [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Thailand Center of Excellence in Physics, Commission on Higher Education, 328 Si Ayutthaya Road, Bangkok 10400 (Thailand); Prakrajang, K. [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Faculty of Science, Maejo University, Chiang Mai 50290 (Thailand); Thopan, P.; Yaopromsiri, C. [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Suwannakachorn, D. [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Thailand Center of Excellence in Physics, Commission on Higher Education, 328 Si Ayutthaya Road, Bangkok 10400 (Thailand); Yu, L.D., E-mail: yuld@fnrf.science.cmu.ac.th [Plasma and Beam Physics Research Facility, Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200 (Thailand); Thailand Center of Excellence in Physics, Commission on Higher Education, 328 Si Ayutthaya Road, Bangkok 10400 (Thailand)

    2013-07-15

    Highlights: ► Detected X-ray emission from metal, plastic and biological samples. ► Characteristic X-ray emission was detected from metal but not from non-metals. ► Low-energy ion bombarded bacteria held in different sample holders. ► Bacteria held in metal holder had higher mutation rate than in plastic holder. ► Ion-beam-induced X-ray from biological sample is not a basic mutation source. -- Abstract: Low-energy ion beam biotechnology has achieved tremendous successes in inducing crop mutation and gene transfer. However, mechanisms involved in the related processes are not yet well understood. In ion-beam-induced mutation, ion-bombardment-produced X-ray has been proposed to be one of the secondary mutation sources, but the speculation has not yet been experimentally tested. We carried out this investigation to test whether the low-energy ion-beam-produced X-ray was a source of ion-beam-induced mutation. In the investigation, X-ray emission from 29-keV nitrogen- or argon- ion beam bombarded bacterial Escherichia coli (E. coli) cells held in a metal or plastic sample holder was in situ detected using a highly sensitive X-ray detector. The ion beam bombarded bacterial cells held in different material holders were observed for mutation induction. The results led to a conclusion that secondary X-ray emitted from ion-beam-bombarded biological living materials themselves was not a, or at least a negligible, mutational source, but the ion-beam-induced X-ray emission from the metal that made the sample holder could be a source of mutation.

  1. Is low-energy-ion bombardment generated X-ray emission a secondary mutational source to ion-beam-induced genetic mutation?

    International Nuclear Information System (INIS)

    Thongkumkoon, P.; Prakrajang, K.; Thopan, P.; Yaopromsiri, C.; Suwannakachorn, D.; Yu, L.D.

    2013-01-01

    Highlights: ► Detected X-ray emission from metal, plastic and biological samples. ► Characteristic X-ray emission was detected from metal but not from non-metals. ► Low-energy ion bombarded bacteria held in different sample holders. ► Bacteria held in metal holder had higher mutation rate than in plastic holder. ► Ion-beam-induced X-ray from biological sample is not a basic mutation source. -- Abstract: Low-energy ion beam biotechnology has achieved tremendous successes in inducing crop mutation and gene transfer. However, mechanisms involved in the related processes are not yet well understood. In ion-beam-induced mutation, ion-bombardment-produced X-ray has been proposed to be one of the secondary mutation sources, but the speculation has not yet been experimentally tested. We carried out this investigation to test whether the low-energy ion-beam-produced X-ray was a source of ion-beam-induced mutation. In the investigation, X-ray emission from 29-keV nitrogen- or argon- ion beam bombarded bacterial Escherichia coli (E. coli) cells held in a metal or plastic sample holder was in situ detected using a highly sensitive X-ray detector. The ion beam bombarded bacterial cells held in different material holders were observed for mutation induction. The results led to a conclusion that secondary X-ray emitted from ion-beam-bombarded biological living materials themselves was not a, or at least a negligible, mutational source, but the ion-beam-induced X-ray emission from the metal that made the sample holder could be a source of mutation

  2. Multielement analysis of minerals from Madagascar by X-ray emission induced by protons and gamma rays

    International Nuclear Information System (INIS)

    Rakotoarisoa, C.

    1990-12-01

    This study is a part of a large multidisciplinary program for the study of soil formation in the south east of Madagascar near the uranothorianite deposit of Tranomaro explaining the particular interest for rare earths, uranium and thorium. X-ray emission principles and physical processes of a X-ray spectra are briefly recalled. The choice of analysis method depends upon sensitivity simplicity and rapidity. Experimental techniques are described and results obtained are discussed. Methods used for qualitative and quantitative interpretation of spectra are exposed. In conclusion performance and limits of the method are examined [fr

  3. Investigation of polyelectrolytes by total reflection x-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Varga, I.; Nagy, M.

    2000-01-01

    Water soluble polyelectrolyte samples containing mono-, bi- and trivalent metal ions were investigated without any pretreatment. Acid digestion of linear polymers may lead to a product insoluble in water so the digestion has to be avoided. The aim of this paper was the determination of analytical characteristics and limitations of the total reflection x-ray fluorescence (TXRF) analysis for poly (vinylalcohol-vinylsulphate) salts and poly (acrylic acid, acrylamide) copolymers containing the following cations: K + , Cs + , Ba 2+ , Cu 2+ and La 3+ . On the basis of our results efficiency of ion-exchange during preparation of polyelectrolytes and stoichiometry of the end-product were determined. TXRF results were compared with data gained by inductively coupled plasma atomic emission spectrometry (ICP-AES) measurements except in the case of Cs + which has poor sensitivity in ICP-AES. Good agreement was found between the results of the two techniques and calculations from titrimetric data. Concentration of Li + and Mg 2+ in polymer samples was measured by ICP-AES. In majority of cases film-like dry residues of aqueous solutions of polyelectrolytes can be characterized by homogeneous spatial distribution of metal ions within the organic matrix. This is because the migration of the ions is hindered during drying process. Determination of metals in polyelectrolyte films by TXRF is quite ideal as model for analysis of plant, animal or human tissues which is a frequent task in environmental and inorganic biomedical analytical chemistry. (author)

  4. X-RAY EMISSION FROM SUPERNOVAE IN DENSE CIRCUMSTELLAR MATTER ENVIRONMENTS: A SEARCH FOR COLLISIONLESS SHOCKS

    International Nuclear Information System (INIS)

    Ofek, E. O.; Gal-Yam, A.; Yaron, O.; Arcavi, I.; Fox, D.; Cenko, S. B.; Filippenko, A. V.; Bloom, J. S.; Sullivan, M.; Gnat, O.; Frail, D. A.; Horesh, A.; Kulkarni, S. R.; Corsi, A.; Quimby, R. M.; Gehrels, N.; Nugent, P. E.; Kasliwal, M. M.; Bildsten, L.; Poznanski, D.

    2013-01-01

    The optical light curve of some supernovae (SNe) may be powered by the outward diffusion of the energy deposited by the explosion shock (the so-called shock breakout) in optically thick (τ ∼> 30) circumstellar matter (CSM). Recently, it was shown that the radiation-mediated and radiation-dominated shock in an optically thick wind must transform into a collisionless shock and can produce hard X-rays. The X-rays are expected to peak at late times, relative to maximum visible light. Here we report on a search, using Swift/XRT and Chandra, for X-ray emission from 28 SNe that belong to classes whose progenitors are suspected to be embedded in dense CSM. Our sample includes 19 Type IIn SNe, one Type Ibn SN, and eight hydrogen-poor superluminous SNe (SLSN-I such as SN 2005ap). Two SNe (SN 2006jc and SN 2010jl) have X-ray properties that are roughly consistent with the expectation for X-rays from a collisionless shock in optically thick CSM. However, the X-ray emission from SN 2006jc can also be explained as originating in an optically thin region. Thus, we propose that the optical light curve of SN 2010jl is powered by shock breakout in CSM. We suggest that two other events (SN 2010al and SN 2011ht) were too X-ray bright during the SN maximum optical light to be explained by the shock-breakout model. We conclude that the light curves of some, but not all, SNe IIn/Ibn are powered by shock breakout in CSM. For the rest of the SNe in our sample, including all of the SLSN-I events, our X-ray limits are not deep enough and were typically obtained too early (i.e., near the SN maximum light) for definitive conclusions about their nature. Late-time X-ray observations are required in order to further test whether these SNe are indeed embedded in dense CSM. We review the conditions required for a shock breakout in a wind profile. We argue that the timescale, relative to maximum light, for the SN to peak in X-rays is a probe of the column density and the density profile above the

  5. CHANDRA CHARACTERIZATION OF X-RAY EMISSION IN THE YOUNG F-STAR BINARY SYSTEM HD 113766

    International Nuclear Information System (INIS)

    Lisse, C. M.; Christian, D. J.; Wolk, S. J.; Günther, H. M.; Chen, C. H.; Grady, C. A.

    2017-01-01

    Using Chandra , we have obtained imaging X-ray spectroscopy of the 10–16 Myr old F-star binary HD 113766. We individually resolve the 1.″4 separation binary components for the first time in the X-ray and find a total 0.3–2.0 keV luminosity of 2.2 × 10 29 erg s −1 , consistent with previous RASS estimates. We find emission from the easternmost, infrared-bright, dusty member HD 113766A to be only ∼10% that of the western, infrared-faint member HD 113766B. There is no evidence for a 3rd late-type stellar or substellar member of HD 113766 with L x  > 6 × 10 25 erg s −1 within 2′ of the binary pair. The ratio of the two stars’ X-ray luminosity is consistent with their assignments as F2V and F6V by Pecaut et al. The emission is soft for both stars, kT Apec  = 0.30–0.50 keV, suggesting X-rays produced by stellar rotation and/or convection in young dynamos, but not accretion or outflow shocks, which we rule out. A possible 2.8 ± 0.15 (2 σ ) hr modulation in the HD 113766B X-ray emission is seen, but at very low confidence and of unknown provenance. Stellar wind drag models corresponding to L x  ∼ 2 × 10 29 erg s −1 argue for a 1 mm dust particle lifetime around HD 113766B of only ∼90,0000 years, suggesting that dust around HD 113766B is quickly removed, whereas 1 mm sized dust around HD 113766A can survive for >1.5 × 10 6 years. At 10 28 –10 29 erg s −1 X-ray luminosity, astrobiologically important effects, like dust warming and X-ray photolytic organic synthesis, are likely for any circumstellar material in the HD 113766 systems.

  6. Relation between X-Ray and γ-Ray Emissions for Fermi Blazars ...

    Indian Academy of Sciences (India)

    Abstract. Using γ-ray band data detected by Fermi Large Area Tele- scope (LAT) and X-ray band data for 78 blazars, we find a medium cor- relation between X-ray and γ-ray fluxes in the average state. A medium anticorrelation is also found between X-ray (1 KeV) mean spectral index αx and γ-ray mean spectral index αγ for ...

  7. Picosecond x-ray streak camera studies

    International Nuclear Information System (INIS)

    Kasyanov, Yu.S.; Malyutin, A.A.; Richardson, M.C.; Chevokin, V.K.

    1975-01-01

    Some initial results of direct measurement of picosecond x-ray emission from laser-produced plasmas are presented. A PIM-UMI 93 image converter tube, incorporating an x-ray sensitive photocathode, linear deflection, and three stages of image amplification was used to analyse the x-ray radiation emanating from plasmas produced from solid Ti targets by single high-intensity picosecond laser pulses. From such plasmas, the x-ray emission typically persisted for times of 60psec. However, it is shown that this detection system should be capable of resolving x-ray phenomena of much shorter duration. (author)

  8. Plasma Emission Profile Recreation using Soft X-Ray Tomography

    Science.gov (United States)

    Page, J. W.; Mauel, M. E.; Levesque, J. P.

    2015-11-01

    With sufficient views from multiple diode arrays, soft X-ray tomography is an invaluable plasma diagnostic because it is a non-perturbing method to reconstruct the emission within the interior of the plasma. In preparation for the installation of new SXR arrays in HBT-EP, we compute high-resolution tomographic reconstructions of discharges having kink-like structures that rotate nearly rigidly. By assuming a uniform angular mapping from the kink mode rotation, Δϕ ~ ωΔ t, a temporal sequence from a single 16-diode fan array represents as many as 16 x 100 independent views. We follow the procedure described by Wang and Granetz and use Bessel basis functions to take the inverse Radon transform. This transform is fit to our data using a least-squares method to estimate the internal SXR emissivity as a sum of polar functions. By varying different parameters of the transformation, we optimize the quality of our recreation of the emission profile and quantify how the reconstruction changes with the azimuthal order of the transform. Supported by U.S. DOE Grant DE-FG02-86ER53222.

  9. The application of proton induced X-ray emission in criminalistics

    International Nuclear Information System (INIS)

    Li Zhenyuan; Xie Shuxian

    1993-01-01

    The determination method of trace elements in high pure gold by proton induced X-ray emission is reported. The target preparation, design of physical experiment, data proceeding and the analysis of gold samples by the internal standard of single-standard are discussed. Using this determination method, the identification of a sample of high pure gold is performed

  10. Where is the X-ray emission coming from in RT Cru Symbiotic System?

    Science.gov (United States)

    Karovska, Margarita

    2014-11-01

    RT Cru is a member of a new sub-class of symbiotic interacting binaries with copious hard X-ray emission. It consists of a high-mass WD (>1.3 Ms) accreting from the wind of an M giant, and it is an important system to study in order to constrain precursor conditions for asymmetric PN and SN Ia. The Chandra HRC-I observation (Dec 2012), and an overlapping Swift observation, detected intermittent soft X-ray flaring, and we find evidence for a significant soft component in the spectrum. The flaring could be a consequence of clumped absorption columns moving in and out of the line of sight, or the variations could be due to changes at the accretion boundary layer. Further observations are needed to determine the origin of the soft emission and its relation to the hard emission.

  11. X-ray survey of the Pleiades: dependence of X-ray luminosity on stellar age

    International Nuclear Information System (INIS)

    Micela, G.; Sciortino, S.; Serio, S.; Vaiana, G.S.; Golub, L.; Harnden, F.R.; Rosner, R.

    1984-01-01

    The study of X-ray emission of stellar clusters, allows to decouple the influence of some individual stellar parameters, as initial conditions, composition and age, on the stellar X-ray function. The authors report preliminary results from an Einstein X-ray survey of the Pleiades. (Auth.)

  12. Einstein X-ray observations of Herbig Ae/Be stars

    Science.gov (United States)

    Damiani, F.; Micela, G.; Sciortino, S.; Harnden, F. R., Jr.

    1994-01-01

    We have investigated the X-ray emission from Herbig Ae/Be stars, using the full set of Einstein Imaging Proportional Counter (IPC) observations. Of a total of 31 observed Herbig stars, 11 are confidently identified with X-ray sources, with four additonal dubious identifications. We have used maximum likelihood luminosity functions to study the distribution of X-ray luminosity, and we find that Be stars are significantly brighter in X-rays than Ae stars and that their X-ray luminosity is independent of projected rotational velocity v sin i. The X-ray emission is instead correlated with stellar bolometric luminosity and with effective temperature, and also with the kinetic luminosity of the stellar wind. These results seem to exclude a solar-like origin for the X-ray emission, a possibility suggested by the most recent models of Herbig stars' structure, and suggest an analogy with the X-ray emission of O (and early B) stars. We also observe correlations between X-ray luminosity and the emission at 2.2 microns (K band) and 25 microns, which strengthen the case for X-ray emission of Herbig stars originating in their circumstellar envelopes.

  13. Determination of non-ionic surfactants in technologic liquors and effluents by X-ray fluorescent spectrometry

    International Nuclear Information System (INIS)

    Dankowski, P.; Majda, J.

    1977-01-01

    The method has been worked out for determination of non-ionic surfactants in technological liquors and effluents, based on the X-ray fluorescent spectrometry with an initial concentration by means of the phosphomolybdic acid. The method is suitable for a quantitative determination of ethylene oxide adducts in a wide range of applicable concentrations, the trace-ones included. (M.Z.)

  14. X-ray emission from plasmas created by smoothed KrF laser irradiation

    International Nuclear Information System (INIS)

    Aglitskiy, Y.; Lehecka, T.; Deniz, A.; Hardgrove, J.; Seely, J.; Brown, C.; Feldman, U.; Pawley, C.; Gerber, K.; Bodner, S.; Obenschain, S.; Lehmberg, R.; McLean, E.; Pronko, M.; Sethian, J.; Stamper, J.; Schmitt, A.; Sullivan, C.; Holland, G.; Laming, M.

    1996-01-01

    The x-ray emission from plasmas created by the Naval Research Laboratory Nike KrF laser [Phys. Plasmas 3, 2098 (1996) ] was characterized using imaging and spectroscopic instruments. The laser wavelength was 1/4 μm, and the beams were smoothed by induced spatial incoherence (ISI). The targets were thin foils of CH, aluminum, titanium, and cobalt and were irradiated by laser energies in the range 100 endash 1500 J. A multilayer mirror microscope operating at an energy of 95 eV recorded images of the plasma with a spatial resolution of 2 μm. The variation of the 95 eV emission across the 800 μm focal spot was 1.3% rms. Using a curved crystal imager operating in the 1 endash 2 keV x-ray region, the density, temperature, and opacity of aluminum plasmas were determined with a spatial resolution of 10 μm perpendicular to the target surface. The spectral line ratios indicated that the aluminum plasmas were relatively dense, cool, and optically thick near the target surface. The absolute radiation flux was determined at 95 eV and in x-ray bandpasses covering the 1 endash 8 keV region. The electron temperature inferred from the slope of the x-ray flux versus energy data in the 5 endash 8 keV region was 900 eV for an incident laser energy of 200 J and an intensity of ≅10 13 W/cm 2

  15. The determination, by x-ray-fluorescence spectrometry, of gold in activated charcoal

    International Nuclear Information System (INIS)

    Austen, C.E.

    1977-01-01

    A rapid method is described for the determination of gold in activated charcoal by X-ray-fluorescence spectrometry. Compensation for matrix effects is achieved by means of platinum that is added for use as an internal standard. Calibration is achieved by use of a series of synthetic standards that are made by the spiking of barren charcoal with gold and platinum. The limit of determination is about 8 p.p.m. of gold, and the relative standard deviation is 1,2 per cent at a concentration level of 2300 p.p.m

  16. VARIABLE O VI AND N V EMISSION FROM THE X-RAY BINARY LMC X-3: HEATING OF THE BLACK HOLE COMPANION

    International Nuclear Information System (INIS)

    Song Limin; Tripp, Todd M.; Wang, Q. Daniel; Yao Yangsen; Cui Wei; Xue Yongquan; Orosz, Jerome A.; Steeghs, Danny; Steiner, James F.; Torres, Manuel A. P.; McClintock, Jeffrey E.

    2010-01-01

    Based on high-resolution ultraviolet spectroscopy obtained with the Far Ultraviolet Spectroscopic Explorer (FUSE) and the Cosmic Origins Spectrograph, we present new detections of O VI and N V emission from the black hole X-ray binary (XRB) system LMC X-3. We also update the ephemeris of the XRB using recent radial velocity measurements obtained with the echelle spectrograph on the Magellan-Clay telescope. We observe significant velocity variability of the UV emission, and we find that the O VI and N V emission velocities follow the optical velocity curve of the XRB. Moreover, the O VI and N V intensities regularly decrease between binary phase = 0.5 and 1.0, which suggests that the source of the UV emission is increasingly occulted as the B star in the XRB moves from superior to inferior conjunction. These trends suggest that illumination of the B star atmosphere by the intense X-ray emission from the accreting black hole creates a hot spot on one side of the B star, and this hot spot is the origin of the O VI and N V emission. However, the velocity semiamplitude of the ultraviolet emission, K UV ∼ 180 km s -1 , is lower than the optical semiamplitude; this difference could be due to rotation of the B star. Comparison of the FUSE observations taken in 2001 November and 2004 April shows a significant change in the O VI emission characteristics: in the 2001 data, the O VI region shows both broad and narrow emission features, while in 2004 only the narrow O VI emission is clearly present. Rossi X-ray Timing Explorer data show that the XRB was in a high/soft state in the 2001 November epoch but was in a transitional state in 2004 April, so the shape of the X-ray spectrum might change the properties of the region illuminated on the B star and thus change the broad versus narrow characteristics of the UV emission. If our hypothesis about the origin of the highly ionized emission is correct, then careful analysis of the emission occultation could, in principle

  17. Measuring conditions for second order X-ray Bragg-spectrometry

    International Nuclear Information System (INIS)

    Dellith, J; Scheffel, A; Wendt, M

    2014-01-01

    The KL 2,3 (α) 1,2 -lines of 19 K, the L 3 M 4,5 (α) 1,2 -lines of 48 Cd, and the M 5 N 6,7 (α) 1,2 -lines of 92 U are lines of comparable energy in the region of approximately 3 keV. In none of these cases were we able to resolve the three doublets when recording the spectra in first order Bragg spectrometry using a PET crystal as the dispersing element. For the purpose of enhancing the resolving power of the spectrometer, the three α spectra were recorded in second order reflection, thereby transferring the lines into another spectral region dominated by X-ray quanta of half the energy. In order to achieve high net peak intensities as well as a high peak-to-background ratio and, consequently, a high level of detection capability, the discriminator settings should be optimized quite carefully. In this manner, we were able to resolve the three α doublets and estimate α 2 /α 1 intensity ratios. Inexplicably, current monographs, e.g., by Goldstein et al, do not contain any indications about the rational use of high order spectrometry. Only a few rather old monographs contain some hints in this regard

  18. CORRELATION OF HARD X-RAY AND WHITE LIGHT EMISSION IN SOLAR FLARES

    Energy Technology Data Exchange (ETDEWEB)

    Kuhar, Matej; Krucker, Säm; Battaglia, Marina; Kleint, Lucia; Casadei, Diego [University of Applied Sciences and Arts Northwestern Switzerland, Bahnhofstrasse 6, 5210 Windisch (Switzerland); Oliveros, Juan Carlos Martinez; Hudson, Hugh S. [Space Sciences Laboratory, University of California, Berkeley, CA 94720-7450 (United States)

    2016-01-01

    A statistical study of the correlation between hard X-ray and white light emission in solar flares is performed in order to search for a link between flare-accelerated electrons and white light formation. We analyze 43 flares spanning GOES classes M and X using observations from the Reuven Ramaty High Energy Solar Spectroscopic Imager and Helioseismic and Magnetic Imager. We calculate X-ray fluxes at 30 keV and white light fluxes at 6173 Å summed over the hard X-ray flare ribbons with an integration time of 45 s around the peak hard-X ray time. We find a good correlation between hard X-ray fluxes and excess white light fluxes, with a highest correlation coefficient of 0.68 for photons with energy of 30 keV. Assuming the thick target model, a similar correlation is found between the deposited power by flare-accelerated electrons and the white light fluxes. The correlation coefficient is found to be largest for energy deposition by electrons above ∼50 keV. At higher electron energies the correlation decreases gradually while a rapid decrease is seen if the energy provided by low-energy electrons is added. This suggests that flare-accelerated electrons of energy ∼50 keV are the main source for white light production.

  19. A LINK BETWEEN X-RAY EMISSION LINES AND RADIO JETS IN 4U 1630-47?

    Energy Technology Data Exchange (ETDEWEB)

    Neilsen, Joseph [Department of Astronomy, Boston University, Boston, MA 02215 (United States); Coriat, Mickaël [Department of Astronomy, University of Cape Town, Private Bag X3, Rondebosch 7701 (South Africa); Fender, Rob; Broderick, Jess W. [Department of Physics, Oxford University, Oxford OX1 3RH (United Kingdom); Lee, Julia C. [Harvard-Smithsonian Center for Astrophysics, Cambridge, MA 02138 (United States); Ponti, Gabriele [Max Planck Institute fur Extraterrestriche Physik, D-85748 Garching (Germany); Tzioumis, Anastasios K.; Edwards, Philip G., E-mail: neilsenj@bu.edu [CSIRO Astronomy and Space Science, Australia Telescope National Facility, P.O. Box 76, Epping, NSW 1710 (Australia)

    2014-03-20

    Recently, Díaz Trigo et al. reported an XMM-Newton detection of relativistically Doppler-shifted emission lines associated with steep-spectrum radio emission in the stellar-mass black hole candidate 4U 1630-47 during its 2012 outburst. They interpreted these lines as indicative of a baryonic jet launched by the accretion disk. Here we present a search for the same lines earlier in the same outburst using high-resolution X-ray spectra from the Chandra HETGS. While our observations (eight months prior to the XMM-Newton campaign) also coincide with detections of steep spectrum radio emission by the Australia Telescope Compact Array, we find no evidence for any relativistic X-ray emission lines. Indeed, despite ∼5 × brighter radio emission, our Chandra spectra allow us to place an upper limit on the flux in the blueshifted Fe XXVI line that is ≳ 20 × weaker than the line observed by Díaz Trigo et al. We explore several scenarios that could explain our differing results, including variations in the geometry of the jet or a mass-loading process or jet baryon content that evolves with the accretion state of the black hole. We also consider the possibility that the radio emission arises in an interaction between a jet and the nearby interstellar medium, in which case the X-ray emission lines might be unrelated to the radio emission.

  20. A LINK BETWEEN X-RAY EMISSION LINES AND RADIO JETS IN 4U 1630-47?

    International Nuclear Information System (INIS)

    Neilsen, Joseph; Coriat, Mickaël; Fender, Rob; Broderick, Jess W.; Lee, Julia C.; Ponti, Gabriele; Tzioumis, Anastasios K.; Edwards, Philip G.

    2014-01-01

    Recently, Díaz Trigo et al. reported an XMM-Newton detection of relativistically Doppler-shifted emission lines associated with steep-spectrum radio emission in the stellar-mass black hole candidate 4U 1630-47 during its 2012 outburst. They interpreted these lines as indicative of a baryonic jet launched by the accretion disk. Here we present a search for the same lines earlier in the same outburst using high-resolution X-ray spectra from the Chandra HETGS. While our observations (eight months prior to the XMM-Newton campaign) also coincide with detections of steep spectrum radio emission by the Australia Telescope Compact Array, we find no evidence for any relativistic X-ray emission lines. Indeed, despite ∼5 × brighter radio emission, our Chandra spectra allow us to place an upper limit on the flux in the blueshifted Fe XXVI line that is ≳ 20 × weaker than the line observed by Díaz Trigo et al. We explore several scenarios that could explain our differing results, including variations in the geometry of the jet or a mass-loading process or jet baryon content that evolves with the accretion state of the black hole. We also consider the possibility that the radio emission arises in an interaction between a jet and the nearby interstellar medium, in which case the X-ray emission lines might be unrelated to the radio emission

  1. X-ray generation by femtosecond laser pulses and its application to soft X-ray imaging microscope

    International Nuclear Information System (INIS)

    Ikeda, Kenichi; Kotaki, Hideyuki; Nakajima, Kazuhisa

    2002-01-01

    We have developed laser-produced plasma X-ray sources using femtosecond laser pulses at 10Hz repetition rate in a table-top size in order to investigate basic mechanism of X-ray emission from laser-matter interactions and its application to a X-ray microscope. In a soft X-ray region over 5 nm wavelength, laser-plasma X-ray emission from a solid target achieved an intense flux of photons of the order of 1011 photons/rad per pulse with duration of a few 100 ps, which is intense enough to make a clear imaging in a short time exposure. As an application of laser-produced plasma X-ray source, we have developed a soft X-ray imaging microscope operating in the wavelength range around 14 nm. The microscope consists of a cylindrically ellipsoidal condenser mirror and a Schwarzshird objective mirror with highly-reflective multilayers. We report preliminary results of performance tests of the soft X-ray imaging microscope with a compact laser-produced plasma X-ray source

  2. A SUZAKU SEARCH FOR NONTHERMAL EMISSION AT HARD X-RAY ENERGIES IN THE COMA CLUSTER

    International Nuclear Information System (INIS)

    Wik, Daniel R.; Sarazin, Craig L.; Finoguenov, Alexis; Matsushita, Kyoko; Nakazawa, Kazuhiro; Clarke, Tracy E.

    2009-01-01

    The brightest cluster radio halo known resides in the Coma cluster of galaxies. The relativistic electrons producing this diffuse synchrotron emission should also produce inverse Compton emission that becomes competitive with thermal emission from the intracluster medium (ICM) at hard X-ray energies. Thus far, claimed detections of this emission in Coma are controversial. We present a Suzaku HXD-PIN observation of the Coma cluster in order to nail down its nonthermal hard X-ray content. The contribution of thermal emission to the HXD-PIN spectrum is constrained by simultaneously fitting thermal and nonthermal models to it and a spatially equivalent spectrum derived from an XMM-Newton mosaic of the Coma field. We fail to find statistically significant evidence for nonthermal emission in the spectra which are better described by only a single- or multitemperature model for the ICM. Including systematic uncertainties, we derive a 90% upper limit on the flux of nonthermal emission of 6.0 x 10 -12 erg s -1 cm -2 (20-80 keV, for Γ = 2.0), which implies a lower limit on the cluster-averaged magnetic field of B>0.15 μG. Our flux upper limit is 2.5 times lower than the detected nonthermal flux from RXTE and BeppoSAX. However, if the nonthermal hard X-ray emission in Coma is more spatially extended than the observed radio halo, the Suzaku HXD-PIN may miss some fraction of the emission. A detailed investigation indicates that ∼50%-67% of the emission might go undetected, which could make our limit consistent with that of Rephaeli and Gruber and Fusco-Femiano et al. The thermal interpretation of the hard Coma spectrum is consistent with recent analyses of INTEGRAL and Swift data.

  3. A Link Between X-ray Emission Lines and Radio Jets in 4U 1630-47?

    Science.gov (United States)

    Neilsen, Joseph; Coriat, Mickaël; Fender, Rob; Lee, Julia C.; Ponti, Gabriele; Tzioumis, A.; Edwards, Phillip; Broderick, Jess

    2014-06-01

    Recently, Díaz Trigo et al. reported an XMM-Newton detection of relativistically Doppler-shifted emission lines associated with steep-spectrum radio emission in the stellar-mass black hole candidate 4U 1630-47 during its 2012 outburst. They interpreted these lines as indicative of a baryonic jet launched by the accretion disk. We present a search for the same lines earlier in the same outburst using high-resolution X-ray spectra from the Chandra HETGS. While our observations (eight months prior to the XMM-Newton campaign) also coincide with detections of steep spectrum radio emission by the Australia Telescope Compact Array, we find a strong disk wind but no evidence for any relativistic X-ray emission lines. Indeed, despite ˜5× brighter radio emission, our Chandra spectra allow us to place an upper limit on the flux in the blueshifted Fe XXVI line that is ˜20× weaker than the line observed by Díaz Trigo et al. Thus we can conclusively say that radio emission is not universally associated with relativistically Doppler-shifted emission lines in 4U 1630-47. We explore several scenarios that could explain our differing results, including variations in the geometry of the jet or a mass-loading process or jet baryon content that evolves with the accretion state of the black hole. We also consider the possibility that the radio emission arises in an interaction between a jet and the nearby ISM, in which case the X-ray emission lines might be unrelated to the radio emission.

  4. Radio and X-Ray Observations of the 1998 Outburst of the Recurrent X-Ray Transient 4U 1630-47

    Science.gov (United States)

    Hjellming, R. M.; Rupen, M. P.; Mioduszewski, A. J.; Kuulkers, E.; McCollough, M.; Harmon, B. A.; Buxton, M.; Sood, R.; Tzioumis, A.; Rayner, D.; Dieters, S.; Durouchoux, P.

    1999-03-01

    We report radio (NRAO VLA and Australia Telescope Compact Array), soft X-ray (Rossi X-Ray Timing Explorer ASM), and hard X-ray (Compton Gamma Ray Observatory BATSE) observations of a 1998 outburst in the recurring X-ray transient 4U 1630-47, where radio emission was detected for the first time. The radio observations identify the position of 4U 1630-47 to within 1". Because the radio emission is optically thin with a spectral index of ~-0.8 during the rise, peak, and decay of the initial radio event, the emission is probably coming from an optically thin radio jet ejected over a period of time. The 20-100 keV emission first appeared 1998 January 28 (MJD 50841), the 2-12 keV emission first appeared 1998 February 3 (MJD 50847), and the first radio emission was detected 1998 February 12.6 (MJD 50856.6). The rise of the radio emission probably began about 1998 February 7 (MJD 50851) when the X-rays were in a very hard fluctuating-hardness state, just before changing to a softer, more stable hardness state.

  5. Revising the Local Bubble Model due to Solar Wind Charge Exchange X-ray Emission

    Science.gov (United States)

    Shelton, Robin L.

    2009-03-01

    The hot Local Bubble surrounding the solar neighborhood has been primarily studied through observations of its soft X-ray emission. The measurements were obtained by attributing all of the observed local soft X-rays to the bubble. However, mounting evidence shows that the heliosphere also produces diffuse X-rays. The source is solar wind ions that have received an electron from another atom. The presence of this alternate explanation for locally produced diffuse X-rays calls into question the existence and character of the Local Bubble. This article addresses these questions. It reviews the literature on solar wind charge exchange (SWCX) X-ray production, finding that SWCX accounts for roughly half of the observed local 1/4 keV X-rays found at low latitudes. This article also makes predictions for the heliospheric O VI column density and intensity, finding them to be smaller than the observational error bars. Evidence for the continued belief that the Local Bubble contains hot gas includes the remaining local 1/4 keV intensity, the observed local O VI column density, and the need to fill the local region with some sort of plasma. If the true Local Bubble is half as bright as previously thought, then its electron density and thermal pressure are 1/sqrt{2} as great as previously thought, and its energy requirements and emission measure are 1/2 as great as previously thought. These adjustments can be accommodated easily, and, in fact, bring the Local Bubble’s pressure more in line with that of the adjacent material. Suggestions for future work are made.

  6. Temporal feature of X-ray laser plasma observed from 3ω0/2, 2ω0 harmonic emission

    International Nuclear Information System (INIS)

    Li Wenhong; Mei Qiyong; Zhao Xuewei; Chen Yuting; Chunyu Shutai

    1995-01-01

    Temporal feature of X-ray laser plasma density was observed from 3ω 0 /2, 2ω 0 harmonic emission in the experiments. The temporal feature of 3ω 0 /2 harmonic emission of the germanium film is much different from that of the slab germanium target. The production of x-ray laser is closely related to 3ω 0 /2 harmonic emission in the slab germanium targets

  7. Time correlation between plasma behaviour and soft x-ray emission in a plasma focus

    International Nuclear Information System (INIS)

    Hirano, Katsumi; Tagaya, Yutaka; Shimoda, Katsuji; Okabe, Yushiro; Yamamoto, Toshikazu

    1986-01-01

    Soft X-rays emitted from a plasma focus are investigated experimentally. In contrast to single-pulsive burst of neutron, hard X-rays, ion- and electron beams, the soft X-rays are observed from the collapse phase to the decay phase of the plasma column, and have typically three successive peaks in its signal. Each peak corresponds to the maximum compression, the disruption and the decay phase of plasma column. It is revealed that the first and the second peaks are radiated by plasma itself, whereas the third peak is caused by emission from the inner electrode face. (author)

  8. Electronic structure of human hemoglobin: ultrasoft X-ray emission study

    International Nuclear Information System (INIS)

    Soldatov, A.V.; Kravtsova, A.N.; Fedorovich, E.N.; Kurmaev, E.Z.; Moewes, A.

    2004-01-01

    Full text: The iron L 2,3 and carbon, nitrogen and oxygen Kα X-ray emission spectra (XES) of human hemoglobin have been recorded at the soft X-ray spectroscopy endstation on Undulator Beam line 8.0 at Advanced Light Source (ALS) located at the Lawrence Berkeley National Laboratory. The theoretical calculations of Fe L 3 -XES have been performed using ab initio code FEFF8.2. The calculations have been carried out for the structure of hemoglobin presented in PDB (entry 3HHB) as well as for the molecule with symmetrical heme plane. It was found that the Fe L 3 emission spectrum calculated for the ideal molecule agrees slightly better with the experiment as compared with those calculated for the real molecule. Thus, one can use the structure of the ideal molecule for theoretical Fe L 3 -XES simulations. The theoretical analysis has shown that the fist peak of experimental Fe L 3 - emission spectrum is enhanced by the nearest nitrogen atoms lying in heme plane around the central iron atom. The theoretical C K- and N K-XES spectra of hemoglobin have been calculated. A good agreement between theoretical and experimental spectra has been obtained. The distribution of the partial electronic densities of states in the valence and conduction bands of hemoglobin has been determined

  9. Working with Detection Limits in X-Ray and Nuclear Spectrometry

    International Nuclear Information System (INIS)

    Van Espen, P.

    2003-01-01

    Full Text: Detection limits are important in many measurement procedures. Especially in analytical work we often need to take a decision about the presence or absence of a compound, or we need to guarantee that or instrument can detect the compound. Especially in regulatory work the concept of detection limits plays a crucial role. Data acquisition in x-ray and gamma-ray spectrometry is done by counting events for a preset time; hence the fluctuations in the observed spectra are governed by Poisson (counting) statistics. This makes the calculation of detection limits in principle very easy. However it is observed that there exists a great deal of confusion concerning the definition(s) and especially concerning the practical calculation and reporting of detection limits. In this contribution a simple but rigorous treatment of the concept of detection limits will be given, emphasizing on aspects such as a-priori and a-posterior i limits and on the effect of sample blank and instrumental blank in the calculation of the true detection limit. The problem of near zero background as observed in e.g. total reflection x-ray fluorescence analysis (T-XRF) and some low level counting applications will also be discussed. In this case Poisson statistics might not be applicable, affecting the decision limits with respect to the presence of absence of a signal. Finally handling data sets that contain detection limit values next to normal measured values, the so called problem of missing data will be discussed. Some suggestions to deal with this frequently occurring situation will be given

  10. Multielement proton-induced x-ray emission analysis of Bangladeshi tobacco

    International Nuclear Information System (INIS)

    Hadi, D.A.; Ali, M.; Biswas, S.K.; Islam, M.M.; Khan, A.H.

    1984-01-01

    The concentration of 12 different elements in cigarette tobacco of different brands, commercially made in Bangladesh, was determined using the proton particle-induced x-ray emission (proton PIXE) method. In all the present experiments, proton beams of 2.0 MeV (on the target in air) and about 30 nA current were used for characteristic x-ray excitation. The concentration of the elements (K, Ca, Ti, Cr, Mn, Fe, Ni, Cu, Zn, Br, Rb and Sr) was determined by comparison with a calibration obtained from the NBS orchard leaf standard SRM 1571. The results have been compared with available data on some foreign brands of tobacco and the probable reasons for the difference in the contents of some of the elements found in the Bangladeshi brands are discussed. (author)

  11. Study of X-ray emission in aluminium z-pinches; Etude de l'emission X dans les plasmas d'aluminium de type Z-pinch

    Energy Technology Data Exchange (ETDEWEB)

    Rosch, R [CEA/DAM-Ile de France, Dept. de Conception et Realisation des Experimentations (DCRE), 91 - Bruyeres-le-Chatel (France); [Paris-11 Univ., 91 - Orsay (France)

    1999-07-01

    Previous experiments, at 0.1. TX level, have shown that stability and x-ray emission of fast Z-pinches, could be strongly increased by imploding an aluminium vapor jet onto a very thin coaxial wire. We present here first results of an aluminium Z-pinch, using a similar liner, but at mega-ampere level. The pinch is driven by AMBIORIX high-power facility, a 2 TW,0.5 {omega}, 2 MA, 50 ns pulse-line generator. We study the effect of an aluminium wire and its diameter (20-50 {mu}m) on the implosion dynamics, on x-ray yield on MHD stability of the column at stagnation. Analysis of A1 jet on A1 wire shots demonstrates that x-ray yield due to emission processes in the H- and He- like ionization stages (i.e. the K-shell) is significantly enhanced, relative to that of A1 jet only ones. The wire also leads to better symmetry of the implosion, and to better reproducibility of shots. X-ray signals exhibit two similar pulses, 10 ns in width, 15 ns spaced. To discern spectral origin of both pulses, experiments are realized with stainless steel wire (25 {mu}m in diameter). Results show that liner and wire radial simultaneously and contribute to both pulses. Analysis of a typical A1 jet on A1 wire shot, using detailed collisional-radiative equilibrium (CRE) model is also given in this thesis. View o the pinch at stagnation as a cola-dense core surrounded by a hot-low density corona reproduces all features of the X-ray data. (author)

  12. Optimization of soft x-ray line emission from laser-produced carbon ...

    Indian Academy of Sciences (India)

    Intense XUV soft x-ray emission from laser-produced plasma sources is currently ... absorption edges of oxygen and carbon respectively) is particularly attractive as it permits ... ability of the target element producing intense discrete lines in the water .... ficient due to Pert [17] and dielectronic recombination coefficient due to ...

  13. Role of screening and angular distributions in resonant soft-x-ray emission of CO

    Energy Technology Data Exchange (ETDEWEB)

    Skytt, P.; Glans, P.; Gunnelin, K. [Uppsala Univ. (Sweden)] [and others

    1997-04-01

    In the present work the authors focus on two particular properties of resonant X-ray emission, namely core hole screening of the excited electron, and anisotropy caused by the polarization of the exciting synchrotron radiation. The screening of the core hole by the excited electron causes energy shifts and intensity variations in resonant spectra compared to the non-resonant case. The linear polarization of the synchrotron radiation and the dipole nature of the absorption process create a preferential alignment selection of the randomly oriented molecules in the case of resonant excitation, producing an anisotropy in the angular distribution of the emitted X-rays. The authors have chosen CO for this study because this molecule has previously served as a showcase for non-resonant X-ray emission, mapping the valence electronic structure differently according to the local selection rules. With the present work they take interest in how this characteristic feature of the spectroscopy is represented in the resonant case.

  14. X-RAY EMISSION FROM THE DOUBLE-BINARY OB-STAR SYSTEM QZ CAR (HD 93206)

    International Nuclear Information System (INIS)

    Parkin, E. R.; Naze, Y.; Rauw, G.; Broos, P. S.; Townsley, L. K.; Pittard, J. M.; Moffat, A. F. J.; Oskinova, L. M.; Waldron, W. L.

    2011-01-01

    X-ray observations of the double-binary OB-star system QZ Car (HD 93206) obtained with the Chandra X-ray Observatory over a period of roughly 2 years are presented. The respective orbits of systems A (O9.7 I+b2 v, P A = 21 days) and B (O8 III+o9 v, P B = 6 days) are reasonably well sampled by the observations, allowing the origin of the X-ray emission to be examined in detail. The X-ray spectra can be well fitted by an attenuated three-temperature thermal plasma model, characterized by cool, moderate, and hot plasma components at kT ≅ 0.2, 0.7, and 2 keV, respectively, and a circumstellar absorption of ≅0.2 x 10 22 cm -2 . Although the hot plasma component could be indicating the presence of wind-wind collision shocks in the system, the model fluxes calculated from spectral fits, with an average value of ≅7 x 10 -13 erg s -1 cm -2 , do not show a clear correlation with the orbits of the two constituent binaries. A semi-analytical model of QZ Car reveals that a stable momentum balance may not be established in either system A or B. Yet, despite this, system B is expected to produce an observed X-ray flux well in excess of the observations. If one considers the wind of the O8 III star to be disrupted by mass transfer, the model and observations are in far better agreement, which lends support to the previous suggestion of mass transfer in the O8 III + o9 v binary. We conclude that the X-ray emission from QZ Car can be reasonably well accounted for by a combination of contributions mainly from the single stars and the mutual wind-wind collision between systems A and B.

  15. Millimeter and X-Ray Emission from the 5 July 2012 Solar Flare

    Science.gov (United States)

    Tsap, Y. T.; Smirnova, V. V.; Motorina, G. G.; Morgachev, A. S.; Kuznetsov, S. A.; Nagnibeda, V. G.; Ryzhov, V. S.

    2018-03-01

    The 5 July 2012 solar flare SOL2012-07-05T11:44 (11:39 - 11:49 UT) with an increasing millimeter spectrum between 93 and 140 GHz is considered. We use space and ground-based observations in X-ray, extreme ultraviolet, microwave, and millimeter wave ranges obtained with the Reuven Ramaty High-Energy Solar Spectroscopic Imager, Solar Dynamics Observatory (SDO), Geostationary Operational Environmental Satellite, Radio Solar Telescope Network, and Bauman Moscow State Technical University millimeter radio telescope RT-7.5. The main parameters of thermal and accelerated electrons were determined through X-ray spectral fitting assuming the homogeneous thermal source and thick-target model. From the data of the Atmospheric Imaging Assembly/SDO and differential-emission-measure calculations it is shown that the thermal coronal plasma gives a negligible contribution to the millimeter flare emission. Model calculations suggest that the observed increase of millimeter spectral flux with frequency is determined by gyrosynchrotron emission of high-energy (≳ 300 keV) electrons in the chromosphere. The consequences of the results are discussed in the light of the flare-energy-release mechanisms.

  16. Absolute Soft X-ray Emission Measurements at the Nike Laser

    Science.gov (United States)

    Weaver, J.; Atkin, R.; Boyer, C.; Colombant, D.; Feldman, U.; Fielding, D.; Gardner, J.; Holland, G.; Klapisch, M.; Mostovych, A. N.; Obenscain, S.; Seely, J. F.

    2002-11-01

    Recent experiments at the Nike laser facility have demonstrated that, when a low intensity prepulse ( 2main laser intensity) is used to heat a thin Au or Pd coating on a planar CH target, the growth of non-uniformities due to laser imprint can be reduced from the growth observed for an uncoated CH target. The absolute radiation intensity in the soft x-ray region (0.1-1 keV) has a important role in the energy balance for layered targets. There is an ongoing effort to characterize the soft x-ray emission using an absolutely calibrated transmission grating spectrometer and filtered diode modules. Measurements of the angular distribution of the emission from unlayered solid targets (Au, Pd, CH) have recently been made using an array of moveable filtered diode modules. The data from the angular distribution studies will be presented. A new absolutely calibrated, time-resolving transmission grating spectrometer has been installed at the Nike. The new version has improved spectral resolution, selectable transmission filters, and the potential for simultaneous temporal, spatial, and spectral resolution. Preliminary data from the new spectrometer will be presented and future experiments will be briefly discussed. *Work was supported by DoE

  17. CHANDRA CHARACTERIZATION OF X-RAY EMISSION IN THE YOUNG F-STAR BINARY SYSTEM HD 113766

    Energy Technology Data Exchange (ETDEWEB)

    Lisse, C. M. [Planetary Exploration Branch, Space Exploration Sector, Johns Hopkins University Applied Physics Laboratory, 11100 Johns Hopkins Road, Laurel, MD 20723 (United States); Christian, D. J. [Department of Physics and Astronomy, California State University Northridge, 18111 Nordhoff Street, Northridge, CA 91330 (United States); Wolk, S. J. [Chandra X-ray Center, Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States); Günther, H. M. [Massachusetts Institute of Technology, Kavli Institute for Astrophysics and Space Research, 77 Massachusetts Avenue, NE83-569, Cambridge, MA 02139 (United States); Chen, C. H. [STScI, 3700 San Martin Drive, Baltimore, MD 21218 (United States); Grady, C. A., E-mail: carey.lisse@jhuapl.edu, E-mail: damian.christian@csun.edu, E-mail: swolk@cfa.harvard.edu, E-mail: hgunther@mit.edu, E-mail: cchen@stsci.edu, E-mail: carol.a.grady@nasa.gov [Eureka Scientific and Goddard Space Flight Center, Code 667, NASA-GSFC, Greenbelt, MD 20771 (United States)

    2017-02-01

    Using Chandra , we have obtained imaging X-ray spectroscopy of the 10–16 Myr old F-star binary HD 113766. We individually resolve the 1.″4 separation binary components for the first time in the X-ray and find a total 0.3–2.0 keV luminosity of 2.2 × 10{sup 29} erg s{sup −1}, consistent with previous RASS estimates. We find emission from the easternmost, infrared-bright, dusty member HD 113766A to be only ∼10% that of the western, infrared-faint member HD 113766B. There is no evidence for a 3rd late-type stellar or substellar member of HD 113766 with L {sub x} > 6 × 10{sup 25} erg s{sup −1} within 2′ of the binary pair. The ratio of the two stars’ X-ray luminosity is consistent with their assignments as F2V and F6V by Pecaut et al. The emission is soft for both stars, kT {sub Apec} = 0.30–0.50 keV, suggesting X-rays produced by stellar rotation and/or convection in young dynamos, but not accretion or outflow shocks, which we rule out. A possible 2.8 ± 0.15 (2 σ ) hr modulation in the HD 113766B X-ray emission is seen, but at very low confidence and of unknown provenance. Stellar wind drag models corresponding to L {sub x} ∼ 2 × 10{sup 29} erg s{sup −1} argue for a 1 mm dust particle lifetime around HD 113766B of only ∼90,0000 years, suggesting that dust around HD 113766B is quickly removed, whereas 1 mm sized dust around HD 113766A can survive for >1.5 × 10{sup 6} years. At 10{sup 28}–10{sup 29} erg s{sup −1} X-ray luminosity, astrobiologically important effects, like dust warming and X-ray photolytic organic synthesis, are likely for any circumstellar material in the HD 113766 systems.

  18. Gamma-ray and X-ray emission from the Galactic centre: hints on the nuclear star cluster formation history

    Science.gov (United States)

    Arca-Sedda, Manuel; Kocsis, Bence; Brandt, Timothy D.

    2018-06-01

    The Milky Way centre exhibits an intense flux in the gamma and X-ray bands, whose origin is partly ascribed to the possible presence of a large population of millisecond pulsars (MSPs) and cataclysmic variables (CVs), respectively. However, the number of sources required to generate such an excess is much larger than what is expected from in situ star formation and evolution, opening a series of questions about the formation history of the Galactic nucleus. In this paper we make use of direct N-body simulations to investigate whether these sources could have been brought to the Galactic centre by a population of star clusters that underwent orbital decay and formed the Galactic nuclear star cluster (NSC). Our results suggest that the gamma ray emission is compatible with a population of MSPs that were mass segregated in their parent clusters, while the X-ray emission is consistent with a population of CVs born via dynamical interactions in dense star clusters. Combining observations with our modelling, we explore how the observed γ ray flux can be related to different NSC formation scenarios. Finally, we show that the high-energy emission coming from the galactic central regions can be used to detect black holes heavier than 105M⊙ in nearby dwarf galaxies.

  19. Studies of soft x-ray emission during solar flares

    International Nuclear Information System (INIS)

    Anandaram, M.N.

    1973-01-01

    Solar flare soft x-ray emission from 0.5 A to 8.5 A was observed during 1967-68 by Bragg crystal (LiF and EDDT) spectrometers aboard the OSO-4 satellite and also by NRL broad-band ionization detectors aboard the OGO-4 satellite. In this work, instrumental parameters for the LiF crystal spectrometer based on experimental values have been determined and used in the data analysis. The total continuum emission in the 0.5 to 3 A and the 1 to 8 A broad band segments has been determined from OGO-4 data for 21 flares. In doing this, a simple and approximate method of converting the total emission based on the gray body approximation (in which the OGO-4 data are reported) to one based on the thermal continuum spectrum has been developed. (author)

  20. X-ray emission spectroscopy of well-characterised non-LTE plasmas

    International Nuclear Information System (INIS)

    Bourgaux, A C; Bastiani-Ceccotti, S; Audebert, P; Marquès, J R; Vassura, L; Vinci, T; Jacquemot, S; Dorchies, F; Leguay, P M; Chung, H K; Bowen, C; Dervieux, V; Renaudin, P; Silvert, V

    2016-01-01

    This paper will present an experimental platform developed on LULI2000 to measure x-ray emission of non-LTE plasmas in well-defined hydrodynamic conditions thanks to implementation of a whole set of diagnostics, including time-resolved electronic and ionic Thomson scattering and self-optical pyrometry. K-, L- and M-shell spectra will be presented and the methodology, that has been developed to analyze them, discussed. (paper)

  1. Theoretically predicted soft x-ray emission and absorption spectra of graphitic-structured BC2N

    Science.gov (United States)

    Muramatsu, Yasuji

    Theoretical B K, C K and N K x-ray emission/absorption spectra of three possible graphitic-structured BC2N clusters are predicted based on the B2p-, C2p-, and N2p- density-of-states (DOS) calculated by discrete variational (DV)-X[alpha] molecular orbital calculations. Several prominent differences in DOS spectral features among BC2Ns, h-BN, and graphite are confirmed from comparison of calculated B2p-, C2p-, and N2p-DOS spectra. These variations in the spectra allow BC2N structures to be positively identified by high-resolution x-ray emission/absorption spectroscopy in the B K, C K, and N K regions.

  2. X-ray emission from a high-atomic-number z-pinch plasma created from compact wire arrays

    International Nuclear Information System (INIS)

    Sanford, T.W.L.; Nash, T.J.; Marder, B.M.

    1996-03-01

    Thermal and nonthermal x-ray emission from the implosion of compact tungsten wire arrays, driven by 5 MA from the Saturn accelerator, are measured and compared with LLNL Radiation-Hydro-Code (RHC) and SNL Hydro-Code (HC) numerical models. Multiple implosions, due to sequential compressions and expansions of the plasma, are inferred from the measured multiple x-radiation bursts. Timing of the multiple implosions and the thermal x-ray spectra measured between 1 and 10 keV are consistent with the RHC simulations. The magnitude of the nonthermal x-ray emission measured from 10 to 100 keV ranges from 0.02 to 0.08% of the total energy radiated and is correlated with bright-spot emission along the z-axis, as observed in earlier Gamble-11 single exploding-wire experiments. The similarities of the measured nonthermal spectrum and bright-spot emission with those measured at 0.8 MA on Gamble-II suggest a common production mechanism for this process. A model of electron acceleration across magnetic fields in highly-collisional, high-atomic-number plasmas is developed, which shows the existence of a critical electric field, E c , below which strong nonthermal electron creation (and the associated nonthermal x rays) do not occur. HC simulations show that significant nonthermal electrons are not expected in this experiment (as observed) because the calculated electric fields are at least one to two orders-of-magnitude below E c . These negative nonthermal results are confirmed by RHC simulations using a nonthermal model based on a Fokker-Plank analysis. Lastly, the lower production efficiency and the larger, more irregular pinch spots formed in this experiment relative to those measured on Gamble II suggest that implosion geometries are not as efficient as single exploding-wire geometries for warm x-ray production

  3. On the properties of synchrotron-like X-ray emission from laser wakefield accelerated electron beams

    Science.gov (United States)

    McGuffey, C.; Schumaker, W.; Matsuoka, T.; Chvykov, V.; Dollar, F.; Kalintchenko, G.; Kneip, S.; Najmudin, Z.; Mangles, S. P. D.; Vargas, M.; Yanovsky, V.; Maksimchuk, A.; Thomas, A. G. R.; Krushelnick, K.

    2018-04-01

    The electric and magnetic fields responsible for electron acceleration in a Laser Wakefield Accelerator (LWFA) also cause electrons to radiate x-ray photons. Such x-ray pulses have several desirable properties including short duration and being well collimated with tunable high energy. We measure the scaling of this x-ray source experimentally up to laser powers greater than 100 TW. An increase in laser power allows electron trapping at a lower density as well as with an increased trapped charge. These effects resulted in an x-ray fluence that was measured to increase non-linearly with laser power. The fluence of x-rays was also compared with that produced from K-α emission resulting from a solid target interaction for the same energy laser pulse. The flux was shown to be comparable, but the LWFA x-rays had a significantly smaller source size. This indicates that such a source may be useful as a backlighter for probing high energy density plasmas with ultrafast temporal resolution.

  4. Modeling Flare Hard X-ray Emission from Electrons in Contracting Magnetic Islands

    Science.gov (United States)

    Guidoni, Silvina E.; Allred, Joel C.; Alaoui, Meriem; Holman, Gordon D.; DeVore, C. Richard; Karpen, Judith T.

    2016-05-01

    The mechanism that accelerates particles to the energies required to produce the observed impulsive hard X-ray emission in solar flares is not well understood. It is generally accepted that this emission is produced by a non-thermal beam of electrons that collides with the ambient ions as the beam propagates from the top of a flare loop to its footpoints. Most current models that investigate this transport assume an injected beam with an initial energy spectrum inferred from observed hard X-ray spectra, usually a power law with a low-energy cutoff. In our previous work (Guidoni et al. 2016), we proposed an analytical method to estimate particle energy gain in contracting, large-scale, 2.5-dimensional magnetic islands, based on a kinetic model by Drake et al. (2010). We applied this method to sunward-moving islands formed high in the corona during fast reconnection in a simulated eruptive flare. The overarching purpose of the present work is to test this proposed acceleration model by estimating the hard X-ray flux resulting from its predicted accelerated-particle distribution functions. To do so, we have coupled our model to a unified computational framework that simulates the propagation of an injected beam as it deposits energy and momentum along its way (Allred et al. 2015). This framework includes the effects of radiative transfer and return currents, necessary to estimate flare emission that can be compared directly to observations. We will present preliminary results of the coupling between these models.

  5. The determination, by x-ray-fluorescence spectrometry, of gold, silver, and base metals on activated carbon

    International Nuclear Information System (INIS)

    Wall, G.; Jacobs, J.J.; Dixon, K.

    1980-01-01

    The method proposed involves ashing of the sample at a low temperature in a muffle furnace, mixing of the ash with alumina and boric acid in a Siebtechnik mill, and briquetting of the mixture. The elements are measured in the briquette by the use of x-ray fluorescence spectrometry. The detailed laboratory method is given in an appendix [af

  6. X-ray Emission from the Radio Jet in 3C 120

    DEFF Research Database (Denmark)

    Harris, D. E.; Hjorth, J.; Sadun, A. C.

    1999-01-01

    We report the discovery of X-ray emission from a radio knot at a projected distance of 25" from the nucleus of the Seyfert galaxy, 3C 120. The data were obtained with the ROSAT High Resolution Imager (HRI). Optical upper limits for the knot preclude a simple power law extension of the radio...

  7. Trace element determination in tomato puree using particle induced X-ray emission and Rutherford backscattering

    International Nuclear Information System (INIS)

    Romero-Davila, E.; Miranda, J.

    2004-01-01

    Particle induced X-ray emission (PIXE) and Rutherford backscattering spectrometry (RBS) were used to determine the concentrations of trace elements in samples of 12 tomato puree brands sold in the Mexican market. While RBS offered information about the main elements present in the matrix, PIXE gave results on trace elements. As a whole, data for 17 elements (C, N, O, Na, Mg, S, Cl, K, Ca, Ti, V, Cr, Mn, Fe, Ni, Cu, and Zn) were obtained. To evaluate the results, a comparison with brands from USA, Japan, Colombia, and Chile was carried out, using tomato purees produced following the domestic technology recipe. Additionally, the results were considered in the light of the Codex Alimentarius and the Mexican standard. It was found that all of the brands fall within the limits established by these standards, being of the same order of magnitude as the foreign brands. (author)

  8. X-RAY EMISSION FROM MAGNETIC MASSIVE STARS

    International Nuclear Information System (INIS)

    Nazé, Yaël; Petit, Véronique; Rinbrand, Melanie; Owocki, Stan; Cohen, David; Ud-Doula, Asif; Wade, Gregg A.

    2014-01-01

    Magnetically confined winds of early-type stars are expected to be sources of bright and hard X-rays. To clarify the systematics of the observed X-ray properties, we have analyzed a large series of Chandra and XMM-Newton observations, corresponding to all available exposures of known massive magnetic stars (over 100 exposures covering ∼60% of stars compiled in the catalog of Petit et al.). We show that the X-ray luminosity is strongly correlated with the stellar wind mass-loss rate, with a power-law form that is slightly steeper than linear for the majority of the less luminous, lower- M-dot B stars and flattens for the more luminous, higher- M-dot O stars. As the winds are radiatively driven, these scalings can be equivalently written as relations with the bolometric luminosity. The observed X-ray luminosities, and their trend with mass-loss rates, are well reproduced by new MHD models, although a few overluminous stars (mostly rapidly rotating objects) exist. No relation is found between other X-ray properties (plasma temperature, absorption) and stellar or magnetic parameters, contrary to expectations (e.g., higher temperature for stronger mass-loss rate). This suggests that the main driver for the plasma properties is different from the main determinant of the X-ray luminosity. Finally, variations of the X-ray hardnesses and luminosities, in phase with the stellar rotation period, are detected for some objects and they suggest that some temperature stratification exists in massive stars' magnetospheres

  9. Detailed EXOSAT and optical observations of the intermediate polar 3A0729+103: discovery of two medium energy X-ray emission regions

    International Nuclear Information System (INIS)

    McHardy, I.M.; Pye, J.P.; Fairall, A.P.; Menzies, J.W.

    1987-01-01

    EXOSAT observations of the intermediate polar cataclysmic variable 3A0729+103 reveal a strong orbital modulation, with the 2-4KeV X-rays being significantly more modulated than the 4-6keV X-rays, indicative of photoelectric absorption. The 913 second modulation which is very prominent in the optical light curve, is weakly detected in the medium-energy X-ray light curve, confirming that it represents the white dwarf spin period. These observations are well explained by a combination of two sources of medium-energy X-ray emission. The presence of two emission regions is also clearly seen in the optical spectroscopy, particularly in the intensity of the He II4686 line which has two peaks during the orbit. The authors identify the two optical emission regions with the two X-ray emission regions. (author)

  10. X rays from radio binaries

    International Nuclear Information System (INIS)

    Apparao, K.M.V.

    1977-01-01

    Reference is made to the radio binary systems CC Cas, AR Lac, β Per (Algol), β Lyr, b Per and Cyg X-1. It is stated that a thermal interpretation of the radiation from Algol requires a much larger x-ray flux than the observed value of 3.8 x 10 -11 erg/cm 2 /sec/keV in the 2 to 6 keV energy range. Observations of some non-thermal flares, together with the small size of the radio source in Algol, indicate that the radio emission is non-thermal in nature. The radio emission is interpreted as synchrotron radiation and it is suggested that the observed x-ray emission is due to inverse Compton scattering of the light of the primary star by the radio electrons. The x-ray emission from other radio binaries is also calculated using this model. The energy for the radio electrons can arise from annihilation of magnetic lines connecting the binary stars, twisted by the rotation of the stars. (U.K.)

  11. Optical and x-ray imaging of electron beams using synchrotron emission

    International Nuclear Information System (INIS)

    Wilke, M.

    1995-01-01

    In the case of very low emittance electron and positron storage ring beams, it is impossible to make intrusive measurements of beam properties without increasing the emittance and possibly disrupting the beam. In cases where electron or positron beams have high average power densities (such as free electron laser linacs), intrusive probes such as wires and optical transition radiation screens or Cherenkov emitting screens can be easily damaged or destroyed. The optical and x-ray emissions from the bends in the storage rings and often from linac bending magnets can be used to image the beam profile to obtain emittance information about the beam. The techniques, advantages and limitations of using both optical and x-ray synchrotron emission to measure beam properties are discussed and the possibility of single bunch imaging is considered. The properties of suitable imagers and converters such as phosphors are described. Examples of previous, existing and planned applications are given where available, including a pinhole imaging system currently being designed for the Advanced Photon Source at Argonne National Laboratory

  12. Optical and x-ray imaging of electron beams using synchrotron emission

    International Nuclear Information System (INIS)

    Wilke, M.D.

    1994-01-01

    In the case of very low eniittance electron and positron storage ring beams, it is impossible to make intrusive measurements of beam properties without increasing the emittance and possibly disrupting the beam. In cases where electron or positron beams have high average power densities (such as free electron laser linacs), intrusive probes such as wires and optical transition radiation screens or Cherenkov emitting screens can be easily damaged or destroyed. The optical and x-ray emissions from the bends in the storage rings and often from linac bending magnets can be used to image the beam profile to obtain emittance information about the beam. The techniques, advantages and limitations of using both optical and x-ray synchrotron emission to measure beam properties are discussed and the possibility of single bunch imaging is considered. The properties of suitable imagers and converters such as phosphors are described. Examples of previous, existing and planned applications are given where available, including a pinhole imaging system currently being designed for the Advanced Photon Source at Argonne National Laboratory

  13. Development and applications of grazing exit micro X-ray fluorescence instrument using a polycapillary X-ray lens

    International Nuclear Information System (INIS)

    Emoto, T.; Sato, Y.; Konishi, Y.; Ding, X.; Tsuji, K.

    2004-01-01

    A polycapillary X-ray lens is an effective optics to obtain a μm-size X-ray beam for micro-X-ray fluorescence spectrometry (μ-XRF). We developed a μ-XRF instrument using a polycapillary X-ray lens, which also enabled us to perform Grazing Exit μ-XRF (GE-μ-XRF). The evaluated diameter of the primary X-ray beam was 48 μm at the focal distance of the X-ray lens. Use of this instrument enabled two-dimensional mapping of the elemental distributions during growth of the plant 'Quinoa'. The results of the mapping revealed elemental transition during growth. In addition, a small region of thin film was analyzed by GE-μ-XRF. We expect that GE-μ-XRF will become an effective method of estimating the film thickness of a small region

  14. SERENDIPITOUS DETECTION OF X-RAY EMISSION FROM THE HOT BORN-AGAIN CENTRAL STAR OF THE PLANETARY NEBULA K 1-16

    Energy Technology Data Exchange (ETDEWEB)

    Montez, Rodolfo Jr. [Department of Physics and Astronomy, Vanderbilt University, Nashville, TN 37235 (United States); Kastner, Joel H., E-mail: rodolfo.montez.jr@gmail.com, E-mail: jhk@cis.rit.edu [Center for Imaging Science and Laboratory for Multiwavelength Astrophysics, Rochester Institute of Technology, 54 Lomb Memorial Drive, Rochester, NY 14623 (United States)

    2013-03-20

    We report the serendipitous detection of point-like X-ray emission from the hot, PG1159-type central star of the planetary nebula (CSPN) K 1-16 by the XMM-Newton and Chandra X-Ray Observatories. The CSPN lies superimposed on a galaxy cluster that includes an X-ray-bright quasar, but we have successfully isolated the CSPN X-ray emission from the strong diffuse background contributed by the quasar and intracluster gas. We have modeled the XMM-Newton and Chandra X-ray data, taking advantage of the contrasting detection efficiencies of the two observatories to better constrain the low-energy spectral response of Chandra's Advanced CCD Imaging Spectrometer. We find that the CSPN X-ray spectrum is well characterized by the combination of a non-local thermodynamic equilibrium model atmosphere with T{sub *} {approx} 135 kK and a carbon-rich, optically thin thermal plasma with T{sub X} {approx} 1 MK. These results for X-ray emission from the K 1-16 CSPN, combined with those obtained for other PG1159-type objects, lend support to the 'born-again' scenario for Wolf-Rayet and PG1159 CSPNe, wherein a late helium shell flash dredges up carbon-rich intershell material and ejects this material into the circumstellar environment.

  15. A DEEP X-RAY VIEW OF THE BARE AGN ARK 120. I. REVEALING THE SOFT X-RAY LINE EMISSION

    Energy Technology Data Exchange (ETDEWEB)

    Reeves, J. N.; Braito, V. [Center for Space Science and Technology, University of Maryland Baltimore County, 1000 Hilltop Circle, Baltimore, MD 21250 (United States); Porquet, D. [Observatoire Astronomique de Strasbourg, Université de Strasbourg, CNRS, UMR 7550, 11 rue de l’Université, F-67000 Strasbourg (France); Nardini, E. [Astrophysics Group, School of Physical and Geographical Sciences, Keele University, Keele, Staffordshire, ST5 5BG (United Kingdom); Lobban, A. [Dept of Physics and Astronomy, University of Leicester, University Road, Leicester LE1 7RH (United Kingdom); Turner, T. J., E-mail: jreeves@umbc.edu, E-mail: j.n.reeves@keele.ac.uk [Department of Physics, University of Maryland Baltimore County, 1000 Hilltop Circle, Baltimore, MD 21250 (United States)

    2016-09-10

    The Seyfert 1 galaxy Ark 120 is a prototype example of the so-called class of bare nucleus active galactic nuclei (AGNs), whereby there is no known evidence for the presence of ionized gas along the direct line of sight. Here deep (>400 ks exposure), high-resolution X-ray spectroscopy of Ark 120 is presented from XMM-Newton observations that were carried out in 2014 March, together with simultaneous Chandra /High Energy Transmission Grating exposures. The high-resolution spectra confirmed the lack of intrinsic absorbing gas associated with Ark 120, with the only X-ray absorption present originating from the interstellar medium (ISM) of our own Galaxy, with a possible slight enhancement of the oxygen abundance required with respect to the expected ISM values in the solar neighborhood. However, the presence of several soft X-ray emission lines are revealed for the first time in the XMM-Newton RGS spectrum, associated with the AGN and arising from the He- and H-like ions of N, O, Ne, and Mg. The He-like line profiles of N, O, and Ne appear velocity broadened, with typical FWHMs of ∼5000 km s{sup −1}, whereas the H-like profiles are unresolved. From the clean measurement of the He-like triplets, we deduce that the broad lines arise from a gas of density n {sub e} ∼ 10{sup 11} cm{sup −3}, while the photoionization calculations infer that the emitting gas covers at least 10% of 4 π steradian. Thus the broad soft X-ray profiles appear coincident with an X-ray component of the optical–UV broad-line region on sub-parsec scales, whereas the narrow profiles originate on larger parsec scales, perhaps coincident with the AGN narrow-line region. The observations show that Ark 120 is not intrinsically bare and substantial X-ray-emitting gas exists out of our direct line of sight toward this AGN.

  16. The Evolution of Normal Galaxy X-Ray Emission Through Cosmic History: Constraints from the 6 MS Chandra Deep Field-South

    Science.gov (United States)

    Lehmer, B. D.; Basu-Zych, A. R.; Mineo, S.; Brandt, W. N.; Eurfrasio, R. T.; Fragos, T.; Hornschemeier, A. E.; Lou, B.; Xue, Y. Q.; Bauer, F. E.; hide

    2016-01-01

    We present measurements of the evolution of normal-galaxy X-ray emission from z (is) approx. 0-7 using local galaxies and galaxy samples in the approx. 6 Ms Chandra Deep Field-South (CDF-S) survey. The majority of the CDF-S galaxies are observed at rest-frame energies above 2 keV, where the emission is expected to be dominated by X-ray binary (XRB) populations; however, hot gas is expected to provide small contributions to the observed-frame (is) less than 1 keV emission at z (is) less than 1. We show that a single scaling relation between X-ray luminosity (L(sub x)) and star-formation rate (SFR) literature, is insufficient for characterizing the average X-ray emission at all redshifts. We establish that scaling relations involving not only SFR, but also stellar mass and redshift, provide significantly improved characterizations of the average X-ray emission from normal galaxy populations at z (is) approx. 0-7. We further provide the first empirical constraints on the redshift evolution of X-ray emission from both low-mass XRB (LMXB) and high-mass XRB (HMXB) populations and their scalings with stellar mass and SFR, respectively. We find L2 -10 keV(LMXB)/stellar mass alpha (1+z)(sub 2-3) and L2 -10 keV(HMXB)/SFR alpha (1+z), and show that these relations are consistent with XRB population-synthesis model predictions, which attribute the increase in LMXB and HMXB scaling relations with redshift as being due to declining host galaxy stellar ages and metallicities, respectively. We discuss how emission from XRBs could provide an important source of heating to the intergalactic medium in the early universe, exceeding that of active galactic nuclei.

  17. Applications of simultaneous ion backscattering and ion-induced x-ray emission

    International Nuclear Information System (INIS)

    Musket, R.G.

    1983-05-01

    Simultaneous ion backscattering and ion-induced x-ray emission (E/sub x/greater than or equal to 300 eV) analyses have been performed using helium ions as probes of the first few hundred nanometers of various materials. These studies serve as a demonstration of the complementary nature of the two types of information obtained. Uncertainties associated with each of the individual techniques were reduced by performing both analyses. The principal advantages of simultaneous analyses over sequential analyses have been delineated

  18. X-ray spectroscopy and X-ray crystallography of metalloenzymes at XFELs

    International Nuclear Information System (INIS)

    Yano, Junko

    2016-01-01

    The ultra-bright femtosecond X-ray pulses provided by X-ray Free Electron Lasers (XFELs) open capabilities for studying the structure and dynamics of a wide variety of biological and inorganic systems beyond what is possible at synchrotron sources. Although the structure and chemistry at the catalytic sites have been studied intensively in both biological and inorganic systems, a full understanding of the atomic-scale chemistry requires new approaches beyond the steady state X-ray crystallography and X-ray spectroscopy at cryogenic temperatures. Following the dynamic changes in the geometric and electronic structure at ambient conditions, while overcoming X-ray damage to the redox active catalytic center, is key for deriving reaction mechanisms. Such studies become possible by using the intense and ultra-short femtosecond X-ray pulses from an XFEL, where sample is probed before it is damaged. We have developed methodology for simultaneously collecting crystallography data and X-ray emission spectra, using an energy dispersive spectrometer at ambient conditions. In addition, we have developed a way to collect metal L-edge data of dilute samples using soft X-rays at XFELs. The advantages and challenges of these methods will be described in this review. (author)

  19. X-Ray Study of Variable Gamma-Ray Pulsar PSR J2021+4026

    Science.gov (United States)

    Wang, H. H.; Takata, J.; Hu, C.-P.; Lin, L. C. C.; Zhao, J.

    2018-04-01

    PSR J2021+4026 showed a sudden decrease in the gamma-ray emission at the glitch that occurred around 2011 October 16, and a relaxation of the flux to the pre-glitch state at around 2014 December. We report X-ray analysis results of the data observed by XMM-Newton on 2015 December 20 in the post-relaxation state. To examine any change in the X-ray emission, we compare the properties of the pulse profiles and spectra at the low gamma-ray flux state and at the post-relaxation state. The phase-averaged spectra for both states can be well described by a power-law component plus a blackbody component. The former is dominated by unpulsed emission and probably originated from the pulsar wind nebula as reported by Hui et al. The emission property of the blackbody component is consistent with the emission from the polar cap heated by the back-flow bombardment of the high-energy electrons or positrons that were accelerated in the magnetosphere. We found no significant change in the X-ray emission properties between two states. We suggest that the change of the X-ray luminosity is at an order of ∼4%, which is difficult to measure with the current observations. We model the observed X-ray light curve with the heated polar cap emission, and we speculate that the observed large pulsed fraction is owing to asymmetric magnetospheric structure.

  20. Measurements of laser generated soft X-ray emission from irradiated gold foils

    Energy Technology Data Exchange (ETDEWEB)

    Davis, J. S.; Keiter, P. A.; Klein, S. R.; Drake, R. P.; Shvarts, D. [University of Michigan, 2455 Hayward St., Ann Arbor, Michigan 48109 (United States); Frank, Y.; Raicher, E.; Fraenkel, M. [Soreq Nuclear Research Center, Yavne (Israel)

    2016-11-15

    Soft x-ray emission from laser irradiated gold foils was measured at the Omega-60 laser system using the Dante photodiode array. The foils were heated with 2 kJ, 6 ns laser pulses and foil thicknesses were varied between 0.5, 1.0, and 2.0 μm. Initial Dante analysis indicates peak emission temperatures of roughly 100 eV and 80 eV for the 0.5 μm and 1.0 μm thick foils, respectively, with little measurable emission from the 2.0 μm foils.

  1. Specific features of thermocouple calorimeter application for measurements of pulsed X-ray emission from plasma

    International Nuclear Information System (INIS)

    Gavrilov, V. V.; Fasakhov, I. K.

    2012-01-01

    It is shown that the accuracy of time-integrated measurements of pulsed X-ray emission from hot plasma with calibrated thermocouple calorimeters is mainly determined by two factors. The first and the most important factor is heating of the filter by the absorbed X-rays; as a result, the calorimeter measures the thermal radiation of the filter, which causes appreciable distortion of the temporal profile and amplitude of the recorded signal. The second factor is the dependence of the effective depth of X-ray absorption in the dielectric that covers the entrance window of the calorimeter on the energy of X-ray photons, i.e., on the recorded radiation spectrum. The results of model calculations of the calorimeter signal are compared with the experimental data.

  2. 14th International Conference on Particle Induced X-ray Emission ("PIXE 2015")

    Science.gov (United States)

    Przybyłowicz, Wojciech Józef; Pineda-Vargas, Carlos

    2015-11-01

    This special issue of Nuclear Instruments and Methods in Physics Research B contains the proceedings of the 14th International Conference on Particle Induced X-ray Emission ("PIXE 2015") that was held in Somerset West (South Africa) from 25th February to 3rd March 2015.

  3. X-ray fluorescence analysis in environmental radiological surveillance using HPGe detectors

    International Nuclear Information System (INIS)

    Herrera Peraza, E.; Renteria Villalobos, M.; Montero Cabrera, M.E.; Munoz Romero, A.

    2004-01-01

    X-ray fluorescence (XRF) has been proven to be a valuable tool for determining trace quantities of heavy metals, such as uranium and lead, in different types of samples. The present paper demonstrates the applicability of XRF spectrometry to measure the concentrations of these heavy metals in samples from natural ore and soil. The values of uranium concentrations in rock from the Pena Blanca uranium ore, in Chihuahua, Mexico, were calculated for the purpose of precertifying the rock powders samples. The comparison with other techniques, such as inductively coupled plasma atomic emission spectrometry, atomic absorption spectrometry, alpha spectrometry and electron microscopy, was used to complete the precertification process, so that the sample powders may be used as secondary standards. The source-sample-detector geometry and the incident angle are the most important factors for obtaining low detection limits. The selected system uses a 57 Co source of about 0.1 mCi to excite the K X-rays from uranium and lead. X-rays were recorded on a CANBERRA HPGe coaxial detector. The comparative results for two incident angles (90 deg and 180 deg ) performed previously by other authors show that the best geometry is the backscattering geometry. In the present paper, using EGS4 code system with Monte Carlo simulation, it was possible to determine the location and distribution of background produced by the Compton edge in the optimized geometry. This procedure allowed to find the minimum detectable concentration of uranium and lead, which was experimentally calculated using standards. The possibility of performing in vivo measurements rapidly and easily, as well as the factors affecting accuracy and the minimum detectable concentration in several samples are also discussed

  4. X-ray fluorescence analysis in environmental radiological surveillance using HPGe detectors

    Energy Technology Data Exchange (ETDEWEB)

    Herrera Peraza, E. [Department of Environmental Radiological Surveillance, Centro de Investigacion en Materiales Avanzados (CIMAV), P.O. Box 31109, Miguel de Cervantes no. 120, Complejo Industrial Chihuahua, Chihuahua (Mexico)]. E-mail: eduardo.herrera@cimav.edu.mx; Renteria Villalobos, M. [Department of Environmental Radiological Surveillance, Centro de Investigacion en Materiales Avanzados (CIMAV), P.O. Box 31109, Miguel de Cervantes no. 120, Complejo Industrial Chihuahua, Chihuahua (Mexico); Montero Cabrera, M.E. [Department of Environmental Radiological Surveillance, Centro de Investigacion en Materiales Avanzados (CIMAV), P.O. Box 31109, Miguel de Cervantes no. 120, Complejo Industrial Chihuahua, Chihuahua (Mexico); Munoz Romero, A. [Department of Environmental Radiological Surveillance, Centro de Investigacion en Materiales Avanzados (CIMAV), P.O. Box 31109, Miguel de Cervantes no. 120, Complejo Industrial Chihuahua, Chihuahua (Mexico)

    2004-10-08

    X-ray fluorescence (XRF) has been proven to be a valuable tool for determining trace quantities of heavy metals, such as uranium and lead, in different types of samples. The present paper demonstrates the applicability of XRF spectrometry to measure the concentrations of these heavy metals in samples from natural ore and soil. The values of uranium concentrations in rock from the Pena Blanca uranium ore, in Chihuahua, Mexico, were calculated for the purpose of precertifying the rock powders samples. The comparison with other techniques, such as inductively coupled plasma atomic emission spectrometry, atomic absorption spectrometry, alpha spectrometry and electron microscopy, was used to complete the precertification process, so that the sample powders may be used as secondary standards. The source-sample-detector geometry and the incident angle are the most important factors for obtaining low detection limits. The selected system uses a {sup 57}Co source of about 0.1 mCi to excite the K X-rays from uranium and lead. X-rays were recorded on a CANBERRA HPGe coaxial detector. The comparative results for two incident angles (90 deg and 180 deg ) performed previously by other authors show that the best geometry is the backscattering geometry. In the present paper, using EGS4 code system with Monte Carlo simulation, it was possible to determine the location and distribution of background produced by the Compton edge in the optimized geometry. This procedure allowed to find the minimum detectable concentration of uranium and lead, which was experimentally calculated using standards. The possibility of performing in vivo measurements rapidly and easily, as well as the factors affecting accuracy and the minimum detectable concentration in several samples are also discussed.

  5. X-Ray Emission from an Asymmetric Blast Wave and a Massive White Dwarf in the Gamma Ray Emitting Nova V407 CYG

    Science.gov (United States)

    Nelson, Thomas; Donato, Davide; Mukai, Koji; Sokoloski, Jennifer; Chomiuk, Laura

    2012-01-01

    Classical nova events in symbiotic stars, although rare, offer a unique opportunity to probe the interaction between ejecta and a dense environment in stellar explosions. In this work, we use X-ray data obtained with Swift and Suzaku during the recent classical nova outburst in V407 Cyg to explore such an interaction. We find evidence of both equilibrium and non-equilibrium ionization plasmas at the time of peak X-ray brightness, indicating a strong asymmetry in the density of the emitting region. Comparing a simple model to the data, we find that the X-ray evolution is broadly consistent with nova ejecta driving a forward shock into the dense wind of the Mira companion. We detect a highly absorbed soft X-ray component in the spectrum during the first 50 days of the outburst that is consistent with supersoft emission from the nuclear burning white dwarf. The high temperature and short turn off time of this emission component, in addition to the observed breaks in the optical and UV lightcurves, indicate that the white dwarf in the binary is extremely massive. Finally, we explore the connections between the X-ray and GeV-ray evolution, and propose that the gamma ray turn-off is due to the stalling of the forward shock as the ejecta reach the red giant surface.

  6. X pinch a point x-ray source

    International Nuclear Information System (INIS)

    Garg, A.B.; Rout, R.K.; Shyam, A.; Srinivasan, M.

    1993-01-01

    X ray emission from an X pinch, a point x-ray source has been studied using a pin-hole camera by a 30 kV, 7.2 μ F capacitor bank. The wires of different material like W, Mo, Cu, S.S.(stainless steel) and Ti were used. Molybdenum pinch gives the most intense x-rays and stainless steel gives the minimum intensity x-rays for same bank energy (∼ 3.2 kJ). Point x-ray source of size (≤ 0.5 mm) was observed using pin hole camera. The size of the source is limited by the size of the pin hole camera. The peak current in the load is approximately 150 kA. The point x-ray source could be useful in many fields like micro lithography, medicine and to study the basic physics of high Z plasmas. (author). 4 refs., 3 figs

  7. Applications of X-ray Computed Tomography and Emission Computed Tomography

    International Nuclear Information System (INIS)

    Seletchi, Emilia Dana; Sutac, Victor

    2005-01-01

    Computed Tomography is a non-destructive imaging method that allows visualization of internal features within non-transparent objects such as sedimentary rocks. Filtering techniques have been applied to circumvent the artifacts and achieve high-quality images for quantitative analysis. High-resolution X-ray computed tomography (HRXCT) can be used to identify the position of the growth axis in speleothems by detecting subtle changes in calcite density between growth bands. HRXCT imagery reveals the three-dimensional variability of coral banding providing information on coral growth and climate over the past several centuries. The Nuclear Medicine imaging technique uses a radioactive tracer, several radiation detectors, and sophisticated computer technologies to understand the biochemical basis of normal and abnormal functions within the brain. The goal of Emission Computed Tomography (ECT) is to accurately determine the three-dimensional radioactivity distribution resulting from the radiopharmaceutical uptake inside the patient instead of the attenuation coefficient distribution from different tissues as obtained from X-ray Computer Tomography. ECT is a very useful tool for investigating the cognitive functions. Because of the low radiation doses associated with Positron Emission Tomography (PET), this technique has been applied in clinical research, allowing the direct study of human neurological diseases. (authors)

  8. X ray emission experiments at 1.06 μm and 0.35 μm

    International Nuclear Information System (INIS)

    Babonneau, D.; Billon, D.; Bocher, J.L.; Di Bona, G.; Fortin, X.; Thiell, G.

    1982-10-01

    Experiments and analyses on high-Z targets X-ray emission are reported. Two kinds of targets have been used: spherical targets with Octal laser (1.06 μm; 10 13 to 10 13 to 10 15 W/cm 2 ) and planar targets with P102 laser (0.35μm; 3 x 10 13 to 3 x 10 14 W/cm 2 ). The influence of the different parameters (laser flux, laser wavelength, atomic number) on emission rates and spectra is discussed. The results about the emission rates are compared with data from other laboratories and an experimental scaling law is proposed. Temperatures can be evaluated from experimental spectra and related to the different plasma regions. Space-time resolved measurements with a streak camera, from spherical targets, in the (1 - 1.3 keV) energy range allow to determine a velocity: about 6 x 10 6 cm/s for the emission region

  9. The EVE plus RHESSI DEM for Solar Flares, and Implications for Residual Non-Thermal X-Ray Emission

    Science.gov (United States)

    McTiernan, James; Caspi, Amir; Warren, Harry

    2016-05-01

    Solar flare spectra are typically dominated by thermal emission in the soft X-ray energy range. The low energy extent of non-thermal emission can only be loosely quantified using currently available X-ray data. To address this issue, we combine observations from the EUV Variability Experiment (EVE) on-board the Solar Dynamics Observatory (SDO) with X-ray data from the Reuven Ramaty High Energy Spectroscopic Imager (RHESSI) to calculate the Differential Emission Measure (DEM) for solar flares. This improvement over the isothermal approximation helps to resolve the ambiguity in the range where the thermal and non-thermal components may have similar photon fluxes. This "crossover" range can extend up to 30 keV.Previous work (Caspi et.al. 2014ApJ...788L..31C) concentrated on obtaining DEM models that fit both instruments' observations well. For this current project we are interested in breaks and cutoffs in the "residual" non-thermal spectrum; i.e., the RHESSI spectrum that is left over after the DEM has accounted for the bulk of the soft X-ray emission. As in our earlier work, thermal emission is modeled using a DEM that is parametrized as multiple gaussians in temperature. Non-thermal emission is modeled as a photon spectrum obtained using a thin-target emission model ('thin2' from the SolarSoft Xray IDL package). Spectra for both instruments are fit simultaneously in a self-consistent manner.For this study, we have examined the DEM and non-thermal resuidual emission for a sample of relatively large (GOES M class and above) solar flares observed from 2011 to 2014. The results for the DEM and non-thermal parameters found using the combined EVE-RHESSI data are compared with those found using only RHESSI data.

  10. The Imaging X-ray Polarimetry Explorer (IXPE

    Directory of Open Access Journals (Sweden)

    Martin C. Weisskopf

    Full Text Available The Imaging X-ray Polarimetry Explorer (IXPE expands observation space by simultaneously adding polarization to the array of X-ray source properties currently measured (energy, time, and location. IXPE will thus open new dimensions for understanding how X-ray emission is produced in astrophysical objects, especially in systems under extreme physical conditions. Keywords: X-ray astronomy, X-ray polarimetry, X-ray imaging

  11. THE RADIATIVE X-RAY AND GAMMA-RAY EFFICIENCIES OF ROTATION-POWERED PULSARS

    International Nuclear Information System (INIS)

    Vink, Jacco; Bamba, Aya; Yamazaki, Ryo

    2011-01-01

    We present a statistical analysis of the X-ray luminosity of rotation-powered pulsars and their surrounding nebulae using the sample of Kargaltsev and Pavlov, and we complement this with an analysis of the γ-ray emission of Fermi-detected pulsars. We report a strong trend in the efficiency with which spin-down power is converted to X-ray and γ-ray emission with characteristic age: young pulsars and their surrounding nebulae are efficient X-ray emitters, whereas in contrast old pulsars are efficient γ-ray emitters. We divided the X-ray sample in a young (τ c 4 yr) and old sample and used linear regression to search for correlations between the logarithm of the X-ray and γ-ray luminosities and the logarithms of the periods and period derivatives. The X-ray emission from young pulsars and their nebulae are both consistent with L X ∝ P-dot 3 /P 6 . For old pulsars and their nebulae the X-ray luminosity is consistent with a more or less constant efficiency η≡L X / E-dot rot ∼8x10 -5 . For the γ-ray luminosity we confirm that L γ ∝ √E-dot rot . We discuss these findings in the context of pair production inside pulsar magnetospheres and the striped wind model. We suggest that the striped wind model may explain the similarity between the X-ray properties of the pulsar wind nebulae and the pulsars themselves, which according to the striped wind model may both find their origin outside the light cylinder, in the pulsar wind zone.

  12. Development and applications of grazing exit micro X-ray fluorescence instrument using a polycapillary X-ray lens

    Energy Technology Data Exchange (ETDEWEB)

    Emoto, T.; Sato, Y.; Konishi, Y.; Ding, X.; Tsuji, K. E-mail: tsuji@a-chem.eng.osaka-cu.ac.jp

    2004-08-31

    A polycapillary X-ray lens is an effective optics to obtain a {mu}m-size X-ray beam for micro-X-ray fluorescence spectrometry ({mu}-XRF). We developed a {mu}-XRF instrument using a polycapillary X-ray lens, which also enabled us to perform Grazing Exit {mu}-XRF (GE-{mu}-XRF). The evaluated diameter of the primary X-ray beam was 48 {mu}m at the focal distance of the X-ray lens. Use of this instrument enabled two-dimensional mapping of the elemental distributions during growth of the plant 'Quinoa'. The results of the mapping revealed elemental transition during growth. In addition, a small region of thin film was analyzed by GE-{mu}-XRF. We expect that GE-{mu}-XRF will become an effective method of estimating the film thickness of a small region.

  13. Application of X-ray fluorescence analytical techniques in phytoremediation and plant biology studies

    International Nuclear Information System (INIS)

    Necemer, Marijan; Kump, Peter; Scancar, Janez; Jacimovic, Radojko; Simcic, Jurij; Pelicon, Primoz; Budnar, Milos; Jeran, Zvonka; Pongrac, Paula; Regvar, Marjana; Vogel-Mikus, Katarina

    2008-01-01

    Phytoremediation is an emerging technology that employs the use of higher plants for the clean-up of contaminated environments. Progress in the field is however handicapped by limited knowledge of the biological processes involved in plant metal uptake, translocation, tolerance and plant-microbe-soil interactions; therefore a better understanding of the basic biological mechanisms involved in plant/microbe/soil/contaminant interactions would allow further optimization of phytoremediation technologies. In view of the needs of global environmental protection, it is important that in phytoremediation and plant biology studies the analytical procedures for elemental determination in plant tissues and soil should be fast and cheap, with simple sample preparation, and of adequate accuracy and reproducibility. The aim of this study was therefore to present the main characteristics, sample preparation protocols and applications of X-ray fluorescence-based analytical techniques (energy dispersive X-ray fluorescence spectrometry-EDXRF, total reflection X-ray fluorescence spectrometry-TXRF and micro-proton induced X-ray emission-micro-PIXE). Element concentrations in plant leaves from metal polluted and non-polluted sites, as well as standard reference materials, were analyzed by the mentioned techniques, and additionally by instrumental neutron activation analysis (INAA) and atomic absorption spectrometry (AAS). The results were compared and critically evaluated in order to assess the performance and capability of X-ray fluorescence-based techniques in phytoremediation and plant biology studies. It is the EDXRF, which is recommended as suitable to be used in the analyses of a large number of samples, because it is multi-elemental, requires only simple preparation of sample material, and it is analytically comparable to the most frequently used instrumental chemical techniques. The TXRF is compatible to FAAS in sample preparation, but relative to AAS it is fast, sensitive and

  14. Soft x-ray Planetary Imager

    Data.gov (United States)

    National Aeronautics and Space Administration — The project is to prototype a soft X-ray Imager for planetary applications that has the sensitivity to observe solar system sources of soft  X-ray emission. A strong...

  15. X-ray heating and ionization of broad-emission-line regions in QSO's and active galaxies

    International Nuclear Information System (INIS)

    Weisheit, J.C.; Shields, G.A.; Tarter, C.B.

    1980-07-01

    Absorption of x-rays deep within the broad-line emitting clouds in QSO's and the nuclei of active galaxies creates extensive zones of warm (T approx. 10 4 K), partially ionized N/sub e//N approx. 0.1) gas. Because Lyman alpha photons are trapped in these regions, the x-ray energy is efficiently channeled into Balmer lines collisionally excited from the n = 2 level. The HI regions plus the HII regions created by ultraviolet photons illuminating the surfaces of the clouds give rise to integrated Lα/Hα line emission ratios between 1 and 2. Enhanced MgII line emission from the HI regions gives rise to integrated MgII/Hα ratios near 0.5. The OI line lambda 8446 is efficiently pumped by trapped Hα photons and in the x-ray heated zone an intensity ratio I (lambda 8446)/I(Hα) approx. < 0.1 is calculated. All of these computed ratios now are in agreement with observations

  16. X-Pinch And Its Applications In X-ray Radiograph

    International Nuclear Information System (INIS)

    Zou Xiaobing; Wang Xinxin; Liu Rui; Zhao Tong; Zeng Naigong; Zhao Yongchao; Du Yanqiang

    2009-01-01

    An X-pinch device and the related diagnostics of x-ray emission from X-pinch were briefly described. The time-resolved x-ray measurements with photoconducting diodes show that the x-ray pulse usually consists of two subnanosecond peaks with a time interval of about 0.5 ns. Being consistent with these two peaks of the x-ray pulse, two point x-ray sources of size ranging from 100 μm to 5 μm and depending on cut-off x-ray photon energy were usually observed on the pinhole pictures. The x-pinch was used as x-ray source for backlighting of the electrical explosion of single wire and the evolution of X-pinch, and for phase-contrast imaging of soft biological objects such as a small shrimp and a mosquito.

  17. Correlated X-ray/UV/optical emission and short-term variability in a Seyfert 1 galaxy NGC 4593

    Science.gov (United States)

    Pal, Main; Naik, Sachindra

    2018-03-01

    We present a detailed multifrequency analysis of an intense monitoring programme of Seyfert 1 galaxy NGC 4593 over a duration of nearly for a month with Swift observatory. We used 185 pointings to study the variability in six ultraviolet/optical and two soft (0.3-1.5 keV) and hard X-ray (1.5-10 keV) bands. The amplitude of the observed variability is found to decrease from high energy to low energy (X-ray to optical) bands. Count-count plots of ultraviolet/optical bands with hard X-rays clearly suggest the presence of a mixture of two major components: (i) highly variable component such as hard X-ray emission, and (ii) slowly varying disc-like component. The variations observed in the ultraviolet/optical emission are strongly correlated with the hard X-ray band. Cross-correlation analysis provides the lags for the longer wavelengths compared to the hard X-rays. Such lags clearly suggest that the changes in the ultraviolet/optical bands follow the variations in the hard X-ray band. This implies that the observed variation in longer wavelengths is due to X-ray reprocessing. Though, the measured lag spectrum (lag versus wavelength) is well described by λ4/3 as expected from the standard disc model, the observed lags are found to be longer than the predicted values from standard disc model. This implies that the actual size of the disc of NGC 4593 is larger than the estimated size of standard thin disc as reported in active galactic nuclei such as NGC 5548 and Fairall 9.

  18. Method and multichannel equipment for chemical analysis by X-ray emission

    International Nuclear Information System (INIS)

    Bacso, J.; Horkay, Gy.; Kalinka, G.; Kertesz, Zs.; Kiss Varga, M.; Lakatos, T.; Mathe, Gy.; Paal, A.; Sulik, B.

    1978-01-01

    In the patent a simple method and an apparatus are described for chemical analysis based on X-ray emission generated by irradiation. The concentrations of pre-selected elements can be determined easily by this method using an equipment containing microprocessor. The number of channels and the elements to be determined can be modified by a simple change in the program. (Sz.J.)

  19. Analysis of trace elements in ceramic prints on automobile glasses for forensic examination using high-energy synchrotron radiation x-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Nishiwaki, Yoshinori; Takatsu, Masahisa; Miyamoto, Naoki; Watanabe, Seiya; Shimoda, Osamu; Muratsu, Seiji; Nakanishi, Toshio; Nakai, Izumi

    2007-01-01

    This study revealed that high-energy SRXRF (synchrotron radiation X-ray fluorescence spectrometry) utilizing 75.5 keV X-rays of SPring-8 is a powerful technique for trace elemental analysis of ceramic prints on automotive glasses for forensic examination. Fragments of 99 ceramic prints were collected from automobiles of various manufacturers, types and model years. Their major heavy element-components were found to be either Pb or Bi. Because of recent environment protection movement for lead-free material, there was a tendency of the shift of material from the Pb Type to the Bi Type with years of the production. A utilization of 75.5 keV X-rays as excitation source allowed us to detect trace heavy-elements, such as Sb, La, Ce, Hf and W, as well as relatively light-elements, such as V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Zr and Mo, in samples using K series of XRF emission lines. XRF intensities of these elements normalized by those of the major heavy-elements (Pb or Bi) became characteristic finger prints, showing the identity of each sample with a size of less than 0.5x0.5 mm 2 . The mean relative standard deviations of the normalized XRF intensities measured for the three fragments of each sample were less than 9.3%. These results show that the ceramic prints on automobile glasses contain rich elemental information for discrimination, and therefore the materials can be important evidence for practical forensic examinations. (author)

  20. Discovery of radio emission from the symbiotic X-ray binary system GX 1+4

    Science.gov (United States)

    van den Eijnden, J.; Degenaar, N.; Russell, T. D.; Miller-Jones, J. C. A.; Wijnands, R.; Miller, J. M.; King, A. L.; Rupen, M. P.

    2018-02-01

    We report the discovery of radio emission from the accreting X-ray pulsar and symbiotic X-ray binary GX 1+4 with the Karl G. Jansky Very Large Array. This is the first radio detection of such a system, wherein a strongly magnetized neutron star accretes from the stellar wind of an M-type giant companion. We measure a 9 GHz radio flux density of 105.3 ± 7.3 μJy, but cannot place meaningful constraints on the spectral index due to a limited frequency range. We consider several emission mechanisms that could be responsible for the observed radio source. We conclude that the observed properties are consistent with shocks in the interaction of the accretion flow with the magnetosphere, a synchrotron-emitting jet, or a propeller-driven outflow. The stellar wind from the companion is unlikely to be the origin of the radio emission. If the detected radio emission originates from a jet, it would show that strong magnetic fields (≥1012 G) do not necessarily suppress jet formation.

  1. Heavy metal determination by X-rays spectrometry in superficial sediments at Havana Bay

    International Nuclear Information System (INIS)

    Gelen, Alina; Izquierdo, Walter; Lopez, Neivy; Corrales, Yasser; Casanova, Amaya O.; Diaz, Oscar; Manso, Maria V.; D'Alessandro, Katia; Reyes, Enma; Toledo, Carlos; Beltran, Jesus; Perez, Marlen; Ramirez, Marta; Soto, Jesus

    2007-01-01

    Havana Bay is a typical bag-type located in the Western-North Coast of the Republic of Cuba. Since 1980 it has been the object of a study for sea bottom rehabilitation and improvement of quality of the waters, where the final objective will be the recovery of the coastal and marine ecosystem. Thirteen surface samples of the Havana Bay (Cuba) were collected and analysed by X-Rays spectrometry. Some majority elements (Si, Ca, K, Na, S, Cl, Al, Fe, Mg, C and O) were measured by scanning electron microscopy (SEM) coupled with microanalysis to perform geomorphologic analysis. Nine elements (Ca, Fe, Ti, Mn, Cu, Zn, Sr, Zr and Pb) have been measured using an Energy Dispersive X-Ray Fluorescence (EDXRF) with a Si(Li) detector. Multivariate statistical was used for the analysis. The concentration levels showed this bay as the most polluted in Cuba. The highest contents of Cu, Zn and Pb were obtained in Atares and Marimelena Cove; these elements are indicators of urban as well as industrial pollution. (author)

  2. Heavy metal determination by X-rays spectrometry in superficial sediments at Havana Bay

    Energy Technology Data Exchange (ETDEWEB)

    Gelen, Alina; Izquierdo, Walter; Lopez, Neivy; Corrales, Yasser; Casanova, Amaya O.; Diaz, Oscar; Manso, Maria V.; D' Alessandro, Katia [Institute for Applied Sciences and Technology, Havana (Cuba)], E-mail: alina@instec.cu; Reyes, Enma; Toledo, Carlos [Central Laboratory Criminology, Havana (Cuba); Beltran, Jesus; Perez, Marlen; Ramirez, Marta [Engineering Centre for Environmental Management of Bays and Coasts, Havana (Cuba)], E-mail: beltran@cimab.transnet.cu; Soto, Jesus [Universidad de Cantabria, Santander (Spain)], E-mail: sotoj@unican.es

    2007-07-01

    Havana Bay is a typical bag-type located in the Western-North Coast of the Republic of Cuba. Since 1980 it has been the object of a study for sea bottom rehabilitation and improvement of quality of the waters, where the final objective will be the recovery of the coastal and marine ecosystem. Thirteen surface samples of the Havana Bay (Cuba) were collected and analysed by X-Rays spectrometry. Some majority elements (Si, Ca, K, Na, S, Cl, Al, Fe, Mg, C and O) were measured by scanning electron microscopy (SEM) coupled with microanalysis to perform geomorphologic analysis. Nine elements (Ca, Fe, Ti, Mn, Cu, Zn, Sr, Zr and Pb) have been measured using an Energy Dispersive X-Ray Fluorescence (EDXRF) with a Si(Li) detector. Multivariate statistical was used for the analysis. The concentration levels showed this bay as the most polluted in Cuba. The highest contents of Cu, Zn and Pb were obtained in Atares and Marimelena Cove; these elements are indicators of urban as well as industrial pollution. (author)

  3. Behavior of hard X-ray emission in discharges with current disruptions in the DAMAVAND and TVD tokamaks

    International Nuclear Information System (INIS)

    Farshi, E.; Amrollahy, R.; Bortnikov, A.V.; Brevnov, N.N.; Gott, Yu.V.; Shurygin, V.A.

    2001-01-01

    Results are presented from studies of the behavior of hard X-ray emission in discharges with current disruptions in the DAMAVAND and TVD tokamaks. The current disruptions are caused by either an MHD instability or the instability related to the vertical displacement of the plasma column. Experiments were conducted at a fixed value of the safety factor at the plasma boundary (q a ≅ 2.3). Experimental data show that, during a disruption caused by an MHD instability, hard X-ray emission is suppressed by this instability if the amplitude of the magnetic field fluctuations exceeds a certain level. If the disruption is caused by the instability related to the vertical displacement of the plasma column, then hard X-ray emission is observed at the instant of disruption. The experimental results show that the physical processes resulting in the generation and suppression of runaway electron beams are almost identical in large and small tokamaks

  4. NuSTAR detection of high-energy X-ray emission and rapid variability from Sagittarius A{sup *} flares

    Energy Technology Data Exchange (ETDEWEB)

    Barrière, Nicolas M.; Tomsick, John A.; Boggs, Steven E.; Craig, William W.; Zoglauer, Andreas [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Baganoff, Frederick K. [Kavli Institute for Astrophysics and Space Research, Massachusetts Institute of Technology, Cambridge, MA 02139-4307 (United States); Christensen, Finn E. [DTU Space, National Space Institute, Technical University of Denmark, Elektrovej 327, DK-2800 Kgs. Lyngby (Denmark); Dexter, Jason [Departments of Physics and Astronomy, University of California, Berkeley, CA 94720 (United States); Grefenstette, Brian; Harrison, Fiona A.; Madsen, Kristin K. [Cahill Center for Astronomy and Astrophysics, Caltech, Pasadena, CA 91125 (United States); Hailey, Charles J.; Mori, Kaya; Zhang, Shuo [Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Stern, Daniel [Jet Propulsion Laboratory, California Institute of Technology, Pasadena, CA 91109 (United States); Zhang, William W. [X-ray Astrophysics Laboratory, NASA Goddard Space Flight Center, Greenbelt, MD 20771 (United States)

    2014-05-01

    Sagittarius A{sup *} harbors the supermassive black hole that lies at the dynamical center of our Galaxy. Sagittarius A{sup *} spends most of its time in a low luminosity emission state but flares frequently in the infrared and X-ray, increasing up to a few hundred fold in brightness for up to a few hours at a time. The physical processes giving rise to the X-ray flares are uncertain. Here we report the detection with the NuSTAR observatory in Summer and Fall 2012 of four low to medium amplitude X-ray flares to energies up to 79 keV. For the first time, we clearly see that the power-law spectrum of Sagittarius A{sup *} X-ray flares extends to high energy, with no evidence for a cutoff. Although the photon index of the absorbed power-law fits are in agreement with past observations, we find a difference between the photon index of two of the flares (significant at the 95% confidence level). The spectra of the two brightest flares (∼55 times quiescence in the 2-10 keV band) are compared to simple physical models in an attempt to identify the main X-ray emission mechanism, but the data do not allow us to significantly discriminate between them. However, we confirm the previous finding that the parameters obtained with synchrotron models are, for the X-ray emission, physically more reasonable than those obtained with inverse Compton models. One flare exhibits large and rapid (<100 s) variability, which, considering the total energy radiated, constrains the location of the flaring region to be within ∼10 Schwarzschild radii of the black hole.

  5. Comparing neutron and X-ray images from NIF implosions

    Directory of Open Access Journals (Sweden)

    Wilson D.C.

    2013-11-01

    Full Text Available Directly laser driven and X-radiation driven DT filled capsules differ in the relationship between neutron and X-ray images. Shot N110217, a directly driven DT-filled glass micro-balloon provided the first neutron images at the National Ignition Facility. As seen in implosions on the Omega laser, the neutron image can be enclosed inside time integrated X-ray images. HYDRA simulations show the X-ray image is dominated by emission from the hot glass shell while the neutron image arises from the DT fuel it encloses. In the absence of mix or jetting, X-ray images of a cryogenically layered THD fuel capsule should be dominated by emission from the hydrogen rather than the cooler plastic shell that is separated from the hot core by cold DT fuel. This cool, dense DT, invisible in X-ray emission, shows itself by scattering hot core neutrons. Germanium X-ray emission spectra and Ross pair filtered X-ray energy resolved images suggest that germanium doped plastic emits in the torus shaped hot spot, probably reducing the neutron yield.

  6. Characteristics of a molybdenum X-pinch X-ray source as a probe source for X-ray diffraction studies

    International Nuclear Information System (INIS)

    Zucchini, F.; Chauvin, C.; Combes, P.; Sol, D.; Loyen, A.; Roques, B.; Grunenwald, J.; Bland, S. N.

    2015-01-01

    X-ray emission from a molybdenum X-pinch has been investigated as a potential probe for the high pressure states made in dynamic compression experiments. Studies were performed on a novel 300 kA, 400 ns generator which coupled the load directly to a low inductance capacitor and switch combination. The X-pinch load consisted of 4 crossed molybdenum wires of 13 μm diameter, crossed at an angle of 62°. The load height was 10 mm. An initial x-ray burst generated at the wire crossing point, radiated in the soft x-ray range (hυ < 10 keV). This was followed, 2–5 ns later, by at least one harder x-ray burst (hυ > 10 keV) whose power ranged from 1 to 7 MW. Time integrated spectral measurements showed that the harder bursts were dominated by K-alpha emission; though, a lower level, wide band continuum up to at least 30 keV was also present. Initial tests demonstrated that the source was capable of driving Laue diffraction experiments, probing uncompressed samples of LiF and aluminium

  7. X-Ray Emission from Compact Sources

    Energy Technology Data Exchange (ETDEWEB)

    Cominsky, L

    2004-03-23

    This paper presents a review of the physical parameters of neutron stars and black holes that have been derived from X-ray observations. I then explain how these physical parameters can be used to learn about the extreme conditions occurring in regions of strong gravity, and present some recent evidence for relativistic effects seen in these systems. A glossary of commonly used terms and a short tutorial on the names of X-ray sources are also included.

  8. X-Ray Spectral Diagnostics of Gamma-Ray Burst Environments.

    Science.gov (United States)

    Paerels; Kuulkers; Heise; Liedahl

    2000-05-20

    Recently, detection of discrete features in the X-ray afterglow spectra of GRB 970508 and GRB 970828 was reported. The most natural interpretation of these features is that they are redshifted Fe K emission complexes. The identification of the line emission mechanism has drastic implications for the inferred mass of radiating material and hence the nature of the burst site. X-ray spectroscopy provides a direct observational constraint on these properties of gamma-ray bursters. We briefly discuss how these constraints arise in the context of an application to the spectrum of GRB 970508.

  9. Variability of X-ray emission from OB stars

    International Nuclear Information System (INIS)

    Collura, A.; Sciortino, S.; Serio, S.; Vaiana, G. S.; Harnden, F.R. JR.; Osservatorio Astronomico, Palermo, Italy; Harvard-Smithsonian Center for Astrophysics, Cambridge, MA)

    1989-01-01

    The variability in soft X-ray emission of 12 OB stars is studied. Two different methods of analysis, one more suitable for detecting short-term variations, the other aimed at detecting long time-scale variations, are applied to all stars in the sample. The long-term variability analysis shows that Cyg-OB2 8A Zeta Pup and Delta Ori exhibit significant count rate variations between different data sections. Similar variations are marginally detected in 15 Mon; the count rate variations for the other eight stars are consistent with statistical fluctuations. The light curve of Cyg-OB2 8A suggests the existence of two different emission levels. The short-term variability analysis detects marginal variability in Tau Sco with an effective amplitude of about 30 percent and a time scale of about 50 s. The upper limits to the effective short-term variability amplitude for all other sample stars are in the 10-30 percent range. 30 refs

  10. X ray emission: a tool and a probe for laser - clusters interaction; L'emission X: un outil et une sonde pour l'interaction laser - agregats

    Energy Technology Data Exchange (ETDEWEB)

    Prigent, Ch

    2004-12-01

    In intense laser-cluster interaction, the experimental results show a strong energetic coupling between radiation and matter. We have measured absolute X-ray yields and charge state distributions under well control conditions as a function of physical parameters governing the interaction; namely laser intensity, pulse duration, wavelength or polarization state of the laser light, the size and the species of the clusters (Ar, Kr, Xe). We have highlighted, for the first time, an intensity threshold in the X-ray production very low ({approx} 2.10{sup 14} W/cm{sup 2} for a pulse duration of 300 fs) which can results from an effect of the dynamical polarisation of clusters in an intense electric field. A weak dependence with the wavelength (400 nm / 800 nm) on the absolute X-ray yields has been found. Moreover, we have observed a saturation of the X-ray emission probability below a critical cluster size. (author)

  11. Spin-polarized x-ray emission of 3d transition-metal ions : A comparison via K alpha and K beta detection

    NARCIS (Netherlands)

    Wang, Xin; deGroot, F.M.F.; Cramer, SP

    1997-01-01

    This paper demonstrates that spin-polarized x-ray-excitation spectra can be obtained using K alpha emission as well as K beta lines. A spin-polarized analysis of K alpha x-ray emission and the excitation spectra by K alpha detection on a Ni compound is reported. A systematic analysis of the

  12. X-Ray Fluorescence Spectrometry. II Determination of Uranium in ores; Espectrometria de fluorescencia de Rayos X. II-Aplicacion a la determinacion de uranio en minerales

    Energy Technology Data Exchange (ETDEWEB)

    Bermudez Polonio, J; Crus Castillo, F. de la; Fernandez Cellini, R

    1961-07-01

    A method of analysis of uranium in ores by X-ray spectrometry was developed, using the internal standard technique. Strontium was found to be the most suitable internal standard for general use. A Norelco Philips X-ray fluorescent spectrometer was used in this work, equipped with a lithium fluoride crystal acting as a diffraction grating analyzer. The intensity of the uranium-L {alpha}{sub 1} spectral line is calculated and related to corresponding strontium-K{sub {alpha}} spectral line, both detected with a Scintillation Counter. (Author) 31 refs.

  13. Diffuse X-ray emission from Abell clusters 401 and 399 - A gravitationally bound system

    Science.gov (United States)

    Ulmer, M. P.; Kinzer, R.; Cruddace, R. G.; Wood, K.; Evans, W.; Byram, E. T.; Chubb, T. A.; Friedman, H.

    1979-01-01

    The X-ray emission from the Abell 401-399 region has been studied using data obtained by the A-1 proportional counter aboard HEAO 1 in two different ways. The first involved routine scanning of the region during the all-sky survey, and the second was an observation in which the instrument was pointed at A401 during a lunar occultation. The emission is shown to be unusually extended and to be centered on a point lying between A401 and A399. The best fit of a uniform disk model to the data yielded a radius of 25.5 + or -4.4 arcmin for the lunar occultation and 42 + or - 17 arcmin for the scans. A possible explanation of the results is that A401 and A399 are both diffuse cluster X-ray sources. Alternatively, the emission may come from a large gas cloud of at least 10 to the 15th solar masses enveloping both clusters.

  14. Conceptual design of the tomographic system for simultaneous studying of soft and hard X-ray emission from dense magnetized plasma

    Energy Technology Data Exchange (ETDEWEB)

    Bielecki, J., E-mail: jakub.bielecki@ifj.edu.edu; Wójcik-Gargula, A.; Scholz, M.

    2016-11-15

    The article presents a new approach for investigation of spatial distributions of soft and hard X-rays emitted from dense magnetized plasma. The approach is based on the application of tomographic methods to the X-ray emission reconstruction in a plasma focus (PF) device. Quantitative investigation of the anisotropy of the reconstructed X–ray plasma emissivity may help to explain the nature of fusion reaction mechanisms in a PF device. The aim of this work is to present a conceptual design of a novel dual-energy X-ray emission tomographic system dedicated to the PF-24 plasma focus device. The system, which enables the simultaneous registration of soft and hard X-rays, is composed of three X‐ray pinhole cameras. Each camera is equipped with a pair of 16-element Si photodiode arrays arranged in two layers separated by an aluminum attenuator. The Geant4 code was used to optimize the layout and parameters of the applied detectors. In addition, a method of tomographic reconstruction from a sparse data set provided by the experimental setup has been presented.

  15. Characterization of Roman glass tesserae from the Coriglia excavation site (Italy) via energy-dispersive X-ray fluorescence spectrometry and Raman spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Donais, Mary Kate; Sparks, Andrew; Redente, Monica [Saint Anselm College, Department of Chemistry, Manchester, NH (United States); Pevenage, Jolien van; Moens, Luc; Vincze, Laszlo [Ghent University, Department of Analytical Chemistry, Ghent (Belgium); George, David B. [Saint Anselm College, Department of Classics, Manchester, NH (United States); Vandenabeele, Peter [Ghent University, Department of Archaeology, Ghent (Belgium)

    2016-12-15

    The combined use of handheld energy-dispersive X-ray fluorescence spectrometry, Raman spectroscopy, and micro-energy-dispersive X-ray fluorescence spectrometry permitted the characterization of Roman glass tesserae excavation from the Coriglia (Italy) archeological site. Analyses of ten different glass colors were conducted as spot analyses on intact samples and as both spot analyses and line scans on select cross-sectioned samples. The elemental and molecular information gained from these spectral measurements allowed for the qualitative chemical characterization of the bulk glass, decolorants, opacifiers, and coloring agents. The use of an antimony opacifier in many of the samples supports the late Imperial phasing as determined through numismatic, fresco, ceramics, and architectural evidence. And dealinization of the exterior glass layers caused by the burial environment was confirmed. (orig.)

  16. Application of neutron activation techniques and x-ray energy dispersion spectrometry, in analysis of metallic traces adsorbed by chelex-100 resin

    International Nuclear Information System (INIS)

    Fernandes, Jair C.; Amaral, Angela M.; Magalhaes, Jesus C.; Pereira, Jose S.J.; Silva, Juliana B. da; Auler, Lucia M.L.A.

    2000-01-01

    In this work, the authors have investigated optimal conditions of adsorption for several ion metallic groups (cations of heavy metals and transition metals, oxyanions metallics and metalloids and cations of rare earths), as traces (ppb), withdrawn and in mixture of groups, by chelex-100 resin. The experiments have been developed by bath techniques in ammonium acetate tamponade solution 40 mM pH 5,52 content 0,5 g of chelex-100 resin. After magnetic agitation for two hours, resins were dried and submitted to X-ray energy dispersion spectrometry, x-ray fluorescence spectrometry and neutron activation analysis. The results have demonstrated that chelex-100 resin adsorb quantitatively transition element groups and rare earth groups in two cases (withdrawn and simultaneously adsorption)

  17. Multi-layer x-ray screens

    International Nuclear Information System (INIS)

    Rabatin, J.G.

    1984-01-01

    Rare earth oxyhalide phosphors activated with thulium ion are employed in X-ray intensifying screens having modified ultraviolet emission characteristics which reduce crossover effects without significant reduction in film speed and further increases screen brightness. Relatively low concentration levels of the thulium activator ion have been found to shift the ultraviolet emission of said phosphor when excited by X-rays to lower wavelengths in both the ultraviolet and near-ultraviolet spectral regions

  18. The Radiative X-ray and Gamma-ray Efficiencies of Rotation-powered Pulsars

    Science.gov (United States)

    Vink, Jacco; Bamba, Aya; Yamazaki, Ryo

    2011-02-01

    We present a statistical analysis of the X-ray luminosity of rotation-powered pulsars and their surrounding nebulae using the sample of Kargaltsev & Pavlov, and we complement this with an analysis of the γ-ray emission of Fermi-detected pulsars. We report a strong trend in the efficiency with which spin-down power is converted to X-ray and γ-ray emission with characteristic age: young pulsars and their surrounding nebulae are efficient X-ray emitters, whereas in contrast old pulsars are efficient γ-ray emitters. We divided the X-ray sample in a young (τ c < 1.7 × 104 yr) and old sample and used linear regression to search for correlations between the logarithm of the X-ray and γ-ray luminosities and the logarithms of the periods and period derivatives. The X-ray emission from young pulsars and their nebulae are both consistent with L_X ∝ \\dot{P}^3/P^6. For old pulsars and their nebulae the X-ray luminosity is consistent with a more or less constant efficiency η ≡ L_X/\\dot{E}_{rot} ≈ 8× 10^{-5}. For the γ-ray luminosity we confirm that L_γ ∝ √{\\dot{E}_{rot}}. We discuss these findings in the context of pair production inside pulsar magnetospheres and the striped wind model. We suggest that the striped wind model may explain the similarity between the X-ray properties of the pulsar wind nebulae and the pulsars themselves, which according to the striped wind model may both find their origin outside the light cylinder, in the pulsar wind zone.

  19. Copper L X-ray spectra measured by a high resolution ion-induced X-ray spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Takahashi, Ryohei; Hamaguchi, Dai; Kageyama, Hiroyoshi [Kyoto Inst. of Tech. (Japan); and others

    1997-03-01

    High resolution L X-ray emission spectra of Cu have been measured by 0.75 MeV/u H, He, and F, 0.73 MeV/u Ar, 0.64 MeV/u Si, and 0.073 MeV/u Si ion impacts with a crystal spectrometer. The X-ray transition energies in the Cu target for L{iota}, L{eta}, L{alpha}{sub 1,2}, L{beta}{sub 1}, and L{beta}{sub 3,4} diagram lines induced by light ion impacts are determined, which are in good agreement with those given in the reference. The difference in L X-ray emission spectra produced by H, He, F, Si, and Ar ions are considered and the L{alpha}{sub 1,2} and L{beta}{sub 1} emission spectra are compared with the calculated ones based on the multiconfiguration Dirac-Fock method. (author)

  20. X-RAY EMISSION AND DYNAMICS FROM LARGE DIAMETER SUPERBUBBLES: THE CASE OF THE N70 SUPERBUBBLE

    International Nuclear Information System (INIS)

    Rodriguez-Gonzalez, A.; Velazquez, P. F.; Esquivel, A.; Toledo-Roy, J. C.; Rosado, M.; Reyes-Iturbide, J.

    2011-01-01

    The morphology, dynamics, and thermal X-ray emission of the superbubble N70 are studied by means of three-dimensional hydrodynamic simulations carried out with the YGUAZU-A code. We consider three possible scenarios: the superbubble being the product of a single supernova remnant, of the stellar winds from an OB association, or of the joint action of stellar winds and a supernova (SN) event. Our results show that, in spite of the fact that all scenarios produce bubbles with the observed physical size, only those in which the bubble is driven by stellar winds and an SN event successfully explain the general morphology, dynamics, and X-ray luminosity of N70. Our models predict temperatures in excess of 10 8 K at the interior of the superbubble; however, the density is too low and thermal X-ray emission above 2 keV is too faint to be detected.

  1. HARD X-RAY EMISSION DURING FLARES AND PHOTOSPHERIC FIELD CHANGES

    International Nuclear Information System (INIS)

    Burtseva, O.; Petrie, G. J. D.; Pevtsov, A. A.; Martínez-Oliveros, J. C.

    2015-01-01

    We study the correlation between abrupt permanent changes of magnetic field during X-class flares observed by the Global Oscillation Network Group and Helioseismic and Magnetic Imager instruments, and the hard X-ray (HXR) emission observed by RHESSI, to relate the photospheric field changes to the coronal restructuring and investigate the origin of the field changes. We find that spatially the early RHESSI emission corresponds well to locations of the strong field changes. The field changes occur predominantly in the regions of strong magnetic field near the polarity inversion line (PIL). The later RHESSI emission does not correspond to significant field changes as the flare footpoints are moving away from the PIL. Most of the field changes start before or around the start time of the detectable HXR signal, and they end at about the same time or later than the detectable HXR flare emission. Some of the field changes propagate with speed close to that of the HXR footpoint at a later phase of the flare. The propagation of the field changes often takes place after the strongest peak in the HXR signal when the footpoints start moving away from the PIL, i.e., the field changes follow the same trajectory as the HXR footpoint, but at an earlier time. Thus, the field changes and HXR emission are spatio-temporally related but not co-spatial nor simultaneous. We also find that in the strongest X-class flares the amplitudes of the field changes peak a few minutes earlier than the peak of the HXR signal. We briefly discuss this observed time delay in terms of the formation of current sheets during eruptions

  2. ORIGIN OF THE GALACTIC DIFFUSE X-RAY EMISSION: IRON K-SHELL LINE DIAGNOSTICS

    Energy Technology Data Exchange (ETDEWEB)

    Nobukawa, Masayoshi [Department of Teacher Training and School Education, Nara University of Education, Takabatake-cho, Nara, 630-8528 (Japan); Uchiyama, Hideki [Faculty of Education, Shizuoka University, 836 Ohya, Suruga-ku, Shizuoka, 422-8529 (Japan); Nobukawa, Kumiko K.; Koyama, Katsuji [Department of Physics, Graduate School of Science, Kyoto University, Kitashirakawa-oiwake-cho, Sakyo-ku, Kyoto, 606-8502 (Japan); Yamauchi, Shigeo, E-mail: nobukawa@nara-edu.ac.jp [Department of Physics, Nara Women’s University, Kitauoyanishimachi, Nara, 630-8506 (Japan)

    2016-12-20

    This paper reports detailed K-shell line profiles of iron (Fe) and nickel (Ni) of the Galactic Center X-ray Emission (GCXE), Galactic Bulge X-ray Emission (GBXE), Galactic Ridge X-ray Emission (GRXE), magnetic Cataclysmic Variables (mCVs), non-magnetic Cataclysmic Variables (non-mCVs), and coronally Active Binaries (ABs). For the study of the origin of the GCXE, GBXE, and GRXE, the spectral analysis is focused on equivalent widths of the Fe i-K α , Fe xxv-He α , and Fe xxvi-Ly α  lines. The global spectrum of the GBXE is reproduced by a combination of the mCVs, non-mCVs, and ABs spectra. On the other hand, the GRXE spectrum shows significant data excesses at the Fe i-K α and Fe xxv-He α  line energies. This means that additional components other than mCVs, non-mCVs, and ABs are required, which have symbiotic phenomena of cold gas and very high-temperature plasma. The GCXE spectrum shows larger excesses than those found in the GRXE spectrum at all the K-shell lines of iron and nickel. Among them the largest ones are the Fe i-K α , Fe xxv-He α , Fe xxvi-Ly α , and Fe xxvi-Ly β  lines. Together with the fact that the scale heights of the Fe i-K α , Fe xxv-He α , and Fe xxvi-Ly α lines are similar to that of the central molecular zone (CMZ), the excess components would be related to high-energy activity in the extreme envelopment of the CMZ.

  3. X-ray observations of the starburst galaxy M82

    International Nuclear Information System (INIS)

    Schaaf, R.; Pietsch, W.; Biermann, P.L.; Kronberg, P.P.; Schmutzler, T.

    1989-01-01

    Long X-ray observations of the starburst galaxy M82 with the European X-ray satellite EXOSAT are reported. The observations with the low-energy imaging instrument confirm that there is extended X-ray emission from above and below the disk, with an overall extent perpendicular to the disk of almost 6 arcmin corresponding to 6 kpc. One of the best defined X-ray spectra yet of a starburst galaxy is presented. The medium energy instrument measurements can be fitted with a power-law spectrum, consistent with inverse Compton emission, or with thermal emission from optically thin hot gas of a temperature of 9 + 9 or -4 keV. Using, in addition, the earlier Einstein HRI and MPC observations, the possible origin of the X-ray emission is discussed. 31 references

  4. The determination of trace elements in commercial human serum albumin solutions by proton-induced X-ray emission spectrometry and neutron activation analysis

    International Nuclear Information System (INIS)

    Maenhaut, W.; De Reu, L.; Tomza, U.; Versieck, J.

    1982-01-01

    Particle induced X-ray emission (p.i.x.e.) and neutron activation analysis (n.a.a.) are proposed for determining the trace element content of human serum albumin. Application of these methods to some commercial albumin solutions provided concentration data for up to 19 elements, most of which were present at a level below a few μg ml -1 . The precision of the p.i.x.e. technique, as determined by irradiating up to 20 targets from one sample, was about 3% for those elements where counting statistics were good. A comparison between the p.i.x.e. and n.a.a. results showed close agreement, indicating that p.i.x.e. can yield data which are accurate to within 10%. Neutron activation showed very good sensitivity for the elements producing long-lived nuclides (tsub(1/2) >= 3 days), but had rather high detection limits for the other elements, unless radiochemical separations were used. (Auth.)

  5. Quality assurance challenges in x-ray emission based analyses

    International Nuclear Information System (INIS)

    Papp, T.

    2005-01-01

    Complete text of publication follows. There is a large scatter in the results of X-ray analysis with solid-state detectors suggesting methodological origin. Although the PIXE (proton induced X-ray emission) analytical technique can work without relation to any physics, as was commented at the recent PIXE conference, one could argue that if the same technique is used for measuring physical quantities reveals problems, then perhaps potential methodological issues can not apriory be excluded. We present a simple example which could be interpreted as indications for methodological considerations. Recently an inter-comparison was made of analysis of the spectra measured at the laboratory of the International Atomic Energy Agency (IAEA). Four participating analytical software packages were used to evaluate the X-ray spectra. There are several thin metal samples spectra, for which common energy scale could not be established. The quality of the spectrum can be judged from the line shape. The line shape is parametrized by the full widths at half maximum (FWHM) of a peak and the so-called low energy tailing. Fitting the spectra individually we obtained FWHM squared values at different energies and determined the linear regression parameters. The parameters suggest a rather poor detector performance. It is generally assumed that the (FWHM) 2 values have a first order polynomial form as a function of X-ray energy. Having done a linear regression analysis, we can plot the standard residual, presented in Fig. 1, which clearly shows a three-sigma deviation. The probability to having a three-sigma deviation is 1%. In other words, the probability that these spectra are in accordance with the expected FWHM functional form is less than 1%. The main problem is that, although the composite spectra were analyzed using four different programs, the difficulty in interpreting the spectra was not commented upon by any of the participants in the inter-comparison. (author)

  6. X-ray stars observed in LAMOST spectral survey

    Science.gov (United States)

    Lu, Hong-peng; Zhang, Li-yun; Han, Xianming L.; Shi, Jianrong

    2018-05-01

    X-ray stars have been studied since the beginning of X-ray astronomy. Investigating and studying the chromospheric activity from X-ray stellar optical spectra is highly significant in providing insights into stellar magnetic activity. The big data of LAMOST survey provides an opportunity for researching stellar optical spectroscopic properties of X-ray stars. We inferred the physical properties of X-ray stellar sources from the analysis of LAMOST spectra. First, we cross-matched the X-ray stellar catalogue (12254 X-ray stars) from ARXA with LAMOST data release 3 (DR3), and obtained 984 good spectra from 713 X-ray sources. We then visually inspected and assigned spectral type to each spectrum and calculated the equivalent width (EW) of Hα line using the Hammer spectral typing facility. Based on the EW of Hα line, we found 203 spectra of 145 X-ray sources with Hα emission above the continuum. For these spectra we also measured the EWs of Hβ, Hγ, Hδ and Ca ii IRT lines of these spectra. After removing novae, planetary nebulae and OB-type stars, we found there are 127 X-ray late-type stars with Hα line emission. By using our spectra and results from the literature, we found 53 X-ray stars showing Hα variability; these objects are Classical T Tauri stars (CTTs), cataclysmic variables (CVs) or chromospheric activity stars. We also found 18 X-ray stars showing obvious emissions in the Ca ii IRT lines. Of the 18 X-ray stars, 16 are CTTs and 2 are CVs. Finally, we discussed the relationships between the EW of Hα line and X-ray flux.

  7. NuSTAR Search for Hard X-ray Emission from the Star Formation Regions in Sh2-104

    Science.gov (United States)

    Gotthelf, Eric V.

    2016-04-01

    We present NuSTAR hard X-ray observations of Sh2-104, a compact Hii region containing several young massive stellar clusters (YMSCs). We have detected distinct hard X-ray sources coincident with localized VERITAS TeV emission recently resolved from the giant gamma-ray complex MGRO J2019+37 in the Cygnus region. Faint, diffuse X-ray emission coincident with the eastern YMSC in Sh2-104 is likely the result of colliding winds of component stars. Just outside the radio shell of Sh2-104 lies 3XMM J201744.7+365045 and nearby nebula NuSTAR J201744.3+364812, whose properties are most consistent with extragalactic objects. The combined XMM-Newton and NuSTAR spectrum of 3XMM J201744.7+365045 is well-fit to an absorbed power-law model with NH = (3.1+/-1.0)E22 1/cm^2 and photon index Gamma = 2.1+/-0.1. Based on possible long-term flux variation and lack of detected pulsations (Sh2-104 will help identify the nature of the X-ray sources and their relation to MGRO J2019+37.

  8. X-ray novae - what are they

    International Nuclear Information System (INIS)

    Wennfors, B.

    1976-01-01

    Ten of the two hundred cosmic X-ray sources exhibit characteristics in their emissions analogous to novae, i.e. after a rapid increase in luminosity, lasting about three days, follows a period of about a month with a slow decrease, and thereafter a rapid decrease to invisibility. The spectra of such sources are discussed in general terms and brief descriptions are given of the five which have been identified with optical objects. Three models for the history of X-ray novae, all based on X-ray emission from a compact object in an orbit very near a larger star, are discussed. (JIW)

  9. Determination of nickel in chloralkali electrolysis brines by X-ray fluorescence spectrometry on a membrane filter

    International Nuclear Information System (INIS)

    Andrade, L.L.; Minzl, E.

    1984-01-01

    X-ray fluorescence spectrometry after ammonium pyrrolidinedithiocarbamate (APDC) preconcentration is proposed for the determination of nickel in chloralkali electrolysis brines. The optimum conditions for the precipitation target tube, peak intensity, background, analysing crystal, counters and exposure time were investigated. The method was applied to chloralkali brines of evaporite salts (halite, sylvinite, carnallite and tachhydrite), sodium, potassium and magnesium salts, explored in Sergipe (Brazil), by Petrobras-Mineracao S.A.(Author) [pt

  10. Low-energy X-ray and gamma spectrometry using silicon photodiodes; Espectrometria de raios X e gama de baixa energia utilizando fotodiodos de silicio

    Energy Technology Data Exchange (ETDEWEB)

    Silva, Iran Jose Oliveira da

    2000-08-01

    The use of semiconductor detectors for radiation detection has increased in recent years due to advantages they present in comparison to other types of detectors. As the working principle of commercially available photodiodes is similar to the semiconductor detector, this study was carried out to evaluate the use of Si photodiodes for low energy x-ray and gamma spectrometry. The photodiodes investigated were SFH-205, SFH-206, BPW-34 and XRA-50 which have the following characteristics: active area of 0,07 cm{sup 2} and 0,25 cm{sup 2}, thickness of the depletion ranging from 100 to 200 {mu}m and junction capacitance of 72 pF. The photodiode was polarized with a reverse bias and connected to a charge sensitive pre-amplifier, followed by a amplifier and multichannel pulse analyzer. Standard radiation source used in this experiment were {sup 241} Am, {sup 109} Cd, {sup 57} Co and {sup 133} Ba. The X-ray fluorescence of lead and silver were also measured through K- and L-lines. All the measurements were made with the photodiodes at room temperature.The results show that the responses of the photodiodes very linear by the x-ray energy and that the energy resolution in FWHM varied between 1.9 keV and 4.4 keV for peaks corresponding to 11.9 keV to 59 keV. The BPW-34 showed the best energy resolution and the lower dark current. The full-energy peak efficiency was also determined and it was observed that the peak efficiency decreases rapidly above 50 keV. The resolution and efficiency are similar to the values obtained with other semiconductor detectors, evidencing that the photodiodes used in that study can be used as a good performance detector for low energy X-ray and gamma spectrometry. (author)

  11. Soft X-ray emission studies of biomaterials

    International Nuclear Information System (INIS)

    Kurmaev, E.Z.; Werner, J.P.; Moewes, A.; Chiuzbaian, S.; Bach, M.; Ching, W.-Y.; Motozaki, W.; Otsuka, T.; Matsuya, S.; Endo, K.; Neumann, M.

    2004-01-01

    Soft X-ray fluorescence measurements are used to characterize three groups of biomaterials: Vitamin B 12 and derivatives, antioxidants (aspirin and paracetamol), and human teeth. We show that the chemical bonding in Vitamin B 12 is characterized by the strong Co-C bond and the relatively weak Co-N bond. The Co-C bond in cyanocobalamin is found to be stronger than that of methylcobalamin leading to their different biological activity. The chemical bonding of paracetamol and aspirin is characterized by the formation of oxygen lone-pair π-orbitals, which can neutralize free radicals and therefore be related to antioxidant activity of these compounds. Carbon Kα emission spectra of a caries lesion suggest that the CaCO 3 like phase exists in sound enamel and that a selective loss of carbonate occurs during the early stages of a caries attack

  12. Experimental studies on pulse soft X-ray generator

    International Nuclear Information System (INIS)

    Li Chengrong; Yang Qinchi; Luo Chengmu; Han Min

    1990-01-01

    Emission sources of soft x rays (2 keV < hv < 6 keV) from hot plasmas have been studied in a small gas-puff Z-pinch. The emission sources are a group of uncontinuous hot spots. The output of soft x rays from the hot spots have been measured and the effect of the initial gas density on the yield of soft x rays has been investigated

  13. Current sheath curvature correlation with the neon soft x-ray emission from plasma focus device

    International Nuclear Information System (INIS)

    Zhang, T; Lin, X; Chandra, K A; Tan, T L; Springham, S V; Patran, A; Lee, P; Lee, S; Rawat, R S

    2005-01-01

    The insulator sleeve length is one of the major parameters that can severely affect the neon soft x-ray yield from a plasma focus. The effect of the insulation sleeve length on various characteristic timings of plasma focus discharges and hence the soft x-ray emission characteristics has been investigated using a resistive divider. The pinhole images and laser shadowgraphy are used to explain the observed variation in the average soft x-ray yield (measured using a diode x-ray spectrometer) with variation of the insulator sleeve length. We have found that for a neon filled plasma focus device the change in insulator sleeve length changes the current sheath curvature angle and thus the length of the focused plasma column. The optimized current sheath curvature angle is found to be between 39 0 and 41 0 , at the specific axial position of 6.2-9.3 cm from the cathode support plate, for our 3.3 kJ plasma focus device. A strong dependence of the neon soft x-ray yield on the current sheath curvature angle has thus been reported

  14. Measurements of fast electron beams and soft X-ray emission from plasma-focus experiments

    Directory of Open Access Journals (Sweden)

    Surała Władysław

    2016-06-01

    Full Text Available The paper reports results of the recent experimental studies of pulsed electron beams and soft X-rays in plasma-focus (PF experiments carried out within a modified PF-360U facility at the NCBJ, Poland. Particular attention was focused on time-resolved measurements of the fast electron beams by means of two different magnetic analyzers, which could record electrons of energy ranging from about 41 keV to about 715 keV in several (6 or 8 measuring channels. For discharges performed with the pure deuterium filling, many strong electron signals were recorded in all the measuring channels. Those signals were well correlated with the first hard X-ray pulse detected by an external scintillation neutron-counter. In some of the analyzer channels, electron spikes (lasting about dozens of nanoseconds and appearing in different instants after the current peculiarity (so-called current dip were also recorded. For several discharges, fast ion beams, which were emitted along the z-axis and recorded with nuclear track detectors, were also investigated. Those measurements confirmed a multibeam character of the ion emission. The time-integrated soft X-ray images, which were taken side-on by means of a pinhole camera and sensitive X-ray films, showed the appearance of some filamentary structures and so-called hot spots. The application of small amounts of admixtures of different heavy noble gases, i.e. of argon (4.8% volumetric, krypton (1.6% volumetric, or xenon (0.8% volumetric, decreased intensity of the recorded electron beams, but increased intensity of the soft X-ray emission and showed more distinct and numerous hot spots. The recorded electron spikes have been explained as signals produced by quasi-mono-energetic microbeams emitted from tiny sources (probably plasma diodes, which can be formed near the observed hot spots.

  15. Elements in normal and cirrhotic human liver. Potassium, iron, copper, zinc and bromine measured by X-ray fluorescence spectrometry

    DEFF Research Database (Denmark)

    Laursen, J.; Milman, N.; Leth, Peter Mygind

    1990-01-01

    Various elements (K, Fe, Cu, Zn, Br) were measured by X-ray flourescence spectrometry in cellular and connective tissue fractions of normal and cirrhotic liver samples obtained at autopsy. Normal livers: 32 subjects (16 males, 16 females) median age 69 years. Cirrhotic livers: 14 subjects (13 mal...

  16. On self-consistent ray-tracing and Fokker-Planck modeling of the hard X-ray emission during lower-hybrid current driven in Tokamaks

    International Nuclear Information System (INIS)

    Bizarro, J.P.; Peysson, Y.; Bonoli, P.T.; Carrasco, J.; Dudok de Wit, T.; Fuchs, V.; Hoang, G.T.; Litaudon, X.; Moreau, D.; Pocheau, C.; Shkarofsky, I.P.

    1993-04-01

    A detailed investigation is presented on the ability of combined ray-tracing and Fokker-Planck calculations to predict the hard x-ray (HXR) emission during lower-hybrid (LH) current drive in tokamaks when toroidally induced-ray-stochasticity is important. A large number of rays is used and the electron distribution function is obtained by self-consistently iterating the appropriate LH power deposition and Fokker-Planck calculations. Most of the experimentally observed features of the HXR emission are correctly predicted. It is found that corrections due to radial diffusion of suprathermal electrons and to radiation scattering by the inner wall can be significant

  17. Characterization of nuclear physics targets using Rutherford backscattering and particle induced X-ray emission

    International Nuclear Information System (INIS)

    Rubehn, T.; Wozniak, G.J.; Phair, L.; Moretto, L.G.; Yu, K.M.

    1997-01-01

    Rutherford backscattering and particle induced X-ray emission have been utilized to precisely characterize targets used in nuclear fission experiments. The method allows for a fast and non-destructive determination of target thickness, homogeneity and element composition. (orig.)

  18. Characterization of offset printing ink tagged with rare-earth taggants by X-ray emission techniques

    International Nuclear Information System (INIS)

    Joseph, D.; Saxena, A.; Choudhury, R.K.; Maind, S.D.

    2007-01-01

    Proton Induced X-ray Emission (PIXE) and Energy Dispersive X-ray Fluorescence (EDXRF) techniques have been used for elemental characterization of offset printing ink tagged with rare-earth taggants. The offset printing ink was tagged with rare-earth (La, Pr, Nd, Sm, Eu and Gd) thenoyltrifluoroacetonate chelates at about 1000-ppm level for each element separately. Small aliquots (approximately 20 mg) of tagged inks were coated on paper supports in the form of small circles having diameter 10-15 mm each and then analyzed. In the case of PIXE, a proton beam of energy 4 MeV and in the case of EDXRF a radioisotope source of 241 Am (100 mCi) was used to excite the samples. The PIXE analysis showed well-resolved rare-earth L X-rays and EDXRF analysis showed the K X-rays of rare earths. Satisfactory results to identify and quantify the taggants were achieved. (author)

  19. Solar X-ray bursts

    International Nuclear Information System (INIS)

    Urnov, A.M.

    1980-01-01

    In the popular form the consideration is given to the modern state tasks and results of X-ray spectrometry of solar bursts. The operation of X-ray spectroheliograph is described. Results of spectral and polarization measurings of X-ray radiation of one powerful solar burst are presented. The conclusion has been drawn that in the process of burst development three characteristic stages may be distingwished: 1) the initial phase; just in this period processes which lead to observed consequences-electromagnetic and corpuscular radiation are born; 2) the impulse phase, or the phase of maximum, is characterised by sharp increase of radiation flux. During this phase the main energy content emanates and some volumes of plasma warm up to high temperatures; 3) the phase of burst damping, during which plasma cools and reverts to the initial condition

  20. Spatially Resolved Hard X-ray Emission in the Central 5 kpc of the Galaxy Merger NGC 6240

    Science.gov (United States)

    Wang, Junfeng; Nardini, E.; Fabbiano, G.; Karovska, M.; Elvis, M.; Pellegrini, S.; Max, C. E.; Risaliti, G.; U, V.; Zezas, A.

    2013-04-01

    We have obtained a deep, sub-arcsecond resolution X-ray image of the nuclear region of the luminous galaxy merger NGC 6240 with Chandra, which resolves the X-ray emission from the pair of active nuclei and the diffuse hot gas in great detail. We detect extended hard X-ray emission from 70 million K hot gas over a spatial scale of 5 kpc, indicating the presence of fast shocks with velocity of 2200 km/s. For the first time we obtain spatial distribution of this highly ionized gas emitting FeXXV and find that it shows a remarkable correspondence to the large scale morphology of H_2(1-0) S(1) line emission and Hα filaments. Propagation of fast shocks originated in the starburst driven wind into the ambient dense gas can account for this morphological correspondence. Both the energetics and the iron mass in the hot gas are consistent with the expected injection from the supernovae explosion during the starburst that is commensurate with its high star formation rate.

  1. Summary of existing information on gamma-ray and X-ray attenuation coefficients of solutions

    DEFF Research Database (Denmark)

    Singh, K.; Gerward, Leif

    2002-01-01

    Accurate values of X-ray and gamma-ray attenuation coefficients of different chemicals are required in spectrometry as well as in many other scientific, engineering and medical disciplines involving photon radiation. The current state of knowledge of experimental and theoretical gamma-ray and X-r......-ray attenuation coefficients in aqueous solutions of salts is presented and exemplified by recent work. The results presented provide a basis for studying X-ray and gamma-ray photon interactions with ions in solution (hydrated ions) rather than ion compounds in solid form....

  2. Imaging of High-Energy X-Ray Emission from Cryogenic Thermonuclear Fuel Implosions on the NIF

    International Nuclear Information System (INIS)

    Ma, T.

    2012-01-01

    Accurately assessing and optimizing the implosion performance of inertial confinement fusion capsules is a crucial step to achieving ignition on the NIF. We have applied differential filtering (matched Ross filter pairs) to provide spectrally resolved time-integrated absolute x-ray self-emission images of the imploded core of cryogenic layered targets. Using bremsstrahlung assumptions, the measured absolute x-ray brightness allows for the inference of electron temperature, electron density, hot spot mass, mix mass, and pressure. Current inertial confinement fusion (ICF) experiments conducted on the National Ignition Facility (NIF) seek to indirectly drive a spherical implosion, compressing and igniting a deuterium-tritium fuel. This DT fuel capsule is cryogenically prepared as a solid ice layer surrounded by a low-Z ablator material. Ignition will occur when the hot spot approaches sufficient temperature (∼3-4 keV) and ρR (∼0.3 g/cm 2 ) such that alpha deposition can further heat the hot spot and generate a self-sustaining burn wave. During the implosion, the fuel mass becomes hot enough to emit large amounts of x-ray radiation, the spectra and spatial variation of which contains key information that can be used to evaluate the implosion performance. The Ross filter diagnostic employs differential filtering to provide spectrally resolved, time-integrated, absolute x-ray self-emission images of the imploded core of cryogenic layered targets.

  3. Determination of fluorine concentrations using wavelength dispersive X-ray fluorescence (WDXRF) spectrometry to analyze fluoride precipitates.

    Science.gov (United States)

    Lee, H. A.; Lee, J.; Kwon, E.; Kim, D.; Yoon, H. O.

    2015-12-01

    In recent times, fluorine has been receiving increasing attention due to the possibility for chemical (HF) leakage accidents and its high toxicity to human and environment. In this respect, a novel approach for the determination of fluorine concentrations in water samples using wavelength dispersive X-ray fluorescence (WDXRF) spectrometry was investigated in this study. The main disadvantage of WDXRF technique for fluorine analysis is low analytical sensitivity for light elements with atomic number (Z) less than 15. To overcome this problem, we employed the precipitation reaction which fluoride is reacted with cation such as Al3+ and/or Ca2+ prior to WDXRF analysis because of their high analytical sensitivity. The cation was added in fluoride solutions to form precipitate (AlF3 and/or CaF2) and then the solution was filtered through Whatman filter. After drying at 60 °C for 5 min, the filter was coated with X-ray film and directly analyzed using WDXRF spectrometry. Consequently, we analyzed the cation on filter and subsequently fluorine concentration was calculated inversely based on chemical form of precipitate. This method can improve the analytical sensitivity of WDXRF technique for fluorine analysis and be applicable to various elements that can make precipitate.

  4. X-ray chemical analyzer for field applications

    International Nuclear Information System (INIS)

    Gamba, O.O.M.

    1977-01-01

    A self-supporting portable field multichannel x-ray chemical analyzer system is claimed. It comprises a lightweight, flexibly connected, remotely locatable, radioisotope-excited sensing probe utilizing a cryogenically-cooled solid state semi-conductor crystal detector for fast in situ non-destructive, qualitative and quantitative analysis of elements in solid, powder, liquid or slurried form, utilizing an x-ray energy dispersive spectrometry technique

  5. A Chandra High-Resolution X-ray Image of Centaurus A.

    Science.gov (United States)

    Kraft; Forman; Jones; Kenter; Murray; Aldcroft; Elvis; Evans; Fabbiano; Isobe; Jerius; Karovska; Kim; Prestwich; Primini; Schwartz; Schreier; Vikhlinin

    2000-03-01

    We present first results from a Chandra X-Ray Observatory observation of the radio galaxy Centaurus A with the High-Resolution Camera. All previously reported major sources of X-ray emission including the bright nucleus, the jet, individual point sources, and diffuse emission are resolved or detected. The spatial resolution of this observation is better than 1&arcsec; in the center of the field of view and allows us to resolve X-ray features of this galaxy not previously seen. In particular, we resolve individual knots of emission in the inner jet and diffuse emission between the knots. All of the knots are diffuse at the 1&arcsec; level, and several exhibit complex spatial structure. We find the nucleus to be extended by a few tenths of an arcsecond. Our image also suggests the presence of an X-ray counterjet. Weak X-ray emission from the southwest radio lobe is also seen, and we detect 63 pointlike galactic sources (probably X-ray binaries and supernova remnants) above a luminosity limit of approximately 1.7x1037 ergs s-1.

  6. Handbook of X-Ray Astronomy

    Science.gov (United States)

    Arnaud, Keith A. (Editor); Smith, Randall K.; Siemiginowska, Aneta

    2011-01-01

    X-ray astronomy was born in the aftermath of World War II as military rockets were repurposed to lift radiation detectors above the atmosphere for a few minutes at a time. These early flights detected and studied X-ray emission from the Solar corona. The first sources beyond the Solar System were detected during a rocket flight in 1962 by a team headed by Riccardo Giaccom at American Science and Engineering, a company founded by physicists from MIT. The rocket used Geiger counters with a system designed to reduce non-X-ray backgrounds and collimators limiting the region of sky seen by the counters. As the rocket spun, the field of view (FOV) happened to pass over what was later found to be the brightest non-Solar X-ray source; later designated See X-1. It also detected a uniform background glow which could not be resolved into individual sources. A follow-up campaign using X-ray detectors with better spatial resolution and optical telescopes identified See X-1 as an interacting binary with a compact (neutron star) primary. This success led to further suborbital rocket flights by a number of groups. More X-ray binaries were discovered, as well as X-ray emission from supernova remnants, the radio galaxies M87 and Cygnus-A, and the Coma cluster. Detectors were improved and Geiger counters were replaced by proportional counters, which provided information about energy spectra of the sources. A constant challenge was determining precise positions of sources as only collimators were available.

  7. Stellar X-Ray Polarimetry

    Science.gov (United States)

    Swank, J.

    2011-01-01

    Most of the stellar end-state black holes, pulsars, and white dwarfs that are X-ray sources should have polarized X-ray fluxes. The degree will depend on the relative contributions of the unresolved structures. Fluxes from accretion disks and accretion disk corona may be polarized by scattering. Beams and jets may have contributions of polarized emission in strong magnetic fields. The Gravity and Extreme Magnetism Small Explorer (GEMS) will study the effects on polarization of strong gravity of black holes and strong magnetism of neutron stars. Some part of the flux from compact stars accreting from companion stars has been reflected from the companion, its wind, or accretion streams. Polarization of this component is a potential tool for studying the structure of the gas in these binary systems. Polarization due to scattering can also be present in X-ray emission from white dwarf binaries and binary normal stars such as RS CVn stars and colliding wind sources like Eta Car. Normal late type stars may have polarized flux from coronal flares. But X-ray polarization sensitivity is not at the level needed for single early type stars.

  8. Analysis of the electronic structure of human hemoglobin from soft X-ray emission

    International Nuclear Information System (INIS)

    Soldatov, A.V.; Kravtsova, A.N.; Fedorovich, E.N.; Ankudinov, A.; Moewes, A.; Kurmaev, E.Z.

    2005-01-01

    We present X-ray emission spectra (XES) of human hemoglobin excited near the iron L 2,3 threshold and the nitrogen and carbon K-edges. The experiment is compared with our calculations of the corresponding spectra and gives good agreement. We find that the Fe L 3 emission is affected by the nearest nitrogen atoms located in the heme plane around the central iron atom. The distribution of the partial electronic densities of states of hemoglobin is determined

  9. The X-ray eclipse geometry of the super-soft X-ray source CAL 87

    Energy Technology Data Exchange (ETDEWEB)

    Ribeiro, T.; Lopes de Oliveira, R. [Departamento de Física, Universidade Federal de Sergipe, Av. Marechal Rondon s/n, 49100-000 São Cristóvão, SE (Brazil); Borges, B. W., E-mail: tribeiro@ufs.br, E-mail: rlopes@ufs.br, E-mail: bernardo@astro.ufsc.br [Universidade Federal de Santa Catarina, Campus Araranguá, 88905-120 Araranguá, SC (Brazil)

    2014-09-01

    We explore XMM-Newton observations of the eclipsing super-soft X-ray source CAL 87 in order to map the accretion structures of the system. Indirect imaging techniques were applied in X-ray light curves to provide eclipse maps. The surface brightness distribution exhibits an extended and symmetric emission, and a feature is revealed from the hardest X-rays that is likely due to a bright spot. A rate of P-dot =(+6±2)×10{sup −10} for changes in the orbital period of the system was derived from the eclipses. There is no significant variation of the emission lines even during eclipses, arguing that the lines are formed in an extended region. The continuum emission dominates the decrease in flux that is observed during eclipses. The O VIII Lyα line reveals a broadening velocity that is estimated to be 365{sub −69}{sup +65} km s{sup –1} (at 1σ), marginal evidence for asymmetry in its profile, and sometimes shows evidence of double-peaked emission. Together, the results support that the wind-driven mass transfer scenario is running in CAL 87.

  10. Miniature x-ray source

    Science.gov (United States)

    Trebes, James E.; Bell, Perry M.; Robinson, Ronald B.

    2000-01-01

    A miniature x-ray source utilizing a hot filament cathode. The source has a millimeter scale size and is capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature source consists of a compact vacuum tube assembly containing the hot filament cathode, an anode, a high voltage feedthru for delivering high voltage to the cathode, a getter for maintaining high vacuum, a connector for initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is fabricated from highly x-ray transparent materials, such as sapphire, diamond, or boron nitride.

  11. Detailed analysis of hollow ions spectra from dense matter pumped by X-ray emission of relativistic laser plasma

    International Nuclear Information System (INIS)

    Hansen, S. B.; Colgan, J.; Abdallah, J.; Faenov, A. Ya.; Pikuz, S. A.; Skobelev, I. Yu.; Wagenaars, E.; Culfa, O.; Dance, R. J.; Tallents, G. J.; Rossall, A. K.; Woolsey, N. C.; Booth, N.; Lancaster, K. L.; Evans, R. G.; Gray, R. J.; McKenna, P.; Kaempfer, T.; Schulze, K. S.; Uschmann, I.

    2014-01-01

    X-ray emission from hollow ions offers new diagnostic opportunities for dense, strongly coupled plasma. We present extended modeling of the x-ray emission spectrum reported by Colgan et al. [Phys. Rev. Lett. 110, 125001 (2013)] based on two collisional-radiative codes: the hybrid-structure Spectroscopic Collisional-Radiative Atomic Model (SCRAM) and the mixed-unresolved transition arrays (MUTA) ATOMIC model. We show that both accuracy and completeness in the modeled energy level structure are critical for reliable diagnostics, investigate how emission changes with different treatments of ionization potential depression, and discuss two approaches to handling the extensive structure required for hollow-ion models with many multiply excited configurations

  12. High resolution X-ray emission spectroscopy: An advanced tool for actinide research

    Science.gov (United States)

    Vitova, T.; Brendebach, B.; Dardenne, K.; Denecke, M. A.; Lebid, A.; Löble, M.; Rothe, J.; Batuk, O. N.; Hormes, J.; Liu, D.; Breher, F.; Geckeis, H.

    2010-03-01

    High resolution X-ray emission spectroscopy (HRXES) is becoming increasingly important for our understanding of electronic and coordination structures. The combination of such information with development of quantum theoretical tools will advance our capability for predicting reactivity and physical behavior especially of 5f elements. HRXES can be used to remove lifetime broadening by registering the partial fluorescence yield emitted by the sample (i.e., recording a windowed signal from the energy dispersed fluorescence emission while varying incident photon energy), thereby yielding highly resolved X-ray absorption fine structure (XAFS) spectra. Such spectra often display resonant features not observed in conventional XAFS. The spectrometer set-up can also be used for a wide range of other experiments, for example, resonant inelastic X-ray scattering (RIXS), where bulk electron configuration information in solids, liquids and gases is obtained. Valence-selective XAFS studies, where the local structure of a selected element's valence state present in a mixture of valence states can be obtained, as well as site-selective XAFS studies, where the coordination structure of a metal bound to selected elements can be differentiated from that of all the other ligating atoms. A HRXES spectrometer has been constructed and is presently being commissioned for use at the INE-Beamline for actinide research at the synchrotron source ANKA at FZK. We present the spectrometer's compact, modular design, optimized for attaining a wide range of energies, and first test measurement results. Examples from HRXES studies of lanthanides, actinides counter parts, are also shown.

  13. X-Ray Spectroscopy of Gold Nanoparticles

    Science.gov (United States)

    Nahar, Sultana N.; Montenegro, M.; Pradhan, A. K.; Pitzer, R.

    2009-06-01

    Inner shell transitions, such as 1s-2p, in heavy elements can absorb or produce hard X-rays, and hence are widely used in nanoparticles. Bio-medical research for cancer treatment has been using heavy element nanoparticles, embeded in malignant tumor, for efficient absorption of irradiated X-rays and leading emission of hard X-rays and energetic electrons to kill the surrounding cells. Ejection of a 1s electron during ionization of the element by absorption of a X-ray photon initiates the Auger cascades of emission of photons and electrons. We have investigated gold nanoparticles for the optimal energy range, below the K-edge (1s) ionization threshold, that corresponds to resonant absorption of X-rays with large attenuation coefficients, orders of magnitude higher over the background as well as to that at K-edge threshold. We applied these attenuation coefficients in Monte Carlo simulation to study the intensities of emission of photons and electrons by Auger cascades. The numerical experiments were carried out in a phantom of water cube with a thin layer, 0.1mm/g, of gold nanoparticles 10 cm inside from the surface using the well-known code Geant4. We will present results on photon and electron emission spectra from passing monochromatic X-ray beams at 67 keV, which is the resonant energy for resonant K_{α} lines, at 82 keV, the K-shell ionization threshold, and at 2 MeV where the resonant effect is non-existent. Our findings show a high peak in the gold nanoparticle absorption curve indicating complete absorption of radiation within the gold layer. The photon and electron emission spectra show resonant features. Acknowledgement: Partially supported by a Large Interdisciplinary Grant award of the Ohio State University and NASA APRA program (SNN). The computational work was carried out on the Cray X1 and Itanium 4 cluster at the Ohio Supercomputer Center, Columbus Ohio. "Resonant X-ray Irradiation of High-Z Nanoparticles For Cancer Theranostics" (refereed

  14. X-Ray Emission Spectrometer Design with Single-Shot Pump-Probe and Resonant Excitation Capabilities

    Energy Technology Data Exchange (ETDEWEB)

    Spoth, Katherine; /SUNY, Buffalo /SLAC

    2012-08-28

    Core-level spectroscopy in the soft X-ray regime is a powerful tool for the study of chemical bonding processes. The ultrafast, ultrabright X-ray pulses generated by the Linac Coherent Light Source (LCLS) allow these reactions to be studied in greater detail than ever before. In this study, we investigated a conceptual design of a spectrometer for the LCLS with imaging in the non-dispersive direction. This would allow single-shot collection of X-ray emission spectroscopy (XES) measurements with varying laser pump X-ray probe delay or a variation of incoming X-ray energy over the illuminated area of the sample. Ray-tracing simulations were used to demonstrate how the components of the spectrometer affect its performance, allowing a determination of the optimal final design. These simulations showed that the spectrometer's non-dispersive focusing is extremely sensitive to the size of the sample footprint; the spectrometer is not able to image a footprint width larger than one millimeter with the required resolution. This is compatible with a single shot scheme that maps out the laser pump X-ray probe delay in the non-dispersive direction as well as resonant XES applications at normal incidence. However, the current capabilities of the Soft X-Ray (SXR) beamline at the LCLS do not produce the required energy range in a small enough sample footprint, hindering the single shot resonant XES application at SXR for chemical dynamics studies at surfaces. If an upgraded or future beamline at LCLS is developed with lower monochromator energy dispersion the width can be made small enough at the required energy range to be imaged by this spectrometer design.

  15. HEAO A-1 observations of x ray emitting clusters of galaxies

    International Nuclear Information System (INIS)

    Johnson, M.W.

    1990-01-01

    Clusters of galaxies were known to be sources of x ray emission. Statistical analysis of how the x ray emission from clusters is related to other cluster properties was limited by the small number of clusters observed in the x ray region and the completeness of the x ray sample being considered. Both of these limitations are solved by producing a flux-limited catalog of x ray emitting Abell clusters of galaxies and using this catalog to investigate how the x ray emission correlates with other cluster properties. X ray data from the HEAO A-1 experiment were used to search for x ray emission from Abell clusters of galaxies. Selection criteria were chosen to ensure that the resulting catalog was complete and as free as possible from selection effects. The resulting identifications and x ray luminosities were used to check correlations with other cluster properties. Special consideration was given to observational selection effects and consistency checks. The data were consistent with all clusters of galaxies being x ray emitters beyond some limiting luminosity, which depends on cluster richness. Furthermore, the x ray luminosity of clusters is correlated with the richness of the cluster, its galaxy content, and the spacial distribution and galaxy content of galaxies within the cluster. It is concluded that the x ray emission from clusters of galaxies depends not only on the richness of the cluster but also the morphology of the cluster

  16. Temporal characteristic analysis of laser-modulated pulsed X-ray source for space X-ray communication

    Science.gov (United States)

    Hang, Shuang; Liu, Yunpeng; Li, Huan; Tang, Xiaobin; Chen, Da

    2018-04-01

    X-ray communication (XCOM) is a new communication type and is expected to realize high-speed data transmission in some special communication scenarios, such as deep space communication and blackout communication. This study proposes a high-speed modulated X-ray source scheme based on the laser-to-X-ray conversion. The temporal characteristics of the essential components of the proposed laser-modulated pulsed X-ray source (LMPXS) were analyzed to evaluate its pulse emission performance. Results show that the LMPXS can provide a maximum modulation rate up to 100 Mbps which is expected to significantly improve the data rate of XCOM.

  17. DISCOVERY OF X-RAY EMISSION FROM THE FIRST Be/BLACK HOLE SYSTEM

    Energy Technology Data Exchange (ETDEWEB)

    Munar-Adrover, P.; Paredes, J. M.; Ribó, M. [Departament d' Astronomia i Meteorologia, Institut de Ciències del Cosmos, Universitat de Barcelona, IEEC-UB, Martí i Franquès 1, E-08028 Barcelona (Spain); Iwasawa, K. [ICREA, Institut de Ciències del Cosmos, Universitat de Barcelona, IEEC-UB, Martí i Franquès 1, E-08028 Barcelona (Spain); Zabalza, V. [Department of Physics and Astronomy, University of Leicester, University Road, Leicester LE1 7RH (United Kingdom); Casares, J. [Instituto de Astrofísica de Canarias, E-38200 La Laguna, Tenerife (Spain)

    2014-05-10

    MWC 656 (=HD 215227) was recently discovered to be the first binary system composed of a Be star and a black hole (BH). We observed it with XMM-Newton, and detected a faint X-ray source compatible with the position of the optical star, thus proving it to be the first Be/BH X-ray binary. The spectrum analysis requires a model fit with two components, a blackbody plus a power law, with k{sub B}T=0.07{sub −0.03}{sup +0.04} keV and a photon index Γ = 1.0 ± 0.8, respectively. The non-thermal component dominates above ≅0.8 keV. The obtained total flux is F(0.3-5.5 keV)=(4.6{sub −1.1}{sup +1.3})×10{sup −14} erg cm{sup –2} s{sup –1}. At a distance of 2.6 ± 0.6 kpc the total flux translates into a luminosity L {sub X} = (3.7 ± 1.7) × 10{sup 31} erg s{sup –1}. Considering the estimated range of BH masses to be 3.8-6.9 M {sub ☉}, this luminosity represents (6.7 ± 4.4) × 10{sup –8} L {sub Edd}, which is typical of stellar-mass BHs in quiescence. We discuss the origin of the two spectral components: the thermal component is associated with the hot wind of the Be star, whereas the power-law component is associated with emission from the vicinity of the BH. We also find that the position of MWC 656 in the radio versus X-ray luminosity diagram may be consistent with the radio/X-ray correlation observed in BH low-mass X-ray binaries. This suggests that this correlation might also be valid for BH high-mass X-ray binaries (HMXBs) with X-ray luminosities down to ∼10{sup –8} L {sub Edd}. MWC 656 will allow the accretion processes and the accretion/ejection coupling at very low luminosities for BH HMXBs to be studied.

  18. EMISSION LINES BETWEEN 1 AND 2 keV IN COMETARY X-RAY SPECTRA

    Energy Technology Data Exchange (ETDEWEB)

    Ewing, Ian; Christian, Damian J. [Department of Physics and Astronomy, California State University, 18111 Nordhoff Street, Northridge, CA 91330 (United States); Bodewits, Dennis [Department of Astronomy, University of Maryland, College Park, MD 20742 (United States); Dennerl, Konrad [Max-Planck-Institut fuer extraterrestrische Physik, Postfach 1312, D-85741 Garching Germany (Germany); Lisse, Carey M. [Planetary Exploration Group, Space Department, Johns Hopkins University Applied Physics Laboratory, 11100 Johns Hopkins Rd, Laurel, MD 20723 (United States); Wolk, Scott J., E-mail: ian.ewing.794@my.csun.edu, E-mail: daman.christian@csun.edu [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States)

    2013-01-20

    We present the detection of new cometary X-ray emission lines in the 1.0-2.0 keV range using a sample of comets observed with the Chandra X-Ray Observatory and ACIS spectrometer. We have selected five comets from the Chandra sample with good signal-to-noise spectra. The surveyed comets are C/1999 S4 (LINEAR), C/1999 T1 (McNaught-Hartley), 153P/2002 (Ikeya-Zhang), 2P/2003 (Encke), and C/2008 8P (Tuttle). We modeled the spectra with an extended version of our solar wind charge exchange (SWCX) emission model. Above 1 keV, we find Ikeya-Zhang to have strong emission lines at 1340 and 1850 eV which we identify as being created by SWCX lines of Mg XI and Si XIII, respectively, and weaker emission lines at 1470, 1600, and 1950 eV formed by SWCX of Mg XII, Mg XI, and Si XIV, respectively. The Mg XI and XII and Si XIII and XIV lines are detected at a significant level for the other comets in our sample (LS4, MH, Encke, 8P), and these lines promise additional diagnostics to be included in SWCX models. The silicon lines in the 1700-2000 eV range are detected for all comets, but with the rising background and decreasing cometary emission, we caution that these detections need further confirmation with higher resolution instruments.

  19. Environmental aspects of ion-induced x-ray emission by infinitely thick targets

    International Nuclear Information System (INIS)

    Van Rinsvelt, H.A.; Dunnam, F.E.; Russell, J.P.; Bolch, W.E.

    1974-01-01

    Elemental analysis through proton and alpha particle induced x-ray emission by infinitely thick samples of environmental interest was found to be feasible. A quantization technique using internal standards and the optimization of the beam energy for optimal sensitivity were investigated. The average limit of detection ranges from about 0.1 ppM for calcium to 1 ppM for strontium

  20. XMM-Newton Detection of Hard X-Ray Emission in the Nitrogen-Type Wolf-Rayet Star WR 110

    Science.gov (United States)

    Skinner, Stephen L.; Zhekov, Svetozar A.; Güdel, Manuel; Schmutz, Werner

    2002-06-01

    We have used the excellent sensitivity of XMM-Newton to obtain the first high-quality X-ray spectrum of a Wolf-Rayet (W-R) star that is not known to be a member of a binary system. Our target, the nitrogen-type star WR 110 (HD 165688), was also observed and detected with the Very Large Array at four different frequencies. The radio flux density increases with frequency according to a power law Sν~ν+0.64+/-0.10, in very good agreement with the behavior expected for free-free wind emission. The radio data give an ionized mass-loss rate M=4.9×10-5 Msolar yr-1 for an assumed spherical constant-velocity wind. The undispersed CCD X-ray spectra reveal strong emission lines from He-like ions of Mg, Si, and S. The emission measure distribution shows a dominant contribution from cool plasma with a characteristic temperature kTcool~0.5 keV (~6 MK). Little or no excess absorption of this cool component above the value expected from the visual extinction is present. We conclude that the bulk of the cool plasma detected by XMM-Newton lies at hundreds of stellar radii or more if the wind is approximately spherical and homogeneous, but it could lie closer to the star if the wind is clumped. If the cool plasma is due to instability-driven wind shocks, then typical shock velocities are vs~340-550 km s-1 and the average filling factor of X-ray-emitting gas in the wind is no larger than f~10-6. A surprising result is the unambiguous detection of a hard X-ray component that is clearly seen in the hard-band images and the spectra. This hard component accounts for about half of the observed flux and can be acceptably fitted by a hot, optically thin thermal plasma or a power-law model. If the emission is thermal, then a temperature kThot>=3 keV is derived. Such high temperatures are not predicted by current instability-driven wind shock models, and a different mechanism is thus required to explain the hard X-rays. We examine several possible mechanisms and show that the hard emission

  1. Sawtooth-like X-ray emission observed in EBIT

    International Nuclear Information System (INIS)

    Radtke, R.; Biedermann, C.; Bachmann, P.

    2003-01-01

    The evolution of a mixture of highly charged Ar and Ba ions was measured in an electron beam ion trap (EBIT) by recording the characteristic X-ray emission from trapped ions. A special feature in the spectra are sawtooth-like intensity variations caused by a periodic collapse of the ion inventory in the trap. The effect requires favorable conditions to become present and is very sensitive to the trapping conditions. Analysis of the measurements is based on a time-dependent calculation of the trapping process. Simulations show that sawtooth activity results from the feedback between the low-Z Ar and high-Z Ba ions (Hopf bifurcation). Sawtooth spectra open up a spectroscopic method to test theoretical EBIT models and probe the dynamics in ion traps and sources

  2. An x ray scatter approach for non-destructive chemical analysis of low atomic numbered elements

    Science.gov (United States)

    Ross, H. Richard

    1993-01-01

    A non-destructive x-ray scatter (XRS) approach has been developed, along with a rapid atomic scatter algorithm for the detection and analysis of low atomic-numbered elements in solids, powders, and liquids. The present method of energy dispersive x-ray fluorescence spectroscopy (EDXRF) makes the analysis of light elements (i.e., less than sodium; less than 11) extremely difficult. Detection and measurement become progressively worse as atomic numbers become smaller, due to a competing process called 'Auger Emission', which reduces fluorescent intensity, coupled with the high mass absorption coefficients exhibited by low energy x-rays, the detection and determination of low atomic-numbered elements by x-ray spectrometry is limited. However, an indirect approach based on the intensity ratio of Compton and Rayleigh scattered has been used to define light element components in alloys, plastics and other materials. This XRS technique provides qualitative and quantitative information about the overall constituents of a variety of samples.

  3. Determination of carbon in natural freshwater biofilms with total reflection X-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Ovari, M.; Streli, C.; Wobrauschek, P.; Zaray, Gy.

    2009-01-01

    There is a growing interest in determination of low Z elements, i.e., carbon to phosphorus, in biological samples. Total reflection X-ray fluorescence spectrometry (TXRF) has been already established as suitable trace element analytical method with low sample demand and quite good quantification limits. Recently, the determinable element range was extended towards Z = 6 (carbon). Biofilms can be used for biomonioring purposes in the aquatic environment. Besides the trace metals, especially the determination of the carbon content is important for the better understanding of the early stage of biofilm formation. For this, an ATI low Z spectrometer equipped with Cr-anode X-ray tube, multilayer monochromator, vacuum chamber, and a Si(Li) detector with ultra thin window was used. Biofilms were grown on two different artificial supports (granite and plexiglass), freeze dried, suspended in high purity water and analyzed. As an internal standard the natural titanium content of the biofilms was used. The accuracy of the method was checked by total carbon measurement using a combusting carbon analyzer.

  4. Determination of carbon in natural freshwater biofilms with total reflection X-ray fluorescence spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Ovari, M. [Department of Analytical Chemistry, Eoetvoes University, Budapest, H-1117, Budapest, Pazmany Peter stny. 1/a. (Hungary)], E-mail: ovari@chem.elte.hu; Streli, C.; Wobrauschek, P. [Atominstitut of the Austrian Universities, TU-Wien, Stadionallee 2, A-1020, Wien (Austria); Zaray, Gy. [Department of Analytical Chemistry, Eoetvoes University, Budapest, H-1117, Budapest, Pazmany Peter stny. 1/a. (Hungary); Cooperative Research Centre of Environmental Chemistry, Eoetvoes University, Budapest, H-1117, Budapest, Pazmany Peter stny. 1/a. (Hungary)

    2009-08-15

    There is a growing interest in determination of low Z elements, i.e., carbon to phosphorus, in biological samples. Total reflection X-ray fluorescence spectrometry (TXRF) has been already established as suitable trace element analytical method with low sample demand and quite good quantification limits. Recently, the determinable element range was extended towards Z = 6 (carbon). Biofilms can be used for biomonioring purposes in the aquatic environment. Besides the trace metals, especially the determination of the carbon content is important for the better understanding of the early stage of biofilm formation. For this, an ATI low Z spectrometer equipped with Cr-anode X-ray tube, multilayer monochromator, vacuum chamber, and a Si(Li) detector with ultra thin window was used. Biofilms were grown on two different artificial supports (granite and plexiglass), freeze dried, suspended in high purity water and analyzed. As an internal standard the natural titanium content of the biofilms was used. The accuracy of the method was checked by total carbon measurement using a combusting carbon analyzer.

  5. Chlorine determination in (U, Pu)C fuel by total reflection X-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Misra, Nand Lal; Dhara, Sangita; Mudher, Khush Dev Singh; Aggarwal, Suresh K.; Thakur, Uday Kumar; Shah, Dipti; Sawant, R.M.; Ramakumar, K.L.

    2007-01-01

    A Total Reflection X-ray Fluorescence (TXRF) method for the determination of chlorine in (U,Pu)C has been developed. The method involves calibration of the instrument with standard solutions and validation of TXRF determination of chlorine using synthetic standard solutions. Cl K α line excited with W L α source was used for TXRF determinations of chlorine. Chlorine present in trace amounts in (U,Pu)C samples was first separated by pyro hydrolysis. The evolved chlorine, in form of HCl, was collected in 5 mM NaOH solution. This solution was analyzed for chlorine by Total Reflection X-ray Fluorescence Spectrometry using cobalt as an internal standard. The TXRF detection limit of chlorine was found to be 3.6 pg with sample size of 30 μL. In order to assess the applicability of TXRF method for chlorine determinations in other nuclear materials, one U 3 O 8 trace element standard was also analyzed for chlorine in similar way. The precision of the method was found to be 25% (1 σ) at ng level in most of the cases. (author)

  6. X-ray spectrometry and X-ray microtomography techniques for soil and geological samples analysis

    International Nuclear Information System (INIS)

    Kubala-Kukuś, A.; Banaś, D.; Braziewicz, J.; Dziadowicz, M.; Kopeć, E.; Majewska, U.; Mazurek, M.; Pajek, M.; Sobisz, M.; Stabrawa, I.; Wudarczyk-Moćko, J.; Góźdź, S.

    2015-01-01

    A particular subject of X-ray fluorescence analysis is its application in studies of the multielemental sample of composition in a wide range of concentrations, samples with different matrices, also inhomogeneous ones and those characterized with different grain size. Typical examples of these kinds of samples are soil or geological samples for which XRF elemental analysis may be difficult due to XRF disturbing effects. In this paper the WDXRF technique was applied in elemental analysis concerning different soil and geological samples (therapeutic mud, floral soil, brown soil, sandy soil, calcium aluminum cement). The sample morphology was analyzed using X-ray microtomography technique. The paper discusses the differences between the composition of samples, the influence of procedures with respect to the preparation of samples as regards their morphology and, finally, a quantitative analysis. The results of the studies were statistically tested (one-way ANOVA and correlation coefficients). For lead concentration determination in samples of sandy soil and cement-like matrix, the WDXRF spectrometer calibration was performed. The elemental analysis of the samples was complemented with knowledge of chemical composition obtained by X-ray powder diffraction.

  7. X-ray spectrometry and X-ray microtomography techniques for soil and geological samples analysis

    Energy Technology Data Exchange (ETDEWEB)

    Kubala-Kukuś, A.; Banaś, D.; Braziewicz, J. [Institute of Physics, Jan Kochanowski University, ul. Świetokrzyska 15, 25-406 Kielce (Poland); Holycross Cancer Center, ul. Artwińskiego 3, 25-734 Kielce (Poland); Dziadowicz, M.; Kopeć, E. [Institute of Physics, Jan Kochanowski University, ul. Świetokrzyska 15, 25-406 Kielce (Poland); Majewska, U. [Institute of Physics, Jan Kochanowski University, ul. Świetokrzyska 15, 25-406 Kielce (Poland); Holycross Cancer Center, ul. Artwińskiego 3, 25-734 Kielce (Poland); Mazurek, M.; Pajek, M.; Sobisz, M.; Stabrawa, I. [Institute of Physics, Jan Kochanowski University, ul. Świetokrzyska 15, 25-406 Kielce (Poland); Wudarczyk-Moćko, J. [Holycross Cancer Center, ul. Artwińskiego 3, 25-734 Kielce (Poland); Góźdź, S. [Holycross Cancer Center, ul. Artwińskiego 3, 25-734 Kielce (Poland); Institute of Public Health, Jan Kochanowski University, IX Wieków Kielc 19, 25-317 Kielce (Poland)

    2015-12-01

    A particular subject of X-ray fluorescence analysis is its application in studies of the multielemental sample of composition in a wide range of concentrations, samples with different matrices, also inhomogeneous ones and those characterized with different grain size. Typical examples of these kinds of samples are soil or geological samples for which XRF elemental analysis may be difficult due to XRF disturbing effects. In this paper the WDXRF technique was applied in elemental analysis concerning different soil and geological samples (therapeutic mud, floral soil, brown soil, sandy soil, calcium aluminum cement). The sample morphology was analyzed using X-ray microtomography technique. The paper discusses the differences between the composition of samples, the influence of procedures with respect to the preparation of samples as regards their morphology and, finally, a quantitative analysis. The results of the studies were statistically tested (one-way ANOVA and correlation coefficients). For lead concentration determination in samples of sandy soil and cement-like matrix, the WDXRF spectrometer calibration was performed. The elemental analysis of the samples was complemented with knowledge of chemical composition obtained by X-ray powder diffraction.

  8. X-ray spectra of clusters of galaxies

    Science.gov (United States)

    Sarazin, Craig L.

    1990-01-01

    X-ray line observations of clusters of galaxies have shown that the X-ray emission in clusters is mainly thermal emission from hot diffuse gas, and that much of this gas has come out of stars, probably having been ejected from galaxies in the cluster. Future high resolution observations should allow us to determine the physical state of the gas. X-ray line measurements and abundance determinations can lead to strong constraints on the origin of the intracluster gas, and on the chemical evolution and history of galaxies. Some of the stronger resonant X-ray lines may be observable as absorption lines against a background quasar. Such X-ray absorption line measurement can be used to directly derive distances to clusters, using a technique similar to (and possibly complementary to) that the well-known method using the Zel'dovich-Syunyaev effect.

  9. Charge exchange laboratory studies relevant to solar-wind-induced cometary and planetary X-ray emission

    Science.gov (United States)

    Eissa, Farhat

    The discovery of cometary X-ray emission for the first time in 1996, from comet Hyukatake using the Röntgen satellite (ROSAT) [Lisse, C. M. et al., 1996] was a highly surprising event. Since then, X-ray and extreme ultra violet (X-EUV) emission has been observed from a number of comets [Lisse, C. M. et al., 2001]. The production of such radiation is strongly believed to be the result of the charge exchange collisions of the minor heavy highly charged solar wind (SW) ions with cometary neutrals. This study reports the first state-selective He- like X-ray spectra resulting from single-electron capture (SEC) in charge exchange collisions of O 7+ and Ne 9+ with He and CO targets at a collision velocity of 800 km/s. The ions and velocity are typical of solar wind ions while the molecular and atomic targets are typical of cometary (CO) and interstellar (He) neutrals. The spectra have been obtained by means of simultaneous cold-target recoil ion momentum spectroscopic (COLTRIMS) and X-ray spectroscopic measurements that involved the triple-coincident detection of X- rays, scattered projectile, and target recoil ions. The spectra test the ability of theories to account for the relative population of triplet and singlet states in He-like product ions following SEC. The O 7+ +He spectra are compared with theoretical spectra based on quantal molecular-orbital close- coupling (QMOCC) and multi-channel Landau-Zener (MCLZ) calculations. In addition, all spectra have been used to extract angular momentum distributions based on the traditional 3:1 triplet-to-singlet ratio assumption for the populated states. The QMOCC and MCLZ calculations and the experimental results, however, suggest significant departures from this assumption. The extracted l - distributions are state-of-the-art at this time for modeling purposes due to the high differentiation power of the experimental procedure.

  10. Polarized X-Ray Emission from Magnetized Neutron Stars: Signature of Strong-Field Vacuum Polarization

    Science.gov (United States)

    Lai, Dong; Ho, Wynn C.

    2003-08-01

    In the atmospheric plasma of a strongly magnetized neutron star, vacuum polarization can induce a Mikheyev-Smirnov-Wolfenstein type resonance across which an x-ray photon may (depending on its energy) convert from one mode into the other, with significant changes in opacities and polarizations. We show that this vacuum resonance effect gives rise to a unique energy-dependent polarization signature in the surface emission from neutron stars. The detection of polarized x rays from neutron stars can provide a direct probe of strong-field quantum electrodynamics and constrain the neutron star magnetic field and geometry.

  11. Polarized x-ray emission from magnetized neutron stars: signature of strong-field vacuum polarization.

    Science.gov (United States)

    Lai, Dong; Ho, Wynn C G

    2003-08-15

    In the atmospheric plasma of a strongly magnetized neutron star, vacuum polarization can induce a Mikheyev-Smirnov-Wolfenstein type resonance across which an x-ray photon may (depending on its energy) convert from one mode into the other, with significant changes in opacities and polarizations. We show that this vacuum resonance effect gives rise to a unique energy-dependent polarization signature in the surface emission from neutron stars. The detection of polarized x rays from neutron stars can provide a direct probe of strong-field quantum electrodynamics and constrain the neutron star magnetic field and geometry.

  12. The Multi-Instrument (EVE-RHESSI) DEM for Solar Flares, and Implications for Residual Non-Thermal Soft X-Ray Emission

    Science.gov (United States)

    McTiernan, James M.; Caspi, Amir; Warren, Harry

    2015-04-01

    In the soft X-ray energy range, solar flare spectra are typically dominated by thermal emission. The low energy extent of non-thermal emission can only be loosely quantified using currently available X-ray data. To address this issue, we combine observations from the EUV Variability Experiment (EVE) on-board the Solar Dynamics Observatory (SDO) with X-ray data from the Reuven Ramaty High Energy Spectroscopic Imager (RHESSI). The improvement over the isothermal approximation is intended to resolve the ambiguity in the range where the thermal and non-thermal components may have similar photon fluxes. This "crossover" range can extend up to 30 keV for medium to large solar flares.Previous work (Caspi et.al. 2014ApJ...788L..31C) has concentrated on obtaining DEM models that fit both instruments' observations well. Now we are interested in any breaks and cutoffs in the "residual" non-thermal spectrum; i.e., the RHESSI spectrum that is left over after the DEM has accounted for the bulk of the soft X-ray emission. Thermal emission is again modeled using a DEM that is parametrized as multiple gaussians in temperature; the non-thermal emission is modeled as a photon spectrum obtained using a thin-target emission model ('thin2' from the SolarSoft Xray IDL package). Spectra for both instruments are fit simultaneously in a self-consistent manner. The results for non-thermal parameters then are compared with those found using RHESSI data alone, with isothermal and double-thermal models.

  13. Soft x-ray emission from postpulse expanding laser-produced plasmas

    International Nuclear Information System (INIS)

    Weaver, J.L.; Feldman, U.; Mostovych, A.N.; Seely, J.F.; Colombant, D.; Holland, G.

    2003-01-01

    A diagnostic spectrometer has been developed at the Naval Research Laboratory to measure the time resolved absolute intensity of radiation emitted from targets irradiated by the Nike laser. The spectrometer consists of a dispersive transmission grating of 2500 lines/mm or 5000 lines/mm and a detection system consisting of an absolutely calibrated Si photodiode array and a charge coupled device camera. In this article, this spectrometer was used to study the spatial distribution of soft x-ray radiation from low Z elements (primarily carbon) that lasted tens of nanoseconds after the main laser illumination was over. We recorded soft x-ray emission as a function of the target material and target orientation with respect to the incoming laser beam and the spectrometer line of sight. While a number of spectral features have been identified in the data, the instrument's combined temporal and spatial resolution allowed observation of the plasma expansion from CH targets for up to ∼25 ns after the cessation of the main laser pulse. The inferred plasma expansion velocities are slightly higher than those previously reported

  14. Soft x-ray emission from postpulse expanding laser-produced plasmas

    Science.gov (United States)

    Weaver, J. L.; Feldman, U.; Mostovych, A. N.; Seely, J. F.; Colombant, D.; Holland, G.

    2003-12-01

    A diagnostic spectrometer has been developed at the Naval Research Laboratory to measure the time resolved absolute intensity of radiation emitted from targets irradiated by the Nike laser. The spectrometer consists of a dispersive transmission grating of 2500 lines/mm or 5000 lines/mm and a detection system consisting of an absolutely calibrated Si photodiode array and a charge coupled device camera. In this article, this spectrometer was used to study the spatial distribution of soft x-ray radiation from low Z elements (primarily carbon) that lasted tens of nanoseconds after the main laser illumination was over. We recorded soft x-ray emission as a function of the target material and target orientation with respect to the incoming laser beam and the spectrometer line of sight. While a number of spectral features have been identified in the data, the instrument's combined temporal and spatial resolution allowed observation of the plasma expansion from CH targets for up to ˜25 ns after the cessation of the main laser pulse. The inferred plasma expansion velocities are slightly higher than those previously reported.

  15. Soft X-ray emission studies of biomaterials

    Energy Technology Data Exchange (ETDEWEB)

    Kurmaev, E.Z. E-mail: kurmaev@ifmlrs.uran.ru; Werner, J.P.; Moewes, A.; Chiuzbaian, S.; Bach, M.; Ching, W.-Y.; Motozaki, W.; Otsuka, T.; Matsuya, S.; Endo, K.; Neumann, M

    2004-07-01

    Soft X-ray fluorescence measurements are used to characterize three groups of biomaterials: Vitamin B{sub 12} and derivatives, antioxidants (aspirin and paracetamol), and human teeth. We show that the chemical bonding in Vitamin B{sub 12} is characterized by the strong Co-C bond and the relatively weak Co-N bond. The Co-C bond in cyanocobalamin is found to be stronger than that of methylcobalamin leading to their different biological activity. The chemical bonding of paracetamol and aspirin is characterized by the formation of oxygen lone-pair {pi}-orbitals, which can neutralize free radicals and therefore be related to antioxidant activity of these compounds. Carbon K{alpha} emission spectra of a caries lesion suggest that the CaCO{sub 3} like phase exists in sound enamel and that a selective loss of carbonate occurs during the early stages of a caries attack.

  16. Early evolution of an X-ray emitting solar active region

    International Nuclear Information System (INIS)

    Wolfson, C.J.; Acton, L.W.; Leibacher, J.W.; Roethig, D.T.

    1977-01-01

    The birth and early evolution of a solar active region has been investigated using X-ray observations from the Lockheed Mapping X-Ray Heliometer on board the OSO-8 spacecraft. X-ray emission is observed within three hours of the first detection of Hα plage. At that time, a plasma temperature of 4 x 10 6 K in a region having a density of the order of 10 10 cm -3 is inferred. During the fifty hours following birth almost continuous flares or flare-like X-ray bursts are superimposed on a monotonically increasing base level of X-ray emission produced by plasma with a temperature of the order 3 x 10 6 K. If it is assumed that the X-rays result from heating due to dissipation of current systems or magnetic field reconnection, it can be concluded that flare-like X-ray emission soon after active region birth implies that the magnetic field probably emerges in a stressed or complex configuration. (Auth.)

  17. Quadrupole effects in core and valence photoelectron emission from crystalline germanium measured via a spatially modulated x-ray interference field

    International Nuclear Information System (INIS)

    Nelson, E.J.; Woicik, J.C.; Pianetta, P.; Vartanyants, I.A.; Cooper, J.W.

    2002-01-01

    Near a crystal x-ray Bragg reflection, the incident and reflected x-ray beams that travel with opposite wave vectors create an x-ray standing-wave (XSW) interference field. The quadrupole (and higher order nondipole) contributions to the photoelectron emission matrix element differ for these two beams due to their different wave vectors. By monitoring the angle-resolved photoelectron yield as a function of photon energy near the (11-1) Bragg back-reflection condition of crystalline Ge, we measure the contribution of nondipole effects to Ge 3p, Ge 3d, and Ge valence-band (4s and 4p) XSW photoelectron emission. Significant changes due to nondipole emission are measured in both the apparent amplitude and phase of the Ge structure factor relative to the true Ge atomic distribution, and compared to theory

  18. A review of molecular effects in gas-phase KL X-ray emission

    Energy Technology Data Exchange (ETDEWEB)

    Guillemin, Renaud; Carniato, Stéphane; Journel, Loïc [UPMC Univ Paris 06, UMR 7614, Laboratoire de Chimie Physique Matière et Rayonnement, F-75005 Paris (France); CNRS, UMR 7614, Laboratoire de Chimie Physique Matière et Rayonnement, F-75005 Paris (France); Stolte, Wayne C. [Department of Chemistry, University of Nevada, Las Vegas, NV 89154-4003 (United States); Marchenko, Tatiana; Khoury, Lara El; Kawerk, Elie; Piancastelli, Maria Novella [UPMC Univ Paris 06, UMR 7614, Laboratoire de Chimie Physique Matière et Rayonnement, F-75005 Paris (France); CNRS, UMR 7614, Laboratoire de Chimie Physique Matière et Rayonnement, F-75005 Paris (France); Hudson, Amanda C.; Lindle, Dennis W. [Department of Chemistry, University of Nevada, Las Vegas, NV 89154-4003 (United States); Simon, Marc, E-mail: marc.simon@upmc.fr [UPMC Univ Paris 06, UMR 7614, Laboratoire de Chimie Physique Matière et Rayonnement, F-75005 Paris (France); CNRS, UMR 7614, Laboratoire de Chimie Physique Matière et Rayonnement, F-75005 Paris (France)

    2013-06-15

    The unique capabilities of resonant inelastic X-ray scattering (RIXS) to provide a deep insight into molecular dynamics following core excitation are reviewed here. Characteristic features of molecular X-ray emission are experimentally observed and theoretically interpreted. Some of our most significant results on molecular dynamics following deep core excitation are presented. In particular, we provide several examples of nuclear dynamics on the femtosecond or subfemtosecond time scale; line-narrowing effects related to the quenching of vibrational structure due to parallelism of intermediate and final state curves; anomalous line dispersion across a resonance, which is due to core-hole lifetime effects; spin–orbit-state populations derived from polarized RIXS experiments. We also show how to connect the RIXS results to the general chemical properties of the investigated systems.

  19. A review of molecular effects in gas-phase KL X-ray emission

    International Nuclear Information System (INIS)

    Guillemin, Renaud; Carniato, Stéphane; Journel, Loïc; Stolte, Wayne C.; Marchenko, Tatiana; Khoury, Lara El; Kawerk, Elie; Piancastelli, Maria Novella; Hudson, Amanda C.; Lindle, Dennis W.; Simon, Marc

    2013-01-01

    The unique capabilities of resonant inelastic X-ray scattering (RIXS) to provide a deep insight into molecular dynamics following core excitation are reviewed here. Characteristic features of molecular X-ray emission are experimentally observed and theoretically interpreted. Some of our most significant results on molecular dynamics following deep core excitation are presented. In particular, we provide several examples of nuclear dynamics on the femtosecond or subfemtosecond time scale; line-narrowing effects related to the quenching of vibrational structure due to parallelism of intermediate and final state curves; anomalous line dispersion across a resonance, which is due to core-hole lifetime effects; spin–orbit-state populations derived from polarized RIXS experiments. We also show how to connect the RIXS results to the general chemical properties of the investigated systems

  20. Plasma heating in solar flares and their soft and hard X-ray emissions

    International Nuclear Information System (INIS)

    Falewicz, R.

    2014-01-01

    In this paper, the energy budgets of two single-loop-like flares observed in X-ray are analyzed under the assumption that nonthermal electrons (NTEs) are the only source of plasma heating during all phases of both events. The flares were observed by RHESSI and GOES on 2002 February 20 and June 2, respectively. Using a one-dimensional (1D) hydrodynamic code for both flares, the energy deposited in the chromosphere was derived applying RHESSI observational data. The use of the Fokker-Planck formalism permits the calculation of distributions of the NTEs in flaring loops and thus spatial distributions of the X-ray nonthermal emissions and integral fluxes for the selected energy ranges that were compared with the observed ones. Additionally, a comparative analysis of the spatial distributions of the signals in the RHESSI images was conducted for the footpoints and for all the flare loops in selected energy ranges with these quantities' fluxes obtained from the models. The best compatibility of the model and observations was obtained for the 2002 June 2 event in the 0.5-4 Å GOES range and total fluxes in the 6-12 keV, 12-25 keV, 20-25 keV, and 50-100 keV energy bands. Results of photometry of the individual flaring structures in a high energy range show that the best compliance occurred for the 2002 June 2 flare, where the synthesized emissions were at least 30% higher than the observed emissions. For the 2002 February 20 flare, synthesized emission is about four times lower than the observed one. However, in the low energy range the best conformity was obtained for the 2002 February 20 flare, where emission from the model is about 11% lower than the observed one. The larger inconsistency occurs for the 2002 June 2 solar flare, where synthesized emission is about 12 times greater or even more than the observed emission. Some part of these differences may be caused by inevitable flaws of the applied methodology, like by an assumption that the model of the flare is