Soft X-ray Foucault test: A path to diffraction-limited imaging

Science.gov (United States)

Ray-Chaudhuri, A. K.; Ng, W.; Liang, S.; Cerrina, F.

1994-08-01

We present the development of a soft X-ray Foucault test capable of characterizing the imaging properties of a soft X-ray optical system at its operational wavelength and its operational configuration. This optical test enables direct visual inspection of imaging aberrations and provides real-time feedback for the alignment of high resolution soft X-ray optical systems. A first application of this optical test was carried out on a Mo-Si multilayer-coated Schwarzschild objective as part of the MAXIMUM project. Results from the alignment procedure are presented as well as the possibility for testing in the hard X-ray regime.

Modeling the focusing efficiency of lobster-eye optics for image shifting depending on the soft x-ray wavelength.

Science.gov (United States)

Su, Luning; Li, Wei; Wu, Mingxuan; Su, Yun; Guo, Chongling; Ruan, Ningjuan; Yang, Bingxin; Yan, Feng

2017-08-01

Lobster-eye optics is widely applied to space x-ray detection missions and x-ray security checks for its wide field of view and low weight. This paper presents a theoretical model to obtain spatial distribution of focusing efficiency based on lobster-eye optics in a soft x-ray wavelength. The calculations reveal the competition mechanism of contributions to the focusing efficiency between the geometrical parameters of lobster-eye optics and the reflectivity of the iridium film. In addition, the focusing efficiency image depending on x-ray wavelengths further explains the influence of different geometrical parameters of lobster-eye optics and different soft x-ray wavelengths on focusing efficiency. These results could be beneficial to optimize parameters of lobster-eye optics in order to realize maximum focusing efficiency.

Alkali Halide Microstructured Optical Fiber for X-Ray Detection

Science.gov (United States)

DeHaven, S. L.; Wincheski, R. A.; Albin, S.

2014-01-01

Microstructured optical fibers containing alkali halide scintillation materials of CsI(Na), CsI(Tl), and NaI(Tl) are presented. The scintillation materials are grown inside the microstructured fibers using a modified Bridgman-Stockbarger technique. The x-ray photon counts of these fibers, with and without an aluminum film coating are compared to the output of a collimated CdTe solid state detector over an energy range from 10 to 40 keV. The photon count results show significant variations in the fiber output based on the materials. The alkali halide fiber output can exceed that of the CdTe detector, dependent upon photon counter efficiency and fiber configuration. The results and associated materials difference are discussed.

Characteristics of soft X-ray lens

International Nuclear Information System (INIS)

Qin Yi

2007-12-01

A soft X-lens was devised with waveguide X-ray optics of total external reflection (TER). The lens consists of a stack of 1 387 TER waveguides with inner diameter of 0.45 mm and outer diameter of 0.60 mm. With the help of plasma sources of soft X-ray radiation, high density of pure soft X-ray radiation (without plasma expansion fragments) with broad-band spectral range can be obtained at the focus of the lens. As laser-plasma is considered, the radiation density of 1.3 x 10 5 W/cm 2 is obtained, the transmission coefficient is 18.6%, the ratio of the density at the focus with and without the lens is 1000 and the radiation capture is 28.9 degree. The density of 0.5 TW/cm 2 can be obtained as far as Qiang-Guang I facility is considered. (authors)

Space- and time-resolved diagnostics of soft x-ray emission from laser plasmas

International Nuclear Information System (INIS)

Richardson, M.C.; Jaanimagi, P.A.; Chen, H.

1988-01-01

The analysis of soft x-ray emission from plasmas created by intense short-wavelength laser radiation can provide much useful information on the density, temperature and ionization distribution of the plasma. Until recently, limitations of sensitivity and the availability of suitable x-ray optical elements have restricted studies of soft x-ray emission from laser plasmas. In this paper, the authors describe novel instrumentation which provides high sensitivity in the soft x-ray spectrum with spatial and temporal resolution in the micron and picosecond ranges respectively. These systems exploit advances made in soft x-ray optic and electro-optic technology. Their application in current studies of laser fusion, x-ray lasers, and high density atomic physics are discussed

X-ray optics and X-ray microscopes: new challenges

International Nuclear Information System (INIS)

Susini, J.

2004-01-01

Soon after the discovery of X-rays in 1895 by W. Roentgen, it became rapidly clear that the methods traditionally used in the visible light regime, namely refraction, diffraction and reflection were difficult to apply for X-ray optics. The physical origins of these difficulties are closely linked to the very nature of interaction of X-rays with matter. The small deviation δ of the refractive index of condensed matter from unity makes it difficult to extend refraction-based optics from the optical spectral region to the X-ray region because the refraction angle is proportional to δ. Similarly it is very challenging to extend diffraction-based focusing techniques to X-rays because the diffraction angle scales inversely with wavelength. Finally, the use of reflection-based optics is also limited by the very small critical angle for total reflection. All those fundamental limitations prevented for almost one century, the development of X-ray microscopy whereas electron microscopy became a standard tool. In the past twenty years, interests for X-ray microscopy revived, mainly because of several major advances in X-ray sources and X-ray optics. X-ray microscopy techniques are now emerging as powerful and complementary tools for submicron investigations. Soft X-ray microscopes offer traditionally the possibility to form direct images of thick hydrated biological material in near-native environment, at a spatial resolution well beyond that achievable with visible light microscopy. Natural contrast is available in the soft X-ray region, in the so-called ''water-window'', due to the presence of absorption edges of the major constituents (C,N,O). Recent advances in manufacturing techniques have enlarged the accessible energy range of micro-focussing optics and offer new applications in a broad range of disciplines. X-ray microscopy in the 1 - 30 keV energy range is better suited for fluorescence to map trace elements, tomography for 3D imaging and micro-diffraction. The

Soft x-ray spectrographs for solar observations

International Nuclear Information System (INIS)

Bruner, M.E.

1988-01-01

This paper surveys some of the recent advances in the state of the art of soft X-ray spectrometers, particularly as they might be applied to Solar Observations. The discussions center on the windowless region from roughly 1 to 100 A, and covers both grating and crystal instruments. The author begins with a short discussion of the solar soft X-ray spectrum and its interpretation, followed by a few general comments on problems peculiar to soft X-ray instruments. The paper reviews of recent developments in spectrometer optical design, which has been a lively field during the last dozen years. This is particularly true in the case of grating spectrometers. The paper concludes with a short section on telescope considerations, and some remarks on future flight opportunities

Optical systems for synchrotron radiation: lecture 4. Soft x-ray imaging systems

International Nuclear Information System (INIS)

Howells, M.R.

1986-04-01

The history and present techniques of soft x-ray imaging are reviewed briefly. The physics of x-ray imaging is described, including the temporal and spatial coherence of x-ray sources. Particular technologies described are: contact x-ray microscopy, zone plate imaging, scanned image zone plate microscopy, scanned image reflection microscopy, and soft x-ray holography and diffraction

A beam intensity monitor for the evaluation beamline for soft x-ray optical elements

International Nuclear Information System (INIS)

Imazono, Takashi; Moriya, Naoji; Harada, Yoshihisa; Sano, Kazuo; Koike, Masato

2012-01-01

Evaluation Beamline for Soft X-Ray Optical Elements (BL-11) at the SR Center of Ritsumeikan University has been operated to measure the wavelength and angular characteristics of soft x-ray optical components in a wavelength range of 0.65-25 nm using a reflecto-diffractometer (RD). The beam intensity monitor that has been equipped in BL-11 has observed the signal of the zero-th order light. For the purpose of more accurate evaluation of the performance of optical components, a new beam intensity monitor to measure the intensity of the first order light from the monochromator in BL-11 has been developed and installed in just front of RD. The strong positive correlation between the signal of the beam monitor and a detector equipped in the RD is shown. It is successful that the beam intensity of the first order light can be monitored in real time.

Soft X-ray imaging of thick carbon-based materials using the normal incidence multilayer optics.

Science.gov (United States)

Artyukov, I A; Feschenko, R M; Vinogradov, A V; Bugayev, Ye A; Devizenko, O Y; Kondratenko, V V; Kasyanov, Yu S; Hatano, T; Yamamoto, M; Saveliev, S V

2010-10-01

The high transparency of carbon-containing materials in the spectral region of "carbon window" (lambda approximately 4.5-5nm) introduces new opportunities for various soft X-ray microscopy applications. The development of efficient multilayer coated X-ray optics operating at the wavelengths of about 4.5nm has stimulated a series of our imaging experiments to study thick biological and synthetic objects. Our experimental set-up consisted of a laser plasma X-ray source generated with the 2nd harmonics of Nd-glass laser, scandium-based thin-film filters, Co/C multilayer mirror and X-ray film UF-4. All soft X-ray images were produced with a single nanosecond exposure and demonstrated appropriate absorption contrast and detector-limited spatial resolution. A special attention was paid to the 3D imaging of thick low-density foam materials to be used in design of laser fusion targets.

A soft X-ray image of the Moon

International Nuclear Information System (INIS)

Schmitt, J.H.M.M.; Aschenbach, B.; Hasinger, G.; Pfeffermann, E.; Predehl, P.; Truemper, J.; Snowden, S.L.; Wisconsin Univ., Madison, WI

1991-01-01

A soft X-ray image of the Moon obtained by the Roentgen Observatory Satellite ROSAT clearly shows a sunlit crescent, demonstrating that the Moon's X-ray luminosity arises from backscattering of solar X-rays. The Moon's optically dark side is also X-ray dark, and casts a distinct shadow on the diffuse cosmic X-ray background. Unexpectedly, the dark side seems to emit X-rays at a level about one per cent that of the bright side; this emission very probably results from energetic solar-wind electrons striking the Moon's surface. (author)

Beam line for experiments with coherent soft x-rays

International Nuclear Information System (INIS)

Howells, M.R.; Kirz, J.; Krinsky, S.

1982-12-01

The advantages of coherent soft x-rays for three-dimensional imaging of biological specimens are discussed, the x-ray source requirements are described, and the general design of the beam line and its optical system are given

A development of laser-plasma-based soft x-ray microscope system

International Nuclear Information System (INIS)

Nam, Ki Yong; Kim, Kyong Woo; Kim, Kyu Gyeom; Kwon, Young Man; Yoon, Kwon Ha

2003-01-01

Soft x-ray nano-imaging microscopy system for biomedical application with a high resolution about 50 nm has been designed and described, and its integrated techniques also have been studied. The system is mainly composed of soft x-ray generation system, nano-scaled control system, x-ray optical device like a condenser or object mirror, a CCD camera coupled with multichannel plate (MCP) and vacuum system. In the system, soft x-ray is generated from the laser-based plasma by focusing Nd:YAG laser beam on tantalum (Ta) target. In an x-ray optical system, a wolter mirror has been considering condensing the x-ray beam on a biological specimen and zone plate was adapted as an object mirror. A Si 3 N 4 was used as specimen holder for keeping a biological sample alive in atmosphere conditions. A back-illuminated-CCD camera coupled with multichannel plate was determined to set up.

A development of laser-plasma-based soft x-ray microscope system

Energy Technology Data Exchange (ETDEWEB)

Nam, Ki Yong; Kim, Kyong Woo; Kim, Kyu Gyeom; Kwon, Young Man; Yoon, Kwon Ha [X-ray Microscopy Research Center, Wonkwang University, Iksan (Korea, Republic of)

2003-07-01

Soft x-ray nano-imaging microscopy system for biomedical application with a high resolution about 50 nm has been designed and described, and its integrated techniques also have been studied. The system is mainly composed of soft x-ray generation system, nano-scaled control system, x-ray optical device like a condenser or object mirror, a CCD camera coupled with multichannel plate (MCP) and vacuum system. In the system, soft x-ray is generated from the laser-based plasma by focusing Nd:YAG laser beam on tantalum (Ta) target. In an x-ray optical system, a wolter mirror has been considering condensing the x-ray beam on a biological specimen and zone plate was adapted as an object mirror. A Si{sub 3}N{sub 4} was used as specimen holder for keeping a biological sample alive in atmosphere conditions. A back-illuminated-CCD camera coupled with multichannel plate was determined to set up.

First images from the Stanford tabletop scanning soft x-ray microscope

International Nuclear Information System (INIS)

Trail, J.A.; Byer, R.L.

1988-01-01

The authors have constructed a scanning soft x-ray microscope which uses a laser-produced plasma as the soft x-ray source and normal incidence multilayer coated mirrors in a Schwarzschild configuration as the focusing optics. The microscope operates at a wavelength of 140 angstrom, has a spatial resolution of 0.5 μm, and has a soft x-ray photon flux through the focus of 10 4 s -1 when operated with only 170 mW of average laser power. The microscope is compact; the complete system, including the laser, fits on a single optical table. In this paper they describe the microscope and present images of metallic microstructures

First application experiments with the Stockholm compact soft x-ray microscope

International Nuclear Information System (INIS)

Bertilson, M; Hofsten, O von; Lindblom, M; Holmberg, A; Takman, P; Vogt, U; Hertz, H; Thieme, J

2009-01-01

Most soft x-ray microscopes operating in the water window (λ = 2.3 - 4.4 nm) rely on synchrotron radiation sources. In the future we believe scientists will use soft x-ray microscopes as one imaging tool among others in their own laboratory. For this purpose we have developed a full field soft x-ray microscope with a laser-plasma source compact enough to fit on an optical table. In this contribution we describe the current status of this microscope now featuring stable operation at λ = 3.37 nm or λ 2.48 nm. In-house fabricated single element zone plates offering the possibility to perform phase contrast imaging have been implemented. We also report on the first application experiments for compact soft x-ray microscopy, including results from studies of clay minerals and colloids existing in nature and results from phase optics experiments. Planned upgrades of the microscope include increasing the source brightness, implementing more efficient condenser optics, and installing a cryo sample stage for tomography. These improvements will open up for further applications, especially in the field of biological imaging.

Transient soft X-ray sources

International Nuclear Information System (INIS)

Hayakawa, S.; Murakami, T.; Nagase, F.; Tanaka, Y.; Yamashita, K.

1976-01-01

A rocket observation of cosmic soft X-rays suggests the existence of transient, recurrent soft X-ray sources which are found variable during the flight time of the rocket. Some of the soft X-ray sources thus far reported are considered to be of this time. These sources are listed and their positions are shown. (Auth.)

Development of NaI(Tl) scintillating films for imaging soft x-rays

International Nuclear Information System (INIS)

Shepherd, J.A.

1993-01-01

Thin film NaI(Tl) scintillators, of areas of up to 130 cm 2 , have been fabricated and characterized for use on soft x-ray imaging photomultiplier tubes. Relevant parameters of photon-counting imaging detectors are defined and used to predict the performance of several materials, including CsI(Na), CsI(Tl), CaF 2 (Eu), Lu 2 (SiO 4 )O:Ce, and NaI(Tl), as thin film scintillators on fiber optic substrates. Also, x-ray imaging methodologies are compared. The NaI(Tl) films were vapor-deposited onto quartz and fiber optic substrates using a powder flash deposition technique. When compared to single crystal NaI(Tl), the films were found to have equally high light yield but lower energy resolution. Light yield optimization was studied in detail including the effects of substrate temperature, activator concentration in the evaporant, and boat temperature. Spatial resolution as well as parallax errors are discussed and measured for film thicknesses up to 61 μm. A technique is described that can substantially increase the light collection of high index films on fiber optic disks. The light collection was improved by 20% by coating the disk with potassium silicate before the NaI(Tl) deposition. Large area films, up to 130 cm 2 , had a spatial uniformity of response within ±1.5% for count rate and ±3.5% for light yield, and their spatial resolution exceeded 16.6 lp mm -1 when deposited onto fiber optic substrates. The 8-keV x-ray detection efficiency of the microchannel plate imaging photomultiplier tube coupled to a NaI(Tl) film scintillator is predicted to be 88%. Other uses for the films are also described

Performance limitations of imaging microscopes for soft x-ray applications

International Nuclear Information System (INIS)

Lewotsky, K.L.; Kotha, A.; Harvey, J.E.

1993-01-01

Recent advances in the fabrication of nanometer-scale multilayer structures have yielded high-reflectance mirrors operating at near-normal incidence for soft X-ray wavelengths. These developments have stimulated renewed interest in high-resolution soft X-ray microscopy. The design of a Schwarzschild imaging microscope for soft X-ray applications has been reported by Hoover and Shealy. Based upon a geometrical ray-trace analysis of the residual design errors, diffraction-limited performance at a wavelength of 100 angstrom was predicted over an object size (diameter) of 0.4 mm. In this paper the authors expand upon the previous analysis of the Schwarzschild X-ray microscope design by determining the total image degradation due to diffraction, geometrical aberrations, alignment errors, and realistic assumptions concerning optical fabrication errors. NASA's Optical Surface Analysis Code (OSAC) is used to model the image degradation effects of residual surface irregularities over the entire range of relevant spatial frequencies. This includes small angle scattering effects due to mid spatial frequency surface errors falling between the traditional figure and finish specifications. Performance predictions are presented parametrically to provide some insight into the optical fabrication and alignment tolerances necessary to meet a particular image quality requirement

Center for X-Ray Optics, 1986

International Nuclear Information System (INIS)

1987-07-01

The Center for X-Ray Optics has made substantial progress during the past year on the development of very high resolution x-ray technologies, the generation of coherent radiation at x-ray wavelengths, and, based on these new developments, had embarked on several scientific investigations that would not otherwise have been possible. The investigations covered in this report are topics on x-ray sources, x-ray imaging and applications, soft x-ray spectroscopy, synchrotron radiation, advanced light source and magnet structures for undulators and wigglers

Soft X-ray spectrographs for solar observations

Science.gov (United States)

Bruner, M. E.

1988-01-01

Recent advances in soft X-ray spectrometery are reviewed, with emphasis on techniques for studying the windowless region from roughly 1-100 A. Recent technological developments considered include multilayer mirrors, large-format CCD detectors which are sensitive to X-rays, position-sensitive photon counting detectors, new kinds of X-ray films, and optical systems based on gratings with nonuniform ruling spacings. Improvements in the extent and accuracy of the atomic physics data sets on which the analysis of spectroscopic observatons depend are also discussed.

Report of workshop on X-ray and nonlinear optics

International Nuclear Information System (INIS)

Nasu, Keiichiro; Namikawa, Kazumichi

1994-07-01

As synchrotron radiation has advanced to high luminance, the possibility of realizing coherent light has heightened, and the nonlinear optical phenomena in soft and hard X-ray regions have become the object of the concern of X-ray researchers, and also the researchers in the fields of quantum electronics and optical properties. This workshop was held on September 21 and 22, 1993 at National Laboratory for High energy Physics. Lectures were given on the generation of second harmonic of X-ray by utilizing dynamic diffraction, X-ray parametric scattering induced by strong laser beam, the resonance enhancement of X-ray inelastic scattering induced by strong visible light, Raman scattering in soft X-ray region, the control of nonlinear optical processes by strong external field; the experiments, though they are fundamental, they have not been carried out; undulator radiation X-ray and X-ray free electron laser, the improvement of the coherence of X-ray laser, superradiance of Frenkel excitor system and the measurement of superhigh speed pulses in X-ray region. The comment from the standpoint of the research on nonlinear optics was given. In this document, the gists of these lectures are collected. (K.I.)

Report of workshop on X-ray and nonlinear optics

Energy Technology Data Exchange (ETDEWEB)

Nasu, Keiichiro; Namikawa, Kazumichi [eds.

1994-07-01

As synchrotron radiation has advanced to high luminance, the possibility of realizing coherent light has heightened, and the nonlinear optical phenomena in soft and hard X-ray regions have become the object of the concern of X-ray researchers, and also the researchers in the fields of quantum electronics and optical properties. This workshop was held on September 21 and 22, 1993 at National Laboratory for High energy Physics. Lectures were given on the generation of second harmonic of X-ray by utilizing dynamic diffraction, X-ray parametric scattering induced by strong laser beam, the resonance enhancement of X-ray inelastic scattering induced by strong visible light, Raman scattering in soft X-ray region, the control of nonlinear optical processes by strong external field; the experiments, though they are fundamental, they have not been carried out; undulator radiation X-ray and X-ray free electron laser, the improvement of the coherence of X-ray laser, superradiance of Frenkel excitor system and the measurement of superhigh speed pulses in X-ray region. The comment from the standpoint of the research on nonlinear optics was given. In this document, the gists of these lectures are collected. (K.I.).

Neutron and soft X-ray emission from wire array Z-pinch imploding onto deuterated fiber

International Nuclear Information System (INIS)

Klir, D.; Kravarik, J.; Kubes, P.

2005-01-01

The implosion of a wire array Z-pinch onto a deuterated fiber was studied. The peak power of soft X-rays exceeded 200 GW and the total emitted energy was 2-8 kJ. The radiation was close to the radiation of the blackbody with the temperature of 40 eV. The neutron yield from the D-D reaction reached 2x10 8 per shot. The mean energy of neutrons determined in the axial direction was shifted from 2.45 MeV towards higher energies [ru

Soft-x-ray magneto-optical Kerr effect and element-specific hysteresis measurement

Energy Technology Data Exchange (ETDEWEB)

Kortright, J.B.; Rice, M. [Lawrence Berkeley National Lab., CA (United States)

1997-04-01

Interest in the utilization of x-ray magneto-optical properties to provide element-specific magnetic information, combined with recent development of tunable linear polarizers for spectroscopic polarization measurement, have led the authors to the study of magneto-optical rotation (MOR) near core levels of magnetic atoms in magnetic multilayer and alloy films. Their initial observation of Faraday rotation (in transmission) demonstrated that for Fe MOR is easily measured and is larger at its L{sub 3} resonance than in the near-visible spectral regions. This work also demonstrated that the spectroscopic behavior of the MOR signal in transmission, resulting from the differential reaction of left- and right-circular components of a linearly polarized beam, is related to the magnetic circular dichroism (MCD), or differential absorption, as expected by a Kramers-Kronig transformation. Thus MCD measurements using circular polarization and MOR measurements using linear polarization can provide complementary, and in some cases equivalent, information. On beamline 6.3.2 the authors have begun to investigate soft x-ray MOR in the reflection geometry, the x-ray magneto-optic Kerr effect (XMOKE). Early measurements have demonstrated the ability to measure element-specific hysteresis loops and large rotations compared to analogous near-visible measurements. The authors are investigating the spectral dependence of the XMOKE signal, and have initiated systematic materials studies of sputter-deposited films of Fe, Fe{sub x}Cr{sub 1{minus}x} alloys, and Fe/Cr multilayers.

Contact microscopy with a soft x-ray laser

International Nuclear Information System (INIS)

DiCicco, D.S.; Kim, D.; Rosser, R.J.; Skinner, C.H.; Suckewer, S.; Gupta, A.P.; Hirschberg, J.G.

1989-03-01

A soft x-ray laser of output energy 1-3 mJ at 19.2 nm has been used to record high resolution images of biological specimens. The contact images were recorded on photoresist which was later viewed in a scanning electron microscope. We also present a Composite Optical X- ray Laser Microscope ''COXRALM'' of novel design. 14 refs., 8 figs., 1 tab

Production of Coherent xuv and soft-x-ray light using a transverse optical klystron

International Nuclear Information System (INIS)

Kincaid, B.M.; Freeman, R.R.

1984-01-01

This section describes the theory of the production of coherent xuv radiation and soft x rays using a transverse optical klystron (TOK). A TOK uses a high-power laser in conjunction with an undulator magnet to produce laserlike output of xuv radiation from a relativistic electron beam. 16 references, 5 figures

Soft x-ray Planetary Imager

Data.gov (United States)

National Aeronautics and Space Administration — The project is to prototype a soft X-ray Imager for planetary applications that has the sensitivity to observe solar system sources of soft  X-ray emission. A strong...

Soft x-ray camera for internal shape and current density measurements on a noncircular tokamak

International Nuclear Information System (INIS)

Fonck, R.J.; Jaehnig, K.P.; Powell, E.T.; Reusch, M.; Roney, P.; Simon, M.P.

1988-05-01

Soft x-ray measurements of the internal plasma flux surface shaped in principle allow a determination of the plasma current density distribution, and provide a necessary monitor of the degree of internal elongation of tokamak plasmas with a noncircular cross section. A two-dimensional, tangentially viewing, soft x-ray pinhole camera has been fabricated to provide internal shape measurements on the PBX-M tokamak. It consists of a scintillator at the focal plane of a foil-filtered pinhole camera, which is, in turn, fiber optically coupled to an intensified framing video camera (/DELTA/t />=/ 3 msec). Automated data acquisition is performed on a stand-alone image-processing system, and data archiving and retrieval takes place on an optical disk video recorder. The entire diagnostic is controlled via a PDP-11/73 microcomputer. The derivation of the polodial emission distribution from the measured image is done by fitting to model profiles. 10 refs., 4 figs

Debris-free soft x-ray source with gas-puff target

Science.gov (United States)

Ni, Qiliang; Chen, Bo; Gong, Yan; Cao, Jianlin; Lin, Jingquan; Lee, Hongyan

2001-12-01

We have been developing a debris-free laser plasma light source with a gas-puff target system whose nozzle is driven by a piezoelectric crystal membrane. The gas-puff target system can utilize gases such as CO2, O2 or some gas mixture according to different experiments. Therefore, in comparison with soft X-ray source using a metal target, after continuously several-hour laser interaction with gas from the gas-puff target system, no evidences show that the light source can produce debris. The debris-free soft X-ray source is prepared for soft X-ray projection lithography research at State Key Laboratory of Applied Optics. Strong emission from CO2, O2 and Kr plasma is observed.

Soft x-ray streak cameras

International Nuclear Information System (INIS)

Stradling, G.L.

1988-01-01

This paper is a discussion of the development and of the current state of the art in picosecond soft x-ray streak camera technology. Accomplishments from a number of institutions are discussed. X-ray streak cameras vary from standard visible streak camera designs in the use of an x-ray transmitting window and an x-ray sensitive photocathode. The spectral sensitivity range of these instruments includes portions of the near UV and extends from the subkilovolt x- ray region to several tens of kilovolts. Attendant challenges encountered in the design and use of x-ray streak cameras include the accommodation of high-voltage and vacuum requirements, as well as manipulation of a photocathode structure which is often fragile. The x-ray transmitting window is generally too fragile to withstand atmospheric pressure, necessitating active vacuum pumping and a vacuum line of sight to the x-ray signal source. Because of the difficulty of manipulating x-ray beams with conventional optics, as is done with visible light, the size of the photocathode sensing area, access to the front of the tube, the ability to insert the streak tube into a vacuum chamber and the capability to trigger the sweep with very short internal delay times are issues uniquely relevant to x-ray streak camera use. The physics of electron imaging may place more stringent limitations on the temporal and spatial resolution obtainable with x-ray photocathodes than with the visible counterpart. Other issues which are common to the entire streak camera community also concern the x-ray streak camera users and manufacturers

Extending the methodology of X-ray crystallography to allow X-ray microscopy without X-ray optics

International Nuclear Information System (INIS)

Miao Jianwei; Kirz, Janos; Sayre, David; Charalambous, Pambos

2000-01-01

We demonstrate that the soft X-ray diffraction pattern from a micron-size noncrystalline specimen can be recorded and inverted to form a high-resolution image. The phase problem is overcome by oversampling the diffraction pattern. The image is obtained using an iterative algorithm. The technique provides a method for X-ray microscopy requiring no high-resolution X-ray optical elements or detectors. In the present work, a resolution of approximately 60 nm was obtained, but we believe that considerably higher resolution can be achieved

Summary of radiation-induced transient absorption and recovery in fiber optic waveguides. [Pulsed electrons and x-rays

Energy Technology Data Exchange (ETDEWEB)

Skoog, C.D.

1976-11-01

The absorption induced in fiber optic waveguides by pulsed electron and X-ray radiation has been measured as a function of optical wavelength from 450 to 950 nm, irradiation temperature from -54 to 71/sup 0/C, and dose from 1 to 500 krads. The fibers studied are Ge-doped silica core fibers (Corning Low Loss), ''pure'' vitreous silica core fibers (Schott, Bell Laboratories, Fiberoptic Cable Corp., and Valtec Fiberoptics), polymethyl-methacrylate core fibers (DuPont CROFON and PFX), and polystyrene core fibers (International Fiber Optics and Polyoptics). Models that have been developed to account for the observed absorption recovery are also summarized.

Use of an axisymmetric microscope with electronic readout for collecting soft X-ray images

International Nuclear Information System (INIS)

Cavailler, C.; Henry, P.; Launspach, J.; De Mascureau, J.; Millerioux, M.; Rostaing, M.; Sauneuf, R.

1984-08-01

The axisymmetric microscope, first discussed by Wolter, provides high resolution and sensitivity for investigating the soft X-ray emission of laser-driven plasmas. Such a device having a 10 X magnification has been constructed. We present a comparison between the images of laser-driven plasmas given by this microscope and by a 10 X pinhole camera. Until now these images were recorded on X-ray film. We have shown that film could be replaced by C.C.D. in a pinhole camera when the photon energy lies within the 1-10 keV range. Below 1 keV the quantum yield is too low so we have used an image converter tube made by RTC. It is a diode-inverter tube with a soft X-ray photocathode and a P20 phosphor deposited on an optic fiber plate. The electronic image appearing on the screen is read by a C.C.D. working in the visible spectral fields. An electronic image readout chain, which is identical to those associated with streak cameras, then processes automatically and immediately the images given by the microscope [fr

Pulsed x-ray induced attenuation measurements of single mode optical fibers and coupler materials

International Nuclear Information System (INIS)

Johan, A.; Charre, P.

1994-01-01

Pulsed X-ray induced transient radiation attenuation measurements of single mode optical fibers have been performed versus total dose, light wavelength, optical power and fiber coil diameter in order to determine the behavior of parameters sensitive to ionizing radiation. The results did not show any photobleaching phenomenon and the attenuation was found independent of the spool diameter. As expected, transient attenuation was lower for higher wave-lengths. The recovery took place in the millisecond range and was independent of total dose, light wavelength and optical power. In optical modules and devices a large range of behaviors was observed according to coupler material i.e., Corning coupler showed a small peak attenuation that remained more than one day later; on the other hand LiTaO 3 material experienced an order of magnitude higher peak attenuation and a recovery in the millisecond range. For applications with optical fibers and integrated optics devices the authors showed that in many cases the optical fiber (length above 100 m) is the most sensitive device in a transient ionizing radiation field

Low energy (soft) x rays

International Nuclear Information System (INIS)

Hoshi, Masaharu; Antoku, Shigetoshi; Russell, W.J.; Miller, R.C.; Nakamura, Nori; Mizuno, Masayoshi; Nishio, Shoji.

1987-05-01

Dosimetry of low-energy (soft) X rays produced by the SOFTEX Model CMBW-2 was performed using Nuclear Associates Type 30 - 330 PTW, Exradin Type A2, and Shonka-Wyckoff ionization chambers with a Keithley Model 602 electrometer. Thermoluminescent (BeO chip) dosimeters were used with a Harshaw Detector 2000-A and Picoammeter-B readout system. Beam quality measurements were made using aluminum absorbers; exposure rates were assessed by the current of the X-ray tube and by exposure times. Dose distributions were established, and the average factors for non-uniformity were calculated. The means of obtaining accurate absorbed and exposed doses using these methods are discussed. Survival of V79 cells was assessed by irradiating them with soft X rays, 200 kVp X rays, and 60 Co gamma rays. The relative biological effectiveness (RBE) values for soft X rays with 0, 0.2, 0.7 mm added thicknesses of aluminum were 1.6, which were compared to 60 Co. The RBE of 200 kVp X rays relative to 60 Co was 1.3. Results of this study are available for reference in future RERF studies of cell survival. (author)

Development of Compact Soft X-ray Source Based on Laser Undulator

CERN Document Server

Kuroda, Ryunosuke; Minamiguchi, S; Saitô, T; Ueyama, D; Washio, Masakazu

2004-01-01

A compact soft X-ray source is required in various research fields such as material and biological science. The laser undulator based on backward Compton scattering has been developed as a compact soft X-ray source for the biological observation at Waseda University. It is performed in a water window region (250eV - 500 eV) using the interaction between 1047 nm Nd:YLF laser and 4 MeV high quality electron beam generated from rf gun system. The range of energy in the water window region has K-shell absorption edges of Oxygen, Carbon and Nitrogen, which mainly constitute of living body. Since the absorption coefficient of water is much smaller than the protein’s coefficient in this range, a dehydration of the specimens is not necessary. As a preliminary experiment, about 300 eV X-ray generation was carried out. As next step, soft X-ray optics with zone plate was proposed for Soft X-ray microscopy. In this conference, we will report details and results of the experiment.

Optical technologies for extreme-ultraviolet and soft X-ray coherent sources

International Nuclear Information System (INIS)

Canova, Federico; Poletto, Luca

2015-01-01

The book reviews the most recent achievements in optical technologies for XUV and X-ray coherent sources. Particular attention is given to free-electron-laser facilities, but also to other sources available at present, such as synchrotrons, high-order laser harmonics and X-ray lasers. The optical technologies relevant to each type of source are discussed. In addition, the main technologies used for photon handling and conditioning, namely multilayer mirrors, adaptive optics, crystals and gratings are explained. Experiments using coherent light received during the last decades a lot of attention for the X-ray regime. Strong efforts were taken for the realization of almost fully coherent sources, e.g. the free-electron lasers, both as independent sources in the femtosecond and attosecond regimes and as seeding sources for free-electron-lasers and X-ray gas lasers. In parallel to the development of sources, optical technologies for photon handling and conditioning of such coherent and intense X-ray beams advanced. New problems were faced for the realization of optical components of beamlines demanding to manage coherent X-ray photons, e.g. the preservation of coherence and time structure of ultra short pulses.

Design of an imaging microscope for soft X-ray applications

Science.gov (United States)

Hoover, Richard B.; Shealy, David L.; Gabardi, David R.; Walker, Arthur B. C., Jr.; Lindblom, Joakim F.

1988-01-01

An imaging soft X-ray microscope with a spatial resolution of 0.1 micron and normal incidence multilayer optics is discussed. The microscope has a Schwarzschild configuration, which consists of two concentric spherical mirrors with radii of curvature which minimize third-order spherical aberration, coma, and astigmatism. The performance of the Stanford/MSFC Cassegrain X-ray telescope and its relevance to the present microscope are addressed. A ray tracing analysis of the optical system indicates that diffraction-limited performance can be expected for an object height of 0.2 mm.

Characterization of diffraction gratings by use of a tabletop soft-x-ray laser

International Nuclear Information System (INIS)

Seminario, Max; Rocca, Jorge J.; Depine, Ricardo A.; Bach, Benny; Bach, Bernie

2001-01-01

We have demonstrated the use of a high-repetition-rate 46.9-mm tabletop laser to characterize diffraction gratings designed for grazing-incidence operation in the soft-x-ray spectral region. The efficiencies for various diffraction orders were measured as a function of angle of incidence and compared with the results of model simulations. This measurement technique provides benchmarks with which to improve electromagnetic codes used in the design of soft-x-ray diffraction gratings. The results illustrate the potential of compact tabletop soft-x-ray lasers for use as a new tool for characterization of short-wavelength optics at the manufacturer's site

Applications of soft x-ray lasers

International Nuclear Information System (INIS)

Skinner, C.H.

1993-01-01

The high brightness and short pulse duration of soft x-ray lasers provide unique advantages for novel applications. Imaging of biological specimens using x-ray lasers has been demonstrated by several groups. Other applications to fields such as chemistry, material science, plasma diagnostics, and lithography are beginning to emerge. We review the current status of soft x-ray lasers from the perspective of applications, and present an overview of the applications currently being developed

Soft X-Ray Second Harmonic Generation as an Interfacial Probe

Energy Technology Data Exchange (ETDEWEB)

Lam, R. K.; Raj, S. L.; Pascal, T. A.; Pemmaraju, C. D.; Foglia, L.; Simoncig, A.; Fabris, N.; Miotti, P.; Hull, C. J.; Rizzuto, A. M.; Smith, J. W.; Mincigrucci, R.; Masciovecchio, C.; Gessini, A.; Allaria, E.; De Ninno, G.; Diviacco, B.; Roussel, E.; Spampinati, S.; Penco, G.; Di Mitri, S.; Trovò, M.; Danailov, M.; Christensen, S. T.; Sokaras, D.; Weng, T. -C.; Coreno, M.; Poletto, L.; Drisdell, W. S.; Prendergast, D.; Giannessi, L.; Principi, E.; Nordlund, D.; Saykally, R. J.; Schwartz, C. P.

2018-01-01

Nonlinear optical processes at soft x-ray wavelengths have remained largely unexplored due to the lack of available light sources with the requisite intensity and coherence. Here we report the observation of soft x-ray second harmonic generation near the carbon K edge (~284 eV) in graphite thin films generated by high intensity, coherent soft x-ray pulses at the FERMI free electron laser. Our experimental results and accompanying first-principles theoretical analysis highlight the effect of resonant enhancement above the carbon K edge and show the technique to be interfacially sensitive in a centrosymmetric sample with second harmonic intensity arising primarily from the first atomic layer at the open surface. This technique and the associated theoretical framework demonstrate the ability to selectively probe interfaces, including those that are buried, with elemental specificity, providing a new tool for a range of scientific problems.

Comparison of nonflare solar soft x ray flux with 10.7-cm radio flux

International Nuclear Information System (INIS)

Donnelly, R.F.

1982-01-01

The similarities and differences of the nonflare solar 1- to 8-A X ray flux and the daily 10.7-cm Ottawa solar radio flux are examined. The radio flux is shown to be much less sensitive than the soft X ray flux on the average to the coronal emission of active regions located near or beyond the solar chromospheric limb relative to regions near the center of the solar disk. This is caused by the solar soft X ray emission's being optically thin while much of the 10.7-cm active region emission is from optical depths of tauapprox.1. The radio flux includes a large quiet sun flux which is emitted mostly from the tenuous chromosphere-corona transition region (Tapprox.10 4 --10 6 0 K) and partly from the cooler portions of the quiet corona Tapprox.1.5 x 10 6 0 K. Conversely, the solar soft X ray flux has a very small quiet sun component

Moving the Frontier of Quantum Control into the Soft X-Ray Spectrum

Directory of Open Access Journals (Sweden)

A. Aquila

2011-01-01

Full Text Available The femtosecond nature of X-ray free electron laser (FEL pulses opens up exciting research possibilities in time-resolved studies including femtosecond photoemission and diffraction. The recent developments of seeding X-ray FELs extend their capabilities by creating stable, temporally coherent, and repeatable pulses. This in turn opens the possibility of spectral engineering soft X-ray pulses to use as a probe for the control of quantum dynamics. We propose a method for extending coherent control pulse-shaping techniques to the soft X-ray spectral range by using a reflective geometry 4f pulse shaper. This method is based on recent developments in asymmetrically cut multilayer optic technology and piezoelectric substrates.

The Soft X-ray Telescope for Solar-A - Design evolution and lessons learned

Science.gov (United States)

Bruner, Marilyn E.

1992-01-01

The Japanese Solar-A satellite mission's Soft X-ray Telescope uses grazing-incidence optics, a CCD detector, and a pair of filter wheels for wavelength selection. A coaxially-mounted visible-light lens furnished sunspot and magnetic plage images, together with aspect information which aids in aligning the soft X-ray images with those from the satellite's Hard X-ray Telescope. Instrument electronics are microprocessor-based, and imbedded in a tightly integrated distributed system. Control software is divided between the instrument microprocessor and the spacecraft control computer.

Synchrotron radiation calibration for soft X-ray detector

International Nuclear Information System (INIS)

Ning, Jiamin; Guo, Cun; Xu, Rongkun; Jiang, Shilun; Xu, Zeping; Chen, Jinchuan; Xia, Guangxin; Xue, Feibiao; Qin, Yi

2009-04-01

The calibration experiments were carried out to X-ray film, scintillator and transmission grating by employing the soft X-ray station at 3W1B beam-line in Beijing synchrotron Radiation Facility. The experiments presented the black intensity curve and energy response curve of soft X-ray film. And the experimental results can be used in diagnosis of X-ray radiation characterization of Z-pinch, such as in the measurement of soft X-ray Power Meter, grating spectrometer, pinhole camera and one-dimension imaging system which can ensure precision of Z-pinch results. (authors)

The influence of glass fibers on elongational viscosity studied by means of optical coherence tomography and X-ray computed tomography

International Nuclear Information System (INIS)

Aigner, M.; Köpplmayr, T.; Lang, C.; Burzic, I.; Miethlinger, J.; Salaberger, D.; Buchsbaum, A.; Leitner, M.; Heise, B.; Schausberger, S. E.; Stifter, D.

2014-01-01

We report on the flow characteristics of glass-fiber-reinforced polymers in elongational rheometry. Unlike polymers with geometrically isotropic fillers, glass-fiber-reinforced polymers exhibit flow behavior and rheology that depend heavily on the orientation, the length distribution and the content of the fibers. One of the primary objectives of this study was to determine the effect of fiber orientation, concentration and distribution on the entrance pressure drop by means of optical coherence tomography (OCT), full-field optical coherence microscopy (FF-OCM), and X-ray computed tomography (X-CT). Both pressure drop and melt flow were analyzed using a special elongation die (Thermo Scientific X-Die [3]) for inline measurements. Samples with a variety of fiber volume fractions, fiber lengths and processing temperatures were measured

The influence of glass fibers on elongational viscosity studied by means of optical coherence tomography and X-ray computed tomography

Science.gov (United States)

Aigner, M.; Salaberger, D.; Buchsbaum, A.; Heise, B.; Schausberger, S. E.; Köpplmayr, T.; Lang, C.; Leitner, M.; Stifter, D.; Burzic, I.; Miethlinger, J.

2014-05-01

We report on the flow characteristics of glass-fiber-reinforced polymers in elongational rheometry. Unlike polymers with geometrically isotropic fillers, glass-fiber-reinforced polymers exhibit flow behavior and rheology that depend heavily on the orientation, the length distribution and the content of the fibers. One of the primary objectives of this study was to determine the effect of fiber orientation, concentration and distribution on the entrance pressure drop by means of optical coherence tomography (OCT), full-field optical coherence microscopy (FF-OCM), and X-ray computed tomography (X-CT). Both pressure drop and melt flow were analyzed using a special elongation die (Thermo Scientific X-Die [3]) for inline measurements. Samples with a variety of fiber volume fractions, fiber lengths and processing temperatures were measured.

X-ray acquisition and electronic digital readout by charge coupled devices

International Nuclear Information System (INIS)

Cavailler, C.; Launspach, J.; Mens, A.; Sauneuf, R.

1985-09-01

X-ray imaging adapted to laser-matter interaction experiments consists in recording plasma images from its X-ray emission; these phenomena have between 100 ps and some nanoseconds duration. Investigation of the laser-driven plasma may require the formation and the detection of two-dimensional images formed by X-ray microscopes or spectrometers in the soft X-ray range (from about 50 eV to some keV). To reach that purpose, we have developed and tested two opto-electronic chains. The first one is built around a small image converter tube with a soft X-ray photocathode and P20 phosphor screen deposited on a fiber optic plate; the electronic image appearing on the screen is read by a C.C.D. working in the visible spectral range. The second one, designed to work below 100eV is realized with a very thin phosphor screen deposited on the fiber optic input of a visible microchannel image intensifier; the output image is then read by a C.C.D. in the same manner than previously

Technology development of the soft X-ray tomography system in Wendelstein 7-X stellarator

Energy Technology Data Exchange (ETDEWEB)

Schülke, M., E-mail: mathias.schuelke@ipp.mpg.de [Max Planck Institute for Plasma Physics, EURATOM Association, Wendelsteinstr. 1, 17491 Greifswald (Germany); Cardella, A.; Hathiramani, D.; Mettchen, S.; Thomsen, H.; Weißflog, S.; Zacharias, D. [Max Planck Institute for Plasma Physics, EURATOM Association, Wendelsteinstr. 1, 17491 Greifswald (Germany)

2013-10-15

Highlights: ► Engineering and design of soft X-ray Multi Camera Tomography System. ► Requirements of in-vessel diagnostics in Wendelstein 7-X. ► Development of internal cooling system including FEM-Analysis. ► Development of lateral shield system with testing for microwave stray radiation compatibility. ► Development of multipin feedthrough including welding qualification and leak tests. -- Abstract: The engineering and design of the soft X-ray Multi Camera Tomography System (XMCTS) in Wendelstein 7-X stellarator (W7-X) must fulfill several additional requirements compared to short pulse machines. The XMCTS has to withstand irradiation and electron cyclotron microwave loads in addition to being ultra high vacuum compatible, having low magnetic permeability and using low neutron activation materials (e.g. Co ≤ 2000 ppm). A further difficulty is the limited space inside the plasma vessel, which requires special engineering solutions. After detailed design development, supported by finite element analyses, prototypes have been manufactured and tested. At the end all test results have successfully proven that the components fulfill the requirements and that reliable and stable measurements will be possible with the XMCTS diagnostics during W7-X operation. The paper describes the design and the technological development, in particular on the electric multipin feedthrough (UHV barrier between in vessel detectors and the preamplifiers), the active cooling of the electronic components (reducing dark current/noise increase), the pneumatic shutter (protection of the detectors from sputtering and during baking) and the fiber optics illumination system (calibration of the detectors)

Spectral tailoring of nanoscale EUV and soft x-ray multilayer optics

Science.gov (United States)

Huang, Qiushi; Medvedev, Viacheslav; van de Kruijs, Robbert; Yakshin, Andrey; Louis, Eric; Bijkerk, Fred

2017-03-01

Extreme ultraviolet and soft X-ray (XUV) multilayer optics have experienced significant development over the past few years, particularly on controlling the spectral characteristics of light for advanced applications like EUV photolithography, space observation, and accelerator- or lab-based XUV experiments. Both planar and three dimensional multilayer structures have been developed to tailor the spectral response in a wide wavelength range. For the planar multilayer optics, different layered schemes are explored. Stacks of periodic multilayers and capping layers are demonstrated to achieve multi-channel reflection or suppression of the reflective properties. Aperiodic multilayer structures enable broadband reflection both in angles and wavelengths, with the possibility of polarization control. The broad wavelength band multilayer is also used to shape attosecond pulses for the study of ultrafast phenomena. Narrowband multilayer monochromators are delivered to bridge the resolution gap between crystals and regular multilayers. High spectral purity multilayers with innovated anti-reflection structures are shown to select spectrally clean XUV radiation from broadband X-ray sources, especially the plasma sources for EUV lithography. Significant progress is also made in the three dimensional multilayer optics, i.e., combining micro- and nanostructures with multilayers, in order to provide new freedom to tune the spectral response. Several kinds of multilayer gratings, including multilayer coated gratings, sliced multilayer gratings, and lamellar multilayer gratings are being pursued for high resolution and high efficiency XUV spectrometers/monochromators, with their advantages and disadvantages, respectively. Multilayer diffraction optics are also developed for spectral purity enhancement. New structures like gratings, zone plates, and pyramids that obtain full suppression of the unwanted radiation and high XUV reflectance are reviewed. Based on the present achievement

Investigation of HF-plasma-treated soft x-ray optical elements

Science.gov (United States)

Eggenstein, F.; Krivenkov, M.; Rudolph, I.; Sertsu, M. G.; Sokolov, A.; Varykhalov, A.; Wolf, J.; Zeschke, T.; Schäfers, F.

2017-09-01

The contamination of optical elements (mirrors and gratings) with carbon still is an issue when using soft x-ray synchrotron radiation. With an in-house developed HF-plasma treatment we are able to decontaminate our optics in-situ from carbon very efficiently. The cleaning device, a simple Al-antenna, is mounted in situ inside the mirror- and grating vacuum chambers. A systematic study of the HF-plasma cleaning efficiency was performed acquired with in-situ and exsitu methods for monitoring: An atomic force microscope (AFM) and a scanning tunneling microscope (STM) were used before and after the cleaning process to determine the surface morphology and roughness. Reflectivity angular scans using the reflectometer at the BESSY-II Metrology Station [1-3] allowed to estimate the thickness of the remaining Clayer after different cleaning steps and thereby helped us to determine the etching rate. Reflection spectra measurements in the range of 200 eV - 900 eV show the complete removal of Carbon from the optics without contaminating it with any other elements due to the plasma treatment. The data show that the plasma process improves the reflectivity and reduces the roughness of the surface. In addition to that, the region of the optical surface where the carbon has been removed becomes passivated.

Diversity of soft X-ray spectra in quasars

International Nuclear Information System (INIS)

Elvis, M.; Wilkes, B.J.; Tananbaum, H.

1985-01-01

Soft X-ray spectra for three quasars obtained with the Einstein Imaging Proportional Counter covering the 0.1-4.0 keV band are reported. Power-law fits to these spectra have best-fit energy indices of 1.2 +0.6 or -0.2, for the quasar NAB 0205 + 024, 0.6 +0.3 or -0.2 for the quasar B2 1028 + 313, and 2.2 + or -0.4 for the quasar PG 1211 + 143. None of the quasars shows any evidence for a column density of cold matter in excess of the galactic values. The derived spectra demonstrate that there is no single universal power law slope for quasar X-ray spectra. The implications of these results for the X-ray background, X-ray continuum emission mechanisms, and the production of the optical/UV emission lines are briefly discussed. 46 references

High spatial resolution soft-x-ray microscopy

Energy Technology Data Exchange (ETDEWEB)

Meyer-Ilse, W.; Medecki, H.; Brown, J.T. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States)] [and others

1997-04-01

A new soft x-ray microscope (XM-1) with high spatial resolution has been constructed by the Center for X-ray Optics. It uses bending magnet radiation from beamline 6.1 at the Advanced Light Source, and is used in a variety of projects and applications in the life and physical sciences. Most of these projects are ongoing. The instrument uses zone plate lenses and achieves a resolution of 43 nm, measured over 10% to 90% intensity with a knife edge test sample. X-ray microscopy permits the imaging of relatively thick samples, up to 10 {mu}m thick, in water. XM-1 has an easy to use interface, that utilizes visible light microscopy to precisely position and focus the specimen. The authors describe applications of this device in the biological sciences, as well as in studying industrial applications including structured polymer samples.

X-ray Optics for BES Light Source Facilities

Energy Technology Data Exchange (ETDEWEB)

Mills, Dennis [Argonne National Lab. (ANL), Argonne, IL (United States); Padmore, Howard [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Lessner, Eliane [Dept. of Energy (DOE), Washington DC (United States). Office of Science

2013-03-27

Each new generation of synchrotron radiation sources has delivered an increase in average brightness 2 to 3 orders of magnitude over the previous generation. The next evolution toward diffraction-limited storage rings will deliver another 3 orders of magnitude increase. For ultrafast experiments, free electron lasers (FELs) deliver 10 orders of magnitude higher peak brightness than storage rings. Our ability to utilize these ultrabright sources, however, is limited by our ability to focus, monochromate, and manipulate these beams with X-ray optics. X-ray optics technology unfortunately lags behind source technology and limits our ability to maximally utilize even today’s X-ray sources. With ever more powerful X-ray sources on the horizon, a new generation of X-ray optics must be developed that will allow us to fully utilize these beams of unprecedented brightness. The increasing brightness of X-ray sources will enable a new generation of measurements that could have revolutionary impact across a broad area of science, if optical systems necessary for transporting and analyzing X-rays can be perfected. The high coherent flux will facilitate new science utilizing techniques in imaging, dynamics, and ultrahigh-resolution spectroscopy. For example, zone-plate-based hard X-ray microscopes are presently used to look deeply into materials, but today’s resolution and contrast are restricted by limitations of the current lithography used to manufacture nanodiffractive optics. The large penetration length, combined in principle with very high spatial resolution, is an ideal probe of hierarchically ordered mesoscale materials, if zone-plate focusing systems can be improved. Resonant inelastic X-ray scattering (RIXS) probes a wide range of excitations in materials, from charge-transfer processes to the very soft excitations that cause the collective phenomena in correlated electronic systems. However, although RIXS can probe high-energy excitations, the most exciting and

X-ray Optics for BES Light Source Facilities

International Nuclear Information System (INIS)

Mills, Dennis; Padmore, Howard; Lessner, Eliane

2013-01-01

Each new generation of synchrotron radiation sources has delivered an increase in average brightness 2 to 3 orders of magnitude over the previous generation. The next evolution toward diffraction-limited storage rings will deliver another 3 orders of magnitude increase. For ultrafast experiments, free electron lasers (FELs) deliver 10 orders of magnitude higher peak brightness than storage rings. Our ability to utilize these ultrabright sources, however, is limited by our ability to focus, monochromate, and manipulate these beams with X-ray optics. X-ray optics technology unfortunately lags behind source technology and limits our ability to maximally utilize even today's X-ray sources. With ever more powerful X-ray sources on the horizon, a new generation of X-ray optics must be developed that will allow us to fully utilize these beams of unprecedented brightness. The increasing brightness of X-ray sources will enable a new generation of measurements that could have revolutionary impact across a broad area of science, if optical systems necessary for transporting and analyzing X-rays can be perfected. The high coherent flux will facilitate new science utilizing techniques in imaging, dynamics, and ultrahigh-resolution spectroscopy. For example, zone-plate-based hard X-ray microscopes are presently used to look deeply into materials, but today's resolution and contrast are restricted by limitations of the current lithography used to manufacture nanodiffractive optics. The large penetration length, combined in principle with very high spatial resolution, is an ideal probe of hierarchically ordered mesoscale materials, if zone-plate focusing systems can be improved. Resonant inelastic X-ray scattering (RIXS) probes a wide range of excitations in materials, from charge-transfer processes to the very soft excitations that cause the collective phenomena in correlated electronic systems. However, although RIXS can probe high-energy excitations, the most exciting

Soft x-ray transmission measurements on thin films used for XMM CCD-filters

Science.gov (United States)

Stephan, K.-H.; Reppin, C.; Maier, H. J.; Frischke, D.; Fuchs, D.; Müller, P.

1997-02-01

We have been developing optical filters for ESA's X-ray astronomy project XMM (X-ray Multi Mirror Mission). Specific CCDs will be used as detectors in the focal plane on board the observatory (1). Since these detectors are sensitive from the X-ray to the near infrared spectral range, X-ray observations require optical filters, which combine a high transparency for photon energies in the soft X-ray region and a high opacity for ultraviolet and visible radiation as well. With respect to the mission goal in orbit three types of flight model filters are designed having different spectral transmittance functions. We report on one of these types, a so-called "thick" filter, which has been realized within the EQM (Electrical Qualification Model)-phase of the project. The filter features a cut-off in the extreme ultraviolet spectral range and suppresses radiation below ˜10 eV photon energy by more than 8 orders of magnitude. It has an effective aperture of 73 mm without any support structure. A 0.35 μm thick polypropylene carrier foil is coated with metallic films of Al and Sn. We describe transmission measurements in the soft X-ray photon energy range to determine the thickness of the individual layers and present the optical performance data of the filter.

Development and characterization of femtosecond laser driven soft x-ray lasers

International Nuclear Information System (INIS)

Bettaibi, I.

2005-06-01

Coherent soft x-ray sources have an important potential for scientific, medical and industrial applications. The development of high intensity laser systems allowed the realization of new coherent and fast soft x-ray sources like high order harmonic generation and soft x-ray lasers. These sources are compact, cheaper than traditional sources such as synchrotrons, and are thus interesting. This thesis presents the study of a new soft x-ray laser pumped by a femto-second laser beam working at 10 Hz. The circularly polarized ultra intense laser is longitudinally focused in a cell filled with xenon or krypton, to obtain the amplification of two lasing lines at 41.8 nm and 32.8 nm in Pd-like xenon and Ni-like krypton respectively. We carry out an experimental and numerical study of the source to understand the importance of different parameters such as the laser intensity and polarization, the gas pressure and the cell length. We have also spatially and temporally characterized the soft x-ray laser beam. To compensate the refraction of the driving laser we have investigated guiding techniques consisting in creating a plasma channel by electric discharge or using the multiple reflections of the driving laser on the internal walls of the dielectric tubes of sapphire or glass. A spectacular improvement of the source performances has been observed in both cases. Finally, we present a preliminary study on a different x-ray scheme: the inner shell photo pumping of neutral atoms. We have developed an optical system, which should create the appropriate conditions for the realisation of short wavelength x-ray amplifier. (author)

Soft X-ray contact microscopy of nematode Caenorhabditis elegans

Czech Academy of Sciences Publication Activity Database

Poletti, G.; Orsini, F.; Batani, D.; Bernadinello, A.; Desai, T.; Ullschmied, Jiří; Skála, Jiří; Králiková, Božena; Krouský, Eduard; Juha, Libor; Pfeifer, Miroslav; Kadlec, Christelle; Mocek, Tomáš; Präg R., Ansgar; Renner, Oldřich; Cotelli, F.; Lamia, C. L.; Zullini, A.

2004-01-01

Roč. 30, č. 2 (2004), s. 235-241 ISSN 1434-6060 R&D Projects: GA MŠk LN00A100 Institutional research plan: CEZ:AV0Z2043910 Keywords : soft X-ray Subject RIV: BH - Optics, Masers, Lasers Impact factor: 1.692, year: 2004

Developments of scintillator-based soft x-ray diagnostic in LHD with CsI:Tl and P47 scintillators

Energy Technology Data Exchange (ETDEWEB)

Bando, T., E-mail: bando.takahiro@nifs.ac.jp [SOKENDAI (The Graduate University for Advanced Studies), 322-6 Oroshi-cho, Toki 509-5292 (Japan); Ohdachi, S.; Suzuki, Y. [SOKENDAI (The Graduate University for Advanced Studies), 322-6 Oroshi-cho, Toki 509-5292 (Japan); National Institute for Fusion Science, 322-6 Oroshi-cho, Toki 509-5292 (Japan)

2016-11-15

Multi-channel soft x-ray (SX) diagnostic has been used in the large helical device (LHD) to research magnetohydrodynamic equilibria and activities. However, in the coming deuterium plasma experiments of LHD, it will be difficult to use semiconductor systems near LHD. Therefore, a new type of SX diagnostic, a scintillator-based type diagnostic, has been investigated in order to avoid damage from the radiation. A fiber optic plate coated by P47 scintillator will be used to detect SX emission. Scintillation light will be transferred by pure silica core optical fibers and detected by photomultiplier tubes. A vertically elongated section of LHD will be covered by a 13 ch. array. Effects from the Deuterium Deuterium neutrons can be negligible when the scintillator is covered by a Pb plate 4 cm in thickness to avoid gamma-rays.

Design and fabrication of soft x-ray mirrors

Energy Technology Data Exchange (ETDEWEB)

Kawata, Masaru; Sasai, Hiroyuki; Sano, Kazuo [Shimadzu Corp., Production Engineering Laboratory, Kyoto (Japan)

2000-03-01

Soft x-ray photoelectron spectroscopic technology is important for measuring the chemical status of material surface in the LSI manufacturing process. We report on non-spherical mirrors focusing laser-induced plasma soft x-ray to fine sample surface. We designed toric and ellipsoidal mirror as soft x-ray condensing means, simulated focusing image, manufactured mirror surface on fused quartz substrate, and measured form accuracy. (author)

Experimental studies on pulse soft X-ray generator

International Nuclear Information System (INIS)

Li Chengrong; Yang Qinchi; Luo Chengmu; Han Min

1990-01-01

Emission sources of soft x rays (2 keV < hv < 6 keV) from hot plasmas have been studied in a small gas-puff Z-pinch. The emission sources are a group of uncontinuous hot spots. The output of soft x rays from the hot spots have been measured and the effect of the initial gas density on the yield of soft x rays has been investigated

Short-wavelength soft-x-ray laser pumped in double-pulse single-beam non-normal incidence

International Nuclear Information System (INIS)

Zimmer, D.; Ros, D.; Guilbaud, O.; Habib, J.; Kazamias, S.; Zielbauer, B.; Bagnoud, V.; Ecker, B.; Aurand, B.; Kuehl, T.; Hochhaus, D. C.; Neumayer, P.

2010-01-01

We demonstrated a 7.36 nm Ni-like samarium soft-x-ray laser, pumped by 36 J of a neodymium:glass chirped-pulse amplification laser. Double-pulse single-beam non-normal-incidence pumping was applied for efficient soft-x-ray laser generation. In this case, the applied technique included a single-optic focusing geometry for large beam diameters, a single-pass grating compressor, traveling-wave tuning capability, and an optimized high-energy laser double pulse. This scheme has the potential for even shorter-wavelength soft-x-ray laser pumping.

Soft x-ray tomography on TFTR

International Nuclear Information System (INIS)

Kuo-Petravic, G.

1988-12-01

The tomographic method used for deriving soft x-ray local emissivities on TFTR, using one horizontal array of 60 soft x-ray detectors, is described. This method, which is based on inversion of Fourier components and subsequent reconstruction, has been applied to the study of a sawtooth crash. A flattening in the soft x-ray profile, which we interpret as an m = 1 island, is clearly visible during the precursor phase and its location and width correlate well with those from electron temperature profiles reconstructed from electron cyclotron emission measurement. The limitations of the Fourier method, due notably to the aperiodic nature of the signals in the fast crash phase and the difficulty of obtaining accurately the higher Fourier harmonics, are discussed. 9 refs., 13 figs

Soft x-ray spectroscopy undulator beamline at the Advanced Photon Source

Energy Technology Data Exchange (ETDEWEB)

Randall, K.J.; Xu, Z.; Moore, J.F.; Gluskin, E.

1997-09-01

Construction of the high-resolution soft x ray spectroscopy undulator beamline, 2ID-C, at the Advanced Photon Source (APS) has been completed. The beamline, one of two soft x ray beamlines at the APS, will cover the photon energy range from 500 to 3,000 eV, with a maximum resolving power between 7,000 and 14,000. The optical design is based on a spherical grating monochromator (SGM) giving both high resolution and high flux throughput. Photon flux is calculated to be approximately 10{sup 12}--10{sup 13} photons per second with a beam size of approximately 1 x 1 mm{sup 2} at the sample.

Optical properties of boron carbide near the boron K edge evaluated by soft-x-ray reflectometry from a Ru/B4C multilayer

Energy Technology Data Exchange (ETDEWEB)

Ksenzov, Dmitriy; Panzner, Tobias; Schlemper, Christoph; Morawe, Christian; Pietsch, Ullrich

2009-12-10

Soft-x-ray Bragg reflection from two Ru/B4C multilayers with 10 and 63 periods was used for independent determination of both real and imaginary parts of the refractive index n = 1 -{delta} + i{beta} close to the boron K edge ({approx}188 eV). Prior to soft x-ray measurements, the structural parameters of the multilayers were determined by x-ray reflectometry using hard x rays. For the 63-period sample, the optical properties based on the predictions made for elemental boron major deviations were found close to the K edge of boron for the 10-period sample explained by chemical bonding of boron to B4C and various boron oxides.

The soft X-ray telescope for the SOLAR-A mission

Science.gov (United States)

Tsuneta, S.; Acton, L.; Bruner, M.; Lemen, J.; Brown, W.; Caravalho, R.; Catura, R.; Freeland, S.; Jurcevich, B.; Owens, J.

1991-01-01

The Soft X-ray Telescope (SXT) of the SOLAR-A mission is designed to produce X-ray movies of flares with excellent angular and time resolution as well as full-disk X-ray images for general studies. A selection of thin metal filters provide a measure of temperature discrimination and aid in obtaining the wide dynamic range required for solar observing. The co-aligned SXT aspect telescope will yield optical images for aspect reference, white-light flare and sunspot studies, and, possibly, helioseismology. This paper describes the capabilities and characteristics of the SXT for scientific observing.

Development of X-ray excitable luminescent probes for scanning X-ray microscopy

International Nuclear Information System (INIS)

Moronne, M.M.

1999-01-01

Transmission soft X-ray microscopy is now capable of achieving resolutions that are typically 5 times better than the best-visible light microscopes. With expected improvements in zone plate optics, an additional factor of two may be realized within the next few years. Despite the high resolution now available with X-ray microscopes and the high X-ray contrast provided by biological molecules in the soft X-ray region (λ=2-5 nm), molecular probes for localizing specific biological targets have been lacking. To circumvent this problem, X-ray excitable molecular probes are needed that can target unique biological features. In this paper we report our initial results on the development of lanthanide-based fluorescent probes for biological labeling. Using scanning luminescence X-ray microscopy (SLXM, Jacobsen et al., J. Microscopy 172 (1993) 121-129), we show that lanthanide organo-polychelate complexes are sufficiently bright and radiation resistant to be the basis of a new class of X-ray excitable molecular probes capable of providing at least a fivefold improvement in resolution over visible light microscopy. Lanthanide probes, able to bind 80-100 metal ions per molecule, were found to give strong luminescent signals with X-ray doses exceeding 10 8 Gy, and were used to label actin stress fibers and in vitro preparations of polymerized tubulin. (Copyright (c) 1999 Elsevier Science B.V., Amsterdam. All rights reserved.)

Human soft tissue analysis using x-ray or gamma-ray techniques

International Nuclear Information System (INIS)

Theodorakou, C; Farquharson, M J

2008-01-01

This topical review is intended to describe the x-ray techniques used for human soft tissue analysis. X-ray techniques have been applied to human soft tissue characterization and interesting results have been presented over the last few decades. The motivation behind such studies is to provide improved patient outcome by using the data obtained to better understand a disease process and improve diagnosis. An overview of theoretical background as well as a complete set of references is presented. For each study, a brief summary of the methodology and results is given. The x-ray techniques include x-ray diffraction, x-ray fluorescence, Compton scattering, Compton to coherent scattering ratio and attenuation measurements. The soft tissues that have been classified using x-rays or gamma rays include brain, breast, colon, fat, kidney, liver, lung, muscle, prostate, skin, thyroid and uterus. (topical review)

SWIFT X-RAY OBSERVATIONS OF CLASSICAL NOVAE. II. THE SUPER SOFT SOURCE SAMPLE

Energy Technology Data Exchange (ETDEWEB)

Schwarz, Greg J. [American Astronomical Society, 2000 Florida Avenue, NW, Suite 400, Washington, DC 20009-1231 (United States); Ness, Jan-Uwe [XMM-Newton Science Operations Centre, ESAC, Apartado 78, 28691 Villanueva de la Canada, Madrid (Spain); Osborne, J. P.; Page, K. L.; Evans, P. A.; Beardmore, A. P. [Department of Physics and Astronomy, University of Leicester, Leicester LE1 7RH (United Kingdom); Walter, Frederick M. [Department of Physics and Astronomy, Stony Brook University, Stony Brook, NY 11794-3800 (United States); Andrew Helton, L. [SOFIA Science Center, USRA, NASA Ames Research Center, M.S. N211-3, Moffett Field, CA 94035 (United States); Woodward, Charles E. [Minnesota Institute of Astrophysics, 116 Church Street S.E., University of Minnesota, Minneapolis, MN 55455 (United States); Bode, Mike [Astrophysics Research Institute, Liverpool John Moores University, Birkenhead CH41 1LD (United Kingdom); Starrfield, Sumner [School of Earth and Space Exploration, Arizona State University, P.O. Box 871404, Tempe, AZ 85287-1404 (United States); Drake, Jeremy J., E-mail: Greg.Schwarz@aas.org [Smithsonian Astrophysical Observatory, 60 Garden Street, MS 3, Cambridge, MA 02138 (United States)

2011-12-01

The Swift gamma-ray burst satellite is an excellent facility for studying novae. Its rapid response time and sensitive X-ray detector provides an unparalleled opportunity to investigate the previously poorly sampled evolution of novae in the X-ray regime. This paper presents Swift observations of 52 Galactic/Magellanic Cloud novae. We included the X-Ray Telescope (0.3-10 keV) instrument count rates and the UltraViolet and Optical Telescope (1700-8000 A) filter photometry. Also included in the analysis are the publicly available pointed observations of 10 additional novae the X-ray archives. This is the largest X-ray sample of Galactic/Magellanic Cloud novae yet assembled and consists of 26 novae with Super Soft X-ray emission, 19 from Swift observations. The data set shows that the faster novae have an early hard X-ray phase that is usually missing in slower novae. The Super Soft X-ray phase occurs earlier and does not last as long in fast novae compared to slower novae. All the Swift novae with sufficient observations show that novae are highly variable with rapid variability and different periodicities. In the majority of cases, nuclear burning ceases less than three years after the outburst begins. Previous relationships, such as the nuclear burning duration versus t{sub 2} or the expansion velocity of the eject and nuclear burning duration versus the orbital period, are shown to be poorly correlated with the full sample indicating that additional factors beyond the white dwarf mass and binary separation play important roles in the evolution of a nova outburst. Finally, we confirm two optical phenomena that are correlated with strong, soft X-ray emission which can be used to further increase the efficiency of X-ray campaigns.

SWIFT X-RAY OBSERVATIONS OF CLASSICAL NOVAE. II. THE SUPER SOFT SOURCE SAMPLE

International Nuclear Information System (INIS)

Schwarz, Greg J.; Ness, Jan-Uwe; Osborne, J. P.; Page, K. L.; Evans, P. A.; Beardmore, A. P.; Walter, Frederick M.; Andrew Helton, L.; Woodward, Charles E.; Bode, Mike; Starrfield, Sumner; Drake, Jeremy J.

2011-01-01

The Swift gamma-ray burst satellite is an excellent facility for studying novae. Its rapid response time and sensitive X-ray detector provides an unparalleled opportunity to investigate the previously poorly sampled evolution of novae in the X-ray regime. This paper presents Swift observations of 52 Galactic/Magellanic Cloud novae. We included the X-Ray Telescope (0.3-10 keV) instrument count rates and the UltraViolet and Optical Telescope (1700-8000 Å) filter photometry. Also included in the analysis are the publicly available pointed observations of 10 additional novae the X-ray archives. This is the largest X-ray sample of Galactic/Magellanic Cloud novae yet assembled and consists of 26 novae with Super Soft X-ray emission, 19 from Swift observations. The data set shows that the faster novae have an early hard X-ray phase that is usually missing in slower novae. The Super Soft X-ray phase occurs earlier and does not last as long in fast novae compared to slower novae. All the Swift novae with sufficient observations show that novae are highly variable with rapid variability and different periodicities. In the majority of cases, nuclear burning ceases less than three years after the outburst begins. Previous relationships, such as the nuclear burning duration versus t 2 or the expansion velocity of the eject and nuclear burning duration versus the orbital period, are shown to be poorly correlated with the full sample indicating that additional factors beyond the white dwarf mass and binary separation play important roles in the evolution of a nova outburst. Finally, we confirm two optical phenomena that are correlated with strong, soft X-ray emission which can be used to further increase the efficiency of X-ray campaigns.

Advances in thin film diffraction instrumentation by X-ray optics

International Nuclear Information System (INIS)

Haase, A.

1996-01-01

The structural characterisation of thin films requires a parallel X-ray beam of high intensity. Parallel beam geometry is commonly used in high resolution and single crystal experiments, but also in the field of X-ray diffraction for polycrystalline material (e.g. in phase, texture and stress analysis). For grazing incidence diffraction (GID), the use of small slits on the primary side and of long soller slits with a flat monochromator on the secondary side is standard. New optical elements have been introduced with polychromatic or monochromatic radiation. By means of different applications the results are compared with those of classical beam optics. X-ray fiber optics utilize total external reflection of X-rays on smooth surfaces. Effects of monochromatization are presented. In many fields of application, fiber optics may replace conventional collimators. The use of primary and secondary channel cut crystals can also produce a high parallel monochromatic X-ray beam. A parabolically bent graded multilayer produces a monochromatic parallel beam of high intensity. Compared with classical Bragg-Brentano (focussing) geometry, excellent results have been obtained, especially for samples with an irregular shape. In combination with a channel cut monochromator there is a substantial gain in intensity leading to an increase of the dynamic intensity range of rocking curves

Advances in thin film diffraction instrumentation by X-ray optics

Energy Technology Data Exchange (ETDEWEB)

Haase, A [Rich. Seifert and Co., Analytical X-ray Systems, Ahrensburg (Germany)

1996-09-01

The structural characterisation of thin films requires a parallel X-ray beam of high intensity. Parallel beam geometry is commonly used in high resolution and single crystal experiments, but also in the field of X-ray diffraction for polycrystalline material (e.g. in phase, texture and stress analysis). For grazing incidence diffraction (GID), the use of small slits on the primary side and of long soller slits with a flat monochromator on the secondary side is standard. New optical elements have been introduced with polychromatic or monochromatic radiation. By means of different applications the results are compared with those of classical beam optics. X-ray fiber optics utilize total external reflection of X-rays on smooth surfaces. Effects of monochromatization are presented. In many fields of application, fiber optics may replace conventional collimators. The use of primary and secondary channel cut crystals can also produce a high parallel monochromatic X-ray beam. A parabolically bent graded multilayer produces a monochromatic parallel beam of high intensity. Compared with classical Bragg-Brentano (focussing) geometry, excellent results have been obtained, especially for samples with an irregular shape. In combination with a channel cut monochromator there is a substantial gain in intensity leading to an increase of the dynamic intensity range of rocking curves.

Laser-produced multi-charged heavy ions as efficient soft x-ray sources

International Nuclear Information System (INIS)

Higashiguchi, Takeshi; Suzuki, Yuhei; Kawasaki, Masato

2016-01-01

We demonstrate EUV and soft x-ray sources in the 2 to 7 nm spectral region related to the beyond EUV (BEUV) question at 6x nm and a water window source based on laser-produced high-Z plasmas. Resonance emission from multiply charged ions merges to produce intense unresolved transition arrays (UTAs), extending below the carbon K edge (4.37 nm). An outline of a microscope design for single-shot live cell imaging is proposed based on a high-Z plasma UTA source, coupled to x-ray optics. We will discuss the progress and Z-scaling of UTA emission spectra to achieve lab-scale table-top, efficient, high-brightness high-Z plasma EUV-soft x-ray sources for in vivo bio-imaging applications. (author)

Novel spectroscopic techniques with using soft x-ray

International Nuclear Information System (INIS)

Gejo, Tatsuo

2010-01-01

Recent progress of experimental techniques related to synchrotron radiation makes possible of detail investigation of molecular dynamics after irradiation of soft X-ray. We introduce several novel spectroscopic techniques with using soft X-ray: Symmetry-resolved zero kinetic energy electron spectroscopy, symmetry-resolved metastable photofragment spectroscopy, soft X-ray emission spectroscopy, time-resolved fluorescence spectroscopy, and time-resolved-fluorescence mass-selected-ion coincidence spectroscopy. We also show new techniques performed by other groups at BL27SU in SPring-8. (author)

Soft x-ray source by laser produced Xe plasma

International Nuclear Information System (INIS)

Amano, Sho; Masuda, Kazuya; Miyamoto, Shuji; Mochizuki, Takayasu

2010-01-01

The laser plasma soft X-ray source in the wavelength rage of 5-17 nm was developed, which consisted of the rotating drum system supplying cryogenic Xe target and the high repetition rate pulse Nd:YAG slab laser. We found the maximum conversion efficiency of 30% and it demonstrated the soft X-ray generation with the high repetition rate pulse of 320 pps and the high average power of 20 W. The soft X-ray cylindrical mirror was developed and successfully focused the soft X-ray with an energy intensity of 1.3 mJ/cm 2 . We also succeeded in the plasma debris mitigation with Ar gas. This will allow a long lifetime of the mirror and a focusing power intensity of 400 mW/cm 2 with 320 pps. The high power soft X-ray is useful for various applications. (author)

X-ray fluorescence imaging with polycapillary X-ray optics

International Nuclear Information System (INIS)

Yonehara, Tasuku; Yamaguchi, Makoto; Tsuji, Kouichi

2010-01-01

X-ray fluorescence spectrometry imaging is a powerful tool to provide information about the chemical composition and elemental distribution of a specimen. X-ray fluorescence spectrometry images were conventionally obtained by using a μ-X-ray fluorescence spectrometry spectrometer, which requires scanning a sample. Faster X-ray fluorescence spectrometry imaging would be achieved by eliminating the process of sample scanning. Thus, we developed an X-ray fluorescence spectrometry imaging instrument without sample scanning by using polycapillary X-ray optics, which had energy filter characteristics caused by the energy dependence of the total reflection phenomenon. In the present paper, we show that two independent straight polycapillary X-ray optics could be used as an energy filter of X-rays for X-ray fluorescence. Only low energy X-rays were detected when the angle between the two optical axes was increased slightly. Energy-selective X-ray fluorescence spectrometry images with projection mode were taken by using an X-ray CCD camera equipped with two polycapillary optics. It was shown that Fe Kα (6.40 keV) and Cu Kα (8.04 keV) could be discriminated for Fe and Cu foils.

Investigations of Caenorhabditis Elegans Using Soft X-ray Contact Microscopy

Czech Academy of Sciences Publication Activity Database

Desai, T.; Batani, D.; Bernardinello, A.; Poletti, G.; Orsini, F.; Ullschmied, Jiří; Skála, Jiří; Králiková, Božena; Krouský, Eduard; Mocek, Karel; Pfeifer, Miroslav; Kadlec, Christelle; Mocek, Tomáš; Präg R., Ansgar; Renner, Oldřich; Juha, Libor; Cotelli, F.; Lamia, C. L.; Zullini, A.

2004-01-01

Roč. 20, č. 3 (2004), s. 121-125 ISSN 1120-1797 R&D Projects: GA MŠk LN00A100 Keywords : C. elegans * soft X-ray contact microscopy * intense laser plasma * gold target Subject RIV: BH - Optics, Masers, Lasers Impact factor: 0.341, year: 2004

Lasers, extreme UV and soft X-ray

Energy Technology Data Exchange (ETDEWEB)

Nilsen, Joseph [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

2015-09-20

Three decades ago, large ICF lasers that occupied entire buildings were used as the energy sources to drive the first X-ray lasers. Today X-ray lasers are tabletop, spatially coherent, high-repetition rate lasers that enable many of the standard optical techniques such as interferometry to be extended to the soft X-ray regime between wavelengths of 10 and 50 nm. Over the last decade X-ray laser performance has been improved by the use of the grazing incidence geometry, diode-pumped solid-state lasers, and seeding techniques. The dominant X-ray laser schemes are the monopole collisional excitation lasers either driven by chirped pulse amplification (CPA) laser systems or capillary discharge. The CPA systems drive lasing in neon-like or nickel-like ions, typically in the 10 – 30 nm range, while the capillary system works best for neon-like argon at 46.9 nm. Most researchers use nickel-like ion lasers near 14 nm because they are well matched to the Mo:Si multilayer mirrors that have peak reflectivity near 13 nm and are used in many applications. As a result, the last decade has seen the birth of the X-ray free electron laser (XFEL) that can reach wavelengths down to 0.15 nm and the inner-shell Ne laser at 1.46 nm.

Soft x-ray emission from gamma-ray bursts observed with ginga

International Nuclear Information System (INIS)

Yoshida, Atsumasa; Murakami, Toshio; Itoh, Masayuki

1989-01-01

The soft X-ray emission of gamma-ray bursts below 10 keV provides information about size, location, and emission mechanism. The Gamma-ray Burst Detector (GBD) on board Ginga, which consists of a proportional counter and a scintillation detector, covers an energy range down to 1.5 keV with 63 cm 2 effective area. In several of the observed gamma-ray bursts, the intensity of the soft X-ray emission showed a longer decay time of 50 to 100s after the higher energy gamma-ray emission had ended. Although we cannot rule out other models, such as bremsstrahlung and thermal cyclotron types, due to poor statistics, the soft X-ray spectra are consistent with a blackbody of 1 to 2 keV in the late phase of the gamma-ray bursts. This enables us to estimate the size of the blackbody responsible for the X-ray emission. (author)

X-ray imaging and detection using plastic scintillating fibers

CERN Document Server

Ikhlef, A; Beddar, A S

2000-01-01

This paper discusses the application of plastic scintillating fiber array in X-ray imaging with low-energy radiation. This array is coupled to a multichannel intensified photocathode and then to a CCD detector via a fiber optics taper. The length of the fiber array is experimentally optimized for the radiation used. We found here that the length of the fibers (interaction medium) does not contribute too much in the degradation of the spatial resolution under 10 keV irradiation along the axis of the fiber array. Modulation Transfer Function (MTF) measurements of the PSF array are compared to the optics MTF of the imaging system (without the sample) and that cross-talk in the fiber array is found to be negligible for a fiber array thickness of 20 mm.

Electron beam requirements for soft x-ray/XUV free-electron lasers

International Nuclear Information System (INIS)

Goldstein, J.C.

1987-01-01

A discussion of the electron beam quality (peak current, energy spread, and transverse emittance) required to drive short wavelength free-electron lasers in the XUV (10-100 nm) and soft x-ray (<10 nm) optical wavelength ranges is presented

The development for small scale soft X-ray spectrometer

International Nuclear Information System (INIS)

Sun Kexu; Jiang Shaoen; Yi Rongqing; Cui Yanli

2004-12-01

For the development of small-scale soft X-ray spectrometer, first, some small-scale soft X-ray detection elements are developed, it is included GaAs irradiated with neutron, GaAs irradiated with proton, multi-layer mirror, plane mirror and small scale X-ray diode et al. Soft X-ray spectrometers built of multi-layer mirror-GaAs (with neutron irradiation), and plane mirror-small-scale XRD, and plane mirror-GaAs (with proton irradiation) are prepared. These spectrometers are examined in Shen Guang-II laser facility, and some external estimation are given. (authors)

Structure in galactic soft X-ray features

International Nuclear Information System (INIS)

Davelaar, J.

1979-01-01

Observations are described of the soft X-ray background in a part of the northern hemisphere in the energy range 0.06 - 3.0 keV. The X-ray instruments, placed onboard a sounding rocket, are a one-dimensional focusing collector with multi-cell proportional counters in the focal plane and eight large area counters on deployable panels. A description of the instruments and their preflight calibration is given. Precautions were taken to prevent UV sensitivity of the X-ray instruments. The observation program, which consisted of a number of pre-programmed slow scans, is outlined. The spectral date on the soft X-ray background in these and previous observations showed that at least two components of different temperature are present. A low temperature component of approximately (3-10)x10 5 is found all over the sky. Components of higher temperature approximately 3x10 6 K are found in regions of soft X-ray enhancement; The North Polar Spur has been observed in two scans at the galactic latitude b=25 0 and b=75 0 . The X-ray ridge structure is found to be strongly energy dependent. The low energy data ( 0 reveals two separate emission features on the ridge, both probably of finite extensions (approximately equal to 0 0 .5). A wider X-ray ridge (approximately equal to 10 0 ) is observed above 0.4 keV. (Auth.)

Black hole and neutron star soft X-ray transients: a hard X-ray view of their outbursts

International Nuclear Information System (INIS)

Yu, W.

2004-01-01

The RXTE public observations of the outbursts of black hole soft X-ray transients XTE J1550-564, XTE J1859+226, 4U 1630-47, XTE J1118+480, XTE J1650-500, and the neutron star soft X-ray transients 4U 1608-52, Aquila X-1, including a variable 'persistent' neutron star low mass X-ray binary 4U 1705-44, are summarized in this paper. The hard X-ray view of those outbursts, which is quite different from that of the soft X-ray band, suggests that there are several types of outbursts which result in different hard X-ray outburst profile - the outburst profiles are energy dependent. One type is the low/hard state outbursts, the other type is the outburst showing transitions from the low/hard state to the high/soft state, or to the intermediate or to the very high state. The later has an initial low/hard state, introducing the phenomena that the hard X-ray precedes the soft X-ray in the outburst rise. Such outbursts in XTE J1550-564, Aql X-1 and 4U 1705-44 support a two-accretion-flow model which involves one Keplerian disk flow and one sub-Keplerian flow for the initial outburst rise

X-ray generation by femtosecond laser pulses and its application to soft X-ray imaging microscope

International Nuclear Information System (INIS)

Ikeda, Kenichi; Kotaki, Hideyuki; Nakajima, Kazuhisa

2002-01-01

We have developed laser-produced plasma X-ray sources using femtosecond laser pulses at 10Hz repetition rate in a table-top size in order to investigate basic mechanism of X-ray emission from laser-matter interactions and its application to a X-ray microscope. In a soft X-ray region over 5 nm wavelength, laser-plasma X-ray emission from a solid target achieved an intense flux of photons of the order of 1011 photons/rad per pulse with duration of a few 100 ps, which is intense enough to make a clear imaging in a short time exposure. As an application of laser-produced plasma X-ray source, we have developed a soft X-ray imaging microscope operating in the wavelength range around 14 nm. The microscope consists of a cylindrically ellipsoidal condenser mirror and a Schwarzshird objective mirror with highly-reflective multilayers. We report preliminary results of performance tests of the soft X-ray imaging microscope with a compact laser-produced plasma X-ray source

Development of small scale soft x-ray lasers

International Nuclear Information System (INIS)

Kim, D.; Suckewer, S.; Princeton Univ., NJ; Skinner, C.H.; Voorhees, D.

1991-05-01

At present rapid progress is being made in the application of soft x-ray lasers to fields such as microscopy and microlithography. A critical factor in the range of suitable applications is the scale and hence cost of the soft x-ray lasers. At Princeton, gain at 183 angstrom has been obtained with relatively low pump laser energies (as low as 6J) in a ''portable'' small-scale soft x-ray laser system. We will also discuss aspects of data interpretation and pitfalls to be avoided in measurements of gain in such systems. 14 refs., 7 figs

Characterization of X-ray optics by soft X-ray diffractometry

International Nuclear Information System (INIS)

Biltoft, P.J.

1988-01-01

The authors have constructed a soft x-ray diffractometer to characterize layered synthetic microstructures (LSMs). The source, sample stage, and counter sections of the diffractometer operate under vacuum. The design differs from most others in two respects: the preamplifier and amplifier that process pulses from the subatmospheric-pressure gas-flow proportional counter are located outside the vacuum chamber and are separated from the proportional counter by approximately 76 cm of shielded cable; in addition, the conventional gear-driven, theta-two-theta diffractometer motion is accomplished with synchronized stepper motors. Characterizations of several LSMs have yielded data on d-spacing (distance between layers of different composition), critical angle, and peak reflectivity. Future work includes incorporation of an improved laser alignment system, in vacuo sample articulation (in addition to the theta-two-theta diffractometer movements), and a higher-flux photon source with a close-coupled fluorescent target carousel. Such a capability will permit multiple-energy diffraction work in a single pumpdown cycle

The soft x ray telescope for Solar-A

Science.gov (United States)

Brown, W. A.; Acton, L. W.; Bruner, M. E.; Lemen, J. R.; Strong, K. T.

1989-01-01

The Solar-A satellite being prepared by the Institute for Sapce and Astronautical Sciences (ISAS) in Japan is dedicated to high energy observations of solar flares. The Soft X Ray Telescope (SXT) is being prepared to provide filtered images in the 2 to 60 A interval. The flight model is now undergoing tests in the 1000 foot tunnel at MSFC. Launch will be in September 1991. Earlier resolution and efficiency tests on the grazing incidence mirror have established its performance in soft x rays. The one-piece, two mirror grazing incidence telescope is supported in a strain free mount separated from the focal plane assembly by a carbon-epoxy metering tube whose windings and filler are chosen to minimize thermal and hygroscopic effects. The CCD detector images both the x ray and the concentric visible light aspect telescope. Optical filters provide images at 4308 and 4700 A. The SXT will be capable of producing over 8000 of the smallest partial frame images per day, or fewer but larger images, up to 1024 x 1024 pixel images. Image sequence with two or more of the five x ray analysis filters, with automatic exposure compensation to optimize the charge collection by the CCD detector, will be used to provide plasma diagnostics. Calculations using a differential emission measure code were used to optimize filter selection over the range of emission measure variations and to avoid redundancy, but the filters were chosen primarily to give ratios that are monotonic in plasma temperature.

The soft x ray telescope for Solar-A

International Nuclear Information System (INIS)

Brown, W.A.; Acton, L.W.; Bruner, M.E.; Lemen, J.R.; Strong, K.T.

1989-01-01

The Solar-A satellite being prepared by the Institute for Sapce and Astronautical Sciences (ISAS) in Japan is dedicated to high energy observations of solar flares. The Soft X Ray Telescope (SXT) is being prepared to provide filtered images in the 2 to 60 A interval. The flight model is now undergoing tests in the 1000 foot tunnel at MSFC. Launch will be in September 1991. Earlier resolution and efficiency tests on the grazing incidence mirror have established its performance in soft x rays. The one-piece, two mirror grazing incidence telescope is supported in a strain free mount separated from the focal plane assembly by a carbon-epoxy metering tube whose windings and filler are chosen to minimize thermal and hygroscopic effects. The CCD detector images both the x ray and the concentric visible light aspect telescope. Optical filters provide images at 4308 and 4700 A. The SXT will be capable of producing over 8000 of the smallest partial frame images per day, or fewer but larger images, up to 1024 x 1024 pixel images. Image sequence with two or more of the five x ray analysis filters, with automatic exposure compensation to optimize the charge collection by the CCD detector, will be used to provide plasma diagnostics. Calculations using a differential emission measure code were used to optimize filter selection over the range of emission measure variations and to avoid redundancy, but the filters were chosen primarily to give ratios that are monotonic in plasma temperature

Soft x rays for radiobiological studies

International Nuclear Information System (INIS)

Ban, Sadayuki; Iida, Shozo; Shimba, Hachiro; Awa, A.A.; Hamilton, H.B.; Clifton, K.H.

1986-04-01

Lethal effects and chromosome aberrations induced in cells exposed to low energy (soft) X rays demonstrated that these relatively low energy X rays are just as effective as those of higher energy for radiobiological studies, and even more effective for irradiating cultured mammalian cells than laboratory animals. (author)

Soft X-ray focusing Telescope aboard AstroSat

DEFF Research Database (Denmark)

Singh, K. P.; Dewangan, G. C.; Chandra, S.

2017-01-01

The Soft X-ray focusing Telescope (SXT) is a moderateresolution X-ray imaging spectrometer supplementing the ultraviolet and hard X-ray payloads for broadband studies of cosmic sources with AstroSat. Well suited for observing bright X-ray sources, SXT observations of nearby active galactic nuclei...

Thin film soft X-ray absorption filters

International Nuclear Information System (INIS)

Stattin, H.

1992-11-01

This report discusses the composition, reparation and performance of soft x-ray transmission filters for a water window soft x-ray microscope. Unbacked thin films of aluminum, silver and vanadium/aluminum were made by evaporation on a substrate from which they were released. Measured transmittances agree reasonably well with calculations. The report also includes some related theory and discussions about film preparation methods, film contamination and evaluation methods. 33 refs

Soft X-ray excited optical luminescence from functional organic materials

Energy Technology Data Exchange (ETDEWEB)

Sham, T.K., E-mail: tsham@uwo.ca

2015-10-01

Highlights: • Many functional organic materials convert X-ray energy into visible light. • The X-ray induced luminescence (XEOL) across an absorption edge can be site and excitation channel specific. • XEOL is composition, morphology, size and crystallinity dependent. • XEOL using the time structure of a synchrotron can reveal the decay and energy transfer dynamics of the sample. • The combined use of XEOL and XAS in the analysis of functional organic materials is illustrated. - Abstract: This brief report reviews some of the recent findings in the study of synchrotron based X-ray excited optical luminescence (XEOL) from representative organic light emitting device (OLED) and related functional organic materials. The systems of interest include Alq{sub 3}, aluminium tris(8-hydroxylquinoline); Ru(bipy){sub 3}{sup 2+}, tris-(2,2-bipyridine) ruthenium(II); Ir(bpy){sub 3}, tris(2-phenyl-bipyridine)iridium; PVK (poly(N-vinylcarbazole)) and [Au{sub 2}(dppe)(bipy)]{sup 2+}, a Au(I) polymer containing 1,2-bis(diphenylphosphino)ethane and the 4,40-bipyridyl ligands, as well as TBPe (2,5,8,11-tetra-tert-butylperylene) polyhedral crystals and fluorescein isothiocyanate (FITC) and FITC-labelled proteins. It is shown that tunable and pulsed X-rays from synchrotron light sources enable the detailed tracking of the optical properties of organic functional materials by monitoring the luminescence in both the energy and time domain as the excitation energy is scanned across an element-specific absorption edge. The use of XEOL and X-ray absorption spectroscopy (XAS) in materials analysis is illustrated.

Multilayer on-chip stacked Fresnel zone plates: Hard x-ray fabrication and soft x-ray simulations

Energy Technology Data Exchange (ETDEWEB)

Li, Kenan; Wojcik, Michael J.; Ocola, Leonidas E.; Divan, Ralu; Jacobsen, Chris

2015-11-01

Fresnel zone plates are widely used as x-ray nanofocusing optics. To achieve high spatial resolution combined with good focusing efficiency, high aspect ratio nanolithography is required, and one way to achieve that is through multiple e-beam lithography writing steps to achieve on-chip stacking. A two-step writing process producing 50 nm finest zone width at a zone thickness of 1.14 µm for possible hard x-ray applications is shown here. The authors also consider in simulations the case of soft x-ray focusing where the zone thickness might exceed the depth of focus. In this case, the authors compare on-chip stacking with, and without, adjustment of zone positions and show that the offset zones lead to improved focusing efficiency. The simulations were carried out using a multislice propagation method employing Hankel transforms.

The advantages of soft X-rays and cryogenic spectrometers for measuring chemical speciation by X-ray spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Drury, Owen B. [Lawrence Livermore National Laboratory, Advanced Detector Group, 7000 East Ave., L-270, Livermore, CA 94550 (United States); UC Davis, Biophysics Graduate Group, 1 Shields Ave, CA 95616 (United States); LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States); Friedrich, Stephan [Lawrence Livermore National Laboratory, Advanced Detector Group, 7000 East Ave., L-270, Livermore, CA 94550 (United States) and LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States)]. E-mail: friedrich1@llnl.gov; George, Simon J. [LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States); Cramer, Stephen P. [UC Davis, Biophysics Graduate Group, 1 Shields Ave, CA 95616 (United States); LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States)

2006-04-15

We have built a 36-pixel high-resolution superconducting tunnel junction (STJ) soft X-ray spectrometer for chemical analysis of dilute metals by fluorescence-detected X-ray absorption spectroscopy (XAS) at the Advanced Light Source synchrotron. Soft X-ray absorption edges are preferred over traditional hard X-ray spectroscopy at the K-edges, since they have narrower natural linewidths and exhibit stronger chemical shifts. STJ detectors are preferred in the soft X-ray band over traditional Ge or grating spectrometers, since they have sufficient energy resolution to resolve transition metal L and M lines from light element K emission, and sufficient detection efficiency to measure the weak lines of dilute specimens within an acceptable time. We demonstrate the capabilities of our STJ spectrometer for chemical analysis with soft XAS measurements of molybdenum speciation on the Mo M{sub 4,5}-edges.

Considerations for a soft x-ray spectromicroscopy beamline

International Nuclear Information System (INIS)

Winn, B.; Hao, X.; Jacobsen, C.

1996-01-01

The X-1A soft x-ray undulator at the NSLS is the source for the experimental programs in spectromicroscopy. The authors require both spatial and temporal coherence. Due to the relatively large horizontal divergence of the electron beam in the low β straight section of the x-ray storage ring, it has been possible to split the beam using a scraping mirror into two branches: X-1A used by the authors' program and X-1B used for high resolution spectroscopy. They are now rebuilding the X-1A beamline to provide improved resolving power and essentially linear trade-off between photon rate at the zone plate and resolving power for the soft x-ray spectromicroscopy experiments. This new beamline will exploit both additional floorspace due to the NSLS building expansion and increases in the brightness of the x-ray ring. The beam will be further split into two separate beamlines, both of which will use toroidal mirrors to focus the source on the monochromator entrance slits horizontally and to focus on the monochromator exit slits vertically. This separation comes at no loss of coherent flux and permits low thermal loading on the optics, since the authors need little more than the coherent fraction of the beam at the Fresnel zone plate for microfocusing. Because of the small angular acceptance for spatially coherent illumination of the zone plates and the use of an approximately satisfied Rowland condition, the monochromators have sufficient resolving power with fixed exit arms. Experiments can then be placed near the exit slits, with spatial coherence established by the exit slit size. Resolving power will be controlled by adjusting the entrance slit alone with no change of spatial coherence. The zone plates will be overfilled to be less sensitive to beam vibration and drift

Coherent hard x-ray focusing optics and applications

Energy Technology Data Exchange (ETDEWEB)

Yun, W.B.; Viccaro, P.J.; Chrzas, J.; Lai, B.

1991-01-01

Coherent hard x-ray beams with a flux exceeding 10{sup 9} photons/second with a bandwidth of 0.1% will be provided by the undulator at the third generation synchrotron radiation sources such as APS, ESRF, and Spring-8. The availability of such high flux coherent x-ray beams offers excellent opportunities for extending the coherence-based techniques developed in the visible and soft x-ray part of the electromagnetic spectrum to the hard x-rays. These x-ray techniques (e.g., diffraction limited microfocusing, holography, interferometry, phase contrast imaging and signal enhancement), may offer substantial advantages over non-coherence-based x-ray techniques currently used. For example, the signal enhancement technique may be used to enhance an anomalous x-ray or magnetic x-ray scattering signal by several orders of magnitude. Coherent x-rays can be focused to a very small (diffraction-limited) spot size, thus allowing high spatial resolution microprobes to be constructed. The paper will discuss the feasibility of the extension of some coherence-based techniques to the hard x-ray range and the significant progress that has been made in the development of diffraction-limited focusing optics. Specific experimental results for a transmission Fresnel phase zone plate that can focus 8.2 keV x-rays to a spot size of about 2 microns will be briefly discussed. The comparison of measured focusing efficiency of the zone plate with that calculated will be made. Some specific applications of zone plates as coherent x-ray optics will be discussed. 17 refs., 4 figs.

Combined optic system based on polycapillary X-ray optics and single-bounce monocapillary optics for focusing X-rays from a conventional laboratory X-ray source

Energy Technology Data Exchange (ETDEWEB)

Sun, Xuepeng; Liu, Zhiguo [The Key Laboratory of Beam Technology and Materials Modification of the Ministry of Education, Beijing Normal University, Beijing 100875 (China); College of Nuclear Science and Technology, Beijing Normal University, Beijing 100875 (China); Beijing Radiation Center, Beijing 100875 (China); Sun, Tianxi, E-mail: stx@bnu.edu.cn [The Key Laboratory of Beam Technology and Materials Modification of the Ministry of Education, Beijing Normal University, Beijing 100875 (China); College of Nuclear Science and Technology, Beijing Normal University, Beijing 100875 (China); Beijing Radiation Center, Beijing 100875 (China); Yi, Longtao; Sun, Weiyuan; Li, Fangzuo; Jiang, Bowen [The Key Laboratory of Beam Technology and Materials Modification of the Ministry of Education, Beijing Normal University, Beijing 100875 (China); College of Nuclear Science and Technology, Beijing Normal University, Beijing 100875 (China); Beijing Radiation Center, Beijing 100875 (China); Ma, Yongzhong [Center for Disease Control and Prevention of Beijing, Beijing 100013 (China); Ding, Xunliang [The Key Laboratory of Beam Technology and Materials Modification of the Ministry of Education, Beijing Normal University, Beijing 100875 (China); College of Nuclear Science and Technology, Beijing Normal University, Beijing 100875 (China); Beijing Radiation Center, Beijing 100875 (China)

2015-12-01

Two combined optic systems based on polycapillary X-ray optics and single-bounce monocapillary optics (SBMO) were designed for focusing the X-rays from a conventional laboratory X-ray source. One was based on a polycapillary focusing X-ray lens (PFXRL) and a single-bounce ellipsoidal capillary (SBEC), in which the output focal spot with the size of tens of micrometers of the PFXRL was used as the “virtual” X-ray source for the SBEC. The other system was based on a polycapillary parallel X-ray lens (PPXRL) and a single-bounce parabolic capillary (SBPC), in which the PPXRL transformed the divergent X-ray beam from an X-ray source into a quasi-parallel X-ray beam with the divergence of sever milliradians as the incident illumination of the SBPC. The experiment results showed that the combined optic systems based on PFXRL and SBEC with a Mo rotating anode X-ray generator with the focal spot with a diameter of 300 μm could obtain a focal spot with the total gain of 14,300 and focal spot size of 37.4 μm, and the combined optic systems based on PPXRL and SBPC with the same X-ray source mentioned above could acquire a focal spot with the total gain of 580 and focal spot size of 58.3 μm, respectively. The two combined optic systems have potential applications in micro X-ray diffraction, micro X-ray fluorescence, micro X-ray absorption near edge structure, full field X-ray microscopes and so on.

Soft x-ray virtual diagnostics for tokamak simulations

Science.gov (United States)

Kim, J. S.; Zhao, L.; Bogatu, I. N.; In, Y.; Turnbull, A.; Osborne, T.; Maraschek, M.; Comer, K.

2009-11-01

The numerical toolset, FAR-TECH Virtual Diagnostic Utility, for generating virtual experimental data based on theoretical models and comparing it with experimental data, has been developed for soft x-ray diagnostics on DIII-D. The virtual (or synthetic) soft x-ray signals for a sample DIII-D discharge are compared with the experimental data. The plasma density and temperature radial profiles needed in the soft x-ray signal modeling are obtained from experimental data, i.e., from Thomson scattering and electron cyclotron emission. The virtual soft x-ray diagnostics for the equilibriums have a good agreement with the experimental data. The virtual diagnostics based on an ideal linear instability also agree reasonably well with the experimental data. The agreements are good enough to justify the methodology presented here for utilizing virtual diagnostics for routine comparison of experimental data. The agreements also motivate further detailed simulations with improved physical models such as the nonideal magnetohydrodynamics contributions (resistivity, viscosity, nonaxisymmetric error fields, etc.) and other nonlinear effects, which can be tested by virtual diagnostics with various stability modeling.

Soft x-ray virtual diagnostics for tokamak simulations

International Nuclear Information System (INIS)

Kim, J. S.; Zhao, L.; Bogatu, I. N.; In, Y.; Turnbull, A.; Osborne, T.; Maraschek, M.; Comer, K.

2009-01-01

The numerical toolset, FAR-TECH Virtual Diagnostic Utility, for generating virtual experimental data based on theoretical models and comparing it with experimental data, has been developed for soft x-ray diagnostics on DIII-D. The virtual (or synthetic) soft x-ray signals for a sample DIII-D discharge are compared with the experimental data. The plasma density and temperature radial profiles needed in the soft x-ray signal modeling are obtained from experimental data, i.e., from Thomson scattering and electron cyclotron emission. The virtual soft x-ray diagnostics for the equilibriums have a good agreement with the experimental data. The virtual diagnostics based on an ideal linear instability also agree reasonably well with the experimental data. The agreements are good enough to justify the methodology presented here for utilizing virtual diagnostics for routine comparison of experimental data. The agreements also motivate further detailed simulations with improved physical models such as the nonideal magnetohydrodynamics contributions (resistivity, viscosity, nonaxisymmetric error fields, etc.) and other nonlinear effects, which can be tested by virtual diagnostics with various stability modeling.

Review of soft x-ray lasers and their applications

International Nuclear Information System (INIS)

Skinner, C.H.

1991-03-01

The emerging technology of soft x-ray lasers is in a transition phase between the first laboratory demonstrations of gain and the acceptance of soft x-ray lasers as practical tools for novel applications. Current research is focused on several fronts. The operational wavelength range has been extended to the ''water window'', important for applications in the life sciences. Gain has also been generated with substantially simpler technology (such as a 6J laser) and this augurs well for the commercially availability in the near future of soft x-ray lasers for a variety of applications. Advanced soft x-ray laser concepts are being developed from investigations into ultra-high intensity laser/matter interactions. The first paper a brief historical perspective of x-ray microscopy and holography have begun. In this paper a brief historical perspective of x-ray laser development will be followed by a review of recent advances in recombination, collisional and photo-pumped systems and applications. A summary of current gain-length performance achieved in laboratories worldwide is presented. Near term prospects for applications to novel fields are discussed. 81 refs., 9 figs., 1 tab

Space power distribution of soft x-ray source ANGARA-5-1

Energy Technology Data Exchange (ETDEWEB)

Dyabilin, K S [High Energy Density Research Center, Moscow (Russian Federation); Fortov, V E; Grabovskij, E V; Lebedev, M E; Smirnov, V P [Troitsk Inst. of Innovative and Fusion Research, Troitsk (Russian Federation)

1997-12-31

The contribution deals with the investigation of shock waves in condensed targets generated by intense pulses of soft X radiation. Main attention is paid to the spatial distribution of the soft x-ray power, which influence strongly the shock wave front uniformity. Hot z-pinch plasma with the temperature of 60-100 eV produced by imploding double liner in the ANGARA-5-1 machine was used as a source of x rays. The maximum pinch current was as high as 3.5 MA. In order to eliminate the thermal heating of the targets, thick stepped Al/Pb, Sn/Pb, or pure Pb targets were used. The velocity of shock waves was determined by means of optical methods. Very uniform shock waves and shock pressures of up to several hundreds of GPa have been achieved. (J.U.). 3 figs., 2 refs.

A compact soft X-ray microscope using an electrode-less Z-pinch source

Science.gov (United States)

Horne, S. F.; Silterra, J.; Holber, W.

2009-09-01

Soft X-rays (medical interest both for imaging and microdosimetry applications. X-ray sources at this low energy present a technological challenge. Synchrotrons, while very powerful and flexible, are enormously expensive national research facilities. Conventional X-ray sources based on electron bombardment can be compact and inexpensive, but low x-ray production efficiencies at low electron energies restrict this approach to very low power applications. Laser-based sources tend to be expensive and unreliable. Energetiq Technology, Inc. (Woburn, MA, USA) markets a 92 eV, 10W(2pi sr) electrode-less Z-pinch source developed for advanced semiconductor lithography. A modified version of this commercial product has produced 400 mW at 430 eV (2pi sr), appropriate for water window soft X-ray microscopy. The US NIH has funded Energetiq to design and construct a demonstration microscope using this source, coupled to a condenser optic, as the illumination system. The design of the condenser optic matches the unique characteristics of the source to the illumination requirements of the microscope, which is otherwise a conventional design. A separate program is underway to develop a microbeam system, in conjunction with the RARAF facility at Columbia University, NY, USA. The objective is to develop a focused, sub-micron beam capable of delivering > 1 Gy/second to the nucleus of a living cell. While most facilities of this type are coupled to a large and expensive particle accelerator, the Z-pinch X-ray source enables a compact, stand-alone design suitable to a small laboratory. The major technical issues in this system involve development of suitable focusing X-ray optics. Current status of these programs will be reported. (Supported by NIH grants 5R44RR022488-03 and 5R44RR023753-03)

Multiwavelength Observations of the 2002 Outburst of GX 339-4: Two Patterns of X-Ray-Optical/Near-Infrared Behavior

Science.gov (United States)

Homan, Jeroen; Buxton, Michelle; Markoff, Sera; Bailyn, Charles D.; Nespoli, Elisa; Belloni, Tomaso

2005-05-01

We report on quasi-simultaneous Rossi X-Ray Timing Explorer and optical/near-infrared (NIR) observations of the black hole candidate X-ray transient GX 339-4. Our observations were made over a time span of more than 8 months in 2002 and cover the initial rise and transition from a hard to a soft spectral state in X-rays. Two distinct patterns of correlated X-ray-optical/NIR behavior were found. During the hard state, the optical/NIR and X-ray fluxes correlated well, with a NIR versus X-ray flux power-law slope similar to that of the correlation found between X-ray and radio fluxes in previous studies of GX 339-4 and other black hole binaries. As the source went through an intermediate state, the optical/NIR fluxes decreased rapidly, and once it had entered the spectrally soft state, the optical/NIR spectrum of GX 339-4 was much bluer, and the ratio of X-ray to NIR flux was higher by a factor of more than 10 compared to the hard state. In the spectrally soft state, changes in the NIR preceded those in the soft X-rays by more than 2 weeks, indicating a disk origin of the NIR emission and providing a measure of the viscous timescale. A sudden onset of NIR flaring of ~0.5 mag on a timescale of 1 day was also observed during this period. We present spectral energy distributions, including radio data, and discuss possible sources for the optical/NIR emission. We conclude that, in the hard state, this emission probably originates in the optically thin part of a jet and that in none of the X-ray states is X-ray reprocessing the dominant source of optical/NIR emission. Finally, comparing the light curves from the all-sky monitor (ASM) and Proportional Counter Array (PCA) instruments, we find that the X-ray/NIR delay depends critically on the sensitivity of the X-ray detector, with the delay inferred from the PCA (if present at all) being a factor of 3-6 times shorter than the delay inferred from the ASM; this may be important in interpreting previously reported X-ray-optical

High efficiency spectro graphs for the EUV and soft x-rays

International Nuclear Information System (INIS)

Cash, W.

1983-01-01

A basic need of modern UV and x-ray astronomy is the capability to perform high resolution spectroscopy of faint stars. The use of modern grazing incidence optics can be coupled to high blaze angle reflection gratings used in the conical diffraction mount to offer a versatile, efficient approach to the design problem. The authors discuss two designs of interest: an echelle spectrograph for use longward of 100 A, and an Objective Reflection Grating Spectrograph for use in the soft x-rays. General design considerations and measurements of grating efficiencies are also presented

Soft X-ray images of the solar corona using normal incidence optics

Science.gov (United States)

Bruner, M. E.; Haisch, B. M.; Brown, W. A.; Acton, L. W.; Underwood, J. H.

1988-01-01

A solar coronal loop system has been photographed in soft X-rays using a normal incidence telescope based on multilayer mirror technology. The telescope consisted of a spherical objective mirror of 4 cm aperture and 1 m focal length, a film cassette, and a focal plane shutter. A metallized thin plastic film filter was used to exclude visible light. The objective mirror was covered with a multilayer coating consisting of alternating layers of tungsten and carbon whose combined thicknesses satisfied the Bragg diffraction condition for 44 A radiation. The image was recorded during a rocket flight on October 25, 1985 and was dominated by emission lines arising from the Si XII spectrum. The rocket also carried a high resolution soft X-ray spectrograph that confirmed the presence of Si XII line radiation in the source. This image represents the first successful use of multilayer technology for astrophysical observations.

Characterization of collisionally pumped optical-field-ionization soft X-ray lasers

Czech Academy of Sciences Publication Activity Database

Mocek, Tomáš; Sebban, S.; Bettaibi, I.; Upcraft, L. M.; Balcou, P.; Breger, P.; Zeitoun, P.; Le Pape, S.; Ros, D.; Klisnick, A.; Carillon, A.; Jamelot, G.; Rus, Bedřich; Wyart, J. F.

2004-01-01

Roč. 78, - (2004), s. 939-944 ISSN 0946-2171 Grant - others:HPRI(XE) 199900086 Institutional research plan: CEZ:AV0Z1010921 Keywords : X-ray lasers * optical-field-ionization * collisional excitation Subject RIV: BH - Optics, Masers, Lasers Impact factor: 2.215, year: 2004

Midinfrared optical rogue waves in soft glass photonic crystal fiber

DEFF Research Database (Denmark)

Buccoliero, Daniel; Steffensen, Henrik; Ebendorff-Heidepriem, Heike

2011-01-01

We investigate numerically the formation of extreme events or rogue waves in soft glass tellurite fibers and demonstrate that optical loss drastically diminishes shot-to-shot fluctuations characteristic of picosecond pumped supercontinuum (SC). When loss is neglected these fluctuations include...... distributions. Our results thus implicitly show that rogue waves will not occur in any SC spectrum that is limited by loss, such as commercial silica fiber based SC sources. © 2011 Optical Society of America....

X-ray testing of fiber composite plastics

International Nuclear Information System (INIS)

Altmann, O.; Lembke, B.

1984-01-01

Besides the ultrasonic test, X-raying is the most important non-destructive test procedure for supporting fibre composite structures. This report presents some auxiliary means and test results regarding the limits of fault detectibility during the X-raying of fiber composite structures, preferrably carbon fiber laminates (CFRP). (orig.) [de

Figure tolerance of a Wolter type I mirror for a soft-x-ray microscope

International Nuclear Information System (INIS)

Chon, Kwon Su; Namba, Yoshiharu; Yoon, Kwon-Ha

2007-01-01

The demand for an x-ray microscope has received much attention because of the desire to study living cells at a high resolution and in a hydrated environment. A Wolter type I mirror used for soft-x-ray microscope optics has many advantages. From the mirror fabrication point of view, it is necessary to perform tolerance analysis, particularly with respect to figure errors that considerably degrade the image quality.The figure tolerance of a Wolter type I mirror for a biological application in terms of the image quality and the state-of-the-art fabrication technology is discussed. The figure errors rapidly destroyed the image quality, and the required slope error depended on the detector used in the soft-x-ray microscope

Be Foil ''Filter Knee Imaging'' NSTX Plasma with Fast Soft X-ray Camera

International Nuclear Information System (INIS)

B.C. Stratton; S. von Goeler; D. Stutman; K. Tritz; L.E. Zakharov

2005-01-01

A fast soft x-ray (SXR) pinhole camera has been implemented on the National Spherical Torus Experiment (NSTX). This paper presents observations and describes the Be foil Filter Knee Imaging (FKI) technique for reconstructions of a m/n=1/1 mode on NSTX. The SXR camera has a wide-angle (28 o ) field of view of the plasma. The camera images nearly the entire diameter of the plasma and a comparable region in the vertical direction. SXR photons pass through a beryllium foil and are imaged by a pinhole onto a P47 scintillator deposited on a fiber optic faceplate. An electrostatic image intensifier demagnifies the visible image by 6:1 to match it to the size of the charge-coupled device (CCD) chip. A pair of lenses couples the image to the CCD chip

Structural mechanics of the solar-A Soft X-ray Telescope

Science.gov (United States)

Jurcevich, B. K.; Bruner, M. E.; Gowen, K. F.

1992-01-01

The Soft X-ray Telescope (SXT) is one of four major instruments that constitute the payload of the NASA-Japanese mission YOHKOH (formerly known as Solar-A), scheduled to be launched in August, 1991. This paper describes the design of the SXT, the key system requirements, and the SXT optical and structural systems. Particular attention is given to the design considerations for stiffness and dimensional stability, temperature compensation, and moisture sensitivyty control. Consideration is also given to the X-ray mirror, the aspect telescope, the entrance filters, the mechanical structure design, the aft support plate and mount, the SXT finite element model, and other subsystems.

Soft x-ray amplification in an ablative capillary discharge

International Nuclear Information System (INIS)

Kwek, K.H.; Low, K.S.; Tan, C.A.; Lim, C.S.

1999-01-01

Soft x-ray amplification in CVI 18.2 nm line is observed in an ablative UHMW-PE capillary discharge. The gain coefficient is measured to be 1.9 cm -1 . The electron density is about 2 x 10 19 cm -3 . This indicates that capillary discharge pumping device can be a source for a compact soft x-ray laser. (author)

Design calculations for a xenon plasma x-ray shield to protect the NIF optical Thomson scattering diagnostic.

Science.gov (United States)

Swadling, G F; Ross, J S; Datte, P; Moody, J; Divol, L; Jones, O; Landen, O

2016-11-01

An Optical Thomson Scattering (OTS) diagnostic is currently being developed for the National Ignition Facility (NIF) at Lawrence Livermore National Laboratory. This diagnostic is designed to make measurements of the hohlraum plasma parameters, such as the electron temperature and the density, during inertial confinement fusion (ICF) experiments. NIF ICF experiments present a very challenging environment for optical measurements; by their very nature, hohlraums produce intense soft x-ray emission, which can cause "blanking" (radiation induced opacity) of the radiation facing optical components. The soft x-ray fluence at the surface of the OTS blast shield, 60 cm from the hohlraum, is estimated to be ∼8 J cm -2 . This is significantly above the expected threshold for the onset of "blanking" effects. A novel xenon plasma x-ray shield is proposed to protect the blast shield from x-rays and mitigate "blanking." Estimates suggest that an areal density of 10 19 cm -2 Xe atoms will be sufficient to absorb 99.5% of the soft x-ray flux. Two potential designs for this shield are presented.

Guiding hard x rays with glass polycapillary fiber

International Nuclear Information System (INIS)

Xiao, Q.F.; Ponomarev, I.Y.; Kolomitsev, A.I.; Gibson, D.M.; Dilmanian, F.A.; Nachaliel, E.

1993-01-01

X rays can be guided through a polycapillary fiber by multiple total reflections from the smooth channel walls of the fiber. Using monochromatic Synchrotron Radiation at energies of 22 and 44 keV, we measured the efficiency of transmission of x rays through polycapillary fibers with channel diameters of about 13 μm. Efficiencies of 57.3% and 54.5% for 22 keV and 44 keV x rays, respectively, were obtained with a 120-mm-long straight polycapillary fiber aligned with the incident beam. These values are close to the open fraction of the fiber, which is about 60%. In addition, transmission efficiency was measured as a function of the tilt angle between the incident beam and the axis of the fiber. We also measured the transmission efficiency as a function of the deflection angle for a 114-mm-long curved polycapillary fiber. The measurements are compared with a ray-tracing simulation

Photothermal lesions in soft tissue induced by optical fiber microheaters.

Science.gov (United States)

Pimentel-Domínguez, Reinher; Moreno-Álvarez, Paola; Hautefeuille, Mathieu; Chavarría, Anahí; Hernández-Cordero, Juan

2016-04-01

Photothermal therapy has shown to be a promising technique for local treatment of tumors. However, the main challenge for this technique is the availability of localized heat sources to minimize thermal damage in the surrounding healthy tissue. In this work, we demonstrate the use of optical fiber microheaters for inducing thermal lesions in soft tissue. The proposed devices incorporate carbon nanotubes or gold nanolayers on the tips of optical fibers for enhanced photothermal effects and heating of ex vivo biological tissues. We report preliminary results of small size photothermal lesions induced on mice liver tissues. The morphology of the resulting lesions shows that optical fiber microheaters may render useful for delivering highly localized heat for photothermal therapy.

TiO2 Nanoparticles as a Soft X-ray Molecular Probe

Energy Technology Data Exchange (ETDEWEB)

Larabell, Carolyn; Ashcroft, Jared M.; Gu, Weiwei; Zhang, Tierui; Hughes, Steven M.; Hartman, Keith B.; Hofmann, Cristina; Kanaras, Antonios G.; Kilcoyne, David A.; Le Gros, Mark; Yin, Yadong; Alivisatos, A. Paul; Larabell, Carolyn A.

2007-06-30

With the emergence of soft x-ray techniques for imaging cells, there is a pressing need to develop protein localization probes that can be unambiguously identified within the region of x-ray spectrum used for imaging. TiO2 nanocrystal colloids, which have a strong absorption cross-section within the "water-window" region of x-rays, areideally suited as soft x-ray microscopy probes. To demonstrate their efficacy, TiO2-streptavidin nanoconjugates were prepared and subsequently labeled microtubules polymerized from biotinylated tubulin. The microtubules were imaged using scanning transmission x-ray microscopy (STXM), and the TiO2 nanoparticle tags were specifically identified using x-ray absorption near edge spectroscopy (XANES). These experiments demonstrate that TiO2 nanoparticles are potential probes for protein localization analyses using soft x-ray microscopy.

Scintillating ribbon x-ray detector

International Nuclear Information System (INIS)

Kinchen, B.E.; Rogers, A.

1995-01-01

A patent in the early 1970's by Aerojet Corporation in Sacramento, CA put forth the idea of using an array of scintillating fibers for x-ray detection and imaging. In about 1975, Pratt and Whitney Aircraft in East Hartford, CT designed and manufactured an imaging system based on the patent. The device was 1.75 in thick in the direction of the x-ray beam and about 4 in. by 4 in. square. The device was used with a 8 MeV x-ray source to image and measure internal clearances within operating aircraft, gas turbines engines. There are significant advantages of fiber optic detectors in x-ray detection. However, the advantages are often outweighed by the disadvantages. Two of the advantages of scintillating fiber optic x-ray detectors are: (1) high limiting spatial frequency -- between 20 and 25 lp/mm; and (2) excellent x-ray stopping power -- they can be made thick and retain spatial resolution. In traditional fiber optic detectors the x-rays are oriented parallel to the long axis of the fiber. For the scintillating ribbon x-ray sensor, the x-rays are oriented normal to the fiber long axis. This ribbon sensor technique has a number of advantages over the two current radiographic techniques digital x-radiography and x-ray film: The main advantage the ribbon has is size and shape. It can be as thin as 0.05 in., virtually any width or length, and flexible. Once positioned in a given location, 20 to 100 square inches of the object being inspected can be imaged with a single x-ray beam sweep. It is clear that conventional digital cameras do not lend themselves to placement between walls of aircraft structures or similar items requiring x-ray inspections. A prototype scintillating ribbon x-ray sensor has been fabricated and tested by Synergistic Detector Designs. Images were acquired on corrosion test panels of aluminum fabricated by Iowa State University

Principles of femtosecond X-ray/optical cross-correlation with X-ray induced transient optical reflectivity in solids

Energy Technology Data Exchange (ETDEWEB)

Eckert, S., E-mail: sebastian.eckert@helmholtz-berlin.de, E-mail: martin.beye@helmholtz-berlin.de; Beye, M., E-mail: sebastian.eckert@helmholtz-berlin.de, E-mail: martin.beye@helmholtz-berlin.de; Pietzsch, A.; Quevedo, W.; Hantschmann, M. [Institute for Methods and Instrumentation in Synchrotron Radiation Research, Helmholtz-Zentrum Berlin für Materialien und Energie GmbH, Albert-Einstein-Str. 15, 12489 Berlin (Germany); Ochmann, M.; Huse, N. [Institute for Nanostructure and Solid State Physics, University of Hamburg, Jungiusstr. 11, 20355 Hamburg, Germany and Max Planck Institute for the Structure and Dynamics of Matter, Center for Free-Electron Laser Science, Luruper Chaussee 149, 22761 Hamburg (Germany); Ross, M.; Khalil, M. [Department of Chemistry, University of Washington, Box 351700, Seattle, Washington 98195 (United States); Minitti, M. P.; Turner, J. J.; Moeller, S. P.; Schlotter, W. F.; Dakovski, G. L. [LCLS, SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, California 94025 (United States); Föhlisch, A. [Institute for Methods and Instrumentation in Synchrotron Radiation Research, Helmholtz-Zentrum Berlin für Materialien und Energie GmbH, Albert-Einstein-Str. 15, 12489 Berlin (Germany); Institut für Physik und Astronomie, Universität Potsdam, Karl-Liebknecht-Str. 24/25, 14476 Potsdam (Germany)

2015-02-09

The discovery of ultrafast X-ray induced optical reflectivity changes enabled the development of X-ray/optical cross correlation techniques at X-ray free electron lasers worldwide. We have now linked through experiment and theory the fundamental excitation and relaxation steps with the transient optical properties in finite solid samples. Therefore, we gain a thorough interpretation and an optimized detection scheme of X-ray induced changes to the refractive index and the X-ray/optical cross correlation response.

LNLS soft x-ray spectroscopy (SXS) beamline

International Nuclear Information System (INIS)

Tolentino, Helio; Rocha, Milton C.; Tamura, Edilson; Cezar, Julio C.; Vicentin, Flavio C.; Giles, Carlos; Compagnon-Cailhol, Valerie; Abbate, Miguel; Cruz, Daniela Z.N.; Mocellin, Alexandra

1996-01-01

The Soft X-ray Spectroscopy beamline will be dedicated to the study of structural, electronic and magnetic properties of materials by using photoabsorption and photoemission techniques, X-ray dischroism will be used to study magnetism of transition metals and rare earths compounds. This beamline is one of the first seven beamlines which were decided to start operation along with the storage ring. Part of the beamline - mostly importations - has been granted by fundings from the state of Sao Paulo (Fapesp). The electron energy analyser came through EEC from a cooperation with a French group at LURE. All components of the beamline are either constructed or bougth and being mounted at the storage ring. The monochromator has already been commissioned under UHV, attaining the specification of 5x10 -9 Torr. To cover the whole energy range, from 800 eV up to 4000 eV, many crystals have been bought, cut and tested. The mirror has been specified in order to focus the source in both directions. Simulations using the Shadow code (source simulation and ray tracing technique) were performed in order to optimize the performance of the optics. We expert to focus 10 mrad down to a spot of 3.0x1.5 mm 2 . The mirror chamber has already been constructed and commissioned under UHV conditions (pressure -9 Torr). The mechanics (mechanical feedthroughs, stability, etc..) has been tested using an X-ray source and has been approved. The experimental chamber has already been used for photoemission experiments using a conventional AL/Mg X-ray source. Many results have been obtained and two master thesis have been performed using this set-up. (author)

Soft x-ray measurements on the PLT Tokamak

International Nuclear Information System (INIS)

Von Goeler, S.; Sauthoff, N.; Bitter, M.

1977-10-01

Four experiments are described that currently run on the PLT tokamak and which utilize the soft x-ray emission of the plasma as a diagnostic: the pulse height analysis system for temperature and impurity measurements; the curved crystal Bragg spectrometer for the determination of ionization states of impurities; ''windowless'' surface barrier detectors for the investigation of the ultra soft x-ray radiation in the energy range 0.1 keV < hν < 1 keV and a silicon diode array for x-ray fluctuation measurements. For each diagnostic a short technical description and some recent results obtained with it on PLT are given in order to demonstrate its use

Highly ionized copper contribution to the soft X-ray emission in a plasma focus device

Energy Technology Data Exchange (ETDEWEB)

Zoita, V; Patran, A [Inst. of Physics and Technology of Radiation Devices, Bucharest (Romania); Larour, J [Ecole Polytechnique, Palaiseau (France). Lab. de Physique des Milieux Ionises

1997-12-31

In order to discriminate between the contributions of the gas plasma and of the anode (solid or plasma) to the soft X-ray emission in a plasma focus device, a series of experiments was carried out using the following combinations of experimental conditions: various gases, different absorption filters and viewing different regions in front of the centre electrode. The experiments were performed on the IPF-2/20 plasma focus device using the following working gases: helium, neon and helium-argon mixtures. The diagnostics used: magnetic probe for current derivative, PIN diode for the minimum pinch radius detection, PIN diodes for the soft X-ray emission, scintillator-photomultiplier detector for the hard X-ray emission. From the analysis of the various diagnostics data recorded with very good time correlation, it followed that the soft K-ray signals had a strong contribution from optical transitions of the highly ionised Cu (Cu XX to XXII) emitting in the range 0.8-1.3 nm. (author). 7 figs., 9 refs.

Utilization of synchrotron radiation in analytical chemistry. Soft X-ray emission and absorption spectroscopy

International Nuclear Information System (INIS)

Muramatsu, Yasuji

2015-01-01

Synchrotron soft X-ray spectroscopy includes three major types of spectroscopy such as X-ray absorption spectroscopy (XAS), X-ray emission spectroscopy (XES), and X-ray photoelectron spectroscopy (XPS). This paper takes up XAS and XES of soft X-rays, and briefly describes the principle. XAS is roughly classified into XANES (X-ray absorption near-edge structure) and EXAFS (extended X-ray absorption fine structure), and XANES is mainly used in the analysis based on XAS of soft X-rays. As the examples of the latest soft X-ray analyses, the following are introduced: (1) bandgap of boron implantation diamond and the local structure of boron, (2) catalytic sites in solid fuel cell carbon electrode, and (3) soft X-ray analysis under atmospheric pressure. (A.O.)

Testing warm Comptonization models for the origin of the soft X-ray excess in AGNs

Science.gov (United States)

Petrucci, P.-O.; Ursini, F.; De Rosa, A.; Bianchi, S.; Cappi, M.; Matt, G.; Dadina, M.; Malzac, J.

2018-03-01

The X-ray spectra of many active galactic nuclei (AGNs) show a soft X-ray excess below 1-2 keV on top of the extrapolated high-energy power law. The origin of this component is uncertain. It could be a signature of relativistically blurred, ionized reflection or the high-energy tail of thermal Comptonization in a warm (kT 1 keV), optically thick (τ ≃ 10-20) corona producing the optical/UV to soft X-ray emission. The purpose of the present paper is to test the warm corona model on a statistically significant sample of unabsorbed, radio-quiet AGNs with XMM-Newton archival data, providing simultaneous optical/UV and X-ray coverage. The sample has 22 objects and 100 observations. We use two thermal Comptonization components to fit the broadband spectra, one for the warm corona emission and one for the high-energy continuum. In the optical/UV, we also include the reddening, the small blue bump, and the Galactic extinction. In the X-rays, we include a warm absorber and a neutral reflection. The model gives a good fit (reduced χ2 uniformly distributed in the 0.1-1 keV range, while the optical depth is in the range 10-40. These values are consistent with a warm corona covering a large fraction of a quasi-passive accretion disk, i.e., that mostly reprocesses the warm corona emission. The disk intrinsic emission represents no more than 20% of the disk total emission. According to this interpretation, most of the accretion power would be released in the upper layers of the accretion flow.

Measurement of soft X-ray power from high-power Z-pinch plasma

International Nuclear Information System (INIS)

Wang Wensheng; Qiu Aici; Sun Fengrong; Luo Jianhui; Zhou Haisheng; He Duohui

2003-01-01

A Ni-film bolometer driven by the pulsed constant-voltage supply was developed for measuring soft X-ray energy under 1 keV generated from the Qiang-Guang-I, while the measuring system of the soft X-ray power was established with an X-ray diode detector. Results of the soft X-ray energy and power measurements were obtained at the experiment of Kr gas-puff high-power Z-pinch plasma

X-ray scattering of soft matter

International Nuclear Information System (INIS)

Stribeck, N.

2007-01-01

This coherently written volume summarizes the analytical power of modern X-ray scattering in the field of soft matter. Applications of X-ray scattering to soft matter have advanced considerably within recent years, both conceptually and technically. There are now mature high-power X-ray sources, synchrotrons and rotating anodes, as well as high-speed detectors, which have become readily available and which make the whole process more viable. High-quality time-resolved experiments on polymer structure can now be performed with ease, a major advancement due to the genuine power of the scattering method. This manual is a detailed description of simple tools that can elucidate the mechanisms of structure evolution in the studied materials. It is also a step-by-step guide to more advanced methods of the latest X-ray scattering techniques, and breaks down these methods. Data analysis based on clear, unequivocal results is rendered simple and straightforward - with a stress on the careful planning of experiments and adequate recording of all required data. This book, then, serves as a useful ready-reference guide. It has been written for the modern scientist who is a generalist and needs a concise reference, and demonstrates typical errors in data evaluation. (orig.)

Soft x-ray streak camera for laser fusion applications

International Nuclear Information System (INIS)

Stradling, G.L.

1981-04-01

This thesis reviews the development and significance of the soft x-ray streak camera (SXRSC) in the context of inertial confinement fusion energy development. A brief introduction of laser fusion and laser fusion diagnostics is presented. The need for a soft x-ray streak camera as a laser fusion diagnostic is shown. Basic x-ray streak camera characteristics, design, and operation are reviewed. The SXRSC design criteria, the requirement for a subkilovolt x-ray transmitting window, and the resulting camera design are explained. Theory and design of reflector-filter pair combinations for three subkilovolt channels centered at 220 eV, 460 eV, and 620 eV are also presented. Calibration experiments are explained and data showing a dynamic range of 1000 and a sweep speed of 134 psec/mm are presented. Sensitivity modifications to the soft x-ray streak camera for a high-power target shot are described. A preliminary investigation, using a stepped cathode, of the thickness dependence of the gold photocathode response is discussed. Data from a typical Argus laser gold-disk target experiment are shown

Effects of soft x-ray irradiation on cell ultrastructure

International Nuclear Information System (INIS)

Ford, T.W.; Page, A.M.; Stead, A.D.; Foster, G.F.

1993-01-01

The future of X-ray microscopy lies mainly in its potential for imaging fresh, hydrated biological material at a resolution superior to that of light microscopy. For the image to be accepted as representing the cellular organization of the living cell, it is essential that artifacts are not introduced as a result of the image collection system. One possible source of artifacts is cellular damage resulting from the irradiation of the material with soft X-rays. Cells of the unicellular alga Chlorella have been examined by transmission electron microscopy (TEM) following exposure to different doses of monochromatic (380eV) soft X-rays. Extreme ultrastructural damage has been detected following doses of 10 3 -10 4 Gy, in particular loss of cellular membranes such as the internal thylakoid membranes of the chloroplast. This is discussed in relation to dosage commonly used for imaging by soft X-ray microscopy

Intense soft x-rays from RS Ophiuchi during the 1985 outburst

International Nuclear Information System (INIS)

Mason, K.O.; Cordova, F.A.; Bode, M.F.; Barr, P.

1985-01-01

Intense soft x-ray emission with a characteristic temperature of a few million degrees has been detected from the recurrent nova RS Oph approximately two months after its January 1985 optical outburst. This is the first detection of x-rays from such a system at outburst. The x-radiation is interpreted as emission from circumstellar gas that is shock heated by the passage of the blast wave from the nova explosion. The rapid decline of the x-ray flux between about 60 and 90 days after the outburst probably occurs because the blast wave has reached the edge of the volume filled, between outbursts, by the stellar wind of the red giant component of the binary system. Residual x-ray emission detected from RS Oph 250 days after the outburst is interpreted as coming from the surface of a white dwarf, at a temperature of approx.300,000K, where thermonuclear burning is persisting. 7 refs., 3 figs

The Columbia University proton-induced soft x-ray microbeam.

Science.gov (United States)

Harken, Andrew D; Randers-Pehrson, Gerhard; Johnson, Gary W; Brenner, David J

2011-09-15

A soft x-ray microbeam using proton-induced x-ray emission (PIXE) of characteristic titanium (K(α) 4.5 keV) as the x-ray source has been developed at the Radiological Research Accelerator Facility (RARAF) at Columbia University. The proton beam is focused to a 120 μm × 50 μm spot on the titanium target using an electrostatic quadrupole quadruplet previously used for the charged particle microbeam studies at RARAF. The proton induced x-rays from this spot project a 50 μm round x-ray generation spot into the vertical direction. The x-rays are focused to a spot size of 5 μm in diameter using a Fresnel zone plate. The x-rays have an attenuation length of (1/e length of ~145 μm) allowing more consistent dose delivery across the depth of a single cell layer and penetration into tissue samples than previous ultra soft x-ray systems. The irradiation end station is based on our previous design to allow quick comparison to charged particle experiments and for mixed irradiation experiments.

Soft X-Ray Observations of a Complete Sample of X-Ray--selected BL Lacertae Objects

Science.gov (United States)

Perlman, Eric S.; Stocke, John T.; Wang, Q. Daniel; Morris, Simon L.

1996-01-01

We present the results of ROSAT PSPC observations of the X-ray selected BL Lacertae objects (XBLs) in the complete Einstein Extended Medium Sensitivity Survey (EM MS) sample. None of the objects is resolved in their respective PSPC images, but all are easily detected. All BL Lac objects in this sample are well-fitted by single power laws. Their X-ray spectra exhibit a variety of spectral slopes, with best-fit energy power-law spectral indices between α = 0.5-2.3. The PSPC spectra of this sample are slightly steeper than those typical of flat ratio-spectrum quasars. Because almost all of the individual PSPC spectral indices are equal to or slightly steeper than the overall optical to X-ray spectral indices for these same objects, we infer that BL Lac soft X-ray continua are dominated by steep-spectrum synchrotron radiation from a broad X-ray jet, rather than flat-spectrum inverse Compton radiation linked to the narrower radio/millimeter jet. The softness of the X-ray spectra of these XBLs revives the possibility proposed by Guilbert, Fabian, & McCray (1983) that BL Lac objects are lineless because the circumnuclear gas cannot be heated sufficiently to permit two stable gas phases, the cooler of which would comprise the broad emission-line clouds. Because unified schemes predict that hard self-Compton radiation is beamed only into a small solid angle in BL Lac objects, the steep-spectrum synchrotron tail controls the temperature of the circumnuclear gas at r ≤ 1018 cm and prevents broad-line cloud formation. We use these new ROSAT data to recalculate the X-ray luminosity function and cosmological evolution of the complete EMSS sample by determining accurate K-corrections for the sample and estimating the effects of variability and the possibility of incompleteness in the sample. Our analysis confirms that XBLs are evolving "negatively," opposite in sense to quasars, with Ve/Va = 0.331±0.060. The statistically significant difference between the values for X-ray

Basic X-ray scattering for soft matter

CERN Document Server

De Jeu, Wim H

2016-01-01

X-ray scattering is a well-established technique in materials science. Several excellent textbooks exist in the field, typically written by physicists who use mathematics to make things clear. Often these books do not reach students and scientists in the field of soft matter (polymers, liquid crystals, colloids, and self-assembled organic systems), who usually have a chemical-oriented background with limited mathematics. Moreover, often these people like to know more about x-ray scattering as a technique to be used, but do not necessarily intend to become an expert. This volume is unique in trying to accommodate both points. The aim of the book is to explain basic principles and applications of x-ray scattering in a simple way. The intention is a paperback of limited size that people will like to have on hand rather than on a shelf. Second, it includes a large variety of examples of x-ray scattering of soft matter with, at the end of each chapter, a more elaborate case study. Third, the book contains a separa...

Single order soft X-ray diffraction with quasi-random radius pinhole array spectroscopic photon sieves

International Nuclear Information System (INIS)

Zhang Qiang-Qiang; Wei Lai; Yang Zu-Hua; Qian Feng; Fan Quan-Ping; Zhang Bo; Gu Yu-Qiu; Cao Lei-Feng

2014-01-01

A novel single order diffraction grating in the soft X-ray region, called quasi-random radius pinhole array spectroscopic photon sieves (QRSPS), is proposed in this paper. This new grating is composed of pinholes on a substrate, whose radii are quasi-random, while their centers are regular. Analysis proves that its transmittance function across the grating bar is similar to that of sinusoidal transmission gratings. Simulation results show that the QRSPS can suppress higher-order diffraction effectively. And the QRSPS would still retain its characteristic of single order diffraction when we take the effect of X-ray penetration into account. These properties indicate that the QRSPS can be used in the soft X-ray spectra measurement. (electromagnetism, optics, acoustics, heat transfer, classical mechanics, and fluid dynamics)

Diagnostics for an XUV/soft x-ray laser

International Nuclear Information System (INIS)

Kauffman, R.L.; Matthews, D.L.; Ceglio, N.; Medecki, H.

1984-01-01

We have begun investigating the production of an XUV/soft x-ray laser, using our high-powered glass lasers as drivers. A major diagnostic for lasing is the measure of the absolute power produced in the lasing line. I have developed a spectrograph to time-resolved lasing lines in the energy range from 50 eV to greater than 200 eV. the spectrograph combines a transmission grating and x-ray streak camera to produce a flat field instrument. A cylindrical mirror is used in front of the grating to image the source and act as a collecting optic. The efficiency of the components is calibrated so that absolute intensities can be measured. I will compare the performance of this instrument with reflection grating systems. I will also discuss planned improvements to the system which should increase total throughput, image quality, and resolving power

X-ray beam transfer between hollow fibers for long-distance transport

International Nuclear Information System (INIS)

Tanaka, Yoshihito; Matsushita, Ryuki; Shiraishi, Ryutaro; Hasegawa, Takayuki; Ishikawa, Kiyoshi; Sawada, Kei; Kohmura, Yoshiki; Takahashi, Isao

2016-01-01

Fiber optics for controlling the x-ray beam trajectory has been examined at the synchrotron facility of SPring-8. Up to now, we have achieved beam deflection by several tens of milli-radian and axis shift of around 75 mm with a 1.5 m-long flexible hollow glass capillary. The achievable beam deflecting angle, axis shift, and timing delay are, in principle, proportional to the length, the square of length and the cube of length, respectively. Thus, for further applications, requiring larger beam shift and pulse delay, longer fibers are indispensable. In order to achieve long-distance transport using the fiber, we thus examined the connection transferring x-rays between fibers in an experimental hutch. The acceptance angle at the input end and the throughput efficiency of the second fiber is consistent with the consideration of the output beam divergence of the first fiber. The enhancement of the transfer efficiency is also discussed for the cases of a closer joint and the use of a refractive lens as a coupler.

X-ray beam transfer between hollow fibers for long-distance transport

Energy Technology Data Exchange (ETDEWEB)

Tanaka, Yoshihito, E-mail: tanaka@sci.u-hyogo.ac.jp; Matsushita, Ryuki; Shiraishi, Ryutaro; Hasegawa, Takayuki; Ishikawa, Kiyoshi [Graduate School of Material Science, University of Hyogo, 3-2-1 Kouto, Kamigori-cho, Sayo-gun, Hyogo 678-1297 (Japan); Sawada, Kei; Kohmura, Yoshiki [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5148 (Japan); Takahashi, Isao [Department of Physics, School of Science and Technology, Kwansei Gakuin University, 2-1 Gakuen, Sanda, Hyogo 669-1337 Japan (Japan)

2016-07-27

Fiber optics for controlling the x-ray beam trajectory has been examined at the synchrotron facility of SPring-8. Up to now, we have achieved beam deflection by several tens of milli-radian and axis shift of around 75 mm with a 1.5 m-long flexible hollow glass capillary. The achievable beam deflecting angle, axis shift, and timing delay are, in principle, proportional to the length, the square of length and the cube of length, respectively. Thus, for further applications, requiring larger beam shift and pulse delay, longer fibers are indispensable. In order to achieve long-distance transport using the fiber, we thus examined the connection transferring x-rays between fibers in an experimental hutch. The acceptance angle at the input end and the throughput efficiency of the second fiber is consistent with the consideration of the output beam divergence of the first fiber. The enhancement of the transfer efficiency is also discussed for the cases of a closer joint and the use of a refractive lens as a coupler.

Linac Coherent Light Source soft x-ray materials science instrument optical design and monochromator commissioning

Czech Academy of Sciences Publication Activity Database

Heimann, P.; Krupin, O.; Schlotter, W.F.; Turner, J.; Krzywinski, J.; Sorgenfrei, F.; Messerschmidt, M.; Bernstein, D.; Chalupský, Jaromír; Hájková, Věra; Hau-Riege, S.; Holmes, M.; Juha, Libor; Kelez, N.; Lüning, J.; Nordlund, D.; Perea, M.F.; Scherz, A.; Soufli, R.; Wurth, W.; Rowen, M.

2011-01-01

Roč. 82, č. 9 (2011), 093104/1-093104/8 ISSN 0034-6748 R&D Projects: GA MŠk(CZ) ME10046 Institutional research plan: CEZ:AV0Z10100523 Keywords : diffraction gratings * light sources * linear accelerators * optical materials * x-ray monochromators * x-ray optics Subject RIV: BH - Optics, Masers, Lasers Impact factor: 1.367, year: 2011

Real-time soft x-ray imaging on composite materials

International Nuclear Information System (INIS)

Polichar, R.

1985-01-01

The increased use of composite materials in aircraft structures has emphasized many of the unique and difficult aspects of the inspection of such components. Ultrasound has been extensively applied to certain configurations since it is relatively sensitive to laminar discontinuities in structure. Conversely, the use of conventional x-ray examination has been severely hampered by the fact that these composite materials are virtually transparent to the x-ray energies commonly encountered in industrial radiography (25 kv and above). To produce images with contrast approaching conventional radiography, one must use x-ray beams with average energies below 10 KEV where the absorption coefficients begin to rise rapidly for these low atomic number materials. This new regime of soft x-rays presents a major challenge to real-time imaging components. Special screen and window technology is required if these lower energy x-rays are to be effectively detected. Moreover, conventional x-ray tubes become very inefficient for generating the required x-ray flux at potentials much below 29 kv and the increased operating currents put significant limitations on conventional power sources. The purpose of this paper is to explore these special problems related to soft x-ray real-time imaging and to define the optimal technologies. Practical results obtained with the latest commerical and developmental instruments for real-time imaging will be shown. These instruments include recently developed imaging systems, new x-ray tubes and various approaches to generator design. The measured results convincingly demonstrate the effectiveness practicality of real-time soft x-ray imaging. They also indicate the major changes in technology and approach that must be taken for practical systems to be truly effective

Design calculations for a xenon plasma x-ray shield to protect the NIF optical Thomson scattering diagnostic

Energy Technology Data Exchange (ETDEWEB)

Swadling, G. F.; Ross, J. S.; Datte, P.; Moody, J.; Divol, L.; Jones, O.; Landen, O. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States)

2016-11-15

An Optical Thomson Scattering (OTS) diagnostic is currently being developed for the National Ignition Facility (NIF) at Lawrence Livermore National Laboratory. This diagnostic is designed to make measurements of the hohlraum plasma parameters, such as the electron temperature and the density, during inertial confinement fusion (ICF) experiments. NIF ICF experiments present a very challenging environment for optical measurements; by their very nature, hohlraums produce intense soft x-ray emission, which can cause “blanking” (radiation induced opacity) of the radiation facing optical components. The soft x-ray fluence at the surface of the OTS blast shield, 60 cm from the hohlraum, is estimated to be ∼8 J cm{sup −2}. This is significantly above the expected threshold for the onset of “blanking” effects. A novel xenon plasma x-ray shield is proposed to protect the blast shield from x-rays and mitigate “blanking.” Estimates suggest that an areal density of 10{sup 19} cm{sup −2} Xe atoms will be sufficient to absorb 99.5% of the soft x-ray flux. Two potential designs for this shield are presented.

Rockets for Extended Source Soft X-ray Spectroscopy

Science.gov (United States)

McEntaffer, Randall

The soft X-ray background surrounds our local galactic environment yet very little is known about the physical characteristics of this plasma. A high-resolution spectrum could unlock the properties of this million degree gas but the diffuse, low intensity nature of the background have made it difficult to observe, especially with a dispersive spectrograph. Previous observations have relied on X-ray detector energy resolution which produces poorly defined spectra that are poorly fit by complex plasma models. Here we propose a series of suborbital rocket flights that will begin the characterization of this elusive source through high-resolution X-ray grating spectroscopy. The rocket-based spectrograph can resolve individual emission lines over the soft X-ray band and place tight constraints on the temperature, density, abundance, ionization state and age of the plasma. These payloads will draw heavily from the heritage gained from previous rocket missions, while also benefiting from related NASA technology development programs. The Pennsylvania State University (PSU) team has a history of designing and flying spectrometer components onboard rockets while also being scientific leaders in the field of diffuse soft X-ray astronomy. The PSU program will provide hands-on training of young scientists in the techniques of instrumental and observational X-ray astronomy. The proposed rocket program will also expose these researchers to a full experiment cycle: design, fabrication, tolerance analysis, assembly, flight-qualification, calibration, integration, launch, and data analysis; using a combination of technologies suitable for adaptation to NASA's major missions. The PSU program in suborbital X-ray astronomy represents an exciting mix of compelling science, heritage, cutting-edge technology development, and training of future scientists.

Update on VUV and soft X-ray facilities at SSRL

International Nuclear Information System (INIS)

Waldhauer, A.

1988-01-01

The number of experimental stations at SSRL devoted to the VUV and soft X-ray region is increasing rapidly. In 1986 there were five VUV/soft X-ray beam lines in regular operation. These consisted of two grasshopper lines, a Seya-Namioka line, a white light lithography line, and the UHV double crystal line, Jumbo. By 1988 ten beam lines, including two with insertion devices, covering the spectral range 5-4000 eV in five overlapping ranges will be operational. With the addition of these new stations, SSRL will have increased dramatically its facilities for performing VUV and soft X-ray research. (orig.)

Soft X-ray excited colour-centre luminescence and XANES studies of calcium oxide

International Nuclear Information System (INIS)

Ko, J.Y.P.; Heigl, F.; Yiu, Y.M.; Zhou, X.-T.; Regier, T.; Blyth, R.I.R.; Sham, T.-K.

2007-01-01

In this study, we show that colour centres can be produced by irradiating calcium oxide with soft X-rays from a synchrotron radiation source. Using the X-ray excited optical Iuminescence (XEOL) technique, two colour centres, F-centre, and F + -centre can be identified. These colour centres emit photons at characteristic wavelengths. In addition, by performing time-resolved XEOL (TRXEOL), we are able to reveal timing and decay characteristics of the colour centres. We also present X-ray absorption near-edge structure (XANES) spectra collected across oxygen K-edge, calcium L 3,2 -edge, and calcium K-edge. Experimental results are compared with density functional theory (DFT) calculations. (author)

Reflection of femtosecond pulses from soft X-ray free-electron laser by periodical multilayers

Energy Technology Data Exchange (ETDEWEB)

Ksenzov, D.; Grigorian, S.; Pietsch, U. [Faculty of Physics, University of Siegen (Germany); Hendel, S.; Bienert, F.; Sacher, M.D.; Heinzmann, U. [Faculty of Physics, University of Bielefeld (Germany)

2009-08-15

Recent experiments on a soft X-ray free-electron laser (FEL) source (FLASH in Hamburg) have shown that multilayers (MLs) can be used as optical elements for highly intense X-ray irradiation. An effort to find most appropriate MLs has to consider the femtosecond time structure and the particular photon energy of the FEL. In this paper we have analysed the time response of 'low absorbing' MLs (e.g. such as La/B{sub 4}C) as a function of the number of periods. Interaction of a pulse train of Gaussian shaped sub-pulses using a realistic ML grown by electron-beam evaporation technique has been analysed in the soft-X-ray range. The structural parameters of the MLs were obtained by reflectivity measurements at BESSY II and subsequent profile fittings. (Abstract Copyright [2009], Wiley Periodicals, Inc.)

Fiber optics in adverse environments

International Nuclear Information System (INIS)

Lyous, P.B.

1982-01-01

Radiation effects in optical fibers are considered, taking into account recent progress in the investigation of radiation resistant optical fibers, radiation damage in optical fibers, radiation-induced transient absorption in optical fibers, X-ray-induced transient attenuation at low temperatures in polymer clad silica (PCS) fibers, optical fiber composition and radiation hardness, the response of irradiated optical waveguides at low temperatures, and the effect of ionizing radiation on fiber-optic waveguides. Other topics explored are related to environmental effects on components of fiber optic systems, and radiation detection systems using optical fibers. Fiber optic systems in adverse environments are also discussed, giving attention to the survivability of Army fiber optics systems, space application of fiber optics systems, fiber optic wavelength multiplexing for civil aviation applications, a new fiber optic data bus topology, fiber optics for aircraft engine/inlet control, and application of fiber optics in high voltage substations

Soft X-Ray amplification in laser plasmas

International Nuclear Information System (INIS)

Louis-Jacquet, M.

1988-01-01

The principles, experiments and theoretical models of soft x-ray, amplification, produced in laser plasmas, are studied. In the discussion of the principles, the laser plasma medium, the definition of the gain, the population inversions, saturation and superradiance are described. The results concerning recombination and collisional excitation experiments, as well as experimental devices are shown. A complete physical simulation to design and interpret x-ray laser experiments is given. Applications of x-ray lasers in grating production techniques, in contact microscopy and holography are considered

Soft X-ray imaging techniques for calculating the Earth's dayside boundaries

Science.gov (United States)

Connor, Hyunju; Kuntz, Kip; Sibeck, David; Collier, Michael; Aryan, Homayon; Branduardi-Raymont, Graziella; Collado-Vega, Yaireska; Porter, Frederick; Purucker, Michael; Snowden, Steven; Raeder, Joachim; Thomas, Nicholas; Walsh, Brian

2016-04-01

Charged particles and neutral atoms exchange electrons in many space plasma venues. Soft X-rays are emitted when highly charged solar wind ions, such as C6+. O7+, and Fe13+, interact with Hydrogen and Helium atoms. Soft X-ray images can be a powerful technique to remotely probe the plasma and neutral density structures created when the solar wind interacts with planetary exospheres, such as those at the Earth, Moon, Mars, Venus, and comets. The recently selected ESA-China joint spacecraft mission, "Solar wind - Magnetosphere - Ionosphere Link Explorer (SMILE)" will have a soft X-ray imager on board and provide pictures of the Earth's dayside system after its launch in 2021. In preparation for this future mission, we simulate soft X-ray images of the Earth's dayside system, using the OpenGGCM global magnetosphere MHD model and the Hodges model of the Earth's exosphere. Then, we discuss techniques to determine the location of the Earth's dayside boundaries (bow shock and magnetopause) from the soft X-ray images.

Soft x-ray circular dichroism of biomolecules

International Nuclear Information System (INIS)

Nakagawa, Kazumichi; Tanaka, Makoto; Agui, Akane

2005-01-01

We succeeded to observe natural circular dichroism NCD for biomolecules in soft X-ray region for the first time. Evaporated films of amino acids, phenylalanine (phe) and serine (ser) were prepared in vacuum with the thickness of about 300 nm. Measurement was carried out at the soft X-ray undulator beamline BL23SU of the Spring-8, where left- and right-circularly polarized light (LCPL and RCPL) was available from an APPLE-2 undulator. Difference spectra DA(hν) was plotted as a function of photon energy hν of soft X-ray to be the difference between absorption coefficient A L for LCPL and absorption coefficient A R for RCPL, namely, DA(hν) ≡ A L (hν) - A R (hν). Values of A L and A R were determined by means of the photoelectric drain current measurement. In the DA(hν) spectra for L-phe films, negative peak was observed at 407 eV. On the contrary, for D-phe films, positive peak was observed at 407 eV with the same magnitude but opposite sign. Moreover, no signal was observed for racemic phenylalanine (DL-phe). In the wavelength region of visible to ultraviolet, there is well-known general law in which NCD signals for D- and L-enantiomers are the same magnitude but opposite sign and racemic compound does not show NCD spectra. Characteristic features in DA(hν) spectra of the L-phe, D-phe and DL-phe were of good agreement with this well-known general law. Based on this good agreement, we concluded that peaks at 407 eV in the DA(hν) spectra are true NCD peaks. For ser films, we assigned peaks at 540 eV and 548 eV to be NCD peaks in the same manner. We hope that our first observation of NCD for biomolecules at soft X-ray region will open new science and technologies such as basic science including elucidation of fundamental mechanism of NCD and application to manipulate biomolecules using circularly polarized soft X-ray beams. (author)

Spectral evolution of soft x-ray emission from optically thin, high electron temperature platinum plasmas

Directory of Open Access Journals (Sweden)

Hiroyuki Hara

2017-08-01

Full Text Available The soft x-ray spectra of heavy element plasmas are frequently dominated by unresolved transition array (UTA emission. We describe the spectral evolution of an intense UTA under optically thin conditions in platinum plasmas. The UTA was observed to have a peak wavelength around 4.6 nm at line-of-sight averaged electron temperatures less than 1.4 keV at electron densities of (2.5–7.5 × 1013 cm−3. The UTA spectral structure was due to emission from 4d–4f transitions in highly charged ions with average charge states of q = 20–40. A numerical simulation successfully reproduced the observed spectral behavior.

Time-dependent nonequilibrium soft x-ray response during a spin crossover

Energy Technology Data Exchange (ETDEWEB)

van Veenendaal, Michel

2018-03-01

The rapid development of high-brilliance pulsed X-ray sources with femtosecond time resolution has created a need for a better theoretical understanding of the time-dependent soft-X-ray response of dissipative many-body quantum systems. It is demonstrated how soft-X-ray spectroscopies, such as X-ray absorption and resonant inelastic X-ray scattering at transition-metal L-edges, can provide insight into intersystem crossings, such as a spin crossover. The photoinduced doublet-to-quartet spin crossover on cobalt in Fe-Co Prussian blue analogues is used as an example to demonstrate how the X-ray response is affected by the dissipative nonequilibrium dynamics. The time-dependent soft-X-ray spectra provide a wealth of information that reflect the changes in the nonequilibrium initial state via continuously changing spectral lineshapes that cannot be decomposed into initial photoexcited and final metastable spectra, strong broadenings, a collapse of clear selection rules during the intersystem crossing, strong fluctuations in the isotropic branching ratio in X-ray absorption, and crystal-field collapse/oscillations and strongly time-dependent anti-Stokes processes in RIXS.

Test facility for astronomical x-ray optics

DEFF Research Database (Denmark)

Christensen, Finn Erland; Lewis, Robert A.; Bordas, J.

1990-01-01

Grazing incidence x-ray optics for x-ray astronomical applications are used outside the earth's atmosphere. These devices require a large collection aperture and the imaging of an x-ray source that is essentially placed at infinity. The ideal testing system for these optical elements has to appro......Grazing incidence x-ray optics for x-ray astronomical applications are used outside the earth's atmosphere. These devices require a large collection aperture and the imaging of an x-ray source that is essentially placed at infinity. The ideal testing system for these optical elements has...... to approximate that encountered under working conditions; however, the testing of these optical elements is notoriously difficult with conventional x-ray generators. Synchrotron radiation (SR) sources are sufficiently brilliant to produce a nearly perfect parallel beam over a large area while still retaining...... a flux considerably higher than that available from conventional x-ray generators. A facility designed for the testing of x-ray optics, particularly in connection with x-ray telescopes, is described. It is proposed that this facility will be accommodated at the Synchrotron Radiation Source...

Homogenious focusing with a transient soft X-ray laser for irradiation experiments

Czech Academy of Sciences Publication Activity Database

Kazamias, S.; Cassou, K.; Guilbaud, O.; Klisnick, A.; Ros, D.; Plé, F.; Jamelot, G.; Rus, Bedřich; Kozlová, Michaela; Stupka, Michal; Mocek, Tomáš; Douillet, D.; Zeitoun, P.; Joyeux, D.; Phalippou, D.

2006-01-01

Roč. 263, - (2006), s. 98-104 ISSN 0030-4018 R&D Projects: GA MŠk(CZ) LC528; GA ČR GA202/05/2316 Institutional research plan: CEZ:AV0Z10100523 Keywords : soft X-Ray laser * focusing * laser plasma * UV radiation * beam profile Subject RIV: BH - Optics, Masers, Lasers Impact factor: 1.480, year: 2006

Linear luminescence for thin plastic scintillator under intense soft X-ray irradiation

International Nuclear Information System (INIS)

Ning Jiamin; Jiang Shilun; Xu Rongkun; Guo Cun

2006-01-01

The basic principle of soft X-ray power meter is introduced in the paper and the experimental process and the result of thin plastic scintillator linear luminescence under intense soft X-ray irradiation are described. A range of flux density of energy for thin plastic scintillator linear luminescence under intense soft X-ray irradiation is included. The upper limit of the flux density is 1.47 x 10 5 W/cm 2 . (authors)

The whispering gallery as an optical component in the X-ray region

International Nuclear Information System (INIS)

Howells, M.R.

1995-08-01

The whispering gallery phenomenon in acoustics has been known and studied for more than a century, and the same effect has been observed to take place with waves other than sound waves. In this paper we review the theoretical basis and attractive features of the whispering gallery as a soft x-ray optical component and indicate some of its potential applications. We then describe what may be its most unique capability which, in favorable cases, is to provide a way. to manipulate the phase difference between the s and p polarization components and thus to generate circularly or elliptically polarized soft x-rays

Demonstration of soft x-ray amplification by optical-field-induced ionization

International Nuclear Information System (INIS)

Midorikawa, Katsumi; Nagata, Yutaka; Kubodera, Shoichi; Obara, Minoru; Tashiro, Hideo; Toyoda, Koichi

1995-01-01

We have demonstrated the amplification of the 13.5-nm Lyman-α transition in hydrogen-like Li + ions, using a novel optical-field-induced ionization. A small-signal gain coefficient of 20 cm -1 was obtained. The use of preformed Li + plasma as an initial laser medium plays important roles for the production of suitable plasma conditions for an optical-field-induced ionization x-ray laser. (author)

Development of small scale soft x-ray lasers: Aspects of data interpretation

International Nuclear Information System (INIS)

Skinner, C.H.; Kim, D.; Voorhees, D.; Suckewer, S.

1990-02-01

The widespread application of soft x-ray laser technology is contingent on the development of small scale soft x-ray lasers that do not require large laser facilities. Progress in the development of soft x-ray lasers pumped by a Nd laser of energy 6-12J is reported below. Some aspects of data interpretation and gain measurements in such systems are discussed. 11 refs., 11 figs

Complex optical/UV and X-ray variability of the Seyfert 1 galaxy 1H 0419-577

Science.gov (United States)

Pal, Main; Dewangan, Gulab C.; Kembhavi, Ajit K.; Misra, Ranjeev; Naik, Sachindra

2018-01-01

We present detailed broad-band UV/optical to X-ray spectral variability of the Seyfert 1 galaxy 1H 0419-577 using six XMM-Newton observations performed during 2002-2003. These observations covered a large amplitude variability event in which the soft X-ray (0.3-2 keV) count rate increased by a factor of ∼4 in six months. The X-ray spectra during the variability are well described by a model consisting of a primary power law, blurred and distant reflection. The 2-10 keV power-law flux varied by a factor of ∼7 while the 0.3-2 keV soft X-ray excess flux derived from the blurred reflection component varied only by a factor of ∼2. The variability event was also observed in the optical and UV bands but the variability amplitudes were only at the 6-10 per cent level. The variations in the optical and UV bands appear to follow the variations in the X-ray band. During the rising phase, the optical bands appear to lag behind the UV band but during the declining phase, the optical bands appear to lead the UV band. Such behaviour is not expected in the reprocessing models where the optical/UV emission is the result of reprocessing of X-ray emission in the accretion disc. The delayed contribution of the broad emission lines in the UV band or the changes in the accretion disc/corona geometry combined with X-ray reprocessing may give rise to the observed behaviour of the variations.

Miniature x-ray point source for alignment and calibration of x-ray optics

International Nuclear Information System (INIS)

Price, R.H.; Boyle, M.J.; Glaros, S.S.

1977-01-01

A miniature x-ray point source of high brightness similar to that of Rovinsky, et al. is described. One version of the x-ray source is used to align the x-ray optics on the Argus and Shiva laser systems. A second version is used to determine the spatial and spectral transmission functions of the x-ray optics. The spatial and spectral characteristics of the x-ray emission from the x-ray point source are described. The physical constraints including size, intensity and thermal limitations, and useful lifetime are discussed. The alignment and calibration techniques for various x-ray optics and detector combinations are described

Soft x-ray interferometry

International Nuclear Information System (INIS)

1993-09-01

The purpose of the soft x-ray interferometry workshop held at Lawrence Berkeley Laboratory was to discuss with the scientific community the proposed technical design of the soft x-ray Fourier-transform spectrometer being developed at the ALS. Different design strategies for the instrument's components were discussed, as well as detection methods, signal processing issues, and how to meet the manufacturing tolerances that are necessary for the instrument to achieve the desired levels of performance. Workshop participants were encouraged to report on their experiences in the field of Fourier transform spectroscopy. The ALS is developing a Fourier transform spectrometer that is intended to operate up to 100 eV. The motivation is solely improved resolution and not the throughput (Jaquinot) or multiplex (Fellgett) advantage, neither of which apply for the sources and detectors used in this spectral range. The proposed implementation of this is via a Mach-Zehnder geometry that has been (1) distorted from a square to a rhombus to get grazing incidence of a suitable angle for 100 eV and (2) provided with a mirror-motion system to make the path difference between the interfering beams tunable. The experiment consists of measuring the emergent light intensity (I(x)) as a function of the path difference (x). The resolving power of the system is limited by the amount of path difference obtainable that is 1 cm (one million half-waves at 200 angstrom wavelength) in the design thus allowing a resolving power of one million. The free spectral range of the system is limited by the closeness with which the function I(x) is sampled. It is proposed to illuminate a helium absorption cell with roughly 1%-band-width light from a monochromator thus allowing one hundred aliases without spectral overlap even for sampling of I(x) at one hundredth of the Nyquist frequency

Progress in compact soft x-ray lasers and their applications

International Nuclear Information System (INIS)

Suckewer, S.; Skinner, C.H.

1995-01-01

The ultra-high brightness and short pulse duration of soft x-ray lasers provide unique advantages for novel applications. A crucial factor in the availability of these devices is their scale and cost. Recent breakthroughs in this field has brought closer the advent of table-top devices, suitable for applications to fields such as x-ray microscopy, chemistry, material science, plasma diagnostics, and lithography. In this article we review recent progress in the development of compact (table-top) soft x-ray lasers

Nano-fabrication of diffractive optics for soft X-ray and atom beam focusing

International Nuclear Information System (INIS)

Rehbein, S.

2002-01-01

Nano-structuring processes are described for manufacturing diffractive optics for the condenser-monochromator set-up of the transmission X-ray microscope (TXM) and for the scanning transmission X-ray microscope (STXM) at the BESSY II electron storage ring in Berlin. Furthermore, a process for manufacturing free-standing nickel zone plates for helium atom beam focusing experiments is presented. (author)

Analysis of neon soft x-ray spectra from short-pulse laser-produced plasmas

International Nuclear Information System (INIS)

Abare, A.C.; Keane, C.J.; Crane, J.K.; DaSilva, L.B.; Lee, R.W.; Perry, M.D.; Falcone, R.W.

1993-04-01

We report preliminary results from the analysis of streaked soft x-ray neon spectra a gas jet target. In obtained from the interaction of a picosecond Nd:glass laser with these experiments streaked spectra show prompt harmonic emission followed by longer time duration soft x-ray line emission. The majority of the line emission observed was found to originate from Li- and Be-like Ne and the major transitions in the observed spectra have been identified. Li-like emission lines were observed to decay faster in time than Be-like transitions, suggesting that recombination is taking place. Line ratios of n=4-2 and n=3-2 transitions supported the view that these lines were optically thin and thick, respectively. The time history of Li-like Ne 2p-4d and 2p-3d lines is in good agreement with a simple adiabatic expansion model coupled to a time dependent collisional-radiative code. Further x-ray spectroscopic analysis is underway which is aimed at diagnosing plasma conditions and assessing the potential of this recombining neon plasma as a quasi-steady-state recombination x-ray laser medium

The possible effect of solar soft X rays on thermospheric nitric oxide

International Nuclear Information System (INIS)

Siskind, D.E.; Barth, C.A.; Cleary, D.D.

1990-01-01

A rocket measurement of thermospheric nitric oxide (NO) is used to evaluate the production of odd nitrogen by solar soft X rays (18-50 angstrom). The rocket observation was performed over White Sands Missile Range on November 9, 1981, at 1500 LT for solar maximum conditions (F10.7 = 233). The peak observed NO density was 6.3 x 10 7 cm -3 at 102 km. A photochemical model which included soft X rays was used for comparison with the data. The soft X rays create photoelectrons which lead to enhanced ionization of N 2 and thus increased odd nitrogen production. A good fit to the data was achieved using a soft X ray flux of 0.75 erg cm -2 s -1

Adjustable Grazing-Incidence X-Ray Optics

Science.gov (United States)

O'Dell, Stephen L.; Reid, Paul B.

2015-01-01

With its unique subarcsecond imaging performance, NASA's Chandra X-ray Observatory illustrates the importance of fine angular resolution for x-ray astronomy. Indeed, the future of x-ray astronomy relies upon x-ray telescopes with comparable angular resolution but larger aperture areas. Combined with the special requirements of nested grazing-incidence optics, mass, and envelope constraints of space-borne telescopes render such advances technologically and programmatically challenging. The goal of this technology research is to enable the cost-effective fabrication of large-area, lightweight grazing-incidence x-ray optics with subarcsecond resolution. Toward this end, the project is developing active x-ray optics using slumped-glass mirrors with thin-film piezoelectric arrays for correction of intrinsic or mount-induced distortions.

Detection of gamma rays using scintillation optical fibers

International Nuclear Information System (INIS)

Park, J. W.; Hong, S. B.

2002-01-01

Scintillating optical fibers have several advantages over other conventional materials used for radiation detection. We have used glass and plastic scintillating fibers to detect gamma rays emitted from 60 Co and 137 Cs, and beta rays from 90 Sr. The sensors are constructed of single strand or multi-strand fibers of 1 mm diameter. The glass scintillating fiber used contains cerium-activated lithium-silicate as scintillating material and the plastic scintillating fiber used is Bicron model BCF-12. In this paper, we report the pulse-height spectra obtained by both sensor types, and analyze them in the aspect of their usability for radiation detectors. Our investigation suggests that the glass fiber can be used to develop gamma ray detectors which will function in high and low gamma ray flux environments. Use of the sensor for the beta ray detection was not satisfactory. The plastic fiber sensor did not work satisfactorily for the weak gamma sources, but did produce somewhat promising results. The scintillating plastic fiber offers some feasibility as beta ray sensor material

Depth Probing Soft X-ray Microprobe (DPSXRM) for High Resolution Probing of Earth's Microstructural Samples

Science.gov (United States)

Dikedi, P. N.

2015-12-01

The Cambrian explosion; occurrence of landslides in very dry weather conditions; rockslides; dead, shriveled-up and crumbled leaves possessing fossil records with the semblance of well preserved, flat leaves; abundance of trilobite tracks in lower and higher rock layers; and sailing stones are enigmas demanding demystifications. These enigmas could be elucidated when data on soil structure, texture and strength are provided by some device with submicrometre accuracy; for these and other reasons, the design of a Depth Probing Soft X-ray Microprobe (DPSXRM), is being proposed; it is expected to deliver soft X-rays, at spatial resolution, ϛ≥600nm and to probe at the depth of 0.5m in 17s. The microprobe is portable compared to a synchrotron radiation facility (Diamond Light Source has land size of 43,300m2); spatial resolution,ϛ , of the DPSXRM surpasses those of the X-ray Fluorescence microanalysis (10µm), electron microprobe (1-3µm) and ion microprobe (5->30µm); the DPSXRM has allowance for multiple targets. Vanadium and Manganese membranes are proposed owing to respective 4.952KeV VKα1 and 5.899KeV MnKα1 X-rays emitted, which best suits micro-probing of Earth's microstructural samples. Compound systems like the Kirk-Patrick and Baez and Wolter optics, aspheric mirrors like elliptical and parabolic optics, small apertures and Abbe sine condition are employed to reduce or remove astigmatism, obliquity, comatic and spherical aberrations—leading to good image quality. Results show that 5.899KeV MnKα1 and 4.952KeV VKα1 soft X-rays will travel a distance of 2.75mm to form circular patches of radii 2.2mm and 2.95mm respectively. Zone plate with nth zone radius of 1.5mm must be positioned 1.5mm and 2mm from the electron gun if circular patches must be formed from 4.952KeV VKα1 and 5.899KeV MnKα1 soft X-rays respectively. The focal lengths of 0.25μm≤ƒ≤1.50μm and 0.04μm≤ƒ≤0.2μm covered by 4.952KeV VKα1 and 5.899KeV Mn Kα1 soft X-Rays, will

Polycapillary x-ray optics for macromolecular crystallography

International Nuclear Information System (INIS)

Owens, S.M.; Gibson, W.M.; Carter, D.C.; Sisk, R.C.; Ho, J.X.

1996-01-01

Polycapillary x-ray optics have found potential application in many different fields, including antiscatter and magnification in mammography, radiography, x-ray fluorescence, x-ray lithography, and x-ray diffraction techniques. In x-ray diffraction, an optic is used to collect divergent x-rays from a point source and redirect them into a quasi-parallel, or slightly focused beam. Monolithic polycapillary optics have been developed recently for macromolecular crystallography and have already shown considerable gains in diffracted beam intensity over pinhole collimation. Development is being pursued through a series of simulations and prototype optics. Many improvements have been made over the stage 1 prototype reported previously, which include better control over the manufacturing process, reducing the diameter of the output beam, and addition of a slight focusing at the output of the optic to further increase x-ray flux at the sample. The authors report the characteristics and performance of the stage 1 and stage 2 optics

Fabrication of the multilayer beam splitters with large area for soft X-ray laser interferometer

International Nuclear Information System (INIS)

Wang Zhanshan; Zhang Zhong; Wang Fengli; Wu Wenjuan; Wang Hongchang; Qin Shuji; Chen Lingyan

2004-01-01

The soft X-ray laser Mach-Zehnder interferometer is an important tool to measure the electron densities of a laser-produced plasma near the critical surface. The design of a multilayer beam splitter at 13.9 nm for soft X-ray laser Mach-Zehnder interferometer is completed based on the standard of maximizing product of reflectivity and transmission of the beam splitter. The beam splitters which is Mo/Si multilayers on 10 mm x 10 mm area Si 3 N 4 membrane are fabricated using the magnetron sputtering. The figure error of the beam splitter has reached the deep nanometer magnitude by using optical profiler and the product of reflectivity and transmission measured by synchrotron radiation is up to to 4%. (authors)

Efficient 'water window' soft x-ray high-Z plasma source

International Nuclear Information System (INIS)

Higashiguchi, T; Otsuka, T; Jiang, W; Endo, A; Li, B; Dunne, P; O'Sullivan, G

2013-01-01

Unresolved transition array (UTA) is scalable to shorter wavelengths, and we demonstrate a table-top broadband emission 'water window' soft x-ray source based on laser-produced plasmas. Resonance emission from multiply charged ions merges to produce intense UTAs in the 2 to 4 nm region, extending below the carbon K edge (4.37 nm). An outline of a microscope design for single-shot live cell imaging is proposed based on a bismuth (Bi) plasma UTA source, coupled to multilayer mirror optics

Thin Films for X-ray Optics

Science.gov (United States)

Conley, Raymond

Laue lens, however my advancements in MLL fabrication technology led to new generations of deposition instruments that were better suited. In order to re-purpose the APS Rotary Deposition System, a concept to upgrade the machine with a suborbital planetary is discussed. The APS Modular Deposition System (MDS) is the state of the art instrument that was designed to keep APS at the forefront of x-ray optics technology for the foreseeable future. By including flexibility in the design, the machine is ideally suited for research on all types of multilayers and thin-films for x-ray optics applications. A new method for in-situ surface metrology is presented which relies on the infrastructure provided by the MDS. The chapter concludes with discussion on several types of reflective multilayers that span a broad range of x-ray wavelengths, from soft x-rays (below 5-10 keV) to hard x-rays (above 5-10keV). A method for fabrication of precision elliptically-figured mirrors called profile coating (conceived at the APS) is covered in Chapter 3. Profile-coating is a technique where a specially shaped mask is designed to partially obscure the sputtering source in order to produce a coating with a specially defined film thickness profile perpendicular to substrate translation. Source shape modeling and mask calculation is presented. Initially, Au was used as the filler material for profile coating, however I found that Pt offered better performance. Rh has also been used to fabricate profile-coated KB mirrors. Performance and commissioning results for the APS profile-coating deposition system (another machine designed by myself) is included. Chapter 4 covers my work on multilayer Laue lens. Motivation and current status are presented, and the nomenclature we devised to name the various MLL types is listed. Following this, a theoretical overview is provided. Important advancements I have spearhead in this field are included, such as the introduction of metal silicides, reactive

Grazing Incidence Wavefront Sensing and Verification of X-Ray Optics Performance

Science.gov (United States)

Saha, Timo T.; Rohrbach, Scott; Zhang, William W.

2011-01-01

Evaluation of interferometrically measured mirror metrology data and characterization of a telescope wavefront can be powerful tools in understanding of image characteristics of an x-ray optical system. In the development of soft x-ray telescope for the International X-Ray Observatory (IXO), we have developed new approaches to support the telescope development process. Interferometrically measuring the optical components over all relevant spatial frequencies can be used to evaluate and predict the performance of an x-ray telescope. Typically, the mirrors are measured using a mount that minimizes the mount and gravity induced errors. In the assembly and mounting process the shape of the mirror segments can dramatically change. We have developed wavefront sensing techniques suitable for the x-ray optical components to aid us in the characterization and evaluation of these changes. Hartmann sensing of a telescope and its components is a simple method that can be used to evaluate low order mirror surface errors and alignment errors. Phase retrieval techniques can also be used to assess and estimate the low order axial errors of the primary and secondary mirror segments. In this paper we describe the mathematical foundation of our Hartmann and phase retrieval sensing techniques. We show how these techniques can be used in the evaluation and performance prediction process of x-ray telescopes.

Soft X-ray imaging by optically stimulated luminescence from color centers in lithium fluoride

Energy Technology Data Exchange (ETDEWEB)

Bonfigli, F. [ENEA, C.R. Frascati, Via E. Fermi, 45, 00044 Frascati (Rome) (Italy)], E-mail: bonfigli@frascati.enea.it; Almaviva, S.; Baldacchini, G.; Bollanti, S.; Flora, F.; Lai, A.; Montereali, R.M. [ENEA, C.R. Frascati, Via E. Fermi, 45, 00044 Frascati (Rome) (Italy); Nichelatti, E. [ENEA, C.R. Casaccia, Via Anguillarese 301, 00060 S.Maria di Galeria (Rome) (Italy); Tomassetti, G.; Ritucci, A.; Reale, L. [Universita de L' Aquila e INFN, Dip. di Fisica, Coppito, L' Aquila (Italy); Faenov, A. Ya.; Pikuz, T.A. [MISDC of VNIIFTRI Mendeleevo, Moscow region, 141570 (Russian Federation); Larciprete, R. [ISC-CNR, Sezione Montelibretti, Via Salaria, Km. 29.3, 00016 Monterotondo Scalo (Rome) (Italy); Gregoratti, L.; Kiskinova, M. [Sincrotrone Trieste, S. S. 14, Km. 163.5, 34012 Basovizza (TS) (Italy)

2007-07-15

An innovative X-ray imaging detector based on Optically Stimulated Luminescence from color centers in lithium fluoride is presented. Regular photoluminescent patterns produced on LiF samples by different intense X-ray sources, like synchrotrons, laser plasma sources and a capillary discharge laser have been investigated by a Confocal Laser Scanning Microscope. The use of a LiF-based imaging plate for X-ray microscopy is also discussed showing microradiographies of small animals.

Evaluation of moisture content distribution in wood by soft X-ray imaging

International Nuclear Information System (INIS)

Tanaka, T.; Avramidis, S.; Shida, S.

2009-01-01

A technique for nondestructive evaluation of moisture content distribution of Japanese cedar (sugi) during drying using a newly developed soft X-ray digital microscope was investigated. Radial, tangential, and cross-sectional samples measuring 100 x 100 x 10 mm were cut from green sugi wood. Each sample was dried in several steps in an oven and upon completion of each step, the mass was recorded and a soft X-ray image was taken. The relationship between moisture content and the average grayscale value of the soft X-ray image at each step was linear. In addition, the linear regressions overlapped each other regardless of the sample sections. These results showed that soft X-ray images could accurately estimate the moisture content. Applying this relationship to a small section of each sample, the moisture content distribution was estimated from the image differential between the soft X-ray pictures obtained from the sample in question and the same sample in the oven-dried condition. Moisture content profiles for 10-mm-wide parts at the centers of the samples were also obtained. The shapes of the profiles supported the evaluation method used in this study

Feasibility Study on Fiber-optic Radiation Sensor for Remote Gamma-ray Spectroscopy

International Nuclear Information System (INIS)

Jeon, Hyesu; Jang, Kyoung Won; Shin, Sang Hun and others

2014-01-01

In this study, we fabricated a fiber-optic radiation sensor using an optical fiber and various scintillators. To select an adequate inorganic scintillator for the sensing probe of fiber-optic radiation sensor, 5 types of scintillators were evaluated. The spectra of gamma-rays emitted from a Na-22 radiation source were measured by using the manufactured sensors. As a result, the BGO was suitable for the sensing probe of fiber-optic radiation sensor due to its high scintillation output and exact photoelectric peak for the gamma-ray energy. The basic principle of radiation detection is to detect the signals caused by interactions between radiations and materials. There are various types of radiation detectors depending on types of radiation to be detected and physical quantities to be measured. As one of the radiation detectors, a fiber-optic radiation sensor using a scintillator and an optical fiber has two advantages such as no space restraint and remote sensing. Moreover, in nuclear environments, this kind of sensor has immunities for electromagnetic field, temperature, and pressure. Thus, the fiber-optic radiation sensor can be used in various fields including nondestructive inspection, radioactive waste management, nuclear safety, radiodiagnosis and radiation therapy. As a fundamental study of the fiber-optic radiation sensor for remote gamma-ray spectroscopy, in this study, we fabricated a fiber-optic radiation sensor using an optical fiber and various scintillators. To select an adequate inorganic scintillator for the sensing probe of fiber-optic radiation sensor, 5 types of scintillators were evaluated. The spectra of gamma-rays emitted from a Na-22 radiation source were measured by using the manufactured sensors

CVD diamond based soft X-ray detector with fast response

International Nuclear Information System (INIS)

Li Fang; Hou Lifei; Su Chunxiao; Yang Guohong; Liu Shenye

2010-01-01

A soft X-ray detector has been made with high quality chemical vapor deposited (CVD) diamond and the electrical structure of micro-strip. Through the measurement of response time on a laser with the pulse width of 10 ps, the full width at half maximum of the data got in the oscilloscope was 115 ps. The rise time of the CVD diamond detector was calculated to be 49 ps. In the experiment on the laser prototype facility, the signal got by the CVD diamond detector was compared with that got by a soft X-ray spectrometer. Both signals coincided well. The detector is proved to be a kind of reliable soft X-ray detector with fast response and high signal-to-noise ratio. (authors)

Absolute pulse energy measurements of soft x-rays at the Linac Coherent Light Source

Czech Academy of Sciences Publication Activity Database

Tiedtke, K.; Sorokin, A. A.; Jastrow, U.; Juranić, P.; Kreis, S.; Gerken, N.; Richter, M.; Arp, U.; Feng, Y.; Nordlund, D.; Soufli, R.; Fernández-Perea, M.; Juha, Libor; Heimann, P.; Nagler, B.; Lee, H.J.; Mack, S.; Cammarata, M.; Krupin, O.; Messerschmidt, M.; Holmes, M.; Rowen, M.; Schlotter, W.; Moeller, S.; Turner, J.J.

2014-01-01

Roč. 22, č. 18 (2014), s. 21214-21226 ISSN 1094-4087 R&D Projects: GA MŠk(CZ) LG13029 Institutional support: RVO:68378271 Keywords : soft x-ray * free electron laser * LCLS * instrumentation * measurement * metrology Subject RIV: BH - Optics, Masers, Lasers Impact factor: 3.488, year: 2014

Soft-X ray electronics for temperature measurement in SST-1 tokamak

International Nuclear Information System (INIS)

Kumari, Praveena; Raval, Jayesh V.; Chauhan, Harsad; Hansalia, C.J.; Joisa, Y.S.; Rajpal, Rachana

2015-01-01

Soft-X ray diagnostic is used for the measurement of core temperature of plasma in tokamak. Signal conditioning electronics is designed, developed and tested for Soft-X ray measurement in SST-1. Silicon Surface Barrier Detectors (SBD) are used for detection of Soft -X ray. The detector is very sensitive and have a large leakage current (1-10) nA/cm"2. The preamplifier is designed to measure (10-100) nA of current signal. Virtual bias is supplied to detector through preamplifier. The front end electronics are mounted directly on the feed through in air side. Detectors are interfaced with feed through by 2-wire shielded cable. In the way of getting good results, problems are identified and troubleshooted. Soft-X ray signals are observed consistently in SST-1 campaign XIII. Different scheme were tested during the plasma experimental shots to get better measurement. This poster will describe the design details, interfacing with detector, problem faced, remedy and results. (author)

Neutron and X-ray optics

CERN Document Server

Cremer, Jay Theodore

2013-01-01

Covering a wide range of topics related to neutron and x-ray optics, this book explores the aspects of neutron and x-ray optics and their associated background and applications in a manner accessible to both lower-level students while retaining the detail necessary to advanced students and researchers. It is a self-contained book with detailed mathematical derivations, background, and physical concepts presented in a linear fashion. A wide variety of sources were consulted and condensed to provide detailed derivations and coverage of the topics of neutron and x-ray optics as well as the background material needed to understand the physical and mathematical reasoning directly related or indirectly related to the theory and practice of neutron and x-ray optics. The book is written in a clear and detailed manner, making it easy to follow for a range of readers from undergraduate and graduate science, engineering, and medicine. It will prove beneficial as a standalone reference or as a complement to textbooks. Su...

Development and present status of the Russian-German soft X-ray beamline at BESSY II

International Nuclear Information System (INIS)

Fedoseenko, S.I.; Iossifov, I.E.; Gorovikov, S.A.; Schmidt, J.-S.; Follath, R.; Molodtsov, S.L.; Adamchuk, V.K.; Kaindl, G.

2001-01-01

We report on further developments of the optical design of the Russian-German soft X-ray beamline at BESSY II. Ray-tracing calculations reveal state-of-the-art characteristics of the modified layout. Resolving power up to 25 000 and photon flux up to 3x10 10 photons/s/100 mA will be available for spectroscopic experiments. Technical details of operation of the precision mechanics used for fine adjustment of the first mirror are presented

Simulation and optimization of the SIRIUS IPE soft x-ray beamline

Science.gov (United States)

Meyer, Bernd C.; Rocha, Tulio C. R.; Luiz, Sergio A. L.; C. Pinto, Artur; Westfahl, Harry

2017-08-01

The soft X-ray beamline IPE is one of the first phase SIRIUS beamlines at the LNLS, Brazil. Divided into two branches, IPE is designed to perform ambient pressure X-ray photo-electron spectroscopy (AP-XPS) and high resolution resonant inelastic X-ray scattering (RIXS) for samples in operando/environmental conditions inside cells and liquid jets. The aim is to maximize the photon flux in the energy range 200-1400 eV generated by an elliptically polarizing undulator source (EPU) and focus it to a 1 μm vertical spot size at the RIXS station and 10 μm at the AP-XPS station. In order to achieve the required resolving power (40.000 at 930 eV) for RIXS both the dispersion properties of the plane grating monochromator (PGM) and the thermal deformation of the optical elements need special attention. The grating parameters were optimized with the REFLEC code to maximize the efficiency at the required resolution. Thermal deformation of the PGM plane mirror limits the possible range of cff parameters depending of the photon energy used. Hence, resolution of the PGM and thermal deformation effects define the boundary conditions of the optical concept and the simulations of the IPE beamline. We compare simulations performed by geometrical ray-tracing (SHADOW) and wave front propagation (SRW) and show that wave front diffraction effects (apertures, optical surface error profiles) has a small effect on the beam spot size and shape.

Marriage of x-ray and optical astronomy

International Nuclear Information System (INIS)

McClintock, J.E.

1975-01-01

An historical discussion of the relation of x-ray and optical astronomy is given including distances within our galaxy, the optical identification of x-ray sources, the binary x-ray stars, neutron stars and black holes, a program in x-ray astronomy, and future missions

Small Angle X-Ray Scattering Detector

Energy Technology Data Exchange (ETDEWEB)

Hessler, Jan P.

2004-06-15

A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., qmax/qmin approx=lO0.

Hard X-ray Optics Technology Development for Astronomy at the Marshall Space Flight Center

Science.gov (United States)

Gubarev, Mikhail; Ramsey, Brian; Kilaru, Kiranmayee

2009-01-01

Grazing-incidence telescopes based on Wolter 1 geometry have delivered impressive advances in astrophysics at soft-x-ray wavelengths, while the hard xray region remains relatively unexplored at fine angular resolution and high sensitivities. The ability to perform ground-breaking science in the hard-x-ray energy range had been the motivation for technology developments aimed at fabricating low-cost, light-weight, high-quality x-ray mirrors. Grazing-incidence x-ray optics for high-energy astrophysical applications is being developed at MSFC using the electroform-nickel replication process.

X-ray/UV variability and the origin of soft X-ray excess emission from II Zw 177

Science.gov (United States)

Pal, Main

We study a detailed broad-band X-ray/UV emission from the narrow line Seyfert 1 galaxy II Zw 177 based on two XMM-Newton and single Swift/XRT observations. Both XMM-Newton observations show the soft X-ray excess emission below 2 keV when the best-fit 2 - 10 keV power law is extrapolated down to 0.3 keV. We find the blurred reflection from an ionized accretion disc and Comptonized disc emission both describe the observed soft excess well. We find a remarkable trend of decreasing UV flux with increasing soft X-ray excess and power law emission. We suggest that this could be due to that the external edge of corona hide a fraction of accretion disk. Co-Author: Prof. Gulab C. Dewangan (IUCAA), Prof. Ranjeev Misra (IUCAA), Pramod Kumar (Nanded university)

A HIGH REPETITION RATE VUV-SOFT X-RAY FEL CONCEPT

International Nuclear Information System (INIS)

Corlett, J.; Byrd, J.; Fawley, W.M.; Gullans, M.; Li, D.; Lidia, S.M.; Padmore, H.; Penn, G.; Pogorelov, I.; Qiang, J.; Robin, D.; Sannibale, F.; Staples, J.W.; Steier, C.; Venturini, M.; Virostek, S.; Wan, W.; Wells, R.; Wilcox, R.; Wurtele, J.; Zholents, A.

2007-01-01

We report on design studies for a seeded FEL light source that is responsive to the scientific needs of the future. The FEL process increases radiation flux by several orders of magnitude above existing incoherent sources, and offers the additional enhancements attainable by optical manipulations of the electron beam: control of the temporal duration and bandwidth of the coherent output, reduced gain length in the FEL, utilization of harmonics to attain shorter wavelengths, and precise synchronization of the x-ray pulse with seed laser systems. We describe an FEL facility concept based on a high repetition rate RF photocathode gun, that would allow simultaneous operation of multiple independent FEL's, each producing high average brightness, tunable over the VUV-soft x-ray range, and each with individual performance characteristics determined by the configuration of the FEL. SASE, enhanced-SASE (ESASE), seeded, harmonic generation, and other configurations making use of optical manipulations of the electron beam may be employed, providing a wide range of photon beam properties to meet varied user demands

Picosecond Soft-X-ray studies of Dense Plasma Regimes Progress Report (April 1, 2006 - March 31, 2007)

International Nuclear Information System (INIS)

Rocca, Jorge; Marconi, Mario; Shlyaptsev, Vyacheslav; Dunn, James; Moon, Stephen; Nilsen, Joseph

2007-01-01

The goal of this project is to investigate and characterize high-density converging plasma configurations using new soft x-ray laser based interferometric techniques. The results are used to verify and validate multi-dimensional hydrodynamic codes in plasma regimes which densities and size exceed those that can be probed with optical laser beams. The dynamics of converging plasmas created by laser irradiation of half-hohlraum cylindrical cavities targets was probed using a compact 46.9 nm soft x-ray laser. The results were used for comparison with extensive simulations conducted with the multi-dimensional hydrodynamic code HYDRA. As part of this study we have also investigated plasma regimes in which the index of refraction of the plasmas can not be defined solely based on the contribution of free electron, as is usually assumed for multiply ionized plasmas. Our results demonstrate the existence of plasma regimes in which the contribution of bound electrons from ions dominates the refractive index at soft x-ray wavelengths. We are also working in extending plasma interferometry to the sub 10 nm wavelength range. In the process we are advancing soft x-ray laser plasma diagnostics techniques to allow the measurement of large-scale, high-density plasmas with picosecond temporal resolution and micrometer spatial resolution, laying the foundations for future advanced diagnostics at high energy density DOE facilities. Dense plasma diagnostics, soft x-ray laser interferometry, converging plasmas

Resolving the Origin of the Diffuse Soft X-ray Background

Science.gov (United States)

Smith, Randall K.; Foster, Adam R.; Edgar, Ricard J.; Brickhouse, Nancy S.; Sanders, Wilton T.

2012-01-01

In January 1993, the Diffuse X-ray Spectrometer (DXS) measured the first high-resolution spectrum of the diffuse soft X-ray background between 44-80A. A line-dominated spectrum characteristic of a 10(exp 6)K collisionally ionized plasma' was expected but while the observed spectrum was clearly line-dominated, no model would fit. Then in 2003 the Cosmic Hot Interstellar Plasma Spectrometer (CHIPS) launched and observed the diffuse extreme-ultraviolet (EUV) spectrum between 90- 265A. Although many emission lines were again expected; only Fe IX at 171.1A was detected. The discovery of X-rays from comets led to the realization that heavy ions (Z=6-28) in the solar wind will emit soft X-rays as the ions interact via charge exchange with neutral atoms in the heliosphere and geocorona. Using a new model for solar wind charge exchange (SWCX) emission, we show that the diffuse soft X-ray background can be understood as a combination of emission from charge exchange onto the slow and fast solar wind together with a more distant and diffuse hot (10(exp 6)K) plasma.

X-Ray Optics: Past, Present, and Future

Science.gov (United States)

Zhang, William W.

2010-01-01

X-ray astronomy started with a small collimated proportional counter atop a rocket in the early 1960s. It was immediately recognized that focusing X-ray optics would drastically improve both source location accuracy and source detection sensitivity. In the past 5 decades, X-ray astronomy has made significant strides in achieving better angular resolution, large photon collection area, and better spectral and timing resolutions, culminating in the three currently operating X-ray observatories: Chandra, XMM/Newton, and Suzaku. In this talk I will give a brief history of X-ray optics, concentrating on the characteristics of the optics of these three observatories. Then I will discuss current X-ray mirror technologies being developed in several institutions. I will end with a discussion of the optics for the International X-ray Observatory that I have been developing at Goddard Space Flight Center.

Optical Synchronization Systems for Femtosecond X-raySources

Energy Technology Data Exchange (ETDEWEB)

Wilcox, Russell; Staples, John W.; Holzwarth, Ronald

2004-05-09

In femtosecond pump/probe experiments using short X-Ray and optical pulses, precise synchronization must be maintained between widely separated lasers in a synchrotron or FEL facility. We are developing synchronization systems using optical signals for applications requiring different ranges of timing error over 100 meter of glass fiber. For stabilization in the hundred femtosecond range a CW laser is amplitude modulated at 1 10 GHz, the signal retroreflected from the far end, and the relative phase used to correct the transit time with a piezoelectric phase modulator. For the sub-10 fsec range the laser frequency itself is upshifted 55 MHz with an acousto-optical modulator, retroreflected, upshifted again and phase compared at the sending end to a 110 MHz reference. Initial experiments indicate less than 1 fsec timing jitter. To lock lasers in the sub-10 fs range we will lock two single-frequency lasers separated by several tera Hertz to a master modelocked fiber laser, transmit the two frequencies over fiber, and lock two comb lines of a slave laser to these frequencies, thus synchronizing the two modelocked laser envelopes.

Optical Synchronization Systems for Femtosecond X-ray Sources

International Nuclear Information System (INIS)

Wilcox, Russell; Staples, John W.; Holzwarth, Ronald

2004-01-01

In femtosecond pump/probe experiments using short X-Ray and optical pulses, precise synchronization must be maintained between widely separated lasers in a synchrotron or FEL facility. We are developing synchronization systems using optical signals for applications requiring different ranges of timing error over 100 meter of glass fiber. For stabilization in the hundred femtosecond range a CW laser is amplitude modulated at 1 10 GHz, the signal retroreflected from the far end, and the relative phase used to correct the transit time with a piezoelectric phase modulator. For the sub-10 fsec range the laser frequency itself is upshifted 55 MHz with an acousto-optical modulator, retroreflected, upshifted again and phase compared at the sending end to a 110 MHz reference. Initial experiments indicate less than 1 fsec timing jitter. To lock lasers in the sub-10 fs range we will lock two single-frequency lasers separated by several tera Hertz to a master modelocked fiber laser, transmit the two frequencies over fiber, and lock two comb lines of a slave laser to these frequencies, thus synchronizing the two modelocked laser envelopes

New trends in space x-ray optics

Science.gov (United States)

Hudec, R.; Maršíková, V.; Pína, L.; Inneman, A.; Skulinová, M.

2017-11-01

The X-ray optics is a key element of various X-ray telescopes, X-ray microscopes, as well as other X-ray imaging instruments. The grazing incidence X-ray lenses represent the important class of X-ray optics. Most of grazing incidence (reflective) X-ray imaging systems used in astronomy but also in other (laboratory) applications are based on the Wolter 1 (or modified) arrangement. But there are also other designs and configurations proposed, used and considered for future applications both in space and in laboratory. The Kirkpatrick-Baez (K-B) lenses as well as various types of Lobster-Eye optics and MCP/Micropore optics serve as an example. Analogously to Wolter lenses, the X-rays are mostly reflected twice in these systems to create focal images. Various future projects in X-ray astronomy and astrophysics will require large segments with multiple thin shells or foils. The large Kirkpatrick-Baez modules, as well as the large Lobster-Eye X-ray telescope modules in Schmidt arrangement may serve as examples. All these space projects will require high quality and light segmented shells (bent or flat foils) with high X-ray reflectivity and excellent mechanical stability. The Multi Foil Optics (MFO) approach represent a promising alternative for both LE and K-B X-ray optical modules. Several types of reflecting substrates may be considered for these applications, with emphasis on thin float glass sheets and, more recently, high quality silicon wafers. This confirms the importance of non- Wolter X-ray optics designs for the future. Future large space X-ray telescopes (such as IXO) require precise and light-weight X-ray optics based on numerous thin reflecting shells. Novel approaches and advanced technologies are to be exploited and developed. In this contribution, we refer on results of tested X-ray mirror shells produced by glass thermal forming (GTF) and by shaping Si wafers. Both glass foils and Si wafers are commercially available, have excellent surface

Optical Observations of X-ray Bright, Optically Normal Galaxies

Science.gov (United States)

Sadun, Alberto C.; Aryan, N. S.; Ghosh, K. K.

2007-05-01

X-ray bright, optically normal galaxies (XBONGs) are galaxies that seem to have normal spectra and morphology, but are relatively bright x-ray sources. The large ratio of the x-ray to optical emission suggests that some activity, similar to that of active galactic nuclei (AGN), is occurring. Since the galaxies do not show any obvious sign of nuclear activity in their optical spectra, one possible explanation is that these galaxies do not have an optically thick accretion disk at small radii, as previously assumed. Previous data for NGC 7626 classifies it as an XBONG, and so we are studying optical features of this galaxy in order to determine better its features. After confirming an x-ray jet, we are now comparing this to optical features that we have found, including warped dust lanes and a possible optical jet.

Application of Laser Plasma Sources of Soft X-rays and Extreme Ultraviolet (EUV) in Imaging, Processing Materials and Photoionization Studies

Science.gov (United States)

Fiedorowicz, H.; Bartnik, A.; Wachulak, P. W.; Jarocki, R.; Kostecki, J.; Szczurek, M.; Ahad, I. U.; Fok, T.; Szczurek, A.; Wȩgrzyński, Ł.

In the paper we present new applications of laser plasma sources of soft X-rays and extreme ultraviolet (EUV) in various areas of plasma physics, nanotechnology and biomedical engineering. The sources are based on a gas puff target irradiated with nanosecond laser pulses from commercial Nd: YAG lasers, generating pulses with time duration from 1 to 10 ns and energies from 0.5 to 10 J at a 10 Hz repetition rate. The targets are produced with the use of a double valve system equipped with a special nozzle to form a double-stream gas puff target which allows for high conversion efficiency of laser energy into soft X-rays and EUV without degradation of the nozzle. The sources are equipped with various optical systems to collect soft X-ray and EUV radiation and form the radiation beam. New applications of these sources in imaging, including EUV tomography and soft X-ray microscopy, processing of materials and photoionization studies are presented.

Soft X-ray radiation power characteristics of tungsten wire arrays on Yang accelerator

International Nuclear Information System (INIS)

Zhang Siqun; Ouyang Kai; Huang Xianbin; Dan Jiakun; Zhou Rongguo; Yang Liang

2013-01-01

A series of experiments were carried out to research the X-ray radiation characteristics of tungsten wire arrays on Yang accelerator. In those experiments, we charged the Marx generator of 60 kV, and the load current of 0.85-1.00 MA, the rise time of 75-90 ns (10%-90%). A soft X-ray scintillator powermeter which responded flatly to 50-1800 eV X-rays was used to measure the power of soft X-ray emitted from implosion plasma. In this paper, we present the measuring results of time-resolved soft X-ray radiation power, and discuss the radiation characteristics of implosion plasma by analyzing the correlations of soft X-ray radiant power and the diameter, length, wire number of the tungsten wire arrays. The optimizing wire array configuration parameters on Yang are as follows: 8 mm array diameter, 15 mm wire length, and 24 wire number. We also present the radiant power difference in radial and axial directions of the wire arrays. (authors)

Contributions of late-type dwarf stars to the soft X-ray diffuse background

Energy Technology Data Exchange (ETDEWEB)

Schmitt, J.H.M.M.; Snowden, S.L. (Max-Planck-Institut fuer Extraterrestrische Physik, Garching (Germany, F.R.) Wisconsin Univ., Madison (USA))

1990-09-01

Comprehensive calculations of the contribution of late-type dwarf stars to the soft X-ray diffuse background are presented. The mean X-ray luminosity as derived from optically and X-ray selected samples is examined, using the Bahcall-Soneira Galaxy model to describe the spatial distribution of stars and recent results on the X-ray spectra. The model calculations are compared with the Wisconsin sky maps in the C, M1, M2, I and J bands to assess the uncertainties of the calculations. Contributions of up to 10 percent to the M2 and I band background at high Galactic latitudes are found, while at low Galactic latitudes late-type stars contribute up to 40 percent of the background. However, a Galactic ridge as well as a relatively isotropic component still remains unexplained, even with the added contribution of the extrapolated high-energy power law. 41 refs.

Contributions of late-type dwarf stars to the soft X-ray diffuse background

Science.gov (United States)

Schmitt, J. H. M. M.; Snowden, S. L.

1990-01-01

Comprehensive calculations of the contribution of late-type dwarf stars to the soft X-ray diffuse background are presented. The mean X-ray luminosity as derived from optically and X-ray selected samples is examined, using the Bahcall-Soneira Galaxy model to describe the spatial distribution of stars and recent results on the X-ray spectra. The model calculations are compared with the Wisconsin sky maps in the C, M1, M2, I and J bands to assess the uncertainties of the calculations. Contributions of up to 10 percent to the M2 and I band background at high Galactic latitudes are found, while at low Galactic latitudes late-type stars contribute up to 40 percent of the background. However, a Galactic ridge as well as a relatively isotropic component still remains unexplained, even with the added contribution of the extrapolated high-energy power law.

X-ray pore optic developments

Science.gov (United States)

Wallace, Kotska; Bavdaz, Marcos; Collon, Maximilien; Beijersbergen, Marco; Kraft, Stefan; Fairbend, Ray; Séguy, Julien; Blanquer, Pascal; Graue, Roland; Kampf, Dirk

2017-11-01

In support of future x-ray telescopes ESA is developing new optics for the x-ray regime. To date, mass and volume have made x-ray imaging technology prohibitive to planetary remote sensing imaging missions. And although highly successful, the mirror technology used on ESA's XMM-Newton is not sufficient for future, large, x-ray observatories, since physical limits on the mirror packing density mean that aperture size becomes prohibitive. To reduce telescope mass and volume the packing density of mirror shells must be reduced, whilst maintaining alignment and rigidity. Structures can also benefit from a modular optic arrangement. Pore optics are shown to meet these requirements. This paper will discuss two pore optic technologies under development, with examples of results from measurement campaigns on samples. One activity has centred on the use of coated, silicon wafers, patterned with ribs, that are integrated onto a mandrel whose form has been polished to the required shape. The wafers follow the shape precisely, forming pore sizes in the sub-mm region. Individual stacks of mirrors can be manufactured without risk to, or dependency on, each other and aligned in a structure from which they can also be removed without hazard. A breadboard is currently being built to demonstrate this technology. A second activity centres on glass pore optics. However an adaptation of micro channel plate technology to form square pores has resulted in a monolithic material that can be slumped into an optic form. Alignment and coating of two such plates produces an x-ray focusing optic. A breadboard 20cm aperture optic is currently being built.

[Experimental investigation of laser plasma soft X-ray source with gas target].

Science.gov (United States)

Ni, Qi-liang; Gong, Yan; Lin, Jing-quan; Chen, Bo; Cao, Jian-lin

2003-02-01

This paper describes a debris-free laser plasma soft X-ray source with a gas target, which has high operating frequency and can produce strong soft X-ray radiation. The valve of this light source is drived by a piezoelectrical ceramic whose operating frequency is up to 400 Hz. In comparison with laser plasma soft X-ray sources using metal target, the light source is debris-free. And it has higher operating frequency than gas target soft X-ray sources whose nozzle is controlled by a solenoid valve. A channel electron multiplier (CEM) operating in analog mode is used to detect the soft X-ray generated by the laser plasma source, and the CEM's output is fed to to a charge-sensitive preamplifier for further amplification purpose. Output charges from the CEM are proportional to the amplitude of the preamplifier's output voltage. Spectra of CO2, Xe and Kr at 8-14 nm wavelength which can be used for soft X-ray projection lithography are measured. The spectrum for CO2 consists of separate spectral lines originate mainly from the transitions in Li-like and Be-like ions. The Xe spectrum originating mainly from 4d-5f, 4d-4f, 4d-6p and 4d-5p transitions in multiply charged xenon ions. The spectrum for Kr consists of separate spectral lines and continuous broad spectra originating mainly from the transitions in Cu-, Ni-, Co- and Fe-like ions.

Soft x-ray free-electron laser induced damage to inorganic scintillators

Czech Academy of Sciences Publication Activity Database

Burian, Tomáš; Hájková, Věra; Chalupský, Jaromír; Vyšín, Luděk; Boháček, Pavel; Přeček, Martin; Wild, J.; Özkan, C.; Coppola, N.; Farahani, S.D.; Schulz, J.; Sinn, H.; Tschentscher, T.; Gaudin, J.; Bajt, S.; Tiedtke, K.; Toleikis, S.; Chapman, H.N.; Loch, R.A.; Jurek, M.; Sobierajski, R.; Krzywinski, J.; Moeller, S.; Harmand, M.; Galasso, G.; Nagasono, M.; Saskl, K.; Sovák, P.; Juha, Libor

2015-01-01

Roč. 5, č. 2 (2015), 254-264 ISSN 2159-3930 R&D Projects: GA ČR(CZ) GAP108/11/1312; GA MŠk EE2.3.30.0057 Grant - others:OP VK 4 POSTDOK(XE) CZ.1.07/2.3.00/30.0057 Institutional support: RVO:68378271 Keywords : fluorescent and luminescent materials * laser damage * free-electron lasers * soft x-rays * laser materials processing Subject RIV: BH - Optics, Masers, Lasers Impact factor: 2.657, year: 2015

Description of EMX computer code. System for measuring soft X rays

International Nuclear Information System (INIS)

Marty, D.A.; Smeulders, P.; Launois, D.

1978-07-01

After briefly describing the system for measuring soft X rays implanted in TFR 600, the objectives and principles of the E.M.X calculation programme are presented. This model is divided into two distinct parts. The ultimate aim of EMX 1, the first part, is to build the soft X ray photo of a plasma with varied characteristics, seen through a certain collimation system (in this case a slit). That of EMX 2, the second part, is to filter the previously built soft X ray photo, by means of the system of absorbents belonging to the measuring system and to calculate the currents generated by each detector aimed at a plasma chord. The first calculation results are commented and discussed [fr

The Elusive Soft Emission from Hard X-ray Symbiotic System RT Cru

Science.gov (United States)

Karovska, Margarita

2014-09-01

RT Cru is a fascinating member of a new class of hard X-ray emitting symbiotic binaries showing X-ray emission extending to over 50keV. While its hard X-ray emission has been studied in detail, the soft component of the spectrum, including flares, remains elusive, since previous observations have focused on the high-energy regime. We propose Chandra HRC-S/LETG observations to determine the spatial, spectral, and temporal characteristics of the source of the soft X-ray emission with a goal to establish the origin of the soft component, and determine whether and how it is tied to the hard component. Determining the origin of the soft emission is a crucial piece of the puzzle to understanding the geometry, energetics, and the environment of WD accretion in this class of symbiotic systems.

Soft X-ray resonant scattering from magnetic heterostructures

International Nuclear Information System (INIS)

Grabis, J.

2005-01-01

Heterogenous magnetic multilayers are of great interest both because of their relevance for technological applications and since they provide model systems to understand magnetic behavior and interactions. Soft x-ray resonant magnetic scattering (XRMS) allows to determine element-specific and depth-resolving information of the local magnetic order of such systems. Within the framework of the present thesis the diffractometer ALICE for soft XRMS has been constructed. XRMS measurements of two different physical systems are presented in this thesis: The antiferromagnetic and ferromagnetic order in interlayer exchange-coupled Fe/Cr(001) superlattices are studied as a function of the applied field by measuring the reflected intensity at different positions in reciprocal space. Thin films and multilayers of the Heusler compound Co 2 MnGe are studied by means of soft x-ray absorption spectroscopy, magnetic circular dichroism and resonant magnetic scattering

Progress in optical-field-ionization soft x-ray lasers at LOA

Czech Academy of Sciences Publication Activity Database

Mocek, Tomáš; Sebban, S.; Bettaibi, I.; Zeitoun, P.; Faivre, G.; Cros, B.; Maynard, G.; Butler, A.; McKenna, C.M.; Spence, D.J.; Gonsavles, A.J.; Hooker, S.M.; Vorontsov, V.; Hallou, S.; Fajardo, M.; Kazamias, S.; Le Pape, S.; Mercere, P.; Morlens, A.S.; Valentin, C.; Balcou, P.

2005-01-01

Roč. 23, - (2005), s. 351-356 ISSN 0263-0346 Grant - others:EU(XE) HPRI-1999-CT-00086; EU(XE) HPMF-CT-2002-01554 Institutional research plan: CEZ:AV0Z10100523 Keywords : collisional excitation * femtosecond * guiding * high harmonic amplification * x-ray laser Subject RIV: BH - Optics, Masers, Lasers Impact factor: 2.590, year: 2005

Aluminum-coated optical fibers as efficient infrared timing fiducial photocathodes for synchronizing x-ray streak cameras

International Nuclear Information System (INIS)

Koch, J.A.; MacGowan, B.J.

1991-01-01

The timing fiducial system at the Nova Two-Beam Facility allows time-resolved x-ray and optical streak camera data from laser-produced plasmas to be synchronized to within 30 ps. In this system, an Al-coated optical fiber is inserted into an aperture in the cathode plate of each streak camera. The coating acts as a photocathode for a low-energy pulse of 1ω (λ = 1.054 μm) light which is synchronized to the main Nova beam. The use of the fundamental (1ω) for this fiducial pulse has been found to offer significant advantages over the use of the 2ω second harmonic (λ = 0.53 μm). These advantages include brighter signals, greater reliability, and a higher relative damage threshold, allowing routine use without fiber replacement. The operation of the system is described, and experimental data and interpretations are discussed which suggest that the electron production in the Al film is due to thermionic emission. The results of detailed numerical simulations of the relevant thermal processes, undertaken to model the response of the coated fiber to 1ω laser pulses, are also presented, which give qualitative agreement with experimental data. Quantitative discrepancies between the modeling results and the experimental data are discussed, and suggestions for further research are given

Soft X-ray Emission from Large-Scale Galactic Outflows in Seyfert Galaxies

Science.gov (United States)

Colbert, E. J. M.; Baum, S.; O'Dea, C.; Veilleux, S.

1998-01-01

Kiloparsec-scale soft X-ray nebulae extend along the galaxy minor axes in several Seyfert galaxies, including NGC 2992, NGC 4388 and NGC 5506. In these three galaxies, the extended X-ray emission observed in ROSAT HRI images has 0.2-2.4 keV X-ray luminosities of 0.4-3.5 x 10(40) erg s(-1) . The X-ray nebulae are roughly co-spatial with the large-scale radio emission, suggesting that both are produced by large-scale galactic outflows. Assuming pressure balance between the radio and X-ray plasmas, the X-ray filling factor is >~ 10(4) times as large as the radio plasma filling factor, suggesting that large-scale outflows in Seyfert galaxies are predominantly winds of thermal X-ray emitting gas. We favor an interpretation in which large-scale outflows originate as AGN-driven jets that entrain and heat gas on kpc scales as they make their way out of the galaxy. AGN- and starburst-driven winds are also possible explanations if the winds are oriented along the rotation axis of the galaxy disk. Since large-scale outflows are present in at least 50 percent of Seyfert galaxies, the soft X-ray emission from the outflowing gas may, in many cases, explain the ``soft excess" X-ray feature observed below 2 keV in X-ray spectra of many Seyfert 2 galaxies.

Measuring device for soft X-rays

International Nuclear Information System (INIS)

Dissing, E.

1978-09-01

An instrument for the measurement of the absorbed energy per unit area of diagnostic X-rays in soft human tissue was developed. The instrument is intended for dosimetry applications in the field of dental and small skeleton radiography and for mammography. The detector assembly consists of a Polyvinyltoluene scintillator 2.54 diametre x 5.08 cm CsSb semitransparent head-on vacuum phototube. Polyvinyltoluene being a pure hydrocarbon may be considered a good representative material of human soft tissue concerning the absorption of X-rays. In the photon energy range of interest, 5 - 40 keV, the mass energy absorption coefficient for muscle tissue and for PVT differ about a factor 2 due to the considerable content of Oxygen in muscle tissue. This is to some extend reflected in the photon energy response characteristic for the instrument. For human adipose, the characteristic is practically flat from 5- 40 keV. The instrument is integrating the absorbed power per unit area and the digital display shows Joules/m 2 . The range for the instrument is from 000.1 μJ/m 2 to 19.99 J/m 2 (absorbed energy in 5 cm tissue). (author)

Introduction of soft X-ray spectromicroscopy as an advanced technique for plant biopolymers research.

Directory of Open Access Journals (Sweden)

Chithra Karunakaran

Full Text Available Soft X-ray absorption spectroscopy coupled with nano-scale microscopy has been widely used in material science, environmental science, and physical sciences. In this work, the advantages of soft X-ray absorption spectromicroscopy for plant biopolymer research were demonstrated by determining the chemical sensitivity of the technique to identify common plant biopolymers and to map the distributions of biopolymers in plant samples. The chemical sensitivity of soft X-ray spectroscopy to study biopolymers was determined by recording the spectra of common plant biopolymers using soft X-ray and Fourier Transform mid Infrared (FT-IR spectroscopy techniques. The soft X-ray spectra of lignin, cellulose, and polygalacturonic acid have distinct spectral features. However, there were no distinct differences between cellulose and hemicellulose spectra. Mid infrared spectra of all biopolymers were unique and there were differences between the spectra of water soluble and insoluble xylans. The advantage of nano-scale spatial resolution exploited using soft X-ray spectromicroscopy for plant biopolymer research was demonstrated by mapping plant cell wall biopolymers in a lentil stem section and compared with the FT-IR spectromicroscopy data from the same sample. The soft X-ray spectromicroscopy enables mapping of biopolymers at the sub-cellular (~30 nm resolution whereas, the limited spatial resolution in the micron scale range in the FT-IR spectromicroscopy made it difficult to identify the localized distribution of biopolymers. The advantages and limitations of soft X-ray and FT-IR spectromicroscopy techniques for biopolymer research are also discussed.

A fiber optic synchronization system for LUX

International Nuclear Information System (INIS)

Wilcox, R.B.; Staples, J.W.; Doolittle, L.R.

2004-01-01

The LUX femtosecond light source concept would support pump-probe experiments that need to synchronize laser light pulses with electron-beam-generated X-ray pulses to less than 50 fs at the experimenter endstations. To synchronize multiple endstation lasers with the X-ray pulse, we are developing a fiber-distributed optical timing network. A high frequency clock signal is distributed via fiber to RF cavities (controlling X-ray probe pulse timing) and mode-locked lasers at endstations (controlling pump pulse timing). The superconducting cavities are actively locked to the optical clock phase. Most of the RF timing error is contained within a 10 kHz bandwidth, so these errors and any others affecting X-ray pulse timing (such as RF gun phase) can be detected and transmitted digitally to correct laser timing at the endstations. Time delay through the fibers will be stabilized by comparing a retro-reflected pulse from the experimenter endstation end with a reference pulse from the sending en d, and actively controlling the fiber length

Bright circularly polarized soft X-ray high harmonics for X-ray magnetic circular dichroism.

Science.gov (United States)

Fan, Tingting; Grychtol, Patrik; Knut, Ronny; Hernández-García, Carlos; Hickstein, Daniel D; Zusin, Dmitriy; Gentry, Christian; Dollar, Franklin J; Mancuso, Christopher A; Hogle, Craig W; Kfir, Ofer; Legut, Dominik; Carva, Karel; Ellis, Jennifer L; Dorney, Kevin M; Chen, Cong; Shpyrko, Oleg G; Fullerton, Eric E; Cohen, Oren; Oppeneer, Peter M; Milošević, Dejan B; Becker, Andreas; Jaroń-Becker, Agnieszka A; Popmintchev, Tenio; Murnane, Margaret M; Kapteyn, Henry C

2015-11-17

We demonstrate, to our knowledge, the first bright circularly polarized high-harmonic beams in the soft X-ray region of the electromagnetic spectrum, and use them to implement X-ray magnetic circular dichroism measurements in a tabletop-scale setup. Using counterrotating circularly polarized laser fields at 1.3 and 0.79 µm, we generate circularly polarized harmonics with photon energies exceeding 160 eV. The harmonic spectra emerge as a sequence of closely spaced pairs of left and right circularly polarized peaks, with energies determined by conservation of energy and spin angular momentum. We explain the single-atom and macroscopic physics by identifying the dominant electron quantum trajectories and optimal phase-matching conditions. The first advanced phase-matched propagation simulations for circularly polarized harmonics reveal the influence of the finite phase-matching temporal window on the spectrum, as well as the unique polarization-shaped attosecond pulse train. Finally, we use, to our knowledge, the first tabletop X-ray magnetic circular dichroism measurements at the N4,5 absorption edges of Gd to validate the high degree of circularity, brightness, and stability of this light source. These results demonstrate the feasibility of manipulating the polarization, spectrum, and temporal shape of high harmonics in the soft X-ray region by manipulating the driving laser waveform.

Surface Slope Metrology on Deformable Soft X-ray Mirrors

International Nuclear Information System (INIS)

Yuan, Sheng; Yashchuk, Valeriy V.; Goldberg, Kenneth A.; Celestre, Rich; Church, Matthew; McKinney, Wayne R.; Morrison, Greg; Warwick, Tony

2010-01-01

We report on the current state of surface slope metrology on deformable mirrors for soft x-rays at the Advanced Light Source (ALS). While we are developing techniques for in situ at-wavelength tuning, we are refining methods of ex situ visible-light optical metrology to achieve sub-100-nrad accuracy. This paper reports on laboratory studies, measurements and tuning of a deformable test-KB mirror prior to its use. The test mirror was bent to a much different optical configuration than its original design, achieving a 0.38 micro-radian residual slope error. Modeling shows that in some cases, by including the image conjugate distance as an additional free parameter in the alignment, along with the two force couples, fourth-order tangential shape errors (the so-called bird shape) can be reduced or eliminated.

Surface Slope Metrology on Deformable Soft X-ray Mirrors

International Nuclear Information System (INIS)

Yuan, S.; Yashchuk, V.V.; Goldberg, K.A.; Celestre, R.; Church, M.; McKinney, W.R.; Morrison, G.; Warwick, T.

2009-01-01

We report on the current state of surface slope metrology on deformable mirrors for soft x-rays at the Advanced Light Source (ALS). While we are developing techniques for in situ at-wavelength tuning, we are refining methods of ex situvisible-light optical metrology to achieve sub-100-nrad accuracy. This paper reports on laboratory studies, measurements and tuning of a deformable test-KB mirror prior to its use. The test mirror was bent to a much different optical configuration than its original design, achieving a 0.38 micro-radian residual slope error. Modeling shows that in some cases, by including the image conjugate distance as an additional free parameter in the alignment, along with the two force couples, fourth-order tangential shape errors (the so-called bird shape) can be reduced or eliminated.

Optics Developments for X-Ray Astronomy

Science.gov (United States)

Ramsey, Brian

2014-01-01

X-ray optics has revolutionized x-ray astronomy. The degree of background suppression that these afford, have led to a tremendous increase in sensitivity. The current Chandra observatory has the same collecting area (approx. 10(exp 3)sq cm) as the non-imaging UHURU observatory, the first x-ray observatory which launched in 1970, but has 5 orders of magnitude more sensitivity due to its focusing optics. In addition, its 0.5 arcsec angular resolution has revealed a wealth of structure in many cosmic x-ray sources. The Chandra observatory achieved its resolution by using relatively thick pieces of Zerodur glass, which were meticulously figured and polished to form the four-shell nested array. The resulting optical assembly weighed around 1600 kg, and cost approximately $0.5B. The challenge for future x-ray astronomy missions is to greatly increase the collecting area (by one or more orders of magnitude) while maintaining high angular resolution, and all within realistic mass and budget constraints. A review of the current status of US optics for x-ray astronomy will be provided along with the challenges for future developments.

Optics for coherent X-ray applications

Energy Technology Data Exchange (ETDEWEB)

Yabashi, Makina, E-mail: yabashi@spring8.or.jp [RIKEN SPring-8 Center, Kouto 1-1-1, Sayo, Hyogo 679-5148 (Japan); Tono, Kensuke [Japan Synchrotron Radiation Research Institute (JASRI), Kouto 1-1-1, Sayo, Hyogo 679-5198 (Japan); Mimura, Hidekazu [The University of Tokyo, Hongo 7-3-1, Bunkyo-ku, Tokyo 113-8656 (Japan); Matsuyama, Satoshi; Yamauchi, Kazuto [Osaka University, 2-1 Yamada-oka, Suita, Osaka 565-0871 (Japan); Tanaka, Takashi; Tanaka, Hitoshi; Tamasaku, Kenji [RIKEN SPring-8 Center, Kouto 1-1-1, Sayo, Hyogo 679-5148 (Japan); Ohashi, Haruhiko; Goto, Shunji [Japan Synchrotron Radiation Research Institute (JASRI), Kouto 1-1-1, Sayo, Hyogo 679-5198 (Japan); Ishikawa, Tetsuya [RIKEN SPring-8 Center, Kouto 1-1-1, Sayo, Hyogo 679-5148 (Japan)

2014-08-27

Developments of optics for coherent X-ray applications and their role in diffraction-limited storage rings are described. Developments of X-ray optics for full utilization of diffraction-limited storage rings (DLSRs) are presented. The expected performance of DLSRs is introduced using the design parameters of SPring-8 II. To develop optical elements applicable to manipulation of coherent X-rays, advanced technologies on precise processing and metrology were invented. With propagation-based coherent X-rays at the 1 km beamline of SPring-8, a beryllium window fabricated with the physical-vapour-deposition method was found to have ideal speckle-free properties. The elastic emission machining method was utilized for developing reflective mirrors without distortion of the wavefronts. The method was further applied to production of diffraction-limited focusing mirrors generating the smallest spot size in the sub-10 nm regime. To enable production of ultra-intense nanobeams at DLSRs, a low-vibration cooling system for a high-heat-load monochromator and advanced diagnostic systems to characterize X-ray beam properties precisely were developed. Finally, new experimental schemes for combinative nano-analysis and spectroscopy realised with novel X-ray optics are discussed.

Nanoscale characterization of local structures and defects in photonic crystals using synchrotron-based transmission soft X-ray microscopy

Science.gov (United States)

Nho, Hyun Woo; Kalegowda, Yogesh; Shin, Hyun-Joon; Yoon, Tae Hyun

2016-01-01

For the structural characterization of the polystyrene (PS)-based photonic crystals (PCs), fast and direct imaging capabilities of full field transmission X-ray microscopy (TXM) were demonstrated at soft X-ray energy. PS-based PCs were prepared on an O2-plasma treated Si3N4 window and their local structures and defects were investigated using this label-free TXM technique with an image acquisition speed of ~10 sec/frame and marginal radiation damage. Micro-domains of face-centered cubic (FCC (111)) and hexagonal close-packed (HCP (0001)) structures were dominantly found in PS-based PCs, while point and line defects, FCC (100), and 12-fold symmetry structures were also identified as minor components. Additionally, in situ observation capability for hydrated samples and 3D tomographic reconstruction of TXM images were also demonstrated. This soft X-ray full field TXM technique with faster image acquisition speed, in situ observation, and 3D tomography capability can be complementally used with the other X-ray microscopic techniques (i.e., scanning transmission X-ray microscopy, STXM) as well as conventional characterization methods (e.g., electron microscopic and optical/fluorescence microscopic techniques) for clearer structure identification of self-assembled PCs and better understanding of the relationship between their structures and resultant optical properties. PMID:27087141

Shot-noise limited throughput of soft X-ray ptychography for nanometrology applications

NARCIS (Netherlands)

Koek, Wouter; Florijn, Bastiaan; Bäumer, Stefan; Kruidhof, Rik; Sadeghian, Hamed

2018-01-01

Due to its potential for high resolution and three-dimensional imaging, soft X-ray ptychography has received interest for nanometrology applications. We have analyzed the measurement time per unit area when using soft X-ray ptychography for various nanometrology applications including mask

Electron-confinement studies on EBT-S using soft-x-ray techniques

International Nuclear Information System (INIS)

Hillis, D.L.; Haste, G.R.; Berry, L.A.

1982-08-01

Soft x-ray bremsstrahlung measurements have been performed on the ELMO Bumpy Torus (EBT-S) plasma to determine the electron temperature T/sub e/ and electron density n/sub e/ using a calibrated Si(Li) detector over a wide range of operating conditions. The purpose of this paper is to outline the necessary assumptions and essential x-ray techniques that are inherent in soft x-ray measurements in order to investigate the electron heating and confinement properties of EBT-S. In addition, by utilizing the electron density as determined by the soft x-ray measurements, the previous EBT-S confinement analyses have been extended. The steady-state plasma of EBT-S is heated by microwaves using a cw gyrotron that can operate up to power levels of 200 kW. From the soft x-ray measurements, both the electron temperature and density are found to increase at higher microwave power levels. For operation at microwave power levels of 200 kW, T/sub e/ approaches 1 keV while n/sub e/ approaches 1.2 x 10 12 cm -3 . In general, confinement properties are found to improve with increased microwave power. The data are compared with neoclassical transport scaling and the electron transport is found to be collisionless (nu/Ω < 1) as well as neoclassical

Study of Cr/Sc-based multilayer reflecting mirrors using soft x-ray reflectivity and standing wave-enhanced x-ray fluorescence

Science.gov (United States)

Wu, Meiyi; Burcklen, Catherine; André, Jean-Michel; Guen, Karine Le; Giglia, Angelo; Koshmak, Konstantin; Nannarone, Stefano; Bridou, Françoise; Meltchakov, Evgueni; Rossi, Sébastien de; Delmotte, Franck; Jonnard, Philippe

2017-11-01

We study Cr/Sc-based multilayer mirrors designed to work in the water window range using hard and soft x-ray reflectivity as well as x-ray fluorescence enhanced by standing waves. Samples differ by the elemental composition of the stack, the thickness of each layer, and the order of deposition. This paper mainly consists of two parts. In the first part, the optical performances of different Cr/Sc-based multilayers are reported, and in the second part, we extend further the characterization of the structural parameters of the multilayers, which can be extracted by comparing the experimental data with simulations. The methodology is detailed in the case of Cr/B4C/Sc sample for which a three-layer model is used. Structural parameters determined by fitting reflectivity curve are then introduced as fixed parameters to plot the x-ray standing wave curve, to compare with the experiment, and confirm the determined structure of the stack.

Demonstration of a Ni-like Kr optical-field-ionization collisional soft x-ray laser at 32.8 nm

Czech Academy of Sciences Publication Activity Database

Sebban, S.; Mocek, Tomáš; Ros, D.; Upcraft, L.; Balcou, P.; Haroutunian, R.; Grillon, G.; Rus, Bedřich; Klisnick, A.; Carillon, A.; Jamelot, G.; Valentin, C.; Rouseau, J. P.; Notebaert, L.; Pittman, M.; Hulin, D.

2002-01-01

Roč. 89, č. 25 (2002), s. 253901-1 - 253901-4 ISSN 0031-9007 R&D Projects: GA MŠk LN00A100 Institutional research plan: CEZ:AV0Z1010921 Keywords : x-ray lasers * laser plasma * x-ray spectroscopy * x-ray optics Subject RIV: BH - Optics, Masers, Lasers Impact factor: 7.323, year: 2002

Probing nucleobase photoprotection with soft x-rays

Directory of Open Access Journals (Sweden)

Osipov T.

2013-03-01

Full Text Available Nucleobases absorb strongly in the ultraviolet region, leading to molecular excitation into reactive states. The molecules avoid the photoreactions by funnelling the electronic energy into less reactive states on an ultrafast timescale via non-Born-Oppenheimer dynamics. Current theory on the nucleobase thymine discusses two conflicting pathways for the photoprotective dynamics. We present our first results of our free electron laser based UV-pump soft x-ray-probe study of the photoprotection mechanism of thymine. We use the high spatial sensitivity of the Auger electrons emitted after the soft x-ray pulse induced core ionization. Our transient spetra show two timescales on the order of 200 fs and 5 ps, in agreement with previous (all UV ultrafast experiments. The timescales appear at different Auger kinetic energies which will help us to decipher the molecular dynamics.

X-ray dense cellular inclusions in the cells of the green alga Chlamydomonas reinhardtii as seen by soft-x-ray microscopy

International Nuclear Information System (INIS)

Stead, A.D.; Ford, T.W.; Page, A.M.; Brown, J.T.; Meyer-Ilse, W.

1997-01-01

Soft x-rays, having a greater ability to penetrate biological material than electrons, have the potential for producing images of intact, living cells. In addition, by using the so-called open-quotes water windowclose quotes area of the soft x-ray spectrum, a degree of natural contrast is introduced into the image due to differential absorption of the wavelengths by compounds with a high carbon content compared to those with a greater oxygen content. The variation in carbon concentration throughout a cell therefore generates an image which is dependent upon the carbon density within the specimen. Using soft x-ray contact microscopy the authors have previously examined the green alga Chlamydomonas reinhardtii, and the most prominent feature of the cells are the numerous x-ray absorbing spheres, But they were not seen by conventional transmission electron microscopy. Similar structures have also been reported by the Goettingen group using their cryo transmission x-ray microscope at BESSY. Despite the fact that these spheres appear to occupy up to 20% or more of the cell volume when seen by x-ray microscopy, they are not visible by transmission electron microscopy. Given the difficulties and criticisms associated with soft x-ray contact microscopy, the present study was aimed at confirming the existence of these cellular inclusions and learning more of their possible chemical composition

X-ray dense cellular inclusions in the cells of the green alga Chlamydomonas reinhardtii as seen by soft-x-ray microscopy

Energy Technology Data Exchange (ETDEWEB)

Stead, A.D.; Ford, T.W.; Page, A.M. [Univ. of London (United Kingdom); Brown, J.T.; Meyer-Ilse, W. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States)

1997-04-01

Soft x-rays, having a greater ability to penetrate biological material than electrons, have the potential for producing images of intact, living cells. In addition, by using the so-called {open_quotes}water window{close_quotes} area of the soft x-ray spectrum, a degree of natural contrast is introduced into the image due to differential absorption of the wavelengths by compounds with a high carbon content compared to those with a greater oxygen content. The variation in carbon concentration throughout a cell therefore generates an image which is dependent upon the carbon density within the specimen. Using soft x-ray contact microscopy the authors have previously examined the green alga Chlamydomonas reinhardtii, and the most prominent feature of the cells are the numerous x-ray absorbing spheres, But they were not seen by conventional transmission electron microscopy. Similar structures have also been reported by the Goettingen group using their cryo transmission x-ray microscope at BESSY. Despite the fact that these spheres appear to occupy up to 20% or more of the cell volume when seen by x-ray microscopy, they are not visible by transmission electron microscopy. Given the difficulties and criticisms associated with soft x-ray contact microscopy, the present study was aimed at confirming the existence of these cellular inclusions and learning more of their possible chemical composition.

Confocal soft X-ray scanning transmission microscopy: setup, alignment procedure and limitations

International Nuclear Information System (INIS)

Späth, Andreas; Raabe, Jörg; Fink, Rainer H.

2015-01-01

A conventional STXM setup has been upgraded with a second micro zone plate and aligned to confocal geometry. Two confocal geometries (in-line and off-axis) have been evaluated and a discussion on prospects and limitations is presented. Zone-plate-based scanning transmission soft X-ray microspectroscopy (STXM) is a well established technique for high-contrast imaging of sufficiently transparent specimens (e.g. ultrathin biological tissues, polymer materials, archaeometric specimens or magnetic thin films) with spatial resolutions in the regime of 20 nm and high spectroscopic or chemical sensitivity. However, due to the relatively large depth of focus of zone plates, the resolution of STXM along the optical axis so far stays unambiguously behind for thicker X-ray transparent specimens. This challenge can be addressed by the implementation of a second zone plate in the detection pathway of the beam, resulting in a confocal arrangement. Within this paper a first proof-of-principle study for a confocal STXM (cSTXM) and an elaborate alignment procedure in transmission and fluorescence geometry are presented. Based on first confocal soft X-ray micrographs of well known specimens, the advantage and limitation of cSTXM as well as further development potentials for future applications are discussed

Confocal soft X-ray scanning transmission microscopy: setup, alignment procedure and limitations

Energy Technology Data Exchange (ETDEWEB)

Späth, Andreas [Friedrich-Alexander Universität Erlangen-Nürnberg (FAU), Egerlandstraße 3, 91058 Erlangen (Germany); Raabe, Jörg [Paul Scherrer Institut, 5232 Villigen (Switzerland); Fink, Rainer H., E-mail: rainer.fink@fau.de [Friedrich-Alexander Universität Erlangen-Nürnberg (FAU), Egerlandstraße 3, 91058 Erlangen (Germany); Friedrich-Alexander Universität Erlangen-Nürnberg (FAU), Egerlandstraße 3, 91058 Erlangen (Germany)

2015-01-01

A conventional STXM setup has been upgraded with a second micro zone plate and aligned to confocal geometry. Two confocal geometries (in-line and off-axis) have been evaluated and a discussion on prospects and limitations is presented. Zone-plate-based scanning transmission soft X-ray microspectroscopy (STXM) is a well established technique for high-contrast imaging of sufficiently transparent specimens (e.g. ultrathin biological tissues, polymer materials, archaeometric specimens or magnetic thin films) with spatial resolutions in the regime of 20 nm and high spectroscopic or chemical sensitivity. However, due to the relatively large depth of focus of zone plates, the resolution of STXM along the optical axis so far stays unambiguously behind for thicker X-ray transparent specimens. This challenge can be addressed by the implementation of a second zone plate in the detection pathway of the beam, resulting in a confocal arrangement. Within this paper a first proof-of-principle study for a confocal STXM (cSTXM) and an elaborate alignment procedure in transmission and fluorescence geometry are presented. Based on first confocal soft X-ray micrographs of well known specimens, the advantage and limitation of cSTXM as well as further development potentials for future applications are discussed.

Soft x-ray spectroscopy for probing electronic and chemical states of battery materials

International Nuclear Information System (INIS)

Yang Wanli; Qiao Ruimin

2016-01-01

The formidable challenge of developing high-performance battery system stems from the complication of battery operations, both mechanically and electronically. In the electrodes and at the electrode–electrolyte interfaces, chemical reactions take place with evolving electron states. In addition to the extensive studies of material synthesis, electrochemical, structural, and mechanical properties, soft x-ray spectroscopy provides unique opportunities for revealing the critical electron states in batteries. This review discusses some of the recent soft x-ray spectroscopic results on battery binder, transition-metal based positive electrodes, and the solid-electrolyte-interphase. By virtue of soft x-ray’s sensitivity to electron states, the electronic property, the redox during electrochemical operations, and the chemical species of the interphases could be fingerprinted by soft x-ray spectroscopy. Understanding and innovating battery technologies need a multimodal approach, and soft x-ray spectroscopy is one of the incisive tools to probe the chemical and physical evolutions in batteries. (topical review)

Phosphor Scanner For Imaging X-Ray Diffraction

Science.gov (United States)

Carter, Daniel C.; Hecht, Diana L.; Witherow, William K.

1992-01-01

Improved optoelectronic scanning apparatus generates digitized image of x-ray image recorded in phosphor. Scanning fiber-optic probe supplies laser light stimulating luminescence in areas of phosphor exposed to x rays. Luminescence passes through probe and fiber to integrating sphere and photomultiplier. Sensitivity and resolution exceed previously available scanners. Intended for use in x-ray crystallography, medical radiography, and molecular biology.

Solar flare hard and soft x ray relationship determined from SMM HXRBS and BCS data

Science.gov (United States)

Toot, G. David

1989-01-01

The exact nature of the solar flare process is still somewhat a mystery. A key element to understanding flares if the relationship between the hard x rays emitted by the most energetic portions of the flare and the soft x rays from other areas and times. This relationship was studied by comparing hard x ray light curved from the Hard X-Ray Burst Spectrometer (HXRBS) with the soft x ray light curve and its derivation from the Bent Crystal Spectrometer (BCS) which is part of the X-Ray Polychrometer (XRP), these instruments being on the Solar Maximum Mission spacecraft (SMM). Data sample was taken from flares observed with the above instruments during 1980, the peak of the previous maximum of solar activity. Flares were chosen based on complete coverage of the event by several instruments. The HXRBS data covers the x ray spectrum from about 25 keV to about 440 keV in 15 spectral channels, while the BCS data used covers a region of the Spectrum around 3 angstroms including emission from the Ca XIX ion. Both sets of data were summed over their spectral ranges and plotted against time at a maximum time resolution of around 3 seconds. The most popular theory of flares holds that a beam of electrons produces the hard x rays by bremsstrahlung while the soft x rays are the thermal response to this energy deposition. The question is whether the rate of change of soft x ray emission might reflect the variability of the electron beam and hence the variability of the hard x rays. To address this, we took the time derivative of the soft x ray light curve and compared it to the hard flares, 12 of them showed very closed agreement between the soft x ray derivative and the hard x ray light curve. The other five did not show this behavior but were similar to each other in general soft x ray behavior. Efforts to determine basic differences between the two kinds of flares continue. In addition the behavior of soft x ray temperature of flares was examined.

Study of the optical and x-ray properties of quasars

International Nuclear Information System (INIS)

Bradley, S.E.

1985-01-01

It is now widely believed that photoionization by the central nucleus is primarily responsible for the emission lines observed in quasars. If this view is correct, x-ray wavelength photons from the nucleus could play a role in determining the emission line strengths of the various chemical species present in quasars. Indeed, recent photoionization models predict the enhancement of some emission lines arising from an extended ionized zone heated by soft x-rays. In an attempt to investigate this possibility, a sample of 17 quasars exhibiting a wide range of x-ray to optical luminosities has been observed spectrophotometrically in an effort to correlate their optical spectroscopic features with published x-ray and radio luminosities. Such correlations are known to exist for Seyfert galaxies, but at present it is unclear whether quasars also exhibit these correlations. All of the quasars in this sample have been previously observed with the Einstein Observatory. Strengths of the broad permitted emission lines as well as the narrow forbidden lines are analyzed for correlations with the x-ray strength and the optical strength; also, ratios of lines such as Hβ to [O III] and Fe II to Hβ are considered, as well as high excitation lines such as [Ne V]. Because of the difficulty in obtaining high signal-to-noise data for objects as faint as quasars, resolving this issue may well require many such studies as this one, each contributing a fraction of knowledge to the whole, before the question can adequately be answered

Imaging mammalian cells with soft x rays: The importance of specimen preparation

Energy Technology Data Exchange (ETDEWEB)

Brown, J.T.; Meyer-Ilse, W. [Ernest Orlando Lawrence Berkeley National Lab., CA (United States)

1997-04-01

Studies of mammalian cell structure and spatial organization are a very prominent part of modern cell biology. The interest in them as well as their size make them very accommodating subject specimens for imaging with soft x-rays using the XM-1 transmission microscope built and operated by The Center for X-ray Optics on Beam Line 6.1 at the Advanced Light Source. The purpose of these experiments was to determine if the fixative protocols normally used in electron or visible light microscopy were adequate to allow imaging cells, either fibroblasts or neurons, with minimal visible radiation damage due to imaging with soft x-rays at 2.4 nm. Two cell types were selected. Fibroblasts are easily cultured but fragile cells which are commonly used as models for the detailed study of cell physiology. Neurons are complex and sensitive cells which are difficult to prepare and to culture for study in isolation from their connections with surrounding cells. These cell types pose problems in their preparation for any microscopy. To improve the contrast and to prevent postmortem alteration of the chemistry and hence the structure of cells extracted from culture or from living organisms, fixation and staining techniques are employed in electron and visible light microscopy. It has been accepted by biologists for years that these treatments create artifacts and false structure. The authors have begun to develop protocols for specimens of each of these two cell types for soft x-ray microscopy which will preserve them in as near normal state as possible using minimal fixation, and make it possible to image them in either a hydrated or dried state free of secondary addition of stains or other labels.

Imaging mammalian cells with soft x rays: The importance of specimen preparation

International Nuclear Information System (INIS)

Brown, J.T.; Meyer-Ilse, W.

1997-01-01

Studies of mammalian cell structure and spatial organization are a very prominent part of modern cell biology. The interest in them as well as their size make them very accommodating subject specimens for imaging with soft x-rays using the XM-1 transmission microscope built and operated by The Center for X-ray Optics on Beam Line 6.1 at the Advanced Light Source. The purpose of these experiments was to determine if the fixative protocols normally used in electron or visible light microscopy were adequate to allow imaging cells, either fibroblasts or neurons, with minimal visible radiation damage due to imaging with soft x-rays at 2.4 nm. Two cell types were selected. Fibroblasts are easily cultured but fragile cells which are commonly used as models for the detailed study of cell physiology. Neurons are complex and sensitive cells which are difficult to prepare and to culture for study in isolation from their connections with surrounding cells. These cell types pose problems in their preparation for any microscopy. To improve the contrast and to prevent postmortem alteration of the chemistry and hence the structure of cells extracted from culture or from living organisms, fixation and staining techniques are employed in electron and visible light microscopy. It has been accepted by biologists for years that these treatments create artifacts and false structure. The authors have begun to develop protocols for specimens of each of these two cell types for soft x-ray microscopy which will preserve them in as near normal state as possible using minimal fixation, and make it possible to image them in either a hydrated or dried state free of secondary addition of stains or other labels

X-ray optics developments at ESA

DEFF Research Database (Denmark)

Bavdaz, M.; Wille, E.; Wallace, K.

2013-01-01

Future high energy astrophysics missions will require high performance novel X-ray optics to explore the Universe beyond the limits of the currently operating Chandra and Newton observatories. Innovative optics technologies are therefore being developed and matured by the European Space Agency (ESA......) in collaboration with research institutions and industry, enabling leading-edge future science missions. Silicon Pore Optics (SPO) [1 to 21] and Slumped Glass Optics (SGO) [22 to 29] are lightweight high performance X-ray optics technologies being developed in Europe, driven by applications in observatory class...... reflective coatings [30 to 35]. In addition, the progress with the X-ray test facilities and associated beam-lines is discussed [36]. © (2013) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only....

Theory and analysis of soft x-ray laser experiments

International Nuclear Information System (INIS)

Whitten, B.L.; Hazi, A.U.

1985-10-01

The atomic modeling of soft x-ray laser schemes presents a formidable challenge to the theorists - a challenge magnified by the recent successful experiments. A complex plasma environment with many ion species present must be simulated. Effects such as turbulence, time dependence, and radiation transport, which are very difficult to model accurately, may be important. We shall describe our efforts to model the recently demonstrated soft x-ray laser in collisionally pumped neon-like selenium, with emphasis on the ionization balance and excited state kinetics. The relative importance of various atomic processes, such as collisional excitation and dielectronic recombination, on the inversion kinetics will be demonstrated. We shall compare our models with experimental results and evaluate the success of this technique in predicting and analyzing the results of x-ray laser experiments. 22 refs., 5 figs., 3 tabs

A Test Facility For Astronomical X-Ray Optics

DEFF Research Database (Denmark)

Lewis, R. A.; Bordas, J.; Christensen, Finn Erland

1989-01-01

Grazing incidence x-ray optics for x-ray astronomical applications are used outside the earths atmosphere. These devices require a large collection aperture and the imaging of an x-ray source which is essentially placed at infinity. The ideal testing system for these optical elements has...... to approximate that encountered under working conditions, however the testing of these optical elements is notoriously difficult with conventional x-ray generators. Synchrotron Radiation (SR) sources are sufficiently brilliant to produce a nearly perfect parallel beam over a large area whilst still retaining...... a flux considerably higher than that available from conventional x-ray generators. A facility designed for the testing of x-ray optics, particularly in connection with x-ray telescopes is described below. It is proposed that this facility will be accommodated at the Synchrotron Radiation Source...

The structure of the coronal soft X-ray source associated with the dark filament disappearance of 1991 September 28 using the Yohkoh Soft X-ray Telescope

Science.gov (United States)

Mcallister, Alan; Uchida, Yutaka; Tsuneta, Saku; Strong, Keith T.; Acton, Loren W.; Hiei, Eijiro; Bruner, Marilyn E.; Watanabe, Takashi; Shibata, Kazunari

1992-01-01

The structure of the coronal soft X-ray source associated with the dark filament disappearance on September 28, 1991, observed with the Soft X-ray Telescope, is examined as a possible example of the 'eruption-reconnection' model of filament disappearance. The results suggest, however, that this model may not fit. There is a strong possibility that much of the dark filament mass remains in the heated unwinding axial field.

The superconducting high-resolution soft X-ray spectrometer at the advanced biological and environmental X-ray facility

Energy Technology Data Exchange (ETDEWEB)

Friedrich, S. [Advanced Detector Group, Lawrence Livermore National Laboratory, 7000 East Avenue, L-188, Livermore, CA 94550 (United States); Advanced Biological and Environmental X-ray Facility, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 94720 (United States)], E-mail: Friedrich1@llnl.gov; Drury, O.B. [Advanced Detector Group, Lawrence Livermore National Laboratory, 7000 East Avenue, L-188, Livermore, CA 94550 (United States); Advanced Biological and Environmental X-ray Facility, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 94720 (United States); Biophysics Group, University of California, 1 Shields Avenue, EU-III, Davis, CA 95616 (United States); George, S.J. [Advanced Biological and Environmental X-ray Facility, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 94720 (United States); Cramer, S.P. [Advanced Biological and Environmental X-ray Facility, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 94720 (United States); Biophysics Group, University of California, 1 Shields Avenue, EU-III, Davis, CA 95616 (United States)

2007-11-11

We have built a 36-pixel superconducting tunnel junction X-ray spectrometer for chemical analysis of dilute samples in the soft X-ray band. It offers an energy resolution of {approx}10-20 eV FWHM below 1 keV, a solid angle coverage of {approx}10{sup -3}, and can be operated at total rates of up to {approx}10{sup 6} counts/s. Here, we describe the spectrometer performance in speciation measurements by fluorescence-detected X-ray absorption spectroscopy at the Advanced Biological and Environmental X-ray facility at the ALS synchrotron.

Optical and X-ray studies of Compact X-ray Binaries in NGC 5904

Science.gov (United States)

Bhalotia, Vanshree; Beck-Winchatz, Bernhard

2018-06-01

Due to their high stellar densities, globular cluster systems trigger various dynamical interactions, such as the formation of compact X-ray binaries. Stellar collisional frequencies have been correlated to the number of X-ray sources detected in various clusters and we hope to measure this correlation for NGC 5904. Optical fluxes of sources from archival HST images of NGC 5904 have been measured using a DOLPHOT PSF photometry in the UV, optical and near-infrared. We developed a data analysis pipeline to process the fluxes of tens of thousands of objects using awk, python and DOLPHOT. We plot color magnitude diagrams in different photometric bands in order to identify outliers that could be X-ray binaries, since they do not evolve the same way as singular stars. Aligning previously measured astrometric data for X-ray sources in NGC 5904 from Chandra with archival astrometric data from HST will filter out the outlier objects that are not X-ray producing, and provide a sample of compact binary systems that are responsible for X-ray emission in NGC 5904. Furthermore, previously measured X-ray fluxes of NGC 5904 from Chandra have also been used to measure the X-ray to optical flux ratio and identify the types of compact X-ray binaries responsible for the X-ray emissions in NGC 5904. We gratefully acknowledge the support from the Illinois Space Grant Consortium.

Investigation of electronic order using resonant soft X-ray diffraction

Energy Technology Data Exchange (ETDEWEB)

Schlappa, J.

2006-12-01

The aim of this PhD work was the application of resonant soft X-ray diffraction technique for the investigation of electronic order in transition metal oxides at the TM L{sub 2,3}-edge, trying to obtain a quantitative understanding of the data. The method was first systematically explored through application to a model system in order to test the feasibility of the technique and to understand of how X-ray optical effects have to be taken into account. Two more complex systems were investigated; stripe order in La{sub 1.8}Sr{sub 0.2}NiO{sub 4} and charge and orbital order in Fe{sub 3}O{sub 4}. The main focus of the work was on the spectroscopic potential of the technique, trying to obtain a level of quantitative description of the data. For X-ray absorption spectroscopy (XAS) from transition metal oxides, cluster configuration interaction calculation provides a powerful and realistic microscopic theory. In the frame work of this thesis cluster theory, considering explicit hybridization effects between the TM-ion and the surrounding oxygen ligands, has been applied for the first time to describe resonant diffraction data. (orig.)

Investigation of electronic order using resonant soft X-ray diffraction

International Nuclear Information System (INIS)

Schlappa, J.

2006-01-01

The aim of this PhD work was the application of resonant soft X-ray diffraction technique for the investigation of electronic order in transition metal oxides at the TM L 2,3 -edge, trying to obtain a quantitative understanding of the data. The method was first systematically explored through application to a model system in order to test the feasibility of the technique and to understand of how X-ray optical effects have to be taken into account. Two more complex systems were investigated; stripe order in La 1.8 Sr 0.2 NiO 4 and charge and orbital order in Fe 3 O 4 . The main focus of the work was on the spectroscopic potential of the technique, trying to obtain a level of quantitative description of the data. For X-ray absorption spectroscopy (XAS) from transition metal oxides, cluster configuration interaction calculation provides a powerful and realistic microscopic theory. In the frame work of this thesis cluster theory, considering explicit hybridization effects between the TM-ion and the surrounding oxygen ligands, has been applied for the first time to describe resonant diffraction data. (orig.)

Optics-free x-ray FEL oscillator

International Nuclear Information System (INIS)

Litvinenko, V.N.; Hao, Y.; Kayran, D.; Trbojevic, D.

2011-01-01

There is a need for an Optics-Free FEL Oscillators (OFFELO) to further the advantages of free-electron lasers and turning them in fully coherent light sources. While SASE (Self-Amplified Spontaneous Emission) FELs demonstrated the capability of providing very high gain and short pulses of radiation and scalability to the X-ray range, the spectra of SASE FELs remains rather wide (∼0.5%-1%) compared with typical short wavelengths FEL-oscillators (0.01%-0.0003% in OK-4 FEL). Absence of good optics in VUV and X-ray ranges makes traditional oscillator schemes with very high average and peak spectral brightness either very complex or, strictly speaking, impossible. In this paper, we discuss lattice of the X-ray optics-free FEL oscillator and present results of initial computer simulations of the feedback process and the evolution of FEL spectrum in X-ray OFFELO. We also discuss main limiting factors and feasibility of X-ray OFFELO.

Optics-free x-ray FEL oscillator

Energy Technology Data Exchange (ETDEWEB)

Litvinenko, V.N.; Hao, Y.; Kayran, D.; Trbojevic, D.

2011-03-28

There is a need for an Optics-Free FEL Oscillators (OFFELO) to further the advantages of free-electron lasers and turning them in fully coherent light sources. While SASE (Self-Amplified Spontaneous Emission) FELs demonstrated the capability of providing very high gain and short pulses of radiation and scalability to the X-ray range, the spectra of SASE FELs remains rather wide ({approx}0.5%-1%) compared with typical short wavelengths FEL-oscillators (0.01%-0.0003% in OK-4 FEL). Absence of good optics in VUV and X-ray ranges makes traditional oscillator schemes with very high average and peak spectral brightness either very complex or, strictly speaking, impossible. In this paper, we discuss lattice of the X-ray optics-free FEL oscillator and present results of initial computer simulations of the feedback process and the evolution of FEL spectrum in X-ray OFFELO. We also discuss main limiting factors and feasibility of X-ray OFFELO.

Coherent Sources of XUV Radiation Soft X-Ray Lasers and High-Order Harmonic Generation

CERN Document Server

Jaeglé, Pierre

2006-01-01

Extreme ultraviolet radiation, also referred to as soft X-rays or XUV, offers very special optical properties. The X-UV refractive index of matter is such that normal reflection cannot take place on polished surfaces whereas beam transmission through one micrometer of almost all materials reduces to zero. Therefore, it has long been a difficult task to imagine and to implement devices designed for complex optics experiments in this wavelength range. Thanks to new sources of coherent radiation - XUV-lasers and High Order Harmonics - the use of XUV radiation, for interferometry, holography, diffractive optics, non-linear radiation-matter interaction, time-resolved study of fast and ultrafast phenomena and many other applications, including medical sciences, is ubiquitous.

53 W average power few-cycle fiber laser system generating soft x rays up to the water window.

Science.gov (United States)

Rothhardt, Jan; Hädrich, Steffen; Klenke, Arno; Demmler, Stefan; Hoffmann, Armin; Gotschall, Thomas; Eidam, Tino; Krebs, Manuel; Limpert, Jens; Tünnermann, Andreas

2014-09-01

We report on a few-cycle laser system delivering sub-8-fs pulses with 353 μJ pulse energy and 25 GW of peak power at up to 150 kHz repetition rate. The corresponding average output power is as high as 53 W, which represents the highest average power obtained from any few-cycle laser architecture so far. The combination of both high average and high peak power provides unique opportunities for applications. We demonstrate high harmonic generation up to the water window and record-high photon flux in the soft x-ray spectral region. This tabletop source of high-photon flux soft x rays will, for example, enable coherent diffractive imaging with sub-10-nm resolution in the near future.

Overview of nanoscale NEXAFS performed with soft X-ray microscopes

Directory of Open Access Journals (Sweden)

Peter Guttmann

2015-02-01

Full Text Available Today, in material science nanoscale structures are becoming more and more important. Not only for the further miniaturization of semiconductor devices like carbon nanotube based transistors, but also for newly developed efficient energy storage devices, gas sensors or catalytic systems nanoscale and functionalized materials have to be analysed. Therefore, analytical tools like near-edge X-ray absorption fine structure (NEXAFS spectroscopy has to be applied on single nanostructures. Scanning transmission X-ray microscopes (STXM as well as full-field transmission X-ray microscopes (TXM allow the required spatial resolution to study individual nanostructures. In the soft X-ray energy range only STXM was used so far for NEXAFS studies. Due to its unique setup, the TXM operated by the Helmholtz-Zentrum Berlin (HZB at the electron storage ring BESSY II is the first one in the soft X-ray range which can be used for NEXAFS spectroscopy studies which will be shown in this review. Here we will give an overview of the different microscopes used for NEXAFS studies and describe their advantages and disadvantages for different samples.

Overview of nanoscale NEXAFS performed with soft X-ray microscopes.

Science.gov (United States)

Guttmann, Peter; Bittencourt, Carla

2015-01-01

Today, in material science nanoscale structures are becoming more and more important. Not only for the further miniaturization of semiconductor devices like carbon nanotube based transistors, but also for newly developed efficient energy storage devices, gas sensors or catalytic systems nanoscale and functionalized materials have to be analysed. Therefore, analytical tools like near-edge X-ray absorption fine structure (NEXAFS) spectroscopy has to be applied on single nanostructures. Scanning transmission X-ray microscopes (STXM) as well as full-field transmission X-ray microscopes (TXM) allow the required spatial resolution to study individual nanostructures. In the soft X-ray energy range only STXM was used so far for NEXAFS studies. Due to its unique setup, the TXM operated by the Helmholtz-Zentrum Berlin (HZB) at the electron storage ring BESSY II is the first one in the soft X-ray range which can be used for NEXAFS spectroscopy studies which will be shown in this review. Here we will give an overview of the different microscopes used for NEXAFS studies and describe their advantages and disadvantages for different samples.

Key electronic states in lithium battery materials probed by soft X-ray spectroscopy

International Nuclear Information System (INIS)

Yang, Wanli; Liu, Xiaosong; Qiao, Ruimin; Olalde-Velasco, Paul; Spear, Jonathan D.; Roseguo, Louis; Pepper, John X.; Chuang, Yi-de; Denlinger, Jonathan D.; Hussain, Zahid

2013-01-01

Highlights: •Key electronic states in battery materials revealed by soft X-ray spectroscopy. •Soft X-ray absorption consistently probes Mn oxidation states in different systems. •Soft X-ray absorption and emission fingerprint battery operations in LiFePO 4 . •Spectroscopic guidelines for selecting/optimizing polymer materials for batteries. •Distinct SEI formation on same electrode material with different crystal orientations. -- Abstract: The formidable challenges for developing a safe, low-cost, high-capacity, and high-power battery necessitate employing advanced tools that are capable of directly probing the key electronic states relevant to battery performance. Synchrotron based soft X-ray spectroscopy directly measures both the occupied and unoccupied states in the vicinity of the Fermi level, including transition-metal-3d and anion-p states. This article presents the basic concepts on how fundamental physics in electronic structure could provide valuable information for lithium-ion battery applications. We then discuss some of our recent studies on transition-metal oxide based cathodes, silicon based anode, and solid-electrolyte-interphase through soft X-ray absorption and emission spectroscopy. We argue that spectroscopic results reveal the evolution of electronic states for fingerprinting, understanding, and optimizing lithium-ion battery operations

Laboratory characterization of Woelter x-ray optics

International Nuclear Information System (INIS)

Remington, B.A.; Morales, R.I.

1994-04-01

We have conducted an extensive series of characterization measurements of a Woe1ter incidence x-ray microscope. The measurements were carried out on 5% sectors of the Woe1ter x-ray optic in a laboratory utilizing a high brightness, ''point'' x-ray source and fall into two categories. (1) Absolute reflectance measurements as a function of x-ray energy were made with Si(Li) detectors to acquire continuum spectra prior to and after reflecting off the Woe1ter optic. (2) Spatial resolution measurements were made using back-illuminated pinholes or grids imaged onto film or an x-ray CCD camera. The depth of field was mapped out by varying the distance between the Woe1ter optic and the backlit grid

Soft x-ray imager (SXI) onboard the NeXT satellite

Science.gov (United States)

Tsuru, Takeshi Go; Takagi, Shin-Ichiro; Matsumoto, Hironori; Inui, Tatsuya; Ozawa, Midori; Koyama, Katsuji; Tsunemi, Hiroshi; Hayashida, Kiyoshi; Miyata, Emi; Ozawa, Hideki; Touhiguchi, Masakuni; Matsuura, Daisuke; Dotani, Tadayasu; Ozaki, Masanobu; Murakami, Hiroshi; Kohmura, Takayoshi; Kitamoto, Shunji; Awaki, Hisamitsu

2006-06-01

We give overview and the current status of the development of the Soft X-ray Imager (SXI) onboard the NeXT satellite. SXI is an X-ray CCD camera placed at the focal plane detector of the Soft X-ray Telescopes for Imaging (SXT-I) onboard NeXT. The pixel size and the format of the CCD is 24 x 24μm (IA) and 2048 x 2048 x 2 (IA+FS). Currently, we have been developing two types of CCD as candidates for SXI, in parallel. The one is front illumination type CCD with moderate thickness of the depletion layer (70 ~ 100μm) as a baseline plan. The other one is the goal plan, in which we develop back illumination type CCD with a thick depletion layer (200 ~ 300μm). For the baseline plan, we successfully developed the proto model 'CCD-NeXT1' with the pixel size of 12μm x 12μm and the CCD size of 24mm x 48mm. The depletion layer of the CCD has reached 75 ~ 85μm. The goal plan is realized by introduction of a new type of CCD 'P-channel CCD', which collects holes in stead of electrons in the common 'N-channel CCD'. By processing a test model of P-channel CCD we have confirmed high quantum efficiency above 10 keV with an equivalent depletion layer of 300μm. A back illumination type of P-channel CCD with a depletion layer of 200μm with aluminum coating for optical blocking has been also successfully developed. We have been also developing a thermo-electric cooler (TEC) with the function of the mechanically support of the CCD wafer without standoff insulators, for the purpose of the reduction of thermal input to the CCD through the standoff insulators. We have been considering the sensor housing and the onboard electronics for the CCD clocking, readout and digital processing of the frame date.

Optical Synchronization Systems for Femtosecond X-Ray Sources

CERN Document Server

Wilcox, Russell; Staples, John W

2005-01-01

In femtosecond pump/probe experiments using short x-ray and optical pulses, precise synchronization must be maintained between widely separated lasers in a synchrotron or FEL facility. We are developing synchronization systems using optical signals for applications requiring different ranges of timing error. For the sub-100fs range we use an amplitude modulated CW laser at 1GHz to transmit RF phase information, and control the delay through a 100m fiber by observing the retroreflected signal. Initial results show 40fs peak-to-peak error above 10Hz, and 200fs long term drift, mainly due to amplitude sensitivity in the analog mixers. For the sub-10fs range we will lock two single-frequency lasers separated by several teraHertz to a master modelocked fiber laser, transmit the two frequencies over fiber, and lock two comb lines of a slave laser to these frequencies, thus synchronizing the two modelocked laser envelopes. For attosecond synchronization we propose a stabilized, free space link using bulk lens wavegu...

THE STRUCTURE OF THE X-RAY AND OPTICAL EMITTING REGIONS OF THE LENSED QUASAR Q 2237+0305

International Nuclear Information System (INIS)

Mosquera, A. M.; Kochanek, C. S.; Blackburne, J. A.; Chen, B.; Dai, X.; Chartas, G.

2013-01-01

We use gravitational microlensing to determine the size of the X-ray and optical emission regions of the quadruple lens system Q 2237+0305. The optical half-light radius, log(R 1/2,V /cm) = 16.41 ± 0.18 (at λ rest = 2018 Å), is significantly larger than the observed soft, log(R 1/2,soft /cm)=15.76 +0.41 -0.34 (1.1-3.5 keV in the rest frame), and hard, log(R 1/2,hard /cm)=15.46 +0.34 -0.29 (3.5-21.5 keV in the rest frame), band X-ray emission. There is weak evidence that the hard component is more compact than the soft, with log(R 1/2,soft /R 1/2,hard )≅0.30 +0.53 -0.45 . This wavelength-dependent structure agrees with recent results found in other lens systems using microlensing techniques, and favors geometries in which the corona is concentrated near the inner edge of the accretion disk. While the available measurements are limited, the size of the X-ray emission region appears to be roughly proportional to the mass of the central black hole.

Perfect-crystal x-ray optics to treat x-ray coherence

International Nuclear Information System (INIS)

Yamazaki, Hiroshi; Ishikawa, Tetsuya

2007-01-01

X-ray diffraction of perfect crystals, which serve as x-ray monochromator and collimator, modifies coherence properties of x-ray beams. From the time-dependent Takagi-Taupin equations that x-ray wavefields obey in crystals, the reflected wavefield is formulated as an integral transform of a general incident wavefield with temporal and spatial inhomogeneity. A reformulation of rocking-curve profiles from the field solution of the Takagi-Taupin equations allows experimental evaluation of the mutual coherence function of x-ray beam. The rigorous relationship of the coherence functions between before and after reflection clarifies how the coherence is transferred by a crystal. These results will be beneficial to developers of beamline optics for the next generation synchrotron sources. (author)

Broadband interference lithography at extreme ultraviolet and soft x-ray wavelengths.

Science.gov (United States)

Mojarad, Nassir; Fan, Daniel; Gobrecht, Jens; Ekinci, Yasin

2014-04-15

Manufacturing efficient and broadband optics is of high technological importance for various applications in all wavelength regimes. Particularly in the extreme ultraviolet and soft x-ray spectra, this becomes challenging due to the involved atomic absorption edges that rapidly change the optical constants in these ranges. Here we demonstrate a new interference lithography grating mask that can be used for nanopatterning in this spectral range. We demonstrate photolithography with cutting-edge resolution at 6.5 and 13.5 nm wavelengths, relevant to the semiconductor industry, as well as using 2.5 and 4.5 nm wavelength for patterning thick photoresists and fabricating high-aspect-ratio metal nanostructures for plasmonics and sensing applications.

X-ray magneto-optic KERR effect studies of spring magnet heterostructures.

Energy Technology Data Exchange (ETDEWEB)

Kortright, J. B.; Kim, S.-K.; Fullerton, E. E.; Jiang, J. S.; Bader, S. D.

2000-11-01

The complex 3-dimensional magnetization reversal behavior of Sin-Co/Fe exchange spring films is used to test the sensitivity of different resonant soft x-ray magneto-optical Kerr effect (MOKE) measurements to changes in longitudinal and transverse moments within the SOIIFe layer and to changes in these moments in depth within the Fe layer. As in the visible MOKE, changes in longitudinal and net transverse moments are resolved by measuring both Kerr rotation and intensity loops in the near the Fe 2p core resonance. These x-ray MOKE signals measured using linear incident polarization are more directly interpreted in terms of longitudinal and transverse moments than are the same signals measured using elliptical polarization. Varying photon energy near the Fe L3line is shown to be an effective means of resolving distinctly different reversal behavior at the top and bottom of the 20 nm thick Fe layer resulting from the strong exchange coupling at the Sin-Co/Fe interface. Measured x-ray MOKE spectra and signals are in qualitative agreement with those calculated using standard magneto-optical formalisms incorporating interference between different layers and measured helicity-dependent magneto-optical constants for Fe.

Development of variable-magnification X-ray Bragg optics.

Science.gov (United States)

Hirano, Keiichi; Yamashita, Yoshiki; Takahashi, Yumiko; Sugiyama, Hiroshi

2015-07-01

A novel X-ray Bragg optics is proposed for variable-magnification of an X-ray beam. This X-ray Bragg optics is composed of two magnifiers in a crossed arrangement, and the magnification factor, M, is controlled through the azimuth angle of each magnifier. The basic properties of the X-ray optics such as the magnification factor, image transformation matrix and intrinsic acceptance angle are described based on the dynamical theory of X-ray diffraction. The feasibility of the variable-magnification X-ray Bragg optics was verified at the vertical-wiggler beamline BL-14B of the Photon Factory. For X-ray Bragg magnifiers, Si(220) crystals with an asymmetric angle of 14° were used. The magnification factor was calculated to be tunable between 0.1 and 10.0 at a wavelength of 0.112 nm. At various magnification factors (M ≥ 1.0), X-ray images of a nylon mesh were observed with an air-cooled X-ray CCD camera. Image deformation caused by the optics could be corrected by using a 2 × 2 transformation matrix and bilinear interpolation method. Not only absorption-contrast but also edge-contrast due to Fresnel diffraction was observed in the magnified images.

Fiber-optic dosimeters for radiation therapy

Science.gov (United States)

Li, Enbang; Archer, James

2017-10-01

According to the figures provided by the World Health Organization, cancer is a leading cause of death worldwide, accounting for 8.8 million deaths in 2015. Radiation therapy, which uses x-rays to destroy or injure cancer cells, has become one of the most important modalities to treat the primary cancer or advanced cancer. The newly developed microbeam radiation therapy (MRT), which uses highly collimated, quasi-parallel arrays of x-ray microbeams (typically 50 μm wide and separated by 400 μm) produced by synchrotron sources, represents a new paradigm in radiotherapy and has shown great promise in pre-clinical studies on different animal models. Measurements of the absorbed dose distribution of microbeams are vitally important for clinical acceptance of MRT and for developing quality assurance systems for MRT, hence are a challenging and important task for radiation dosimetry. On the other hand, during the traditional LINAC based radiotherapy and breast cancer brachytherapy, skin dose measurements and treatment planning also require a high spatial resolution, tissue equivalent, on-line dosimeter that is both economical and highly reliable. Such a dosimeter currently does not exist and remains a challenge in the development of radiation dosimetry. High resolution, water equivalent, optical and passive x-ray dosimeters have been developed and constructed by using plastic scintillators and optical fibers. The dosimeters have peak edge-on spatial resolutions ranging from 50 to 500 microns in one dimension, with a 10 micron resolution dosimeter under development. The developed fiber-optic dosimeters have been test with both LINAC and synchrotron x-ray beams. This work demonstrates that water-equivalent and high spatial resolution radiation detection can be achieved with scintillators and optical fiber systems. Among other advantages, the developed fiber-optic probes are also passive, energy independent, and radiation hard.

Present status and future prospect of x-ray microscopes. Is it possible to realize x-ray 1 nm imaging?

International Nuclear Information System (INIS)

Aoki, Sadao

2010-01-01

High resolution X-ray imaging has been developed by using various optical elements and optical systems. In the soft X-ray region (∼3 nm) about 20 nm spatial resolution has been obtained, while in the hard X-ray (∼0.1 nm) about 50 nm. In the research frontier the spatial resolution better than 10 nm has been reported. The possibility to approach 1 nm spatial resolution is presented. (author)

Soft X-ray beam induced current technique

Energy Technology Data Exchange (ETDEWEB)

Watts, B; Ade, H [Department of Physics, North Carolina State University, Raleigh, NC 27695 (United States); Queen, D; Hellman, F [Department of Physics, University of California, Berkeley, CA 94720 (United States); Kilcoyne, A L D; Tyliszczak, T, E-mail: benjamin.watts@gmail.co [Advanced Light Source, Lawrence Berkeley Nat. Lab., Berkeley, CA 94720 (United States)

2009-09-01

Direct mapping of the charge transport efficiency of polymer solar cell devices using a soft X-ray beam induced current (SoXBIC) method is described. By fabricating a polymer solar cell on an x-ray transparent substrate, we demonstrate the ability to map polymer composition and nanoscale structure within an operating solar cell device and to simultaneously measure the local charge transport efficiency via the short-circuit current. A simple model is calculated and compared to experimental SoXBIC data of a PFB:F8BT bulk-heterojunction device in order to gain greater insight into the device operation and physics.

Soft X-ray multilayers and filters

CERN Document Server

Wang Zhan Shan; Tang Wei Xing; Qin Shuji; Zhou Bing; Chen Ling Ya

2002-01-01

The periodic and non-periodic multilayers were designed by using a random number to change each layer and a suitable merit function. Ion beam sputtering and magnetron sputtering were used to fabricate various multilayers and beam splitters in soft X-ray range. The characterization of multilayers by small angle X-ray diffraction, Auger electron spectroscopy, Rutherford back scattering spectroscopy and reflectivity illustrated the multilayers had good structures and smooth interlayers. The reflectivity and transmission of a beam splitter is about 5%. The fabrication and transmission properties of Ag, Zr were studied. The Rutherford back scattering spectroscopy and auger electron spectroscopy were used to investigate the contents and distributions of impurities and influence on qualities of filters. The attenuation coefficients were corrected by the data obtained by measurements

Method for spatially modulating X-ray pulses using MEMS-based X-ray optics

Science.gov (United States)

Lopez, Daniel; Shenoy, Gopal; Wang, Jin; Walko, Donald A.; Jung, Il-Woong; Mukhopadhyay, Deepkishore

2015-03-10

A method and apparatus are provided for spatially modulating X-rays or X-ray pulses using microelectromechanical systems (MEMS) based X-ray optics. A torsionally-oscillating MEMS micromirror and a method of leveraging the grazing-angle reflection property are provided to modulate X-ray pulses with a high-degree of controllability.

Innovative diffraction gratings for high-resolution resonant inelastic soft x-ray scattering spectroscopy

International Nuclear Information System (INIS)

Voronov, D.L.; Warwick, T.; Gullikson, E. M.; Salmassi, F.; Padmore, H. A.

2016-01-01

High-resolution Resonant Inelastic X-ray Scattering (RIXS) requires diffraction gratings with very exacting characteristics. The gratings should provide both very high dispersion and high efficiency which are conflicting requirements and extremely challenging to satisfy in the soft x-ray region for a traditional grazing incidence geometry. To achieve high dispersion one should increase the groove density of a grating; this however results in a diffraction angle beyond the critical angle range and results in drastic efficiency loss. The problem can be solved by use of multilayer coated blazed gratings (MBG). In this work we have investigated the diffraction characteristics of MBGs via numerical simulations and have developed a procedure for optimization of grating design for a multiplexed high resolution imaging spectrometer for RIXS spectroscopy to be built in sector 6 at the Advanced Light Source (ALS). We found that highest diffraction efficiency can be achieved for gratings optimized for 4"t"h or 5"t"h order operation. Fabrication of such gratings is an extremely challenging technological problem. We present a first experimental prototype of these gratings and report its performance. High order and high line density gratings have the potential to be a revolutionary new optical element that should have great impact in the area of soft x-ray RIXS.

Progress toward a soft X-ray FEL

International Nuclear Information System (INIS)

Pellegrini, C.

1988-01-01

We review the FEL physics and obtain scaling laws for the extension of its operation to the soft X-ray region. We also discuss the properties of an electron beam needed to drive such an FEL, and the present state of the art for the beam production. (orig.)

Soft x-ray emission from the direction of the Coma cluster

International Nuclear Information System (INIS)

Hayakawa, Satio; Tanaka, Yasuo; Yamashita, Koujun; Bleeker, J.A.M.; Deerenberg, A.J.M.

1975-01-01

A soft X-ray source was observed in the direction of the Coma cluster. The flux in the energy range 0.2--0.4 keV was found to change within a time scale shorter than 80 s. The fast transient and the energy spectrum prohibit identification of this source with the Coma cluster. It is suggested that this source belongs to a class of nearby transient soft X-ray sources. (auth.)

Observations of several disruptions in PLT using soft and ultra-soft x-ray radiation

International Nuclear Information System (INIS)

Eames, D.R.; von Goeler, S.; Sauthoff, N.R.; Stodiek, W.

1979-03-01

The evolution of ultra-soft x-ray radiation (USX, hν approx. > 100 eV) is compared to that of the soft x-ray radiation (SX, hν approx. > 1000 eV) during several disruptions in PLT. Spatial resolution is obtained in both cases by arrays of silicon surface barrier detectors viewing along different chords. During some disruptions the USX behaves quite differently from the SX, and a classification is made based on the USX behavior. Different interpretations of the data are discussed, along with the possibility that these measurements may distinguish between the roles of temperature and impurity density changes during disruptions

Coordinated soft X-ray and H-alpha observation of solar flares

Science.gov (United States)

Zarro, D. M.; Canfield, R. C.; Metcalf, T. R.; Lemen, J. R.

1988-01-01

Soft X-ray, Ca XIX, and H-alpha observations obtained for a set of four solar flares in the impulsive phase are analyzed. A blue asymmetry was observed in the coronal Ca XIX line during the soft-Xray rise phase in all of the events. A red asymmetry was observed simultaneously in chromospheric H-alpha at spatial locations associated with enhanced flare heating. It is shown that the impulsive phase momentum of upflowing soft X-ray plasma equalled that of the downflowing H-alpha plasma to within an order of magnitude. This supports the explosive chromospheric evaporation model of solar flares.

Thin absorbers for large-area soft X-ray microcalorimeters

Energy Technology Data Exchange (ETDEWEB)

Rocks, L. [Department of Physics, University of Wisconsin, Madison, WI 53706 (United States)]. E-mail: rocks@wisp.physics.wisc.edu; Anderson, M.B. [Department of Physics, University of Wisconsin, Madison, WI 53706 (United States); Bilgri, N. [Department of Physics, University of Wisconsin, Madison, WI 53706 (United States); Brekosky, R. [NASA/Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Gwynne Crowder, S. [Department of Physics, University of Wisconsin, Madison, WI 53706 (United States); Figueroa-Feliciano, E. [NASA/Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Kelley, R. [NASA/Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Kilbourne, C.A. [NASA/Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Lai, T. [Department of Physics, University of Wisconsin, Madison, WI 53706 (United States); Lindeman, M.A. [Department of Physics, University of Wisconsin, Madison, WI 53706 (United States); Man, J. [Department of Physics, University of Wisconsin, Madison, WI 53706 (United States); McCammon, D. [Department of Physics, University of Wisconsin, Madison, WI 53706 (United States); Nelms, K.L. [Department of Physics, University of Wisconsin, Madison, WI 53706 (United States); Porter, F.S. [NASA/Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Sivananthan, S. [University of Illinois at Chicago, Chicago, IL 60607 (United States); Vidugiris, G. [Department of Physics, University of Wisconsin, Madison, WI 53706 (United States); Zhao, J. [University of Illinois at Chicago, Chicago, IL 60607 (United States)

2006-04-15

The X-ray Quantum Calorimeter (XQC) sounding rocket experiment utilizes a microcalorimeter array for observing the diffuse soft X-ray background. Observations of such low surface-brightness targets require a large-area detector. We will be using an array of large absorbers. Good absorbers must rapidly and completely thermalize photons, have small heat capacity for high stopping efficiency and have good lateral thermal transport. For observing the soft X-ray background (energies <1 keV), the volume and heat capacity of absorber material can be kept to a minimum by making the absorbers only as thick as needed for high quantum efficiency at these low energies. These thin, large-area absorbers are not self-supporting and have poor lateral heat transport. Depositing the absorber material on a Si substrate provides support and improves lateral thermal conduction. We present heat capacity results for thin HgTe and thin Bi, each on Si substrates. We also describe the HgTe absorber fabrication.

The Correlation between Hard X-Ray Peak Flux and Soft X-Ray Peak Flux in the Outburst Rise of Low-Mass X-Ray Binaries

NARCIS (Netherlands)

Yu, W.; van der Klis, M.; Fender, R.P.

2004-01-01

We have analyzed Rossi X-Ray Timing Explorer pointed observations of the outbursts of black hole and neutron star soft X-ray transients in which an initial low/hard state, or ``island'' state, followed by a transition to a softer state was observed. In three sources-the black hole transient XTE

Optical metrology for analysis of lobster-eye x-ray optics

International Nuclear Information System (INIS)

Irving, Thomas H.K.; Peele, Andrew G.; Nugent, Keith A.

2003-01-01

A new method that uses optical microscopy to determine the physical structure of lobster-eye x-ray optics is described. This approach offers the ability to predict x-ray performance without having to take an x-ray measurement. An overlapping series of images of the entrance and exit faces of an optic are obtained and examined by purpose-built software. A 24-parameter description of each channel is obtained from which a quantitative analysis of all the major optic defects, except surface roughness, is performed. Results for a planar lobster-eye optic are used to illustrate this technique and discuss its abilities as well as directions for future enhancements

Fast Soft X-ray Images of MHD Phenomena in NSTX

International Nuclear Information System (INIS)

Bush, C.E.; Stratton, B.C.; Robinson, J.; Zakharov, L.E.; Fredrickson, E.D.; Stutman, D.; Tritz, K.

2008-01-01

A variety of magnetohydrodynamic (MHD) phenomena have been observed on the National Spherical Torus Experiment (NSTX). Many of these affect fast particle losses, which are of major concern for future burning plasma experiments. Usual diagnostics for studying these phenomena are arrays of Mirnov coils for magnetic oscillations and PIN diode arrays for soft x-ray emission from the plasma core. Data reported here are from an unique fast soft x-ray imaging camera (FSXIC) with a wide-angle (pinhole) tangential view of the entire plasma minor cross section. The camera provides a 64x64 pixel image, on a CCD chip, of light resulting from conversion of soft x-rays incident on a phosphor to the visible. We have acquired plasma images at frame rates of 1-500 kHz (300 frames/shot), and have observed a variety of MHD phenomena: disruptions, sawteeth, fishbones, tearing modes, and ELMs. New data including modes with frequency > 90 kHz are also presented. Data analysis and modeling techniques used to interpret the FSXIC data are described and compared, and FSXIC results are compared to Mirnov and PIN diode array results.

Design and optimization of the grating monochromator for soft X-ray self-seeding FELs

Energy Technology Data Exchange (ETDEWEB)

Serkez, Svitozar

2015-10-15

The emergence of Free Electron Lasers (FEL) as a fourth generation of light sources is a breakthrough. FELs operating in the X-ray range (XFEL) allow one to carry out completely new experiments that probably most of the natural sciences would benefit. Self-amplified spontaneous emission (SASE) is the baseline FEL operation mode: the radiation pulse starts as a spontaneous emission from the electron bunch and is being amplified during an FEL process until it reaches saturation. The SASE FEL radiation usually has poor properties in terms of a spectral bandwidth or, on the other side, longitudinal coherence. Self-seeding is a promising approach to narrow the SASE bandwidth of XFELs significantly in order to produce nearly transformlimited pulses. It is achieved by the radiation pulse monochromatization in the middle of an FEL amplification process. Following the successful demonstration of the self-seeding setup in the hard X-ray range at the LCLS, there is a need for a self-seeding extension into the soft X-ray range. Here a numerical method to simulate the soft X-ray self seeding (SXRSS) monochromator performance is presented. It allows one to perform start-to-end self-seeded FEL simulations along with (in our case) GENESIS simulation code. Based on this method, the performance of the LCLS self-seeded operation was simulated showing a good agreement with an experiment. Also the SXRSS monochromator design developed in SLAC was adapted for the SASE3 type undulator beamline at the European XFEL. The optical system was studied using Gaussian beam optics, wave optics propagation method and ray tracing to evaluate the performance of the monochromator itself. Wave optics analysis takes into account the actual beam wavefront of the radiation from the coherent FEL source, third order aberrations and height errors from each optical element. The monochromator design is based on a toroidal VLS grating working at a fixed incidence angle mounting without both entrance and exit

Design and optimization of the grating monochromator for soft X-ray self-seeding FELs

International Nuclear Information System (INIS)

Serkez, Svitozar

2015-10-01

The emergence of Free Electron Lasers (FEL) as a fourth generation of light sources is a breakthrough. FELs operating in the X-ray range (XFEL) allow one to carry out completely new experiments that probably most of the natural sciences would benefit. Self-amplified spontaneous emission (SASE) is the baseline FEL operation mode: the radiation pulse starts as a spontaneous emission from the electron bunch and is being amplified during an FEL process until it reaches saturation. The SASE FEL radiation usually has poor properties in terms of a spectral bandwidth or, on the other side, longitudinal coherence. Self-seeding is a promising approach to narrow the SASE bandwidth of XFELs significantly in order to produce nearly transformlimited pulses. It is achieved by the radiation pulse monochromatization in the middle of an FEL amplification process. Following the successful demonstration of the self-seeding setup in the hard X-ray range at the LCLS, there is a need for a self-seeding extension into the soft X-ray range. Here a numerical method to simulate the soft X-ray self seeding (SXRSS) monochromator performance is presented. It allows one to perform start-to-end self-seeded FEL simulations along with (in our case) GENESIS simulation code. Based on this method, the performance of the LCLS self-seeded operation was simulated showing a good agreement with an experiment. Also the SXRSS monochromator design developed in SLAC was adapted for the SASE3 type undulator beamline at the European XFEL. The optical system was studied using Gaussian beam optics, wave optics propagation method and ray tracing to evaluate the performance of the monochromator itself. Wave optics analysis takes into account the actual beam wavefront of the radiation from the coherent FEL source, third order aberrations and height errors from each optical element. The monochromator design is based on a toroidal VLS grating working at a fixed incidence angle mounting without both entrance and exit

Soft x-ray tomography on the Alcator C tokamak

International Nuclear Information System (INIS)

Camacho, J.F.

1985-06-01

A soft x-ray tomography experiment has been performed on the Alcator C tokamak. An 80-chord array of detectors consisting of miniature PIN photodiodes was used to obtain tomographic reconstructions of the soft x-ray emissivity function's poloidal cross-section. The detectors are located around the periphery of the plasma at one toroidal location (top and bottom ports) and are capable of yielding useful information over a wide range of plasma operating parameters and conditions. The reconstruction algorithm employed makes no assumption whatsoever about plasma rotation, position, or symmetry. Its performance was tested, and it was found to work well and to be fairly insensitive to estimated levels of random and systematic errors in the data

Optical synchronization system for femtosecond X-ray sources

Science.gov (United States)

Wilcox, Russell B [El Cerrito, CA; Holzwarth, Ronald [Munich, DE

2011-12-13

Femtosecond pump/probe experiments using short X-Ray and optical pulses require precise synchronization between 100 meter-10 km separated lasers in a various experiments. For stabilization in the hundred femtosecond range a CW laser is amplitude modulated at 1-10 GHz, the signal retroreflected from the far end, and the relative phase used to correct the transit time with various implementations. For the sub-10 fsec range the laser frequency itself is upshifted 55 MHz with an acousto-optical modulator, retroreflected, upshifted again and phase compared at the sending end to a 110 MHz reference. Initial experiments indicate less than 1 fsec timing jitter. To lock lasers in the sub-10 fs range two single-frequency lasers separated by several teraHertz will be lock to a master modelocked fiber laser, transmit the two frequencies over fiber, and lock two comb lines of a slave laser to these frequencies, thus synchronizing the two modelocked laser envelopes.

Optical observations of binary X-ray sources

International Nuclear Information System (INIS)

Boynton, P.E.

1975-01-01

The contribution to the recent progress in astronomy made by optical observations is pointed out. The optical properties of X-ray sources help to establish the physical nature of these objects. The current observational evidence on the binary X-ray sources HZ Her/Her X-1 and HDE 226868/Cyg X-1 is reported. (P.J.S.)

Soft x-ray induced femtosecond solid-to-solid phase transition

Czech Academy of Sciences Publication Activity Database

Tavella, F.; Höppner, H.; Tkachenko, V.; Medvedev, Nikita; Capotondi, F.; Golz, T.; Kai, Y.; Manfredda, M.; Pedersoli, E.; Prandolini, M.J.; Stojanovic, N.; Tanikawa, T.; Teubner, U.; Toleikis, S.; Ziaja, B.

Roč. 24, Sep (2017), s. 22-27 ISSN 1574-1818 Institutional support: RVO:68378271 Keywords : soft x-ray * ultrashort x-ray pulses * grafitization of diamond * non-thermal phase transition Subject RIV: BL - Plasma and Gas Discharge Physics OBOR OECD: Fluids and plasma physics (including surface physics) Impact factor: 0.908, year: 2016

Radiation resistant characteristics of optical fibers

International Nuclear Information System (INIS)

Nakasuji, Masaaki; Tanaka, Gotaro; Watanabe, Minoru; Kyodo, Tomohisa; Mukunashi, Hiroaki

1983-01-01

It is required to develop the optical fibers with good radiation resistivity because the fibers cause the increase of transmission loss due to glass colouring when they are used under the presence of radiation such as γ-ray. Generally, it is known that SI (step index) fibers are more resistive to radiation than GI (graded index) fibers. However, since a wide band can not be obtained with SI fibers, the development of radiation resistive GI optical fibers is desirable. In this report, the production for trial of the GI fibers of fluorine-doped silica core, the examination of radiation effect on their optical transmission loss by exposing them to γ-ray, thermal and fast neutron beams and also of mechanical strength are described. The GI fibers of fluorine-doped silica core show better radiation resistivity than Ge-doped ones. The B- and F-doped GI fibers show small increase of loss due to γ-ray, but large increase of loss due to thermal neutron beam. This is supposed to be caused by the far greater neutron absorption cross-section of boron than that of other elements. Significant increase of loss was not recognized when 14 MeV fast neutrons (8.6 x 10 4 n/cm 2 .s) were applied by 1.8 x 10 9 n/cm 2 . It was found that ETFE-covered fiber cores generated fluorine-containing gas due to γ irradiation, and the strength was remarkably lowered, but the lowering of strength can be prevented by adding titanium-white to the covering material. (Wakatsuki, Y.)

Hard X-ray/soft gamma-ray telescope designs for future astrophysics missions

DEFF Research Database (Denmark)

Ferreira, Desiree Della Monica; Christensen, Finn Erland; Pivovaroff, Michael J.

2013-01-01

We present several concept designs of hard X-ray/soft λ-ray focusing telescopes for future astrophysics missions. The designs are based on depth graded multilayer coatings. These have been successfully employed on the NuSTAR mission for energies up to 80 keV. Recent advances in demonstrating...

Soft x-ray absorption spectra of ilmenite family.

Science.gov (United States)

Agui, A; Mizumaki, M; Saitoh, Y; Matsushita, T; Nakatani, T; Fukaya, A; Torikai, E

2001-03-01

We have carried out soft x-ray absorption spectroscopy to study the electronic structure of ilmenite family, such as MnTiO3, FeTiO3, and CoTiO3 at the soft x-ray beamline, BL23SU, at the SPring-8. The Ti and M L2,3 absorption spectra of MTiO3 (M=Mn, Fe, and Co) show spectra of Ti4+ and M2+ electron configurations, respectively. Except the Fe L2,3 spectrum, those spectra were understood within the O(h) symmetry around the transition metal ions. The Fe L3-edge spectrum clearly shows a doublet peak at the L3 edge, which is attributed to Fe2+ state, moreover the very high-resolution the L-edge spectra of transition metals show fine structures. The spectra of those ilmenites are compared.

Glass capillary optics for making x-ray beams of 0.1 to 50 microns diameter

International Nuclear Information System (INIS)

Bilderback, Donald H.; Fontes, Ernest

1997-01-01

We have fabricated a unique computerized glass puller that can make parabolic or elliptically tapered glass capillaries for microbeam x-ray experiments from hollow glass tubing. We have produced optics that work in a single-bounce imaging mode or in a multi-bounce condensing mode. The imaging-mode capillaries have been used to create 20 to 50 micron diameter x-ray beams at 12 keV that are quite useful for imaging diffraction patterns from tiny bundles of carbon and Kevlar fibers. The condensing-mode capillaries are useful for creating submicron diameter beams and show great promise in x-ray fluorescence applications with femtogram sensitivity for patterned Er and Ti dopants diffused into an optically-active lithium niobate wafer

13.1 micrometers hard X-ray focusing by a new type monocapillary X-ray optic designed for common laboratory X-ray source

Science.gov (United States)

Sun, Xuepeng; zhang, Xiaoyun; Zhu, Yu; Wang, Yabing; Shang, Hongzhong; Zhang, Fengshou; Liu, Zhiguo; Sun, Tianxi

2018-04-01

A new type of monocapillary X-ray optic, called 'two bounces monocapillary X-ray optics' (TBMXO), is proposed for generating a small focal spot with high power-density gain for micro X-ray analysis, using a common laboratory X-ray source. TBMXO is consists of two parts: an ellipsoidal part and a tapered part. Before experimental testing, the TBMXO was simulated by the ray tracing method in MATLAB. The simulated results predicted that the proposed TBMXO would produce a smaller focal spot with higher power-density gain than the ellipsoidal monocapillary X-ray optic (EMXO). In the experiment, the TBMXO performance was tested by both an optical device and a Cu target X-ray tube with focal spot of 100 μm. The results indicated that the TBMXO had a slope error of 57.6 μrad and a 13.1 μm focal spot and a 1360 gain in power density were obtained.

The Solar-A soft X-ray telescope experiment

Science.gov (United States)

Acton, L.; Bruner, M.; Brown, W.; Lemen, J.; Hirayama, T.

1988-01-01

The Japanese Solar-A mission for the study of high energy solar physics is timed to observe the sun during the next activity maximum. This small spacecraft includes a carefully coordinated complement of instruments for flare studies. In particular, the soft X-ray telescope (SXT) will provide X-ray images of flares with higher sensitivity and time resolution than have been available before. This paper describes the scientific capabilities of the SXT and illustrates its application to the study of an impulsive compact flare.

Time-Resolved Soft X-ray Diffraction Reveals Transient Structural Distortions of Ternary Liquid Crystals

Directory of Open Access Journals (Sweden)

Klaus Mann

2009-11-01

Full Text Available Home-based soft X-ray time-resolved scattering experiments with nanosecond time resolution (10 ns and nanometer spatial resolution were carried out at a table top soft X-ray plasma source (2.2–5.2 nm. The investigated system was the lyotropic liquid crystal C16E7/paraffin/glycerol/formamide/IR 5. Usually, major changes in physical, chemical, and/or optical properties of the sample occur as a result of structural changes and shrinking morphology. Here, these effects occur as a consequence of the energy absorption in the sample upon optical laser excitation in the IR regime. The liquid crystal shows changes in the structural response within few hundred nanoseconds showing a time decay of 182 ns. A decrease of the Bragg peak diffracted intensity of 30% and a coherent macroscopic movement of the Bragg reflection are found as a response to the optical pump. The Bragg reflection movement is established to be isotropic and diffusion controlled (1 μs. Structural processes are analyzed in the Patterson analysis framework of the time-varying diffraction peaks revealing that the inter-lamellar distance increases by 2.7 Å resulting in an elongation of the coherently expanding lamella crystallite. The present studies emphasize the possibility of applying TR-SXRD techniques for studying the mechanical dynamics of nanosystems.

Soft X-ray spectromicroscopy of biological and synthetic polymer systems

International Nuclear Information System (INIS)

Hitchcock, A.; Morin, C.; Araki, T.; Zhang, X.; Dynes, J.; Stover, H.; Brash, J.

2004-01-01

Full text: Scanning transmission X-ray microscopy (STXM) and X-ray photoemission electron microscopy (X-PEEM) are synchrotron based, soft X-ray spectromicroscopy techniques which provide chemical speciation at 50 nm spatial resolution based on near edge X-ray absorption spectral (NEXAFS) contrast. The instrumentation and techniques of soft X-ray spectro- microscopy will be described and illustrated with applications to wet biofilms, protein interactions with patterned polymer surfaces, and polymer microstructure optimization. STXM can be applied to samples in air, He, vacuum, or a fully hydrated environment. With many collaborators, my group is using STXM to study fundamental and applied aspects of polymer microstructure, to map metal ions and anti-microbial agents in wet biofilms, and to identify sites of selective adsorption of proteins on phase separated polymer thin films in the presence of an overlayer of protein solution. X-PEEM has greater surface sensitivity than STXM but requires a flat, conductive, and vacuum-compatible sample. Comparison of X-PEEM and STXM for the same system - fibrinogen adsorption on a PS:PMMA blend, will be used to illustrate advantages and limitations of each technique. Measurements at 5.3.2 STXM and 7.3.1 PEEM at the Advanced Light Source, funded by DoE under contract DE-AC03- 76SF00098. Research supported by NSERC (Canada), AFMnet (Advanced Food and Biomaterials Network) and the Canada Research Chair program

Scandium/carbon filters for soft x rays

NARCIS (Netherlands)

Artioukov, IA; Kasyanov, YS; Kopylets, IA; Pershin, YP; Romanova, SA

2003-01-01

This Note deals with thin-film soft x-ray filters for operation at the wavelengths near carbon K edge (similar to4.5 nm). The filters were fabricated by magnetron sputtering deposition of thin layers of scandium (total thickness 0.1-0.2 mum) onto films of polypropylene (thickness 1.5 mum) and

X-ray focusing with Wolter microchannel plate optics

CERN Document Server

Price, G J; Beijersbergen, M W; Fraser, G W; Bavdaz, M; Boutot, J P; Fairbend, R; Flyckt, S O; Peacock, A; Tomaselli, E

2002-01-01

Square-pore microchannel plate (MCP) X-ray optics of the 'lobster-eye' geometry have frequently been described in the literature. We have now investigated the use of a radial channel packing geometry which, in the context of an MCP pair slumped to the correct radii of curvature, can form a conic approximation to the Wolter Type I grazing incidence X-ray optic. Such an optic can provide a large effective area with very low mass and may be ideally suited for use in applications such as planetary imaging X-ray fluorescence. We present here the results of X-ray illumination of the first such optic, fabricated by Photonis SAS, France.

Localization of proteins and nucleic acids using soft x-ray microscopy

International Nuclear Information System (INIS)

Larabell, Carolyn A.; Yager, Deborah; Meyer-Ilse, Werner

2000-01-01

The high-resolution soft x-ray microscope (XM-1) at the Advanced Light Source was used to examine whole, hydrated mammalian cells, both chemically fixed and rapidly frozen and viewed in a cryostage. Using x-ray microscopy, high contrast information about the organization of the cytoplasm and nucleus of these cells was revealed at unsurpassed resolution. It is important to note that cryo-fixed cells have been examined in a state that most closely resembles their natural environment in that the cells were not exposed to chemical fixatives or chemical contrast enhancement reagents. We also used the power of soft x-ray microscopy to examine the localization of proteins and nucleic acids in whole, hydrated cells using silver-enhanced, immunogold labeling techniques. With this approach, we have obtained information about the distribution of such molecules with respect to cellular ultrastructure at five times better resolution than light microscopy. The power of soft x-ray microscopy to provide superb resolution information about the subcellular localization of proteins and nucleic acids places it in a commanding position to contribute to our understanding of the numerous molecules being identified through modern molecular biology techniques

Optimization of soft X-ray tomography on the COMPASS tokamak

Czech Academy of Sciences Publication Activity Database

Imríšek, Martin; Mlynář, Jan; Löffelmann, Viktor; Weinzettl, Vladimír; Odstrčil, T.; Odstrčil, M.; Tomeš, Matěj

2016-01-01

Roč. 61, č. 4 (2016), s. 403-408 ISSN 0029-5922. [Summer School of Plasma Diagnostics PhDiaFusion 2015: “Soft X-ray Diagnostics for Fusion Plasma”. Bezmiechowa, 16.06.2015-20.06.2015] R&D Projects: GA MŠk(CZ) LM2011021; GA MŠk LG14002; GA MŠk(CZ) 8D15001 EU Projects: European Commission(XE) 633053 - EUROfusion Institutional support: RVO:61389021 Keywords : soft X-ray * tomography * Tikhonov regularization * tokamak Subject RIV: BL - Plasma and Gas Discharge Physics Impact factor: 0.760, year: 2016 http://www.ichtj.waw.pl/nukleonikaa/?p=1256

X-ray and Optical Explorations of Spiders

Science.gov (United States)

Roberts, M.; Al Noori, H.; Torres, R.; Russell, D.; Mclaughlin, M.; Gentile, P.

2017-10-01

Black widows and redbacks are binary systems consisting of a millisecond pulsar in a close binary with a companion which is having matter driven off of its surface by the pulsar wind. X-rays due to an intrabinary shock have been observed from many of these systems, as well as orbital variations in the optical emission from the companion due to heating and tidal distortion. We have been systematically studying these systems in radio, optical and X-rays. Here we will present an overview of X-ray and optical studies of these systems, including new XMM-Newton data obtained from several of these systems, along with new optical photometry.

Resolving the origin of the diffuse soft X-ray background

Energy Technology Data Exchange (ETDEWEB)

Smith, Randall K.; Foster, Adam R.; Edgar, Richard J.; Brickhouse, Nancy S. [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge MA 02138 (United States)

2014-05-20

The ubiquitous diffuse soft (1/4 keV) X-ray background was one of the earliest discoveries of X-ray astronomy. At least some of the emission may arise from charge exchange between solar wind ions and neutral atoms in the heliosphere, but no detailed models have been fit to the available data. Here, we report on a new model for charge exchange in the solar wind, which, when combined with a diffuse hot plasma component, filling the Local Cavity provides a good fit to the only available high-resolution soft X-ray and extreme ultraviolet spectra using plausible parameters for the solar wind. The implied hot plasma component is in pressure equilibrium with the local cloud that surrounds the solar system, creating for the first time a self-consistent picture of the local interstellar medium.

Prototyping a Global Soft X-Ray Imaging Instrument for Heliophysics, Planetary Science, and Astrophysics Science

Science.gov (United States)

Collier, M. R.; Porter, F. S.; Sibeck, D. G.; Carter, J. A.; Chiao, M. P.; Chornay, D. J.; Cravens, T.; Galeazzi, M.; Keller, J. W.; Koutroumpa, D.;

Prototyping a Global Soft X-ray Imaging Instrument for Heliophysics, Planetary Science, and Astrophysics Science

Science.gov (United States)

Collier, Michael R.; Porter, F. Scott; Sibeck, David G.; Carter, Jenny A.; Chiao, Meng P.; Chornay, Dennis J.; Cravens, Thomas; Galeazzi, Massimiliano; Keller, John W.; Koutroumpa, Dimitra;

Actinide science with soft x-ray synchrotron radiation

International Nuclear Information System (INIS)

Shuh, D.

2002-01-01

Several workshops, some dating back more than fifteen years, recognised both the potential scientific impact and opportunities that would be made available by the capability to investigate actinide materials in the vacuum ultraviolet (VUV)/soft X-ray region of the synchrotron radiation (SR) spectrum. This spectral region revolutionized the approach to surface materials chemistry and physics nearly two decades ego. The actinide science community was unable to capitalize on these SR methodologies for the study of actinide materials until recently because of radiological safety concerns. ,The Advanced Light Source (ALS) at LBNL is a third-generation light source providing state-of-the-art performance in the VUV/soft X-ray region. Along with corresponding improvements in detector and vacuum technology, the ALS has rendered experiments with small amounts of actinide materials possible. In particular, it has been the emergence and development of micro-spectroscopic techniques that have enabled investigations of actinide materials at the ALS. The primary methods for the experimental investigation of actinide materials in the VUV/soft X-ray region are the complementary photoelectron spectroscopies, near-edge X-ray absorption fine structure (NEXAFS) and X-ray emission spectroscopy (XES) techniques. Resonant photo-emission is capable of resolving the 5f electron contributions to actinide bonding and can be used to characterise the electronic structure of actinide materials. This technique is clearly a most important methodology afforded by the tunable SR source. Core level and valence band photoelectron spectroscopies are valuable for the characterisation of the electronic properties of actinide materials, as well as for general analytical purposes. High-resolution core-level photo-emission and resonant photo-emission measurements from the a (monoclinic) and δ (FCC) allotropic phases of plutonium metal have been collected on beam line 7.0 at the ALS and the spectra show

The soft x-ray transform

International Nuclear Information System (INIS)

Klukowska, Joanna; Herman, Gabor T; Otón, Joaquin; Marabini, Roberto; Carazo, José-María

2014-01-01

Several new forward models are introduced as mathematical formalizations of the processes that take place during image formation in transmission soft x-ray microscopy, which has the unique capability of imaging whole cells in their native environment with high resolution. Mathematical solutions of some of the associated inverse problems are provided by deriving closed-form formulas specifying the inverse transforms. Numerical experimental results are presented to demonstrate how the inverse transforms can be used to improve the reconstructions computed from data acquired according to the forward models. (paper)

Stress Free Multilayer Coating for High Resolution X-ray Mirrors

Data.gov (United States)

National Aeronautics and Space Administration — Most of X-ray optics research and development in the US is to build a high resolution, large collecting area and light-weight optic, namely an soft X-ray mirror for...

Radiobiological investigations of soft X-rays near carbon, nitrogen, oxygen K-shell edges on Aspergillus oryzae spores

International Nuclear Information System (INIS)

Chen, L.; Jiang, S. P.; Wan, L. B.; Ma, X. D.; Li, M. F.

2008-01-01

Soft X-rays at carbon, nitrogen, oxygen K-shell edges have special radiobiological effects. Using Aspergillus oryzae spores as sample, the radiation effects of soft X-rays near the K-shell edges of C, N and O elements from synchrotron radiation were investigated. Also the dose depositions of different X-ray energies in spore were discussed. At the same time, the spores were irradiated by gamma rays from 60 Co and relative biological effects were compared with those produced by soft X-rays. The results showed that soft X-rays near K-shell edges of O element had higher ability of radiation damage than that of X-rays near K-shell edges of C and N elements as compared with one another. But they all had higher killing abilities per unit dose than that of gamma rays from 60 Co. The relative biological effects (RBEs), the comparison of dose to gamma rays at 10% survival level, of the three soft X-rays were 1.65, 1.73 and 1.91, respectively. (authors)

The Development of a Scanning Soft X-Ray Microscope.

Science.gov (United States)

Rarback, Harvey Miles

We have developed a scanning soft X-ray microscope, which can be used to image natural biological specimens at high resolution and with less damage than electron microscopy. The microscope focuses a monochromatic beam of synchrotron radiation to a nearly diffraction limited spot with the aid of a high resolution Fresnel zone plate, specially fabricated for us at the IBM Watson Research Center. The specimen at one atmosphere is mechanically scanned through the spot and the transmitted radiation is efficiently detected with a flow proportional counter. A computer forms a realtime transmission image of the specimen which is displayed on a color monitor. Our first generation optics have produced images of natural wet specimens at a resolution of 300 nm.

Geant4 simulations of soft proton scattering in X-ray optics. A tentative validation using laboratory measurements

Science.gov (United States)

Fioretti, Valentina; Mineo, Teresa; Bulgarelli, Andrea; Dondero, Paolo; Ivanchenko, Vladimir; Lei, Fan; Lotti, Simone; Macculi, Claudio; Mantero, Alfonso

2017-12-01

Low energy protons (process responsible for the grazing angle scattering processes is mandatory to evaluate the impact of such events on the performance (e.g. observation time, sensitivity) of future X-ray telescopes as the ESA ATHENA mission. The Remizovich model describes particles reflected by solids at glancing angles in terms of the Boltzmann transport equation using the diffuse approximation and the model of continuous slowing down in energy. For the first time this solution, in the approximation of no energy losses, is implemented, verified, and qualitatively validated on top of the Geant4 release 10.2, with the possibility to add a constant energy loss to each interaction. This implementation is verified by comparing the simulated proton distribution to both the theoretical probability distribution and with independent ray-tracing simulations. Both the new scattering physics and the Coulomb scattering already built in the official Geant4 distribution are used to reproduce the latest experimental results on grazing angle proton scattering. At 250 keV multiple scattering delivers large proton angles and it is not consistent with the observation. Among the tested models, the single scattering seems to better reproduce the scattering efficiency at the three energies but energy loss obtained at small scattering angles is significantly lower than the experimental values. In general, the energy losses obtained in the experiment are higher than what obtained by the simulation. The experimental data are not completely representative of the soft proton scattering experienced by current X-ray telescopes because of the lack of measurements at low energies (distribution at the exit of X-ray optics.

Quantifying the Exospheric Component of Soft X-ray Emission

Science.gov (United States)

Kuntz, Kip; Collier, Michael R.; Snowden, Steven L.; Robertson, Ina; Hansen, Kenneth; Cravens, Thomas

2007-01-01

High charge state heavy ions in the solar wind exchange charge with ambient neutral gas. This process creates a product ion in an excited state. During the radiative cascade process, EUV and X-ray photons are emitted with energies in the range of about 100 eV to 1 keV. Because the terrestrial exospheric density at the nominal magnetopause location is relatively high, approx. 10 cu cm, solar wind charge exchange, or SWCX, can be observed by Earth-orbiting soft X-ray instruments such as the ROSAT Position Sensitive Proportional Counters (PSPC). In this presentation, we will compare simulated and observed soft Xray emission during an event on August 18-19, 1991 and discuss the role of exospheric SWCX emission for this and other events.

Towards 10 meV resolution: The design of an ultrahigh resolution soft X-ray RIXS spectrometer.

Science.gov (United States)

Dvorak, Joseph; Jarrige, Ignace; Bisogni, Valentina; Coburn, Scott; Leonhardt, William

2016-11-01

We present the optical design of the Centurion soft X-ray resonant inelastic X-ray scattering (RIXS) spectrometer to be located on the SIX beamline at NSLS-II. The spectrometer is designed to reach a resolving power of 100 000 at 1000 eV at its best resolution. It is also designed to have continuously variable 2θ motion over a range of 112° using a custom triple rotating flange. We have analyzed several possible spectrometer designs capable of reaching the target resolution. After careful analysis, we have adopted a Hettrick-Underwood spectrometer design, with an additional plane mirror to maintain a fixed direction for the outgoing beam. The spectrometer can cancel defocus and coma aberrations at all energies, has an erect focal plane, and minimizes mechanical motions of the detector. When the beamline resolution is accounted for, the net spectral resolution will be 14 meV at 1000 eV. This will open up many low energy excitations to study and will expand greatly the power of soft X-ray RIXS.

Towards 10 meV resolution: The design of an ultrahigh resolution soft X-ray RIXS spectrometer

Science.gov (United States)

Dvorak, Joseph; Jarrige, Ignace; Bisogni, Valentina; Coburn, Scott; Leonhardt, William

2016-11-01

We present the optical design of the Centurion soft X-ray resonant inelastic X-ray scattering (RIXS) spectrometer to be located on the SIX beamline at NSLS-II. The spectrometer is designed to reach a resolving power of 100 000 at 1000 eV at its best resolution. It is also designed to have continuously variable 2θ motion over a range of 112° using a custom triple rotating flange. We have analyzed several possible spectrometer designs capable of reaching the target resolution. After careful analysis, we have adopted a Hettrick-Underwood spectrometer design, with an additional plane mirror to maintain a fixed direction for the outgoing beam. The spectrometer can cancel defocus and coma aberrations at all energies, has an erect focal plane, and minimizes mechanical motions of the detector. When the beamline resolution is accounted for, the net spectral resolution will be 14 meV at 1000 eV. This will open up many low energy excitations to study and will expand greatly the power of soft X-ray RIXS.

Impulsive behavior in solar soft X-radiation

Science.gov (United States)

Hudson, H. S.; Strong, K. T.; Dennis, B. R.; Zarro, D.; Inda, M.; Kosugi, T.; Sakao, T.

1994-01-01

The Yohkoh soft X-ray telescope has observed impulsive, thermal, soft X-ray emission at the footpoints of magnetic loops during solar flares. The soft X-ray (thermal) time profiles at the footpoints closely match the hard X-ray (nonthermal) time profiles, directly demonstrating the heating of the lower solar atmosphere on short timescales during the interval of nonthermal energy release. This phenomenon is the rule, rather than the exception, occurring in the majority of flares that we have examined with the Yohkoh data. We illustrate the impulsive behavior with data from the major flare of 1992 January 26. For this flare, the soft X-ray peak times matched the hard X-ray peak times within the time resolution of the soft X-ray measurements (about 10 s), and the soft and hard X-ray locations match within the resolution of the hard X-ray imager. The impulsive soft X-ray emission clearly has a thermal spectral signature, but not at the high temperature of a 'superhot' source. We conclude that the impulsive soft X-ray emission comes from material heated by precipitating electrons at loop footpoints and evaporating from the deeper atmosphere into the flaring flux tube.

Soft x-ray measurements from the PDX tokamak

International Nuclear Information System (INIS)

Silver, E.H.; Bitter, M.; Brau, K.; Eames, D.; Greenberger, A.; Hill, K.W.; Meade, D.M.; Roney, W.; Sauthoff, N.R.; von Goeler, S.

1982-05-01

Temporally and spatially-resolved profiles of the PDX soft x-ray spectra have been measured during single tokamak pulses of circular and divertor plasmas with a recently developed pulse height analyzer. This detection system incorporates an array of five vertically displaced sets of lithium-drifted silicon detectors, each consisting of three independent channels optimized for rapid data collection in adjacent energy regions. Simultaneous measurement of x-ray emission integrated along five chords of the plasma cross section can thereby be achieved. Abel inversion of these data yields temporally-resolved radial profiles of the local electron temperature from the slope of the continuum, concentrations of high-Z impurities from the characteristic line intensities, and a measure of Z/sub eff/ from the continuum intensity. The techniques of x-ray pulse height analysis, with illustrations featuring the results from the initial PDX circular plasma experiments are discussed in detail. In addition, comparisons between circular and divertor plasmas on PDX, derived from the x-ray measurements, are also presented

Multilayer beam splitter used in a soft X-ray Mach-Zehnder interferometer at working wavelength of 13.9 nm

International Nuclear Information System (INIS)

Zhang Zhong; Wang Zhanshan; Wang Hongchang; Wang Fengli; Wu Wenjuan; Zhang Shumin; Qin Shuji; Chen Lingyan

2006-01-01

The soft X-ray Mach-Zehnder interferometer is an important tool in measuring the electron densities of laser-produced plasma near the critical surface. The design, fabrication and characterization of multilayer beam splitters at 13.9 nm for soft X-ray Mach-Zehnder interferometer are presented in the paper. The design of beam splitter is completed based on the standard of maximizing product of reflectivity and transmission of the beam splitter at 13.9 nm. The beam splitters, which are Mo/Si multi-layer deposited on 10 mm x 10 mm area, 100 nm thickness Si 3 N 4 membranes, are fabricated using the magnetron sputtering. A method based on extended He-Ne laser beam is developed to analyze the figure error of the beam splitters. The data measured by an optical profiler prove that the method based on visible light is effective to analyze the figure of the beam splitters. The rms figure error of a beam splitter reaches 1.757 nm in the center area 3.82 mm x 3.46 mm and satisfies the need of soft X-ray interference experiment. The product of reflectivity and transmission measured by synchrotron radiation is near to 4%. The Mach-Zehnder interferometer at 13.9 nm based on the multilayer beam splitters is used in 13.9 nm soft X-ray laser interference experiment, in which a clear interferograms of C 8 H 8 laser-produced plasma is got. (authors)

Fast Fiber-Coupled Imaging of X-rays Events, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — HyperV Technologies Corp. proposes to construct a long-record-length, fiber-coupled, fast imaging diagnostic for recording X-ray back-lit material flows and X-ray...

X-ray microscopy in Aarhus

International Nuclear Information System (INIS)

Uggerhoej, Erik; Abraham-Peskir, Joanna V.

2000-01-01

The Aarhus imaging soft X-ray microscope is now a busy multi-user facility. The optical set-up will be described and project highlights discussed. a) Metal-induced structural changes in whole cells in solution. The effects of aluminum, copper, nickel and zinc on protozoa investigated by using a combination of light microscopy, confocal scanning laser microscopy and X-ray microscopy. b) Botanical studies by X-ray microscopy used to compliment electron microscopy studies. c) Sludge morphology and iron precipitation in Danish freshwater plants by combining X-ray, scanning electron and transmission electron microscopy

Heating of low-density CHO-foam layers by means of soft X-rays

Energy Technology Data Exchange (ETDEWEB)

Rosmej, O.N., E-mail: o.rosmej@gsi.de [GSI Helmholtzzentrum fuer Schwerionenforschung, Planckstrasse 1, 164291 Darmstadt (Germany); Bagnoud, V.; Eisenbarth, U. [GSI Helmholtzzentrum fuer Schwerionenforschung, Planckstrasse 1, 164291 Darmstadt (Germany); Vatulin, V.; Zhidkov, N.; Suslov, N.; Kunin, A.; Pinegin, A. [All Russian Scientific Research Institute of Experimental Physics, RFNC-VNIIEF, Mira St. 37, Sarov (Russian Federation); Schaefer, D.; Nisius, Th.; Wilhein, Th. [RheinAhrCampus Remagen, Institute for X-optics, Suedallee 2, 53424 Remagen (Germany); Rienecker, T.; Wiechula, J.; Jacoby, J. [Goethe University, Frankfurt am Main (Germany); Zhao, Y. [Institute of Modern Physics, CAS, Nanchang Road 509, 730000 Lanzhou (China); Vergunova, G.; Borisenko, N. [Lebedev Physical Institute, Leninskii Prospekt, 65 Moscow (Russian Federation); Orlov, N. [Joint Institute for High Temperatures RAS, Institute for High Energy Density, Izhorskaya. 13, building 2, 125412 Moscow (Russian Federation)

2011-10-11

Interaction of soft X-ray thermal radiation with polymer foam layers has been studied experimentally. Indirectly heated CHO-foams were used to create a plasma target for applications in combined heavy ion beam-laser experiments that are aimed at investigation of the heavy ion energy loss in ionized matter. In this work, we report experimental results on heating of low Z foams by means of the Planckian radiation generated in gold hohlraums. The experimental goal was to study the hohlraum radiation field, duration of the soft X-ray pulse, the conversion efficiency of the laser energy into soft X-rays, measurements of the absorption properties of foam layers and parameters of the foam targets heated by the Plankian radiation.

Heating of low-density CHO-foam layers by means of soft X-rays

International Nuclear Information System (INIS)

Rosmej, O.N.; Bagnoud, V.; Eisenbarth, U.; Vatulin, V.; Zhidkov, N.; Suslov, N.; Kunin, A.; Pinegin, A.; Schaefer, D.; Nisius, Th.; Wilhein, Th.; Rienecker, T.; Wiechula, J.; Jacoby, J.; Zhao, Y.; Vergunova, G.; Borisenko, N.; Orlov, N.

2011-01-01

Interaction of soft X-ray thermal radiation with polymer foam layers has been studied experimentally. Indirectly heated CHO-foams were used to create a plasma target for applications in combined heavy ion beam-laser experiments that are aimed at investigation of the heavy ion energy loss in ionized matter. In this work, we report experimental results on heating of low Z foams by means of the Planckian radiation generated in gold hohlraums. The experimental goal was to study the hohlraum radiation field, duration of the soft X-ray pulse, the conversion efficiency of the laser energy into soft X-rays, measurements of the absorption properties of foam layers and parameters of the foam targets heated by the Plankian radiation.

Soft X-ray reflectivity: from quasi-perfect mirrors to accelerator walls

CERN Document Server

Schäfers, F.

2013-04-22

Reflection of light from surfaces is a very common, but complex phenomenon not only in science and technology, but in every day life. The underlying basic optical principles have been developed within the last five centuries using visible light available from the sun or other laboratory light sources. X-rays were detected in 1895, and the full potential of soft- and hard-x ray radiation as a probe for the electronic and geometric properties of matter, for material analysis and its characterisation is available only since the advent of synchrotron radiation sources some 50 years ago. On the other hand high-brilliance and high power synchrotron radiation of present-days 3rd and 4th generation light sources is not always beneficial. Highenergy machines and accelerator-based light sources can suffer from a serious performance drop or limitations due to interaction of the synchrotron radiation with the accelerator walls, thus producing clouds of photoelectrons (e-cloud) which in turn interact with the accelerated ...

Soft X-ray induced chemical modification of polysaccharides in vascular plant cell walls

International Nuclear Information System (INIS)

Cody, George D.; Brandes, Jay; Jacobsen, Chris; Wirick, Susan

2009-01-01

Scanning transmission X-ray microscopy and micro carbon X-ray Absorption Near Edge Spectroscopy (C-XANES) can provide quantitative information regarding the distribution of the biopolymers cellulose, hemicellulose, and lignin in vascular plant cell walls. In the case of angiosperms, flowering plants, C-XANES may also be able to distinguish variations in lignin monomer distributions throughout the cell wall. Polysaccharides are susceptible to soft X-ray irradiation induced chemical transformations that may complicate spectral analysis. The stability of a model polysaccharide, cellulose acetate, to variable doses of soft X-rays under conditions optimized for high quality C-XANES spectroscopy was investigated. The primary chemical effect of soft X-ray irradiation on cellulose acetate involves mass loss coincident with de-acetylation. A lesser amount of vinyl ketone formation also occurs. Reduction in irradiation dose via defocusing does enable high quality pristine spectra to be obtained. Radiation induced chemical modification studies of oak cell wall reveals that cellulose and hemicellulose are less labile to chemical modification than cellulose acetate. Strategies for obtaining pristine C-XANES spectra of polysaccharides are presented.

Soft X-ray observations of two BL Lacertae objects - markarian 421 and 501

International Nuclear Information System (INIS)

Singh, K.P.; Garmire, G.P.

1985-01-01

This paper reports on the soft X-ray (0.15-2.8 keV) observations of two BL Lacertae-type objects, viz., Mrk 421 and Mrk 501. The observations were made with the low-energy detectors on the HEAO 1 satellite during the period 1977 August-1978 December. Steep, soft X-ray power-law spectra with photon index Gamma = 3 are found for both Mrk 421 and Mrk 501. The power-law models are found to give a significantly better fit than the thermal models to the observed pulse-height spectra of Mrk 421 and Mrk 501. Day-to-day soft X-ray (0.25 keV band) intensity variations are observed only in Mrk 501. No significant change is found in Gamma from both the BL Lac objects during the period of observations. However, the sum of all the X-ray observations from 1976 until 1980 can be understood in terms of two spectral components of variable intensity to account for the X-ray emission observed between 0.15 and 20 keV from Mrk 421 and Mrk 501. 24 references

Soft x-ray imaging by a commercial solid-state television camera

International Nuclear Information System (INIS)

Matsushima, I.; Koyama, K.; Tanimoto, M.; Yano, M.

1987-01-01

A commerical, solid-state television camera has been used to record images of soft x radiation (0.8--12 keV). The performance of the camera is theoretically analyzed and experimentally evaluated compared with an x-ray photographic film (Kodak direct exposure film). In the application, the camera has been used to provide image patterns of x rays from laser-produced plasmas. It is demonstrated that the camera has several advantages over x-ray photographic film

Recent progress of soft X-ray photoelectron spectroscopy studies of uranium compounds

Energy Technology Data Exchange (ETDEWEB)

Fujimori, Shin-ichi; Takeda, Yukiharu; Okane, Tetsuo; Saitoh, Yuji [Condensed Matter Science Divisions, Japan Atomic Energy Agency, Sayo, Hyogo (Japan); Fujimori, Atsushi [Condensed Matter Science Divisions, Japan Atomic Energy Agency, Sayo, Hyogo (Japan); Department of Physics, University of Tokyo, Hongo, Tokyo 113-0033 (Japan); Yamagami, Hiroshi [Condensed Matter Science Divisions, Japan Atomic Energy Agency, Sayo, Hyogo (Japan); Department of Physics, Faculty of Science, Kyoto Sangyo University, Kyoto 603-8555 (Japan); Yamamoto, Etsuji; Haga, Yoshinori [Advanced Science Research Center, Japan Atomic Energy Agency, Tokai, Ibaraki 319-1195 (Japan); Ōnuki, Yoshichika [Advanced Science Research Center, Japan Atomic Energy Agency, Tokai, Ibaraki 319-1195 (Japan); Faculty of Science, University of the Ryukyus, Nishihara, Okinawa 903-0213 (Japan)

2016-04-15

Recent progresses in the soft X-ray photoelectron spectroscopy (PES) studies (hν ≳ 100 eV) for uranium compounds are briefly reviewed. The soft X-ray PES has enhanced sensitivities for the bulk U 5f electronic structure, which is essential to understand the unique physical properties of uranium compounds. In particular, the recent remarkable improvement in energy resolutions from an order of 1 eV to 100 meV made it possible to observe fine structures in U 5f density of states. Furthermore, soft X-ray ARPES becomes available due to the increase of photon flux at beamlines in third generation synchrotron radiation facilities.The technique made it possible to observe bulk band structures and Fermi surfaces of uranium compounds and therefore, the results can be directly compared with theoretical models such as band-structure calculations. The core-level spectra of uranium compounds show a systematic behavior depending on their electronic structures, suggesting that they can be utilized to determine basic physical parameters such as the U 5f-ligand hybridizations or Comlomb interaction between U 5f electrons. It is shown that soft X-ray PES provides unique opportunities to understand the electronic structures of uranium compounds.

Coronal temperature diagnostics from high-resolution soft X-ray spectra

Science.gov (United States)

Strong, K. T.; Claflin, E. S.; Lemen, J. R.; Linford, G. A.

1988-01-01

The problem of deriving the temperature of the coronal plasma from soft X-ray spectra is discussed. Spectral atlas scans of the soft X-ray spectrum from the Flat Crystal Spectrometer on the Solar Maximum Mission are compared with theoretical predictions of the relative intensities of some of the brighter lines to determine which line intensity ratios give the most reliable temperature diagnostics. The techniques considered include line widths, He-like G ratios, intensity ratios, and ratios of lines formed by different elements. It is found that the best temperature diagnostics come from the ratios of lines formed by successive ionization stages of the same element.

Soft x-ray spectroscopy optimisation for the direct determination of valence

International Nuclear Information System (INIS)

Wison, N.C.; MacRae, C.M.; Nelson, S.

2002-01-01

Full text: Measuring the valence of elements and mapping their occurrence throughout a sample can give important insights into the chemistry of complex systems. The toxic nature of Cr 6+ gives great concern over its disposal in the environment. Being able to resolve Cr 6+ from Cr 3+ allows us to tackle these important problems. The electron probe micro-analyser (EPMA) is routinely used to provide micron resolution chemical analysis. However it is often possible to resolve changes in soft X-ray peak shape and position that reflect changes in the chemical state and crystal structure. A soft x-rays is usually considered to be one of less than 1.5 keV in energy In this study we have compared a range of Cr containing compounds, and measured the differences in the Cr Lα line. In some samples, the Cr L line can be 'relatively weak, so to maximise its excitation probability, a set of Monte Carlo simulations were performed using the CASINO V2.0 package and the most efficient excitation voltage was determined. We also investigate the soft x-ray spectroscopy using electronic structure calculations to produce theoretical Density of States (DOS) for comparison with the measured spectra. The theoretical calculations can aid in understanding spectrum shape and polarisation of the soft x-ray signal in unknown samples, when a full range of standards is not available. Copyright (2002) Australian Society for Electron Microscopy Inc

Electro-optical behaviour of silica optical fibers under transient ionizing irradiation

International Nuclear Information System (INIS)

Johan, A.; Charre, P.

1989-01-01

Centre d'Etudes de GRAMAT has perfected an experimental method on behaviour study for optical fiber under X-ray transient irradiation. This method allows recording of working light intensity in the fiber core or induced light (luminescence) during and after irradiation. The measured phenomena are the luminescence photon production and working light absorption. Monomode and multimode fiber behaviours have been studied and compared versus dose irradiation, light wavelength and injected optical power [fr

Exploring the Hard and Soft X-ray Emission of Magnetic Cataclysmic Variables

Science.gov (United States)

de Martino, D.; Anzolin, G.; Bonnet-Bidaud, J.-M.; Falanga, M.; Matt, G.; Mouchet, M.; Mukai, K.; Masetti, N.

2009-05-01

A non-negligible fraction of galactic hard (>20 keV) X-ray sources were identified as CVs of the magnetic Intermediate Polar type in INTEGRAL, SWIFT and RXTE surveys, that suggests a still hidden but potentially important population of faint hard X-ray sources. Simbol-X has the unique potential to simultaneously characterize their variable and complex soft and hard X-ray emission thus allowing to understand their putative role in galactic populations of X-ray sources.

Cellulose/inorganic-composite fibers for producing textile fabrics of high X-ray absorption properties

Energy Technology Data Exchange (ETDEWEB)

Günther, Karoline; Giebing, Christina; Askani, Antonia [FTB, Hochschule Niederrhein – University of Applied Science, Faculty of Textile and Clothing Technology, Webschulstr. 31, 41065 Mönchengladbach (Germany); Leisegang, Tilmann [Saxray GmbH, Maria-Reiche-Str. 1, 01109 Dresden (Germany); Krieg, Marcus [TITK, Thüringisches Institut für Textil- und Kunststoff-Forschung e.V., Breitscheidstraße 97, 07407 Rudolstadt (Germany); Kyosev, Yordan; Weide, Thomas [FTB, Hochschule Niederrhein – University of Applied Science, Faculty of Textile and Clothing Technology, Webschulstr. 31, 41065 Mönchengladbach (Germany); Mahltig, Boris, E-mail: Boris.Mahltig@hs-niederrhein.de [FTB, Hochschule Niederrhein – University of Applied Science, Faculty of Textile and Clothing Technology, Webschulstr. 31, 41065 Mönchengladbach (Germany)

2015-11-01

Common textile materials as cotton or polyester do not possess reliable X-ray absorption properties. This is due to their morphology and chemical composition in particular. Common fibers are built up from organic polymers containing mainly the elements carbon, hydrogen, oxygen and nitrogen. These “light” elements only have low X-ray absorption coefficients. In contrast, inorganic materials composed of “heavy” elements with high atomic numbers, e.g. barium or bismuth, exhibit X-ray absorption coefficients higher by up to two orders of magnitude. To obtain a flexible yarn with high X-ray absorption properties both these materials, the organic polymer and the inorganic X-ray absorber, are combined to an inorganic/organic composite fiber material. Hence, as the organic component cellulose from modified Lyocell-process is used as carrier fiber and blended with inorganic absorber particles of low toxicity and high absorption coefficients, as bariumsulphate, bariumtitanate or bismuthoxide. A content of inorganic absorber particles equally distributed in the whole fiber of up to 20% is achieved. The composite fibers are produced as staple or filament fibers and processed to multifilament or staple fiber yarns. The staple fiber yarns are rotor-spinned to increase the comfort of the subsequent textile material. Several woven fabrics, considering multilayer structure and different warp/weft density, are developed. The energy dependent X-ray shielding properties are determined in dependence on the different yarn compositions, yarn types and structural parameters of the woven fabrics. As a result, a production process of textile materials with comfortable and dedicated X-ray absorption properties is established. It offers a promising opportunity for manufacturing of specialized textiles, working clothes or uniforms applicable for medicine, air craft and security personal, mining as well as for innovative composite materials. - Highlights: • Preparation of cellulosic

Cellulose/inorganic-composite fibers for producing textile fabrics of high X-ray absorption properties

International Nuclear Information System (INIS)

Günther, Karoline; Giebing, Christina; Askani, Antonia; Leisegang, Tilmann; Krieg, Marcus; Kyosev, Yordan; Weide, Thomas; Mahltig, Boris

2015-01-01

Common textile materials as cotton or polyester do not possess reliable X-ray absorption properties. This is due to their morphology and chemical composition in particular. Common fibers are built up from organic polymers containing mainly the elements carbon, hydrogen, oxygen and nitrogen. These “light” elements only have low X-ray absorption coefficients. In contrast, inorganic materials composed of “heavy” elements with high atomic numbers, e.g. barium or bismuth, exhibit X-ray absorption coefficients higher by up to two orders of magnitude. To obtain a flexible yarn with high X-ray absorption properties both these materials, the organic polymer and the inorganic X-ray absorber, are combined to an inorganic/organic composite fiber material. Hence, as the organic component cellulose from modified Lyocell-process is used as carrier fiber and blended with inorganic absorber particles of low toxicity and high absorption coefficients, as bariumsulphate, bariumtitanate or bismuthoxide. A content of inorganic absorber particles equally distributed in the whole fiber of up to 20% is achieved. The composite fibers are produced as staple or filament fibers and processed to multifilament or staple fiber yarns. The staple fiber yarns are rotor-spinned to increase the comfort of the subsequent textile material. Several woven fabrics, considering multilayer structure and different warp/weft density, are developed. The energy dependent X-ray shielding properties are determined in dependence on the different yarn compositions, yarn types and structural parameters of the woven fabrics. As a result, a production process of textile materials with comfortable and dedicated X-ray absorption properties is established. It offers a promising opportunity for manufacturing of specialized textiles, working clothes or uniforms applicable for medicine, air craft and security personal, mining as well as for innovative composite materials. - Highlights: • Preparation of cellulosic

Soft X-ray Focusing Telescope Aboard AstroSat: Design, Characteristics and Performance

DEFF Research Database (Denmark)

Singh, K; Stewart, G.; Westergaard, Niels Jørgen Stenfeldt

2017-01-01

The Soft X-ray focusing Telescope (SXT), India’s first X-ray telescope based on the principle of grazing incidence, was launched aboard the AstroSat and made operational on October 26, 2015. X-rays in the energy band of 0.3–8.0 keV are focussed on to a cooled charge coupled device thus providing ...

A simple, semi-quantitative method for measuring pulsed soft x-rays

International Nuclear Information System (INIS)

Takahama, Y.; Du, J.; Yanagidaira, T.; Hirano, K.

1993-01-01

A simple semi-quantitative measurement and image processing system for pulsed soft X-rays with a time and spatial resolution is proposed. Performance of the system is examined using a cylindrical soft X-ray source generated with a plasma device. The system consists of commercial facilities which are easily obtained such as a microchannel plate-phosphor screen combination, a CCD camera, an image memory board and a personal computer. To make a quantitative measurement possible, the image processing and observation of the phosphor screen current are used in conjunction. (author)

Soft X-ray radio-sensitivities of pollens in several fruit species

International Nuclear Information System (INIS)

Hu Chungen; Deng Xiuxin

1996-01-01

Irradiated with different dosages of soft X-ray, pollen germinations of prunus baimang, pear kieffer, trifoliate orange and pummelo, were investigated immediately or several days later after irradiation. The results revealed that the pollens of these fruit tress had different sensitivites to soft X-ray and various responses to storage duration. Therefore, even to the same kind of pollen, irradiation with different optimal exposure doses, as well as pollination at different times during storage, should be adopted variously according to the different aims and methods of breeding programs. (author)

Synchrotron radiation sources and condensers for projection x-ray lithography

International Nuclear Information System (INIS)

Murphy, J.B.; MacDowell, A.A.; White, D.L.; Wood, O.R. II

1992-01-01

The design requirements for a compact electron storage ring that could be used as a soft x-ray source for projection lithography are discussed. The design concepts of the x-ray optics that are required to collect and condition the radiation in divergence, uniformity and direction to properly illuminate the mask and the particular x-ray projection camera used are discussed. Preliminary designs for an entire soft x-ray projection lithography system using an electron storage ring as a soft X-ray source are presented. It is shown that by combining the existing technology of storage rings with large collection angle condensers, a powerful and reliable source of 130 Angstrom photons for production line projection x-ray lithography is possible

Generation of attosecond soft X-ray pulses in a longitudinal space charge amplifier

Energy Technology Data Exchange (ETDEWEB)

Dohlus, M.; Schneidmiller, E.A.; Yurkov, M.V. [Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)

2011-03-15

A longitudinal space charge amplifier (LSCA), operating in soft X-ray regime, was recently proposed. Such an amplifier consists of a few amplification cascades (focusing channel and chicane) and a short radiator undulator in the end. Broadband nature of LSCA supports generation of few-cycle pulses as well as wavelength compression. In this paper we consider an application of these properties of LSCA for generation of attosecond X-ray pulses. It is shown that a compact and cheap addition to the soft X-ray free electron laser facility FLASH would allow to generate 60 attosecond (FWHM) long X-ray pulses with the peak power at 100 MW level and a contrast above 98%. (orig.)

Generation of attosecond soft X-ray pulses in a longitudinal space charge amplifier

International Nuclear Information System (INIS)

Dohlus, M.; Schneidmiller, E.A.; Yurkov, M.V.

2011-03-01

A longitudinal space charge amplifier (LSCA), operating in soft X-ray regime, was recently proposed. Such an amplifier consists of a few amplification cascades (focusing channel and chicane) and a short radiator undulator in the end. Broadband nature of LSCA supports generation of few-cycle pulses as well as wavelength compression. In this paper we consider an application of these properties of LSCA for generation of attosecond X-ray pulses. It is shown that a compact and cheap addition to the soft X-ray free electron laser facility FLASH would allow to generate 60 attosecond (FWHM) long X-ray pulses with the peak power at 100 MW level and a contrast above 98%. (orig.)

Numerical experiments on plasma focus for soft x-ray yield scaling laws derivation using Lee model

International Nuclear Information System (INIS)

Akel, M.

2012-09-01

The required plasma parameters of krypton and xenon at different temperatures were calculated, the x-ray emission properties of plasmas were studied, and based on the corona model the suitable temperature range for generating H-like and He-like ions (therefore soft x-ray emissions) of different gases plasma were found. The code is applied to characterize the plasma focus in different plasma focus devices, and for optimizing the nitrogen, oxygen, neon, argon, krypton and xenon soft x-ray yields based on bank, tubes and operating parameters. It is found that the soft x-ray yield increases with changing pressure until it reaches the maximum value for each plasma focus device. Keeping the bank parameters, operational voltage unchanged but systematically changing other parameters, numerical experiments were performed finding the optimum combination of P o , Z o and 'a' for the maximum soft x-ray yield. Thus we expect to increase the soft x-ray yield of plasma focus device several-fold from its present typical operation; without changing the capacitor bank, merely by changing the electrode configuration and the operating pressure. The Lee model code was also used to run numerical experiments on plasma focus devices for optimizing soft x-ray yield with reducing L o , varying L o and 'a' to get engineering designs with maximum soft x-ray yield for these devices at different experimental conditions and gases. Numerical experiments showed the influence of the gas used in plasma focus and its properties on soft x-ray emission and its properties and then on its applications. Scaling laws for soft x-ray of nitrogen, oxygen, neon, argon, krypton and xenon plasma focus, in terms of energy, peak discharge current and focus pinch current were found. Radiative cooling effects are studied indicating that radiative collapse may be observed for heavy noble gases (Ar, Kr, Xe) for pinch currents even below 100 kA. The results show that the line radiation emission and tube voltages have

Numerical experiments on plasma focus for soft x-ray yield scaling laws derivation using Lee model

International Nuclear Information System (INIS)

Akel, M.

2015-01-01

The required plasma parameters of krypton and xenon at different temperatures were calculated, the x-ray emission properties of plasmas were studied, and based on the corona model the suitable temperature range for generating H-like and He-like ions (therefore soft x-ray emissions) of different gases plasma were found. The code is applied to characterize the plasma focus in different plasma focus devices, and for optimizing the nitrogen, oxygen, neon, argon, krypton and xenon soft x-ray yields based on bank, tubes and operating parameters. It is found that t he soft x-ray yield increases with changing pressure until it reaches the maximum value for each plasma focus device. Keeping the bank parameters, operational voltage unchanged but systematically changing other parameters, numerical experiments were performed finding the optimum combination of Po, z0 and 'a' for the maximum soft x-ray yield. Thus we expect to increase the soft x-ray yield of plasma focus device several-fold from its present typical operation; without changing the capacitor bank, merely by changing the electrode configuration and the operating pressure. The Lee model code was also used to run numerical experiments on plasma focus devices for optimizing soft x-ray yield with reducing Lo, varying z0 and 'a' to get engineering designs with maximum soft x-ray yield for these devices at different experimental conditions and gases. Numerical experiments showed the influence of the gas used in plasma focus and its propor ties on soft x-ray emission and its propor ties and then on its applications. Scaling laws for soft x-ray of nitrogen, oxygen, neon, argon, krypton and xenon plasma focus in terms of energy, peak discharge current and focus pinch current were found. Radiative cooling effects are studied indicating that radiative collapse may be observed for heavy noble gases (Ar, Kr, Xe) for pinch currents even below 100 k A. The results show that the line radiation emission and

Long-term storage method for soft X-ray irradiated 'Hyuganatsu' pollen

International Nuclear Information System (INIS)

Yano, S.; Tanaka, M.; Ohara, N.

2008-01-01

The long-term storage conditions for 'Hyuganatsu ' pollen that had been irradiated with soft X-rays was examined. This study, was aimed at production of 'Tosa-buntan' without formation of nuclear fruit. 1. We evaluated the germination rate of pollen that had been irradiated with soft X-ray (500 or 1,000 Gy) and stored at 3 deg C, -20 deg C, and -40 deg C. The germination rate was the same as that of unirradiated pollen, even after storage for 1 year. Soft X-ray irradiation did not influence the storage attributes of pollen. 2. In unirradiated pollen and pollen that had been irradiated with soft X-ray (500 or 1,000 Gy), temperature conditions necessary for storing from 3 months to 1 year were -20 deg C or less, and pollen stored at -40 deg C had a higher germination rate after 1 year. 3. The germination rate was 1% or less in 4 months if silica gel was sealed into a gas barrier bag with 1,000 Gy-irradiated pollen at a rate of 10:1 (w/w). The ability to germinate was completely lost after 1 year in these conditions. 4. We evaluated the effect of sealing methods on 1,000 Gy-irradiated pollen stored at -20 deg C. There was no difference in germination rates among pollen stored in gas-barrier bags, vacuum-packaged pollen, and pollen stored with nitrogen in gas-barrier bags. Moreover, the germination rate of 750 Gy-irradiated pollen stored at -20 deg C decreased from 3 months onwards when pollen was stored with a free-oxygen absorber (Ageless ZP). 5. Pollen that was treated with acetone before or after soft X-ray irradiation (750 Gy) withstood long-term storage of 1 year. Long-term storage was possible if pollen was stored at -20 deg C, as is the case for rough pollen

The JET multi-camera soft X-ray diagnostic

Energy Technology Data Exchange (ETDEWEB)

Alper, B; Blackler, K; Dillon, S F; Edwards, A W; Gill, R D; Lyadina, E; Mulligan, W; Staunton-Lambert, S A.B.; Thompson, D G; Wilson, D J [Commission of the European Communities, Abingdon (United Kingdom). JET Joint Undertaking

1994-07-01

A new soft X-ray detector system has been constructed for the pumped divertor phase of JET which incorporates a number of enhancements over the previous system in both hardware and data acquisition. The hardware improvements include: six independent views of the plasma at one toroidal location (as opposed to two in the old system), spatial resolution improved from 7 cm to 3 cm, frequency response increased from 30 khz to 100 khz and improved toroidal mode resolution. These enhancements will allow the study of MHD activity in finer detail. The tomographic reconstruction of soft X-ray emissivities will be improved to include Fourier terms up to cos(5{theta}) compared with only cos(2{theta}) before. Through the implementation of a fast central acquisition and trigger system, data from a range of diagnostics will be available at high bandwidth to allow processing of plasma phenomena of far greater complexity than was possible before. (authors). 2 refs., 5 figs.

Wolter type I x-ray focusing mirror using multilayer coatings

International Nuclear Information System (INIS)

Chon, Kwon Su; Namba, Yoshiharu; Yoon, Kwon-Ha

2006-01-01

A multilayer coating is a useful addition to a mirror in the x-ray region and has been applied to normal incidence mirrors used with soft x rays. When a multilayer coating is used on grazing incidence optics, higher performance can be achieved than without it.Cr/Sc multilayers coated on a Wolter type I mirror substrate for a soft x-ray microscope are considered. The reflectivity and effective solid angle are calculated for Wolter type I mirrors with uniform and laterally graded multilayer coatings. The laterally graded multilayer mirror showed superior x-ray performance, and the multilayer tolerances were relaxed. This multilayer mirror could be especially useful in the soft x-ray microscope intended for biological applications

CCD-based X-ray detectors for X-ray diffraction studies

International Nuclear Information System (INIS)

Ito, K.; Amemiya, Y.

1999-01-01

CCD-based X-ray detectors are getting to be used for X-ray diffraction studies especially in the studies where real time (automated) measurements and time-resolved measurements are required. Principles and designs of two typical types of CCD-based detectors are described; one is ths system in which x-ray image intensifiers are coupled to maximize the detective quantum efficiency for time-resolved measurements, and the other is the system in which tapered optical fibers are coupled for the reduction of the image into the CCD, which is optimized for automated measurements for protein crystallography. These CCD-based X-ray detectors have an image distortion and non-uniformity of response to be corrected by software. Correction schemes which we have developed are also described. (author)

Soft X-Ray Measurements of Z-Pinch-Driven Vacuum Hohlraums

International Nuclear Information System (INIS)

Baker, K.L.; Porter, J.L.; Ruggles, L.E.; Chandler, G.A.; Deeney, Chris; Varas, M.; Moats, Ann; Struve, Ken; Torres, J.; McGurn, J.; Simpson, W.W.; Fehl, D.L.; Chrien, R.E.; Matuska, W.; Idzorek, G.C.

1999-01-01

This article reports the experimental characterization of a z-pinch driven-vacuum hohlraum. The authors have measured soft x-ray fluxes of 5 x 10 12 W/cm 2 radiating from the walls of hohlraums which are 2.4--2.5 cm in diameter by 1 cm tall. The x-ray source used to drive these hohlraums was a z-pinch consisting of a 300 wire tungsten array driven by a 2 MA, 100 ns current pulse. In this hohlraum geometry, the z-pinch x-ray source can produce energies in excess of 800 kJ and powers in excess of 100 TW to drive these hohlraums. The x-rays released in these hohlraums represent greater than a factor of 25 in energy and more than a factor of three in x-ray power over previous laboratory-driven hohlraums

X-ray microscope with a Wolter mirror

International Nuclear Information System (INIS)

Watanabe, Norio; Aoki, Sadao

2003-01-01

A Wolter mirror as an objective of an X-ray microscope is described. In comparison with other optical elements, a Wolter mirror has several advantages, such as a large numerical aperture and no chromatic aberration. Recent developments of fabrication process enabled us to make a Wolter mirror objective for X-rays. The fabrication process and the applications to a soft X-ray microscope and an X-ray fluorescence microscope are described. (author)

Refractive optics to compensate x-ray mirror shape-errors

Science.gov (United States)

Laundy, David; Sawhney, Kawal; Dhamgaye, Vishal; Pape, Ian

2017-08-01

Elliptically profiled mirrors operating at glancing angle are frequently used at X-ray synchrotron sources to focus X-rays into sub-micrometer sized spots. Mirror figure error, defined as the height difference function between the actual mirror surface and the ideal elliptical profile, causes a perturbation of the X-ray wavefront for X- rays reflecting from the mirror. This perturbation, when propagated to the focal plane results in an increase in the size of the focused beam. At Diamond Light Source we are developing refractive optics that can be used to locally cancel out the wavefront distortion caused by figure error from nano-focusing elliptical mirrors. These optics could be used to correct existing optical components on synchrotron radiation beamlines in order to give focused X-ray beam sizes approaching the theoretical diffraction limit. We present our latest results showing measurement of the X-ray wavefront error after reflection from X-ray mirrors and the translation of the measured wavefront into a design for refractive optical elements for correction of the X-ray wavefront. We show measurement of the focused beam with and without the corrective optics inserted showing reduction in the size of the focus resulting from the correction to the wavefront.

An X-ray and optical study of the ultracompact X-ray binary A 1246-58

NARCIS (Netherlands)

in 't Zand, J.J.M.; Bassa, C.G.; Jonker, P.G.; Keek, L.; Verbunt, F.W.M.; Méndez, M.; Markwardt, C.B.

2008-01-01

Results are discussed of an X-ray and optical observation campaign of the low-mass X-ray binary A 1246-58 performed with instruments on Satellite per Astronomia X ("BeppoSAX"), the Rossi X-ray Timing Explorer (RXTE), the X-ray Multi-mirror Mission ("XMM-Newton"), the Swift mission, and the Very

Soft X-ray microscopy and lithography with synchrotron radiation

International Nuclear Information System (INIS)

Gudat, W.

1977-12-01

Considerable progress in the technique microscopy with soft X-ray radiation has been achieved in particular through the application of synchrotron radiation. Various methods which are currently being studied theoretically or already being used practically will be described briefly. Attention is focussed on the method of contact microscopy. Various biological specimens have been investigated by this method with a resolution as good as 100 A. X-ray lithography which in the technical procedure is very similar to contact microscopy gives promise for the fabrication of high quality submicron structures in electronic device production. Important factors limiting the resolution and determining the performance of contact microscopy and X-ray lithography will be discussed. (orig.) [de

Study of soft X-ray energy spectra from gas-puff Z-pinch plasma

International Nuclear Information System (INIS)

Zou Xiaobing; Wang Xinxin; Zhang Guixin; Han Min; Luo Chengmu

2006-01-01

A ROSS-FILTER-PIN spectrometer in the spectral range of 0.28 keV-1.56 keV was developed to study the soft X-ray radiation emitted from gas-puff Z-pinch plasma. It is composed of five channels covering the energy interval of interest without gaps. Soft X-ray spectral energy cuts were determined by the L absorption edges of selected filter elements (K absorption edges being used for light filter elements), and the optimum thickness of filter material was designed using computer code. To minimize the residual sensitivity outside the sensitivity range of each channel, element of the first filter was added into the second filter of all the Ross pair. To diminish the area of each filter, PIN detector with small sensitive area of 1 mm 2 was adopted for the spectrometer. A filter with small area is easy to fabricate and would be helpful to withstand the Z-pinch discharge shock wave. With this ROSS-FILTER-PIN spectrometer, the energy spectra of soft X-ray from a small gas-puff Z-pinch were investigated, and the correlation between the soft X-ray yield and the plasma implosion state was also studied. (authors)

MODELING THE THERMAL DIFFUSE SOFT AND HARD X-RAY EMISSION IN M17

International Nuclear Information System (INIS)

Velázquez, P. F.; Rodríguez-González, A.; Esquivel, A.; Rosado, M.; Reyes-Iturbide, J.

2013-01-01

We present numerical models of very young wind driven superbubbles. The parameters chosen for the simulations correspond to the particular case of the M17 nebula, but are appropriate for any young superbubble in which the wind sources have not completely dispersed their parental cloud. From the simulations, we computed the diffuse emission in the soft ([0.5-1.5] keV) and hard ([1.5-5] keV) X-ray bands. The total luminosity in our simulations agrees with the observations of Hyodo et al., about two orders of magnitude below the prediction of the standard model of Weaver et al.. The difference with respect to the standard (adiabatic) model is the inclusion of radiative cooling, which is still important in such young bubbles. We show that for this type of object the diffuse hard X-ray luminosity is significant compared to that of soft X-rays, contributing as much as 10% of the total luminosity, in contrast with more evolved bubbles where the hard X-ray emission is indeed negligible, being at least four orders of magnitude lower than the soft X-ray emission.

Empirical electro-optical and x-ray performance evaluation of CMOS active pixels sensor for low dose, high resolution x-ray medical imaging

International Nuclear Information System (INIS)

Arvanitis, C. D.; Bohndiek, S. E.; Royle, G.; Blue, A.; Liang, H. X.; Clark, A.; Prydderch, M.; Turchetta, R.; Speller, R.

2007-01-01

Monolithic complementary metal oxide semiconductor (CMOS) active pixel sensors with high performance have gained attention in the last few years in many scientific and space applications. In order to evaluate the increasing capabilities of this technology, in particular where low dose high resolution x-ray medical imaging is required, critical electro-optical and physical x-ray performance evaluation was determined. The electro-optical performance includes read noise, full well capacity, interacting quantum efficiency, and pixels cross talk. The x-ray performance, including x-ray sensitivity, modulation transfer function, noise power spectrum, and detection quantum efficiency, has been evaluated in the mammographic energy range. The sensor is a 525x525 standard three transistor CMOS active pixel sensor array with more than 75% fill factor and 25x25 μm pixel pitch. Reading at 10 f/s, it is found that the sensor has 114 electrons total additive noise, 10 5 electrons full well capacity with shot noise limited operation, and 34% interacting quantum efficiency at 530 nm. Two different structured CsI:Tl phosphors with thickness 95 and 115 μm, respectively, have been optically coupled via a fiber optic plate to the array resulting in two different system configurations. The sensitivity of the two different system configurations was 43 and 47 electrons per x-ray incident on the sensor. The MTF at 10% of the two different system configurations was 9.5 and 9 cycles/mm with detective quantum efficiency of 0.45 and 0.48, respectively, close to zero frequency at ∼0.44 μC/kg (1.72 mR) detector entrance exposure. The detector was quantum limited at low spatial frequencies and its performance was comparable with high resolution a:Si and charge coupled device based x-ray imagers. The detector also demonstrates almost an order of magnitude lower noise than active matrix flat panel imagers. The results suggest that CMOS active pixel sensors when coupled to structured CsI:Tl can

Correlated X-ray/UV/optical emission and short-term variability in a Seyfert 1 galaxy NGC 4593

Science.gov (United States)

Pal, Main; Naik, Sachindra

2018-03-01

We present a detailed multifrequency analysis of an intense monitoring programme of Seyfert 1 galaxy NGC 4593 over a duration of nearly for a month with Swift observatory. We used 185 pointings to study the variability in six ultraviolet/optical and two soft (0.3-1.5 keV) and hard X-ray (1.5-10 keV) bands. The amplitude of the observed variability is found to decrease from high energy to low energy (X-ray to optical) bands. Count-count plots of ultraviolet/optical bands with hard X-rays clearly suggest the presence of a mixture of two major components: (i) highly variable component such as hard X-ray emission, and (ii) slowly varying disc-like component. The variations observed in the ultraviolet/optical emission are strongly correlated with the hard X-ray band. Cross-correlation analysis provides the lags for the longer wavelengths compared to the hard X-rays. Such lags clearly suggest that the changes in the ultraviolet/optical bands follow the variations in the hard X-ray band. This implies that the observed variation in longer wavelengths is due to X-ray reprocessing. Though, the measured lag spectrum (lag versus wavelength) is well described by λ4/3 as expected from the standard disc model, the observed lags are found to be longer than the predicted values from standard disc model. This implies that the actual size of the disc of NGC 4593 is larger than the estimated size of standard thin disc as reported in active galactic nuclei such as NGC 5548 and Fairall 9.

Observation of spectral gain narrowing in a high-order harmonic seeded soft-x-ray amplifier

Czech Academy of Sciences Publication Activity Database

Tissandier, F.; Sebban, S.; Ribière, M.; Gautier, J.; Zeitoun, Ph.; Lambert, G.; Barszczak Sardinha, A.; Goddet, J.Ph.; Burgy, F.; Lefrou, T.; Valentin, C.; Rousse, A.; Guilbaud, O.; Klisnick, A.; Nejdl, Jaroslav; Mocek, Tomáš; Maynard, G.

2010-01-01

Roč. 81, č. 6 (2010), 063833/1-063833/4 ISSN 1050-2947 R&D Projects: GA AV ČR IAA100100911 Institutional research plan: CEZ:AV0Z10100523 Keywords : high-order harmonic * soft-x-ray * amplification * OFI * gain narrowing * Ni-like krypton plasma Subject RIV: BH - Optics, Masers, Lasers Impact factor: 2.861, year: 2010 http://pra.aps.org/abstract/PRA/v81/i6/e063833

Detectability of Sungrazing Comet Soft X-ray Irradiance

Directory of Open Access Journals (Sweden)

Su Yeon Oh

2007-12-01

Full Text Available Originating from the Oort cloud, some comets disappear to impact against the Sun or to split up by strong gravitational force. Then they don't go back to the Oort cloud. They are called sungrazing comets. The comets are detected by sublimation of ices and ejection of gas and dust through solar heat close to the Sun. There exists the charge transfer from heavy ions in the solar wind to neutral atoms in the cometary atmosphere by interaction with the solar wind. Cometary atoms would be excited to high electronic levels and their de-excitation would result in X-ray emission, or it would be scattering of solar X-ray emission by very small cometary grains. We calculated the X-ray emission applying the model suggested by Mendis & Flammer (1984 and Cravens (1997. In our estimation, the sungrazing comet whose nucleus size is about 1 km in radius might be detectable within a distance of 3 solar radius from the sun on soft X-ray solar camera.

Generation of attosecond soft x-ray pulses in a longitudinal space charge amplifier

Directory of Open Access Journals (Sweden)

M. Dohlus

2011-09-01

Full Text Available A longitudinal space charge amplifier (LSCA, operating in soft x-ray regime, was recently proposed. Such an amplifier consists of a few amplification cascades (focusing channel and chicane and a short radiator undulator in the end. The broadband nature of LSCA supports generation of few-cycle pulses as well as wavelength compression. In this paper we consider an application of these properties of LSCA for generation of attosecond x-ray pulses. It is shown that a compact and cheap addition to the soft x-ray free-electron laser facility FLASH would allow one to generate 60 attosecond (FWHM long x-ray pulses with the peak power at the 100 MW level and a contrast above 98%.

Laser interaction with matter as a source of U.V. and soft X-ray radiation: application to X-ray cinematography

International Nuclear Information System (INIS)

Tonon, G.F.; Colombant, Denis; Delmare, Claude; Rabeau, Maxime

A new detecting device is described. It allows one to get the frequency, the time and space resolution of pictures of U.V. and soft X ray emission of a laser created plasma in a single shot: X ray pictures of such a plasma are presented. After these preliminary results, it is possible to set up readily an X ray framing camera. A laser created plasma is an X ray source of special interest: the emitted power can be 10% of the laser intensity and the emitted spectrum is centered around 1A wavelength [fr

Design of a normal incidence multilayer imaging X-ray microscope

Science.gov (United States)

Shealy, David L.; Gabardi, David R.; Hoover, Richard B.; Walker, Arthur B. C., Jr.; Lindblom, Joakim F.

Normal incidence multilayer Cassegrain X-ray telescopes were flown on the Stanford/MSFC Rocket X-ray Spectroheliograph. These instruments produced high spatial resolution images of the sun and conclusively demonstrated that doubly reflecting multilayer X-ray optical systems are feasible. The images indicated that aplanatic imaging soft X-ray/EUV microscopes should be achievable using multilayer optics technology. A doubly reflecting normal incidence multilayer imaging X-ray microscope based on the Schwarzschild configuration has been designed. The design of the microscope and the results of the optical system ray trace analysis are discussed. High resolution aplanatic imaging X-ray microscopes using normal incidence multilayer X-ray mirrors should have many important applications in advanced X-ray astronomical instrumentation, X-ray lithography, biological, biomedical, metallurgical, and laser fusion research.

Soft X-ray production by photon scattering in pulsating binary neutron star sources

International Nuclear Information System (INIS)

Bussard, R.W.; Meszaros, P.; Alexander, S.

1985-01-01

A new mechanism is proposed as a source of soft (less than 1 keV) radiation in binary pulsating X-ray sources, in the form of photon scattering which leaves the electron in an excited Landau level. In a plasma with parameters typical of such sources, the low-energy X-ray emissivity of this mechanism far exceeds that of bremsstrahlung. This copious source of soft photons is quite adequate to provide the seed photons needed to explain the power-law hard X-ray spectrum by inverse Comptonization on the hot electrons at the base of the accretion column. 13 references

Present status of research and development on X-ray microprobe

International Nuclear Information System (INIS)

Koike, Masaki; Suzuki, I.H.

1991-01-01

X-ray beam micro-analysis has advanced rapidly in these years in conjunction with the development of powerful X-ray sources. Among a variety of methods being attempted, the method using a collimated narrow beam has been important because of high brightness, and of usability in both regions of soft and hard X-rays. In the soft X-ray region, the focused beam is formed by a fresnel zone plate or a Schwaltzschild mirror assembly, and can be used for scanning transmission microscope or scanning photoelectron microscope. In the hard X-ray region, the beam is formed by grazing incidence mirrors, and can be used for X-ray fluorescence micro-analysis for obtaining elemental mapping. In this report, the recent progress on the soft X-ray scanning microscopy and the X-ray microprobe has been surveyed, together with the improvement on the related optical elements. (author) 84 refs

Soft x-ray scanning microtomography with submicron resolution

International Nuclear Information System (INIS)

McNulty, I.; Haddad, W.S.; Trebes, J.E.; Anderson, E.H.

1994-01-01

Scanning soft x-ray microtomography was used to obtain high-resolution three-dimensional images of a microfabricated test object. Using a special rotation stage mounted on the scanning transmission x-ray microscope at the XIA Beamline at the National Synchrotron Light Source, we recorded nine two-dimensional projections of the 3D test object over an angular range of -50 degrees to +55 degrees. The x-ray wavelength was 3.6 nm and the radiation dose to the object per projection was approximately 2 x 10 6 Gy. The object consisted of two gold patterns supported on transparent silicon nitride membranes, separated by 4.75 Jim, with 100 to 300-nm wide and 65-nm thick features. We reconstructed a volumetric data set of the test object from the two-dimensional projections using an algebraic reconstruction technique algorithm. Features of the test object were resolved to ∼100 nm in transverse and longitudinal extent in three-dimensional images rendered from the volumetric set

A Soft X-ray Imager for MIRAX

International Nuclear Information System (INIS)

Zand, Jean in 't; Mels, Wim; Heise, John

2006-01-01

The flight spare model of the BeppoSAX Wide Field Cameras is being considered as the Soft X-ray Imager for MIRAX. A description is provided of this instrument, the performance of its siblings on BeppoSAX, and the prospects of flying it on MIRAX. Like on BeppoSAX, the instrument on MIRAX will excel in the study of transient phenomena lasting shorter than 1 day

Current sheath curvature correlation with the neon soft x-ray emission from plasma focus device

International Nuclear Information System (INIS)

Zhang, T; Lin, X; Chandra, K A; Tan, T L; Springham, S V; Patran, A; Lee, P; Lee, S; Rawat, R S

2005-01-01

The insulator sleeve length is one of the major parameters that can severely affect the neon soft x-ray yield from a plasma focus. The effect of the insulation sleeve length on various characteristic timings of plasma focus discharges and hence the soft x-ray emission characteristics has been investigated using a resistive divider. The pinhole images and laser shadowgraphy are used to explain the observed variation in the average soft x-ray yield (measured using a diode x-ray spectrometer) with variation of the insulator sleeve length. We have found that for a neon filled plasma focus device the change in insulator sleeve length changes the current sheath curvature angle and thus the length of the focused plasma column. The optimized current sheath curvature angle is found to be between 39 0 and 41 0 , at the specific axial position of 6.2-9.3 cm from the cathode support plate, for our 3.3 kJ plasma focus device. A strong dependence of the neon soft x-ray yield on the current sheath curvature angle has thus been reported

Experimental characterization of X-ray transverse coherence in the presence of beam transport optics

DEFF Research Database (Denmark)

Chubar, O.; Fluerasu, A.; Chu, Y.S.

2013-01-01

A simple Boron fiber based interference scheme [1] and other similar schemes are currently routinely used for X-ray coherence estimation at 3rd generation synchrotron radiation sources. If such a scheme is applied after a perfect monochromator and without any focusing / transport optics...... in the optical path, the interpretation of the measured interference pattern is relatively straightforward and can be done in terms of the basic parameters of the source [2]. However, if the interference scheme is used after some focusing optics, e.g. close to the X-ray beam waist, the visibility of fringes can...... be significantly affected by the new shape of the focused beam phase-space. At the same time, optical element imperfections still have a negative impact on the transverse coherence. In such situations, which are frequently encountered in experiments at beamlines, the quantitative interpretation of a measured...

Triggering photochemical processes in frozen extraterrestrial worlds by soft X-rays

International Nuclear Information System (INIS)

Pilling, Sergio; Bergantini, Alexandre; Vasconcelos, Fredson A; Rocha, Will R M

2015-01-01

We presents and experimental investigation on the effects produced by broad band soft X-rays (combined with a small fraction of vacuum ultra violet photons and possibly secondary elec-trons) on the surface of three moons of giant planets: Europa, Titan and Enceladus. Such environ-ments are constantly exposed to space ionizing agents (UV and soft X-rays photons, electrons and ions) allowing photodissociation processes, surface photochemistry and prebiotic chemistry. The processing of such spatial ices have promoted an enhancement in the chemical complexity, similar what may have happened in the early earth triggering the arising of life. (paper)

X-ray spectra of PG quasars. II - the X-ray-ultraviolet excess of PG 1211 + 143

International Nuclear Information System (INIS)

Bechtold, J.; Czerny, B.; Elvis, M.; Fabbiano, G.; Green, R.F.; Harvard-Smithsonian Center for Astrophysics, Cambridge, MA; Kitt Peak National Observatory, Tucson, AZ)

1987-01-01

Observations of the quasar PG 1211 + 143 are presented and its continuum is modelled in terms of an accretion disk and an underlying power law. The X-ray spectrum in the Einstein imaging proportional counter band is well described by a power law with the very steep spectral index 2.2 + or - 0.4. The overall continuum spectral energy distribution can be described as a power law with alpha roughly 1.2 from the infrared to about 1 keV, with the optical, ultraviolet, and soft X-rays forming a large excess above this power law. If the soft X-ray excess is attributed to emission from a physically thin, optically thick accretion disk, then the implied accretion rate is super-Eddington, from which it is concluded that the application of this simple model is not valid. The observed broad-line ratios in PG 1211 + 143 imply broad-line cloud densities that are somewhat higher than those usually derived for quasars. 82 references

Soft X-ray radiation damage in EM-CCDs used for Resonant Inelastic X-ray Scattering

Science.gov (United States)

Gopinath, D.; Soman, M.; Holland, A.; Keelan, J.; Hall, D.; Holland, K.; Colebrook, D.

2018-02-01

Advancement in synchrotron and free electron laser facilities means that X-ray beams with higher intensity than ever before are being created. The high brilliance of the X-ray beam, as well as the ability to use a range of X-ray energies, means that they can be used in a wide range of applications. One such application is Resonant Inelastic X-ray Scattering (RIXS). RIXS uses the intense and tuneable X-ray beams in order to investigate the electronic structure of materials. The photons are focused onto a sample material and the scattered X-ray beam is diffracted off a high resolution grating to disperse the X-ray energies onto a position sensitive detector. Whilst several factors affect the total system energy resolution, the performance of RIXS experiments can be limited by the spatial resolution of the detector used. Electron-Multiplying CCDs (EM-CCDs) at high gain in combination with centroiding of the photon charge cloud across several detector pixels can lead to sub-pixel spatial resolution of 2-3 μm. X-ray radiation can cause damage to CCDs through ionisation damage resulting in increases in dark current and/or a shift in flat band voltage. Understanding the effect of radiation damage on EM-CCDs is important in order to predict lifetime as well as the change in performance over time. Two CCD-97s were taken to PTB at BESSY II and irradiated with large doses of soft X-rays in order to probe the front and back surfaces of the device. The dark current was shown to decay over time with two different exponential components to it. This paper will discuss the use of EM-CCDs for readout of RIXS spectrometers, and limitations on spatial resolution, together with any limitations on instrument use which may arise from X-ray-induced radiation damage.

A new streaked soft x-ray imager for the National Ignition Facility

Energy Technology Data Exchange (ETDEWEB)

Benstead, J., E-mail: james.benstead@awe.co.uk; Morton, J.; Guymer, T. M.; Garbett, W. J.; Rubery, M. S.; Skidmore, J. W. [AWE, Aldermaston, Reading, Berkshire RG7 4PR (United Kingdom); Moore, A. S.; Ahmed, M. F.; Soufli, R.; Pardini, T.; Hibbard, R. L.; Bailey, C. G.; Bell, P. M.; Hau-Riege, S. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Bedzyk, M.; Shoup, M. J.; Reagan, S.; Agliata, T.; Jungquist, R. [Laboratory for Laser Energetics, University of Rochester, Rochester, New York 14623 (United States); Schmidt, D. W. [Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States); and others

2016-05-15

A new streaked soft x-ray imager has been designed for use on high energy-density (HED) physics experiments at the National Ignition Facility based at the Lawrence Livermore National Laboratory. This streaked imager uses a slit aperture, single shallow angle reflection from a nickel mirror, and soft x-ray filtering to, when coupled to one of the NIF’s x-ray streak cameras, record a 4× magnification, one-dimensional image of an x-ray source with a spatial resolution of less than 90 μm. The energy band pass produced depends upon the filter material used; for the first qualification shots, vanadium and silver-on-titanium filters were used to gate on photon energy ranges of approximately 300–510 eV and 200–400 eV, respectively. A two-channel version of the snout is available for x-ray sources up to 1 mm and a single-channel is available for larger sources up to 3 mm. Both the one and two-channel variants have been qualified on quartz wire and HED physics target shots.

Active x-ray optics for high resolution space telescopes

Science.gov (United States)