WorldWideScience

Sample records for sem thermal analysis

  1. Technical damage analysis of a mechanical seal based on thermal waves and correlated with EDX and SEM

    Science.gov (United States)

    Haj-Daoud, A.; Katscher, U.; Bein, B. K.; Pelzl, J.; Bach, H.; Oswald, W.

    1999-03-01

    A seal which had been in contact with sea water of high salt concentration, has been analysed, in order to characterize the erosion effects and throw light on the erosion mechanisms. The measured effective thermal depth profiles have been interpreted phenomenologically and have been correlated with energy-dispersive X-ray microanalysis (EDX) and scanning electron microscopy (SEM).

  2. SEM analysis for irradiated materials

    International Nuclear Information System (INIS)

    Liu Xiaosong; Yao Liang

    2008-06-01

    A radiation-proof Scanning Electron Microscope (SEM) system is introduced. It has been widely used in various areas. For analyzing radioactive samples, normal SEM system needs lots of alterations. Based on KYKY-2800B SEM, the sample room, belt line, operating table and aerator were updated. New radiation-proof SEM system has used to analytic surface contaminated samples and RPV materials samples. An elementary means of SEM analysis for radioactive samples was studied, and this examination supported some available references for further irradiated fuel researches. (authors)

  3. Framework for SEM contour analysis

    Science.gov (United States)

    Schneider, L.; Farys, V.; Serret, E.; Fenouillet-Beranger, C.

    2017-03-01

    SEM images provide valuable information about patterning capability. Geometrical properties such as Critical Dimension (CD) can be extracted from them and are used to calibrate OPC models, thus making OPC more robust and reliable. However, there is currently a shortage of appropriate metrology tools to inspect complex two-dimensional patterns in the same way as one would work with simple one-dimensional patterns. In this article we present a full framework for the analysis of SEM images. It has been proven to be fast, reliable and robust for every type of structure, and particularly for two-dimensional structures. To achieve this result, several innovative solutions have been developed and will be presented in the following pages. Firstly, we will present a new noise filter which is used to reduce noise on SEM images, followed by an efficient topography identifier, and finally we will describe the use of a topological skeleton as a measurement tool that can extend CD measurements on all kinds of patterns.

  4. The application of thermal analysis, XRD and SEM to study the hydration behavior of tricalcium silicate in the presence of a polycarboxylate superplasticizer

    International Nuclear Information System (INIS)

    Liu, Ming; Lei, Jiaheng; Guo, Liping; Du, Xiaodi; Li, Junsheng

    2015-01-01

    Highlights: • The initial hydration process of C 3 S is markedly retarded by PC. • The decomposition temperature of Ca(OH) 2 is slightly lower after PC modification. • The adsorption amount of PC on C 3 S increases progressively with the hydration time. • The size of Ca(OH) 2 crystals are changed due to the adsorption of PC. - Abstract: Hydration behavior of tricalcium silicate (C 3 S) in the presence of a polycarboxylate (PC) superplasticizer was investigated by means of isothermal calorimetry, differential thermal analysis and X-ray diffraction. In addition, the adsorption characteristics of PC and morphology change of Ca(OH) 2 crystals were also examined, respectively. The results showed that initial hydration process of C 3 S was markedly retarded by PC and the retardation effect depended on the dosage of PC. The decomposition temperature of the Ca(OH) 2 was slightly lower after PC modification. Moreover, the size of Ca(OH) 2 crystals were found to be changed due to the adsorption of PC. The results obtained in this research allowed us to gain insights into the interactions between PC and cement

  5. Role of scanning electron microscope )SEM) in metal failure analysis

    International Nuclear Information System (INIS)

    Shaiful Rizam Shamsudin; Hafizal Yazid; Mohd Harun; Siti Selina Abd Hamid; Nadira Kamarudin; Zaiton Selamat; Mohd Shariff Sattar; Muhamad Jalil

    2005-01-01

    Scanning electron microscope (SEM) is a scientific instrument that uses a beam of highly energetic electrons to examine the surface and phase distribution of specimens on a micro scale through the live imaging of secondary electrons (SE) and back-scattered electrons (BSE) images. One of the main activities of SEM Laboratory at MINT is for failure analysis on metal part and components. The capability of SEM is excellent for determining the root cause of metal failures such as ductility or brittleness, stress corrosion, fatigue and other types of failures. Most of our customers that request for failure analysis are from local petrochemical plants, manufacturers of automotive components, pipeline maintenance personnel and engineers who involved in the development of metal parts and component. This paper intends to discuss some of the technical concepts in failure analysis associated with SEM. (Author)

  6. Correlative SEM SERS for quantitative analysis of dimer nanoparticles.

    Science.gov (United States)

    Timmermans, F J; Lenferink, A T M; van Wolferen, H A G M; Otto, C

    2016-11-14

    A Raman microscope integrated with a scanning electron microscope was used to investigate plasmonic structures by correlative SEM-SERS analysis. The integrated Raman-SEM microscope combines high-resolution electron microscopy information with SERS signal enhancement from selected nanostructures with adsorbed Raman reporter molecules. Correlative analysis is performed for dimers of two gold nanospheres. Dimers were selected on the basis of SEM images from multi aggregate samples. The effect of the orientation of the dimer with respect to the polarization state of the laser light and the effect of the particle gap size on the Raman signal intensity is observed. Additionally, calculations are performed to simulate the electric near field enhancement. These simulations are based on the morphologies observed by electron microscopy. In this way the experiments are compared with the enhancement factor calculated with near field simulations and are subsequently used to quantify the SERS enhancement factor. Large differences between experimentally observed and calculated enhancement factors are regularly detected, a phenomenon caused by nanoscale differences between the real and 'simplified' simulated structures. Quantitative SERS experiments reveal the structure induced enhancement factor, ranging from ∼200 to ∼20 000, averaged over the full nanostructure surface. The results demonstrate correlative Raman-SEM microscopy for the quantitative analysis of plasmonic particles and structures, thus enabling a new analytical method in the field of SERS and plasmonics.

  7. SEM Analysis of Surface Impact on Biofilm Antibiotic Treatment.

    Science.gov (United States)

    Gomes, Luciana Calheiros; Mergulhão, Filipe José

    2017-01-01

    The aim of this work was to use scanning electron microscopy (SEM) to investigate the effect of ampicillin treatment on Escherichia coli biofilms formed on two surface materials with different properties, silicone (SIL) and glass (GLA). Epifluorescence microscopy (EM) was initially used to assess biofilm formation and killing efficiency on both surfaces. This technique showed that higher bacterial colonization was obtained in the hydrophobic SIL than in the hydrophilic GLA. It has also shown that higher biofilm inactivation was attained for GLA after the antibiotic treatment (7-log reduction versus 1-log reduction for SIL). Due to its high resolution and magnification, SEM enabled a more detailed analysis of the antibiotic effect on biofilm cells, complementing the killing efficiency information obtained by EM. SEM micrographs revealed that ampicillin-treated cells have an elongated form when compared to untreated cells. Additionally, it has shown that different materials induced different levels of elongation on cells exposed to antibiotic. Biofilms formed on GLA showed a 37% higher elongation than those formed on SIL. Importantly, cell elongation was related to viability since ampicillin had a higher bactericidal effect on GLA-formed biofilms. These findings raise the possibility of using SEM for understanding the efficacy of antimicrobial treatments by observation of biofilm morphology.

  8. Analysis of microtraces in invasive traumas using SEM/EDS.

    Science.gov (United States)

    Vermeij, E J; Zoon, P D; Chang, S B C G; Keereweer, I; Pieterman, R; Gerretsen, R R R

    2012-01-10

    Scanning electron microscopy in combination with energy-dispersive X-ray spectrometry (SEM/EDS) is a proven forensic tool and has been used to analyze several kinds of trace evidence. A forensic application of SEM/EDS is the examination of morphological characteristics of tool marks that tools and instruments leave on bone. The microtraces that are left behind by these tools and instruments on the bone are, however, often ignored or not noticed at all. In this paper we will describe the use of SEM/EDS for the analysis of microtraces in invasive sharp-force, blunt-force and bone-hacking traumas in bone. This research is part of a larger multi-disciplinary approach in which pathologists, forensic anthropologists, toolmark and microtrace experts work together to link observed injuries to a suspected weapon or, in case of an unknown weapon, to indicate a group of objects that could have been used as a weapon. Although there are a few difficulties one have to consider, the method itself is rather simple and straightforward to apply. A sample of dry and clean bone is placed into the SEM sample chamber and brightness and contrast are set such that bone appears grey, metal appears white and organic material appears black. The sample is then searched manually to find relevant features. Once features are found their elemental composition is measured by an energy dispersive X-ray spectrometer (EDS). This method is illustrated using several cases. It is shown that SEM/EDS analysis of microtraces in bone is a valuable tool to get clues about an unknown weapon and can associate a specific weapon with injuries on the basis of appearance and elemental composition. In particular the separate results from the various disciplines are complementary and may be combined to reach a conclusion with a stronger probative value. This is not only useful in the courtroom but above all in criminal investigations when one have to know for what weapon or object to look for. Copyright © 2011

  9. Analysis list: sem-4 [Chip-atlas[Archive

    Lifescience Database Archive (English)

    Full Text Available sem-4 Larvae + ce10 http://dbarchive.biosciencedbc.jp/kyushu-u/ce10/target/sem-4.1....tsv http://dbarchive.biosciencedbc.jp/kyushu-u/ce10/target/sem-4.5.tsv http://dbarchive.biosciencedbc.jp/kyushu-u/ce10/target/sem...-4.10.tsv http://dbarchive.biosciencedbc.jp/kyushu-u/ce10/colo/sem-4.Larvae.tsv http://dbarchive.biosciencedbc.jp/kyushu-u/ce10/colo/Larvae.gml ...

  10. Thermal Properties and Thermal Analysis:

    Science.gov (United States)

    Kasap, Safa; Tonchev, Dan

    The chapter provides a summary of the fundamental concepts that are needed to understand the heat capacity C P, thermal conductivity κ, and thermal expansion coefficient α L of materials. The C P, κ, and α of various classes of materials, namely, semiconductors, polymers, and glasses, are reviewed, and various typical characteristics are summarized. A key concept in crystalline solids is the Debye theory of the heat capacity, which has been widely used for many decades for calculating the C P of crystals. The thermal properties are interrelated through Grüneisen's theorem. Various useful empirical rules for calculating C P and κ have been used, some of which are summarized. Conventional differential scanning calorimetry (DSC) is a powerful and convenient thermal analysis technique that allows various important physical and chemical transformations, such as the glass transition, crystallization, oxidation, melting etc. to be studied. DSC can also be used to obtain information on the kinetics of the transformations, and some of these thermal analysis techniques are summarized. Temperature-modulated DSC, TMDSC, is a relatively recent innovation in which the sample temperature is ramped slowly and, at the same time, sinusoidally modulated. TMDSC has a number of distinct advantages compared with the conventional DSC since it measures the complex heat capacity. For example, the glass-transition temperature T g measured by TMDSC has almost no dependence on the thermal history, and corresponds to an almost step life change in C P. The new Tzero DSC has an additional thermocouple to calibrate better for thermal lags inherent in the DSC measurement, and allows more accurate thermal analysis.

  11. Automated SEM Modal Analysis Applied to the Diogenites

    Science.gov (United States)

    Bowman, L. E.; Spilde, M. N.; Papike, James J.

    1996-01-01

    Analysis of volume proportions of minerals, or modal analysis, is routinely accomplished by point counting on an optical microscope, but the process, particularly on brecciated samples such as the diogenite meteorites, is tedious and prone to error by misidentification of very small fragments, which may make up a significant volume of the sample. Precise volume percentage data can be gathered on a scanning electron microscope (SEM) utilizing digital imaging and an energy dispersive spectrometer (EDS). This form of automated phase analysis reduces error, and at the same time provides more information than could be gathered using simple point counting alone, such as particle morphology statistics and chemical analyses. We have previously studied major, minor, and trace-element chemistry of orthopyroxene from a suite of diogenites. This abstract describes the method applied to determine the modes on this same suite of meteorites and the results of that research. The modal abundances thus determined add additional information on the petrogenesis of the diogenites. In addition, low-abundance phases such as spinels were located for further analysis by this method.

  12. FIB/SEM and SEM/EDS microstructural analysis of metal-ceramic and zirconia-ceramic interfaces.

    Science.gov (United States)

    Massimi, F; Merlati, G; Sebastiani, M; Battaini, P; Menghini, P; Bemporad, E

    2012-01-10

    Recently introduced FIB/SEM analysis in microscopy seems to provide a high-resolution characterization of the samples by 3D (FIB) cross-sectioning and (SEM) high resolution imaging. The aim of this study was to apply the FIB/SEM and SEM/EDS analysis to the interfaces of a metal-ceramic vs. two zirconia-ceramic systems. Plate samples of three different prosthetic systems were prepared in the dental lab following the manufacturers' instructions, where metal-ceramic was the result of a ceramic veneering (porcelain-fused-to-metal) and the two zirconia-ceramic systems were produced by the dedicated CAD-CAM procedures of the zirconia cores (both with final sintering) and then veneered by layered or heat pressed ceramics. In a FIB/SEM equipment (also called DualBeam), a thin layer of platinum (1 μm) was deposited on samples surface crossing the interfaces, in order to protect them during milling. Then, increasingly deeper trenches were milled by a focused ion beam, first using a relatively higher and later using a lower ion current (from 9 nA to 0.28 nA, 30KV). Finally, FEG-SEM (5KV) micrographs (1000-50,000X) were acquired. In a SEM the analysis of the morphology and internal microstructure was performed by 13KV secondary and backscattered electrons signals (in all the samples). The compositional maps were then performed by EDS probe only in the metal-ceramic system (20kV). Despite the presence of many voids in all the ceramic layers, it was possible to identify: (1) the grain structures of the metallic and zirconia substrates, (2) the thin oxide layer at the metal-ceramic interface and its interactions with the first ceramic layer (wash technique), (3) the roughness of the two different zirconia cores and their interactions with the ceramic interface, where the presence of zirconia grains in the ceramic layer was reported in two system possibly due to sandblasting before ceramic firing.

  13. Bottom-up nanoarchitecture of semiconductor nano-building blocks by controllable in situ SEM-FIB thermal soldering method

    KAUST Repository

    Zhang, Xuan

    2017-08-10

    Here we demonstrate that the building blocks of semiconductor WO3 nanowires can be controllably soldered together by a novel nano-soldering technique of in situ SEM-FIB thermal soldering, in which the soldering temperature can precisely remain in an optimal range to avoid a strong thermal diffusion.

  14. Bottom-up nanoarchitecture of semiconductor nano-building blocks by controllable in situ SEM-FIB thermal soldering method

    KAUST Repository

    Zhang, Xuan; Zheng, Xiujun; Zhang, Hong; Zhang, Junli; Fu, Jiecai; Zhang, Qiang; Peng, Chaoyi; Bai, Feiming; Zhang, Xixiang; Peng, Yong

    2017-01-01

    Here we demonstrate that the building blocks of semiconductor WO3 nanowires can be controllably soldered together by a novel nano-soldering technique of in situ SEM-FIB thermal soldering, in which the soldering temperature can precisely remain in an optimal range to avoid a strong thermal diffusion.

  15. Multiple-Group Analysis Using the sem Package in the R System

    Science.gov (United States)

    Evermann, Joerg

    2010-01-01

    Multiple-group analysis in covariance-based structural equation modeling (SEM) is an important technique to ensure the invariance of latent construct measurements and the validity of theoretical models across different subpopulations. However, not all SEM software packages provide multiple-group analysis capabilities. The sem package for the R…

  16. SEM/TIMS analysis trials on hotswipe samples taken from a shielded cell at Harwell

    International Nuclear Information System (INIS)

    Tushingham, J.; Vatter, I.; Cooke, R.

    1998-09-01

    The IAEA require advanced techniques and procedures for the detection of traces of actinides to be applied to their environmental sampling programme for nuclear safeguards as a means to detect undeclared activities. 'Swipe' samples taken from within nuclear facilities by IAEA inspectors require analysis to determine their actinide content and composition by bulk and particle measurements. The use of analytical equipment capable of analysing individual particles, particularly of actinides, is essential to optimise the IAEA's aim to monitor Member State's nuclear activities more proficiently. A trial has been undertaken at the Harwell Laboratory of AEA Technology to establish the efficacy of scanning electron microscopy (SEM) and thermal ionisation mass spectrometry (TIMS) for the particle and bulk characterisation, respectively, of actinides on samples taken from within a shielded cell. These measurements were supported by γ-spectrometry and α-spectrometry. 'Hotswipe' samples taken from within a shielded cell with a well-known recent history have been prepared for particle and bulk analysis. SEM has been used to characterise individual particles from the swipe samples and the results have been related to known cell activities. Samples were prepared for SEM using a simple procedure to minimise the potential for sample contamination. The method proved to be capable of identifying 1 μm particles that contained U, Pu, Pa and Np. The measurement of U/Pu ratios was limited to particles that contained >2% Pu in U by weight. TIMS, together with alpha spectrometry, has been used to determine the bulk actinide composition of the samples whilst gamma spectrometry has been used to determine the fission product composition. Further work to improve the potential of SEM, and also secondary ionisation mass spectrometry (SIMS), for the measurement of hotswipe samples has been proposed. (author)

  17. A Proposal on the Quantitative Homogeneity Analysis Method of SEM Images for Material Inspections

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Song Hyun; Kim, Jong Woo; Shin, Chang Ho [Hanyang University, Seoul (Korea, Republic of); Choi, Jung-Hoon; Cho, In-Hak; Park, Hwan Seo [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2015-05-15

    A scanning electron microscope (SEM) is a method to inspect the surface microstructure of materials. The SEM uses electron beams for imaging high magnifications of material surfaces; therefore, various chemical analyses can be performed from the SEM images. Therefore, it is widely used for the material inspection, chemical characteristic analysis, and biological analysis. For the nuclear criticality analysis field, it is an important parameter to check the homogeneity of the compound material for using it in the nuclear system. In our previous study, the SEM was tried to use for the homogeneity analysis of the materials. In this study, a quantitative homogeneity analysis method of SEM images is proposed for the material inspections. The method is based on the stochastic analysis method with the information of the grayscales of the SEM images.

  18. A Proposal on the Quantitative Homogeneity Analysis Method of SEM Images for Material Inspections

    International Nuclear Information System (INIS)

    Kim, Song Hyun; Kim, Jong Woo; Shin, Chang Ho; Choi, Jung-Hoon; Cho, In-Hak; Park, Hwan Seo

    2015-01-01

    A scanning electron microscope (SEM) is a method to inspect the surface microstructure of materials. The SEM uses electron beams for imaging high magnifications of material surfaces; therefore, various chemical analyses can be performed from the SEM images. Therefore, it is widely used for the material inspection, chemical characteristic analysis, and biological analysis. For the nuclear criticality analysis field, it is an important parameter to check the homogeneity of the compound material for using it in the nuclear system. In our previous study, the SEM was tried to use for the homogeneity analysis of the materials. In this study, a quantitative homogeneity analysis method of SEM images is proposed for the material inspections. The method is based on the stochastic analysis method with the information of the grayscales of the SEM images

  19. Comparative SEM analysis of nine F22 aligner cleaning strategies.

    Science.gov (United States)

    Lombardo, Luca; Martini, Marco; Cervinara, Francesca; Spedicato, Giorgio Alfredo; Oliverio, Teresa; Siciliani, Giuseppe

    2017-12-01

    The orthodontics industry has paid great attention to the aesthetics of orthodontic appliances, seeking to make them as invisible as possible. There are several advantages to clear aligner systems, including aesthetics, comfort, chairside time reduction, and the fact that they can be removed for meals and oral hygiene procedures. Five patients were each given a series of F22 aligners, each to be worn for 14 days and nights, with the exception of meal and brushing times. Patients were instructed to clean each aligner using a prescribed strategy, and sections of the used aligners were observed under SEM. One grey-scale SEM image was saved per aligner in JPEG format with an 8-bit colour depth, and a total of 45 measurements on the grey scale ("Value" variable) were made. This dataset was analysed statistically via repeated measures ANOVA to determine the effect of each of the nine cleaning strategies in each of the five patients. A statistically significant difference in the efficacy of the cleaning strategies was detected. Specifically, rinsing with water alone was significantly less efficacious, and a combination of cationic detergent solution and ultrasonication was significantly more efficacious than the other methods (p aligners.

  20. Comparative SEM analysis of nine F22 aligner cleaning strategies

    Directory of Open Access Journals (Sweden)

    Luca Lombardo

    2017-09-01

    Full Text Available Abstract Background The orthodontics industry has paid great attention to the aesthetics of orthodontic appliances, seeking to make them as invisible as possible. There are several advantages to clear aligner systems, including aesthetics, comfort, chairside time reduction, and the fact that they can be removed for meals and oral hygiene procedures. Methods Five patients were each given a series of F22 aligners, each to be worn for 14 days and nights, with the exception of meal and brushing times. Patients were instructed to clean each aligner using a prescribed strategy, and sections of the used aligners were observed under SEM. One grey-scale SEM image was saved per aligner in JPEG format with an 8-bit colour depth, and a total of 45 measurements on the grey scale (“Value” variable were made. This dataset was analysed statistically via repeated measures ANOVA to determine the effect of each of the nine cleaning strategies in each of the five patients. Results A statistically significant difference in the efficacy of the cleaning strategies was detected. Specifically, rinsing with water alone was significantly less efficacious, and a combination of cationic detergent solution and ultrasonication was significantly more efficacious than the other methods (p < 0.05. Conclusions Of the nine cleaning strategies examined, only that involving 5 min of ultrasonication at 42 k Hz combined with a 0.3% germicidal cationic detergent was observed to be statistically effective at removing the bacterial biofilm from the surface of F22 aligners.

  1. Quality control of clinker products by SEM and XRF analysis

    International Nuclear Information System (INIS)

    Ziad Abu Kaddourah; Khairun Azizi

    1996-01-01

    The microstructure and chemical properties of industrial Portland cement clinkers have been examined by SEM and XRF methods to establish the nature of the clinkers and how variations in the clinker characteristics can be used to control the clinker quality. The clinker nodules were found to show differences in the chemical composition and microstructure between the inner and outer parts of the clinker nodules. Microstructure studies of industrial Portland cement clinker have shown that the outer part of the nodules are enriched in silicate more than the inner part. There is better crystallization and larger alite crystal size in the outer part than in the inner part. The alite crystal size varied between 16.2 -46.12 μ m. The clinker chemical composition was found to affect the residual >45 μ m, where a higher belite content causes an increase in the residual >45 μ m in the the cement product and will cause a decrease in the concrete strength of the cement product. The aluminate and ferrite crystals and the microcracks within the alite crystal are clear in some clinker only. The quality of the raw material preparation, burning and cooling stages can be controlled using the microstructure of the clinker product

  2. stainless steel by SEM-XRD and image analysis

    Directory of Open Access Journals (Sweden)

    Robinson Constanzo-R.

    2014-01-01

    Full Text Available El objetivo de este trabajo fue realizar un análisis cualitativ o de la distribución de un electrodepósito de cobre en el inter ior de electrodos porosos (EP de acero inoxidable y carbono grafito. Para ello, se reali zaron pruebas de electrodepositación de cobre a nivel de labora torio, con un posterior análisis de cortes de muestras de acero y grafito vía Microscopía Estereoscópica, Microscopía SEM-DRX y Análisis de Imagen, los cuales mostraron que el cobre no se deposita en forma uniforme al interior del electrodo. En el electrodo de acero, la penetra ción del depósito en el espesor fue alrededor de 50%, mientras que para el grafito a lrededor de 90%. En forma general, se observó un aumento de la cantidad de depósito hacia el extremo frente al ánodo y con sitios de difer ente crecimiento en depósito de cobre. Esto demuestra una distr ibución de corriente y potencial, función de parámetros físicos de electrodo y de la s características fisicoquímicas e hidrodinámicos del electroli to.

  3. The relationship between cost estimates reliability and BIM adoption: SEM analysis

    Science.gov (United States)

    Ismail, N. A. A.; Idris, N. H.; Ramli, H.; Rooshdi, R. R. Raja Muhammad; Sahamir, S. R.

    2018-02-01

    This paper presents the usage of Structural Equation Modelling (SEM) approach in analysing the effects of Building Information Modelling (BIM) technology adoption in improving the reliability of cost estimates. Based on the questionnaire survey results, SEM analysis using SPSS-AMOS application examined the relationships between BIM-improved information and cost estimates reliability factors, leading to BIM technology adoption. Six hypotheses were established prior to SEM analysis employing two types of SEM models, namely the Confirmatory Factor Analysis (CFA) model and full structural model. The SEM models were then validated through the assessment on their uni-dimensionality, validity, reliability, and fitness index, in line with the hypotheses tested. The final SEM model fit measures are: P-value=0.000, RMSEA=0.0790.90, TLI=0.956>0.90, NFI=0.935>0.90 and ChiSq/df=2.259; indicating that the overall index values achieved the required level of model fitness. The model supports all the hypotheses evaluated, confirming that all relationship exists amongst the constructs are positive and significant. Ultimately, the analysis verified that most of the respondents foresee better understanding of project input information through BIM visualization, its reliable database and coordinated data, in developing more reliable cost estimates. They also perceive to accelerate their cost estimating task through BIM adoption.

  4. STEM mode in the SEM for the analysis of cellular sections prepared by ultramicrotome sectioning

    International Nuclear Information System (INIS)

    Hondow, N; Harrington, J; Brydson, R; Brown, A

    2012-01-01

    The use of the dual imaging capabilities of a scanning electron microscope fitted with a transmitted electron detector is highlighted in the analysis of samples with importance in the field of nanotoxicology. Cellular uptake of nanomaterials is often examined by transmission electron microscopy of thin sections prepared by ultramicrotome sectioning. Examination by SEM allows for the detection of artefacts caused by sample preparation (eg. nanomaterial pull-out) and the complementary STEM mode permits study of the interaction between nanomaterials and cells. Thin sections of two nanomaterials of importance in nanotoxicology (cadmium selenide quantum dots and single walled carbon nanotubes) are examined using STEM mode in the SEM.

  5. Analysis the fatigue using pro taper rotary instruments durin instrumentation of extrated mandibular premolars. SEM observation.

    OpenAIRE

    Siragusa, Martha; Racciatti, Gabriela; García, María

    2007-01-01

    Recibido: Marzo 2007 Aceptado: Julio 2007 Siragusa, Martha; Racciatti, Gabriela y García, María. Analysis the fatigue using pro taper rotary instruments durin instrumentation of extrated mandibular premolars. SEM observation. Electronic Journal of Endodontics Rosario [Online], Volumen 2 Número 13. [octubre 2007]. http://www.endojournal.com.ar/journal/index.php/ejer/article/view/44. ISSN 1666-6143.

  6. The use of SEM/EDS method in mineralogical analysis of ordinary chondritic meteorite

    Directory of Open Access Journals (Sweden)

    Breda Mirtič

    2009-12-01

    Full Text Available The aim of this study was to evaluate the potential of scanning electron microscopy coupled with energy dispersiveX-ray spectroscopy (SEM/EDS for determination of mineral phases according to their stoichiometry and assessment of mineral composition of ordinary chondritic meteorite. For the purposes of this study, H3 type ordinary chondritic meteorite Abbott was selected. SEM/EDS allows identification and characterisation of mineralphases, whose size is below the resolution of an optical microscope. Mineral phases in chondrules and interstitial matrix were located in backscattered electron (BSE mode and were assessed from atomic proportions of constituent elements, obtained by the EDS analysis. SEM/EDS analyses of mineral phases showed that Abbott meteorite is characterised by Fe-rich (Fe, Ni-alloy kamacite, Fe-sulphide troilite or pyrrhotite, chromite, Mg-rich olivine, orthopyroxene bronzite or hypersthene, clinopyroxene Al-diopside, acid plagioclase oligoclase, accessory mineral chlorapatite and secondary minerals Fe-hydroxides (goethite or lepidocrocite. Results of semi-quantitative analyses confirmed that most of analysed mineralphases conform well to stoichiometric minerals with minor deviations of oxygen from stoichiometric proportions. Comparison between mineral phases in chondrules and interstitial matrix was also performed, however it showed no significant differences in elemental composition.Differences in chemical composition between minerals in interstitial matrix and chondrules are sometimes too small to be discernedby the SEM/EDS, therefore knowledge of SEM/EDS capabilities is important for correct interpretation of chondrite formation.

  7. A Data Matrix Method for Improving the Quantification of Element Percentages of SEM/EDX Analysis

    Science.gov (United States)

    Lane, John

    2009-01-01

    A simple 2D M N matrix involving sample preparation enables the microanalyst to peer below the noise floor of element percentages reported by the SEM/EDX (scanning electron microscopy/ energy dispersive x-ray) analysis, thus yielding more meaningful data. Using the example of a 2 3 sample set, there are M = 2 concentration levels of the original mix under test: 10 percent ilmenite (90 percent silica) and 20 percent ilmenite (80 percent silica). For each of these M samples, N = 3 separate SEM/EDX samples were drawn. In this test, ilmenite is the element of interest. By plotting the linear trend of the M sample s known concentration versus the average of the N samples, a much higher resolution of elemental analysis can be performed. The resulting trend also shows how the noise is affecting the data, and at what point (of smaller concentrations) is it impractical to try to extract any further useful data.

  8. Quantitative Analysis of Micro-porosity of Eco-material by Using SEM Technique

    Institute of Scientific and Technical Information of China (English)

    ZHANG Ji-ru; LIU Yuan-zhi; LIU Zu-de

    2004-01-01

    Microstructure of the eco-material combining vegetation recovery with slope protection is important for determining plant-growing properties.Several techniques for analyzing the eco-material microstructure are presented,including the freeze-cut-drying method of preparing samples for scanning electronic microscopy (SEM),the SEM image processing technique and quantifying analysis method of the SEM images,and etc.The aggregates and pores in SEM images are identified using the different mathematics operators,and their effects are compared.The areas of aggregates and pores are obtained using the operator of morphology,and the influences of different thresholds in image segmentation are also discussed.The results show that the method,in which the variation of non-maximum grey-level gradient is limited,improves the effect of edge detections due to a weak distinction existing at the edge between the aggregates and pores in image.The determination of the threshold should combine the image characteristic with filling operation,so as to assure the precision of the image analysis,in which the contact-segmentation is the simplest and most effective method.The results also show that the pore areas in eco-materials are generally larger than those in the correlative soils,and their increment is large as soil fabric being fine.These differences are related to admixture of expansive perliticThe operator of morphology provides a new method for the image analysis of other porous material microstructure such as soils and concretes.

  9. A two-step FEM-SEM approach for wave propagation analysis in cable structures

    Science.gov (United States)

    Zhang, Songhan; Shen, Ruili; Wang, Tao; De Roeck, Guido; Lombaert, Geert

    2018-02-01

    Vibration-based methods are among the most widely studied in structural health monitoring (SHM). It is well known, however, that the low-order modes, characterizing the global dynamic behaviour of structures, are relatively insensitive to local damage. Such local damage may be easier to detect by methods based on wave propagation which involve local high frequency behaviour. The present work considers the numerical analysis of wave propagation in cables. A two-step approach is proposed which allows taking into account the cable sag and the distribution of the axial forces in the wave propagation analysis. In the first step, the static deformation and internal forces are obtained by the finite element method (FEM), taking into account geometric nonlinear effects. In the second step, the results from the static analysis are used to define the initial state of the dynamic analysis which is performed by means of the spectral element method (SEM). The use of the SEM in the second step of the analysis allows for a significant reduction in computational costs as compared to a FE analysis. This methodology is first verified by means of a full FE analysis for a single stretched cable. Next, simulations are made to study the effects of damage in a single stretched cable and a cable-supported truss. The results of the simulations show how damage significantly affects the high frequency response, confirming the potential of wave propagation based methods for SHM.

  10. Quantitative Determination of Noa (Naturally Occurring Asbestos) in Rocks : Comparison Between Pcom and SEM Analysis

    Science.gov (United States)

    Baietto, Oliviero; Amodeo, Francesco; Giorgis, Ilaria; Vitaliti, Martina

    2017-04-01

    The quantification of NOA (Naturally Occurring Asbestos) in a rock or soil matrix is complex and subject to numerous errors. The purpose of this study is to compare two fundamental methodologies used for the analysis: the first one uses Phase Contrast Optical Microscope (PCOM) while the second one uses Scanning Electron Microscope (SEM). The two methods, although they provide the same result, which is the asbestos mass to total mass ratio, have completely different characteristics and both present pros and cons. The current legislation in Italy involves the use of SEM, DRX, FTIR, PCOM (DM 6/9/94) for the quantification of asbestos in bulk materials and soils and the threshold beyond which the material is considered as hazardous waste is a concentration of asbestos fiber of 1000 mg/kg.(DM 161/2012). The most used technology is the SEM which is the one among these with the better analytical sensitivity.(120mg/Kg DM 6 /9/94) The fundamental differences among the analyses are mainly: - Amount of analyzed sample portion - Representativeness of the sample - Resolution - Analytical precision - Uncertainty of the methodology - Operator errors Due to the problem of quantification of DRX and FTIR (1% DM 6/9/94) our Asbestos Laboratory (DIATI POLITO) since more than twenty years apply the PCOM methodology and in the last years the SEM methodology for quantification of asbestos content. The aim of our research is to compare the results obtained from a PCOM analysis with the results provided by SEM analysis on the base of more than 100 natural samples both from cores (tunnel-boring or explorative-drilling) and from tunnelling excavation . The results obtained show, in most cases, a good correlation between the two techniques. Of particular relevance is the fact that both techniques are reliable for very low quantities of asbestos, even lower than the analytical sensitivity. This work highlights the comparison between the two techniques emphasizing strengths and weaknesses of

  11. SEM AutoAnalysis: enhancing photomask and NIL defect disposition and review

    Science.gov (United States)

    Schulz, Kristian; Egodage, Kokila; Tabbone, Gilles; Ehrlich, Christian; Garetto, Anthony

    2017-06-01

    For defect disposition and repair verification regarding printability, AIMS™ is the state of the art measurement tool in industry. With its unique capability of capturing aerial images of photomasks it is the one method that comes closest to emulating the printing behaviour of a scanner. However for nanoimprint lithography (NIL) templates aerial images cannot be applied to evaluate the success of a repair process. Hence, for NIL defect dispositioning scanning, electron microscopy (SEM) imaging is the method of choice. In addition, it has been a standard imaging method for further root cause analysis of defects and defect review on optical photomasks which enables 2D or even 3D mask profiling at high resolutions. In recent years a trend observed in mask shops has been the automation of processes that traditionally were driven by operators. This of course has brought many advantages one of which is freeing cost intensive labour from conducting repetitive and tedious work. Furthermore, it reduces variability in processes due to different operator skill and experience levels which at the end contributes to eliminating the human factor. Taking these factors into consideration, one of the software based solutions available under the FAVOR® brand to support customer needs is the aerial image evaluation software, AIMS™ AutoAnalysis (AAA). It provides fully automated analysis of AIMS™ images and runs in parallel to measurements. This is enabled by its direct connection and communication with the AIMS™tools. As one of many positive outcomes, generating automated result reports is facilitated, standardizing the mask manufacturing workflow. Today, AAA has been successfully introduced into production at multiple customers and is supporting the workflow as described above. These trends indeed have triggered the demand for similar automation with respect to SEM measurements leading to the development of SEM AutoAnalysis (SAA). It aims towards a fully automated SEM image

  12. SEM/XPS analysis of fractured adhesively bonded graphite fibre-reinforced polyimide composites

    Science.gov (United States)

    Devilbiss, T. A.; Messick, D. L.; Wightman, J. P.; Progar, D. J.

    1985-01-01

    The surfaces of the graphite fiber-reinforced polyimide composites presently pretreated prior to bonding with polyimide adhesive contained variable amounts of a fluoropolymer, as determined by X-ray photoelectron spectroscopy. Lap shear strengths were determined for unaged samples and for those aged over 500- and 1000-hour periods at 177 and 232 C. Unaged sample lap strengths, which were the highest obtained, exhibited no variation with surface pretreatment, but a significant decrease is noted with increasing aging temperature. These thermally aged samples, however, had increased surface fluorine concentration, while a minimal concentration was found in unaged samples. SEM demonstrated a progressive shift from cohesive to adhesive failure for elevated temperature-aged composites.

  13. Nanosecond pulsed laser ablation of Ge investigated by employing photoacoustic deflection technique and SEM analysis

    Energy Technology Data Exchange (ETDEWEB)

    Yaseen, Nazish; Bashir, Shazia; Shabbir, Muhammad Kaif; Jalil, Sohail Abdul; Akram, Mahreen; Hayat, Asma; Mahmood, Khaliq; Haq, Faizan-ul; Ahmad, Riaz; Hussain, Tousif

    2016-06-01

    Nanosecond pulsed laser ablation phenomena of single crystal Ge (100) has been investigated by employing photoacoustic deflection as well as SEM analysis techniques. Nd: YAG laser (1064 nm, 10 ns, 1–10 Hz) at various laser fluences ranging from 0.2 to 11 J cm{sup −2} is employed as pump beam to ablate Ge targets. In order to evaluate in-situe ablation threshold fluence of Ge by photoacoustic deflection technique, Continuous Wave (CW) He–Ne laser (632 nm, power 10 mW) is employed as a probe beam. It travels parallel to the target surface at a distance of 3 mm and after passing through Ge plasma it causes deflection due to density gradient of acoustic waves. The deflected signal is detected by photodiode and is recorded by oscilloscope. The threshold fluence of Ge, the velocity of ablated species and the amplitude of the deflected signal are evaluated. The threshold fluence of Ge comes out to be 0.5 J cm{sup −2} and is comparable with the analytical value. In order to compare the estimated value of threshold with ex-situe measurements, the quantitative analysis of laser irradiated Ge is performed by using SEM analysis. For this purpose Ge is exposed to single and multiple shots of 5, 10, 50 and 100 at various laser fluences ranging from 0.2 to 11 J cm{sup −2}. The threshold fluence for single and multiple shots as well as incubation coefficients are evaluated. It is observed that the value of incubation co-efficient decreases with increasing number of pulses and is therefore responsible for lowering the threshold fluence of Ge. SEM analysis also reveals the growth of various features such as porous structures, non-uniform ripples and blisters on the laser irradiated Ge. It is observed that both the fluence as well as number of laser shots plays a significant role for the growth of these structures.

  14. Nanosecond pulsed laser ablation of Ge investigated by employing photoacoustic deflection technique and SEM analysis

    International Nuclear Information System (INIS)

    Yaseen, Nazish; Bashir, Shazia; Shabbir, Muhammad Kaif; Jalil, Sohail Abdul; Akram, Mahreen; Hayat, Asma; Mahmood, Khaliq; Haq, Faizan-ul; Ahmad, Riaz; Hussain, Tousif

    2016-01-01

    Nanosecond pulsed laser ablation phenomena of single crystal Ge (100) has been investigated by employing photoacoustic deflection as well as SEM analysis techniques. Nd: YAG laser (1064 nm, 10 ns, 1–10 Hz) at various laser fluences ranging from 0.2 to 11 J cm"−"2 is employed as pump beam to ablate Ge targets. In order to evaluate in-situe ablation threshold fluence of Ge by photoacoustic deflection technique, Continuous Wave (CW) He–Ne laser (632 nm, power 10 mW) is employed as a probe beam. It travels parallel to the target surface at a distance of 3 mm and after passing through Ge plasma it causes deflection due to density gradient of acoustic waves. The deflected signal is detected by photodiode and is recorded by oscilloscope. The threshold fluence of Ge, the velocity of ablated species and the amplitude of the deflected signal are evaluated. The threshold fluence of Ge comes out to be 0.5 J cm"−"2 and is comparable with the analytical value. In order to compare the estimated value of threshold with ex-situe measurements, the quantitative analysis of laser irradiated Ge is performed by using SEM analysis. For this purpose Ge is exposed to single and multiple shots of 5, 10, 50 and 100 at various laser fluences ranging from 0.2 to 11 J cm"−"2. The threshold fluence for single and multiple shots as well as incubation coefficients are evaluated. It is observed that the value of incubation co-efficient decreases with increasing number of pulses and is therefore responsible for lowering the threshold fluence of Ge. SEM analysis also reveals the growth of various features such as porous structures, non-uniform ripples and blisters on the laser irradiated Ge. It is observed that both the fluence as well as number of laser shots plays a significant role for the growth of these structures.

  15. Emanation thermal analysis of SiC based materials

    Czech Academy of Sciences Publication Activity Database

    Bálek, V.; Zeleňák, V.; Mitsuhashi, T.; Bakardjieva, Snejana; Šubrt, Jan; Haneda, H.

    2002-01-01

    Roč. 67, č. 1 (2002), s. 83-89 ISSN 1418-2874 R&D Projects: GA MŠk ME 180 Grant - others:EFDA(XE) TTMA-001 Institutional research plan: CEZ:AV0Z4032918 Keywords : emanation thermal analysis * SEM * SiC nanocomposites Subject RIV: CA - Inorganic Chemistry Impact factor: 0.598, year: 2002

  16. SEM Anthology

    Science.gov (United States)

    Rodgers, Michelle; Zimar, Heather

    2004-01-01

    The "SEM Anthology" is a compilation of articles by more than 30 enrollment management professionals from a variety of institutions across the country. This collection, which has appeared in SEM Monthly over the past year, chronicles Strategic Enrollment Management efforts at campuses nationwide. The book illustrates the successes and challenges…

  17. A time-resolved current method and TSC under vacuum conditions of SEM: Trapping and detrapping processes in thermal aged XLPE insulation cables

    Science.gov (United States)

    Boukezzi, L.; Rondot, S.; Jbara, O.; Boubakeur, A.

    2017-03-01

    Thermal aging of cross-linked polyethylene (XLPE) can cause serious concerns in the safety operation in high voltage system. To get a more detailed picture on the effect of thermal aging on the trapping and detrapping process of XLPE in the melting temperature range, Thermal Stimulated Current (TSC) have been implemented in a Scanning Electron Microscope (SEM) with a specific arrangement. The XLPE specimens are molded and aged at two temperatures (120 °C and 140 °C) situated close to the melting temperature of the material. The use of SEM allows us to measure both leakage and displacement currents induced in samples under electron irradiation. The first represents the conduction process of XLPE and the second gives information on the trapping of charges in the bulk of the material. TSC associated to the SEM leads to show spectra of XLPE discharge under thermal stimulation using both currents measured after electron irradiation. It was found that leakage current in the charging process may be related to the physical defects resulting in crystallinity variation under thermal aging. However the trapped charge can be affected by the carbonyl groups resulting from the thermo-oxidation degradation and the disorder in the material. It is evidenced from the TSC spectra of unaged XLPE that there is no detrapping charge under heat stimulation. Whereas the presence of peaks in the TSC spectra of thermally aged samples indicates that there is some amount of trapped charge released by heating. The detrapping behavior of aged XLPE is supported by the supposition of the existence of two trap levels: shallow traps and deep traps. Overall, physico-chemical reactions under thermal aging at high temperatures leads to the enhancement of shallow traps density and changes in range of traps depth. These changes induce degradation of electrical properties of XLPE.

  18. Thermal analysis with expendable cartridge

    International Nuclear Information System (INIS)

    Susaki, K.; Landgraf, F.J.G.

    1981-01-01

    The pratical method of thermal analysis with expendable cartridge and some aspects of its use are presented. The results of the method applied to the system Nb-Mn are presented together with data from microprobe. (Author) [pt

  19. The influence of different skin types on GSR sampling by tape lifting for SEM analysis.

    Science.gov (United States)

    Kara, İlker

    2017-12-01

    In this study, the change in the amounts the gunshot residues (GSR) collected by the "swab" method from shooter's right hand was analyzed using Scanning Electron Microscope-Energy Dispersive Spectroscopy (SEM-EDS) to test dependency on various conditions (such as skin color of the shooter, various physical properties, hair density of hands, size of the hands, sweaty or creamy (oiliness) hands). As a result of the analysis, there was no significant difference in the amount of GSR according to skin color, however, there was a change in the amount of GSR depending on the physical characteristics of the shooter. These results thought to have practical benefits for the experts performing GSR analysis using the swab technique to assess the incidence. © 2017 Wiley Periodicals, Inc.

  20. Structure and surface morphology studies of cerium oxide system using XRD and SEM analysis

    International Nuclear Information System (INIS)

    Ahmad Jais Alimin; Farid Nasir Ani; Wan Azelee Wan Abu Bakar

    2000-01-01

    Conventional Precious Group Materials (PGM) catalyst systems have been using CeO 2 as an Oxygen Storage Capacity component in the catalyst washcoat. Due to the limitations of the PGM catalyst, researches are now focusing on improving or replacing this conventional system. In a previous work, the potential of a copper-ceria (Cu-Ce) oxide as a catalyst system has been identified. In this paper, the morphology and characterisation of Cu-Ce oxides analysed using XRD and SEM will be described. The Cu-Ce samples were prepared at a fixed ratio under temperatures of 400 o C and 800 o C. XRD diffractograms showed CeO 2 is in a cubic phase at 400 o C and 800 o C. At 800 o C, the CuO particle is visible, presumably has incorporated with the lattice structure of ceria, indicating an absent of solid state condition between copper and ceria. Analysis by SEM revealed significant increase in particle sizes with increasing calcination temperatures. (Author)

  1. Site specific SEM/FIB/TEM for analysis of lubricated sliding wear of aluminium alloy composites

    International Nuclear Information System (INIS)

    Walker, J C; Jones, H; Rainforth, W M

    2006-01-01

    Although extensive research has been undertaken into the dry sliding wear of aluminium alloys, only limited work has been reported on lubricated wear. In this paper, the lubricated sliding wear of some powder derived aluminium alloy composites is reported. Stereo pairs of the worn surface were obtained in the SEM and digitally reconstructed to give an accurate projection of the surface topography. Analysis of the average surface roughness (R a ) along chosen sections provided quantitative information about the wear mechanism. Following this, dual beam focused ion beam (FIB) was undertaken to further explore the features revealed by the SEM surface reconstructions, with TEM sections removed from selected regions. Surface deformation was confined to a narrow layer, typically 1μm thick. Subgrain size within the subsurface layer was comparable to that found in dry sliding wear tests. Reinforcement fracture occurred in the surface particles only. The resultant fragments were often incorporated back into the surface following detachment, such that the total volume fraction reinforcement at the surface was greater than in the bulk. Thus, the dynamic surface topography was a result of three factors: surface deformation, local detachment of reinforcement and re-incorporation of the fragments back into the surface

  2. SEM analysis of enamel surface treated by Er:YAG laser: influence of irradiation distance.

    Science.gov (United States)

    Souza-Gabriel, A E; Chinelatti, M A; Borsatto, M C; Pécora, J D; Palma-Dibb, R G; Corona, S A M

    2008-07-01

    Depending on the distance of laser tip to dental surface a specific morphological pattern should be expected. However, there have been limited reports that correlate the Er:YAG irradiation distance with dental morphology. To assess the influence of Er:YAG laser irradiation distance on enamel morphology, by means of scanning electron microscopy (SEM). Sixty human third molars were employed to obtain discs (approximately =1 mm thick) that were randomly assigned to six groups (n=10). Five groups received Er:YAG laser irradiation (80 mJ/2 Hz) for 20 s, according to the irradiation distance: 11, 12, 14, 16, or 17 mm and the control group was treated with 37% phosphoric acid for 15 s. The laser-irradiated discs were bisected. One hemi-disc was separated for superficial analysis without subsequent acid etching, and the other one, received the phosphoric acid for 15 s. Samples were prepared for SEM. Laser irradiation at 11 and 12 mm provided an evident ablation of enamel, with evident fissures and some fused areas. At 14, 16 and 17 mm the superficial topography was flatter than in the other distances. The subsequent acid etching on the lased-surface partially removed the disorganized tissue. Er:YAG laser in defocused mode promoted slight morphological alterations and seems more suitable for enamel conditioning than focused irradiation. The application of phosphoric acid on lased-enamel surface, regardless of the irradiation distance, decreased the superficial irregularities.

  3. Simulation of FIB-SEM images for analysis of porous microstructures.

    Science.gov (United States)

    Prill, Torben; Schladitz, Katja

    2013-01-01

    Focused ion beam nanotomography-scanning electron microscopy tomography yields high-quality three-dimensional images of materials microstructures at the nanometer scale combining serial sectioning using a focused ion beam with SEM. However, FIB-SEM tomography of highly porous media leads to shine-through artifacts preventing automatic segmentation of the solid component. We simulate the SEM process in order to generate synthetic FIB-SEM image data for developing and validating segmentation methods. Monte-Carlo techniques yield accurate results, but are too slow for the simulation of FIB-SEM tomography requiring hundreds of SEM images for one dataset alone. Nevertheless, a quasi-analytic description of the specimen and various acceleration techniques, including a track compression algorithm and an acceleration for the simulation of secondary electrons, cut down the computing time by orders of magnitude, allowing for the first time to simulate FIB-SEM tomography. © Wiley Periodicals, Inc.

  4. SEM method for direct visual tracking of nanoscale morphological changes of platinum based electrocatalysts on fixed locations upon electrochemical or thermal treatments

    Energy Technology Data Exchange (ETDEWEB)

    Zorko, Milena [National Institute of Chemistry, Hajdrihova 19, Ljubljana (Slovenia); Centre of Excellence for Low-Carbon Technologies, Hajdrihova 19, Ljubljana (Slovenia); Jozinović, Barbara [Centre of Excellence for Low-Carbon Technologies, Hajdrihova 19, Ljubljana (Slovenia); Bele, Marjan [National Institute of Chemistry, Hajdrihova 19, Ljubljana (Slovenia); Centre of Excellence for Low-Carbon Technologies, Hajdrihova 19, Ljubljana (Slovenia); Hodnik, Nejc, E-mail: nejc.hodnik@ki.si [National Institute of Chemistry, Hajdrihova 19, Ljubljana (Slovenia); Gaberšček, Miran [National Institute of Chemistry, Hajdrihova 19, Ljubljana (Slovenia); Centre of Excellence for Low-Carbon Technologies, Hajdrihova 19, Ljubljana (Slovenia)

    2014-05-01

    A general method for tracking morphological surface changes on a nanometer scale with scanning electron microscopy (SEM) is introduced. We exemplify the usefulness of the method by showing consecutive SEM images of an identical location before and after the electrochemical and thermal treatments of platinum-based nanoparticles deposited on a high surface area carbon. Observations reveal an insight into platinum based catalyst degradation occurring during potential cycling treatment. The presence of chloride clearly increases the rate of degradation. At these conditions the dominant degradation mechanism seems to be the platinum dissolution with some subsequent redeposition on the top of the catalyst film. By contrast, at the temperature of 60 °C, under potentiostatic conditions some carbon corrosion and particle aggregation was observed. Temperature treatment simulating the annealing step of the synthesis reveals sintering of small platinum based composite aggregates into uniform spherical particles. The method provides a direct proof of induced surface phenomena occurring on a chosen location without the usual statistical uncertainty in usual, random SEM observations across relatively large surface areas. - Highlights: • A new SEM method for observations of identical locations. • Nanoscale morphological consecutive changes on identical locations. • Electrochemical and thermal treatments on platinum based nanoparticles. • Potential cycling induces platinum dissolution with redeposition on top of the film. • At 1.4 V vs. RHE and 60 °C carbon corrosion and particle aggregation is observed.

  5. Thermal analysis of compositionally modulated Fe/Y films

    International Nuclear Information System (INIS)

    Kajiura, M.; Morishita, T.; Togami, Y.; Tsushima, K.

    1987-01-01

    Structures of compositionally modulated Fe/Y films were studied by thermal analysis. The exothermic peak found in the DSC curve of (Fe 12 A/Y 12 A) most probably corresponds to crystallization of an amorphous material. SEM analysis suggested that the composition of crystallized (Fe 12 A/Y 12 A) was YFe2. It is concluded that a compositionally modulated (Fe 12 A/Y 12 A) is amorphous in structure as well as in magnetic properties

  6. Thermal Analysis of Solar Panels

    Science.gov (United States)

    Barth, Nicolas; de Correia, João Pedro Magalhães; Ahzi, Saïd; Khaleel, Mohammad Ahmed

    In this work, we propose to analyze the thermal behavior of PV panels using finite element simulations (FEM). We applied this analysis to compute the temperature distribution in a PV panel BP 350 subjected to different atmospheric conditions. This analysis takes into account existing formulations in the literature and, based on NOCT conditions, meteorological data was used to validate our approach for different wind speed and solar irradiance. The electrical performance of the PV panel was also studied. The proposed 2D FEM analysis is applied to different region's climates and was also used to consider the role of thermal inertia on the optimization of the PV device efficiency.

  7. A novel study based on adaptive metal tolerance behavior in fungi and SEM-EDX analysis.

    Science.gov (United States)

    Chen, Si Hui; Ng, Si Ling; Cheow, Yuen Lin; Ting, Adeline Su Yien

    2017-07-15

    Four fungal isolates: Simplicillium chinense (iso 9, accession no. KX425621), Penicillium simplicissimum (iso 10, KP713758), Trichoderma asperellum (iso 11, KP792512), and Coriolopsis sp. (1c3, KM403574) were subjected to a series of induced-tolerance training under high metal concentrations to determine if greater tolerance could be achieved from constant exposure to such conditions. Adaptive tolerance assay (Tolerance Index, TI) and Field-Emission Scanning Electron Microscopy with Energy Dispersive X-ray (SEM-EDX) characterized their metal tolerance. "Untrained" S. chinense, P. simplicissimum and T. asperellum showed tolerance towards 4000-4500ppm Al(III) (TI: 0.64-0.71), 1000ppm Cr(III) (0.52-0.83) and Pb(II) (0.32-0.88). With tolerance training, tolerance towards 2000-6000ppm Al(III), 500-3000ppm Pb(II) and 2000-3000ppm Cr(III) were achieved (TI: 0.01-0.82) compared to untrained cultures (0.00-0.59). In contrast, tolerance training for Coriolopsis sp. and P. simplicissimum was less successful, with TI values similar or lower than untrained cultures. SEM-EDX analysis proposed biosorption and bioaccumulation as mechanisms for metal removal. The latter was demonstrated with the removal of Cr(III) and Pb(II) by S. chinense (12.37 and 11.52mgg -1 , respectively) and T. asperellum (10.44 and 7.50mgg -1 ). Induced-tolerance training may render benefit in the long run, but this delicate approach is suggestively species and metal dependent. Copyright © 2017 Elsevier B.V. All rights reserved.

  8. SEM analysis of defects and wear on Ni-Ti rotary instruments.

    Science.gov (United States)

    Arantes, Werington Borges; da Silva, Celso Monteiro; Lage-Marques, José Luiz; Habitante, Sandramarcia; da Rosa, Luiz Carlos Laureano; de Medeiros, João Marcelo Ferreira

    2014-01-01

    SEM analysis of endodontic instruments from a Ni-Ti rotary system was assessed, before and after using them, considering their defects and deformations. Twenty Twisted File®, BioRąCe®, Mtwo®, and EndoWave® instruments were micrographed at 190× magnification. The files were washed and micrographed again to view alterations as to the presence or absence of irregular edges, grooves, microcavities, and scraping. Simulated root canal preparations were performed using these instruments. The instruments were cleaned and received a microscopic analysis after being used five times. After analysis tests were tested using Fisher's exact test and Kappa to evaluate the concordance among examiners. There was a statistically significant difference with respect to deformations between Twisted File® and other instruments (p  0.05). All Twisted File® instruments showed the same defects; however damage were lower than those found in BioRace® and Mtwo®. The Endowave® did not show the same defects. In accordance with the data we conclude that the presence of defects was higher in Twisted File® instruments as the instruments and BioRace® Mtwo® brand, the defect rate was smaller and Endowave® instruments had no defects. Regarding the presence of wear after five uses among the groups all instruments showed changes in their cutting blades. © 2014 Wiley Periodicals, Inc.

  9. Automated transmission-mode scanning electron microscopy (tSEM for large volume analysis at nanoscale resolution.

    Directory of Open Access Journals (Sweden)

    Masaaki Kuwajima

    Full Text Available Transmission-mode scanning electron microscopy (tSEM on a field emission SEM platform was developed for efficient and cost-effective imaging of circuit-scale volumes from brain at nanoscale resolution. Image area was maximized while optimizing the resolution and dynamic range necessary for discriminating key subcellular structures, such as small axonal, dendritic and glial processes, synapses, smooth endoplasmic reticulum, vesicles, microtubules, polyribosomes, and endosomes which are critical for neuronal function. Individual image fields from the tSEM system were up to 4,295 µm(2 (65.54 µm per side at 2 nm pixel size, contrasting with image fields from a modern transmission electron microscope (TEM system, which were only 66.59 µm(2 (8.160 µm per side at the same pixel size. The tSEM produced outstanding images and had reduced distortion and drift relative to TEM. Automated stage and scan control in tSEM easily provided unattended serial section imaging and montaging. Lens and scan properties on both TEM and SEM platforms revealed no significant nonlinear distortions within a central field of ∼100 µm(2 and produced near-perfect image registration across serial sections using the computational elastic alignment tool in Fiji/TrakEM2 software, and reliable geometric measurements from RECONSTRUCT™ or Fiji/TrakEM2 software. Axial resolution limits the analysis of small structures contained within a section (∼45 nm. Since this new tSEM is non-destructive, objects within a section can be explored at finer axial resolution in TEM tomography with current methods. Future development of tSEM tomography promises thinner axial resolution producing nearly isotropic voxels and should provide within-section analyses of structures without changing platforms. Brain was the test system given our interest in synaptic connectivity and plasticity; however, the new tSEM system is readily applicable to other biological systems.

  10. Characterization of ash pond ashes from 3rd thermal power plant by SEM/EDX and XRD methods

    OpenAIRE

    A Minjigmaa; Ts Zolzaya; E Bayanjargal; B Davaabal; J Temuujin

    2014-01-01

      Coal combustion by products from ash pond of 3rdthermal power plant of Ulaanbaatar city have been collected in 2010 and 2013 years. The ash samples have been characterized by XRD, XRF and SEM-EDX methods in order to evaluate their chemical and mineralogical composition changes with disposed times. The mineralogical composition of ash varies with time though the chemical composition of the ashes were close each other. Possibly, inefficient operating condition of the TPS shows influence on th...

  11. SEM analysis of particle size during conventional treatment of CMP process wastewater

    International Nuclear Information System (INIS)

    Roth, Gary A.; Neu-Baker, Nicole M.; Brenner, Sara A.

    2015-01-01

    Engineered nanomaterials (ENMs) are currently employed by many industries and have different physical and chemical properties from their bulk counterparts that may confer different toxicity. Nanoparticles used or generated in semiconductor manufacturing have the potential to enter the municipal waste stream via wastewater and their ultimate fate in the ecosystem is currently unknown. This study investigates the fate of ENMs used in chemical mechanical planarization (CMP), a polishing process repeatedly utilized in semiconductor manufacturing. Wastewater sampling was conducted throughout the wastewater treatment (WWT) process at the fabrication plant's on-site wastewater treatment facility. The goal of this study was to assess whether the WWT processes resulted in size-dependent filtration of particles in the nanoscale regime by analyzing samples using scanning electron microscopy (SEM). Statistical analysis demonstrated no significant differences in particle size between sampling points, indicating low or no selectivity of WWT methods for nanoparticles based on size. All nanoparticles appeared to be of similar morphology (near-spherical), with a high variability in particle size. EDX verified nanoparticles composition of silicon- and/or aluminum-oxide. Nanoparticle sizing data compared between sampling points, including the final sampling point before discharge from the facility, suggested that nanoparticles could be released to the municipal waste stream from industrial sources. - Highlights: • The discrete treatments of a semiconductor wastewater treatment system were examined. • A sampling scheme and method for analyzing nanoparticles in wastewater was devised. • The wastewater treatment process studied is not size-selective for nanoparticles

  12. COMMIT at SemEval-2017 Task 5: Ontology-based Method for Sentiment Analysis of Financial Headlines

    NARCIS (Netherlands)

    Schouten, Kim; Frasincar, Flavius; de Jong, F.M.G.

    2017-01-01

    This paper describes our submission to Task 5 of SemEval 2017, Fine-Grained Sentiment Analysis on Financial Microblogs and News, where we limit ourselves to performing sentiment analysis on news headlines only (track 2). The approach presented in this paper uses a Support Vector Machine to do the

  13. Soft tissue digestion of Paradiplozoon vaalense for SEM of sclerites and simultaneous molecular analysis.

    Science.gov (United States)

    Dos Santos, Q M; Avenant-Oldewage, A

    2015-02-01

    Classification of most monogeneans is primarily based on size, shape, and arrangement of haptoral sclerites. These structures are often obscured or misinterpreted when studied using light microscopy, leading to confusion regarding defining characters. Scanning electron microscopy (SEM) has predominantly been used to study haptoral sclerites in smaller monogeneans, focusing on hooks and anchors. In the Diplozoidae, SEM has not been used to study haptoral sclerites. Using new and modified techniques, the sclerites of diplozoids collected in South Africa were successfully studied using SEM. The digestion buffer from a DNA extraction kit was used to digest the surrounding tissue, and Poly-L-lysine-coated and concavity slides were employed to limit the movement and loss of sclerites, with the latter being more user-friendly. In addition to the success of visualizing the sclerites using SEM, the digested tissue from as little as half of the haptor provided viable genetic material for molecular characterization. From the results presented here, the study of the sclerites of larger monogeneans using SEM, including those bearing clamps, is a viable possibility for future research. Also, this method may be beneficial for the study of other, non-haptoral sclerites, such as cirri in other families of monogeneans. During this study, Labeo capensis was noted as a valid host of Paradiplozoon vaalense in a region of the Vaal River where the type host, Labeo umbratus, appears to be absent.

  14. SEM method for direct visual tracking of nanoscale morphological changes of platinum based electrocatalysts on fixed locations upon electrochemical or thermal treatments.

    Science.gov (United States)

    Zorko, Milena; Jozinović, Barbara; Bele, Marjan; Hodnik, Nejc; Gaberšček, Miran

    2014-05-01

    A general method for tracking morphological surface changes on a nanometer scale with scanning electron microscopy (SEM) is introduced. We exemplify the usefulness of the method by showing consecutive SEM images of an identical location before and after the electrochemical and thermal treatments of platinum-based nanoparticles deposited on a high surface area carbon. Observations reveal an insight into platinum based catalyst degradation occurring during potential cycling treatment. The presence of chloride clearly increases the rate of degradation. At these conditions the dominant degradation mechanism seems to be the platinum dissolution with some subsequent redeposition on the top of the catalyst film. By contrast, at the temperature of 60°C, under potentiostatic conditions some carbon corrosion and particle aggregation was observed. Temperature treatment simulating the annealing step of the synthesis reveals sintering of small platinum based composite aggregates into uniform spherical particles. The method provides a direct proof of induced surface phenomena occurring on a chosen location without the usual statistical uncertainty in usual, random SEM observations across relatively large surface areas. Copyright © 2014 Elsevier B.V. All rights reserved.

  15. Characterization of ash pond ashes from 3rd thermal power plant by SEM/EDX and XRD methods

    Directory of Open Access Journals (Sweden)

    A Minjigmaa

    2014-10-01

    Full Text Available   Coal combustion by products from ash pond of 3rdthermal power plant of Ulaanbaatar city have been collected in 2010 and 2013 years. The ash samples have been characterized by XRD, XRF and SEM-EDX methods in order to evaluate their chemical and mineralogical composition changes with disposed times. The mineralogical composition of ash varies with time though the chemical composition of the ashes were close each other. Possibly, inefficient operating condition of the TPS shows influence on the mineralogical composition.DOI: http://dx.doi.org/10.5564/mjc.v14i0.201Mongolian Journal of Chemistry 14 (40, 2013, p61-65

  16. Sem and phylogenetic analysis of naturalized and cultivated Epidendrum in Hawaii

    International Nuclear Information System (INIS)

    White, Ingelia P.; Porter, Brad W.; Chinen, Kimberley; Fay, Michael F.

    2013-01-01

    Naturalized populations of Epidendrum L. are found on a rocky hillside in Nuuanu-Pali and Olomana in the Koolau Mountains of Oahu, Hawaii. Scanning electron micrographs were taken to observe polymorphism among the pollinia, petals, leaves, and root tips of two Epidendrum specimens (one naturalized specimen from Nuuanu-Pali and one cultivated specimen in the greenhouse). SEM images of pollen from the naturalized Epidendrum have revealed a length of 830.31 μm and a width of 462.58 μm. Pollen length from the cultivated cultivar, by comparison, has been 724.60 μm and the width 276.17 μm. Differing cell structures on the lower surface of the petals were also observed. Polyhedral concave cells with numerous fossae (pits) were seen on the naturalized cultivar and elongated flattened cells on the cultivated one. Transections of the leaf of the naturalized specimen have been much thinner (546.33 μm) compared to the thickness of the cultivated cultivar leaf (1505.83 μm), which has contained more spongy parenchyma cells. A thinner root tip (1094.19 μm) was seen in the naturalized cultivar, as opposed to 1636.34 μm in the cultivated specimen. Relationships were compared between these two specimens along with ten other unknown Epidendrum cultivars, the plastid trnL-F gene region and conducted parsimony analysis were sequenced among the naturalized Epidendrum from Nuuanu-Pali At least six changes have separated these specimens into two clades. Shorter and longer plastid simple sequence has repeated (cpSSR) from the rps16-trnK region support separation of the five Epidendrum genotypes evaluated into these two groups, including a naturalized Epidendrum from Olomana. (author)

  17. SEM examination and analysis of the interface character in surface modified aramid-epoxy composite

    International Nuclear Information System (INIS)

    Hussain, S.; Khan, M.B.; Hussain, R.

    2011-01-01

    The surface of Kevlar fibers is chemically modified by treatment with Phthalic anhydride (PA) and the effect is examined by SEM for the laser cut, three point bending and interlaminar shear delaminated surfaces. The surface modification improved the adhesion to epoxy resin that clearly leads to cohesive fracture as opposed to interfacial failure in the untreated specimen. SEM reveals marginal surface roughening of fibers without compromising their strength. The interface modification technique described in this paper is attractive thermodynamically as it does not compromise surface free energy of the polymer matrix or that of the fiber itself to enhance wet ability. (author)

  18. SEM analysis of ionizing radiation effects in linear integrated circuits. [Scanning Electron Microscope

    Science.gov (United States)

    Stanley, A. G.; Gauthier, M. K.

    1977-01-01

    A successful diagnostic technique was developed using a scanning electron microscope (SEM) as a precision tool to determine ionization effects in integrated circuits. Previous SEM methods radiated the entire semiconductor chip or major areas. The large area exposure methods do not reveal the exact components which are sensitive to radiation. To locate these sensitive components a new method was developed, which consisted in successively irradiating selected components on the device chip with equal doses of electrons /10 to the 6th rad (Si)/, while the whole device was subjected to representative bias conditions. A suitable device parameter was measured in situ after each successive irradiation with the beam off.

  19. Marginal adaptation of a low-shrinkage silorane-based composite: A SEM-analysis

    DEFF Research Database (Denmark)

    Schmidt, Malene; Bindslev, Preben Hørsted; Poulsen, Sven

    2012-01-01

    shrinkage, has been marketed. Objective. To investigate whether reduced polymerization shrinkage improves the marginal adaptation of composite restorations. Material and methods. A total of 156 scanning electron microscopy (SEM) pictures (78 baseline, 78 follow-up) of the occlusal part of Class II......-casts of the restorations were used for SEM pictures at x 16 magnification. Pictures from baseline and follow-up (398 days, SD 29 days) were randomized and the examiner was blinded to the material and the age of the restoration. Stereologic measurements were used to calculate the length and the width of the marginal...

  20. Separating topographical and chemical analysis of nanostructure of polymer composite in low voltage SEM

    International Nuclear Information System (INIS)

    Wan, Q; Plenderleith, R A; Claeyssens, F; Rodenburg, C; Dapor, M; Rimmer, S

    2015-01-01

    The possibility of separating the topographical and chemical information in a polymer nano-composite using low-voltage SEM imaging is demonstrated, when images are acquired with a Concentric Backscattered (CBS) detector. This separation of chemical and topographical information is based on the different angular distribution of electron scattering which were calculated using a Monte Carlo simulation. The simulation based on angular restricted detection was applied to a semi-branched PNIPAM/PEGDA interpenetration network for which a linear relationship of topography SEM contrast and feature height data was observed. (paper)

  1. Latent vs. Observed Variables : Analysis of Irrigation Water Efficiency Using SEM and SUR

    NARCIS (Netherlands)

    Tang, Jianjun; Folmer, Henk

    In this paper we compare conceptualising single factor technical and allocative efficiency as indicators of a single latent variable, or as separate observed variables. In the former case, the impacts on both efficiency types are analysed by means of structural equationmodeling (SEM), in the latter

  2. Fractal analysis of SEM images and mercury intrusion porosimetry data for the microstructural characterization of microcrystalline cellulose-based pellets

    International Nuclear Information System (INIS)

    Gomez-Carracedo, A.; Alvarez-Lorenzo, C.; Coca, R.; Martinez-Pacheco, R.; Concheiro, A.; Gomez-Amoza, J.L.

    2009-01-01

    The microstructure of theophylline pellets prepared from microcrystalline cellulose, carbopol and dicalcium phosphate dihydrate, according to a mixture design, was characterized using textural analysis of gray-level scanning electron microscopy (SEM) images and thermodynamic analysis of the cumulative pore volume distribution obtained by mercury intrusion porosimetry. Surface roughness evaluated in terms of gray-level non-uniformity and fractal dimension of pellet surface depended on agglomeration phenomena during extrusion/spheronization. Pores at the surface, mainly 1-15 μm in diameter, determined both the mechanism and the rate of theophylline release, and a strong negative correlation between the fractal geometry and the b parameter of the Weibull function was found for pellets containing >60% carbopol. Theophylline mean dissolution time from these pellets was about two to four times greater. Textural analysis of SEM micrographs and fractal analysis of mercury intrusion data are complementary techniques that enable complete characterization of multiparticulate drug dosage forms

  3. XRD and SEM analysis of hydroxyapatite during immersion in stimulated physiological solutions

    International Nuclear Information System (INIS)

    Yusof Abdullah; Idris Besar; Rosmamuhamadani Ramli; Abd Razak Daud

    2000-01-01

    XRD and SEM techniques were used to analyse the apatite layer developed on the synthetic hydroxyapatite surface following immersion in the simulated body fluid (SBF) that mimics the conditions of material experiences after implantation in the human body. Initially, the new layers formed after 7 day's incubation and increased with immersion time as crystallization of apatite phase. The XRD confirmed that the deposited layer was hydroxyapatite and crystallographically. With time, the crystal growth become more random and the intensity of the peaks decreased. During immersion, hydroxyapatite was precipitated from the SBF and coherently scattered with very small crystal. The SEM observation shows that the new precipitates were increased as well as incubation period increased. Therefore, hydroxyapatite ceramics are suggested to have very good biocompatibility. (Author)

  4. SEM-analysis of grain boundary porosity in three S-176 specimens

    International Nuclear Information System (INIS)

    Malen, K.; Birath, S.; Mattsson, O.

    1980-10-01

    Porosity in UO 2 -fuel has been studied in scanning electron microscope (SEM). The aim was to obtain a basis for evaluation of porosity in high burnup power reactor fuel. Three specimens have been analyzed. In the high temperature zones porosity can be seen both on grain boundaries and at grain edges. In the low temperature regions very little changes seem to have occurred during irradiation. (author)

  5. 3-D Analysis of Graphite Nodules in Ductile Cast Iron Using FIB-SEM

    DEFF Research Database (Denmark)

    D'Angelo, Luca; Jespersen, Freja N.; MacDonald, A. Nicole

    Ductile cast iron samples were analysed in a Focused Ion Beam Scanning Electron Microscope, FIB-SEM. The focussed ion beam was used to carefully remove layers of the graphite nodules to reveal internal structures in the nodules. The sample preparation and milling procedure for sectioning graphite...... inside the nodules, their orientation in relation to the graphite and the chemistry of the inclusions is analysed and described. Formation of the structures during solidification and subsequent cooling to room temperature is discussed....

  6. Thermal damage study on diamond tools at varying laser heating time and temperature by Raman spectroscopy and SEM

    CSIR Research Space (South Africa)

    Masina, BN

    2011-07-01

    Full Text Available 1400 G O B I c a m e r a t e m p e r a t u r e ( K e l v i n ) Blackbody object temperature (Kelvin) y = 0.96 x Slide 10 Physical changes on the diamond tool samples due to the laser heating Initial 5 min – 895 K 15 min – 968 K 25 min – 979 K... stream_source_info Masina_2011_ABSTRACT ONLY.pdf.txt stream_content_type text/plain stream_size 3683 Content-Encoding UTF-8 stream_name Masina_2011_ABSTRACT ONLY.pdf.txt Content-Type text/plain; charset=UTF-8 Thermal...

  7. Advanced SEM imaging

    International Nuclear Information System (INIS)

    Joy, D. C.; Newbury, D. E.

    1998-01-01

    The scanning electron microscope (SEM) represents the most promising tool for metrology, defect review, and for the analysis of ULSI structures, but both fundamental problems such as electron-solid interactions, and practical considerations such as electron-optical constraints, are now setting a limit to performance. This paper examines the directions in which an advanced SEM might be developed to overcome these constraints. The SEM also offers considerable promise as a tool for the high spatial resolution X-ray microanalysis, especially for those situations where a thin cross-section is not practical and first surface analysis is required. The ways in which this capability can be incorporated in an advanced SEM are examined

  8. Advanced SEM imaging

    International Nuclear Information System (INIS)

    Joy, D.C.; Newbury, D.E.; Newbury, D.E.

    1998-01-01

    The scanning electron microscope (SEM) represents the most promising tool for metrology, defect review, and for the analysis of ULSI structures, but both fundamental problems such as electron-solid interactions, and practical considerations such as electron-optical constraints, are now setting a limit to performance. This paper examines the directions in which an advanced SEM might be developed to overcome these constraints. The SEM also offers considerable promise as a tool for the high spatial resolution X-ray microanalysis, especially for those situations where a thin cross-section is not practical and first surface analysis is required. The ways in which this capability can be incorporated in an advanced SEM are examined. copyright 1998 American Institute of Physics

  9. Equipment for dekryptonation thermal analysis

    International Nuclear Information System (INIS)

    Lukac, P.; Pruzinec, J.

    Emanation thermal analysis is used for studying changes in the dynamic temperature conditions during kinetics studies of some reactions in solids. A kryptonated sample is placed in a furnace with a programmable temperature controller. 85 Kr released from the sample is entrapped by the carrier gas in a through-flow Geiger-Mueller detector. The detector signal is processed into an integral form and recorded. Examples are given of the study of modification transformations in NH 4 NO 3 , pearlite and PVC. (M.D.)

  10. THERMAL CONDUCTIVITY ANALYSIS OF GASES

    Science.gov (United States)

    Clark, W.J.

    1949-06-01

    This patent describes apparatus for the quantitative analysis of a gaseous mixture at subatmospheric pressure by measurement of its thermal conductivity. A heated wire forms one leg of a bridge circuit, while the gas under test is passed about the wire at a constant rate. The bridge unbalance will be a measure of the change in composition of the gas, if compensation is made for the effect due to gas pressure change. The apparatus provides a voltage varying with fluctuations of pressure in series with the indicating device placed across the bridge, to counterbalance the voltage change caused by fluctuations in the pressure of the gaseous mixture.

  11. In situ SEM and ToF-SIMS analysis of IgG conjugated gold nanoparticles at aqueous surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Yang, Li; Zhu, Zihua; Yu, Xiao-Ying; Rodek, Gene; Saraf, Laxmikant V.; Thevuthasan, Suntharampillai; Cowin, James P.

    2014-04-01

    In this study, we report new results of in situ study of 5 nm goat anti-mouse IgG gold nanoparticles in a novel portable vacuum compatible microfluidic device using scanning electron microscope (SEM) and time-of-flight secondary ion mass spectrometry (ToF-SIMS). The unique feature of the liquid flow cell is that the detection window is open to the vacuum allowing direct probing of the liquid surface. The flow cell is composed of a silicon nitride (SiN) membrane and polydimethylsiloxane (PDMS), and it is fully compatible with vacuum operations for surface analysis. The aperture can be drilled through the 100 nm SiN membrane using a focused ion beam. Characteristic signals of the conjugated gold nanoparticles were successfully observed through the aperture by both energy-dispersive X-ray spectroscopy (EDX) in SEM and ToF-SIMS. Comparison was also made among wet samples, dry samples, and liquid sample in the flow cell using SEM/EDX. Stronger gold signal can be observed in our novel portable device by SEM/EDX compared with the wet or dry samples, respectively. Our results indicate that analyses of the nanoparticle components are better made in their native liquid environment. This is made possible using our unique microfluidic flow cell.

  12. SEM-EDX analysis of an unknown "known" white powder found in a shipping container from Peru

    Science.gov (United States)

    Albright, Douglas C.

    2009-05-01

    In 2008, an unknown white powder was discovered spilled inside of a shipping container of whole kernel corn during an inspection by federal inspectors in the port of Baltimore, Maryland. The container was detained and quarantined while a sample of the powder was collected and sent to a federal laboratory where it was screened using chromatography for the presence of specific poisons and pesticides with negative results. Samples of the corn kernels and the white powder were forwarded to the Food and Drug Administration, Forensic Chemistry Center for further analysis. Stereoscopic Light Microscopy (SLM), Scanning Electron Microscopy/Energy Dispersive X-ray Spectrometry (SEM/EDX), and Polarized Light Microscopy/Infrared Spectroscopy (PLM-IR) were used in the analysis of the kernels and the unknown powder. Based on the unique particle analysis by SLM and SEM as well as the detection of the presence of aluminum and phosphorous by EDX, the unknown was determined to be consistent with reacted aluminum phosphide (AlP). While commonly known in the agricultural industry, aluminum phosphide is relatively unknown in the forensic community. A history of the use and acute toxicity of this compound along with some very unique SEM/EDX analysis characteristics of aluminum phosphide will be discussed.

  13. Thermal Power Plant Performance Analysis

    CERN Document Server

    2012-01-01

    The analysis of the reliability and availability of power plants is frequently based on simple indexes that do not take into account the criticality of some failures used for availability analysis. This criticality should be evaluated based on concepts of reliability which consider the effect of a component failure on the performance of the entire plant. System reliability analysis tools provide a root-cause analysis leading to the improvement of the plant maintenance plan.   Taking in view that the power plant performance can be evaluated not only based on  thermodynamic related indexes, such as heat-rate, Thermal Power Plant Performance Analysis focuses on the presentation of reliability-based tools used to define performance of complex systems and introduces the basic concepts of reliability, maintainability and risk analysis aiming at their application as tools for power plant performance improvement, including: ·         selection of critical equipment and components, ·         defini...

  14. Morphological, chemical and structural characterisation of deciduous enamel: SEM, EDS, XRD, FTIR and XPS analysis.

    Science.gov (United States)

    Zamudio-Ortega, C M; Contreras-Bulnes, R; Scougall-Vilchis, R J; Morales-Luckie, R A; Olea-Mejía, O F; Rodríguez-Vilchis, L E

    2014-09-01

    The purpose of this study was to characterise the enamel surface of sound deciduous teeth in terms of morphology, chemical composition, structure and crystalline phases. The enamel of 30 human deciduous teeth was examined by: Scanning Electron Microscopy (SEM), Energy Dispersive X-Ray Spectroscopy (EDS), X-ray Powder Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), and X-ray Photoelectron Spectroscopy (XPS). Chemical differences between incisors and canines were statistically evaluated using the Mann-Whitney U test (p ≤ 0.05). Three enamel patterns were observed by SEM: 'mostly smooth with some groves', 'abundant microporosities' and 'exposed prisms'. The average Ca/P molar ratios were 1.37 and 1.03 by EDS and XPS, respectively. The crystallite size determined by XRD was 210.82 ± 16.78 Å. The mean ratio between Ca bonded to phosphate and Ca bonded to hydroxyl was approximately 10:1. The enamel of sound deciduous teeth showed two main patterns: 'mostly smooth with some groves' and 'abundant microporosities'. 'Exposed prisms' was a secondary pattern. There were slight variations among the Ca/P molar ratios found by EDS and XPS, suggesting differences in the mineral content from the enamel surface to the interior. The crystalline phases found in enamel were hydroxyapatite and carbonate apatite, with major type B than type A carbonate incorporation.

  15. HRB-22 preirradiation thermal analysis

    International Nuclear Information System (INIS)

    Acharya, R.; Sawa, K.

    1995-05-01

    This report describes the preirradiation thermal analysis of the HRB-22 capsule designed for irradiation in the removable beryllium (RB) position of the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory (ORNL). CACA-2 a heavy isotope and fission product concentration calculational code for experimental irradiation capsules was used to determine time dependent fission power for the fuel compacts. The Heat Engineering and Transfer in Nine Geometries (HEATING) computer code, version 7.2, was used to solve the steady-state heat conduction problem. The diameters of the graphite fuel body that contains the compacts and the primary pressure vessel were selected such that the requirements of running the compacts at an average temperature of < 1,250 C and not exceeding a maximum fuel temperature of 1,350 C was met throughout the four cycles of irradiation

  16. HANARO thermal hydraulic accident analysis

    Energy Technology Data Exchange (ETDEWEB)

    Park, Chul; Kim, Heon Il; Lee, Bo Yook; Lee, Sang Yong [Korea Atomic Energy Research Institute, Taejon (Korea, Republic of)

    1996-06-01

    For the safety assessment of HANARO, accident analyses for the anticipated operational transients, accident scenarios and limiting accident scenarios were conducted. To do this, the commercial nuclear reactor system code. RELAP5/MOD2 was modified to RELAP5/KMRR; the thermal hydraulic correlations and the heat exchanger model was changed to incorporate HANARO characteristics. This report summarizes the RELAP/KMRR calculation results and the subchannel analyses results based on the RELAP/KMRR results. During the calculation, major concern was placed on the integrity of the fuel. For all the scenarios, the important accident analysis parameters, i.e., fuel centerline temperatures and the minimum critical heat flux ratio(MCHFR), satisfied safe design limits. It was verified, therefore, that the HANARO was safely designed. 21 tabs., 89 figs., 39 refs. (Author) .new.

  17. Three-dimensional analysis of somatic mitochondrial dynamics in fission-deficient injured motor neurons using FIB/SEM.

    Science.gov (United States)

    Tamada, Hiromi; Kiryu-Seo, Sumiko; Hosokawa, Hiroki; Ohta, Keisuke; Ishihara, Naotada; Nomura, Masatoshi; Mihara, Katsuyoshi; Nakamura, Kei-Ichiro; Kiyama, Hiroshi

    2017-08-01

    Mitochondria undergo morphological changes through fusion and fission for their quality control, which are vital for neuronal function. In this study, we examined three-dimensional morphologies of mitochondria in motor neurons under normal, nerve injured, and nerve injured plus fission-impaired conditions using the focused ion beam/scanning electron microscopy (FIB/SEM), because the FIB/SEM technology is a powerful tool to demonstrate both 3D images of whole organelle and the intra-organellar structure simultaneously. Crossing of dynamin-related protein 1 (Drp1) gene-floxed mice with neuronal injury-specific Cre driver mice, Atf3:BAC Tg mice, allowed for Drp1 ablation specifically in injured neurons. FIB/SEM analysis demonstrated that somatic mitochondrial morphologies in motor neurons were not altered before or after nerve injury. However, the fission impairment resulted in prominent somatic mitochondrial enlargement, which initially induced complex morphologies with round regions and long tubular processes, subsequently causing a decrease in the number of processes and further enlargement of the round regions, which eventually resulted in big spheroidal mitochondria without processes. The abnormal mitochondria exhibited several degradative morphologies: local or total cristae collapse, vacuolization, and mitophagy. These suggest that mitochondrial fission is crucial for maintaining mitochondrial integrity in injured motor neurons, and multiple forms of mitochondria degradation may accelerate neuronal degradation. © 2017 Wiley Periodicals, Inc.

  18. A study of equilibrium and FTIR, SEM/EDS analysis of trimethoprim adsorption onto K10

    Science.gov (United States)

    Bekçi, Zehra; Seki, Yoldaş; Kadir Yurdakoç, M.

    2007-02-01

    The sorption behavior of K10, a type of montmorillonite for trimethoprim (TMP) drug, was studied by using batch technique under different pH and temperature. The interaction between K10 and TMP was investigated using SEM, and FTIR. It was observed that adsorption was increased between pH 2.5 and 6.3. By performing kinetic experiments, the pseudo-second-order kinetic model provides the best fit for TMP adsorption onto K10 montmorillonite. The sorption of TMP reached the equilibrium state after 6 h sorption time and has been described by using Langmuir, Freundlich and Dubinin-Radushkevich equations to obtain adsorption capacity values. The results indicate that the relative adsorption capacity values ( Kf) are decreasing with the increase of temperature in the range of 298-318 K. The sorption energy values obtained from DR isotherm show that sorption of TMP onto K10 can be explained by ion exchange mechanism at 298, 308 and 318 K. The thermodynamic studies were conducted to find the thermodynamic parameters Δ H°, Δ S° and Δ G°. It was determined that adsorption process is spontaneous and exothermic in nature.

  19. SEM Analysis of MTAD Efficacy for Smear Layer Removal from Periodontally Affected Root Surfaces

    Directory of Open Access Journals (Sweden)

    R. K. Tabor

    2011-12-01

    Full Text Available Objective: Biopure® MTAD (Dentsply Tulsa Dental, USA has been developed as a final irrigant following root canal shaping to remove intracanal smear layer. Many of the unique properties of MTAD potentially transfer to the conditioning process of tooth roots during periodontal therapy. The aim of this ex vivo studywas to evaluate the effect of MTAD on the removal of smear layer from root surfaces.Materials and Methods: Thirty two longitudinally sectioned specimens from 16 freshly extracted teeth diagnosed with advanced periodontal disease were divided into four groups. In group 1 and 2, the root surfaces were scaled using Gracey curettes. In group 3 and 4, 0.5 mm of the root surface was removed using a fissure bur. The specimens in group 1 and 3 were then irrigated by normal saline. Thespecimens in groups 2 and 4 were irrigated with Biopure MTAD.All specimens were prepared for SEM and scored according to the presence of smear layer.Results: MTAD significantly increased (P=0.001 the smear layer removal in both groups 2 and 4 compared to the associated control groups, in which only saline was used.Conclusion: MTAD increased the removal of the smear layer from periodontally affected root surfaces. Use of MTAD as a periodontal conditioner may be suggested.

  20. Transient thermal analysis of Vega launcher structures

    Energy Technology Data Exchange (ETDEWEB)

    Gori, F. [University of Rome ' Tor Vergata' , Rome (Italy); De Stefanis, M. [Thales Alenia Space Italia, Rome (Italy); Worek, W.M. [University of Illinois at Chicago, Chicago (United States)], E-mail: wworek@uic.edu; Minkowycz, W.J. [University of Illinois at Chicago, Chicago (United States)

    2008-12-15

    A transient thermal analysis is carried out to verify the base cover thermal protection system of Vega 2nd stage Solid Rocket Motor (SRM) and the flange coupling of the inter-stage 2/3. The analysis is performed with a finite element code. The work has developed suitable numerical Fortran subroutines to assign radiation and convection boundary conditions. The thermal behaviour of the structures is presented.

  1. Relation of expansion due to alkali silica reaction to the degree of reaction measured by SEM image analysis

    International Nuclear Information System (INIS)

    Haha, M. Ben; Gallucci, E.; Guidoum, A.; Scrivener, K.L.

    2007-01-01

    Scanning Electron Microscopy Image Analysis (SEM-IA) was used to quantify the degree of alkali silica reaction in affected microbars, mortar and concrete prisms. It was found that the degree of reaction gave a unique correlation with the macroscopic expansion for three different aggregates, stored at three temperatures and with two levels of alkali. The relationships found for the concretes and the mortars overlap when normalised by the aggregate content. This relationship seems to be linear up to a critical reaction degree which coincides with crack initiation within the reactive aggregates

  2. Spin-polarized SEM

    International Nuclear Information System (INIS)

    Konoto, Makoto

    2007-01-01

    Development of highly effective evaluation technology of magnetic structures on a nanometric scale is a key to understanding spintronics and related phenomena. A high-resolution spin-polarized scanning electron microscope (spin SEM) developed recently is quite suitable for probing such nanostructures because of the capability of analyzing local magnetization vectors in three dimensions. Utilizing the spin SEM, a layered antiferromagnetic structure with the 1nm-alternation of bilayer-sheet magnetization has been successfully resolved. The real-space imaging with full analysis of the temperature-dependent magnetization vectors will be demonstrated. (author)

  3. Thermal analysis studies of ammonium uranyl carbonate

    International Nuclear Information System (INIS)

    Cao Xinsheng; Ma Xuezhong; Wang Fapin; Liu Naixin; Ji Changhong

    1988-01-01

    The simultaneous thermogravimetry and differential thermal analysis of the ammonium uranyl carbonate powder were performed with heat balance in the following atmosphers: Air, Ar and Ar-8%H 2 . The thermogravimetry and differential thermal analysis curves of the ammonium uranyl carbonate powder obtained from different source were reported and discussed

  4. Use of emanation thermal analysis in the microstructure diagnostics of aluminia coatings

    Czech Academy of Sciences Publication Activity Database

    Balek, V.; Beneš, M.; Šubrt, Jan

    2008-01-01

    Roč. 52, č. 2 (2008), s. 85-89 ISSN 0862-5468 Institutional research plan: CEZ:AV0Z40320502 Keywords : aluminia coatings * emanation thermal analysis * SEM Subject RIV: CA - Inorganic Chemistry Impact factor: 0.644, year: 2008

  5. Temperature Modulated Nanomechanical Thermal Analysis

    DEFF Research Database (Denmark)

    Alves, Gustavo Marcati A.; Bose-Goswami, Sanjukta; Mansano, Ronaldo D.

    2018-01-01

    The response of microcantilever deflection to complex heating profiles was used to study thermal events like glass transition and enthalpy relaxation on nanograms of the biopolymer Poly(lactic-co-glycolic acid) (PLGA). The use of two heating rates enables the separation of effects on the deflection...... response that depends on previous thermal history (non-reversing signal) and effects that depends only on the heating rate variation (reversing signal). As these effects may appear superposed in the total response, temperature modulation can increase the measurement sensitivity to some thermal events when...

  6. Tensile bond strength and SEM analysis of enamel etched with Er:YAG laser and phosphoric acid: a comparative study in vitro

    International Nuclear Information System (INIS)

    Sasaki, Luis H.; Tanaka, Celso Shin-Ite; Lobo, Paulo D.C.; Villaverde, Antonio B.; Moriyama, Eduardo H.; Brugnera Junior, Aldo; Moriyama, Yumi; Watanabe, Ii-Sei

    2008-01-01

    Er:YAG laser has been studied as a potential tool for restorative dentistry due to its ability to selectively remove oral hard tissue with minimal or no thermal damage to the surrounding tissues. The purpose of this study was to evaluate in vitro the tensile bond strength (TBS) of an adhesive/composite resin system to human enamel surfaces treated with 37% phosphoric acid, Er:YAG laser (λ=2.94 μm) with a total energy of 16 J (80 mJ/pulse, 2Hz, 200 pulses, 250 ms pulse width), and Er:YAG laser followed by phosphoric acid etching. Analysis of the treated surfaces was performed by scanning electron microscopy (SEM) to assess morphological differences among the groups. TBS means (in MPa) were as follows: Er:YAG laser + acid (11.7 MPa) > acid (8.2 MPa) > Er:YAG laser (6.1 MPa), with the group treated with laser+acid being significantly from the other groups (p=0.0006 and p= 0.00019, respectively). The groups treated with acid alone and laser alone were significantly different from each other (p=0.0003). The SEM analysis revealed morphological changes that corroborate the TBS results, suggesting that the differences in TBS means among the groups are related to the different etching patterns produced by each type of surface treatment. The findings of this study indicate that the association between Er:YAG laser and phosphoric acid can be used as a valuable resource to increase bond strength to laser-prepared enamel. (author)

  7. Thermal energy systems design and analysis

    CERN Document Server

    Penoncello, Steven G

    2015-01-01

    IntroductionThermal Energy Systems Design and AnalysisSoftwareThermal Energy System TopicsUnits and Unit SystemsThermophysical PropertiesEngineering DesignEngineering EconomicsIntroductionCommon Engineering Economics NomenclatureEconomic Analysis Tool: The Cash Flow DiagramTime Value of MoneyTime Value of Money ExamplesUsing Software to Calculate Interest FactorsEconomic Decision MakingDepreciation and TaxesProblemsAnalysis of Thermal Energy SystemsIntroductionNomenclatureThermophysical Properties of SubstancesSuggested Thermal Energy Systems Analysis ProcedureConserved and Balanced QuantitiesConservation of MassConservation of Energy (The First Law of Thermodynamics)Entropy Balance (The Second Law of Thermodynamics)Exergy Balance: The Combined LawEnergy and Exergy Analysis of Thermal Energy CyclesDetailed Analysis of Thermal Energy CyclesProblemsFluid Transport in Thermal Energy SystemsIntroductionPiping and Tubing StandardsFluid Flow FundamentalsValves and FittingsDesign and Analysis of Pipe NetworksEconomi...

  8. How Hedstrom files fail during clinical use? A retrieval study based on SEM, optical microscopy and micro-XCT analysis.

    Science.gov (United States)

    Zinelis, Spiros; Al Jabbari, Youssef S

    2018-05-01

    This study was conducted to evaluate the failure mechanism of clinically failed Hedstrom (H)-files. Discarded H-files (n=160) from #8 to #40 ISO sizes were collected from different dental clinics. Retrieved files were classified according to their macroscopic appearance and they were investigated under scanning electron microscopy (SEM) and X-ray micro-computed tomography (mXCT). Then the files were embedded in resin along their longitudinal axis and after metallographic grinding and polishing, studied under an incident light microscope. The macroscopic evaluation showed that small ISO sizes (#08-#15) failed by extensive plastic deformation, while larger sizes (≥#20) tended to fracture. Light microscopy and mXCT results coincided showing that unused and plastically deformed files were free of internal defects, while fractured files demonstrate the presence of intense cracking in the flute region. SEM analysis revealed the presence of striations attributed to the fatigue mechanism. Secondary cracks were also identified by optical microscopy and their distribution was correlated to fatigue under bending loading. Experimental results demonstrated that while overloading of cutting instruments is the predominating failure mechanism of small file sizes (#08-#15), fatigue should be considered the fracture mechanism for larger sizes (≥#20).

  9. Thermal analysis of iron hydroxide microspheres

    International Nuclear Information System (INIS)

    Turcanu, C.N.; Cornescu, M.

    1979-03-01

    The thermal treatment is an important step in the preparative technology of the iron oxids microspheres with well established mechanical, physical and chemical characteristics. The first indications on the heating procedure have been obtained from the thermal analysis on iron hydroxide microspheres prepared by the support precipitation and internal gelification methods. (author)

  10. Microprobe and SEM Analysis of a Meteorite from the Campo del Cielo Fall

    International Nuclear Information System (INIS)

    Cabanillas, E. D.; Palacios, T. A.

    2003-01-01

    Full Text: Meteorites are unique pieces in nature having not only the enigmatic connotations of the unknown but also are the easier obtained samples of the exterior universe. Furthermore they are the unique alloys that suffered modifications done during enormous periods of time in space and in land The Campo del Cielo fall, occurred more than 5000 years ago, gave hundredths of pieces some of them well studied. We have studied one of the minor pieces from the fall and with microprobe and scanning electronic microscopy analysis we determined the composition of Schreibersite and Rhabdite phosphides of iron and nickel. This study was performed to establish relationships between the duration of alloys and the design of disposal of high level and long lived radioactive waste

  11. Cervical and incisal marginal discrepancy in ceramic laminate veneering materials: A SEM analysis

    Directory of Open Access Journals (Sweden)

    Hemalatha Ranganathan

    2017-01-01

    Full Text Available Context: Marginal discrepancy influenced by the choice of processing material used for the ceramic laminate veneers needs to be explored further for better clinical application. Aims: This study aimed to evaluate the amount of cervical and incisal marginal discrepancy associated with different ceramic laminate veneering materials. Settings and Design: This was an experimental, single-blinded, in vitro trial. Subjects and Methods: Ten central incisors were prepared for laminate veneers with 2 mm uniform reduction and heavy chamfer finish line. Ceramic laminate veneers fabricated over the prepared teeth using four different processing materials were categorized into four groups as Group I - aluminous porcelain veneers, Group II - lithium disilicate ceramic veneers, Group III - lithium disilicate-leucite-based veneers, Group IV - zirconia-based ceramic veneers. The cervical and incisal marginal discrepancy was measured using a scanning electron microscope. Statistical Analysis Used: ANOVA and post hoc Tukey honest significant difference (HSD tests were used for statistical analysis. Results: The cervical and incisal marginal discrepancy for four groups was Group I - 114.6 ± 4.3 μm, 132.5 ± 6.5 μm, Group II - 86.1 ± 6.3 μm, 105.4 ± 5.3 μm, Group III - 71.4 ± 4.4 μm, 91.3 ± 4.7 μm, and Group IV - 123.1 ± 4.1 μm, 142.0 ± 5.4 μm. ANOVA and post hoc Tukey HSD tests observed a statistically significant difference between the four test specimens with regard to cervical marginal discrepancy. The cervical and incisal marginal discrepancy scored F = 243.408, P < 0.001 and F = 180.844, P < 0.001, respectively. Conclusion: This study concluded veneers fabricated using leucite reinforced lithium disilicate exhibited the least marginal discrepancy followed by lithium disilicate ceramic, aluminous porcelain, and zirconia-based ceramics. The marginal discrepancy was more in the incisal region than in the cervical region in all the groups.

  12. Insights into the Toba Super-Eruption using SEM Analysis of Ash Deposits

    Science.gov (United States)

    Gatti, E.; Achyuthan, H.; Durant, A. J.; Gibbard, P.; Mokhtar, S.; Oppenheimer, C.; Raj, R.; Shridar, A.

    2010-12-01

    The ~74 ka Youngest Toba Tuff (YTT) super-eruption of Toba volcano, Northern Sumatra, was the largest eruption of the Quaternary (magnitude M= 8.8) and injected massive quantities of volcanic gases and ash into the stratosphere. YTT deposits covered at least 40,000,000 km2 of Southeast Asia and are preserved in river valleys across peninsular India and Malaysia, and in deep-sea tephra layers in the Indian Ocean, Bay of Bengal and South China Sea. Initial studies hypothesized the eruption caused immediate and substantial global cooling during the ~ 1 kyr between Dansgaard-Oeschger events 19 and 20 which devastated ecosystems and hominid populations. A more recent review argues against severe post-YTT climatic deterioration and cannot find clear evidence for considerable impacts on ecosystems or bio-diversity. The determination of the eruptive parameters is crucial in this issue to document the eruption and understand the potential impacts from future super-volcanic eruptions. Volcanic ash deposits can offer dramatic insights into key eruptive parameters, including magnitude, duration and plume height. The composition and shape of volcanic ashes can be used to interpret physical properties of an erupting magma and tephra transport, while textural characteristics such as grain roughness and surface vescicularity can provide insights into degassing history, volatile content and explosive activity of the volcano. We present a stratigraphic and sedimentological analysis of YTT deposits in stratified contexts at three localities in India, at two sites in Peninsular Malaysia, and at several localities around Lake Toba and on Samosir Island, Sumatra. These sites offer excellent constraints on the spatial distribution of YTT deposits which can be used to infer dispersal directions of the cloud, and provide insights into environmental controls on preservation of tephra beds. The research aims at a systematic interpretation of the Toba tephra to understand the volcanic

  13. Stability, rheology and thermal analysis of functionalized alumina- thermal oil-based nanofluids for advanced cooling systems

    International Nuclear Information System (INIS)

    Ilyas, Suhaib Umer; Pendyala, Rajashekhar; Narahari, Marneni; Susin, Lim

    2017-01-01

    Highlights: • Alumina nanoparticles are functionalized with oleic acid. • Functionalization of alumina nanoparticles gives better dispersion in thermal oil. • Thermophysical properties of nanofluids are experimentally measured. • TGA confirms the improvement in life of nanofluids. - Abstract: Thermal oils are widely used as cooling media in heat transfer processes. However, their potential has not been utilised exquisitely in many applications due to low thermal properties. Thermal oil-based nanofluids are prepared by dispersing functionalized alumina with varying concentrations of 0.5–3 wt.% to enhance thermal properties of oil for advanced cooling systems. The oleic acid coated alumina is prepared and then dispersed in the oil to overcome the aggregation of nanoparticles in base fluid. The surface characterizations of functionalized nanoparticles are performed using different analysis such as XRD, EDS, SEM, TEM and FTIR. Dispersion behaviour and agglomeration studies are conducted at natural and functionalized conditions using different analysis to ensure long-term stability of nanofluids. In addition, rheological behaviour of non-Newtonian nanofluids is studied at high shear rates (100–2000 s"−"1). Effective densities and enhancement in thermal conductivities are measured for different nanofluids concentrations. Specific heat capacity is measured using Differential Scanning Calorimetry. The correlations are developed for thermophysical properties of nanofluids. Thermogravimetric analysis is performed with respect to temperature and time to exploit the effect of the addition of nanoparticles on the degradation of nanofluids. Significant improvement in the thermal properties of oil is observed using highly stable functionalized alumina nano-additives.

  14. Quick Spacecraft Thermal Analysis Tool, Phase II

    Data.gov (United States)

    National Aeronautics and Space Administration — For spacecraft design and development teams concerned with cost and schedule, the Quick Spacecraft Thermal Analysis Tool (QuickSTAT) is an innovative software suite...

  15. Quality assurance aspects of GSR analysis by SEM/EDX: a report of first-hand experiences

    Science.gov (United States)

    Charles, Sebastien; Dehan, Didier; Geusens, Nadia; Nys, Bart

    2009-05-01

    Like many forensic science labs, the Belgian National Institute of Forensic Science (NICC) is involved in a Quality Assurance program aiming towards an ISO17025 Accreditation. Since last year, a project is underway in the GSR lab to validate the method used in the analysis of GSR samples acquired from the hands of suspects by SEM/EDX. The project is well underway, and is planned to lead to accreditation for this technique by the start of 2010. The presentation will discuss several aspects of the functioning of the lab that have to be addressed when preparing for this accreditation. Some of these issues and problems are so involved that separate sub-projects were defined in order to provide a manageable solution. The following topics will be treated in detail: definition of the scope of the accreditation, the validation of the SEM/EDX method with respect to : accuracy, precision, reproducibility and robustness, and the documentation of the Chain of Custody (CoC) of the samples and their storage. One specific sub-project that will be discussed is the study of contamination monitoring in different relevant locations of the lab. Finally, as we have recently acquired a new microscope, the technical criteria we used in the acquisition study will be presented with a focus on their relevance in a QA context. We feel this discussion is informative, both for labs that are pursuing a formal accreditation in the future, and those that work already in such a context and are in the process of acquiring new equipment.

  16. Molecular thermal transistor: Dimension analysis and mechanism

    Science.gov (United States)

    Behnia, S.; Panahinia, R.

    2018-04-01

    Recently, large challenge has been spent to realize high efficient thermal transistors. Outstanding properties of DNA make it as an excellent nano material in future technologies. In this paper, we introduced a high efficient DNA based thermal transistor. The thermal transistor operates when the system shows an increase in the thermal flux despite of decreasing temperature gradient. This is what called as negative differential thermal resistance (NDTR). Based on multifractal analysis, we could distinguish regions with NDTR state from non-NDTR state. Moreover, Based on dimension spectrum of the system, it is detected that NDTR state is accompanied by ballistic transport regime. The generalized correlation sum (analogous to specific heat) shows that an irregular decrease in the specific heat induces an increase in the mean free path (mfp) of phonons. This leads to the occurrence of NDTR.

  17. The ITZ in concrete with natural and recycled aggregates : Study of microstructures based on image and SEM analysis

    NARCIS (Netherlands)

    Bonifazi, G.; Capobianco, G.; Serranti, S.; Eggimann, M.; Wagner, E.; Di Maio, F.; Lotfi, S.

    2015-01-01

    Aim of this work was to investigate the microstructure of the Interfacial Transition Zone (ITZ) between cement paste and aggregate in concrete utilizing Scanning Electron Microscope (SEM) in order to identify possible effects on the ITZ related to different recipes and production parameters. SEM is

  18. Thermal Analysis of TRIO-CINEMA Mission

    Directory of Open Access Journals (Sweden)

    Jaegun Yoo

    2012-03-01

    Full Text Available Thermal analysis and control design are prerequisite essential to design the satellite. In the space environment, it makes satellite survive from extreme hot and cold conditions. In recent years CubeSat mission is developed for many kinds of purpose. Triplet Ionospheric Observatory (TRIO–CubeSat for Ion, Neutral, Electron, MAgnetic fields (CINEMA is required to weigh less than 3 kg and operate on minimal 3 W power. In this paper we describe the thermal analysis and control design for TRIO-CINEMA mission. For this thermal analysis, we made a thermal model of the CubeSat with finite element method and NX6.0 TMG software is used to simulate this analysis model. Based on this result, passive thermal control method has been applied to thermal design of CINEMA. In order to get the better conduction between solar panel and chassis, we choose aluminum 6061-T6 for the material property of standoff. We can increase the average temperature of top and bottom solar panels from -70°C to -40°C and decrease the average temperature of the magnetometer from +93°C to -4°C using black paint on the surface of the chassis, inside of top & bottom solar panels, and magnetometer.

  19. SEM/EDS analysis of soil and roasting vessels fragments from ancient mercury ore roasting sites at Idrija area

    Directory of Open Access Journals (Sweden)

    Tamara Teršič

    2011-06-01

    Full Text Available Numerous roasting vessels fragments can be found at ancient roasting site areas in the surroundings of Idrija town, which were used for ore roasting in the first 150 years of Hg production in Idrija. The earthen vessels fragments lay just below the surface humus layer and in some parts they stretch more than 1 meter deep; they arecovered with red (cinnabar or black (metacinnabar coatings.SEM/EDS analysis of roasting vessels fragments and soil samples from roasting site areas P{enk and Frbejžene trate was performed in order to characterize the solid forms of Hg in applied sampling material. Mercuric sulphide HgS was found to be the main mercury compound present in the samples. Analysis of earthen vessels fragmentsshowed abundant HgS coatings on the surface of ceramics, forming either crust-like aggregates on matrix or isolated grains. Some well-shaped grains with indicated structure and the size of up to 200 μm could also be observed. In soil HgS was present as powder-like concentrations scattered in soil samples, frequently coating silicate and quartz crystals and clay-minerals. Polycristalline, mercury- and sulphur- rich particles comprising silica, clay mineralsand Al-, Fe- and Mg-oxides that were also observed in the samples were interpreted as soil aggregates infiltrated by mercuric and sulphur vapours and by liquid mercury spilled during roasting. These particles suggest a possible presence of mercury-sulphur associations other than HgS.

  20. Thermodynamical analysis of human thermal comfort

    International Nuclear Information System (INIS)

    Prek, Matjaz

    2006-01-01

    Traditional methods of human thermal comfort analysis are based on the first law of thermodynamics. These methods use an energy balance of the human body to determine heat transfer between the body and its environment. By contrast, the second law of thermodynamics introduces the useful concept of exergy. It enables the determination of the exergy consumption within the human body dependent on human and environmental factors. Human body exergy consumption varies with the combination of environmental (room) conditions. This process is related to human thermal comfort in connection with temperature, heat, and mass transfer. In this paper a thermodynamic analysis of human heat and mass transfer based on the 2nd law of thermodynamics in presented. It is shown that the human body's exergy consumption in relation to selected human parameters exhibits a minimal value at certain combinations of environmental parameters. The expected thermal sensation also shows that there is a correlation between exergy consumption and thermal sensation. Thus, our analysis represents an improvement in human thermal modelling and gives more information about the environmental impact on expected human thermal sensation

  1. Root cause analysis of thermal sleeve separation

    Energy Technology Data Exchange (ETDEWEB)

    Jo, J. C.; Jhung, M. J.; Yu, S. O.; Kim, H. J.; Yune, Y. K.; Park, J. Y

    2006-01-15

    Thermal sleeves in the shape of thin wall cylinder seated inside the nozzle part of each Safety Injection (SI) line at Pressurized Water Reactors (PWRs) have such functions as prevention and relief of potential excessive transient thermal stress in the wall of SI line nozzle part which is initially heated up with hot water flowing in the primary coolant piping system when cold water is injected into the system through the SI nozzles during the SI operation mode. Recently, mechanical failures that the sleeves were separated from the SI branch pipe and fell into the connected cold leg main pipe occurred in sequence at some typical PWR plants in Korea. To find out the root cause of thermal sleeve breakaway failures, the flow situation in the junction of primary coolant main pipe and SI branch pipe, and the vibration modal characteristics of the thermal sleeve are investigated in detail by using both Computational Fluid Dynamic (CFD) code and structure analysis finite element code. As the results, the transient response in fluid force exerting on the local part of thermal sleeve wall surface to the primary coolant flow through the pipe junction area during the normal reactor operation mode shows oscillatory characteristics with frequencies ranging from 17 to 18, which coincide with one of the lower mode natural frequencies of thermal sleeve having a pinned support condition on the circumferential prominence on the outer surface of thermal sleeve which is put into the circumferential groove on the inner surface of SI nozzle at the mid-height of the thermal sleeve. In addition, the variation of force on the thermal sleeve surface yields alternating torques in the directions of two rectangular axes which are perpendicular to the longitudinal axis of cylindrical thermal sleeve, which cause rolling, pitching and rotating motions of the thermal sleeve. Consequently, it is seen that this flow situation surrounding the thermal sleeve during the normal reactor operation can

  2. Plutonium storage thermal analysis (U)

    International Nuclear Information System (INIS)

    Hensel, S.J.; Lee, S.Y.; Schaade, J.B.

    1997-01-01

    Thermal modeling of plutonium metal ingots stored in food pack cans provides information useful for performing stored material safety evaluations. Four storage can geometries were modeled, and several conclusions can be made from the 14 cases analyzed. The ingot temperature increased from 7 degrees F to 12 degrees F (depending on can configuration) per additional watt of power. Including internal convection lowers computed ingot temperatures by 70 degrees F. Accounting for the heat flow through the bottom of the cans to the storage rack lowered computed ingot temperatures by an additional 70 degrees F to 80 degrees F. In the rimmed can systems storing ingots with a power of 10.35 watts, the ingot temperature varies from 190 degrees F to 213 degrees F. Including a plastic bag between the inner and outer can increases the ingot temperature by 15 degrees F. Adding a label to the outer can side reduces the outer can side temperature by 13 degrees F. Changes in ambient temperature affect the outer can temperatures more than the ingot temperature by a factor of 3. Similarly, a 5 degrees F drop in outer can temperature due to increased convection lowered the ingot temperature by only 2 degrees F

  3. Thermal Analysis of Filler Reinforced Polymeric Composites

    Science.gov (United States)

    Ghadge, Mahesh Devidas

    compared with that predicted by mean field theories. At low volume fractions the FEM and mean field theory results are matching. However, at high volume fractions, the results obtained by the two methods are not in agreement. This is due to the fact that mean field theory do not consider the particle interactions happening at higher volume fractions. The present analysis can be used to tailor the thermal properties of ESBR for required thermal conductivity for a wide range of applications such as racing tires, electronic gadgets or aeronautical components. In addition, the proposed FEM models can be used to design and optimize the properties of new composite materials providing more insight into the thermal conductivity of composite polymers and aid in understanding heat transfer mechanism of reinforced polymers.

  4. Defect window analysis by using SEM-contour based shape quantifying method for sub-20nm node production

    Science.gov (United States)

    Hibino, Daisuke; Hsu, Mingyi; Shindo, Hiroyuki; Izawa, Masayuki; Enomoto, Yuji; Lin, J. F.; Hu, J. R.

    2013-04-01

    The impact on yield loss due to systematic defect which remains after Optical Proximity Correction (OPC) modeling has increased, and achieving an acceptable yield has become more difficult in the leading technology beyond 20 nm node production. Furthermore Process-Window has become narrow because of the complexity of IC design and less process margin. In the past, the systematic defects have been inspected by human-eyes. However the judgment by human-eyes is sometime unstable and not accurate. Moreover an enormous amount of time and labor will have to be expended on the one-by-one judgment for several thousands of hot-spot defects. In order to overcome these difficulties and improve the yield and manufacturability, the automated system, which can quantify the shape difference with high accuracy and speed, is needed. Inspection points could be increased for getting higher yield, if the automated system achieves our goal. Defect Window Analysis (DWA) system by using high-precision-contour extraction from SEM image on real silicon and quantifying method which can calculate the difference between defect pattern and non-defect pattern automatically, which was developed by Hitachi High-Technologies, has been applied to the defect judgment instead of the judgment by human-eyes. The DWA result which describes process behavior might be feedback to design or OPC or mask. This new methodology and evaluation results will be presented in detail in this paper.

  5. A Miniaturized Variable Pressure Scanning Electron Microscope (MVP-SEM) for In-Situ Mars Surface Sample Analysis

    Science.gov (United States)

    Edmunson, J.; Gaskin, J. A.; Jerman, G. A.; Harvey, R. P.; Doloboff, I. J.; Neidholdt, E. L.

    2016-01-01

    The Miniaturized Variable Pressure Scanning Electron Microscope (MVP-SEM) project, funded by the NASA Planetary Instrument Concepts for the Advancement of Solar System Observations (PICASSO) Research Opportunities in Space and Earth Sciences (ROSES), will build upon previous miniaturized SEM designs and recent advancements in variable pressure SEM's to design and build a SEM to complete analyses of samples on the surface of Mars using the atmosphere as an imaging medium. This project is a collaboration between NASA Marshall Space Flight Center (MSFC), the Jet Propulsion Laboratory (JPL), electron gun and optics manufacturer Applied Physics Technologies, and small vacuum system manufacturer Creare. Dr. Ralph Harvery and environmental SEM (ESEM) inventor Dr. Gerry Danilatos serve as advisors to the team. Variable pressure SEMs allow for fine (nm-scale) resolution imaging and micron-scale chemical study of materials without sample preparation (e.g., carbon or gold coating). Charging of a sample is reduced or eliminated by the gas surrounding the sample. It is this property of ESEMs that make them ideal for locations where sample preparation is not yet feasible, such as the surface of Mars. In addition, the lack of sample preparation needed here will simplify the sample acquisition process and allow caching of the samples for future complementary payload use.

  6. Analysis of uncertainties of thermal hydraulic calculations

    International Nuclear Information System (INIS)

    Macek, J.; Vavrin, J.

    2002-12-01

    In 1993-1997 it was proposed, within OECD projects, that a common program should be set up for uncertainty analysis by a probabilistic method based on a non-parametric statistical approach for system computer codes such as RELAP, ATHLET and CATHARE and that a method should be developed for statistical analysis of experimental databases for the preparation of the input deck and statistical analysis of the output calculation results. Software for such statistical analyses would then have to be processed as individual tools independent of the computer codes used for the thermal hydraulic analysis and programs for uncertainty analysis. In this context, a method for estimation of a thermal hydraulic calculation is outlined and selected methods of statistical analysis of uncertainties are described, including methods for prediction accuracy assessment based on the discrete Fourier transformation principle. (author)

  7. Thermal analysis of kieselguhr sludge

    Directory of Open Access Journals (Sweden)

    S. T. Antipov

    2013-01-01

    Full Text Available It’s currently necessary to clarify the mechanisms of thermodynamic and mass transfer processes in capillary porous media. In this paper we obtain the thermogravimetric curves of evaporation drying kieselguhr sludge. It is also an analysis of the curves, allowing to choose the optimum conditions of drying.

  8. Thermal analysis of spices decontaminated by irradiation

    Energy Technology Data Exchange (ETDEWEB)

    Varsanyi, I; Farkas, J [Koezponti Elelmiszeripari Kutato Intezet, Budapest (Hungary); Liptay, G; Petrik-Brandt, E [Budapesti Mueszaki Egyetem (Hungary)

    1979-01-01

    The cell-count-reducing effect of ionizing radiations is well known. To reduce microbiological contamination in the most frequently used spices, ground paprika, black pepper and a mixture of seven spices, a radiation dose of 1.5 Mrad (15 kGy) was applied. The aim of the investigation was to find out whether this dose caused significant changes in the spices which could be detected by thermal analysis. The results unambiguously show that the applied dose does not cause significant changes detectable by thermal analysis. This finding supports earlier experiences according to which no structural changes, disadvantageously influencing utilization of radiation treated spices, are caused by similar or smaller doses.

  9. SEM-EDS analysis of ancient gold leaf glass mosaic tesserae. A contribution to the dating of the materials

    International Nuclear Information System (INIS)

    Conventi, A; Verità, M; Neri, E

    2012-01-01

    Metal leaf (gold, silver or their alloys) glass tesserae began to be used in wall mosaics in the first century AD (the first examples are in Rome) and their use has been uninterrupted up to day. The metal leaf could be obtained from circulating coins, jewellery or refining. According to various techniques that have changed over the centuries, the leaf was hot fixed between two glass layers. From an archaeological point of view, it is interesting to know when and where these tesserae were made, if they were new made or if they were reused tesserae recovered from earlier dismantled mosaics. The determination of the glass composition of the tesserae is not of great help in this connection, for the same kind of glass was used over long periods. Available information is still scanter for glasses produced between the 1st to 8th centuries when the batch of raw materials (a natural soda called natron and a silica-lime sand) was melted in large tank furnaces and chunks of raw glass were transported all over the Mediterranean to be remelted and shaped into manufacts in small pot furnaces. The SEM-EDS analysis is proposed in this study as a useful tool to investigate the composition of both the glass and the gold alloy in leaf tesserae from mosaics of the 1st - 9th centuries. The comparison of the composition of the gold leaf of the tesserae with that of circulating gold coins (for which an important analytical data base is available), adds further information to the glass analysis, allowing us to improve the dating of the tesserae and increase the knowledge that may result from scientific analyses. The results demonstrate that good quantitative analyses of the metal leaf can be performed and that metal leaves made of pure gold or gold-silver alloys were used.

  10. Analysis of enamel microbiopsies in shed primary teeth by Scanning Electron Microscopy (SEM) and Polarizing Microscopy (PM)

    International Nuclear Information System (INIS)

    Costa de Almeida, Glauce Regina; Molina, Gabriela Ferian; Meschiari, Cesar Arruda; Barbosa de Sousa, Frederico; Gerlach, Raquel Fernanda

    2009-01-01

    The aims of this study were 1) to verify how close to the theoretically presumed areas are the areas of enamel microbiopsies carried out in vivo or in exfoliated teeth; 2) to test whether the etching solution penetrates beyond the tape borders; 3) to test whether the etching solution demineralizes the enamel in depth. 24 shed upper primary central incisors were randomly divided into two groups: the Rehydrated Teeth Group and the Dry Teeth Group. An enamel microbiopsy was performed, and the enamel microbiopsies were then analyzed by Scanning Electron Microscopy (SEM) and Polarizing Microscopy (PM). Quantitative birefringence measurements were performed. The 'true' etched area was determined by measuring the etched enamel using the NIH Image analysis program. Enamel birefringence was compared using the paired t test. There was a statistically significant difference when the etched areas in the Rehydrated teeth were compared with those of the Dry teeth (p = 0.04). The etched areas varied from - 11.6% to 73.5% of the presumed area in the Rehydrated teeth, and from 6.6% to 61.3% in the Dry teeth. The mean percentage of variation in each group could be used as a correction factor for the etched area. Analysis of PM pictures shows no evidence of in-depth enamel demineralization by the etching solution. No statistically significant differences in enamel birefringence were observed between values underneath and outside the microbiopsy area in the same tooth, showing that no mineral loss occurred below the enamel superficial layer. Our data showed no evidence of in-depth enamel demineralization by the etching solution used in the enamel microbiopsy proposed for primary enamel. This study also showed a variation in the measured diameter of the enamel microbiopsy in nineteen teeth out of twenty four, indicating that in most cases the etching solution penetrated beyond the tape borders.

  11. Ao leitor sem medo

    Directory of Open Access Journals (Sweden)

    José Eisenberg

    2000-05-01

    Full Text Available O texto resenha Ao leitor sem medo, de Renato Janine Ribeiro (Belo Horizonte, UFMG, 1999.This text is a review of Ao leitor sem medo by Renato Janine Ribeiro (Belo Horizonte, UFMG, 1999

  12. Micro-thermal analysis of polyester coatings

    NARCIS (Netherlands)

    Fischer, H.R.

    2010-01-01

    The application and suitability of micro-thermal analysis to detect changes in the chemical and physical properties of coating due to ageing and especially photo-degradation is demonstrated using a model polyester coating based on neopentyl glycol isophthalic acid. The changes in chemical structure

  13. Use of labelled atoms in thermal analysis

    International Nuclear Information System (INIS)

    Balek, V.; Beckman, I.N.

    1985-01-01

    The article informs of the preparation of labelled samples for which the most frequently used radionuclides are 14 C, 3 H or 2 H, 32 P, 35 S and others as well as radioactive gases such as 85 Kr, 133 Xe or 220 Rn and 222 Rn. The equipment is described for the application of labelled atoms in thermal analysis consisting of a detector for measuring radioactivity and a system for measuring thermal analysis parameters. Examples are given of the use of labelled atoms in the study of chemical reactions of solids, in autoradiography or in Moessbauer spectroscopy. The greatest attention is devoted to the use of labelled atoms in emanation thermal analysis. By this technique it is possible to study chemical reactions and phase transformations, to continuously monitor changes in the surface and morphology of dispersion substances, to characterize the mobility of defects in the structure of solids and the active state of the structure of solids and to ascertain mechanical, radiation and chemical effects on solids. Attention is also devoted to the technological applications of emanation thermal analysis (the solidification of cement paste, calcination and the firing of the mixture of oxides for the manufacture of ferrites). (E.S.)

  14. Thermal effects in concrete containment analysis

    International Nuclear Information System (INIS)

    Pfeiffer, P.A.; Kennedy, J.M.; Marchertas, A.H.

    1988-01-01

    Analyses of the thermo-mechanical response of the 1:6-scale reinforced concrete containment are presented. Three temperature- pressure scenarios are analyzed to complete loss of the pressure integrity. These results are compared to the analysis of pressure alone, to assess the importance of thermal effects. 19 refs., 9 figs., 8 tabs

  15. Thermal analysis of the SSC beam scraper

    International Nuclear Information System (INIS)

    Tran, N.; Dao, B.

    1993-04-01

    When a particle beam impacts a beam scraper, heat is generated resulting in a rise in the temperature of the material. The maximum temperature rise should be kept to a minimum in order to maintain scraper efficiency and performance. In this paper the results of a thermal analysis of a scraper are presented

  16. Thermal analysis of a gas centrifuge

    International Nuclear Information System (INIS)

    Andrade, D.A.; Bastos, J.L.F.; Maiorino, J.R.

    1996-01-01

    The centrifuge separation efficiency is the result of the composition of the centrifuge field to the secondary flow in the axial direction near to the rotor wall. For a given machine, the centrifuge field can not be altered and the effort to augment the separation efficiency should be concentrated on the secondary flow. The secondary flow has a mechanical and a thermal component. The mechanical component is due to the deceleration of the gas at the scoop region. The thermal component is due to the temperature differences at the rotor. This paper presents a thermal model of a centrifuge in order to understand the main heat transfer mechanisms and to establish the boundary conditions for a fluid flow computer code. The heat transfer analysis takes into account conduction at the structure parts of the rotor and shell, radiation with multi-reflections between the rotor and the shell, and convection to the ambient. (author)

  17. Urban thermal landscape characterization and analysis

    International Nuclear Information System (INIS)

    Xue, Y; Fung, T; Tsou, J

    2014-01-01

    Urban warming is sensitive to the nature (thermal properties, including albedo, water content, heat capacity and thermal conductivity) and the placement (surface geometry or urban topography) of urban surface. In this research, the pattern and variation of urban surface temperature is regarded as one kind of landscape, urban thermal landscape, which is assumed as the presentation of local surface heating process upon urban landscape. The goal of this research is to develop a research framework incorporating geospatial statistics, thermal infrared remote sensing and landscape ecology to study the urban effect on local surface thermal landscape regarding both the pattern and process. This research chose Hong Kong as the case study. Within the study area, urban and rural area coexists upon a hilly topography. In order to probe the possibility of local surface warming mechanism discrepancy between urban and rural area, the sample points are grouped into urban and rural categories in according with the land use map taken into a linear regression model separately to examine the possible difference in local warming mechanism. Global regression analysis confirmed the relationship between environmental factors and surface temperature and the urban-rural distinctive mechanism of dominating diurnal surface warming is uncovered

  18. Bimodal Nuclear Thermal Rocket Analysis Developments

    Science.gov (United States)

    Belair, Michael; Lavelle, Thomas; Saimento, Charles; Juhasz, Albert; Stewart, Mark

    2014-01-01

    Nuclear thermal propulsion has long been considered an enabling technology for human missions to Mars and beyond. One concept of operations for these missions utilizes the nuclear reactor to generate electrical power during coast phases, known as bimodal operation. This presentation focuses on the systems modeling and analysis efforts for a NERVA derived concept. The NERVA bimodal operation derives the thermal energy from the core tie tube elements. Recent analysis has shown potential temperature distributions in the tie tube elements that may limit the thermodynamic efficiency of the closed Brayton cycle used to generate electricity with the current design. The results of this analysis are discussed as well as the potential implications to a bimodal NERVA type reactor.

  19. Structural Equation Modeling (SEM) for Satisfaction and Dissatisfaction Ratings; Multiple Group Invariance Analysis across Scales with Different Response Format

    Science.gov (United States)

    Mazaheri, Mehrdad; Theuns, Peter

    2009-01-01

    The current study evaluates three hypothesized models on subjective well-being, comprising life domain ratings (LDR), overall satisfaction with life (OSWL), and overall dissatisfaction with life (ODWL), using structural equation modeling (SEM). A sample of 1,310 volunteering students, randomly assigned to six conditions, rated their overall life…

  20. Use of GSR particle analysis program on an analytical SEM to identify sources of emission of airborne particles

    International Nuclear Information System (INIS)

    Chan, Y.C.; Trumper, J.; Bostrom, T.

    2002-01-01

    Full text: High concentrations of airborne particles, in particular PM 10 (particulate matter 10 , but has been little used in Australia for airborne particulates. Two sets of 15 mm PM 10 samples were collected in March and April 2000 from two sites in Brisbane, one within a suburb and one next to an arterial road. The particles were collected directly onto double-sided carbon tapes with a cascade impactor attached to a high-volume PM 10 sampler. The carbon tapes were analysed in a JEOL 840 SEM equipped with a Be-window energy-dispersive X-ray detector and Moran Scientific microanalysis system. An automated Gun Shot Residue (GSR) program was used together with backscattered electron imaging to characterise and analyse individual particulates. About 6,000 particles in total were analysed for each set of impactor samples. Due to limitations of useful pixel size, only particles larger than about 0.5 μm could be analysed. The size, shape and estimated elemental composition (from Na to Pb) of the particles were subjected to non-hierarchical cluster analysis and the characteristics of the clusters were related to their possible sources of emission. Both samples resulted in similar particle clusters. The particles could be classified into three main categories non-spherical (58% of the total number of analysed particles, shape factor >1 1), spherical (15%) and 'carbonaceous' (27%, ie with unexplained % of elemental mass >75%). Non-spherical particles were mainly sea salt and soil particles, and a small amount of iron, lead and mineral dust. The spherical particles were mainly sea salt particles and flyash, and a small amount of iron, lead and secondary sulphate dust. The carbonaceous particles included carbon material mixed with secondary aerosols, roadside dust, sea salt or industrial dust. The arterial road sample also contained more roadside dust and less secondary aerosols than the suburb sample. Current limitations with this method are the minimum particle size

  1. Thermal analysis of spices decontaminated by irradiation

    International Nuclear Information System (INIS)

    Varsanyi, I.; Farkas, J.; Liptay, G.; Petrik-Brandt, E.

    1979-01-01

    The cell-count-reducing effect of ionizing radiations is well known. To reduce microbiological contamination in the most frequently used spices, ground paprika, black pepper and a mixture of seven spices, a radiation dose of 1.5 Mrad (15 kGy) was applied. The aim of the investigation was to find out whether this dose caused significant changes in the spices which could be detected by thermal analysis. The results unambiguously show that the applied dose does not cause significant changes detectable by thermal analysis. This finding supports earlier experiences according to which no structural changes, disadvantageously influencing utilization of radiation treated spices, are caused by similar or smaller doses. (author)

  2. Thermal analysis applied to irradiated propolis

    Energy Technology Data Exchange (ETDEWEB)

    Matsuda, Andrea Harumi; Machado, Luci Brocardo; Mastro, N.L. del E-mail: nelida@usp.br

    2002-03-01

    Propolis is a resinous hive product, collected by bees. Raw propolis requires a decontamination procedure and irradiation appears as a promising technique for this purpose. The valuable properties of propolis for food and pharmaceutical industries have led to increasing interest in its technological behavior. Thermal analysis is a chemical analysis that gives information about changes on heating of great importance for technological applications. Ground propolis samples were {sup 60}Co gamma irradiated with 0 and 10 kGy. Thermogravimetry curves shown a similar multi-stage decomposition pattern for both irradiated and unirradiated samples up to 600 deg. C. Similarly, through differential scanning calorimetry , a coincidence of melting point of irradiated and unirradiated samples was found. The results suggest that the irradiation process do not interfere on the thermal properties of propolis when irradiated up to 10 kGy.

  3. SEM and Raman Spectroscopy Applied to Biomass Analysis for Application in the Field of Biofuels and Food Industry

    Czech Academy of Sciences Publication Activity Database

    Samek, Ota; Hároniková, A.; Vaškovicová, Naděžda; Hrubanová, Kamila; Ježek, Jan; Márová, I.; Krzyžánek, Vladislav; Zemánek, Pavel

    2015-01-01

    Roč. 21, S3 (2015), s. 1775-1776 ISSN 1431-9276 R&D Projects: GA MŠk(CZ) LO1212; GA MŠk ED0017/01/01; GA ČR(CZ) GA14-20012S Institutional support: RVO:68081731 Keywords : SEM * Raman spetroscopy Subject RIV: JA - Electronics ; Optoelectronics, Electrical Engineering Impact factor: 1.730, year: 2015

  4. Application of Thermal Network Model to Transient Thermal Analysis of Power Electronic Package Substrate

    Directory of Open Access Journals (Sweden)

    Masaru Ishizuka

    2011-01-01

    Full Text Available In recent years, there is a growing demand to have smaller and lighter electronic circuits which have greater complexity, multifunctionality, and reliability. High-density multichip packaging technology has been used in order to meet these requirements. The higher the density scale is, the larger the power dissipation per unit area becomes. Therefore, in the designing process, it has become very important to carry out the thermal analysis. However, the heat transport model in multichip modules is very complex, and its treatment is tedious and time consuming. This paper describes an application of the thermal network method to the transient thermal analysis of multichip modules and proposes a simple model for the thermal analysis of multichip modules as a preliminary thermal design tool. On the basis of the result of transient thermal analysis, the validity of the thermal network method and the simple thermal analysis model is confirmed.

  5. Parameter Uncertainty for Repository Thermal Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Hardin, Ernest [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Hadgu, Teklu [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Greenberg, Harris [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Dupont, Mark [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL)

    2015-10-01

    This report is one follow-on to a study of reference geologic disposal design concepts (Hardin et al. 2011a). Based on an analysis of maximum temperatures, that study concluded that certain disposal concepts would require extended decay storage prior to emplacement, or the use of small waste packages, or both. The study used nominal values for thermal properties of host geologic media and engineered materials, demonstrating the need for uncertainty analysis to support the conclusions. This report is a first step that identifies the input parameters of the maximum temperature calculation, surveys published data on measured values, uses an analytical approach to determine which parameters are most important, and performs an example sensitivity analysis. Using results from this first step, temperature calculations planned for FY12 can focus on only the important parameters, and can use the uncertainty ranges reported here. The survey of published information on thermal properties of geologic media and engineered materials, is intended to be sufficient for use in generic calculations to evaluate the feasibility of reference disposal concepts. A full compendium of literature data is beyond the scope of this report. The term “uncertainty” is used here to represent both measurement uncertainty and spatial variability, or variability across host geologic units. For the most important parameters (e.g., buffer thermal conductivity) the extent of literature data surveyed samples these different forms of uncertainty and variability. Finally, this report is intended to be one chapter or section of a larger FY12 deliverable summarizing all the work on design concepts and thermal load management for geologic disposal (M3FT-12SN0804032, due 15Aug2012).

  6. Development of disruption thermal analysis code DREAM

    Energy Technology Data Exchange (ETDEWEB)

    Yamazaki, Seiichiro; Kobayahsi, Takeshi [Kawasaki Heavy Industries Ltd., Kobe (Japan); Seki, Masahiro

    1989-07-01

    When a plasma disruption takes place in a tokamak type fusion reactor, plasma facing componenets such as first wall and divertor/limiter are subjected to a intensse heat load in a short duration. At the surface of the wall, temperature rapidly rises, and melting and evaporation occurs. It causes reduction of wall thickness and crack initiation/propagation. As lifetime of the components is significantly affected by them, the transient analysis in consideration of phase changes and radiation heat loss in required in the design of these components. This paper describes the computer code DREAM, developed to perform the disruption thermal analysis, taking phase changes and radiation into account. (author).

  7. Development of disruption thermal analysis code DREAM

    International Nuclear Information System (INIS)

    Yamazaki, Seiichiro; Kobayahsi, Takeshi; Seki, Masahiro.

    1989-01-01

    When a plasma disruption takes place in a tokamak type fusion reactor, plasma facing componenets such as first wall and divertor/limiter are subjected to a intensse heat load in a short duration. At the surface of the wall, temperature rapidly rises, and melting and evaporation occurs. It causes reduction of wall thickness and crack initiation/propagation. As lifetime of the components is significantly affected by them, the transient analysis in consideration of phase changes and radiation heat loss in required in the design of these components. This paper describes the computer code DREAM, developed to perform the disruption thermal analysis, taking phase changes and radiation into account. (author)

  8. Availability Performance Analysis of Thermal Power Plants

    Science.gov (United States)

    Bhangu, Navneet Singh; Singh, Rupinder; Pahuja, G. L.

    2018-03-01

    This case study presents the availability evaluation method of thermal power plants for conducting performance analysis in Indian environment. A generic availability model has been proposed for a maintained system (thermal plants) using reliability block diagrams and fault tree analysis. The availability indices have been evaluated under realistic working environment using inclusion exclusion principle. Four year failure database has been used to compute availability for different combinatory of plant capacity, that is, full working state, reduced capacity or failure state. Availability is found to be very less even at full rated capacity (440 MW) which is not acceptable especially in prevailing energy scenario. One of the probable reason for this may be the difference in the age/health of existing thermal power plants which requires special attention of each unit from case to case basis. The maintenance techniques being used are conventional (50 years old) and improper in context of the modern equipment, which further aggravate the problem of low availability. This study highlights procedure for finding critical plants/units/subsystems and helps in deciding preventive maintenance program.

  9. Current lead thermal analysis code 'CURRENT'

    International Nuclear Information System (INIS)

    Yamaguchi, Masahito; Tada, Eisuke; Shimamoto, Susumu; Hata, Kenichiro.

    1985-08-01

    Large gas-cooled current lead with the capacity more than 30 kA and 22 kV is required for superconducting toroidal and poloidal coils for fusion application. The current lead is used to carry electrical current from the power supply system at room temperature to the superconducting coil at 4 K. Accordingly, the thermal performance of the current lead is significantly important to determine the heat load requirements of the coil system at 4 K. Japan Atomic Energy Research Institute (JAERI) has being developed the large gas-cooled current leads with the optimum condition in which the heat load is around 1 W per 1 kA at 4 K. In order to design the current lead with the optimum thermal performances, JAERI developed thermal analysis code named as ''CURRENT'' which can theoretically calculate the optimum geometric shape and cooling conditions of the current lead. The basic equations and the instruction manual of the analysis code are described in this report. (author)

  10. Thermal transient analysis applied to horizontal wells

    Energy Technology Data Exchange (ETDEWEB)

    Duong, A.N. [Society of Petroleum Engineers, Canadian Section, Calgary, AB (Canada)]|[ConocoPhillips Canada Resources Corp., Calgary, AB (Canada)

    2008-10-15

    Steam assisted gravity drainage (SAGD) is a thermal recovery process used to recover bitumen and heavy oil. This paper presented a newly developed model to estimate cooling time and formation thermal diffusivity by using a thermal transient analysis along the horizontal wellbore under a steam heating process. This radial conduction heating model provides information on the heat influx distribution along a horizontal wellbore or elongated steam chamber, and is therefore important for determining the effectiveness of the heating process in the start-up phase in SAGD. Net heat flux estimation in the target formation during start-up can be difficult to measure because of uncertainties regarding heat loss in the vertical section; steam quality along the horizontal segment; distribution of steam along the wellbore; operational conditions; and additional effects of convection heating. The newly presented model can be considered analogous to pressure transient analysis of a buildup after a constant pressure drawdown. The model is based on an assumption of an infinite-acting system. This paper also proposed a new concept of a heating ring to measure the heat storage in the heated bitumen at the time of testing. Field observations were used to demonstrate how the model can be used to save heat energy, conserve steam and enhance bitumen recovery. 18 refs., 14 figs., 2 appendices.

  11. The micro thermal analysis of polymers

    International Nuclear Information System (INIS)

    Grandy, David Brian

    2002-01-01

    This study is concerned with the development of micro-thermal analysis as a technique for characterising heterogeneous polymers. It is divided into two main parts. In the first part, the use of miniature Wollaston wire near-field thermal probes mounted in an atomic force microscope (AFM) to carry out highly localised thermal analysis (L-TA) of amorphous and semi-crystalline polymers is investigated. Here, the temperature of the probe sensor or tip is scanned over a pre-selected temperature range while in contact with the surface of a sample. It is thereby used to heat a volume of material of the order of several cubic micrometres. The effect of the glass transition, cold crystallisation, melting and degree of crystallinity on L-TA measurements is investigated. The materials used are poly(ethylene terephthalate), polystyrene and fluorocarbon-coated poly(butylene terephthalate). The primary measurements are the micro- or localised analogues of thermomechanical analysis (L-TMA) and differential thermal analysis (L-DTA). The effect of applying a sinusoidal modulation to the temperature of the probe is also investigated. In the second part, conventional ultra-sharp inert AFM probes are used, in conjunction with a variable-temperature microscope stage, to conduct variable-temperature mechanical property-based imaging of phase-separated polymer blends and copolymers. Here, the temperature of the whole sample is varied and the temperature of the probe tip remains essentially the same as that of the sample. The primary AFM imaging mode is pulsed force mode (PFM-AFM). This is an intermittent contact (IC) method in which a mechanical modulation is applied to the probe cantilever. The methodology is demonstrated on a model 50:50 blend of polystyrene and poly(methyl methacrylate) (PS-PMMA) and three segmented polyurethane (SPU) elastomers containing different chain extenders. In doing so, it is shown that PFM-AFM imaging can be carried out successfully over a temperature range

  12. Poly(vinylidene fluoride)-based ion track membranes with different pore diameters and shapes. SEM observations and conductometric analysis

    International Nuclear Information System (INIS)

    Nuryanthi, Nunung; Yamaki, Tetsuya; Koshikawa, Hiroshi; Asano, Masaharu; Enomoto, Kazuyuki; Sawada, Shin-ichi; Maekawa, Yasunari; Voss, Kay-Obbe; Trautmann, Christina; Neumann, Reinhard

    2010-01-01

    Poly(vinylidene fluoride) (PVDF) membranes with conical and cylindrical nanopores were prepared in a controlled manner by the ion-track technique, which involved heavy-ion beam irradiation and subsequent alkaline etching. The etching behavior mainly depended on the energy deposition of the ion beams, and thus its depth distribution, estimated by theoretical simulation, was successfully applied to control the shapes and diameters of the etched pores. Scanning electron microscopy (SEM) and electrolytic conductometry provided an insight into the critical experimental parameters. Interestingly, applying a higher voltage to the conductometry cell promoted track etching up to breakthrough probably because electrophoretic migration of the dissolved products occurred out of each pore. (author)

  13. Use of SEM and EDS analysis in the investigation of Al-Si-Cu piston alloy cast porosity

    Directory of Open Access Journals (Sweden)

    D. Kakaš

    2009-07-01

    Full Text Available Porosity formation was detected in the casting thinnest section in the proximity of the as cast surface and near the wall centerline. In order to investigate the cause of the porosity formation light microscopy was used to define as cast structure. After initial findings SEM and EDS analyses were performed. Based on the results it is possible to define cause of the observed porosity. A number of pores originates from the mould filling stage and entrainment of the oxide films, while others appear due to insufficient feeding during solidification.

  14. Study of copper deposit on a porous electrode of carbon and stainless steel by sem-xrd and image analysis

    OpenAIRE

    Constanzo-R., Robinson; Pagliero-N., Antonio; Vergara-G., Froilán

    2014-01-01

    El objetivo de este trabajo fue realizar un análisis cualitativ o de la distribución de un electrodepósito de cobre en el inter ior de electrodos porosos (EP) de acero inoxidable y carbono grafito. Para ello, se reali zaron pruebas de electrodepositación de cobre a nivel de labora torio, con un posterior análisis de cortes de muestras de acero y grafito vía Microscopía Estereoscópica, Microscopía SEM-DRX y Análisis de Imagen, los cuales mostraron que el cobre no se deposita en forma uniforme ...

  15. Determination of the fractal dimension surface of the fracture from SEM images with assistance of the computer image quantitative analysis system

    International Nuclear Information System (INIS)

    Wawszczak, J.

    1999-01-01

    This paper presents a procedure for quantitative image analysis for determination of the fractal dimension from SEM surface images of the fracture 0H14N5CuNb steel. Investigated quenched and tempered samples of the steel after impact tests (in room and -85 o C temperatures). This method can be useful for analysing local fractal dimension of any surface parts (not oriented) of the fracture with different topography of this surface. (author)

  16. Remote Thermal Analysis Through the Internet

    Science.gov (United States)

    Malroy, Eric T.

    2002-07-01

    The Heater of the Hypersonic Tunnel Facility (HTF) was modeled using SINDA/FLUINT thermal software. A description of the model is given. The project presented the opportunity of interfacing the thermal model with the Internet and was a demonstration that complex analysis is possible through the Internet. Some of the issues that need to be addressed related to interfacing software with the Internet are the following: justification for using the Internet, selection of the web server, choice of the CGI language, security of the system, communication among the parties, maintenance of state between web pages, and simultaneous users on the Internet system. The opportunities available for using the Internet for analysis are many and can present a significant jump in technology. This paper presents a vision how interfacing with the Internet could develop in the future. Using a separate Optical Internet (OI) for analysis, coupled with virtual reality analysis rooms (VRAR), could provide a synergistic environment to couple together engineering analysis within industry, academia, and government. The process of analysis could be broken down into sub-components so that specialization could occur resulting in superior quality, minimized cost and reduced time for engineering analysis and manufacturing. Some possible subcomponents of the system are solver routines, databases, Graphical User Interfaces, engineering design software, VRARs, computer processing, CAD systems, manufacturing, and a plethora of other options only limited by ones imagination. On a larger scope, the specialization of companies on the optical network would allow companies to rapidly construct and reconstruct their infrastructure based on changing economic conditions. This could transform business.

  17. Coastal surface sediment quality assessment in Leizhou Peninsula (South China Sea) based on SEM-AVS analysis.

    Science.gov (United States)

    Li, Feng; Lin, Jin-qin; Liang, Yan-yan; Gan, Hua-yang; Zeng, Xiang-yun; Duan, Zhi-peng; Liang, Kai; Liu, Xing; Huo, Zhen-hai; Wu, Chang-hua

    2014-07-15

    Surface sediments from the coastal area of the Leizhou Peninsula in the South China Sea were collected and analyzed and the potential ecological risks in the area were assessed based on acid-volatile sulfide (AVS) model. The AVS levels are between 0.109 and 55.6 μmol g(-1), with the average at 4.45 μmol g(-1). The high AVS-concentration zones include the aquaculture areas of Liusha Bay and the densely populated areas of Zhanjiang Bay. The simultaneously extracted metals (SEM) range from 0.026 μmol g(-1) to 8.61 μmol g(-1), with the average at 0.843 μmol g(-1). Most of high SEM-concentration stations were located in ports or aquaculture zones. Most of the coastal surface sediments of the Leizhou Peninsula (90%) had no adverse biological effects according to the criterion proposed by USEPA (2005); while adverse effects were uncertain in some stations (8%); even in 2 stations (2%) adverse biological effects may be expected. Copyright © 2014 Elsevier Ltd. All rights reserved.

  18. Fluorine concentrations of ore fluids in the Illinois-Kentucky district: Evidence from SEM-EDS analysis of fluid inclusion decrepitates

    Science.gov (United States)

    Kenderes, Stuart M.; Appold, Martin S.

    2017-08-01

    The Illinois-Kentucky district is an atypical occurrence of Mississippi Valley-type (MVT) mineralization that consists predominantly of fluorite rather than metal sulfide minerals. A long-standing assumption for the predominance of fluorite in the Illinois-Kentucky district is that the ore fluids there were anomalously rich in dissolved fluorine compared to typical sedimentary brines and other MVT ore fluids. This hypothesis is based on the unusual close temporal and spatial association of fluorine-rich ultramafic igneous rocks to MVT mineralization in the district, high K and Sr concentrations in the igneous rocks and in MVT ore-hosted fluid inclusions, a significant mantle 3He/4He component in ore-hosted fluid inclusions, and reaction path models that show titration of a HF-rich fluid into sedimentary brine is capable of producing a fluorite-dominated MVT ore mineral assemblage. The purpose of the present study was to test this hypothesis more directly by determining the fluorine concentration of the Illinois-Kentucky ore fluid through SEM-EDS analysis of evaporative solute mounds resulting from thermal decrepitation of fluid inclusions hosted in sphalerite. All 26 evaporative solute mounds from Illinois-Kentucky sphalerite samples analyzed contained detectable concentrations of fluorine of 1-4 weight percent. Based on calibration to standard solutions and previously published fluid inclusion major element concentrations, these solute mound fluorine concentrations correspond to fluid inclusion fluorine concentrations of about 680-4300 ppm, indicating that the Illinois-Kentucky ore fluids were quite rich in fluorine compared to typical sedimentary brines, which have fluorine concentrations mainly on the order of 1's to 10's of ppm. In contrast, solute mounds from sphalerite-hosted fluid inclusions from the Tri-State district did not contain fluorine in excess of the detection limit. The detection limit equates to an aqueous fluorine concentration between 87 and

  19. SEM, TEM, and IHC Analysis of the Sinus Node and Its Implications for the Cardiac Conduction System

    Directory of Open Access Journals (Sweden)

    D. Mandrioli

    2013-01-01

    Full Text Available More than 100 years after the discovery of the sinus node (SN by Keith and Flack, the function and structure of the SN have not been completely established yet. The anatomic architecture of the SN has often been described as devoid of an organized structure; the origin of the sinus impulse is still a matter of debate, and a definite description of the long postulated internodal specialized tract conducting the impulse from the SN to the atrioventricular node (AVN is still missing. In our previously published study, we proposed a morphologically ordered structure for the SN. As a confirmation of what was presented then, we have added the results of additional observations regarding the structural particularities of the SN. We investigated the morphology of the sinus node in the human hearts of healthy individuals using histochemical, immunohistochemical, optical, and electron microscopy (SEM, TEM. Our results confirmed that the SN presents a previously unseen highly organized architecture.

  20. Foundation heat transfer analysis for buildings with thermal piles

    International Nuclear Information System (INIS)

    Almanza Huerta, Luis Enrique; Krarti, Moncef

    2015-01-01

    Highlights: • A numerical transient thermal model for thermo-active foundations is developed. • Thermal interactions between thermal piles and building foundations are evaluated. • A simplified analysis method of thermal interactions between thermal piles and building foundations is developed. - Abstract: Thermal piles or thermo-active foundations utilize heat exchangers embedded within foundation footings to heat and/or cool buildings. In this paper, the impact of thermal piles on building foundation heat transfer is investigated. In particular, a simplified analysis method is developed to estimate the annual ground-coupled foundation heat transfer when buildings are equipped with thermal piles. First, a numerical analysis of the thermal performance of thermo-active building foundations is developed and used to assess the interactions between thermal piles and slab-on-grade building foundations. The impact of various design parameters and operating conditions is evaluated including foundation pile depth, building slab width, foundation insulation configuration, and soil thermal properties. Based on the results of a series of parametric analyses, a simplified analysis method is presented to assess the impact of the thermal piles on the annual heat fluxes toward or from the building foundations. A comparative evaluation of the predictions of the simplified analysis method and those obtained from the detailed numerical analysis indicated good agreement with prediction accuracy lower than 5%. Moreover, it is found that thermal piles can affect annual building foundation heat loss/gain by up to 30% depending on foundation size and insulation level

  1. Assessment of metal pollution sources by SEM/EDS analysis of solid particles in snow: a case study of Žerjav, Slovenia.

    Science.gov (United States)

    Miler, Miloš; Gosar, Mateja

    2013-12-01

    Solid particles in snow deposits, sampled in mining and Pb-processing area of Žerjav, Slovenia, have been investigated using scanning electron microscopy/energy-dispersive X-ray spectroscopy (SEM/EDS). Identified particles were classified as geogenic-anthropogenic, anthropogenic, and secondary weathering products. Geogenic-anthropogenic particles were represented by scarce Zn- and Pb-bearing ore minerals, originating from mine waste deposit. The most important anthropogenic metal-bearing particles in snow were Pb-, Sb- and Sn-bearing oxides and sulphides. The morphology of these particles showed that they formed at temperatures above their melting points. They were most abundant in snow sampled closest to the Pb-processing plant and least abundant in snow taken farthest from the plant, thus indicating that Pb processing was their predominant source between the last snowfall and the time of sampling. SEM/EDS analysis showed that Sb and Sn contents in these anthropogenic phases were higher and more variable than in natural Pb-bearing ore minerals. The most important secondary weathering products were Pb- and Zn-containing Fe-oxy-hydroxides whose elemental composition and morphology indicated that they mostly resulted from oxidation of metal-bearing sulphides emitted from the Pb-processing plant. This study demonstrated the importance of single particle analysis using SEM/EDS for differentiation between various sources of metals in the environment.

  2. SBWR core thermal hydraulic analysis during startup

    International Nuclear Information System (INIS)

    Lin, J.H.; Huang, R.L.; Sawyer, C.D.

    1993-01-01

    This paper reports on a thermal hydraulic analysis of the SIMPLIFIED BOILING WATER REACTOR (SBWR) during startup. The potential instability during a SBWR startup has drawn the attention of designers, researchers, and engineers. It has not been a concern for a Boiling Water Reactor (BWR) with forced recirculation; however, for SBWR with natural circulation the concern exists. The concern is about the possibility of a geysering mode oscillation during SBWR startup from a cold temperature and a low system pressure with a low natural circulation flow rate. A thermal hydraulic analysis of the SBWR is performed in simulation of the startup using the TRACG computer code. The temperature, pressure, and reactor power profiles of SBWR during the startup are presented. The results are compared with the data of a natural circulation boiling water reactor, the DODEWAARD plant, in which no instabilities have been observed during many startups. It is shown that a SBWR startup which follows proper procedures, geysering and other modes of oscillations can be avoided

  3. Thermal-Signature-Based Sleep Analysis Sensor

    Directory of Open Access Journals (Sweden)

    Ali Seba

    2017-10-01

    Full Text Available This paper addresses the development of a new technique in the sleep analysis domain. Sleep is defined as a periodic physiological state during which vigilance is suspended and reactivity to external stimulations diminished. We sleep on average between six and nine hours per night and our sleep is composed of four to six cycles of about 90 min each. Each of these cycles is composed of a succession of several stages of sleep that vary in depth. Analysis of sleep is usually done via polysomnography. This examination consists of recording, among other things, electrical cerebral activity by electroencephalography (EEG, ocular movements by electrooculography (EOG, and chin muscle tone by electromyography (EMG. Recordings are made mostly in a hospital, more specifically in a service for monitoring the pathologies related to sleep. The readings are then interpreted manually by an expert to generate a hypnogram, a curve showing the succession of sleep stages during the night in 30s epochs. The proposed method is based on the follow-up of the thermal signature that makes it possible to classify the activity into three classes: “awakening,” “calm sleep,” and “restless sleep”. The contribution of this non-invasive method is part of the screening of sleep disorders, to be validated by a more complete analysis of the sleep. The measure provided by this new system, based on temperature monitoring (patient and ambient, aims to be integrated into the tele-medicine platform developed within the framework of the Smart-EEG project by the SYEL–SYstèmes ELectroniques team. Analysis of the data collected during the first surveys carried out with this method showed a correlation between thermal signature and activity during sleep. The advantage of this method lies in its simplicity and the possibility of carrying out measurements of activity during sleep and without direct contact with the patient at home or hospitals.

  4. SEM/XPS analysis of fractured adhesively bonded graphite fibre surface resin-rich/graphite fibre composites

    Science.gov (United States)

    Devilbiss, T. A.; Wightman, J. P.; Progar, D. J.

    1988-01-01

    Samples of graphite fiber-reinforced polyimide were fabricated allowing the resin to accumulate at the composite surface. These surface resin-rich composites were then bonded together and tested for lap shear strength both before and after thermal aging. Lap shear strength did not appear to show a significant improvement over that previously recorded for resin-poor samples and was shown to decrease with increasing aging time and temperature.

  5. Analysis of thermal process of pozzolan production

    Directory of Open Access Journals (Sweden)

    Mejía De Gutiérrez, R.

    2004-06-01

    Full Text Available The objective of this study was evaluated the effect of heat treatment parameters on the pozzolanic activity of natural kaolin clays. The experimental design included three factors: kaolin type, temperature and time. Five types of Colombian kaolin clays were thermally treated from 400 to 1000 °C by 1, 2, and 3 hours. The raw materials and the products obtained were characterized by X-Ray Diffraction (XRD, Fourier Transform Infrared Spectroscopy (FTIR and Differential Thermal / Thermo gravimetric Analysis (DTAJ TGA. The pozzolanic activity of thermally treated samples according to chemical and mechanical tests was investigated.

    El objetivo de este estudio fue caracterizar las variables de producción de un metacaolín de alta reactividad puzolánica. El diseño experimental utilizó un modelo factorial que consideró tres factores: tipo de caolín (C, temperatura y tiempo. A partir del conocimiento de las fuentes de caolín y el contacto con proveedores y distribuidores del producto a nivel nacional, se seleccionaron cinco muestras representativas de arcillas caoliníticas, las cuales se sometieron a un tratamiento térmico entre 400 y 1.000 ºC (seis niveles de temperatura y tres tiempos de exposición, 1, 2 y 3 horas. Los caolines de origen y los productos obtenidos de cada proceso térmico fueron evaluados mediante técnicas de tipo físico y químico, difracción de rayos X, infrarrojo FTIR, y análisis térmico diferencial (OTA, TGA. Complementariamente se evalúa la actividad puzolánica, tanto química como mecánica, del producto obtenido a diferentes temperaturas de estudio.

  6. In situ oxidation of zirconium binary alloys by environmental SEM and analysis by AFM, FIB, and TEM

    International Nuclear Information System (INIS)

    Proff, C.; Abolhassani, S.; Dadras, M.M.; Lemaignan, C.

    2010-01-01

    Binary Zr-alloys containing 1%Fe and 1% Ni (large precipitates) and 1% Cr and 0.6% Nb (small precipitates), as well as a pure Zr sample were exposed in situ at 130 Pa water vapour pressure at 415 o C in an environmental SEM. The surface topography and composition of each sample was characterised before in situ experiments, during and after oxidation. After oxidation the surface was characterised by SEM and EDS, AFM and TEM combined with EDS. Focused ion beam was used to prepare cross sections of the metal-oxide interface and for the preparation of TEM thin foils. The oxidation behaviour of precipitates for these alloying elements can be characterised into two large families, those which show a rapid oxidation and those which induce a delayed oxidation in comparison with the Zr-matrix. At 415 o C after 1 h of oxidation for Zr1%Fe and Zr1%Ni, the formation of protrusions could be detected at the surface, being related to underlying SPP in the oxide. On Zr1%Cr and Zr0.6%Nb unoxidised SPPs were observed in the oxide, close to the metal-oxide interface. These SPPs were, however, oxidised close to the outer surface of the oxide. The surface roughness was increased for all materials after in situ oxidation, however, only for Zr1%Fe and Zr1%Ni protrusions appeared on the surface during oxidation. It was subsequently demonstrated that these latter correspond to the position of SPPs. For Zr1%Fe the surface roughness increased more than in the other materials and on these protrusions small iron oxide crystals have been observed at the surface. These observations confirm that Fe has a different behaviour compared to the other SPP forming elements, and it diffuses out to the free surface of the material. These alloying elements being the constituents of the commercial alloys (Fe and Cr for Zircaloy-4; Fe, Cr and Ni for Zircaloy-2 and Nb for all Nb-containing alloys), this study allows to separate their individual influence and can allow a subsequent comparison to the behaviour

  7. Thermal analysis on motorcycle disc brake geometry

    Science.gov (United States)

    W. M. Zurin W., S.; Talib, R. J.; Ismail, N. I.

    2017-08-01

    Braking is a phase of slowing and stop the movement of motorcycle. During braking, the frictional heat was generated and the energy was ideally should be faster dissipated to surrounding to prevent the built up of the excessive temperature which may lead to brake fluid vaporization, thermoelastic deformation at the contact surface, material degradation and failure. In this paper, solid and ventilated type of motorcycle disc brake are being analyse using Computational Fluid Dynamic (CFD) software. The main focus of the analysis is the thermal behaviour during braking for solid and ventilated disc brake. A comparison between both geometries is being discussed to determine the better braking performance in term of temperature distribution. It is found that ventilated disc brake is having better braking performance in terms of heat transfer compare to solid disc.

  8. The effect of MTAD, an endodontic irrigant, on fibroblast attachment to periodontally affected root surfaces: A SEM analysis

    Directory of Open Access Journals (Sweden)

    Mostafa Ghandi

    2013-01-01

    Full Text Available Background: Root surface debridement (RSD is necessary to create an environment suitable for reattachment of the periodontium. Root surface conditioning may aid the formation of a biocompatible surface suitable for cell reattachment. BioPure™ MTAD (mixture of Doxycycline, citric acid and a detergent is an endodontic irrigant with antibacterial properties and the ability to remove smear layer. It was hypothesized that MTAD may be useful for root surface conditioning. The efficacy of MTAD as a conditioner was measured by examining fibroblast attachment to root surfaces. Materials and Methods: Thirty-two specimens of human teeth with advanced periodontal disease were used. The surfaces were root planed until smooth. Half of the specimens were treated with 0.9% saline and the other samples with Biopure MTAD. As a negative control group, five further samples were left unscaled with surface calculus. Human gingival fibroblast cells HGF1-PI1 were cultured and poured over the tooth specimens and incubated. After fixation, the samples were sputter-coated with gold and examined with a SEM. The morphology and number of attached, fixed viable cells were examined. The data was analysed using the Mann-Whitney-U statistical test. Results: There was no significant difference between the numbers of attached cells in the experimental group treated with MTAD and the control group treated with saline. Little or no attached cells were seen in the negative control group. Conclusion: RSD created an environment suitable for cell growth and attachment in a laboratory setting. The use of MTAD did not promote the attachment and growth of cells on the surface of human roots following RSD.

  9. The effect of MTAD, an endodontic irrigant, on fibroblast attachment to periodontally affected root surfaces: A SEM analysis.

    Science.gov (United States)

    Ghandi, Mostafa; Houshmand, Behzad; Nekoofar, Mohammad H; Tabor, Rachel K; Yadeghari, Zahra; Dummer, Paul M H

    2013-03-01

    Root surface debridement (RSD) is necessary to create an environment suitable for reattachment of the periodontium. Root surface conditioning may aid the formation of a biocompatible surface suitable for cell reattachment. BioPure™ MTAD (mixture of Doxycycline, citric acid and a detergent) is an endodontic irrigant with antibacterial properties and the ability to remove smear layer. It was hypothesized that MTAD may be useful for root surface conditioning. The efficacy of MTAD as a conditioner was measured by examining fibroblast attachment to root surfaces. Thirty-two specimens of human teeth with advanced periodontal disease were used. The surfaces were root planed until smooth. Half of the specimens were treated with 0.9% saline and the other samples with Biopure MTAD. As a negative control group, five further samples were left unscaled with surface calculus. Human gingival fibroblast cells HGF1-PI1 were cultured and poured over the tooth specimens and incubated. After fixation, the samples were sputter-coated with gold and examined with a SEM. The morphology and number of attached, fixed viable cells were examined. The data was analysed using the Mann-Whitney-U statistical test. There was no significant difference between the numbers of attached cells in the experimental group treated with MTAD and the control group treated with saline. Little or no attached cells were seen in the negative control group. RSD created an environment suitable for cell growth and attachment in a laboratory setting. The use of MTAD did not promote the attachment and growth of cells on the surface of human roots following RSD.

  10. Thermal analysis of transportation packaging for nuclear spent fuel

    International Nuclear Information System (INIS)

    Akamatsu, Hiroshi; Taniuchi, Hiroaki

    1989-01-01

    Safety analysis of transportation packaging for nuclear spent fuel comprises structural, thermal, containment, shielding and criticality factors, and the safety of a packaging is verified by these analyses. In thermal analysis, the temperature of each part of the packaging is calculated under normal and accident test conditions. As an example of thermal analysis, the temperature distribution of a packaging being subjected to a normal test was calculated by the TRUMP code and compared with measured data. (author)

  11. Thermal Analysis: A Complementary Method to Study the Shurijeh Clay Minerals

    Directory of Open Access Journals (Sweden)

    Golnaz Jozanikohan

    2015-06-01

    Full Text Available Clay minerals are considered the most important components of clastic reservoir rock evaluation studies. The Shurijeh gas reservoir Formation, represented by shaly sandstones of the Late Jurassic-Early Cretaceous age, is the main reservoir rock in the Eastern Kopet-Dagh sedimentary Basin, NE Iran. In this study, X-ray diffraction (XRD, X-ray fluorescence (XRF, scanning electron microscopic (SEM studies, and thermal analysis including differential thermal analysis (DTA, and thermogravimetric analysis (TGA techniques were utilized in the characterization of the Shurijeh clay minerals in ten representative samples. The XRF studies showed that silica and aluminum oxides are present quantities. The XRD test was then used to determine the mineralogical composition of bulk components, as well as the clay fraction. The XRD patterns indicated the presence of dominant amount of quartz and plagioclase, with moderate to minor amounts of alkali feldspar, anhydrite, carbonates (calcite and dolomite, hematite and clay minerals. The most common clays in the Shurijeh Formation were illite, chlorite, and kaolinite. However, in very few samples, glauconite, smectite, and mixed layer clay minerals of both illite-smectite and chlorite-smectite types were also recognized. The XRD results were quantified, using the elemental information from the XRF test, showing that each Shurijeh exhibited low to moderate amounts of clay minerals, typically up to 21%. The amount of illite, the most dominant clay mineral, reached maximum of 13.5%, while the other clay types were significantly smaller. Based on the use of SEM and thermal data, the results of the identification of clay minerals, corresponded with the powder X-ray diffraction analysis, which can be taken into account as an evidence of the effectiveness of the thermal analysis technique in clay typing, as a complementary method besides the XRD.

  12. SEM microcharacterization of semiconductors

    CERN Document Server

    Holt, D B

    1989-01-01

    Applications of SEM techniques of microcharacterization have proliferated to cover every type of material and virtually every branch of science and technology. This book emphasizes the fundamental physical principles. The first section deals with the foundation of microcharacterization in electron beam instruments and the second deals with the interpretation of the information obtained in the main operating modes of a scanning electron microscope.

  13. Thermal Conductivity Analysis and Lifetime Testing of Suspension Plasma-Sprayed Thermal Barrier Coatings

    Directory of Open Access Journals (Sweden)

    Nicholas Curry

    2014-08-01

    Full Text Available Suspension plasma spraying (SPS has become an interesting method for the production of thermal barrier coatings for gas turbine components. The development of the SPS process has led to structures with segmented vertical cracks or column-like structures that can imitate strain-tolerant air plasma spraying (APS or electron beam physical vapor deposition (EB-PVD coatings. Additionally, SPS coatings can have lower thermal conductivity than EB-PVD coatings, while also being easier to produce. The combination of similar or improved properties with a potential for lower production costs makes SPS of great interest to the gas turbine industry. This study compares a number of SPS thermal barrier coatings (TBCs with vertical cracks or column-like structures with the reference of segmented APS coatings. The primary focus has been on lifetime testing of these new coating systems. Samples were tested in thermo-cyclic fatigue at temperatures of 1100 °C for 1 h cycles. Additional testing was performed to assess thermal shock performance and erosion resistance. Thermal conductivity was also assessed for samples in their as-sprayed state, and the microstructures were investigated using SEM.

  14. Influence of hydroxyapatite granule size, porosity, and crystallinity on tissue reaction in vivo. Part A: synthesis, characterization of the materials, and SEM analysis.

    Science.gov (United States)

    Maté Sánchez de Val, José E; Calvo-Guirado, José L; Gómez-Moreno, Gerardo; Pérez-Albacete Martínez, Carlos; Mazón, Patricia; De Aza, Piedad N

    2016-11-01

    The aim of this study was the synthesis and analysis of the tissue reaction to three different Hydroxyapatite (HA)-based bone substitute materials differing only in granule size, porosity, and crystallinity through an animal experimental model at 60 days. Three different HA-based biomaterials were synthesized and characterized by X-ray diffraction, SEM, and EDS analysis, the resultant product was ground in three particle sizes: Group I (2000-4000 μm), Group II (1000-2000 μm), and Group III (600-1000 μm). Critical size defects were created in both tibias of 15 rabbits. Four defects per rabbit for a total of 60 defects were grafted with the synthesized materials as follows: Group I (15 defects), Group II (15 defects), Group III (15 defects), and empty (15 defects control). After animals sacrifice at 60 days samples were obtained and processed for SEM and EDS evaluation of Ca/P ratios, elemental mapping was performed to determine the chemical degradation process and changes to medullary composition in all the four study groups. The tendency for the density was to increase with the increasing annealing temperature; in this way it was possible to observe that the sample that shows highest crystallinity and crystal size corresponding to that of group I. The SEM morphological examination showed that group III implant showed numerous resorption regions, group II implant presented an average resorption rate of all the implants. The group I displayed smoother surface features, in comparison with the other two implants. The data from this study show that changing the size, porosity, and crystallinity of one HA-based bone substitute material can influence the integration of the biomaterials within the implantation site and the new bone formation. © 2015 John Wiley & Sons A/S. Published by John Wiley & Sons Ltd.

  15. Ninth Thermal and Fluids Analysis Workshop Proceedings

    Science.gov (United States)

    Sakowski, Barbara (Compiler)

    1999-01-01

    The Ninth Thermal and Fluids Analysis Workshop (TFAWS 98) was held at the Ohio Aerospace Institute in Cleveland, Ohio from August 31 to September 4, 1998. The theme for the hands-on training workshop and conference was "Integrating Computational Fluid Dynamics and Heat Transfer into the Design Process." Highlights of the workshop (in addition to the papers published herein) included an address by the NASA Chief Engineer, Dr. Daniel Mulville; a CFD short course by Dr. John D. Anderson of the University of Maryland; and a short course by Dr. Robert Cochran of Sandia National Laboratories. In addition, lectures and hands-on training were offered in the use of several cutting-edge engineering design and analysis-oriented CFD and Heat Transfer tools. The workshop resulted in international participation of over 125 persons representing aerospace and automotive industries, academia, software providers, government agencies, and private corporations. The papers published herein address issues and solutions related to the integration of computational fluid dynamics and heat transfer into the engineering design process. Although the primary focus is aerospace, the topics and ideas presented are applicable to many other areas where these and other disciplines are interdependent.

  16. Analysis of thermal power calibration method

    International Nuclear Information System (INIS)

    Zagar, T.; Ravnik, M.; Persic, A.

    2000-01-01

    The methods for determining fuel element burnup have recently become interesting because of activities related to the shipment of highly enriched fuel elements back to the United States for final disposal before 2009. The most common and practical method for determining fuel element burnup in research reactors is reactor calculation. Experience has shown that burnup calculations become complicated and biased with uncertainties if a long period of reactor operation must be reproduced. Besides this, accuracy of calculated burnup is always limited with accuracy of reactor power calibration, since burnup calculation is based on calculated power density distribution, which is usually expressed in terms of power released per fuel element and normalised to the reactor power It is obvious that reactor thermal power calibration is very important for precise fuel element burnup calculation. Calculated fuel element burnup is linearly dependent on the thermal reactor power. The reactor power level may be determined from measured absolute thermal flux distribution across the core in the horizontal and vertical planes. Flux distributions are measured with activation of cadmium covered and bare foils irradiated by the steady reactor power. But it should be realised that this method is time consuming and not accurate. This method is practical only for zero power reactors and is in practice very seldom performed for other reactors (e.g. for TRIGA reactor in Ljubljana absolute thermal flux distribution was not performed since reactor reconstruction in 1991). In case of power reactors and research reactors in which a temperature rise across the core is produced and measured than a heat balance method is the most common and accurate method of determining the power output of the core. The purpose of this paper is to analyse the accuracy of calorimetric reactor power calibration method and to analyse the influence of control rod position on nuclear detector reading for TRIGA reactors

  17. Differential-thermal analysis of irradiated lignite

    International Nuclear Information System (INIS)

    Chichek, F.; Eyubova, N.

    2006-01-01

    Full text: In this theme our purpose is to explain thermo-differential analysis of lignites irradiated. During experiment Caraman Ermenek (washed), Caraman Ermenek (crude), Nevshehir (crude), Slopi (crude), Trakya Harman (washed) lignite coals were used. Five of five kinds of coal samples with 3mm and 1gr of each sample were obtained. Then they were filled into the Tubes after having dried total 25 samples with 1 gr at 1000 degrees temperature for one hour. Air in the tubes was pumped out and closed. Coal samples in vacuum medium were irradiated by gamma rays of Co60 at 5.5 kGy, 19.2 kGy, 65.7 kGy, 169.6 kGy, 411.2 kGy doses to the normal conditions. Then differential thermal analysis was carried out both in original and the samples irradiated. Argon gas was used to make inert medium in the camera. T=200-8500 degrees temperature was selected. At the experiment done from 1000-1300 degrees temperatures too great endothermic reaction pick was begun to form by being observed thermal changings. At 3000-4200 degrees temperature exothermic reaction picks and at 7000 degrees parallel exothermic reaction picks were observed. Initial endothermic and exothermic reaction picks in five lignite samples were observed like a sharp curve. At the end coal irradiated samples were compared with original coal samples. At the result of experiment it was revealed that in comparison with original coal samples coal samples irradiated form exothermic and endothermic curves at very reaction pick and temperature intervals of these pick were large. Besides loss of weight was observed to begin at low temperatures in samples irradiated and especially momentary weight loss at some heats in the rang of known temperatures was observed in the coal Slopi contain in bitumen. Because of heat the weigh loss in the non irradiated samples forms parabolic curve and because of heat the weight loss in the samples irradiated forms stepped curves. It has shown that the coal irradiated can be easily departed by

  18. Characterisation of heavy metal-bearing phases in stream sediments of the Meza River Valley, Slovenia, by means of SEM/EDS analysis

    International Nuclear Information System (INIS)

    Miler, M; Gosar, M

    2010-01-01

    Stream sediment reflects the rock structure of the catchment area, its geochemical characteristics and possible recent contamination upstream of the sampling point and thus, it is most frequently used in geochemical researches of heavy metal pollution. Stream sediment samples were collected along the Mez'a River and its tributaries and the Drava River, located in the NNE part of Slovenia. Previous geochemical studies have shown that these sediments are heavily polluted with heavy metals as a consequence of past mining of Pb-Zn ore and steelworks activities. Conventional geochemical analyses (ICP-MS, AAS, etc.) provided limited information on mineralogy, morphology and sources of heavy metal-bearing phases therefore SEM/EDS was utilized. Several problems were confronted with during EDS analysis, which are related to identification and quantification of light elements, identification of elements due to peak overlaps and quantification of spectra from unpolished samples. These problems were successfully dealt with. SEM/EDS enabled successful identification of heavy metal-bearing phases in stream sediments. Ore mineral phases, such as cerussite, sphalerite, smithsonite and galena, different heavy metal-bearing Fe-alloys, Fe-oxides and spherical particles and common rock-forming and accessory mineral phases, such as barite, rutile, ilmenite, zircon and monazite, were identified using solely SEM/EDS. These results were used for subsequent geochemical interpretation and source apportionment of heavy metals, according to associations of different heavy metal-bearing phases. Heavy metal-bearing phases were arranged by their source and genesis into three groups, denoted as geogenic/technogenic, technogenic and geogenic.

  19. Characterisation of heavy metal-bearing phases in stream sediments of the Meža River Valley, Slovenia, by means of SEM/EDS analysis

    Science.gov (United States)

    Miler, M.; Gosar, M.

    2010-02-01

    Stream sediment reflects the rock structure of the catchment area, its geochemical characteristics and possible recent contamination upstream of the sampling point and thus, it is most frequently used in geochemical researches of heavy metal pollution. Stream sediment samples were collected along the Meža River and its tributaries and the Drava River, located in the NNE part of Slovenia. Previous geochemical studies have shown that these sediments are heavily polluted with heavy metals as a consequence of past mining of Pb-Zn ore and steelworks activities. Conventional geochemical analyses (ICP-MS, AAS, etc.) provided limited information on mineralogy, morphology and sources of heavy metal-bearing phases therefore SEM/EDS was utilized. Several problems were confronted with during EDS analysis, which are related to identification and quantification of light elements, identification of elements due to peak overlaps and quantification of spectra from unpolished samples. These problems were successfully dealt with. SEM/EDS enabled successful identification of heavy metal-bearing phases in stream sediments. Ore mineral phases, such as cerussite, sphalerite, smithsonite and galena, different heavy metal-bearing Fe-alloys, Fe-oxides and spherical particles and common rock-forming and accessory mineral phases, such as barite, rutile, ilmenite, zircon and monazite, were identified using solely SEM/EDS. These results were used for subsequent geochemical interpretation and source apportionment of heavy metals, according to associations of different heavy metal-bearing phases. Heavy metal-bearing phases were arranged by their source and genesis into three groups, denoted as geogenic/technogenic, technogenic and geogenic.

  20. Comparison of Enamel Morphologic Characteristics after Conditioning with Various Combinations of Acid Etchant and Er:YAG Laser in Bonding and Rebonding Procedures: A SEM Analysis

    Directory of Open Access Journals (Sweden)

    Mohammad Sadegh Ahmad Akhoundi

    2017-10-01

    Full Text Available Objectives: Many studies have evaluated re-etched enamel by using scanning electron microscopy (SEM; however, there is no evidence regarding the use of Erbium-doped yttrium aluminium garnet (Er:YAG laser at primary and secondary bonding instead of acid etching with regards to enamel surface changes. The purpose of the present study was to determine that whether or not the methods of primary and secondary enamel preparation affect enamel characteristics after rebonding, by using SEM analysis.Materials and Methods: Twelve freshly extracted premolars were divided into 4 groups. The samples in each group were conditioned by acid etchant or Er:YAG laser at primary conditioning, according to the instructions. Afterwards, they were bonded with orthodontic brackets. After debonding, the samples were prepared for second conditioning. Also, two samples were conditioned only once with acid etchant or laser, to compare enamel morphology changes with those after re-etching. Finally, buccal enamel surfaces were evaluated using SEM.Results: Enamel etching patterns were observed in the samples which had been acid-conditioned at first or at both conditionings. The samples irradiated by Er:YAG laser showed amorphous and irregular surfaces, with no signs of typical etching patterns. A large deep gap was seen in one of the samples irradiated with laser at primary and secondary conditionings, which might have penetrated the underling layers of enamel and dentin.Conclusions: Enamel surface preparation with Er:YAG laser produces irregular and indistinct morphologic changes, completely different from those produced after acid etching at both conditioning and reconditioning. Therefore, it is recommended to use this laser with caution to avoid permanent enamel damage.

  1. Analysis of Non-contact Acousto Thermal Signature Data (Postprint)

    Science.gov (United States)

    2016-02-01

    AFRL-RX-WP-JA-2016-0321 ANALYSIS OF NON-CONTACT ACOUSTO-THERMAL SIGNATURE DATA (POSTPRINT) Amanda K. Criner AFRL/RX...October 2014 – 16 September 2015 4. TITLE AND SUBTITLE ANALYSIS OF NON-CONTACT ACOUSTO-THERMAL SIGNATURE DATA (POSTPRINT) 5a. CONTRACT NUMBER...words) The non-contact acousto-thermal signature (NCATS) is a nondestructive evaluation technique with potential to detect fatigue in materials such as

  2. Quantitative analysis of thermal insulation coatings

    DEFF Research Database (Denmark)

    Kiil, Søren

    2014-01-01

    This work concerns the development of simulation tools for mapping of insulation properties of thermal insulation coatings based on selected functional filler materials. A mathematical model, which includes the underlying physics (i.e. thermal conductivity of a heterogeneous two-component coating...

  3. Space Experiment Module (SEM)

    Science.gov (United States)

    Brodell, Charles L.

    1999-01-01

    The Space Experiment Module (SEM) Program is an education initiative sponsored by the National Aeronautics and Space Administration (NASA) Shuttle Small Payloads Project. The program provides nationwide educational access to space for Kindergarten through University level students. The SEM program focuses on the science of zero-gravity and microgravity. Within the program, NASA provides small containers or "modules" for students to fly experiments on the Space Shuttle. The experiments are created, designed, built, and implemented by students with teacher and/or mentor guidance. Student experiment modules are flown in a "carrier" which resides in the cargo bay of the Space Shuttle. The carrier supplies power to, and the means to control and collect data from each experiment.

  4. Micro-thermal analysis of polyester coatings

    Science.gov (United States)

    Fischer, Hartmut R.

    2010-04-01

    The application and suitability of micro-thermal analysis to detect changes in the chemical and physical properties of coating due to ageing and especially photo-degradation is demonstrated using a model polyester coating based on neopentyl glycol isophthalic acid. The changes in chemical structure like chain scission and cross-linking are manifested by a shift of the LTA detectable Tg and by a change of the slope of the part of the LTA graph responsible for the penetration of the hot sensor into the material after passing the glass transition temperature. As such LTA is a valuable tool to have a quick look into coating surfaces and especially their ageing. The photo-degradation of polyester in air leads to the formation of a cross-linked network at a surface layer of about 3-4 μm coupled with an increase in hardness and of the glass transition temperature by ˜90 K, the effect is less drastic for a photo-degradation in a nitrogen environment. Moreover, the presence of a non-equilibrium dense surface layer with a higher Tg formed during the drying of the coating formulation and the film solidification can be shown.

  5. Pharmaceutical applications of dynamic mechanical thermal analysis.

    Science.gov (United States)

    Jones, David S; Tian, Yiwei; Abu-Diak, Osama; Andrews, Gavin P

    2012-04-01

    The successful development of polymeric drug delivery and biomedical devices requires a comprehensive understanding of the viscoleastic properties of polymers as these have been shown to directly affect clinical efficacy. Dynamic mechanical thermal analysis (DMTA) is an accessible and versatile analytical technique in which an oscillating stress or strain is applied to a sample as a function of oscillatory frequency and temperature. Through cyclic application of a non-destructive stress or strain, a comprehensive understanding of the viscoelastic properties of polymers may be obtained. In this review, we provide a concise overview of the theory of DMTA and the basic instrumental/operating principles. Moreover, the application of DMTA for the characterization of solid pharmaceutical and biomedical systems has been discussed in detail. In particular we have described the potential of DMTA to measure and understand relaxation transitions and miscibility in binary and higher-order systems and describe the more recent applications of the technique for this purpose. © 2011 Elsevier B.V. All rights reserved.

  6. THERMAL HYDRAULIC ANALYSIS OF FIRE DIVERTOR

    International Nuclear Information System (INIS)

    C.B. bAXI; M.A. ULRICKSON; D.E. DRIMEYER; P. HEITZENROEDER

    2000-01-01

    The Fusion Ignition Research Experiment (FIRE) is being designed as a next step in the US magnetic fusion program. The FIRE tokamak has a major radius of 2 m, a minor radius of 0.525 m, and liquid nitrogen cooled copper coils. The aim is to produce a pulse length of 20 s with a plasma current of 6.6 MA and with alpha dominated heating. The outer divertor and baffle of FIRE are water cooled. The worst thermal condition for the outer divertor and baffle is the baseline D-T operating mode (10 T, 6.6 MA, 20 s) with a plasma exhaust power of 67 MW and a peak heat flux of 20 MW/m 2 . A swirl tape (ST) heat transfer enhancement method is used in the outer divertor cooling channels to increase the heat transfer coefficient and the critical heat flux (CHF). The plasma-facing surface consists of tungsten brush. The finite element (FE) analysis shows that for an inlet water temperature of 30 C, inlet pressure of 1.5 MPa and a flow velocity of 10 m/s, the incident critical heat flux is greater than 30 MW/m 2 . The peak copper temperature is 490 C, peak tungsten temperature is 1560 C, and the pressure drop is less than 0.5 MPa. All these results fulfill the design requirements

  7. Compatibility analysis of DUPIC fuel(4) - thermal hydraulic analysis

    Energy Technology Data Exchange (ETDEWEB)

    Park, Jee Won; Chae, Kyung Myung; Choi, Hang Bok

    2000-07-01

    Thermal-hydraulic compatibility of the DUPIC fuel bundle in the CANDU reactor has been studied. The critical channel power, the critical power ratio, the channel exit quality and the channel flow are calculated for the DUPIC and the standard fuels by using the NUCIRC code. The physical models and associated parametric values for the NUCIRC analysis of the fuels are also presented. Based upon the slave channel analysis, the critical channel power and the critical power ratios have been found to be very similar for the two fuel types. The same dryout model is used in this study for the standard and the DUPIC fuel bundles. To assess the dryout characteristics of the DUPIC fuel bundle, the ASSERT-PV code has been used for the subchannel analysis. Based upon the results of the subchannel analysis, it is found that the dryout location and the power for the two fuel types are indeed very similar. This study shows that thermal performance of the DUPIC fuel is not significantly different from that of the standard fuel.

  8. Thermal analysis methods in the characterization of photocatalytic titania precursors

    Czech Academy of Sciences Publication Activity Database

    Pulišová, Petra; Večerníková, Eva; Maříková, Monika; Balek, V.; Boháček, Jaroslav; Šubrt, Jan

    2012-01-01

    Roč. 108, č. 2 (2012), s. 489-492 ISSN 1388-6150 R&D Projects: GA MŠk 1M0577 Institutional research plan: CEZ:AV0Z40320502 Keywords : differential thermal analysis * thermogravimetry * emanation thermal analysis * titanium dioxide * photocatalyst Subject RIV: CA - Inorganic Chemistry Impact factor: 1.982, year: 2012

  9. An Integrated Approach to Thermal Analysis of Pharmaceutical Solids

    Science.gov (United States)

    Riley, Shelley R. Rabel

    2015-01-01

    A three-tiered experiment for undergraduate Instrumental Analysis students is presented in which students characterize the solid-state thermal behavior of an active pharmaceutical ingredient (acetaminophen) and excipient (a-lactose hydrate) using differential scanning calorimetry, thermogravimetric analysis, and thermal microscopy. Students are…

  10. Performance testing of thermal analysis codes for nuclear fuel casks

    International Nuclear Information System (INIS)

    Sanchez, L.C.

    1987-01-01

    In 1982 Sandia National Laboratories held the First Industry/Government Joint Thermal and Structural Codes Information Exchange and presented the initial stages of an investigation of thermal analysis computer codes for use in the design of nuclear fuel shipping casks. The objective of the investigation was to (1) document publicly available computer codes, (2) assess code capabilities as determined from their user's manuals, and (3) assess code performance on cask-like model problems. Computer codes are required to handle the thermal phenomena of conduction, convection and radiation. Several of the available thermal computer codes were tested on a set of model problems to assess performance on cask-like problems. Solutions obtained with the computer codes for steady-state thermal analysis were in good agreement and the solutions for transient thermal analysis differed slightly among the computer codes due to modeling differences

  11. Thermal and Alignment Analysis of the Instrument-Level ATLAS Thermal Vacuum Test

    Science.gov (United States)

    Bradshaw, Heather

    2012-01-01

    This paper describes the thermal analysis and test design performed in preparation for the ATLAS thermal vacuum test. NASA's Advanced Topographic Laser Altimeter System (ATLAS) will be flown as the sole instrument aboard the Ice, Cloud, and land Elevation Satellite-2 (ICESat-2). It will be used to take measurements of topography and ice thickness for Arctic and Antarctic regions, providing crucial data used to predict future changes in worldwide sea levels. Due to the precise measurements ATLAS is taking, the laser altimeter has very tight pointing requirements. Therefore, the instrument is very sensitive to temperature-induced thermal distortions. For this reason, it is necessary to perform a Structural, Thermal, Optical Performance (STOP) analysis not only for flight, but also to ensure performance requirements can be operationally met during instrument-level thermal vacuum testing. This paper describes the thermal model created for the chamber setup, which was used to generate inputs for the environmental STOP analysis. This paper also presents the results of the STOP analysis, which indicate that the test predictions adequately replicate the thermal distortions predicted for flight. This is a new application of an existing process, as STOP analyses are generally performed to predict flight behavior only. Another novel aspect of this test is that it presents the opportunity to verify pointing results of a STOP model, which is not generally done. It is possible in this case, however, because the actual pointing will be measured using flight hardware during thermal vacuum testing and can be compared to STOP predictions.

  12. Thermal Analysis of Sintered Silver Nanoparticles Film

    Directory of Open Access Journals (Sweden)

    M. Keikhaie

    2014-07-01

    Full Text Available Thin bonded films have many applications in antireflection and reflection coating, insulating and conducting films and semiconductor industries. Thermal conductivity is one of the most important parameter for power packaging since the thermal resistance of the interconnections is directly related to the heat removal capability and thermal management of the power package. The defects in materials play very important role on the effective thermal conductivity. In this paper, finite element method (FEM was utilized to simulate the effect of pores on the effective thermal conductivity of sintered silver nanoparticles film. The simulation results indicate that the effective thermal conductivity of film is different at different directions and would be enhanced when the pore angle is 90. The simulation results will help us to further understand the heat transfer process across highly porous structures and will provide us a powerful guide to design coating with high thermal insulation or conductor property. Because of there is no similar experimental data for this simulation results, this paper is a comparative work among three different models.

  13. Chemical and structural analysis of the bone-implant interface by TOF-SIMS, SEM, FIB and TEM: Experimental study in animal

    International Nuclear Information System (INIS)

    Palmquist, Anders; Emanuelsson, Lena; Sjövall, Peter

    2012-01-01

    Although bone-anchored implants are widely used in reconstructive medicine, the mechanism of osseointegration is still not fully understood. Novel analytical tools are needed to further understand this process, where both the chemical and structural aspects of the bone-implant interface are important. The aim of this study was to evaluate the advantages of combining time-of-flight secondary ion mass spectroscopy (TOF-SIMS) with optical (LM), scanning (SEM) and transmission electron microscopy (TEM) techniques for studying the bone-implant interface of bone-anchored implants. Laser-modified titanium implants with surrounded bone retrieved after 8 weeks healing in rabbit were dehydrated and resin embedded. Three types of sample preparation were studied to evaluate the information gained by combining TOF-SIMS, SEM, FIB and TEM. The results show that imaging TOF-SIMS can provide detailed chemical information, which in combination with structural information from microscopy methods provide a more complete characterization of anatomical structures at the bone-implant interface. By investigating various sample preparation techniques, it is shown that grinded cross section samples can be used for chemical imaging using TOF-SIMS, if careful consideration of potential preparation artifacts is taken into account. TOF-SIMS analysis of FIB-prepared bone/implant cross section samples show distinct areas corresponding to bone tissue and implant with a sharp interface, although without chemical information about the organic components.

  14. Thermal and Structural Analysis of FIMS Grating

    Directory of Open Access Journals (Sweden)

    K.-I. Seon

    2001-06-01

    Full Text Available Far ultraviolet IMaging Spectrograph (FIMS should be designed to maintain its structural stability and to minimize optical performance degradation in launch and in operation enviroments. The structural and thermal analyzes of grating and grating mount system, which are directly related to FIMS optical performance, was performed using finite element method. The grating mount was made to keep the grating stress down, while keeping the natural frequency of the grating mount higher than 100 Hz. Transient and static thermal analyzes were also performed and the results shows that the thermal stress on the grating can be attenuated sufficiently The optical performance variation due to temperature variation was within the allowed range.

  15. Thermal analysis and design of passive solar buildings

    CERN Document Server

    Athienitis, AK

    2013-01-01

    Passive solar design techniques are becoming increasingly important in building design. This design reference book takes the building engineer or physicist step-by-step through the thermal analysis and design of passive solar buildings. In particular it emphasises two important topics: the maximum utilization of available solar energy and thermal storage, and the sizing of an appropriate auxiliary heating/cooling system in conjunction with good thermal control.Thermal Analysis and Design of Passive Solar Buildings is an important contribution towards the optimization of buildings as systems th

  16. Thermal creep force: analysis and application

    OpenAIRE

    Wolfe, David M.

    2016-01-01

    Approved for public release; distribution is unlimited The existence of two motive forces on a Crookes radiometer has complicated the investigation of either force independently. The thermal creep shear force, in particular, has been subject to differing interpretations of the direction in which it acts and its order of magnitude. A horizontal vane radiometer design is provided, which isolates the thermal creep shear force. The horizontal vane radiometer is explored through experiment, kin...

  17. Finite Element Analysis of Interfacial Debonding in Copper/Diamond Composites for Thermal Management Applications.

    Science.gov (United States)

    Zain-Ul-Abdein, Muhammad; Ijaz, Hassan; Saleem, Waqas; Raza, Kabeer; Mahfouz, Abdullah Salmeen Bin; Mabrouki, Tarek

    2017-07-02

    Copper/diamond (Cu/D) composites are famous in thermal management applications for their high thermal conductivity values. They, however, offer some interface related problems like high thermal boundary resistance and excessive debonding. This paper investigates interfacial debonding in Cu/D composites subjected to steady-state and transient thermal cyclic loading. A micro-scale finite element (FE) model was developed from a SEM image of the Cu/20 vol % D composite sample. Several test cases were assumed with respect to the direction of heat flow and the boundary interactions between Cu/uncoated diamonds and Cu/Cr-coated diamonds. It was observed that the debonding behavior varied as a result of the differences in the coefficients of thermal expansions (CTEs) among Cu, diamond, and Cr. Moreover, the separation of interfaces had a direct influence upon the equivalent stress state of the Cu-matrix, since diamond particles only deformed elastically. It was revealed through a fully coupled thermo-mechanical FE analysis that repeated heating and cooling cycles resulted in an extremely high stress state within the Cu-matrix along the diamond interface. Since these stresses lead to interfacial debonding, their computation through numerical means may help in determining the service life of heat sinks for a given application beforehand.

  18. SEM-based characterization techniques

    International Nuclear Information System (INIS)

    Russell, P.E.

    1986-01-01

    The scanning electron microscope is now a common instrument in materials characterization laboratories. The basic role of the SEM as a topographic imaging system has steadily been expanding to include a variety of SEM-based analytical techniques. These techniques cover the range of basic semiconductor materials characterization to live-time device characterization of operating LSI or VLSI devices. This paper introduces many of the more commonly used techniques, describes the modifications or additions to a conventional SEM required to utilize the techniques, and gives examples of the use of such techniques. First, the types of signals available from a sample being irradiated by an electron beam are reviewed. Then, where applicable, the type of spectroscopy or microscopy which has evolved to utilize the various signal types are described. This is followed by specific examples of the use of such techniques to solve problems related to semiconductor technology. Techniques emphasized include: x-ray fluorescence spectroscopy, electron beam induced current (EBIC), stroboscopic voltage analysis, cathodoluminescnece and electron beam IC metrology. Current and future trends of some of the these techniques, as related to the semiconductor industry are discussed

  19. Acoustic Emission Analysis of Damage Progression in Thermal Barrier Coatings Under Thermal Cyclic Conditions

    Science.gov (United States)

    Appleby, Matthew; Zhu, Dongming; Morscher, Gregory

    2015-01-01

    Damage evolution of electron beam-physical vapor deposited (EBVD-PVD) ZrO2-7 wt.% Y2O3 thermal barrier coatings (TBCs) under thermal cyclic conditions was monitored using an acoustic emission (AE) technique. The coatings were heated using a laser heat flux technique that yields a high reproducibility in thermal loading. Along with AE, real-time thermal conductivity measurements were also taken using infrared thermography. Tests were performed on samples with induced stress concentrations, as well as calcium-magnesium-alumino-silicate (CMAS) exposure, for comparison of damage mechanisms and AE response to the baseline (as-produced) coating. Analysis of acoustic waveforms was used to investigate damage development by comparing when events occurred, AE event frequency, energy content and location. The test results have shown that AE accumulation correlates well with thermal conductivity changes and that AE waveform analysis could be a valuable tool for monitoring coating degradation and provide insight on specific damage mechanisms.

  20. Thermal analysis of annular fins with temperature-dependent thermal properties

    Institute of Scientific and Technical Information of China (English)

    I. G. AKSOY

    2013-01-01

    The thermal analysis of the annular rectangular profile fins with variable thermal properties is investigated by using the homotopy analysis method (HAM). The thermal conductivity and heat transfer coefficient are assumed to vary with a linear and power-law function of temperature, respectively. The effects of the thermal-geometric fin parameter and the thermal conductivity parameter variations on the temperature distribution and fin efficiency are investigated for different heat transfer modes. Results from the HAM are compared with numerical results of the finite difference method (FDM). It can be seen that the variation of dimensionless parameters has a significant effect on the temperature distribution and fin efficiency.

  1. Study of selection and purification of Brazilian bentonite clay by elutriation: a XRF, SEM and Rietveld analysis

    Energy Technology Data Exchange (ETDEWEB)

    Alves, J.L.; Zanini, A.E.; Souza, M.E. de; Nascimento, M.L.F., E-mail: jeff_eq@yahoo.com.br, E-mail: mlfn@ufba.br [Universidade Federal da Bahia (UFBA/PROTEC/PEI), Salvador, BA (Brazil). Departamento de Engenharia Quimica

    2016-01-15

    Clays obtained from nature have a lot of impurities. Therefore, for best using of these materials, it is necessary its selection and purification. Thus, the aim of this work is to separate and to purify the smectite fractions using water as a solvent at a low flux mixed with a bentonite clay extracted from a mine in Vitoria da Conquista - Bahia / Brazil. For this a separation method of fractions of expandable clays based on the Stokes' Law was applied - this process is called elutriation, in order to ensure and to expand possible industrial applications of this material. The samples were characterized by analysis of X-ray diffraction, X-ray fluorescence and scanning electron microscopy. The Rietveld method enabled the quantification of main phase minerals: montmorillonite, kaolinite, nontronite and quartz, reaching 85% in mass of montmorillonite phase at the end of the process. Results showed that the method used was efficient to remove almost all quartz, carbonates and organic matter from the sample. It was also observed a monomodal grain size distribution of elutriated materials with thinner grains, around (18.1 ± 1.8) μm at the end of the process. It has been concluded that the method developed and applied showed promising characters to be applied to elutriate kilograms of clays and could be used in industrial scale. (author)

  2. Study of selection and purification of Brazilian bentonite clay by elutriation: a XRF, SEM and Rietveld analysis

    Directory of Open Access Journals (Sweden)

    J. L. Alves

    2016-03-01

    Full Text Available Abstract Clays obtained from nature have a lot of impurities. Therefore, for best using of these materials, it is necessary its selection and purification. Thus, the aim of this work is to separate and to purify the smectite fractions using water as a solvent at a low flux mixed with a bentonite clay extracted from a mine in Vitória da Conquista - Bahia / Brazil. For this a separation method of fractions of expandable clays based on the Stokes' Law was applied - this process is called elutriation, in order to ensure and to expand possible industrial applications of this material. The samples were characterized by analysis of X-ray diffraction, X-ray fluorescence and scanning electron microscopy. The Rietveld method enabled the quantification of main phase minerals: montmorillonite, kaolinite, nontronite and quartz, reaching 85% in mass of montmorillonite phase at the end of the process. Results showed that the method used was efficient to remove almost all quartz, carbonates and organic matter from the sample. It was also observed a monomodal grain size distribution of elutriated materials with thinner grains, around (18.1 ± 1.8 μm at the end of the process. It has been concluded that the method developed and applied showed promising characters to be applied to elutriate kilograms of clays and could be used in industrial scale.

  3. Study of selection and purification of Brazilian bentonite clay by elutriation: a XRF, SEM and Rietveld analysis

    International Nuclear Information System (INIS)

    Alves, J.L.; Zanini, A.E.; Souza, M.E. de; Nascimento, M.L.F.

    2016-01-01

    Clays obtained from nature have a lot of impurities. Therefore, for best using of these materials, it is necessary its selection and purification. Thus, the aim of this work is to separate and to purify the smectite fractions using water as a solvent at a low flux mixed with a bentonite clay extracted from a mine in Vitoria da Conquista - Bahia / Brazil. For this a separation method of fractions of expandable clays based on the Stokes' Law was applied - this process is called elutriation, in order to ensure and to expand possible industrial applications of this material. The samples were characterized by analysis of X-ray diffraction, X-ray fluorescence and scanning electron microscopy. The Rietveld method enabled the quantification of main phase minerals: montmorillonite, kaolinite, nontronite and quartz, reaching 85% in mass of montmorillonite phase at the end of the process. Results showed that the method used was efficient to remove almost all quartz, carbonates and organic matter from the sample. It was also observed a monomodal grain size distribution of elutriated materials with thinner grains, around (18.1 ± 1.8) μm at the end of the process. It has been concluded that the method developed and applied showed promising characters to be applied to elutriate kilograms of clays and could be used in industrial scale. (author)

  4. O Cinema sem Imagens

    Directory of Open Access Journals (Sweden)

    Paulo Andrade

    2001-12-01

    Full Text Available A obra cinematográfica de Marguerite Duras, praticamente desconhecida pelo grande público, estabeleça intricadas relações com sua obra literária, ao promover a indiscernibilidade entre os dois campo, sem, contudo, instituir qualquer tipo de subordinação de um ao outro. O processo de criação do filme Lê camion, de 1977, aponta para outras possibilidades de se pensar o cinema e a literatura.

  5. Interrelation of Sport Participation, Physical Activity, Social Capital and Mental Health in Disadvantaged Communities: A SEM-Analysis.

    Science.gov (United States)

    Marlier, Mathieu; Van Dyck, Delfien; Cardon, Greet; De Bourdeaudhuij, Ilse; Babiak, Kathy; Willem, Annick

    2015-01-01

    The Health through Sport conceptual model links sport participation with physical, social and psychological outcomes and stresses the need for more understanding between these outcomes. The present study aims to uncover how sport participation, physical activity, social capital and mental health are interrelated by examining these outcomes in one model. A cross-sectional survey was conducted in nine disadvantaged communities in Antwerp (Belgium). Two hundred adults (aged 18-56) per community were randomly selected and visited at home to fill out a questionnaire on socio-demographics, sport participation, physical activity, social capital and mental health. A sample of 414 adults participated in the study. Structural Equation Modeling analysis showed that sport participation (β = .095) and not total physical activity (β = .027) was associated with better mental health. No association was found between sport participation and community social capital (β = .009) or individual social capital (β = .045). Furthermore, only community social capital was linked with physical activity (β = .114), individual social capital was not (β = -.013). In contrast, only individual social capital was directly associated with mental health (β = .152), community social capital was not (β = .070). This study emphasizes the importance of sport participation and individual social capital to improve mental health in disadvantaged communities. It further gives a unique insight into the functionalities of how sport participation, physical activity, social capital and mental health are interrelated. Implications for policy are that cross-sector initiatives between the sport, social and health sector need to be supported as their outcomes are directly linked to one another.

  6. Craniotomia sem tricotomia: avaliação de 640 casos Craniotomy without tricotomy: analysis of 640 cases

    Directory of Open Access Journals (Sweden)

    Amylcar E. Dvilevicius

    2004-03-01

    Full Text Available A remoção do cabelo para realização de craniotomia utilizada rotineiramente na maioria dos serviços de neurocirurgia para procedimentos cranianos diversos questionada em sua necessidade a partir da avaliação retrospectiva de 640 pacientes submetidos a cirurgias cranianas, em que foi observada uma porcentagem de infecção de ferida cirúrgica de 1,09 %, não superior àquelas com tricotomia revisadas na literatura. Nos 7 casos com infecção, 3 pacientes foram submetidos a derivações liquóricas, 3 pacientes eram vítimas de traumatismo crânio-encefálico e uma paciente substituida a craniotomia para tratamento de tumor cerebral. A técnica para preservação e manuseio do cabelo, suas vantagens e desvantagens são descritas e discutidas.The hair shaving in preparation for neurosurgeris frequently used in most of neurosurgical centers to perform craniotomy. We question about its necessity after our retrospective analysis of 640 patients undergoing cranial procedures without previous hair shaving. We had the overall surgical wound infection rate of 1.09%, not higher than tricotomy in the review of the literature. In 7 cases with infection, 3 patients were undergoing to CSF shunts, 3 patients had head injury, and one had brain tumor. The technique for preparing skin and hair for cranial procedures, its advantages and disvantages are described and discussed.

  7. Interrelation of Sport Participation, Physical Activity, Social Capital and Mental Health in Disadvantaged Communities: A SEM-Analysis

    Science.gov (United States)

    Marlier, Mathieu; Van Dyck, Delfien; Cardon, Greet; De Bourdeaudhuij, Ilse; Babiak, Kathy; Willem, Annick

    2015-01-01

    Background The Health through Sport conceptual model links sport participation with physical, social and psychological outcomes and stresses the need for more understanding between these outcomes. The present study aims to uncover how sport participation, physical activity, social capital and mental health are interrelated by examining these outcomes in one model. Methods A cross-sectional survey was conducted in nine disadvantaged communities in Antwerp (Belgium). Two hundred adults (aged 18–56) per community were randomly selected and visited at home to fill out a questionnaire on socio-demographics, sport participation, physical activity, social capital and mental health. A sample of 414 adults participated in the study. Results Structural Equation Modeling analysis showed that sport participation (β = .095) and not total physical activity (β = .027) was associated with better mental health. No association was found between sport participation and community social capital (β = .009) or individual social capital (β = .045). Furthermore, only community social capital was linked with physical activity (β = .114), individual social capital was not (β = -.013). In contrast, only individual social capital was directly associated with mental health (β = .152), community social capital was not (β = .070). Conclusion This study emphasizes the importance of sport participation and individual social capital to improve mental health in disadvantaged communities. It further gives a unique insight into the functionalities of how sport participation, physical activity, social capital and mental health are interrelated. Implications for policy are that cross-sector initiatives between the sport, social and health sector need to be supported as their outcomes are directly linked to one another. PMID:26451731

  8. Cross Cultural Logistics and Supply Chain Management Towards Organizational Effectiveness within the Asean/Thai Automotive Industries: A Sem Analysis

    Directory of Open Access Journals (Sweden)

    Dansomboon Suwaj

    2016-09-01

    . Communication (0.836, trust (0.834 and collaboration (0.824 were ranked as significant components of cross-cultural Supply Chain Management effectiveness. The research also confirmed that the hypothesized difficulty from cultural diversity is difficult to manage and to coordinate. Analysis also confirmed the ongoing and significant problems to the global automotive supply chain by natural disasters and the consequential economic losses.

  9. Cemented carbide cutting tool: Laser processing and thermal stress analysis

    Energy Technology Data Exchange (ETDEWEB)

    Yilbas, B.S. [Mechanical Engineering Department, KFUPM, Box 1913, Dhahran 31261 (Saudi Arabia)]. E-mail: bsyilbas@kfupm.edu.sa; Arif, A.F.M. [Mechanical Engineering Department, KFUPM, Box 1913, Dhahran 31261 (Saudi Arabia); Karatas, C. [Engineering Faculty, Hacettepe University, Ankara (Turkey); Ahsan, M. [Mechanical Engineering Department, KFUPM, Box 1913, Dhahran 31261 (Saudi Arabia)

    2007-04-15

    Laser treatment of cemented carbide tool surface consisting of W, C, TiC, TaC is examined and thermal stress developed due to temperature gradients in the laser treated region is predicted numerically. Temperature rise in the substrate material is computed numerically using the Fourier heating model. Experiment is carried out to treat the tool surfaces using a CO{sub 2} laser while SEM, XRD and EDS are carried out for morphological and structural characterization of the treated surface. Laser parameters were selected include the laser output power, duty cycle, assisting gas pressure, scanning speed, and nominal focus setting of the focusing lens. It is found that temperature gradient attains significantly high values below the surface particularly for titanium and tantalum carbides, which in turn, results in high thermal stress generation in this region. SEM examination of laser treated surface and its cross section reveals that crack initiation below the surface occurs and crack extends over the depth of the laser treated region.

  10. SLAC divertor channel entrance thermal stress analysis

    International Nuclear Information System (INIS)

    Johnson, G.L.; Stein, W.; Lu, S.C.; Riddle, R.A.

    1985-01-01

    X-ray beams emerging from the new SLAC electron-positron storage ring (PEP) impinge on the entrance to tangential divertor channels causing highly localized heating in the channel structure. Analyses were completed to determine the temperatures and thermally-induced stresses due to this heating. These parts are cooled with water flowing axially over them at 30 0 C. The current design and operating conditions should result in the entrance to the new divertor channel operating at a peak temperature of 123 0 C with a peak thermal stress at 91% of yield. Any micro-cracks that form due to thermally-induced stresses should not propagate to the coolant wall nor form a path for the coolant to leak into the storage ring vacuum. 34 figs., 4 tabs

  11. Thermal analysis of a glass bending process

    International Nuclear Information System (INIS)

    Buonanno, G.; Dell'Isola, M.; Frattolillo, A.; Giovinco, G.

    2005-01-01

    The paper presents the thermal simulation of naturally ventilated ovens used in glass sheets hot forming for windscreen production. The determination of thermal and flow conditions in the oven and, consequently, the windshield temperature distribution is necessary both for the productive process optimisation and to assure beforehand, without any iterative tuning process, the required characteristics of the product considered. To this purpose, the authors carried out a 3D numerical simulation of the thermal interaction between the glass and the oven internal surfaces during the whole heating process inside the oven. In particular, a finite volumes method was used to take into account both the convective, conductive and radiative heat transfer in the oven. The numerical temperature distribution in the glass was validated through the comparison with the data obtained from an experimental apparatus designed and built for the purpose

  12. Small thermal oscillation analysis of the MOTA

    International Nuclear Information System (INIS)

    Guthrie, G.L.

    1978-09-01

    The MOTA (Materials Open Test Assembly) was designed to achieve a degree of thermal regulation compatible with the generation of useful materials property data obtained by irradiation of candidate reactor structural materials in the FFTF. Attaining a high degree of regulation is limited by the necessity to avoid undamped thermal oscillations. The report documents some of the analyses used to select usable configurations and determine effects of parameter choices, and investigates limitations on allowable gains of the sensor-control-valve assembly. The main purpose of the document is to make the methods available to others, rather than to give a tabulation of specific numerical results

  13. Thermal analysis of cold vacuum drying of spent nuclear fuel

    Energy Technology Data Exchange (ETDEWEB)

    Piepho, M.G.

    1998-07-20

    The thermal analysis examined transient thermal and chemical behavior of the Multi canister Overpack (MCO) container for a broad range of cases that represent the Cold Vacuum Drying (CVD) processes. The cases were defined to consider both normal and off-normal operations at the CVD Facility for an MCO with Mark IV N, Reactor spent fuel in four fuel baskets and one scrap basket. This analysis provides the basis for the MCO thermal behavior at the CVD Facility for its Phase 2 Safety Analysis Report (revision 4).

  14. Inverse thermal analysis method to study solidification in cast iron

    DEFF Research Database (Denmark)

    Dioszegi, Atilla; Hattel, Jesper

    2004-01-01

    Solidification modelling of cast metals is widely used to predict final properties in cast components. Accurate models necessitate good knowledge of the solidification behaviour. The present study includes a re-examination of the Fourier thermal analysis method. This involves an inverse numerical...... solution of a 1-dimensional heat transfer problem connected to solidification of cast alloys. In the analysis, the relation between the thermal state and the fraction solid of the metal is evaluated by a numerical method. This method contains an iteration algorithm controlled by an under relaxation term...... inverse thermal analysis was tested on both experimental and simulated data....

  15. Thermal analysis of the IDENT 1578 fuel pin shipping container

    International Nuclear Information System (INIS)

    Ingham, J.G.

    1980-01-01

    The IDENT 1578 container, which is a 110-in. long 5.5-in. OD tube, is designed for shipping FFTF fuel elements in T-3 casks between HEDL, HFEF, and other laboratories. The thermal analysis was conducted to evaluate whether or not the container satisfies its thermal design criteria

  16. Thermal analysis elements of liquefied gas storage tanks

    Science.gov (United States)

    Yanvarev, I. A.; Krupnikov, A. V.

    2017-08-01

    Tasks of solving energy and resource efficient usage problems, both for oil producing companies and for companies extracting and transporting natural gas, are associated with liquefied petroleum gas technology development. Improving the operation efficiency of liquefied products storages provides for conducting structural, functional, and appropriate thermal analysis of tank parks in the general case as complex dynamic thermal systems.

  17. Lumped thermal capacitance analysis of transient heat conduction ...

    African Journals Online (AJOL)

    Lumped thermal capacitance analysis has been undertaken to investigate the transient temperature variations, associated induced thermal stress distributions, and the structural integrity of Ghana Research Reactor-1 (GHAR R-1) vessel after 15 years of operation. The beltline configuration of the cylindrical vessel of the ...

  18. Statistical analysis of thermal conductivity of nanofluid containing ...

    Indian Academy of Sciences (India)

    Thermal conductivity measurements of nanofluids were analysed via two-factor completely randomized design and comparison of data means is carried out with Duncan's multiple-range test. Statistical analysis of experimental data show that temperature and weight fraction have a reasonable impact on the thermal ...

  19. Thermal-buckling analysis of an LMFBR overflow vessel

    International Nuclear Information System (INIS)

    Severud, L.K.

    1983-01-01

    During a reactor scram, cold sodium flows into the hot overflow vessel. The effect on the vessel is a compressive thermal stress in a zone just above the sodium level. This condition must be sufficiently controlled to preclude thermal buckling. Also, under repeated scrams, the vessel should not suffer thermal stress low cycle fatigue. To evaluate the closeness to buckling and satisfaction of ASMA Code limits, a combination of simple approximations, detailed elastic shell buckling analyses, and correlations to results of thermal buckling tests were employed. This paper describes the analysis methods, special considerations, and evaluations accomplished for this FFTF vessel to assure satisfaction of ASME buckling design criteria, rules, and limits

  20. Thermodynamic analysis of pumped thermal electricity storage

    International Nuclear Information System (INIS)

    White, Alexander; Parks, Geoff; Markides, Christos N.

    2013-01-01

    The increasing use of renewable energy technologies for electricity generation, many of which have an unpredictably intermittent nature, will inevitably lead to a greater need for electricity storage. Although there are many existing and emerging storage technologies, most have limitations in terms of geographical constraints, high capital cost or low cycle life, and few are of sufficient scale (in terms of both power and storage capacity) for integration at the transmission and distribution levels. This paper is concerned with a relatively new concept which will be referred to here as Pumped Thermal Electricity Storage (PTES), and which may be able to make a significant contribution towards future storage needs. During charge, PTES makes use of a high temperature ratio heat pump to convert electrical energy into thermal energy which is stored as ‘sensible heat’ in two thermal reservoirs, one hot and one cold. When required, the thermal energy is then converted back to electricity by effectively running the heat pump backwards as a heat engine. The paper focuses on thermodynamic aspects of PTES, including energy and power density, and the various sources of irreversibility and their impact on round-trip efficiency. It is shown that, for given compression and expansion efficiencies, the cycle performance is controlled chiefly by the ratio between the highest and lowest temperatures in each reservoir rather than by the cycle pressure ratio. The sensitivity of round-trip efficiency to various loss parameters has been analysed and indicates particular susceptibility to compression and expansion irreversibility

  1. Experimental analysis of current conduction through thermally ...

    Indian Academy of Sciences (India)

    Electrical properties of SiO2 grown on the Si-face of the epitaxial 4H-SiC ... Thermal oxide reliability is one of the most critical concerns in the realization of ... material for high temperature, high power, high frequency, and nonvolatile .... conduction mechanism in MOSiC system with varying oxide thicknesses has been.

  2. Thermal CFD Analysis of Tubular Light Guides

    Directory of Open Access Journals (Sweden)

    Ondřej Šikula

    2013-12-01

    Full Text Available Tubular light guides are applicable for daylighting of windowless areas in buildings. Despite their many positive indoor climate aspects they can also present some problems with heat losses and condensation. A computer CFD model focused on the evaluation of temperature distribution and air flow inside tubular light guides of different dimensions was studied. The physical model of the tested light guides of lengths more than 0.60 m proves shows that Rayleigh numbers are adequate for a turbulent air flow. The turbulent model was applied despite the small heat flux differences between the turbulent and laminar model. The CFD simulations resulted into conclusions that the growing ratio of length/diameter increases the heat transmission loss/linear transmittance as much as by 50 percent. Tubular light guides of smaller diameters have lower heat transmission losses compared to the wider ones of the same lengths with the same outdoor temperature being taken into account. The simulation results confirmed the thermal bridge effect of the tubular light guide tube inside the insulated flat roof details. The thermal transmittance of the studied light guides in the whole roof area was substituted with the point thermal bridges. This substitution gives possibility for simple thermal evaluation of the tubular light pipes in roof constructions.

  3. Contact Thermal Analysis and Wear Simulation of a Brake Block

    Directory of Open Access Journals (Sweden)

    Nándor Békési

    2013-01-01

    Full Text Available The present paper describes an experimental test and a coupled contact-thermal-wear analysis of a railway wheel/brake block system through the braking process. During the test, the friction, the generated heat, and the wear were evaluated. It was found that the contact between the brake block and the wheel occurs in relatively small and slowly moving hot spots, caused by the wear and the thermal effects. A coupled simulation method was developed including numerical frictional contact, transient thermal and incremental wear calculations. In the 3D simulation, the effects of the friction, the thermal expansion, the wear, and the temperature-dependent material properties were also considered. A good agreement was found between the results of the test and the calculations, both for the thermal and wear results. The proposed method is suitable for modelling the slowly oscillating wear caused by the thermal expansions in the contact area.

  4. Phosphorus Sorption Characteristics in Aluminum-based Water Treatment Residuals Reacted with Dairy Wastewater: 1. Isotherms, XRD, and SEM-EDS Analysis.

    Science.gov (United States)

    Zohar, Iris; Massey, Michael S; Ippolito, James A; Litaor, M Iggy

    2018-05-01

    We examined P sorption characteristics in Al-based water treatment residuals (Al-WTR) generated from slightly alkaline surface water and in an organic residual composite (WW-Al/O-WTR), produced by using the Al-WTR to treat organic-rich and high P concentration dairy wastewater. Solids from both residuals were examined using scanning electron microscopy-energy dispersive spectroscopy (SEM-EDS) and X-ray diffraction (XRD), and exposed to P additions of 0 to 4000 mg L in a sorption experiment. The Al-WTR removed ∼97% of the added P, whereas WW-Al/O-WTR removed only 78% of the added P in the addition range of 0 to 100 mg P L. With P additions of ≥100 mg L, the removal rate declined to XRD indicated that the major mineral was calcite, with some silica and poorly crystalline Al hydroxides. Analysis by SEM-EDS, which used three-element overlay maps of the residual surfaces, indicated that P was sparsely sorbed on both calcic and Al (hydr)oxide surfaces, along with a few clusters, even at low P concentrations of the treated waters. Ternary clusters of P, Al, and Ca were more abundant on the WW-Al/O-WTR. Carbon distribution suggested that organic substances covered Al surfaces. Sorption of P onto WW-Al/O-WTR may be reversible due to relatively weak Ca-P and Al-P bonds induced by the slight alkaline nature and in the presence of organic moieties, enhancing the WW-Al/O-WTR potential to act as a P source, rather than a P sink, in agricultural applications. Copyright © by the American Society of Agronomy, Crop Science Society of America, and Soil Science Society of America, Inc.

  5. Evaluation of Thermal Margin Analysis Models for SMART

    International Nuclear Information System (INIS)

    Seo, Kyong Won; Kwon, Hyuk; Hwang, Dae Hyun

    2011-01-01

    Thermal margin of SMART would be analyzed by three different methods. The first method is subchannel analysis by MATRA-S code and it would be a reference data for the other two methods. The second method is an on-line few channel analysis by FAST code that would be integrated into SCOPS/SCOMS. The last one is a single channel module analysis by safety analysis. Several thermal margin analysis models for SMART reactor core by subchannel analysis were setup and tested. We adopted a strategy of single stage analysis for thermal analysis of SMART reactor core. The model should represent characteristics of the SMART reactor core including hot channel. The model should be simple as possible to be evaluated within reasonable time and cost

  6. Decomposition of thin titanium deuteride films: thermal desorption kinetics studies combined with microstructure analysis

    NARCIS (Netherlands)

    Lisowski, W.F.; Keim, Enrico G.; Kaszkur, Zbigniew; Smithers, M.A.; Smithers, Mark A.

    2008-01-01

    The thermal evolution of deuterium from thin titanium films, prepared under UHV conditions and deuterated in situ at room temperature, has been studied by means of thermal desorption mass spectrometry (TDMS) and a combination of scanning electron microscopy (SEM), transmission electron microscopy

  7. Performance analysis of a lunar based solar thermal power system with regolith thermal storage

    International Nuclear Information System (INIS)

    Lu, Xiaochen; Ma, Rong; Wang, Chao; Yao, Wei

    2016-01-01

    The manned deep-space exploration is a hot topic of the current space activities. The continuous supply of thermal and electrical energy for the scientific equipment and human beings is a crucial issue for the lunar outposts. Since the night lasts for periods of about 350 h at most locations on the lunar surface, massive energy storage is required for continuous energy supply during the lengthy lunar night and the in-situ resource utilization is demanded. A lunar based solar thermal power system with regolith thermal storage is presented in this paper. The performance analysis is carried out by the finite-time thermodynamics to take into account major irreversible losses. The influences of some key design parameters are analyzed for system optimization. The analytical results shows that the lunar based solar thermal power system with regolith thermal storage can meet the requirement of the continuous energy supply for lunar outposts. - Highlights: • A lunar based solar thermal power system with regolith thermal storage is presented. • The performance analysis is carried out by the finite-time thermodynamics. • The influences of some key design parameters are analyzed.

  8. Thermal protection system gap analysis using a loosely coupled fluid-structural thermal numerical method

    Science.gov (United States)

    Huang, Jie; Li, Piao; Yao, Weixing

    2018-05-01

    A loosely coupled fluid-structural thermal numerical method is introduced for the thermal protection system (TPS) gap thermal control analysis in this paper. The aerodynamic heating and structural thermal are analyzed by computational fluid dynamics (CFD) and numerical heat transfer (NHT) methods respectively. An interpolation algorithm based on the control surface is adopted for the data exchanges on the coupled surface. In order to verify the analysis precision of the loosely coupled method, a circular tube example was analyzed, and the wall temperature agrees well with the test result. TPS gap thermal control performance was studied by the loosely coupled method successfully. The gap heat flux is mainly distributed in the small region at the top of the gap which is the high temperature region. Besides, TPS gap temperature and the power of the active cooling system (CCS) calculated by the traditional uncoupled method are higher than that calculated by the coupled method obviously. The reason is that the uncoupled method doesn't consider the coupled effect between the aerodynamic heating and structural thermal, however the coupled method considers it, so TPS gap thermal control performance can be analyzed more accurately by the coupled method.

  9. Dynamic thermal analysis of machines in running state

    CERN Document Server

    Wang, Lihui

    2014-01-01

    With the increasing complexity and dynamism in today’s machine design and development, more precise, robust and practical approaches and systems are needed to support machine design. Existing design methods treat the targeted machine as stationery. Analysis and simulation are mostly performed at the component level. Although there are some computer-aided engineering tools capable of motion analysis and vibration simulation etc., the machine itself is in the dry-run state. For effective machine design, understanding its thermal behaviours is crucial in achieving the desired performance in real situation. Dynamic Thermal Analysis of Machines in Running State presents a set of innovative solutions to dynamic thermal analysis of machines when they are put under actual working conditions. The objective is to better understand the thermal behaviours of a machine in real situation while at the design stage. The book has two major sections, with the first section presenting a broad-based review of the key areas of ...

  10. Finite element analysis of thermal stress distribution in different ...

    African Journals Online (AJOL)

    Nigerian Journal of Clinical Practice • Jan-Feb 2016 • Vol 19 • Issue 1. Abstract ... Key words: Amalgam, finite element method, glass ionomer cement, resin composite, thermal stress ... applications for force analysis and assessment of different.

  11. Shuttle TPS thermal performance and analysis methodology

    Science.gov (United States)

    Neuenschwander, W. E.; Mcbride, D. U.; Armour, G. A.

    1983-01-01

    Thermal performance of the thermal protection system was approximately as predicted. The only extensive anomalies were filler bar scorching and over-predictions in the high Delta p gap heating regions of the orbiter. A technique to predict filler bar scorching has been developed that can aid in defining a solution. Improvement in high Delta p gap heating methodology is still under study. Minor anomalies were also examined for improvements in modeling techniques and prediction capabilities. These include improved definition of low Delta p gap heating, an analytical model for inner mode line convection heat transfer, better modeling of structure, and inclusion of sneak heating. The limited number of problems related to penetration items that presented themselves during orbital flight tests were resolved expeditiously, and designs were changed and proved successful within the time frame of that program.

  12. Thermal-hydraulic analysis of nuclear reactors

    CERN Document Server

    Zohuri, Bahman

    2015-01-01

    This text covers the fundamentals of thermodynamics required to understand electrical power generation systems and the application of these principles to nuclear reactor power plant systems. It is not a traditional general thermodynamics text, per se, but a practical thermodynamics volume intended to explain the fundamentals and apply them to the challenges facing actual nuclear power plants systems, where thermal hydraulics comes to play.  Written in a lucid, straight-forward style while retaining scientific rigor, the content is accessible to upper division undergraduate students and aimed at practicing engineers in nuclear power facilities and engineering scientists and technicians in industry, academic research groups, and national laboratories. The book is also a valuable resource for students and faculty in various engineering programs concerned with nuclear reactors. This book also: Provides extensive coverage of thermal hydraulics with thermodynamics in nuclear reactors, beginning with fundamental ...

  13. LOFT blowdown loop piping thermal analysis Class I review

    International Nuclear Information System (INIS)

    Kinnaman, T.L.

    1978-01-01

    In accordance with ASME Code, Section III requirements, all analyses of Class I components must be independently reviewed. Since the LOFT blowdown loop piping up through the blowdown valve is a Class I piping system, the thermal analyses are reviewed. The Thermal Analysis Branch comments to this review are also included. It is the opinion of the Thermal Analysis Branch that these comments satisfy all of the reviewers questions and that the analyses should stand as is, without additional considerations in meeting the ASME Code requirements and ANC Specification 60139

  14. Window design : visual and thermal consequences : analysis of the thermal and daylighting performance of windows

    NARCIS (Netherlands)

    Bergem-Jansen, P.M. van; Soeleman, R.S.

    1979-01-01

    Selected results of an analysis for the thermal and lighting requirements associated with windows in utility buildings are presented. This analysis concerns the effects of r¡indow size and shape, orientation and of different ways of supplementing the daylight by artifieial light for a typical office

  15. The risk assessment of heavy metals in Futian mangrove forest sediment in Shenzhen Bay (South China) based on SEM-AVS analysis.

    Science.gov (United States)

    Chai, Minwei; Shen, Xiaoxue; Li, Ruili; Qiu, Guoyu

    2015-08-15

    The risks of heavy metal in Futian mangrove forest sediment were assessed using the acid-volatile sulfide (AVS) and simultaneously extracted metals (SEM) methods. The results indicated that AVS distributions were more variable than the SEM distributions at all 16 sampling sites. The positive correlation between AVS and SEM indicated that their similar formative and existing conditions and that AVS acted as an important carrier for SEM. The major SEM component was Zn (69.7.3-94.2%), whereas the Cd contribution (the most toxic metal present) to SEM was no more than 1%. The possible adverse effects caused by heavy metals at ten sampling sites may be due to higher levels of SEMs, rather than AVSs. The total organic carbon (TOC) was an important metal-binding phase in the sediments. Taking into account the TOC concentration, there were no adverse effects due to heavy metals in any of the Futian mangrove forest sediments. Copyright © 2015 Elsevier Ltd. All rights reserved.

  16. A Study of the Oxidation Behaviour of Pile Grade A (PGA) Nuclear Graphite Using Thermogravimetric Analysis (TGA), Scanning Electron Microscopy (SEM) and X-Ray Tomography (XRT).

    Science.gov (United States)

    Payne, Liam; Heard, Peter J; Scott, Thomas B

    2015-01-01

    Pile grade A (PGA) graphite was used as a material for moderating and reflecting neutrons in the UK's first generation Magnox nuclear power reactors. As all but one of these reactors are now shut down there is a need to understand the residual state of the material prior to decommissioning of the cores, in particular the location and concentration of key radio-contaminants such as 14C. The oxidation behaviour of unirradiated PGA graphite was studied, in the temperature range 600-1050°C, in air and nitrogen using thermogravimetric analysis, scanning electron microscopy and X-ray tomography to investigate the possibility of using thermal degradation techniques to examine 14C distribution within irradiated material. The thermal decomposition of PGA graphite was observed to follow the three oxidation regimes historically identified by previous workers with limited, uniform oxidation at temperatures below 600°C and substantial, external oxidation at higher temperatures. This work demonstrates that the different oxidation regimes of PGA graphite could be developed into a methodology to characterise the distribution and concentration of 14C in irradiated graphite by thermal treatment.

  17. The analysis of thermally stimulated processes

    CERN Document Server

    Chen, R; Pamplin, Brian

    1981-01-01

    Thermally stimulated processes include a number of phenomena - either physical or chemical in nature - in which a certain property of a substance is measured during controlled heating from a 'low' temperature. Workers and graduate students in a wide spectrum of fields require an introduction to methods of extracting information from such measurements. This book gives an interdisciplinary approach to various methods which may be applied to analytical chemistry including radiation dosimetry and determination of archaeological and geological ages. In addition, recent advances are included, such

  18. Viscoelastic Analysis of Thermally Stiffening Polymer Nanocomposites

    Science.gov (United States)

    Ehlers, Andrew; Rende, Deniz; Senses, Erkan; Akcora, Pinar; Ozisik, Rahmi

    Poly(ethylene oxide), PEO, filled with silica nanoparticles coated with poly(methyl methacrylate), PMMA, was shown to present thermally stiffening behavior above the glass transition temperature of both PEO and PMMA. In the current study, the viscoelastic beahvior of this nanocomposite system is investigated via nanoindenation experiments to complement on going rheological studies. Results were compared to neat polymers, PEO and PMMA, to understand the effect of coated nanoparticles. This material is based upon work supported by the National Science Foundation under Grant No. CMMI-1538730.

  19. A real time analysis of the self-assembly process using thermal analysis inside the differential scanning calorimeter instrument.

    Science.gov (United States)

    Roy, Debmalya; Shastri, Babita; Mukhopadhyay, K

    2012-07-12

    The supramolecular assembly of the regioregular poly-3-hexylthiophene (rr-P3HT) in solution has been investigated thoroughly in the past. In the current study, our focus is on the enthalpy of nanofiber formation using thermal analysis techniques by performing the self-assembly process inside the differential scanning calorimetry (DSC) instrument. Thermogravimetric analysis (TGA) was carried out to check the concentration of the solvent during the self-assembly process of P3HT in p-xylene. Ultraviolet visible (UV-vis) spectophotometric technique, small-angle X-ray scattering (SAXS) experiment, atomic force microscopic (AFM), and scanning electron microscopic (SEM) images were used to characterize the different experimental yields generated by cooling the reaction mixture at desired temperatures. Comparison of the morphologies of self-assembled products at different fiber formation temperatures gives us an idea about the possible crystallization parameters which could affect the P3HT nanofiber morphology.

  20. Thermal stress analysis of space shuttle orbiter wing skin panel and thermal protection system

    Science.gov (United States)

    Ko, William L.; Jenkins, Jerald M.

    1987-01-01

    Preflight thermal stress analysis of the space shuttle orbiter wing skin panel and the thermal protection system (TPS) was performed. The heated skin panel analyzed was rectangular in shape and contained a small square cool region at its center. The wing skin immediately outside the cool region was found to be close to the state of elastic instability in the chordwise direction based on the conservative temperature distribution. The wing skin was found to be quite stable in the spanwise direction. The potential wing skin thermal instability was not severe enough to tear apart the strain isolation pad (SIP) layer. Also, the preflight thermal stress analysis was performed on the TPS tile under the most severe temperature gradient during the simulated reentry heating. The tensile thermal stress induced in the TPS tile was found to be much lower than the tensile strength of the TPS material. The thermal bending of the TPS tile was not severe enough to cause tearing of the SIP layer.

  1. Thermal conductivity analysis and applications of nanocellulose materials

    Science.gov (United States)

    Uetani, Kojiro; Hatori, Kimihito

    2017-01-01

    Abstract In this review, we summarize the recent progress in thermal conductivity analysis of nanocellulose materials called cellulose nanopapers, and compare them with polymeric materials, including neat polymers, composites, and traditional paper. It is important to individually measure the in-plane and through-plane heat-conducting properties of two-dimensional planar materials, so steady-state and non-equilibrium methods, in particular the laser spot periodic heating radiation thermometry method, are reviewed. The structural dependency of cellulose nanopaper on thermal conduction is described in terms of the crystallite size effect, fibre orientation, and interfacial thermal resistance between fibres and small pores. The novel applications of cellulose as thermally conductive transparent materials and thermal-guiding materials are also discussed. PMID:29152020

  2. Thermal Analysis Of 3013/9975 Configuration

    International Nuclear Information System (INIS)

    Gupta, N.

    2009-01-01

    The 3013 containers are designed in accordance with the DOE-STD-3013-2004 and are qualified to store plutonium (Pu) bearing materials for 50 years. The U.S. Department of Energy (DOE) certified Model 9975 shipping package is used to transport the 3013 containers to the K-Area Material Storage (KAMS) facility at the Savannah River Site (SRS) and to store the containers until the plutonium can be properly dispositioned. Detailed thermal analyses to support the storage in the KAMS facility are given in References 2, 3, and 4. The analyses in this paper serve to provide non-accident condition, non-bounding, specific 3013 container temperatures for use in the surveillance activities. This paper presents a methodology where critical component temperatures are estimated using numerical methods over a range of package and storage parameters. The analyses include factors such as ambient storage temperature and the content weight, density, heat generation rate, and fill height, that may impact the thermal response of the packages. Statistical methods are used to develop algebraic equations for ease of computations to cover the factor space. All computations were performed in BTU-FT-Hr- o F units.

  3. Pressurized Thermal Shock Analysis for OPR1000 Pressure Vessel

    Energy Technology Data Exchange (ETDEWEB)

    Bhowmik, P. K.; Shamim, J. A.; Gairola, A.; Suh, Kune Y. [Seoul National Univ., Seoul (Korea, Republic of)

    2014-10-15

    The study provides a brief understanding of the analysis procedure and techniques using ANSYS, such as the acceptance criteria, selection and categorization of events, thermal analysis, structural analysis including fracture mechanics assessment, crack propagation and evaluation of material properties. PTS may result from instrumentation and control malfunction, inadvertent steam dump, and postulated accidents such as smallbreak (SB) LOCA, large-break (LB) LOCA, main steam line break (MSLB), feedwater line breaks and steam generator overfill. In this study our main focus is to consider only the LB LOCA due to a cold leg break of the Optimized Power Reactor 1000 MWe (OPR1000). Consideration is given as well to the emergency core cooling system (ECCS) specific sequence with the operating parameters like pressure, temperature and time sequences. The static structural and thermal analysis to investigate the effects of PTS on RPV is the main motivation of this study. Specific surface crack effects and its propagation is also considered to measure the integrity of the RPV. This study describes the procedure for pressurized thermal shock analysis due to a loss of coolant accidental condition and emergency core cooling system operation for reactor pressure vessel.. Different accidental events that cause pressurized thermal shock to nuclear RPV that can also be analyzed in the same way. Considering the limitations of low speed computer only the static analysis is conducted. The modified LBLOCA phases and simplified geometry can is utilized to analyze the effect of PTS on RPV for general understanding not for specific specialized purpose. However, by integrating the disciplines of thermal and structural analysis, and fracture mechanics analysis a clearer understanding of the total aspect of the PTS problem has resulted. By adopting the CFD, thermal hydraulics, uncertainties and risk analysis for different type of accidental conditions, events and sequences with proper

  4. Sem Analysis of particles from the 28, 000 B.P El Zaguan debris avalanche deposit, Nevado de Toluca volcano, Central Mexico: evidences of flow behavior during emplacement

    Science.gov (United States)

    Caballero, L.; Capra, L.

    2008-12-01

    The Zaguan deposit originated at 28, 000 yr. B.P from the flank collapse of the Nevado de Toluca volcano, a dacitic stratovolcano of the Transmexican Volcanic Belt. A Scanning Electron Microprobe analysis (SEM) was made to some clasts of this deposit to observe microtextures produced during transport and emplacement of the debris avalanche flow. Particles from 2, 0 and -2 Φ granulometric classes were randomly selected and their surface textures were described. The textures observed were divided in two groups, collision and shear structures indicating different clast interaction. Shear textures were observed predominantly on the basal part of the deposit and consisted of parallel ridges, parallel grooves, scratches and lips. Collision textures were mainly present in the upper part of the deposit and consisted of fractures, percussion marks, and broken or grinded crystals. These characteristics, coupled with field observation, like the presence of clast dikes and deformed lacustrine megaclasts, indicate that the basal part of the debris avalanche was moving in a partially liquefied state, were particles were not able to move freely because of the confinement exerted by the upper part of the flow, so shear stresses dominated. On the contrary, the particles in the upper part were able to move freely so the principal mechanism of interaction between particles was collision. These microscopic textures are in agreement with previously described behavior of emplacement of debris avalanches of volcanic origin, that suggest a stratified flow dominated by different transport and depositional mechanism depending on flow depth and possible fluid content at their base.

  5. The Peltier driven frequency domain approach in thermal analysis.

    Science.gov (United States)

    De Marchi, Andrea; Giaretto, Valter

    2014-10-01

    The merits of Frequency Domain analysis as a tool for thermal system characterization are discussed, and the complex thermal impedance approach is illustrated. Pure AC thermal flux generation with negligible DC component is possible with a Peltier device, differently from other existing methods in which a significant DC component is intrinsically attached to the generated AC flux. Such technique is named here Peltier Driven Frequency Domain (PDFD). As a necessary prerequisite, a novel one-dimensional analytical model for an asymmetrically loaded Peltier device is developed, which is general enough to be useful in most practical situations as a design tool for measurement systems and as a key for the interpretation of experimental results. Impedance analysis is possible with Peltier devices by the inbuilt Seebeck effect differential thermometer, and is used in the paper for an experimental validation of the analytical model. Suggestions are then given for possible applications of PDFD, including the determination of thermal properties of materials.

  6. Analysis of Thermal Comfort in an Intelligent Building

    Science.gov (United States)

    Majewski, Grzegorz; Telejko, Marek; Orman, Łukasz J.

    2017-06-01

    Analysis of thermal comfort in the ENERGIS Building, an intelligent building in the campus of the Kielce University of Technology, Poland is the focus of this paper. For this purpose, air temperature, air relative humidity, air flow rate and carbon dioxide concentration were measured and the mean radiant temperature was determined. Thermal sensations of the students occupying the rooms of the building were evaluated with the use of a questionnaire. The students used a seven-point scale of thermal comfort. The microclimate measurement results were used to determine the Predicted Mean Vote and the Predicted Percentage Dissatisfied indices.

  7. Temperature and thermal stress analysis of a switching tube anode

    International Nuclear Information System (INIS)

    Sutton, S.B.

    1979-01-01

    In the design of high power density switching tubes which are subjected to cyclic thermal loads, the temperature induced stresses must be minimized in order to maximize the life expectancy of the tube. Following are details of an analysis performed for the Magnetic Fusion Program at the Lawrence Livermore Laboratory on a proposed tube. The tube configuration is given. The problem was simplified to one-dimensional approximations for both the thermal and stress analyses. The underlying assumptions and their implications are discussed

  8. NUMERICAL THERMAL ANALYSIS OF A CAR BRAKING SYSTEM

    Directory of Open Access Journals (Sweden)

    Patryk Różyło

    2017-06-01

    Full Text Available The study involved performing a numerical thermal analysis of selected components in a car braking system. The primary goal of the study was to determine the regions which are the most susceptible to variations in temperature, and to determine the degree of thermal impact upon them. The analysis was performed using the Abaqus environment. The examined components of the braking system were made of materials reflecting the mechanical properties of the real subassemblies. The FEM analysis enabled determination of the distribution of temperature in the system with respect to the properties of the investigated materials and applied boundary conditions.

  9. Probing the heat sources during thermal runaway process by thermal analysis of different battery chemistries

    Science.gov (United States)

    Zheng, Siqi; Wang, Li; Feng, Xuning; He, Xiangming

    2018-02-01

    Safety issue is very important for the lithium ion battery used in electric vehicle or other applications. This paper probes the heat sources in the thermal runaway processes of lithium ion batteries composed of different chemistries using accelerating rate calorimetry (ARC) and differential scanning calorimetry (DSC). The adiabatic thermal runaway features for the 4 types of commercial lithium ion batteries are tested using ARC, whereas the reaction characteristics of the component materials, including the cathode, the anode and the separator, inside the 4 types of batteries are measured using DSC. The peaks and valleys of the critical component reactions measured by DSC can match the fluctuations in the temperature rise rate measured by ARC, therefore the relevance between the DSC curves and the ARC curves is utilized to probe the heat source in the thermal runaway process and reveal the thermal runaway mechanisms. The results and analysis indicate that internal short circuit is not the only way to thermal runaway, but can lead to extra electrical heat, which is comparable with the heat released by chemical reactions. The analytical approach of the thermal runaway mechanisms in this paper can guide the safety design of commercial lithium ion batteries.

  10. Thermal Analysis of Fluidized Bed and Fixed Bed Latent Heat Thermal Storage System

    Science.gov (United States)

    Beemkumar, N.; Karthikeyan, A.; Shiva Keshava Reddy, Kota; Rajesh, Kona; Anderson, A.

    2017-05-01

    Thermal energy storage technology is essential because its stores available energy at low cost. Objective of the work is to store the thermal energy in a most efficient method. This work is deal with thermal analysis of fluidized bed and fixed bed latent heat thermal storage (LHTS) system with different encapsulation materials (aluminium, brass and copper). D-Mannitol has been used as phase change material (PCM). Encapsulation material which is in orbicular shape with 4 inch diameter and 2 mm thickness orbicular shaped product is used. Therminol-66 is used as a heat transfer fluid (HTF). Arrangement of encapsulation material is done in two ways namely fluidized bed and fixed bed thermal storage system. Comparison was made between the performance of fixed bed and fluidized bed with different encapsulation material. It is observed that from the economical point of view aluminium in fluidized bed LHTS System has highest efficiency than copper and brass. The thermal energy storage system can be analyzed with fixed bed by varying mass flow rate of oil paves a way to find effective heat energy transfer.

  11. Nonlinear Transient Thermal Analysis by the Force-Derivative Method

    Science.gov (United States)

    Balakrishnan, Narayani V.; Hou, Gene

    1997-01-01

    High-speed vehicles such as the Space Shuttle Orbiter must withstand severe aerodynamic heating during reentry through the atmosphere. The Shuttle skin and substructure are constructed primarily of aluminum, which must be protected during reentry with a thermal protection system (TPS) from being overheated beyond the allowable temperature limit, so that the structural integrity is maintained for subsequent flights. High-temperature reusable surface insulation (HRSI), a popular choice of passive insulation system, typically absorbs the incoming radiative or convective heat at its surface and then re-radiates most of it to the atmosphere while conducting the smallest amount possible to the structure by virtue of its low diffusivity. In order to ensure a successful thermal performance of the Shuttle under a prescribed reentry flight profile, a preflight reentry heating thermal analysis of the Shuttle must be done. The surface temperature profile, the transient response of the HRSI interior, and the structural temperatures are all required to evaluate the functioning of the HRSI. Transient temperature distributions which identify the regions of high temperature gradients, are also required to compute the thermal loads for a structural thermal stress analysis. Furthermore, a nonlinear analysis is necessary to account for the temperature-dependent thermal properties of the HRSI as well as to model radiation losses.

  12. Thermal Analysis of LANL Ion Exchange Column

    International Nuclear Information System (INIS)

    Laurinat, J.E.

    1999-01-01

    This document reports results from an ion exchange column heat transfer analysis requested by Los Alamos National Laboratory (LANL). The object of the analysis is to demonstrate that the decay heat from the Pu-238 will not cause resin bed temperatures to increase to a level where the resin significantly degrades

  13. Thermal stress analysis of a planar SOFC stack

    Science.gov (United States)

    Lin, Chih-Kuang; Chen, Tsung-Ting; Chyou, Yau-Pin; Chiang, Lieh-Kwang

    The aim of this study is, by using finite element analysis (FEA), to characterize the thermal stress distribution in a planar solid oxide fuel cell (SOFC) stack during various stages. The temperature profiles generated by an integrated thermo-electrochemical model were applied to calculate the thermal stress distributions in a multiple-cell SOFC stack by using a three-dimensional (3D) FEA model. The constructed 3D FEA model consists of the complete components used in a practical SOFC stack, including positive electrode-electrolyte-negative electrode (PEN) assembly, interconnect, nickel mesh, and gas-tight glass-ceramic seals. Incorporation of the glass-ceramic sealant, which was never considered in previous studies, into the 3D FEA model would produce more realistic results in thermal stress analysis and enhance the reliability of predicting potential failure locations in an SOFC stack. The effects of stack support condition, viscous behavior of the glass-ceramic sealant, temperature gradient, and thermal expansion mismatch between components were characterized. Modeling results indicated that a change in the support condition at the bottom frame of the SOFC stack would not cause significant changes in thermal stress distribution. Thermal stress distribution did not differ significantly in each unit cell of the multiple-cell stack due to a comparable in-plane temperature profile. By considering the viscous characteristics of the glass-ceramic sealant at temperatures above the glass-transition temperature, relaxation of thermal stresses in the PEN was predicted. The thermal expansion behavior of the metallic interconnect/frame had a greater influence on the thermal stress distribution in the PEN than did that of the glass-ceramic sealant due to the domination of interconnect/frame in the volume of a planar SOFC assembly.

  14. Long term energy performance analysis of Egbin thermal power ...

    African Journals Online (AJOL)

    This study is aimed at providing an energy performance analysis of Egbin thermal power plant. The plant operates on Regenerative Rankine cycle with steam as its working fluid .The model equations were formulated based on some performance parameters used in power plant analysis. The considered criteria were plant ...

  15. Use of emanation thermal analysis to characterize thermal reactivity of brannerite mineral

    Czech Academy of Sciences Publication Activity Database

    Balek, V.; Vance, E.R.; Zeleňák, V.; Málek, Z.; Šubrt, Jan

    2007-01-01

    Roč. 88, č. 1 (2007), s. 93-98 ISSN 1388-6150 Grant - others:GA MŠk(CZ) LA 292; GA MŠk(CZ) ME 879 Institutional research plan: CEZ:AV0Z40320502 Keywords : brannerite * emanation thermal analysis Subject RIV: CA - Inorganic Chemistry Impact factor: 1.483, year: 2007

  16. Thermal analysis of RFETS SS and C

    International Nuclear Information System (INIS)

    Korinko, P.S.

    2000-01-01

    In support of the gas generation test program (GGTP) for the 9975 shipping container, thermogravimetric analysis (TGA) was conducted. The objective of this activity was to determine the moisture content as an input to the gas generation model

  17. Thermal Analysis for Condition Monitoring of Machine Tool Spindles

    International Nuclear Information System (INIS)

    Clough, D; Fletcher, S; Longstaff, A P; Willoughby, P

    2012-01-01

    Decreasing tolerances on parts manufactured, or inspected, on machine tools increases the requirement to have a greater understanding of machine tool capabilities, error sources and factors affecting asset availability. Continuous usage of a machine tool during production processes causes heat generation typically at the moving elements, resulting in distortion of the machine structure. These effects, known as thermal errors, can contribute a significant percentage of the total error in a machine tool. There are a number of design solutions available to the machine tool builder to reduce thermal error including, liquid cooling systems, low thermal expansion materials and symmetric machine tool structures. However, these can only reduce the error not eliminate it altogether. It is therefore advisable, particularly in the production of high value parts, for manufacturers to obtain a thermal profile of their machine, to ensure it is capable of producing in tolerance parts. This paper considers factors affecting practical implementation of condition monitoring of the thermal errors. In particular is the requirement to find links between temperature, which is easily measureable during production and the errors which are not. To this end, various methods of testing including the advantages of thermal images are shown. Results are presented from machines in typical manufacturing environments, which also highlight the value of condition monitoring using thermal analysis.

  18. Structure–property relationships of synthetic organophosphorus flame retardant oligomers by thermal analysis

    International Nuclear Information System (INIS)

    Bai, Zhiman; Wang, Xin; Tang, Gang; Song, Lei; Hu, Yuan; Yuen, Richard K.K.

    2013-01-01

    Highlights: • Oligomers with different chemical components in molecular chains were synthesized. • FP-3 containing three IFR components possessed high thermal stability. • FP-3 possessed lowest flammability. • FP-3 exhibited a synergistic interaction between gas and condensed phase. - Abstract: A series of flame retardant oligomers with different chemical components in molecular chains, designated as FP-1, FP-2 and FP-3, respectively, were successfully synthesized using solution polycondensation and well characterized. The thermal properties and flammability of these oligomers were investigated by thermogravimetric analysis (TGA) and microscale combustion calorimeter (MCC). The results demonstrated that FP-3 had the lowest flammability in terms of the lowest maximum mass loss rate, and FP-1 possessed the highest thermal stability and char yield, due to its higher stable hexatomic ring structure of piperazine compared with the linear alkane chain structure of neopentyl glycol. The gases evolved during decomposition were analyzed using Fourier transform infrared coupled with the thermogravimetric analyzer (TG–IR) technique. The char residues of the flame retardant oligomers were investigated by scanning electron microscopy (SEM) and Raman spectroscopy. The results demonstrated that FP-3 exhibited a synergistic interaction between the gas phase and condensation phase, increasing its flame retardancy

  19. Some selected quantitative methods of thermal image analysis in Matlab.

    Science.gov (United States)

    Koprowski, Robert

    2016-05-01

    The paper presents a new algorithm based on some selected automatic quantitative methods for analysing thermal images. It shows the practical implementation of these image analysis methods in Matlab. It enables to perform fully automated and reproducible measurements of selected parameters in thermal images. The paper also shows two examples of the use of the proposed image analysis methods for the area of ​​the skin of a human foot and face. The full source code of the developed application is also provided as an attachment. The main window of the program during dynamic analysis of the foot thermal image. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  20. Thermal stratification and fatigue stress analysis for pressurizer surge line

    International Nuclear Information System (INIS)

    Yu Xiaofei; Zhang Yixiong

    2011-01-01

    Thermal stratification of pressurizer surge line induced by the inside fluid results in the global bending moments, local thermal stresses, unexpected displacements and support loadings of the pipe system. In order to avoid a costly three-dimensional computation, a combined 1D/2D technique has been developed and implemented to analyze the thermal stratification and fatigue stress of pressurize surge line of QINSHAN Phase II Extension Nuclear Power Project in this paper, using the computer codes SYSTUS and ROCOCO. According to the mechanical analysis results of stratification, the maximum stress and cumulative usage factor are obtained. The results indicate that the stress and fatigue intensity considering thermal stratification satisfies RCC-M criterion. (authors)

  1. Thermoreflectance spectroscopy—Analysis of thermal processes in semiconductor lasers

    Science.gov (United States)

    Pierścińska, D.

    2018-01-01

    This review focuses on theoretical foundations, experimental implementation and an overview of experimental results of the thermoreflectance spectroscopy as a powerful technique for temperature monitoring and analysis of thermal processes in semiconductor lasers. This is an optical, non-contact, high spatial resolution technique providing high temperature resolution and mapping capabilities. Thermoreflectance is a thermometric technique based on measuring of relative change of reflectivity of the surface of laser facet, which provides thermal images useful in hot spot detection and reliability studies. In this paper, principles and experimental implementation of the technique as a thermography tool is discussed. Some exemplary applications of TR to various types of lasers are presented, proving that thermoreflectance technique provides new insight into heat management problems in semiconductor lasers and in particular, that it allows studying thermal degradation processes occurring at laser facets. Additionally, thermal processes and basic mechanisms of degradation of the semiconductor laser are discussed.

  2. Development of regulatory technology for thermal-hydraulic safety analysis

    International Nuclear Information System (INIS)

    Bang, Young Seok; Lee, S. H.; Ryu, Y. H.

    2001-02-01

    The present study aims to develop the regulation capability in thermal-hydraulic safety analysis which was required for the reasonable safety regulation in the current NPP, the next generation reactors, and the future-type reactors. The fourth fiscal year of the first phase of the research was focused on the following research topics: Investigation on the current status of the thermal-hydraulic safety analysis technology outside and inside of the country; Review on the improved features of the thermal-hydraulic safety analysis regulatory audit code, RELAP5/MOD3; Assessments of code with LOFT L9-3 ATWS experiment and LSTF SB-SG-10 multiple SGTR experiment; Application of the RELAP5/CANDU code to analyses of SLB and LBLOCA and evaluation of its effect on safety; Application of the code to IAEA PHWR ISP analysis; Assessments of RELAP5 and TRAC with UPTF downcomer injection test and Analysis of LBLOCA with RELAP5 for the performance evaluation of KNGR DVI; Setup of a coupled 3-D kinetics and thermal-hydraulics and application it to a reactivity accident analysis; and Extension of database and improvement of plant input decks. For supporting the resolution of safety issues, loss of RHR event during midloop operation was analyzed for Kori Unit 3, issues on high burnup fuel were reviewed and performance of FRAPCON-3 assessed. Also MSLB was analyzed to figure out the sensitivity of downcomer temperature supporting the PTS risk evaluation of Kori Unit 1. Thermal stratification in pipe was analyzed using the method proposed. And a method predicting the thermal-hydraulic performance of IRWST of KNGR was explored. The PWR ECCS performance criteria was issued as a MOST Article 200-19.and a regulatory guide on evaluation methodology was improved to cover concerns raised from the related licensing review process

  3. Mechanism of Action of TiF4 on Dental Enamel Surface: SEM/EDX, KOH-Soluble F, and X-Ray Diffraction Analysis.

    Science.gov (United States)

    Comar, Lívia P; Souza, Beatriz M; Al-Ahj, Luana P; Martins, Jessica; Grizzo, Larissa T; Piasentim, Isabelle S; Rios, Daniela; Buzalaf, Marília Afonso Rabelo; Magalhães, Ana Carolina

    2017-10-12

    This in vitro study aimed to evaluate the action of TiF4 on sound and carious bovine and human enamel. Sound (S) and pre-demineralised (DE) bovine and human (primary and permanent) enamel samples were treated with TiF4 (pH 1.0) or NaF varnishes (pH 5.0), containing 0.95, 1.95, or 2.45% F for 12 h. The enamel surfaces were analysed using SEM-EDX (scanning electron microscopy/energy-dispersive X-ray spectroscopy) (n = 10, 5 S and 5 DE) and KOH-soluble fluoride was quantified (n = 20, 10 S and 10 DE). Hydroxyapatite powder produced by precipitation method was treated with the corresponding fluoride solutions for 1 min (n = 2). The formed compounds were detected using X-ray diffraction (XRD). All TiF4 varnishes produced a coating layer rich in Ti and F on all types of enamel surface, with micro-cracks in its extension. TiF4 (1.95 and 2.45% F) provided higher fluoride deposition than NaF, especially for bovine enamel (p enamel. The Ti content was higher for bovine and human primary enamel than human permanent enamel, with some differences between S and DE. The XRD analysis showed that TiF4 induced the formation of new compounds such as CaF2, TiO2, and Ti(HPO4)2·H2O. In conclusion, TiF4 (>0.95% F) interacts better, when compared to NaF, with bovine and human primary enamel than with human permanent enamel. TiF4 provoked higher F deposition compared to NaF. Carious enamel showed higher F uptake than sound enamel by TiF4 application, while Ti uptake was dependent on the enamel condition and origin. © 2017 S. Karger AG, Basel.

  4. Metallography and thermal analysis of ceramic nuclear fuels

    International Nuclear Information System (INIS)

    Tebaldi, V.

    1988-01-01

    The book contains two parts: the ceramography laboratory and the thermal treatment laboratory. After general remarks on sintering the first part includes sample preparation for ceramography (grinding, polishing, etching), microscopic examination and quantitative image analysis. The second part deals with temperature measurement, oxide/metal ratio determination, thermogravimetry, differential thermal analysis (DTA), melting point determination and constitution of phase diagrams. Installation of a Pu laboratory, sample decontamination, and research with a microprobe are described. 188 photomicrographs present the microstructure of ceramics based on U, Pu and higher actinides

  5. Automated thermal mapping techniques using chromatic image analysis

    Science.gov (United States)

    Buck, Gregory M.

    1989-01-01

    Thermal imaging techniques are introduced using a chromatic image analysis system and temperature sensitive coatings. These techniques are used for thermal mapping and surface heat transfer measurements on aerothermodynamic test models in hypersonic wind tunnels. Measurements are made on complex vehicle configurations in a timely manner and at minimal expense. The image analysis system uses separate wavelength filtered images to analyze surface spectral intensity data. The system was initially developed for quantitative surface temperature mapping using two-color thermographic phosphors but was found useful in interpreting phase change paint and liquid crystal data as well.

  6. Thermal performance analysis of a phase change thermal storage unit for space heating

    Energy Technology Data Exchange (ETDEWEB)

    Halawa, E.; Saman, W. [Institute for Sustainable Systems and Technologies School of Advanced Manufacturing and Mechanical Engineering, University of South Australia, Mawson Lakes SA 5095 (Australia)

    2011-01-15

    This paper presents the results of a comprehensive numerical study on the thermal performance of an air based phase change thermal storage unit (TSU) for space heating. The unit is designed for integration into space heating and cooling systems. The unit consists of a number of one dimensional phase change material (PCM) slabs contained in a rectangular duct where air passes between the slabs. The numerical analysis was based on an experimentally validated model. A parametric study has been carried out including the study on the effects of charge and discharge temperature differences, air mass flow rate, slab thicknesses, air gaps and slab dimensions on the air outlet temperatures and heat transfer rates of the thermal storage unit. The paper introduces and discusses quantities called charge and discharge temperature differences which play an important role in the melting and freezing processes. (author)

  7. On the analysis of the thermal line shift and thermal line width of ions in solids

    Energy Technology Data Exchange (ETDEWEB)

    Walsh, Brian M., E-mail: brian.m.walsh@nasa.gov [NASA Langley Research Center, Hampton, VA 23681 (United States); Di Bartolo, Baldassare, E-mail: baldassare.dibartolo@bc.edu [Boston College, Department of Physics, Chestnut Hill, MA 23667 (United States)

    2015-02-15

    A method of analysis for the thermally induced line shift and line width of spectral lines regarding the Raman process of ions in solids utilizing rational approximations for the Debye functions is presented. The {sup 2}E level unsplit R-line in V{sup 2+}:MgO is used as an example to illustrate the utility of the methods discussed here in providing a new analytical tool for researchers. - Highlights: • We use rational approximations for Debye functions. • We discuss limits and ranges of applicability of the rational approximations. • We formulate expressions for thermal shift and thermal linewidth for Raman processes using the rational approximations of the Debye functions. • We present an application of the methods to analyze the temperature dependent linewidth and lineshift in V2+:MgO.

  8. Global thermal analysis of air-air cooled motor based on thermal network

    Science.gov (United States)

    Hu, Tian; Leng, Xue; Shen, Li; Liu, Haidong

    2018-02-01

    The air-air cooled motors with high efficiency, large starting torque, strong overload capacity, low noise, small vibration and other characteristics, are widely used in different department of national industry, but its cooling structure is complex, it requires the motor thermal management technology should be high. The thermal network method is a common method to calculate the temperature field of the motor, it has the advantages of small computation time and short time consuming, it can save a lot of time in the initial design phase of the motor. The domain analysis of air-air cooled motor and its cooler was based on thermal network method, the combined thermal network model was based, the main components of motor internal and external cooler temperature were calculated and analyzed, and the temperature rise test results were compared to verify the correctness of the combined thermal network model, the calculation method can satisfy the need of engineering design, and provide a reference for the initial and optimum design of the motor.

  9. CFD Analysis of Thermal Control System Using NX Thermal and Flow

    Science.gov (United States)

    Fortier, C. R.; Harris, M. F. (Editor); McConnell, S. (Editor)

    2014-01-01

    The Thermal Control Subsystem (TCS) is a key part of the Advanced Plant Habitat (APH) for the International Space Station (ISS). The purpose of this subsystem is to provide thermal control, mainly cooling, to the other APH subsystems. One of these subsystems, the Environmental Control Subsystem (ECS), controls the temperature and humidity of the growth chamber (GC) air to optimize the growth of plants in the habitat. The TCS provides thermal control to the ECS with three cold plates, which use Thermoelectric Coolers (TECs) to heat or cool water as needed to control the air temperature in the ECS system. In order to optimize the TCS design, pressure drop and heat transfer analyses were needed. The analysis for this system was performed in Siemens NX Thermal/Flow software (Version 8.5). NX Thermal/Flow has the ability to perform 1D or 3D flow solutions. The 1D flow solver can be used to represent simple geometries, such as pipes and tubes. The 1D flow method also has the ability to simulate either fluid only or fluid and wall regions. The 3D flow solver is similar to other Computational Fluid Dynamic (CFD) software. TCS performance was analyzed using both the 1D and 3D solvers. Each method produced different results, which will be evaluated and discussed.

  10. de redes sem fio

    Directory of Open Access Journals (Sweden)

    William Carlos de J. Rodrigues

    2007-01-01

    Full Text Available The technique of the site survey in wireless networks makes possible the graphical mapping, the analysis of wi-fi signals and the detection of vulnerabilities in wireless networks. The acquaintance with this tool is essential to determine the viability of its implantation and to analyze radio frequency signals, collaborating to the execution of wireless networks projects with quality, efficiency and security.

  11. Determination of structural and mechanical properties, diffractometry, and thermal analysis of chitosan and hydroxypropylmethylcellulose (HPMC films plasticized with sorbitol

    Directory of Open Access Journals (Sweden)

    Jefferson Rotta

    2011-06-01

    Full Text Available In this work, the structural, mechanical, diffractometric, and thermal parameters of chitosan-hydroxypropylmethylcellulose (HPMC films plasticized with sorbitol were studied. Solutions of HPMC (2% w/v in water and chitosan (2% w/v in 2% acetic acid solution were prepared. The concentration of sorbitol used was 10% (w/w to both polymers. This solutions were mixed at different proportions (100/0; 70/30; 50/50; 30/70, and 0/100 of chitosan and HPMC, respectively, and 20 mL was cast in Petri dishes for further analysis of dried films. The miscibility of polymers was assessed by X-ray diffraction, scanning electronic microscopy (SEM, differential scanning calorimetry (DSC, and thermal gravimetric analysis (TGA. The results obtained indicate that the films are not fully miscible at a dry state despite the weak hydrogen bonding between the polymer functional groups.

  12. Development of analysis methodology on turbulent thermal stripping

    Energy Technology Data Exchange (ETDEWEB)

    Yoo, Geun Jong; Jeon, Won Dae; Han, Jin Woo; Gu, Byong Kook [Changwon National University, Changwon(Korea)

    2001-03-01

    For developing analysis methodology, important governing factors of thermal stripping phenomena are identified as geometric configuration and flow characteristics such as velocity. Along these factors, performance of turbulence models in existing analysis methodology are evaluated against experimental data. Status of DNS application is also accessed based on literature. Evaluation results are reflected in setting up the new analysis methodology. From the evaluation of existing analysis methodology, Full Reynolds Stress model is identified as best one among other turbulence models. And LES is found to be able to provide time dependent turbulence values. Further improvements in near-wall region and temperature variance equation are required for FRS and implementation of new sub-grid scale models is also required for LES. Through these improvements, new reliable analysis methodology for thermal stripping can be developed. 30 refs., 26 figs., 6 tabs. (Author)

  13. Determination of Polymers Thermal Degradation by Color Change Analysis

    Directory of Open Access Journals (Sweden)

    Andrés Felipe Rojas González

    2016-01-01

    Full Text Available Context: It has been observed that thermal degradation of thermoplastic polymers, when they are reprocessed by injection, extrusion and extrusion / injection, undergo color changes in the product, although it not has been established as this change occurs. Method: It analyzed the effect on thermal degradation caused by polymer type, processing type, polymer grade, rotation speed of the extrusion screw and number of reprocessing, which is quantified by the color change using an empirical equation, with experimental data obtained by analysis through a microcolor colorimeter. Results: It was found that the color change analysis provides information about progress of the thermal degradation and stability of thermoplastic polymers, which are undergoing to multiple reprocessing events and processes. Conclusions: It was established that this technique can be implemented as a simple and efficient measure of thermoplastic products quality control, according to their color change.

  14. PANTHER - Polarisation Analysis with Thermal neutron

    International Nuclear Information System (INIS)

    Deen, P.P.; Fennell, T.; Schober, H.; Orecchini, A.; Rols, S.; Andersen, K.H.; Stewart, J.R.

    2011-01-01

    PANTHER will build on the success of IN4, the world's most intense time-of-flight spectrometer. A large position-sensitive detector (PSD) will improve data collection rates significantly, the background will be greatly reduced, and it will incorporate features indispensable for magnetic studies (small angles, polarisation analysis, high magnetic field devices). The new instrument will enable rapid surveys of (Q,ω) space, as well as more detailed studies in fields ranging from magnetism to the structural excitations - phonon densities of states, dispersion of collective modes and molecular vibrations - that govern the behaviour of many important physical and chemical systems. (authors)

  15. Chromatic Image Analysis For Quantitative Thermal Mapping

    Science.gov (United States)

    Buck, Gregory M.

    1995-01-01

    Chromatic image analysis system (CIAS) developed for use in noncontact measurements of temperatures on aerothermodynamic models in hypersonic wind tunnels. Based on concept of temperature coupled to shift in color spectrum for optical measurement. Video camera images fluorescence emitted by phosphor-coated model at two wavelengths. Temperature map of model then computed from relative brightnesses in video images of model at those wavelengths. Eliminates need for intrusive, time-consuming, contact temperature measurements by gauges, making it possible to map temperatures on complex surfaces in timely manner and at reduced cost.

  16. Thermal-economic analysis of cogeneration systems

    International Nuclear Information System (INIS)

    Walter, A.C.S.; Bajay, S.V.

    1992-01-01

    Approximately 80 countries produce sugar, and fortuitously alcohol, from sugar cane. In all these countries the cogeneration technology of steam turbines is utilized, although almost always inefficient. The greater potential of cogeneration in Brazil is in sugar and alcohol sector, because of the use of sugar cane bagasse as combustible. This work applies the techniques of simulation and economic analysis to different configuration of plants, to determine power generation and associated costs of each alternative. The application of the same procedure at operating condition of several configurations in transient system permits the determination of production profile of exceeding during one day. (C.M.)

  17. Thermodynamic analysis of thermal efficiency and power of Minto engine

    International Nuclear Information System (INIS)

    He, Wei; Hou, Jingxin; Zhang, Yang; Ji, Jie

    2011-01-01

    Minto engine is a kind of liquid piston heat engine that operates on a small temperature gradient. But there is no power formula for it yet. And its thermal efficiency is low and formula sometimes is misused. In this paper, deriving the power formula and simplifying the thermal efficiency formula of Minto engine based on energy distribution analysis will be discussed. To improve the original Minto engine, a new design of improved Minto engine is proposed and thermal efficiency formula and power formula are also given. A computer program was developed to analyze thermal efficiency and power of original and improved Minto engines operating between low and high-temperature heat sources. The simulation results show that thermal efficiency of improved Minto engine can reach over 7% between 293.15 K and 353.15 K which is much higher than that of original one; the temperature difference between upper and lower containers is lower than half of that between low and high temperature of heat sources when the original Minto engines output the maximum power; on the contrary, it is higher in the improved Minto engines. -- Highlights: ► The thermal efficiency formula of Minto engine is simplified and the power formula is established. ► A high-powered design of improved Minto engine is proposed. ► A computer simulation program based on real operating environment is developed.

  18. Thermal Management Tools for Propulsion System Trade Studies and Analysis

    Science.gov (United States)

    McCarthy, Kevin; Hodge, Ernie

    2011-01-01

    Energy-related subsystems in modern aircraft are more tightly coupled with less design margin. These subsystems include thermal management subsystems, vehicle electric power generation and distribution, aircraft engines, and flight control. Tighter coupling, lower design margins, and higher system complexity all make preliminary trade studies difficult. A suite of thermal management analysis tools has been developed to facilitate trade studies during preliminary design of air-vehicle propulsion systems. Simulink blocksets (from MathWorks) for developing quasi-steady-state and transient system models of aircraft thermal management systems and related energy systems have been developed. These blocksets extend the Simulink modeling environment in the thermal sciences and aircraft systems disciplines. The blocksets include blocks for modeling aircraft system heat loads, heat exchangers, pumps, reservoirs, fuel tanks, and other components at varying levels of model fidelity. The blocksets have been applied in a first-principles, physics-based modeling and simulation architecture for rapid prototyping of aircraft thermal management and related systems. They have been applied in representative modern aircraft thermal management system studies. The modeling and simulation architecture has also been used to conduct trade studies in a vehicle level model that incorporates coupling effects among the aircraft mission, engine cycle, fuel, and multi-phase heat-transfer materials.

  19. Cooling Curve Analysis of Micro- and Nanographite Particle-Embedded Salt-PCMs for Thermal Energy Storage Applications

    Science.gov (United States)

    Sudheer, R.; Prabhu, K. N.

    2017-08-01

    In recent years, the focus of phase change materials (PCM) research was on the development of salt mixtures with particle additives to improve their thermal energy storage (TES) functionalities. The effect of addition of microsized (50 μm) and nanosized (400 nm) graphite particles on TES parameters of potassium nitrate was analyzed in this work. A novel technique of computer-aided cooling curve analysis was employed here to study the suitability of large inhomogeneous PCM samples. The addition of graphite micro- and nanoparticles reduced the solidification time of the PCM significantly enhancing the heat removal rates, in the first thermal cycle. The benefits of dispersing nanoparticles diminished in successive 10 thermal cycles, and its performance was comparable to the microparticle-embedded PCM thereafter. The decay of TES functionalities on thermal cycling is attributed to the agglomeration of nanoparticles which was observed in SEM images. The thermal diffusivity property of the PCM decreased with addition of graphite particles. With no considerable change in the cooling rates and a simultaneous decrease in thermal diffusivity, it is concluded that the addition of graphite particles increased the specific heat capacity of the PCM. It is also suggested that the additive concentration should not be greater than 0.1% by weight of the PCM sample.

  20. Thermal Analysis of Bending Under Tension Test

    DEFF Research Database (Denmark)

    Ceron, Ermanno; Martins, Paulo A.F.; Bay, Niels

    2014-01-01

    during testing is similar to the one in the production tool. A universal sheet tribo-tester has been developed, which can run multiple tests automatically from coil. This allows emulating the temperature increase as in production. The present work performs finite element analysis of the evolution......The tribological conditions in deep drawing can be simulated in the Bending Under Tension test to evaluate the performance of new lubricants, tool materials, etc. Deep drawing production with automatic handling runs normally at high rate. This implies considerable heating of the tools, which...... sometimes can cause lubricant film breakdown and galling. In order to replicate the production conditions in bending under tension testing it is thus important to control the tool/workpiece interface temperature. This can be done by pre-heating the tool, but it is essential that the interface temperature...

  1. Product analysis for polyethylene degradation by radiation and thermal ageing

    International Nuclear Information System (INIS)

    Sugimoto, Masaki; Shimada, Akihiko; Kudoh, Hisaaki; Tamura, Kiyotoshi; Seguchi, Tadao

    2013-01-01

    The oxidation products in crosslinked polyethylene for cable insulation formed during thermal and radiation ageing were analyzed by FTIR-ATR. The products were composed of carboxylic acid, carboxylic ester, and carboxylic anhydride for all ageing conditions. The relative yields of carboxylic ester and carboxylic anhydride increased with an increase of temperature for radiation and thermal ageing. The carboxylic acid was the primary oxidation product and the ester and anhydride were secondary products formed by the thermally induced reactions of the carboxylic acids. The carboxylic acid could be produced by chain scission at any temperature followed by the oxidation of the free radicals formed in the polyethylene. The results of the analysis led to formulation of a new oxidation mechanism which was different from the chain reactions via peroxy radicals and peroxides. - Highlights: ► Products analysis of polyethylene degradation by radiation and thermal ageing. ► Components of carbonyl compounds produced in polyethylene by thermal and radiation oxidation were determined by FTIR. ► Carbonyl compounds comprised carboxylic acid, carboxylic ester, and carboxylic anhydride. ► Carboxylic acid was the primary oxidation product of chain scission at any oxidation temperature. ► Carboxylic ester and carboxylic anhydride are secondary products formed from carboxylic acid at higher temperature.

  2. Analysis of piping response to thermal and operational transients

    International Nuclear Information System (INIS)

    Wang, C.Y.

    1987-01-01

    The reactor piping system is an extremely complex three-dimensional structure. Maintaining its structural integrity is essential to the safe operation of the reactor and the steam-supply system. In the safety analysis, various transient loads can be imposed on the piping which may cause plastic deformation and possible damage to the system, including those generated from hydrodynamic wave propagations, thermal and operational transients, as well as the seismic events. At Argonne National Laboratory (ANL), a three-dimensional (3-D) piping code, SHAPS, aimed for short-duration transients due to wave propagation, has been developed. Since 1984, the development work has been shifted to the long-duration accidents originating from the thermal and operational transient. As a result, a new version of the code, SHAPS-2, is being established. This paper describes many features related to this later development. To analyze piping response generated from thermal and operational transients, a 3-D implicit finite element algorithm has been developed for calculating the hoop, flexural, axial, and torsional deformations induced by the thermomechanical loads. The analysis appropriately accounts for stresses arising from the temperature dependence of the elastic material properties, the thermal expansion of the materials, and the changes in the temperature-dependent yield surface. Thermal softening, failure, strain rate, creep, and stress ratching can also be considered

  3. Heat transfer and thermal stress analysis in grooved tubes

    Indian Academy of Sciences (India)

    Heat transfer and thermal stresses, induced by temperature differencesin the internally grooved tubes of heat transfer equipment, have been analysed numerically. The analysis has been conducted for four different kinds of internally grooved tubes and three different mean inlet water velocities. Constant temperature was ...

  4. Thermal analysis of building roof assisted with water heater and ...

    Indian Academy of Sciences (India)

    D Prakash

    2018-03-14

    Mar 14, 2018 ... Thermal analysis; building roof; solar water heating system; roof ... These solar collec- ... several benefits, such as its wide range of storage temper- ... rugated plate, rear plate and back insulation material [12]. ..... [7] Weiss W and Rommel M 2008 Process heat collectors. State of the art within Task 33/IV.

  5. Thermal stresses in the space shuttle orbiter: Analysis versus test

    International Nuclear Information System (INIS)

    Grooms, H.R.; Gibson, W.F. Jr.; Benson, P.L.

    1984-01-01

    Significant temperature differences occur between the internal structure and the outer skin of the Space Shuttle Orbiter as it returns from space. These temperature differences cause important thermal stresses. A finite element model containing thousands of degrees of freedom is used to predict these stresses. A ground test was performed to verify the prediction method. The analysis and test results compare favorably. (orig.)

  6. Thermo-economic analysis of Shiraz solar thermal power plant

    Energy Technology Data Exchange (ETDEWEB)

    Yaghoubi, M. [Academy of Science, Tehran (Iran, Islamic Republic of); Mokhtari, A.; Hesami, R. [Shiraz Univ., Shiraz (Iran, Islamic Republic of). School of Engineering

    2007-07-01

    The Shiraz solar thermal power plant in Iran has 48 parabolic trough collectors (PTCs) which are used to heat the working oil. There is potential to significantly increase the performance and reduce the cost of PTC solar thermal electric technologies. Conventional energy analysis based on the first law of thermodynamics does qualitatively assess the various losses occurring in the components. Therefore, exergy analysis, based on the second law of thermodynamics, can be applied to better assess various losses quantitatively as well as qualitatively. This paper presented a newly developed exergy-economic model for the Shiraz solar thermal power plant. The objective was to find the minimum exergetic production cost (EPC), based on the second law of thermodynamics. The application of exergy-economic analysis includes the evaluation of utility supply costs for production plants, and the energy costs for process operations. The purpose of the analysis was to minimize the total operating costs of the solar thermal power plant by assuming a fixed rate of electricity production and process steam. 21 refs., 3 tabs., 8 figs.

  7. Occupancy Analysis of Sports Arenas Using Thermal Imaging

    DEFF Research Database (Denmark)

    Gade, Rikke; Jørgensen, Anders; Moeslund, Thomas B.

    2012-01-01

    This paper presents a system for automatic analysis of the occupancy of sports arenas. By using a thermal camera for image capturing the number of persons and their location on the court are found without violating any privacy issues. The images are binarised with an automatic threshold method...

  8. Advanced metrology by offline SEM data processing

    Science.gov (United States)

    Lakcher, Amine; Schneider, Loïc.; Le-Gratiet, Bertrand; Ducoté, Julien; Farys, Vincent; Besacier, Maxime

    2017-06-01

    Today's technology nodes contain more and more complex designs bringing increasing challenges to chip manufacturing process steps. It is necessary to have an efficient metrology to assess process variability of these complex patterns and thus extract relevant data to generate process aware design rules and to improve OPC models. Today process variability is mostly addressed through the analysis of in-line monitoring features which are often designed to support robust measurements and as a consequence are not always very representative of critical design rules. CD-SEM is the main CD metrology technique used in chip manufacturing process but it is challenged when it comes to measure metrics like tip to tip, tip to line, areas or necking in high quantity and with robustness. CD-SEM images contain a lot of information that is not always used in metrology. Suppliers have provided tools that allow engineers to extract the SEM contours of their features and to convert them into a GDS. Contours can be seen as the signature of the shape as it contains all the dimensional data. Thus the methodology is to use the CD-SEM to take high quality images then generate SEM contours and create a data base out of them. Contours are used to feed an offline metrology tool that will process them to extract different metrics. It was shown in two previous papers that it is possible to perform complex measurements on hotspots at different process steps (lithography, etch, copper CMP) by using SEM contours with an in-house offline metrology tool. In the current paper, the methodology presented previously will be expanded to improve its robustness and combined with the use of phylogeny to classify the SEM images according to their geometrical proximities.

  9. Spent nuclear fuel storage pool thermal-hydraulic analysis

    International Nuclear Information System (INIS)

    Gay, R.R.

    1984-01-01

    Storage methods and requirements for spent nuclear fuel at U.S. commercial light water reactors are reviewed in Section 1. Methods of increasing current at-reactor storage capabilities are also outlined. In Section 2 the development of analytical methods for the thermal-hydraulic analysis of spent fuel pools is chronicled, leading up to a discussion of the GFLOW code which is described in Section 3. In Section 4 the verification of GFLOW by comparisons of the code's predictions to experimental data taken inside the fuel storage pool at the Maine Yankee nuclear power plant is presented. The predictions of GFLOW using 72, 224, and 1584 node models of the storage pool are compared to each other and to the experimental data. An example of thermal licensing analysis for Maine Yankee using the GFLOW code is given in Section 5. The GFLOW licensing analysis is compared to previous licensing analysis performed by Yankee Atomic using the RELAP-4 computer code

  10. Differential-thermal analysis of irradiated lignite

    International Nuclear Information System (INIS)

    Chichek, F; Eyubova, N.

    2006-01-01

    Full text: In this theme our purpose is to explain thermo-differential analysis of lignite's irradiated. During experiment Caraman Ermenek (washed), Caraman Ermenek (crude), Nevshehir (crude), Slopi (crude), Trakya Harman (washed) lignite coals were used. Five of five kinds of coal samples with 3mm and 1 gr of each sample were obtained. Then they were filled into the Tubes after having dried total 25 samples with 1 gr at 1000C temperature for one hour. Air in the tubes was pumped out and closed. Coal samples in vacuum medium were irradiated by gamma rays of Co-60 at 5.5 kGy, 19.2 kGy, 65.7 kGy, 169.6 kGy, 411.2 kGy, doses to the normal conditions. At the end coal irradiated samples were compared with original coal samples. At the result of experiment it was revealed that in comparison with original coal samples coal samples irradiated from exothermic and endothermic curves at very reaction pick and temperature intervals of these pick were large. Besides loss of weight was observed to begin at low temperatures in samples irradiated and especially momentary weight loss at some heats in the rang of known temperatures was observed in the coal Slopi contain in bitumen. Because of heat the weight loss in the non irradiated samples forms parabolic curve and because of heat the weight loss in the samples irradiated forms stepped curves. It was shown that the coal irradiated can be easily departed by heat because of the chemical structure in comparison the original one.

  11. Studies of the thermal properties of horn keratin by dielectric spectroscopy, thermogravimetric analysis and differential thermal analysis

    International Nuclear Information System (INIS)

    Marzec, E.; Piskunowicz, P.; Jaroszyk, F.

    2002-01-01

    The dielectric and thermal properties of horn keratin have been studied bu dielectric spectroscopy in the frequency range 10 1 -10 5 Hz, thermogravimetric analysis (TG) and different thermal analysis (DTA). Measurement of non-irradiated and g amma - irradiated keratin with doses 5, 50 kGy were performed at temperature from 22 to 260 o C. The results revealed the occurrence of phase transitions related to release of loosely bound water and bound water up to 200 o Cand the denaturation of the crystalline structure above this temperature. The influence of γ-irradiation on the thermal behaviour of keratin is significant only in the temperature range of denaturation. The decrease in the temperature of denaturation would suggest that γ-irradiation initiates main-chain degradation. (authors)

  12. Investigation on by-products of bioenergy systems (anaerobic digestion and gasification) as potential crop nutrient using FTIR, XRD, SEM analysis and phyto-toxicity test.

    Science.gov (United States)

    Kataki, Sampriti; Hazarika, Samarendra; Baruah, D C

    2017-07-01

    Success and acceptability of the bio energy conversion technology to a large extent depend upon management of the inevitable by-products generated during the conversion process. By-products can be considered favourable as organic fertilizer as they retain nutrients with varying composition depending upon input biomass. However, characteristics of these heterogeneous resources with respect to feedstock and processing conditions have to be assessed to state on their agricultural and environmental benefits. Therefore, 3 types of anaerobic digestion by-products (digestate) from surplus biomass viz. cow dung, Ipomoea carnea:cow dung (60:40 dry weight basis) and rice straw:green gram stover:cow dung (30:30:40 dry weight basis) and one gasification by-product (biochar) from rice husk are considered to understand the fertilizer prospects. Considering 3 potential application options, digestate from each feedstock option was further processed as separated solid, separated liquid and ash from solid digestates. Thus, a total of 10 by-products were investigated for understanding their prospects as fertilizer using Fourier Transform Infrared Spectroscopy (FTIR), X-ray diffraction (XRD), Scanning Electron Microscopy (SEM) and Energy Dispersive X ray Spectroscopy (EDX) and phyto-toxicity test to have a broad insight in terms of their organic, mineral, elemental composition, morphological feature and potential phyto-toxicity. In general, irrespective of origin of feedstock, solid digestate, ash digestate and char showed similarity in terms of composition of functional groups with some degree of variation in relative content as reflected by FTIR analysis. Dominance of organic functional groups in separated solid digestates compared to liquid fraction indicated the former as favourable organic amendments. Quartz was the prevalent mineral phase in all separated solid, ash digestate and rice husk char. Digestates in ash phase represent more concentrated plant nutrient source with

  13. CFD and thermal analysis applications at General Motors

    International Nuclear Information System (INIS)

    Johnson, J.P.

    2002-01-01

    The presentation will include a brief history of the growth of CFD and thermal analysis in GM's vehicle program divisions. Its relationship to the underlying computer infrastructure will be sketched. Application results will be presented for calculations in aerodynamics, flow through heat exchangers, engine compartment thermal studies, HVAC systems and others. Current technical challenges will be outlined including grid generation, turbulence modeling, heat transfer, and solution algorithms. The introduction of CFD and heat transfer results into Virtual Vehicle Reviews, and its potential impact on a company's CAE infrastructure will be noted. Finally, some broad comments will be made on the management of CFD and heat transfer technology across a global corporate enterprise. (author)

  14. Interim report on nuclear waste depository thermal analysis

    International Nuclear Information System (INIS)

    Altenbach, T.J.

    1978-01-01

    A thermal analysis of a deep geologic depository for spent nuclear fuel is being conducted. The TRUMP finite difference heat transfer code is used to analyze a 3-dimensional model of the depository. The model uses a unit cell consisting of one spent fuel canister buried in salt beneath a ventilated room in the depository. A base case was studied along with several parametric variations. It is concluded that this method is appropriate for analyzing the thermal response of the system, and that the most important parameter in determining the maximum temperatures is the canister heat generation rate. The effects of room ventilation and different depository media are secondary

  15. Thermally emissive sensing materials for chemical spectroscopy analysis

    Science.gov (United States)

    Poole, Zsolt; Ohodnicki, Paul R.

    2018-05-08

    A sensor using thermally emissive materials for chemical spectroscopy analysis includes an emissive material, wherein the emissive material includes the thermally emissive materials which emit electromagnetic radiation, wherein the electromagnetic radiation is modified due to chemical composition in an environment; and a detector adapted to detect the electromagnetic radiation, wherein the electromagnetic radiation is indicative of the chemical interaction changes and hence chemical composition and/or chemical composition changes of the environment. The emissive material can be utilized with an optical fiber sensor, with the optical fiber sensor operating without the emissive material probed with a light source external to the material.

  16. Mathematical model for thermal and entropy analysis of thermal solar collectors by using Maxwell nanofluids with slip conditions, thermal radiation and variable thermal conductivity

    Science.gov (United States)

    Aziz, Asim; Jamshed, Wasim; Aziz, Taha

    2018-04-01

    In the present research a simplified mathematical model for the solar thermal collectors is considered in the form of non-uniform unsteady stretching surface. The non-Newtonian Maxwell nanofluid model is utilized for the working fluid along with slip and convective boundary conditions and comprehensive analysis of entropy generation in the system is also observed. The effect of thermal radiation and variable thermal conductivity are also included in the present model. The mathematical formulation is carried out through a boundary layer approach and the numerical computations are carried out for Cu-water and TiO2-water nanofluids. Results are presented for the velocity, temperature and entropy generation profiles, skin friction coefficient and Nusselt number. The discussion is concluded on the effect of various governing parameters on the motion, temperature variation, entropy generation, velocity gradient and the rate of heat transfer at the boundary.

  17. Building a SEM Analytics Reporting Portfolio

    Science.gov (United States)

    Goff, Jay W.; Williams, Brian G.; Kilgore, Wendy

    2016-01-01

    Effective strategic enrollment management (SEM) efforts require vast amounts of internal and external data to ensure that meaningful reporting and analysis systems can assist managers in decision making. A wide range of information is integral for leading effective and efficient student recruitment and retention programs. This article is designed…

  18. A computational model for thermal fluid design analysis of nuclear thermal rockets

    International Nuclear Information System (INIS)

    Given, J.A.; Anghaie, S.

    1997-01-01

    A computational model for simulation and design analysis of nuclear thermal propulsion systems has been developed. The model simulates a full-topping expander cycle engine system and the thermofluid dynamics of the core coolant flow, accounting for the real gas properties of the hydrogen propellant/coolant throughout the system. Core thermofluid studies reveal that near-wall heat transfer models currently available may not be applicable to conditions encountered within some nuclear rocket cores. Additionally, the possibility of a core thermal fluid instability at low mass fluxes and the effects of the core power distribution are investigated. Results indicate that for tubular core coolant channels, thermal fluid instability is not an issue within the possible range of operating conditions in these systems. Findings also show the advantages of having a nonflat centrally peaking axial core power profile from a fluid dynamic standpoint. The effects of rocket operating conditions on system performance are also investigated. Results show that high temperature and low pressure operation is limited by core structural considerations, while low temperature and high pressure operation is limited by system performance constraints. The utility of these programs for finding these operational limits, optimum operating conditions, and thermal fluid effects is demonstrated

  19. Chemical and thermal analysis for characterisation of building materials

    International Nuclear Information System (INIS)

    Kumar, S.C.; Sudersanan, M.; Ravindran, P.V.; Kalekar, B.B.; Mathur, P.K.

    2000-01-01

    Cement and other construction materials are extensively used for the construction of shielding materials for nuclear and high energy radiations. The design and optimum utilisation of such materials need an accurate analysis of their chemical composition. The moisture content and presence of bound water and other volatile materials are also important. The use of thermal analysis supplements the data obtained by chemical analysis and enables a distinction of moisture and chemically bound water. It also enables an identification of the process leading to the loss on ignition. The work carried out on the analysis of sand, cement and other aggregate materials used for the preparation of concrete is described in the paper. (author)

  20. Horizontal steam generator PGV-1000 thermal-hydraulic analysis

    Energy Technology Data Exchange (ETDEWEB)

    Ubra, O. [Skoda Company, Prague (Switzerland); Doubek, M. [Czech Technical Univ., Prague (Switzerland)

    1995-12-31

    A computer program for the steady state thermal-hydraulic analysis of horizontal steam generator PGV-1000 is presented. The program provides the capability to analyze steam generator PGV-1000 primary side flow and temperature distribution, primary side pressure drops, heat transfer between the primary and secondary sides and multidimensional heat flux distribution. A special attention is paid to the thermal-hydraulics of the secondary side. The code predicts 3-D distribution of the void fraction at the secondary side, mass redistribution under the submerged perforated sheet and the steam generator level profile. By means of developed computer program a detailed thermal-hydraulic study of the PGV-1000 has been carried out. A wide range of calculations has been performed and a set of important steam generator characteristics has been obtained. Some of them are presented in the paper. (orig.). 5 refs.

  1. Photovoltaic thermal module concepts and their performance analysis: A review

    International Nuclear Information System (INIS)

    Hasan, M. Arif; Sumathy, K.

    2010-01-01

    This paper presents a review of the available literature covering the latest module aspects of different photovoltaic/thermal (PV/T) collectors and their performances in terms of electrical as well as thermal output. The review covers detailed description of flat-plate and concentrating PV/T systems, using liquid or air as the working fluid, numerical model analysis, experimental work and qualitative evaluation of thermal and electrical output. Also an in-depth review on the performance parameters such as, optimum mass flow rate, PV/T dimensions, air channel geometry is presented in this study. Based on the thorough review, it is clear that PV/T modules are very promising devices and there exists lot of scope to further improve their performances. Appropriate recommendations are made which will aid PV/T systems to improve their efficiency and reducing their cost, making them more competitive in the present market. (author)

  2. Non-linear elastic thermal stress analysis with phase changes

    International Nuclear Information System (INIS)

    Amada, S.; Yang, W.H.

    1978-01-01

    The non-linear elastic, thermal stress analysis with temperature induced phase changes in the materials is presented. An infinite plate (or body) with a circular hole (or tunnel) is subjected to a thermal loading on its inner surface. The peak temperature around the hole reaches beyond the melting point of the material. The non-linear diffusion equation is solved numerically using the finite difference method. The material properties change rapidly at temperatures where the change of crystal structures and solid-liquid transition occur. The elastic stresses induced by the transient non-homogeneous temperature distribution are calculated. The stresses change remarkably when the phase changes occur and there are residual stresses remaining in the plate after one cycle of thermal loading. (Auth.)

  3. Horizontal steam generator PGV-1000 thermal-hydraulic analysis

    International Nuclear Information System (INIS)

    Ubra, O.; Doubek, M.

    1995-01-01

    A computer program for the steady state thermal-hydraulic analysis of horizontal steam generator PGV-1000 is presented. The program provides the capability to analyze steam generator PGV-1000 primary side flow and temperature distribution, primary side pressure drops, heat transfer between the primary and secondary sides and multidimensional heat flux distribution. A special attention is paid to the thermal-hydraulics of the secondary side. The code predicts 3-D distribution of the void fraction at the secondary side, mass redistribution under the submerged perforated sheet and the steam generator level profile. By means of developed computer program a detailed thermal-hydraulic study of the PGV-1000 has been carried out. A wide range of calculations has been performed and a set of important steam generator characteristics has been obtained. Some of them are presented in the paper. (orig.)

  4. Horizontal steam generator PGV-1000 thermal-hydraulic analysis

    Energy Technology Data Exchange (ETDEWEB)

    Ubra, O [Skoda Company, Prague (Switzerland); Doubek, M [Czech Technical Univ., Prague (Switzerland)

    1996-12-31

    A computer program for the steady state thermal-hydraulic analysis of horizontal steam generator PGV-1000 is presented. The program provides the capability to analyze steam generator PGV-1000 primary side flow and temperature distribution, primary side pressure drops, heat transfer between the primary and secondary sides and multidimensional heat flux distribution. A special attention is paid to the thermal-hydraulics of the secondary side. The code predicts 3-D distribution of the void fraction at the secondary side, mass redistribution under the submerged perforated sheet and the steam generator level profile. By means of developed computer program a detailed thermal-hydraulic study of the PGV-1000 has been carried out. A wide range of calculations has been performed and a set of important steam generator characteristics has been obtained. Some of them are presented in the paper. (orig.). 5 refs.

  5. Photovoltaic thermal module concepts and their performance analysis: A review

    Energy Technology Data Exchange (ETDEWEB)

    Hasan, M. Arif; Sumathy, K. [Department of Mechanical Engineering, North Dakota State University, Fargo, ND (United States)

    2010-09-15

    This paper presents a review of the available literature covering the latest module aspects of different photovoltaic/thermal (PV/T) collectors and their performances in terms of electrical as well as thermal output. The review covers detailed description of flat-plate and concentrating PV/T systems, using liquid or air as the working fluid, numerical model analysis, experimental work and qualitative evaluation of thermal and electrical output. Also an in-depth review on the performance parameters such as, optimum mass flow rate, PV/T dimensions, air channel geometry is presented in this study. Based on the thorough review, it is clear that PV/T modules are very promising devices and there exists lot of scope to further improve their performances. Appropriate recommendations are made which will aid PV/T systems to improve their efficiency and reducing their cost, making them more competitive in the present market. (author)

  6. Kinetic analysis of thermally relativistic flow with dissipation

    International Nuclear Information System (INIS)

    Yano, Ryosuke; Suzuki, Kojiro

    2011-01-01

    Nonequilibrium flow of thermally relativistic matter with dissipation is considered in the framework of the relativistic kinetic theory. As an object of the analysis, the supersonic rarefied flow of thermally relativistic matter around the triangle prism is analyzed using the Anderson-Witting model. Obtained numerical results indicate that the flow field changes in accordance with the flow velocity and temperature of the uniform flow owing to both effects derived from the Lorentz contraction and thermally relativistic effects, even when the Mach number of the uniform flow is fixed. The profiles of the heat flux along the stagnation streamline can be approximated on the basis of the relativistic Navier-Stokes-Fourier (NSF) law except for a strong nonequilibrium regime such as the middle of the shock wave and the vicinity of the wall, whereas the profile of the heat flux behind the triangle prism cannot be approximated on the basis of the relativistic NSF law owing to rarefied effects via the expansion behind the triangle prism. Additionally, the heat flux via the gradient of the static pressure is non-negligible owing to thermally relativistic effects. The profile of the dynamic pressure is different from that approximated on the basis of the NSF law, which is obtained by the Eckart decomposition. Finally, variations of convections of the mass and momentum owing to the effects derived from the Lorentz contraction and thermally relativistic effects are numerically confirmed.

  7. Thermal analysis of the vertical disposal for HLW

    International Nuclear Information System (INIS)

    Zhao Honggang; Wang Ju; Liu Yuemiao; Su Rui

    2013-01-01

    The temperature on the canister surface is set to be no more than 100℃ in the high level radioactive waste (HLW) repository, it is a criterion to dictate the thermal dimension of the repository. The factors that affect the temperature on the canister surface include the initial power of the canister, the thermal properties of material as the engineered barrier system (EBS), the gaps around the canister in the EBS, the initial ground temperature and thermal properties of the host rock, the repository layout, etc. This article examines the thermal properties of the material in host rock and the EBS, the thermal conductivity properties of the different gaps in the EBS, the temperature evolution around the single canister by using the analysis method and the numerical method. The findings are as follows: 1) The most important and the sensitive parameter is the initial disposal power of the canister; 2) The two key factors that affect the highest temperature on the canister surface are the parameter of uncertainty and nature variability of material as the host rock and the EBS, and the gaps around the canister in the EBS; 3) The temperature difference between the canister and bentonite is no more than 10℃ , and the bigger the inner gaps are, the bigger the temperature difference will be; when the gap between the bentonite and the host rock is filled with water, the temperature difference becomes small, but it will be 1∼3℃ higher than the gaps filled will air. (authors)

  8. Thermal hydrodynamic analysis of a countercurrent gas centrifuge

    International Nuclear Information System (INIS)

    Andrade, Delvonei Alves de

    1999-01-01

    The influence of the thermal countercurrent on the separative performance of countercurrent centrifuges is treated in this work. The methodology used consists in modeling the gas flow inside the rotor under thermal boundary conditions supplied by the structural thermal model. The gas flow model, also called hydrodynamical model, is based on the Finite Volume Method for cylindrical geometry with azimuthal symmetry. The structural thermal model is based on the Nodal Method and take into account simultaneously, the conduction convection and radiation phenomena. The procedure adopted for this study consisted in the definition of the operational and geometric conditions of a centrifuge which was used as a pattern to the accomplished analysis. This configuration, called 'Standard Centrifuge', was used for the accomplishment of several simulations where the importance of the realistic boundary thermal conditions for the numerical evaluation of the centrifuge separative capacity was evidenced. A selective alteration for the optical properties based on simple engineering procedures was proposed. An improvement of 5% was obtained with this alteration. (author)

  9. FIB-SEM tomography in biology.

    Science.gov (United States)

    Kizilyaprak, Caroline; Bittermann, Anne Greet; Daraspe, Jean; Humbel, Bruno M

    2014-01-01

    Three-dimensional information is much easier to understand than a set of two-dimensional images. Therefore a layman is thrilled by the pseudo-3D image taken in a scanning electron microscope (SEM) while, when seeing a transmission electron micrograph, his imagination is challenged. First approaches to gain insight in the third dimension were to make serial microtome sections of a region of interest (ROI) and then building a model of the object. Serial microtome sectioning is a tedious and skill-demanding work and therefore seldom done. In the last two decades with the increase of computer power, sophisticated display options, and the development of new instruments, an SEM with a built-in microtome as well as a focused ion beam scanning electron microscope (FIB-SEM), serial sectioning, and 3D analysis has become far easier and faster.Due to the relief like topology of the microtome trimmed block face of resin-embedded tissue, the ROI can be searched in the secondary electron mode, and at the selected spot, the ROI is prepared with the ion beam for 3D analysis. For FIB-SEM tomography, a thin slice is removed with the ion beam and the newly exposed face is imaged with the electron beam, usually by recording the backscattered electrons. The process, also called "slice and view," is repeated until the desired volume is imaged.As FIB-SEM allows 3D imaging of biological fine structure at high resolution of only small volumes, it is crucial to perform slice and view at carefully selected spots. Finding the region of interest is therefore a prerequisite for meaningful imaging. Thin layer plastification of biofilms offers direct access to the original sample surface and allows the selection of an ROI for site-specific FIB-SEM tomography just by its pronounced topographic features.

  10. Ionic liquid thermal stabilities: decomposition mechanisms and analysis tools.

    Science.gov (United States)

    Maton, Cedric; De Vos, Nils; Stevens, Christian V

    2013-07-07

    The increasing amount of papers published on ionic liquids generates an extensive quantity of data. The thermal stability data of divergent ionic liquids are collected in this paper with attention to the experimental set-up. The influence and importance of the latter parameters are broadly addressed. Both ramped temperature and isothermal thermogravimetric analysis are discussed, along with state-of-the-art methods, such as TGA-MS and pyrolysis-GC. The strengths and weaknesses of the different methodologies known to date demonstrate that analysis methods should be in line with the application. The combination of data from advanced analysis methods allows us to obtain in-depth information on the degradation processes. Aided with computational methods, the kinetics and thermodynamics of thermal degradation are revealed piece by piece. The better understanding of the behaviour of ionic liquids at high temperature allows selective and application driven design, as well as mathematical prediction for engineering purposes.

  11. Analysis of phase formation in Ni-rich alloys of the Ni-Ta-W system by calorimetry, DTA, SEM, and TEM

    Energy Technology Data Exchange (ETDEWEB)

    Witusiewicz, V.T.; Hecht, U.; Warnken, N.; Fries, S.G. [Access e.V., Aachen (Germany); Hu Weiping [Inst. fuer Metallkunde und Metallphysik der RWTH Aachen (Germany)

    2006-04-15

    The partial enthalpies of dissolution of pure Ni, W and Ta in liquid ternary Ni-Ta-W alloys have been determined at (1773 {+-} 5) K using a high temperature isoperibolic calorimeter. Measurements were performed in Ni-rich alloys (from 80 to 100 at.% Ni) along sections with constant Ta:W atomic ratios 1:0, 2:1, 1:2, and 0:1. The partial enthalpies and thereby the integral enthalpy of mixing of these ternary alloys are calculated from the partial enthalpies of dissolution using SGTE Gibbs energies for pure elements as reference. The obtained thermochemical data confirm that in the investigated Ni-rich alloys the binary interactions between Ta and W as well as the ternary Ni-Ta-W interactions are negligibly small. Due to this the variation of the integral enthalpy of mixing of the ternary alloys is well described as linear combination of the constituent Ni-Ta and Ni-W binaries. Such behaviour of the ternary liquid alloys is related to a very low probability of new ternary stable phases to occur in solid state. This prediction is confirmed by differential thermal analysis, scanning electron microscopy, and transmission electron microscopy of the as-solidified and annealed samples obtained as last alloy compositions in the series of calorimetric dissolution. (orig.)

  12. Disilicate Dental Ceramic Surface Preparation by 1070 nm Fiber Laser: Thermal and Ultrastructural Analysis

    Directory of Open Access Journals (Sweden)

    Carlo Fornaini

    2018-01-01

    Full Text Available Lithium disilicate dental ceramic bonding, realized by using different resins, is strictly dependent on micro-mechanical retention and chemical adhesion. The aim of this in vitro study was to investigate the capability of a 1070 nm fiber laser for their surface treatment. Samples were irradiated by a pulsed fiber laser at 1070 nm with different parameters (peak power of 5, 7.5 and 10 kW, repetition rate (RR 20 kHz, speed of 10 and 50 mm/s, and total energy density from 1.3 to 27 kW/cm2 and the thermal elevation during the experiment was recorded by a fiber Bragg grating (FBG temperature sensor. Subsequently, the surface modifications were analyzed by optical microscope, scanning electron microscope (SEM, and energy dispersive X-ray spectroscopy (EDS. With a peak power of 5 kW, RR of 20 kHz, and speed of 50 mm/s, the microscopic observation of the irradiated surface showed increased roughness with small areas of melting and carbonization. EDS analysis revealed that, with these parameters, there are no evident differences between laser-processed samples and controls. Thermal elevation during laser irradiation ranged between 5 °C and 9 °C. A 1070 nm fiber laser can be considered as a good device to increase the adhesion of lithium disilicate ceramics when optimum parameters are considered.

  13. Quantitative subsurface analysis using frequency modulated thermal wave imaging

    Science.gov (United States)

    Subhani, S. K.; Suresh, B.; Ghali, V. S.

    2018-01-01

    Quantitative depth analysis of the anomaly with an enhanced depth resolution is a challenging task towards the estimation of depth of the subsurface anomaly using thermography. Frequency modulated thermal wave imaging introduced earlier provides a complete depth scanning of the object by stimulating it with a suitable band of frequencies and further analyzing the subsequent thermal response using a suitable post processing approach to resolve subsurface details. But conventional Fourier transform based methods used for post processing unscramble the frequencies with a limited frequency resolution and contribute for a finite depth resolution. Spectral zooming provided by chirp z transform facilitates enhanced frequency resolution which can further improves the depth resolution to axially explore finest subsurface features. Quantitative depth analysis with this augmented depth resolution is proposed to provide a closest estimate to the actual depth of subsurface anomaly. This manuscript experimentally validates this enhanced depth resolution using non stationary thermal wave imaging and offers an ever first and unique solution for quantitative depth estimation in frequency modulated thermal wave imaging.

  14. Using fractal analysis of thermal signatures for thyroid disease evaluation

    Science.gov (United States)

    Gavriloaia, Gheorghe; Sofron, Emil; Gavriloaia, Mariuca-Roxana; Ghemigean, Adina-Mariana

    2010-11-01

    The skin is the largest organ of the body and it protects against heat, light, injury and infection. Skin temperature is an important parameter for diagnosing diseases. Thermal analysis is non-invasive, painless, and relatively inexpensive, showing a great potential research. Since the thyroid regulates metabolic rate it is intimately connected to body temperature, more than, any modification of its function generates a specific thermal image on the neck skin. The shapes of thermal signatures are often irregular in size and shape. Euclidean geometry is not able to evaluate their shape for different thyroid diseases, and fractal geometry is used in this paper. Different thyroid diseases generate different shapes, and their complexity are evaluated by specific mathematical approaches, fractal analysis, in order to the evaluate selfsimilarity and lacunarity. Two kinds of thyroid diseases, hyperthyroidism and papillary cancer are analyzed in this paper. The results are encouraging and show the ability to continue research for thermal signature to be used in early diagnosis of thyroid diseases.

  15. Thermal Analysis of the Fastrac Chamber/Nozzle

    Science.gov (United States)

    Davis, Darrell

    2001-01-01

    This paper will describe the thermal analysis techniques used to predict temperatures in the film-cooled ablative rocket nozzle used on the Fastrac 60K rocket engine. A model was developed that predicts char and pyrolysis depths, liner thermal gradients, and temperatures of the bondline between the overwrap and liner. Correlation of the model was accomplished by thermal analog tests performed at Southern Research, and specially instrumented hot fire tests at the Marshall Space Flight Center. Infrared thermography was instrumental in defining nozzle hot wall surface temperatures. In-depth and outboard thermocouple data was used to correlate the kinetic decomposition routine used to predict char and pyrolysis depths. These depths were anchored with measured char and pyrolysis depths from cross-sectioned hot-fire nozzles. For the X-34 flight analysis, the model includes the ablative Thermal Protection System (TPS) material that protects the overwrap from the recirculating plume. Results from model correlation, hot-fire testing, and flight predictions will be discussed.

  16. Thermal Analysis of the MC-1 Chamber/Nozzle

    Science.gov (United States)

    Davis, Darrell W.; Phelps, Lisa H. (Technical Monitor)

    2001-01-01

    This paper will describe the thermal analysis techniques used to predict temperatures in the film-cooled ablative rocket nozzle used on the MC-1 60K rocket engine. A model was developed that predicts char and pyrolysis depths, liner thermal gradients, and temperatures of the bondline between the overwrap and liner. Correlation of the model was accomplished by thermal analog tests performed at Southern Research, and specially instrumented hot fire tests at the Marshall Space Flight Center. Infrared thermography was instrumental in defining nozzle hot wall surface temperatures. In-depth and outboard thermocouple data was used to correlate the kinetic decomposition routine used to predict char and pyrolysis depths. These depths were anchored with measured char and pyrolysis depths from cross-sectioned hot-fire nozzles. For the X-34 flight analysis, the model includes the ablative Thermal Protection System (TPS) material that protects the overwrap from the recirculating plume. Results from model correlation, hot-fire testing, and flight predictions will be discussed.

  17. COMTA - a computer code for fuel mechanical and thermal analysis

    International Nuclear Information System (INIS)

    Basu, S.; Sawhney, S.S.; Anand, A.K.; Anantharaman, K.; Mehta, S.K.

    1979-01-01

    COMTA is a generalized computer code for integrity analysis of the free standing fuel cladding, with natural UO 2 or mixed oxide fuel pellets. Thermal and Mechanical analysis is done simultaneously for any power history of the fuel pin. For analysis, the fuel cladding is assumed to be axisymmetric and is subjected to axisymmetric load due to contact pressure, gas pressure, coolant pressure and thermal loads. Axial variation of load is neglected and creep and plasticity are assumed to occur at constant volume. The pellet is assumed to be made of concentric annuli. The fission gas release integral is dependent on the temperature and the power produced in each annulus. To calculate the temperature distribution in the fuel pin, the variation of bulk coolant temperature is given as an input to the code. Gap conductance is calculated at every time step, considering fuel densification, fuel relocation and gap closure, filler gas dilution by released fission gas, gap closure by expansion and irradiation swelling. Overall gap conductance is contributed by heat transfer due to the three modes; conduction convection and radiation as per modified Ross and Stoute model. Equilibrium equations, compatibility equations, stress strain relationships (including thermal strains and permanent strains due to creep and plasticity) are used to obtain triaxial stresses and strains. Thermal strain is assumed to be zero at hot zero power conditions. The boundary conditions are obtained for radial stresses at outside and inside surfaces by making these equal to coolant pressure and internal pressure respectively. A multi-mechanism creep model which accounts for thermal and irradiation creep is used to calculate the overall creep rate. Effective plastic strain is a function of effective stress and material constants. (orig.)

  18. Thermal analysis of the effect of thick thermal barrier coatings on diesel engine performance

    International Nuclear Information System (INIS)

    Hoag, K.L.; Frisch, S.R.; Yonushonis, T.M.

    1986-01-01

    The reduction of heat rejection from the diesel engine combustion chamber has been the subject of a great deal of focus in recent years. In the pursuit of this goal, Cummins Engine Company has received a contract from the Department of Energy for the development of thick thermal barrier coatings for combustion chamber surfaces. This contract involves the analysis of the impact of coatings on diesel engine performance, bench test evaluation of various coating designs, and single cylinder engine tests. The efforts reported in this paper center on the analysis of the effects of coatings on engine performance and heat rejection. For this analysis the conventional water cooled engine was compared with an engine having limited oil cooling, and utilizing zirocnia coated cylinder had firedecks and piston crowns. The analysis showed little or no benefits of similarly coating the valves or cylinder liner

  19. Pressure thermal shock analysis for nuclear reactor pressure vessel

    International Nuclear Information System (INIS)

    Galik, G.; Kutis, V.; Jakubec, J.; Paulech, J.; Murin, J.

    2015-01-01

    The appearance of structural weaknesses within the reactor pressure vessel or its structural failure caused by crack formation during pressure thermal shock processes pose as a severe environmental hazard. Coolant mixing during ECC cold water injection was simulated in a detailed CFD analysis. The temperature distribution acting on the pipe wall internal surface was calculated. Although, the results show the formation of high temperature differences and intense gradients, an additional structural analysis is required to determine the possibility of structural damage from PTS. Such an analysis will be the subject of follow-up research. (authors)

  20. Transient thermal performance analysis of micro heat pipes

    International Nuclear Information System (INIS)

    Liu, Xiangdong; Chen, Yongping

    2013-01-01

    A theoretical analysis of transient fluid flow and heat transfer in a triangular micro heat pipes (MHP) has been conducted to study the thermal response characteristics. By introducing the system identification theory, the quantitative evaluation of the MHP's transient thermal performance is realized. The results indicate that the evaporation and condensation processes are both extended into the adiabatic section. During the start-up process, the capillary radius along axial direction of MHP decreases drastically while the liquid velocity increases quickly at the early transient stage and an approximately linear decrease in wall temperature arises along the axial direction. The MHP behaves as a first-order LTI control system with the constant input power as the 'step input' and the evaporator wall temperature as the 'output'. Two corresponding evaluation criteria derived from the control theory, time constant and temperature constant, are able to quantitatively evaluate the thermal response speed and temperature level of MHP under start-up, which show that a larger triangular groove's hydraulic diameter within 0.18–0.42 mm is able to accelerate the start-up and decrease the start-up temperature level of MHP. Additionally, the MHP starts up fastest using the fluid of ethanol and most slowly using the working fluid of methanol, and the start-up temperature reaches maximum level for acetone and minimum level for the methanol. -- Highlights: • Transient thermal response of micro heat pipe is simulated by an improved model. • Control theory is introduced to quantify the thermal response of micro heat pipe. • Evaluation criteria are proposed to represent thermal response of micro heat pipe. • Effects of groove dimensions and working fluids on start-up of micro heat pipe are evaluated

  1. Thermal analysis of high temperature phase transformations of steel

    Directory of Open Access Journals (Sweden)

    K. Gryc

    2013-10-01

    Full Text Available The series of thermal analysis measurements of high temperature phase transformations of real grain oriented electrical steel grade under conditions of two analytical devices (Netzsch STA 449 F3 Jupiter; Setaram SETSYS 18TM were carried out. Two thermo analytical methods were used (DTA and Direct thermal analysis. The different weight of samples was used (200 mg, 23 g. The stability/reproducibility of results obtained by used methodologies was verified. The liquidus and solidus temperatures for close to equilibrium conditions and during cooling (20 °C/min; 80 °C/min were determined. It has been shown that the higher cooling rate lead to lower temperatures for start and end of solidification process of studied steel grade.

  2. Role of thermal analysis in uranium oxide fuel fabrication process

    International Nuclear Information System (INIS)

    Balaji Rao, Y.; Yadav, R.B.

    2006-01-01

    The present paper discusses the application of thermal analysis, particularly, differential thermal analysis (Dta) at various stages of fuel fabrication process. The useful role of Dta in knowing the decomposition pattern and calcination temperature of Adu along with de-nitration temperature is explained. The decomposition pattern depends upon the type of drying process adopted for wet ADU cake (ADU C). Also, the paper highlights the utility of DTA in determining the APS and SSA of UO 2+x and U 3 O 8 powders as an alternate technique. Further, the temperature difference (ΔT max ) between the two exothermic peaks obtained in UO 2+x powder oxidation is related to sintered density of UO 2 pellets. (author)

  3. Thermal analysis of cement pastes with superabsorbent polymers

    DEFF Research Database (Denmark)

    Esteves, Luis Pedro; Jensen, Ole Mejlhede; Lukosiute, Irena

    2013-01-01

    Thermal analysis of cement systems is very helpful in the understanding of many different properties of cementitious compounds, both for the original reacting compounds, and also for the resulting hydration products. Superabsorbent polymers can be added to cement systems with many different reasons......, so it is relevant that fundamental knowledge of this new compound on the development of hydration is well understood [1-3]. This paper reports research on thermal analysis of cement pastes with superabsorbent polymers. We have studied several parameters: the concentration of SAP in the system......, the effect of particle size distribution, and their influence on the hydration process with focus on cement-silica systems. This is done at different thermodynamic conditions, so the energy of activation in the different systems can be accessed. This paper provides information relevant to hydration modelling...

  4. The utilisation of thermal analysis to optimise radiocarbon dating procedures

    International Nuclear Information System (INIS)

    Brandova, D.; Keller, W.A.; Maciejewski, M.

    1999-01-01

    Thermal analysis combined with mass spectrometry was applied to radiocarbon dating procedures (age determination of carbon-containing samples). Experiments carried out under an oxygen atmosphere were used to determine carbon content and combustion range of soil and wood samples. Composition of the shell sample and its decomposition were investigated. The quantification of CO 2 formed by the oxidation of carbon was done by the application of pulse thermal analysis. Experiments carried out under an inert atmosphere determined the combustion range of coal with CuO as an oxygen source. To eliminate a possible source of contamination in the radiocarbon dating procedures the adsorption of CO 2 by CuO was investigated. (author)

  5. Computational Analysis on Performance of Thermal Energy Storage (TES) Diffuser

    Science.gov (United States)

    Adib, M. A. H. M.; Adnan, F.; Ismail, A. R.; Kardigama, K.; Salaam, H. A.; Ahmad, Z.; Johari, N. H.; Anuar, Z.; Azmi, N. S. N.

    2012-09-01

    Application of thermal energy storage (TES) system reduces cost and energy consumption. The performance of the overall operation is affected by diffuser design. In this study, computational analysis is used to determine the thermocline thickness. Three dimensional simulations with different tank height-to-diameter ratio (HD), diffuser opening and the effect of difference number of diffuser holes are investigated. Medium HD tanks simulations with double ring octagonal diffuser show good thermocline behavior and clear distinction between warm and cold water. The result show, the best performance of thermocline thickness during 50% time charging occur in medium tank with height-to-diameter ratio of 4.0 and double ring octagonal diffuser with 48 holes (9mm opening ~ 60%) acceptable compared to diffuser with 6mm ~ 40% and 12mm ~ 80% opening. The conclusion is computational analysis method are very useful in the study on performance of thermal energy storage (TES).

  6. Computational Analysis on Performance of Thermal Energy Storage (TES) Diffuser

    International Nuclear Information System (INIS)

    Adib, M A H M; Ismail, A R; Kardigama, K; Salaam, H A; Ahmad, Z; Johari, N H; Anuar, Z; Azmi, N S N; Adnan, F

    2012-01-01

    Application of thermal energy storage (TES) system reduces cost and energy consumption. The performance of the overall operation is affected by diffuser design. In this study, computational analysis is used to determine the thermocline thickness. Three dimensional simulations with different tank height-to-diameter ratio (HD), diffuser opening and the effect of difference number of diffuser holes are investigated. Medium HD tanks simulations with double ring octagonal diffuser show good thermocline behavior and clear distinction between warm and cold water. The result show, the best performance of thermocline thickness during 50% time charging occur in medium tank with height-to-diameter ratio of 4.0 and double ring octagonal diffuser with 48 holes (9mm opening ∼ 60%) acceptable compared to diffuser with 6mm ∼ 40% and 12mm ∼ 80% opening. The conclusion is computational analysis method are very useful in the study on performance of thermal energy storage (TES).

  7. Infrared X-ray and thermal analysis of terbium soaps

    International Nuclear Information System (INIS)

    Mehrotra, K.N.; Sharma, N.

    1996-01-01

    Terbium sops (laureate, myristate and palmitate) were synthesized by direct metathesis of corresponding potassium soap with an aqueous solution of terbium nitrate. The physico-chemical characteristics of soaps in solid state were investigated by IR spectra, X-ray diffraction patterns and TGA measurements. The IR results revealed that the fatty acids exist in dimeric state through hydrogen bonding while the soaps possess partial ionic character. The X-ray analysis showed that the soaps have double layer structure with molecular axes slightly inclined to the basal plane. The thermal analysis suggested that the decomposition of soaps occur in two steps. The energy of activation, order of reaction and various kinetic parameters (i.e. frequency factor, entropy of activation and free energy) for the thermal decomposition of soaps were evaluated. (author). 26 refs, 4 figs, 4 tabs

  8. Thermal test and analysis of a spent fuel storage cask

    International Nuclear Information System (INIS)

    Yamakawa, H.; Gomi, Y.; Ozaki, S.; Kosaki, A.

    1993-01-01

    A thermal test simulated with full-scale cask model for the normal storage was performed to verify the storage skill of the spent fuels of the cask. The maximum temperature at each point in the test was lower than the allowable temperature. The integrity of the cask was maintained. It was observed that the safety of containment system was also kept according to the check of the seal before and after the thermal test. Therefore it was shown that using the present skill, it is possible to store spent fuels in the dry-type cask safely. Moreover, because of the good agreement between analysis and experimental results, it was shown that the analysis model was successfully established to estimate the temperature distribution of the fuel cladding and the seal portion. (J.P.N.)

  9. Development of realistic thermal hydraulic system analysis code

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Won Jae; Chung, B. D; Kim, K. D. [and others

    2002-05-01

    The realistic safety analysis system is essential for nuclear safety research, advanced reactor development, safety analysis in nuclear industry and 'in-house' plant design capability development. In this project, we have developed a best-estimate multi-dimensional thermal-hydraulic system code, MARS, which is based on the integrated version of the RELAP5 and COBRA-TF codes. To improve the realistic analysis capability, we have improved the models for multi-dimensional two-phase flow phenomena and for advanced two-phase flow modeling. In addition, the GUI (Graphic User Interface) feature were developed to enhance the user's convenience. To develop the coupled analysis capability, the MARS code were linked with the three-dimensional reactor kinetics code (MASTER), the core thermal analysis code (COBRA-III/CP), and the best-estimate containment analysis code (CONTEMPT), resulting in MARS/MASTER/COBRA/CONTEMPT. Currently, the MARS code system has been distributed to 18 domestic organizations, including research, industrial, regulatory organizations and universities. The MARS has been being widely used for the safety research of existing PWRs, advanced PWR, CANDU and research reactor, the pre-test analysis of TH experiments, and others.

  10. Development of realistic thermal hydraulic system analysis code

    International Nuclear Information System (INIS)

    Lee, Won Jae; Chung, B. D; Kim, K. D.

    2002-05-01

    The realistic safety analysis system is essential for nuclear safety research, advanced reactor development, safety analysis in nuclear industry and 'in-house' plant design capability development. In this project, we have developed a best-estimate multi-dimensional thermal-hydraulic system code, MARS, which is based on the integrated version of the RELAP5 and COBRA-TF codes. To improve the realistic analysis capability, we have improved the models for multi-dimensional two-phase flow phenomena and for advanced two-phase flow modeling. In addition, the GUI (Graphic User Interface) feature were developed to enhance the user's convenience. To develop the coupled analysis capability, the MARS code were linked with the three-dimensional reactor kinetics code (MASTER), the core thermal analysis code (COBRA-III/CP), and the best-estimate containment analysis code (CONTEMPT), resulting in MARS/MASTER/COBRA/CONTEMPT. Currently, the MARS code system has been distributed to 18 domestic organizations, including research, industrial, regulatory organizations and universities. The MARS has been being widely used for the safety research of existing PWRs, advanced PWR, CANDU and research reactor, the pre-test analysis of TH experiments, and others

  11. Preliminary hazards analysis of thermal scrap stabilization system. Revision 1

    International Nuclear Information System (INIS)

    Lewis, W.S.

    1994-01-01

    This preliminary analysis examined the HA-21I glovebox and its supporting systems for potential process hazards. Upon further analysis, the thermal stabilization system has been installed in gloveboxes HC-21A and HC-21C. The use of HC-21C and HC-21A simplified the initial safety analysis. In addition, these gloveboxes were cleaner and required less modification for operation than glovebox HA-21I. While this document refers to glovebox HA-21I for the hazards analysis performed, glovebox HC-21C is sufficiently similar that the following analysis is also valid for HC-21C. This hazards analysis document is being re-released as revision 1 to include the updated flowsheet document (Appendix C) and the updated design basis (Appendix D). The revised Process Flow Schematic has also been included (Appendix E). This Current revision incorporates the recommendations provided from the original hazards analysis as well. The System Design Description (SDD) has also been appended (Appendix H) to document the bases for Safety Classification of thermal stabilization equipment

  12. Thermal-hydraulic analysis for wire-wrapped PWR cores

    Energy Technology Data Exchange (ETDEWEB)

    Diller, P. [General Electric Company, 3901 Castle Hayne Rd., Wilmington, NC 28401 (United States)], E-mail: pdiller@gmail.com; Todreas, N. [Massachusetts Institute of Technology, Cambridge, MA 02139 (United States)], E-mail: todreas@mit.edu; Hejzlar, P. [Massachusetts Institute of Technology, Cambridge, MA 02139 (United States)

    2009-08-15

    This work focuses on the steady-state and transient thermal-hydraulic analyses for PWR cores using wire wraps in a hexagonal array with either U (45% w/o)-ZrH{sub 1.6} (referred to as U-ZrH{sub 1.6}) or UO{sub 2} fuels. Equivalences (thermal-hydraulic and neutronic) were created between grid spacer and wire wrap designs, and were used to apply results calculated for grid spacers to wire wrap designs. Design limits were placed on the pressure drop, critical heat flux (CHF), fuel and cladding temperature and vibrations. The vibrations limits were imposed for flow-induced vibrations (FIV) and thermal-hydraulic vibrations (THV). The transient analysis examined an overpower accident, loss of coolant accident (LOCA) and loss of flow accident (LOFA). The thermal-hydraulic performance of U-ZrH{sub 1.6} and UO{sub 2} were found very similar. Relative to grid spacer designs, wire wrap designs were found to have smaller fretting wear, substantially lower pressure drop and higher CHF. As a result, wire wrap cores were found to offer substantially higher maximum powers than grid spacer cores, allowing for a 25% power increase relative to the grid spacer uprate [Shuffler, C.A., Malen, J.A., Trant, J.M., Todreas, N.E., 2009a. Thermal-hydraulic analysis for grid supported and inverted fueled PWR cores. Nuclear Technology (this special issue devoted to hydride fuel in LWRs)] and a 58% power increase relative to the reference core.

  13. Application of thermal analysis in nuclear waste management

    International Nuclear Information System (INIS)

    Raje, Naina; Kalekar, Bhupesh; Acharekar, Darshana; Reddy, A.V.R.

    2009-01-01

    Thermal decomposition of zirconium raffinate and ammonium nitrate has been studied using simultaneous TG - DTA - MS/FTIR measurements. Based on non-isothermal analysis, isothermal measurements have been carried out at different temperatures to fix the calcination temperature/s. Decomposition of ammonium nitrate was studied in inert, oxidizing and reducing environments and the results suggest that the decomposition mechanism is same in inert/oxidizing atmosphere but is different in reducing environment. (author)

  14. Thermal analysis of NNWSI conceptual waste package designs

    International Nuclear Information System (INIS)

    Stein, W.; Hockman, J.N.; O'Neal, W.C.

    1984-04-01

    Lawrence Livermore National Laboratory is involved in the design and testing of high-level nuclear waste packages. Many of the aspects of waste package design and testing (e.g., corrosion and leaching) depend in part on the temperature history of the emplaced packages. This report discusses thermal modeling and analysis of various emplaced waste package conceptual designs including the models used, the assumptions and approximations made, and the results obtained. 16 references

  15. The analysis of thermal-hydraulic models in MELCOR code

    Energy Technology Data Exchange (ETDEWEB)

    Kim, M H; Hur, C; Kim, D K; Cho, H J [POhang Univ., of Science and TECHnology, Pohang (Korea, Republic of)

    1996-07-15

    The objective of the present work is to verify the prediction and analysis capability of MELCOR code about the progression of severe accidents in light water reactor and also to evaluate appropriateness of thermal-hydraulic models used in MELCOR code. Comparing the results of experiment and calculation with MELCOR code is carried out to achieve the above objective. Specially, the comparison between the CORA-13 experiment and the MELCOR code calculation was performed.

  16. Proceedings of the 11th Thermal and Fluids Analysis Workshop

    Science.gov (United States)

    Sakowski, Barbara

    2002-07-01

    The Eleventh Thermal & Fluids Analysis WorkShop (TFAWS 2000) was held the week of August 21-25 at The Forum in downtown Cleveland. This year's annual event focused on building stronger links between research community and the engineering design/application world and celebrated the theme "Bridging the Gap Between Research and Design". Dr. Simon Ostrach delivered the keynote address "Research for Design (R4D)" and encouraged a more deliberate approach to performing research with near-term engineering design applications in mind. Over 100 persons attended TFAWS 2000, including participants from five different countries. This year's conference devoted a full-day seminar to the discussion of analysis and design tools associated with aeropropulsion research at the Glenn Research Center. As in previous years, the workshop also included hands-on instruction in state-of-the-art analysis tools, paper sessions on selected topics, short courses and application software demonstrations. TFAWS 2000 was co-hosted by the Thermal/Fluids Systems Design and Analysis Branch of NASA GRC and by the Ohio Aerospace Institute and was co-chaired by Barbara A. Sakowski and James R. Yuko. The annual NASA Delegates meeting is a standard component of TFAWS where the civil servants of the various centers represented discuss current and future events which affect the Community of Applied Thermal and Fluid ANalystS (CATFANS). At this year's delegates meeting the following goals (among others) were set by the collective body of delegates participation of all Centers in the NASA material properties database (TPSX) update: (1) developing and collaboratively supporting multi-center proposals; (2) expanding the scope of TFAWS to include other federal laboratories; (3) initiation of a white papers on thermal tools and standards; and (4) formation of an Agency-wide TFAWS steering committee.

  17. Thermal Analysis of Iodine Satellite (iSAT)

    Science.gov (United States)

    Mauro, Stephanie

    2015-01-01

    This paper presents the progress of the thermal analysis and design of the Iodine Satellite (iSAT). The purpose of the iSAT spacecraft (SC) is to demonstrate the ability of the iodine Hall Thruster propulsion system throughout a one year mission in an effort to mature the system for use on future satellites. The benefit of this propulsion system is that it uses a propellant, iodine, that is easy to store and provides a high thrust-to-mass ratio. The spacecraft will also act as a bus for an earth observation payload, the Long Wave Infrared (LWIR) Camera. Four phases of the mission, determined to either be critical to achieving requirements or phases of thermal concern, are modeled. The phases are the Right Ascension of the Ascending Node (RAAN) Change, Altitude Reduction, De-Orbit, and Science Phases. Each phase was modeled in a worst case hot environment and the coldest phase, the Science Phase, was also modeled in a worst case cold environment. The thermal environments of the spacecraft are especially important to model because iSAT has a very high power density. The satellite is the size of a 12 unit cubesat, and dissipates slightly more than 75 Watts of power as heat at times. The maximum temperatures for several components are above their maximum operational limit for one or more cases. The analysis done for the first Design and Analysis Cycle (DAC1) showed that many components were above or within 5 degrees Centigrade of their maximum operation limit. The battery is a component of concern because although it is not over its operational temperature limit, efficiency greatly decreases if it operates at the currently predicted temperatures. In the second Design and Analysis Cycle (DAC2), many steps were taken to mitigate the overheating of components, including isolating several high temperature components, removal of components, and rearrangement of systems. These changes have greatly increased the thermal margin available.

  18. Analysis of shape and spatial interaction of synaptic vesicles using data from focused ion beam scanning electron microscopy (FIB-SEM)

    DEFF Research Database (Denmark)

    Khanmohammadi, Mahdieh; Waagepetersen, Rasmus Plenge; Sporring, Jon

    2015-01-01

    deviations from spherical shape and systematic trends in their orientation. We studied three-dimensional representations of synapses obtained by manual annotation of focused ion beam scanning electron microscopy (FIB-SEM) images of male mouse brain. The configurations of synaptic vesicles were regarded...... in excitatory synapses appeared to be of oblate ellipsoid shape and in inhibitory synapses appeared to be of cigar ellipsoid shape, and followed a systematic pattern regarding their orientation towards the active zone. Moreover, there was strong evidence of spatial alignment in the orientations of pairs...

  19. Theory and practice of near-field thermal probes for microscopy and thermal analysis

    International Nuclear Information System (INIS)

    Hodges, C.S.

    1999-03-01

    Bacterial mats called biofilms that form on the surfaces of industrial steel pipes can cause corrosion of the pipe. Examining the steel surface of the corroded pipe usually involves removal of the biofilm using acid. This acid can also cause corrosion of the pipe so that the observed corrosion cracks and pits are the result of both the acid and the biofilm. It was thought that non-invasive examination of the corrosion caused by the biofilm may be obtained by using a thin wire bent into a loop that acts as both a heat source a nd a detector of heat, measuring the changes in heat flow out of the wire as the wire passes over the steel with the biofilm still present. This technique of using a heated probe to scan samples on a microscopic scale is called Scanning Thermal Microscopy (SThM) and uses an alternating current to produce a.c. thermal waves that emanate from the probe tip into the sample. The alternating current allows better signal-to-noise ratios and also selective depth imaging of the sample since the thermal wave penetrates into the sample a distance inversely proportional to the applied current frequency. Reversal in the contrast of SThM images on biofilms and subsequently all samples was observed as either the frequency or the amplitude of the temperature waves was altered. Whilst changing the time constant of the feedback circuit attached to the SThM probe did go some way to explain this effect, a full explanation is still wanting. Despite many efforts to image the biofilm/steel interface with the biofilm still present, often the biofilm was either too thick or too complicated to do this. A simpler thermal test sample is required to calibrate the thermal probe. In addition to SThM, one may select a point on a sample surface and ramp the temperature of the probe to obtain a Localised Thermal Analysis (LTA) temperature scan looking for melts, recrystallisations, glass transitions of the part of the sample in contact with the probe. This technique is a

  20. Numerical analysis and nuclear standard code application to thermal fatigue

    International Nuclear Information System (INIS)

    Merola, M.

    1992-01-01

    The present work describes the Joint Research Centre Ispra contribution to the IAEA benchmark exercise 'Lifetime Behaviour of the First Wall of Fusion Machines'. The results of the numerical analysis of the reference thermal fatigue experiment are presented. Then a discussion on the numerical analysis of thermal stress is tackled, pointing out its particular aspects in view of their influence on the stress field evaluation. As far as the design-allowable number of cycles are concerned the American nuclear code ASME and the French code RCC-MR are applied and the reasons for the different results obtained are investigated. As regards a realistic fatigue lifetime evaluation, the main problems to be solved are brought out. This work, is intended as a preliminary basis for a discussion focusing on the main characteristics of the thermal fatigue problem from both a numerical and a lifetime assessment point of view. In fact the present margin of discretion left to the analyst may cause undue discrepancies in the results obtained. A sensitivity analysis of the main parameters involved is desirable and more precise design procedures should be stated

  1. Thermal analysis of the horizontal disposal for HLW

    International Nuclear Information System (INIS)

    Zhao Honggang

    2012-01-01

    The temperature on the canister surface is set to be not more than 100 in the repository, a criterion which dictates the dimension of the repository. The factors that affect the highest temperature on the canister surface include the initial power of the canister, the material thermal properties of the engineered barrier system (EBS), the gaps around the canister in the EBS, the initial ground temperature and thermal properties of the host rock, the repository layout, etc. The article examines the material thermal properties of the host rock and the EBS, the thermal conductivity properties of the different gaps in the EBS, the temperature evolution around the single canister by using the analysis method and the numerical method for horizontal disposal concept. The findings are as follows: 1) The most important and the most sensitive parameter is the initial disposal power of the canister; 2) The two key factors that affect the highest temperature on the canister surface are the material parameter's uncertainty and nature variability of the host rock and the EBS, and the gaps around the canister in the EBS; 3) The temperature offsets between the canister and bentonite is not more than 10, and the bigger the inner gaps, the bigger temperature offsets between the canister and bentonite; When the gap between the bentonite and the host rock is filled with water, the gap's temperature offsets is small, but it will be 1∼3 higher when the gaps between the bentonite and the host rock is filled with air. (author)

  2. Thermal spike analysis of highly charged ion tracks

    International Nuclear Information System (INIS)

    Karlušić, M.; Jakšić, M.

    2012-01-01

    The irradiation of material using swift heavy ion or highly charged ion causes excitation of the electron subsystem at nanometer scale along the ion trajectory. According to the thermal spike model, energy deposited into the electron subsystem leads to temperature increase due to electron–phonon coupling. If ion-induced excitation is sufficiently intensive, then melting of the material can occur, and permanent damage (i.e., ion track) can be formed upon rapid cooling. We present an extension of the analytical thermal spike model of Szenes for the analysis of surface ion track produced after the impact of highly charged ion. By applying the model to existing experimental data, more than 60% of the potential energy of the highly charged ion was shown to be retained in the material during the impact and transformed into the energy of the thermal spike. This value is much higher than 20–40% of the transferred energy into the thermal spike by swift heavy ion. Thresholds for formation of highly charged ion track in different materials show uniform behavior depending only on few material parameters.

  3. Performance analysis of photovoltaic thermal (PVT) water collectors

    International Nuclear Information System (INIS)

    Fudholi, Ahmad; Sopian, Kamaruzzaman; Yazdi, Mohammad H.; Ruslan, Mohd Hafidz; Ibrahim, Adnan; Kazem, Hussein A.

    2014-01-01

    Highlights: • Performances analysis of PVT collector based on energy efficiencies. • New absorber designs of PVT collectors were presented. • Comparison present study with other absorber collector designs was presented. • High efficiencies were obtained for spiral flow absorber. - Abstract: The electrical and thermal performances of photovoltaic thermal (PVT) water collectors were determined under 500–800 W/m 2 solar radiation levels. At each solar radiation level, mass flow rates ranging from 0.011 kg/s to 0.041 kg/s were introduced. The PVT collectors were tested with respect to PV efficiency, thermal efficiency, and a combination of both (PVT efficiency). The results show that the spiral flow absorber exhibited the highest performance at a solar radiation level of 800 W/m 2 and mass flow rate of 0.041 kg/s. This absorber produced a PVT efficiency of 68.4%, a PV efficiency of 13.8%, and a thermal efficiency of 54.6%. It also produced a primary-energy saving efficiency ranging from 79% to 91% at a mass flow rate of 0.011–0.041 kg/s

  4. Analysis of an Attached Sunspace with a Thermal Inertia Floor

    Directory of Open Access Journals (Sweden)

    María José Suárez López

    2018-05-01

    Full Text Available An attached sunspace is a partially or fully glazed enclosure, usually located on the first floor, facing south (in the Northern Hemisphere and adjacent to a conditioned room. Because of the length and orientation of the glazed area, the temperature in the sunspace is usually higher than outside the building. As a Trombe–Mitchel wall, the sunspace has a considerable mass that accumulates thermal energy, but in this case the thermal mass is located in the floor. This capacity to accumulate thermal energy confers the attached sunspace features beyond passive insulation. The sunspace studied in this paper is part of an experimental building located in the North of Spain that was built in the frame of the so-called ARFRISOL project. It consists of a south-facing glazed exterior wall with both clear glass and semi-transparent photovoltaic panels, an intermediate space with a thick layer of sand over a concrete floor, and a partially glazed interior wall. In this paper, a three-dimensional computational model has been implemented to analyse the thermal behaviour inside the sunspace. This analysis takes into account, among other factors, the effects of sun position, incident solar irradiation and temperature both inside and outside.

  5. Methodology for a thermal analysis of a proposed SFR transport cask with the thermal code SYRTHES

    International Nuclear Information System (INIS)

    Peniguel, C.; Rupp, I.; Schneider, J. P.

    2010-01-01

    Fast reactors with liquid metal coolant have received a renewed interest owing to the need of a more efficient usage of the primary uranium resources, and they are one of the proposal for the next Generation IV. In the framework of the 2006 French law on sustainable management of radioactive materials and waste, an evaluation of the industrial perspectives of minor actinides transmutation advantages and drawbacks in Generation IV fast spectrum reactors system is requested for 2012. The CEA is in charge of studying the global problem, but on some aspects, EDF is interested to do its own exploratory studies. Among other points, transport is seen as important for the nuclear industry, to link points of production and treatment. Nuclear fuel is generally transported in thick walled rail or truck casks. These packages are designed to provide confinement, shielding and criticality protection during normal and severe transport conditions. Heat generated within the fuel (and a contribution of solar heating) makes the package becoming quite hot, but one must demonstrate that the cladding temperature does not exceed a long term temperature limit during normal transport. This paper presents a thermal study done on a package in which 9 SFR assemblies are included. Each of them is of hexagonal shape and contains 271 fuel pins. The approach followed for these calculations is to rely on an explicit representation of all pins. For these calculations a 2D analysis is performed thanks to the thermal code SYRTHES. Conduction is solved thanks to a finite element method, while thermal radiation is handled through a radiosity approach. The main aim of this paper is to present a possible numerical methodology to handle the thermal problem. (authors)

  6. thermal analysis of a small scale solid waste-fired steam boiler

    African Journals Online (AJOL)

    user

    Thermal analysis of a small scale solid waste-fired steam generator is presented in this paper. The analysis was based on the chosen design specifications which are operating steam ... include: wind, bio-energy, geothermal, solar thermal,.

  7. Thermal analysis and its application in evaluation of fluorinated polyimide membranes for gas separation

    KAUST Repository

    Qiu, Wulin; Chen, Chien-Chiang; Kincer, Matthew R.; Koros, William J.

    2011-01-01

    by reaction with acetic anhydride to produce polyimide (PI). The resulting polymers were characterized using thermal analysis techniques including TGA, derivative weight analysis, TGA-MS, and DSC. The decarboxylation-induced thermal cross-linking, ester cross

  8. Thermal treatment investigation of natural lizardite at the atmospheric pressure, based on XRD and differential thermal analysis/thermal gravimetric analysis methods

    International Nuclear Information System (INIS)

    Dabiri, R.; Karimi Shahraki, B.; Mollaei, H.; Ghaffari, M.

    2009-01-01

    Determination of stability limits, mineralogical changes and thermal reaction of serpentine minerals are very important for the investigation of magmatism, mechanism and depth of plates of subduction. During the subduction process, serpentine (Lizardite) minerals will release their water due to thermal reactions. This dehydration can play an important role in volcanism processes related to the subduction, In this study, serpentine minerals (Lizardite) collected from the Neyriz Ophiolite Complex were dehydrated under the constant atmospheric pressure. These mineralogical changes were determined by X-Ray diffraction and differential thermal analysis-thermal gravimetric analyses methods. This study shows natural lizardites that heated for about one hour is stable up to 550 d eg C . Dehydration reactions on lizardite started at approximately between 100 to 150 d eg C and dehydroxylation reactions started at approximately 550-690 d eg C . As a result of thermal reaction, the decomposition of lizardite will take place and then changes in to olivine (forsterite). Crystallization of olivine (forsterite) will start at 600 d eg C . This mineral is stable up to 700 d eg C and then crystallization of enstatite will start at 700 d eg C . During this dehydration and crystallization reaction, amorphous processes will start at 600 d eg C and some amount water and silica will release.

  9. Development of intelligent system for a thermal analysis instrument

    International Nuclear Information System (INIS)

    Xu Xiaoli; Wu Guoxin; Shi Yongchao

    2005-01-01

    The key techniques for the intelligent analysis instrument developed are proposed. Based on the technique of virtual instrumentation, the intelligent PID control algorithm to control the temperature of thermal analysis instrument is described. The dynamic character and the robust performance of traditional PID controls are improved through the dynamic gain factor, temperature rate change factor, the forecast factor, and the temperature correction factor is introduced. Using the graphic development environment of LabVIEW, the design of system modularization and the graphic display are implemented. By means of multiple mathematical modules, intelligent data processing is realized

  10. Deformation analysis considering thermal expansion of injection mold

    International Nuclear Information System (INIS)

    Kim, Jun Hyung; Yi, Dae Eun; Jang, Jeong Hui; Lee, Min Seok

    2015-01-01

    In the design of injection molds, the temperature distribution and deformation of the mold is one of the most important parameters that affect the flow characteristics, flash generation, and surface appearance, etc. Plastic injection analyses have been carried out to predict the temperature distribution of the mold and the pressure distribution on the cavity surface. As the input loads, we transfer the temperature and pressure results to the structural analysis. We compare the structural analysis results with the thermal expansion effect using the actual flash and step size of a smartphone cover part. To reduce the flash problem, we proposed a new mold design, and verified the results by performing simulations

  11. Deformation analysis considering thermal expansion of injection mold

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Jun Hyung; Yi, Dae Eun; Jang, Jeong Hui; Lee, Min Seok [Samsung Electronics Co., LTD., Seoul (Korea, Republic of)

    2015-09-15

    In the design of injection molds, the temperature distribution and deformation of the mold is one of the most important parameters that affect the flow characteristics, flash generation, and surface appearance, etc. Plastic injection analyses have been carried out to predict the temperature distribution of the mold and the pressure distribution on the cavity surface. As the input loads, we transfer the temperature and pressure results to the structural analysis. We compare the structural analysis results with the thermal expansion effect using the actual flash and step size of a smartphone cover part. To reduce the flash problem, we proposed a new mold design, and verified the results by performing simulations.

  12. Thermal-hydraulic analysis of PWR cores in transient condition

    International Nuclear Information System (INIS)

    Silva Galetti, M.R. da.

    1984-01-01

    A calculational methodology for thermal - hydraulic analysis of PWR cores under steady-state and transient condition was selected and made available to users. An evaluation of the COBRA-IIIP/MIT code, used for subchannel analysis, was done through comparison of the code results with experimental data on steady state and transient conditions. As a result, a comparison study allowing spatial and temporal localization of critical heat flux was obtained. A sensitivity study of the simulation model to variations in some empirically determined parameter is also presented. Two transient cases from Angra I FSAR were analysed, showing the evolution of minimum DNBR with time. (Author) [pt

  13. Secondary emission monitor (SEM) grids.

    CERN Multimedia

    Patrice Loïez

    2002-01-01

    A great variety of Secondary Emission Monitors (SEM) are used all over the PS Complex. At other accelerators they are also called wire-grids, harps, etc. They are used to measure beam density profiles (from which beam size and emittance can be derived) in single-pass locations (not on circulating beams). Top left: two individual wire-planes. Top right: a combination of a horizontal and a vertical wire plane. Bottom left: a ribbon grid in its frame, with connecting wires. Bottom right: a SEM-grid with its insertion/retraction mechanism.

  14. Diurnal thermal analysis of microencapsulated PCM-concrete composite walls

    International Nuclear Information System (INIS)

    Thiele, Alexander M.; Sant, Gaurav; Pilon, Laurent

    2015-01-01

    Highlights: • Transient heat conduction across microencapsulated PCM-concrete walls was simulated. • Equivalent homogeneous wall with effective thermal properties was rigorously derived. • Adding PCM to the wall increases daily energy savings and delays peak thermal load. • Energy savings is maximum when PCM melting temperature equals indoor temperature. • Energy savings are limited in extreme climates but time delay can be large. - Abstract: This paper examines the benefits of adding microencapsulated phase change material (PCM) to concrete used in building envelopes to reduce energy consumption and costs. First, it establishes that the time-dependent thermal behavior of microencapsulated PCM-concrete composite walls can be accurately predicted by an equivalent homogeneous wall with appropriate effective thermal properties. The results demonstrate that adding microencapsulated PCM to concrete resulted in a reduction and a time-shift in the maximum heat flux through the composite wall subjected to diurnal sinusoidal outdoor temperature and solar radiation heat flux. The effects of the PCM volume fraction, latent heat of fusion, phase change temperature and temperature window, and outdoor temperature were evaluated. Several design rules were established including (i) increasing the PCM volume fraction and/or enthalpy of phase change increased the energy flux reduction and the time delay, (ii) the energy flux reduction was maximized when the PCM phase change temperature was close to the desired indoor temperature, (iii) the optimum phase change temperature to maximize the time delay increased with increasing average outdoor temperature, (iv) in extremely hot or cold climates, the thermal load could be delayed even though the reduction in daily energy flux was small, and (v) the choice of phase change temperature window had little effect on the energy flux reduction and on the time delay. This analysis can serve as a framework to design PCM composite walls

  15. Two-dimensional disruption thermal analysis code DREAM

    International Nuclear Information System (INIS)

    Yamazaki, Seiichiro; Kobayashi, Takeshi; Seki, Masahiro.

    1988-08-01

    When a plasma disruption takes place in a tokamak type fusion reactor, plasma facing components such as first wall and divertor/limiter are subjected to an intense heat load with very high heat flux and short duration. At the surface of the wall, temperature rapidly rises, and melting and evaporation occurs, it causes reduction of wall thickness and crack initiation/propagation. As lifetime of the components is significantly affected by them, the transient analysis in consideration of phase changes (melting/evaporation) and radiation heat loss is required in the design of these components. This paper describes the computer code DREAM developed to perform the two-dimensional transient thermal analysis that takes phase changes and radiation into account. The input and output of the code and a sample analysis on a disruption simulation experiment are also reported. The user's input manual is added as an appendix. The profiles and time variations of temperature, and melting and evaporated thicknesses of the material subjected to intense heat load can be obtained, using this computer code. This code also gives the temperature data for elastoplastic analysis with FEM structural analysis codes (ADINA, MARC, etc.) to evaluate the thermal stress and crack propagation behavior within the wall materials. (author)

  16. Thermal analysis of an instrumented capsule using an ANSYS program

    International Nuclear Information System (INIS)

    Choi, Myoung Hwan; Choo, Kee Nam; Kang, Young Hwan; Cho, Man Soon; Sohn, Jae Min; Kim, Bong Goo

    2006-01-01

    An instrumented capsule has been used for an irradiation test of various nuclear materials in the research reactor, HANARO. To obtain the design data of the instrumented capsule, a thermal analysis is performed using a finite element analysis program, ANSYS. The 2-dimensional model for a cross section of the capsule including the specimens is generated, and a gamma-heating rate of the materials for the HANARO power of 24 or 30 MW is considered as an input force. The effect of the gap size and the control rod position on the temperature of the specimens or other components is discussed. From the analysis it is found that the gap between the thermal media and the external tube has a significant effect on the temperature of the specimen. In the case of the material capsule, the maximum temperature for the reactor power of 24 MW is 255degC for an irradiation test and 257degC for a FE analysis at the center stage of the capsule in the axial direction. It is expected that the analysis models using an ANSYS program will be useful in designing the instrumented capsules for an irradiation test and estimating the test results. (author)

  17. Transient thermal analysis of semiconductor diode lasers under pulsed operation

    Science.gov (United States)

    Veerabathran, G. K.; Sprengel, S.; Karl, S.; Andrejew, A.; Schmeiduch, H.; Amann, M.-C.

    2017-02-01

    Self-heating in semiconductor lasers is often assumed negligible during pulsed operation, provided the pulses are `short'. However, there is no consensus on the upper limit of pulse width for a given device to avoid-self heating. In this paper, we present an experimental and theoretical analysis of the effect of pulse width on laser characteristics. First, a measurement method is introduced to study thermal transients of edge-emitting lasers during pulsed operation. This method can also be applied to lasers that do not operate in continuous-wave mode. Secondly, an analytical thermal model is presented which is used to fit the experimental data to extract important parameters for thermal analysis. Although commercial numerical tools are available for such transient analyses, this model is more suitable for parameter extraction due to its analytical nature. Thirdly, to validate this approach, it was used to study a GaSb-based inter-band laser and an InP-based quantum cascade laser (QCL). The maximum pulse-width for less than 5% error in the measured threshold currents was determined to be 200 and 25 ns for the GaSb-based laser and QCL, respectively.

  18. Drift scale thermomechanical analysis for thermal loading and retrievability studies

    International Nuclear Information System (INIS)

    Tsai, F.C.

    1995-01-01

    The repository portion of the Mined Geologic Disposal System for the disposal of spent nuclear fuel and high-level radioactive waste is currently in the advanced conceptual design stage. In support of systems studies, a numerical method was used to estimate the stability of emplacement drifts. Thermomechanical analyses, using the Discontinuous Deformation Analysis code, were performed using input data from Yucca Mountain documents. The analysis found that the stresses produced in the rock at thermal loads of 27.4 kilograms uranium per m2 (KgU/m2) would exceed stability criteria and could result in tunnel instability. At thermal loads between 20.5 KgU/m2, the drift is predicted to be stable and its structural integrity remains after thermal loading. In this case, the smaller diameter drift emplacement appears to have better stability. However, local rock spalling may occur. According to the numerical prediction, more rock fall may occur during the retrieval period due to the stress relaxation caused by the rapid cooling in the immediate drift area

  19. Thermal fatigue crack growth analysis in a nozzle corner

    International Nuclear Information System (INIS)

    Blauel, J.G.; Hodulak, L.

    1983-01-01

    Calculations of the crack growth under local thermal shock fatigue are performed. Estimates of crack growth are based on stress distributions obtained by a finite element analysis for thermal transients in the structure without crack. Stress intensity factors are calculated using interpolation formulae derived from known basic solutions for part-through cracks under constant and linearly varying load. The crack propagation at selected parts of the crack front is calculated stepwise by integration of the Paris law with material constants C and n interpolated from test results on compact specimens at constant temperatures. Experimental results for the model vessel test MB1 at an internal pressure of 14 N/mm 2 and a temperature of 320 0 C exposed to a repeated local spraying with cold water are presented and compared to predictions

  20. Thermal analysis of rare earth gallates and aluminates

    International Nuclear Information System (INIS)

    O'Bryan, H.M.; Gallagher, P.K.; Berkstresser, G.W.; Brandle, C.D.

    1990-01-01

    Dilatometry, high-temperature x-ray diffraction, differential thermal analysis, and differential scanning calorimetry have been performed on LaGaO 3 , NdGaO 3 , PrGaO 3 , SmAlO 3 , and LaAlO 3 single crystals grown by the Czochralski technique. First order phase transitions have been located at 145 degree C for LaGaO 3 and 785 degree C for SmAlO 3 , and ΔH has been measured for the LaGaO 3 transition. Second order transitions have been identified for LaGaO 3 , PrGaO 3 , NdGaO 3 , and LaAlO 3 . The usefulness of these compounds as substrates for high temperature superconducting films is discussed in terms of thermal expansion matching

  1. Parametric thermal analysis of 75 MHz heavy ion RFQ

    International Nuclear Information System (INIS)

    Mishra, N.K.; Mehrotra, N.; Verma, V.; Gupta, A.K.; Bhagwat, P.V.

    2015-01-01

    An ECR based Heavy Ion Accelerator comprising of a superconducting Electron Cyclotron Resonance (ECR) Ion Source, normal conducting RFQ (Radio Frequency Quadrupole) and superconducting Niobium resonators is being developed at BARC under XII plan. A state-of-the-art 18 GHz superconducting ECR ion source (PK-ISIS) jointly configured with Pantechnik, France is operational at Van-de-Graaff, BARC. The electromagnetic design of the improved version of 75 MHz heavy ion RFQ has been reported earlier. The previous thermal study of 51 cm RFQ model showed large temperature variation axially along the vane tip. A new coolant flow scheme has been worked out to optimize the axial temperature gradient. In this paper the thermal analysis including parametric study of coolant flow rates and inlet temperature variation will be presented. (author)

  2. Thermal and Electrical Analysis of Mars Rover RTGs

    Energy Technology Data Exchange (ETDEWEB)

    Schock, Alfred; Or, Chuen T; Skrabek, Emanuel A

    2012-01-19

    The RTG designs described in the preceding paper in these proceedings were analyzed for their thermal and electrical performance. Each analysis consisted of coupled thermal, thermoelectric, and electrical analyses, using Fairchild-generated specialized computer codes. These were supplemented with preliminary structural and mass analyses. For each design, various cases representing different operating conditions (water-cooled/radiation-cooled, BOM/EOM, summer/winter, day/night) and different thermoelectric performance assumptions (from conservative to optimistic) were analyzed; and for every case, the heat flow rates, temperatures and electrical performance of each layer of thermoelectric elements and of the overall RTG were determined. The analyses were performed in great detail, to obtain accurate answers permitting meaningful comparisons between different designs. The results presented show the RTG performance achievable with current technology, and the performance improvements that would be achievable with various technology developments.

  3. Stochastic thermal stress analysis of clad cylindrical fuel elements

    International Nuclear Information System (INIS)

    Barrett, P.R.

    1975-01-01

    After a review of deterministic elastic thermal stress analysis by means of the displacement method for a cylindrical system in which the temperature distribution is not only radially variable but azimuthally and axially variable also, a method is shown for the determination of the statistical moments of the stress components when (a) the outer boundary of the cladding is a stochastic quantity, and (b) the uncertainties in the elastic and thermal constants of the materials and in the magnitude of the heat generation term are taken into account. A typical model is proposed for describing the statistics of the outer radius of the cladding which is a stochastic variable owing to uncertainties produced by the extrusion process. The theory is illustrated by means of a simple example by examining a meaningful reliability index and the relative importance of each of the uncertainties. (Auth.)

  4. Uncertainty and sensitivity analysis of the nuclear fuel thermal behavior

    Energy Technology Data Exchange (ETDEWEB)

    Boulore, A., E-mail: antoine.boulore@cea.fr [Commissariat a l' Energie Atomique (CEA), DEN, Fuel Research Department, 13108 Saint-Paul-lez-Durance (France); Struzik, C. [Commissariat a l' Energie Atomique (CEA), DEN, Fuel Research Department, 13108 Saint-Paul-lez-Durance (France); Gaudier, F. [Commissariat a l' Energie Atomique (CEA), DEN, Systems and Structure Modeling Department, 91191 Gif-sur-Yvette (France)

    2012-12-15

    Highlights: Black-Right-Pointing-Pointer A complete quantitative method for uncertainty propagation and sensitivity analysis is applied. Black-Right-Pointing-Pointer The thermal conductivity of UO{sub 2} is modeled as a random variable. Black-Right-Pointing-Pointer The first source of uncertainty is the linear heat rate. Black-Right-Pointing-Pointer The second source of uncertainty is the thermal conductivity of the fuel. - Abstract: In the global framework of nuclear fuel behavior simulation, the response of the models describing the physical phenomena occurring during the irradiation in reactor is mainly conditioned by the confidence in the calculated temperature of the fuel. Amongst all parameters influencing the temperature calculation in our fuel rod simulation code (METEOR V2), several sources of uncertainty have been identified as being the most sensitive: thermal conductivity of UO{sub 2}, radial distribution of power in the fuel pellet, local linear heat rate in the fuel rod, geometry of the pellet and thermal transfer in the gap. Expert judgment and inverse methods have been used to model the uncertainty of these parameters using theoretical distributions and correlation matrices. Propagation of these uncertainties in the METEOR V2 code using the URANIE framework and a Monte-Carlo technique has been performed in different experimental irradiations of UO{sub 2} fuel. At every time step of the simulated experiments, we get a temperature statistical distribution which results from the initial distributions of the uncertain parameters. We then can estimate confidence intervals of the calculated temperature. In order to quantify the sensitivity of the calculated temperature to each of the uncertain input parameters and data, we have also performed a sensitivity analysis using the Sobol' indices at first order.

  5. An Optimized Thermal Analysis of Electronic Unit Used in Aircraft

    International Nuclear Information System (INIS)

    Shah, A.N.; Mir, F.; Farooq, M.; Farooq, M.

    2014-01-01

    In a field where change and growth is inevitable, new electronic packaging problems continuously arise. Smaller, but more powerful devices are prone to overheating causing intermittent system failures, corrupted signals and outright system failure. Current study is focused on the analysis of the optimized working of electronic equipment from thermal point of view. In order to achieve the objective, an approach was developed for the thermal analysis of Printed Circuit Board (PCB) including the heat dissipation of its electronic components and then removal of the heat in a sophisticated manner by considering the conduction and convection modes of heat transfer. Mathematical modeling was carried out for a certain problem to address the thermal design, and then a program was developed in MATLAB for the solution of model by using Newton-Raphson method. The proposed unit is to be mounted on an aircraft having suspected thermal characteristics owing to abrupt changes in pressure and temperature as aircraft moves quickly from a lower altitude to higher altitude. In current study, dominant mode of heat transfer was conduction revealing that the major portion of heat transfer takes place by copper cladding and that heat conduction along the length of PCB can be improved enormously by using even thin layer of copper. The results confirmed that temperatures of all the electronic components were within derated values. Meanwhile, it was known that convection also plays a significant role in the reduction of temperatures of the components. The reduction in nodal temperature was in the range of 13 to 42 %. Furthermore, altitude variation from sea level to 15240 m (above sea level) caused the reduction in pressure from 1atm to 0.1095 atm. Consequently, the temperature of the electronic components increased from 73.25 degree C to 83.83 degree C for first node 'a', and from 66.04 degree C to 68.47 degree C for last node 'n' because of the decrease in the convective heat transfer

  6. SEM investigation of heart tissue samples

    Energy Technology Data Exchange (ETDEWEB)

    Saunders, R; Amoroso, M [Physics Department, University of the West Indies, St. Augustine, Trinidad and Tobago, West Indies (Trinidad and Tobago)

    2010-07-01

    We used the scanning electron microscope to examine the cardiac tissue of a cow (Bos taurus), a pig (Sus scrofa), and a human (Homo sapiens). 1mm{sup 3} blocks of left ventricular tissue were prepared for SEM scanning by fixing in 96% ethanol followed by critical point drying (cryofixation), then sputter-coating with gold. The typical ridged structure of the myofibrils was observed for all the species. In addition crystal like structures were found in one of the samples of the heart tissue of the pig. These structures were investigated further using an EDVAC x-ray analysis attachment to the SEM. Elemental x-ray analysis showed highest peaks occurred for gold, followed by carbon, oxygen, magnesium and potassium. As the samples were coated with gold for conductivity, this highest peak is expected. Much lower peaks at carbon, oxygen, magnesium and potassium suggest that a cystallized salt such as a carbonate was present in the tissue before sacrifice.

  7. SEM investigation of heart tissue samples

    International Nuclear Information System (INIS)

    Saunders, R; Amoroso, M

    2010-01-01

    We used the scanning electron microscope to examine the cardiac tissue of a cow (Bos taurus), a pig (Sus scrofa), and a human (Homo sapiens). 1mm 3 blocks of left ventricular tissue were prepared for SEM scanning by fixing in 96% ethanol followed by critical point drying (cryofixation), then sputter-coating with gold. The typical ridged structure of the myofibrils was observed for all the species. In addition crystal like structures were found in one of the samples of the heart tissue of the pig. These structures were investigated further using an EDVAC x-ray analysis attachment to the SEM. Elemental x-ray analysis showed highest peaks occurred for gold, followed by carbon, oxygen, magnesium and potassium. As the samples were coated with gold for conductivity, this highest peak is expected. Much lower peaks at carbon, oxygen, magnesium and potassium suggest that a cystallized salt such as a carbonate was present in the tissue before sacrifice.

  8. SEM: A Cultural Change Agent

    Science.gov (United States)

    Barnes, Bradley; Bourke, Brian

    2015-01-01

    The authors advance the concept that institutional culture is a purposeful framework by which to view SEM's utility, particularly as a cultural change agent. Through the connection of seemingly independent functions of performance and behavior, implications emerge that deepen the understanding of the influence of culture on performance outcomes…

  9. Microstructure analysis and damage patterns of thermally cycled Ti–49.7Ni (at.%) wires

    International Nuclear Information System (INIS)

    Karhu, Marjaana; Lindroos, Tomi

    2012-01-01

    Long-term behaviour and fatigue endurance are the key issues in the utilization of SMA actuators, but systematic research work is still needed in this field. This study concentrates on the effects of three major design parameters on the long-term behaviour of binary Ti–49.7Ni-based actuators: the effect of the temperature interval used on thermal cycling, the effect of the stress level used and the effect of the heat-treatment state of the wire used. The long-term behaviour of the wires was studied in a custom-built fatigue test frame in which the wires were thermally cycled under a constant stress level. Before the fatigue testing, a series of heat treatments was carried out to generate optimal actuator properties for the wires. This paper concentrates on the systematic fractographic analysis of the fatigue fractured Ti–49.7Ni wires. The aim was to discover the relationships between the macro-scale behaviour and the microstructural changes of the material. During thermal cycling the surfaces of the Ti–49.7Ni wires were examined with an optical microscope. Clear connections between the detected surface defects and fracture nucleation sites were not established. Multiple cracks were initiated and grew during thermal cycling. SEM examinations showed that the fracture surfaces can be divided into different and separate zones: a smooth surface region with radial marks indicating the fatigue crack propagation area, a rougher ductile fracture surface region area and the roughest surface region on the interface of these two surfaces. It was detected that the size of the crack propagation area is related to the fatigue lives of the thermally cycled wires. Surface cracking and subsequent crack growth proved to be responsible for the accumulation of fatigue damage in the studied wires. It was detected from the fracture surface cross-sections that cracks were not initiated at the oxide layer. The major factor for nucleating the surface cracking and then shortening the

  10. Thermal analysis of LOFT modular DTT for LOCE transient

    International Nuclear Information System (INIS)

    Martin, C.M.

    1978-01-01

    A thermal analysis was performed on the LOFT modular drag-disc turbine transducer (MDTT) modular assembly. The purpose of this analysis was to determine the maximum temperature difference between the MDTT shroud and end cap during a LOCE. This temperature difference is needed for stress analysis of the MDTT endcap to fairing welds. The thermal analysis was done using TRIPLE, a three dimensional finite element code. A three dimensional model of the MDTT was made and transient temperature solutions were found for the different MDTT locations. The fluid temperature transients used for the solutions at all locations were from RELAP4 predictions of the LOFT L2-4 test which is considered the most severe temperature transient. Results of these calculations show the maximum temperature difference is 92 0 C (165 0 F) and occurs in the intact loop cold leg. This value and those found at other locations, are evaluated from the best available RELAP predicted temperatures during a nuclear LOCE

  11. Integrated Software Environment for Pressurized Thermal Shock Analysis

    Directory of Open Access Journals (Sweden)

    Dino Araneo

    2011-01-01

    Full Text Available The present paper describes the main features and an application to a real Nuclear Power Plant (NPP of an Integrated Software Environment (in the following referred to as “platform” developed at University of Pisa (UNIPI to perform Pressurized Thermal Shock (PTS analysis. The platform is written in Java for the portability and it implements all the steps foreseen in the methodology developed at UNIPI for the deterministic analysis of PTS scenarios. The methodology starts with the thermal hydraulic analysis of the NPP with a system code (such as Relap5-3D and Cathare2, during a selected transient scenario. The results so obtained are then processed to provide boundary conditions for the next step, that is, a CFD calculation. Once the system pressure and the RPV wall temperature are known, the stresses inside the RPV wall can be calculated by mean a Finite Element (FE code. The last step of the methodology is the Fracture Mechanics (FM analysis, using weight functions, aimed at evaluating the stress intensity factor (KI at crack tip to be compared with the critical stress intensity factor KIc. The platform automates all these steps foreseen in the methodology once the user specifies a number of boundary conditions at the beginning of the simulation.

  12. Thermal Performance Analysis of a Geologic Borehole Repository

    Energy Technology Data Exchange (ETDEWEB)

    Reagin, Lauren [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL)

    2016-08-16

    The Brazilian Nuclear Research Institute (IPEN) proposed a design for the disposal of Disused Sealed Radioactive Sources (DSRS) based on the IAEA Borehole Disposal of Sealed Radioactive Sources (BOSS) design that would allow the entirety of Brazil’s inventory of DSRS to be disposed in a single borehole. The proposed IPEN design allows for 170 waste packages (WPs) containing DSRS (such as Co-60 and Cs-137) to be stacked on top of each other inside the borehole. The primary objective of this work was to evaluate the thermal performance of a conservative approach to the IPEN proposal with the equivalent of two WPs and two different inside configurations using Co-60 as the radioactive heat source. The current WP configuration (heterogeneous) for the IPEN proposal has 60% of the WP volume being occupied by a nuclear radioactive heat source and the remaining 40% as vacant space. The second configuration (homogeneous) considered for this project was a homogeneous case where 100% of the WP volume was occupied by a nuclear radioactive heat source. The computational models for the thermal analyses of the WP configurations with the Co-60 heat source considered three different cooling mechanisms (conduction, radiation, and convection) and the effect of mesh size on the results from the thermal analysis. The results of the analyses yielded maximum temperatures inside the WPs for both of the WP configurations and various mesh sizes. The heterogeneous WP considered the cooling mechanisms of conduction, convection, and radiation. The temperature results from the heterogeneous WP analysis suggest that the model is cooled predominantly by conduction with effect of radiation and natural convection on cooling being negligible. From the thermal analysis comparing the two WP configurations, the results suggest that either WP configuration could be used for the design. The mesh sensitivity results verify the meshes used, and results obtained from the thermal analyses were close to

  13. Thermal Hydraulic Analysis on Containment Filtered Venting System

    Energy Technology Data Exchange (ETDEWEB)

    Bang, Young Suk; Park, Tong Kyu; Lee, Doo Yong; Lee, Byung Chul [FNC Technology Co. Ltd., Yongin (Korea, Republic of); Lee, Sang Won; Kim, Hyeong Taek [KHNP-Central Research Institute, Daejeon (Korea, Republic of)

    2014-05-15

    In this study, the thermal hydraulic conditions (e. g. pressure and flow rate) at each component have been examined and the sensitivity analysis on CFVS design parameters (e. g. water inventory, volumetric flow rate). The purpose is to know the possible range of flow conditions at each component to determine the optimum size of filtration system. GOTHIC code has been used to simulate the thermal-hydraulic behavior inside of CFVS. The behavior of flows in the CFVS has been investigated. The vessel water level and the flow rates during the CFVS operation are examined. It was observed that the vessel water level would be changed significantly due to steam condensation/thermal expansion and steam evaporation. Therefore, the vessel size and the initial water inventory should be carefully determined to keep the minimum water level required for filtration components and not to flood the components in the upper side of the vessel. It has been also observed that the volumetric flow rate is maintained during the CFVS operation, which is beneficial for pool scrubbing units. However, regarding the significant variations at the orifice downstream, careful design would be necessary.

  14. Comparative environmental analysis of waste brominated plastic thermal treatments

    International Nuclear Information System (INIS)

    Bientinesi, M.; Petarca, L.

    2009-01-01

    The aim of this research activity is to investigate the environmental impact of different thermal treatments of waste electric and electronic equipment (WEEE), applying a life cycle assessment methodology. Two scenarios were assessed, which both allow the recovery of bromine: (A) the co-combustion of WEEE and green waste in a municipal solid waste combustion plant, and (B) the staged-gasification of WEEE and combustion of produced syngas in gas turbines. Mass and energy balances on the two scenarios were set and the analysis of the life cycle inventory and the life cycle impact assessment were conducted. Two impact assessment methods (Ecoindicator 99 and Impact 2002+) were slightly modified and then used with both scenarios. The results showed that scenario B (staged-gasification) had a potentially smaller environmental impact than scenario A (co-combustion). In particular, the thermal treatment of staged-gasification was more energy efficient than co-combustion, and therefore scenario B performed better than scenario A, mainly in the impact categories of 'fossil fuels' and 'climate change'. Moreover, the results showed that scenario B allows a higher recovery of bromine than scenario A; however, Br recovery leads to environmental benefits for both the scenarios. Finally the study demonstrates that WEEE thermal treatment for energy and matter recovery is an eco-efficient way to dispose of this kind of waste

  15. lsnjbhakta@gmail.com A Comparative SEM-EDS Elemental

    African Journals Online (AJOL)

    Michael Horsfall

    effect on food production in terrestrial and aquatic compartment in ... Processing and SEM-EDS analysis of mud: In the laboratory, the ... and for SEM image observation was 15 kV, applying .... by weathering in the Omi acid clay deposit, Japan.

  16. Thermal and structural analysis of the TPX divertor

    International Nuclear Information System (INIS)

    Reis, E.E.; Baxi, C.B.; Chin, E.; Redler, K.M.

    1995-01-01

    The high heat flux on the surfaces of the TPX divertor will require a design in which a carbon-carbon (C-C) tile material is brazed to water cooled copper tubes. Thermal and structural analyses were performed to assist in the design selection of a divertor tile concept and C-C material. The relevancy of finite element analysis (FEA) for evaluating tile design was examined by conducting a literature survey to compare FEA stress results to subsequent brazing and thermal test results. The thermal responses for five tile concepts and four C-C materials were analyzed for a steady-state heat flux of 7.5 MW/m 2 . Elastic-plastic stress analyses were performed to calculate the residual stresses due to brazing C-C tiles to soft copper heat sinks for the various tile designs. Monoblock and archblock divertor tile concepts were analyzed for residual stresses in which elevated temperature creep effects were included with the elastic-plastic behavior of the copper heat sink for an assumed braze cooldown cycle. As a result of these 2D studies, the archblock concept with a 3D fine weave C-C was initially found to be a preferred design for the divertor. A 3D elastic-plastic analysis for brazing of the arch block tile was performed to investigate the singularity effects at the C-C to copper interface in the direction of the tube axis. This analysis showed that the large residual stresses at the tube and tile edge intersection would produce cracks in the C-C and possible delamination along the braze interface. These results, coupled with the difficulties experienced in brazing archblocks for the Tore Supra Limiter, required that other tile designs be considered

  17. Thermal design and analysis of high power star sensors

    Directory of Open Access Journals (Sweden)

    Fan Jiang

    2015-09-01

    Full Text Available The requirement for the temperature stability is very high in the star sensors as the high precision needs for the altitude information. Thermal design and analysis thus is important for the high power star sensors and their supporters. CCD, normally with Peltier thermoelectric cooler (PTC, is the most important sensor component in the star sensors, which is also the main heat source in the star sensors suite. The major objective for the thermal design in this paper is to design a radiator to optimize the heat diffusion for CCD and PTC. The structural configuration of star sensors, the heat sources and orbit parameters were firstly introduced in this paper. The influences of the geometrical parameters and coating material characteristics of radiators on the heat diffusion were investigated by heat flux analysis. Carbon–carbon composites were then chosen to improve the thermal conductivity for the sensor supporters by studying the heat transfer path. The design is validated by simulation analysis and experiments on orbit. The satellite data show that the temperatures of three star sensors are from 17.8 °C to 19.6 °C, while the simulation results are from 18.1 °C to 20.1 °C. The temperatures of radiator are from 16.1 °C to 16.8 °C and the corresponding simulation results are from 16.0 °C to 16.5 °C. The temperature variety of each star sensor is less than 2 °C, which satisfies the design objectives.

  18. Thermal Analysis of Concrete Storage Cask with Bird Screen Meshes

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Ju-Chan; Bang, K.S.; Yu, S.H.; Cho, S.S.; Choi, W.S. [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2016-10-15

    In this study, a thermal analysis of the cask with bird screen meshes has been performed using a porous media model. The overpack consists of a structural material, a concrete shielding, and a ventilation system. Heat is removed from the cask to the environment by a passive means only. Air inlet and outlet ducts are installed at the bottom and top of the cask for a ventilation system. Bird screen meshes are installed at the air inlet and outlet ducts to inhibit intrusion of debris from the external environment. The presence of this screens introduce an additional resistance to air flow through the ducts. Five types of meshes for bird screen were considered in this study. The bird screen meshes at the inlet and outlet vents reduce the open area for flow by about 44 - 79 %. Flow resistance coefficients for porous media model were deduced from the fluid flow analysis of bird screen meshes. Thermal analyses for the concrete cask have been carried out using a porous media model. The analysis results agreed well with the test results. Therefore, it was shown that the porous media model for the screen mesh was established to estimate the cask temperatures.

  19. Experimental investigation of thermal neutron analysis based landmine detection technology

    International Nuclear Information System (INIS)

    Zeng Jun; Chu Chengsheng; Ding Ge; Xiang Qingpei; Hao Fanhua; Luo Xiaobing

    2013-01-01

    Background: Recently, the prompt gamma-rays neutron activation analysis method is wildly used in coal analysis and explosive detection, however there were less application about landmine detection using neutron method especially in the domestic research. Purpose: In order to verify the feasibility of Thermal Neutron Analysis (TNA) method used in landmine detection, and explore the characteristic of this technology. Methods: An experimental system of TNA landmine detection was built based on LaBr 3 (Ce) fast scintillator detector and 252 Cf isotope neutron source. The system is comprised of the thermal neutron transition system, the shield system, and the detector system. Results: On the basis of the TNA, the wide energy area calibration method especially to the high energy area was investigated, and the least detection time for a typical mine was defined. In this study, the 72-type anti-tank mine, the 500 g TNT sample and several interferential objects are tested in loess, red soil, magnetic soil and sand respectively. Conclusions: The experimental results indicate that TNA is a reliable demining method, and it can be used to confirm the existence of Anti-Tank Mines (ATM) and large Anti-Personnel Mines (APM) in complicated condition. (authors)

  20. Thermal Analysis of Concrete Storage Cask with Bird Screen Meshes

    International Nuclear Information System (INIS)

    Lee, Ju-Chan; Bang, K.S.; Yu, S.H.; Cho, S.S.; Choi, W.S.

    2016-01-01

    In this study, a thermal analysis of the cask with bird screen meshes has been performed using a porous media model. The overpack consists of a structural material, a concrete shielding, and a ventilation system. Heat is removed from the cask to the environment by a passive means only. Air inlet and outlet ducts are installed at the bottom and top of the cask for a ventilation system. Bird screen meshes are installed at the air inlet and outlet ducts to inhibit intrusion of debris from the external environment. The presence of this screens introduce an additional resistance to air flow through the ducts. Five types of meshes for bird screen were considered in this study. The bird screen meshes at the inlet and outlet vents reduce the open area for flow by about 44 - 79 %. Flow resistance coefficients for porous media model were deduced from the fluid flow analysis of bird screen meshes. Thermal analyses for the concrete cask have been carried out using a porous media model. The analysis results agreed well with the test results. Therefore, it was shown that the porous media model for the screen mesh was established to estimate the cask temperatures

  1. Measuring energy expenditure in sports by thermal video analysis

    DEFF Research Database (Denmark)

    Gade, Rikke; Larsen, Ryan Godsk; Moeslund, Thomas B.

    2017-01-01

    Estimation of human energy expenditure in sports and exercise contributes to performance analyses and tracking of physical activity levels. The focus of this work is to develop a video-based method for estimation of energy expenditure in athletes. We propose a method using thermal video analysis...... to automatically extract the cyclic motion pattern, in walking and running represented as steps, and analyse the frequency. Experiments are performed with one subject in two different tests, each at 5, 8, 10, and 12 km/h. The results of our proposed video-based method is compared to concurrent measurements...

  2. Thermal coupling system analysis of a nuclear desalination plant

    International Nuclear Information System (INIS)

    Adak, A.K.; Srivastava, V.K.; Tewari, P.K.

    2010-01-01

    When a nuclear reactor is used to supply steam for desalination plant, the method of coupling has a significant technical and economic impact. The exact method of coupling depends upon the type of reactor and type of desalination plant. As a part of Nuclear Desalination Demonstration Project (NDDP), BARC has successfully commissioned a 4500 m 3 /day MSF desalination plant coupled to Madras Atomic Power Station (MAPS) at Kalpakkam. Desalination plant coupled to nuclear power plant of Pressurized Heavy Water Reactor (PHWR) type is a good example of dual-purpose nuclear desalination plant. This paper presents the thermal coupling system analysis of this plant along with technical and safety aspects. (author)

  3. Transient thermal analysis of cryocondensation pump for JET

    International Nuclear Information System (INIS)

    Baxi, C.B.; Obert, W.

    1993-08-01

    A cryopump with pumping speed of 50,000 1/sec is planned to be installed in the Joint European Torus (JET) as part of the pumped divertor. The purpose of this pump is to control the plasma impurities. The pump consists of a helium panel cooled by supercritical helium and a nitrogen shield cooled by liquid nitrogen. This paper presents the following transient thermal flow analysis for this cryopump: 1. Consequences of loss of torus vacuum on helium panel. 2. Cool down of the nitrogen shield form 300 K to 80 K

  4. Momentum integral network method for thermal-hydraulic transient analysis

    International Nuclear Information System (INIS)

    Van Tuyle, G.J.

    1983-01-01

    A new momentum integral network method has been developed, and tested in the MINET computer code. The method was developed in order to facilitate the transient analysis of complex fluid flow and heat transfer networks, such as those found in the balance of plant of power generating facilities. The method employed in the MINET code is a major extension of a momentum integral method reported by Meyer. Meyer integrated the momentum equation over several linked nodes, called a segment, and used a segment average pressure, evaluated from the pressures at both ends. Nodal mass and energy conservation determined nodal flows and enthalpies, accounting for fluid compression and thermal expansion

  5. Progressive reduction of the thermal wall system by modal analysis

    Energy Technology Data Exchange (ETDEWEB)

    Mokhtari, A.; Meslem, A.; Bounif, A.; Kadi, L. [Universite des Sciences et de la Technologie, Oran (Algeria)

    1993-12-31

    A reduction method of thermal systems called ``progress`` using the modal Analysis is presented. It allows to do, at each time of simulation, a synthesis information in the system evolution. Consequently, the limited number of descriptive and significant parameters (proper modes), can produce some extremely useful indication about dynamic evolution. However this method can eliminate proper modes of which the energetic contribution will be neglected or amortized. Some examples were studied, showing the efficiency of this method by reducing the computing time, as well as, having high precision on predicted dynamic response over time of simulation. (Authors). 4 refs., 4 figs.

  6. Thermal mechanical analysis of applications with internal heat generation

    Science.gov (United States)

    Govindarajan, Srisharan Garg

    control blade, spatial variations in temperature within the control blade occur from the non-uniform heat generation within the BORAL as a result of the non-uniform thermal neutron flux along the longitudinal direction when the control blade is partially withdrawn. There is also variation in the heating profile through the thickness and about the circumferential width of the control blade. Mathematical curve-fits are generated for the non-uniform volumetric heat generation profile caused by the thermal neutron absorption and the functions are applied as heating conditions within a finite element model of the control blade built using the commercial finite element code Abaqus FEA. The finite element model is solved as a fully coupled thermal mechanical problem as in the case of the annular target. The resulting deflection is compared with the channel gap to determine if there is a significant risk of the control blade binding during reactor operation. Hence, this dissertation will consist of two sections. The first section will seek to present the thermal and structural safety analyses of the annular targets for the production of molybdenum-99. Since there hasn't been any detailed, documented, study on these annular targets in the past, the work complied in this dissertation will help to understand the thermal-mechanical behavior and failure margins of the target during in-vessel irradiation. As the work presented in this dissertation provides a general performance analysis envelope for the annular target, the tools developed in the process can also be used as useful references for future analyses that are specific to any reactor. The numerical analysis approach adopted and the analytical models developed, can also be applied to other applications, outside the Mo-99 project domain, where internal heat generation exists such as in electronic components and nuclear reactor control blades. The second section will focus on estimating the thermally induced deflection and hence

  7. Thermal Analysis of Pure Uranium Metal, UMo and UMoSi Alloys Using a Differential Thermal Analyzer

    International Nuclear Information System (INIS)

    Yanlinastuti; Sutri Indaryati; Rahmiati

    2010-01-01

    Thermal analysis of pure uranium metal, U-7%Mo and U-7%Mo-1%Si alloys have been done using a Differential Thermal Analyzer (DTA). The experiments are conducted in order to measure the thermal stability, thermochemical properties of elevated temperature and enthalpy of the specimens. From the analysis results it is showed that uranium metal will transform from α to β phases at temperature of 667.16°C and enthalpy of 2.3034 cal/g and from β to γ phases at temperature of 773.05 °C and enthalpy of 2.8725 cal/g and start melting at temperature of 1125.26 °C and enthalpy of 2.1316 cal/g. The U-7%Mo shows its thermal stability up to temperature of 650 °C and its thermal changes at temperature of 673.75 °C indicated by the formation of an endothermic peak and enthalpy of 0.0257 cal/g. The U-7%Mo-1%Si alloys shows its thermal stability up to temperature of 550 °C and its thermal changes at temperature of 574.18 °C indicated by the formation of an endothermic peak and enthalpy of 0.613 cal/g. From the three specimens it is showed that they have a good thermal stability at temperature up to 550 °C. (author)

  8. Chemical form analysis of reaction products in Cs-adsorption on stainless steel by means of HAXPES and SEM/EDX

    Science.gov (United States)

    Kobata, M.; Okane, T.; Nakajima, K.; Suzuki, E.; Ohwada, K.; Kobayashi, K.; Yamagami, H.; Osaka, M.

    2018-01-01

    In this study, for the understandings of Cesium (Cs) adsorption behavior on structure materials in severe accidents in a light water nuclear reactor, the chemical state of Cs and its distribution on the surface of SUS304 stainless steel (SS) with different Si concentrations was investigated by hard X-ray photoelectron spectroscopy (HAXPES) and scanning electron microscope/energy dispersive X-ray spectroscopy (SEM/EDX). As a result, it was found that Cs is selectively adsorbed at the site where Si distributes with a high concentration. CsFeSiO4 is the dominant Cs products in case of low Si content, while Cs2Si2O5 and Cs2Si4O9 are formed in addition to CsFeSiO4 in case of high Si content. The chemical forms of the Cs compounds produced in the adsorption process on the SS surface have a close correlation with the concentration and chemical states of Si originally included in SS.

  9. Analysis of 19th century ceramic fragments excavated from Pirenópolis (Goiás, Brazil) using FT-IR, Raman, XRF and SEM

    Science.gov (United States)

    Freitas, Renato P.; Coelho, Filipe A.; Felix, Valter S.; Pereira, Marcelo O.; de Souza, Marcos André Torres; Anjos, Marcelino J.

    2018-03-01

    This study used Raman, FT-IR and XRF spectroscopy and SEM to analyze ceramic fragments dating from the 19th century, excavated from an old farm in the municipality of Pirenópolis, Goiás, Brazil. The results show that the samples were produced in an open oven at a firing temperature below 500 °C, using raw materials including kaolinite, hematite, magnetite, quartz, microcline, albite, anhydrite, calcite, illite, orthoclase and MnO2. Although the analyses showed similarities in the manufacturing process and the presence of many minerals was common in all samples, multivariate statistical methods (PCA) allowed a more detailed assessment of similarities and differences in the mineral composition of the samples. The results of the PCA showed that the samples excavated in one of the slave quarters (senzalas) group with those excavated at the farmhouse, where the landowner lived, which indicates a paternalistic attitude towards captives, including the sharing of ceramic materials of everyday use.

  10. Modal analysis of the thermal conductivity of nanowires: examining unique thermal transport features

    Science.gov (United States)

    Samaraweera, Nalaka; Larkin, Jason M.; Chan, Kin L.; Mithraratne, Kumar

    2018-06-01

    In this study, unique thermal transport features of nanowires over bulk materials are investigated using a combined analysis based on lattice dynamics and equilibrium molecular dynamics (EMD). The evaluation of the thermal conductivity (TC) of Lenard–Jones nanowires becomes feasible due to the multi-step normal mode decomposition (NMD) procedure implemented in the study. A convergence issue of the TC of nanowires is addressed by the NMD implementation for two case studies, which employ pristine nanowires (PNW) and superlattice nanowires. Interestingly, mode relaxation times at low frequencies of acoustic branches exhibit signs of approaching constant values, thus indicating the convergence of TC. The TC evaluation procedure is further verified by implementing EMD-based Green–Kubo analysis, which is based on a fundamentally different physical perspective. Having verified the NMD procedure, the non-monotonic trend of the TC of nanowires is addressed. It is shown that the principal cause for the observed trend is due to the competing effects of long wavelength phonons and phonon–surface scatterings as the nanowire’s cross-sectional width is changed. A computational procedure is developed to decompose the different modal contribution to the TC of shell alloy nanowires (SANWs) using virtual crystal NMD and the Allen–Feldman theory. Several important conclusions can be drawn from the results. A propagons to non-propagons boundary appeared, resulting in a cut-off frequency (ω cut); moreover, as alloy atomic mass is increased, ω cut shifts to lower frequencies. The existence of non-propagons partly causes the low TC of SANWs. It can be seen that modes with low frequencies demonstrate a similar behavior to corresponding modes of PNWs. Moreover, lower group velocities associated with higher alloy atomic mass resulted in a lower TC of SANWs.

  11. Analysis result for OECD benchmark on thermal fatigue problem

    International Nuclear Information System (INIS)

    Kamaya, Masayuki; Nakamura, Akira; Fujii, Yuzou

    2005-01-01

    The main objective of this analysis is to understand the crack growth behavior under three-dimensional (3D) thermal fatigue by conducting 3D crack initiation and propagation analyses. The possibility of crack propagation through the wall thickness of pipe, and the accuracy of the prediction of crack initiation and propagation are of major interest. In this report, in order to estimate the heat transfer coefficients and evaluate the thermal stress, conventional finite element analysis (FEA) is conducted. Then, the crack driving force is evaluated by using the finite element alternating method (FEAM), which can derive the stress intensity factor (SIF) under 3D mechanical loading based on finite element analysis without generating the mesh for a cracked body. Through these two realistic 3D numerical analyses, it has been tried to predict the crack initiation and propagation behavior. The thermal fatigue crack initiation and propagation behavior were numerically analyzed. The conventional FEA was conducted in order to estimate the heat transfer coefficient and evaluate the thermal stress. Then, the FEAM was conducted to evaluate the SIFs of surface single cracks and interacting multiple cracks, and crack growth was evaluated. The results are summarized as follows: 1. The heat transfer coefficients were estimated as H air = 40 W/m 2 K and H water = 5000 W/m 2 K. This allows simulation of the change in temperature with time at the crack initiation points obtained by the experiment. 2. The maximum stress occurred along the line of symmetry and the maximum Mises equivalent stress was 572 MPa. 3. By taking the effect of mean stress into account according to the modified Goodman diagram, the equivalent stress range and the number of cycles to crack initiation were estimated as 1093 MPa and 3.8x10 4 , respectively, although the tensile strength was assumed to be 600 MPa. 4. It was shown from the evaluated SIFs that longitudinal cracks can penetrate the wall of the pipe

  12. Three dimensional, thermal stress analysis of a welded plate

    International Nuclear Information System (INIS)

    Koening, H.A.; Lai, C.K.-F.; Morral, J.E.

    1985-01-01

    A general finite element thermal stress analysis has been developed. The analysis can be uncoupled to solve either the heat transfer problem or the stress problem independently and it can accommodate non-linear material behavior, initial states of stress and strain, and moving boundary conditions. A unique feature of the model it that it properly accounts for the latent heat effect during phase changes. Applying the moving heat flux boundary condition to simulate arc welding, the model has been used to predict the transient thermal mechanical response of a welded plate. It is the absorption and liberation of latent heat in the fusion zone of a weld which complicates numerical methods of treating welding. For pure materials and eutectic alloys the latent heat effect is less of a problem because phase changes take place at a specific temperature. But for most alloys, phase changes take place over a range of temperatures bounded by the solidus, T S , and liquidus, T L , and the latent heat effect occurs continuously over the temperature range. (author)

  13. A powerful methodology for reactor vessel pressurized thermal shock analysis

    International Nuclear Information System (INIS)

    Boucau, J.; Mager, T.

    1994-01-01

    The recent operating experience of the Pressurized Water Reactor (PWR) Industry has focused increasing attention on the issue of reactor vessel pressurized thermal shock (PTS). More specifically, the review of the old WWER-type of reactors (WWER 440/230) has indicated a sensitive behaviour to neutron embrittlement. This led already to some remedial actions including safety injection water preheating or vessel annealing. Such measures are usually taken based on the analysis of a selected number of conservative PTS events. Consideration of all postulated cooldown events would draw attention to the impact of operator action and control system effects on reactor vessel PTS. Westinghouse has developed a methodology which couples event sequence analysis with probabilistic fracture mechanics analyses, to identify those events that are of primary concern for reactor vessel integrity. Operating experience is utilized to aid in defining the appropriate event sequences and event frequencies of occurrence for the evaluation. Once the event sequences of concern are identified, detailed deterministic thermal-hydraulic and structural evaluations can be performed to determine the conditions required to minimize the extension of postulated flaws or enhance flaw arrest in the reactor vessel. The results of these analyses can then be used to better define further modifications in vessel and plant system design and to operating procedures. The purpose of the present paper will be to describe this methodology and to show its benefits for decision making. (author). 1 ref., 3 figs

  14. Simultaneous thermal analysis and thermodilatometry of hybrid fiber reinforced UHPC

    Science.gov (United States)

    Scheinherrová, Lenka; Fořt, Jan; Pavlík, Zbyšek; Černý, Robert

    2017-07-01

    Development of concrete technology and the availability of variety of materials such as silica fume, mineral microfillers and high-range water-reducing admixtures make possible to produce Ultra-High Performance Concrete (UHPC) with compressive strength higher than 160 MPa. However, UHPC is prone to spall under high temperatures what limits its use for special applications only, such as offshore and marine structures, industrial floors, security barriers etc. The spalling is caused by the thermal stresses due to the temperature gradient during heating, and by the splitting force owing to the release of water vapour. Hybrid fibre reinforcement based on combination of steel and polymer fibres is generally accepted by concrete community as a functional solution preventing spalling. In this way, Ultra-High Performance Fibre Reinforced Concrete (UHPFRC) is produced possessing high mechanical strength, durability and resistance to water and salt ingress. Since UHPFRC find use in construction industry in tunnel linings, precast tunnel segments, and high-rise buildings, its behaviour during the high-temperature exposure and its residual parameters are of the particular importance. On this account, Simultaneous Thermal Analysis (STA) and Thermodilatometry Analysis (TDA) were done in the paper to identify the structural and chemical changes in UHPFRC during its high-temperature load. Based on the experimental results, several physical and chemical processes that studied material underwent at high-temperatures were recognized. The obtained data revealed changes in the composition of the studied material and allowed identification of critical temperatures for material damage.

  15. Turbopump Design and Analysis Approach for Nuclear Thermal Rockets

    International Nuclear Information System (INIS)

    Chen, Shucheng S.; Veres, Joseph P.; Fittje, James E.

    2006-01-01

    A rocket propulsion system, whether it is a chemical rocket or a nuclear thermal rocket, is fairly complex in detail but rather simple in principle. Among all the interacting parts, three components stand out: they are pumps and turbines (turbopumps), and the thrust chamber. To obtain an understanding of the overall rocket propulsion system characteristics, one starts from analyzing the interactions among these three components. It is therefore of utmost importance to be able to satisfactorily characterize the turbopump, level by level, at all phases of a vehicle design cycle. Here at the NASA Glenn Research Center, as the starting phase of a rocket engine design, specifically a Nuclear Thermal Rocket Engine design, we adopted the approach of using a high level system cycle analysis code (NESS) to obtain an initial analysis of the operational characteristics of a turbopump required in the propulsion system. A set of turbopump design codes (PumpDes and TurbDes) were then executed to obtain sizing and performance parameters of the turbopump that were consistent with the mission requirements. A set of turbopump analyses codes (PUMPA and TURBA) were applied to obtain the full performance map for each of the turbopump components; a two dimensional layout of the turbopump based on these mean line analyses was also generated. Adequacy of the turbopump conceptual design will later be determined by further analyses and evaluation. In this paper, descriptions and discussions of the aforementioned approach are provided and future outlooks are discussed

  16. Thermal Analysis of Fission Moly Target Solid Waste Storage

    Energy Technology Data Exchange (ETDEWEB)

    Son, Hyung Min; Park, Jonghark [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2016-10-15

    There are various ways to produce Mo-99. Among them, nuclear transmutation of uranium target became the major one owing to its superior specific activity. After the fission molybdenum (FM) target is irradiated, it is transported to treatment facility to extract wanted isotope. During the process, various forms of wastes are produced including filter cake and other solid wastes. The filter cake is mostly consisted of decaying uranium compounds. The solid wastes are then packaged and moved to storage facility which will stay there for considerable amount of time. Being the continuous source of heat, the solid wastes are required to be cooled for the certain amount of time before transported to the storage area. In this study, temperature evaluation of the storage facility is carried out with pre-cooling time sensitivity to check its thermal integrity. In this study, thermal analysis on the FM target solid waste storage is performed. Finite volume method is utilized to numerically discretize and solve the geometry of interest. Analysis shows that the developed method can simulate temperature behavior during storage process, but needs to be checked against other code to see calculation accuracy. Highest temperature distribution is observed when every hole is filled with waste containers. Sensitivity results on pre-cooling time shows that at least 13 months of cooling is necessary to keep the structure integrity.

  17. Transient Thermal Analysis of 3-D Integrated Circuits Packages by the DGTD Method

    KAUST Repository

    Li, Ping; Dong, Yilin; Tang, Min; Mao, Junfa; Jiang, Li Jun; Bagci, Hakan

    2017-01-01

    Since accurate thermal analysis plays a critical role in the thermal design and management of the 3-D system-level integration, in this paper, a discontinuous Galerkin time-domain (DGTD) algorithm is proposed to achieve this purpose

  18. Development of thermal hydraulic analysis code for IHX of FBR

    International Nuclear Information System (INIS)

    Kumagai, Hiromichi; Naohara, Nobuyuki

    1991-01-01

    In order to obtain flow resistance correlations for thermal-hydrauric analysis code concerned with an intermediate heat exchanger (IHX) of FBR, the hydraulic experiment by air was carried out through a bundle of tubes arranged in an in-line and staggard fashion. The main results are summarized as follows. (1) On pressure loss per unit length of a tube bundle, which is densely a regular triangle arrangement, the in-line fashion is almost the same as the staggard one. (2) In case of 30deg sector model for IHX tube bundle, pressure loss is 1/3 in comparison with the in-line or staggard arrangement. (3) By this experimental data, flow resistance correlations for thermalhydrauric analysis code are obtained. (author)

  19. LOFT ECC Pitot Tube and Thermocouple Rake Penetration thermal analysis

    International Nuclear Information System (INIS)

    Tolan, B.J.

    1977-01-01

    A thermal analysis of the LOFT ECC Pitot Tube and Thermocouple Rake Penetration was performed using COUPLE, a two-dimensional finite element computer code. Four transients which conservatively cover all transients the rake will be exposed to were included in this analysis in order to comply with the ASME Code Section III requirements. The transients conservatively cover hot and cold leg operation, and nuclear and nonnuclear operation. The four transients include the LOCE with ECC injection transient, the single control rod drop transient, the scram transient, and the heatup with 0 to 100% load change transient. Temperature distributions in the rake were obtained for each of the four transients and several plots of node temperatures vs. time are given

  20. Thermal stress analysis of the fuel storage facility

    International Nuclear Information System (INIS)

    Chen, W.W.

    1991-12-01

    This paper presents the results of a nonlinear finite-element analysis to determine the structural integrity of the walls of the nuclear fuel storage room in the Radio Isotope Power System Facility of the Fuels and Materials Examination Facility (FMEF) Project. The analysis was performed to assess the effects of thermal loading on the walls that would result from a loss-of-cooling accident. The results obtained from using the same three-dimensional finite-element model with different types of elements, the eight-node brick element and the nonlinear concrete element, and the calculated results using the analytical solutions, are compared. The concrete responses in terms of octahedral normal and shearing stresses are described. The crack and crush states of the concrete were determined on the basis of multiaxial failure criteria

  1. Thermal hydraulic analysis of the encapsulated nuclear heat source

    Energy Technology Data Exchange (ETDEWEB)

    Sienicki, J.J.; Wade, D.C. [Argonne National Lab., IL (United States)

    2001-07-01

    An analysis has been carried out of the steady state thermal hydraulic performance of the Encapsulated Nuclear Heat Source (ENHS) 125 MWt, heavy liquid metal coolant (HLMC) reactor concept at nominal operating power and shutdown decay heat levels. The analysis includes the development and application of correlation-type analytical solutions based upon first principles modeling of the ENHS concept that encompass both pure as well as gas injection augmented natural circulation conditions, and primary-to-intermediate coolant heat transfer. The results indicate that natural circulation of the primary coolant is effective in removing heat from the core and transferring it to the intermediate coolant without the attainment of excessive coolant temperatures. (authors)

  2. Validation of the TEXSAN thermal-hydraulic analysis program

    International Nuclear Information System (INIS)

    Burns, S.P.; Klein, D.E.

    1992-01-01

    The TEXSAN thermal-hydraulic analysis program has been developed by the University of Texas at Austin (UT) to simulate buoyancy driven fluid flow and heat transfer in spent fuel and high level nuclear waste (HLW) shipping applications. As part of the TEXSAN software quality assurance program, the software has been subjected to a series of test cases intended to validate its capabilities. The validation tests include many physical phenomena which arise in spent fuel and HLW shipping applications. This paper describes some of the principal results of the TEXSAN validation tests and compares them to solutions available in the open literature. The TEXSAN validation effort has shown that the TEXSAN program is stable and consistent under a range of operating conditions and provides accuracy comparable with other heat transfer programs and evaluation techniques. The modeling capabilities and the interactive user interface employed by the TEXSAN program should make it a useful tool in HLW transportation analysis

  3. Thermal analysis and in vitro bioactivity of bioactive glass-alumina composites

    Energy Technology Data Exchange (ETDEWEB)

    Chatzistavrou, Xanthippi, E-mail: x.chatzistavrou@imperial.ac.uk [Solid State Physics Section, Physics Department, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Kantiranis, Nikolaos, E-mail: kantira@geo.auth.gr [School of Geology, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Kontonasaki, Eleana, E-mail: kont@dent.auth.gr [School of Dentistry, Department of Fixed Prosthesis and Implant Prosthodontics, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Chrissafis, Konstantinos, E-mail: hrisafis@physics.auth.gr [Solid State Physics Section, Physics Department, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Papadopoulou, Labrini, E-mail: lambrini@geo.auth.gr [School of Geology, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Koidis, Petros, E-mail: pkoidis@dent.auth.gr [School of Dentistry, Department of Fixed Prosthesis and Implant Prosthodontics, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Boccaccini, Aldo R., E-mail: a.boccaccini@imperial.ac.uk [Department of Materials, Faculty of Engineering, Imperial College, SW7 2AZ London (United Kingdom); Paraskevopoulos, Konstantinos M., E-mail: kpar@auth.gr [Solid State Physics Section, Physics Department, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece)

    2011-01-15

    Bioactive glass-alumina composite (BA) pellets were fabricated in the range 95/5-60/40 wt.% respectively and were heat-treated under a specific thermal treatment up to 950 {sup o}C. Control (unheated) and heat-treated pellets were immersed in Simulated Body Fluid (SBF) for bioactivity testing. All pellets before and after immersion in SBF were studied by Fourier Transform Infrared spectroscopy (FTIR), Scanning Electron Microscopy (SEM-EDS) and X-ray Diffraction (XRD) analysis. All composite pellets presented bioactive response. On the surface of the heat-treated pellets the development of a rich biological hydroxyapatite (HAp) layer was delayed for one day, compared to the respective control pellets. Independent of the proportion of the two components, all composites of each group (control and heat-treated) presented the same bioactive response as a function of immersion time in SBF. It was found that by the applied methodology, Al{sub 2}O{sub 3} can be successfully applied in bioactive glass composites without obstructing their bioactive response. - Research Highlights: {yields} Isostatically pressed glass-alumina composites presented apatite-forming ability. {yields} The interaction with SBF resulted in an aluminium phosphate phase formation. {yields} The formation of an aluminium phosphate phase enhanced the in vitro apatite growth.

  4. The influence of speed abilities and technical skills in early adolescence on adult success in soccer: A long-term prospective analysis using ANOVA and SEM approaches

    Science.gov (United States)

    2017-01-01

    Several talent development programs in youth soccer have implemented motor diagnostics measuring performance factors. However, the predictive value of such tests for adult success is a controversial topic in talent research. This prospective cohort study evaluated the long-term predictive value of 1) motor tests and 2) players’ speed abilities (SA) and technical skills (TS) in early adolescence. The sample consisted of 14,178 U12 players from the German talent development program. Five tests (sprint, agility, dribbling, ball control, shooting) were conducted and players’ height, weight as well as relative age were assessed at nationwide diagnostics between 2004 and 2006. In the 2014/15 season, the players were then categorized as professional (n = 89), semi-professional (n = 913), or non-professional players (n = 13,176), indicating their adult performance level (APL). The motor tests’ prognostic relevance was determined using ANOVAs. Players’ future success was predicted by a logistic regression threshold model. This structural equation model comprised a measurement model with the motor tests and two correlated latent factors, SA and TS, with simultaneous consideration for the manifest covariates height, weight and relative age. Each motor predictor and anthropometric characteristic discriminated significantly between the APL (p < .001; η2 ≤ .02). The threshold model significantly predicted the APL (R2 = 24.8%), and in early adolescence the factor TS (p < .001) seems to have a stronger effect on adult performance than SA (p < .05). Both approaches (ANOVA, SEM) verified the diagnostics’ predictive validity over a long-term period (≈ 9 years). However, because of the limited effect sizes, the motor tests’ prognostic relevance remains ambiguous. A challenge for future research lies in the integration of different (e.g., person-oriented or multilevel) multivariate approaches that expand beyond the “traditional” topic of single tests’ predictive

  5. Synthesis, characterization and thermal analysis of urea-formaldehyde/nanoSiO{sub 2} resins

    Energy Technology Data Exchange (ETDEWEB)

    Roumeli, E. [Solid State Physics Dept., School of Physics, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Papadopoulou, E. [Chimar Hellas S.A., Sofouli 88, 55131 Thessaloniki (Greece); Pavlidou, E.; Vourlias, G. [Solid State Physics Dept., School of Physics, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Bikiaris, D. [Department of Chemistry, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Paraskevopoulos, K.M. [Solid State Physics Dept., School of Physics, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece); Chrissafis, K., E-mail: hrisafis@physics.auth.gr [Solid State Physics Dept., School of Physics, Aristotle University of Thessaloniki, 54124 Thessaloniki (Greece)

    2012-01-10

    Highlights: Black-Right-Pointing-Pointer UF/nanosilica resins have been produced using the minimum cost method. Black-Right-Pointing-Pointer The new resins had good dispersion and enhanced properties. Black-Right-Pointing-Pointer Nanosilica interacts with polymer chains as was proved by FTIR and DSC. Black-Right-Pointing-Pointer Nanosilica does not affect the resin's thermal stability but enhances its mechanical properties. - Abstract: In the present work urea-formaldehyde resins (UF) containing different amounts of SiO{sub 2} nanoparticles were synthesized and studied in depth. All the hybrids were characterized with Fourier transform infrared spectroscopy (FTIR) and powder X-ray diffractometry (XRD), while the dispersion of nanoparticles was studied with scanning electron microscopy with associated energy dispersive X-ray spectrometer (SEM/EDS). It was found that even though silanol groups of SiO{sub 2} can interact with UF resin and form hydrogen bonds, aggregates of SiO{sub 2} nanoparticles can still be formed in UF resin. Their size increases as SiO{sub 2} content is increased. The curing reactions were examined with differential scanning calorimetry (DSC) and it was revealed that curing temperature of UF resin is slightly affected by the addition of nanoparticles. Furthermore, the activation energy of the curing reactions, for every hybrid, was calculated using the Kissinger's method, which implied the existence of interactions between the nanoparticles and the polymer chain. Thermogravimetric analysis (TGA) revealed that SiO{sub 2} nanoparticles do not have an effect in the thermal stability of the resin. From the application of the prepared UF/SiO{sub 2} resins in wood panels it was found that the mechanical properties of the panels, like the internal bond and the modulus of rapture, are enhanced with increasing nanoSiO{sub 2} concentration.

  6. Thermal hydraulic analysis of the JMTR improved LEU-core

    Energy Technology Data Exchange (ETDEWEB)

    Tabata, Toshio; Nagao, Yoshiharu; Komukai, Bunsaku; Naka, Michihiro; Fujiki, Kazuo [Japan Atomic Energy Research Inst., Oarai, Ibaraki (Japan). Oarai Research Establishment; Takeda, Takashi [Radioactive Waste Management and Nuclear Facility Decommissioning Technology Center, Tokai, Ibaraki (Japan)

    2003-01-01

    After the investigation of the new core arrangement for the JMTR reactor in order to enhance the fuel burn-up and consequently extend the operation period, the ''improved LEU core'' that utilized 2 additional fuel elements instead of formerly installed reflector elements, was adopted. This report describes the results of the thermal-hydraulic analysis of the improved LEU core as a part of safety analysis for the licensing. The analysis covers steady state, abnormal operational transients and accidents, which were described in the annexes of the licensing documents as design bases events. Calculation conditions for the computer codes were conservatively determined based on the neutronic analysis results and others. The results of the analysis, that revealed the safety criteria were satisfied on the fuel temperature, DNBR and primary coolant temperature, were used in the licensing. The operation license of the JMTR with the improved LEU core was granted in March 2001, and the reactor operation with new core started in November 2001 as 142nd operation cycle. (author)

  7. International Conference on SEMS 2012

    CERN Document Server

    Liu, Chuang; Scientific explanation and methodology of science; SEMS 2012

    2014-01-01

    This volume contains the contributed papers of invitees to SEMS 2012 who have also given talks at the conference. The invitees are experts in philosophy of science and technology from Asia (besides China), Australia, Europe, Latin America, North America, as well as from within China. The papers in this volume represent the latest work of each researcher in his or her expertise; and as a result, they give a good representation of the cutting-edge researches in diverse areas in different parts of the world.

  8. An algorithm for nonlinear thermal analysis of fuel bearing pads

    International Nuclear Information System (INIS)

    Attia, M.H.; D'Silva, N.

    1983-01-01

    An algorithm has been developed for accurate prediction of the temperature field in a CANDU fuel bearing pad and the extent of the nucleate boiling in the crevice region. The methodology recognizes the nonlinear nature of the problem due to the fact that local boiling is both controlling and being controlled by the conditions of heat transfer at the boundaries. The finite difference model accounts for the volumetric effect of the thermal contact resistance at the bearing pad/pressure tube interface. It also allows the evaluation of the thermal barrier effect caused by applying an oxide film on the radiused surface of the bearing pad. Information pertaining to the distribution of the coefficient of heat transfer over water-cooled surfaces has been generated. Analysis of the results indicated the significance of considering the nonlinear behaviour of the system in determining its state of equilibrium. It also indicated that, depending on the thickness of the oxide layer and the position of the bearing pad along the core of the reactor, the nucleate boiling process can be prevented

  9. ANALYSIS OF THERMAL-CHEMICAL CHARACTERISTICS OF BIOMASS ENERGY PELLETS

    Directory of Open Access Journals (Sweden)

    Zorica Gluvakov

    2014-09-01

    Full Text Available In modern life conditions, when emphasis is on environmental protection and sustainable development, fuels produced from biomass are increasingly gaining in importance, and it is necessary to consider the quality of end products obtained from biomass. Based on the existing European standards, collected literature and existing laboratory methods, this paper presents results of testing individual thermal - chemical properties of biomass energy pellets after extrusion and cooling the compressed material. Analysing samples based on standard methods, data were obtained on the basis of which individual thermal-chemical properties of pellets were estimated. Comparing the obtained results with the standards and literature sources, it can be said that moisture content, ash content and calorific values are the most important parameters for quality analysis which decide on applicability and use-value of biomass energy pellets, as biofuel. This paper also shows the impact of biofuels on the quality of environmental protection. The conclusion provides a clear statement of quality of biomass energy pellets.

  10. Challenges in thermal and hydraulic analysis of ADS target systems

    International Nuclear Information System (INIS)

    Groetzbach, G.; Batta, A.; Lefhalm, C.-H.; Otic, I.

    2004-01-01

    The liquid metal cooled spallation targets of Accelerator Driven nuclear reactor Systems obey high thermal loads; in addition some flow and cooling conditions are of a prototypical character; in contrast the operating conditions for the engaged materials are narrow; thus, the target development requires a very careful analysis by experimental and numerical means. Especially the cooling of the steel window, which is heated by the proton beam, needs special care. Some of the main goals of the experimental and numerical analyses of the thermal dynamics of those systems are discusses. The prediction of locally detached flows and of flows with larger recirculation areas suffers from insufficient turbulence modeling; this has to be compensated by using prototypical model experiments, e.g. with water, to select the adequate models and numerical schemes. The well known problems with the Reynolds analogy in predicting the heat transfer in liquid metals requires always prototypic liquid metal experiments to select and adapt the turbulent heat flux models. The uncertainties in liquid metal experiments cannot be neglected; so it is necessary to perform CFD calculations and experiments always hand in hand and to develop improve turbulent heat flux models. One contribution to an improved 3 or 4-equation model is deduced from recent Direct Numerical Simulation (DNS) data. (author)

  11. Thermal hydraulics analysis of LIBRA-SP target chamber

    International Nuclear Information System (INIS)

    Mogahed, E.A.

    1996-01-01

    LIBRA-SP is a conceptual design study of an inertially confined 1000 MWe fusion power reactor utilizing self-pinched light ion beams. There are 24 ion beams which are arranged around the reactor cavity. The reaction chamber is an upright cylinder with an inverted conical roof resembling a mushroom, and a pool floor. The vertical sides of the cylinder are occupied by a blanket zone consisting of many perforated rigid HT-9 ferritic steel tubes called PERITs (PEr-forated RIgid Tube). The breeding/cooling material, liquid lead-lithium, flows through the PERITs, providing protection to the reflector/vacuum chamber so as to make it a lifetime component. The neutronics analysis and cavity hydrodynamics calculations are performed to account for the neutron heating and also to determine the effects of vaporization/condensation processes on the surface heat flux. The steady state nuclear heating distribution at the midplane is used for thermal hydraulics calculations. The maximum surface temperature of the HT-9 is chosen to not exceed 625 degree C to avoid drastic deterioration of the metal's mechanical properties. This choice restricts the thermal hydraulics performance of the reaction cavity. The inlet first surface coolant bulk temperature is 370 degree C, and the heat exchanger inlet coolant bulk temperature is 502 degree C. 4 refs., 6 figs., 2 tabs

  12. Thermal analysis on x-ray tube for exhaust process

    Science.gov (United States)

    Kumar, Rakesh; Rao Ratnala, Srinivas; Veeresh Kumar, G. B.; Shivakumar Gouda, P. S.

    2018-02-01

    It is great importance in the use of X-rays for medical purposes that the dose given to both the patient and the operator is carefully controlled. There are many types of the X- ray tubes used for different applications based on their capacity and power supplied. In present thesis maxi ray 165 tube is analysed for thermal exhaust processes with ±5% accuracy. Exhaust process is usually done to remove all the air particles and to degasify the insert under high vacuum at 2e-05Torr. The tube glass is made up of Pyrex material, 95%Tungsten and 5%rhenium is used as target material for which the melting point temperature is 3350°C. Various materials are used for various parts; during the operation of X- ray tube these waste gases are released due to high temperature which in turn disturbs the flow of electrons. Thus, before using the X-ray tube for practical applications it has to undergo exhaust processes. Initially we build MX 165 model to carry out thermal analysis, and then we simulate the bearing temperature profiles with FE model to match with test results with ±5%accuracy. At last implement the critical protocols required for manufacturing processes like MF Heating, E-beam, Seasoning and FT.

  13. FFTF vertical sodium storage tank preliminary thermal analysis

    International Nuclear Information System (INIS)

    Irwin, J.J.

    1995-01-01

    In the FFTF Shutdown Program, sodium from the primary and secondary heat transport loops, Interim Decay Storage (IDS), and Fuel Storage Facility (FSF) will be transferred to four large storage tanks for temporary storage. Three of the storage tanks will be cylindrical vertical tanks having a diameter of 28 feet, height of 22 feet and fabricated from carbon steel. The fourth tank is a horizontal cylindrical tank but is not the subject of this report. The storage tanks will be located near the FFTF in the 400 Area and rest on a steel-lined concrete slab in an enclosed building. The purpose of this work is to document the thermal analyses that were performed to ensure that the vertical FFTF sodium storage tank design is feasible from a thermal standpoint. The key criterion for this analysis is the time to heat up the storage tank containing frozen sodium at ambient temperature to 400 F. Normal operating conditions include an ambient temperature range of 32 F to 120 F. A key parameter in the evaluation of the sodium storage tank is the type of insulation. The baseline case assumed six inches of calcium silicate insulation. An alternate case assumed refractory fiber (Cerablanket) insulation also with a thickness of six inches. Both cases assumed a total electrical trace heat load of 60 kW, with 24 kW evenly distributed on the bottom head and 36 kW evenly distributed on the tank side wall

  14. Thermal Hydraulic Analysis of RPV Support Cooling System for HTGR

    International Nuclear Information System (INIS)

    Min Qi; Wu Xinxin; Li Xiaowei; Zhang Li; He Shuyan

    2014-01-01

    Passive safety is now of great interest for future generation reactors because of its reduction of human interaction and avoidance of failures of active components. reactor pressure vessel (RPV) support cooling system (SCS) for high temperature gas-cooled reactor (HTGR) is a passive safety system and is used to cool the concrete seats for the four RPV supports at its bottom. The SCS should have enough cooling capacity to ensure the temperature of the concrete seats for the supports not exceeding the limit temperature. The SCS system is composed of a natural circulation water loop and an air cooling tower. In the water loop, there is a heat exchanger embedded in the concrete seat, heat is transferred by thermal conduction and convection to the cooling water. Then the water is cooled by the air cooler mounted in the air cooling tower. The driving forces for water and air are offered by the density differences caused by the temperature differences. In this paper, the thermal hydraulic analysis for this system was presented. Methods for decoupling the natural circulation and heat transfer between the water loop and air flow were introduced. The operating parameters for different working conditions and environment temperatures were calculated. (author)

  15. Space Shuttle Communications Coverage Analysis for Thermal Tile Inspection

    Science.gov (United States)

    Kroll, Quin D.; Hwu, Shian U.; Upanavage, Matthew; Boster, John P.; Chavez, Mark A.

    2009-01-01

    The space shuttle ultra-high frequency Space-to-Space Communication System has to provide adequate communication coverage for astronauts who are performing thermal tile inspection and repair on the underside of the space shuttle orbiter (SSO). Careful planning and quantitative assessment are necessary to ensure successful system operations and mission safety in this work environment. This study assesses communication systems performance for astronauts who are working in the underside, non-line-of-sight shadow region on the space shuttle. All of the space shuttle and International Space Station (ISS) transmitting antennas are blocked by the SSO structure. To ensure communication coverage at planned inspection worksites, the signal strength and link margin between the SSO/ISS antennas and the extravehicular activity astronauts, whose line-of-sight is blocked by vehicle structure, was analyzed. Investigations were performed using rigorous computational electromagnetic modeling techniques. Signal strength was obtained by computing the reflected and diffracted fields along the signal propagation paths between transmitting and receiving antennas. Radio frequency (RF) coverage was determined for thermal tile inspection and repair missions using the results of this computation. Analysis results from this paper are important in formulating the limits on reliable communication range and RF coverage at planned underside inspection and repair worksites.

  16. Thermal analysis and safety information for metal nanopowders by DSC

    Energy Technology Data Exchange (ETDEWEB)

    Tseng, J.M.; Huang, S.T. [Institute of Safety and Disaster Prevention Technology, Central Taiwan University of Science and Technology, 666, Buzih Road, Beitun District, Taichung 40601, Taiwan, ROC (China); Duh, Y.S.; Hsieh, T.Y.; Sun, Y.Y. [Department of Safety Health and Environmental Engineering, National United University, Miaoli, Taiwan, ROC (China); Lin, J.Z. [Institute of Safety and Disaster Prevention Technology, Central Taiwan University of Science and Technology, 666, Buzih Road, Beitun District, Taichung 40601, Taiwan, ROC (China); Wu, H.C. [Institute of Occupational Safety and Health, Council of Labor Affairs, Taipei, Taiwan, ROC (China); Kao, C.S., E-mail: jcsk@nuu.edu.tw [Department of Safety Health and Environmental Engineering, National United University, Miaoli, Taiwan, ROC (China)

    2013-08-20

    Highlights: • Metal nanopowders are common and frequently employed in industry. • Nano iron powder experimental results of T{sub o} were 140–150 °C. • Safety information can benefit relevant metal powders industries. - Abstract: Metal nanopowders are common and frequently employed in industry. Iron is mostly applied in high-performance magnetic materials and pollutants treatment for groundwater. Zinc is widely used in brass, bronze, die casting metal, alloys, rubber, and paints, etc. Nonetheless, some disasters induced by metal powders are due to the lack of related safety information. In this study, we applied differential scanning calorimetry (DSC) and used thermal analysis software to evaluate the related thermal safety information, such as exothermic onset temperature (T{sub o}), peak of temperature (T{sub p}), and heat of reaction (ΔH). The nano iron powder experimental results of T{sub o} were 140–150 °C, 148–158 °C, and 141–149 °C for 15 nm, 35 nm, and 65 nm, respectively. The ΔH was larger than 3900 J/g, 5000 J/g, and 3900 J/g for 15 nm, 35 nm, and 65 nm, respectively. Safety information can benefit the relevant metal powders industries for preventing accidents from occurring.

  17. Scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX) and aerosol time-of-flight mass spectrometry (ATOFMS) single particle analysis of metallurgy plant emissions

    International Nuclear Information System (INIS)

    Arndt, J.; Deboudt, K.; Anderson, A.; Blondel, A.; Eliet, S.; Flament, P.; Fourmentin, M.; Healy, R.M.; Savary, V.; Setyan, A.; Wenger, J.C.

    2016-01-01

    The chemical composition of single particles deposited on industrial filters located in three different chimneys of an iron-manganese (Fe–Mn) alloy manufacturing plant have been compared using aerosol time-of-flight mass spectrometry (ATOFMS) and scanning electron microscopy–energy dispersive X-ray spectrometry (SEM-EDX). Very similar types of particles were observed using both analytical techniques. Calcium-containing particles dominated in the firing area of the sintering unit, Mn and/or Al-bearing particles were observed at the cooling area of the sintering unit, while Mn-containing particles were dominant at the smelting unit. SEM-EDX analysis of particles collected downstream of the industrial filters showed that the composition of the particles emitted from the chimneys is very similar to those collected on the filters. ATOFMS analysis of ore samples was also performed to identify particulate emissions that could be generated by wind erosion and manual activities. Specific particle types have been identified for each emission source (chimneys and ore piles) and can be used as tracers for source apportionment of ambient PM measured in the vicinity of the industrial site. - Highlights: • Similar composition for emitted particles as those collected on the chimney filters. • Emitted particles dominated by Ca-, Mn and/or Al-containing particles. • Identification of specific particle types emitted by the different process units. - The particles emitted by metallurgy activities are fully described by ATOFMS and SEM-EDX, enabling the identification of specific particle types from the different units of the process.

  18. Analysis of carbon based materials under fusion relevant thermal loads

    International Nuclear Information System (INIS)

    Compan, Jeremie Saint-Helene

    2008-01-01

    how anisotropy can be tailored and on the strategies which were applied for the production of the investigated materials. Textures of fibers and microstructures of matrices were also described. Thermo-physical properties such as thermal conductivity and thermal expansion of some CFCs were studied for different materials' orientations. For the first time, some off-axis results of thermal conductivity and thermal expansion for fusion related CFCs are displayed. Room temperature bending and tensile loading of CFCs were performed and they allowed relating the microstructural findings to the anisotropic mechanical response. Fiber architecture of CFCs and interfacial shear strength between the fiber and the matrix appeared to be the main parameters which dictate the fracture mechanisms. In addition, the analysis of five batches of one CFC permitted to understand the difficulty of reproducing such advanced material. The differences in terms of needling process were related to the variations of the tensile properties in the various fibrous directions. Finally, fusion-relevant transient heat loads were simulated on the investigated CBMs within various high heat flux facilities, i.e. electron beam, ion beam and plasma gun. Erosion scenarios at different scales were compiled in relation to the CBM properties but also the type of the transient event. The locally preferential erosion and ejection of material from the surface of the CBM are comprehensively described as well as their implications. This ejection of hot particles from the CBM surface (so-called Brittle Destruction (BD) mechanism) was defined, explained and analyzed. An experimental thermal shock resistance criterion based on thermal-shock induced weight loss is presented. After analyzing the anisotropic response of CFCs to transient heat loads in their three orthotropic fiber directions, attempts to reduce BD were done by loading them under off-axis orientations. It partly succeeded and led to the observation of

  19. Assessment of RANS CFD modelling for pressurised thermal shock analysis

    International Nuclear Information System (INIS)

    Sander M Willemsen; Ed MJ Komen; Sander Willemsen

    2005-01-01

    in the cold leg and downcomer. The initial computations were performed using the commonly used porous medium representation for the core and omission of the lower plenum internals. These assumption, however, lead to unrealistic circumferential flow oscillations in the downcomer, and consequently, a wrong prediction of the thermal load on the RPV wall. Therefore, a detailed geometrical model with a refined numerical mesh was used, which suppressed these erroneous oscillations. Furthermore, it was confirmed that an extended k-ε or SST k-ω turbulence model which include turbulence production/destruction terms due to buoyancy has to be used in order to correctly predict the thermal stratification in the cold leg. The measurements in the downcomer show rapidly fluctuating signals, which indicate vigorous turbulent mixing and/or oscillations. It was found that reasonable agreement could be achieved with RANS type turbulence modelling for the prediction of the phenomena occurring in the downcomer. Improvement of these results can be expected from non-statistically averaged turbulent modelling like Large Eddy Simulations. It is concluded that the current RANS models already provide a significant improvement over thermal-hydraulic system code analysis, since three-dimensional effects are predicted and no tuning of the code to expensive experiments is needed. (authors)

  20. Thermal behaviour analysis of SRF cavities and superconducting HOM couplers

    International Nuclear Information System (INIS)

    Fouaidy, M.; Junquera, T.

    1993-01-01

    Two individual papers appear in this report, titled Thermal model calculations in superconducting RF cavities, and Thermal study of HOM couplers for superconducting RF cavities. Both were indexed separately for the INIS database. (R.P.)

  1. Orbital maneuvering vehicle thermal design and analysis techniques

    Science.gov (United States)

    Chapter, J.

    1986-01-01

    This paper describes the OMV thermal design that is required to maintain components within temperature limits for all mission phases. A key element in the OMV thermal design is the application of a motorized thermal shade assembly that is a replacement for the more conventional variable conductance heat pipes or louvers. The thermal shade assembly covers equipment module radiator areas, and based upon the radiator temperature input to onboard computer, opens and closes the shade, varying the effective radiator area. Thermal design verification thermal analyses results are presented. Selected thermal analyses methods, including several unique subroutines, are discussed. A representation of enclosure Script F equations, in matrix form, is also included. Personal computer application to the development of the OMV thermal design is summarized.

  2. Finite element analysis of thermal stress distribution in different ...

    African Journals Online (AJOL)

    Nigerian Journal of Clinical Practice. Journal Home ... Von Mises and thermal stress distributions were evaluated. Results: In all ... distribution. Key words: Amalgam, finite element method, glass ionomer cement, resin composite, thermal stress ...

  3. Heat transfer and thermal stress analysis in grooved tubes

    Indian Academy of Sciences (India)

    ANSYS (1997) computer code has been used to analyse the thermal ... The numerical method is used succesfully to solve the governing equations ... thermal stress is an important criterion for consideration in the design of new compact heat.

  4. Nonlinear thermal reduced model for Microwave Circuit Analysis

    OpenAIRE

    Chang, Christophe; Sommet, Raphael; Quéré, Raymond; Dueme, Ph.

    2004-01-01

    With the constant increase of transistor power density, electro thermal modeling is becoming a necessity for accurate prediction of device electrical performances. For this reason, this paper deals with a methodology to obtain a precise nonlinear thermal model based on Model Order Reduction of a three dimensional thermal Finite Element (FE) description. This reduced thermal model is based on the Ritz vector approach which ensure the steady state solution in every case. An equi...

  5. Isotopic analysis of boron by thermal ionization mass spectrometry

    International Nuclear Information System (INIS)

    Kakazu, M.H.; Sarkis, J.E.S.; Souza, I.M.S.

    1991-07-01

    This paper presents a methodology for isotopic analysis of boron by thermal ionization mass spectrometry technique through the ion intensity measurement of Na 2 BO + 2 in H 3 BO 3 , B o and B 4 C. The samples were loaded on single tantalum filaments by different methods. In the case of H 3 BO 3 , the method of neutralization with NaOH was used. For B 4 C the alcaline fusion with Na 2 CO 3 and for B o dissolution with 1:1 nitric sulfuric acid mixture followed by neutralization with NaOH was used. The isotopic ratio measurements were obtained by the use of s Faraday cup detector with external precision of ±0,4% and accuracy of ±0,1%, relative to H 3 BO 3 isotopic standard NBS 951. The effects of isotopic fractionation was studied in function of the time during the analyses and the different chemical forms of deposition. (author)

  6. Thermal dynamic analysis of sulfur removal from coal by electrolysis

    Energy Technology Data Exchange (ETDEWEB)

    Li, D.; Gao, J.; Meng, F. [Qinghua University, Beijing (China). Dept. of Thermal Engineering

    2002-06-01

    The electrolytic reactions about sulfur removal from coal were studied by using chemical thermal dynamic analysis. According to the thermodynamical data, the Gibbs free energy value of the electrolytic reactions of pyritic and organic sulfur removal from coal is higher than zero. So, these electrolytic reactions are not spontaneous chemical reactions. In order to carry out desulfurisation by electrolysis, a certain voltage is necessary and important. Because theoretic decomposition voltage of pyrite and some parts of organic sulfur model compound is not very high, electrolysis reactions are easily to be carried out by using electrolysis technology. Mn ion and Fe ion are added into electrolysis solutions to accelerate the desulfurisation reaction. The electrolytic decomposition of coal is discussed. Because the theoretical decomposition voltage of some organic model compound is not high, the coal decomposition might happen. 17 refs., 4 tabs.

  7. The analysis of thermal stability of detonation nanodiamond

    International Nuclear Information System (INIS)

    Efremov, V P; Zakatilova, E I

    2016-01-01

    The detonation nanodiamond is a new perspective material. Ammunition recycling with use of high explosives and obtaining nanodiamond as the result of the detonation synthesis have given a new motivation for searching of their application areas. In this work nanodiamond powder has been investigated by the method of synchronous thermal analysis. Experiments have been carried out at atmospheric pressure in the environment of argon. Nanodiamond powder has been heated in the closed corundum crucible at the temperature range of 30-1500 °C. The heating rates were varied from 2 K/min to 20 K/min. After the heat treatment, the samples have been studied by the x-ray diffraction and the electron microscopy. As one of the results of this work, it has been found that the detonation nanodiamond has not started the transition into graphite at the temperature below 800 °C. (paper)

  8. Thermal analysis of gyrotron traveling-wave tube collector

    International Nuclear Information System (INIS)

    Zheng Zhiqing; Luo Yong; Jiang Wei; Tang Yong

    2013-01-01

    In order to solve cooling problem of the gyrotron traveling-wave tube(TWT) collector and guarantee the gyrotron TWT's reliability and stability, the electron trajectories in the gyrotron TWT are simulated using CST electron simulation software. Thermal analysis of the collector with finite element software ANSYS is performed. The ways of applying boundary that affects the distribution of collector temperature are compared. The influence of the water temperature and flow rate on collector temperature distribution under actual heat fluxes (boundary condition) is researched. The size and number of collector fins are optimized, and a relatively perfect structure is obtained finally. The result estimated by simulation is consistent with the experiment and proves that the model and method employed in this work are suitable. (authors)

  9. TAPIR, Thermal Analysis of HTGR with Graphite Sleeve Fuel Elements

    International Nuclear Information System (INIS)

    Weicht, U.; Mueller, W.

    1983-01-01

    1 - Nature of the physical problem solved: Thermal analysis of a reactor core containing internally and/or externally gas cooled prismatic fuel elements of various geometries, rating, power distribution, and material properties. 2 - Method of solution: A fuel element in this programme is regarded as a sector of a fuelled annulus with graphite sleeves of any shape on either side and optional annular gaps between fuel and graphite and/or within the graphite. It may have any centre angle and the fuelled annulus may become a solid cylindrical rod. Heat generation in the fuel is assumed to be uniform over the cross section and peripheral heat flux into adjacent sectors is ignored. Fuel elements and coolant channels are treated separately, then linked together to fit a specified pattern. 3 - Restrictions on the complexity of the problem: Maxima of: 50 fuel elements; 50 cooled channels; 25 fuel geometries; 25 coolant channel geometries; 10 axial power distributions; 10 graphite conductivities

  10. Analysis of thermal systems using the entropy balance method

    Energy Technology Data Exchange (ETDEWEB)

    Huang, C L.D.; Fartaj, S A; Fenton, D L [Kansas State Univ., Manhattan, KS (United States). Dept. of Mechanical Engineering

    1992-04-01

    This study investigates the applicability of the second law of thermodynamics using an entropy balance method to analyse and design thermal systems. As examples, the entropy balance method is used to analyse a single stage chiller system and a single stage heat transformer, both with lithium-bromide/water as the working fluid. The entropy method yields not only the same information as is conveyed by the methods of energy and exergy analysis, but it also predicts clearly the influence of irreversibilities of individual components on the coefficient of performance and its effectiveness, based on the process properties, rather than on ambient conditions. Furthermore, this method is capable of presenting the overall distribution of the heat input by displaying the additional heat required to overcome irreversibility of each component without ambiguity. (Author).

  11. The analysis of thermal stability of detonation nanodiamond

    Science.gov (United States)

    Efremov, V. P.; Zakatilova, E. I.

    2016-11-01

    The detonation nanodiamond is a new perspective material. Ammunition recycling with use of high explosives and obtaining nanodiamond as the result of the detonation synthesis have given a new motivation for searching of their application areas. In this work nanodiamond powder has been investigated by the method of synchronous thermal analysis. Experiments have been carried out at atmospheric pressure in the environment of argon. Nanodiamond powder has been heated in the closed corundum crucible at the temperature range of 30-1500 °C. The heating rates were varied from 2 K/min to 20 K/min. After the heat treatment, the samples have been studied by the x-ray diffraction and the electron microscopy. As one of the results of this work, it has been found that the detonation nanodiamond has not started the transition into graphite at the temperature below 800 °C.

  12. Model-based analysis of thermal insulation coatings

    DEFF Research Database (Denmark)

    Kiil, Søren

    2014-01-01

    Thermal insulation properties of coatings based on selected functional filler materials are investigated. The underlying physics, thermal conductivity of a heterogeneous two-component coating, and porosity and thermal conductivity of hollow spheres (HS) are quantified and a mathematical model for...

  13. Modelling and analysis of radial thermal stresses and temperature ...

    African Journals Online (AJOL)

    A theoretical investigation has been undertaken to study operating temperatures, heat fluxes and radial thermal stresses in the valves of a modern diesel engine with and without air-cavity. Temperatures, heat fluxes and radial thermal stresses were measured theoretically for both cases under all four thermal loading ...

  14. Computer aided analysis, simulation and optimisation of thermal sterilisation processes.

    Science.gov (United States)

    Narayanan, C M; Banerjee, Arindam

    2013-04-01

    Although thermal sterilisation is a widely employed industrial process, little work is reported in the available literature including patents on the mathematical analysis and simulation of these processes. In the present work, software packages have been developed for computer aided optimum design of thermal sterilisation processes. Systems involving steam sparging, jacketed heating/cooling, helical coils submerged in agitated vessels and systems that employ external heat exchangers (double pipe, shell and tube and plate exchangers) have been considered. Both batch and continuous operations have been analysed and simulated. The dependence of del factor on system / operating parameters such as mass or volume of substrate to be sterilised per batch, speed of agitation, helix diameter, substrate to steam ratio, rate of substrate circulation through heat exchanger and that through holding tube have been analysed separately for each mode of sterilisation. Axial dispersion in the holding tube has also been adequately accounted for through an appropriately defined axial dispersion coefficient. The effect of exchanger characteristics/specifications on the system performance has also been analysed. The multiparameter computer aided design (CAD) software packages prepared are thus highly versatile in nature and they permit to make the most optimum choice of operating variables for the processes selected. The computed results have been compared with extensive data collected from a number of industries (distilleries, food processing and pharmaceutical industries) and pilot plants and satisfactory agreement has been observed between the two, thereby ascertaining the accuracy of the CAD softwares developed. No simplifying assumptions have been made during the analysis and the design of associated heating / cooling equipment has been performed utilising the most updated design correlations and computer softwares.

  15. Validation and further development of a novel thermal analysis method

    Energy Technology Data Exchange (ETDEWEB)

    Mathews, E.H.; Shuttleworth, A.G.; Rousseau, P.G. [Pretoria Univ. (South Africa). Dept. of Mechanical Engineering

    1994-12-31

    The design of thermal and energy efficient buildings requires inter alia the investigation of the passive performance, natural ventilation, mechanical ventilation as well as structural and evaporative cooling of the building. Only when these fail to achieve the desired thermal comfort should mechanical cooling systems be considered. Few computer programs have the ability to investigate all these comfort regulating methods at the design stage. The QUICK design program can simulate these options with the exception of mechanical cooling. In this paper, Quick`s applicability is extended to include the analysis of basic air-conditioning systems. Since the design of these systems is based on indoor loads, it was necessary to validate QUICK`s load predictions before extending it. This article addresses validation in general and proposes a procedure to establish the efficiency of a program`s load predictions. This proposed procedure is used to compare load predictions by the ASHRAE, CIBSE, CARRIER, CHEETAH, BSIMAC and QUICK methods for 46 case studies involving 36 buildings in various climatic conditions. Although significant differences in the results of the various methods were observed, it is concluded that QUICK can be used with the same confidence as the other methods. It was further shown that load prediction programs usually under-estimate the effect of building mass and therefore over-estimate the peak loads. The details for the 46 case studies are available to other researchers for further verification purposes. With the confidence gained in its load predictions, QUICK was extended to include air-conditioning system analysis. The program was then applied to different case studies. It is shown that system size and energy usage can be reduced by more than 60% by using a combination of passive and mechanical cooling systems as well as different control strategies. (author)

  16. Scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX) and aerosol time-of-flight mass spectrometry (ATOFMS) single particle analysis of metallurgy plant emissions.

    Science.gov (United States)

    Arndt, J; Deboudt, K; Anderson, A; Blondel, A; Eliet, S; Flament, P; Fourmentin, M; Healy, R M; Savary, V; Setyan, A; Wenger, J C

    2016-03-01

    The chemical composition of single particles deposited on industrial filters located in three different chimneys of an iron-manganese (Fe-Mn) alloy manufacturing plant have been compared using aerosol time-of-flight mass spectrometry (ATOFMS) and scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX). Very similar types of particles were observed using both analytical techniques. Calcium-containing particles dominated in the firing area of the sintering unit, Mn and/or Al-bearing particles were observed at the cooling area of the sintering unit, while Mn-containing particles were dominant at the smelting unit. SEM-EDX analysis of particles collected downstream of the industrial filters showed that the composition of the particles emitted from the chimneys is very similar to those collected on the filters. ATOFMS analysis of ore samples was also performed to identify particulate emissions that could be generated by wind erosion and manual activities. Specific particle types have been identified for each emission source (chimneys and ore piles) and can be used as tracers for source apportionment of ambient PM measured in the vicinity of the industrial site. Copyright © 2015 Elsevier Ltd. All rights reserved.

  17. Geochemical and mineralogical analysis of stone anchors from west coast of India: Provenance study using thin sections, XRF and SEM-EDS

    Digital Repository Service at National Institute of Oceanography (India)

    Tripati, S.; Mudholkar, A.V.; Vora, K.H.; Rao, B.R.; Gaur, A.S.; Sundaresh

    for petrographical and geochemical analysis. One surface of the rock chip was ground to finesmoothnessandwasmountedontotheglassslidewithhelp of Araldite C210 (resin & hardner) and then clamped to prevent developmentof air bubbles. After overnight cooling and curing...

  18. Applications of artificial neural networks for thermal analysis of heat exchangers - A review

    International Nuclear Information System (INIS)

    Mohanraj, M.; Jayaraj, S.; Muraleedharan, C.

    2015-01-01

    Artificial neural networks (ANN) have been widely used for thermal analysis of heat exchangers during the last two decades. In this paper, the applications of ANN for thermal analysis of heat exchangers are reviewed. The reported investigations on thermal analysis of heat exchangers are categorized into four major groups, namely (i) modeling of heat exchangers, (ii) estimation of heat exchanger parameters, (iii) estimation of phase change characteristics in heat exchangers and (iv) control of heat exchangers. Most of the papers related to the applications of ANN for thermal analysis of heat exchangers are discussed. The limitations of ANN for thermal analysis of heat exchangers and its further research needs in this field are highlighted. ANN is gaining popularity as a tool, which can be successfully used for the thermal analysis of heat exchangers with acceptable accuracy. (authors)

  19. The thermal analysis of low heat generating radioactive wastes in land disposal facilities

    International Nuclear Information System (INIS)

    Lympany, S.D.

    1984-08-01

    A procedure is developed which allows a simple thermal analysis of a radioactive waste repository. The procedure is used to establish if the thermally induced groundwater flow is important when considering the transport of radionuclides from the repository, and thereby indicates if this flow should be taken into account in a detailed thermal assessment. (author)

  20. CFD thermal-hydraulic analysis of a CANDU fuel channel

    International Nuclear Information System (INIS)

    Catana, A.; Prisecaru, I.; Dupleac, D.; Danila, N.

    2009-01-01

    This paper presents the numerical investigation of a CANDU fuel channel using CFD (Computational fluid dynamics) methodology approach. Limited computer power available at Bucharest University POLITEHNICA forced the authors to analyse only segments of fuel channel namely the significant ones: fuel bundle junctions with adjacent segments, fuel bundle spacer planes with adjacent segments, regular segments of fuel bundles. The computer code used is FLUENT. Fuel bundles contained in pressure tubes forms a complex flow domain. The flow is characterized by high turbulence and in some parts of fuel channel also by multi-phase flow. The flow in the fuel channel has been simulated by solving the equations for conservation of mass and momentum. For turbulence modelling the standard k-e model is employed although other turbulence models can be used as well. In this paper we do not consider heat generation and heat transfer capabilities of CFD methods. Since we consider only some relatively short segments of a CANDU fuel channel we can assume, for this starting stage, that heat transfer is not very important for these short segments of fuel channel. The boundary conditions for CFD analysis are provided by system and sub-channel analysis. In this paper the discussion is focused on some flow parameters behaviour at the bundle junction, spacer's plane configuration, etc. In this paper we present results for Standard CANDU 6 Fuel Bundles as a basis for CFD thermal-hydraulic analysis of INR proposed SEU43 and other new nuclear fuels. (authors)

  1. CFD analysis of aircraft fuel tanks thermal behaviour

    Science.gov (United States)

    Zilio, C.; Longo, G. A.; Pernigotto, G.; Chiacchio, F.; Borrelli, P.; D'Errico, E.

    2017-11-01

    This work is carried out within the FP7 European research project TOICA (Thermal Overall Integrated Conception of Aircraft, http://www.toica-fp7.eu/). One of the tasks foreseen for the TOICA project is the analysis of fuel tanks as possible heat sinks for future aircrafts. In particular, in the present paper, commercial regional aircraft is considered as case study and CFD analysis with the commercial code STAR-CCM+ is performed in order to identify the potential capability to use fuel stored in the tanks as a heat sink for waste heat dissipated by other systems. The complex physical phenomena that characterize the heat transfer inside liquid fuel, at the fuel-ullage interface and inside the ullage are outlined. Boundary conditions, including the effect of different ground and flight conditions, are implemented in the numerical simulation approach. The analysis is implemented for a portion of aluminium wing fuel tank, including the leading edge effects. Effect of liquid fuel transfer among different tank compartments and the air flow in the ullage is included. According to Fuel Tank Flammability Assessment Method (FTFAM) proposed by the Federal Aviation Administration, the results are exploited in terms of exponential time constants and fuel temperature difference to the ambient for the different cases investigated.

  2. Exergy Analysis of Operating Lignite Fired Thermal Power Plant

    Directory of Open Access Journals (Sweden)

    K. Murugesan

    2009-01-01

    Full Text Available The energy assessment must be made through the energy quantity as well as the quality. But the usual energy analysisevaluates the energy generally on its quantity only. However, the exergy analysis assesses the energy on quantity as well asthe quality. The aim of the exergy analysis is to identify the magnitudes and the locations of real energy losses, in order toimprove the existing systems, processes or components. The present paper deals with an exergy analysis performed on anoperating 50MWe unit of lignite fired steam power plant at Thermal Power Station-I, Neyveli Lignite Corporation Limited,Neyveli, Tamil Nadu, India. The exergy losses occurred in the various subsystems of the plant and their components havebeen calculated using the mass, energy and exergy balance equations. The distribution of the exergy losses in several plantcomponents during the real time plant running conditions has been assessed to locate the process irreversibility. The Firstlaw efficiency (energy efficiency and the Second law efficiency (exergy efficiency of the plant have also been calculated.The comparison between the energy losses and the exergy losses of the individual components of the plant shows that themaximum energy losses of 39% occur in the condenser, whereas the maximum exergy losses of 42.73% occur in the combustor.The real losses of energy which has a scope for the improvement are given as maximum exergy losses that occurredin the combustor.

  3. The Effect of Nonnormality on CB-SEM and PLS-SEM Path Estimates

    OpenAIRE

    Z. Jannoo; B. W. Yap; N. Auchoybur; M. A. Lazim

    2014-01-01

    The two common approaches to Structural Equation Modeling (SEM) are the Covariance-Based SEM (CB-SEM) and Partial Least Squares SEM (PLS-SEM). There is much debate on the performance of CB-SEM and PLS-SEM for small sample size and when distributions are nonnormal. This study evaluates the performance of CB-SEM and PLS-SEM under normality and nonnormality conditions via a simulation. Monte Carlo Simulation in R programming language was employed to generate data based on the theoretical model w...

  4. Stochastic analysis of uncertain thermal parameters for random thermal regime of frozen soil around a single freezing pipe

    Science.gov (United States)

    Wang, Tao; Zhou, Guoqing; Wang, Jianzhou; Zhou, Lei

    2018-03-01

    The artificial ground freezing method (AGF) is widely used in civil and mining engineering, and the thermal regime of frozen soil around the freezing pipe affects the safety of design and construction. The thermal parameters can be truly random due to heterogeneity of the soil properties, which lead to the randomness of thermal regime of frozen soil around the freezing pipe. The purpose of this paper is to study the one-dimensional (1D) random thermal regime problem on the basis of a stochastic analysis model and the Monte Carlo (MC) method. Considering the uncertain thermal parameters of frozen soil as random variables, stochastic processes and random fields, the corresponding stochastic thermal regime of frozen soil around a single freezing pipe are obtained and analyzed. Taking the variability of each stochastic parameter into account individually, the influences of each stochastic thermal parameter on stochastic thermal regime are investigated. The results show that the mean temperatures of frozen soil around the single freezing pipe with three analogy method are the same while the standard deviations are different. The distributions of standard deviation have a great difference at different radial coordinate location and the larger standard deviations are mainly at the phase change area. The computed data with random variable method and stochastic process method have a great difference from the measured data while the computed data with random field method well agree with the measured data. Each uncertain thermal parameter has a different effect on the standard deviation of frozen soil temperature around the single freezing pipe. These results can provide a theoretical basis for the design and construction of AGF.

  5. Mitigation method of thermal transient stress by thermalhydraulic-structure total analysis

    International Nuclear Information System (INIS)

    Kasahara, Naoto; Jinbo, Masakazu; Hosogai, Hiromi

    2003-01-01

    This study proposes a rational evaluation and mitigation method of thermal transient loads in fast reactor components by utilizing relationships among plant system parameters and stresses induced by thermal transients of plants. A thermalhydraulic-structure total analysis procedure helps us to grasp relationship among system parameters and thermal stresses. Furthermore, it enables mitigation of thermal transient loads by adjusting system parameters. In order to overcome huge computations, a thermalhydraulic-structure total analysis code and the Design of Experiments methodology are utilized. The efficiency of the proposed mitigation method is validated through thermal stress evaluation of an intermediate heat exchanger in Japanese demonstration fast reactor. (author)

  6. Single Particulate SEM-EDX Analysis of Iron-Containing Coarse Particulate Matter in an Urban Environment: Sources and Distribution of Iron within Cleveland, Ohio

    Science.gov (United States)

    The physicochemical properties of coarse-mode, iron-containing particles, and their temporal and spatial distributions are poorly understood. Single particle analysis combining x-ray elemental mapping and computer-controlled scanning electron microscopy (CCSEM-EDX) of passively ...

  7. Thermal safety analysis of a dry storage cask for the Korean standard spent fuel - 16159

    International Nuclear Information System (INIS)

    Cha, Jeonghun; Kim, S.N.; Choi, K.W.

    2009-01-01

    A conceptual dry storage facility, which is based on a commercial dry storage facility, was designed for the Korea standard spent nuclear fuel (SNF) and preliminary thermal safety analysis was performed in this study. To perform the preliminary thermal analysis, a thermal analysis method was proposed. The thermal analysis method consists of 2 parts. By using the method, the surface temperature of the storage canister corresponding to the SNF clad temperature was calculated and the adequate air duct area was decided using the calculation result. The initial temperature of the facility was calculated and the fire condition and half air duct blockage were analyzed. (authors)

  8. Fluid-structure interaction analysis for pressurizer surge line subjected to thermal stratification

    International Nuclear Information System (INIS)

    Kang, Dong Gu; Jhung, Myung Jo; Chang, Soon Heung

    2011-01-01

    Research highlights: → Temperature of surge line due to stratified flow is defined using CFD analysis. → Fluid-structure interaction analysis is performed to investigate the response characteristics due to thermal stress. → Fatigue usage factors due to thermal stratification are relatively low. → Simplifying temperature distribution in surge line is not always conservative. - Abstract: Serious mechanical damages such as cracks and plastic deformations due to excessive thermal stress caused by thermal stratification have been experienced in several nuclear power plants. In particular, the thermal stratification in the pressurizer surge line has been addressed as one of the significant safety and technical issues. In this study, a detailed unsteady computational fluid dynamics (CFD) analysis involving conjugate heat transfer analysis is performed to obtain the transient temperature distributions in the wall of the pressurizer surge line subjected to stratified internal flows either during out-surge or in-surge operation. The thermal loads from CFD calculations are transferred to the structural analysis code which is employed for the thermal stress analysis to investigate the response characteristics, and the fatigue analysis is ultimately performed. In addition, the thermal stress and fatigue analysis results obtained by applying the realistic temperature distributions from CFD calculations are compared with those by assuming the simplified temperature distributions to identify some requirements for a realistic and conservative thermal stress analysis from a safety point of view.

  9. Transmutation technology development; thermal hydraulic power analysis and structure analysis of the HYPER target beam window

    Energy Technology Data Exchange (ETDEWEB)

    Choi, J. H.; Ju, E. S.; Song, M. K.; Jeon, Y. Z. [Gyeongsang National University, Jinju (Korea)

    2002-03-01

    A thermal hydraulic power analysis, a structure analysis and optimization computation for some design factor for the design of spallation target suitable for HYPER with 1000 MW thermal power in this study was performed. Heat generation formula was used which was evaluated recently based on the LAHET code, mainly to find the maximum beam current under given computation conditions. Thermal hydraulic power of HYPER target system was calculated using FLUENT code, structure conducted by inputting the data into ANSYS. On the temp of beam windows and the pressure distribution calculated using FLUENT. Data transformation program was composed apply the data calculated using FLUENT being commercial CFD code and ANSYS being FEM code for CFX structure analysis. A basic study was conducted on various singular target to obtain fundamental data on the shape for optimum target design. A thermal hydraulic power analysis and structure analysis were conducted on the shapes of parabolic, uniform, scanning beams to choose the optimum shape of beam current analysis was done according to some turbulent model to simulate the real flow. To evaluate the reliability of numerical analysis result, benchmarking of FLUENT code reformed at SNU and Korea Advanced Institute of Science and Technology and it was compared to CFX in the possession of Korea Atomic Energy Research Institute and evaluated. Reliable deviation was observed in the results calculated using FLUENT code, but temperature deviation of about 200 .deg. C was observed in the result from CFX analysis at optimum design condition. Several benchmarking were performed on the basis of numerical analysis concerning conventional HYPER. It was possible to allow a beam arrests of 17.3 mA in the case of the {phi} 350 mm parabolic beam suggested to the optimum in nuclear transmutation when stress equivalent to VON-MISES was calculated to be 140 MPa. 29 refs., 109 figs. (Author)

  10. Generic repository design concepts and thermal analysis (FY11)

    International Nuclear Information System (INIS)

    Howard, Robert; Dupont, Mark; Blink, James A.; Fratoni, Massimiliano; Greenberg, Harris; Carter, Joe; Hardin, Ernest L.; Sutton, Mark A.

    2011-01-01

    Reference concepts for geologic disposal of used nuclear fuel and high-level radioactive waste in the U.S. are developed, including geologic settings and engineered barriers. Repository thermal analysis is demonstrated for a range of waste types from projected future, advanced nuclear fuel cycles. The results show significant differences among geologic media considered (clay/shale, crystalline rock, salt), and also that waste package size and waste loading must be limited to meet targeted maximum temperature values. In this study, the UFD R and D Campaign has developed a set of reference geologic disposal concepts for a range of waste types that could potentially be generated in advanced nuclear FCs. A disposal concept consists of three components: waste inventory, geologic setting, and concept of operations. Mature repository concepts have been developed in other countries for disposal of spent LWR fuel and HLW from reprocessing UNF, and these serve as starting points for developing this set. Additional design details and EBS concepts will be considered as the reference disposal concepts evolve. The waste inventory considered in this study includes: (1) direct disposal of SNF from the LWR fleet, including Gen III+ advanced LWRs being developed through the Nuclear Power 2010 Program, operating in a once-through cycle; (2) waste generated from reprocessing of LWR UOX UNF to recover U and Pu, and subsequent direct disposal of used Pu-MOX fuel (also used in LWRs) in a modified-open cycle; and (3) waste generated by continuous recycling of metal fuel from fast reactors operating in a TRU burner configuration, with additional TRU material input supplied from reprocessing of LWR UOX fuel. The geologic setting provides the natural barriers, and establishes the boundary conditions for performance of engineered barriers. The composition and physical properties of the host medium dictate design and construction approaches, and determine hydrologic and thermal responses of

  11. Generic repository design concepts and thermal analysis (FY11).

    Energy Technology Data Exchange (ETDEWEB)

    Howard, Robert (Oak Ridge National Laboratory, Oak Ridge, TN); Dupont, Mark (Savannah River Nuclear Solutions, Aiken, SC); Blink, James A. (Lawrence Livermore National Laboratory, Livermore, CA); Fratoni, Massimiliano (Lawrence Livermore National Laboratory, Livermore, CA); Greenberg, Harris (Lawrence Livermore National Laboratory, Livermore, CA); Carter, Joe (Savannah River Nuclear Solutions, Aiken, SC); Hardin, Ernest L.; Sutton, Mark A. (Lawrence Livermore National Laboratory, Livermore, CA)

    2011-08-01

    Reference concepts for geologic disposal of used nuclear fuel and high-level radioactive waste in the U.S. are developed, including geologic settings and engineered barriers. Repository thermal analysis is demonstrated for a range of waste types from projected future, advanced nuclear fuel cycles. The results show significant differences among geologic media considered (clay/shale, crystalline rock, salt), and also that waste package size and waste loading must be limited to meet targeted maximum temperature values. In this study, the UFD R&D Campaign has developed a set of reference geologic disposal concepts for a range of waste types that could potentially be generated in advanced nuclear FCs. A disposal concept consists of three components: waste inventory, geologic setting, and concept of operations. Mature repository concepts have been developed in other countries for disposal of spent LWR fuel and HLW from reprocessing UNF, and these serve as starting points for developing this set. Additional design details and EBS concepts will be considered as the reference disposal concepts evolve. The waste inventory considered in this study includes: (1) direct disposal of SNF from the LWR fleet, including Gen III+ advanced LWRs being developed through the Nuclear Power 2010 Program, operating in a once-through cycle; (2) waste generated from reprocessing of LWR UOX UNF to recover U and Pu, and subsequent direct disposal of used Pu-MOX fuel (also used in LWRs) in a modified-open cycle; and (3) waste generated by continuous recycling of metal fuel from fast reactors operating in a TRU burner configuration, with additional TRU material input supplied from reprocessing of LWR UOX fuel. The geologic setting provides the natural barriers, and establishes the boundary conditions for performance of engineered barriers. The composition and physical properties of the host medium dictate design and construction approaches, and determine hydrologic and thermal responses of the

  12. Thermal behavior analysis of U-Mo/Al dispersion fuel

    Energy Technology Data Exchange (ETDEWEB)

    Ryu, Ho Jin; Park, Jong Mang; Lee, Yoon Sang; Kim, Chang Kyu [Korea Atomic Energy Research Institute, Taejon (Korea, Republic of)

    2004-07-01

    According to the non-proliferation policy under the reduced enrichment for research and test reactors (RERTR) program, low enriched uranium(LEU) fuel such as uranium silicide dispersion fuels are being used in research reactors. Because of a lower enrichment higher uranium density fuels are required for some high performance research reactors. Some uranium alloys with a high uranium density such as U-Mo alloys have been considered as one of the most promising candidates for a dispersion fuel due to the good irradiation performance. An international qualification program to replace the uranium silicide dispersion fuel with U-Mo dispersion fuel is being carried out under the RERTR program. Although U-Mo powders are conventionally supplied by the mechanical comminuting of as-cast U-Mo alloys, KAERI developed a centrifugal atomization method in order to simplify the preparation process and improve the properties. The centrifugally atomized powders have a rapidly solidified gamma uranium structure and a spherical shape. During the in-reactor operation of a dispersion fuel, interdiffusion or chemical reactions between the fuel particles and the matrix occurr. Intermetallic compounds in the form of UAlx are formed as a result of the diffusional reaction. Because the intermetallic compounds are less dense than the combined reactants, the volume of the fuel element increases after the reaction. In addition to the effect on the swelling performance, the reaction layers between the U-Mo and the Al matrix induces a degradation of the thermal properties of the U-Mo/Al dispersion fuels. It is important to investigate the thermal behavior of U-Mo/Al dispersion fuel according to reaction between the fuel particles and the matrix with the burnup and linear power. In this study, a finite element analysis was used for the calculation of the temperature distribution of the U-Mo/Al dispersion fuel with a burnup and linear power. Kinetics data of the reaction layers such as the growth

  13. Thermal behavior analysis of U-Mo/Al dispersion fuel

    International Nuclear Information System (INIS)

    Ryu, Ho Jin; Park, Jong Mang; Lee, Yoon Sang; Kim, Chang Kyu

    2004-01-01

    According to the non-proliferation policy under the reduced enrichment for research and test reactors (RERTR) program, low enriched uranium(LEU) fuel such as uranium silicide dispersion fuels are being used in research reactors. Because of a lower enrichment higher uranium density fuels are required for some high performance research reactors. Some uranium alloys with a high uranium density such as U-Mo alloys have been considered as one of the most promising candidates for a dispersion fuel due to the good irradiation performance. An international qualification program to replace the uranium silicide dispersion fuel with U-Mo dispersion fuel is being carried out under the RERTR program. Although U-Mo powders are conventionally supplied by the mechanical comminuting of as-cast U-Mo alloys, KAERI developed a centrifugal atomization method in order to simplify the preparation process and improve the properties. The centrifugally atomized powders have a rapidly solidified gamma uranium structure and a spherical shape. During the in-reactor operation of a dispersion fuel, interdiffusion or chemical reactions between the fuel particles and the matrix occurr. Intermetallic compounds in the form of UAlx are formed as a result of the diffusional reaction. Because the intermetallic compounds are less dense than the combined reactants, the volume of the fuel element increases after the reaction. In addition to the effect on the swelling performance, the reaction layers between the U-Mo and the Al matrix induces a degradation of the thermal properties of the U-Mo/Al dispersion fuels. It is important to investigate the thermal behavior of U-Mo/Al dispersion fuel according to reaction between the fuel particles and the matrix with the burnup and linear power. In this study, a finite element analysis was used for the calculation of the temperature distribution of the U-Mo/Al dispersion fuel with a burnup and linear power. Kinetics data of the reaction layers such as the growth

  14. Thermal properties of graphite oxide, thermally reduced graphene and chemically reduced graphene

    Science.gov (United States)

    Jankovský, Ondřej; Sedmidubský, David; Lojka, Michal; Sofer, Zdeněk

    2017-07-01

    We compared thermal behavior and other properties of graphite oxide, thermally reduced graphene and chemically reduced graphene. Graphite was oxidized according to the Hofmann method using potassium chlorate as oxidizing agent in strongly acidic environment. In the next step, the formed graphite oxide was chemically or thermally reduced yielding graphene. The mechanism of thermal reduction was studied using STA-MS. Graphite oxide and both thermally and chemically reduced graphenes were analysed by SEM, EDS, elemental combustion analysis, XPS, Raman spectroscopy, XRD and BET. These findings will help for the large scale production of graphene with appropriate chemical composition.

  15. Revised Thermal Analysis of LANL Ion Exchange Column

    Energy Technology Data Exchange (ETDEWEB)

    Laurinat, J

    2006-04-11

    This document updates a previous calculation of the temperature distributions in a Los Alamos National Laboratory (LANL) ion exchange column.1 LANL operates two laboratory-scale anion exchange columns, in series, to extract Pu-238 from nitric acid solutions. The Defense Nuclear Facilities Safety Board has requested an updated analysis to calculate maximum temperatures for higher resin loading capacities obtained with a new formulation of the Reillex HPQ anion exchange resin. The increased resin loading capacity will not exceed 118 g plutonium per L of resin bed. Calculations were requested for normal operation of the resin bed at the minimum allowable solution feed rate of 30 mL/min and after an interruption of flow at the end of the feed stage, when one of the columns is fully loaded. The object of the analysis is to demonstrate that the decay heat from the Pu-238 will not cause resin bed temperatures to increase to a level where the resin significantly degrades. At low temperatures, resin bed temperatures increase primarily due to decay heat. At {approx}70 C a Low Temperature Exotherm (LTE) resulting from the reaction between 8-12 M HNO{sub 3} and the resin has been observed. The LTE has been attributed to an irreversible oxidation of pendant ethyl benzene groups at the termini of the resin polymer chains by nitric acid. The ethyl benzene groups are converted to benzoic acid moities. The resin can be treated to permanently remove the LTE by heating a resin suspension in 8M HNO{sub 3} for 30-45 minutes. No degradation of the resin performance is observed after the LTE removal treatment. In fact, heating the resin in boiling ({approx}115-120 C) 12 M HNO{sub 3} for 3 hr displays thermal stability analogous to resin that has been treated to remove the LTE. The analysis is based on a previous study of the SRS Frames Waste Recovery (FWR) column, performed in support of the Pu-238 production campaign for NASA's Cassini mission. In that study, temperature transients

  16. Water Outgassing from PBX-9502 powder by isoconversional thermal analysis

    International Nuclear Information System (INIS)

    Dinh, L.N.; Glascoe, E.L.; Small, W.

    2009-01-01

    Temperature programmed desorption/decomposition (TPD) were performed on PBX-9502 after 3 hours of vacuum pump. TPD data were analyzed by the technique of isoconversional analysis to obtain outgassing kinetics and moisture content of PBX-9502 powder as well as to construct water outgassing models for PBX-9502 powder as a function of time and temperature. Following 3 hours of vacuum pump, dry storage of PBX-9502 at 300K, quickly gives rise to 180-330 ppm moisture in the first few years. Thereafter, the moisture outgassing continues at a much slower rate, totaling only to ∼ 210-380 ppm after 100 years of storage. In an effort to understand the nature of the moisture outgassing in PBX-9502, we have measured moisture content and outgassing kinetics in PBX-9502 by the experimental technique of TPD and the isoconversional thermal analysis. The results of these measurements were then used to construct moisture outgassing models for PBX-9502 in a dry environment (following 3 hours of vacuum pump)

  17. Thermal buckling comparative analysis using Different FE (Finite Element) tools

    Energy Technology Data Exchange (ETDEWEB)

    Banasiak, Waldemar; Labouriau, Pedro [INTECSEA do Brasil, Rio de Janeiro, RJ (Brazil); Burnett, Christopher [INTECSEA UK, Surrey (United Kingdom); Falepin, Hendrik [Fugro Engineers SA/NV, Brussels (Belgium)

    2009-12-19

    High operational temperature and pressure in offshore pipelines may lead to unexpected lateral movements, sometimes call lateral buckling, which can have serious consequences for the integrity of the pipeline. The phenomenon of lateral buckling in offshore pipelines needs to be analysed in the design phase using FEM. The analysis should take into account many parameters, including operational temperature and pressure, fluid characteristic, seabed profile, soil parameters, coatings of the pipe, free spans etc. The buckling initiation force is sensitive to small changes of any initial geometric out-of-straightness, thus the modeling of the as-laid state of the pipeline is an important part of the design process. Recently some dedicated finite elements programs have been created making modeling of the offshore environment more convenient that has been the case with the use of general purpose finite element software. The present paper aims to compare thermal buckling analysis of sub sea pipeline performed using different finite elements tools, i.e. general purpose programs (ANSYS, ABAQUS) and dedicated software (SAGE Profile 3D) for a single pipeline resting on an the seabed. The analyses considered the pipeline resting on a flat seabed with a small levels of out-of straightness initiating the lateral buckling. The results show the quite good agreement of results of buckling in elastic range and in the conclusions next comparative analyses with sensitivity cases are recommended. (author)

  18. Nuclear reactor thermal hydraulics safety analysis and thoughts on FUKUSHIMA

    International Nuclear Information System (INIS)

    Ninokata, Hisashi

    2012-01-01

    The first part of this article is to show my thoughts on the accident at Fukushima Daiichi Nuclear Power Station. It is cited from a summary of my lecture talk in Indonesia, in the beginning of the last December, 2011. This talk was based on my previous lecture and seminar talks including those delivered at MIT, June 16, at the ANS Annual Meeting in Hollywood, Florida, June 28 at NURETH-13 in Toronto, September 27, and others. The content is based on the open and latest information available to date in Japan. It may contain some erroneous or uncertain information. I tried to minimize it to my best capability. Also I tried to eliminate any critical issues or opinions that may jeopardize some people who were involved in. The latter half of this article will be excerpts of my recent R and D activities related to the safety-by-design for sodium cooled fast reactors and light water reactors, thermal hydraulics analysis focusing on the simulation-based technology, in particular subchannel analysis and computational fluid dynamics. (J.P.N.)

  19. Simultaneous Thermal Analysis of Remediated Nitrate Salt Surrogates

    Energy Technology Data Exchange (ETDEWEB)

    Wayne, David Matthew [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-05-13

    The actinide engineering and science group (MET-1) have completed simultaneous thermal analysis and offgas analysis by mass spectrometry (STA-MS) of remediated nitrate salt (RNS) surrogates formulated by the high explosives science and technology group (M-7). The 1.0 to 1.5g surrogate samples were first analyzed as received, then a new set was analyzed with 100-200mL 10M HNO3 +0.3 MHF added, and a third set was analyzed after 200 mL of a concentrated Pu-AM spike (in 10M HNO3 +0.3 MHF) was added. The acid and spike solutions were formulated by the actinide analytical chemistry group (C-AAC) using reagent-grade HNO3 and HF, which was also used to dissolve a small quantity of mixed, high-fired PuO2/ AmO2 oxide.

  20. Design Considerations, Modeling and Analysis for the Multispectral Thermal Imager

    International Nuclear Information System (INIS)

    Borel, C.C.; Clodius, W.B.; Cooke, B.J.; Smith, B.W.; Weber, P.G.

    1999-01-01

    The design of remote sensing systems is driven by the need to provide cost-effective, substantive answers to questions posed by our customers. This is especially important for space-based systems, which tend to be expensive, and which generally cannot be changed after they are launched. We report here on the approach we employed in developing the desired attributes of a satellite mission, namely the Multispectral Thermal Imager. After an initial scoping study, we applied a procedure which we call: ''End-to-end modeling and analysis (EEM).'' We began with target attributes, translated to observable signatures and then propagated the signatures through the atmosphere to the sensor location. We modeled the sensor attributes to yield a simulated data stream, which was then analyzed to retrieve information about the original target. The retrieved signature was then compared to the original to obtain a figure of merit: hence the term ''end-to-end modeling and analysis.'' We base the EEM in physics to ensure high fidelity and to permit scaling. As the actual design of the payload evolves, and as real hardware is tested, we can update the EEM to facilitate trade studies, and to judge, for example, whether components that deviate from specifications are acceptable

  1. Multicriteria analysis of thermal and energy systems for tourist facilities

    International Nuclear Information System (INIS)

    Raguzin, I.

    1999-01-01

    The introductory part of the paper briefly presents the technological, economic and environmental optimisation procedure of thermal and energy systems for tourist facilities with the multicriteria ranging method when choosing an optimum solution. The procedure described includes a systematic analysis of the system's structure, energy-mass balance, balance of costs, environmental impact analysis and the choice of an optimum solution. Special attention was paid to criteria quantification for the choice of solution and the most appropriate ranging method.The procedure's application has been illustrated on an example of a potential tourist facility on the Island of Loinj, i.e. the locality with a potential highest category tourist development. This example includes (a) consumers (heating of rooms, preparation of hot water, heating of swimming pool water and cooling of rooms), and (b) producers (boiler room, cooling engine-rooms, a cogeneration plant and heat pumps). The data have been supplied from the project documentation for the reconstruction of the existing facilities mainly preliminary designs. The multicriteria ranging was conducted based on an appropriate computer programme for problem solution. (author)

  2. The effect of different growth media, carbon source and pgrs on dendrobium broga giant orchid's protocorm-like bodies (plbs) proliferation supported with sem and tem analysis

    International Nuclear Information System (INIS)

    Uddain, J.; Gnasekaran, P.; Zakaria, L.

    2015-01-01

    Dendrobium Broga Giant (Dendrobium Bobby Messina * Dendrobium Superbiens) is a new orchid hybrid in Malaysia. The aim of this study was to investigate the effect of different growth media, carbon sources and PGRs on Dendrobium Broga Giant orchid's protocorm-like bodies (PLBs) proliferation supported with SEM and TEM analysis. The PLBs were cultured on different strength of semi-solid and liquid MS medium and the proliferation rate was recorded based on the fresh weight basis. The maximum PLBs proliferation (12.31% 0.57) was obtained in MS semi-solid medium. PLBs were cultured on MS semi-solid media supplemented with different sucrose concentrations (0, 10, 20, 30 and 40 g L-1). The highest proliferation rate of PLBs (15.48% 1.20) was recorded from MS supplemented with 20 g L-1 sucrose. Different concentrations of BAP (0, 0.5, 1.0, 2.0 mg.L-1) and NAA (0, 0.5, 1.0, 2.0 mgL-1) were added to MS semi-solid medium. Combinations of 1.0 mg L-1 BAP and 0.5 mg.L-1 NAA produced higher PLBs proliferation. Micromorphological studies by SEM and TEM displayed trichome, leaf primordial, stomata, various sizes of mitochondria, vacuoles, different shapes of chloroplast were found in PLBs which ameliorated the slow proliferation nature of plantlets. (author)

  3. Analysis of the sensitivity and sample-furnace thermal-lag of a differential thermal analyzer

    International Nuclear Information System (INIS)

    Roura, P.; Farjas, J.

    2005-01-01

    The heat exchange between the horizontal furnace of a differential thermal analyzer (DTA) and the sample is analyzed with the aim of understanding the parameters governing the thermal signal. The resistance due to radiation and conduction through the gas has been calculated and compared to the experimental values of the thermal-lag between the sample and furnace and apparatus sensitivity. The overall evolution of these parameters with the temperature and their relative values are well understood by considering the temperature differences that arise between the sample and holder. Two RC thermal models are used for describing the apparatus performance at different temperature ranges. Finally, the possibility of improving the signal quality through the control of the leak resistances is stressed

  4. Geographic analysis of thermal equilibria: A bioenergetic model for predicting thermal response of aquatic insect communities

    International Nuclear Information System (INIS)

    Sweeney, B.W.; Newbold, J.D.; Vannote, R.L.

    1991-12-01

    The thermal regime immediately downstream from bottom release reservoirs is often characterized by reduced diel and seasonal (winter warm/summer cool) conditions. These unusual thermal patterns have often been implicated as a primary factor underlying observed downstream changes in the species composition of aquatic macroinvertebrate communities. The potential mechanisms for selective elimination of benthic species by unusual thermal regimes has been reviewed. Although the effects of temperature on the rate and magnitude of larval growth and development has been included in the list of potential mechanisms, only recently have field studies below dams focused on this interrelationship. This study investigates the overall community structure as well as the seasonal pattern of larval growth and development for several univoltine species of insects in the Delaware River below or near the hypolimnetic discharge of the Cannonsville and Pepeacton dams. These dams, which are located on the West and East branches of the Delaware River, respectively, produce a thermal gradient extending about 70 km downstream

  5. Thermal behaviour of layered double hydroxides studied by emanation thermal analysis

    Czech Academy of Sciences Publication Activity Database

    Dorničák, V.; Balek, V.; Kovanda, F.; Večerníková, Eva

    90-91, - (2003), s. 475-480 ISSN 1012-0394 Institutional research plan: CEZ:AV0Z4032918 Keywords : hydrotalcite * layered double hydroxides * thermal decomposition Subject RIV: CA - Inorganic Chemistry Impact factor: 0.687, year: 2003

  6. Thermal Analysis of Cryocooler-Cooled Bi2223 Pulsed Coil

    International Nuclear Information System (INIS)

    Miyazaki, H; Chigusa, S; Tanaka, I; Iwakuma, M; Funaki, K; Hayashi, H; Tomioka, A

    2006-01-01

    We fabricated a cryocooler-cooled Bi2223 superconducting pulsed coil and experimentally studied thermal runaway in dc or ac operation. We carried out numerical simulation of thermal properties of the coil in order to explain thermal runaway of the coil. Firstly, we analyzed the total heat generation of flux-flow loss and ac loss inside the winding from the experimental results of the external field losses and the E-J characteristics for the Bi2223 strands. Secondly, we numerically simulated the thermal properties by using 2- dimensional heat conduction equation with axial symmetry. The numerical simulation shows the relation between the initiation of thermal runaway and the temperature distribution with highly concentrated heat source in the winding. We have a semi-quantitative agreement between the numerical results and the experimental ones for the condition of the thermal runaway

  7. Thermal Failure Analysis of Fiber-Reinforced Silica Aerogels under Liquid Nitrogen Thermal Shock

    Directory of Open Access Journals (Sweden)

    Ai Du

    2018-06-01

    Full Text Available Aerogel materials are recognized as promising candidates for the thermal insulator and have achieved great successes for the aerospace applications. However, the harsh environment on the exoplanet, especially for the tremendous temperature difference, tends to affect the tenuous skeleton and performances of the aerogels. In this paper, an evaluation method was proposed to simulate the environment of exoplanet and study the influence on the fiber-reinforced silica aerogels with different supercritical point drying (SPD technology. Thermal conductivity, mechanical property and the microstructure were characterized for understanding the thermal failure mechanism. It was found that structure and thermal property were significantly influenced by the adsorbed water in the aerogels under the thermal shocks. The thermal conductivity of CO2-SPD aerogel increased 35.5% after the first shock and kept in a high value, while that of the ethanol-SPD aerogel increased only 19.5% and kept in a relatively low value. Pore size distribution results showed that after the first shock the peak pore size of the CO2-SPD aerogel increased from 18 nm to 25 nm due to the shrinkage of the skeleton, while the peak pore size of the ethanol-SPD aerogel kept at ~9 nm probably induced by the spring-back effect. An 80 °C treatment under vacuum was demonstrated to be an effective way for retaining the good performance of ethanol-SPD aerogels under the thermal shock. The thermal conductivity increases of the ethanol-SPD aerogels after 5 shocks decreased from ~30 to ~0% via vacuum drying, while the increase of the CO2-SPD aerogels via the same treatments remains ~28%. The high-strain hardening and low-strain soften behaviors further demonstrated the skeleton shrinkage of the CO2-SPD aerogel.

  8. Gas Analysis and Control Methods for Thermal Batteries

    Science.gov (United States)

    2013-09-01

    when using highly efficient microporous thermal insulation packages. An easily implemented method of H2 gas removal from vendor thermal batteries is... microporous thermal insulation packages (1, 4, 5) or reduce volume requirements significantly. More rigorous gas control methods combined with...measured from the DCM pressures and known internal volumes of the 3 GHS that were measured using the ideal gas law with a 10-cc internal volume SS

  9. Distribution analysis of thermal effusivity for sub-micrometer YBCO thin films using thermal microscope

    International Nuclear Information System (INIS)

    Yagi, T.; Taketoshi, N.; Kato, H.

    2004-01-01

    Thermal effusivity measurements have been carried out for sub-micrometer YBCO superconducting films using thermal microscope based upon thermoreflectance technique. Two samples were prepared: c-axis aligned YBCO thin films with 800 nm in thickness synthesized on MgO and SrTiO 3 substrates. Measured thermal effusivities perpendicular to the surface, i.e. in parallel with c-axis were determined to be 1770 J/m 2 s 0.5 K on MgO substrate and 1420 J/m 2 s 0.5 K for that on SrTiO 3 substrate, respectively. The scatter of the measurements is estimated to be lower than ±5.2%. These values are consistent with reported values of YBCO single crystal in the direction of c-axis. In addition, 2D profiling image, that is, in-plane distribution of thermal effusivity was well obtained for the YBCO film on MgO substrate by operating this thermal microscope in a scanning mode. Its standard deviation of the in-plane thermal effusivity scattering due to the non-uniformity is evaluated to be ±5.7%

  10. Thermal stress ratcheting analysis of a time-hardening structure

    International Nuclear Information System (INIS)

    Hada, Kazuhiko

    1999-01-01

    Thermal stress ratcheting and shakedown is analyzed for a time-hardening structure: the yield stress increases as time goes on under exposure to neutron irradiation or thermal aging. New three modes of ratcheting and shakedown are identified as transition to other deformation modes. Stress regimes and thermal ratchet strains are formulated as a function of time-increasing yield stress. Moreover, a new model of trouble occurrence frequency as a modification to a bath-tube curve is proposed for calculating a time period of a thermal cycle. Application of the proposed formulation tells us a benefit of taking into account the time hardening due to neutron irradiation. (author)

  11. Sexual Arousal and Sexually Explicit Media (SEM)

    DEFF Research Database (Denmark)

    Hald, Gert Martin; Stulhofer, Aleksandar; Lange, Theis

    2018-01-01

    -mainstream and mainstream SEM groups, and (iii) to explore the validity and predictive accuracy of the Non-Mainstream Pornography Arousal Scale (NPAS). METHODS: Online cross-sectional survey of 2,035 regular SEM users in Croatia. MAIN OUTCOMES MEASURES: Patterns of sexual arousal to 27 different SEM themes, sexual...

  12. The Phebus FP thermal-hydraulic analysis with Melcor

    International Nuclear Information System (INIS)

    Akgane, Kikuo; Kiso, Yoshihiro; Fukahori, Takanori; Yoshino, Mamoru

    1995-01-01

    The severe accident analysis code MELCOR, version 1.8.2, has been applied for thermal-hydraulic pre-test analysis of the first test of the Phebus FP program (test FPT-0) to study the best test parameters and the applicability of the code. The Phebus FP program is an in-pile test program which has been planned by the French Commissariate a L'Energie Atomique and the Commission of the European Union. The experiments are being conducted by an international collaboration to study the release and transport of fission products (FPs) under conditions assumed to be the most representative of those that would occur in a severe accident. The Phebus FP test apparatus simulates a test bundle of an in-pile section, the circuit including the steam generator U-tubes and the containment. The FPT-0 test was designed to simulate the heat-up and subsequent fuel bundle degradation after a loss of coolant severe accident, using fresh fuel. Two options for fuel degradation models in MELCOR have been applied to fuel degradation behavior. the first model assumes that fuel debris will be formed immediately after the fuel support fails by cladding relocation due to the candling process. The other is the uncollapsed bare fuel pellets option, in which the fuel pellets remain standing in a columnar shape until the fuel reaches its melting point, even if the cladding has been relocated by candling. The thermal-hydraulic behaviors in the circuit and containment of Phebus FP are discussed herein. Flow velocities in the Phebus FP circuit are high in order to produce turbulent flow in a small diameter test pipe. The MELCOR calculation has shown that the length of the hot leg and steam generator are adequate to attain steam temperatures or 700 degrees C and 150 degrees C in the respective outlets. The containment atmosphere temperature and humidity derived by once through integral system calculation show that objective test conditions would be satisfied in the Phebus FP experiment

  13. The Phebus FP thermal-hydraulic analysis with Melcor

    Energy Technology Data Exchange (ETDEWEB)

    Akgane, Kikuo; Kiso, Yoshihiro [Nuclear Power Engineering Corporation, Tokyo (Japan); Fukahori, Takanori [Hitachi Engineering Company, Ltd., Hitachi-shi Ibaraki-ken (Japan); Yoshino, Mamoru [Nuclear Engineering Ltd., Tosabori Nishi-ku (Japan)

    1995-09-01

    The severe accident analysis code MELCOR, version 1.8.2, has been applied for thermal-hydraulic pre-test analysis of the first test of the Phebus FP program (test FPT-0) to study the best test parameters and the applicability of the code. The Phebus FP program is an in-pile test program which has been planned by the French Commissariate a L`Energie Atomique and the Commission of the European Union. The experiments are being conducted by an international collaboration to study the release and transport of fission products (FPs) under conditions assumed to be the most representative of those that would occur in a severe accident. The Phebus FP test apparatus simulates a test bundle of an in-pile section, the circuit including the steam generator U-tubes and the containment. The FPT-0 test was designed to simulate the heat-up and subsequent fuel bundle degradation after a loss of coolant severe accident, using fresh fuel. Two options for fuel degradation models in MELCOR have been applied to fuel degradation behavior. the first model assumes that fuel debris will be formed immediately after the fuel support fails by cladding relocation due to the candling process. The other is the uncollapsed bare fuel pellets option, in which the fuel pellets remain standing in a columnar shape until the fuel reaches its melting point, even if the cladding has been relocated by candling. The thermal-hydraulic behaviors in the circuit and containment of Phebus FP are discussed herein. Flow velocities in the Phebus FP circuit are high in order to produce turbulent flow in a small diameter test pipe. The MELCOR calculation has shown that the length of the hot leg and steam generator are adequate to attain steam temperatures or 700{degrees}C and 150{degrees}C in the respective outlets. The containment atmosphere temperature and humidity derived by once through integral system calculation show that objective test conditions would be satisfied in the Phebus FP experiment.

  14. Detection of land mines using fast and thermal neutron analysis

    International Nuclear Information System (INIS)

    Bach, P.

    1998-01-01

    The detection of land mines is made possible by using nuclear sensor based on neutron interrogation. Neutron interrogation allows to detect the sensitive elements (C, H, O, N) of the explosives in land mines or in unexploded shells: the evaluation of characteristic ratio N/O and C/O in a volume element gives a signature of high explosives. Fast neutron interrogation has been qualified in our laboratories as a powerful close distance method for identifying the presence of a mine or explosive. This method could be implemented together with a multisensor detection system - for instance IR or microwave - to reduce the false alarm rate by addressing the suspected area. Principle of operation is based on the measurement of gamma rays induced by neutron interaction with irradiated nuclei from the soil and from a possible mine. Specific energy of these gamma rays allows to recognise the elements at the origin of neutron interaction. Several detection methods can be used, depending on nuclei to be identified. Analysis of physical data, computations by simulation codes, and experimentations performed in our laboratory have shown the interest of Fast Neutron Analysis (FNA) combined with Thermal Neutron Analysis (TNA) techniques, especially for detection of nitrogen 14 N, carbon 12 C and oxygen 16 O. The FNA technique can be implemented using a 14 MeV sealed neutron tube, and a set of detectors. The mines detection has been demonstrated from our investigations, using a low power neutron generator working in the 10 8 n/s range, which is reasonable when considering safety rules. A fieldable demonstrator would be made with a detection head including tube and detectors, and with remote electronics, power supplies and computer installed in a vehicle. (author)

  15. Study of Selected Composites Copper Concentrate-Plastic Waste Using Thermal Analysis

    Science.gov (United States)

    Szyszka, Danuta

    2017-12-01

    The paper presents thermal analysis of selected composites (copper concentrate, plastic waste) in two stages. The first stage consisted in thermogravimetric analysis and differential thermal analysis on the applied plastic waste and copper concentrate, and subsequently, a comparative study has been carried out on products obtained, constituting composites of those materials. As a result of analyses, it was found that up to ca. 400 °C composites show high thermal stability, whereas above that temperature, a thermal decomposition of the composite occurs, resulting in emissions of organic compounds, i.e. hydrocarbon compounds and organic oxygenate derivatives.

  16. The Modeling and Simulation of Thermal Analysis at Hydro Generator Stator Winding Insulation

    Directory of Open Access Journals (Sweden)

    Mihaela Raduca

    2006-10-01

    Full Text Available This paper presents the modelling and simulation of thermal analysis at hydro generator stator winding. The winding stator is supplied at high voltage of 11 kV for high power hydro generator. To present the thermal analysis for stator winding is presented at supply of coil by 11 kV, when coil is heat and thermal transfer in insulation at ambient temperature.

  17. Thermal Analysis of Cold Vacuum Drying (CVD) of Spent Nuclear Fuel (SNF)

    International Nuclear Information System (INIS)

    PIEPHO, M.G.

    2000-01-01

    The thermal analysis examined transient thermal and chemical behavior of the Multi-Canister Overpack (MCO) container for a broad range of cases that represent the Cold Vacuum Drying (CVD) processes. The cases were defined to consider both normal and off-normal operations at the CVD Facility for an MCO with N Reactor spent fuel. This analysis provides the basis for the MCO thermal behavior at the CVD Facility in support of the safety basis documentation

  18. Automated CD-SEM metrology for efficient TD and HVM

    Science.gov (United States)

    Starikov, Alexander; Mulapudi, Satya P.

    2008-03-01

    CD-SEM is the metrology tool of choice for patterning process development and production process control. We can make these applications more efficient by extracting more information from each CD-SEM image. This enables direct monitors of key process parameters, such as lithography dose and focus, or predicting the outcome of processing, such as etched dimensions or electrical parameters. Automating CD-SEM recipes at the early stages of process development can accelerate technology characterization, segmentation of variance and process improvements. This leverages the engineering effort, reduces development costs and helps to manage the risks inherent in new technology. Automating CD-SEM for manufacturing enables efficient operations. Novel SEM Alarm Time Indicator (SATI) makes this task manageable. SATI pulls together data mining, trend charting of the key recipe and Operations (OPS) indicators, Pareto of OPS losses and inputs for root cause analysis. This approach proved natural to our FAB personnel. After minimal initial training, we applied new methods in 65nm FLASH manufacture. This resulted in significant lasting improvements of CD-SEM recipe robustness, portability and automation, increased CD-SEM capacity and MT productivity.

  19. Transient thermal analysis of flux switching PM machines

    NARCIS (Netherlands)

    Ilhan, E.; Kremers, M.F.J.; Motoasca, T.E.; Paulides, J.J.H.; Lomonova, E.

    2013-01-01

    Flux switching permanent magnet (FSPM) machines bring together the merits of switched reluctance and PM synchronous motors. FSPM employs armature windings and PMs together in the stator region, therefore the proximity of the windings PMs makes a thermal model mandatory. In literature, thermal

  20. Thermal analysis and two-directional air flow thermal management for lithium-ion battery pack

    Science.gov (United States)

    Yu, Kuahai; Yang, Xi; Cheng, Yongzhou; Li, Changhao

    2014-12-01

    Thermal management is a routine but crucial strategy to ensure thermal stability and long-term durability of the lithium-ion batteries. An air-flow-integrated thermal management system is designed in the present study to dissipate heat generation and uniformize the distribution of temperature in the lithium-ion batteries. The system contains of two types of air ducts with independent intake channels and fans. One is to cool the batteries through the regular channel, and the other minimizes the heat accumulations in the middle pack of batteries through jet cooling. A three-dimensional anisotropic heat transfer model is developed to describe the thermal behavior of the lithium-ion batteries with the integration of heat generation theory, and validated through both simulations and experiments. Moreover, the simulations and experiments show that the maximum temperature can be decreased to 33.1 °C through the new thermal management system in comparison with 42.3 °C through the traditional ones, and temperature uniformity of the lithium-ion battery packs is enhanced, significantly.

  1. Analysis of thermal fatigue events in light water reactors

    Energy Technology Data Exchange (ETDEWEB)

    Okuda, Yasunori [Institute of Nuclear Safety System Inc., Seika, Kyoto (Japan)

    2000-09-01

    Thermal fatigue events, which may cause shutdown of nuclear power stations by wall-through-crack of pipes of RCRB (Reactor Coolant Pressure Boundary), are reported by licensees in foreign countries as well as in Japan. In this paper, thermal fatigue events reported in anomalies reports of light water reactors inside and outside of Japan are investigated. As a result, it is clarified that the thermal fatigue events can be classified in seven patterns by their characteristics, and the trend of the occurrence of the events in PWRs (Pressurized Water Reactors) has stronger co-relation to operation hours than that in BWRs (Boiling Water Reactors). Also, it is concluded that precise identification of locations where thermal fatigue occurs and its monitoring are important to prevent the thermal fatigue events by aging or miss modification. (author)

  2. Thermal hydraulics analysis of the Advanced High Temperature Reactor

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Dean, E-mail: Dean_Wang@uml.edu [University of Massachusetts Lowell, One University Avenue, Lowell, MA 01854 (United States); Yoder, Graydon L.; Pointer, David W.; Holcomb, David E. [Oak Ridge National Laboratory, 1 Bethel Valley RD #6167, Oak Ridge, TN 37831 (United States)

    2015-12-01

    Highlights: • The TRACE AHTR model was developed and used to define and size the DRACS and the PHX. • A LOFF transient was simulated to evaluate the reactor performance during the transient. • Some recommendations for modifying FHR reactor system component designs are discussed. - Abstract: The Advanced High Temperature Reactor (AHTR) is a liquid salt-cooled nuclear reactor design concept, featuring low-pressure molten fluoride salt coolant, a carbon composite fuel form with embedded coated particle fuel, passively triggered negative reactivity insertion mechanisms, and fully passive decay heat rejection. This paper describes an AHTR system model developed using the Nuclear Regulatory Commission (NRC) thermal hydraulic transient code TRAC/RELAP Advanced Computational Engine (TRACE). The TRACE model includes all of the primary components: the core, downcomer, hot legs, cold legs, pumps, direct reactor auxiliary cooling system (DRACS), the primary heat exchangers (PHXs), etc. The TRACE model was used to help define and size systems such as the DRACS and the PHX. A loss of flow transient was also simulated to evaluate the performance of the reactor during an anticipated transient event. Some initial recommendations for modifying system component designs are also discussed. The TRACE model will be used as the basis for developing more detailed designs and ultimately will be used to perform transient safety analysis for the reactor.

  3. Ocean Thermal Energy Conversion (OTEC) Programmatic Environmental Analysis--Appendices

    Energy Technology Data Exchange (ETDEWEB)

    Authors, Various

    1980-01-01

    The programmatic environmental analysis is an initial assessment of Ocean Thermal Energy Conversion (OTEC) technology considering development, demonstration and commercialization. It is concluded that the OTEC development program should continue because the development, demonstration, and commercialization on a single-plant deployment basis should not present significant environmental impacts. However, several areas within the OTEC program require further investigation in order to assess the potential for environmental impacts from OTEC operation, particularly in large-scale deployments and in defining alternatives to closed-cycle biofouling control: (1) Larger-scale deployments of OTEC clusters or parks require further investigations in order to assess optimal platform siting distances necessary to minimize adverse environmental impacts. (2) The deployment and operation of the preoperational platform (OTEC-1) and future demonstration platforms must be carefully monitored to refine environmental assessment predictions, and to provide design modifications which may mitigate or reduce environmental impacts for larger-scale operations. These platforms will provide a valuable opportunity to fully evaluate the intake and discharge configurations, biofouling control methods, and both short-term and long-term environmental effects associated with platform operations. (3) Successful development of OTEC technology to use the maximal resource capabilities and to minimize environmental effects will require a concerted environmental management program, encompassing many different disciplines and environmental specialties. This volume contains these appendices: Appendix A -- Deployment Scenario; Appendix B -- OTEC Regional Characterization; and Appendix C -- Impact and Related Calculations.

  4. Intelligent trend analysis for a solar thermal energy collector field

    Science.gov (United States)

    Juuso, E. K.

    2018-03-01

    Solar thermal power plants collect available solar energy in a usable form at a temperature range which is adapted to the irradiation levels and seasonal variations. Solar energy can be collected only when the irradiation is high enough to produce the required temperatures. During the operation, a trade-off of the temperature and the flow is needed to achieve a good level for the collected power. The scaling approach brings temporal analysis to all measurements and features: trend indices are calculated by comparing the averages in the long and short time windows, a weighted sum of the trend index and its derivative detects the trend episodes and severity of the trend is estimated by including also the variable level in the sum. The trend index, trend episodes and especially, the deviation index reveal early evolving changes in the operating conditions, including cloudiness and load disturbances. The solution is highly compact: all variables, features and indices are transformed to the range [-2, 2] and represented in natural language which is important in integrating data-driven solutions with domain expertise. The special situations detected during the test campaigns are explained well.

  5. Comparative thermal buckling analysis of functionally graded plate

    Directory of Open Access Journals (Sweden)

    Čukanović Dragan V.

    2017-01-01

    Full Text Available A thermal buckling analysis of functionally graded thick rectangular plates accord¬ing to von Karman non-linear theory is presented. The material properties of the functionally graded plate, except for the Poisson’s ratio, were assumed to be graded in the thickness direction, according to a power-law distribution, in terms of the volume fractions of the metal and ceramic constituents. Formulations of equilibrium and stability equations are derived using the high order shear deformation theory based on different types of shape functions. Analytical method for determination of the critical buckling temperature for uniform increase of temperature, linear and non-linear change of temperature across thickness of a plate is developed. Numeri¬cal results were obtained in МATLAB software using combinations of symbolic and numeric values. The paper presents comparative results of critical buckling tempera¬ture for different types of shape functions. The accuracy of the formulation presented is verified by comparing to results available from the literature.

  6. Thermal Desorption Analysis of Effective Specific Soil Surface Area

    Science.gov (United States)

    Smagin, A. V.; Bashina, A. S.; Klyueva, V. V.; Kubareva, A. V.

    2017-12-01

    A new method of assessing the effective specific surface area based on the successive thermal desorption of water vapor at different temperature stages of sample drying is analyzed in comparison with the conventional static adsorption method using a representative set of soil samples of different genesis and degree of dispersion. The theory of the method uses the fundamental relationship between the thermodynamic water potential (Ψ) and the absolute temperature of drying ( T): Ψ = Q - aT, where Q is the specific heat of vaporization, and a is the physically based parameter related to the initial temperature and relative humidity of the air in the external thermodynamic reservoir (laboratory). From gravimetric data on the mass fraction of water ( W) and the Ψ value, Polyanyi potential curves ( W(Ψ)) for the studied samples are plotted. Water sorption isotherms are then calculated, from which the capacity of monolayer and the target effective specific surface area are determined using the BET theory. Comparative analysis shows that the new method well agrees with the conventional estimation of the degree of dispersion by the BET and Kutilek methods in a wide range of specific surface area values between 10 and 250 m2/g.

  7. Thermally-induced voltage alteration for integrated circuit analysis

    Energy Technology Data Exchange (ETDEWEB)

    Cole, E.I. Jr.

    2000-06-20

    A thermally-induced voltage alteration (TIVA) apparatus and method are disclosed for analyzing an integrated circuit (IC) either from a device side of the IC or through the IC substrate to locate any open-circuit or short-circuit defects therein. The TIVA apparatus uses constant-current biasing of the IC while scanning a focused laser beam over electrical conductors (i.e. a patterned metallization) in the IC to produce localized heating of the conductors. This localized heating produces a thermoelectric potential due to the Seebeck effect in any conductors with open-circuit defects and a resistance change in any conductors with short-circuit defects, both of which alter the power demand by the IC and thereby change the voltage of a source or power supply providing the constant-current biasing. By measuring the change in the supply voltage and the position of the focused and scanned laser beam over time, any open-circuit or short-circuit defects in the IC can be located and imaged. The TIVA apparatus can be formed in part from a scanning optical microscope, and has applications for qualification testing or failure analysis of ICs.

  8. Thermal decomposition kinetics of sorghum straw via thermogravimetric analysis.

    Science.gov (United States)

    Dhyani, Vaibhav; Kumar, Jitendra; Bhaskar, Thallada

    2017-12-01

    The thermal decomposition of sorghum straw was investigated by non-isothermal thermogravimetric analysis, where the determination of kinetic triplet (activation energy, pre-exponential factor, and reaction model), was the key objective. The activation energy was determined using different isoconversional methods: Friedman, Flynn-Wall-Ozawa (FWO), Kissinger-Akahira-Sunose (KAS), Starink, Iterative method of Chai & Chen, Vyazovkin AIC method, and Li & Tang equation. The pre-exponential factor was calculated using Kissinger's equation; while the reaction model was predicted by comparison of z-master plot obtained from experimental values with the theoretical plots. The values of activation energy obtained from isoconversional methods were further used for evaluation of thermodynamic parameters, enthalpy, entropy and Gibbs free energy. Results showed three zones of pyrolysis having average activation energy values of 151.21kJ/mol, 116.15kJ/mol, and 136.65kJ/mol respectively. The data was well fitting with two-dimension 'Valensi' model for conversion values from 0 to 0.4 with a coefficient of determination (R 2 ) value of 0.988, and with third order reaction model for values from 0.4 to 0.9 with an R 2 value of 0.843. Copyright © 2017 Elsevier Ltd. All rights reserved.

  9. The Storage of Thermal Reactor Safety Analysis data (STRESA)

    International Nuclear Information System (INIS)

    Tanarro Colodron, J.

    2016-01-01

    Full text: Storage of Thermal Reactor Safety Analysis data (STRESA) is an online information system that contains three technical databases: 1) European Nuclear Research Facilities, open to all online visitors; 2) Nuclear Experiments, available only to registered users; 3) Results Data, being the core content of the information system, its availability depends on the role and organisation of each user. Its main purpose is to facilitate the exchange of experimental data produced by large Euratom funded scientific projects addressing severe accidents, providing at the same time a secure repository for this information. Due to its purpose and architecture, it has become an important asset for networks of excellence as SARNET or NUGENIA. The Severe Accident ResearchNetwork of Excellence (SARNET)was set up in 2004 under the aegis of the research Euratom Framework Programmes to study severe accidents in watercooled nuclear power plants. Coordinated by the IRSN, SARNET unites 43 organizations involved in research on nuclear reactor safety in 18 European countries plus the USA, Canada, South Korea and India. In 2013, SARNET became fully integrated in the Technical Area N2(TA2), named “Severe accidents” of NUGENIA association, devoted to R&D on fission technology of Generation II and III. (author

  10. Mechanical and Thermal Analysis of Classical Functionally Graded Coated Beam

    Directory of Open Access Journals (Sweden)

    Toudehdehghan Abdolreza

    2018-01-01

    Full Text Available The governing equation of a classical rectangular coated beam made of two layers subjected to thermal and uniformly distributed mechanical loads are derived by using the principle of virtual displacements and based on Euler-Bernoulli deformation beam theory (EBT. The aim of this paper was to analyze the static behavior of clamped-clamped thin coated beam under thermo-mechanical load using MATLAB. Two models were considered for composite coated. The first model was consisting of ceramic layer as a coated and substrate which was metal (HC model. The second model was consisting of Functionally Graded Material (FGM as a coated layer and metal substrate (FGC model. From the result it was apparent that the superiority of the FGC composite against conventional coated composite has been demonstrated. From the analysis, the stress level throughout the thickness at the interface of the coated beam for the FGC was reduced. Yet, the deflection in return was observed to increase. Therefore, this could cater to various new engineering applications where warrant the utilization of material that has properties that are well-beyond the capabilities of the conventional or yesteryears materials.

  11. Analysis and optimization of hybrid electric vehicle thermal management systems

    Science.gov (United States)

    Hamut, H. S.; Dincer, I.; Naterer, G. F.

    2014-02-01

    In this study, the thermal management system of a hybrid electric vehicle is optimized using single and multi-objective evolutionary algorithms in order to maximize the exergy efficiency and minimize the cost and environmental impact of the system. The objective functions are defined and decision variables, along with their respective system constraints, are selected for the analysis. In the multi-objective optimization, a Pareto frontier is obtained and a single desirable optimal solution is selected based on LINMAP decision-making process. The corresponding solutions are compared against the exergetic, exergoeconomic and exergoenvironmental single objective optimization results. The results show that the exergy efficiency, total cost rate and environmental impact rate for the baseline system are determined to be 0.29, ¢28 h-1 and 77.3 mPts h-1 respectively. Moreover, based on the exergoeconomic optimization, 14% higher exergy efficiency and 5% lower cost can be achieved, compared to baseline parameters at an expense of a 14% increase in the environmental impact. Based on the exergoenvironmental optimization, a 13% higher exergy efficiency and 5% lower environmental impact can be achieved at the expense of a 27% increase in the total cost.

  12. Thermal Analysis of Solid Fuels in an Inert Atmosphere

    Science.gov (United States)

    Kijo-Kleczkowska, Agnieszka; Szumera, Magdalena; Środa, Katarzyna

    2017-12-01

    The paper takes the analysis of thermal studies of different types of fuels. It allowed diversification of fuels depending on their composition and origin. Consideration of coal, biomass and waste (coal mule, sewage sludge) as fuel is nowadays an important aspect of energy in our country. It should be emphasized that Poland power engineering is based up to 95% on coal - the primary fuel. Mining industry, forced to deliver power engineering more and better fuel, must however, use a deeper cleaning of coal. This results in a continuous increase waste in the form of mule flotation. The best method of disposing these mule is combustion and co-combustion with other fuels. On the other hand, commonly increasing awareness state of the environment and the need to reduce CO2 emissions energy industry have committed to implement alternative solutions in order to gain power, through, i.a.: development technologies use of biomass, which is one of the most promising renewable energy sources in Poland. The paper presents the results of research TG-DTA fuels made in an inert atmosphere.

  13. Unsteady thermal analysis of gas-cooled fast reactor core

    International Nuclear Information System (INIS)

    Lakkis, I.A.

    1993-01-01

    This thesis presents numerical analysis of transient heat transfer in an equivalent coolant-fuel rod cell of a typical gas cooled, fast nuclear reactor core. The transient performance is assumed to follow a complete sudden loss of coolant starting from steady state operation. Steady state conditions are obtained from solving a conduction problem in the fuel rod and a parabolic turbutent convection problem in the coolant section. The coupling between the two problems is accomplished by ensuring continuity of the thermal conditions at the interface between the fuel rod and the coolant. to model turbulence, the mixing tenght theory is used. Various fuel rod configurations have been tested for optimal transient performance. Actually, the loss of coolant accident occurs gradually at an exponential rate. Moreover, a time delay before shutting down the reactor by insertion of control rods usually exists. It is required to minimize maximum steady state cladding temperature so that the time required to reach its limiting value during transient state is maximum. This will prevent the escape of radioactive gases that endanger the environment and the public. However, the case considered here is a limiting case representing what could actually happen in the worst probable accident. So, the resutls in this thesis are very indicative regarding selection of the fuel rode configuration for better transient performance in case of accidents in which complete loss of collant occurs instantaneously

  14. Remote sensing analysis of thermal plumes at the Savannah River Plant

    International Nuclear Information System (INIS)

    Doak, E.L.

    1985-01-01

    The nuclear reactors of the Savannah River Plant (SRP) in Aiken, South Carolina, use cold water diverted from the Savannah River to dissipate unused thermal energy. This water is heated by heat exchangers of the reactors during the materials production process, and then returned to the natural drainage system. Thermal effluents were monitored by an airborne thermal infrared scanner during predawn overlights. Images were generated to show the surface temperature distribution of the thermal outfall plumes into the Savannah River. The thermal analysis provides information related to compliance with permit requirements of the regulatory agencies

  15. Thermal analysis of dry eye subjects and the thermal impulse perturbation model of ocular surface.

    Science.gov (United States)

    Zhang, Aizhong; Maki, Kara L; Salahura, Gheorghe; Kottaiyan, Ranjini; Yoon, Geunyoung; Hindman, Holly B; Aquavella, James V; Zavislan, James M

    2015-03-01

    In this study, we explore the usage of ocular surface temperature (OST) decay patterns to distinguished between dry eye patients with aqueous deficient dry eye (ADDE) and meibomian gland dysfunction (MGD). The OST profiles of 20 dry eye subjects were measured by a long-wave infrared thermal camera in a standardized environment (24 °C, and relative humidity (RH) 40%). The subjects were instructed to blink every 5 s after 20 ∼ 25 min acclimation. Exponential decay curves were fit to the average temperature within a region of the central cornea. We find the MGD subjects have both a higher initial temperature (p model, referred to as the thermal impulse perturbation (TIP) model. We conclude that long-wave-infrared thermal imaging is a plausible tool in assisting with the classification of dry eye patient. Copyright © 2015 Elsevier Ltd. All rights reserved.

  16. Stress analysis in curved composites due to thermal loading

    Science.gov (United States)

    Polk, Jared Cornelius

    Many structures in aircraft, cars, trucks, ships, machines, tools, bridges, and buildings, consist of curved sections. These sections vary from straight line segments that have curvature at either one or both ends, segments with compound curvatures, segments with two mutually perpendicular curvatures or Gaussian curvatures, and segments with a simple curvature. With the advancements made in multi-purpose composites over the past 60 years, composites slowly but steadily have been appearing in these various vehicles, compound structures, and buildings. These composite sections provide added benefits over isotropic, polymeric, and ceramic materials by generally having a higher specific strength, higher specific stiffnesses, longer fatigue life, lower density, possibilities in reduction of life cycle and/or acquisition cost, and greater adaptability to intended function of structure via material composition and geometry. To be able to design and manufacture a safe composite laminate or structure, it is imperative that the stress distributions, their causes, and effects are thoroughly understood in order to successfully accomplish mission objectives and manufacture a safe and reliable composite. The objective of the thesis work is to expand upon the knowledge of simply curved composite structures by exploring and ascertaining all pertinent parameters, phenomenon, and trends in stress variations in curved laminates due to thermal loading. The simply curved composites consist of composites with one radius of curvature throughout the span of the specimen about only one axis. Analytical beam theory, classical lamination theory, and finite element analysis were used to ascertain stress variations in a flat, isotropic beam. An analytical method was developed to ascertain the stress variations in an isotropic, simply curved beam under thermal loading that is under both free-free and fixed-fixed constraint conditions. This is the first such solution to Author's best knowledge

  17. Hydrocarbon Fuel Thermal Performance Modeling based on Systematic Measurement and Comprehensive Chromatographic Analysis

    Science.gov (United States)

    2016-07-31

    distribution unlimited Hydrocarbon Fuel Thermal Performance Modeling based on Systematic Measurement and Comprehensive Chromatographic Analysis Matthew...vital importance for hydrocarbon -fueled propulsion systems: fuel thermal performance as indicated by physical and chemical effects of cooling passage... analysis . The selection and acquisition of a set of chemically diverse fuels is pivotal for a successful outcome since test method validation and

  18. Development of the finite element method in the thermal field. TRIO-EF software for thermal and radiation analysis

    International Nuclear Information System (INIS)

    Casalotti, N.; Magnaud, J.P.

    1989-01-01

    The possibilities of the TRIO-EF software in the thermal field are presented. The TRIO-EF is a computer program based on the finite element method and used for three-dimensional incompressible flow analysis. It enables the calculation of three-dimensional heat transfer and the fluid/structure analysis. The geometrically complex radiative reactor systems are taken into account in the form factor calculation. The implemented algorithms are described [fr

  19. Analysis of non-thermal velocities in the solar corona

    Directory of Open Access Journals (Sweden)

    L. Contesse

    2004-09-01

    Full Text Available We describe new ground-based spectroscopic observations made using a 40-cm aperture coronagraph over a whole range of radial distances (up to heights of 12' above the limb and along four different heliocentric directions N, E, S and W. The analysis is limited to the study of the brightest forbidden emission line of Fe XIV at 530.3nm, in order to reach the best possible signal-to-noise ratio. To make the results statistically more significant, the extracted parameters are averaged over the whole length of the slit, and measurements are repeated fives times at each position; the corresponding dispersions in the results obtained along the slit are given. Central line profile intensities and full line widths (FWHM are plotted and compared to measurements published by other authors closer to the limb. We found widths and turbulent (non-thermal velocities of significantly higher values above the polar regions, especially when a coronal hole is present along the line of sight. We do not see a definitely decreasing behaviour of widths and turbulent velocities in equatorial directions for larger radial distances, as reported in the literature, although lower values are measured compared to the values in polar regions. The variation in the high corona is rather flat and a correlation diagram indicates that it is different for different regions and different radial distances. This seems to be the first analysis of the profiles of this coronal line, up to large heights above the limb for both equatorial and polar regions.

  20. Thermal-Hydraulics analysis of pressurized water reactor core by using single heated channel model

    Directory of Open Access Journals (Sweden)

    Reza Akbari

    2017-08-01

    Full Text Available Thermal hydraulics of nuclear reactor as a basis of reactor safety has a very important role in reactor design and control. The thermal-hydraulic analysis provides input data to the reactor-physics analysis, whereas the latter gives information about the distribution of heat sources, which is needed to perform the thermal-hydraulic analysis. In this study single heated channel model as a very fast model for predicting thermal hydraulics behavior of pressurized water reactor core has been developed. For verifying the results of this model, we used RELAP5 code as US nuclear regulatory approved thermal hydraulics code. The results of developed single heated channel model have been checked with RELAP5 results for WWER-1000. This comparison shows the capability of single heated channel model for predicting thermal hydraulics behavior of reactor core.

  1. Techniques for the thermal/hydraulic analysis of LMFBR check valves

    International Nuclear Information System (INIS)

    Cho, S.M.; Kane, R.S.

    1979-01-01

    A thermal/hydraulic analysis of the check valves in liquid sodium service for LMFBR plants is required to provide temperature data for thermal stress analysis of the valves for specified transient conditions. Because of the complex three-dimensional flow pattern within the valve, the heat transfer analysis techniques for less complicated shapes could not be used. This paper discusses the thermal analysis techniques used to assure that the valve stress analysis is conservative. These techniques include a method for evaluating the recirculating flow patterns and for selecting appropriately conservative heat transfer correlations in various regions of the valve

  2. Thermal Conductivity Measurement and Analysis of Fully Ceramic Microencapsulated fuel

    International Nuclear Information System (INIS)

    Lee, H. G.; Kim, D. J.; Park, J. Y.; Kim, W. J.; Lee, S. J.

    2015-01-01

    FCM nuclear fuel is composed of tristructural isotropic(TRISO) fuel particle and SiC ceramic matrix. SiC ceramic matrix play an essential part in protecting fission product. In the FCM fuel concept, fission product is doubly protected by TRISO coating layer and SiC ceramic matrix in comparison with the current commercial UO2 fuel system of LWR. In addition to a safety enhancement of FCM fuel, thermal conductivity of SiC ceramic matrix is better than that of UO2 fuel. Because the centerline temperature of FCM fuel is lower than that of the current UO2 fuel due to the difference of thermal conductivity of fuel, an operational release of fission products from the fuel can be reduced. SiC ceramic has attracted for nuclear fuel application due to its high thermal conductivity properties with good radiation tolerant properties, a low neutron absorption cross-section and a high corrosion resistance. Thermal conductivity of ceramic matrix composite depends on the thermal conductivity of each component and the morphology of reinforcement materials such as fibers and particles. There are many results about thermal conductivity of fiber-reinforced composite like as SiCf/SiC composite. Thermal conductivity of SiC ceramics and FCM pellets with the volume fraction of TRISO particles were measured and analyzed by analytical models. Polycrystalline SiC ceramics and FCM pellets with TRISO particles were fabricated by hot press sintering with sintering additives. Thermal conductivity of the FCM pellets with TRISO particles of 0 vol.%, 10 vol.%, 20 vol.%, 30 vol.% and 40 vol.% show 68.4, 52.3, 46.8, 43.0 and 34.5 W/mK, respectively. As the volume fraction of TRISO particles increased, the measured thermal conductivity values closely followed the prediction of Maxwell's equation

  3. Thermal and structural analysis of a cryogenic conduction cooling system for a HTS NMR magnet

    Energy Technology Data Exchange (ETDEWEB)

    In, Se Hwan; Hong, Yong Jun; Yeom, Han Kil; Ko, Hyo Bong; Park, Seong Je [Korea Institute of Machinery and Materials, Daejeon (Korea, Republic of)

    2016-03-15

    The superconducting NMR magnets have used cryogen such as liquid helium for their cooling. The conduction cooling method using cryocoolers, however, makes the cryogenic cooling system for NMR magnets more compact and user-friendly than the cryogen cooling method. This paper describes the thermal and structural analysis of a cryogenic conduction cooling system for a 400 MHz HTS NMR magnet, focusing on the magnet assembly. The highly thermo-conductive cooling plates between HTS double pancake coils are used to transfer the heat generated in coils, namely Joule heating at lap splice joints, to thermal link blocks and finally the cryocooler. The conduction cooling structure of the HTS magnet assembly preliminarily designed is verified by thermal and structural analysis. The orthotropic thermal properties of the HTS coil, thermal contact resistance and radiation heat load are considered in the thermal analysis. The thermal analysis confirms the uniform temperature distribution for the present thermal design of the NMR magnet within 0.2 K. The mechanical stress and the displacement by the electromagnetic force and the thermal contraction are checked to verify structural stability. The structural analysis indicates that the mechanical stress on each component of the magnet is less than its material yield strength and the displacement is acceptable in comparison with the magnet dimension.

  4. Performance analysis of a hybrid photovoltaic thermal solar air heater

    International Nuclear Information System (INIS)

    Othman, Mohd Yusof; Yatim, Baharudin; Abu Bakar, Mohd Nazari; Sopian, Kamaruzzaman

    2006-01-01

    A photovoltaic (PV/T) air heater is a collector that combines thermal and photovoltaic systems in one single hybrid generating unit. It generators both thermal and electrical energies simultaneously. A new design of a double-pass photovoltaic-thermal solar air collector with CPC and fins was successfully developed and fabricated at Universiti Kebangsaam Malaysia. This collector tested under actual environmental conditions to study its performance over a range of operating conditions. The test set-up, instrumentation and measurement are described further. It was found that the performance of the collector was in agreement with the theoretical prediction. Results of the outdoors test are presented and discussed(Author)

  5. Modeling and analysis of a robust thermal control system based on forced convection thermal switches

    Science.gov (United States)

    Williams, Andrew D.; Palo, Scott E.

    2006-05-01

    There is a critical need, not just in the Department of Defense (DOD) but the entire space industry, to reduce the development time and overall cost of satellite missions. To that end, the DOD is actively pursuing the capability to reduce the deployment time of a new system from years to weeks or even days. The goal is to provide the advantages space affords not just to the strategic planner but also to the battlefield commanders. One of the most challenging aspects of this problem is the satellite's thermal control system (TCS). Traditionally the TCS must be vigorously designed, analyzed, tested, and optimized from the ground up for every satellite mission. This "reinvention of the wheel" is costly and time intensive. The next generation satellite TCS must be modular and scalable in order to cover a wide range of applications, orbits, and mission requirements. To meet these requirements a robust thermal control system utilizing forced convection thermal switches was investigated. The problem was investigated in two separate stages. The first focused on the overall design of the bus. The second stage focused on the overarching bus architecture and the design impacts of employing a thermal switch based TCS design. For the hot case, the fan provided additional cooling to increase the heat transfer rate of the subsystem. During the cold case, the result was a significant reduction in survival heater power.

  6. Theoretical basis for a transient thermal elastic-plastic stress analysis of nuclear reactor fuel elements

    International Nuclear Information System (INIS)

    Hsu, T.R.; Bertels, A.W.M.; Banerjee, S.; Harrison, W.C.

    1976-07-01

    This report presents the theoretical basis for a transient thermal elastic-plastic stress analysis of a nuclear reactor fuel element subject to severe transient thermo-mechanical loading. A finite element formulation is used for both the non-linear stress analysis and thermal analysis. These two major components are linked together to form an integrated program capable of predicting fuel element transient behaviour in two dimensions. Specific case studies are presented to illustrate capabilities of the analysis. (author)

  7. Preliminary analysis of geothermal aspects of Brazilian thermal spring

    International Nuclear Information System (INIS)

    Hurter, S.J.; Hamza, V.M.

    1982-01-01

    Information on more than 400 geothermal springs in Brazil has been assembled. On the basis of the data colected the temperatures at the maximum depths of circulation of spring waters are calculated using the quality of silica dissolved in water. For some thermal springs temperatures are calculated on the basis of silica determination carrried out by us. Applying linear relations between silica temperature and geothermal flux the average depths of water circulation in the Parana Basin and the Brazilian folded belts surrounding the San Francisco craton are calculated. The radioactivity of the water, derived mainly from the dissolved radon can be correlated with the temperature of the spring. An inverse correlation, as was observed for thermal springs of Pocos de Caldas, can be used to calculate the ascent velocity of thermal waters, where as, a positive correlations could be interpreted as due to the mixing of thermal with surface waters. (Author) [pt

  8. Modelling and analysis of radial thermal stresses and temperature ...

    African Journals Online (AJOL)

    user

    The temperature field, heat transfer rate and thermal stresses were investigated with numerical simulation models using FORTRAN FE (finite element) software. ...... specific heats, International Communications in Heat and Mass Transfer, Vol.

  9. Joint Removal Implications : Thermal Analysis and Life-Cycle Cost

    Science.gov (United States)

    2018-04-01

    Deck joints are causing significant bridge deterioration and maintenance problems for Departments of Transportation (DOTs). Colorado State University researchers partnered with the Colorado DOT to analyze the effects of temperature change and thermal...

  10. Analysis of regenerative thermal storage geometries for solar gas turbines

    CSIR Research Space (South Africa)

    Klein, P

    2014-08-01

    Full Text Available Ceramic heat regenerators are suited to providing thermal storage for concentrating solar power stations based on a recuperated gas turbine cycle. Randomly packed beds of spheres and saddles; honeycombs and checker bricks were identified...

  11. Statistical analysis of thermal conductivity of nanofluid containing ...

    Indian Academy of Sciences (India)

    Administrator

    four temperatures for thermal conductivity of pristine. MWCNTs ... MWCNTs. In other words, the augmentation of the ... TiO2 nanofluid, means with different letters are significantly different .... Chen L and Xie H 2010 Thermochim Acta 497 67.

  12. PCB-level Electro thermal Coupling Simulation Analysis

    Science.gov (United States)

    Zhou, Runjing; Shao, Xuchen

    2017-10-01

    Power transmission network needs to transmit more current with the increase of the power density. The problem of temperature rise and the reliability is becoming more and more serious. In order to accurately design the power supply system, we must consider the influence of the power supply system including Joule heat, air convection and other factors. Therefore, this paper analyzes the relationship between the electric circuit and the thermal circuit on the basis of the theory of electric circuit and thermal circuit.

  13. Temperature and Thermal Stress Analysis of Refractory Products

    Directory of Open Access Journals (Sweden)

    Shaoyang Shi

    2013-05-01

    Full Text Available Firstly current status of temperature and thermal stress research of refractory product at home and aboard are analyzed. Finite element model of two classical refractory products is building by using APDL language. Distribution law of temperature and thermal stress of two typical refractory products-ladles and tundish are analyzed and their structures are optimized. Stress of optimal structure is dropped obviously, and operation life is increased effectively.

  14. Dynamic response analysis of an aircraft structure under thermal-acoustic loads

    International Nuclear Information System (INIS)

    Cheng, H; Li, H B; Zhang, W; Wu, Z Q; Liu, B R

    2016-01-01

    Future hypersonic aircraft will be exposed to extreme combined environments includes large magnitude thermal and acoustic loads. It presents a significant challenge for the integrity of these vehicles. Thermal-acoustic test is used to test structures for dynamic response and sonic fatigue due to combined loads. In this research, the numerical simulation process for the thermal acoustic test is presented, and the effects of thermal loads on vibro-acoustic response are investigated. To simulate the radiation heating system, Monte Carlo theory and thermal network theory was used to calculate the temperature distribution. Considering the thermal stress, the high temperature modal parameters are obtained with structural finite element methods. Based on acoustic finite element, modal-based vibro-acoustic analysis is carried out to compute structural responses. These researches are very vital to optimum thermal-acoustic test and structure designs for future hypersonic vehicles structure (paper)

  15. Analysis of thermal water utilization in the northeastern Slovenia

    Directory of Open Access Journals (Sweden)

    Nina Rman

    2012-12-01

    Full Text Available The presented research aims at identification of thermal water users in NE Slovenia, at finding type and amountof the produced thermal water as well as its utilization practice. The energetic overview has been upgradedby a description of current observational monitoring practice and thermal waste water management, but technologicalproblems of thermal water use and their mitigation are discussed also. We have ascertained that 14 of 26active geothermalwells tap the Mura Formation aquifer in which the only reinjection well is perforated also. Totalthermal water abstraction summed to 3.29 million m3 in 2011. Cascade use of thermal water is abundant, whereindividual space and sanitary water heating is followed by heating of spa infrastructure and balneology. Greenhouseheating systems and district heating were also identified. Operational monitoring of these geothermal wellsis generally insufficient, and geothermal aquifers are overexploited due to decades of historical water abstraction.All these facts indicate the need for applying appropriate measures which will improve their natural conditions aswell as simultaneously enable further and even higher thermal water utilization in the future.

  16. SEM and elemental analysis of composite resins

    International Nuclear Information System (INIS)

    Hosoda, H.; Yamada, T.; Inokoshi, S.

    1990-01-01

    Twenty-four chemically cured, 21 light-cured anterior, three light-cured anterior/posterior, and 18 light-cured posterior composite resins were examined using scanning electron microscopy, and the elemental composition of their filler particles was analyzed with an energy dispersive electron probe microanalyzer. According to the results obtained, the composite resins were divided into five groups (traditional, microfilled type, submicrofilled type, hybrid type, and semihybrid), with two additional hypothetical categories (microfilled and hybrid). Characteristics of each type were described with clinical indications for selective guidance of respective composite resins for clinical use

  17. Thermal Analysis Evaluation of Spent Fuel Storage Rack for Research Reactor

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Sangjin; Oh, Jinho; Kwak, Jinsung; Lee, Jongmin [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2016-10-15

    Spent fuel storage rack is to store spent fuel assemblies. The spent fuel storage rack is submerged in the designated pool for cooling. Due to the condition change of the pool water, the effect of thermal load on spent fuel storage rack must be analyzed and evaluated. In this paper, thermal stress analysis is performed and evaluated on a spent fuel storage rack. For thermal stress evaluation of the spent fuel storage rack, load combinations and allowable criteria in ASME Sec. III NB-3220 are applied. In cases of A-1 and B-1, the same temperature applied on the whole model, thermal stress doesn't occur because there is no constraint about the thermal expansion. The support frame is located on the pool bottom in free standing type and the racks are located in the support frame with enough space. Thermal expansion was considered and reflected in the design of spent fuel storage rack in advance. Thermal stress analysis is performed and evaluated on a spent fuel storage rack with consideration of pool water temperature variation. The thermal analysis including a linear heat transfer and the thermal stress analysis is performed for the racks and support frame and resulted stresses are within allowable criteria.

  18. High performance thermal stress analysis on the earth simulator

    International Nuclear Information System (INIS)

    Noriyuki, Kushida; Hiroshi, Okuda; Genki, Yagawa

    2003-01-01

    In this study, the thermal stress finite element analysis code optimized for the earth simulator was developed. A processor node of which of the earth simulator is the 8-way vector processor, and each processor can communicate using the message passing interface. Thus, there are two ways to parallelize the finite element method on the earth simulator. The first method is to assign one processor for one sub-domain, and the second method is to assign one node (=8 processors) for one sub-domain considering the shared memory type parallelization. Considering that the preconditioned conjugate gradient (PCG) method, which is one of the suitable linear equation solvers for the large-scale parallel finite element methods, shows the better convergence behavior if the number of domains is the smaller, we have determined to employ PCG and the hybrid parallelization, which is based on the shared and distributed memory type parallelization. It has been said that it is hard to obtain the good parallel or vector performance, since the finite element method is based on unstructured grids. In such situation, the reordering is inevitable to improve the computational performance [2]. In this study, we used three reordering methods, i.e. Reverse Cuthil-McKee (RCM), cyclic multicolor (CM) and diagonal jagged descending storage (DJDS)[3]. RCM provides the good convergence of the incomplete lower-upper (ILU) PCG, but causes the load imbalance. On the other hand, CM provides the good load balance, but worsens the convergence of ILU PCG if the vector length is so long. Therefore, we used the combined-method of RCM and CM. DJDS is the method to store the sparse matrices such that longer vector length can be obtained. For attaining the efficient inter-node parallelization, such partitioning methods as the recursive coordinate bisection (RCM) or MeTIS have been used. Computational performance of the practical large-scale engineering problems will be shown at the meeting. (author)

  19. Thermodynamic study of ibuprofen by adiabatic calorimetry and thermal analysis

    International Nuclear Information System (INIS)

    Xu Fen; Sun Lixian; Tan Zhicheng; Liang Jianguo; Li Ruilian

    2004-01-01

    Molar heat capacities of ibuprofen were precisely measured with a small sample precision automated adiabatic calorimeter over the temperature range from 80 to 400 K. The polynomial functions of C p,m (J K -1 mol -1 ) versus T were established on the heat capacity measurements by means of the least fitting square method. The functions are as follows: for solid ibuprofen, at the temperature range of 79.105 K≤T≤333.297 K, C p,m =144.27+77.046X+3.5171X 2 +10.925X 3 +11.224X 4 , where X=(T-206.201)/127.096; for liquid ibuprofen, at the temperature range of 353.406 K≤T≤378.785 K, C p,m =325.79+8.9696X-1.6073X 2 -1.5145X 3 , where X=(T-366.095)/12.690. A fusion transition at T=348.02 K was found from the C p -T curve. The molar enthalpy and entropy of the fusion transition were determined to be 26.65 kJ mol -1 and 76.58 J mol -1 K -1 , respectively. The thermodynamic functions on the base of the reference temperature of 298.15 K, (H T -H 298.15 ) and (S T -S 298.15 ), were derived. Thermal characteristic of ibuprofen was studied by thermo-gravimetric analysis (TG-DTG) and differential scanning calorimeter (DSC). The temperature of fusion, the molar enthalpy and entropy of fusion obtained by DSC were well consistent with those obtained by adiabatic calorimeter. The evaporation process of ibuprofen was investigated further by TG and DTG, and the activation energy of the evaporation process was determined to be 80.3±1.4 kJ mol -1

  20. Antagonistic effects of Bacillus subtilis subsp. subtilis and B. amyloliquefaciens against Macrophomina phaseolina: SEM study of fungal changes and UV-MALDI-TOF MS analysis of their bioactive compounds.

    Science.gov (United States)

    Torres, M J; Brandan, C Pérez; Petroselli, G; Erra-Balsells, R; Audisio, M C

    2016-01-01

    The antifungal effect of Bacillus subtilis subsp. subtilis PGPMori7 and Bacillus amyloliquefaciens PGPBacCA1 was evaluated against Macrophomina phaseolina (Tassi) Goid. Cell suspension (CS), cell-free supernatant (CFS) and the lipopeptide fraction (LF) of PGPMori7 and PGPBacCA1 were screened against three different M. phaseolina strains. CS exhibited the highest inhibitory effect (around 50%) when compared to those of CFS and LF, regardless of the fungal strain studied. The synthesis of lipopeptides was studied by UV-MALDI TOF. Chemical analysis of Bacillus metabolite synthesis revealed that surfactin and iturin were mainly produced in liquid medium. Potential fengycin was also co-produced when both Bacillus were cultivated in solid medium. In co-culture assays, the bacterial colony-fungal mycelium interface at the inhibition zone was evaluated by both scanning electron microscopy (SEM) and UV-MALDI TOF, the former to determine the structural changes on M. phaseolina cells and the latter to identify the main bioactive molecules involved in the inhibitory effect. PGPBacCA1 produced surfactin, iturin and fengycin in the inhibition zone while PGPMori7 only produced these metabolites within its colony and not in the narrow inhibition zone. Interestingly, SEM revealed that PGPBacCA1 induced damage in M. phaseolina sclerotia, generating a fungicidal effect as no growth was observed when normal growth conditions were reestablished. In turn, PGPMori7 inhibited the growth of the Macrophomina mycelium without fungal injury, resulting only in a fungistatic activity. From these results, it was determined that the two bacilli significantly inhibited the growth of an important phytopathogenic fungus by at least two different mechanisms: lipopeptide synthesis and competition among microorganisms. Copyright © 2015 Elsevier GmbH. All rights reserved.