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Sample records for sand-packed column tests

  1. Fluoride retardation from quartz sand-packed column tests

    Directory of Open Access Journals (Sweden)

    Eduardo Usunoff

    2009-06-01

    Full Text Available Inasmuch as both low and high concentrations of F- in groundwater have different detrimental effects on human health (increased dental caries, and mottled enamel or even severe structural bone deformations, respectively, many efforts have focused on the movement of such anion in aqueous systems. It is so because water drinking is the main intake of F- by humans. This paper presents the results of seven dynamic experiments in which solutions of varying [F-], pH, and flow velocities circulated through columns packed with clean quartz sand. The breakthrough data were analyzed by means of a computer code adapted to the estimation of equilibrium and non-equilibrium solute transport parameters from miscible displacement experiments in a steady-state, uniform flow field using a pulse-type or continuous source. It was found that larger retardation factors (R are associated with low pH, low [F-] in the feed solutions, and larger flow velocities. Such results appear to be related to the form of the F species, the rather weak bond between the adsorbate and the quartz sand, and stronger anion repulsion at low pore velocities. The estimated values for R vary between 1,22 and 1,50, whereas the distribution coefficients were in the range of 0,1 to 0,05 L kg-1. It should be said that the breakthrough curves display hysteresis, leading to a desorption behavior that proceeds faster than the adsorption process.Puesto que tanto valores bajos como altos de F- en las aguas subterráneas tienen efectos adversos en la salud de los humanos (mayor cantidad de caries, y manchas del esmalte dental e incluso deformaciones óseas, respectivamente, han sido muchos los esfuerzos destinados a dilucidar el movimiento de especies fluoradas en ambientes acuosos. Ello es así porque el consumo de agua por parte de seres humanos representa la mayor fuente de ingreso de F-. Este trabajo presenta los resultados de siete experimentos dinámicos en los que soluciones de diferentes [F

  2. HYDRAULIC ELEVATOR INSTALLATION ESTIMATION FOR THE WATER SOURCE WELL SAND-PACK CLEANING UP

    Directory of Open Access Journals (Sweden)

    V. V. Ivashechkin

    2016-01-01

    Full Text Available The article offers design of a hydraulic elevator installation for cleaning up water-source wells of sand packs. It considerers the installation hydraulic circuit according to which the normal pump feeds the high-level tank water into the borehole through two parallel water lines. The water-jet line with washing nozzle for destroying the sand-pack and the supply pipe-line coupled with the operational nozzle of the hydraulic elevator containing the inlet and the supply pipelines for respectively intaking the hydromixture and removing it from the well. The paper adduces equations for fluid motion in the supply and the water-jet pipelines and offers expressions for evaluating the required heads in them. For determining water flow in the supply and the water-jet pipe lines the author proposes to employ graphical approach allowing finding the regime point in Q–H chart by means of building characteristics of the pump and the pipe-lines. For calculating the useful vertical head, supply and dimensions of the hydraulic elevator the article employs the equation of motion quantity with consistency admission of the motion quantity before and after mixing the flows in the hydraulic elevator. The suggested correlations for evaluating the hydraulic elevator efficiency determine the sand pack removal duration as function of its sizes and the ejected fluid flow rate. A hydraulic-elevator installation parameters estimation example illustrates removing a sand pack from a water-source borehole of 41 m deep and 150 mm diameter bored in the village of Uzla of Myadelsk region, of Minsk oblast. The working efficiency of a manufactured and laboratory tested engineering prototype of the hydraulic elevator installation was acknowledged in actual tests at the indicated borehole site. With application of graphical approach, the suggested for the hydraulic elevator installation parameters calculation procedure allows selecting, with given depth and the borehole diameter

  3. Interpretation of the lime column penetration test

    International Nuclear Information System (INIS)

    Liyanapathirana, D S; Kelly, R B

    2010-01-01

    Dry soil mix (DSM) columns are used to reduce the settlement and to improve the stability of embankments constructed on soft clays. During construction the shear strength of the columns needs to be confirmed for compliance with technical assumptions. A specialized blade shaped penetrometer known as the lime column probe, has been developed for testing DSM columns. This test can be carried out as a pull out resistance test (PORT) or a push in resistance test (PIRT). The test is considered to be more representative of average column shear strength than methods that test only a limited area of the column. Both PORT and PIRT tests require empirical correlations of measured resistance to an absolute measure of shear strength, in a similar manner to the cone penetration test. In this paper, finite element method is used to assess the probe factor, N, for the PORT test. Due to the large soil deformations around the probe, an Arbitrary Lagrangian Eulerian (ALE) based finite element formulation has been used. Variation of N with rigidity index and the friction at the probe-soil interface are investigated to establish a range for the probe factor.

  4. Investigation of Asphaltene Adsorption onto Zeolite Beta Nanoparticles to Reduce Asphaltene Deposition in a Silica Sand Pack

    Directory of Open Access Journals (Sweden)

    Kashefi Sepideh

    2018-01-01

    Full Text Available Zeolite beta nanoparticles were used as a new asphaltene adsorbent for reducing asphaltene deposition during fluid injection into a silica sand pack. At first, the asphaltene adsorption efficiency and capacity of zeolite beta nanoparticles were determined by UV-Vis spectrophotometer. It was found that the proper concentration of nanoparticles for asphaltene adsorption was 10 g/L and the maximum asphaltene adsorption onto zeolite beta was 1.98 mg/m2. Second, two dynamic experiments including co-injection of crude oil and n-heptane (as an asphaltene precipitant with and without use of zeolite beta nanoparticles in the sand pack was carried out. The results showed that the use of zeolite beta nanoparticles increased the permeability ratio and outlet fluid's asphaltene content about 22% and 40% compared to without use of nanoparticles, respectively. Moreover, a model based on monolayer asphaltene adsorption onto nanoparticles and asphaltene deposition mechanisms including surface deposition, entrainment and pore throat plugging was developed to determine formation damage during co-injection of crude oil and n-heptane into the sand pack. The proposed model presented good prediction of permeability and porosity ratios with AAD% of 1.07 and 0.07, respectively.

  5. Column Selection for Biomedical Analysis Supported by Column Classification Based on Four Test Parameters.

    Science.gov (United States)

    Plenis, Alina; Rekowska, Natalia; Bączek, Tomasz

    2016-01-21

    This article focuses on correlating the column classification obtained from the method created at the Katholieke Universiteit Leuven (KUL), with the chromatographic resolution attained in biomedical separation. In the KUL system, each column is described with four parameters, which enables estimation of the FKUL value characterising similarity of those parameters to the selected reference stationary phase. Thus, a ranking list based on the FKUL value can be calculated for the chosen reference column, then correlated with the results of the column performance test. In this study, the column performance test was based on analysis of moclobemide and its two metabolites in human plasma by liquid chromatography (LC), using 18 columns. The comparative study was performed using traditional correlation of the FKUL values with the retention parameters of the analytes describing the column performance test. In order to deepen the comparative assessment of both data sets, factor analysis (FA) was also used. The obtained results indicated that the stationary phase classes, closely related according to the KUL method, yielded comparable separation for the target substances. Therefore, the column ranking system based on the FKUL-values could be considered supportive in the choice of the appropriate column for biomedical analysis.

  6. Nondestructive evaluation of warm mix asphalt through resonant column testing.

    Science.gov (United States)

    2014-02-01

    Non-destructive testing has been used for decades to characterize engineering properties of hot-mix asphalt. Among such tests is the resonant column (RC) test, which is commonly used to characterize soil materials. The resonant column device at Penn ...

  7. Ultrasonic testing device having an adjustable water column

    Science.gov (United States)

    Roach, Dennis P.; Neidigk, Stephen O.; Rackow, Kirk A.; Duvall, Randy L.

    2015-09-01

    An ultrasonic testing device having a variable fluid column height is disclosed. An operator is able to adjust the fluid column height in real time during an inspection to to produce optimum ultrasonic focus and separate extraneous, unwanted UT signals from those stemming from the area of interest.

  8. Groundwater arsenic remediation using zerovalent iron: Batch and column tests

    Science.gov (United States)

    Recently, increasing efforts have been made to explore the applicability and limitations of zerovalent iron (Fe0) for the treatment of arsenicbearing groundwater and wastewater. The experimental batch and column tests have demonstrated that arsenate and arsenite are removed effec...

  9. Resonant Column Tests and Nonlinear Elasticity in Simulated Rocks

    Science.gov (United States)

    Sebastian, Resmi; Sitharam, T. G.

    2018-01-01

    Rocks are generally regarded as linearly elastic even though the manifestations of nonlinearity are prominent. The variations of elastic constants with varying strain levels and stress conditions, disagreement between static and dynamic moduli, etc., are some of the examples of nonlinear elasticity in rocks. The grain-to-grain contact, presence of pores and joints along with other compliant features induce the nonlinear behavior in rocks. The nonlinear elastic behavior of rocks is demonstrated through resonant column tests and numerical simulations in this paper. Resonant column tests on intact and jointed gypsum samples across varying strain levels have been performed in laboratory and using numerical simulations. The paper shows the application of resonant column apparatus to obtain the wave velocities of stiff samples at various strain levels under long wavelength condition, after performing checks and incorporating corrections to the obtained resonant frequencies. The numerical simulation and validation of the resonant column tests using distinct element method are presented. The stiffness reductions of testing samples under torsional and flexural vibrations with increasing strain levels have been analyzed. The nonlinear elastic behavior of rocks is reflected in the results, which is enhanced by the presence of joints. The significance of joint orientation and influence of joint spacing during wave propagation have also been assessed and presented using the numerical simulations. It has been found that rock joints also exhibit nonlinear behavior within the elastic limit.

  10. Engineered Barrier System Thermal-Hydraulic-Chemical Column Test Report

    International Nuclear Information System (INIS)

    W.E. Lowry

    2001-01-01

    The Engineered Barrier System (EBS) Thermal-Hydraulic-Chemical (THC) Column Tests provide data needed for model validation. The EBS Degradation, Flow, and Transport Process Modeling Report (PMR) will be based on supporting models for in-drift THC coupled processes, and the in-drift physical and chemical environment. These models describe the complex chemical interaction of EBS materials, including granular materials, with the thermal and hydrologic conditions that will be present in the repository emplacement drifts. Of particular interest are the coupled processes that result in mineral and salt dissolution/precipitation in the EBS environment. Test data are needed for thermal, hydrologic, and geochemical model validation and to support selection of introduced materials (CRWMS M and O 1999c). These column tests evaluated granular crushed tuff as potential invert ballast or backfill material, under accelerated thermal and hydrologic environments. The objectives of the THC column testing are to: (1) Characterize THC coupled processes that could affect performance of EBS components, particularly the magnitude of permeability reduction (increases or decreases), the nature of minerals produced, and chemical fractionation (i.e., concentrative separation of salts and minerals due to boiling-point elevation). (2) Generate data for validating THC predictive models that will support the EBS Degradation, Flow, and Transport PMR, Rev. 01

  11. Comparison of the release of constituents from granular materials under batch and column testing.

    Science.gov (United States)

    Lopez Meza, Sarynna; Garrabrants, Andrew C; van der Sloot, Hans; Kosson, David S

    2008-01-01

    Column leaching testing can be considered a better basis for assessing field impact data than any other available batch test method and thus provides a fundamental basis from which to estimate constituent release under a variety of field conditions. However, column testing is time-intensive compared to the more simplified batch testing, and may not always be a viable option when making decisions for material reuse. Batch tests are used most frequently as a simple tool for compliance or quality control reasons. Therefore, it is important to compare the release that occurs under batch and column testing, and establish conservative interpretation protocols for extrapolation from batch data when column data are not available. Five different materials (concrete, construction debris, aluminum recycling residue, coal fly ash and bottom ash) were evaluated via batch and column testing, including different column flow regimes (continuously saturated and intermittent unsaturated flow). Constituent release data from batch and column tests were compared. Results showed no significant difference between the column flow regimes when constituent release data from batch and column tests were compared. In most cases batch and column testing agreed when presented in the form of cumulative release. For arsenic in carbonated materials, however, batch testing underestimates the column constituent release for most LS ratios and also on a cumulative basis. For cases when As is a constituent of concern, column testing may be required.

  12. Ion Exchange Column Tests Supporting Technetium Removal Resin Maturation

    Energy Technology Data Exchange (ETDEWEB)

    Nash, C. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); McCabe, D. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); Hamm, L. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); Smith, F. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL); Morse, M. [Savannah River Site (SRS), Aiken, SC (United States). Savannah River National Lab. (SRNL)

    2013-12-20

    The primary treatment of the tank waste at the DOE Hanford site will be done in the Waste Treatment and Immobilization Plant, currently under construction. The baseline plan for this facility is to treat the waste, splitting it into High Level Waste (HLW) and Low Activity Waste (LAW). Both waste streams are then separately vitrified as glass and sealed in canisters. The LAW glass will be disposed on site. There are currently no plans to treat the waste to remove technetium, so its disposition path is the LAW glass. Due to the soluble properties of pertechnetate and long half-life of 99Tc, effective management of 99Tc is important. Options are being explored to immobilize the supplemental LAW portion of the tank waste, as well as to examine the volatility of 99Tc during the vitrification process. Removal of 99Tc, followed by off-site disposal has potential to reduce treatment and disposal costs. A conceptual flow sheets for supplemental LAW treatment and disposal that could benefit from technetium removal will specifically examine removing 99Tc from the LAW feed stream to supplemental immobilization. SuperLig® 639 is an elutable ion exchange resin. In the tank waste, 99Tc is predominantly found in the tank supernate as pertechnetate (TcO4-). Perrhenate (ReO4-) has been shown to be a good non-radioactive surrogate for pertechnetate in laboratory testing for this ion exchange resin. This report contains results of experimental ion exchange distribution coefficient and column resin maturation kinetics testing using the resin SuperLig® 639a to selectively remove perrhenate from simulated LAW. This revision includes results from testing to determine effective resin operating temperature range. Loading tests were performed at 45°C, and the computer modeling was updated to include the temperature effects. Equilibrium contact testing indicated that this batch of

  13. Mitigation of Oil in Water Column: Mitigation Prototype Tests

    Science.gov (United States)

    2017-06-01

    designed with an open end to allow aquatic animals to escape. After the treated foam becomes saturated with submerged oil, the net would be lifted...needed openings to allow the frame to pass through the water column without causing severe drag resistance . However, this also allows oil to flow...to the water and should only help the regions of hypoxia caused by microbial degradation of the oil. However, the proposed field set up with

  14. Multi-Column Experimental Test Bed for Xe/Kr Separation

    International Nuclear Information System (INIS)

    Greenhalgh, Mitchell Randy; Garn, Troy Gerry; Welty, Amy Keil; Lyon, Kevin Lawrence; Watson, Tony Leroy

    2015-01-01

    Previous research studies have shown that INL-developed engineered form sorbents are capable of capturing both Kr and Xe from various composite gas streams. The previous experimental test bed provided single column testing for capacity evaluations over a broad temperature range. To advance research capabilities, the employment of an additional column to study selective capture of target species to provide a defined final gas composition for waste storage was warranted. The second column addition also allows for compositional analyses of the final gas product to provide for final storage determinations. The INL krypton capture system was modified by adding an additional adsorption column in order to create a multi-column test bed. The purpose of this modification was to investigate the separation of xenon from krypton supplied as a mixed gas feed. The extra column was placed in a Stirling Ultra-low Temperature Cooler, capable of controlling temperatures between 190 and 253K. Additional piping and valves were incorporated into the system to allow for a variety of flow path configurations. The new column was filled with the AgZ-PAN sorbent which was utilized as the capture medium for xenon while allowing the krypton to pass through. The xenon-free gas stream was then routed to the cryostat filled with the HZ-PAN sorbent to capture the krypton at 191K. Selectivities of xenon over krypton were determined using the new column to verify the system performance and to establish the operating conditions required for multi-column testing. Results of these evaluations verified that the system was operating as designed and also demonstrated that AgZ-PAN exhibits excellent selectivity for xenon over krypton in air at or near room temperature. Two separation tests were performed utilizing a feed gas consisting of 1000 ppmv xenon and 150 ppmv krypton with the balance being made up of air. The AgZ-PAN temperature was held at 295 or 253K while the HZ-PAN was held at 191K for both

  15. Performance tests on column materials for {sup 99}Mo-{sup 99m}Tc generator

    Energy Technology Data Exchange (ETDEWEB)

    Sombrito, E Z; Bulos, A D; Tangonan, M C [Chemistry Research Section, Atomic Research Div., Philippine Nuclear Research Inst., Quezon (Philippines)

    1998-10-01

    To meet the need of producing a {sup 99}Mo-{sup 99m}Tc generator, based on low specific activity reactor-produced {sup 99}Mo, different procedures for preparing zirconium molybdate gels were tested. Performance tests were done on molybdate gel columns prepared using the procedures developed by Vietnam and China, and recently, on a polyzirconium compound (PZC) prepared in Japan. The conditions for the batch drying of a large volume of the gel material were studied as well as the conditions in preparing a column to concentrate technetium-99m. The performance of PZC sample as column material for the generator was also evaluated. (author)

  16. Multi-Column Experimental Test Bed Using CaSDB MOF for Xe/Kr Separation

    Energy Technology Data Exchange (ETDEWEB)

    Welty, Amy Keil [Idaho National Lab. (INL), Idaho Falls, ID (United States); Greenhalgh, Mitchell Randy [Idaho National Lab. (INL), Idaho Falls, ID (United States); Garn, Troy Gerry [Idaho National Lab. (INL), Idaho Falls, ID (United States)

    2016-03-01

    Processing of spent nuclear fuel produces off-gas from which several volatile radioactive components must be separated for further treatment or storage. As part of the Off-gas Sigma Team, parallel research at INL and PNNL has produced several promising sorbents for the selective capture of xenon and krypton from these off-gas streams. In order to design full-scale treatment systems, sorbents that are promising on a laboratory scale must be proven under process conditions to be considered for pilot and then full-scale use. To that end, a bench-scale multi-column system with capability to test multiple sorbents was designed and constructed at INL. This report details bench-scale testing of CaSDB MOF, produced at PNNL, and compares the results to those reported last year using INL engineered sorbents. Two multi-column tests were performed with the CaSDB MOF installed in the first column, followed with HZ-PAN installed in the second column. The CaSDB MOF column was placed in a Stirling cryocooler while the cryostat was employed for the HZ-PAN column. Test temperatures of 253 K and 191 K were selected for the first column while the second column was held at 191 K for both tests. Calibrated volume sample bombs were utilized for gas stream analyses. At the conclusion of each test, samples were collected from each column and analyzed for gas composition. While CaSDB MOF does appear to have good capacity for Xe, the short time to initial breakthrough would make design of a continuous adsorption/desorption cycle difficult, requiring either very large columns or a large number of smaller columns. Because of the tenacity with which Xe and Kr adhere to the material once adsorbed, this CaSDB MOF may be more suitable for use as a long-term storage solution. Further testing is recommended to determine if CaSDB MOF is suitable for this purpose.

  17. Significance of Iron(II,III) Hydroxycarbonate Green Rust in Arsenic Remediation Using Zerovalent Iron in Laboratory Column Tests

    Science.gov (United States)

    We examined the corrosion products of zerovalent iron used in three column tests for removing arsenic from water under dynamic flow conditions. Each column test lasted three- to four-months using columns consisting of a 10.3-cm depth of 50 : 50 (w : w, Peerless iron : sand) in t...

  18. The Inter Facility Testing of a Standard Oscillating Water Column (OWC) Type Wave Energy Converter (WEC)

    DEFF Research Database (Denmark)

    Andersen, Morten Thøtt; Thomsen, Jonas Bjerg

    This report describes the behavior and preliminary performance of a simplified standard oscillating water column (OWC) wave energy converter (WEC). The same tests will be conducted at different scales at 6 different test facilities and the results obtained will be used for comparison. This project...

  19. Application of column tests and electrical resistivity methods for leachate transport monitoring

    Directory of Open Access Journals (Sweden)

    Wychowaniak Dorota

    2015-09-01

    Full Text Available Development of the human civilization leads to the pollution of environment. One of the contamination which are a real threat to soil and groundwater are leachates from landfills. In this paper the solute transport through soil was considered. For this purpose, the laboratory column tests of chlorides tracer and leachates transport on two soil samples have been carried out. Furthermore, the electrical resistivity method was applied as auxiliary tool to follow the movements of solute through the soil column what allowed to compare between the results obtained with column test method and electrical resistivity measurements. Breakthrough curves obtained by conductivity and resistivity methods represents similar trends which leads to the conclusion about the suitability of electrical resistivity methods for contamination transport monitoring in soil-water systems.

  20. One stacked-column vibration test and analysis for VHTR core

    International Nuclear Information System (INIS)

    Ikushima, Takeshi; Ishizuka, Hiroshi; Ide, Akira; Hayakawa, Hitoshi; Shingai, Kazuteru.

    1978-07-01

    This paper describes experimental results of the vibration test on a single stacked-column and compares them with the analytical results. A 1/2 scale model of the core element of a very high temperature gas-cooled reactor (VHTR) was set on a shaking table. Sinusoidal waves, response time history waves, beat wave and step wave of input acceleration 100 - 900 gal in the frequency of 0.5 to 15 Hz were used to vibrate the table horizontally. Results are as follows: (1) The column has a non-linear resonance and exhibits a hysteresis response with jump points. (2) The column vibration characteristics is similar to that of the finite beams connected with non-linear soft spring. (3) The column resonance frequency decreases with increasing input acceleration. (4) The impact force increases with increasing input acceleration and boundary gap width. (5) Good correlation in vibration behavior of the stacked-column and impact force on the boundary between test and analysis was obtained. (auth.)

  1. Analysis and seismic tests of composite shear walls with CFST columns and steel plate deep beams

    Science.gov (United States)

    Dong, Hongying; Cao, Wanlin; Wu, Haipeng; Zhang, Jianwei; Xu, Fangfang

    2013-12-01

    A composite shear wall concept based on concrete filled steel tube (CFST) columns and steel plate (SP) deep beams is proposed and examined in this study. The new wall is composed of three different energy dissipation elements: CFST columns; SP deep beams; and reinforced concrete (RC) strips. The RC strips are intended to allow the core structural elements — the CFST columns and SP deep beams — to work as a single structure to consume energy. Six specimens of different configurations were tested under cyclic loading. The resulting data are analyzed herein. In addition, numerical simulations of the stress and damage processes for each specimen were carried out, and simulations were completed for a range of location and span-height ratio variations for the SP beams. The simulations show good agreement with the test results. The core structure exhibits a ductile yielding mechanism characteristic of strong column-weak beam structures, hysteretic curves are plump and the composite shear wall exhibits several seismic defense lines. The deformation of the shear wall specimens with encased CFST column and SP deep beam design appears to be closer to that of entire shear walls. Establishing optimal design parameters for the configuration of SP deep beams is pivotal to the best seismic behavior of the wall. The new composite shear wall is therefore suitable for use in the seismic design of building structures.

  2. Reproducibility of up-flow column percolation tests for contaminated soils.

    Directory of Open Access Journals (Sweden)

    Tetsuo Yasutaka

    Full Text Available Up-flow column percolation tests are used at laboratory scale to assess the leaching behavior of hazardous substance from contaminated soils in a specific condition as a function of time. Monitoring the quality of these test results inter or within laboratory is crucial, especially if used for Environment-related legal policy or for routine testing purposes. We tested three different sandy loam type soils (Soils I, II and III to determine the reproducibility (variability inter laboratory of test results and to evaluate the difference in the test results within laboratory. Up-flow column percolation tests were performed following the procedure described in the ISO/TS 21268-3. This procedure consists of percolating solution (calcium chloride 1 mM from bottom to top at a flow rate of 12 mL/h through softly compacted soil contained in a column of 5 cm diameter and 30 ± 5 cm height. Eluate samples were collected at liquid-to-solid ratio of 0.1, 0.2, 0.5, 1, 2, 5 and 10 L/kg and analyzed for quantification of the target elements (Cu, As, Se, Cl, Ca, F, Mg, DOC and B in this research. For Soil I, 17 institutions in Japan joined this validation test. The up-flow column experiments were conducted in duplicate, after 48 h of equilibration time and at a flow rate of 12 mL/h. Column percolation test results from Soils II and III were used to evaluate the difference in test results from the experiments conducted in duplicate in a single laboratory, after 16 h of equilibration time and at a flow rate of 36 mL/h. Overall results showed good reproducibility (expressed in terms of the coefficient of variation, CV, calculated by dividing the standard deviation by the mean, as the CV was lower than 30% in more than 90% of the test results associated with Soil I. Moreover, low variability (expressed in terms of difference between the two test results divided by the mean was observed in the test results related to Soils II and III, with a variability lower than 30

  3. A simple subcritical chromatographic test for an extended ODS high performance liquid chromatography column classification.

    Science.gov (United States)

    Lesellier, Eric; Tchapla, Alain

    2005-12-23

    This paper describes a new test designed in subcritical fluid chromatography (SFC) to compare the commercial C18 stationary phase properties. This test provides, from a single analysis of carotenoid pigments, the absolute hydrophobicity, the silanol activity and the steric separation factor of the ODS stationary phases. Both the choice of the analytical conditions and the validation of the information obtained from the chromatographic measurements are detailed. Correlations of the carotenoid test results with results obtained from other tests (Tanaka, Engelhard, Sander and Wise) performed both in SFC and HPLC are discussed. Two separation factors, calculated from the retention of carotenoid pigments used as probe, allowed to draw a first classification diagram. Columns, which present identical chromatographic behaviors are located in the same area on this diagram. This location can be related to the stationary phase properties: endcapping treatments, bonding density, linkage functionality, specific area or silica pore diameter. From the first classification, eight groups of columns are distinguished. One group of polymer coated silica, three groups of polymeric octadecyl phases, depending on the pore size and the endcapping treatment, and four groups of monomeric stationary phases. An additional classification of the four monomeric groups allows the comparison of these stationary phases inside each group by using the total hydrophobicity. One hundred and twenty-nine columns were analysed by this simple and rapid test, which allows a comparison of columns with the aim of helping along their choice in HPLC.

  4. Laboratory-Scale SuperLig 639 Column Tests With Hanford Waste Simulants

    International Nuclear Information System (INIS)

    King, William D.; Spencer, William A.; Bussey, Myra Pettis

    2003-01-01

    This report describes the results of SuperLig 639 column tests conducted at the Savannah River Technology Center (SRTC) in support of the Hanford River Protection Project - Waste Treatment Plant (RPP-WTP). The RPP-WTP contract was awarded to Bechtel National Inc. (BNI) for the design, construction, and initial operation of a plant for the treatment and vitrification of millions of gallons of radioactive waste currently stored in tanks at Hanford, WA. Part of the current treatment process involves the removal of technetium from tank supernate solutions using columns containing SuperLig 639 resin. This report is part of a body of work intended to quantify and optimize the operation of the technetium removal columns with regard to various parameters (such as liquid flow rate, column aspect ratio, resin particle size, loading and elution temperature, etc.). The tests were conducted using nonradioactive simulants of the actual tank waste samples containing rhenium as a surrogate for the technetium in the actual waste. A previous report focused on the impacts of liquid flow rate and column aspect ratio upon performance. More recent studies have focused on the impacts of resin particle size, solution composition, and temperature. This report describes column loading experiments conducted varying temperature and solution composition. Each loading experiment was followed by high temperature elution of the sorbed rhenium. Results from limited testing are also described which were intended to evaluate the physical stability of SuperLig 639 resin during exposure to repeated temperature cycles covering the range of potential processing extremes

  5. Comparing Repaired and Undamaged Specimens Test Results of Post-Tensioned Beam to Column Connections

    OpenAIRE

    Mustafa Kaya

    2015-01-01

    Since, it is essential to provide homeless people by the earthquake with safe, habitable accommodation repairing medium and slight levels of damage at the connection parts should be undertaken. In order to prove that a repaired connection was sufficiently strong, a precast beam to column post tensioned connection was tested in three phases. In phase one, the middle level damage was observed at 6% drift at these connections. As a result of the extra loads applied, little d...

  6. Safety Evaluation for Packaging for onsite Transfer of plutonium recycle test reactor ion exchange columns

    International Nuclear Information System (INIS)

    Smith, R.J.

    1995-01-01

    The purpose of this Safety Evaluation for Packaging (SEP) is to authorize the use of three U.S. Department of Transportation (DOT) 7A, Type A metal boxes (Capital Industries Part No. S 0600-0600-1080- 0104) to package 12 Plutonium Recycle Test Reactor (PRTR) ion exchange columns as low-level waste (LLW). The packages will be transferred from the 309 Building in the 300 Area to low level waste burial in the 200 West Area. Revision 1 of WHC-SD-TP-SEP-035 (per ECN No. 621467) documents that the boxes containing ion exchange columns and grout will maintain the payload under normal conditions of transport if transferred without the box lids

  7. Technetium removal column flow testing with alkaline, high salt, radioactive tank waste

    International Nuclear Information System (INIS)

    Blanchard, D.L. Jr.; Kurath, D.E.; Golcar, G.R.; Conradson, S.D.

    1996-01-01

    This report describes two bench-scale column tests conducted to demonstrate the removal of Tc-99 from actual alkaline high salt radioactive waste. The waste used as feed for these tests was obtained from the Hanford double shell tank AW-101, which contains double shell slurry feed (DSSF). The tank sample was diluted to approximately 5 M Na with water, and most of the Cs-137 was removed using crystalline silicotitanates. The tests were conducted with two small columns connected in series, containing, 10 mL of either a sorbent, ABEC 5000 (Eichrom Industries, Inc.), or an anion exchanger Reillex trademark-HPQ (Reilly Industries, Inc.). Both materials are selective for pertechnetate anion (TcO 4 - ). The process steps generally followed those expected in a full-scale process and included (1) resin conditioning, (2) loading, (3) caustic wash to remove residual feed and prevent the precipitation of Al(OH) 3 , and (4) elution. A small amount of Tc-99m tracer was added as ammonium pertechnetate to the feed and a portable GEA counter was used to closely monitor the process. Analyses of the Tc-99 in the waste was performed using ICP-MS with spot checks using radiochemical analysis. Technetium x-ray absorption spectroscopy (XAS) spectra of 6 samples were also collected to determine the prevalence of non-pertechnetate species [e.g. Tc(IV)

  8. Evaluation of bioleaching column test of sulphide copper ore and copper concentrate using preconditioned surface

    Directory of Open Access Journals (Sweden)

    Videla Leiva Alvaro

    2016-01-01

    Full Text Available Bacterial activity can be related to the presence of Fe+3 in the solution, which drives copper oxidation during the secondary copper low grade sulfide ore leaching process. The present work evaluates improvements in kinetics of leaching when ferroxidans are preconditioned in an inert surface helping to build a biofilm which improves metabolism of the colony. The present work shows evaluation using laboratory columns to perform bioleaching during a 30 days period under three conditions: a base column with no inert surface, a column with loofa available for bacterial growth and conditioning, and finally a column with the loofa surface ground and distributed in the column among the particles.

  9. Mobility of heavy metals through granitic soils using mini column infiltration test

    Science.gov (United States)

    Zarime, Nur'Aishah; Yaacob, W. Z. W.

    2014-09-01

    This study is about the mobility of cadmium through compacted granitic soils. Two granitic soils namely the Broga (BGR) and Kajang (KGR) granitic soils were collected in Selangor, Malaysia. Physical and chemical tests were applied for both granitic soils to determine the physical and chemical properties of soil materials. Physical test results shows granitic soils (BGR and KGR) have high percentage of sand ranging between 54%-63% and 46%-54% respectively, an intermediate and intermediate to high plasticity index as well as high specific gravity ie; 2.50-2.59 and 2.45-2.66 respectively. For chemical test, granitic soils shows acidic pH values ranged from 5.35-5.85 for BGR and pH 5.32-5.54 for KGR. For organic matter, SSA and CEC test, it shows low values ranged from 0.22%-0.34% and 0.39%- 0.50% respectively for organic matter test, 17.96 m2/g-21.93 m2/g and 25.76 m2/g-26.83 m2/g respectively for SSA test and 0.79 meq/100g-1.35 meq/100g and 1.31 meq/100g-1.35 meq/100g respectively for CEC test. Mini column infiltration test was conducted to determine the retention of cadmium while flowing through granite soils. This test conducted based on the falling head permeability concepts. Different G-force ranging from 231G to 1442G was used in this test. The breakthrough curves show the concentration of Cd becomes higher with the increasing of G-force for both granitic samples (BGR and KGR). The selectivity sorption for both granites ranked in the following decreasing order of; 231G>519G>923G>1442G. Results demonstrated that granitic soils also have low buffering capacity due to low resist of pH changes.

  10. Radiation hardness tests of double-sided 3D strip sensors with passing-through columns

    Energy Technology Data Exchange (ETDEWEB)

    Dalla Betta, Gian-Franco, E-mail: gianfranco.dallabetta@unitn.it [Dipartimento di Ingegneria Industriale, Università degli Studi di Trento, Via Sommarive 9, I-38123 Trento (Italy); INFN TIFPA, Via Sommarive 14, I-38123 Trento (Italy); Betancourt, Christopher [Institute of Physics, University of Freiburg, Hermann-Herder-Str. 3, 79104 Freiburg (Germany); Boscardin, Maurizio; Giacomini, Gabriele [Fondazione Bruno Kessler, Centro per i Materiali e i Microsistemi (FBK-CMM), Via Sommarive 18, I-38123 Trento (Italy); Jakobs, Karl; Kühn, Susanne [Institute of Physics, University of Freiburg, Hermann-Herder-Str. 3, 79104 Freiburg (Germany); Lecini, Besnik [Dipartimento di Ingegneria Industriale, Università degli Studi di Trento, Via Sommarive 9, I-38123 Trento (Italy); Mendicino, Roberto [Dipartimento di Ingegneria Industriale, Università degli Studi di Trento, Via Sommarive 9, I-38123 Trento (Italy); INFN TIFPA, Via Sommarive 14, I-38123 Trento (Italy); Mori, Riccardo; Parzefall, Ulrich [Institute of Physics, University of Freiburg, Hermann-Herder-Str. 3, 79104 Freiburg (Germany); Povoli, Marco [Dipartimento di Ingegneria Industriale, Università degli Studi di Trento, Via Sommarive 9, I-38123 Trento (Italy); Thomas, Maira [Institute of Physics, University of Freiburg, Hermann-Herder-Str. 3, 79104 Freiburg (Germany); Zorzi, Nicola [Fondazione Bruno Kessler, Centro per i Materiali e i Microsistemi (FBK-CMM), Via Sommarive 18, I-38123 Trento (Italy)

    2014-11-21

    This paper deals with a radiation hardness study performed on double-sided 3D strip sensors with passing-through columns. Selected results from the characterization of the irradiated sensors with a beta source and a laser setup are reported and compared to pre-irradiation results and to TCAD simulations. The sensor performance in terms of signal efficiency is found to be in good agreement with that of other 3D sensors irradiated at the same fluences and tested under similar experimental conditions. - Highlights: • We report results from 3D silicon strip detectors irradiated up to HL-LHC fluences. • I–V curves, noise, charge collection measurements and laser scans are shown. • In all sensors, signals are distinguished from the noise already at low voltage. • Signal efficiency is in agreement with values expected from the electrode geometry. • Efficiency and spatial uniformity would benefit from higher operation voltages.

  11. Radiation hardness tests of double-sided 3D strip sensors with passing-through columns

    International Nuclear Information System (INIS)

    Dalla Betta, Gian-Franco; Betancourt, Christopher; Boscardin, Maurizio; Giacomini, Gabriele; Jakobs, Karl; Kühn, Susanne; Lecini, Besnik; Mendicino, Roberto; Mori, Riccardo; Parzefall, Ulrich; Povoli, Marco; Thomas, Maira; Zorzi, Nicola

    2014-01-01

    This paper deals with a radiation hardness study performed on double-sided 3D strip sensors with passing-through columns. Selected results from the characterization of the irradiated sensors with a beta source and a laser setup are reported and compared to pre-irradiation results and to TCAD simulations. The sensor performance in terms of signal efficiency is found to be in good agreement with that of other 3D sensors irradiated at the same fluences and tested under similar experimental conditions. - Highlights: • We report results from 3D silicon strip detectors irradiated up to HL-LHC fluences. • I–V curves, noise, charge collection measurements and laser scans are shown. • In all sensors, signals are distinguished from the noise already at low voltage. • Signal efficiency is in agreement with values expected from the electrode geometry. • Efficiency and spatial uniformity would benefit from higher operation voltages

  12. A Low-Cost Automated Test Column to Estimate Soil Hydraulic Characteristics in Unsaturated Porous Media

    Directory of Open Access Journals (Sweden)

    J. Salas-García

    2017-01-01

    Full Text Available The estimation of soil hydraulic properties in the vadose zone has some issues, such as accuracy, acquisition time, and cost. In this study, an inexpensive automated test column (ATC was developed to characterize water flow in a homogeneous unsaturated porous medium by the simultaneous estimation of three hydraulic state variables: water content, matric potential, and water flow rates. The ATC includes five electrical resistance probes, two minitensiometers, and a drop counter, which were tested with infiltration tests using the Hydrus-1D model. The results show that calibrations of electrical resistance probes reasonably match with similar studies, and the maximum error of calibration of the tensiometers was 4.6% with respect to the full range. Data measured by the drop counter installed in the ATC exhibited a high consistency with the electrical resistance probes, which provides an independent verification of the model and indicates an evaluation of the water mass balance. The study results show good performance of the model against the infiltration tests, which suggests a robustness of the methodology developed in this study. An extension to the applicability of this system could be successfully used in low-budget projects in large-scale field experiments, which may be correlated with resistivity changes.

  13. Mobility of heavy metals through granitic soils using mini column infiltration test

    International Nuclear Information System (INIS)

    Zarime, Nur 'Aishah; Yaacob, W. Z.W.

    2014-01-01

    This study is about the mobility of cadmium through compacted granitic soils. Two granitic soils namely the Broga (BGR) and Kajang (KGR) granitic soils were collected in Selangor, Malaysia. Physical and chemical tests were applied for both granitic soils to determine the physical and chemical properties of soil materials. Physical test results shows granitic soils (BGR and KGR) have high percentage of sand ranging between 54%–63% and 46%–54% respectively, an intermediate and intermediate to high plasticity index as well as high specific gravity ie; 2.50–2.59 and 2.45–2.66 respectively. For chemical test, granitic soils shows acidic pH values ranged from 5.35–5.85 for BGR and pH 5.32–5.54 for KGR. For organic matter, SSA and CEC test, it shows low values ranged from 0.22%–0.34% and 0.39%– 0.50% respectively for organic matter test, 17.96 m 2 /g–21.93 m 2 /g and 25.76 m 2 /g–26.83 m 2 /g respectively for SSA test and 0.79 meq/100g–1.35 meq/100g and 1.31 meq/100g–1.35 meq/100g respectively for CEC test. Mini column infiltration test was conducted to determine the retention of cadmium while flowing through granite soils. This test conducted based on the falling head permeability concepts. Different G-force ranging from 231G to 1442G was used in this test. The breakthrough curves show the concentration of Cd becomes higher with the increasing of G-force for both granitic samples (BGR and KGR). The selectivity sorption for both granites ranked in the following decreasing order of; 231G>519G>923G>1442G. Results demonstrated that granitic soils also have low buffering capacity due to low resist of pH changes

  14. Axial Compression Tests on Corroded Reinforced Concrete Columns Consolidated with Fibre Reinforced Polymers

    Directory of Open Access Journals (Sweden)

    Bin Ding

    2017-06-01

    Full Text Available Reinforced concrete structure featured by strong bearing capacity, high rigidity, good integrity, good fire resistance, and extensive applicability occupies a mainstream position in contemporary architecture. However, with the development of social economy, people need higher requirements on architectural structure; durability, especially, has been extensively researched. Because of the higher requirement on building material, ordinary reinforced concrete structure has not been able to satisfy the demand. As a result, some new materials and structures have emerged, for example, fibre reinforced polymers. Compared to steel reinforcement, fibre reinforced polymers have many advantages, such as high tensile strength, good durability, good shock absorption, low weight, and simple construction. The application of fibre reinforced polymers in architectural structure can effectively improve the durability of the concrete structure and lower the maintenance, reinforcement, and construction costs in severe environments. Based on the concepts of steel tube concrete, fibre reinforced composite material confined concrete, and fibre reinforced composite material tubed concrete, this study proposes a novel composite structure, i.e., fibre reinforced composite material and steel tube concrete composite structure. The structure was developed by pasting fibre around steel tube concrete and restraining core concrete using fibre reinforced composite material and steel tubes. The bearing capacity and ultimate deformation capacity of the structure was tested using column axial compression test.

  15. Laboratory-Scale Column Testing Using IONSIV IE-911 for Removing Cesium from Acidic Tank Waste Simulant. 2: Determination of Cesium Exchange Capacity and Effective Mass Transfer Coefficient from a 500-cm3 Column Experiment

    International Nuclear Information System (INIS)

    T.J. Tranter; R.D. Tillotson; T.A. Todd

    2005-01-01

    A semi-scale column test was performed using a commercial form of crystalline silicotitanate (CST) for removing radio-cesium from a surrogate acidic tank solution, which represents liquid waste stored at the Idaho National Engineering and Environmental Laboratory (INEEL). The engineered form of CST ion exchanger, known as IONSIVtmIE-911 (UOP, Mt. Laurel, NJ, USA), was tested in a 500-cm3 column to obtain a cesium breakthrough curve. The cesium exchange capacity of this column matched that obtained from previous testing with a 15-mc3 column. A numerical algorithm using implicit finite difference approximations was developed to solve the governing mass transport equations for the CST columns. An effective mass transfer coefficient was derived from solving these equations for previously reported 15 cm3 tests. The effective mass transfer coefficient was then used to predict the cesium breakthrough curve for the 500-cm3 column and compared to the experimental data reported in this paper. The calculated breakthrough curve showed excellent agreement with the data from the 500-cm3 column even though the interstitial velocity was a factor of two greater. Thus, this approach should provide a reasonable method for scale up to larger columns for treating actual tank waste

  16. Developing and Validating a Rapid Small-Scale Column Test Procedure for GAC Selection using Reconstituted Lyophilized NOM

    Science.gov (United States)

    Cost effective design and operation of Granular Activated Carbon (GAC) facilities requires the selection of GAC that is optimal for a specific site. Rapid small-scale column tests (RSSCTs) are widely used for GAC assessment due to several advantages, including the ability to simu...

  17. ROLE OF IRON (II, III) HYDROXYCARBONATE GREEN RUST IN ARSENIC REMEDIATION USING ZEROVALENT IRON IN COLUMN TESTS

    Science.gov (United States)

    We examined corrosion products of zerovalent iron (Peerless iron) that was used in three column tests for removing arsenic under dynamic flow conditions with and without added phosphate and silicate. Iron(II, III) hydroxycarbonate and magnetite were major iron corrosion products...

  18. PILOT SCALE TESTING OF MONOSODIUM TITANATE MIXING FOR THE SRS SMALL COLUMN ION EXCHANGE PROCESS - 11224

    Energy Technology Data Exchange (ETDEWEB)

    Poirier, M.; Restivo, M.; Williams, M.; Herman, D.; Steeper, T.

    2011-01-25

    The Small Column Ion Exchange (SCIX) process is being developed to remove cesium, strontium, and select actinides from Savannah River Site (SRS) Liquid Waste using an existing waste tank (i.e., Tank 41H) to house the process. Savannah River National Laboratory (SRNL) is conducting pilot-scale mixing tests to determine the pump requirements for suspending monosodium titanate (MST), crystalline silicotitanate (CST), and simulated sludge. The purpose of this pilot scale testing is to determine the requirements for the pumps to suspend the MST particles so that they can contact the strontium and actinides in the liquid and be removed from the tank. The pilot-scale tank is a 1/10.85 linear scaled model of SRS Tank 41H. The tank diameter, tank liquid level, pump nozzle diameter, pump elevation, and cooling coil diameter are all 1/10.85 of their dimensions in Tank 41H. The pump locations correspond to the proposed locations in Tank 41H by the SCIX program (Risers B5 and B2 for two pump configurations and Risers B5, B3, and B1 for three pump configurations). The conclusions from this work follow: (i) Neither two standard slurry pumps nor two quad volute slurry pumps will provide sufficient power to initially suspend MST in an SRS waste tank. (ii) Two Submersible Mixer Pumps (SMPs) will provide sufficient power to initially suspend MST in an SRS waste tank. However, the testing shows the required pump discharge velocity is close to the maximum discharge velocity of the pump (within 12%). (iii) Three SMPs will provide sufficient power to initially suspend MST in an SRS waste tank. The testing shows the required pump discharge velocity is 66% of the maximum discharge velocity of the pump. (iv) Three SMPs are needed to resuspend MST that has settled in a waste tank at nominal 45 C for four weeks. The testing shows the required pump discharge velocity is 77% of the maximum discharge velocity of the pump. Two SMPs are not sufficient to resuspend MST that settled under these

  19. Characterize Behaviour of Emerging Pollutants in Artificial Recharge: Column Experiments - Experiment Design and Results of Preliminary Tests

    Science.gov (United States)

    Wang, H.; Carrera, J.; Ayora, C.; Licha, T.

    2012-04-01

    Emerging pollutants (EPs) have been detected in water resources as a result of human activities in recent years. They include pharmaceuticals, personal care products, dioxins, flame retardants, etc. They are a source of concern because many of them are resistant to conventional water treatment, and they are harmful to human health, even in low concentrations. Generally, this study aims to characterize the behaviour of emerging pollutants in reclaimed water in column experiments which simulates artificial recharge. One column set includes three parts: influent, reactive layer column (RLC) and aquifer column (AC). The main influent is decided to be Secondary Effluent (SE) of El Prat Wastewater Treatment Plant, Barcelona. The flow rate of the column experiment is 0.9-1.5 mL/min. the residence time of RLC is designed to be about 1 day and 30-40 days for AC. Both columns are made of stainless steel. Reactive layer column (DI 10cm * L55cm) is named after the filling material which is a mixture of organic substrate, clay and goethite. One purpose of the application of the mixture is to increase dissolve organic carbon (DOC). Leaching test in batchs and columns has been done to select proper organic substrate. As a result, compost was selected due to its long lasting of releasing organic matter (OM). The other purpose of the application of the mixture is to enhance adsorption of EPs. Partition coefficients (Kow) of EPs indicate the ability of adsorption to OM. EPs with logKow>2 could be adsorbed to OM, like Ibuprofen, Bezafibrate and Diclofenac. Moreover, some of EPs are charged in the solution with pH=7, according to its acid dissociation constant (Ka). Positively charged EPs, for example Atenolol, could adsorb to clay. In the opposite, negatively charged EPs, for example Gemfibrozil, could adsorb to goethite. Aquifer column (DI 35cm * L1.5m) is to simulate the processes taking place in aquifer in artificial recharge. The filling of AC has two parts: silica sand and

  20. Lighting columns. Research on the behaviour of lighting columns in sideways- on and head-on impact tests with private cars.

    NARCIS (Netherlands)

    1978-01-01

    Lighting columns can be made more safe by providing them with a sliding construction. This construction makes it possible that the column slides from his ground construction in case of an accident. Aluminium lighting can be constructed in such a way that the break off in case of a car collides

  1. Calculating carbon mass balance from unsaturated soil columns treated with CaSO₄₋minerals: test of soil carbon sequestration.

    Science.gov (United States)

    Han, Young-Soo; Tokunaga, Tetsu K

    2014-12-01

    Renewed interest in managing C balance in soils is motivated by increasing atmospheric concentrations of CO2 and consequent climate change. Here, experiments were conducted in soil columns to determine C mass balances with and without addition of CaSO4-minerals (anhydrite and gypsum), which were hypothesized to promote soil organic carbon (SOC) retention and soil inorganic carbon (SIC) precipitation as calcite under slightly alkaline conditions. Changes in C contents in three phases (gas, liquid and solid) were measured in unsaturated soil columns tested for one year and comprehensive C mass balances were determined. The tested soil columns had no C inputs, and only C utilization by microbial activity and C transformations were assumed in the C chemistry. The measurements showed that changes in C inventories occurred through two processes, SOC loss and SIC gain. However, the measured SOC losses in the treated columns were lower than their corresponding control columns, indicating that the amendments promoted SOC retention. The SOC losses resulted mostly from microbial respiration and loss of CO2 to the atmosphere rather than from chemical leaching. Microbial oxidation of SOC appears to have been suppressed by increased Ca(2+) and SO4(2)(-) from dissolution of CaSO4 minerals. For the conditions tested, SIC accumulation per m(2) soil area under CaSO4-treatment ranged from 130 to 260 g C m(-1) infiltrated water (20-120 g C m(-1) infiltrated water as net C benefit). These results demonstrate the potential for increasing C sequestration in slightly alkaline soils via CaSO4-treatment. Copyright © 2014 Elsevier Ltd. All rights reserved.

  2. Construction and demolition waste: Comparison of standard up-flow column and down-flow lysimeter leaching tests.

    Science.gov (United States)

    Butera, Stefania; Hyks, Jiri; Christensen, Thomas H; Astrup, Thomas F

    2015-09-01

    Five samples of construction and demolition waste (C&DW) were investigated in order to quantify leaching of inorganic elements under percolation conditions according to two different experimental setups: standardised up-flow saturated columns (<4mm particle size) and unsaturated, intermittent down-flow lysimeters (<40mm particle size). While standardised column tests are meant primarily to provide basic information on characteristic leaching properties and mechanisms and not to reproduce field conditions, the lysimeters were intended to mimic the actual leaching conditions when C&DW is used in unbound geotechnical layers. In practice, results from standardised percolation tests are often interpreted as estimations of actual release from solid materials in percolation scenarios. In general, the two tests yielded fairly similar results in terms of cumulative release at liquid-to-solid ratio (L/S) 10l·kgTS; however, significant differences were observed for P, Pb, Ba, Mg and Zn. Further differences emerged in terms of concentration in the early eluates (L/S<5l·kg(-1)TS) for Al, As, Ba, Cd, Cu, DOC, Mg, Mn, Ni, P, Pb, Sb, Se, Si, Zn. Observed differences between tests are likely to be due to differences in pH related to crushing and exposure of fresh particle surfaces, as well as in equilibrium conditions. In the case of C&DW, the standardised column tests, which are more practical, are considered to acceptably describe cumulative releases at L/S 10l·kg(-1)TS in percolation scenarios. However, when the focus is on estimation of initial concentrations for (for example) risk assessment, data from standardised column tests may not be fully applicable, and data from lysimeters may be used for validation purposes. Se, Cr and, to a lesser extent, SO4 and Sb were leaching from C&DW in critical amounts compared with existing limit values. Copyright © 2015 Elsevier Ltd. All rights reserved.

  3. Evaluation of pharmaceuticals removal by sewage sludge-derived adsorbents with rapid small-scale column tests

    Science.gov (United States)

    Zhang, P.; Ding, R.; Wallace, R.; Bandosz, T.

    2015-12-01

    New composite adsorbents were developed by pyrolyzing sewage sludge and fish waste (75:25 or 90:10 dry mass ratio) at 650 oC and 950 oC. Batch adsorption experiments demonstrated that the composite adsorbents were able to adsorb a wide range of organic contaminants (volatile organic compounds, pharmaceuticals and endocrine disrupting compounds (EDCs), and nitrosamine disinfection byproducts) with high capacities. Here we further examine the performance of the adsorbents for the simultaneous removal of 8 pharmaceuticals and EDCs with rapid small-scale column tests (RSSCT). Results show that the order of breakthrough in RSSCT is in general consistent with the affinity determined via batch tests. As expected, the maximum amount of adsorption for each compound obtained from RSSCT is identical to or less than that obtained from batch tests (with only one exception), due to adsorption kinetics. However, despite the very different input concentration (1 mg/L vs. 100 mg/L) and contact time (2 min empty bed contact time vs. 16 hour equilibrium time) used in RSSCT and batch tests, the maximum amount of pharmaceuticals and EDCs adsorbed under RSSCT is still about one half of that under equilibrium batch tests, validating the approach of using batch tests with much higher input concentrations to determine adsorption capacities. Results of a pilot-scale column test in a drinking water treatment plant for pharmaceuticals removal will also be presented.

  4. Small Column Ion Exchange

    International Nuclear Information System (INIS)

    Huff, Thomas

    2010-01-01

    Small Column Ion Exchange (SCIX) leverages a suite of technologies developed by DOE across the complex to achieve lifecycle savings. Technologies are applicable to multiple sites. Early testing supported multiple sites. Balance of SRS SCIX testing supports SRS deployment. A forma Systems Engineering Evaluation (SEE) was performed and selected Small Column Ion Exchange columns containing Crystalline Silicotitanate (CST) in a 2-column lead/lag configuration. SEE considered use of Spherical Resorcinol-Formaldehyde (sRF). Advantages of approach at SRS include: (1) no new buildings, (2) low volume of Cs waste in solid form compared to aqueous strip effluent; and availability of downstream processing facilities for immediate processing of spent resin.

  5. Ranking nano-enabled hybrid media for simultaneous removal of contaminants with different chemistries: Pseudo-equilibrium sorption tests versus column tests.

    Science.gov (United States)

    Custodio, Tomas; Garcia, Jose; Markovski, Jasmina; McKay Gifford, James; Hristovski, Kiril D; Olson, Larry W

    2017-12-15

    The underlying hypothesis of this study was that pseudo-equilibrium and column testing conditions would provide the same sorbent ranking trends although the values of sorbents' performance descriptors (e.g. sorption capacity) may vary because of different kinetics and competition effects induced by the two testing approaches. To address this hypothesis, nano-enabled hybrid media were fabricated and its removal performances were assessed for two model contaminants under multi-point batch pseudo-equilibrium and continuous-flow conditions. Calculation of simultaneous removal capacity indices (SRC) demonstrated that the more resource demanding continuous-flow tests are able to generate the same performance rankings as the ones obtained by conducing the simpler pseudo-equilibrium tests. Furthermore, continuous overlap between the 98% confidence boundaries for each SRC index trend, not only validated the hypothesis that both testing conditions provide the same ranking trends, but also pointed that SRC indices are statistically the same for each media, regardless of employed method. In scenarios where rapid screening of new media is required to obtain the best performing synthesis formulation, use of pseudo-equilibrium tests proved to be reliable. Considering that kinetics induced effects on sorption capacity must not be neglected, more resource demanding column test could be conducted only with the top performing media that exhibit the highest sorption capacity. Copyright © 2017 Elsevier B.V. All rights reserved.

  6. Development of a Long-Column Method to Test Constitutive Relations for LNAPL Movement in Two-Phase Systems

    Science.gov (United States)

    Oostrom, M.; Zhong, L.; Wietsma, T.; Covert, M.

    2007-12-01

    Multifluid relative permeability - saturation - capillary pressure (k-S-P) empirical constitutive models are components of numerical simulators that are used to predict fluid distributions following a nonaqueous phase liquid (NAPL) contamination event or during remediation. The S-P parameter values for these empirical models are either obtained from the literature or determined experimentally by fitting the models to measured data. Most of the experimental emphasis so far has been on testing the S-P component of the k-S-P constitutive relations. Due to the difficulties in obtaining quality relative permeability laboratory data for multiphase systems, testing of the k-S models that are used in multifluid flow simulators has been virtually non-existent. A new tool, the Multiple Location Saturation Pressure Apparatus (MLSPA), located in PNNL's EMSL Subsurface Flow and Transport Laboratory, has been developed to obtain data sets that can be used to test both S-P and k-S relationships for two-phase NAPL-water systems. The MLSPA is a long column (~1 m) equipped with several hydrophilic and hydrophobic pressure transducers. Fluid saturations are determined along the length of a column using a dual-energy gamma radiation system. Although the MLSPA is limited to porous media with a relatively small entry pressure and fairly homogeneous pore-size distributions, it offers the distinct advantage of obtaining S-P data at multiple locations. Besides for static determinations of S-P relations, the MLSPA offers the benefit that it can be used for more dynamic experiments where fluid pressures are changed more rapidly. The data sets produced by the dynamic experiments can be used in relative permeability models. Results of several experiments with crude-oil brine systems will be presented.

  7. The potential of compost-based biobarriers for Cr(VI) removal from contaminated groundwater: Column test

    International Nuclear Information System (INIS)

    Boni, Maria Rosaria; Sbaffoni, Silvia

    2009-01-01

    This paper presents the results of a column reactor test, aiming at evaluating the performance of a biological permeable barrier made of low-cost waste materials, for Cr(VI) removal from contaminated groundwater. A 1:1 by volume mixture of green compost and siliceous gravel was tested as reactive medium in the experimental activity. A 10 mg/l Cr(VI) contaminated solution was used and the residual Cr(VI) concentration along the column height and in the outlet was determined in the water samples collected daily. Also pH, redox potential and COD were analyzed. At the end of the test, the reactive medium was characterized in terms of Cr(VI) and total chromium. The Cr(VI) removal efficiency was higher than 99% during the entire experimental activity. The influence of the biological activity on Cr(VI) removal efficiency was evaluated by varying the organic carbon and nitrogen dosages in the contaminated solution fed to the system; a removal decrease was observed when the organic carbon was not enough to sustain the microbial metabolism. The Cr(VI) removal was strictly linked to the biological activity of the native biomass of compost. No Cr(III) was detected in the outlet: the Cr(III) produced was entrapped in the solid matrix. Two main processes involved were: adsorption on the organic-based matrix and reduction into Cr(III) mediated by the anaerobic microbial metabolism of the bacteria residing in green compost. Siliceous gravel was used as the structure matrix, since its contribution to the removal was almost negligible. Thanks to the proven efficiency and to the low-cost, the reactive medium used can represent a valid alternative to conventional approaches to chromium remediation.

  8. Laboratory-Scale Column Testing Using IONSIV IE-911 for Removing Cesium from Acidic Tank Waste Simulant. 1: Cesium Exchange Capacity of a 15-cm3 Column and Dynamic Stability of the Exchange Media

    International Nuclear Information System (INIS)

    T.J. Tranter; R.D. Tillotson; T.A. Todd

    2005-01-01

    Bench-scale column tests were performed using a commercial form of crystalline silicotitanate (CST) for removing radio-cesium from a surrogate acidic tank solution representative of liquid waste stored at the Idaho National Engineering and Environmental Laboratory (INEEL). An engineered form of CST ion exchanger, known as IONSIVtm IE-911 (UOP, Mt Laurel, NJ, USA), was tested in 15 cm3 columns at a flow rate of 5 bed volumes per hour. These experiments showed the ion exchange material to have reasonable selectivity and capacity for removing cesium from the complex chemical matrix of the solution. However, previous testing indicated that partial neutralization of the feed stream was necessary to increase the stability of the ion exchange media. Thus, in these studies, CST degradation was determined as a function of throughput in order to better assess the stability characteristics of the exchanger for potential future waste treatment applications. Results of these tests indicate that the degradation of the CST reaches a maximum very soon after the acidic feed is introduced to the column and then rapidly declines. Total dissolution of bed material did not exceed 3% under the experimental regime used

  9. Simplified mathematical models for interpreting the results of tests carried out by labelling the whole piezometric column in water wells

    International Nuclear Information System (INIS)

    Munera, H.A.

    1974-01-01

    Approximate methods used to interpret the results of tests based on radioactive tracer dilution in a single water well by labelling the whole piezometric column are described; these simple mathematical models have been used to obtain semi-quantitative data on the apparent velocity (horizontal) in non-homogeneous aquifers with flow rates of metres daily. Measurements have also been made in a homogeneous aquifer with velocities of centimetres daily. Interpretation is based on determination of the average concentration for the various well zones; this involves recognition of a mean velocity for each region. All the tracer dilution effects that are not due to horizontal or vertical flow between two zones, i.e. convection, artificial mixing, diffusion and so on, are grouped together as a single term, which is taken arbitrarily to be proportional to the difference in concentration between the regions under consideration; its value is obtained from the experimental dilution curve. The model was applied to the solution of the three cases encountered most frequently during our measurements in Colombia: (a) when the well penetrates a permeable zone and adjacent impermeable zone; (b) when the well penetrates a permeable zone contained between impermeable regions; and (c) when the well traverses an aquifer with two adjacent zones of different permeability contained between impermeable zones. The shape of the dilution curve (logarithm of concentration versus time, usually with two or more slopes) is predicted by the model, the approximate nature of which is consistent with the fact that the method of labelling the whole piezometric column is semi-quantitative. The results obtained for measurements made when there are considerable vertical flows are apparently correct, but there is no other experimental measurement available to confirm them. (author) [es

  10. Rapid small-scale column testing of granular activated carbon for organic micro-pollutant removal in treated domestic wastewater.

    Science.gov (United States)

    Zietzschmann, F; Müller, J; Sperlich, A; Ruhl, A S; Meinel, F; Altmann, J; Jekel, M

    2014-01-01

    This study investigates the applicability of the rapid small-scale column test (RSSCT) concept for testing of granular activated carbon (GAC) for organic micro-pollutants (OMPs) removal from wastewater treatment plant (WWTP) effluent. The chosen experimental setup was checked using pure water, WWTP effluent, different GAC products, and variable hydrodynamic conditions with different flow velocities and differently sized GAC, as well as different empty bed contact times (EBCTs). The setup results in satisfying reproducibility and robustness. RSSCTs in combination with WWTP effluent are effective when comparing the OMP removal potentials of different GAC products and are a useful tool for the estimation of larger filters. Due to the potentially high competition between OMPs and bulk organics, breakthrough curves are likely to have unfavorable shapes when treating WWTP effluent. This effect can be counteracted by extending the EBCT. With respect to the strong competition observed in GAC treatment of WWTP effluent, the small organic acid and neutral substances are retained longer in the RSSCT filters and are likely to cause the majority of the observed adsorption competition with OMPs.

  11. Impact of pre-equilibration and diffusion limited release kinetics on effluent concentration in column leaching tests: Insights from numerical simulations.

    Science.gov (United States)

    Finkel, Michael; Grathwohl, Peter

    2017-05-01

    Column leaching tests have become a standard method for assessing leaching of pollutants from materials used, e.g., for road and railway constructions and in landscaping measures. Column tests showed to be practical in laboratories yielding robust and reproducible results. However, considerable uncertainty still exists related particularly to the degree of equilibration of the pore water with the solids during preparation (pre-equilibration) and percolation of the column. We analyse equilibration time scales and sensitivity of concentrations in column leachate with respect to initial conditions in a series of numerical experiments covering a broad spectrum of material and solute properties. Slow release of pollutants from solid materials is described by a spherical diffusion model of kinetic sorption accounting for multiple grain size fractions and sorption capacities. Results show that the cumulative concentrations are rather independent of the pre-equilibration level for a broad spectrum of parameter settings, e.g. if intra-particle porosity is high, grain size is small, or if the sorption coefficient is large. Sensitivity increases with decreasing liquid solid ratios and contact time during percolation. Significant variations with initial column conditions are to be expected for material and compound properties leading to slow release kinetics. In these cases, sensitivity to initial conditions may have to be considered. Copyright © 2016 Elsevier Ltd. All rights reserved.

  12. PULSE COLUMN

    Science.gov (United States)

    Grimmett, E.S.

    1964-01-01

    This patent covers a continuous countercurrent liquidsolids contactor column having a number of contactor states each comprising a perforated plate, a layer of balls, and a downcomer tube; a liquid-pulsing piston; and a solids discharger formed of a conical section at the bottom of the column, and a tubular extension on the lowest downcomer terminating in the conical section. Between the conical section and the downcomer extension is formed a small annular opening, through which solids fall coming through the perforated plate of the lowest contactor stage. This annular opening is small enough that the pressure drop thereacross is greater than the pressure drop upward through the lowest contactor stage. (AEC)

  13. Evaluation of Packed Distillation Columns I - Atmospheric Pressure

    National Research Council Canada - National Science Library

    Reynolds, Thaine

    1951-01-01

    .... Four column-packing combinations of the glass columns and four column-packing combinations of the steel columns were investigated at atmospheric pressure using a test mixture of methylcyclohexane...

  14. Small zeolite column tests for removal of cesium from high radioactive contaminated water in Fukushima Daiichi Nuclear Power Station

    International Nuclear Information System (INIS)

    Hijikata, Takatoshi; Uozumi, Koichi; Tukada, Takeshi; Koyama, Tadafumi; Ishikawa, Keiji; Ono, Shoichi; Suzuki, Shunichi; Denton, Mark; Raymont, John

    2011-01-01

    After the earthquake on March 11th 2011, a large amount (more than 0.12 million m 3 ) of highly radioactive contaminated water had pooled in Fukushima Daiichi nuclear power station. As an urgent issue, highly radioactive nuclides should be removed from this contaminated water to reduce radioactivity in the turbine buildings and nuclear reactor buildings. Removal of Cs from this contaminated water is a key issue, because 134 Cs and 137 Cs are highly radioactive γ-emitting nuclides. The zeolite column system was used for Cs and Sr removal from the radioactive water of Three-Mile Island Unit 2, and modified columns were then developed as a Cs removal method for high-level radioactive water in US national laboratories (WRSC, ORNL, PNNL, Hanford, etc.). In order to treat Fukushima's highly contaminated water with a similar system, it was necessary to understand the properties of zeolite to remove Cs from sea salt as well as the applicability of the column system to a high throughput of around 1200 m 3 /d. The kinetic characteristics of the column were another property to be understood before actual operation. Hence, a functional small-scale zeolite column system was installed in CRIEPI for conducting the experiments to understand decontamination behaviors. Each column has a 2- or 3-cm inner diameter and a 12-cm height, and 12 g of zeolite-type media was packed into the column. The column experiments were carried out with Kurion-zeolite, Herschelite, at different feed rates of simulated water with different concentrations of Cs and sea salt. As for the water with 4 ppm Cs and 0 ppm sea salt, only a 10% Cs concentration was observed in the effluent after 20,000 bed volumes were fed at a rate of 33 cm/min, which corresponds to the actual system. On the other hand, a 40% Cs concentration was observed in the effluent after only 50 bed volumes were passed for water with 2 ppm Cs and 3.4 wt.% sea salt at a feed rate of 34 cm/min. As the absorption of Cs is hampered by the

  15. Distillation Column Flooding Predictor

    Energy Technology Data Exchange (ETDEWEB)

    George E. Dzyacky

    2010-11-23

    /vapor traffic that produce increased contact area and lead to substantial increases in separation efficiency – which translates to a 10% increase in energy efficiency on a BTU/bbl basis. The Flooding Predictor™ operates on the principle that between five to sixty minutes in advance of a flooding event, certain column variables experience an oscillation, a pre-flood pattern. The pattern recognition system of the Flooding Predictor™ utilizes the mathematical first derivative of certain column variables to identify the column’s pre-flood pattern(s). This pattern is a very brief, highly repeatable, simultaneous movement among the derivative values of certain column variables. While all column variables experience negligible random noise generated from the natural frequency of the process, subtle pre-flood patterns are revealed among sub-sets of the derivative values of column variables as the column approaches its hydraulic limit. The sub-set of column variables that comprise the pre-flood pattern is identified empirically through in a two-step process. First, 2ndpoint’s proprietary off-line analysis tool is used to mine historical data for pre-flood patterns. Second, the column is flood-tested to fine-tune the pattern recognition for commissioning. Then the Flooding Predictor™ is implemented as closed-loop advanced control strategy on the plant’s distributed control system (DCS), thus automating control of the column at its hydraulic limit.

  16. Annular pulse column development studies

    International Nuclear Information System (INIS)

    Benedict, G.E.

    1980-01-01

    The capacity of critically safe cylindrical pulse columns limits the size of nuclear fuel solvent extraction plants because of the limited cross-sectional area of plutonium, U-235, or U-233 processing columns. Thus, there is a need to increase the cross-sectional area of these columns. This can be accomplished through the use of a column having an annular cross section. The preliminary testing of a pilot-plant-scale annular column has been completed and is reported herein. The column is made from 152.4-mm (6-in.) glass pipe sections with an 89-mm (3.5-in.) o.d. internal tube, giving an annular width of 32-mm (1.25-in.). Louver plates are used to swirl the column contents to prevent channeling of the phases. The data from this testing indicate that this approach can successfully provide larger-cross-section critically safe pulse columns. While the capacity is only 70% of that of a cylindrical column of similar cross section, the efficiency is almost identical to that of a cylindrical column. No evidence was seen of any non-uniform pulsing action from one side of the column to the other

  17. Construction and demolition waste: Comparison of standard up-flow column and down-flow lysimeter leaching tests

    DEFF Research Database (Denmark)

    Butera, Stefania; Hyks, Jiri; Christensen, Thomas Højlund

    2015-01-01

    Five samples of construction and demolition waste (C&DW) were investigated in order to quantify leaching of inorganic elements under percolation conditions according to two different experimental setups: standardised up-flow saturated columns (-1TS) for Al, As, Ba, Cd, Cu, DOC, Mg, Mn, Ni, P, Pb...

  18. Supercritical Fluid Chromatography of Drugs: Parallel Factor Analysis for Column Testing in a Wide Range of Operational Conditions

    Science.gov (United States)

    Al-Degs, Yahya; Andri, Bertyl; Thiébaut, Didier; Vial, Jérôme

    2017-01-01

    Retention mechanisms involved in supercritical fluid chromatography (SFC) are influenced by interdependent parameters (temperature, pressure, chemistry of the mobile phase, and nature of the stationary phase), a complexity which makes the selection of a proper stationary phase for a given separation a challenging step. For the first time in SFC studies, Parallel Factor Analysis (PARAFAC) was employed to evaluate the chromatographic behavior of eight different stationary phases in a wide range of chromatographic conditions (temperature, pressure, and gradient elution composition). Design of Experiment was used to optimize experiments involving 14 pharmaceutical compounds present in biological and/or environmental samples and with dissimilar physicochemical properties. The results showed the superiority of PARAFAC for the analysis of the three-way (column × drug × condition) data array over unfolding the multiway array to matrices and performing several classical principal component analyses. Thanks to the PARAFAC components, similarity in columns' function, chromatographic trend of drugs, and correlation between separation conditions could be simply depicted: columns were grouped according to their H-bonding forces, while gradient composition was dominating for condition classification. Also, the number of drugs could be efficiently reduced for columns classification as some of them exhibited a similar behavior, as shown by hierarchical clustering based on PARAFAC components. PMID:28695040

  19. Characterization and testing of 30 kV, 60 kW electron optical column for melting applications

    Energy Technology Data Exchange (ETDEWEB)

    Baibhaw, Prakash; Gupta, Sachin; Malik, Pravanjan, E-mail: bprakash@barc.gov.in [Bhabha Atomic Research Centre, Mumbai (India)

    2014-07-01

    High energy electron beams (30-150 keV) are widely used as intense heat source in welding, melting and evaporation of refractory metals. These operations are mostly carried out in high vacuum (10{sup -4}-10{sup -5} mbar) to aid unimpeded flow of electrons from generation to the point of application. A 30 kV, 60 kW Electron beam optical column (EOC) is designed and developed under the high power beam technology programme. The optical column consists of an electron gun and twin electromagnetic focusing lenses. The heating power of emitter, gun perveance, grid voltage control, beam focusing with the twin electromagnetic lenses and beam spot size measurements are reported in this paper. The results are compared with the design values. Operational issues during the high power melting and the strategy for automation of the electron gun are discussed. (author)

  20. Supercritical Fluid Chromatography of Drugs: Parallel Factor Analysis for Column Testing in a Wide Range of Operational Conditions

    Directory of Open Access Journals (Sweden)

    Ramia Z. Al Bakain

    2017-01-01

    Full Text Available Retention mechanisms involved in supercritical fluid chromatography (SFC are influenced by interdependent parameters (temperature, pressure, chemistry of the mobile phase, and nature of the stationary phase, a complexity which makes the selection of a proper stationary phase for a given separation a challenging step. For the first time in SFC studies, Parallel Factor Analysis (PARAFAC was employed to evaluate the chromatographic behavior of eight different stationary phases in a wide range of chromatographic conditions (temperature, pressure, and gradient elution composition. Design of Experiment was used to optimize experiments involving 14 pharmaceutical compounds present in biological and/or environmental samples and with dissimilar physicochemical properties. The results showed the superiority of PARAFAC for the analysis of the three-way (column × drug × condition data array over unfolding the multiway array to matrices and performing several classical principal component analyses. Thanks to the PARAFAC components, similarity in columns’ function, chromatographic trend of drugs, and correlation between separation conditions could be simply depicted: columns were grouped according to their H-bonding forces, while gradient composition was dominating for condition classification. Also, the number of drugs could be efficiently reduced for columns classification as some of them exhibited a similar behavior, as shown by hierarchical clustering based on PARAFAC components.

  1. Evaluation through column leaching tests of metal release from contaminated estuarine sediment subject to CO2 leakages from Carbon Capture and Storage sites

    International Nuclear Information System (INIS)

    Payán, M. Cruz; Galan, Berta; Coz, Alberto; Vandecasteele, Carlo; Viguri, Javier R.

    2012-01-01

    The pH change and the release of organic matter and metals from sediment, due to the potential CO 2 acidified seawater leakages from a CCS (Carbon Capture and Storage) site are presented. Column leaching test is used to simulate a scenario where a flow of acidified seawater is in contact with recent contaminated sediment. The behavior of pH, dissolved organic carbon (DOC) and metals As, Cd, Cr, Cu, Ni, Pb, Zn, with liquid to solid (L/S) ratio and pH is analyzed. A stepwise strategy using empirical expressions and a geochemical model was conducted to fit experimental release concentrations. Despite the neutralization capacity of the seawater-carbonate rich sediment system, important acidification and releases are expected at local scale at lower pH. The obtained results would be relevant as a line of evidence input of CCS risk assessment, in an International context where strategies to mitigate the climate change would be applied. - Highlights: ► Tier structured approach for assessment of the release of metals from sediment. ► Standard column leaching test to simulate CO 2 acidified seawater CCS leakages. ► Metal and DOC release from marine sediment in contact to CO 2 acidified seawater. ► From empirical to geochemical modeling approaches of DOC and metals release in column tests. ► Contamination line of evidence input of CCS risk assessment. - Column metal release from CO 2 acidified seawater leakages in contact with estuarine contaminated sediment in CCS sites

  2. Column-to-column packing variation of disposable pre-packed columns for protein chromatography.

    Science.gov (United States)

    Schweiger, Susanne; Hinterberger, Stephan; Jungbauer, Alois

    2017-12-08

    In the biopharmaceutical industry, pre-packed columns are the standard for process development, but they must be qualified before use in experimental studies to confirm the required performance of the packed bed. Column qualification is commonly done by pulse response experiments and depends highly on the experimental testing conditions. Additionally, the peak analysis method, the variation in the 3D packing structure of the bed, and the measurement precision of the workstation influence the outcome of qualification runs. While a full body of literature on these factors is available for HPLC columns, no comparable studies exist for preparative columns for protein chromatography. We quantified the influence of these parameters for commercially available pre-packed and self-packed columns of disposable and non-disposable design. Pulse response experiments were performed on 105 preparative chromatography columns with volumes of 0.2-20ml. The analyte acetone was studied at six different superficial velocities (30, 60, 100, 150, 250 and 500cm/h). The column-to-column packing variation between disposable pre-packed columns of different diameter-length combinations varied by 10-15%, which was acceptable for the intended use. The column-to-column variation cannot be explained by the packing density, but is interpreted as a difference in particle arrangement in the column. Since it was possible to determine differences in the column-to-column performance, we concluded that the columns were well-packed. The measurement precision of the chromatography workstation was independent of the column volume and was in a range of±0.01ml for the first peak moment and±0.007 ml 2 for the second moment. The measurement precision must be considered for small columns in the range of 2ml or less. The efficiency of disposable pre-packed columns was equal or better than that of self-packed columns. Copyright © 2017 The Author(s). Published by Elsevier B.V. All rights reserved.

  3. An analysis of lethal and sublethal interactions among type I and type II pyrethroid pesticide mixtures using standard Hyalella azteca water column toxicity tests.

    Science.gov (United States)

    Hoffmann, Krista Callinan; Deanovic, Linda; Werner, Inge; Stillway, Marie; Fong, Stephanie; Teh, Swee

    2016-10-01

    A novel 2-tiered analytical approach was used to characterize and quantify interactions between type I and type II pyrethroids in Hyalella azteca using standardized water column toxicity tests. Bifenthrin, permethrin, cyfluthrin, and lambda-cyhalothrin were tested in all possible binary combinations across 6 experiments. All mixtures were analyzed for 4-d lethality, and 2 of the 6 mixtures (permethrin-bifenthrin and permethrin-cyfluthrin) were tested for subchronic 10-d lethality and sublethal effects on swimming motility and growth. Mixtures were initially analyzed for interactions using regression analyses, and subsequently compared with the additive models of concentration addition and independent action to further characterize mixture responses. Negative interactions (antagonistic) were significant in 2 of the 6 mixtures tested, including cyfluthrin-bifenthrin and cyfluthrin-permethrin, but only on the acute 4-d lethality endpoint. In both cases mixture responses fell between the additive models of concentration addition and independent action. All other mixtures were additive across 4-d lethality, and bifenthrin-permethrin and cyfluthrin-permethrin were also additive in terms of subchronic 10-d lethality and sublethal responses. Environ Toxicol Chem 2016;35:2542-2549. © 2016 SETAC. © 2016 SETAC.

  4. Mobility of coated and uncoated TiO2 nanomaterials in soil columns--Applicability of the tests methods of OECD TG 312 and 106 for nanomaterials.

    Science.gov (United States)

    Nickel, Carmen; Gabsch, Stephan; Hellack, Bryan; Nogowski, Andre; Babick, Frank; Stintz, Michael; Kuhlbusch, Thomas A J

    2015-07-01

    Nanomaterials are commonly used in everyday life products and during their life cycle they can be released into the environment. Soils and sediments are estimated as significant sinks for those nanomaterials. To investigate and assess the behaviour of nanomaterials in soils and sediments standardized test methods are needed. In this study the applicability of two existing international standardized test guidelines for the testing of nanomaterials, OECD TG 106 "Adsorption/Desorption using a Bath Equilibrium Method" and the OECD TG 312 "Leaching in Soil Columns", were investigated. For the study one coated and two uncoated TiO2 nanomaterials were used, respectively. The results indicate that the OECD TG 106 is not applicable for nanomaterials. However, the test method according to OECD TG 312 was found to be applicable if nano-specific adaptations are applied. The mobility investigations of the OECD TG 312 indicated a material-dependent mobility of the nanomaterials, which in some cases may lead to an accumulation in the upper soil layers. Whereas no significant transport was observed for the uncoated materials for the double-coated material (coating with dimethicone and aluminiumoxide) a significant transport was detected and attributed to the coating. Copyright © 2015 Elsevier Ltd. All rights reserved.

  5. A new first-order turbulence mixing model for the stable atmospheric boundary-layer: development and testing in large-eddy and single column models

    Science.gov (United States)

    Huang, J.; Bou-Zeid, E.; Golaz, J.

    2011-12-01

    Parameterization of the stably-stratified atmospheric boundary-layer is of crucial importance to different aspects of numerical weather prediction at regional scales and climate modeling at global scales, such as land-surface temperature forecasts, fog and frost prediction, and polar climate. It is well-known that most operational climate models require excessive turbulence mixing of the stable boundary-layer to prevent decoupling of the atmospheric component from the land component under strong stability, but the performance of such a model is unlikely to be satisfactory under weakly and moderately stable conditions. In this study we develop and test a general turbulence mixing model of the stable boundary-layer which works under different stabilities and for steady as well as unsteady conditions. A-priori large-eddy simulation (LES) tests are presented to motivate and verify the new parameterization. Subsequently, an assessment of this model using the GFDL single-column model (SCM) is performed. Idealized test cases including continuously varying stability, as well as stability discontinuity, are used to test the new SCM against LES results. A good match of mean and flux profiles is found when the new parameterization is used, while other traditional first-order turbulence models using the concept of stability function perform poorly. SCM spatial resolution is also found to have little impact on the performance of the new turbulence closure, but temporal resolution is important and a numerical stability criterion based on the model time step is presented.

  6. Bench-scale testing of on-line control of column flotation using a novel analyzer. Third quarterly technical progress report, April 1, 1993--June 30, 1993

    Energy Technology Data Exchange (ETDEWEB)

    1993-08-24

    This document contains the third quarterly technical progress report for PTI`s Bench-Scale Testing Project of a circuit integrating PTI`s KEN-FLOTETM Column Flotation Technology and PTI`s On-Line Quality Monitor and Control System. The twelve-month project involves installation and testing of a 200--300 lb/hr. bench-scale flotation circuit at PETC`s Coal Preparation Process Research Facility (CPPRF) for two bituminous coals (Upper Freeport and Pittsburgh No. 8 Seam Raw Coals). Figure 1 contains the project plan, as well as the approach to completing the major tasks within the twelve-month project schedule. The project is broken down into three phases, which include: Phase I -- Preparation: The preparation phase was performed principally at PTI`s Calumet offices from October through December, 1992. It involved building of the equipment and circuitry, as well as some preliminary design and equipment testing; Phase II -- ET Circuit Installation and Testing: This installation and testing phase of the project was performed at PETC`s CPPRF from January through June, 1993, and was the major focus of the project. It involved testing of the continuous 200--300 lb/hr. circuit; and Phase III -- Project Finalization: The project finalization phase is occurring from July through September, 1993, at PTI`s Calumet offices and involves finalizing analytical work and data evaluation, as well as final project reporting. This Third Quarterly Technical Progress Report principally summarizes the results from the benchscale testing with the second coal (Pittsburgh No. 8 Seam Coal), which occurred in April through June, 1993. It also contains preliminary economic evaluations that will go into the Final Report, as well as the plan for the final reporting task.

  7. Column: Every Last Byte

    Directory of Open Access Journals (Sweden)

    Simson Garfinkel

    2011-06-01

    Full Text Available Inheritance powder is the name that was given to poisons, especially arsenic, that were commonly used in the 17th and early 18th centuries to hasten the death of the elderly. For most of the 17th century, arsenic was deadly but undetectable, making it nearly impossible to prove that someone had been poisoned. The first arsenic test produced a gas—hardly something that a scientist could show to a judge. Faced with a growing epidemic of poisonings, doctors and chemists spent decades searching for something better.(see PDF for full column

  8. MODEL TESTS AND 3D ELASTIC FINITE ELEMENT ANALYSIS FOR STEEL PIPE PILES WITH WINGS IN STALLED IN SOIL CEMENT COLUMN

    Science.gov (United States)

    Tamai, Toshiyuki; Teramoto, Shuntarou; Kimura, Makoto

    Steel pipe piles with wings installed in soil cement column is a composite foundation of pile consisting of soil improvement with cement and steel pipe with wings. This type of pile shows higher vertical bearing capacity when compared to steel pipe piles that are installed without soil cement. It is thought the wings contribute to higher bearing capacity of this type of piles. The wings are also thought to play the role of structural unification of pile foundations and load transfer. In this study, model test and 3D elastic finite element analysis was carried out in order to elucidate the effect of wings on the structural unification of pile foundation and the load transfer mechanism. Firstly, the model test was carried out in order to grasp the influence of pile with and without wings, the shape of wings of the pile and the unconfined compression strength of the soil cement on the structural unification of the pile foundation. The numerical analysis of the model test was then carried out on the intermediate part of the pile foundation with wings and mathematical model developed. Finally load tran sfer mechanism was checked for the entire length of the pile through this mathematical model and the load sharing ratio of the wings and stress distribution occurring in the soil cement clarified. In addition, the effect of the wing interval on the structural unification of the pile foundation and load transfer was also checked and clarified.

  9. Evaluation of non destructive testing to characterize the resistance of the prefabricated system of columns and floor tiles for single family homes of a level: permeability meter, determination of wave velocity by ultrasound, Schmidt sclerometer and metal detector

    International Nuclear Information System (INIS)

    Quesada Chacon, Dannell

    2014-01-01

    Non destructive testing are determined to be correlated with resistance to compression and flexion of elements belonging to prefabricated system of columns and floor tiles for single family homes of a level. The characteristics of the non destructive testing are described, such as: measurer of permeability, Schmidt sclerometer, determination of wave velocity by ultrasound and metal detector. The columns and floor tiles are elaborated with 2 mixtures of different resistances at 28 days. The first more than 30 MPa and the second less than 25 MPa are sampled together with the control cylinders necessary to obtain the actual resistance according to ASTM C39. Last resistance testings to compression and Schmidt sclerometer are realized to control cylinders to 1, 2, and 4 weeks after being cast. Non destructive testings (permeability meter Torrent, Schmidt sclerometer and determination of wave velocity by ultrasound) are performed in columns and floor tiles to 1, 2, and 4 weeks after being cast. Last resistance testings to flexion is obtained by means of destructive tests of the columns and floor tiles sampled. The correlation of the data obtained is determined to derive values of compression resistance from non destructive testing [es

  10. Modeling Stone Columns.

    Science.gov (United States)

    Castro, Jorge

    2017-07-11

    This paper reviews the main modeling techniques for stone columns, both ordinary stone columns and geosynthetic-encased stone columns. The paper tries to encompass the more recent advances and recommendations in the topic. Regarding the geometrical model, the main options are the "unit cell", longitudinal gravel trenches in plane strain conditions, cylindrical rings of gravel in axial symmetry conditions, equivalent homogeneous soil with improved properties and three-dimensional models, either a full three-dimensional model or just a three-dimensional row or slice of columns. Some guidelines for obtaining these simplified geometrical models are provided and the particular case of groups of columns under footings is also analyzed. For the latter case, there is a column critical length that is around twice the footing width for non-encased columns in a homogeneous soft soil. In the literature, the column critical length is sometimes given as a function of the column length, which leads to some disparities in its value. Here it is shown that the column critical length mainly depends on the footing dimensions. Some other features related with column modeling are also briefly presented, such as the influence of column installation. Finally, some guidance and recommendations are provided on parameter selection for the study of stone columns.

  11. Immobilization of Cd, Zn, and Pb from Soil Treated by Limestone with Variation of pH Using a Column Test

    Directory of Open Access Journals (Sweden)

    Sung-Wook Yun

    2015-01-01

    Full Text Available Decades of mining in South Korea have resulted in the contamination of large amounts of soil by metals. The most feasible approach to site restoration requires the use of a stabilization agent to reduce metal mobility. This study examined the leaching characteristics of limestone used as a stabilization agent when subjected to solutions of differing pH. In a laboratory-scale column test, solutions with pH values of 3.5, 4.6, and 5.6, representing acidic to nonacidic rainfall, were applied to soil mixed with limestone. Test results indicate that metal components can be released with the addition of acidic solutions, even if the soil is highly alkaline. Cd and Zn, in particular, exhibited abrupt or continuous leaching when exposed to acid solutions, indicating the potential for contamination of water systems as metal-laden soils are exposed to the slightly acidic rainfall typical of South Korea. Treatment using stabilization agents such as limestone may reduce leaching of metals from the contaminated soil. Stabilizing metal-contaminated farmland is an economical and feasible way to reduce pollutants around abandoned metal mines.

  12. ( Anogeissus leiocarpus ) timber columns

    African Journals Online (AJOL)

    A procedure for designing axially loaded Ayin (Anogeissus leiocarpus) wood column or strut has been investigated. Instead of the usual categorization of columns into short, intermediate and slender according to the value of slenderness ratio, a continuous column formula representing the three categories was derived.

  13. Column Liquid Chromatography.

    Science.gov (United States)

    Majors, Ronald E.; And Others

    1984-01-01

    Reviews literature covering developments of column liquid chromatography during 1982-83. Areas considered include: books and reviews; general theory; columns; instrumentation; detectors; automation and data handling; multidimensional chromatographic and column switching techniques; liquid-solid chromatography; normal bonded-phase, reversed-phase,…

  14. Picobubble enhanced column flotation of fine coal

    Energy Technology Data Exchange (ETDEWEB)

    Tao, D.; Yu, S.; Parekh, B.K. [University of Kentucky, Lexington, KY (United States). Mining Engineering

    2006-07-01

    The purpose is to study the effectiveness of picobubbles in the column flotation of -28 mesh fine coal particles. A flotation column with a picobubble generator was developed and tested for enhancing the recovery of ultrafine coal particles. The picobubble generator was designed using the hydrodynamic cavitation principle. A metallurgical and a steam coal were tested in the apparatus. The results show that the use of picobubbles in a 2in. flotation column increased the recovery of fine coal by 10 to 30%. The recovery rate varied with feed rate, collector dosage, and other column conditions. 40 refs., 8 figs., 2 tabs.

  15. Validated stability indicating liquid chromatographic determination of ebastine in pharmaceuticals after pre column derivatization: Application to tablets and content uniformity testing

    Directory of Open Access Journals (Sweden)

    Eid Manal

    2011-05-01

    Full Text Available Abstract An accurate, simple, sensitive and selective reversed phase liquid chromatographic method has been developed for the determination of ebastine in its pharmaceutical preparations. The proposed method depends on the complexation ability of the studied drug with Zn2+ ions. Reversed phase chromatography was conducted using an ODS C18 (150 × 4.6 mm id stainless steel column at ambient temperature with UV-detection at 260 nm. A mobile phase containing 0.025%w/v Zn2+ in a mixture of (acetonitril/methanol; 1/4 and Britton Robinson buffer (65:35, v/v adjusted to pH 4.2, has been used for the determination of ebastine at a flow rate of 1 ml/min. The calibration curve was rectilinear over the concentration range of 0.3 - 6.0 μg/ml with a detection limit (LOD of 0.13 μg/ml, and quantification limit (LOQ of 0.26 μg/ml. The proposed method was successfully applied for the analysis of ebastine in its dosage forms, the obtained results were favorably compared with those obtained by a comparison method. Furthermore, content uniformity testing of the studied pharmaceutical formulations was also conducted. The composition of the complex as well as its stability constant was also investigated. Moreover, the proposed method was found to be a stability indicating one and was utilized to investigate the kinetics of alkaline and ultraviolet induced degradation of the drug. The first-order rate constant and half life of the degradation products were calculated.

  16. Validation of the design of small diameter pulsed columns for the process line DRA. Tests reliability compared with the industrial scale

    International Nuclear Information System (INIS)

    Leybros, J.

    2000-01-01

    As part of the Spin program related to the management of nuclear wastes, studies have been undertaken to develop partitioning processes like Diamex process. The process line CCBP/DRA in Atalante facility forms one of the main equipment devoted to these studies. On this line industrial apparatus are used but some like pulsed columns need to be adapted because of the specificity of the installation: limiting amount of nuclear matter, gaseous waste minimization, safety, limiting amounts of new extractants,... This article presents the comparison of 2 air pulsed columns, one with a standard diameter of 25 (DN25), the other with a reduced diameter of 15 (DN15). This comparison is based on 3 main criteria: pulsation capability, superficial throughput and mass transfer efficiency. The overall comparison shows that a DN15 pulsed column can be considered as a representative tool of research and development. Particularly, the study demonstrates the possibility of scaling up the results

  17. Thermally stable dexsil-400 glass capillary columns

    International Nuclear Information System (INIS)

    Maskarinec, M.P.; Olerich, G.

    1980-01-01

    The factors affecting efficiency, thermal stability, and reproducibility of Dexsil-400 glass capillary columns for gas chromatography in general, and for polycyclic aromatic hydrocarbons (PAHs) in particular were investigated. Columns were drawn from Kimble KG-6 (soda-lime) glass or Kimox (borosilicate) glass. All silylation was carried out at 200 0 C. Columns were coated according to the static method. Freshly prepared, degassed solutions of Dexsil-400 in pentane or methylene chloride were used. Thermal stability of the Dexsil 400 columns with respect to gas chromatography/mass spectrometry (GC/MS) were tested. Column-to-column variability is a function of each step in the fabrication of the columns. The degree of etching, extent of silylation, and stationary phase film thickness must be carefully controlled. The variability in two Dexsil-400 capillary column prepared by etching, silylation with solution of hexa methyl disilazone (HMDS), and static coating is shown and also indicates the excellent selectivity of Dexsil-400 for the separation of alkylated aromatic compounds. The wide temperature range of Dexsil-400 and the high efficiency of the capillary columns also allow the analysis of complex mixtures with minimal prefractionation. Direct injection of a coal liquefaction product is given. Analysis by GC/MS indicated the presence of parent PAHs, alkylated PAHs, nitrogen and sulfur heterocycles, and their alkylated derivatives. 4 figures

  18. JCE Feature Columns

    Science.gov (United States)

    Holmes, Jon L.

    1999-05-01

    The Features area of JCE Online is now readily accessible through a single click from our home page. In the Features area each column is linked to its own home page. These column home pages also have links to them from the online Journal Table of Contents pages or from any article published as part of that feature column. Using these links you can easily find abstracts of additional articles that are related by topic. Of course, JCE Online+ subscribers are then just one click away from the entire article. Finding related articles is easy because each feature column "site" contains links to the online abstracts of all the articles that have appeared in the column. In addition, you can find the mission statement for the column and the email link to the column editor that I mentioned above. At the discretion of its editor, a feature column site may contain additional resources. As an example, the Chemical Information Instructor column edited by Arleen Somerville will have a periodically updated bibliography of resources for teaching and using chemical information. Due to the increase in the number of these resources available on the WWW, it only makes sense to publish this information online so that you can get to these resources with a simple click of the mouse. We expect that there will soon be additional information and resources at several other feature column sites. Following in the footsteps of the Chemical Information Instructor, up-to-date bibliographies and links to related online resources can be made available. We hope to extend the online component of our feature columns with moderated online discussion forums. If you have a suggestion for an online resource you would like to see included, let the feature editor or JCE Online (jceonline@chem.wisc.edu) know about it. JCE Internet Features JCE Internet also has several feature columns: Chemical Education Resource Shelf, Conceptual Questions and Challenge Problems, Equipment Buyers Guide, Hal's Picks, Mathcad

  19. Behaviour of FRP confined concrete in square columns

    OpenAIRE

    Diego Villalón, Ana de; Arteaga Iriarte, Ángel; Fernandez Gomez, Jaime Antonio; Perera Velamazán, Ricardo; Cisneros, Daniel

    2015-01-01

    A significant amount of research has been conducted on FRP-confined circular columns, but much less is known about rectangular/square columns in which the effectiveness of confinement is much reduced. This paper presents the results of experimental investigations on low strength square concrete columns confined with FRP. Axial compression tests were performed on ten intermediate size columns. The tests results indicate that FRP composites can significantly improve the bearing capacity and duc...

  20. Nuclear reactor control column

    International Nuclear Information System (INIS)

    Bachovchin, D.M.

    1982-01-01

    The nuclear reactor control column comprises a column disposed within the nuclear reactor core having a variable cross-section hollow channel and containing balls whose vertical location is determined by the flow of the reactor coolant through the column. The control column is divided into three basic sections wherein each of the sections has a different cross-sectional area. The uppermost section of the control column has the greatest crosssectional area, the intermediate section of the control column has the smallest cross-sectional area, and the lowermost section of the control column has the intermediate cross-sectional area. In this manner, the area of the uppermost section can be established such that when the reactor coolant is flowing under normal conditions therethrough, the absorber balls will be lifted and suspended in a fluidized bed manner in the upper section. However, when the reactor coolant flow falls below a predetermined value, the absorber balls will fall through the intermediate section and into the lowermost section, thereby reducing the reactivity of the reactor core and shutting down the reactor

  1. Reprocessing of spent nuclear fuel, Annex 1: Experimental facility for testing and development of pulsed columns and auxiliary devices; Prerada isluzenog nuklearnog goriva, Prilog 1: Opitno postrojenje za ispitivanje i razvoj pulsnih kolona i pomocnih uredjaja

    Energy Technology Data Exchange (ETDEWEB)

    Gal, I [Institute of Nuclear Sciences Boris Kidric, Laboratorija za hemiju visoke aktivnosti, Vinca, Beograd (Serbia and Montenegro)

    1964-12-15

    After completing the design project for building the experimental facility for testing and development of pulsed columns for spent fuel reprocessing, the construction started by the end of 1963 and was completed in August 1964. The facility was built in Kjeller, Norway within cooperation project between out country and Norway. This report covers a brief description of the facility and the action plan of its implementation.

  2. Improvements in solvent extraction columns

    International Nuclear Information System (INIS)

    Aughwane, K.R.

    1987-01-01

    Solvent extraction columns are used in the reprocessing of irradiated nuclear fuel. For an effective reprocessing operation a solvent extraction column is required which is capable of distributing the feed over most of the column. The patent describes improvements in solvent extractions columns which allows the feed to be distributed over an increased length of column than was previously possible. (U.K.)

  3. Performance evaluation of granular activated carbon system at Pantex: Rapid small-scale column tests to simulate removal of high explosives from contaminated groundwater

    Energy Technology Data Exchange (ETDEWEB)

    Henke, J.L.; Speitel, G.E. [Univ. of Texas, Austin, TX (United States). Dept. of Civil Engineering

    1998-08-01

    A granular activated carbon (GAC) system is now in operation at Pantex to treat groundwater from the perched aquifer that is contaminated with high explosives. The main chemicals of concern are RDX and HMX. The system consists of two GAC columns in series. Each column is charged with 10,000 pounds of Northwestern LB-830 GAC. At the design flow rate of 325 gpm, the hydraulic loading is 6.47 gpm/ft{sup 2}, and the empty bed contact time is 8.2 minutes per column. Currently, the system is operating at less than 10% of its design flow rate, although flow rate increases are expected in the relatively near future. This study had several objectives: Estimate the service life of the GAC now in use at Pantex; Screen several GACs to provide a recommendation on the best GAC for use at Pantex when the current GAC is exhausted and is replaced; Determine the extent to which natural organic matter in the Pantex groundwater fouls GAC adsorption sites, thereby decreasing the adsorption capacity for high explosives; and Determine if computer simulation models could match the experimental results, thereby providing another tool to follow system performance.

  4. Performance evaluation of granular activated carbon system at Pantex: Rapid small-scale column tests to simulate removal of high explosives from contaminated groundwater

    International Nuclear Information System (INIS)

    Henke, J.L.; Speitel, G.E.

    1998-08-01

    A granular activated carbon (GAC) system is now in operation at Pantex to treat groundwater from the perched aquifer that is contaminated with high explosives. The main chemicals of concern are RDX and HMX. The system consists of two GAC columns in series. Each column is charged with 10,000 pounds of Northwestern LB-830 GAC. At the design flow rate of 325 gpm, the hydraulic loading is 6.47 gpm/ft 2 , and the empty bed contact time is 8.2 minutes per column. Currently, the system is operating at less than 10% of its design flow rate, although flow rate increases are expected in the relatively near future. This study had several objectives: Estimate the service life of the GAC now in use at Pantex; Screen several GACs to provide a recommendation on the best GAC for use at Pantex when the current GAC is exhausted and is replaced; Determine the extent to which natural organic matter in the Pantex groundwater fouls GAC adsorption sites, thereby decreasing the adsorption capacity for high explosives; and Determine if computer simulation models could match the experimental results, thereby providing another tool to follow system performance

  5. Capacity of columns with splice imperfections

    International Nuclear Information System (INIS)

    Popov, E.P.; Stephen, R.M.

    1977-01-01

    To study the behavior of spliced columns subjected to tensile forces simulating situations which may develop in an earthquake, all of the spliced specimens were tested to failure in tension after first having been subjected to large compressive loads. The results of these tests indicate that the lack of perfect contact at compression splices of columns may not be important, provided that the gaps are shimmed and welding is used to maintain the sections in alignment

  6. Center column design of the PLT

    International Nuclear Information System (INIS)

    Citrolo, J.; Frankenberg, J.

    1975-01-01

    The center column of the PLT machine is a secondary support member for the toroidal field coils. Its purpose is to decrease the bending moment at the nose of the coils. The center column design was to have been a stainless steel casting with the toroidal field coils grouped around the casting at installation, trapping it in place. However, the castings developed cracks during fabrication and were unsuitable for use. Installation of the coils proceeded without the center column. It then became necessary to redesign a center column which would be capable of installation with the toroidal field coils in place. The final design consists of three A-286 forgings. This paper discusses the final center column design and the influence that new knowledge, obtained during the power tests, had on the new design

  7. SPEEDUPtrademark ion exchange column model

    International Nuclear Information System (INIS)

    Hang, T.

    2000-01-01

    A transient model to describe the process of loading a solute onto the granular fixed bed in an ion exchange (IX) column has been developed using the SpeedUptrademark software package. SpeedUp offers the advantage of smooth integration into other existing SpeedUp flowsheet models. The mathematical algorithm of a porous particle diffusion model was adopted to account for convection, axial dispersion, film mass transfer, and pore diffusion. The method of orthogonal collocation on finite elements was employed to solve the governing transport equations. The model allows the use of a non-linear Langmuir isotherm based on an effective binary ionic exchange process. The SpeedUp column model was tested by comparing to the analytical solutions of three transport problems from the ion exchange literature. In addition, a sample calculation of a train of three crystalline silicotitanate (CST) IX columns in series was made using both the SpeedUp model and Purdue University's VERSE-LC code. All test cases showed excellent agreement between the SpeedUp model results and the test data. The model can be readily used for SuperLigtrademark ion exchange resins, once the experimental data are complete

  8. Gas Chromatograph Method Optimization Trade Study for RESOLVE: 20-meter Column v. 8-meter Column

    Science.gov (United States)

    Huz, Kateryna

    2014-01-01

    RESOLVE is the payload on a Class D mission, Resource Prospector, which will prospect for water and other volatile resources at a lunar pole. The RESOLVE payload's primary scientific purpose includes determining the presence of water on the moon in the lunar regolith. In order to detect the water, a gas chromatograph (GC) will be used in conjunction with a mass spectrometer (MS). The goal of the experiment was to compare two GC column lengths and recommend which would be best for RESOLVE's purposes. Throughout the experiment, an Inficon Fusion GC and an Inficon Micro GC 3000 were used. The Fusion had a 20m long column with 0.25mm internal diameter (Id). The Micro GC 3000 had an 8m long column with a 0.32mm Id. By varying the column temperature and column pressure while holding all other parameters constant, the ideal conditions for testing with each column length in their individual instrument configurations were determined. The criteria used for determining the optimal method parameters included (in no particular order) (1) quickest run time, (2) peak sharpness, and (3) peak separation. After testing numerous combinations of temperature and pressure, the parameters for each column length that resulted in the most optimal data given my three criteria were selected. The ideal temperature and pressure for the 20m column were 95 C and 50psig. At this temperature and pressure, the peaks were separated and the retention times were shorter compared to other combinations. The Inficon Micro GC 3000 operated better at lower temperature mainly due to the shorter 8m column. The optimal column temperature and pressure were 70 C and 30psig. The Inficon Micro GC 3000 8m column had worse separation than the Inficon Fusion 20m column, but was able to separate water within a shorter run time. Therefore, the most significant tradeoff between the two column lengths was peak separation of the sample versus run time. After performing several tests, it was concluded that better

  9. Buckling of liquid columns

    NARCIS (Netherlands)

    Habibi, M.; Rahmani, Y.; Bonn, D.; Ribe, N.M.

    2010-01-01

    Under appropriate conditions, a column of viscous liquid falling onto a rigid surface undergoes a buckling instability. Here we show experimentally and theoretically that liquid buckling exhibits a hitherto unsuspected complexity involving three different modes—viscous, gravitational, and

  10. Solvent extraction columns

    International Nuclear Information System (INIS)

    Middleton, P.; Smith, J.R.

    1979-01-01

    In pulsed columns for use in solvent extraction processes, e.g. the reprocessing of nuclear fuel, the horizontal perforated plates inside the column are separated by interplate spacers manufactured from metallic neutron absorbing material. The spacer may be in the form of a spiral or concentric circles separated by radial limbs, or may be of egg-box construction. Suitable neutron absorbing materials include stainless steel containing boron or gadolinium, hafnium metal or alloys of hafnium. (UK)

  11. Removal efficiency of multiple poly- and perfluoroalkyl substances (PFASs) in drinking water using granular activated carbon (GAC) and anion exchange (AE) column tests.

    Science.gov (United States)

    McCleaf, Philip; Englund, Sophie; Östlund, Anna; Lindegren, Klara; Wiberg, Karin; Ahrens, Lutz

    2017-09-01

    Poly- and perfluoroalkyl substances (PFASs) have been detected in drinking water at relatively high concentrations throughout the world which has led to implementation of regulatory guidelines for specific PFASs in drinking water in several European countries and in the U.S. The Swedish National Food Agency has determined that the drinking water of over one third of the country's municipal consumers is at risk or already affected by PFAS contamination. The present study investigated the effects of perfluorocarbon chain length, functional group and isomer structure (branched or linear) on removal of multiple PFASs using granular activated carbon (GAC, Filtrasorb ® 400) and anion exchange (AE, Purolite ® A600) column experiments. The removal of 14 different PFASs, i.e. the C 3 C 11 , C 14 perfluoroalkyl carboxylic acids (PFCAs) (PFBA, PFPeA, PFHxA, PFHpA, PFOA, PFNA, PFDA, PFUnDA, PFDoDA, PFTeDA), perfluorooctane sulfonamide (FOSA), and the C 4 , C 6 , C 8 perfluoroalkyl sulfonic acids (PFSAs) (PFBS, PFHxS, PFOS), was monitored for a 217 day period. The results indicate the selective nature of PFAS removal as the absorbents are loaded with PFASs and dissolved organic carbon (DOC). A clear relationship between perfluorocarbon chain length and removal efficiency of PFASs using GAC and AE was found while PFASs with sulfonate functional groups displayed greater removal efficiency than those with carboxylate groups. Similarly, time to column breakthrough increased with increasing perfluorocarbon chain length and was greater for the PFSAs than the PFCAs for both GAC and AE. Shorter carbon chained PFASs such as PFBA, PFPeA, PFHxA showed desorption behavior and long-chained PFASs showed increased removal towards the end of the experiment indicating agglomeration or micelle development. Linear isomers of PFOS, PFHxS, and perfluorooctane sulfonamide (FOSA) had greater column removal efficiencies using GAC (and also for AE at greater bed volume throughput) than the branched

  12. PRTR ion exchange vault column sampling

    International Nuclear Information System (INIS)

    Cornwell, B.C.

    1995-01-01

    This report documents ion exchange column sampling and Non Destructive Assay (NDA) results from activities in 1994, for the Plutonium Recycle Test Reactor (PRTR) ion exchange vault. The objective was to obtain sufficient information to prepare disposal documentation for the ion exchange columns found in the PRTR Ion exchange vault. This activity also allowed for the monitoring of the liquid level in the lower vault. The sampling activity contained five separate activities: (1) Sampling an ion exchange column and analyzing the ion exchange media for purpose of waste disposal; (2) Gamma and neutron NDA testing on ion exchange columns located in the upper vault; (3) Lower vault liquid level measurement; (4) Radiological survey of the upper vault; and (5) Secure the vault pending waste disposal

  13. Assembly for connecting the column ends of two capillary columns

    International Nuclear Information System (INIS)

    Kolb, B.; Auer, M.; Pospisil, P.

    1984-01-01

    In gas chromatography, the column ends of two capillary columns are inserted into a straight capillary from both sides forming annular gaps. The capillary is located in a tee out of which the capillary columns are sealingly guided, and to which carrier gas is supplied by means of a flushing flow conduit. A ''straight-forward operation'' having capillary columns connected in series and a ''flush-back operation'' are possible. The dead volume between the capillary columns can be kept small

  14. Interpretation of Actinide-Distribution Data Obtained from Non-Destructive and Destructive Post-Test Analyses of an Intact-Core Column of Culebra Dolomite

    International Nuclear Information System (INIS)

    LUCERO, DANIEL A.; PERKINS, W. GEORGE

    1999-01-01

    The US DOE, with technical assistance from Sandia National Laboratories, has successfully received EPA certification and opened the Waste Isolation Pilot Plant (WIPP), a nuclear waste disposal facility located approximately 42 km east of Carlsbad, New Mexico. Performance assessment analyses indicate that human intrusions by inadvertent, intermittent drilling for resources provide the only credible mechanisms for releases of radionuclides from the disposal system. In modeling long-term brine releases, subsequent to a drilling event, potential migration pathways through the permeable layers of rock above the Salado formation were analyzed. Major emphasis is placed on the Culebra Member of the Rustler Formation because this is the most transmissive geologic layer overlying the WIPP site. In order to help quantify parameters for the calculated releases, radionuclide transport experiments have been earned out using intact-core columns obtained from the Culebra dolomite member of the Rustler Formation within the WIPP site. This paper deals primarily with results of analyses for 241 Pu and 241 Am distributions developed during transport experiments in one of these cores. Transport experiments were done using a synthetic brine that simulates Culebra brine at the core recovery location (the WIPP air-intake shaft--AIS). Hydraulic characteristics (i.e., apparent porosity and apparent dispersion coefficient) for intact-core columns were obtained via experiments using the conservative tracer 22 Na. Elution experiments carried out over periods of a few days with tracers 232 U and 239 Np indicated that these tracers were weakly retarded as indicated by delayed elution of the species. Elution experiments with tracers 241 Pu and 241 Am were attempted, but no elution of either species has been observed to date, including experiments of many months' duration. In order to quantify retardation of the non-eluted species 241 Pu and 241 Am after a period of brine flow, non-destructive and

  15. Behavior of reinforced concrete columns strenghtened by partial jacketing

    Directory of Open Access Journals (Sweden)

    D. B. FERREIRA

    Full Text Available This article presents the study of reinforced concrete columns strengthened using a partial jacket consisting of a 35mm self-compacting concrete layer added to its most compressed face and tested in combined compression and uniaxial bending until rupture. Wedge bolt connectors were used to increase bond at the interface between the two concrete layers of different ages. Seven 2000 mm long columns were tested. Two columns were cast monolithically and named PO (original column e PR (reference column. The other five columns were strengthened using a new 35 mm thick self-compacting concrete layer attached to the column face subjected to highest compressive stresses. Column PO had a 120mm by 250 mm rectangular cross section and other columns had a 155 mm by 250mm cross section after the strengthening procedure. Results show that the ultimate resistance of the strengthened columns was more than three times the ultimate resistance of the original column PO, indicating the effectiveness of the strengthening procedure. Detachment of the new concrete layer with concrete crushing and steel yielding occurred in the strengthened columns.

  16. Columns in Clay

    Science.gov (United States)

    Leenhouts, Robin

    2010-01-01

    This article describes a clay project for students studying Greece and Rome. It provides a wonderful way to learn slab construction techniques by making small clay column capitols. With this lesson, students learn architectural vocabulary and history, understand the importance of classical architectural forms and their influence on today's…

  17. Slender CRC Columns

    DEFF Research Database (Denmark)

    Aarup, Bendt; Jensen, Lars Rom; Ellegaard, Peter

    2005-01-01

    CRC is a high-performance steel fibre reinforced concrete with a typical compressive strength of 150 MPa. Design methods for a number of structural elements have been developed since CRC was invented in 1986, but the current project set out to further investigate the range of columns for which...

  18. Practical column design guide

    CERN Document Server

    Nitsche, M

    2017-01-01

    This book highlights the aspects that need to be considered when designing distillation columns in practice. It discusses the influencing parameters as well as the equations governing them, and presents several numerical examples. The book is intended both for experienced designers and for those who are new to the subject.

  19. Nine Words - Nine Columns

    DEFF Research Database (Denmark)

    Trempe Jr., Robert B.; Buthke, Jan

    2016-01-01

    This book records the efforts of a one-week joint workshop between Master students from Studio 2B of Arkitektskolen Aarhus and Master students from the Harbin Institute of Technology in Harbin, China. The workshop employed nine action words to instigate team-based investigation into the effects o...... as formwork for the shaping of wood veneer. The resulting columns ‘wear’ every aspect of this design pipeline process and display the power of process towards an architectural resolution....

  20. Column studies on BTEX biodegradation under microaerophilic and denitrifying conditions

    International Nuclear Information System (INIS)

    Hutchins, S.R.; Moolenaar, S.W.; Rhodes, D.E.

    1992-01-01

    Two column tests were conducted using aquifer material to simulate the nitrate field demonstration project carried out earlier at Traverse City, Michigan. The objectives were to better define the effect nitrate addition had on biodegradation of benzene, toluene, ethylbenzene, xylenes, and trimethylbenzenes (BTEX) in the field study, and to determine whether BTEX removal can be enhanced by supplying a limited amount of oxygen as a supplemental electron acceptor. Columns were operated using limited oxygen, limited oxygen plus nitrate, and nitrate alone. In the first column study, benzene was generally recalcitrant compared to the alkylbenzenes (TEX), although some removal did occur. In the second column study, nitrate was deleted from the feed to the column originally receiving nitrate alone and added to the feed of the column originally receiving limited oxygen alone. Although the requirement for nitrate for optimum TEX removal was clearly demonstrated in these columns, there were significant contributions by biotic and abiotic processes other than denitrification which could not be quantified

  1. NMFS Water Column Sonar Database

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — Water column sonar data are an important component of fishery independent surveys, habitat studies and other research. NMFS water column sonar data are archived here.

  2. Strengthening of Steel Columns under Load: Torsional-Flexural Buckling

    Directory of Open Access Journals (Sweden)

    Martin Vild

    2016-01-01

    Full Text Available The paper presents experimental and numerical research into the strengthening of steel columns under load using welded plates. So far, the experimental research in this field has been limited mostly to flexural buckling of columns and the preload had low effect on the column load resistance. This paper focuses on the local buckling and torsional-flexural buckling of columns. Three sets of three columns each were tested. Two sets corresponding to the base section (D and strengthened section (E were tested without preloading and were used for comparison. Columns from set (F were first preloaded to the load corresponding to the half of the load resistance of the base section (D. Then the columns were strengthened and after they cooled, they were loaded to failure. The columns strengthened under load (F had similar average resistance as the columns welded without preloading (E, meaning the preload affects even members susceptible to local buckling and torsional-flexural buckling only slightly. This is the same behaviour as of the tested columns from previous research into flexural buckling. The study includes results gained from finite element models of the problem created in ANSYS software. The results obtained from the experiments and numerical simulations were compared.

  3. Water hammer and column separation due to accidental simultaneous closure of control valves in a large scale two-phase flow experimental test rig

    NARCIS (Netherlands)

    Bergant, A.; Westende, van 't J.M.C.; Koppel, T.; Gale, J.; Hou, Q.; Pandula, Z.; Tijsseling, A.S.

    2010-01-01

    A large-scale pipeline test rig at Deltares, Delft, The Netherlands has been used for filling and emptying experiments. Tests have been conducted in a horizontal 250 mm diameter PVC pipe of 258 m length with control valves at the downstream and upstream ends. This paper investigates the accidental

  4. Applicability of hydroxylamine nitrate reductant in pulse-column contactors

    International Nuclear Information System (INIS)

    Reif, D.J.

    1983-05-01

    Uranium and plutonium separations were made from simulated breeder reactor spent fuel dissolver solution with laboratory-sized pulse column contactors. Hydroxylamine nitrate (HAN) was used for reduction of plutonium (1V). An integrated extraction-partition system, simulating a breeder fuel reprocessing flowsheet, carried out a partial partition of uranium and plutonium in the second contactor. Tests have shown that acceptable coprocessing can be ontained using HAN as a plutonium reductant. Pulse column performance was stable even though gaseous HAN oxidation products were present in the column. Gas evolution rates up to 0.27 cfm/ft 2 of column cross section were tested and found acceptable

  5. Elevator frames two columns

    OpenAIRE

    Marín Jiménez, Juan Francisco

    2015-01-01

    This project aims to solve the problem of vertical transport of charges raised by a company with the standard UNE 58-132-91/6. The purpose of this project is the industrial design of a system of load handling by a bi-columned lifting device, tractioned by flat belts and steel cables from a transport level to a different level in order to connect two different assembly lines situated at different heights. The goal of this project is lifting a 780 Kg load at a 2.400 mm height....

  6. A CONCEPTUAL DESIGN OF NEUTRON COLLIMATOR IN THE THERMAL COLUMN OF KARTINI RESEARCH REACTOR FOR IN VITRO AND IN VIVO TEST OF BORON NEUTRON CAPTURE THERAPY

    Directory of Open Access Journals (Sweden)

    Nina Fauziah

    2015-03-01

    Full Text Available Studies were carried out to design a collimator which results in epithermal neutron beam for IN VITRO and IN VIVO of Boron Neutron Capture Therapy (BNCT at the Kartini research reactor by means of Monte Carlo N-Particle (MCNP codes. Reactor within 100 kW of thermal power was used as the neutron source. The design criteria were based on recommendation from the International Atomic Energy Agency (IAEA. All materials used were varied in size, according to the value of mean free path for each material. MCNP simulations indicated that by using 5 cm thick of Ni as collimator wall, 60 cm thick of Al as moderator, 15 cm thick of 60Ni as filter, 2 cm thick of Bi as γ-ray shielding, 3 cm thick of 6Li2CO3-polyethylene as beam delimiter, with 1 to 5 cm varied aperture size, epithermal neutron beam with maximum flux of 7.65 x 108 n.cm-2.s-1 could be produced. The beam has minimum fast neutron and γ-ray components of, respectively, 1.76 x 10-13 Gy.cm2.n-1 and 1.32 x 10-13 Gy.cm2.n-1, minimum thermal neutron per epithermal neutron ratio of 0.008, and maximum directionality of 0.73. It did not fully pass the IAEA’s criteria, since the epithermal neutron flux was below the recommended value, 1.0 x 109 n.cm-2.s-1. Nonetheless, it was still usable with epithermal neutron flux exceeding 5.0 x 108 n.cm-2.s-1. When it was assumed that the graphite inside the thermal column was not discharged but only the part which was going to be replaced by the collimator, the performance of the collimator became better within the positive effect from the surrounding graphite that the beam resulted passed all criteria with epithermal neutron flux up to 1.68 x 109 n.cm-2.s-1. Keywords: design, collimator, epithermal neutron beam, BNCT, MCNP, criteria   Telah dilakukan penelitian tentang desain kolimator yang menghasilkan radiasi netron epitermal untuk uji in vitro dan in vivo pada Boron Neutron Capture Therapy (BNCT di Reaktor Riset Kartini dengan menggunakan program Monte

  7. Circular Raft Footings Strengthened by Stone Columns under Static Loads

    OpenAIRE

    R. Ziaie Moayed; B. Mohammadi-Haji

    2016-01-01

    Stone columns have been widely employed to improve the load-settlement characteristics of soft soils. The results of two small scale displacement control loading tests on stone columns were used in order to validate numerical finite element simulations. Additionally, a series of numerical calculations of static loading have been performed on strengthened raft footing to investigate the effects of using stone columns on bearing capacity of footings. The bearing capacity of single and group of ...

  8. Cesium ion exchange using actual waste: Column size considerations

    International Nuclear Information System (INIS)

    Brooks, K.P.

    1996-04-01

    It is presently planned to remove cesium from Hanford tank waste supernates and sludge wash solutions using ion exchange. To support the development of a cesium ion exchange process, laboratory experiments produced column breakthrough curves using wastes simulants in 200 mL columns. To verify the validity of the simulant tests, column runs with actual supernatants are being planned. The purpose of these actual waste tests is two-fold. First, the tests will verify that use of the simulant accurately reflects the equilibrium and rate behavior of the resin compared to actual wastes. Batch tests and column tests will be used to compare equilibrium behaviors and rate behaviors, respectively. Second, the tests will assist in clarifying the negative interactions between the actual waste and the ion exchange resin, which cannot be effectively tested with simulant. Such interactions include organic fouling of the resin and salt precipitation in the column. These effects may affect the shape of the column breakthrough curve. The reduction in column size also may change the shape of the curve, making the individual effects even more difficult to sort out. To simplify the evaluation, the changes due to column size must be either understood or eliminated. This report describes the determination of the column size for actual waste testing that best minimizes the effect of scale-down. This evaluation will provide a theoretical basis for the dimensions of the column. Experimental testing is still required before the final decision can be made. This evaluation will be confined to the study of CS-100 and R-F resins with NCAW simulant and to a limited extent DSSF waste simulant. Only the cesium loading phase has been considered

  9. Column: File Cabinet Forensics

    Directory of Open Access Journals (Sweden)

    Simson Garfinkel

    2011-12-01

    Full Text Available Researchers can spend their time reverse engineering, performing reverse analysis, or making substantive contributions to digital forensics science. Although work in all of these areas is important, it is the scientific breakthroughs that are the most critical for addressing the challenges that we face.Reverse Engineering is the traditional bread-and-butter of digital forensics research. Companies like Microsoft and Apple deliver computational artifacts (operating systems, applications and phones to the commercial market. These artifacts are bought and used by billions. Some have evil intent, and (if society is lucky, the computers end up in the hands of law enforcement. Unfortunately the original vendors rarely provide digital forensics tools that make their systems amenable to analysis by law enforcement. Hence the need for reverse engineering.(see PDF for full column

  10. Partial strengthening of R.C square columns using CFRP

    Directory of Open Access Journals (Sweden)

    Ahmed Shaban Abdel-Hay

    2014-12-01

    An experimental program was undertaken testing ten square columns 200 × 200 × 2000 mm. One of them was a control specimen and the other nine specimens were strengthened with CFRP. The main parameters studied in this research were the compressive strength of the upper part, the height of the upper poor concrete part, and the height of CFRP wrapped part of column. The experimental results including mode of failure, ultimate load, concrete strain, and fiber strains were analyzed. The main conclusion of this research was, partial strengthening of square column using CFRP can be permitted and gives good results of the column carrying capacity.

  11. Compact electron beam focusing column

    Science.gov (United States)

    Persaud, Arun; Leung, Ka-Ngo; Reijonen, Jani

    2001-12-01

    A novel design for an electron beam focusing column has been developed at LBNL. The design is based on a low-energy spread multicusp plasma source which is used as a cathode for electron beam production. The focusing column is 10 mm in length. The electron beam is focused by means of electrostatic fields. The column is designed for a maximum voltage of 50 kV. Simulations of the electron trajectories have been performed by using the 2D simulation code IGUN and EGUN. The electron temperature has also been incorporated into the simulations. The electron beam simulations, column design and fabrication will be discussed in this presentation.

  12. Comparison of monolithic silica and polymethacrylate capillary columns for LC

    Czech Academy of Sciences Publication Activity Database

    Moravcová, D.; Jandera, P.; Urban, J.; Planeta, Josef

    2004-01-01

    Roč. 27, 10-11 (2004), s. 789-800 ISSN 1615-9306 R&D Projects: GA ČR(CZ) GA203/02/0023 Keywords : monolithic column s * capillary HPLC * column testing Subject RIV: CB - Analytical Chemistry, Separation Impact factor: 1.927, year: 2004

  13. Cow-in-a-Column – A Synthetic Food Replicator

    Data.gov (United States)

    National Aeronautics and Space Administration — The project tested the concept for combining waste degradation and food production in a single reactor or column, i.e., a "Cow-in-a-Column".  The inputs could...

  14. A stochastic view on column efficiency.

    Science.gov (United States)

    Gritti, Fabrice

    2018-03-09

    A stochastic model of transcolumn eddy dispersion along packed beds was derived. It was based on the calculation of the mean travel time of a single analyte molecule from one radial position to another. The exchange mechanism between two radial positions was governed by the transverse dispersion of the analyte across the column. The radial velocity distribution was obtained by flow simulations in a focused-ion-beam scanning electron microscopy (FIB-SEM) based 3D reconstruction from a 2.1 mm × 50 mm column packed with 2 μm BEH-C 18 particles. Accordingly, the packed bed was divided into three coaxial and uniform zones: (1) a 1.4 particle diameter wide, ordered, and loose packing at the column wall (velocity u w ), (2) an intermediate 130 μm wide, random, and dense packing (velocity u i ), and (3) the bulk packing in the center of the column (velocity u c ). First, the validity of this proposed stochastic model was tested by adjusting the predicted to the observed reduced van Deemter plots of a 2.1 mm × 50 mm column packed with 2 μm BEH-C 18 fully porous particles (FPPs). An excellent agreement was found for u i  = 0.93u c , a result fully consistent with the FIB-SEM observation (u i  = 0.95u c ). Next, the model was used to measure u i  = 0.94u c for 2.1 mm × 100 mm column packed with 1.6 μm Cortecs-C 18 superficially porous particles (SPPs). The relative velocity bias across columns packed with SPPs is then barely smaller than that observed in columns packed with FPPs (+6% versus + 7%). u w =1.8u i is measured for a 75 μm × 1 m capillary column packed with 2 μm BEH-C 18 particles. Despite this large wall-to-center velocity bias (+80%), the presence of the thin and ordered wall packing layer has no negative impact on the kinetic performance of capillary columns. Finally, the stochastic model of long-range eddy dispersion explains why analytical (2.1-4.6 mm i.d.) and capillary (columns can all be

  15. Application of a Fast Separation Method for Anti-diabetics in Pharmaceuticals Using Monolithic Column: Comparative Study With Silica Based C-18 Particle Packed Column.

    Science.gov (United States)

    Hemdan, A; Abdel-Aziz, Omar

    2018-04-01

    Run time is a predominant factor in HPLC for quality control laboratories especially if there is large number of samples have to be analyzed. Working at high flow rates cannot be attained with silica based particle packed column due to elevated backpressure issues. The use of monolithic column as an alternative to traditional C-18 column was tested for fast separation of pharmaceuticals, where the results were very competitive. The performance comparison of both columns was tested for separation of anti-diabetic combination containing Metformin, Pioglitazone and Glimepiride using Gliclazide as an internal standard. Working at high flow rates with less significant backpressure was obtained with the monolithic column where the run time was reduced from 6 min in traditional column to only 1 min in monolithic column with accepted resolution. The structure of the monolith contains many pores which can adapt the high flow rate of the mobile phase. Moreover, peak symmetry and equilibration time were more efficient with monolithic column.

  16. Safety barriers and lighting columns.

    NARCIS (Netherlands)

    Schreuder, D.A.

    1972-01-01

    Problems arising from the sitting of lighting columns on the central reserve are reviewed, and remedial measures such as break-away lighting supports and installation of safety fences on the central reserve on both sides of the lighting columns are examined.

  17. REUSABILITY OF BOND ELUT CERTIFY COLUMNS FOR THE EXTRACTION OF DRUGS FROM PLASMA

    NARCIS (Netherlands)

    CHEN, XH; FRANKE, JP; WIJSBEEK, J; DEZEEUW, RA

    1993-01-01

    The reusability of Bond Elut Certify columns for the extraction of toxicologically relevant drugs from plasma has been evaluated. Pentobarbital, hexobarbital, mepivacaine, trimipramine and clonazepam were selected as test drugs to represent various classes of drugs. The columns were regenerated

  18. Response of steel box columns in fire conditions

    Directory of Open Access Journals (Sweden)

    Mahmood Yahyai

    2017-05-01

    Full Text Available Effect of elevated temperatures on the mechanical properties of steel, brings the importance of investigating the effect of fire on the steel structures anxiously. Columns, as the main load-carrying part of a structure, can be highly vulnerable to the fire. In this study, the behavior of steel gravity columns with box cross section exposed to fire has been investigated. These kinds of columns are widely used in common steel structures design in Iran. In current study, the behavior of such columns in fire conditions is investigated through the finite element method. To perform this, the finite element model of a steel column which has been previously tested under fire condition, was prepared. Experimental loading and boundary conditions were considered in the model and was analyzed. Results were validated by experimental data and various specimens of gravity box columns were designed according to the Iran’s steel buildings code, and modeled and analyzed using Abaqus software. The effect of width to thickness ratio of column plates, the load ratio and slenderness on the ultimate strength of the column was investigated, and the endurance time was estimated under ISO 834 standard fire curve. The results revealed that an increase in width to thickness ratio and load ratio leads to reduction of endurance time and the effect of width to thickness ratio on the ultimate strength of the column decreases with temperature increase.

  19. Ultrasonic Monitoring of CO2 Uptake and Release from Sand Packs*

    Science.gov (United States)

    Toffelmier, D. A.; Dufrane, W. L.; Bonner, B. P.; Viani, B. E.; Berge, P. A.

    2002-12-01

    Sequestration of atmospheric CO2 occurs naturally during the formation of calcite cement in sedimentary rock. Acceleration of this process has been proposed as a means of reducing the atmospheric concentration of CO2, which is a major cause of global warming. Calcite may also be precipitated when highly alkaline waste fluid is introduced into the vadose zone from leaking storage tanks. Seismic methods have potential for monitoring these processes. We devised an experiment, guided by geochemical modeling, to determine how the formation of calcite cement in unsaturated sand affects wave propagation. We used the ultrasonic pulse transmission method to measure compressional (P) and shear (S) wave velocities at ultrasonic frequencies (100-500 kHz) through packs of Ottawa sand containing chemically active pore fluids. The samples were saturated with water containing 0.1mol/L of Ca(OH)2 and 0.1mol/L of NaCl and then drained by flowing water saturated, CO2 free N2 gas, to a residual saturation of ~5%, so that the remaining pore fluid resides mainly in pendular spaces between the sand grains. Ambient air saturated with water and containing atmospheric concentration of CO2 was then passed through the sample to effect the precipitation of calcite. Finally, pure water saturated CO2, was flushed through the sample to dissolve most of the precipitated calcite. Over a three day period, measurable changes in Vp and Vs were observed following water saturation, desaturation, calcite precipitation, and calcite dissolution treatments. Changes in the contents of the pore space require waveforms to be recorded before and after each stage of the experiment so both the short and long range effects can be seen. Wave velocities were slow, as is typical for unconsolidated materials, for the dry sand, with values of 365m/s for Vp and 163m/s for Vs. Compressional velocities increased upon desaturation (443m/s), and again following calcite precipitation (460m/s). The compressional velocity measured following the CO2 flush to dissolve the calcite decreased (451m/s). The shear velocities varied similarly to the compressional velocities except that the dry sand shear velocity was faster than the other shear velocities. These preliminary results suggest that ultrasonics could provide a tool to locate the path of certain types of waste fluid in the vadose zone. *This work was performed under the auspices of the U.S. Department of Energy by the University of California, Lawrence Livermore National Laboratory under contract number W-7405-ENG-48 and was supported specifically by the Environmental Management Science Program of the Office of Environmental Management and the Office of Energy Research.

  20. Mush Column Magma Chambers

    Science.gov (United States)

    Marsh, B. D.

    2002-12-01

    Magma chambers are a necessary concept in understanding the chemical and physical evolution of magma. The concept may well be similar to a transfer function in circuit or time series analysis. It does what needs to be done to transform source magma into eruptible magma. In gravity and geodetic interpretations the causative body is (usually of necessity) geometrically simple and of limited vertical extent; it is clearly difficult to `see' through the uppermost manifestation of the concentrated magma. The presence of plutons in the upper crust has reinforced the view that magma chambers are large pots of magma, but as in the physical representation of a transfer function, actual magma chambers are clearly distinct from virtual magma chambers. Two key features to understanding magmatic systems are that they are vertically integrated over large distances (e.g., 30-100 km), and that all local magmatic processes are controlled by solidification fronts. Heat transfer considerations show that any viable volcanic system must be supported by a vertically extensive plumbing system. Field and geophysical studies point to a common theme of an interconnected stack of sill-like structures extending to great depth. This is a magmatic Mush Column. The large-scale (10s of km) structure resembles the vertical structure inferred at large volcanic centers like Hawaii (e.g., Ryan et al.), and the fine scale (10s to 100s of m) structure is exemplified by ophiolites and deeply eroded sill complexes like the Ferrar dolerites of the McMurdo Dry Valleys, Antarctica. The local length scales of the sill reservoirs and interconnecting conduits produce a rich spectrum of crystallization environments with distinct solidification time scales. Extensive horizontal and vertical mushy walls provide conditions conducive to specific processes of differentiation from solidification front instability to sidewall porous flow and wall rock slumping. The size, strength, and time series of eruptive behavior

  1. Behaviour of normal reinforced concrete columns exposed to different soils

    Directory of Open Access Journals (Sweden)

    Rasheed Laith

    2018-01-01

    Full Text Available Concrete resistance to sulfate attack is one of the most important characteristics for maintaining the durability of concrete. In this study, the effect of the attack of sulfate salts on normal reinforced concrete column was investigated by burying these columns in two types of soils (sandy and clayey in two pits at a depth of 3 m in one of the agricultural areas in the holy city of Karbala, one containing sandy soil (SO3 = 10.609% and the other containing clayey soil with (SO3 = 2.61%. The tests were used (pure axial compression test of reinforced concrete columns, compressive strength test, and splitting tensile strength test, absorption, voids ratio and finally density. It`s found that the strength of RC columns decreasing by (12.51% for age (240 days, for columns buried in clayey soil, where the strength increased by (11.71% for the same period, for columns buried in sandy soils, with respect to the reference column.

  2. Mitigating oil spills in the water column

    International Nuclear Information System (INIS)

    Barry, Edward; Libera, Joseph A.; Mane, Anil University; Avila, Jason R.; DeVitis, David

    2017-01-01

    The scale and scope of uncontrolled oil spills can be devastating. Diverse marine environments and fragile ecologies are some of the most susceptible to the many ill effects, while the economic costs can be crippling. A notoriously difficult challenge with no known technological solution is the successful removal of oil dispersed in the water column. Here, we address this problem through cheap and reusable oil sorbents based on the chemical modification of polymer foams. Interfacial chemistry was optimized and subsequently tested in a simulated marine environment at the National Oil Spill Response Research & Renewable Energy Test Facility, Ohmsett. We find favorable performance for surface oil mitigation and, for the first time, demonstrate the advanced sorbent's efficiency and efficacy at pilot scale in extraction of crude oil and refined petroleum products dispersed in the water column. As a result, this is a potentially disruptive technology, opening a new field of environmental science focused on sub-surface pollutant sequestration.

  3. HETP evaluation of structured packing distillation column

    Directory of Open Access Journals (Sweden)

    A. E. Orlando Jr.

    2009-09-01

    Full Text Available Several tests with a hydrocarbon mixture of known composition (C8-C14, obtained from DETEN Chemistry S.A., have been performed in a laboratory distillation column, having 40mm of nominal diameter and 2.2m high, with internals of Sulzer DX gauze stainless steel structured packing. The main purpose of this work was to evaluate HETP of a structured packing laboratory scale distillation column, operating continuously. Six HETP correlations available in the literature were compared in order to find out which is the most appropriate for structured packing columns working with medium distillates. Prior to the experimental tests, simulation studies using commercial software PRO/II® were performed in order to establish the optimum operational conditions for the distillation, especially concerning operating pressure, top and bottom temperatures, feed location and reflux ratio. The results of PRO/II® were very similar to the analysis of the products obtained during continuous operation, therefore permitting the use of the properties calculated by that software on the theoretical models investigated. The theoretical models chosen for HETP evaluation were: Bravo, Rocha and Fair (1985; Rocha, Bravo and Fair (1993, 1996; Brunazzi and Pagliant (1997; Carlo, Olujić and Pagliant (2006; Olujić et al., (2004. Modifications concerning calculation of specific areas were performed on the correlations in order to fit them for gauze packing HETP evaluation. As the laboratory distillation column was operated continuously, different HETP values were found by the models investigated for each section of the column. The low liquid flow rates in the top section of the column are a source of error for HETP evaluation by the models; therefore, more reliable HETP values were found in the bottom section, in which liquid flow rates were much greater. Among the theoretical models, Olujić et al. (2004 has shown good results relative to the experimental tests. In addition, the

  4. Column-Oriented Database Systems (Tutorial)

    NARCIS (Netherlands)

    D. Abadi; P.A. Boncz (Peter); S. Harizopoulos

    2009-01-01

    textabstractColumn-oriented database systems (column-stores) have attracted a lot of attention in the past few years. Column-stores, in a nutshell, store each database table column separately, with attribute values belonging to the same column stored contiguously, compressed, and densely packed, as

  5. EX1302 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1302: Ship Shakedown, Patch Test and...

  6. EX1301 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1301: Ship Shakedown and Patch Test...

  7. Comments on Simplified Calculation Method for Fire Exposed Concrete Columns

    DEFF Research Database (Denmark)

    Hertz, Kristian Dahl

    1998-01-01

    The author has developed new simplified calculation methods for fire exposed columns. Methods, which are found In ENV 1992-1-2 chapter 4.3 and in proposal for Danish code of Practise DS411 chapter 9. In the present supporting document the methods are derived and 50 eccentrically loaded fire expos...... columns are calculated and compared to results of full-scale tests. Furthermore 500 columns are calculated in order to present each test result related to a variation of the calculation in time of fire resistance....

  8. Effects of water content on reactive transport of Sr in Chernobyl sand columns

    International Nuclear Information System (INIS)

    Szenknect, S.; Dewiere, L.; Ardois, C.; Gaudet, J.P.

    2005-01-01

    Full text of publication follows: While transport of non-reactive solutes has been studied extensively in unsaturated porous media, much less is known about the factors that control the transport of sorbing solutes in unsaturated conditions. Three laboratory techniques were used to analyze the transport of Sr in the aeolian sand from Chernobyl Pilot Site [1] in both saturated and unsaturated flow conditions. Batch experiments were performed to study the chemical equilibrium state of the soil/solution system. Stirred flow-through reactor (SFTR) experiments were performed to study the kinetics and reversibility of sorption reactions at the surface of solid particles. Column experiments were also performed in saturated and unsaturated steady flow conditions. Experimental data pointed out a non-linear, instantaneous and reversible sorption process of Sr. A suitable cation-exchange model was used to describe the solute/soil reaction. The former model was coupled with transport models to describe behavior of Sr in saturated [2] and unsaturated flow conditions. Transport properties of sand packed columns have been determined with an inert tracer (HTO). BTCs obtained under saturated conditions exhibit a small amount of dispersion compared to those obtained under unsaturated conditions. Classical advection-dispersion model described successfully saturated tritium breakthrough curves (BTCs), whereas a mobile-immobile model (MIM) was required to described asymmetrical unsaturated BTCs. The MIM assumes that the porous medium contains a mobile water phase in which convective-dispersive transport occurs, and a immobile water phase with which solutes can exchange with a first order kinetic. In our experiments, transport by advection in the mobile phase is the predominant process whatever the flow conditions and mass transfer rate between the mobile and immobile regions is the predominant process for broadening the BTCs. Since dispersion is blurred by mass transfer resistance, the

  9. Evolution of strike-slip fault systems and associated geomorphic structures. Model test

    International Nuclear Information System (INIS)

    Ueta, Keichi

    2003-01-01

    Sandbox experiments were performed to investigate evolution of fault systems and its associated geomorphic structures caused by strike-slip motion on basement faults. A 200 cm long, 40 cm wide, 25 cm high sandbox was used in a strike-slip fault model test. Computerized X-ray tomography applied to the sandbox experiments made it possible to analyze the kinematic evaluation, as well as the three-dimensional geometry, of the faults. The deformation of the sand pack surface was analyzed by use of a laser method 3D scanner, which is a three-dimensional noncontact surface profiling instrument. A comparison of the experimental results with natural cases of active faults reveals the following: In the left-lateral strike-slip fault experiments, the deformation of the sand pack with increasing basement displacement is observed as follows. 1) In three dimensions, the right-stepping shears that have a cirque'/'shell'/'shipbody' shape develop on both sides of the basement fault. The shears on one side of the basement fault join those on the other side, resulting in helicoidal shaped shear surfaces. Shears reach the surface of the sand near or above the basement fault and en echelon Riedel shears are observed at the surface of the sand. The region between two Riedels is always an up-squeezed block. 2) lower-angle shears generally branch off from the first Riedel shears. 3) Pressure ridges develop within the zone defined by the right-stepping helicoidal shaped lower-angle shears. 4) Grabens develop between the pressure ridges. 5) Y-shears offset the pressure ridges. 6) With displacement concentrated on the central throughgoing fault zone, a liner trough developed directly above the basement fault. R1 shear and P foliation are observed in the liner trough. Such evolution of the shears and its associated structures in the fault model tests agrees well with that of strike-slip fault systems and its associated geomorphic structures. (author)

  10. Water Column Sonar Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — The collection and analysis of water column sonar data is a relatively new avenue of research into the marine environment. Primary uses include assessing biological...

  11. LIQUID-LIQUID EXTRACTION COLUMNS

    Science.gov (United States)

    Thornton, J.D.

    1957-12-31

    This patent relates to liquid-liquid extraction columns having a means for pulsing the liquid in the column to give it an oscillatory up and down movement, and consists of a packed column, an inlet pipe for the dispersed liquid phase and an outlet pipe for the continuous liquid phase located in the direct communication with the liquid in the lower part of said column, an inlet pipe for the continuous liquid phase and an outlet pipe for the dispersed liquid phase located in direct communication with the liquid in the upper part of said column, a tube having one end communicating with liquid in the lower part of said column and having its upper end located above the level of said outlet pipe for the dispersed phase, and a piston and cylinder connected to the upper end of said tube for applying a pulsating pneumatic pressure to the surface of the liquid in said tube so that said surface rises and falls in said tube.

  12. Column-Oriented Database Systems (Tutorial)

    OpenAIRE

    Abadi, D.; Boncz, Peter; Harizopoulos, S.

    2009-01-01

    textabstractColumn-oriented database systems (column-stores) have attracted a lot of attention in the past few years. Column-stores, in a nutshell, store each database table column separately, with attribute values belonging to the same column stored contiguously, compressed, and densely packed, as opposed to traditional database systems that store entire records (rows) one after the other. Reading a subset of a table’s columns becomes faster, at the potential expense of excessive disk-head s...

  13. Transformation of 3-chloroallyl alcohol in water-saturated subsoil studied with a column method

    NARCIS (Netherlands)

    Beltman, W.H.J.; Leistra, M.; Matser, A.M.

    1996-01-01

    The performance of a newly developed column method for pesticide transformation rate measurements in the subsoil was tested using (Z)- and (E)-3-chloroallyl alcohol as model compounds. The subsoil columns were filled in situ. In the column experiment the half-life ranged from 0.5-5.2 d for

  14. Impact of Holes on the Buckling of RHS Steel Column

    Directory of Open Access Journals (Sweden)

    Najla'a H. AL-Shareef

    2018-03-01

    Full Text Available This study presented an experimental and theoretical study on the effect of hole on the behavior of rectangular hollow steel columns subjected to axial compression load. Specimens were tested to investigated the ultimate capacity and the load- axial displacement behavior of steel columns. In this paper finite element analysis is done by using general purpose ANSYS 12.0 to investigate the behavior of rectangular hollow steel column with hole. In the experimental work, rectangular hollow steel columns with rounded corners were used in the constriction of the specimens which have dimensions of cross section (50*80mm and height of (250 and 500mm with thickness of (1.25,4 and 6mm with hole ((α*80*80mm when α is equal to (0.2,0.4,0.6 and 0.8. Twenty four columns under compression load were tested in order to investigate the effect of hole on the ultimate load of rectangular hollow steel column. The experimental results indicated that the typical failure  mode for all the tested hollow specimen was the local buckling. The tested results indicated that the increasing of hole dimension leads to reduction in ultimate loads of tested column to 75%. The results show the reducing of load by 94.7% due to decreasing  the thickness of  column while the hole size is constant (0.2*80*80. The buckling load decreases by 84.62% when hole position changes from Lo=0.25L to 0.75L. Holes can be made in the middle of column with dimension up to 0.4 of column's length. The AISC (2005 presents the values closest to the experimental results for the nominal yielding compressive strength. The effect for increasing of slendeness ratio and thickness to area ratio(t/A leading to decreacing the critical stresses and the failure of column with large size of hole and (t/A ratio less than 0.74% was due to lacal  buckling while the global buckling failure was abserve for column with small size of hole and (t/A ratio above than 0.74%. The compersion  between the experimental

  15. Radiotracer Imaging of Sediment Columns

    Science.gov (United States)

    Moses, W. W.; O'Neil, J. P.; Boutchko, R.; Nico, P. S.; Druhan, J. L.; Vandehey, N. T.

    2010-12-01

    Nuclear medical PET and SPECT cameras routinely image radioactivity concentration of gamma ray emitting isotopes (PET - 511 keV; SPECT - 75-300 keV). We have used nuclear medical imaging technology to study contaminant transport in sediment columns. Specifically, we use Tc-99m (T1/2 = 6 h, Eγ = 140 keV) and a SPECT camera to image the bacteria mediated reduction of pertechnetate, [Tc(VII)O4]- + Fe(II) → Tc(IV)O2 + Fe(III). A 45 mL bolus of Tc-99m (32 mCi) labeled sodium pertechnetate was infused into a column (35cm x 10cm Ø) containing uranium-contaminated subsurface sediment from the Rifle, CO site. A flow rate of 1.25 ml/min of artificial groundwater was maintained in the column. Using a GE Millennium VG camera, we imaged the column for 12 hours, acquiring 44 frames. As the microbes in the sediment were inactive, we expected most of the iron to be Fe(III). The images were consistent with this hypothesis, and the Tc-99m pertechnetate acted like a conservative tracer. Virtually no binding of the Tc-99m was observed, and while the bolus of activity propagated fairly uniformly through the column, some inhomogeneity attributed to sediment packing was observed. We expect that after augmentation by acetate, the bacteria will metabolically reduce Fe(III) to Fe(II), leading to significant Tc-99m binding. Imaging sediment columns using nuclear medicine techniques has many attractive features. Trace quantities of the radiolabeled compounds are used (micro- to nano- molar) and the half-lives of many of these tracers are short (Image of Tc-99m distribution in a column containing Rifle sediment at four times.

  16. Performance evaluation of a rectifier column using gamma column scanning

    Directory of Open Access Journals (Sweden)

    Aquino Denis D.

    2017-12-01

    Full Text Available Rectifier columns are considered to be a critical component in petroleum refineries and petrochemical processing installations as they are able to affect the overall performance of these facilities. It is deemed necessary to monitor the operational conditions of such vessels to optimize processes and prevent anomalies which could pose undesired consequences on product quality that might lead to huge financial losses. A rectifier column was subjected to gamma scanning using a 10-mCi Co-60 source and a 2-inch-long detector in tandem. Several scans were performed to gather information on the operating conditions of the column under different sets of operating parameters. The scan profiles revealed unexpected decreases in the radiation intensity at vapour levels between trays 2 and 3, and between trays 4 and 5. Flooding also occurred during several scans which could be attributed to parametric settings.

  17. Study on Predicting Axial Load Capacity of CFST Columns

    Science.gov (United States)

    Ravi Kumar, H.; Muthu, K. U.; Kumar, N. S.

    2017-11-01

    This work presents an analytical study and experimental study on the behaviour and ultimate load carrying capacity of axially compressed self-compacting concrete-filled steel tubular columns. Results of tests conducted by various researchers on 213 samples concrete-filled steel tubular columns are reported and present authors experimental data are reported. Two theoretical equations were derived for the prediction of the ultimate axial load strength of concrete-filled steel tubular columns. The results from prediction were compared with the experimental data. Validation to the experimental results was made.

  18. Numerical Simulation of Fluid Dynamics in a Monolithic Column

    Directory of Open Access Journals (Sweden)

    Kazuhiro Yamamoto

    2017-01-01

    Full Text Available As for the measurement of polycyclic aromatic hydrocarbons (PAHs, ultra-performance liquid chromatography (UPLC is used for PAH identification and densitometry. However, when a solvent containing a substance to be identified passes through a column of UPLC, a dedicated high-pressure-proof device is required. Recently, a liquid chromatography instrument using a monolithic column technology has been proposed to reduce the pressure of UPLC. The present study tested five types of monolithic columns produced in experiments. To simulate the flow field, the lattice Boltzmann method (LBM was used. The velocity profile was discussed to decrease the pressure drop in the ultra-performance liquid chromatography (UPLC system.

  19. Hydrodynamic Study Of Column Bioleaching Processes

    Directory of Open Access Journals (Sweden)

    Sadowski Zygmunt

    2015-06-01

    Full Text Available The modelling of flow leaching solution through the porous media has been considered. The heap bioleaching process can be tested using the column experimental equipment. This equipment was employed to the hydrodynamic studies of copper ore bioleaching. The copper ore (black shale ore with the support, inertial materials (glass small balls and polyethylene beads was used to the bioleaching tests. The packed beds were various composition, the ore/support ratio was changed. The correlation between the bed porosity and bioleaching kinetics, and copper recovery was investigated.

  20. Post column derivatisation analyses review. Is post-column derivatisation incompatible with modern HPLC columns?

    Science.gov (United States)

    Jones, Andrew; Pravadali-Cekic, Sercan; Dennis, Gary R; Shalliker, R Andrew

    2015-08-19

    Post Column derivatisation (PCD) coupled with high performance liquid chromatography or ultra-high performance liquid chromatography is a powerful tool in the modern analytical laboratory, or at least it should be. One drawback with PCD techniques is the extra post-column dead volume due to reaction coils used to enable adequate reaction time and the mixing of reagents which causes peak broadening, hence a loss of separation power. This loss of efficiency is counter-productive to modern HPLC technologies, -such as UHPLC. We reviewed 87 PCD methods published from 2009 to 2014. We restricted our review to methods published between 2009 and 2014, because we were interested in the uptake of PCD methods in UHPLC environments. Our review focused on a range of system parameters including: column dimensions, stationary phase and particle size, as well as the geometry of the reaction loop. The most commonly used column in the methods investigated was not in fact a modern UHPLC version with sub-2-micron, (or even sub-3-micron) particles, but rather, work-house columns, such as, 250 × 4.6 mm i.d. columns packed with 5 μm C18 particles. Reaction loops were varied, even within the same type of analysis, but the majority of methods employed loop systems with volumes greater than 500 μL. A second part of this review illustrated briefly the effect of dead volume on column performance. The experiment evaluated the change in resolution and separation efficiency of some weak to moderately retained solutes on a 250 × 4.6 mm i.d. column packed with 5 μm particles. The data showed that reaction loops beyond 100 μL resulted in a very serious loss of performance. Our study concluded that practitioners of PCD methods largely avoid the use of UHPLC-type column formats, so yes, very much, PCD is incompatible with the modern HPLC column. Copyright © 2015. Published by Elsevier B.V.

  1. Permanent magnet finger-size scanning electron microscope columns

    Energy Technology Data Exchange (ETDEWEB)

    Nelliyan, K., E-mail: elenk@nus.edu.sg [Department of Electrical and Computer Engineering, National University of Singapore, 4 Engineering Drive 3, Singapore 117576 (Singapore); Khursheed, A. [Department of Electrical and Computer Engineering, National University of Singapore, 4 Engineering Drive 3, Singapore 117576 (Singapore)

    2011-07-21

    This paper presents permanent magnet scanning electron microscope (SEM) designs for both tungsten and field emission guns. Each column makes use of permanent magnet technology and operates at a fixed primary beam voltage. A prototype column operating at a beam voltage of 15 kV was made and tested inside the specimen chamber of a conventional SEM. A small electrostatic stigmator unit and dedicated scanning coils were integrated into the column. The scan coils were wound directly around the objective lens iron core in order to reduce its size. Preliminary experimental images of a test grid specimen were obtained through the prototype finger-size column, demonstrating that it is in principle feasible.

  2. Permanent magnet finger-size scanning electron microscope columns

    International Nuclear Information System (INIS)

    Nelliyan, K.; Khursheed, A.

    2011-01-01

    This paper presents permanent magnet scanning electron microscope (SEM) designs for both tungsten and field emission guns. Each column makes use of permanent magnet technology and operates at a fixed primary beam voltage. A prototype column operating at a beam voltage of 15 kV was made and tested inside the specimen chamber of a conventional SEM. A small electrostatic stigmator unit and dedicated scanning coils were integrated into the column. The scan coils were wound directly around the objective lens iron core in order to reduce its size. Preliminary experimental images of a test grid specimen were obtained through the prototype finger-size column, demonstrating that it is in principle feasible.

  3. Fire response of composite columns subject to sway

    DEFF Research Database (Denmark)

    Virdi, Kuldeep

    Composite columns, using profiled steel sections encased in concrete or steel tubes filled with concrete, are increasingly used in practice taking advantage of speed of erection as well as offering cost-effective solutions. While the design of braced and unbraced composite columns under ambient...... conditions is adequately covered in the relevant standard, Eurocode 4, simplified design of unbraced composite columns for the fire limit state has not been included. Recognising this, a collaborative research project was undertaken with funding from the Research Fund for Coal and Steel. The paper describes...... the scope of the project which covered control tests under ambient conditions, carried out by the author while at City University London. Other aspects covered in the project included fire tests carried out by CTICM in France, on isolated columns and on two frames designed by Leibniz Universität Hannover...

  4. NOx retention in scrubbing column

    International Nuclear Information System (INIS)

    Nakazone, A.K.; Costa, R.E.; Lobao, A.S.T.; Matsuda, H.T.; Araujo, B.F.

    1988-07-01

    During the UO 2 dissolution in nitric acid, some different species of NO x are released. The off gas can either be refluxed to the dissolver or be released and retained on special columns. The final composition of the solution is the main parameter to take in account. A process for nitrous gases retention using scubber columns containing H 2 O or diluted HNO 3 is presented. Chemiluminescence measurement was employed to NO x evalution before and after scrubbing. Gas flow, temperature, residence time are the main parameters considered in this paper. For the dissolution of 100g UO 2 in 8M nitric acid, a 6NL/h O 2 flow was the best condition for the NO/NO 2 oxidation with maximum adsorption in the scrubber columns. (author) [pt

  5. Evaluation of Seismic Behaviors of Partially Deteriorated Reinforced Concrete Circular Columns Retrofitted with CFRP

    Directory of Open Access Journals (Sweden)

    Dongxu Hou

    2014-01-01

    Full Text Available Deficiency of the concrete strength in some regions of reinforced concrete (RC columns in practice may weaken the seismic behaviors of columns. Its effects on RC columns should be well understood. This paper aims to investigate the influences of deteriorated segment on the seismic behaviors of partially deteriorated RC columns and attempts to recover the seismic behaviors of partially deteriorated columns with Carbon Fiber Reinforced Polymer (CFRP composites. A finite element analysis was carried out to simulate the seismic behaviors of CFRP-confined partially deteriorated RC columns. The numerical results were verified by the laboratory tests of six specimens. Based on the finite element results, the failure location of partially deteriorated columns in an earthquake was predicted, and the effectiveness of CFRP retrofitted on partially deteriorated columns was evaluated.

  6. Employing anatomical knowledge in vertebral column labeling

    Science.gov (United States)

    Yao, Jianhua; Summers, Ronald M.

    2009-02-01

    The spinal column constitutes the central axis of human torso and is often used by radiologists to reference the location of organs in the chest and abdomen. However, visually identifying and labeling vertebrae is not trivial and can be timeconsuming. This paper presents an approach to automatically label vertebrae based on two pieces of anatomical knowledge: one vertebra has at most two attached ribs, and ribs are attached only to thoracic vertebrae. The spinal column is first extracted by a hybrid method using the watershed algorithm, directed acyclic graph search and a four-part vertebra model. Then curved reformations in sagittal and coronal directions are computed and aggregated intensity profiles along the spinal cord are analyzed to partition the spinal column into vertebrae. After that, candidates for rib bones are detected using features such as location, orientation, shape, size and density. Then a correspondence matrix is established to match ribs and vertebrae. The last vertebra (from thoracic to lumbar) with attached ribs is identified and labeled as T12. The rest of vertebrae are labeled accordingly. The method was tested on 50 CT scans and successfully labeled 48 of them. The two failed cases were mainly due to rudimentary ribs.

  7. Strength degradation of oxidized graphite support column in VHTR

    International Nuclear Information System (INIS)

    Park, Byung Ha; No, Hee Cheon

    2010-01-01

    Air-ingress events caused by large pipe breaks are important accidents considered in the design of Very High Temperature Gas-Cooled Reactors (VHTRs). A main safety concern for this type of event is the possibility of core collapse following the failure of the graphite support column, which can be oxidized by ingressed air. In this study, the main target is to predict the strength of the oxidized graphite support column. Through compression tests for fresh and oxidized graphite columns, the compressive strength of IG-110 was obtained. The buckling strength of the IG-110 column is expressed using the following empirical straight-line formula: σ cr,buckling =91.34-1.01(L/r). Graphite oxidation in Zone 1 is volume reaction and that in Zone 3 is surface reaction. We notice that the ultimate strength of the graphite column oxidized in Zones 1 and 3 only depends on the slenderness ratio and bulk density. Its strength degradation oxidized in Zone 1 is expressed in the following nondimensional form: σ/σ 0 =exp(-kd), k=0.114. We found that the strength degradation of a graphite column, oxidized in Zone 3, follows the above buckling empirical formula as the slenderness of the column changes. (author)

  8. Internet delivered question and answer column for patients with schizophrenia.

    Science.gov (United States)

    Maijala, Riikka; Anttila, Minna; Koivunen, Marita; Pitkänen, Anneli; Kuosmanen, Lauri; Välimäki, Maritta

    2015-01-01

    The purpose of this study was to describe the use of an Internet delivered question and answer column among patients with schizophrenia. The column was developed for research purposes. The study sample consisted of patients (N = 100) admitted to acute inpatient psychiatric care in two hospital districts. Descriptive data were collected from the column to which a nurse replied within 3 days and analysed using qualitative content analysis. The column had four to five questions weekly. The most common age of users was 18-24 years, and the gender distribution was almost equal. Column use was heaviest among students (44%) and least among unemployed people (19%). Out of 85 questions or comments sent to the column, 25 (29%) were related to program training and the remaining 60 (71%) were related to medication (31%), illness and tests (25%), other questions or comments (9%), daily life and coping with it (4%), and places to receive treatment (2%). An Internet delivered question and answer column can be included in the care of patients with schizophrenia. However, it requires a new type of basic and additional education in the field of mental health care in order for nurses to be able to provide nursing via the Internet forum.

  9. Experimental and Numerical Study of FRP Encased Composite Concrete Columns

    Directory of Open Access Journals (Sweden)

    Mohsen Ishaghian

    2017-02-01

    Full Text Available A new type of composite column is presented and assessed through experimental testing and numerical modeling. The objective of this research is to investigate design options for a composite column without the use of ferrous materials. This is to avoid the current problem of deterioration of concrete due to expansion of rusting reinforcement members. Such a target can be achieved by replacing the steel reinforcement of concrete columns with pultruded I-shape glass FRP structural sections. The composite column utilizes a glass FRP tube that surrounds a pultruded I-section glass FRP, which is subsequently filled with concrete. The GFRP tube acts as a stay-in-place form in addition to providing confinement to the concrete. A total of four composite columns were tested under monotonic axial loading. The experimental ultimate capacity of each of the tested composite column was compared to the predicted numerical capacity using ANSYS program. The comparison showed that the predicted numerical values were in good agreement with the experimental ones.

  10. Chromatographic properties PLOT multicapillary columns.

    Science.gov (United States)

    Nikolaeva, O A; Patrushev, Y V; Sidelnikov, V N

    2017-03-10

    Multicapillary columns (MCCs) for gas chromatography make it possible to perform high-speed analysis of the mixtures of gaseous and volatile substances at a relatively large amount of the loaded sample. The study was performed using PLOT MCCs for gas-solid chromatography (GSC) with different stationary phases (SP) based on alumina, silica and poly-(1-trimethylsilyl-1-propyne) (PTMSP) polymer as well as porous polymers divinylbenzene-styrene (DVB-St), divinylbenzene-vinylimidazole (DVB-VIm) and divinylbenzene-ethylene glycol dimethacrylate (DVB-EGD). These MCCs have the efficiency of 4000-10000 theoretical plates per meter (TP/m) and at a column length of 25-30cm can separate within 10-20s multicomponent mixtures of substances belonging to different classes of chemical compounds. The sample amount not overloading the column is 0.03-1μg and depends on the features of a porous layer. Examples of separations on some of the studied columns are considered. Copyright © 2017 Elsevier B.V. All rights reserved.

  11. Seismic performance of a grout-repaired construction defect in a column plastic hinge

    International Nuclear Information System (INIS)

    Budek, A.

    2006-01-01

    A column built to test the use of high-strength transverse reinforcement in seismically-loaded shear-critical columns was found to have a construction defect. The column was built to be loaded in double bending and as such was expected to develop two plastic hinges, one at each end of column. In the plastic hinge region at the column top, a void was formed because the concrete could not pass through the load stub's reinforcing steel cage. This void was repaired using nonshrink grout placed in a fluid state. The column was tested after repair and performed satisfactorily. The grouted repair was able to support large plastic rotations and allowed the column to reach a high level of ductility. The only effects of the repair were slightly reduced concrete dilation and stiffness in the repaired hinge. (author)

  12. Short steel and concrete columns under high temperatures

    Directory of Open Access Journals (Sweden)

    A. E. P. G. A. Jacintho

    Full Text Available The growing demand for knowledge about the effect of high temperatures on structures has stimulated increasing research worldwide. This article presents experimental results for short composite steel and concrete columns subjected to high temperatures in ovens with or without an axial compression load, numerically analyzes the temperature distribution in these columns after 30 and 60 minutes and compares them with experimental results. The models consist of concrete-filled tubes of three different thicknesses and two different diameters, and the concrete fill has conventional properties that remained constant for all of the models. The stress-strain behavior of the composite columns was altered after exposure to high temperatures relative to the same columns at room temperature, which was most evident in the 60-minute tests due to the higher temperatures reached. The computational analysis adopted temperature rise curves that were obtained experimentally.

  13. Column leaching from biomass combustion ashes

    DEFF Research Database (Denmark)

    Maresca, Alberto; Astrup, Thomas Fruergaard

    2015-01-01

    The utilization of biomass combustion ashes for forest soil liming and fertilizing has been addressed in literature. Though, a deep understanding of the ash chemical composition and leaching behavior is necessary to predict potential benefits and environmental risks related to this practice....... In this study, a fly ash sample from an operating Danish power plant based on wood biomass was collected, chemically characterized and investigated for its leaching release of nutrients and heavy metals. A column leaching test was employed. The strongly alkaline pH of all the collected eluates suggested...

  14. Column properties and flow profiles of a flat, wide column for high-pressure liquid chromatography.

    Science.gov (United States)

    Mriziq, Khaled S; Guiochon, Georges

    2008-04-11

    The design and the construction of a pressurized, flat, wide column for high-performance liquid chromatography (HPLC) are described. This apparatus, which is derived from instruments that implement over-pressured thin layer chromatography, can carry out only uni-dimensional chromatographic separations. However, it is intended to be the first step in the development of more powerful instruments that will be able to carry out two-dimensional chromatographic separations, in which case, the first separation would be a space-based separation, LC(x), taking place along one side of the bed and the second separation would be a time-based separation, LC(t), as in classical HPLC but proceeding along the flat column, not along a tube. The apparatus described consists of a pressurization chamber made of a Plexiglas block and a column chamber made of stainless steel. These two chambers are separated by a thin Mylar membrane. The column chamber is a cavity which is filled with a thick layer (ca. 1mm) of the stationary phase. Suitable solvent inlet and outlet ports are located on two opposite sides of the sorbent layer. The design allows the preparation of a homogenous sorbent layer suitable to be used as a chromatographic column, the achievement of effective seals of the stationary phase layer against the chamber edges, and the homogenous flow of the mobile phase along the chamber. The entire width of the sorbent layer area can be used to develop separations or elute samples. The reproducible performance of the apparatus is demonstrated by the chromatographic separations of different dyes. This instrument is essentially designed for testing detector arrays to be used in a two-dimensional LC(x) x LC(t) instrument. The further development of two-dimension separation chromatographs based on the apparatus described is sketched.

  15. Testing the Role of Microbial Ecology, Redox-Mediated Deep Water Production and Hypersalinity on TEX86: Lipids and 16s Sequences from Archaea and Bacteria in the Water Column and Sediments of Orca Basin

    Science.gov (United States)

    Warren, C.; Romero, I.; Ellis, G.; Goddard, E.; Krishnan, S.; Nigro, L. M.; Super, J. R.; Zhang, Y.; Zhuang, G.; Hollander, D. J.; Pagani, M.

    2014-12-01

    Mesophilic marine archaea and bacteria are known to substantially contribute to the oceanic microbial biomass and play critical roles in global carbon, nitrogen and nutrient cycles. The Orca Basin, a 2400 meter deep bathymetric depression on the continental slope of the north-central Gulf of Mexico, is an ideal environment to examine how redox-dependent biochemical processes control the input and cycling of bacterial and archaea-derived lipid compounds from formation in near-surface water, through secondary recycling processes operating at the redox-transition in the water column, to sedimentary diagenetic processes operating in oxic to anoxic zones within the basin. The lowermost 180 meters of the Orca Basin is characterized by an anoxic, hypersaline brine that is separated from the overlying oxic seawater by a well-defined redox sequence associated with a systematic increasing in salinity from 35 - 250‰. While surface water conditions are viewed as normal marine with a seasonally productive water column, the sub-oxic to anoxic transition zones within the deep-water column and the sediment spans over 200 m allowing the unique opportunity for discrete sampling of resident organisms and lipids. Here we present 16s rRNA sequence data of Bacteria and Archaea collected parallel to GDGT lipid profiles and in situ environmental measurements from the sediment and overlying water column in the intermediate zone of the basin, where movements of chemical transition zones are preserved. We evaluated GDGTs and corresponding taxa across the surface water, chlorophyll maximum, thermocline, and the deep redox boundary, including oxygenation, denitrification, manganese, iron and sulfate reduction zones, to determine if GDGTs are being produced under these conditions and how surface-derived GDGT lipids and the TEX86 signal may be altered. The results have implications for the application of the TEX86 paleotemperature proxy.

  16. Modeling of column apparatus processes

    CERN Document Server

    Boyadjiev, Christo; Boyadjiev, Boyan; Popova-Krumova, Petya

    2016-01-01

    This book presents a new approach for the modeling of chemical and interphase mass transfer processes in industrial column apparatuses, using convection-diffusion and average-concentration models. The convection-diffusion type models are used for a qualitative analysis of the processes and to assess the main, small and slight physical effects, and then reject the slight effects. As a result, the process mechanism can be identified. It also introduces average concentration models for quantitative analysis, which use the average values of the velocity and concentration over the cross-sectional area of the column. The new models are used to analyze different processes (simple and complex chemical reactions, absorption, adsorption and catalytic reactions), and make it possible to model the processes of gas purification with sulfur dioxide, which form the basis of several patents.

  17. Studies of column supported towers

    International Nuclear Information System (INIS)

    Chauvel, D.; Costaz, J.-L.

    1991-01-01

    As a result of a research and development programme into the civil engineering of cooling towers launched in 1978 by Electricite de France, very high cooling towers were built at Golfech and Chooz, in France, using column supports. This paper discusses the evolution of this new type of support from classical diagonal supports, presents some of the results of design calculations and survey measurements taken during construction of the shell and analyses the behaviour of the structure. (author)

  18. Calculation code PULCO for Purex process in pulsed column

    International Nuclear Information System (INIS)

    Gonda, Kozo; Matsuda, Teruo

    1982-03-01

    The calculation code PULCO, which can simulate the Purex process using a pulsed column as an extractor, has been developed. The PULCO is based on the fundamental concept of mass transfer that the mass transfer within a pulsed column occurs through the interface of liquid drops and continuous phase fluid, and is the calculation code different from conventional ones, by which various phenomena such as the generation of liquid drops, their rising and falling, and the unification of liquid drops actually occurring in a pulsed column are exactly reflected and can be correctly simulated. In the PULCO, the actually measured values of the fundamental quantities representing the extraction behavior of liquid drops in a pulsed column are incorporated, such as the mass transfer coefficient of each component, the diameter and velocity of liquid drops in a pulsed column, the holdup of dispersed phase, and axial turbulent flow diffusion coefficient. The verification of the results calculated with the PULCO was carried out by installing a pulsed column of 50 mm inside diameter and 2 m length with 40 plate stage in a glove box for unirradiated uranium-plutonium mixed system. The results of the calculation and test were in good agreement, and the validity of the PULCO was confirmed. (Kako, I.)

  19. Seismic performance of recycled concrete-filled square steel tube columns

    Science.gov (United States)

    Chen, Zongping; Jing, Chenggui; Xu, Jinjun; Zhang, Xianggang

    2017-01-01

    An experimental study on the seismic performance of recycled concrete-filled square steel tube (RCFST) columns is carried out. Six specimens were designed and tested under constant axial compression and cyclic lateral loading. Two parameters, replacement percentage of recycled coarse aggregate (RCA) and axial compression level, were considered in the test. Based on the experimental data, the hysteretic loops, skeleton curves, ductility, energy dissipation capacity and stiffness degradation of RCFST columns were analyzed. The test results indicate that the failure modes of RCFST columns are the local buckling of the steel tube at the bottom of the columns, and the hysteretic loops are full and their shapes are similar to normal CFST columns. Furthermore, the ductility coefficient of all specimens are close to 3.0, and the equivalent viscous damping coefficient corresponding to the ultimate lateral load ranges from 0.323 to 0.360, which demonstrates that RCFST columns exhibit remarkable seismic performance.

  20. Two generalizations of column-convex polygons

    International Nuclear Information System (INIS)

    Feretic, Svjetlan; Guttmann, Anthony J

    2009-01-01

    Column-convex polygons were first counted by area several decades ago, and the result was found to be a simple, rational, generating function. In this work we generalize that result. Let a p-column polyomino be a polyomino whose columns can have 1, 2, ..., p connected components. Then column-convex polygons are equivalent to 1-convex polyominoes. The area generating function of even the simplest generalization, namely 2-column polyominoes, is unlikely to be solvable. We therefore define two classes of polyominoes which interpolate between column-convex polygons and 2-column polyominoes. We derive the area generating functions of those two classes, using extensions of existing algorithms. The growth constants of both classes are greater than the growth constant of column-convex polyominoes. Rather tight lower bounds on the growth constants complement a comprehensive asymptotic analysis.

  1. 29 CFR 1926.755 - Column anchorage.

    Science.gov (United States)

    2010-07-01

    ... 29 Labor 8 2010-07-01 2010-07-01 false Column anchorage. 1926.755 Section 1926.755 Labor... (CONTINUED) SAFETY AND HEALTH REGULATIONS FOR CONSTRUCTION Steel Erection § 1926.755 Column anchorage. (a) General requirements for erection stability. (1) All columns shall be anchored by a minimum of 4 anchor...

  2. Adsorption columns for use in radioimmunoassays

    International Nuclear Information System (INIS)

    1976-01-01

    Adsorption columns are provided which can be utilized in radioimmunoassay systems such as those involving the separation of antibody-antigen complexes from free antigens. The preparation of the columns includes the treatment of retaining substrate material to render it hydrophilic, preparation and degassing of the separation material and loading the column

  3. Thermal process of an air column

    International Nuclear Information System (INIS)

    Lee, F.T.

    1994-01-01

    Thermal process of a hot air column is discussed based on laws of thermodynamics. The kinetic motion of the air mass in the column can be used as a power generator. Alternatively, the column can also function as a exhaust/cooler

  4. Influence of Connection Placement to the Behavior of Precast Concrete Exterior Beam-Column Joint

    Directory of Open Access Journals (Sweden)

    Elly Tjahjono

    2010-10-01

    Full Text Available This paper presents an experimental study on the influence of connection placement to the behaviour of exterior beamcolumn joint of precast concrete structure under semi cyclic loading. Four half-scale beam-column specimens were investigated. Three beam-columns were jointed through connection that are placed in beam-column joint region and the forth is connected at the plastic hinge potensial region of the beam. Crack patterns, strength, stiffness and ductility of the test specimens have been evaluated. The test result indicated that all beam-column specimens show good ductility behavior.

  5. Experimental analysis of reinforced concrete columns strengthened with Self-Compacting concrete

    Directory of Open Access Journals (Sweden)

    M. Y. M. Omar

    Full Text Available This paper presents the results of reinforced concrete columns strengthened by addition of a self-compacting concrete overlay at the compressed and at the tensioned face of the member, with and without addition of longitudinal steel bars. Eight columns were submit- ted to loading with an initial eccentricity of 60 mm . These columns had 120 mm x 250 mm of rectangular cross section, 2000 mm in length and four longitudinal reinforcement steel bars with 10 mm in diameter. Reference columns P1 and P2 were tested to failure without any type of rehabilitation. Columns P3 to P8 were loaded to a predefined load (close to the initial yield point of tension reinforce- ment, then unloaded and strengthened for a subsequent test until failure. Results showed that the method of rehabilitation used was effective, increasing the loading capacity of the strengthened pieces by 2 to 5 times the ultimate load of the reference column.

  6. Towards point of care testing for C. difficile infection by volatile profiling, using the combination of a short multi-capillary gas chromatography column with metal oxide sensor detection

    International Nuclear Information System (INIS)

    McGuire, N D; Ewen, R J; De Lacy Costello, B; Garner, C E; Vaughan, K; Ratcliffe, N M; Probert, C S J

    2014-01-01

    Rapid volatile profiling of stool sample headspace was achieved using a combination of short multi-capillary chromatography column (SMCC), highly sensitive heated metal oxide semiconductor sensor and artificial neural network software. For direct analysis of biological samples this prototype offers alternatives to conventional gas chromatography (GC) detectors and electronic nose technology. The performance was compared to an identical instrument incorporating a long single capillary column (LSCC). The ability of the prototypes to separate complex mixtures was assessed using gas standards and homogenized in house ‘standard’ stool samples, with both capable of detecting more than 24 peaks per sample. The elution time was considerably faster with the SMCC resulting in a run time of 10 min compared to 30 min for the LSCC. The diagnostic potential of the prototypes was assessed using 50 C. difficile positive and 50 negative samples. The prototypes demonstrated similar capability of discriminating between positive and negative samples with sensitivity and specificity of 85% and 80% respectively. C. difficile is an important cause of hospital acquired diarrhoea, with significant morbidity and mortality around the world. A device capable of rapidly diagnosing the disease at the point of care would reduce cases, deaths and financial burden. (paper)

  7. New method for evaluating irreversible adsorption and stationary phase bleed in gas chromatographic capillary columns.

    Science.gov (United States)

    Wright, Bob W; Wright, Cherylyn W

    2012-10-26

    A novel method is described for the evaluation of irreversible adsorption and column bleed in gas chromatographic (GC) columns using a tandem GC approach. This work specifically determined the degree of irreversible adsorption behavior of specific sulfur and phosphorous containing test probe compounds at levels ranging from approximately 50 picograms (pg) to 1 nanogram (ng) on selected gas chromatographic columns. This method does not replace existing evaluation methods that characterize reversible adsorption but provides an additional tool. The test compounds were selected due to their ease of adsorption and their importance in the specific trace analytical detection methodology being developed. Replicate chromatographic columns with 5% phenylmethylpolysiloxane (PMS), polyethylene glycol (wax), trifluoropropylpolysiloxane (TFP), or 78% cyanopropylpolysiloxane stationary phases from a variety of vendors were evaluated. As expected, the results demonstrate that the different chromatographic phases exhibit differing degrees of irreversible adsorption behavior. The results also indicate that all manufacturers do not produce equally inert columns nor are columns from a given manufacturer identical. The wax-coated columns for the test probes used were more inert as a group than 5% PMS coated columns, and they were more reproducibly manufactured. Both TFP and 78% cyanopropylpolysiloxane columns displayed superior inertness to the test compounds compared to either 5% PMS- or wax-coated columns. Irreversible adsorption behavior was characterized for a limited range of stationary phase film thicknesses. In addition, the method was shown effective for characterizing column bleed and methods to remove bleed components. This method is useful in screening columns for demanding applications and to obtain diagnostic information related to improved preparation methods. Copyright © 2012 Elsevier B.V. All rights reserved.

  8. Influence of Connection Placement to the Behavior of Precast Concrete Exterior Beam-Column Joint

    OpenAIRE

    Elly Tjahjono; Heru Purnomo

    2010-01-01

    This paper presents an experimental study on the influence of connection placement to the behaviour of exterior beamcolumn joint of precast concrete structure under semi cyclic loading. Four half-scale beam-column specimens were investigated. Three beam-columns were jointed through connection that are placed in beam-column joint region and the forth is connected at the plastic hinge potensial region of the beam. Crack patterns, strength, stiffness and ductility of the test specimens have been...

  9. Experimental Verification of the Structural Glass Beam-Columns Strength

    Science.gov (United States)

    Pešek, Ondřej; Melcher, Jindřich; Balázs, Ivan

    2017-10-01

    This paper deals with experimental research of axially and laterally loaded members made of structural (laminated) glass. The purpose of the research is the evaluation of buckling strength and actual behaviour of the beam-columns due to absence of standards for design of glass load-bearing structures. The experimental research follows the previous one focusing on measuring of initial geometrical imperfections of glass members, testing of glass beams and columns. Within the frame of the research 9 specimens were tested. All of them were of the same geometry (length 2000 mm, width 200 mm and thickness 16 mm) but different composition - laminated double glass made of annealed glass or fully tempered glass panes bonded together by PVB or EVASAFE foil. Specimens were at first loaded by axial force and then by constantly increasing bending moment up to failure. During testing lateral deflections, vertical deflection and normal stresses at mid-span were measured. A maximum load achieved during testing has been adopted as flexural-lateral-torsional buckling strength. The results of experiments were statistically evaluated according to the European standard for design of structures EN 1990, appendix D. There are significant differences between specimens made of annealed glass or fully tempered glass. Differences between specimens loaded by axial forces 1 kN and 2 kN are negligible. The next step was to determine the design strength by calculation procedure based on buckling curves approach intended for design of steel columns and develop interaction criterion for glass beams-columns.

  10. Pressure Control in Distillation Columns: A Model-Based Analysis

    DEFF Research Database (Denmark)

    Mauricio Iglesias, Miguel; Bisgaard, Thomas; Kristensen, Henrik

    2014-01-01

    A comprehensive assessment of pressure control in distillation columns is presented, including the consequences for composition control and energy consumption. Two types of representative control structures are modeled, analyzed, and benchmarked. A detailed simulation test, based on a real...... industrial distillation column, is used to assess the differences between the two control structures and to demonstrate the benefits of pressure control in the operation. In the second part of the article, a thermodynamic analysis is carried out to establish the influence of pressure on relative volatility...

  11. Gravity Effects on the Free Vibration of a Graphite Column

    International Nuclear Information System (INIS)

    Ki, Dong-Ok; Kim, Jong-Bum; Park, Keun-Bae; Lee, Won-Jae

    2006-01-01

    The gravity effects on the free vibration of a graphite column are studied. Graphite block is a key component of a HTGR (High Temperature Gas Cooled Reactor). The major core elements, such as the fuel blocks and neutron reflector blocks, of HTTR (High Temperature Test Reactor, Japan) and GT-MHR (Gas Turbine- Modular Helium Reactor, USA) consist of stacked hexagonal graphite blocks forming a group of columns. The vibration of the columns induced by earthquakes may lead to solid impacts between graphite blocks and structural integrity problems. The study of free vibration characteristics of the graphite block column is the first step in the core internal structure dynamic analysis. Gravity force bring a negative stiffness term to the transverse vibration analysis of heavy long column structures, and results in natural frequency reductions. Generally it is not considered in the not so tall structure cases, because the gravity term makes the analysis and design complicated. Therefore it is important to check whether the gravity effect is severe or not

  12. Development of pulsed plate columns for fast reactor fuel reprocessing

    International Nuclear Information System (INIS)

    Jenkins, J.A.; Logsdail, D.H.; Lyall, E.; Myers, P.E.; Partridge, B.A.

    1987-01-01

    The UK Atomic Energy Authority has undertaken a development programme on solvent extraction equipment for reprocessing fast reactor fuels. As part of this programme a solvent extraction pilot plant has been built at Harwell in which a variety of flowsheet conditions can be simulated using the system uranyl nitrate/nitric acid (UN/HNO 3 ) - 20% tri-n-butyl phosphate in odourless kerosene (TBP/OK). The main purpose of present pilot plant operations is to study the performance of pulsed plate columns, with the following specific objectives: to measure the volumetric throughput capacity of the columns, - to study the effect of scale-up of column diameter on U mass transfer performance, - to provide hydraulic and mass transfer data for a dynamic simulation model of pulsed column operation, - to develop and test instruments and ancillary equipment. This poster describes the pilot plant and is illustrated by experimental data, with particular reference to an external settler for controlling the removal of aqueous phase from columns operated with the aqueous phase dispersed

  13. Comparison of SX of uranium using mixer settler and columns

    International Nuclear Information System (INIS)

    Grinbaum, B.; Kotze, M.; Buchalter, E.

    2010-01-01

    Two types of equipment are used in the industry for solvent extraction (SX) of U: mixer-settlers (MS) and columns. Currently the only published type of columns applied in U SX is the Bateman Pulsed Columns (BPC). These columns have been applied for extraction of U for more than 13 years in Olympic Dam plant in Australia and in recent years were also introduced to additional plants in Australia and South Africa. Other plants are using MS of various types. The columns are currently used in the extraction battery only. For stripping and scrubbing only MS are currently used. Although pilot tests prove that the pH gradient required in the stripping may be successfully obtained in the BPC, they have not yet been applied in the industry. The paper compares the extraction and stripping in both types of equipment, regarding the capital cost, operating costs and operating conditions. The capital cost of the BPC is lower by 33-40%, depending on the size of the plant and the quality of the ore. The operating costs with the BPC are slightly lower, due to smaller losses of solvent. From operating point of view the BPC has the ability to recover from phase inversion and precipitation of yellow cake without the need to shut down the plant, if the problem is addressed within a few minutes. (author)

  14. Integrity of Bolted Angle Connections Subjected to Simulated Column Removal

    Science.gov (United States)

    Weigand, Jonathan M.; Berman, Jeffrey W.

    2016-01-01

    Large-scale tests of steel gravity framing systems (SGFSs) have shown that the connections are critical to the system integrity, when a column suffers damage that compromises its ability to carry gravity loads. When supporting columns were removed, the SGFSs redistributed gravity loads through the development of an alternate load path in a sustained tensile configuration resulting from large vertical deflections. The ability of the system to sustain such an alternate load path depends on the capacity of the gravity connections to remain intact after undergoing large rotation and axial extension demands, for which they were not designed. This study experimentally evaluates the performance of steel bolted angle connections subjected to loading consistent with an interior column removal. The characteristic connection behaviors are described and the performance of multiple connection configurations are compared in terms of their peak resistances and deformation capacities. PMID:27110059

  15. Experimental investigation on temperature distribution of foamed concrete filled steel tube column under standard fire

    Science.gov (United States)

    Kado, B.; Mohammad, S.; Lee, Y. H.; Shek, P. N.; Kadir, M. A. A.

    2018-04-01

    Standard fire test was carried out on 3 hollow steel tube and 6 foamed concrete filled steel tube columns. Temperature distribution on the columns was investigated. 1500 kg/m3 and 1800 kg/m3 foamed concrete density at 15%, 20% and 25% load level are the parameters considered. The columns investigated were 2400 mm long, 139.7 mm outer diameter and 6 mm steel tube thickness. The result shows that foamed concrete filled steel tube columns has the highest fire resistance of 43 minutes at 15% load level and low critical temperature of 671 ºC at 25% load level using 1500 kg/m3 foamed concrete density. Fire resistance of foamed concrete filled column increases with lower foamed concrete strength. Foamed concrete can be used to provide more fire resistance to hollow steel column or to replace normal weight concrete in concrete filled columns. Since filling hollow steel with foamed concrete produce column with high fire resistance than unfilled hollow steel column. Therefore normal weight concrete can be substituted with foamed concrete in concrete filled column, it will reduces the self-weight of the structure because of its light weight at the same time providing the desired fire resistance.

  16. Oscillating water column structural model

    Energy Technology Data Exchange (ETDEWEB)

    Copeland, Guild [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Bull, Diana L [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Jepsen, Richard Alan [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Gordon, Margaret Ellen [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)

    2014-09-01

    An oscillating water column (OWC) wave energy converter is a structure with an opening to the ocean below the free surface, i.e. a structure with a moonpool. Two structural models for a non-axisymmetric terminator design OWC, the Backward Bent Duct Buoy (BBDB) are discussed in this report. The results of this structural model design study are intended to inform experiments and modeling underway in support of the U.S. Department of Energy (DOE) initiated Reference Model Project (RMP). A detailed design developed by Re Vision Consulting used stiffeners and girders to stabilize the structure against the hydrostatic loads experienced by a BBDB device. Additional support plates were added to this structure to account for loads arising from the mooring line attachment points. A simplified structure was designed in a modular fashion. This simplified design allows easy alterations to the buoyancy chambers and uncomplicated analysis of resulting changes in buoyancy.

  17. Ultimate strength and ductility of steel reinforced concrete beam-columns

    International Nuclear Information System (INIS)

    Shohara, Ryoichi

    1991-01-01

    The ultimate strength and ductility of SRC beam-columns are investigated using the data gathered in Architectural Institute of Japan. Though the simple superposed strength formula in AIJ standard underestimates the strength of SRC beam-column failed in flexure, the generalized superposed strength formula estimates it satisfactory. The strength formula in AIJ standard does not good agreement with test data. The SRC beam-column failed in shear has almost equalductility with that failed in flexure owing to the encased steel. Author presents the formulas which estimate the ultimate deformation angle for SRC beam-columns. (author)

  18. Detection of uranium extraction zone by axial temperature profiles in a pulsed column for Purex process

    International Nuclear Information System (INIS)

    Tsukada, T.; Takahashi, K.

    1991-01-01

    A new method was presented for detecting uranium extraction zone in a pulsed column by means of measuring axial temperature profile originated from reaction heat during uranium extraction. Key parameters of the temperature profiles were estimated with a code developed for calculating temperature profiles in a direct-contact heat exchanger such as a pulsed column, and were verified using data from a small pulsed column simulating reaction heat with injecting hot water. Finally, the results were compared with those from an actual uranium extraction tests, indicating that the method presented was promising for detecting uranium extraction zone in a pulsed column. (author)

  19. FORTRAN program for calculating liquid-phase and gas-phase thermal diffusion column coefficients

    International Nuclear Information System (INIS)

    Rutherford, W.M.

    1980-01-01

    A computer program (COLCO) was developed for calculating thermal diffusion column coefficients from theory. The program, which is written in FORTRAN IV, can be used for both liquid-phase and gas-phase thermal diffusion columns. Column coefficients for the gas phase can be based on gas properties calculated from kinetic theory using tables of omega integrals or on tables of compiled physical properties as functions of temperature. Column coefficients for the liquid phase can be based on compiled physical property tables. Program listings, test data, sample output, and users manual are supplied for appendices

  20. Discussion on the Influence of Various Technological Parameters on Jet Grouting Columns Geometry

    Directory of Open Access Journals (Sweden)

    Bzówka Joanna

    2015-06-01

    Full Text Available One of the most popular elements created by using jet grouting technology are columns. During designing such columns, it is a problem of estimating their shape and dimensions. The main factors that influence on columns geometry are soil characteristic and technological parameters. At the frame of Authors scientific research, following technological factors were taken into account: system of jet grouting, injection pressure, dimension of nozzles and rotation speed during injection. In the paper some results of the field tests of jet grouting columns are presented

  1. Smart aggregate based damage detection of circular RC columns under cyclic combined loading

    International Nuclear Information System (INIS)

    Moslehy, Yashar; Belarbi, Abdeldjelil; Mo, Y L; Gu, Haichang; Song, Gangbing

    2010-01-01

    Structural health monitoring is an important issue for the maintenance of large-scale civil infrastructures, especially for bridge columns. In this paper, an innovative piezoceramic-based approach is developed for the structural health monitoring of reinforced concrete columns. An innovative piezoceramic-based device, the smart aggregate, is utilized as a transducer for the purpose of health monitoring. To investigate the seismic behavior of reinforced concrete (RC) bridge columns, structural health monitoring tests were performed on two bridge columns under combined reversed cyclic loading at the Missouri University of Science and Technology. The proposed smart aggregate based approach successfully evaluated the health status of concrete columns during the loading procedure. Sensor energy plots and 3D normalized sensor energy plots demonstrated that the damage inside attenuated the transmitted energy. The wavelet packet based damage index and sensor history damage index evaluate the damage development in concrete columns under cyclic loading

  2. Hemifield columns co-opt ocular dominance column structure in human achiasma.

    Science.gov (United States)

    Olman, Cheryl A; Bao, Pinglei; Engel, Stephen A; Grant, Andrea N; Purington, Chris; Qiu, Cheng; Schallmo, Michael-Paul; Tjan, Bosco S

    2018-01-01

    In the absence of an optic chiasm, visual input to the right eye is represented in primary visual cortex (V1) in the right hemisphere, while visual input to the left eye activates V1 in the left hemisphere. Retinotopic mapping In V1 reveals that in each hemisphere left and right visual hemifield representations are overlaid (Hoffmann et al., 2012). To explain how overlapping hemifield representations in V1 do not impair vision, we tested the hypothesis that visual projections from nasal and temporal retina create interdigitated left and right visual hemifield representations in V1, similar to the ocular dominance columns observed in neurotypical subjects (Victor et al., 2000). We used high-resolution fMRI at 7T to measure the spatial distribution of responses to left- and right-hemifield stimulation in one achiasmic subject. T 2 -weighted 2D Spin Echo images were acquired at 0.8mm isotropic resolution. The left eye was occluded. To the right eye, a presentation of flickering checkerboards alternated between the left and right visual fields in a blocked stimulus design. The participant performed a demanding orientation-discrimination task at fixation. A general linear model was used to estimate the preference of voxels in V1 to left- and right-hemifield stimulation. The spatial distribution of voxels with significant preference for each hemifield showed interdigitated clusters which densely packed V1 in the right hemisphere. The spatial distribution of hemifield-preference voxels in the achiasmic subject was stable between two days of testing and comparable in scale to that of human ocular dominance columns. These results are the first in vivo evidence showing that visual hemifield representations interdigitate in achiasmic V1 following a similar developmental course to that of ocular dominance columns in V1 with intact optic chiasm. Copyright © 2017 Elsevier Inc. All rights reserved.

  3. Local connections between the columns of the periaqueductal gray matter: a case for intrinsic neuromodulation.

    Science.gov (United States)

    Jansen, A S; Farkas, E; Mac Sams, J; Loewy, A D

    1998-02-16

    Chemical stimulation of the lateral or ventrolateral columns of the midbrain periaqueductal gray matter (PAG) in conscious animals produces opposite responses (viz., defensive behavior and pressor responses from the lateral column vs. quiescence and depressor responses from the ventrolateral column), raising the possibility that the two columns are interconnected. To test this hypothesis, two types of anatomical experiments were performed in rats. First, the anterograde axonal marker Phaseolus vulgaris leuco-agglutinin (PHA-L) was injected into individual PAG columns or adjoining regions which included the Edinger-Westphal, dorsal raphe, and precommissural nuclei. The results shows that each column projects bilaterally to all of the other PAG columns, and also provides local connections within its own column. Furthermore, the Edinger-Westphal and precommissural nuclei project to all four PAG columns, while the dorsal raphe nucleus projects only to the ventrolateral and lateral columns. In a second experiment, we found that cardiovascular-related PAG projection neurons of both the lateral and ventrolateral columns receive an input from the reciprocal PAG column. This was demonstrated by a double tracer neuroanatomical study in which PHA-L was first iontophoretically ejected into either the lateral or ventrolateral PAG columns and then, several days later the retrograde transneuronal viral tracer, pseudorabies virus, was injected into the stellate sympathetic ganglion. Intra-PAG circuits were visualized by a dual immunohistochemical procedure. These results suggest that during the fight-or-flight response when the 'fight' program is activated, inhibition of the 'flight' PAG network may occur and the converse situation may occur during the flight response. Copyright 1997 Elsevier Science B.V.

  4. Cyclic behavior of non-seismically designed interior reinforced concrete beam-column connections

    Directory of Open Access Journals (Sweden)

    Amorn Pimanmas

    2008-05-01

    Full Text Available This paper presents a test of non-seismically detailed reinforced concrete beam-column connections under reversedcyclic load. The tested specimens represented those of the actual mid-rise reinforced concrete frame buildings, designedaccording to the non-seismic provisions of the ACI building code. The evaluation of 10 existing reinforced concrete frameswas conducted to identify key structural and geometrical indices. It was found that there existed correlation VS structuraland geometrical characteristics and the column tributary area. Hence, the column tributary area was chosen as a parameterfor classifying the specimens. The test results showed that specimens representing small and medium column tributary areafailed by brittle joint shear, while specimen representing large column tributary area failed by ductile flexure, even thoughno ductile seismic details were provided.

  5. Laser surface wakefield in a plasma column

    International Nuclear Information System (INIS)

    Gorbunov, L.M.; Mora, P.; Ramazashvili, R.R.

    2003-01-01

    The structure of the wakefield in a plasma column, produced by a short intense laser pulse, propagating through a gas affected by tunneling ionization is investigated. It is shown that besides the usual plasma waves in the bulk part of the plasma column [see Andreev et al., Phys. Plasmas 9, 3999 (2002)], the laser pulse also generates electromagnetic surface waves propagating along the column boundary. The length of the surface wake wave substantially exceeds the length of the plasma wake wave and its electromagnetic field extends far outside the plasma column

  6. Graphite oxidation and structural strength of graphite support column in VHTR

    International Nuclear Information System (INIS)

    Park, Byung Ha; No, Hee Cheno; Kim, Eung Soo; Oh, Chang H.

    2009-01-01

    The air-ingress event by a large pipe break is an important accident considered in design of very high-temperature gas-cooled reactors (VHTR). Core-collapse prediction is a main safety issue. Structural failure model are technically required. The objective of this study is to develop structural failure model for the supporting graphite material in the lower plenum of the GT-MHR (gas-turbine-modular high temperature reactor). Graphite support column is important for VHTR structural integrity. Graphite support columns are under the axial load. Critical strength of graphite column is related to slenderness ratio and bulk density. Through compression tests for fresh and oxidized graphite columns we show that compressive strength of IG-110 was 79.46 MPa. And, the buckling strength of IG-110 column was expressed by the empirical formula: σ 0 =σ straight-line - C L/r, σ straight-line =91.31 MPa, C=1.01. The results of uniform and non-uniform oxidation tests show that the strength degradation of oxidized graphite column is expressed in the following non-dimensional form: σ/σ 0 =exp(-kd), k=0.111. Also, from the results of the uniform oxidation test with a complicated-shape column, we found out that the above non-dimensional equation obtained from the uniform oxidation test is applicable to a uniform oxidation case with a complicated-shape column. (author)

  7. Failure Investigation of Debonded Sandwich Columns: An Experimental and Numerical Study

    DEFF Research Database (Denmark)

    Moslemian, Ramin; Berggreen, Christian; Carlsson, Leif A.

    2009-01-01

    Failure of compression loaded sandwich columns with an implanted through-width face/core debond is examined. Compression tests were conducted on sandwich columns containing implemented face/core debonds. The strains and out-of-plane displacements of the debonded region were monitored using the di...

  8. Carbon dioxide degassing in fresh and saline water I: Degassing performance of a cascade column

    DEFF Research Database (Denmark)

    Moran, Damian

    2010-01-01

    A study was undertaken to measure carbon dioxide degassing in a cascade column operating with both fresh (0‰) and saline water (35‰ NaCl) at 15 °C. The cascade column contained bio-block type packing material, was 1.7 m long in each dimension, and was tested both with and without countercurrent a...

  9. SPR Hydrostatic Column Model Verification and Validation.

    Energy Technology Data Exchange (ETDEWEB)

    Bettin, Giorgia [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Lord, David [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Rudeen, David Keith [Gram, Inc. Albuquerque, NM (United States)

    2015-10-01

    A Hydrostatic Column Model (HCM) was developed to help differentiate between normal "tight" well behavior and small-leak behavior under nitrogen for testing the pressure integrity of crude oil storage wells at the U.S. Strategic Petroleum Reserve. This effort was motivated by steady, yet distinct, pressure behavior of a series of Big Hill caverns that have been placed under nitrogen for extended period of time. This report describes the HCM model, its functional requirements, the model structure and the verification and validation process. Different modes of operation are also described, which illustrate how the software can be used to model extended nitrogen monitoring and Mechanical Integrity Tests by predicting wellhead pressures along with nitrogen interface movements. Model verification has shown that the program runs correctly and it is implemented as intended. The cavern BH101 long term nitrogen test was used to validate the model which showed very good agreement with measured data. This supports the claim that the model is, in fact, capturing the relevant physical phenomena and can be used to make accurate predictions of both wellhead pressure and interface movements.

  10. Column: Factors Affecting Data Decay

    Directory of Open Access Journals (Sweden)

    Kevin Fairbanks

    2012-06-01

    Full Text Available In nuclear physics, the phrase decay rate is used to denote the rate that atoms and other particles spontaneously decompose. Uranium-235 famously decays into a variety of daughter isotopes including Thorium and Neptunium, which themselves decay to others. Decay rates are widely observed and wildly different depending on many factors, both internal and external. U-235 has a half-life of 703,800,000 years, for example, while free neutrons have a half-life of 611 seconds and neutrons in an atomic nucleus are stable.We posit that data in computer systems also experiences some kind of statistical decay process and thus also has a discernible decay rate. Like atomic decay, data decay fluctuates wildly. But unlike atomic decay, data decay rates are the result of so many different interplaying processes that we currently do not understand them well enough to come up with quantifiable numbers. Nevertheless, we believe that it is useful to discuss some of the factors that impact the data decay rate, for these factors frequently determine whether useful data about a subject can be recovered by forensic investigation.(see PDF for full column

  11. Gaseous carbon dioxide absorbing column

    International Nuclear Information System (INIS)

    Harashina, Heihachi.

    1994-01-01

    The absorbing column of the present invention comprises a cyclone to which CO 2 gas and Ca(OH) 2 are blown to form CaCO 3 , a water supply means connected to an upper portion of the cyclone for forming a thin water membrane on the inner wall thereof, and a water processing means connected to a lower portion of the cyclone for draining water incorporating CaCO 3 . If a mixed fluid of CO 2 gas and Ca(OH) 2 is blown in a state where a flowing water membrane is formed on the inner wall of the cyclone, formation of CaCO 3 is promoted also in the inside of the cyclone in addition to the formation of CaCO 3 in the course of blowing. Then, formed CaCO 3 is discharged from the lower portion of the cyclone together with downwardly flowing water. With such procedures, solid contents such as CaCO 3 separated at the inner circumferential wall are sent into the thin water membrane, adsorbed and captured, and the solid contents are successively washed out, so that a phenomenon that the solid contents deposit and grow on the inner wall of the cyclone can be prevented effectively. (T.M.)

  12. Rasch models with exchangeable rows and columns

    DEFF Research Database (Denmark)

    Lauritzen, Steffen Lilholt

    The article studies distributions of doubly infinite binary matrices with exchangeable rows and columns which satify the further property that the probability of any $m \\times n$ submatrix is a function of the row- and column sums of that matrix. We show that any such distribution is a (unique...

  13. The general packed column : an analytical solution

    NARCIS (Netherlands)

    Gielen, J.L.W.

    2000-01-01

    The transient behaviour of a packed column is considered. The column, uniformly packed on a macroscopic scale, is multi-structured on the microscopic level: the solid phase consists of particles, which may differ in incidence, shape or size, and other relevant physical properties. Transport in the

  14. Fringing-field effects in acceleration columns

    International Nuclear Information System (INIS)

    Yavor, M.I.; Weick, H.; Wollnik, H.

    1999-01-01

    Fringing-field effects in acceleration columns are investigated, based on the fringing-field integral method. Transfer matrices at the effective boundaries of the acceleration column are obtained, as well as the general transfer matrix of the region separating two homogeneous electrostatic fields with different field strengths. The accuracy of the fringing-field integral method is investigated

  15. Water Column Exploration Field Trial I (EX0904, EM302) aboard the NOAA Ship Okeanos Explorer in the Gorda Ridge, off the coasts of Oregon and California

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — This cruise is a water column exploration field trial cruise, designed to test and refine operations for conducting water column exploration using NOAA Ship Okeanos...

  16. Evaluation of chromatographic columns packed with semi- and fully porous particles for benzimidazoles separation.

    Science.gov (United States)

    Gonzalo-Lumbreras, Raquel; Sanz-Landaluze, Jon; Cámara, Carmen

    2015-07-01

    The behavior of 15 benzimidazoles, including their main metabolites, using several C18 columns with standard or narrow-bore diameters and different particle size and type were evaluated. These commercial columns were selected because their differences could affect separation of benzimidazoles, and so they can be used as alternative columns. A simple screening method for the analysis of benzimidazole residues and their main metabolites was developed. First, the separation of benzimidazoles was optimized using a Kinetex C18 column; later, analytical performances of other columns using the above optimized conditions were compared and then individually re-optimized. Critical pairs resolution, analysis run time, column type and characteristics, and selectivity were considered for chromatographic columns comparison. Kinetex XB was selected because it provides the shortest analysis time and the best resolution of critical pairs. Using this column, the separation conditions were re-optimized using a factorial design. Separations obtained with the different columns tested can be applied to the analysis of specific benzimidazoles residues or other applications. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  17. Seismic fragility analysis of lap-spliced reinforced concrete columns retrofitted by SMA wire jackets

    International Nuclear Information System (INIS)

    Choi, Eunsoo; Park, Sun-Hee; Chung, Young-Soo; Kim, Hee Sun

    2013-01-01

    The aim of this study is to provide seismic fragility curves of reinforced concrete columns retrofitted by shape memory alloy wire jackets and thus assess the seismic performance of the columns against earthquakes, comparing them with reinforced concrete columns with lap-spliced and continuous reinforcement. For that purpose, this study first developed analytical models of the experimental results of the three types of columns, (1) lap-spliced reinforcement, (2) continuous reinforcement and (3) lap-spliced reinforcement and retrofitted by SMA wire jackets, using the OpenSEES program, which is oriented to nonlinear dynamic analysis. Then, a suite of ten recorded ground motions was used to conduct dynamic analyses of the analytical models with scaling of the peak ground acceleration from 0.1g to 1.0g in steps of 0.1g. From the static experimental tests, the column retrofitted with SMA wire jackets had a larger displacement ductility by a factor of 2.3 times that of the lap-spliced column, which was 6% larger compared with the ductility of the continuous reinforcement column. From the fragility analyses, the SMA wire jacketed column had median values of 0.162g and 0.567g for yield and collapse, respectively. For the yield damage state, the SMA wire jacketed column had a median value similar to the continuous reinforcement column. However, for the complete damage state, the SMA wire jacketed column showed a 1.33 times larger median value than the continuously reinforcement column. (paper)

  18. Admittance Scanning for Whole Column Detection.

    Science.gov (United States)

    Stamos, Brian N; Dasgupta, Purnendu K; Ohira, Shin-Ichi

    2017-07-05

    Whole column detection (WCD) is as old as chromatography itself. WCD requires an ability to interrogate column contents from the outside. Other than the obvious case of optical detection through a transparent column, admittance (often termed contactless conductance) measurements can also sense changes in the column contents (especially ionic content) from the outside without galvanic contact with the solution. We propose here electromechanically scanned admittance imaging and apply this to open tubular (OT) chromatography. The detector scans across the column; the length resolution depends on the scanning velocity and the data acquisition frequency, ultimately limited by the physical step resolution (40 μm in the present setup). Precision equal to this step resolution was observed for locating an interface between two immiscible liquids inside a 21 μm capillary. Mechanically, the maximum scanning speed was 100 mm/s, but at 1 kHz sampling rate and a time constant of 25 ms, the highest practical scan speed (no peak distortion) was 28 mm/s. At scanning speeds of 0, 4, and 28 mm/s, the S/N for 180 pL (zone length of 1.9 mm in a 11 μm i.d. column) of 500 μM KCl injected into water was 6450, 3850, and 1500, respectively. To facilitate constant and reproducible contact with the column regardless of minor variations in outer diameter, a double quadrupole electrode system was developed. Columns of significant length (>1 m) can be readily scanned. We demonstrate its applicability with both OT and commercial packed columns and explore uniformity of retention along a column, increasing S/N by stopped-flow repeat scans, etc. as unique applications.

  19. Temperature of Steel Columns under Natural Fire

    Directory of Open Access Journals (Sweden)

    F. Wald

    2004-01-01

    Full Text Available Current fire design models for time-temperature development within structural elements as well as for structural behaviour are based on isolated member tests subjected to standard fire regimes, which serve as a reference heating, but do not model natural fire. Only tests on a real structure under a natural fire can evaluate future models of the temperature developments in a fire compartment, of the transfer of heat into the structure and of the overall structural behaviour under fire.To study overall structural behaviour, a research project was conducted on an eight storey steel frame building at the  Cardington Building Research Establishment laboratory on January 16, 2003. A fire compartment 11×7 m was prepared on the fourth floor. A fire load of 40 kg/m2 was applied with 100 % permanent mechanical load and 65 % of imposed load. The paper summarises the experimental programme and shows the temperature development of the gas in the fire compartment and of the fire protected columns bearing the unprotected floors.

  20. Seismic Performance of High-Ductile Fiber-Reinforced Concrete Short Columns

    Directory of Open Access Journals (Sweden)

    Mingke Deng

    2018-01-01

    Full Text Available This study mainly aims to investigate the effectiveness of high-ductile fiber-reinforced concrete (HDC as a means to enhance the seismic performance of short columns. Six HDC short columns and one reinforced concrete (RC short column were designed and tested under lateral cyclic loading. The influence of the material type (concrete or HDC, axial load, stirrup ratio, and shear span ratio on crack patterns, hysteresis behavior, shear strength, deformation capacity, energy dissipation, and stiffness degradation was presented and discussed, respectively. The test results show that the RC short column failed in brittle shear with poor energy dissipation, while using HDC to replace concrete can effectively improve the seismic behavior of the short columns. Compared with the RC short column, the shear strength of HDC specimens was improved by 12.6–30.2%, and the drift ratio and the energy dissipation increases were 56.9–88.5% and 237.7–336.7%, respectively, at the ultimate displacement. Additionally, the prediction model of the shear strength for RC columns based on GB50010-2010 (Chinese code can be safely adopted to evaluate the shear strength of HDC short columns.

  1. Column Grid Array Rework for High Reliability

    Science.gov (United States)

    Mehta, Atul C.; Bodie, Charles C.

    2008-01-01

    Due to requirements for reduced size and weight, use of grid array packages in space applications has become common place. To meet the requirement of high reliability and high number of I/Os, ceramic column grid array packages (CCGA) were selected for major electronic components used in next MARS Rover mission (specifically high density Field Programmable Gate Arrays). ABSTRACT The probability of removal and replacement of these devices on the actual flight printed wiring board assemblies is deemed to be very high because of last minute discoveries in final test which will dictate changes in the firmware. The questions and challenges presented to the manufacturing organizations engaged in the production of high reliability electronic assemblies are, Is the reliability of the PWBA adversely affected by rework (removal and replacement) of the CGA package? and How many times can we rework the same board without destroying a pad or degrading the lifetime of the assembly? To answer these questions, the most complex printed wiring board assembly used by the project was chosen to be used as the test vehicle, the PWB was modified to provide a daisy chain pattern, and a number of bare PWB s were acquired to this modified design. Non-functional 624 pin CGA packages with internal daisy chained matching the pattern on the PWB were procured. The combination of the modified PWB and the daisy chained packages enables continuity measurements of every soldered contact during subsequent testing and thermal cycling. Several test vehicles boards were assembled, reworked and then thermal cycled to assess the reliability of the solder joints and board material including pads and traces near the CGA. The details of rework process and results of thermal cycling are presented in this paper.

  2. A cryogenic distillation column cascade for a fusion reactor

    International Nuclear Information System (INIS)

    Kinoshita, M.

    1984-01-01

    A cryogenic distillation column cascade composed of only two columns is proposed. Compared with the Tritium Systems Test Assembly (TSTA) cascade, the tritium inventory is about 1.5 times more and the packed height of the highest column increases by about 40%. However, the number of the columns is halved with the separation performance unchanged. The number of the instruments needed and the number of the process parameters to be monitored are also reduced. Unlike in the case of the TSTA cascade, the performance of the proposed cascade is not subject to the flow rate of the neutral beam injector recycle stream. The high performance can be maintained even if the protium percentage in the raw fuel input increases significantly (e.g., from 1 to 3%), just by adjusting the flow rates of the top, bottom, and side streams. Because of this great flexibility, it is worthwhile to build and study the proposed cascade as a possible alternative to the TSTA cascade

  3. Collapse of tall granular columns in fluid

    Science.gov (United States)

    Kumar, Krishna; Soga, Kenichi; Delenne, Jean-Yves

    2017-06-01

    Avalanches, landslides, and debris flows are geophysical hazards, which involve rapid mass movement of granular solids, water, and air as a multi-phase system. In order to describe the mechanism of immersed granular flows, it is important to consider both the dynamics of the solid phase and the role of the ambient fluid. In the present study, the collapse of a granular column in fluid is studied using 2D LBM - DEM. The flow kinematics are compared with the dry and buoyant granular collapse to understand the influence of hydrodynamic forces and lubrication on the run-out. In the case of tall columns, the amount of material destabilised above the failure plane is larger than that of short columns. Therefore, the surface area of the mobilised mass that interacts with the surrounding fluid in tall columns is significantly higher than the short columns. This increase in the area of soil - fluid interaction results in an increase in the formation of turbulent vortices thereby altering the deposit morphology. It is observed that the vortices result in the formation of heaps that significantly affects the distribution of mass in the flow. In order to understand the behaviour of tall columns, the run-out behaviour of a dense granular column with an initial aspect ratio of 6 is studied. The collapse behaviour is analysed for different slope angles: 0°, 2.5°, 5° and 7.5°.

  4. Field Applications of Gamma Column Scanning Technology

    International Nuclear Information System (INIS)

    Aquino, Denis D.; Mallilin, Janice P.; Nuñez, Ivy Angelica A.; Bulos, Adelina DM.

    2015-01-01

    The Isotope Techniques Section (ITS) under the Nuclear Service Division (NSD) of the Philippine Nuclear Research Institute (PNRI) conducts services, research and development on radioisotope and sealed source application in the industry. This aims to benefit the manufacturing industries such as petroleum, petrochemical, chemical, energy, waste, column treatment plant, etc. through on line inspection and troubleshooting of a process vessel, column or pipe that could optimize the process operation and increase production efficiency. One of the most common sealed source techniques for industrial applications is the gamma column scanning technology. Gamma column scanning technology is an established technique for inspection, analysis and diagnosis of industrial columns for process optimization, solving operational malfunctions and management of resources. It is a convenient non-intrusive, cost effective and cost-efficient technique to examine inner details of an industrial process vessel such as a distillation column while it is in operation. The Philippine Nuclear Research Institute (PNRI) recognize the importance and benefits of this technology and has implemented activities to make gamma column scanning locally available to benefit the Philippine industries. Continuous effort for capacity building is being pursued thru the implementation of in-house and on-the-job training abroad and upgrading of equipment. (author)

  5. Numerical Evaluation on the Different Shapes of Gravelly Sand Columns to Increase the Loading Capacity of Soft Clay

    Directory of Open Access Journals (Sweden)

    Meghzili Sif Allah

    2017-01-01

    Full Text Available Improvement on soft clay by the installation of stone column is one of the most popular methods followed worldwide. Different analytical and numerical solutions have already been developed for understanding the load transfer mechanism of soft soil reinforced with stone column. This study investigated a bearing capacity of the gravelly sand column, installed in soft clay bed at 15kpa of undrained shear strength. The column variable of length and diameter ratio at 7, 8 and 9 were evaluated. On top of that, the combination of two diameters in single column was tested and the uniform diameter was used as a control. In the numerical analysis, Mohrcoulomb model was adopted in the idealization of the behaviour of the gravelly sand column and soft clay materials. The results revealed that the optimum design that gave the highest loading capacity of the combination 11=12 of column diameter was the length and diameter ratio of 8.

  6. Dynamic effects of diabatization in distillation columns

    DEFF Research Database (Denmark)

    Bisgaard, Thomas; Huusom, Jakob Kjøbsted; Abildskov, Jens

    2013-01-01

    The dynamic effects of diabatization in distillation columns are investigated in simulation emphasizing the heat-integrated distillation column (HIDiC). A generic, dynamic, first-principle model has been formulated, which is flexible enough to describe various diabatic distillation configurations....... Dynamic Relative Gain Array and Singular Value Analysis have been applied in a comparative study of a conventional distillation column and a HIDiC. The study showed increased input-output coupling due to diabatization. Feasible SISO control structures for the HIDiC were also found and control...

  7. Dynamic Effects of Diabatization in Distillation Columns

    DEFF Research Database (Denmark)

    Bisgaard, Thomas; Huusom, Jakob Kjøbsted; Abildskov, Jens

    2012-01-01

    The dynamic eects of diabatization in distillation columns are investigated in simulation with primary focus on the heat-integrated distillation column (HIDiC). A generic, dynamic, rst-principle model has been formulated, which is exible to describe various diabatic distillation congurations....... Dynamic Relative Gain Array and Singular Value Analysis have been applied in a comparative study of a conventional distillation column and a HIDiC. The study showed increased input-output coupling due to diabatization. Feasible SISO control structures for the HIDiC were also found. Control...

  8. Column-oriented database management systems

    OpenAIRE

    Možina, David

    2013-01-01

    In the following thesis I will present column-oriented database. Among other things, I will answer on a question why there is a need for a column-oriented database. In recent years there have been a lot of attention regarding a column-oriented database, even if the existence of a columnar database management systems dates back in the early seventies of the last century. I will compare both systems for a database management – a colum-oriented database system and a row-oriented database system ...

  9. Steel hollow columns with an internal profile filled with self-compacting concrete under fire conditions

    OpenAIRE

    Chu, Thi Binh; Gernay, Thomas; Dotreppe, Jean-Claude; Franssen, Jean-Marc

    2016-01-01

    A detailed experimental and numerical investigation has been performed on the behavior under fire conditions of concrete filled steel hollow section (CFSHS) columns. In this study the internal reinforcement consists of another profile (tube or H section) being embedded with the concrete, and filling is realized by self-compacting concrete (SCC). Ten columns filled with self-compacting concrete embedding another steel profile have been tested in the Fire Testing Laboratory of the University of...

  10. Empirical Approach for Determining Axial Strength of Circular Concrete Filled Steel Tubular Columns

    Science.gov (United States)

    Jayalekshmi, S.; Jegadesh, J. S. Sankar; Goel, Abhishek

    2018-03-01

    The concrete filled steel tubular (CFST) columns are highly regarded in recent years as an interesting option in the construction field by designers and structural engineers, due to their exquisite structural performance, with enhanced load bearing capacity and energy absorption capacity. This study presents a new approach to simulate the capacity of circular CFST columns under axial loading condition, using a large database of experimental results by applying artificial neural network (ANN). A well trained network is established and is used to simulate the axial capacity of CFST columns. The validation and testing of the ANN is carried out. The current study is focused on proposing a simplified equation that can predict the ultimate strength of the axially loaded columns with high level of accuracy. The predicted results are compared with five existing analytical models which estimate the strength of the CFST column. The ANN-based equation has good prediction with experimental data, when compared with the analytical models.

  11. Gamma ray scanning as troubleshooting tool for unusual and large diameter refinery vacuum columns

    International Nuclear Information System (INIS)

    Sarkar, T.K.; Chawla, R.; Banik, S.; Chopra, S.J.; Singh, G.; Pant, H.J.; Sreeramakrishnan, P.; Dhar, D.C.; Pushpangathan, P.N.; Sharma, V.K.

    1997-01-01

    Gamma scanning of trayed and packed columns is widely used to obtain density profiles and identify on-line problems such as: damaged tray or packing, foaming, flooding, maldistribution, weeping and entrainment, etc. However, scanning of large diameter tray or packed columns requires expertise in handling high intensity gamma sources along with thorough understanding of distillation engineering. Engineers India Limited and the Bhabha Atomic Research Centre undertook scanning of two such large diameter (8.4 m and 7.4 m) trayed and packed refinery vacuum distillation columns and successfully diagnosed the problems and suggested remedial actions. Radiography testing of small diameter columns can be used to confirm gamma scanning results. One such example for ammonia separator column is given

  12. Column studies on the sorption of radioactive isotopes by some natural clay minerals

    International Nuclear Information System (INIS)

    Abdel-Gawad, A.S.; Misak, N.Z.; Maghrawy, H.B.; Shafik, A.

    1982-01-01

    Different types of naturally occuring minerals have been investigated in respect of the sorption of various radioisotopes. The present work deals with column studies of the sorption of 89 Sr and 60 Co on four natural bentonites. Columns having a cross section of 1.47 cm 2 were used for determining the breakthrough capacities for both Sr and Co. The applicability of the Glueckauf plate theory to the systems was tested. It was found that HETP is constant for a given system of column and cationic species, which proves the applicability of the theory. From this, it follows that the data obtained for the short laboratory columns can be used to predict the breakthrough behaviour for longer columns. (author)

  13. Empirical Approach for Determining Axial Strength of Circular Concrete Filled Steel Tubular Columns

    Science.gov (United States)

    Jayalekshmi, S.; Jegadesh, J. S. Sankar; Goel, Abhishek

    2018-06-01

    The concrete filled steel tubular (CFST) columns are highly regarded in recent years as an interesting option in the construction field by designers and structural engineers, due to their exquisite structural performance, with enhanced load bearing capacity and energy absorption capacity. This study presents a new approach to simulate the capacity of circular CFST columns under axial loading condition, using a large database of experimental results by applying artificial neural network (ANN). A well trained network is established and is used to simulate the axial capacity of CFST columns. The validation and testing of the ANN is carried out. The current study is focused on proposing a simplified equation that can predict the ultimate strength of the axially loaded columns with high level of accuracy. The predicted results are compared with five existing analytical models which estimate the strength of the CFST column. The ANN-based equation has good prediction with experimental data, when compared with the analytical models.

  14. Results of the eruptive column model inter-comparison study

    Science.gov (United States)

    Costa, Antonio; Suzuki, Yujiro; Cerminara, M.; Devenish, Ben J.; Esposti Ongaro, T.; Herzog, Michael; Van Eaton, Alexa; Denby, L.C.; Bursik, Marcus; de' Michieli Vitturi, Mattia; Engwell, S.; Neri, Augusto; Barsotti, Sara; Folch, Arnau; Macedonio, Giovanni; Girault, F.; Carazzo, G.; Tait, S.; Kaminski, E.; Mastin, Larry G.; Woodhouse, Mark J.; Phillips, Jeremy C.; Hogg, Andrew J.; Degruyter, Wim; Bonadonna, Costanza

    2016-01-01

    This study compares and evaluates one-dimensional (1D) and three-dimensional (3D) numerical models of volcanic eruption columns in a set of different inter-comparison exercises. The exercises were designed as a blind test in which a set of common input parameters was given for two reference eruptions, representing a strong and a weak eruption column under different meteorological conditions. Comparing the results of the different models allows us to evaluate their capabilities and target areas for future improvement. Despite their different formulations, the 1D and 3D models provide reasonably consistent predictions of some of the key global descriptors of the volcanic plumes. Variability in plume height, estimated from the standard deviation of model predictions, is within ~ 20% for the weak plume and ~ 10% for the strong plume. Predictions of neutral buoyancy level are also in reasonably good agreement among the different models, with a standard deviation ranging from 9 to 19% (the latter for the weak plume in a windy atmosphere). Overall, these discrepancies are in the range of observational uncertainty of column height. However, there are important differences amongst models in terms of local properties along the plume axis, particularly for the strong plume. Our analysis suggests that the simplified treatment of entrainment in 1D models is adequate to resolve the general behaviour of the weak plume. However, it is inadequate to capture complex features of the strong plume, such as large vortices, partial column collapse, or gravitational fountaining that strongly enhance entrainment in the lower atmosphere. We conclude that there is a need to more accurately quantify entrainment rates, improve the representation of plume radius, and incorporate the effects of column instability in future versions of 1D volcanic plume models.

  15. Family of columns isospectral to gravity-loaded columns with tip force: A discrete approach

    Science.gov (United States)

    Ramachandran, Nirmal; Ganguli, Ranjan

    2018-06-01

    A discrete model is introduced to analyze transverse vibration of straight, clamped-free (CF) columns of variable cross-sectional geometry under the influence of gravity and a constant axial force at the tip. The discrete model is used to determine critical combinations of loading parameters - a gravity parameter and a tip force parameter - that cause onset of dynamic instability in the CF column. A methodology, based on matrix-factorization, is described to transform the discrete model into a family of models corresponding to weightless and unloaded clamped-free (WUCF) columns, each with a transverse vibration spectrum isospectral to the original model. Characteristics of models in this isospectral family are dependent on three transformation parameters. A procedure is discussed to convert the isospectral discrete model description into geometric description of realistic columns i.e. from the discrete model, we construct isospectral WUCF columns with rectangular cross-sections varying in width and depth. As part of numerical studies to demonstrate efficacy of techniques presented, frequency parameters of a uniform column and three types of tapered CF columns under different combinations of loading parameters are obtained from the discrete model. Critical combinations of these parameters for a typical tapered column are derived. These results match with published results. Example CF columns, under arbitrarily-chosen combinations of loading parameters are considered and for each combination, isospectral WUCF columns are constructed. Role of transformation parameters in determining characteristics of isospectral columns is discussed and optimum values are deduced. Natural frequencies of these WUCF columns computed using Finite Element Method (FEM) match well with those of the given gravity-loaded CF column with tip force, hence confirming isospectrality.

  16. Unbonded Prestressed Columns for Earthquake Resistance

    Science.gov (United States)

    2012-05-01

    Modern structures are able to survive significant shaking caused by earthquakes. By implementing unbonded post-tensioned tendons in bridge columns, the damage caused by an earthquake can be significantly lower than that of a standard reinforced concr...

  17. Anomalous electrical signals associated with microbial activity: Results from Iron and Nitrate-Reducing Columns

    Science.gov (United States)

    Aaron, R. B.; Zheng, Q.; Flynn, P.; Singha, K.; Brantley, S.

    2008-12-01

    Three flow-through columns outfitted with Ag/AgCl electrodes were constructed to test the effects of different microbial processes on the geophysical measurements of self potential (SP), bulk electrical conductivity (σ b), and induced polarization (IP). The columns were filled with sieved, Fe-bearing subsurface sediment from the Delmarva Peninsula near Oyster, VA, inoculated (9:1 ratio) with a freshly-collected, shallow subsurface sediment from a wetland floodplain (Dorn Creek) near Madison, WI. Each of the columns was fed anoxic and sterile PIPES buffered artificial groundwater (PBAGW) containing different concentrations of acetate and nitrate. The medium fed to Column 1 (nitrate-reducing) was amended with 100 μM acetate and 2 mM nitrate. Column 2 (iron-reducing) was run with PBAGW containing 1.0 mM acetate and 0 mM nitrate. Column 3 (alternating redox state) was operated under conditions designed to alternately stimulate nitrate-reducing and iron-reducing populations to provide conditions, i.e., the presence of both nitrate and microbially-produced Fe(II), that would allow growth of nitrate-dependent Fe(II)-oxidizing populations. We operated Column 3 with a cycling strategy of 14-18 days of high C medium (1 mM acetate and 100 μ M nitrate) followed by 14-18 days of low C medium (100 μ M acetate and 2 mM nitrate). Effluent chemistry (NO3-, NO2-, NH4+, acetate, and Fe2+) was sampled daily for four months so as to be concurrent with the electrical measurements. We observed chemical evidence of iron reduction (dissolved [Fe(II)] = 0.2mM) in the effluent from the iron reduction and alternating redox columns. Chemical depletion of NO3- ([NO3-] ranged from 1 to 0.02mM), the production of NO2-, and possible production of NH4+ (0.2 mM) was observed in the nitrate reducing column as well as the alternating redox column. All three columns displayed loss of acetate as microbial activity progressed. σ b remained constant in the alternating redox column (~0.15 S

  18. Comparison of twin-cell centrifugal partition chromatographic columns with different cell volume.

    Science.gov (United States)

    Goll, Johannes; Audo, Gregoire; Minceva, Mirjana

    2015-08-07

    Two twin-cell centrifugal partition chromatographic columns (SCPC 250 and SCPE-250-BIO, Armen Instrument, France) with the same column volume but different cell size and number were compared in terms of stationary phase retention and column efficiency. The columns were tested with two types of solvent systems: a commonly used organic solvent based biphasic system from the ARIZONA solvent system family and a polymer/salt based aqueous two phase system (ATPS). The efficiency of the columns was evaluated by pulse injection experiments of two benzenediols (pyrocatechol and hydroquinone) in the case of the ARIZONA system and a protein mixture (myoglobin and lysozyme) in the case of the ATPS. As result of high stationary phase retention, the column with the lower number of larger twin-cells (SCPE-250-BIO) is suitable for protein separations using ATPS. On the other hand, due to higher column efficiency, the column with the greater number of smaller cells (SCPC 250) is superior for batch elution separations performed with standard liquid-liquid chromatography organic solvent based biphasic systems. Copyright © 2015 Elsevier B.V. All rights reserved.

  19. Analysis of an industrial process simulator column using third-generation computed tomography

    International Nuclear Information System (INIS)

    Kirita, Rodrigo; Carvalho, Diego Vergacas de Sousa; Mesquita, Carlos Henrique de; Vasquez, Pablo Antonio S.; Hamada, Margarida Mizue

    2011-01-01

    The CT methodology must be tested using a simulator column in the laboratory before applying it in the industrial plants. In this work, using the third-generation industrial computed tomography developed at the IPEN, a gas absorption column, used as a simulator column for industrial process was evaluated. It is a glass cylindrical tube of 90 mm diameter and 1400 mm height constituted the following parts: random packed column, liquid circuit (water), gas circuit and analysis was used as a simulator column. Gamma ray tomography experiments were carried out, using this simulator column empty and filled with water. In this work the scanner was setting for 90 views and 19 projections for each detector totalizing 11970 projections. The resulting images describe the presence of liquid or gas phases and are possible to evaluate the linear attenuation coefficients inside the column. In this case, linear attenuation coefficient for water was 0.0813 cm-1. It was established that the newly developed third-generation fan-beam arrangement gamma scanner unit has a good spatial resolution acceptable given the size of the column used in this study. (author)

  20. Investigation of Limit States Specified for Reinforced Concrete Column Members in TEC–2007

    Directory of Open Access Journals (Sweden)

    Umut HASGÜL

    2016-01-01

    Full Text Available In this study, the deformation based limit states stipulated for reinforced concrete members in the Turkish Earthquake Code (TEC were experimentally investigated. Thus four RC cantilever columns which have low concrete compressive strengths and have not adequate confinement, were subjected to constant axial load and cyclic lateral load history. In the study, firstly, the strain values representing the damage limits were converted to top of the column lateral displacements by using fundamentals of structural mechanics. Subsequently the column damages corresponding to the displacement demands were observed, hence limit states were evaluated. After conducting all column tests, it was noted that no column damage was observed for the immediate occupancy (IO performance level defined in the code. For the life safety (LS and collapse prevention (CP performance levels, though somewhat residual deformations occurred on the critical regions, the column members can pretty much sustain their lateral load capacities. It was also observed for all columns that significant damages and strength losses occurred beyond the collapse prevention level. The results of experimental study indicate that the evaluation procedure in the TEC is still in good relationship with the limit states even if the columns have not adequate compressive strength and confinement.

  1. The handedness of historiated spiral columns.

    Science.gov (United States)

    Couzin, Robert

    2017-09-01

    Trajan's Column in Rome (AD 113) was the model for a modest number of other spiral columns decorated with figural, narrative imagery from antiquity to the present day. Most of these wind upwards to the right, often with a congruent spiral staircase within. A brief introductory consideration of antique screw direction in mechanical devices and fluted columns suggests that the former may have been affected by the handedness of designers and the latter by a preference for symmetry. However, for the historiated columns that are the main focus of this article, the determining factor was likely script direction. The manner in which this operated is considered, as well as competing mechanisms that might explain exceptions. A related phenomenon is the reversal of the spiral in a non-trivial number of reproductions of the antique columns, from Roman coinage to Renaissance and baroque drawings and engravings. Finally, the consistent inattention in academic literature to the spiral direction of historiated columns and the repeated publication of erroneous earlier reproductions warrants further consideration.

  2. Topographic shear and the relation of ocular dominance columns to orientation columns in primate and cat visual cortex.

    Science.gov (United States)

    Wood, Richard J.; Schwartz, Eric L.

    1999-03-01

    Shear has been known to exist for many years in the topographic structure of the primary visual cortex, but has received little attention in the modeling literature. Although the topographic map of V1 is largely conformal (i.e. zero shear), several groups have observed topographic shear in the region of the V1/V2 border. Furthermore, shear has also been revealed by anisotropy of cortical magnification factor within a single ocular dominance column. In the present paper, we make a functional hypothesis: the major axis of the topographic shear tensor provides cortical neurons with a preferred direction of orientation tuning. We demonstrate that isotropic neuronal summation of a sheared topographic map, in the presence of additional random shear, can provide the major features of cortical functional architecture with the ocular dominance column system acting as the principal source of the shear tensor. The major principal axis of the shear tensor determines the direction and its eigenvalues the relative strength of cortical orientation preference. This hypothesis is then shown to be qualitatively consistent with a variety of experimental results on cat and monkey orientation column properties obtained from optical recording and from other anatomical and physiological techniques. In addition, we show that a recent result of Das and Gilbert (Das, A., & Gilbert, C. D., 1997. Distortions of visuotopic map match orientation singularities in primary visual cortex. Nature, 387, 594-598) is consistent with an infinite set of parameterized solutions for the cortical map. We exploit this freedom to choose a particular instance of the Das-Gilbert solution set which is consistent with the full range of local spatial structure in V1. These results suggest that further relationships between ocular dominance columns, orientation columns, and local topography may be revealed by experimental testing.

  3. Mass transfer model liquid phase catalytic exchange column simulation applicable to any column composition profile

    Energy Technology Data Exchange (ETDEWEB)

    Busigin, A. [NITEK USA Inc., Ocala, FL (United States)

    2015-03-15

    Liquid Phase Catalytic Exchange (LPCE) is a key technology used in water detritiation systems. Rigorous simulation of LPCE is complicated when a column may have both hydrogen and deuterium present in significant concentrations in different sections of the column. This paper presents a general mass transfer model for a homogenous packed bed LPCE column as a set of differential equations describing composition change, and equilibrium equations to define the mass transfer driving force within the column. The model is used to show the effect of deuterium buildup in the bottom of an LPCE column from non-negligible D atom fraction in the bottom feed gas to the column. These types of calculations are important in the design of CECE (Combined Electrolysis and Catalytic Exchange) water detritiation systems.

  4. Development of spent salt treatment technology by zeolite column system. Performance evaluation of zeolite column

    International Nuclear Information System (INIS)

    Miura, Hidenori; Uozumi, Koichi

    2009-01-01

    At electrorefining process, fission products(FPs) accumulate in molten salt. To avoid influence on heating control by decay heat and enlargement of FP amount in the recovered fuel, FP elements must be removed from the spent salt of the electrorefining process. For the removal of the FPs from the spent salt, we are investigating the availability of zeolite column system. For obtaining the basic data of the column system, such as flow property and ion-exchange performance while high temperature molten salt is passing through the column, and experimental apparatus equipped with fraction collector was developed. By using this apparatus, following results were obtained. 1) We cleared up the flow parameter of column system with zeolite powder, such as flow rate control by argon pressure. 2) Zeolite 4A in the column can absorb cesium that is one of the FP elements in molten salt. From these results, we got perspective on availability of the zeolite column system. (author)

  5. Structural Decoupling and Disturbance Rejection in a Distillation Column

    DEFF Research Database (Denmark)

    Bahar, Mehrdad; Jantzen, Jan; Commault, C.

    1996-01-01

    Introduction, distillation column model, input-output decoupling, disturbance rejection, concluding remarks, references.......Introduction, distillation column model, input-output decoupling, disturbance rejection, concluding remarks, references....

  6. Relating pressure tuned coupled column ensembles with the solvation parameter model for tunable selectivity in gas chromatography.

    Science.gov (United States)

    Sharif, Khan M; Kulsing, Chadin; Chin, Sung-Tong; Marriott, Philip J

    2016-07-15

    The differential pressure drop of carrier gas by tuning the junction point pressure of a coupled column gas chromatographic system leads to a unique selectivity of the overall separation, which can be tested using a mixture of compounds with a wide range of polarity. This study demonstrates a pressure tuning (PT) GC system employing a microfluidic Deans switch located at the mid-point of the two capillary columns. This PT system allowed variations of inlet-outlet pressure differences of the two columns in a range of 52-17psi for the upstream column and 31-11psi for the downstream column. Peak shifting (differential migration) of compounds due to PT difference are related to a first order regression equation in a Plackett-Burman factorial study. Increased first (upstream) column pressure drop makes the second column characteristics more significant in the coupled column retention behavior, and conversely increased second (downstream) column pressure drop makes the first column characteristics more apparent; such variation can result in component swapping between polar and non-polar compounds. The coupled column system selectivity was evaluated in terms of linear solvation energy relationship (LSER) parameters, and their relation with different pressure drop effects has been constructed by applying multivariate principle component analysis (PCA). It has been found that the coupled column PT system descriptors provide a result that shows a clear clustering of different pressure settings, somewhat intermediate between those of the two commercial columns. This is equivalent to that obtained from a conventional single-column GC analysis where the interaction energy contributed from the stationary phases can be significantly adjusted by choice of midpoint PT. This result provides a foundation for pressure differentiation for selectivity enhancement. Copyright © 2016 Elsevier B.V. All rights reserved.

  7. Strengthening of defected beam–column joints using CFRP

    Directory of Open Access Journals (Sweden)

    Mohamed H. Mahmoud

    2014-01-01

    Full Text Available This paper presents an experimental study for the structural performance of reinforced concrete (RC exterior beam–column joints rehabilitated using carbon-fiber-reinforced polymer (CFRP. The present experimental program consists of testing 10 half-scale specimens divided into three groups covering three possible defects in addition to an adequately detailed control specimen. The considered defects include the absence of the transverse reinforcement within the joint core, insufficient bond length for the beam main reinforcement and inadequate spliced implanted column on the joint. Three different strengthening schemes were used to rehabilitate the defected beam–column joints including externally bonded CFRP strips and sheets in addition to near surface mounted (NSM CFRP strips. The failure criteria including ultimate capacity, mode of failure, initial stiffness, ductility and the developed ultimate strain in the reinforcing steel and CFRP were considered and compared for each group for the control and the CFRP-strengthened specimens. The test results showed that the proposed CFRP strengthening configurations represented the best choice for strengthening the first two defects from the viewpoint of the studied failure criteria. On the other hand, the results of the third group showed that strengthening the joint using NSM strip technique enabled the specimen to outperform the structural performance of the control specimen while strengthening the joints using externally bonded CFRP strips and sheets failed to restore the strengthened joints capacity.

  8. Strengthening of defected beam-column joints using CFRP.

    Science.gov (United States)

    Mahmoud, Mohamed H; Afefy, Hamdy M; Kassem, Nesreen M; Fawzy, Tarek M

    2014-01-01

    This paper presents an experimental study for the structural performance of reinforced concrete (RC) exterior beam-column joints rehabilitated using carbon-fiber-reinforced polymer (CFRP). The present experimental program consists of testing 10 half-scale specimens divided into three groups covering three possible defects in addition to an adequately detailed control specimen. The considered defects include the absence of the transverse reinforcement within the joint core, insufficient bond length for the beam main reinforcement and inadequate spliced implanted column on the joint. Three different strengthening schemes were used to rehabilitate the defected beam-column joints including externally bonded CFRP strips and sheets in addition to near surface mounted (NSM) CFRP strips. The failure criteria including ultimate capacity, mode of failure, initial stiffness, ductility and the developed ultimate strain in the reinforcing steel and CFRP were considered and compared for each group for the control and the CFRP-strengthened specimens. The test results showed that the proposed CFRP strengthening configurations represented the best choice for strengthening the first two defects from the viewpoint of the studied failure criteria. On the other hand, the results of the third group showed that strengthening the joint using NSM strip technique enabled the specimen to outperform the structural performance of the control specimen while strengthening the joints using externally bonded CFRP strips and sheets failed to restore the strengthened joints capacity.

  9. Masonry Columns Confined by Steel Fiber Composite Wraps

    Directory of Open Access Journals (Sweden)

    Marco Corradi

    2011-01-01

    Full Text Available The application of steel fiber reinforced polymer (SRP as a means of increasing the capacity of masonry columns is investigated in this study. The behavior of 23 solid-brick specimens that are externally wrapped by SRP sheets in low volumetric ratios is presented. The specimens are subjected to axial monotonic load until failure occurs. Two widely used types of masonry columns of differing square cross-sections were tested in compression (square and octagonal cross-sections. It is concluded that SRP-confined masonry behaves very much like fiber reinforced polymers (FRP-confined masonry. Confinement increases both the load-carrying capacity and the deformability of masonry almost linearly with average confining stress. A comparative analysis between experimental and theoretical values computed in compliance with the Italian Council of Research (CNR was also developed.

  10. Emergency repair of severely damaged reinforced concrete columns using active confinement with shape memory alloys

    International Nuclear Information System (INIS)

    Shin, Moochul; Andrawes, Bassem

    2011-01-01

    This experimental study focuses on investigating the feasibility of utilizing spirals made of shape memory alloys (SMAs) to conduct emergency repair on severely damaged reinforced concrete (RC) columns. The thermally triggered shape memory feature of SMAs is sought in this study, to apply active confinement pressure on the column's damaged region. Two severely damaged 1/3-scale RC columns are repaired using the proposed technique and tested under a quasi-static lateral cyclic load. The repair of each column is conducted in less than 15 h, and the columns are tested 24 h after the starting of the repair process. The experimental results show that the new repair technique is successful in either fully restoring the as-built lateral strength, stiffness, and flexural ductility of the columns or making them even better. The efficacy of the proposed repair technique is mainly attributed to the ability of the SMA spirals to apply and maintain active confining pressure on the damaged region of the columns, which increases the strength of the already damaged concrete and delays its damage

  11. Recent advances in column switching sample preparation in bioanalysis.

    Science.gov (United States)

    Kataoka, Hiroyuki; Saito, Keita

    2012-04-01

    Column switching techniques, using two or more stationary phase columns, are useful for trace enrichment and online automated sample preparation. Target fractions from the first column are transferred online to a second column with different properties for further separation. Column switching techniques can be used to determine the analytes in a complex matrix by direct sample injection or by simple sample treatment. Online column switching sample preparation is usually performed in combination with HPLC or capillary electrophoresis. SPE or turbulent flow chromatography using a cartridge column and in-tube solid-phase microextraction using a capillary column have been developed for convenient column switching sample preparation. Furthermore, various micro-/nano-sample preparation devices using new polymer-coating materials have been developed to improve extraction efficiency. This review describes current developments and future trends in novel column switching sample preparation in bioanalysis, focusing on innovative column switching techniques using new extraction devices and materials.

  12. Impact Analysis of Reinforced Concrete Columns with Side Openings Subjected to Eccentric Axial Loads

    Directory of Open Access Journals (Sweden)

    Nazar Kamil Ali

    2015-02-01

    Full Text Available In this research the behavior of reinforced concrete columns with large side openings under impact loads was studied. The overall cross sectional dimensions of the column specimens used in this research were (500*1400 mm with total height of (14000 mm. The dimensions of side openings were (600*2000 mm. The column was reinforced with (20 mm diameter in longitudinal direction, while (12 mm ties were used in the transverse direction. The effect of eccentric impact loads on the horizontal and vertical displacement for this column was studied. Nonlinear finite element analysis has been carried out using ready computer finite element package (ANSYS to simulate the behavior of the reinforced concrete column with large side openings. Two load cases were considered in this investigation (C1, C2 with three different load values for each case. In the first case (C1 the loads was applied to one side of the column and in the second case (C2 the loads was applied to both sides. An Equilateral triangular load-time function was used for simulation the impact load results from gantry cranes supported by the column with total time duration (0.1 sec. In order to verify the analysis method, as no experimental data exist for comparing the obtained results, another analysis is made for tested conventional column under impact load at mid-height and good agreement has been obtained. For the above mentioned column, the maximum displacements were (33.3, 22.2 mm in the horizontal and longitudinal direction respectively, location of the maximum horizontal displacement was at the crown of the column. By comparing the results of the first loading case with the second one it is shown that in the horizontal direction, maximum displacement increases by (139%, (208%, and (147% respectively, also the maximum vertical displacement increases by (150%, (172%, and (172% respectively.

  13. ADAM28 localizes to HLA-G+ trophoblasts and promotes column cell outgrowth.

    Science.gov (United States)

    De Luca, L C; Le, H T; Mara, D L; Beristain, A G

    2017-07-01

    Trophoblast progenitor cell differentiation towards the extravillous trophoblast (EVT) lineage initiates within proximal regions of anchoring columns of first trimester placental villi. While molecular processes controlling the initial stages of progenitor cell differentiation along the EVT pathway have been described, much remains unknown about factors important in distal column cell differentiation into invasive EVTs. ADAMs are proteases that regulate growth factor signaling, cell-matrix adhesion, and matrix proteolysis, and thus impact many processes relevant in placentation. Global gene expression studies identified the ADAM subtype, ADAM28, to be highly expressed in EVT-like trophoblasts, suggesting that it may play a role in EVT function. This study aims to test the functional importance of ADAM28 in column cell outgrowth and maintenance. ADAM28 mRNA levels and protein localization were determined by qPCR and immunofluorescence microscopy analyses in purified placental villi cell populations and tissues. ADAM28 function in trophoblast column outgrowth was examined using ADAM28-targetting siRNAs in Matrigel-imbedded placental explant cultures. Within placental villi, ADAM28 mRNA levels were highest in HLA-G + column trophoblasts, and consistent with this, ADAM28 was preferentially localized to HLA-G + trophoblasts within distal anchoring columns and decidual tissue. siRNA-directed loss of ADAM28 impaired trophoblast column outgrowth and resulted in increased apoptosis in matrix-invading trophoblasts. Our findings suggest that ADAM28 promotes column outgrowth by providing survival cues within anchoring column cells. This study also provides insight into a possible role for ADAM28 in driving differentiation of column trophoblasts into invasive HLA-G + EVT subsets. Copyright © 2017 Elsevier Ltd. All rights reserved.

  14. Experimental Study on Fibre-reinforced Cementitious Matrix Confined Concrete Columns under Axial Compression

    Directory of Open Access Journals (Sweden)

    Lan Zeng

    2017-03-01

    Full Text Available Poor fire resistance of fibre-reinforced polymer (FRP restricts its further application in construction structures. In this paper, a novel fibre-reinforced cementitious matrix confined concrete column (FRCMCC using fireproof grout as the fibre matrix was developed, and experiments were conducted to establish its performance and analyse the mechanical properties under axial compression. The test results show that its failure mode was more moderate compared to the traditional fibre-reinforced resinous matrix confined concrete column (FRRMCC, and the concrete columns confined with multi-layer fibres and end reinforcement could provide both good strength and ductility.

  15. Contributions to reversed-phase column selectivity: III. Column hydrogen-bond basicity.

    Science.gov (United States)

    Carr, P W; Dolan, J W; Dorsey, J G; Snyder, L R; Kirkland, J J

    2015-05-22

    Column selectivity in reversed-phase chromatography (RPC) can be described in terms of the hydrophobic-subtraction model, which recognizes five solute-column interactions that together determine solute retention and column selectivity: hydrophobic, steric, hydrogen bonding of an acceptor solute (i.e., a hydrogen-bond base) by a stationary-phase donor group (i.e., a silanol), hydrogen bonding of a donor solute (e.g., a carboxylic acid) by a stationary-phase acceptor group, and ionic. Of these five interactions, hydrogen bonding between donor solutes (acids) and stationary-phase acceptor groups is the least well understood; the present study aims at resolving this uncertainty, so far as possible. Previous work suggests that there are three distinct stationary-phase sites for hydrogen-bond interaction with carboxylic acids, which we will refer to as column basicity I, II, and III. All RPC columns exhibit a selective retention of carboxylic acids (column basicity I) in varying degree. This now appears to involve an interaction of the solute with a pair of vicinal silanols in the stationary phase. For some type-A columns, an additional basic site (column basicity II) is similar to that for column basicity I in primarily affecting the retention of carboxylic acids. The latter site appears to be associated with metal contamination of the silica. Finally, for embedded-polar-group (EPG) columns, the polar group can serve as a proton acceptor (column basicity III) for acids, phenols, and other donor solutes. Copyright © 2015 Elsevier B.V. All rights reserved.

  16. ON THE ORIGIN OF THE HIGH COLUMN DENSITY TURNOVER IN THE H I COLUMN DENSITY DISTRIBUTION

    International Nuclear Information System (INIS)

    Erkal, Denis; Gnedin, Nickolay Y.; Kravtsov, Andrey V.

    2012-01-01

    We study the high column density regime of the H I column density distribution function and argue that there are two distinct features: a turnover at N H I ≈ 10 21 cm –2 , which is present at both z = 0 and z ≈ 3, and a lack of systems above N H I ≈ 10 22 cm –2 at z = 0. Using observations of the column density distribution, we argue that the H I-H 2 transition does not cause the turnover at N H I ≈ 10 21 cm –2 but can plausibly explain the turnover at N H I ∼> 10 22 cm –2 . We compute the H I column density distribution of individual galaxies in the THINGS sample and show that the turnover column density depends only weakly on metallicity. Furthermore, we show that the column density distribution of galaxies, corrected for inclination, is insensitive to the resolution of the H I map or to averaging in radial shells. Our results indicate that the similarity of H I column density distributions at z = 3 and 0 is due to the similarity of the maximum H I surface densities of high-z and low-z disks, set presumably by universal processes that shape properties of the gaseous disks of galaxies. Using fully cosmological simulations, we explore other candidate physical mechanisms that could produce a turnover in the column density distribution. We show that while turbulence within giant molecular clouds cannot affect the damped Lyα column density distribution, stellar feedback can affect it significantly if the feedback is sufficiently effective in removing gas from the central 2-3 kpc of high-redshift galaxies. Finally, we argue that it is meaningful to compare column densities averaged over ∼ kpc scales with those estimated from quasar spectra that probe sub-pc scales due to the steep power spectrum of H I column density fluctuations observed in nearby galaxies.

  17. Influence of the column rectangularity index and of the boundary conditions in the punching resistance of slab-column connections

    Directory of Open Access Journals (Sweden)

    O. S. PAIVA

    Full Text Available Experimental evidence indicates that both the column rectangularity index and the boundary conditions of the connection may affect the ultimate punching resistance. This paper presents general aspects of these topics and, through the analysis of experimental results of tests on 131 slabs, evaluates the accuracy and suitability of recommendations presented by ABNT NBR 6118, Eurocode 2, ACI 318 and fib Model Code 2010. Experimental results showed that the security level of normative estimates trend to reduce as the column rectangularity increases, and in some cases, the punching resistance was overestimated. Finally, adjustments are suggested in equations presented by NBR 6118 and MC2010 in order to eliminate this trend of unsafe results.

  18. Vertebral Column Resection for Rigid Spinal Deformity.

    Science.gov (United States)

    Saifi, Comron; Laratta, Joseph L; Petridis, Petros; Shillingford, Jamal N; Lehman, Ronald A; Lenke, Lawrence G

    2017-05-01

    Broad narrative review. To review the evolution, operative technique, outcomes, and complications associated with posterior vertebral column resection. A literature review of posterior vertebral column resection was performed. The authors' surgical technique is outlined in detail. The authors' experience and the literature regarding vertebral column resection are discussed at length. Treatment of severe, rigid coronal and/or sagittal malalignment with posterior vertebral column resection results in approximately 50-70% correction depending on the type of deformity. Surgical site infection rates range from 2.9% to 9.7%. Transient and permanent neurologic injury rates range from 0% to 13.8% and 0% to 6.3%, respectively. Although there are significant variations in EBL throughout the literature, it can be minimized by utilizing tranexamic acid intraoperatively. The ability to correct a rigid deformity in the spine relies on osteotomies. Each osteotomy is associated with a particular magnitude of correction at a single level. Posterior vertebral column resection is the most powerful posterior osteotomy method providing a successful correction of fixed complex deformities. Despite meticulous surgical technique and precision, this robust osteotomy technique can be associated with significant morbidity even in the most experienced hands.

  19. Effect of backmixing on pulse column performance

    International Nuclear Information System (INIS)

    Miao, Y.W.

    1979-05-01

    A critical survey of the published literature concerning dispersed phase holdup and longitudinal mixing in pulsed sieve-plate extraction columns has been made to assess the present state-of-the-art in predicting these two parameters, both of which are of critical importance in the development of an accurate mathematical model of the pulse column. Although there are many conflicting correlations of these variables as a function of column geometry, operating conditions, and physical properties of the liquid systems involved it has been possible to develop new correlations which appear to be useful and which are consistent with much of the available data over the limited range of variables most likely to be encountered in plant sized equipment. The correlations developed were used in a stagewise model of the pulse column to predict product concentrations, solute inventory, and concentration profiles in a column for which limited experimental data were available. Reasonable agreement was obtained between the mathematical model and the experimental data. Complete agreement, however, can only be obtained after a correlation for the extraction efficiency has been developed. The correlation of extraction efficiency was beyond the scope of this work

  20. A study on the behavior of beam-column connections in precast concrete structures: experimental analysis

    Directory of Open Access Journals (Sweden)

    M. N. Kataoka

    Full Text Available Due to the large increase in the use of precast concrete structures in multistory buildings, this work covers a study on the behavior of beam-column connection with emphasis on the continuity provided by the slab reinforcement. Two prototypes were tested, each one with a different detail of the continuity reinforcement distribution. In both connections, the steel area used on the concrete cover of the hollow core slab was the same, varying the amount of bars that passed through the column and the ones that were placed adjacent to the column. The experimental results showed that the connection with bars adjacent to the column presented stiffness increase and a better cracking control. According to the classification the two tested connections can be considered semi-rigid.

  1. Radio Column Chromatographic Assay of H3-Labelled Substances

    International Nuclear Information System (INIS)

    Scharpenseel, H.W.; Menke, K.H.

    1962-01-01

    Combined radio-chromatographic investigations of H 3 -labelled substances are an integral part of the majority of biochemical experiments with H 3 -labelled compounds. H 3 -radio paper chromatography yields, in a scanner with a windowless flow counter, a counting efficiency of 0,5 -1,5%, depending largely on the thickness of the paper and the self-absorption of the labelled compound. The radio gas chromatography of tritiated compounds presents no major problem. Successful use is being made of a combination of a gas chromatograph with a flow ionization chamber and vibrating reed electrometer, a system originated by K. E. Wilzbach and P. Riessz, and improved by H. Dutton, L. Mason and L. Blair. Through the use of ''Teflon'' and silicone-rubber for the insulating parts of the flow ion chamber, it can be operated at close to 300 o C. Radio column chromatography with tritium holds little promise, when the column effluent is spread out as a shallow layer and slowly passes under a windowless flow counter or a scintillation counter, as was successfully tried with C 14 . Liquid scintillation spectrometry is likely to be the chosen method. Essentially, there are two different approaches feasible. These have been compared: 1. The column effluent is passed through a coil of plastic scintillator tubing, which is wound around a ''Plexiglas'' cylinder and placed in a bath of silicone oil in a light pipe with TiO 2 -reflector. Similarly, the HP-containing effluent can be directed through a test vial, filled - very much as in Steinberg's method - with plastic scintillator beads. These two approaches, that operate highly satisfactorily in the case of C 14 , offer low counting efficiencies of less than 1% for H 3 due to the unfavourable surface to volume ratio. 2. The column effluent is combined 1:30 with a mixture of 3:2 toluene/ethanol by the action of a magnet-vibrator before being assayed while passing through a K 40 -free glass - coiled between the analyser- and monitor

  2. Burning test on a storage drum filled with a mixture of sodiumnitrate and bitumen

    International Nuclear Information System (INIS)

    Knotik, K.; Leichter, P.; Spalek, K.

    1979-01-01

    A burning test on a common storage drum filled with a mixture of sodiumnitrate and bitumen was carried out to show the incinerability of said mixture. A 50 l mild steel drum was filled with 80,7 kg sodiumnitrate/bitumen-mixture. The drum was packed in a 200 l mild steel drum, the remaining space was filled with enough sand to cover the top of the inner drum with 15 cm of sand. The sand packing was then soaked with 70 l of light distillate fuel and ignited. The fuel burned until self-extinguishing occurred. 30 % (22,2 l) of the fuel was burned. 0,7 % of the energy potential was absorbed in the sand layer. The highest measured temperature was 34 0 C at the top of the test drum. It can be concluded, that even under severe external actions the ignition temperature of 400 0 C for bitumen/waste mixtures cannot be reached, providing correct technical storage conditions, which means that the void space in the cavities is filled with unburnable absorbing material like sand or salt. (author)

  3. Mathematical solution of the stone column effect on the load bearing capacity and settlement using numerical analysis

    Science.gov (United States)

    Madun, A.; Meghzili, S. A.; Tajudin, SAA; Yusof, M. F.; Zainalabidin, M. H.; Al-Gheethi, A. A.; Dan, M. F. Md; Ismail, M. A. M.

    2018-04-01

    The most important application of various geotechnical construction techniques is for ground improvement. Many soil improvement project had been developed due to the ongoing increase in urban and industrial growth and the need for greater access to lands. Stone columns are one of the best effective and feasible techniques for soft clay soil improvement. Stone columns increase the bearing capacity and reduce the settlement of soil. Finite element analyses were performed using the program PLAXIS 2D. An elastic-perfectly plastic constitutive relation, based on the Mohr–Coulomb criterion, governs the soft clay and stone column behaviour. This paper presents on how the response surface methodology (RSM) software is used to optimize the effect of the diameters and lengths of column on the load bearing capacity and settlement of soft clay. Load tests through the numerical modelling using Plaxis 2D were carried out on the loading plate at 66 mm. Stone column load bearing capacity increases with the increasing diameter of the column and settlement decreases with the increasing length of the column. Results revealed that the bigger column diameter, the higher load bearing capacity of soil while the longer column length, the lower settlement of soil. However, the optimum design of stone column was varied with each factor (diameter and length) separately for improvement.

  4. Mathematical modeling of alcohol distillation columns

    Directory of Open Access Journals (Sweden)

    Ones Osney Pérez

    2011-04-01

    Full Text Available New evaluation modules are proposed to extend the scope of a modular simulator oriented to the sugar cane industry, called STA 4.0, in a way that it can be used to carry out x calculation and analysis in ethanol distilleries. Calculation modules were developed for the simulation of the columns that are combined in the distillation area. Mathematical models were supported on materials and energy balances, equilibrium relations and thermodynamic properties of the ethanol-water system. Ponchon-Savarit method was used for the evaluation of the theoretical stages in the columns. A comparison between the results using Ponchon- Savarit method and those obtained applying McCabe-Thiele method was done for a distillation column. These calculation modules for ethanol distilleries were applied to a real case for validation.

  5. Inert carriers for column extraction chromatography

    International Nuclear Information System (INIS)

    Katykhin, G.S.

    1978-01-01

    Inert carriers used in column extraction chromatography are reviewed. Such carriers are devided into two large groups: hydrophilic carriers which possess high surface energy and are well wetted only with strongly polar liquids (kieselguhrs, silica gels, glasses, cellulose, Al 2 O 3 ) and water-repellent carriers which possess low surface energy and are well wetted with various organic solvents (polyethylene, polytetrafluorethylene polytrifluorochlorethylene). Properties of various carriers are presented: structure, chemical and radiation stability, adsorption properties, extracting agent capacity. The effect of structure and sizes of particles on the efficiency of chromatography columns is considered. Ways of immovable phase deposition on the carrier and the latter's regeneration. Peculiarities of column packing for preparative and continuous chromatography are discussed

  6. Computational analysis of ozonation in bubble columns

    International Nuclear Information System (INIS)

    Quinones-Bolanos, E.; Zhou, H.; Otten, L.

    2002-01-01

    This paper presents a new computational ozonation model based on the principle of computational fluid dynamics along with the kinetics of ozone decay and microbial inactivation to predict the performance of ozone disinfection in fine bubble columns. The model can be represented using a mixture two-phase flow model to simulate the hydrodynamics of the water flow and using two transport equations to track the concentration profiles of ozone and microorganisms along the height of the column, respectively. The applicability of this model was then demonstrated by comparing the simulated ozone concentrations with experimental measurements obtained from a pilot scale fine bubble column. One distinct advantage of this approach is that it does not require the prerequisite assumptions such as plug flow condition, perfect mixing, tanks-in-series, uniform radial or longitudinal dispersion in predicting the performance of disinfection contactors without carrying out expensive and tedious tracer studies. (author)

  7. Failure analysis of edge flat-slab column connections with shear reinforcement

    OpenAIRE

    Bompa, Dan V.; Muttoni, Aurelio

    2013-01-01

    Flat-slab column connections are susceptible to brittle failure, which lead to the necessity of improving ductility and ultimate strength. In case of edge connections, the behaviour at ultimate state is highly influenced by nonsymmetrical distribution of stresses originated by a moment transfer between the slab and the column. The paper presents the test results of three full-scale reinforced concrete flat-slab edge connections with stud-rail shear reinforcement subjected to concentrated load...

  8. A study on the behavior of beam-column connections in precast concrete structures: experimental analysis

    OpenAIRE

    Kataoka,M. N.; Ferreira,M. A.; El Debs,A. L. H. C.

    2012-01-01

    Due to the large increase in the use of precast concrete structures in multistory buildings, this work covers a study on the behavior of beam-column connection with emphasis on the continuity provided by the slab reinforcement. Two prototypes were tested, each one with a different detail of the continuity reinforcement distribution. In both connections, the steel area used on the concrete cover of the hollow core slab was the same, varying the amount of bars that passed through the column and...

  9. Internal slab-column connections under monotonic and cyclic imposed rotations

    OpenAIRE

    Drakatos, Ioannis-Sokratis; Muttoni, Aurelio; Beyer, Katrin

    2016-01-01

    Reinforced concrete flat slabs supported by slender columns are often used as gravity load resisting system for buildings in regions of moderate seismicity. Current codes of practice determine the displacement capacity of slab-column connections using empirical formulas which were calibrated against experimental studies. This article reviews and compares test configurations used in past experimental studies and presents the adopted configuration for an experimental investigation on 13 full-sc...

  10. Multi-column step-gradient chromatography system for automated ion exchange separations

    International Nuclear Information System (INIS)

    Rucker, T.L.

    1985-01-01

    A multi-column step-gradient chromatography system has been designed to perform automated sequential separations of radionuclides by ion exchange chromatography. The system consists of a digital programmer with automatic stream selection valve, two peristaltic pumps, ten columns, and a fraction collector. The automation allows complicated separations of radionuclides to be made with minimal analyst attention and allows for increased productivity and reduced cost of analyses. Results are reported for test separations on mixtures of radionuclides by the system

  11. CUB DI (Deionization) column control system

    International Nuclear Information System (INIS)

    Seino, K.C.

    1999-01-01

    For the old MR (Main Ring), deionization was done with two columns in CUB, using an ion exchange process. Typically 65 GPM of LCW flew through a column, and the resistivity was raised from 3 Mohm-cm to over 12 Mohm-cm. After a few weeks, columns lost their effectiveness and had to be regenerated in a process involving backwashing and adding hydrochloric acid and sodium hydroxide. For normal MR operations, LCW returned from the ring and passed through the two columns in parallel for deionization, although the system could have been operated satisfactorily with only one in use. A 3000 gallon reservoir (the Spheres) provided a reserve of LCW for allowing water leaks and expansions in the MR. During the MI (Main Injector) construction period, the third DI column was added to satisfy requirements for the MI. When the third column was added, the old regeneration controller was replaced with a new controller based on an Allen-Bradley PLC (i.e., SLC-5/04). The PLC is widely used and well documented, and therefore it may allow us to modify the regeneration programs in the future. In addition to the above regeneration controller, the old control panels (which were used to manipulate pumps and valves to supply LCW in Normal mode and to do Int. Recir. (Internal Recirculation) and Makeup) were replaced with a new control system based on Sixtrak Gateway and I/O modules. For simplicity, the new regeneration controller is called as the US Filter system, and the new control system is called as the Fermilab system in this writing

  12. Ground improvement using soil–cement columns: Experimental investigation

    Directory of Open Access Journals (Sweden)

    Ahmed Farouk

    2013-12-01

    Full Text Available The construction of heavy structures on soils of low relative density is a challenging task. The inclusion of soil–cement columns produced by the deep mixing method is one of the soil stabilizing techniques that could be applied successfully to overcome this challenge. Nevertheless, this technique did not receive a considerable attention in Egypt yet. In the first part of this study, two different natural silty sand soils extracted from the Delta of the River Nile were mixed with cement to prepare samples of different cement doses and different water cement ratios. After curing, the hardened samples were tested and their unconfined compressive strength was investigated. The second part of this study investigates the interaction between a strip footing model and Nile deltaic soil improved by a group of soil–cement columns. Results of the first part of this study showed that the compressive strength of the investigated Nile delta soils could be increased even at lower values of cement doses. Results extracted from the second part of this study showed that a considerable settlement reduction up to 80% could be achieved depending on both the number and the length of the soil–cement columns that is used to improve the soil.

  13. Operation of the annular pulsed column, (2)

    International Nuclear Information System (INIS)

    Takahashi, Keiki; Tsukada, Takeshi

    1988-01-01

    The heat of reaction generated form the uranium extraction is considered to from the temperature profile inside the pulsed column. A simulation code was developed to estimate the temperature profile, considering heat generation and counter-current heat transfer. The temperature profiles calculated using this code was found to depend on both the position of the extraction zone and the operating condition. The reported experimental result was fairly represented by this simulation code. We consider that this presented simulation code is capable of providing with the temperature profile in the pulsed column and useful for the monitoring of the uranium extraction zone. (author)

  14. Distillation columns inspection through gamma scanning

    International Nuclear Information System (INIS)

    Garcia, Marco

    1999-09-01

    The application of nuclear energy is very wide and it allows the saving of economic resources since the investigation of a certain process is carried out without stop the plant. The gamma scanning of oil c racking c olumns are practical examples, they allow to determine the hydraulic operation of the inspected columns. A source of Co-60 22mCi and a detector with a crystal of INa(TI) are used. This paper shows the results got from a profile carried out in a column distillation

  15. Mathematical Modeling of Column-Base Connections under Monotonic Loading

    Directory of Open Access Journals (Sweden)

    Gholamreza Abdollahzadeh

    2014-12-01

    Full Text Available Some considerable damage to steel structures during the Hyogo-ken Nanbu Earthquake occurred. Among them, many exposed-type column bases failed in several consistent patterns, such as brittle base plate fracture, excessive bolt elongation, unexpected early bolt failure, and inferior construction work, etc. The lessons from these phenomena led to the need for improved understanding of column base behavior. Joint behavior must be modeled when analyzing semi-rigid frames, which is associated with a mathematical model of the moment–rotation curve. The most accurate model uses continuous nonlinear functions. This article presents three areas of steel joint research: (1 analysis methods of semi-rigid joints; (2 prediction methods for the mechanical behavior of joints; (3 mathematical representations of the moment–rotation curve. In the current study, a new exponential model to depict the moment–rotation relationship of column base connection is proposed. The proposed nonlinear model represents an approach to the prediction of M–θ curves, taking into account the possible failure modes and the deformation characteristics of the connection elements. The new model has three physical parameters, along with two curve-fitted factors. These physical parameters are generated from dimensional details of the connection, as well as the material properties. The M–θ curves obtained by the model are compared with published connection tests and 3D FEM research. The proposed mathematical model adequately comes close to characterizing M–θ behavior through the full range of loading/rotations. As a result, modeling of column base connections using the proposed mathematical model can give crucial beforehand information, and overcome the disadvantages of time consuming workmanship and cost of experimental studies.

  16. The Fire Resistance Performance of Recycled Aggregate Concrete Columns with Different Concrete Compressive Strengths.

    Science.gov (United States)

    Dong, Hongying; Cao, Wanlin; Bian, Jianhui; Zhang, Jianwei

    2014-12-08

    In order to ascertain the fire resistance performance of recycled aggregate concrete (RAC) components with different concrete compressive strengths, four full-scaled concrete columns were designed and tested under high temperature. Two of the four specimens were constructed by normal concrete with compressive strength ratings of C20 and C30, respectively, while the others were made from recycled coarse aggregate (RCA) concrete of C30 and C40, respectively. Identical constant axial forces were applied to specimens while being subjected to simulated building fire conditions in a laboratory furnace. Several parameters from the experimental results were comparatively analyzed, including the temperature change, vertical displacement, lateral deflection, fire endurance, and failure characteristics of specimens. The temperature field of specimens was simulated with ABAQUS Software (ABAQUS Inc., Provindence, RI, USA) and the results agreed quite well with those from the experiments. Results show that the rate of heat transfer from the surface to the interior of the column increases with the increase of the concrete's compressive strength for both RAC columns and normal concrete columns. Under the same initial axial force ratio, for columns with the same cross section, those with lower concrete compressive strengths demonstrate better fire resistance performance. The fire resistance performance of RAC columns is better than that of normal concrete columns, with the same concrete compressive strength.

  17. Design and Operation of Cryogenic Distillation Research Column for Ultra-Low Background Experiments

    Science.gov (United States)

    Chiller, Christopher; Alanson Chiller, Angela; Jasinski, Benjamin; Snyder, Nathan; Mei, Dongming

    2013-04-01

    Motivated by isotopically enriched germanium (76Ge and 73Ge) for monocrystalline crystal growth for neutrinoless double-beta decay and dark matter experiments, a cryogenic distillation research column was developed. Without market availability of distillation columns in the temperature range of interest with capabilities necessary for our purposes, we designed, fabricated, tested, refined and operated a two-meter research column for purifying and separating gases in the temperature range from 100-200K. Due to interest in defining stratification, purity and throughput optimization, capillary lines were integrated at four equidistant points along the length of the column such that real-time residual gas analysis could guide the investigation. Interior gas column temperatures were monitored and controlled within 0.1oK accuracy at the top and bottom. Pressures were monitored at the top of the column to four significant figures. Subsequent impurities were measured at partial pressures below 2E-8torr. We report the performance of the column in this paper.

  18. Compensated Row-Column Ultrasound Imaging System Using Multilayered Edge Guided Stochastically Fully Connected Random Fields.

    Science.gov (United States)

    Ben Daya, Ibrahim; Chen, Albert I H; Shafiee, Mohammad Javad; Wong, Alexander; Yeow, John T W

    2017-09-06

    The row-column method received a lot of attention for 3-D ultrasound imaging. By reducing the number of connections required to address the 2-D array and therefore reducing the amount of data to handle, this addressing method allows for real time 3-D imaging. Row-column still has its limitations: the issues of sparsity, speckle noise inherent to ultrasound, the spatially varying point spread function, and the ghosting artifacts inherent to the row-column method must all be taken into account when building a reconstruction framework. In this research, we build on a previously published system and propose an edge-guided, compensated row-column ultrasound imaging system that incorporates multilayered edge-guided stochastically fully connected conditional random fields to address the limitations of the row-column method. Tests carried out on simulated and real row-column ultrasound images show the effectiveness of our proposed system over other published systems. Visual assessment show our proposed system's potential at preserving edges and reducing speckle. Quantitative analysis shows that our proposed system outperforms previously published systems when evaluated with metrics such as Peak Signal-to-Noise Ratio, Coefficient of Correlation, and Effective Number of Looks. These results show the potential of our proposed system as an effective tool for enhancing 3-D row-column imaging.

  19. The Fire Resistance Performance of Recycled Aggregate Concrete Columns with Different Concrete Compressive Strengths

    Science.gov (United States)

    Dong, Hongying; Cao, Wanlin; Bian, Jianhui; Zhang, Jianwei

    2014-01-01

    In order to ascertain the fire resistance performance of recycled aggregate concrete (RAC) components with different concrete compressive strengths, four full-scaled concrete columns were designed and tested under high temperature. Two of the four specimens were constructed by normal concrete with compressive strength ratings of C20 and C30, respectively, while the others were made from recycled coarse aggregate (RCA) concrete of C30 and C40, respectively. Identical constant axial forces were applied to specimens while being subjected to simulated building fire conditions in a laboratory furnace. Several parameters from the experimental results were comparatively analyzed, including the temperature change, vertical displacement, lateral deflection, fire endurance, and failure characteristics of specimens. The temperature field of specimens was simulated with ABAQUS Software (ABAQUS Inc., Provindence, RI, USA) and the results agreed quite well with those from the experiments. Results show that the rate of heat transfer from the surface to the interior of the column increases with the increase of the concrete’s compressive strength for both RAC columns and normal concrete columns. Under the same initial axial force ratio, for columns with the same cross section, those with lower concrete compressive strengths demonstrate better fire resistance performance. The fire resistance performance of RAC columns is better than that of normal concrete columns, with the same concrete compressive strength. PMID:28788279

  20. Performance of RC columns with partial length corrosion

    International Nuclear Information System (INIS)

    Wang Xiaohui; Liang Fayun

    2008-01-01

    Experimental and analytical studies on the load capacity of reinforced concrete (RC) columns with partial length corrosion are presented, where only a fraction of the column length was corroded. Twelve simply supported columns were eccentrically loaded. The primary variables were partial length corrosion in tensile or compressive zone and the corrosion level within this length. The failure of the corroded column occurs in the partial length, mainly developed from or located nearby or merged with the longitudinal corrosion cracks. For RC column with large eccentricity, load capacity of the column is mainly influenced by the partial length corrosion in tensile zone; while for RC column with small eccentricity, load capacity of the column greatly decreases due to the partial length corrosion in compressive zone. The destruction of the longitudinally mechanical integrality of the column in the partial length leads to this great reduction of the load capacity of the RC column

  1. Ultrasound-Guided Laryngeal Air Column Width Difference as a New Predictor for Postextubation Stridor in Children.

    Science.gov (United States)

    El Amrousy, Doaa; Elkashlan, Mohamed; Elshmaa, Nagat; Ragab, Ahmed

    2018-03-01

    To assess the efficacy of ultrasound-guided laryngeal air column width difference in predicting postextubation stridor in children. Prospective observational study. Single, tertiary care pediatric hospital. This study was carried out at PICU and surgical ICU, Tanta University Hospital on 400 ventilated children between January 2015 and May 2017. Patients who received mechanical ventilation and met criteria for a weaning trial were included. Laryngeal ultrasound and cuff leak test. Ultrasound-guided laryngeal air column width and cuff leak test were measured before extubation. Laryngeal air column width is the width of air between the vocal cords seen by laryngeal ultrasonography. Laryngeal air column width difference is the width difference of air column passed through vocal cords with the balloon cuff inflated and deflated. Three-hundred fifty six patients (89%) had no postextubation stridor, whereas 44 patients (11%) developed postextubation stridor. Postextubation stridor was associated with younger age, less weight, female gender, prolonged duration of intubation, and ICU stay (p column width difference and cuff leak test showed significant decrease (p column width difference at cutoff point of less than 0.8 mm gave a sensitivity of 93%, specificity of 86%, and accuracy of 91%, whereas cuff leak test at less than 11% yielded a sensitivity of (61%), specificity of (53%), and accuracy of (59%) for predicting postextubation stridor. Laryngeal air column width difference measurement may serve as a simple reliable noninvasive method for predicting postextubation stridor in children.

  2. Seabed gallery intakes: Investigation of the water pretreatment effectiveness of the active layer using a long-term column experiment

    KAUST Repository

    Dehwah, Abdullah; Missimer, Thomas M.

    2017-01-01

    ) in improving raw water quality was conducted by using a long-term bench-scale columns experiment. Two different media types, silica and carbonate sand, were tested in 1 m columns to evaluate the effectiveness of media type in terms of algae, bacteria, Natural

  3. Characterization of wide-pore reversed-phase columns for biopolymer separations. I. Single-parametric evaluation

    NARCIS (Netherlands)

    Bede, A; Rippel, G; Szepesy, L; Claessens, H.A.

    1996-01-01

    Nine prepacked wide-pore columns recommended for protein separation were studied. The stationary phases investigated were widely different with respect to the type of ligands. In order to characterize the columns, measurements were made with six different test mixtures containing two different

  4. Continuous treatment of heavy metal contaminated clay soils by extraction in stirred tanks and in a countercurrent column

    NARCIS (Netherlands)

    Tuin, B.J.W.; Tels, M.

    1991-01-01

    Extn. of metals from 2 contaminated waste site clay soils by 0.1-0.3 N HCl solns. was tested in 3 lab. scale, continuous processes: 2 stirred tank reactors (CSTR' s) in series; a countercurrent sieve-plate column fed with flocculated clay soil materials; and a combination of tank reactor and column.

  5. Behaviour of FRP confined concrete in square columns

    Directory of Open Access Journals (Sweden)

    de Diego, A.

    2015-12-01

    Full Text Available A significant amount of research has been conducted on FRP-confined circular columns, but much less is known about rectangular/square columns in which the effectiveness of confinement is much reduced. This paper presents the results of experimental investigations on low strength square concrete columns confined with FRP. Axial compression tests were performed on ten intermediate size columns. The tests results indicate that FRP composites can significantly improve the bearing capacity and ductility of square section reinforced concrete columns with rounded corners. The strength enhancement ratio is greater the lower the concrete strength and also increases with the stiffness of the jacket. The confined concrete behaviour was predicted according to the more accepted theoretical models and compared with experimental results. There are two key parameters which critically influence the fitting of the models: the strain efficiency factor and the effect of confinement in non-circular sections.La mayoría de las investigaciones sobre hormigón confinado con FRP se han realizado sobre pilares de sección circular, pero el comportamiento en secciones cuadradas/rectangulares, donde el confinamiento es menos eficaz, es mucho menos conocido. Este trabajo presenta los resultados de un estudio experimental sobre probetas de hormigón de baja resistencia y sección cuadrada. Se han ensayado a compresión centrada diez probetas de tamaño intermedio. Los resultados indican que el confinamiento mejora significativamente la resistencia y ductilidad del hormigón en columnas de sección cuadrada con las esquinas redondeadas. El incremento de resistencia es mayor cuanto menor es la resistencia del hormigón sin confinar y también aumenta con la rigidez del encamisado. Los resultados se compararon con los obtenidos según los modelos teóricos más aceptados. Hay dos parámetros críticos en el ajuste de los modelos: el factor de eficiencia de la deformación y el

  6. Scalability of pre-packed preparative chromatography columns with different diameters and lengths taking into account extra column effects.

    Science.gov (United States)

    Schweiger, Susanne; Jungbauer, Alois

    2018-02-16

    Small pre-packed columns are commonly used to estimate the optimum run parameters for pilot and production scale. The question arises if the experiments obtained with these columns are scalable, because there are substantial changes in extra column volume when going from a very small scale to a benchtop column. In this study we demonstrate the scalability of pre-packed disposable and non-disposable columns of volumes in the range of 0.2-20 ml packed with various media using superficial velocities in the range of 30-500 cm/h. We found that the relative contribution of extra column band broadening to total band broadening was not only high for columns with small diameters, but also for columns with a larger volume due to their wider diameter. The extra column band broadening can be more than 50% for columns with volumes larger than 10 ml. An increase in column diameter leads to high additional extra column band broadening in the filter, frits, and adapters of the columns. We found a linear relationship between intra column band broadening and column length, which increased stepwise with increases in column diameter. This effect was also corroborated by CFD simulation. The intra column band broadening was the same for columns packed with different media. An empirical engineering equation and the data gained from the extra column effects allowed us to predict the intra, extra, and total column band broadening just from column length, diameter, and flow rate. Copyright © 2018 The Author(s). Published by Elsevier B.V. All rights reserved.

  7. Convolutional Codes with Maximum Column Sum Rank for Network Streaming

    OpenAIRE

    Mahmood, Rafid; Badr, Ahmed; Khisti, Ashish

    2015-01-01

    The column Hamming distance of a convolutional code determines the error correction capability when streaming over a class of packet erasure channels. We introduce a metric known as the column sum rank, that parallels column Hamming distance when streaming over a network with link failures. We prove rank analogues of several known column Hamming distance properties and introduce a new family of convolutional codes that maximize the column sum rank up to the code memory. Our construction invol...

  8. Optimization and simulation of tandem column supercritical fluid chromatography separations using column back pressure as a unique parameter.

    Science.gov (United States)

    Wang, Chunlei; Tymiak, Adrienne A; Zhang, Yingru

    2014-04-15

    Tandem column supercritical fluid chromatography (SFC) has demonstrated to be a useful technique to resolve complex mixtures by serially coupling two columns of different selectivity. The overall selectivity of a tandem column separation is the retention time weighted average of selectivity from each coupled column. Currently, the method development merely relies on extensive screenings and is often a hit-or-miss process. No attention is paid to independently adjust retention and selectivity contributions from individual columns. In this study, we show how tandem column SFC selectivity can be optimized by changing relative dimensions (length or inner diameter) of the coupled columns. Moreover, we apply column back pressure as a unique parameter for SFC optimization. Continuous tuning of tandem column SFC selectivity is illustrated through column back pressure adjustments of the upstream column, for the first time. In addition, we show how and why changing coupling order of the columns can produce dramatically different separations. Using the empirical mathematical equation derived in our previous study, we also demonstrate a simulation of tandem column separations based on a single retention time measurement on each column. The simulation compares well with experimental results and correctly predicts column order and back pressure effects on the separations. Finally, considerations on instrument and column hardware requirements are discussed.

  9. Built for speed: strain in the cartilaginous vertebral columns of sharks.

    Science.gov (United States)

    Porter, M E; Diaz, Candido; Sturm, Joshua J; Grotmol, Sindre; Summers, A P; Long, John H

    2014-02-01

    In most bony fishes vertebral column strain during locomotion is almost exclusively in the intervertebral joints, and when these joints move there is the potential to store and release strain energy. Since cartilaginous fishes have poorly mineralized vertebral centra, we tested whether the vertebral bodies undergo substantial strain and thus may be sites of energy storage during locomotion. We measured axial strains of the intervertebral joints and vertebrae in vivo and ex vivo to characterize the dynamic behavior of the vertebral column. We used sonomicrometry to directly measure in vivo and in situ strains of intervertebral joints and vertebrae of Squalus acanthias swimming in a flume. For ex vivo measurements, we used a materials testing system to dynamically bend segments of vertebral column at frequencies ranging from 0.25 to 1.00 Hz and a range of physiologically relevant curvatures, which were determined using a kinematic analysis. The vertebral centra of S. acanthias undergo strain during in vivo volitional movements as well as in situ passive movements. Moreover, when isolated segments of vertebral column were tested during mechanical bending, we measured the same magnitudes of strain. These data support our hypothesis that vertebral column strain in lateral bending is not limited to the intervertebral joints. In histological sections, we found that the vertebral column of S. acanthias has an intracentral canal that is open and covered with a velum layer. An open intracentral canal may indicate that the centra are acting as tunics around some sections of a hydrostat, effectively stiffening the vertebral column. These data suggest that the entire vertebral column of sharks, both joints and centra, is mechanically engaged as a dynamic spring during locomotion. Copyright © 2013 Elsevier GmbH. All rights reserved.

  10. Influence of pressure on the properties of chromatographic columns. II. The column hold-up volume.

    Science.gov (United States)

    Gritti, Fabrice; Martin, Michel; Guiochon, Georges

    2005-04-08

    The effect of the local pressure and of the average column pressure on the hold-up column volume was investigated between 1 and 400 bar, from a theoretical and an experimental point of view. Calculations based upon the elasticity of the solids involved (column wall and packing material) and the compressibility of the liquid phase show that the increase of the column hold-up volume with increasing pressure that is observed is correlated with (in order of decreasing importance): (1) the compressibility of the mobile phase (+1 to 5%); (2) in RPLC, the compressibility of the C18-bonded layer on the surface of the silica (+0.5 to 1%); and (3) the expansion of the column tube (columns packed with the pure Resolve silica (0% carbon), the derivatized Resolve-C18 (10% carbon) and the Symmetry-C18 (20% carbon) adsorbents, using water, methanol, or n-pentane as the mobile phase. These solvents have different compressibilities. However, 1% of the relative increase of the column hold-up volume that was observed when the pressure was raised is not accounted for by the compressibilities of either the solvent or the C18-bonded phase. It is due to the influence of the pressure on the retention behavior of thiourea, the compound used as tracer to measure the hold-up volume.

  11. Pulsing flow in trickle bed columns

    NARCIS (Netherlands)

    Blok, Jan Rudolf

    1981-01-01

    In the operation of a packed column with cocurrent downflow of gas and liquid (trickle bed) several flowpatterns can be observed depending on the degree of interaction between gas and liquid. At low liquid and gas flow rates - low interaction - gascontinuous flow occurs. In this flowregime, the

  12. Revive your columns with cyclic distillation

    NARCIS (Netherlands)

    Kiss, Anton A.; Bîldea, Costin Sorin

    2015-01-01

    The process intensification (PI) technique involves changing a tower?s internals and operating mode and the separate movement of the liquid and vapor phases. This can significantly increase column throughput and reduce energy requirements, while improving separation performance. PI is a set of

  13. Robust Geometric Control of a Distillation Column

    DEFF Research Database (Denmark)

    Kymmel, Mogens; Andersen, Henrik Weisberg

    1987-01-01

    A frequency domain method, which makes it possible to adjust multivariable controllers with respect to both nominal performance and robustness, is presented. The basic idea in the approach is that the designer assigns objectives such as steady-state tracking, maximum resonance peaks, bandwidth, m...... is used to examine and improve geometric control of a binary distillation column....

  14. On Row Rank Equal Column Rank

    Science.gov (United States)

    Khalili, Parviz

    2009-01-01

    We will prove a well-known theorem in Linear Algebra, that is, for any "m x n" matrix the dimension of row space and column space are the same. The proof is based on the subject of "elementary matrices" and "reduced row-echelon" form of a matrix.

  15. On Stability of a Bubble Column

    Czech Academy of Sciences Publication Activity Database

    Růžička, Marek

    2013-01-01

    Roč. 91, č. 2 (2013), s. 191-203 ISSN 0263-8762 R&D Projects: GA ČR GA104/07/1110 Institutional support: RVO:67985858 Keywords : bubble column * flow regimes * steady solution Subject RIV: CI - Industrial Chemistry, Chemical Engineering Impact factor: 2.281, year: 2013

  16. Thermal Analysis of LANL Ion Exchange Column

    International Nuclear Information System (INIS)

    Laurinat, J.E.

    1999-01-01

    This document reports results from an ion exchange column heat transfer analysis requested by Los Alamos National Laboratory (LANL). The object of the analysis is to demonstrate that the decay heat from the Pu-238 will not cause resin bed temperatures to increase to a level where the resin significantly degrades

  17. Column Stores as an IR Prototyping Tool

    NARCIS (Netherlands)

    H.F. Mühleisen (Hannes); T. Samar (Thaer); J.J.P. Lin (Jimmy); A.P. de Vries (Arjen)

    2014-01-01

    textabstract. We make the suggestion that instead of implementing custom index structures and query evaluation algorithms, IR researchers should simply store document representations in a column-oriented relational database and write ranking models using SQL. For rapid prototyping, this is

  18. Sol-gel open tubular ODS columns with reversed electroosmotic flow for capillary electrochromatography.

    Science.gov (United States)

    Hayes, J D; Malik, A

    2001-03-01

    Sol-gel chemistry was successfully used for the fabrication of open tubular columns with surface-bonded octadecylsilane (ODS) stationary-phase coating for capillary electrochromatography (OT-CEC). Following column preparations, a series of experiments were performed to investigate the performance of the sol-gel coated ODS columns in OT-CEC. The incorporation of N-octadecyldimethyl[3-(trimethoxysilyl)propyl]ammonium chloride as one of the sol-gel precursors played an important role in the electrochromatographic performance of the prepared columns. This chemical reagent possesses a chromatographically favorable, bonded ODS moiety, in conjunction with three methoxy groups allowing for sol-gel reactivity. In addition, a positively charged nitrogen atom is present in the molecular structure of this reagent and provides a positively charged capillary surface responsible for the reversed electroosmotic flow (EOF) in the columns during CEC operation. Comparative studies involving the EOF within such sol-gel ODS coated and uncoated capillaries were performed using acetonitrile and methanol as the organic modifiers in the mobile phase. The use of a deactivating reagent, phenyldimethylsilane, in the sol-gel solution was evaluated. Efficiency values of over 400,000 theoretical plates per meter were achieved in CEC on a 64 cm x 25 microm i.d. sol-gel ODS open tubular column. Test mixtures of polycyclic aromatic hydrocarbons, benzene derivatives, and aromatic aldehydes and ketones were used to evaluate the CEC performances of both nondeactivated and deactivated open tubular sol-gel columns. The effects of mobile-phase organic modifier contents and pH on EOF in such columns were evaluated. The prepared sol-gel ODS columns are characterized by switchable electroosmotic flow. A pH value of approximately 8.5 was found correspond to the isoelectric point for the prepared sol-gel ODS coatings.

  19. Multi-Column Xe/Kr Separation with AgZ-PAN and HZ-PAN

    International Nuclear Information System (INIS)

    Greenhalgh, Mitchell Randy; Garn, Troy Gerry; Welty, Amy Keil; Watson, Tony Leroy

    2016-01-01

    Previous multi-column xenon/krypton separation tests have demonstrated the capability of separating xenon from krypton in a mixed gas feed stream. The results of this initial testing with AgZ-PAN and HZ-PAN indicated that an excellent separation of xenon from krypton could be achieved. Building upon these initial results, a series of additional multi-column testing were performed in FY-16. The purpose of this testing was to scale up the sorbent beds, test a different composition of feed gas and attempt to improve the accuracy of the analysis of the individual capture columns' compositions. Two Stirling coolers were installed in series to perform this testing. The use of the coolers instead of the cryostat provided two desired improvements, 1) removal of the large dilution due to the internal volume of the cryostat adsorption chamber, and 2) ability to increase the sorbent bed size for scale-up. The AgZ-PAN sorbent, due to its xenon selectivity, was loaded in the first column to capture the xenon while allowing the krypton to flow through and be routed to a second column containing the HZ-PAN for capture and analysis. The gases captured on both columns were sampled with evacuated sample bombs and subsequently analyzed via GC-MS for both krypton and xenon. The results of these tests can be used to develop the scope of future testing and analysis using this test bed for demonstrating the capture and separation of xenon and krypton using sorbents, for demonstrating desorption and regeneration of the sorbents, and for determining compositions of the desorbed gases. They indicate a need for future desorption studies in order to better quantify co-adsorbed species and final krypton purity.

  20. Single column and two-column H-D-T distillation experiments at TSTA

    International Nuclear Information System (INIS)

    Yamanishi, T.; Yoshida, H.; Hirata, S.; Naito, T.; Naruse, Y.; Sherman, R.H.; Bartlit, J.R.; Anderson, J.L.

    1988-01-01

    Cryogenic distillation experiments were peformed at TSTA with H-D-T system by using a single column and a two-column cascade. In the single column experiment, fundamental engineering data such as the liquid holdup and the HETP were measured under a variety of operational condtions. The liquid holdup in the packed section was about 10 /approximately/ 15% of its superficial volume. The HETP values were from 4 to 6 cm, and increased slightly with the vapor velocity. The reflux ratio had no effect on the HETP. For the wo-colunn experiemnt, dynamic behavior of the cascade was observed. 8 refs., 7 figs., 2 tabs

  1. The central column structure in SPHEX

    International Nuclear Information System (INIS)

    Duck, R.C.; French, P.A.; Browning, P.K.; Cunningham, G.; Gee, S.J.; al-Karkhy, A.; Martin, R.; Rusbridge, M.G.

    1994-01-01

    SPHEX is a gun injected spheromak in which a magnetised Marshall gun generates and maintains an approximately axisymmetric toroidal plasma within a topologically spherical flux conserving vessel. The central column has been defined as a region of high mean floating potential, f > up to ∼ 150 V, aligned with the geometric axis of the device. It has been suggested that this region corresponds to the open magnetic flux which is connected directly to the central electrode of the gun and links the toroidal annulus (in which f > ∼ 0 V). Poynting vector measurements have shown that the power required to drive toroidal current in the annulus is transmitted out of the column by the coherent 20 kHz mode which pervades the plasma. Measurements of the MHD dynamo in the column indicate an 'antidynamo' electric field due to correlated fluctuations in v and B at the 20 kHz mode frequency which is consistent with the time-averaged Ohm's Law. On shorting the gun electrodes, the density in the column region decays rapidly leaving a 'hole' of radius R c ∼ 7 cm. This agrees with the estimated dimension of the open flux from mean internal B measurements and axisymmetric force-free equilibrium modelling, but is considerably smaller than the radius of ∼ 13 cm inferred from the time-averaged potential. In standard operating conditions the gun delivers a current of I G ∼ 60 kA at V G ∼ 500 V for ∼ 1 ms, driving a toroidal current of I t ∼ 60 kA. Ultimately we wish to understand the mechanism which drives toroidal current in the annulus; the central column is of interest because of the crucial role it plays in this process. (author) 8 refs., 6 figs

  2. A simple, fast, and accurate thermodynamic-based approach for transfer and prediction of gas chromatography retention times between columns and instruments Part III: Retention time prediction on target column.

    Science.gov (United States)

    Hou, Siyuan; Stevenson, Keisean A J M; Harynuk, James J

    2018-03-27

    This is the third part of a three-part series of papers. In Part I, we presented a method for determining the actual effective geometry of a reference column as well as the thermodynamic-based parameters of a set of probe compounds in an in-house mixture. Part II introduced an approach for estimating the actual effective geometry of a target column by collecting retention data of the same mixture of probe compounds on the target column and using their thermodynamic parameters, acquired on the reference column, as a bridge between both systems. Part III, presented here, demonstrates the retention time transfer and prediction from the reference column to the target column using experimental data for a separate mixture of compounds. To predict the retention time of a new compound, we first estimate its thermodynamic-based parameters on the reference column (using geometric parameters determined previously). The compound's retention time on a second column (of previously determined geometry) is then predicted. The models and the associated optimization algorithms were tested using simulated and experimental data. The accuracy of predicted retention times shows that the proposed approach is simple, fast, and accurate for retention time transfer and prediction between gas chromatography columns. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  3. Lithium-sodium separation by ion-exchange. Particular study of a pulsed column

    International Nuclear Information System (INIS)

    Auvert, H.

    1966-02-01

    A study is made of the operational conditions and constraints in the case of a moving-bed ion-exchange column subjected to pulses. The example chosen to illustrate its application concerns the lithium-sodium separation in a hydroxide medium (LiOH, NaOH). In the first part, the physico-chemical characteristics of the exchange and the kinetic characteristics of the exchange-reaction are considered. In the second part, the operation of the pulsed column is studied. Using the results obtained in the first part, the conditions required for study state operation are determined. When this is obtained, it is possible to calculate the height equivalent of the theoretical plate (HETP) of the installation. A study is also made of 'sliding', a phenomenon peculiar to pulsed columns. The results obtained show that it is possible, using laboratory tests, to determine the characteristics and the operational condition of a moving-bed ion-exchange column. (author) [fr

  4. Simulation and control synthesis for a pulse column separation system for plutonium--uranium recovery

    International Nuclear Information System (INIS)

    McCutcheon, E.B.

    1975-05-01

    Control of a plutonium-uranium partitioning column was studied using a mathematical model developed to simulate the dynamic response and to test postulated separation mechanisms. The column is part of a plutonium recycle flowsheet developed for the recovery of plutonium and uranium from metallurgical scrap. In the first step of the process, decontamination from impurities is achieved by coextracting plutonium and uranium in their higher oxidation states. In the second step, reduction of the plutonium to a lower oxidation state allows partitioning of the plutonium and uranium. The use of hydroxylamine for the plutonium reduction in this partitioning column is a unique feature of the process. The extraction operations are carried out in pulse columns. (U.S.)

  5. Numerical and experimental analysis of time-dependent load transfer in reinforced concrete columns

    Directory of Open Access Journals (Sweden)

    L. T. Kataoka

    Full Text Available A study was conducted to assess the influence of the steel reinforcement ratio in concrete columns on their properties of creep and shrinkage. Experimental tests and three-dimensional finite element-based simulations of the experimental curves from plain concrete cylinders and plain concrete columns derived by curve fitting were performed using the ACI 209 model available in DIANA 9.3. Columns with longitudinal reinforcement ratios of 0%, 1.4% and 2.8%, loaded to 30% and 40% of their 7-day compressive strength, were investigated. The results indicated that numerical simulation does not predict experimental data for a long period. However, simulations fitted with experimental curves derived from plain concrete columns presented values close to those of experimental data for 91 days.

  6. Behavior of FRP-Confined Concrete-Filled Steel Tube Columns

    Directory of Open Access Journals (Sweden)

    Yiyan Lu

    2014-05-01

    Full Text Available This paper presents the results of an experimental study into the behavior of concrete-filled steel tube columns confined by fiber-reinforced polymer (FRP. Eleven columns were tested to investigate the effects of the FRP layer number, the thickness of the steel tube and concrete strength on their load capacity and axial deformation capacity. The experimental results indicated that the FRP wrap can effectively confine the concrete expansion and delay the local buckling of the steel tube. Both the load capacity and the axial deformation capacity of concrete-filled steel tube columns can be substantially enhanced with FRP confinement. A model is proposed to predict the load capacity of the FRP-confined concrete-filled steel tube columns. The predicted results are generally in good agreement with the experimental ones obtained in this study and in the literature.

  7. Effect of load eccentricity on the buckling of thin-walled laminated C-columns

    Science.gov (United States)

    Wysmulski, Pawel; Teter, Andrzej; Debski, Hubert

    2018-01-01

    The study investigates the behaviour of short, thin-walled laminated C-columns under eccentric compression. The tested columns are simple-supported. The effect of load inaccuracy on the critical and post-critical (local buckling) states is examined. A numerical analysis by the finite element method and experimental tests on a test stand are performed. The samples were produced from a carbon-epoxy prepreg by the autoclave technique. The experimental tests rest on the assumption that compressive loads are 1.5 higher than the theoretical critical force. Numerical modelling is performed using the commercial software package ABAQUS®. The critical load is determined by solving an eigen problem using the Subspace algorithm. The experimental critical loads are determined based on post-buckling paths. The numerical and experimental results show high agreement, thus demonstrating a significant effect of load inaccuracy on the critical load corresponding to the column's local buckling.

  8. Punching shear in reinforced concrete flat slabs with hole adjacent to the column and moment transfer

    Directory of Open Access Journals (Sweden)

    D. C. Oliveira

    Full Text Available The structural behavior and the ultimate punching shear resistance of internal reinforced concrete flat slab-column connections, with one hole adjacent to the column, with or without flexural moment transfer of the slab to the column was investigated. Main variables were: the existence whether or not hole, flexural reinforcement layout and ratio, the direction and sense of the moment transferred and the eccentricity of the load (M (moment transferred to column / V (shear ratio at the connection - 0,50 m or 0,25 m. Seven internal slab-column joining were tested and ultimate loads, cracking, deflections, concrete and reinforcement strains were analyzed. The existence of hole adjacent to the smaller column dimension, the hole dimension, flexural reinforcement rate and placing, the variation of relation Mu/Vu in function of the load, and, than, of eccentricity of the load, influenced the slabs behavior and rupture load. Test results were compared with the estimations from CEB-FIP/MC1990 [7], EC2/2004 [12], ACI-318:2011 [1] and NBR 6118:2007 [5]. ACI [1] and EC2 [12] presented most conservative estimates, although have presented some non conservative estimates. Brazilian NBR [5], even though being partly based in EC2 [12], presented smaller conservative estimates and more non conservative estimates. A modification on all codes is proposed for taking in account the moment caused by the eccentricity at the critical perimeter for slabs with holes.

  9. Numerical Investigation of Slab-Column Connection by Finite Element Method

    International Nuclear Information System (INIS)

    Akram, T.; Shaikh, M.A.; Memon, A.A.

    2007-01-01

    The flat slab-on-column construction subjected to high transverse stresses concentrated at the slab-column connection can lead to a non-ductile, sudden and brittle punching failure and results in the accidental collapse of flat slab buildings. The major parameters affecting the slab-column connection are the concrete strength, slab thickness, slab reinforcement and aspect ratio of column. The application of numerical methods based on the finite element theory for solving practical tasks allow to perform virtual testing of structures and explore their behavior under load and other effects in different conditions taking into account the elastic and plastic behavior of materials, appearance and development of cracks and other damages (disintegrations), and finally to simulate the failure mechanism and its consequences. In this study, the models are developed to carry out the finite element analysis of slab- column connection using ADINA (Automatic Dynamic Incremental Nonlinear Analysis) by varying the slab thickness and slab confining reinforcement and to investigate their effect on the deflection and load carrying capacity. Test results indicate that by increasing the slab thickness, the deflection and the load carrying capacity of slab-column connection increases, more over, by increasing the slab confining reinforcement, the deflection decreases where as the load carrying capacity increases. (author)

  10. Determination of the vildagliptin intermediate enantiomer by chiralce-columns

    Directory of Open Access Journals (Sweden)

    Weina LI

    2017-06-01

    Full Text Available In order to establish a NP-HPLC method for the determination of enantiomer in vildagliptin intermediate, the determination is carried out on the column of ChiralpakAD-H(250 mm×4.6 mm, 5 μm, with the mobile phase of n-hexane, ethanol and methanol(volume ratio of 65∶25∶10)at flow rate of 0.8 mL/min. The sample volume is 10 μL, the wavelength is 210 nm and the column temperature is 35 ℃. The result shows that the vildagliptin intermediate and its enantiomer could be well separated and detected effectively; blank solvent doesn't interfere with the enantiomer assaying; the detection limit is 27 ng/mL and the quantification limit is 81 ng/mL; in repetitive test, the RSD of enantiomer assaying of samples are no more than 2.0%; in stability test, the RSD are no more than 2.0% in 12 h; the vildagliptin intermediate and its enantiomer could be well separated in the test of durability with all RSDs below 2.0%. The method is simple, reliable, accurate and durable, and can be used for determination of enantiomer in vildagliptin intermediate.

  11. Test

    DEFF Research Database (Denmark)

    Bendixen, Carsten

    2014-01-01

    Bidrag med en kortfattet, introducerende, perspektiverende og begrebsafklarende fremstilling af begrebet test i det pædagogiske univers.......Bidrag med en kortfattet, introducerende, perspektiverende og begrebsafklarende fremstilling af begrebet test i det pædagogiske univers....

  12. Comparative Analysis of Existing RC Columns Jacketed with CFRP or FRCC

    Directory of Open Access Journals (Sweden)

    Marta Del Zoppo

    2018-03-01

    Full Text Available Reinforced concrete (RC columns typical of existing structures often exhibit premature failures during seismic events (i.e., longitudinal bars buckling and shear interaction mechanisms due to the poor quality concrete and the absence of proper seismic details in the potential plastic hinge region. The Fiber Reinforced Polymers (FRP externally bonded reinforcement is known to be a valid technique to improve the shear capacity or the ductility of existing RC columns. However, few experimental tests have proven its effectiveness in the case of columns affected by shear interaction mechanisms. In this work, the behavior of existing RC columns with border line behavior between flexure and shear have been investigated in the case of poor quality concrete and light FRP strengthening with local jacketing and medium quality concrete and strong FRP strengthening with local jacketing, in order to highlight the effect of concrete strength on the effectiveness of the retrofit intervention. As an alternative to FRP jacketing; the effectiveness of the Fiber Reinforced Cementitious Composite (FRCC jacketing for the seismic strengthening of columns with highly deteriorated concrete cover or columns already damaged by an earthquake is also evaluated. Six full-scale RC columns have been tested under cyclic loading: one was used as a control specimen; four were strengthened in the potential plastic hinge region with carbon FRP (CFRP; and one was fully jacketed with FRCC. The comparison between poor and medium quality concrete columns showed that the CFRP local jacketing is more effective in the case of poor quality concrete. The FRCC jacketing appears to be a sound repair strategy and a suitable alternative to the FRP jacketing in case of poor quality; however, more experimental research is needed for improving this retrofit technique.

  13. Column, particularly extraction column, for fission and/or breeder materials

    International Nuclear Information System (INIS)

    Vietzke, H.; Pirk, H.

    1980-01-01

    An absorber rod with a B 4 C insert is situated in the long extraction column for a uranyl nitrate solution or a plutonium nitrate solution. The geometrical dimensions are designed for a high throughput with little corrosion. (DG) [de

  14. RETENTION TIME EFFECT ON METAL REMOVAL BY PEAT COLUMNS

    Energy Technology Data Exchange (ETDEWEB)

    Nelson, E

    2007-02-28

    The potential use of a peat bed to treat the H-12 Outfall discharge to bring it to new compliance limits was previously investigated and reported utilizing a 7 hour retention time. The influence of retention time (contact time) of water with peat moss on the removal of copper from the water was investigated under laboratory conditions using vertical flow peat moss columns. Reduction of the necessary retention time has a large influence on the design sizing of any peat bed that would be constructed to treat the H-12 discharge on a full scale basis. Retention times of 5 hours, 3 hours and 1 hour were tested to determine the copper removal by the peat columns using vertical flow. Water samples were collected after 4, 8, 12, and 16 water volumes had passed through the columns and analyzed for a suite of metals, with quantitative emphasis on copper. Laboratory results indicated that copper removal was very high at each of the 3 retention times tested, ranging from 99.6 % removal at 5 and 3 hours to 98.8% removal at 1 hour. All these values are much lower that the new compliance limit for the outfall. The results also indicated that most divalent metals were removed to their normal reporting detection limit for the analytical methods used, including zinc. Lead levels in the H-12 discharge used in this study were below PQL in all samples analyzed. While each of the retention times studied removed copper very well, there were indications that 1 hour is probably too short for an operational, long-term facility. At that retention time, there was about 6% compaction of the peat in the column due to the water velocity, and this may affect long term hydraulic conductivity of the peat bed. At that retention time, copper concentration in the effluent was higher than the other times tested, although still very low. Because of the potential compacting and somewhat reduced removal efficiency at a 1 hour retention time, it would be prudent to design to at least a 3 hour retention

  15. Joint and column behaviour of slotted cold-formed steel studs

    DEFF Research Database (Denmark)

    Andreassen, Michael Joachim; Jönsson, Jeppe

    2015-01-01

    the behaviour of the studs and the track joints. The experiments include a joint design with a special web stiffener used in practice. The studs are made of C-profiles and the tracks of U-profiles. Eight different test series are performed. The test series each have different column lengths, thicknesses...

  16. Evaluation of a timber column bent substructure after more than 60 years in-service

    Science.gov (United States)

    James P. Wacker; Xiping Wang; Douglas R. Rammer; William J. Nelson

    2011-01-01

    This paper describes both the field evaluation and laboratory testing of two timber-column-bent bridge substructures. These substructures served as intermediate pier supports for the East Deer Park Drive Bridge located in Gaithersburg, Maryland. A field evaluation of the bridge substructure was conducted in September 2008. Nondestructive testing was performed with a...

  17. Joint and column behaviour of slotted cold-formed steel studs

    DEFF Research Database (Denmark)

    Andreassen, Michael Joachim; Jönsson, Jeppe

    2015-01-01

    the behaviour of the studs and the track joints. The experiments included a joint design with a special web stiffener used in practice. The studs were C-sections and the tracks were U-sections. Eight different test series were performed. Each test series had different column lengths and thicknesses, both...

  18. Assembly procedure for column cutting platform

    International Nuclear Information System (INIS)

    Routh, R.D.

    1995-01-01

    This supporting document describes the assembly procedure for the Column Cutting Platform and Elevation Support. The Column Cutting Platform is a component of the 241-SY-101 Equipment Removal System. It is set up on the deck of the Strongback Trailer to provide work access to cut off the upper portion of the Mitigation Pump Assembly (MPA). The Elevation Support provides support for the front of the Storage Container with the Strongback at an inclined position. The upper portion of the MPA must be cut off to install the Containment Caps on the Storage Container. The storage Container must be maintained in an inclined position until the Containment Caps are installed to prevent any residual liquids from migrating forward in the Storage Container

  19. Modeling of Crystalline Silicotitanate Ion Exchange Columns

    International Nuclear Information System (INIS)

    Walker, D.D.

    1999-01-01

    Non-elutable ion exchange is being considered as a potential replacement for the In-Tank Precipitation process for removing cesium from Savannah River Site (SRS) radioactive waste. Crystalline silicotitanate (CST) particles are the reference ion exchange medium for the process. A major factor in the construction cost of this process is the size of the ion exchange column required to meet product specifications for decontaminated waste. To validate SRS column sizing calculations, SRS subcontracted two reknowned experts in this field to perform similar calculations: Professor R. G. Anthony, Department of Chemical Engineering, Texas A ampersand 038;M University, and Professor S. W. Wang, Department of Chemical Engineering, Purdue University. The appendices of this document contain reports from the two subcontractors. Definition of the design problem came through several meetings and conference calls between the participants and SRS personnel over the past few months. This document summarizes the problem definition and results from the two reports

  20. Sands subjected to repetitive vertical loading under zero lateral strain: accumulation models, terminal densities, and settlement

    KAUST Repository

    Chong, Song Hun; Santamarina, Carlos

    2016-01-01

    ). Repetitive vertical loading tests under zero lateral strain conditions are conducted using three different sands packed at initially low and high densities. Test results show that plastic strain accumulation for all sands and density conditions can

  1. Seismic Response of a Platform-Frame System with Steel Columns

    Directory of Open Access Journals (Sweden)

    Davide Trutalli

    2017-04-01

    Full Text Available Timber platform-frame shear walls are characterized by high ductility and diffuse energy dissipation but limited in-plane shear resistance. A novel lightweight constructive system composed of steel columns braced with oriented strand board (OSB panels was conceived and tested. Preliminary laboratory tests were performed to study the OSB-to-column connections with self-drilling screws. Then, the seismic response of a shear wall was determined performing a quasi-static cyclic-loading test of a full-scale specimen. Results presented in this work in terms of force-displacement capacity show that this system confers to shear walls high in-plane strength and stiffness with good ductility and dissipative capacity. Therefore, the incorporation of steel columns within OSB bracing panels results in a strong and stiff platform-frame system with high potential for low- and medium-rise buildings in seismic-prone areas.

  2. Behavior and Three-Dimensional Finite Element Modeling of Circular Concrete Columns Partially Wrapped with FRP Strips

    Directory of Open Access Journals (Sweden)

    Junjie Zeng

    2018-03-01

    Full Text Available Fiber-reinforced polymer (FRP jacketing/wrapping has become an attractive strengthening technique for concrete columns. Wrapping an existing concrete column with continuous FRP jackets with the fiber in the jacket being oriented in the hoop direction is referred to as FRP full wrapping strengthening technique. In practice, however, strengthening concrete columns with vertically discontinuous FRP strips is also favored and this technique is referred to as FRP partial wrapping strengthening technique. Existing research has demonstrated that FRP partial wrapping strengthening technique is a promising and economical alternative to the FRP full wrapping strengthening technique. Although extensive experimental investigations have hitherto been conducted on partially FRP-confined concrete columns, the confinement mechanics of confined concrete in partially FRP-confined circular columns remains unclear. In this paper, an experimental program consisting of fifteen column specimens was conducted and the test results were presented. A reliable three-dimensional (3D finite element (FE approach for modeling of partially FRP-confined circular columns was established. In the proposed FE approach, an accurate plastic-damage model for concrete under multiaxial compression is employed. The accuracy of the proposed FE approach was verified by comparisons between the numerical results and the test results. Numerical results from the verified FE approach were then presented to gain an improved understanding of the behavior of confined concrete in partially FRP-confined concrete columns.

  3. Study on application of single-crystal ice `Kurobe ice column` to high-speed skating rinks. Demonstration test result at Olympic memorial arena `M wave` in Nagano city; Tankesshohyo `Kurobe no hyojun` no kosoku skate link eno tekiyosei kenkyu. Naganoshi olympic kinen arina `Emu Wave` deno jissho shiken kekka

    Energy Technology Data Exchange (ETDEWEB)

    Iwasaki, M. [Kansai Electric Power Co. Inc., Osaka (Japan)

    1999-06-10

    For high-speed low-friction skating rinks, research was made on sticking artificial ice columns (ice bamboo shoot). The ice columns were fabricated with the ice column production equipment equipped with 4-line water droplet dropping devices which were installed at intervals of 0.3m on both sides of a pathway of 200m long, 2.6m wide and 1.8m high in the lateral adit of Kurobegawa No.4 hydroelectric power station. The grown ice columns were processed for high-speed skating rinks through cutting, confirmation of single crystal and crystal orientation, slicing for every 7mm thickness and packaging. The ice columns were spread all over the rink while sliding them to prevent mixing of bubbles after spraying distilled water of nearly 25 degreesC onto base ices. In addition, hot water of nearly 40 degreesC was sprayed to produce the final ice rink of 30mm thick by nearly 5mm a day. The dynamic friction coefficient of the ice column rink reduced to 0.0038 by nearly 16% as compared with 0.0045 of conventional rinks. (NEDO)

  4. Optimization of the isotope separation in columns

    International Nuclear Information System (INIS)

    Kaminskij, V.A.; Vetsko, V.M.; Tevzadze, G.A.; Devdariani, O.A.; Sulaberidze, G.A.

    1982-01-01

    The general method for the multi-parameter optimization of cascade plants of packed columns is proposed. As an optimization effectiveness function a netcost of the isotopic product is selected. The net cost is comprehensively characterizing the sum total of capital costs for manufacturing the products as well as determining the choice of the most effective directions for capital investments and rational limits of improvement of the products quality. The method is based on main representations of the cascade theory, such as the ideal flow profile and form efficiency as well as mathematical model of the packed column specifying the bonds between its geometric and operating parameters. As a result, the isotopic products cost function could be bound with such parameters as the equilibrium stage height, ultimate packing capacity, its element dimensions, column diameter. It is concluded that the suggested approach to the optimization of isotope separation processes is rather a general one. It permits to solve a number of special problems, such as estimation of advisability of using heat-pump circuits and determining the rational automation level. Besides, by means of the method suggested one can optimize the process conditions with regard to temperature and pressure

  5. Local buckling of composite channel columns

    Science.gov (United States)

    Szymczak, Czesław; Kujawa, Marcin

    2018-05-01

    The investigation concerns local buckling of compressed flanges of axially compressed composite channel columns. Cooperation of the member flange and web is taken into account here. The buckling mode of the member flange is defined by rotation angle a flange about the line of its connection with the web. The channel column under investigation is made of unidirectional fibre-reinforced laminate. Two approaches to member orthotropic material modelling are performed: the homogenization with the aid of theory of mixture and periodicity cell or homogenization upon the Voigt-Reuss hypothesis. The fundamental differential equation of local buckling is derived with the aid of the stationary total potential energy principle. The critical buckling stress corresponding to a number of buckling half-waves is assumed to be a minimum eigenvalue of the equation. Some numerical examples dealing with columns are given here. The analytical results are compared with the finite element stability analysis carried out by means of ABAQUS software. The paper is focused on a close analytical solution of the critical buckling stress and the associated buckling mode while the web-flange cooperation is assumed.

  6. Stress-Strain Relationship of Synthetic Fiber Reinforced Concrete Columns

    Directory of Open Access Journals (Sweden)

    Rosidawani

    2017-01-01

    Full Text Available Many empirical confinement models for normal and high strength concrete have been developed. Nevertheless, reported studies in the term of confinement of fiber reinforced concrete are limited. Whereas, the use of fiber reinforced concrete in structural elements has become the subject of the research and has indicated positive experiences. Since the stress-strain relationship of concrete in compression is required for analysis of structural members, the study of the stress-strain relationship for synthetic fiber reinforced concrete is substantial. The aim of the study is to examine the capabilities of the various models available in the literature to predict the actual experimental behavior of synthetic fiber reinforced high-strength concrete columns. The experimental data used are the results of the circular column specimens with the spiral spacing and the volume fraction of synthetic fiber as the test variables. The axial stress-strain curves from the tests are then compared with the various models of confinement from the literature. The performance index of each model is measured by using the coefficient of variation (COV concept of stress and strain behavior parameter. Among the confinement models, Cusson model shows the closest valid value of the coefficient of variation.

  7. Experimental analysis of reinforced concrete columns strengthened with self-compacting concrete and connectors

    Directory of Open Access Journals (Sweden)

    P. P. Nascimento

    Full Text Available There are many problems involving cases of destruction of buildings and other structures. The columns can deteriorate for several reasons such as the evolution and changing habits of the loads. The experimental phase of this work was based on a test involving nine reinforced concrete columns under combined bending and axial compression, at an initial eccentricity of 60 mm. Two columns were used as reference, one having the original dimensions of the column and the other, monolithic, had been cast along the thickness of the strengthened piece. The remaining columns received a 35 mm thick layer of self-compacting concrete on their compressed face. For the preparation of the interface between the two materials, this surface was scarified and furrowed and connectors were inserted onto the columns' shear reinforcement in various positions and amounts.As connectors, 5 mm diameter steel bars were used (the same as for stirrups, bent in the shape of a "C" with 25 mm coatings. >As a conclusion, not only the quantity, but mainly, the location of the connectors used in the link between substrate and reinforcement is crucial to increase strength and to change failure mode.

  8. Sorption of nitrate onto amine-crosslinked wheat straw: characteristics, column sorption and desorption properties.

    Science.gov (United States)

    Xing, Xu; Gao, Bao-Yu; Zhong, Qian-Qian; Yue, Qin-Yan; Li, Qian

    2011-02-15

    The nitrate removal process was evaluated using a fixed-bed column packed with amine-crosslinked wheat straw (AC-WS). Column sorption and desorption characteristics of nitrate were studied extensively. Solid-state (13)C NMR and zeta potential analysis validated the existence of crosslinked amine groups in AC-WS. Raman shift of the nitrate peaks suggested the electrostatic attraction between the adsorbed ions and positively charged amine sites. The column sorption capacity (q(ed)) of the AC-WS for nitrate was 87.27 mg g(-1) in comparison with the raw WS of 0.57 mg g(-1). Nitrate sorption in column was affected by bed height, influent nitrate concentration, flow rate and pH, and of all these, influent pH demonstrated an essential effect on the performance of the column. In addition, desorption and dynamic elution tests were repeated for several cycles, with high desorption rate and slight losses in its initial column sorption capacity. Copyright © 2010 Elsevier B.V. All rights reserved.

  9. Flow rate dependent extra-column variance from injection in capillary liquid chromatography.

    Science.gov (United States)

    Aggarwal, Pankaj; Liu, Kun; Sharma, Sonika; Lawson, John S; Dennis Tolley, H; Lee, Milton L

    2015-02-06

    Efficiency and resolution in capillary liquid chromatography (LC) can be significantly affected by extra-column band broadening, especially for isocratic separations. This is particularly a concern in evaluating column bed structure using non-retained test compounds. The band broadening due to an injector supplied with a commercially available capillary LC system was characterized from experimental measurements. The extra-column variance from the injection valve was found to have an extra-column contribution independent of the injection volume, showing an exponential dependence on flow rate. The overall extra-column variance from the injection valve was found to vary from 34 to 23 nL. A new mathematical model was derived that explains this exponential contribution of extra-column variance on chromatographic performance. The chromatographic efficiency was compromised by ∼130% for a non-retained analyte because of injection valve dead volume. The measured chromatographic efficiency was greatly improved when a new nano-flow pumping system with integrated injection valve was used. Copyright © 2014 Elsevier B.V. All rights reserved.

  10. Leaching behavior of mineral processing waste: Comparison of batch and column investigations

    Energy Technology Data Exchange (ETDEWEB)

    Al-Abed, Souhail R. [National Risk Management Research Laboratory, U.S. Environmental Protection Agency, 26 West Martin Luther King Drive, Cincinnati, OH 45268 (United States)], E-mail: al-abed.souhail@epa.gov; Jegadeesan, G. [Pegasus Technical Services Inc., 46 East Hollister Street, Cincinnati, OH 45219 (United States); Purandare, J. [Englandgeosystem Inc., 15375 Barranca Pkwy, Suite F-106, Irvine, CA 92618 (United States); Allen, D. [National Risk Management Research Laboratory, U.S. Environmental Protection Agency, 26 West Martin Luther King Drive, Cincinnati, OH 45268 (United States)

    2008-05-30

    In this study, a comparison of laboratory batch and column experiments on metal release profile from a mineral processing waste (MPW) is presented. Batch (equilibrium) and column (dynamic) leaching tests were conducted on ground MPW at different liquid-solid ratios (LS) to determine the mechanisms controlling metal release. Additionally, the effect of pH on metal release is also discussed. It was observed that acidic pH conditions induced dissolution of As, Zn and Cu. Negligible leaching at alkaline pH was observed. However, Se depicted amphoteric behavior with high release at low and high pH. The batch and column data showed that As and Se release increased with LS ratio, while that of Cu and Zn increased initially and tapered towards equilibrium values at high LS ratios. The results on metal release from the MPW suggested that dissolution of the metal was the controlling mechanism. Leaching profiles from the batch and column data corresponded well for most LS ratios. This is most likely due to the acidic character of the waste, minimal changes in pH during the column operation and granular structure of the waste. From a waste management perspective, low cost batch equilibrium studies in lieu of high cost column experiments can be used for decision making on its disposal only when the waste exhibits characteristics similar to the mineral processing waste.

  11. Leaching behavior of mineral processing waste: Comparison of batch and column investigations

    International Nuclear Information System (INIS)

    Al-Abed, Souhail R.; Jegadeesan, G.; Purandare, J.; Allen, D.

    2008-01-01

    In this study, a comparison of laboratory batch and column experiments on metal release profile from a mineral processing waste (MPW) is presented. Batch (equilibrium) and column (dynamic) leaching tests were conducted on ground MPW at different liquid-solid ratios (LS) to determine the mechanisms controlling metal release. Additionally, the effect of pH on metal release is also discussed. It was observed that acidic pH conditions induced dissolution of As, Zn and Cu. Negligible leaching at alkaline pH was observed. However, Se depicted amphoteric behavior with high release at low and high pH. The batch and column data showed that As and Se release increased with LS ratio, while that of Cu and Zn increased initially and tapered towards equilibrium values at high LS ratios. The results on metal release from the MPW suggested that dissolution of the metal was the controlling mechanism. Leaching profiles from the batch and column data corresponded well for most LS ratios. This is most likely due to the acidic character of the waste, minimal changes in pH during the column operation and granular structure of the waste. From a waste management perspective, low cost batch equilibrium studies in lieu of high cost column experiments can be used for decision making on its disposal only when the waste exhibits characteristics similar to the mineral processing waste

  12. Novel design for centrifugal counter-current chromatography: VI. Ellipsoid column.

    Science.gov (United States)

    Gu, Dongyu; Yang, Yi; Xin, Xuelei; Aisa, Haji Akber; Ito, Yoichiro

    2015-01-01

    A novel ellipsoid column was designed for centrifugal counter-current chromatography. Performance of the ellipsoid column with a capacity of 3.4 mL was examined with three different solvent systems composed of 1-butanol-acetic acid-water (4:1:5, v/v) (BAW), hexane-ethyl acetate-methanol-0.1 M HCl (1:1:1:1, v/v) (HEMH), and 12.5% (w/w) PEG1000 and 12.5% (w/w) dibasic potassium phosphate in water (PEG-DPP) each with suitable test samples. In dipeptide separation with BAW system, both stationary phase retention (Sf) and peak resolution (Rs) of the ellipsoid column were much higher at 0° column angle (column axis parallel to the centrifugal force) than at 90° column angle (column axis perpendicular to the centrifugal force), where elution with the lower phase at a low flow rate produced the best separation yielding Rs at 2.02 with 27.8% Sf at a flow rate of 0.07 ml/min. In the DNP-amino acid separation with HEMW system, the best results were obtained at a flow rate of 0.05 ml/min with 31.6% Sf yielding high Rs values at 2.16 between DNP-DL-glu and DNP-β-ala peaks and 1.81 between DNP-β-ala and DNP-L-ala peaks. In protein separation with PEG-DPP system, lysozyme and myolobin were resolved at Rs of 1.08 at a flow rate of 0.03 ml/min with 38.9% Sf. Most of those Rs values exceed those obtained from the figure-8 column under similar experimental conditions previously reported.

  13. Analysis of separation quality of scandium-46 and titanium using silica gel column

    International Nuclear Information System (INIS)

    Muhamad Basit Febrian; Yanuar Setiadi; Duyeh Setiawan; Titin Sri Mulyati; Nana Suherman

    2015-01-01

    In this study, quality test of scandium and titanium mixture separation system using a silica gel column has been conducted. This system will be used in the separation of medical radioisotopes of 47 Sc from TiO 2 enriched targets. 20 mg of TiO 2 and 5 mg of Sc 2 O 3 dissolved using 0.5 mL of 50% HF solvent with gentle heating at 60°C - 80°C for 1 hour then 4.5 mL H 2 O was added. Sc and Ti mixture is separated by passing it through a column of silica gel. In the determination of scandium released from silica gel, Sc-46 radiotracer was used. Only 51.60 ± 4.5% of 5 mg of scandium could be retained in the silica gel column. From 51.60% of absorbed scandium in the column, 98.29 ± 3.4% were eluted with 5 mL of H 2 O eluent. During elution of scandium from silica gel column, 2.81 grams of 20 mg of titanium came apart as breakthrough. In determination of recovery of titanium from silica gel, 51.76 ± 5.5% of the 20 mg Ti can be recovered from silica gel column using 5M HCl eluent, whereas remaining Ti were eluted using 40 ml of HCl 5M. Based on those result, it can be concluded that there are still titanium portion in scandium after the separation using a silica gel column. Further purification step using fresh silica gel column, can separate escaped titanium from scandium. (author)

  14. Performance of lap splices in large-scale column specimens affected by ASR and/or DEF-extension phase.

    Science.gov (United States)

    2015-03-01

    A large experimental program, consisting of the design, construction, curing, exposure, and structural load : testing of 16 large-scale column specimens with a critical lap splice region that were influenced by varying : stages of alkali-silica react...

  15. Adiabatic packed column supercritical fluid chromatography using a dual-zone still-air column heater.

    Science.gov (United States)

    Helmueller, Shawn C; Poe, Donald P; Kaczmarski, Krzysztof

    2018-02-02

    An approach to conducting SFC separations under pseudo-adiabatic condition utilizing a dual-zone column heater is described. The heater allows for efficient separations at low pressures above the critical temperature by imposing a temperature profile along the column wall that closely matches that for isenthalpic expansion of the fluid inside the column. As a result, the efficiency loss associated with the formation of radial temperature gradients in this difficult region can be largely avoided in packed analytical scale columns. For elution of n-octadecylbenzene at 60 °C with 5% methanol modifier and a flow rate of 3 mL/min, a 250 × 4.6-mm column packed with 5-micron Kinetex C18 particles began to lose efficiency (8% decrease in the number of theoretical plates) at outlet pressures below 142 bar in a traditional forced air oven. The corresponding outlet pressure for onset of excess efficiency loss was decreased to 121 bar when the column was operated in a commercial HPLC column heater, and to 104 bar in the new dual-zone heater operated in adiabatic mode, with corresponding increases in the retention factor for n-octadecylbenzene from 2.9 to 6.8 and 14, respectively. This approach allows for increased retention and efficient separations of otherwise weakly retained analytes. Applications are described for rapid SFC separation of an alkylbenzene mixture using a pressure ramp, and isobaric separation of a cannabinoid mixture. Copyright © 2018 Elsevier B.V. All rights reserved.

  16. Ductility of reinforced concrete columns confined with stapled strips

    International Nuclear Information System (INIS)

    Tahir, M.F.; Khan, Q.U.Z.; Shabbir, F.; Sharif, M.B.; Ijaz, N.

    2015-01-01

    Response of three 150x150x450mm short reinforced concrete (RC) columns confined with different types of confining steel was investigated. Standard stirrups, strips and stapled strips, each having same cross-sectional area, were employed as confining steel around four comer column bars. Experimental work was aimed at probing into the affect of stapled strip confinement on post elastic behavior and ductility level under cyclic axial load. Ductility ratios, strength enhancement factor and core concrete strengths were compared to study the affect of confinement. Results indicate that strength enhancement in RC columns due to strip and stapled strip confinement was not remarkable as compared to stirrup confined column. It was found that as compared to stirrup confined column, stapled strip confinement enhanced the ductility of RC column by 183% and observed axial capacity of stapled strip confined columns was 41 % higher than the strip confined columns. (author)

  17. EX0904 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX0904: Water Column Exploration Field...

  18. Assessment on Ultimate Load of Cold-formed Steel Channel (CFSC Stub Column

    Directory of Open Access Journals (Sweden)

    Mohd Sani Mohd Syahrul Hisyam

    2015-01-01

    Full Text Available Cold-formed steel is used as the non-structural and structural material in civil engineering work and building. Cold-formed steel channel is selected and cut into 100 mm, 200 mm, 300 mm, 400 mm and 500 mm. The slenderness ratio is calculated and noted as a stub or short column because below 40. The column is tested by using Universal Testing Machine to determine the ultimate load of the stub column. Besides, the CFSC is determined the material properties of CFSC for checking it’s the originality of steel based material. The experimental data are tested and compared with the Direct Strength Method (DSM. It showed that the CFSC1 with a height of 100 mm is reported to have a higher value of ultimate load when compared with other samples. When the height of the stub column increased, the ultimate load of the sample is decreased. Then, the CFSC1 also showed a higher in initial stiffness when compared with other samples. All samples are shown having a higher data in ultimate load when compared with the Direct Strength Method prediction. The ultimate load of experimental and DSM all gave a ratio below 1.03. Finally, all samples can further recommend determining the relation between the ultimate loads with variations of height of the column.

  19. Consolidated Fuel Reprocessing Program. Operating experience with pulsed-column holdup estimators

    International Nuclear Information System (INIS)

    Ehinger, M.H.

    1986-01-01

    Methods for estimating pulsed-column holdup are being investigated as part of the Safeguards Assessment task of the Consolidated Fuel Reprocessing Program (CFRP) at the Oak Ridge National Laboratory. The CFRP was a major sponsor of test runs at the Barnwell Nuclear Fuel plant (BNFP) in 1980 and 1981. During these tests, considerable measurement data were collected for pulsed columns in the plutonium purification portion of the plant. These data have been used to evaluate and compare three available methods of holdup estimation

  20. The prediction of concentration profiles for a NIMCIX column absorbing uranium from aqueous solution

    International Nuclear Information System (INIS)

    Wright, R.S.

    1979-01-01

    A procedure is proposed for the prediction of concentration profiles for a countercurrent ion-exchange absorption column, use being made of equilibrium and kinetic data derived from small-scale batch tests. A comparison is presented between the predictions and the measured performance of a column (2,5 m in diameter) absorbing uranium from solution. The method is shown to be adequate for design purposes provided that the data used are from tests in which the solution and resin conditions approximate those for which the plant is being designed [af

  1. Cross flow cyclonic flotation column for coal and minerals beneficiation

    Science.gov (United States)

    Lai, Ralph W.; Patton, Robert A.

    2000-01-01

    An apparatus and process for the separation of coal from pyritic impurities using a modified froth flotation system. The froth flotation column incorporates a helical track about the inner wall of the column in a region intermediate between the top and base of the column. A standard impeller located about the central axis of the column is used to generate a centrifugal force thereby increasing the separation efficiency of coal from the pyritic particles and hydrophillic tailings.

  2. Modalization in the Political Column of Tempo Magazine

    OpenAIRE

    Rahmah, Maria Betti Sinaga and

    2017-01-01

    The study focuses on analyzing the use of modalization in the Political Column of Tempo Magazine. The objectives were to find out the type of modalization and to describe the use of modalization in the Political Column of Tempo magazine. The data were taken from Political Column of Tempo magazine published in June and July 2017. The source of data was Political Column in Tempo magazine. The data analysis applied descriptive qualitative research. There were 135 clauses which contained Modaliza...

  3. Numerical Simulations of Settlement of Jet Grouting Columns

    Directory of Open Access Journals (Sweden)

    Juzwa Anna

    2016-03-01

    Full Text Available The paper presents the comparison of results of numerical analyses of interaction between group of jet grouting columns and subsoil. The analyses were conducted for single column and groups of three, seven and nine columns. The simulations are based on experimental research in real scale which were carried out by authors. The final goal for the research is an estimation of an influence of interaction between columns working in a group.

  4. column frame for design of reinforced concrete sway frames

    African Journals Online (AJOL)

    adminstrator

    design of slender reinforced concrete columns in sway frames according .... concrete,. Ac = gross cross-sectional area of the columns. Step 3: Effective Buckling Length Factors. The effective buckling length factors of columns in a sway frame shall be computed by .... shall have adequate resistance to failure in a sway mode ...

  5. 46 CFR 174.085 - Flooding on column stabilized units.

    Science.gov (United States)

    2010-10-01

    ... 46 Shipping 7 2010-10-01 2010-10-01 false Flooding on column stabilized units. 174.085 Section 174... Units § 174.085 Flooding on column stabilized units. (a) Watertight compartments that are outboard of... of the unit, must be assumed to be subject to flooding as follows: (1) When a column is subdivided...

  6. Water hammer with column separation : a historical review

    NARCIS (Netherlands)

    Bergant, A.; Simpson, A.R.; Tijsseling, A.S.

    2006-01-01

    Column separation refers to the breaking of liquid columns in fully filled pipelines. This may occur in a water-hammer event when the pressure in a pipeline drops to the vapor pressure at specific locations such as closed ends, high points or knees (changes in pipe slope). The liquid columns are

  7. Multi-Column Xe/Kr Separation with AgZ-PAN and HZ-PAN

    Energy Technology Data Exchange (ETDEWEB)

    Greenhalgh, Mitchell Randy [Idaho National Lab. (INL), Idaho Falls, ID (United States); Garn, Troy Gerry [Idaho National Lab. (INL), Idaho Falls, ID (United States); Welty, Amy Keil [Idaho National Lab. (INL), Idaho Falls, ID (United States); Watson, Tony Leroy [Idaho National Lab. (INL), Idaho Falls, ID (United States)

    2016-08-01

    Previous multi-column xenon/krypton separation tests have demonstrated the capability of separating xenon from krypton in a mixed gas feed stream. The results of this initial testing with AgZ-PAN and HZ-PAN indicated that an excellent separation of xenon from krypton could be achieved. Building upon these initial results, a series of additional multi-column testing were performed in FY-16. The purpose of this testing was to scale up the sorbent beds, test a different composition of feed gas and attempt to improve the accuracy of the analysis of the individual capture columns’ compositions. Two Stirling coolers were installed in series to perform this testing. The use of the coolers instead of the cryostat provided two desired improvements, 1) removal of the large dilution due to the internal volume of the cryostat adsorption chamber, and 2) ability to increase the sorbent bed size for scale-up. The AgZ-PAN sorbent, due to its xenon selectivity, was loaded in the first column to capture the xenon while allowing the krypton to flow through and be routed to a second column containing the HZ-PAN for capture and analysis. The gases captured on both columns were sampled with evacuated sample bombs and subsequently analyzed via GC-MS for both krypton and xenon. The results of these tests can be used to develop the scope of future testing and analysis using this test bed for demonstrating the capture and separation of xenon and krypton using sorbents, for demonstrating desorption and regeneration of the sorbents, and for determining compositions of the desorbed gases. They indicate a need for future desorption studies in order to better quantify co-adsorbed species and final krypton purity.

  8. Determination of solute organic concentration in contaminated soils using a chemical-equilibrium soil column system

    DEFF Research Database (Denmark)

    Gamst, Jesper; Kjeldsen, Peter; Christensen, Thomas Højlund

    2007-01-01

    using two soils with different content of organic carbon (f(oc) of 1.5 and 6.5%, respectively). A quadruple blind test of the ER-V system using glass beads in stead of soil showed an acceptable recovery (65-85%) of all of the 11 VOCs tested. Only for the most volatile compound (heptane, K-H similar...... to 80) an unacceptable recovery was found (9%). The contact time needed for obtaining chemical equilibrium was tested in the ER-H system by performing five test with different duration (1, 2, 4, 7 and 19 days) using the low organic carbon soil. Seven days of contact time appeared sufficient...... for determination of solute concentration in a contaminated soil were developed; (1) a chemical Equilibrium and Recirculation column test for Volatile organic chemicals (ER-V) and (2) a chemical Equilibrium and Recirculation column test for Hydrophobic organic chemicals (ER-H). The two test systems were evaluated...

  9. Flotation in column applied to fines of the Itataia phosphoro-uraniferous ore, CE, Brazil

    International Nuclear Information System (INIS)

    Furtado, J.R.V.; Peres, A.E.C.

    1985-01-01

    An adequate process to treat the fine fraction was developed in the present investigation, after size and chemical characterization of the fines,. Emphasis was placed on construction, assembling and operation of a 5.2 cm diameter and 6.0 m high continuos flotation column. The column was fed with the pilot plant desliming cyclone overflow, below 10 m. Tests were also carried out with the underflow of the same cyclone and with the very fine underflow of a 20 mm cyclone. The column presented a better performance than a rougher laboratory mechanical cell when tested with the underflow of 20 mm cyclone. Concentrates with 24.5% P 2 O 5 , with recovery levels above 60% were achieved from feed grades of 10.3%P 2 O 5 , it is worth mentioning that the rougher flotation reagents scheme is not effective to deppress carbonatic gangue irrespective of the size range. (Author) [pt

  10. Two-dimensional liquid chromatography consisting of twelve second-dimension columns for comprehensive analysis of intact proteins.

    Science.gov (United States)

    Ren, Jiangtao; Beckner, Matthew A; Lynch, Kyle B; Chen, Huang; Zhu, Zaifang; Yang, Yu; Chen, Apeng; Qiao, Zhenzhen; Liu, Shaorong; Lu, Joann J

    2018-05-15

    A comprehensive two-dimensional liquid chromatography (LCxLC) system consisting of twelve columns in the second dimension was developed for comprehensive analysis of intact proteins in complex biological samples. The system consisted of an ion-exchange column in the first dimension and the twelve reverse-phase columns in the second dimension; all thirteen columns were monolithic and prepared inside 250 µm i.d. capillaries. These columns were assembled together through the use of three valves and an innovative configuration. The effluent from the first dimension was continuously fractionated and sequentially transferred into the twelve second-dimension columns, while the second-dimension separations were carried out in a series of batches (six columns per batch). This LCxLC system was tested first using standard proteins followed by real-world samples from E. coli. Baseline separation was observed for eleven standard proteins and hundreds of peaks were observed for the real-world sample analysis. Two-dimensional liquid chromatography, often considered as an effective tool for mapping proteins, is seen as laborious and time-consuming when configured offline. Our online LCxLC system with increased second-dimension columns promises to provide a solution to overcome these hindrances. Copyright © 2018 Elsevier B.V. All rights reserved.

  11. Production and characterisation of glycolipid biosurfactant by Halomonas sp. MB-30 for potential application in enhanced oil recovery.

    Science.gov (United States)

    Dhasayan, Asha; Kiran, G Seghal; Selvin, Joseph

    2014-12-01

    Biosurfactant-producing Halomonas sp. MB-30 was isolated from a marine sponge Callyspongia diffusa, and its potency in crude oil recovery from sand pack column was investigated. The biosurfactant produced by the strain MB-30 reduced the surface tension to 30 mN m(-1) in both glucose and hydrocarbon-supplemented minimal media. The critical micelle concentration of biosurfactant obtained from glucose-based medium was at 0.25 mg ml(-1) at critical micelle dilution 1:10. The chemical structure of glycolipid biosurfactant was characterised by infrared spectroscopy and proton magnetic resonance spectroscopy. The emulsification activity of MB-30 biosurfactant was tested with different hydrocarbons, and 93.1 % emulsification activity was exhibited with crude oil followed by kerosene (86.6 %). The formed emulsion was stable for up to 1 month. To identify the effectiveness of biosurfactant for enhanced oil recovery in extreme environments, the interactive effect of pH, temperature and salinity on emulsion stability with crude oil and kerosene was evaluated. The stable emulsion was formed at and above pH 7, temperature >80 °C and NaCl concentration up to 10 % in response surface central composite orthogonal design model. The partially purified biosurfactant recovered 62 % of residual crude oil from sand pack column. Thus, the stable emulsifying biosurfactant produced by Halomonas sp. MB-30 could be used for in situ biosurfactant-mediated enhanced oil recovery process and hydrocarbon bioremediation in extreme environments.

  12. Experimental evaluation of the prevention methods for the interface between masonry infill walls and concrete columns

    Directory of Open Access Journals (Sweden)

    A. P. Tramontin

    Full Text Available Cracks that form at the interfaces between masonry structures are common uncontrolled occurrences in buildings. Numerous methods have been proposed by the construction industry to address this problem. Cracks continuously form in the joints between concrete columns and masonry infill walls. In this study, the most common methods for preventing these types of cracks were evaluated in laboratory experiments. Column masonry models were constructed using different types of joints between concrete columns and masonry infill walls, such as steel bars and steel mesh. The efficiency of each type of joint method was evaluated by performing direct tensile tests (pullout tests on the models and monitoring the evolution of the crack opening in the joint between the column and wall, as a function of load applied to the model. The results from this study indicate that the model composed of "electrowelded wire mesh without steel angles" is the best model for controlling cracking in the joints between concrete columns and masonry infill walls.

  13. Design of Steel Beam-Column Connections

    Directory of Open Access Journals (Sweden)

    Bogatinoski Z.

    2014-05-01

    Full Text Available In this paper a theoretical and experimental research of the steel beam-column connections is presented. Eight types of specimens were being researched, composed of rigid and semi-rigid connections from which 4 connections are with IPE - profile and 4 connections with tube's section for the beam. From the numerical analysis of the researched models, and especially from the experimental research at the Laboratory for Structures in the Faculty of Mechanical Engineering - Skopje, specific conclusions were received that ought to have theoretical and practical usage for researchers in this area of interest.

  14. Buckling driven debonding in sandwich columns

    DEFF Research Database (Denmark)

    Østergaard, Rasmus Christian

    2008-01-01

    results from two mechanisms: (a) interaction of local debond buckling and global buckling and (b) the development of a damaged zone at the debond crack tip. Based on the pronounced imperfection sensitivity, the author predicts that an experimental measurement of the strength of sandwich structures may......A compression loaded sandwich column that contains a debond is analyzed using a geometrically non-linear finite element model. The model includes a cohesive zone along one face sheet/core interface whereby the debond can extend by interface crack growth. Two geometrical imperfections are introduced...

  15. Dynamic Deformation and Collapse of Granular Columns

    Science.gov (United States)

    Uenishi, K.; Tsuji, K.; Doi, S.

    2009-12-01

    Large dynamic deformation of granular materials may be found in nature not only in the failure of slopes and cliffs — due to earthquakes, rock avalanches, debris flows and landslides — but also in earthquake faulting itself. Granular surface flows often consist of solid grains and intergranular fluid, but the effect of the fluid may be usually negligible because the volumetric concentration of grains is in many cases high enough for interparticle forces to dominate momentum transport. Therefore, the investigation of dry granular flow of a mass might assist in further understanding of the above mentioned geophysical events. Here, utilizing a high-speed digital video camera system, we perform a simple yet fully-controlled series of laboratory experiments related to the collapse of granular columns. We record, at an interval of some microseconds, the dynamic transient granular mass flow initiated by abrupt release of a tube that contains dry granular materials. The acrylic tube is partially filled with glass beads and has a cross-section of either a fully- or semi-cylindrical shape. Upon sudden removal of the tube, the granular solid may fragment under the action of its own weight and the particles spread on a rigid horizontal plane. This study is essentially the extension of the previous ones by Lajeunesse et al. (Phys. Fluids 2004) and Uenishi and Tsuji (JPGU 2008), but the striped layers of particles in a semi-cylindrical tube, newly introduced in this contribution, allow us to observe the precise particle movement inside the granular column: The development of slip lines inside the column and the movement of particles against each other can be clearly identified. The major controlling parameters of the spreading dynamics are the initial aspect ratio of the granular (semi-)cylindrical column, the frictional properties of the horizontal plane (substrate) and the size of beads. We show the influence of each parameter on the average flow velocity and final radius

  16. A review of oscillating water columns.

    Science.gov (United States)

    Heath, T V

    2012-01-28

    This paper considers the history of oscillating water column (OWC) systems from whistling buoys to grid-connected power generation systems. The power conversion from the wave resource through to electricity via pneumatic and shaft power is discussed in general terms and with specific reference to Voith Hydro Wavegen's land installed marine energy transformer (LIMPET) plant on the Scottish island of Islay and OWC breakwater systems. A report on the progress of other OWC systems and power take-off units under commercial development is given, and the particular challenges faced by OWC developers reviewed.

  17. Preinjector for Linac 1, accelerating column

    CERN Multimedia

    1974-01-01

    For a description of the Linac 1 preinjector, please see first 7403070X. High up on the wall of the Faraday cage (7403073X) is this drum-shaped container of the ion source (7403083X). It is mounted at the HV end of the accelerating column through which the ions (usually protons; many other types of ions in the course of its long history) proceed through the Faraday cage wall to the low-energy end (at ground potential) of Linac 1. The 520 kV accelerating voltage was supplied by a SAMES generator (7403074X).

  18. PHOTOGRAMMETRIC APPROACH IN DETERMINING BEAM-COLUMN CONNECTION DEFORMATIONS

    Directory of Open Access Journals (Sweden)

    Ali Koken

    Full Text Available In accordance with the advances in technology, displacement calculation techniques are ever developing. Photogrammetry has become preferable in some new disciplines with the advances in the image processing methods. In this study, the authors have used two different measurement techniques to determine the angles of rotation in beam-column connections that are subjected to reversible cyclic loading. The first of these is the method that is widely used, the conventional method in structural mechanics experiments, where Linear Variable Differential Transformers (LVDTs are utilized; and the second is the photogrammetric measurement technique. The rotation angles were determined using these techniques in a total of ten steel beam-column connection experiments. After discussing the test procedures of the aforementioned methods, the results were presented. It was observed that the rotation angles measured by each method were very close to each other. It was concluded that the photogrammetric measurement technique could be used as an alternative to conventional methods, where electronic LVDTs are used.

  19. Hydrodynamics of Bubble Columns: Turbulence and Population Balance Model

    Directory of Open Access Journals (Sweden)

    Camila Braga Vieira

    2018-03-01

    Full Text Available This paper presents an in-depth numerical analysis on the hydrodynamics of a bubble column. As in previous works on the subject, the focus here is on three important parameters characterizing the flow: interfacial forces, turbulence and inlet superficial Gas Velocity (UG. The bubble size distribution is taken into account by the use of the Quadrature Method of Moments (QMOM model in a two-phase Euler-Euler approach using the open-source Computational Fluid Dynamics (CFD code OpenFOAM (Open Field Operation and Manipulation. The interfacial forces accounted for in all the simulations presented here are drag, lift and virtual mass. For the turbulence analysis in the water phase, three versions of the Reynolds Averaged Navier-Stokes (RANS k-ε turbulence model are examined: namely, the standard, modified and mixture variants. The lift force proves to be of major importance for a trustworthy prediction of the gas volume fraction profiles for all the (superficial gas velocities tested. Concerning the turbulence, the mixture k-ε model is seen to provide higher values of the turbulent kinetic energy dissipation rate in comparison to the other models, and this clearly affects the prediction of the gas volume fraction in the bulk region, and the bubble-size distribution. In general, the modified k-ε model proves to be a good compromise between modeling simplicity and accuracy in the study of bubble columns of the kind undertaken here.

  20. Investigation of in-plane moment connections of I-beams to square concrete-filled steel tube columns under gravity loads

    Directory of Open Access Journals (Sweden)

    Abdelrahim K. Dessouki

    2015-04-01

    Full Text Available This paper focuses on experimental and analytical behavior of the ultimate moment of the connections of steel I-beams to square concrete-filled steel tube columns. External stiffeners around the columns are used at the beam flange levels. Five specimens are tested monotonically. The test parameters are the column stiffener dimensions and filling the steel tube column with concrete. Two types of failure modes are observed; beam flange failure and stiffener failure. The experimental results show that the ultimate moment of the connection is increased by increasing stiffener’s dimensions and filling the steel tube column with concrete. ANSYS finite element program is used to simulate the behavior, taking into account both geometric and material nonlinearities. Analytical results that are in fair agreement with the experimental ones are then used to discuss the influence of the main geometric parameters on the connection behavior. The parameters are the stiffener and column dimensions as well as filling the steel tube column with concrete. Different square column cross sections are chosen to cover the three classes of section classifications according to Egyptian code of practice, which are: compact, non compact or slender. The increase in the ultimate moment of the connections is based upon both column cross sections’ compactness and stiffener dimensions while the maximum advantages occur with slender columns.

  1. Spinal column damage from water ski jumping

    International Nuclear Information System (INIS)

    Horne, J.; Cockshott, W.P.; Shannon, H.S.

    1987-01-01

    We conducted a radiographic survey of 117 competitive water ski jumpers to determine whether this sport can cause spinal column damage and, if so, whether damage is more likely to occur in those who participate during the period of spinal growth and development (age 15 years or younger). We found a high prevalence of two types of abnormality: Scheuermann (adolescent) spondylodystrophy (present in 26% of the skiers) and vertebral body wedging (present in 34%). The prevalence of adolescent spondylodystrophy increased with the number of years of participation in the sport before age 15 years or less. Of those in this age group who had skied for 5 years or more, 57 showed adolescent spondylodystrophy; of those in the same age group who had skied for 9 years or more, 100% were affected. Wedged vertebrae increased as time of participation increased, regardless of the age at which exposure began. We conclude that competitive water ski jumping may damage the spinal column and that consideration should be given to regulating this sport, particularly for children. (orig.)

  2. Spinal column damage from water ski jumping.

    Science.gov (United States)

    Horne, J; Cockshott, W P; Shannon, H S

    1987-01-01

    We conducted a radiographic survey of 117 competitive water ski jumpers to determine whether this sport can cause spinal column damage and, if so, whether damage is more likely to occur in those who participate during the period of spinal growth and development (age 15 years or younger). We found a high prevalence of two types of abnormality: Scheuermann (adolescent) spondylodystrophy (present in 26% of the skiers) and vertebral body wedging (present in 34%). The prevalence of adolescent spondylodystrophy increased with the number of years of participation in the sport before age 15 years or less. Of those in this age group who had skied for 5 years or more, 57 showed adolescent spondylodystrophy; of those in the same age group who had skied for 9 years or more, 100% were affected. Wedged vertebrae increased as time of participation increased, regardless of the age at which exposure began. We conclude that competitive water ski jumping may damage the spinal column and that consideration should be given to regulating this sport, particularly for children.

  3. Picobubble column flotation of fine coal

    Energy Technology Data Exchange (ETDEWEB)

    Daniel Tao; Samuel Yu; Xiaohua Zhou; R.Q. Honaker; B.K. Parekh [University of Kentucky, Lexington, KY (United States). Department of Mining Engineering

    2008-01-15

    Froth flotation is widely used in the coal industry to clean -28 mesh (0.6 mm) or -100 mesh (0.15 mm) fine coal. A successful recovery of particles by flotation depends on efficient particle-bubble collision and attachment with minimal subsequent particle detachment from bubble. Flotation is effective in a narrow size range, nominally 10-100 {mu}m, beyond which the flotation efficiency drops sharply. A fundamental analysis has shown that use of picobubbles can significantly improve the flotation recovery of particles by increasing the probability of collision and attachment and reducing the probability of detachment. A specially designed column with a picobubble generator has been developed for enhanced recovery of fine coal particles. Picobubbles were produced based on the hydrodynamic cavitation principle. Experimental results have shown that the use of picobubbles in a 5-cm diameter column flotation increased the combustible recovery of a highly floatable coal by up to 10% and that of a poorly floatable coal by up to 40%, depending on the feed rate, collector dosage, and other flotation conditions. 14 refs.

  4. Spinal column damage from water ski jumping

    Energy Technology Data Exchange (ETDEWEB)

    Horne, J.; Cockshott, W.P.; Shannon, H.S.

    1987-11-01

    We conducted a radiographic survey of 117 competitive water ski jumpers to determine whether this sport can cause spinal column damage and, if so, whether damage is more likely to occur in those who participate during the period of spinal growth and development (age 15 years or younger). We found a high prevalence of two types of abnormality: Scheuermann (adolescent) spondylodystrophy (present in 26% of the skiers) and vertebral body wedging (present in 34%). The prevalence of adolescent spondylodystrophy increased with the number of years of participation in the sport before age 15 years or less. Of those in this age group who had skied for 5 years or more, 57 showed adolescent spondylodystrophy; of those in the same age group who had skied for 9 years or more, 100% were affected. Wedged vertebrae increased as time of participation increased, regardless of the age at which exposure began. We conclude that competitive water ski jumping may damage the spinal column and that consideration should be given to regulating this sport, particularly for children. (orig.)

  5. Hydrogen isotope exchange in metal hydride columns

    International Nuclear Information System (INIS)

    Wiswall, R.; Reilly, J.; Bloch, F.; Wirsing, E.

    1977-01-01

    Several metal hydrides were shown to act as chromatographic media for hydrogen isotopes. The procedure was to equilibrate a column of hydride with flowing hydrogen, inject a small quantity of tritium tracer, and observe its elution behavior. Characteristic retention times were found. From these and the extent of widening of the tritium band, the heights equivalent to a theoretical plate could be calculated. Values of around 1 cm were obtained. The following are the metals whose hydrides were studied, together with the temperature ranges in which chromatographic behavior was observed: vanadium, 0 to 70 0 C; zirconium, 500 to 600 0 C; LaNi 5 , -78 to +30 0 C; Mg 2 Ni, 300 to 375 0 C; palladium, 0 to 70 0 C. A dual-temperature isotope separation process based on hydride chromatography was demonstrated. In this, a column was caused to cycle between two temperatures while being supplied with a constant stream of tritium-traced hydrogen. Each half-cycle was continued until ''breakthrough,'' i.e., until the tritium concentration in the effluent was the same as that in the feed. Up to that point, the effluent was enriched or depleted in tritium, by up to 20%

  6. Improved focusing-and-deflection columns

    International Nuclear Information System (INIS)

    Mui, P.H.; Szilagyi, M.

    1995-01-01

    Our earlier design procedures for constructing quadrupole columns are further expanded to include octupole corrector units and ''octupole'' deflectors with no third-order harmonics. The additional complications are finer partitioning of the plates and increased number of voltage controllers. Two sample designs, one having only the additional octupole deflectors and one having both the deflectors and the correctors, are presented and compared to our previous quadrupole system. The additional octupole components are shown to be capable of increasing the current density from 30% to more than 300% for a four-plate system, designed to focus and scan the electron beam over a circular area of 0.25 mm radius. The electron beam is assumed to have an initial divergence of ±2.3 mrad, an initial energy of 6 kV, a total energy spread of 1 eV, and a final acceleration of 30 keV. These systems are then slightly reoptimized for a superficial comparison with the commercially available column by Micrion Corporation. The numerical results indicate a potential for substantial improvements, demonstrating the power of this design procedure. Finally, a discussion is presented on how the individual components can interact with each other to reduce the various aberrations. copyright 1995 American Vacuum Society

  7. Synthesis of focusing-and-deflection columns

    International Nuclear Information System (INIS)

    Szilagyi, M.; Mui, P.H.

    1995-01-01

    Szilagyi and Szep have demonstrated that focusing lenses of high performances can be constructed from a column of circular plate electrodes. Later, Szilagyi modified that system to include dipole, quadrupole, and octupole components by partitioning each plate into eight equal sectors. It has already been shown that the additional quadrupole components can indeed bring about substantial improvements in the focusing of charged particle beams. In this article, that design procedure is expanded to construct columns capable of both focusing and deflecting particle beams by just introducing additional dipole components. In this new design, the geometry of the system remains unchanged. The only extra complication is the demand for more individual controls of the sector voltages. Two sample designs, one for negative ions and one for electrons, are presented showing that in both cases a ±2.3 mrad diverging beam can be focused down to a spot of less than 50 nm in radius over a scanning circular area of radius 0.25 mm. The details of the two systems are given in Sec. IV along with the source conditions. The performance of the negative ion system is found to be comparable to the published data. For the relativistic electron system, the interaction of individual components to reduce various aberrations is investigated. copyright 1995 American Vacuum Society

  8. In situ quantitative characterisation of the ocean water column using acoustic multibeam backscatter data

    Science.gov (United States)

    Lamarche, G.; Le Gonidec, Y.; Lucieer, V.; Lurton, X.; Greinert, J.; Dupré, S.; Nau, A.; Heffron, E.; Roche, M.; Ladroit, Y.; Urban, P.

    2017-12-01

    Detecting liquid, solid or gaseous features in the ocean is generating considerable interest in the geoscience community, because of their potentially high economic values (oil & gas, mining), their significance for environmental management (oil/gas leakage, biodiversity mapping, greenhouse gas monitoring) as well as their potential cultural and traditional values (food, freshwater). Enhancing people's capability to quantify and manage the natural capital present in the ocean water goes hand in hand with the development of marine acoustic technology, as marine echosounders provide the most reliable and technologically advanced means to develop quantitative studies of water column backscatter data. This is not developed to its full capability because (i) of the complexity of the physics involved in relation to the constantly changing marine environment, and (ii) the rapid technological evolution of high resolution multibeam echosounder (MBES) water-column imaging systems. The Water Column Imaging Working Group is working on a series of multibeam echosounder (MBES) water column datasets acquired in a variety of environments, using a range of frequencies, and imaging a number of water-column features such as gas seeps, oil leaks, suspended particulate matter, vegetation and freshwater springs. Access to data from different acoustic frequencies and ocean dynamics enables us to discuss and test multifrequency approaches which is the most promising means to develop a quantitative analysis of the physical properties of acoustic scatterers, providing rigorous cross calibration of the acoustic devices. In addition, high redundancy of multibeam data, such as is available for some datasets, will allow us to develop data processing techniques, leading to quantitative estimates of water column gas seeps. Each of the datasets has supporting ground-truthing data (underwater videos and photos, physical oceanography measurements) which provide information on the origin and

  9. Performance of soft clay stabilized with sand columns treated by silica fume

    Directory of Open Access Journals (Sweden)

    Samueel Zeena

    2018-01-01

    Full Text Available In many road construction projects, if weak soil exists, then uncontrollable settlement and critical load carrying capacity are major difficult problems to the safety and serviceability of roads in these areas. Thus ground improvement is essential to achieve the required level of performance. The paper presents results of the tests of four categories. First category was performed on saturated soft bed of clay without any treatment, the second category shed light on the improvement achieved in loading carrying capacity and settlement as a result of reinforcing with conventional sand columns at area replacement ratio = 0.196. The third set investigates the bed reinforced by sand columns stabilized with dry silica fume at different percentages (3, 5 and 7% and the fourth set investigates the behavior of sand columns treated with slurry silica fume at two percentages (10 and 12%. All sand columns models were constructed at (R.D= 60%. Model tests were performed on bed of saturated soil prepared at undrained shear strength between 16-20 kPa for all models. For all cases, the model test was loaded gradually by stress increments up to failure. Stress deformation measurements are recorded and analyzed in terms of bearing improvement ratio and settlement reduction ratio. Optimum results were indicated from soil treated with sand columns stabilized with 7% dry silica fume at medium state reflecting the highest bearing improvement ratio (3.04 and the settlement reduction ratio (0.09 after 7 days curing. While soil treated with sand columns stabilized with 10% slurry silica fume provided higher bearing improvement ratio 3.13 with lower settlement reduction ratio of 0.57 after 7-days curing.

  10. The effects of carbide column to swelling potential and Atterberg limit on expansive soil with column to soil drainage

    Science.gov (United States)

    Muamar Rifa'i, Alfian; Setiawan, Bambang; Djarwanti, Noegroho

    2017-12-01

    The expansive soil is soil that has a potential for swelling-shrinking due to changes in water content. Such behavior can exert enough force on building above to cause damage. The use of columns filled with additives such as Calcium Carbide is done to reduce the negative impact of expansive soil behavior. This study aims to determine the effect of carbide columns on expansive soil. Observations were made on swelling and spreading of carbides in the soil. 7 Carbide columns with 5 cm diameter and 20 cm height were installed into the soil with an inter-column spacing of 8.75 cm. Wetting is done through a pipe at the center of the carbide column for 20 days. Observations were conducted on expansive soil without carbide columns and expansive soil with carbide columns. The results showed that the addition of carbide column could reduce the percentage of swelling by 4.42%. Wetting through the center of the carbide column can help spread the carbide into the soil. The use of carbide columns can also decrease the rate of soil expansivity. After the addition of carbide column, the plasticity index value decreased from 71.76% to 4.3% and the shrinkage index decreased from 95.72% to 9.2%.

  11. Heat Transfer Analysis for a Fixed CST Column

    International Nuclear Information System (INIS)

    Lee, S.Y.

    2004-01-01

    In support of a small column ion exchange (SCIX) process for the Savannah River Site waste processing program, a transient two-dimensional heat transfer model that includes the conduction process neglecting the convection cooling mechanism inside the crystalline silicotitanate (CST) column has been constructed and heat transfer calculations made for the present design configurations. For this situation, a no process flow condition through the column was assumed as one of the reference conditions for the simulation of a loss-of-flow accident. A series of the modeling calculations has been performed using a computational heat transfer approach. Results for the baseline model indicate that transit times to reach 130 degrees Celsius maximum temperature of the CST-salt solution column are about 96 hours when the 20-in CST column with 300 Ci/liter heat generation source and 25 degrees Celsius initial column temperature is cooled by natural convection of external air as a primary heat transfer mechanism. The modeling results for the 28-in column equipped with water jacket systems on the external wall surface of the column and water coolant pipe at the center of the CST column demonstrate that the column loaded with 300 Ci/liter heat source can be maintained non-boiling indefinitely. Sensitivity calculations for several alternate column sizes, heat loads of the packed column, engineered cooling systems, and various ambient conditions at the exterior wall of the column have been performed under the reference conditions of the CST-salt solution to assess the impact of those parameters on the peak temperatures of the packed column for a given transient time. The results indicate that a water-coolant pipe at the center of the CST column filled with salt solution is the most effective one among the potential design parameters related to the thermal energy dissipation of decay heat load. It is noted that the cooling mechanism at the wall boundary of the column has significant

  12. Investigating the Effect of Column Geometry on Separation Efficiency using 3D Printed Liquid Chromatographic Columns Containing Polymer Monolithic Phases.

    Science.gov (United States)

    Gupta, Vipul; Beirne, Stephen; Nesterenko, Pavel N; Paull, Brett

    2018-01-16

    Effect of column geometry on the liquid chromatographic separations using 3D printed liquid chromatographic columns with in-column polymerized monoliths has been studied. Three different liquid chromatographic columns were designed and 3D printed in titanium as 2D serpentine, 3D spiral, and 3D serpentine columns, of equal length and i.d. Successful in-column thermal polymerization of mechanically stable poly(BuMA-co-EDMA) monoliths was achieved within each design without any significant structural differences between phases. Van Deemter plots indicated higher efficiencies for the 3D serpentine chromatographic columns with higher aspect ratio turns at higher linear velocities and smaller analysis times as compared to their counterpart columns with lower aspect ratio turns. Computational fluid dynamic simulations of a basic monolithic structure indicated 44%, 90%, 100%, and 118% higher flow through narrow channels in the curved monolithic configuration as compared to the straight monolithic configuration at linear velocities of 1, 2.5, 5, and 10 mm s -1 , respectively. Isocratic RPLC separations with the 3D serpentine column resulted in an average 23% and 245% (8 solutes) increase in the number of theoretical plates as compared to the 3D spiral and 2D serpentine columns, respectively. Gradient RPLC separations with the 3D serpentine column resulted in an average 15% and 82% (8 solutes) increase in the peak capacity as compared to the 3D spiral and 2D serpentine columns, respectively. Use of the 3D serpentine column at a higher flow rate, as compared to the 3D spiral column, provided a 58% reduction in the analysis time and 74% increase in the peak capacity for the isocratic separations of the small molecules and the gradient separations of proteins, respectively.

  13. Study on automatic control of high uranium concentration solvent extraction with pulse sieve-plate column

    International Nuclear Information System (INIS)

    You Wenzhi; Xing Guangxuan; Long Maoxiong; Zhang Jianmin; Zhou Qin; Chen Fuping; Ye Lingfeng

    1998-01-01

    The author mainly described the working condition of the automatic control system of high uranium concentration solvent extraction with pulse sieve-plate column on a large scale test. The use of the automatic instrument and meter, automatic control circuit, and the best feedback control point of the solvent extraction processing with pulse sieve-plate column are discussed in detail. The writers point out the success of this experiment on automation, also present some questions that should be cared for the automatic control, instruments and meters in production in the future

  14. Behavior of partially defected R.C columns strengthened using steel jackets

    Directory of Open Access Journals (Sweden)

    Ahmed Shaban Abdel-Hay

    2015-08-01

    The main parameters studied were the type of steel jacket used and height of partial strengthened part of column. One of the tested specimens was a control specimen and the other six were partially strengthened with different types of steel jackets such as using 4 steel angles at corners connected with straps, using external ties with different spacings, and using 4 steel plates with different thicknesses welded together and connected to column by anchor bolts. Finally, the experimental results were analyzed and compared with results obtained from finite element analysis using ANSYS program.

  15. A Pilot Study On A Moment Carrying Beam-column Connection For Precast Structures

    OpenAIRE

    Kaplan, Vedat

    2010-01-01

    In this study, a moment carrying beam-column connection detail for precast structures has been investigated in the experimental and analytical manner. The 1/2 scaled beam-column test specimen is representing a real exterior precast connection detail. The cast-in-situ welded connection is applied at bottom face of the beams and additional re-bars and cast-in-situ concrete is introduced at the upper part of the beams. The experimental study is conducted in the form of varying beam top diplaceme...

  16. Design and research of seal structure for thermocouple column assembly

    International Nuclear Information System (INIS)

    Rao Qiqi; Li Na; Zhao Wei; Ma Zhigang

    2015-01-01

    The new seal structure was designed to satisfy the function of thermocouple column assembly and the reactor structure. This seal structure uses the packing graphite ring and adopts the self-sealing principle. Cone angle is brought to the seal face of seal structure which is conveniently to assembly and disassembly. After the sealing principle analysis and stress calculation of graphite ring which adopt the cone angle, the cone angle increases the radial force of seal structure and improves the seal effect. The stress analysis result shows the seal structure strength satisfies the regulation requirement. The cold and hot function test results shows the sealing effect is good, and the design requirement is satisfied. (authors)

  17. COLUMN2 - A computer program for simulating migration

    International Nuclear Information System (INIS)

    Nielsen, O.J.; Bo, P.; Carlsen, L.

    1985-10-01

    COLUMN2 is a 1D FORTRAN77 computer program designed for studies of the effects of various physicochemical processes on migration. It solves the solute transport equation and cant take into account dispersion, sorption, ion exchange, first and second order homogeneous chemical reactions. Spacial variations of input pulses and retention factors are possible. The method of solution is based on a finite difference discretion followed by the application of the method of characteristics and two separate grid systems. This report explains the mathematical and numerical methods used, describes the necessary input, contains a number of test examples, provides a listing of the program and explains how to acquire the program, adapt it to other computers and run it. This report serves as a manual for the program. (author)

  18. Materials performance in prototype Thermal Cycling Absorption Process (TCAP) columns

    International Nuclear Information System (INIS)

    Clark, E.A.

    1992-01-01

    Two prototype Thermal Cycling Absorption Process (TCAP) columns have been metallurgically examined after retirement, to determine the causes of failure and to evaluate the performance of the column container materials in this application. Leaking of the fluid heating and cooling subsystems caused retirement of both TCAP columns, not leaking of the main hydrogen-containing column. The aluminum block design TCAP column (AHL block TCAP) used in the Advanced Hydride Laboratory, Building 773-A, failed in one nitrogen inlet tube that was crimped during fabrication, which lead to fatigue crack growth in the tube and subsequent leaking of nitrogen from this tube. The Third Generation stainless steel design TCAP column (Third generation TCAP), operated in 773-A room C-061, failed in a braze joint between the freon heating and cooling tubes (made of copper) and the main stainless steel column. In both cases, stresses from thermal cycling and local constraint likely caused the nucleation and growth of fatigue cracks. No materials compatibility problems between palladium coated kieselguhr (the material contained in the TCAP column) and either aluminum or stainless steel column materials were observed. The aluminum-stainless steel transition junction appeared to be unaffected by service in the AHL block TCAP. Also, no evidence of cracking was observed in the AHL block TCAP in a location expected to experience the highest thermal shock fatigue in this design. It is important to limit thermal stresses caused by constraint in hydride systems designed to work by temperature variation, such as hydride storage beds and TCAP columns

  19. Refreshment topics II: Design of distillation columns

    Directory of Open Access Journals (Sweden)

    Milojević Svetomir

    2006-01-01

    Full Text Available For distillation column design it is necessary to define all the variable parameters such as component concentrations in different streams temperatures, pressures, mass and energy flow, which are used to represent the separation process of some specific system. They are related to each other according to specific laws, and if the number of such parameters exceeds the number of their relationships, in order to solve a problem some of them must be specified in advance or some constraints assumed for the mass balance, the balance of energy, phase equilibria or chemical equilibria. Knowledge of specific elements which are the constituents of a distillation unit must be known to define the number of design parameters as well as some additional apparati also necessary to realize the distilation. Each separate apparatus might be designed and constructed only if all the necessary and variable parameters for such a unit are defined. This is the right route to solve a distilation unit in many different cases. The construction of some distillation unit requires very good knowledge of mass, heat and momentum transfer phenomena. Moreover, the designer needs to know which kind of apparatus will be used in the distillation unit to realize a specific production process. The most complicated apparatus in a rectification unit is the distillation column. Depending on the complexity of the separation process one, two or more columns are often used. Additional equipment are heat exchangers (reboilers, condensers, cooling systems, heaters, separators, tanks for reflux distribution, tanks and pumps for feed transportation, etc. Such equipment is connected by pipes and valves, and for the normal operation of a distillation unit other instruments for measuring the flow rate, temperature and pressure are also required. Problems which might arise during the determination and selection of such apparati and their number requires knowledge of the specific systems which must

  20. Development of a sealed source radiation detector system for gamma ray scanning of petroleum distillation columns

    International Nuclear Information System (INIS)

    Vasquez Salvador, Pablo Antonio

    2004-01-01

    Gamma Ray Scanning is an online technique to 'view' the hydraulic performance of an operating column, with no disruption to operating processes conditions (pressure and temperature), as a cost-effective solution. The principle of this methodology consists of a small suitably sealed gamma radiation source and a radiation detector experimentally positioned to the column, moving concurrently in small increments on opposite sides and the quantity of gamma transmitted. The source-detector system consists of: a sealed ''6 0 Co radioactive source in a panoramic lead radiator, a scintillator detector coupled to a ratemeter / analyzer and a mobile system. In this work, a gamma scanning sealed source-detector system for distillation columns, was developed, comparing two scintillator detectors: NaI(Tl) (commercial) and CsI(Tl) (IPEN). In order to project the system, a simulated model of a tray-type distillation column was used. The equipment developed was tested in an industrial column for water treatment (6.5 m diameter and 40 m height). The required activities of 6 ''0Co, laboratory (11.1 MBq) and industrial works (1.48 TBq) were calculated by simulation software. Both, the NaI(Tl) and the CsI(Tl) detectors showed good proprieties for gamma scanning applications, determining the position and presence or absence of trays. (author)

  1. Review of design codes of concrete encased steel short columns under axial compression

    Directory of Open Access Journals (Sweden)

    K.Z. Soliman

    2013-08-01

    Full Text Available In recent years, the use of encased steel concrete columns has been increased significantly in medium-rise or high-rise buildings. The aim of the present investigation is to assess experimentally the current methods and codes for evaluating the ultimate load behavior of concrete encased steel short columns. The current state of design provisions for composite columns from the Egyptian codes ECP203-2007 and ECP-SC-LRFD-2012, as well as, American Institute of Steel Construction, AISC-LRFD-2010, American Concrete Institute, ACI-318-2008, and British Standard BS-5400-5 was reviewed. The axial capacity portion of both the encased steel section and the concrete section was also studied according to the previously mentioned codes. Ten encased steel concrete columns have been investigated experimentally to study the effect of concrete confinement and different types of encased steel sections. The measured axial capacity of the tested ten composite columns was compared with the values calculated by the above mentioned codes. It is concluded that non-negligible discrepancies exist between codes and the experimental results as the confinement effect was not considered in predicting both the strength and ductility of concrete. The confining effect was obviously influenced by the shape of the encased steel section. The tube-shaped steel section leads to better confinement than the SIB section. Among the used codes, the ECP-SC-LRFD-2012 led to the most conservative results.

  2. Mechanical behavior of confined self-compacting reinforced concrete circular columns under concentric axial loading

    Directory of Open Access Journals (Sweden)

    Fouad Khairallah

    2013-12-01

    Full Text Available While there is abundant research information on ordinary confined concrete, there are little data on the behavior of Self-Compacting Concrete (SCC under such condition. Due to higher shrinkage and lower coarse aggregate content of SCC compared to that of Normal Concrete (NC, its composite performance under confined conditions needs more investigation. This paper has been devoted to investigate and compare the mechanical behavior of confined concrete circular columns cast with SCC and NC under concentric axial loading. The parameters affecting are including concrete compressive strength and confinement configuration. Twenty column specimens were casted and confined using four confinement techniques, CFRP wrap, FRP tube, GFRP wrap, and spiral steel hoops. The performance of the tested column specimens is evaluated based on mode of failure, load–displacement curve, stress–strain characteristics, ultimate strength, ductility, and degree of confinement.

  3. A Hybrid Column Generation approach for an Industrial Waste Collection Routing Problem

    DEFF Research Database (Denmark)

    Hauge, Kristian; Larsen, Jesper; Lusby, Richard Martin

    2014-01-01

    , while empty containers must be returned to the depot to await further assignments. Unlike, the traditional ROROR problem, where vehicles may transport one skip container at a time regardless of whether it is full or not, we consider cases in which a vehicle can transport up to eight containers, at most...... two of which can be full. We propose a Generalized Set Partitioning formulation of the problem and describe a hybrid column generation procedure to solve it. A fast Tabu Search heuristic is used to generate new columns. The proposed methodology is tested on nine data sets, four of which are actual......, real-world problem instances. Results indicate that the hybrid column generation outperforms a purely heuristic approach in terms of both running time and solution quality. High quality solutions to problems containing up to 100 orders can be solved in approximately 15 minutes....

  4. Preparation of Affinity Column Based on Zr4+ Ion for Phosphoproteins Isolation

    International Nuclear Information System (INIS)

    Lee, Seon Mi; Bae, In Ae; Park, Jung Hyen; Kim, Tae Dong; Choi, Seong Ho

    2009-01-01

    This paper has described about preparation of Zr 4+ affinity column based on the poly(styreneco- glycidyl methacrylate) prepared by emulsion polymerization of styrene and glycidyl methacrylate in order to isolate phosphopeptide. The Zr 4+ ions were introduced after the phophonation of an epoxy group on polymeric microspheres. The successful preparation of Zr 4+ -immobilized polymeric microsphere stationary phase was confirmed through Fourier transform infrared spectra, optical microscopy, scanning electron microscopy, X-ray photoelectron spectra and inductively coupled plasma-atomic emission spectrometer. The separation efficiency for Zr 4+ affinity column prepared by slurry packing was tested to phosphonated casein and dephosphonated casein. The resolution time (min) of the phosphonated casein was higher than that of dephosphated casein for Zr 4+ affinity polymeric microsphere by liquid chromatography. This Zr 4+ affinity column can be used for isolation of phosphonated casein from casein using liquid chromatography

  5. Preparation of Affinity Column Based on Zr{sup 4+} Ion for Phosphoproteins Isolation

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Seon Mi; Bae, In Ae; Park, Jung Hyen; Kim, Tae Dong; Choi, Seong Ho [Hannam University, Daejeon (Korea, Republic of)

    2009-06-15

    This paper has described about preparation of Zr{sup 4+} affinity column based on the poly(styreneco- glycidyl methacrylate) prepared by emulsion polymerization of styrene and glycidyl methacrylate in order to isolate phosphopeptide. The Zr{sup 4+} ions were introduced after the phophonation of an epoxy group on polymeric microspheres. The successful preparation of Zr{sup 4+}-immobilized polymeric microsphere stationary phase was confirmed through Fourier transform infrared spectra, optical microscopy, scanning electron microscopy, X-ray photoelectron spectra and inductively coupled plasma-atomic emission spectrometer. The separation efficiency for Zr{sup 4+} affinity column prepared by slurry packing was tested to phosphonated casein and dephosphonated casein. The resolution time (min) of the phosphonated casein was higher than that of dephosphated casein for Zr{sup 4+} affinity polymeric microsphere by liquid chromatography. This Zr{sup 4+} affinity column can be used for isolation of phosphonated casein from casein using liquid chromatography.

  6. Twin column chromatography: A new technique for treating limited amounts of waste

    International Nuclear Information System (INIS)

    Wenzel, U.

    1995-01-01

    The authors set up a chromatographic unit for the decontamination of analytical discards from Am and Pu. The unit is based on the twin column concept, i.e. the chromatographic support is accommodated in two identical columns and the detector placed between the columns. Thus, they could employ the wall effects model allowing the evaluation of breakthrough chromatograms at low effluent concentrations and the determination of the design parameters for the lay-out of the unit. The authors verified the model with the unit and obtained a good agreement between measured and calculated parameters. In the test phase, they processed 47 liters discards, they obtained 56 liters decontaminated waste with a DF Am of 770 and a total DF α of 7,000 and 22 liters eluate which was reduced by evaporation to 0.8 liters

  7. Numerical analysis of stone columns in mitigating liquefaction effects in embankment fills

    Energy Technology Data Exchange (ETDEWEB)

    Borghei, Z.; Soroush, A. [Amirkabir University of Technology, Tehran, (Iran, Islamic Republic of); Noorzad, A. [Power and Water University of Technology, Tehran, (Iran, Islamic Republic of)

    2010-07-01

    The traditional approach to liquefaction in embankment fills is to use in-situ densification. The use of stone columns offers the possibility of preventing liquefaction and associated settlements while reducing the cost and time required for treatment. This paper investigated the behaviour of stone columns using a numerical method. The study focused on a case study, a sand layer beneath two wall tanks, butane and propane NGL, located on Siri Island, Persian Gulf, Iran. Numerical analyses were carried out to evaluate the rate of excess pore pressure build-up in the improved ground. The numerical model results were compared to the simulation results from a centrifuge test for a uniform 19m-thick liquefiable sand layer. The numerical methodology was verified. The results showed that the stone columns can significantly increase the rate of pore pressure dissipation and reduce the settlement. It was found that the installation process densifies the surrounding soil, decreasing the liquefaction potential.

  8. A multicomponent ion-exchange equilibrium model for chabazite columns treating ORNL wastewaters

    International Nuclear Information System (INIS)

    Perona, J.J.

    1993-06-01

    Planned near-term and long-term upgrades of the Oak Ridge National Laboratory (ORNL) Process Waste Treatment Plant (PWTP) will use chabazite columns to remove 90 Sr and 137 Cs from process wastewater. A valid equilibrium model is required for the design of these columns and for evaluating their performance when influent wastewater composition changes. The cations exchanged, in addition to strontium and cesium, are calcium, magnesium, and sodium. A model was developed using the Wilson equation for the calculation of the solid-phase activity coefficients. The model was tested against chabazite column runs on two different wastewaters and found to be valid. A sensitivity analysis was carried out for the projected wastewater compositions, in which the model was used to predict changes in relative separation factors for strontium and cesium subject to changes in calcium, magnesium, and sodium concentrations

  9. RpeakChrom: Novel R package for the automated characterization and optimization of column efficiency in high-performance liquid chromatography analysis.

    Science.gov (United States)

    Peris-Díaz, Manuel David; Alcoriza-Balaguer, Maria Isabel; García-Cañaveras, Juan Carlos; Santonja, Francisco; Sentandreu, Enrique; Lahoz, Agustín

    2017-11-01

    Characterization of chromatographic columns using the traditional van Deemter method is limited by the necessity of calculating extra-column variance, issue particularly relevant when modeling asymmetrical peaks eluted from monolithic columns. A novel R package that implements Parabolic Variance Modified Gaussian approach for accurate peak modeling, van Deemter equation and two alternatives approaches, based on van Deemter, has been developed to calculate the height equivalent to a theoretical plate (HETP). To assess package capabilities conventional packed reverse-phase and monolithic HPLC columns were characterized. Peaks eluted from the monolithic column showed a high value of factor asymmetry due, in part, to the contribution of extra-column factors. Such deviation can be circumvented by the two alternatives approaches implemented in the R-package. Furthermore, increased values of eddy diffusion and mass transfer kinetics terms in HETP were observed for the packed column, while accuracy was below 9% in all cases. These results showed the usefulness of the R-package for both modeling chromatographic peaks and assessing column efficiency. The RpeakChrom package could become a helpful tool for testing new stationary phases during column development and to evaluate column during its lifetime. This R tool is freely available from CRAN (https://CRAN.R-project.org/package=RpeakChrom). © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  10. Retention of nitrous gases in scrubber columns

    International Nuclear Information System (INIS)

    Nakazone, A.K.; Costa, R.C.; Lobao, A.S.T.; Matsuda, H.T.; Araujo, B.F. de

    1988-01-01

    During the UO 2 dissolution in nitric acid, some different species of NO (sub)x are released. The off gas can either be refluxed to the dissolver or be released and retained on special colums. The final composition of the solution is the main parameter to take in account. A process for nitrous gases retention using scrubber colums containing H 2 O or diluted HNO 3 is presented. Chemiluminescence measurement was employed to NO x evaluation before and after scrubing. Gas flow, temperature, residence time are the main parameters considered in this paper. For the dissolution of 100g UO 2 in 8M nitric acid, a 6NL/h O 2 flow was the best condition for the NO/NO 2 oxidation with maximum absorption in the scrubber columns. (author) [pt

  11. Education and training column: the learning collaborative.

    Science.gov (United States)

    MacDonald-Wilson, Kim L; Nemec, Patricia B

    2015-03-01

    This column describes the key components of a learning collaborative, with examples from the experience of 1 organization. A learning collaborative is a method for management, learning, and improvement of products or processes, and is a useful approach to implementation of a new service design or approach. This description draws from published material on learning collaboratives and the authors' experiences. The learning collaborative approach offers an effective method to improve service provider skills, provide support, and structure environments to result in lasting change for people using behavioral health services. This approach is consistent with psychiatric rehabilitation principles and practices, and serves to increase the overall capacity of the mental health system by structuring a process for discovering and sharing knowledge and expertise across provider agencies. (PsycINFO Database Record (c) 2015 APA, all rights reserved).

  12. [Lateral column lengthening osteotomy of calcaneus].

    Science.gov (United States)

    Hintermann, B

    2015-08-01

    Lengthening of the lateral column for adduction of forefoot and restoration of the medial arch. Stabilization of the ankle joint complex. Supple flatfoot deformity (posterior tibial tendon dysfunction stage II). Instability of the medial ankle joint complex (superficial deltoid and spring ligament). Posttraumatic valgus and pronation deformity of the foot. Rigid flatfoot deformity (posterior tibial tendon dysfunction stage III and IV). Talocalcaneal and naviculocalcaneal coalition. Osteoarthritis of calcaneocuboid joint. Exposition of calcaneus at sinus tarsi. Osteotomy through sinus tarsi and widening until desired correction of the foot is achieved. Insertion of bone graft. Screw fixation. Immobilization in a cast for 6 weeks. Weight-bearing as tolerated from the beginning. In the majority of cases, part of hindfoot reconstruction. Reliable and stable correction. Safe procedure with few complications.

  13. Yield stress independent column buckling curves

    DEFF Research Database (Denmark)

    Stan, Tudor‐Cristian; Jönsson, Jeppe

    2017-01-01

    of the yield stress is to some inadequate degree taken into account in the Eurocode by specifying that steel grades of S460 and higher all belong to a common set of “raised” buckling curves. This is not satisfying as it can be shown theoretically that the current Eurocode formulation misses an epsilon factor......Using GMNIA and shell finite element modelling of steel columns it is ascertained that the buckling curves for given imperfections and residual stresses are not only dependent on the relative slenderness ratio and the cross section shape but also on the magnitude of the yield stress. The influence...... in the definition of the normalised imperfection magnitudes. By introducing this factor it seems that the GMNIA analysis and knowledge of the independency of residual stress levels on the yield stress can be brought together and give results showing consistency between numerical modelling and a simple modified...

  14. Calculation of a TBP extraction column

    International Nuclear Information System (INIS)

    Lima Soares, M.L. de.

    1973-01-01

    Problems involving the number of stages in an extraction column and the equipment needed in most aqueous methods of reprocessing of nuclear fuels were studied. A solution for the separation of uranium from fission products in a feed solution that contains these components plus nitric acid, thorium and protactinium is obtained. The program has peculiarities such as treatment of tracer components; acceptance of decontamination and recuperation factors better than the set values for the solution; occurrence of niaxima concentrations; change of key component; criterion for ending of section; corrections for interaction; input data not including concentration estimates of the raffinate and organic extract; set of limitations for the concentrations based on input data to help convergence

  15. Experimental validation of pulsed column inventory estimators

    International Nuclear Information System (INIS)

    Beyerlein, A.L.; Geldard, J.F.; Weh, R.; Eiben, K.; Dander, T.; Hakkila, E.A.

    1991-01-01

    Near-real-time accounting (NRTA) for reprocessing plants relies on the timely measurement of all transfers through the process area and all inventory in the process. It is difficult to measure the inventory of the solvent contractors; therefore, estimation techniques are considered. We have used experimental data obtained at the TEKO facility in Karlsruhe and have applied computer codes developed at Clemson University to analyze this data. For uranium extraction, the computer predictions agree to within 15% of the measured inventories. We believe this study is significant in demonstrating that using theoretical models with a minimum amount of process data may be an acceptable approach to column inventory estimation for NRTA. 15 refs., 7 figs

  16. Use of a pulsed column contactor as a continuous oxalate precipitation reactor

    International Nuclear Information System (INIS)

    Borda, Gilles; Brackx, Emmanuelle; Boisset, Laurence; Duhamet, Jean; Ode, Denis

    2011-01-01

    Research highlights: → A new type of continuous precipitating device was patented by CEA and tested with reaction between a surrogate nitrate cerium(III) or neodymium(III) and oxalate complexing agent. → Precipitate is confined in aqueous phase emulsion in tetrapropylene hydrogen and does not form deposit on the vessel walls. → Measure size of the precipitate ranges from 20 to 40 μm, it meets the process requirements to filter, and the precipitation reaction is complete. → The laboratory design can be extrapolated to an industrial uranium(IV) and minor actinide(III) coprecipitating column. - Abstract: The current objective of coprecipitating uranium, and minor actinides in order to fabricate a new nuclear fuel by direct (co)precipitation for further transmutation, requires to develop specific technology in order to meet the following requirements: nuclear maintenance, criticity, and potentially high flowrates due to global coprecipitation. A new type of device designed and patented by the CEA was then tested in 2007 under inactive conditions and with uranium. The patent is for organic confinement in a pulsed column (PC). Actually, pulsed columns have been working for a long time in a nuclear environment, as they allow high capacity, sub-critical design (annular geometry) and easy high activity maintenance. The precipitation reaction between the oxalate complexing agent and a surrogate nitrate - cerium(III) or neodymium(III) alone, or coprecipitated uranium(IV) and cerium(III) - occurs within an emulsion created in the device by these two phases flowing with a counter-current chemically inert organic phase (for example tetrapropylene hydrogen-TPH) produced by the stirring action of the column pulsator. The precipitate is confined and thus does not form deposits on the vessel walls (which are also water-repellent); it flows downward by gravity and exits the column continuously into a settling tank. The results obtained for precipitation of cerium or

  17. Nde of Frp Wrapped Columns Using Infrared Thermography

    Science.gov (United States)

    Halabe, Udaya B.; Dutta, Shasanka Shekhar; GangaRao, Hota V. S.

    2008-02-01

    This paper investigates the feasibility of using Infrared Thermography (IRT) for detecting debonds in Fiber Reinforced Polymer (FRP) wrapped columns. Laboratory tests were conducted on FRP wrapped concrete cylinders of size 6″×12″ (152.4 mm×304.8 mm) in which air-filled and water-filled debonds of various sizes were placed underneath the FRP wraps. Air-filled debonds were made by cutting plastic sheets into the desired sizes whereas water-filled debonds were made by filling water in custom made polyethylene pouches. Both carbon and glass fiber reinforced wraps were considered in this study. Infrared tests were conducted using a fully radiometric digital infrared camera which was successful in detecting air-filled as well as water-filled subsurface debonds. In addition to the laboratory testing, two field trips were made to Moorefield, West Virginia for detecting subsurface debonds in FRP wrapped timber piles of a railroad bridge using infrared testing. The results revealed that infrared thermography can be used as an effective nondestructive evaluation tool for detecting subsurface debonds in structural components wrapped with carbon or glass reinforced composite fabrics.

  18. Novel field emission SEM column with beam deceleration technology

    Energy Technology Data Exchange (ETDEWEB)

    Jiruše, Jaroslav; Havelka, Miloslav; Lopour, Filip

    2014-11-15

    A novel field-emission SEM column has been developed that features Beam Deceleration Mode, high-probe current and ultra-fast scanning. New detection system in the column is introduced to detect true secondary electron signal. The resolution power at low energy was doubled for conventional SEM optics and moderately improved for immersion optics. Application examples at low landing energies include change of contrast, imaging of non-conductive samples and thin layers. - Highlights: • A novel field-emission SEM column has been developed. • Implemented beam deceleration improves the SEM resolution at 1 keV two times. • New column maintains high analytical potential and wide field of view. • Detectors integrated in the column allow gaining true SE and BE signal separately. • Performance of the column is demonstrated on low energy applications.

  19. Novel field emission SEM column with beam deceleration technology

    International Nuclear Information System (INIS)

    Jiruše, Jaroslav; Havelka, Miloslav; Lopour, Filip

    2014-01-01

    A novel field-emission SEM column has been developed that features Beam Deceleration Mode, high-probe current and ultra-fast scanning. New detection system in the column is introduced to detect true secondary electron signal. The resolution power at low energy was doubled for conventional SEM optics and moderately improved for immersion optics. Application examples at low landing energies include change of contrast, imaging of non-conductive samples and thin layers. - Highlights: • A novel field-emission SEM column has been developed. • Implemented beam deceleration improves the SEM resolution at 1 keV two times. • New column maintains high analytical potential and wide field of view. • Detectors integrated in the column allow gaining true SE and BE signal separately. • Performance of the column is demonstrated on low energy applications

  20. Three-dimensional motion pattern of the caudal lumbar and lumbosacral portions of the vertebral column of dogs.

    Science.gov (United States)

    Benninger, Monika I; Seiler, Gabriela S; Robinson, Leanne E; Ferguson, Stephen J; Bonél, Harald M; Busato, André R; Lang, Johann

    2004-05-01

    To evaluate the 3-dimensional motion pattern including main and coupled motions of the caudal lumbar and lumbosacral portions of the vertebral column of dogs. Vertebral columns of 9 German Shepherd Dogs (GSDs) and 16 dogs of other breeds with similar body weights and body conditions. Main and coupled motions of the caudal lumbar and lumbosacral portions of the vertebral column (L4 to S1) were determined by use of a testing apparatus that permitted precise application of known pure moments to the vertebral column. Motion was compared between GSDs and dogs of other breeds. All specimens had a similar motion pattern consisting of main motion and a certain amount of coupled motion including translation. Vertebral columns of GSDs had significantly less main motion in all directions than that of dogs of other breeds. Translation was similar in GSDs and dogs of other breeds and was smallest at the lumbosacral motion segment. Results indicated that motion in the caudal lumbar and lumbosacral portions of the vertebral column of dogs is complex and provided a basis for further studies evaluating abnormal vertebral columns.

  1. Estimation of bearing capacity of floating group of stone columns

    OpenAIRE

    Fattah, Mohammed Y.; Al-Neami, Mohammed A.; Shamel Al-Suhaily, Ahmed

    2017-01-01

    Stone column is one of the ground improvement techniques. This technique has a proven performance, short time schedule, durability, constructability and low costs. The stone column technique has been used as a method of reinforcement of soft ground over the past 30 years. The bearing capacity of the stone column still has high level of uncertainties because the existing formulas for the estimation of the bearing capacity are general and do not take into consideration the type of the stone col...

  2. Uncertain Buckling Load and Reliability of Columns with Uncertain Properties

    DEFF Research Database (Denmark)

    Köylüoglu, H. U.; Nielsen, Søren R. K.; Cakmak, A. S.

    Continuous and finite element methods are utilized to determine the buckling load of columns with material and geometrical uncertainties considering deterministic, stochastic and interval models for the bending rigidity of columns. When the bending rigidity field is assumed to be deterministic, t....... for structural design, the lower bound is of crucial interest. The buckling load of fixed-free, simple-supported, pinned-fixed, fixed-fixed columns and a sample frame are calculated....

  3. Flow-through Column Experiments and Modeling of Microbially Mediated Cr(VI) Reduction at Hanford 100H

    Science.gov (United States)

    Yang, L.; Molins, S.; Beller, H. R.; Brodie, E. L.; Steefel, C.; Nico, P. S.; Han, R.

    2010-12-01

    Fe(II) and Mn(II) released from the sediment could account for the observed Cr(VI) removal. The biogeochemical modeling was employed to test two hypotheses that could explain the release of Fe(II) and Mn(II) from the column sediments: 1) acetate produced by lactate fermentation provided the substrate for the growth of iron(III) and manganese(IV) oxide reducers, and 2) direct reduction of iron(III) and manganese(IV) oxides by hydrogen sulfide generated during sulfate reduction. Overall, experimental and modeling results suggested that Cr(VI) reduction in the sulfate-reducing columns occurred through a complex network of microbial reactions that included fermentation, sulfate reduction, and possibly the stimulated iron-reducing communities.

  4. Phase II investigation of the response of columns to short duration loadings: scaling report. Mark I Program, Task 3.2.1. Teledyne report TR-2488(e)

    International Nuclear Information System (INIS)

    1978-03-01

    Phase II of a two-phase column testing program which will determine short-term load capacities for the Mark I containment columns is now under way. The scaling report is submitted to outline the scaling procedures and also to present the scaled quantities such as geometry, load eccentricity, and load time duration. Dimensional analysis and similarity techniques were applied to the experimental models to obtain a set of twelve scaling laws. These scaling laws provide a rational basis for modeling the columns. The scaling laws give nondimensional relationships which are common to both the model and prototype. Parameters which are known to be important in column buckling and which were found to be important during Phase I testing were used as the independent variables in the scaling laws. Column specimens for Phase II testing have been designed to be representative of the prototype columns. Combined bending and compression are characteristic of the Mark I columns with the maximum moment applied at the column-ring girder junction. The experimental columns reflect these characteristics, even though special fixtures and equipment will be required to perform the tests. The column specimens include the scaled rotational stiffness of the ring girder as well as the boundary condition of the pinned or sliding end. To properly incorporate the effects of residual stress, the models will be constructed from ''off-the-shelf', carbon steel pipe and rolled sections, and built-up sections will be fabricated from standard plate. The column geometries scale almost exactly, even though ''replica'' modeling was not used

  5. Experimental investigations on steel-concrete composite columns for varying parameters

    Science.gov (United States)

    Aparna, V.; Vivek, D.; Neelima, Kancharla; Karthikeyan, B.

    2017-07-01

    In this study, the experimental investigations on steel tubes filled with different types of concrete are presented. Steel tubes filled with fibre reinforced concrete using lathe waste and steel tube with concerned confined with steel mesh were investigated. The combinations were compared with steel tubes with conventional concrete. A total of 4 concrete filled steel tube (CFST) combinations were made with tubes of diameter 100 mm with wall thickness 1.6 mm and a height of 300 mm. Axial compression test to examine the resisting capacity of the columns and push-out test for noting the bond strength were performed. Coupon tests were also conducted to determine the mechanical properties of steel. The structural behaviour of the composite columns was evaluated from on the test results. It was observed that steel tube filled fibre reinforced possessed better bond strength and resistance to axial load.

  6. The design of a new concept chromatography column.

    Science.gov (United States)

    Camenzuli, Michelle; Ritchie, Harald J; Ladine, James R; Shalliker, R Andrew

    2011-12-21

    Active Flow Management is a new separation technique whereby the flow of mobile phase and the injection of sample are introduced to the column in a manner that allows migration according to the principles of the infinite diameter column. A segmented flow outlet fitting allows for the separation of solvent or solute that elutes along the central radial section of the column from that of the sample or solvent that elutes along the wall region of the column. Separation efficiency on the analytical scale is increased by 25% with an increase in sensitivity by as much as 52% compared to conventional separations.

  7. Simulation of startup period of hydrogen isotope separation distillation column

    International Nuclear Information System (INIS)

    Sazonov, A.B.; Kagramanov, Z.G.; Magomedbekov, Eh.P.

    2003-01-01

    Kinetic procedure for the mathematical simulation of start-up regime of rectification columns for molecular hydrogen isotope separation was developed. Nonstationary state (start-up period) of separating column for rectification of multi-component mixture was calculated. Full information on equilibrium and kinetic physicochemical properties of components in separating mixtures was used for the calculations. Profile of concentration of components by height of column in task moment of time was calculated by means of differential equilibriums of nonstationary mass transfer. Calculated results of nonstationary state of column by the 2 m height, 30 mm diameter during separation of the mixture: 5 % protium, 70 % deuterium, 25 % tritium were illustrated [ru

  8. Evaluation of Controller Tuning Methods Applied to Distillation Column Control

    DEFF Research Database (Denmark)

    Nielsen, Kim; W. Andersen, Henrik; Kümmel, Professor Mogens

    A frequency domain approach is used to compare the nominal performance and robustness of dual composition distillation column control tuned according to Ziegler-Nichols (ZN) and Biggest Log Modulus Tuning (BLT) for three binary distillation columns, WOBE, LUVI and TOFA. The scope of this is to ex......A frequency domain approach is used to compare the nominal performance and robustness of dual composition distillation column control tuned according to Ziegler-Nichols (ZN) and Biggest Log Modulus Tuning (BLT) for three binary distillation columns, WOBE, LUVI and TOFA. The scope...

  9. Performance of zeolite scavenge column in Xe monitoring system

    International Nuclear Information System (INIS)

    Wang Qian; Wang Hongxia; Li Wei; Bian Zhishang

    2010-01-01

    In order to improve the performance of zeolite scavenge column, its ability of removal of humidity and carbon dioxide was studied by both static and dynamic approaches. The experimental results show that various factors, including the column length and diameter, the mass of zeolite, the content of water in air, the temperature rise during adsorption, and the activation effectiveness all effect the performance of zeolite column in scavenging humanity and carbon dioxide. Based on these results and previous experience, an optimized design of the zeolite column is made for use in xenon monitoring system. (authors)

  10. Mini-columns for Conducting Breakthrough Experiments. Design and Construction

    Energy Technology Data Exchange (ETDEWEB)

    Dittrich, Timothy M. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Reimus, Paul William [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Ware, Stuart Douglas [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2015-06-11

    Experiments with moderately and strongly sorbing radionuclides (i.e., U, Cs, Am) have shown that sorption between experimental solutions and traditional column materials must be accounted for to accurately determine stationary phase or porous media sorption properties (i.e., sorption site density, sorption site reaction rate coefficients, and partition coefficients or Kd values). This report details the materials and construction of mini-columns for use in breakthrough columns to allow for accurate measurement and modeling of sorption parameters. Material selection, construction techniques, wet packing of columns, tubing connections, and lessons learned are addressed.

  11. Experimental investigation on full scale RC beam-column joint of NPP structures

    International Nuclear Information System (INIS)

    Thandavamoorthy, T.S.; Lakshmanan, N.; Reddy, G.R.; Kushwaha, H.S.

    2003-01-01

    The Nuclear Power Plant (NPP) structures in India are constructed using reinforced concrete. The beam-column joint in these structures are critical sub-assemblages because they ensure continuity of a structure and transfer forces from one element to another. Under seismic excitation, the beam-column joint region is subjected to horizontal and vertical shear forces whose magnitudes are typically many times higher than those within the adjacent beams and columns. In view of the increased incidence of seismicity in the country, the safety of these structures against earthquake loading assumes greater significance. There is a growing need to look into the seismic safety aspect of existing RC frame type structures in NPPs, which have been designed as per codes prevalent at the time of their construction. Seismic performance of such joints has not been studied extensively in India. Therefore experimental testing of full scale joint identical to those available in the existing NPP structures, was carried out to study its behaviour and evaluate its capacity. The size of the beam of the joint was 2000 mm x 610 mm x 915 mm and column 2915 mm x 610 mm x 915 mm. The percentage reinforcement of the beam was 4.95 and column 1.5. Such full scale and heavily reinforced concrete joint was cast successfully in the laboratory and tested under monotonic loading. The paper presents a complete description of the experimental testing, observations made during testing as for cracking, deflection and rotation of joint, discussion of results obtained, etc. Conclusions drawn from the investigation are also presented. (author)

  12. Comparison and Analysis of Steel Frame Based on High Strength Column and Normal Strength Column

    Science.gov (United States)

    Liu, Taiyu; An, Yuwei

    2018-01-01

    The anti-seismic performance of high strength steel has restricted its industrialization in civil buildings. In order to study the influence of high strength steel column on frame structure, three models are designed through MIDAS/GEN finite element software. By comparing the seismic performance and economic performance of the three models, the three different structures are comprehensively evaluated to provide some references for the development of high strength steel in steel structure.

  13. Experimental Ion Exchange Column With SuperLig 639 And Simulant Formulation

    Energy Technology Data Exchange (ETDEWEB)

    Morse, Megan; Nash, C.

    2013-08-26

    SuperLig®639 ion exchange resin was tested as a retrieval mechanism for pertechnetate, through decontamination of a perrhenate spiked 5M Simple Average Na{sup +} Mass Based Simulant. Testing included batch contacts and a three-column ion exchange campaign. A decontamination of perrhenate exceeding 99% from the liquid feed was demonstrated. Analysis of the first formulation of a SBS/WESP simulant found unexpectedly low concentrations of soluble aluminum. Follow-on work will complete the formulation.

  14. On-column reduction of catecholamine quinones in stainless steel columns during liquid chromatography.

    Science.gov (United States)

    Xu, R; Huang, X; Kramer, K J; Hawley, M D

    1995-10-10

    The chromatographic behavior of quinones derived from the oxidation of dopamine and N-acetyldopamine has been studied using liquid chromatography (LC) with both a diode array detector and an electrochemical detector that has parallel dual working electrodes. When stainless steel columns are used, an anodic peak for the oxidation of the catecholamine is observed at the same retention time as a cathodic peak for the reduction of the catecholamine quinone. In addition, the anodic peak exhibits a tail that extends to a second anodic peak for the catecholamine. The latter peak occurs at the normal retention time of the catecholamine. The origin of this phenomenon has been studied and metallic iron in the stainless steel components of the LC system has been found to reduce the quinones to their corresponding catecholamines. The simultaneous appearance of a cathodic peak for the reduction of catecholamine quinone and an anodic peak for the oxidation of the corresponding catecholamine occurs when metallic iron in the exit frit reduces some of the quinones as the latter exits the column. This phenomenon is designated as the "concurrent anodic-cathodic response." It is also observed for quinones of of 3,4-dihydroxybenzoic acid and probably occurs with o- or p-quinones of other dihydroxyphenyl compounds. The use of nonferrous components in LC systems is recommended to eliminate possible on-column reduction of quinones.

  15. Strengthening of Masonry Columns with BFRCM or with Steel Wires: An Experimental Study

    Directory of Open Access Journals (Sweden)

    Marinella Fossetti

    2016-05-01

    Full Text Available Nowadays, innovative materials are more frequently adopted for strengthening historical constructions and masonry structures. The target of these techniques is to improve the structural efficiency with retrofitting methods while having a reduced aesthetical impact. In particular, the use of basalt fiber together with a cementitious matrix emerges as a new technique. This kind of fiber is obtained by basalt rock without other components, and consequently it could be considered a natural material, compatible with masonry. Another innovative technique for strengthening masonry columns consists of applying steel wires in the correspondence of mortar joints. Both techniques have been recently proposed and some aspects of their structural performances are still open. This paper presents the results of an experimental study on the compressive behavior of clay brick masonry columns reinforced either with Basalt Fiber–Reinforced Cementitious Matrix (BFRCM or with steel wire collaring. Uniaxial compressive tests were performed on eight retrofitted columns and four control specimens until failure. Two masonry grades were considered by varying the mix used for the mortar. Results are presented and discussed in terms of axial stress-strain curves, failure modes and crack patterns of tested specimens. Comparisons with unreinforced columns show the capability of these techniques in increasing ductility with limited strength enhancements.

  16. Behavior of Reinforced Hybrid Concrete Corbel-Column Connection with Vertical Construction Joint

    Directory of Open Access Journals (Sweden)

    Ammar Yasir Ali

    2017-03-01

    Full Text Available In this paper, shear behavior of reinforced hybrid concrete connection of corbel-column is experimentally investigated. Nine homogenous and hybrid concrete corbel-column connections subjected to vertical applied loads were constructed and tested within two test groups (A, B. The experimental program included the effect of several variables such as type of hybrid concrete;high strength concrete (HSC or steel fiber reinforced concrete (SFRC, monolithic casting of hybrid concrete connection, and presence of construction joint at the interface of corbel-column. Experimental results showed significant effects of concrete hybridization on the structural behavior of connection specimens such as: ultimate strength, cracking loads, cracking patterns, and failure modes. Hybridization process in group (A included hybrid connection of corbel-column with HSC or SFRC corbel instated of NSC. This process led to increase the capacity of connection by (26%, 38% and shear cracking loads by (20%, 120% respectively. Moreover, connections of hybrid concrete corbels cast monolithically improved the shear capacity of corbels by (19%, 42% for HSC or SFRC respectively. In group (B, presence of construction joint at connection region reduced the shear capacity of connectionsby (10% to 22% and cracking loads by (23%-62% compared with connections cast monolithically.

  17. Influence of column type and chromatographic conditions on the ion-exchange chromatography of immunoglobulins.

    Science.gov (United States)

    Yang, Y B; Harrison, K

    1996-08-30

    Immunoglobulins are often purified by affinity chromatography. However, this technique is costly, can result in poor resolution for subclasses (or is only group specific), and leads to possible leaching of contaminants into the purified products. Ion-exchange chromatography has shown great potential and has found an increased usage in the purification of immunoglobulins. The aim of this study is to further understand the separation mechanism with emphasis on the influence of column type and chromatographic conditions on the peak shape, selectivity and changes in the elution patterns. Included are strong cation-exchange, strong anion-exchange and weak anion-exchange columns. Five immunoglobulin G antibodies were used as test probes. Some sera and ascites were also used in the study. Among the chromatographic conditions examined were mobile phase pH, buffer type, buffer concentration, gradient rate, and column temperature. Significant differences in the chromatographic behavior (elution pattern, peak shape and selectivity) of the test samples are discussed in regard to the column type and the chromatographic conditions.

  18. An experimental study on inelastic behavior for exposed-type steel column bases under three-dimensional loadings

    Energy Technology Data Exchange (ETDEWEB)

    Choi, Jae Hyouk [Chosun University, Gwangju (Korea, Republic of); Choi, Yeol [Kyungpook National University, Daegu (Korea, Republic of)

    2013-03-15

    Considerable damage occurred to steel structures during the Kobe earthquake in Japan. Numerous exposed-type column bases failed in several consistent patterns caused by brittle base plate fracture, excessive anchor bolt elongation, unexpected early anchor bolt failure, and inferior construction work. An exposed-type column base receives axial force and biaxial bending when receiving an arbitrary multidirectional earthquake motion. Up to now, numerous researchers have examined methods to identify their stiffness and strength, but those studies have heretofore been restricted to in-plane behaviors. Therefore, it is necessary to clarify the inelastic behavior of exposed type steel column bases under biaxial lateral loading and axially compressive-tensile loading, which is a closer simulation of the real seismic excitation. In this study, exposed type steel column bases with different failure types, anchor bolt yielding and base plate yielding, are tested under different loading programs, then moment resisting mechanisms and failure modes are investigated.

  19. An experimental study on inelastic behavior for exposed-type steel column bases under three-dimensional loadings

    International Nuclear Information System (INIS)

    Choi, Jae Hyouk; Choi, Yeol

    2013-01-01

    Considerable damage occurred to steel structures during the Kobe earthquake in Japan. Numerous exposed-type column bases failed in several consistent patterns caused by brittle base plate fracture, excessive anchor bolt elongation, unexpected early anchor bolt failure, and inferior construction work. An exposed-type column base receives axial force and biaxial bending when receiving an arbitrary multidirectional earthquake motion. Up to now, numerous researchers have examined methods to identify their stiffness and strength, but those studies have heretofore been restricted to in-plane behaviors. Therefore, it is necessary to clarify the inelastic behavior of exposed type steel column bases under biaxial lateral loading and axially compressive-tensile loading, which is a closer simulation of the real seismic excitation. In this study, exposed type steel column bases with different failure types, anchor bolt yielding and base plate yielding, are tested under different loading programs, then moment resisting mechanisms and failure modes are investigated

  20. NONLINEAR FINITE ELEMENT ANALYSIS OF NONSEISMICALLY DETAILED INTERIOR RC BEAM-COLUMN CONNECTION UNDER REVERSED CYCLIC LOAD

    Directory of Open Access Journals (Sweden)

    Teeraphot Supaviriyakit

    2017-11-01

    Full Text Available This paper presents a nonlinear finite element analysis of non-seismically detailed RC beam column connections under reversed cyclic load. The test of half-scale nonductile reinforced concrete beam-column joints was conducted. The tested specimens represented those of the actual mid-rise reinforced concrete frame buildings designed according to the non-seismic provisions of the ACI building code.  The test results show that specimens representing small and medium column tributary area failed in brittle joint shear while specimen representing large column tributary area failed by ductile flexure though no ductile reinforcement details were provided. The nonlinear finite element analysis was applied to simulate the behavior of the specimens. The finite element analysis employs the smeared crack approach for modeling beam, column and joint, and employs the discrete crack approach for modeling the interface between beam and joint face. The nonlinear constitutive models of reinforced concrete elements consist of coupled tension-compression model to model normal force orthogonal and parallel to the crack and shear transfer model to capture the shear sliding mechanism. The FEM shows good comparison with test results in terms of load-displacement relations, hysteretic loops, cracking process and the failure mode of the tested specimens. The finite element analysis clarifies that the joint shear failure was caused by the collapse of principal diagonal concrete strut.

  1. Selective detachment process in column flotation froth

    Energy Technology Data Exchange (ETDEWEB)

    Honaker, R.Q.; Ozsever, A.V.; Parekh, B.K. [University of Kentucky, Lexington, KY (United States). Dept. of Mining Engineering

    2006-05-15

    The selectivity in flotation columns involving the separation of particles of varying degrees of floatability is based on differential flotation rates in the collection zone, reflux action between the froth and collection zones, and differential detachment rates in the froth zone. Using well-known theoretical models describing the separation process and experimental data, froth zone and overall flotation recovery values were quantified for particles in an anthracite coal that have a wide range of floatability potential. For highly floatable particles, froth recovery had a very minimal impact on overall recovery while the recovery of weakly floatable material was decreased substantially by reductions in froth recovery values. In addition, under carrying-capacity limiting conditions, selectivity was enhanced by the preferential detachment of the weakly floatable material. Based on this concept, highly floatable material was added directly into the froth zone when treating the anthracite coal. The enriched froth phase reduced the product ash content of the anthracite product by five absolute percentage points while maintaining a constant recovery value.

  2. GPR Diagnostics of columns in archaeological contexts

    Science.gov (United States)

    Soldovieri, Francesco; Masini, Nicola; Persico, Raffaele; Catapano, Ilaria

    2017-04-01

    In the last decade the use of Ground Penetrating radar (GPR) applied to cultural heritage has been strongly increasing thanks to both technological development of sensors and softwares for data processing and cultural reasons such as the increasing awareness of conservators and archaeologist of the benefits of this method in terms of reduction of costs and time and risk associated with restoration works. This made GPR a mature technique for investigating different types of works of art and building elements of historical interest, including masonry structures, frescoes, mosaics [1-3], in the context of scientific projects, decision support activities aimed at the diagnosis of decay pathologies, and educational activities. One of the most complex building elements to be investigated by GPR are the columns both for the geometry of the object and for the several expected features to be detected including fractures, dishomogeneities and metallic connection elements. The work deals with the Ground Penetrating Radar diagnostic surveys at the prestigious archaeological site of Pompei. In particular, GPR surveys were carried out in two different areas, Palestra Grande and Tempio di Giove. The first campaign was carried out also as educational activity of the "International School "GEOPHYSICS AND REMOTE SENSING FOR ARCHAEOLOGY". The School aimed at giving the opportunity to scholars, PhD students, researchers and specialists in Geophysics, Remote Sensing and Archaeology to deepen their knowledge and expertise with geophysical and remote sensing techniques for archaeology and cultural heritage documentation and management. This survey was carried on two kinds of columns, with circular and rectangular section in order to detect possible hidden defects affecting their integrity. The second survey was carried out at Tempio di Giove, on request of the Soprintendenza Pompei, in order to gain information about the presence of reinforcement structures, which may be put inside the

  3. Evaluation of an ambient air sampling system for tritium (as tritiated water vapor) using silica gel adsorbent columns

    International Nuclear Information System (INIS)

    Patton, G.W.; Cooper, A.T.; Tinker, M.R.

    1995-08-01

    Ambient air samples for tritium analysis (as the tritiated water vapor [HTO] content of atmospheric moisture) are collected for the Hanford Site Surface Environmental Surveillance Project (SESP) using the solid adsorbent silica gel. The silica gel has a moisture sensitive indicator which allows for visual observation of moisture movement through a column. Despite using an established method, some silica gel columns showed a complete change in the color indicator for summertime samples suggesting that breakthrough had occurred; thus a series of tests was conducted on the sampling system in an environmental chamber. The purpose of this study was to determine the maximum practical sampling volume and overall collection efficiency for water vapor collected on silica gel columns. Another purpose was to demonstrate the use of an impinger-based system to load water vapor onto silica gel columns to provide realistic analytical spikes and blanks for the Hanford Site SESP. Breakthrough volumes (V b ) were measured and the chromatographic efficiency (expressed as the number of theoretical plates [N]) was calculated for a range of environmental conditions. Tests involved visual observations of the change in the silica gel's color indicator as a moist air stream was drawn through the column, measurement of the amount of a tritium tracer retained and then recovered from the silica gel, and gravimetric analysis for silica gel columns exposed in the environmental chamber

  4. Behaviour of fibre reinforced polymer confined reinforced concrete columns under fire condition

    Science.gov (United States)

    Chowdhury, Ershad Ullah

    In recent years, fibre reinforced polymer (FRP) materials have demonstrated enormous potential as materials for repairing and retrofitting concrete bridges that have deteriorated from factors such as electro-chemical corrosion and increased load requirements. However, concerns associated with fire remain an obstacle to applications of FRP materials in buildings and parking garages due to FRP's sensitivity to high temperatures as compared with other structural materials and to limited knowledge on their thermal and mechanical behaviour in fire. This thesis presents results from an ongoing study on the fire performance of FRP materials, fire insulation materials and systems, and FRP wrapped reinforced concrete columns. The overall goal of the study is to understand the fire behaviour of FRP materials and FRP strengthened concrete columns and ultimately, provide rational fire safety design recommendations and guidelines for FRP strengthened concrete columns. A combined experimental and numerical investigation was conducted to achieve the goals of this research study. The experimental work consisted of both small-scale FRP material testing at elevated temperatures and full-scale fire tests on FRP strengthened columns. A numerical model was developed to simulate the behaviour of unwrapped reinforced concrete and FRP strengthened reinforced concrete square or rectangular columns in fire. After validating the numerical model against test data available in literature, it was determined that the numerical model can be used to analyze the behaviour of concrete axial compressive members in fire. Results from this study also demonstrated that although FRP materials experience considerable loss of their mechanical and bond properties at temperatures somewhat below the glass transition temperature of the resin matrix, externally-bonded FRP can be used in strengthening concrete structural members in buildings, if appropriate supplemental fire protection system is provided over

  5. Test facilities for HTR, (2)

    International Nuclear Information System (INIS)

    Ishizuka, Hiroshi; Hayakawa, Hitoshi; Miki, Toshiya.

    1981-01-01

    The core of the multi-purpose high temperature gas-cooled experimental reactor is a circular column as a whole, in which the columns of stacked graphite blocks of hexagonal prism are arranged. The blocks in a column are doweled so as not to move horizontally, but adjacent columns vibrate while colliding mutually at the time of an earthquake because there is a gap between them. For the purpose to know the vibrating characteristics of a column surrounded by gap, Fuji Electric Co., Ltd., carried out the experiment. The tested column, the testing setup and the test result are reported. The distribution of flow rate in the core must be clarified, and the design data must be established early for confirming the feasibility of core design. The core structure tester was installed in Japan Atomic Energy Research Institute. The 1/2.75 scale model of the reactor bed was used, and the sealing performance of the block assemblies was tested. The sealing tester is related also to the distribution of flow rate in the core, and the basic performance of seal elements and the cross flow in fuel blocks were tested. The one-column tester and the seal element/two-column tester, the piping unit and the blower filter unit compose this tester. (Kako, I.)

  6. Water column methanotrophy controlled by a rapid oceanographic switch

    NARCIS (Netherlands)

    Steinle, L.; Graves, C.A.; Treude, T.; Ferré, B.; Biastoch, A.; Bussmann, I.; Berndt, C.; Krastel, S.; James, R.H.; Behrens, E.; Böning, C.W.; Greinert, J.; Sapart, C.-J.; Scheinert, M.; Sommer, S.; Lehmann, M.F.; Niemann, H.

    2015-01-01

    From the seabed to the water column, where it may be consumed by aerobic methanotrophic bacteria. The size and activity of methanotrophic communities, which determine the amount of methane consumed in the water column,are thought to be mainly controlled by nutrient and redoxdynamics3–7. Here, we

  7. Alpha-contained laboratory scale pulse column facility for SRL

    International Nuclear Information System (INIS)

    Reif, D.J.; Cadieux, J.R.; Fauth, D.J.; Thompson, M.C.

    1980-01-01

    For studying solvent extraction processes, a laboratory-sized pulse column facility was constructed at the Savannah River Laboratory. This facility, in conjunction with existing miniature mixer-settler equipment and the centrifugal contactor facility currently under construction at SRL, provides capability for cross comparison of solvent extraction technology. This presentation describes the design and applications of the Pulse Column Facility at SRL

  8. Hydrodynamic chromatography of polystyrene microparticles in micropillar array columns

    NARCIS (Netherlands)

    Op de Beeck, Jeff; de Malsche, Wim; Vangelooven, Joris; Gardeniers, Johannes G.E.; Desmet, Gert

    2010-01-01

    We report on the possibility to perform HDC in micropillar array columns and the potential advantages of such a system. The HDC performance of a pillar array column with pillar diameter = 5 μm and an interpillar distance of 2.5 μm has been characterized using both a low MW tracer (FITC) and

  9. Simulators of tray distillation columns as tools for interpreting ...

    African Journals Online (AJOL)

    ... at 0.05 m intervals were determined from top to the bottom of simulators of tray distillation columns exposed to 20 mCi of 137 Cs. Signals generated from the simulators were identical with the experimental signals obtained from the Stabilizer Column of the crude oil distillation unit at the Tema Oil Refinery Ghana Limited.

  10. Dynamic stability of a lightly damped column trapped by a ...

    African Journals Online (AJOL)

    In this paper we initiate an analytical approach for determining the dynamic buckling load of a finite viscously damped column acted upon by a harmonically slowly varying explicitly time dependent load. The viscous damping is considered light and the column rests on an elastic foundation that produces a nonlinear ...

  11. Localized giant cell tumors in the spinal column radiologic presentation

    International Nuclear Information System (INIS)

    Fernandez Echeverria, M.A.; Parra Blanco, J.A.; Pagola Serrano, M.A.; Mellado Santos, J.M.; Bueno Lopez, J.; Gonzalez Tutor, A.

    1994-01-01

    Given the uncommonness of the location of giant cell tumors (GCT) in the spinal column and the limited number of studies published, we present a case of GCT located in the spinal column, which involved both vertebral bodies and partially destroyed the adjacent rib. (Author)

  12. Monitoring aged reversed-phase high performance liquid chromatography columns

    NARCIS (Netherlands)

    Bolck, A; Smilde, AK; Bruins, CHP

    1999-01-01

    In this paper, a new approach for the quality assessment of routinely used reversed-phase high performance liquid chromatography columns is presented. A used column is not directly considered deteriorated when changes in retention occur. If attention is paid to the type and magnitude of the changes,

  13. Retrofit of distillation columns in biodiesel production plants

    International Nuclear Information System (INIS)

    Nguyen, Nghi; Demirel, Yasar

    2010-01-01

    Column grand composite curves and the exergy loss profiles produced by the Column-Targeting Tool of the Aspen Plus simulator are used to assess the performance of the existing distillation columns, and reduce the costs of operation by appropriate retrofits in a biodiesel production plant. Effectiveness of the retrofits is assessed by means of thermodynamics and economic improvements. We have considered a biodiesel plant utilizing three distillation columns to purify biodiesel (fatty acid methyl ester) and byproduct glycerol as well as reduce the waste. The assessments of the base case simulation have indicated the need for modifications for the distillation columns. For column T202, the retrofits consisting of a feed preheating and reflux ratio modification have reduced the total exergy loss by 47%, while T301 and T302 columns exergy losses decreased by 61% and 52%, respectively. After the retrofits, the overall exergy loss for the three columns has decreased from 7491.86 kW to 3627.97 kW. The retrofits required a fixed capital cost of approximately $239,900 and saved approximately $1,900,000/year worth of electricity. The retrofits have reduced the consumption of energy considerably, and leaded to a more environmentally friendly operation for the biodiesel plant considered.

  14. Dynamics and Control of Distillation Columns - A Critical Survey

    Directory of Open Access Journals (Sweden)

    Sigurd Skogestad

    1997-07-01

    Full Text Available Distillation column dynamics and control have been viewed by many as a very mature or even dead field. However, as is discussed in this paper significant new results have appeared over the last 5-10 years. These results include multiple steady states and instability in simple columns with ideal thermodynamics (which was believed to be impossible, the understanding of the difference between various control configurations and the systematic transformation between these, the feasibility of using the distillate-bottom structure, for control (which was believed to be impossible, the importance of flow dynamics for control studies, the fundamental problems in identifying models from open-loops responses, the use of simple regression estimators to estimate composition from temperatures, and an improved general understanding of the dynamic behavior of distillation columns which includes a better understanding of the fundamental difference between internal and external flow, simple formulas for estimating the dominant time constant, and a derivation of the linearizing effect of logarithmic transformations. These issues apply to all columns, even for ideal mixtures and simple columns with only two products. In addition, there have been significant advances for cases with complex thermodynamics and complex column configurations. These include the behavior and control of azeotropic distillation columns, and the possible complex dynamics of nonideal mixtures and of interlinked columns. However, both for the simple and more complex cases there are still a number of areas where further research is needed.

  15. Gas chromatographic column for the Viking 1975 molecular analysis experiment

    Science.gov (United States)

    Novotny, M.; Hayes, J. M.; Bruner, F.; Simmonds, P. G.

    1975-01-01

    A gas chromatographic column has been developed for use in the remote analysis of the Martian surface. The column, which utilizes a liquid-modified organic adsorbent (Tenax) as the stationary phase, provides efficient transmission and resolution of nanogram quantities of organic materials in the presence of millionfold excesses of water and carbon dioxide.

  16. A Modeling Framework for Conventional and Heat Integrated Distillation Columns

    DEFF Research Database (Denmark)

    Bisgaard, Thomas; Huusom, Jakob Kjøbsted; Abildskov, Jens

    2013-01-01

    In this paper, a generic, modular model framework for describing fluid separation by distillation is presented. At present, the framework is able to describe a conventional distillation column and a heat-integrated distillation column, but due to a modular structure the database can be further...

  17. Graph Modelling Approach: Application to a Distillation Column

    DEFF Research Database (Denmark)

    Hovelaque, V.; Commault, C.; Bahar, Mehrdad

    1997-01-01

    Introduction, structured systems and digraphs, distillation column model, generic input-output decoupling problem, generic disturbance rejection problem, concluding remarks.......Introduction, structured systems and digraphs, distillation column model, generic input-output decoupling problem, generic disturbance rejection problem, concluding remarks....

  18. HEAT TRANSFER ANALYSIS FOR FIXED CST AND RF COLUMNS

    International Nuclear Information System (INIS)

    Lee, S

    2007-01-01

    In support of a small column ion exchange (SCIX) process for the Savannah River Site waste processing program, transient and steady state two-dimensional heat transfer models have been constructed for columns loaded with cesium-saturated crystalline silicotitanate (CST) or spherical Resorcinol-Formaldehyde (RF) beads and 6 molar sodium tank waste supernate. Radiolytic decay of sorbed cesium results in heat generation within the columns. The models consider conductive heat transfer only with no convective cooling and no process flow within the columns (assumed column geometry: 27.375 in ID with a 6.625 in OD center-line cooling pipe). Heat transfer at the column walls was assumed to occur by natural convection cooling with 35 C air. A number of modeling calculations were performed using this computational heat transfer approach. Minimal additional calculations were also conducted to predict temperature increases expected for salt solution processed through columns of various heights at the slowest expected operational flow rate of 5 gpm. Results for the bounding model with no process flow and no active cooling indicate that the time required to reach the boiling point of ∼130 C for a CST-salt solution mixture containing 257 Ci/liter of Cs-137 heat source (maximum expected loading for SCIX applications) at 35 C initial temperature is about 6 days. Modeling results for a column actively cooled with external wall jackets and the internal coolant pipe (inlet coolant water temperature: 25 C) indicate that the CST column can be maintained non-boiling under these conditions indefinitely. The results also show that the maximum temperature of an RF-salt solution column containing 133 Ci/liter of Cs-137 (maximum expected loading) will never reach boiling under any conditions (maximum predicted temperature without cooling: 88 C). The results indicate that a 6-in cooling pipe at the center of the column provides the most effective cooling mechanism for reducing the maximum

  19. Gain-scheduled {{\\mathscr{H}}}_{\\infty } buckling control of a circular beam-column subject to time-varying axial loads

    Science.gov (United States)

    Schaeffner, Maximilian; Platz, Roland

    2018-06-01

    For slender beam-columns loaded by axial compressive forces, active buckling control provides a possibility to increase the maximum bearable axial load above that of a purely passive structure. In this paper, an approach for gain-scheduled {{\\mathscr{H}}}∞ buckling control of a slender beam-column with circular cross-section subject to time-varying axial loads is investigated experimentally. Piezo-elastic supports with integrated piezoelectric stack actuators at the beam-column ends allow an active stabilization in arbitrary lateral directions. The axial loads on the beam-column influence its lateral dynamic behavior and, eventually, cause the beam-column to buckle. A reduced modal model of the beam-column subject to axial loads including the dynamics of the electrical components is set up and calibrated with experimental data. Particularly, the linear parameter-varying open-loop plant is used to design a model-based gain-scheduled {{\\mathscr{H}}}∞ buckling control that is implemented in an experimental test setup. The beam-column is loaded by ramp- and step-shaped time-varying axial compressive loads that result in a lateral deformation of the beam-column due to imperfections, such as predeformation, eccentric loading or clamping moments. The lateral deformations and the maximum bearable loads of the beam-column are analyzed and compared for the beam-column with and without gain-scheduled {{\\mathscr{H}}}∞ buckling control or, respectively, active and passive configuration. With the proposed gain-scheduled {{\\mathscr{H}}}∞ buckling control it is possible to increase the maximum bearable load of the active beam-column by 19% for ramp-shaped axial loads and to significantly reduce the beam-column deformations for step-shaped axial loads compared to the passive structure.

  20. Determination of 3-hydroxypropylmercapturic acid in urine by three column-switching high-performance liquid chromatography with electrochemical detection using a diamond electrode.

    Science.gov (United States)

    Higashi, Kyohei; Shibasaki, Mana; Kuni, Kyoshiro; Uemura, Takeshi; Waragai, Masaaki; Uemura, Kenichi; Igarashi, Kazuei; Toida, Toshihiko

    2017-09-29

    A three column-switching high-performance liquid chromatography (HPLC) using an electrochemical detector (ECD) equipped with a diamond electrode was established to determine 3-hydroxypropylmercapturic acid (3-HPMA) in urine. An extracted urine sample was consecutively fractionated using a strong anion-exchange column (first column) and a C8 column (second column) via a switching valve before application on an Octa Decyl Silyl (ODS) column (third column), followed by ECD analysis. The% recovery of 3-HPMA standard throughout the three-column process and limit of detection (LOD) were 94±1% and 0.1pmol, respectively. A solid phase extraction step is required for the sensitive analysis of 3-HPMA in urine by column-switching HPLC-ECD despite a decreased% recovery (55%) of urine sample spiked with 100pmol of 3-HPMA. To test the utility of our column-switching HPLC-ECD method, 3-HPMA levels of 27 urine samples were determined, and the correlation between HPLC-ECD and LC-Electrospray ionization (ESI)-MS/MS method was examined. As a result, the median values of μmol 3-HPMA/g Creatinine (Cre) in urine obtained by column-switching HPLC-ECD and LC-MS/MS were 2.19±2.12μmol/g Cre and 2.13±3.38μmol/g Cre, respectively, and the calibration curve (y=1.5171x-1.007) exhibited good linearity within a defined range (r 2 =0.907). These results indicate that the combination of column-switching HPLC and ECD is a powerful tool for the specific, reliable detection of 3-HPMA in urine. Copyright © 2017 Elsevier B.V. All rights reserved.

  1. Characterization of retentivity of reversed phase liquid chromatography columns.

    Science.gov (United States)

    Ying, P T; Dorsey, J G

    1991-03-01

    There are dozens of commercially available reversed phase columns, most marketed as C-8 or C-18 materials, but with no useful way of classifying their retentivity. A useful way of ranking these columns in terms of column "strength" or retentivity is presented. The method utilizes a value for ln k'(w), the estimated retention of a solute from a mobile phase of 100% water, and the slope of the plot of ln k' vsE(T)(30), the solvent polarity. The method is validated with 26 solutes varying in ln k'(w) from about 2 to over 20, on 14 different reversed phase columns. In agreement with previous work, it is found that the phase volume ratio of the column is the most important parameter in determining retentivity. It is strongly suggested that manufacturers adopt a uniform method of calculating this value and that it be made available in advertising, rather than the uninterpretable "% carbon".

  2. A Modelling Framework for Conventional and Heat Integrated Distillation Columns

    DEFF Research Database (Denmark)

    Bisgaard, Thomas; Huusom, Jakob Kjøbsted; Abildskov, Jens

    2013-01-01

    of hydrocarbons such as separations of equimolar mixtures of benzene/toluene or propane/propene described by simple models, a generic, modular, model framework is presented in this work. At present, the framework is able to describe a conventional distillation column, a mechanical vapor recompression column......Diabatic operation of distillation columns can lead to signicant reductions in energy utilization and operation cost compared to conventional (adiabatic) distillation columns, at an expense of an increased complexity of design and operation. The earliest diabatic distillation conguration dates back...... to the late 70s, and various dierent congurations have appeared since. However, at present, no full-scale diabatic distillation columns are currently operating in the industry. Current studies related to alternative distillation congurations report very dierent gures for potential energy savings which...

  3. INNOVATIVE MIOR PROCESS UTILIZING INDIGENOUS RESERVOIR CONSTITUENTS

    Energy Technology Data Exchange (ETDEWEB)

    D.O. Hitzman; S.A. Bailey

    2000-01-01

    This research program is directed at improving the knowledge of reservoir ecology and developing practical microbial solutions for improving oil production. The goal is to identify indigenous microbial populations which can produce beneficial metabolic products and develop a methodology to stimulate those select microbes with inorganic nutrient amendments to increase oil recovery.This microbial technology has the capability of producing multiple oil releasing agents. The potential of the system will be illustrated and demonstrated by the example of biopolymer production on oil recovery. Research has begun on the program and experimental laboratory work is underway. Polymer-producing cultures have been isolated from produced water samples and initially characterized. Concurrently, a microcosm scale sand-packed column has been designed and developed for testing cultures of interest, including polymer-producing strains. In research that is planned to begin in future work, comparative laboratory studies demonstrating in situ production of microbial products as oil recovery agents will be conducted in sand pack and cores with synthetic and natural field waters at concentrations, flooding rates, and with cultures and conditions representative of oil reservoirs.

  4. Cost effectiveness of detritiating water with resin columns

    International Nuclear Information System (INIS)

    Drake, R.H.; Williams, D.S.

    1997-10-01

    There are technologies in use for cleaning up concentrated tritiated process water. These are not cost effective for tritiated water with low concentrations of tritium. There are currently no cost-effective technologies for cleaning up low-tritium-concentration tritiated water, such as most tritiated groundwater, spent fuel storage basin water, or underground storage tank water. Resin removal of tritium from tritiated water at low concentrations (near the order of magnitude of drinking water standard maximums) is being tested on TA-SO (Los Alamos National Laboratory's Liquid Radioactive Waste Treatment Facility) waste streams. There are good theoretical and test indications that this may be a technologically effective means of removing tritium from tritiated water. Because of likely engineering design similarity, it is reasonable to anticipate that a resin column system's costs will be similar to some common commercial water treatment systems. Thus, the potential cost effectiveness of a resin treatment system offers hope for treating tritiated water at affordable costs. The TA-50 resin treatment cost projection of $18 per 1,000 gallons is within the same order of magnitude as cost data for typical commercial groundwater cleanup projects. The prospective Los Alamos National Laboratory (LANL) resin treatment system at $18 per 1,000 gallons appears to have a likely cost advantage of at least an order of magnitude over the competing, developmental, water detritiation technologies

  5. A bridge column with superelastic NiTi SMA and replaceable rubber hinge for earthquake damage mitigation

    Science.gov (United States)

    Varela, Sebastian; ‘Saiid' Saiidi, M.

    2016-07-01

    This paper reports a unique concept for resilient bridge columns that can undergo intense earthquake loading and remain functional with minimal damage and residual drift. In this concept, the column is designed so that its components can be easily disassembled and reassembled to facilitate material recycling and component reuse. This is meant to foster sustainability of bridge systems while minimizing monetary losses from earthquakes. Self-centering and energy dissipation in the column were provided by unbonded superelastic nickel-titanium (NiTi) shape memory alloy bars placed inside a plastic hinge element made of rubber. This replaceable plastic hinge was in turn attached to a concrete-filled carbon fiber-reinforced polymer tube and a precast concrete footing that were designed to behave elastically. The proposed concept was evaluated experimentally by testing a ¼-scale column model under simulated near-fault earthquake motions on a shake table. After testing, the model was disassembled, reassembled and tested again. The seismic performance of the reassembled model was found to be comparable to that of the ‘virgin’ model. A relatively simple computational model of the column tested that was developed in OpenSees was able to match some of the key experimental response parameters.

  6. Column-by-column compositional mapping by Z-contrast imaging

    Energy Technology Data Exchange (ETDEWEB)

    Molina, S.I. [Departamento de Ciencia de los Materiales e I.M. y Q.I., Facultad de Ciencias, Universidad de Cadiz, Campus Rio San Pedro, s/n, 11510 Puerto Real, Cadiz (Spain)], E-mail: sergio.molina@uca.es; Sales, D.L. [Departamento de Ciencia de los Materiales e I.M. y Q.I., Facultad de Ciencias, Universidad de Cadiz, Campus Rio San Pedro, s/n, 11510 Puerto Real, Cadiz (Spain); Galindo, P.L. [Departamento de Lenguajes y Sistemas Informaticos, CASEM, Universidad de Cadiz, Campus Rio San Pedro, s/n, 11510 Puerto Real, Cadiz (Spain); Fuster, D.; Gonzalez, Y.; Alen, B.; Gonzalez, L. [Instituto de Microelectronica de Madrid (CNM, CSIC), Isaac Newton 8, 28760 Tres Cantos, Madrid (Spain); Varela, M.; Pennycook, S.J. [Materials Science and Technology Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831 (United States)

    2009-01-15

    A phenomenological method is developed to determine the composition of materials, with atomic column resolution, by analysis of integrated intensities of aberration-corrected Z-contrast scanning transmission electron microscopy images. The method is exemplified for InAs{sub x}P{sub 1-x} alloys using epitaxial thin films with calibrated compositions as standards. Using this approach we have determined the composition of the two-dimensional wetting layer formed between self-assembled InAs quantum wires on InP(0 0 1) substrates.

  7. Shrinkage stress in concrete under dry-wet cycles: an example with concrete column

    Science.gov (United States)

    Gao, Yuan; Zhang, Jun; Luosun, Yiming

    2014-02-01

    This paper focuses on the simulation of shrinkage stress in concrete structures under dry-wet environments. In the modeling, an integrative model for autogenous and drying shrinkage predictions of concrete under dry-wet cycles is introduced first. Second, a model taking both cement hydration and moisture diffusion into account synchronously is used to calculate the distribution of interior humidity in concrete. Using the above two models, the distributions of shrinkage strain and stress in concrete columns made by normal and high strength concrete respectively under dry-wet cycles are calculated. The model results show that shrinkage gradient along the radial direction of the column from the center to outer surface increases with age as the outer circumference suffers to dry. The maximum and minimum shrinkage occur at the outer surface and the center of the column, respectively, under drying condition. As wetting starts, the shrinkage strain decreases with increase of interior humidity. The closer to the wetting face, the higher the humidity and the lower the shrinkage strain, as well as the lower the shrinkage stress. As results of the dry-wet cycles acting on the outer circumference of the column, cyclic stress status is developed within the area close to the outer surface of the column. The depth of the influencing zone of dry-wet cyclic action is influenced by concrete strength and dry-wet regime. For low strength concrete, relatively deeper influencing zone is expected compared with that of high strength concrete. The models are verified by concrete-steel composite ring tests and a good agreement between model and test results is found.

  8. Comparison Study of Axial Behavior of RPC-CFRP Short Columns

    Directory of Open Access Journals (Sweden)

    Taghreed Khaleefa Mohammed Ali

    2015-05-01

    Full Text Available In this paper, the axial behaviors of reactive powder     concrete (RPC short  columns confined with carbon fiber reinforced polymer (CFRP were   investigated. All the specimens have square cross section of 100 mm × 100   mm and length of 400 mm with aspect ratio 4. The experimental work consists   of three groups. The first group consists of six specimens of RPC with 2%  micro steel fiber, without ordinary reinforcing steel and confining by zero, one and two layer of CFRP respectively. The second group consists of six    specimens of RPC with 2% micro steel fiber and minimum ordinary reinforcing  steel and confining by zero, one and two layers of CFRP respectively. The third  group consists of four specimens of RPC without micro steel fiber and ordinary  reinforcing steel and confining by one and two layers of CFRP respectively.  Experimental data for strength, longitudinal and lateral displacement and  failure mode were obtained for each test. The toughness (area under the curve  for each test was obtained by using numerical integration. The RPC columns confined with CFRP showed stiffer behavior compared with RPC columns without CFRP. The ultimate load of the RPC columns with 2% micro steel  fiber + two layers of CFRP + minimum ordinary reinforcement were more than that of the RPC columns with 2% micro steel fiber + minimum ordinary   reinforcement and without CFRP by about 1.333.

  9. Study on two phase flow characteristics in annular pulsed extraction column with different ratio of annular width to column diameter

    International Nuclear Information System (INIS)

    Qin Wei; Dai Youyuan; Wang Jiading

    1994-01-01

    Annular pulsed extraction column can successfully provide large throughput and can be made critically safe for fuel reprocessing. This investigation is to study the two phase flow characteristics in annular pulsed extraction column with four different annular width. 30% TBP (in kerosene)-water is used (water as continuous phase). Results show that modified Pratt correlation is valid under the experimental operation conditions for the annular pulsed extraction column. The characteristic velocity U K decreased with the increase of energy input and increased with the increase of the ratio of annular width to column diameter. Flooding velocity correlation is suggested. The deviation of the calculated values from the experimental data is within +20% for four annular width in a pulsed extraction column

  10. Consolidation Theory for a Stone Column Composite Foundation under Multistage Loading

    Directory of Open Access Journals (Sweden)

    Shenggen Huang

    2016-01-01

    Full Text Available The consolidation theories considering instant load cannot fully reveal the consolidation mechanism of a stone column composite foundation used in the expressway embankments due to the time effect of loading; that is, the expressway embankments are often constructed in several stages for a long time. Meanwhile, owing to the special property that the pile-soil stress ratio is larger than 1, the consolidation theory for sand drain well foundation cannot be used directly in the consolidation analysis of stone column composite foundation. Based on the principle that the vertical load applied on the composite foundation is shared by the stone column and the surrounding soil, the governing solutions for the stone column composite foundation under a multistage load are established. By virtue of the separation of variables, the corresponding solutions of degree of consolidation for loading stage and maintaining load stage are derived separately. According to the Carrillo theorem, the solution for the average total degree of consolidation of entire composite foundation is also obtained. Finally, the reasonableness of the present solution has been verified by comparing the consolidation curve calculated by the present solution with that measured by site test.

  11. Development Of ABEC Column For Separation Of Tc-99 From Northstar Dissolved Target Solution

    Energy Technology Data Exchange (ETDEWEB)

    Stepinski, Dominique C. [Argonne National Lab. (ANL), Argonne, IL (United States); Bennett, Megan E. [Argonne National Lab. (ANL), Argonne, IL (United States); Naik, Seema R. [Argonne National Lab. (ANL), Argonne, IL (United States); ling, lei [Argonne National Lab. (ANL), Argonne, IL (United States); Wang, N-H. Linda [Argonne National Lab. (ANL), Argonne, IL (United States); Vandegrift, George F. [Argonne National Lab. (ANL), Argonne, IL (United States)

    2016-12-01

    Batch and column breakthrough experiments were performed to determine isotherms and mass-transfer parameters for adsorption of Tc on aqueous biphasic extraction chromatographic (ABEC) sorbent in two solutions: 200 g/L Mo, 5.1 M K+, 1 M OH-, and 0.1 M NO3- (Solution A) and 200 g/L Mo, 9.3 M K+, 5 M OH-, and 0.1 M NO3- (Solution B). Good agreement was found between the isotherm values obtained by batch and column breakthrough studies for both Solutions A and B. Potassium-pertechnetate intra-particle diffusivity on ABEC resin was estimated by VERSE simulations, and good agreement was found among a series of column-breakthrough experiments at varying flow velocities, column sizes, and technetium concentrations. However, testing of 10 cc cartridges provided by NorthStar with Solutions A and B did not give satisfactory results, as significant Tc breakthrough was observed and ABEC cartridge performance varied widely among experiments. These different experimental results are believed to be due to inconsistent preparation of the ABEC resin prior to packing and/or inconsistent packing.

  12. Residual diesel measurement in sand columns after surfactant/alcohol washing

    International Nuclear Information System (INIS)

    Martel, R.; Gelinas, P.J.

    1996-01-01

    A new simple gravimetric technique has been designed to determine residual oil saturation of complex hydrocarbon mixtures (e.g., diesel) in sand column experiments because reliable methods are lacking. The He/N 2 technique is based on drying of sand columns by circulating helium gas to drag oil droplets in a cold trap (liquid nitrogen). With this technique, residual diesel measurement can be performed easily immediately after alcohol/surfactant washing and in the same lab. For high residual diesel content in Ottawa sand (25 to 30 g/kg), the technique is much more accurate (± 2% or 600 mg/kg) than the standard analytical methods for the determination of mineral oil and grease. The average relative error on partial diesel dissolution in sand column estimated after alcohol/surfactant flooding (residual saturation of 10 to 15 g/kg) is as low as 5%. The precision of the He/N 2 technique is adequate to compare relative efficiency of washing solutions when partial extraction of residual oil in Ottawa sand columns is performed. However, this technique is not adapted for determination of traces of oil in sediment or for environmental control of contaminated soils. Each diesel determination by the He/N 2 technique costs less than $8 in chemical products (helium and liquid nitrogen). A simple laboratory drying setup can be built for less than $400 which makes this technique valuable for diesel analyses when a large number of tests are required

  13. Blind column selection protocol for two-dimensional high performance liquid chromatography.

    Science.gov (United States)

    Burns, Niki K; Andrighetto, Luke M; Conlan, Xavier A; Purcell, Stuart D; Barnett, Neil W; Denning, Jacquie; Francis, Paul S; Stevenson, Paul G

    2016-07-01

    The selection of two orthogonal columns for two-dimensional high performance liquid chromatography (LC×LC) separation of natural product extracts can be a labour intensive and time consuming process and in many cases is an entirely trial-and-error approach. This paper introduces a blind optimisation method for column selection of a black box of constituent components. A data processing pipeline, created in the open source application OpenMS®, was developed to map the components within the mixture of equal mass across a library of HPLC columns; LC×LC separation space utilisation was compared by measuring the fractional surface coverage, fcoverage. It was found that for a test mixture from an opium poppy (Papaver somniferum) extract, the combination of diphenyl and C18 stationary phases provided a predicted fcoverage of 0.48 and was matched with an actual usage of 0.43. OpenMS®, in conjunction with algorithms designed in house, have allowed for a significantly quicker selection of two orthogonal columns, which have been optimised for a LC×LC separation of crude extractions of plant material. Copyright © 2016 Elsevier B.V. All rights reserved.

  14. Study on the dynamic holdup distribution of the pulsed extraction column

    International Nuclear Information System (INIS)

    Wang, S.; Chen, J.; Wu, Q.

    2013-01-01

    In the study, a CSTR cascade dynamic hydraulic model was developed to investigate the dynamic holdup distribution of the pulsed extraction column. It is assumed that the dynamic process of the dispersed phase holdup of pulsed extraction column has equal effects with the operational process of multiple cascade CSTRs. The process is consistent with the following assumptions: the holdups vary on different stages but maintain uniform on each stage; the changes of the hydraulic parameters have impact initially on the inlet of dispersed phase, and stability will be reached gradually through stage-by-stage blending. The model was tested and verified utilizing time domain response curves of the average holdup. Nearly 150 experiments were carried out with different capillary columns, various feed liquids, and diverse continuous phases and under different operation conditions. The regression curves developed by the model show a good consistency with the experimental results. After linking parameters of the model with operational conditions, the study further found that the parameters are only linearly correlated with pulse conditions and have nothing to do with flow rate for a specific pulsed extraction column. The accuracy of the model is measured by the average holdup, and the absolute error is ±0.01. The model can provide supports for the boundary studies on hydraulics and mass transfer by making simple and reliable prediction of the dynamic holdup distribution, with relatively less accessible hydraulic experimental data. (authors)

  15. Study on the dynamic holdup distribution of the pulsed extraction column

    Energy Technology Data Exchange (ETDEWEB)

    Wang, S.; Chen, J.; Wu, Q. [Tsinghua University, Beijing 100084 (China)

    2013-07-01

    In the study, a CSTR cascade dynamic hydraulic model was developed to investigate the dynamic holdup distribution of the pulsed extraction column. It is assumed that the dynamic process of the dispersed phase holdup of pulsed extraction column has equal effects with the operational process of multiple cascade CSTRs. The process is consistent with the following assumptions: the holdups vary on different stages but maintain uniform on each stage; the changes of the hydraulic parameters have impact initially on the inlet of dispersed phase, and stability will be reached gradually through stage-by-stage blending. The model was tested and verified utilizing time domain response curves of the average holdup. Nearly 150 experiments were carried out with different capillary columns, various feed liquids, and diverse continuous phases and under different operation conditions. The regression curves developed by the model show a good consistency with the experimental results. After linking parameters of the model with operational conditions, the study further found that the parameters are only linearly correlated with pulse conditions and have nothing to do with flow rate for a specific pulsed extraction column. The accuracy of the model is measured by the average holdup, and the absolute error is ±0.01. The model can provide supports for the boundary studies on hydraulics and mass transfer by making simple and reliable prediction of the dynamic holdup distribution, with relatively less accessible hydraulic experimental data. (authors)

  16. Design of fixed-bed ion exchange columns for wastewater treatment

    International Nuclear Information System (INIS)

    Robinson, S.M.; Arnold, W.D.; Byers, C.H.

    1990-01-01

    Oak Ridge National Laboratory plans to use chabazite zeolites for decontamination of process wastewater which contains ppb levels of Sr-90 and Cs-137. Treatability studies have indicated that chabazite zeolites have high selectivities and loadings for removal of trace amounts of Cs-137 and Sr-90 from wastewater containing high concentrations of calcium and magnesium. These studies also indicated that the efficiency of the zeolite system is dependent on the column design and operating conditions. Results from 20-mL, 566-L, and 3,760-L column tests indicated that the optimized design of full-scale columns could halve the generation rate of loaded zeolite. The corresponding annual waste disposal costs for loaded zeolite generated at the ORNL plant varied from $80,000 to $170,000 based on the present disposal charges of $1400/m 3 indicating that design of zeolite ion exchange systems for minimization of secondary waste is imperative. This report summarizes the results of study to model multicomponent ion-exchange columns. 7 refs., 10 figs., 5 tabs

  17. THE PERFORMANCE ANALYSIS OF A PACKED COLUMN : CALIBRATION OF AN ORIFICE

    Directory of Open Access Journals (Sweden)

    Aynur ŞENOL

    2003-01-01

    Full Text Available Investigations to develop data for this study were made using a pilot scale glass column of 9 cm inside diameter randomly filled to a depth of 1.90 cm with a Raschig type ring at a slightly modified geometry. The geometrical characteristics of packing are: the total area of a single particle ad = 2.3 cm2; specific area ap = 10.37 cm2/cm3; voidage ? = 0.545 m3/m3. The efficiency tests were run using trichloroethylene/n-heptane system under total reflux conditions. Using the modified versions of the Eckert flooding model and the Bravo effective area (ae approach, as well as the Onda wetted area (aw and individual mass transfer coefficient models, it has been attempted to estimate the packing efficiency theoretically. This article also deals with the design strategies attributed to a randomly packed column. Emphasis is mainly placed on the way to formulate an algorithm of designing a pilot scale column through the models being attributed to the film theory. Using the column dry pressure drop properties based on the air flowing it has been achieved a generalized flow rate approach for calibrating of an orifice through which the air passes.

  18. Design of fixed-bed ion exchange columns for wastewater treatment

    International Nuclear Information System (INIS)

    Robinson, S.M.; Arnold, W.D.; Byers, C.H.

    1990-01-01

    Oak Ridge National Laboratory plans to use chabazite zeolites for decontamination of process wastewater which contains ppb levels of Sr-90 and Cs-137. Treatability studies have indicated that chabazite zeolites have high selectivities and loadings for removal of trace amounts of Cs-137 and Sr-90 from wastewater containing high concentrations of calcium and magnesium. These studies also indicated that the efficiency of the zeolite system is dependent on the column design and operating conditions. Results from 20-mL, 566-L, and 3,760-L column tests indicated that the optimized design of full-scale columns could halve the generation rate of loaded zeolite. The corresponding annual waste disposal costs for loaded zeolite generated at the ORNL plant varied from $80,000 to $170,000 based on the present disposal charges of $1400/m 3 indicating that design of zeolite ion exchange systems for minimization of secondary waste is imperative. This report summarizes the results of a study to model multicomponent ion-exchange columns. 7 refs., 10 figs., 5 tabs

  19. Cervical column morphology and craniofacial profiles in monozygotic twins.

    Science.gov (United States)

    Sonnesen, Liselotte; Pallisgaard, Carsten; Kjaer, Inger

    2008-02-01

    Previous studies have described the relationships between cervical column morphology and craniofacial morphology. The aims of the present study were to describe cervical column morphology in 38 pairs of adult monozygotic (MZ) twins, and compare craniofacial morphology in twins with fusions with craniofacial morphology in twins without fusion. Visual assessment of cervical column morphology and cephalometric measurements of craniofacial morphology were performed on profile radiographs. In the cervical column, fusion between corpora of the second and third vertebrae was registered as fusion. In the twin group, 8 twin pairs had fusion of the cervical column in both individuals within the pair (sub-group A), 25 pairs had no fusions (subgroup B), and in 5 pairs, cervical column morphology was different within the pair (subgroup C), as one twin had fusion and the other did not. Comparison of craniofacial profiles showed a tendency to increased jaw retrognathia, larger cranial base angle, and larger mandibular inclination in subgroup A than in subgroup B. The same tendency was observed within subgroup C between the individual twins with fusion compared with those without fusion. These results confirm that cervical fusions and craniofacial morphology may be interrelated in twins when analysed on profile radiographs. The study also documents that differences in cervical column morphology can occur in individuals within a pair of MZ twins. It illustrates that differences in craniofacial morphology between individuals within a pair of MZ twins can be associated with cervical fusion.

  20. Modeling atrazine transport in soil columns with HYDRUS-1D

    Directory of Open Access Journals (Sweden)

    John Leju Celestino Ladu

    2011-09-01

    Full Text Available Both physical and chemical processes affect the fate and transport of herbicides. It is useful to simulate these processes with computer programs to predict solute movement. Simulations were run with HYDRUS-1D to identify the sorption and degradation parameters of atrazine through calibration from the breakthrough curves (BTCs. Data from undisturbed and disturbed soil column experiments were compared and analyzed using the dual-porosity model. The study results show that the values of dispersivity are slightly lower in disturbed columns, suggesting that the more heterogeneous the structure is, the higher the dispersivity. Sorption parameters also show slight variability, which is attributed to the differences in soil properties, experimental conditions and methods, or other ecological factors. For both of the columns, the degradation rates were similar. Potassium bromide was used as a conservative non-reactive tracer to characterize the water movement in columns. Atrazine BTCs exhibited significant tailing and asymmetry, indicating non-equilibrium sorption during solute transport. The dual-porosity model was verified to best fit the BTCs of the column experiments. Greater or lesser concentration of atrazine spreading to the bottom of the columns indicated risk of groundwater contamination. Overall, HYDRUS-1D successfully simulated the atrazine transport in soil columns.

  1. Stability of embankments over cement deep soil mixing columns

    International Nuclear Information System (INIS)

    Morilla Moar, P.; Melentijevic, S.

    2014-01-01

    The deep soil mixing (DSM) is one of the ground improvement methods used for the construction of embankments over soft soils. DSM column-supported embankments are constructed over soft soils to accelerate its construction, improve embankment stability, increase bearing capacity and control of total and differential settlements. There are two traditional design methods, the Japanese (rigid columns) and the scandinavian (soft and semi-rigid columns). Based on Laboratory analysis and numerical analysis these traditional approaches have been questioned by several authors due to its overestimation of the embankment stability considering that the most common failures types are not assumed. This paper presents a brief review of traditional design methods for embankments on DSM columns constructed in soft soils, studies carried out determine the most likely failure types of DSM columns, methods to decrease the overestimation when using limit equilibrium methods and numerical analysis methods that permit detect appropriate failure modes in DSM columns. Finally a case study was assessed using both limited equilibrium and finite element methods which confirmed the overestimation in the factors of safety on embankment stability over DSM columns. (Author)

  2. Reliability assessment of slender concrete columns at the stability failure

    Science.gov (United States)

    Valašík, Adrián; Benko, Vladimír; Strauss, Alfred; Täubling, Benjamin

    2018-01-01

    The European Standard for designing concrete columns within the use of non-linear methods shows deficiencies in terms of global reliability, in case that the concrete columns fail by the loss of stability. The buckling failure is a brittle failure which occurs without warning and the probability of its formation depends on the columns slenderness. Experiments with slender concrete columns were carried out in cooperation with STRABAG Bratislava LTD in Central Laboratory of Faculty of Civil Engineering SUT in Bratislava. The following article aims to compare the global reliability of slender concrete columns with slenderness of 90 and higher. The columns were designed according to methods offered by EN 1992-1-1 [1]. The mentioned experiments were used as basis for deterministic nonlinear modelling of the columns and subsequent the probabilistic evaluation of structural response variability. Final results may be utilized as thresholds for loading of produced structural elements and they aim to present probabilistic design as less conservative compared to classic partial safety factor based design and alternative ECOV method.

  3. Effects of Irregular Bridge Columns and Feasibility of Seismic Regularity

    Science.gov (United States)

    Thomas, Abey E.

    2018-05-01

    Bridges with unequal column height is one of the main irregularities in bridge design particularly while negotiating steep valleys, making the bridges vulnerable to seismic action. The desirable behaviour of bridge columns towards seismic loading is that, they should perform in a regular fashion, i.e. the capacity of each column should be utilized evenly. But, this type of behaviour is often missing when the column heights are unequal along the length of the bridge, allowing short columns to bear the maximum lateral load. In the present study, the effects of unequal column height on the global seismic performance of bridges are studied using pushover analysis. Codes such as CalTrans (Engineering service center, earthquake engineering branch, 2013) and EC-8 (EN 1998-2: design of structures for earthquake resistance. Part 2: bridges, European Committee for Standardization, Brussels, 2005) suggests seismic regularity criterion for achieving regular seismic performance level at all the bridge columns. The feasibility of adopting these seismic regularity criterions along with those mentioned in literatures will be assessed for bridges designed as per the Indian Standards in the present study.

  4. Experimental and theoretical investigation of column - flat slab joint ductility

    International Nuclear Information System (INIS)

    Iskhakov, I.; Ribakov, Y.; Shah, A.

    2009-01-01

    Most modern seismic codes use ductility as one of the basic design parameters. Actually, ductility defines the ability of a structure or its elements to absorb energy by plastic deformations. Until the end of the previous century ductility was defined qualitatively. Most research works related to ductility are focused on structural elements' sections. This study was aimed at complex experimental and theoretical investigation of flat slab-column joints ductility. It is one of the first attempts to obtain quantitative values of joint's ductility for the case of high strength concrete columns and normal strength concrete slabs. It was shown that the flat slab-column joint is a three-dimension (3D) element and its ductility in horizontal and vertical directions are different. This is the main difference between ductility of elements and joint ductility. In case of flat slab-column joints, essential contribution to joint's ductility can be obtained due to the slab's confining effect. Based on experimental data, the authors demonstrate that flat slab-column joint's ductility depends on the joint's confining effect in two horizontal and vertical directions. Furthermore, the influence of slab load intensity and slab reinforcement ratio on the joint's ductility is performed in this study. It is also demonstrated that the effect of the ratio between the slab thickness and the column's section dimension on the ductility parameter is significant. Equations for obtaining a quantitative value of a flat slab-column joint's ductility parameter were developed.

  5. Investigation of Gas Holdup in a Vibrating Bubble Column

    Science.gov (United States)

    Mohagheghian, Shahrouz; Elbing, Brian

    2015-11-01

    Synthetic fuels are part of the solution to the world's energy crisis and climate change. Liquefaction of coal during the Fischer-Tropsch process in a bubble column reactor (BCR) is a key step in production of synthetic fuel. It is known from the 1960's that vibration improves mass transfer in bubble column. The current study experimentally investigates the effect that vibration frequency and amplitude has on gas holdup and bubble size distribution within a bubble column. Air (disperse phase) was injected into water (continuous phase) through a needle shape injector near the bottom of the column, which was open to atmospheric pressure. The air volumetric flow rate was measured with a variable area flow meter. Vibrations were generated with a custom-made shaker table, which oscillated the entire column with independently specified amplitude and frequency (0-30 Hz). Geometric dependencies can be investigated with four cast acrylic columns with aspect ratios ranging from 4.36 to 24, and injector needle internal diameters between 0.32 and 1.59 mm. The gas holdup within the column was measured with a flow visualization system, and a PIV system was used to measure phase velocities. Preliminary results for the non-vibrating and vibrating cases will be presented.

  6. Improved Separation of Complex Polycyclic Aromatic Hydrocarbon Mixtures Using Novel Column Combinations in GC×GC/ToF-MS

    Science.gov (United States)

    Manzano, Carlos; Hoh, Eunha; Simonich, Staci L. Massey

    2012-01-01

    Complex mixtures of polycyclic aromatic hydrocarbons (PAHs) are difficult to resolve because of the high degree of overlap in compound vapor pressures, boiling points and mass spectral fragmentation patterns. The objective of this research was to improve the separation of complex PAH mixtures (including 97 different parent, alkyl-, nitro-, oxy-, thio-, chloro-, bromo-, and high molecular weight PAHs) using GC×GC/ToF-MS by maximizing the orthogonality of different GC column combinations and improving the separation of PAHs from the sample matrix interferences, including unresolved complex mixtures (UCM). Four different combinations of non-polar, polar, liquid crystal and nano-stationary phase columns were tested. Each column combination was optimized and evaluated for orthogonality using a method based on conditional entropy that considers the quantitative peak distribution in the entire two-dimensional space. Finally, an atmospheric particulate matter with diameter column in the first dimension and a 1.2 m × 0.10 mm × 0.10 µm NSP-35 nano-stationary phase column in the second dimension. In addition, the use of this column combination in GC×GC/ToF-MS resulted in significantly shorter analysis times (176 min) for complex PAH mixtures compared to one-dimensional GC/MS (257 min), as well as potentially reduced sample preparation time. PMID:22769970

  7. Recycling of drinking water treatment residue as an additional medium in columns for effective P removal from eutrophic surface water.

    Science.gov (United States)

    Wang, Changhui; Wu, Yu; Bai, Leilei; Zhao, Yaqian; Yan, Zaisheng; Jiang, Helong; Liu, Xin

    2018-07-01

    This study assesses the feasibility of recycling drinking water treatment residue (DWTR) to treat eutrophic surface water in a one-year continuous flow column test. Heat-treated DWTR was used as an additional medium (2%-4%) in columns in case excessive organic matter and N were released from the DWTR to surface water. The results indicated that with minimal undesirable effects on other water properties, DWTR addition substantially enhanced P removal, rendering P concentrations in treated water oligotrophic and treated water unsuitable for Microcystis aeruginosa breeding. Long-term stable P removal by DWTR-column treatment was mainly attributed to the relatively low P levels in raw water (cycles and multiple pollution control (e.g., Dechloromonas, Geobacter, Leucobacter, Nitrospira, Rhodoplanes, and Sulfuritalea); an apparent decrease in Mycobacterium with potential pathogenicity was observed in DWTR-columns. Regardless, limited denitrification of DWTR-columns was observed as a result of low bioavailability of C in surface water. This finding indicates that DWTR can be used with other methods to ensure denitrification for enhanced treatment effects. Overall, the use of DWTR as an additional medium in column systems can potentially treat eutrophic surface water. Copyright © 2018 Elsevier Ltd. All rights reserved.

  8. Separation of cesium by ion exchange columns

    International Nuclear Information System (INIS)

    Bonini, Alberto; Falcon, Marcelo F.; Devida, Claudio A.; Tadey, D.; Vaccaro, Jorge O.; Maset, Elvira

    2003-01-01

    Crystalline silico titanate (CST) has been tested as a selective inorganic ion exchanger to separate Cs 137 from the residual fission product s solution of the Mo 99 plant. The tests are described in detail and show decontamination factors higher than 6000 and a good elution yield

  9. Characterisation of the NA62 GigaTracker End of Column Demonstrator Hybrid Pixel Detector

    Science.gov (United States)

    Noy, M.; Aglieri Rinella, G.; Cotta Ramusino, A.; Fiorini, M.; Jarron, P.; Kaplon, J.; Kluge, A.; Martin, E.; Morel, M.; Perktold, L.; Poltorak, K.; Riedler, P.

    2011-11-01

    The architecture and characterisation of the NA62 GigaTracker End of Column Demonstrator Hybrid Pixel Detector (HPD) are presented. This detector must perform time stamping to 200 ps (RMS) or better, provide 300 μm pitch position information and operate with a dead time of 1% or less for 800 MHz-1 GHz beam rate. The demonstrator HPD Assembly comprises a readout chip with a test column of 45 pixels, alongside other test structures, bump bonded to a p-in-n detector 200 μm in thickness. Validation of the performance of the HPD and the time-over-threshold timewalk compensation mechanism with both beam particles and a high precision laser system was performed and is presented. Confirmation of better than the required time stamping precision has been demonstrated and subsequent work on the design of the full-scale ASIC, dubbed TDCPix, is underway. An overview of the TDCPix architecure is given.

  10. Self-sensing of carbon nanofiber concrete columns subjected to reversed cyclic loading

    Science.gov (United States)

    Howser, R. N.; Dhonde, H. B.; Mo, Y. L.

    2011-08-01

    Civil infrastructures are generally a country's most expensive investment, and concrete is the most widely used material in the construction of civil infrastructures. During a structure's service life, concrete ages and deteriorates, leading to substantial loss of structural integrity and potentially resulting in catastrophic disasters such as highway bridge collapses. A solution for preventing such occurrences is the use of structural health monitoring (SHM) technology for concrete structures containing carbon nanofibers (CNF). CNF concrete has many structural benefits. CNF restricts the growth of nanocracks in addition to yielding higher strength and ductility. Additionally, test results indicate a relationship between electrical resistance and concrete strain, which can be well utilized for SHM. A series of reinforced concrete (RC) columns were built and tested under a reversed cyclic loading using CNF as a SHM device. The SHM device detected and assessed the level of damage in the RC columns, providing a real-time health monitoring system for the structure's overall integrity.

  11. A new oxalate co-conversion technology based on liquid/liquid extraction columns

    International Nuclear Information System (INIS)

    Borda, Gilles; Ode, Denis; Duhamet, Jean; Allegri, Patrick

    2008-01-01

    The current objective of fabricating non proliferating nuclear fuel by 'direct' coprecipitation of uranium, plutonium and minor actinides requires a new process to replace the (co)precipitation step. The technological impact of an increased capacity on the work zone could require the development of a different concept for a continuous device capable of ensuring the proposed goal. A new type of device designed and patented by the Cea was tested in 2007. The patent is for organic confinement in a pulsed column. First, precipitation of cerium or neodymium alone has been carried out in this device, with satisfactory results. Moreover, a recent test campaign demonstrated that a uranium-cerium co-precipitate easily forms when the two nitrates are mixed in a pulsed column of the same size operating under very similar process conditions. Qualitatively, the co-precipitate meets the process requirements. (authors)

  12. A new oxalate co-conversion technology based on liquid/liquid extraction columns

    Energy Technology Data Exchange (ETDEWEB)

    Borda, Gilles; Ode, Denis; Duhamet, Jean; Allegri, Patrick [CEA Nuclear Energy Division - Fuel Cycle Technology Division - System and Chemical Engineering Device Marcoule - 30207 Bagnols sur Ceze (France)

    2008-07-01

    The current objective of fabricating non proliferating nuclear fuel by 'direct' coprecipitation of uranium, plutonium and minor actinides requires a new process to replace the (co)precipitation step. The technological impact of an increased capacity on the work zone could require the development of a different concept for a continuous device capable of ensuring the proposed goal. A new type of device designed and patented by the Cea was tested in 2007. The patent is for organic confinement in a pulsed column. First, precipitation of cerium or neodymium alone has been carried out in this device, with satisfactory results. Moreover, a recent test campaign demonstrated that a uranium-cerium co-precipitate easily forms when the two nitrates are mixed in a pulsed column of the same size operating under very similar process conditions. Qualitatively, the co-precipitate meets the process requirements. (authors)

  13. Self-sensing of carbon nanofiber concrete columns subjected to reversed cyclic loading

    International Nuclear Information System (INIS)

    Howser, R N; Dhonde, H B; Mo, Y L

    2011-01-01

    Civil infrastructures are generally a country's most expensive investment, and concrete is the most widely used material in the construction of civil infrastructures. During a structure's service life, concrete ages and deteriorates, leading to substantial loss of structural integrity and potentially resulting in catastrophic disasters such as highway bridge collapses. A solution for preventing such occurrences is the use of structural health monitoring (SHM) technology for concrete structures containing carbon nanofibers (CNF). CNF concrete has many structural benefits. CNF restricts the growth of nanocracks in addition to yielding higher strength and ductility. Additionally, test results indicate a relationship between electrical resistance and concrete strain, which can be well utilized for SHM. A series of reinforced concrete (RC) columns were built and tested under a reversed cyclic loading using CNF as a SHM device. The SHM device detected and assessed the level of damage in the RC columns, providing a real-time health monitoring system for the structure's overall integrity

  14. Confinement of Reinforced-Concrete Columns with Non-Code Compliant Confining Reinforcement plus Supplemental Pen-Binder

    Directory of Open Access Journals (Sweden)

    Anang Kristianto

    2012-11-01

    Full Text Available One of the important requirements for earthquake resistant building related to confinement is the use of seismic hooks in the hoop or confining reinforcement of reinforced-concrete column elements. However, installation of a confining reinforcement with a 135-degree hook is not easy. Therefore, in practice, many construction workers apply a confining reinforcement with a 90-degreehook (non-code compliant. Based on research and records of recent earthquakes in Indonesia, the use of a non-code compliant confining reinforcement for concrete columns produces structures with poor seismic performance. This paper presents a study that introduces an additional element that is expected to improve the effectiveness of concrete columns confined with a non-code compliant confining reinforcement. The additional element, named a pen-binder, is used to keep the non-code compliant confining reinforcement in place. The effectiveness of this element under pure axial concentric loading was investigatedcomprehensively.The specimens tested in this study were 18 concrete columns,with a cross-section of 170 mm x 170 mm and a height of 480 mm. The main test variables were the material type of the pen-binder, the angle of the hook, and the confining reinforcement configuration.The test results indicate that adding pen-binders can effectively improve the strength and ductility of the column specimens confined with a non-code compliant confining reinforcement

  15. SENSITIVITY ANALYSIS FOR SALTSTONE DISPOSAL UNIT COLUMN DEGRADATION ANALYSES

    Energy Technology Data Exchange (ETDEWEB)

    Flach, G.

    2014-10-28

    PORFLOW related analyses supporting a Sensitivity Analysis for Saltstone Disposal Unit (SDU) column degradation were performed. Previous analyses, Flach and Taylor 2014, used a model in which the SDU columns degraded in a piecewise manner from the top and bottom simultaneously. The current analyses employs a model in which all pieces of the column degrade at the same time. Information was extracted from the analyses which may be useful in determining the distribution of Tc-99 in the various SDUs throughout time and in determining flow balances for the SDUs.

  16. Partial Path Column Generation for the Vehicle Routing Problem

    DEFF Research Database (Denmark)

    Jepsen, Mads Kehlet; Petersen, Bjørn

    This paper presents a column generation algorithm for the Capacitated Vehicle Routing Problem (CVRP) and the Vehicle Routing Problem with Time Windows (VRPTW). Traditionally, column generation models of the CVRP and VRPTW have consisted of a Set Partitioning master problem with each column...... of the giant tour’; a so-called partial path, i.e., not necessarily starting and ending in the depot. This way, the length of the partial path can be bounded and a better control of the size of the solution space for the pricing problem can be obtained....

  17. Control structure selection for energy integrated distillation column

    DEFF Research Database (Denmark)

    Hansen, J.E.; Jørgensen, Sten Bay

    1998-01-01

    This paper treats a case study on control structure selection for an almost binary distillation column. The column is energy integrated with a heat pump in order to transfer heat from the condenser to the reboiler. This integrated plant configuration renders the possible control structures somewhat...... different from what is usual for binary distillation columns. Further the heat pump enables disturbances to propagate faster through the system. The plant has six possible actuators of which three must be used to stabilize the system. Hereby three actuators are left for product purity control. An MILP...

  18. Characterization of Bubble Size Distributions within a Bubble Column

    OpenAIRE

    Shahrouz Mohagheghian; Brian R. Elbing

    2018-01-01

    The current study experimentally examines bubble size distribution (BSD) within a bubble column and the associated characteristic length scales. Air was injected into a column of water via a single injection tube. The column diameter (63–102 mm), injection tube diameter (0.8–1.6 mm) and superficial gas velocity (1.4–55 mm/s) were varied. Large samples (up to 54,000 bubbles) of bubble sizes measured via 2D imaging were used to produce probability density functions (PDFs). The PDFs were used to...

  19. The Fire Resistance Performance of Recycled Aggregate Concrete Columns with Different Concrete Compressive Strengths

    OpenAIRE

    Dong, Hongying; Cao, Wanlin; Bian, Jianhui; Zhang, Jianwei

    2014-01-01

    In order to ascertain the fire resistance performance of recycled aggregate concrete (RAC) components with different concrete compressive strengths, four full-scaled concrete columns were designed and tested under high temperature. Two of the four specimens were constructed by normal concrete with compressive strength ratings of C20 and C30, respectively, while the others were made from recycled coarse aggregate (RCA) concrete of C30 and C40, respectively. Identical constant axial forces were...

  20. Investigations on the propagation of free surface boiling in a vertical superheated liquid column

    Energy Technology Data Exchange (ETDEWEB)

    Das, P.K.; Bhat, G.S.; Arakeri, V.H.

    1987-04-01

    Some experimental studies on boiling propagation in a suddenly depressurized superheated vertical liquid column are reported. The propagation velocity of this phase change has been measured using an optical method. This velocity is strongly dependent on liquid superheat, liquid purity and test section size. The measured velocities of less than 5 m s/sup -1/ are significantly lower than the sonic velocity. Present observations suggest that the dominant mechanism for boiling propagation is convection.

  1. Investigations on the propagation of free surface boiling in a vertical superheated liquid column

    International Nuclear Information System (INIS)

    Das, P.K.; Bhat, G.S.; Arakeri, V.H.

    1987-01-01

    Some experimental studies on boiling propagation in a suddenly depressurized superheated vertical liquid column are reported. The propagation velocity of this phase change has been measured using an optical method. This velocity is strongly dependent on liquid superheat, liquid purity and test section size. The measured velocities of less than 5 m s -1 are significantly lower than the sonic velocity. Present observations suggest that the dominant mechanism for boiling propagation is convection. (author)

  2. Design data, liquid distributors and condenser for a distillation column to enrich tritium in metallic lithium

    International Nuclear Information System (INIS)

    Barnert, E.

    1984-01-01

    Tritium, one fuel component of the fusion reactor is bred from the reactors blanket material lithium. Before extracting the tritium from, for instance, metallic lithium by permeation it has to be enriched in the lithium by high temperature distillation. In this report design data for a column for high temperature distillation are given. About the testing of two distributors for small liquid quantities and of a condenser is reported. (orig.) [de

  3. Engineering evaluation of 55-year-old timber columns recycled from an industrial military building

    Science.gov (United States)

    Robert H. Falk; David Green; Douglas Rammer; Scott F. Lantz

    2000-01-01

    A large sample of timber was collected from a 548,000-ft.2 (50,900-m2) World War II era industrial military building containing approximately 1, 875,000 board feet (4,400 m3) of lumber and timber. Sixty 12-foot- (3.6-m-) long, nominal 8- by 8-inches (190-by 190-mm) Douglas-fir columns were tested at the USDA Forest Service, Forest Products Laboratory, and the results...

  4. Fabrication of a micrometer Ni–Cu alloy column coupled with a Cu micro-column for thermal measurement

    International Nuclear Information System (INIS)

    Lin, J C; Chang, T K; Yang, J H; Jeng, J H; Lee, D L; Jiang, S B

    2009-01-01

    Micrometer Ni–Cu alloy columns have been fabricated by the micro-anode-guided electroplating (MAGE) process in the citrate bath. The surface morphology and chemical composition of the micro-columns were determined by copper concentration in the bath and by the electrical bias of MAGE. When fabricated in a bath of dilute copper (i.e. 4 mM) at lower voltages (e.g. 3.8 and 4.0 V), the alloy micro-columns revealed uniform diameter and smooth appearance. The alloy composition demonstrated an increase in the wt% ratio of Ni/Cu from 75/25, 80/20, 83/17 to 87/13 with increasing electrical bias from 3.8, 4.0, 4.2 to 4.4 V. However, it decreases from 75/25, 57/43 to 47/53 with increasing copper concentration from 4, 8 to 12 mM in the bath. Citrate plays a role in forming complexes with nickel and copper at similar reduction potentials, thus reducing simultaneously to Ni–Cu alloy. The mechanism for fabricating alloy micro-columns could be delineated on the basis of cathodic polarization of the complexes. A couple of micro-columns were fabricated using MAGE in constructing a pure copper micro-column on the top of a Ni/Cu (at 47/53) alloy micro-column. This micro-thermocouple provides a satisfactory measurement with good sensitivity and precision

  5. NON-LINEAR ANALYSIS OF AN EXPERIMENTAL JOINT OF COLUMN AND BEAMS OF ARMED CONCRETE-STEEL COLUMN FOR FRAME

    Directory of Open Access Journals (Sweden)

    Nelson López

    2017-12-01

    Full Text Available In this research, the nonlinear behavior of a real-scale experimental joint (node is studied, consisting of three reinforced concrete elements, one column and two beams joined to a structural steel column at the upper level. In the numerical analysis the model of the union was analyzed in the inelastic range, this model was elaborated with the finite element program based on fibers, SeismoStruct to analyze as a function of time, the traction and compression efforts in the confined area and not confined area of the concrete column and in the longitudinal reinforcement steel, as well as verification of the design of the base plate that joins the two columns. The results showed that tensile stresses in the unconfined zone surpassed the concrete breaking point, with cracking occurring just below the lower edge of the beams; in the confined area the traction efforts were much lower, with cracks occurring later than in the non-confined area. The concrete column-steel column joint behaved as a rigid node, so the elastic design was consistent with the calculation methodology of base plates for steel columns.

  6. Computerized tomography of the vertebral column following traumatic lesion

    International Nuclear Information System (INIS)

    Taenzer, B.; Gmelin, E.; Burmester, E.; Babaian, E.; Weiss, H.D.; Hohlbach, G.

    1984-01-01

    In 58 patients with lesions of the vertebral column in the thoracal and lumbar section established by conventional X-ray, the informative power of computerized tomography was tested. Axial projection with the superimposition-free presentation of bone and soft-tissue structures in the motional segment clears up the diagnostically decisive question of the extent of the lesion and form of fracture, and thus provides information on the stability or instability of the fracture relevant for the therapeutic action taken. All patients had compression fractures of vertebrae, with a fragment of the front edge broken away in 50 cases and one of the back edge broken away in 17 cases. In 30 cases the intervertebral disks were damaged. 43 fractures were stable, 25 were unstable. The instability of 13 fractures was only recognized by CT. In essence, the diagnostic action to be taken begins with a grand-survey X-ray in two planes as a screening, with computerized tomography following in the positive case. Conventional tomograms are not necessary. (BWU) [de

  7. Electronic Nose using Gas Chromatography Column and Quartz Crystal Microbalance

    Directory of Open Access Journals (Sweden)

    Hari Agus Sujono

    2011-08-01

    Full Text Available The conventional electronic nose usually consists of an array of dissimilar chemical sensors such as quartz crystal microbalance (QCM combined with pattern recognition algorithm such as Neural network. Because of parallel processing, the system needs a huge number of sensors and circuits which may emerge complexity and inter-channel crosstalk problems. In this research, a new type of odor identification which combines between gas chromatography (GC and electronic nose methods has been developed. The system consists of a GC column and a 10-MHz quartz crystal microbalance sensor producing a unique pattern for an odor in time domain. This method offers advantages of substantially reduced size, interferences and power consumption in comparison to existing odor identification system. Several odors of organic compounds were introduced to evaluate the selectivity of the system. Principle component analysis method was used to visualize the classification of each odor in two-dimensional space. This system could resolve common organic solvents, including molecules of different classes (aromatic from alcohols as well as those within a particular class (methanol from ethanol and also fuels (premium from pertamax. The neural network can be taught to recognize the odors tested in the experiment with identification rate of 85 %. It is therefore the system may take the place of human nose, especially for poisonous odor evaluations.

  8. REALIGNED MODEL PREDICTIVE CONTROL OF A PROPYLENE DISTILLATION COLUMN

    Directory of Open Access Journals (Sweden)

    A. I. Hinojosa

    Full Text Available Abstract In the process industry, advanced controllers usually aim at an economic objective, which usually requires closed-loop stability and constraints satisfaction. In this paper, the application of a MPC in the optimization structure of an industrial Propylene/Propane (PP splitter is tested with a controller based on a state space model, which is suitable for heavily disturbed environments. The simulation platform is based on the integration of the commercial dynamic simulator Dynsim® and the rigorous steady-state optimizer ROMeo® with the real-time facilities of Matlab. The predictive controller is the Infinite Horizon Model Predictive Control (IHMPC, based on a state-space model that that does not require the use of a state observer because the non-minimum state is built with the past inputs and outputs. The controller considers the existence of zone control of the outputs and optimizing targets for the inputs. We verify that the controller is efficient to control the propylene distillation system in a disturbed scenario when compared with a conventional controller based on a state observer. The simulation results show a good performance in terms of stability of the controller and rejection of large disturbances in the composition of the feed of the propylene distillation column.

  9. Effects of Predamaged Level on Confined HSC Columns

    Directory of Open Access Journals (Sweden)

    Ma Chau-Khun

    2017-01-01

    Full Text Available In the design of repair works for damaged concrete, an accurate and representative stress-strain model is of important. The stress-strain model for damaged high strength concrete (HSC repaired with post-tensioning steel straps confinement yet available, although the confining method has been proven to be effective in improving the performance of non-damaged HSC. A series of experimental test was carried out to investigate the stress-strain relationships of such concrete. A total of 24 HSC cylinders were compressed until certain damaged levels, then repaired by using steel straps. Two important parameters have been identified to have significant effects on the stress-strain relationship of such repaired concrete, namely the confining volumetric ratio and damaged levels. These parameters were incorporated into the development of stressstrain model, which later was shown to correlate well with the experimental results. This paper also has evidenced that existing stressstrain models of damaged concrete are not suitable to be directly applied to the design of repair works using post-tensioning steel straps confinement that produce external lateral stress on damaged columns before subsequent loading applied.

  10. The role of the notochord in amniote vertebral column segmentation.

    Science.gov (United States)

    Ward, Lizzy; Pang, Angel S W; Evans, Susan E; Stern, Claudio D

    2018-07-01

    The vertebral column is segmented, comprising an alternating series of vertebrae and intervertebral discs along the head-tail axis. The vertebrae and outer portion (annulus fibrosus) of the disc are derived from the sclerotome part of the somites, whereas the inner nucleus pulposus of the disc is derived from the notochord. Here we investigate the role of the notochord in vertebral patterning through a series of microsurgical experiments in chick embryos. Ablation of the notochord causes loss of segmentation of vertebral bodies and discs. However, the notochord cannot segment in the absence of the surrounding sclerotome. To test whether the notochord dictates sclerotome segmentation, we grafted an ectopic notochord. We find that the intrinsic segmentation of the sclerotome is dominant over any segmental information the notochord may possess, and no evidence that the chick notochord is intrinsically segmented. We propose that the segmental pattern of vertebral bodies and discs in chick is dictated by the sclerotome, which first signals to the notochord to ensure that the nucleus pulposus develops in register with the somite-derived annulus fibrosus. Later, the notochord is required for maintenance of sclerotome segmentation as the mature vertebral bodies and intervertebral discs form. These results highlight differences in vertebral development between amniotes and teleosts including zebrafish, where the notochord dictates the segmental pattern. The relative importance of the sclerotome and notochord in vertebral patterning has changed significantly during evolution. Copyright © 2018 The Authors. Published by Elsevier Inc. All rights reserved.

  11. Acoustic emission monitoring of concrete columns and beams strengthened with fiber reinforced polymer sheets

    Science.gov (United States)

    Ma, Gao; Li, Hui; Zhou, Wensong; Xian, Guijun

    2012-04-01

    Acoustic emission (AE) technique is an effective method in the nondestructive testing (NDT) field of civil engineering. During the last two decades, Fiber reinforced polymer (FRP) has been widely used in repairing and strengthening concrete structures. The damage state of FRP strengthened concrete structures has become an important issue during the service period of the structure and it is a meaningful work to use AE technique as a nondestructive method to assess its damage state. The present study reports AE monitoring results of axial compression tests carried on basalt fiber reinforced polymer (BFRP) confined concrete columns and three-point-bending tests carried on BFRP reinforced concrete beams. AE parameters analysis was firstly utilized to give preliminary results of the concrete fracture process of these specimens. It was found that cumulative AE events can reflect the fracture development trend of both BFRP confined concrete columns and BFRP strengthened concrete beams and AE events had an abrupt increase at the point of BFRP breakage. Then the fracture process of BFRP confined concrete columns and BFRP strengthened concrete beams was studied through RA value-average frequency analysis. The RA value-average frequency tendencies of BFRP confined concrete were found different from that of BFRP strengthened concrete beams. The variation tendency of concrete crack patterns during the loading process was revealed.

  12. Damage Detection of a Concrete Column Subject to Blast Loads Using Embedded Piezoceramic Transducers.

    Science.gov (United States)

    Xu, Kai; Deng, Qingshan; Cai, Lujun; Ho, Siuchun; Song, Gangbing

    2018-04-28

    Some of the most severe structural loadings come in the form of blast loads, which may be caused by severe accidents or even terrorist activities. Most commonly after exposure to explosive forces, a structure will suffer from different degrees of damage, and even progress towards a state of collapse. Therefore, damage detection of a structure subject to explosive loads is of importance. This paper proposes a new approach to damage detection of a concrete column structure subjected to blast loads using embedded piezoceramic smart aggregates (SAs). Since the sensors are embedded in the structure, the proposed active-sensing based approach is more sensitive to internal or through cracks than surface damage. In the active sensing approach, the embedded SAs act as actuators and sensors, that can respectively generate and detect stress waves. If the stress wave propagates across a crack, the energy of the wave attenuates, and the reduction of the energy compared to the healthy baseline is indicative of a damage. With a damage index matrix constructed by signals obtained from an array of SAs, cracks caused by blast loads can be detected throughout the structure. Conventional sensing methods such as the measurement of dynamic strain and acceleration were included in the experiment. Since columns are critical elements needed to prevent structural collapse, knowledge of their integrity and damage conditions is essential for safety after exposure to blast loads. In this research, a concrete column with embedded SAs was chosen as the specimen, and a series of explosive tests were conducted on the column. Experimental results reveal that surface damages, though appear severe, cause minor changes in the damage index, and through cracks result in significant increase of the damage index, demonstrating the effectiveness of the active sensing, enabled by embedded SAs, in damage monitoring of the column under blast loads, and thus providing a reliable indication of structural

  13. A new co conversion technology based on liquid/liquid extraction column

    Energy Technology Data Exchange (ETDEWEB)

    Borda, Gilles; Ode, Denis; Duhamet, Jean; Brackx, Emmanuelle [CEA Valrho - Marcoule - BP 17171 - 30207 Bagnols sur Ceze Cedex (France)

    2009-06-15

    The current objective of implementing 'direct' coprecipitation of uranium, plutonium and minor actinides for nuclear fuel re-fabrication leads to reconsider the (co)precipitation step, and more precisely its adaptability to new flowrates' specifications. Indeed, coprecipitation of a uranium fraction together with plutonium results in an appreciable increase in the process flow rates for this step. The technological impact of the increase in capacity could require the development of a different concept for a continuous device capable of ensuring the proposed process. A new type of device designed and patented by the CEA has been tested since 2007. The patent is for organic confinement in a pulsed column (PC) or Couette column (CC). The precipitation reaction between the oxalate complexing agent and a surrogate nitrate-cerium(II) or neodymium(III) alone, or coprecipitated uranium(IV) and cerium(III), occurs within an emulsion created in the device by these two phases flowing with a counter-current chemically inert organic phase (for example TPH) produced by the stirring action of the pulsator (PC) or the central rotor (CC). The precipitate is confined and thus does not form deposits on the vessel walls (which are also water-repellent); it flows downward by gravity and exits the column continuously into a settling tank. This paper describes the recent results obtained with this new technology for precipitation of Ce and Nd and coprecipitation of U + Ce in pulsed column and Couette column. It describes a first modeling allowing further extrapolation of this device to high capacities. (authors)

  14. Bubble column and CFD simulation for chemical recycling of polyethylene terephthalate

    Science.gov (United States)

    Alzuhairi, Mohammed

    2018-05-01

    Computational Fluid Dynamics (CFD) is an important simulation tool, which uses powerful computer to get optimal design in industrial processes. New approach technique of bubble column for three phases has been used with respect to chemical recycling of Polyethylene Terephthalate (PET). The porous ceramic has been used in thin plate (5 mm) with a narrow pore size distribution. Excellent agreement between CFD has been predicted and experimental profiles of hold-up and velocity close to wall have been observed for a column diameter 0.08 m, column height 0.15 m (HD), and superficial gas velocity (VG) 0.05 m/s. The main purpose of the current study is to highlight depolymerization of PET chemically by using the close system of Ethylene Glycol, PET-Catalyzed, and Nitrogen glycolysis process in bubble column of three phases technique by using Nano catalyst, SiO2 with various weight percent (0.01, 0.02, 0.05, 0.1, 0.2, and 0.5) based on PET weight and preheated Nitrogen up to 100° C by extra heater in bubble column reactor. The depolymerization time could be reduced in order to improve heat and mass transfer in comparison with the traditional methods. Little amount not exceeding 0.01% of Nano SiO2 is enough for completing depolymerization. The final product of PET depolymerization has full characterization by FTIR, AFM, CHN tests and has been used as a vital additive for Bitumen, it has been investigated as a moisture-proof, water seepage-proof material, and as a tough resistant to environmental conditions.

  15. EX1005 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1005: Guam to Honolulu, HI Transit...

  16. Associations between the Cervical Vertebral Column and Craniofacial Morphology

    DEFF Research Database (Denmark)

    Sonnesen, Ane Liselotte

    2010-01-01

    Aim. To summarize recent studies on morphological deviations of the cervical vertebral column and associations with craniofacial morphology and head posture in nonsyndromic patients and in patients with obstructive sleep apnoea (OSA). Design. In these recent studies, visual assessment of the cerv......Aim. To summarize recent studies on morphological deviations of the cervical vertebral column and associations with craniofacial morphology and head posture in nonsyndromic patients and in patients with obstructive sleep apnoea (OSA). Design. In these recent studies, visual assessment...... of the cervical vertebral column and cephalometric analysis of the craniofacial skeleton were performed on profile radiographs of subjects with neutral occlusion, patients with severe skeletal malocclusions and patients with OSA. Material from human triploid foetuses and mouse embryos was analysed histologically....... Results. Recent studies have documented associations between fusion of the cervical vertebral column and craniofacial morphology, including head posture in patients with severe skeletal malocclusions. Histological studies on prenatal material supported these findings. Conclusion. It is suggested...

  17. EX1701 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1701: Kingman/Palmyra, Jarvis (Mapping)...

  18. EX1102 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1102: ROV and Camera Sled Integration...

  19. EX1403 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1403: East Coast Mapping and Exploration...

  20. EX1104 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1104: Mid-Cayman Rise Exploration...

  1. EX1204 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1204: Northeastern Canyons and...

  2. EX1003 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1003: Transit from Hawaii to Guam...

  3. EX0905 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX0905: Mapping Field Trials II Mendocino...

  4. Pulse amplitude and frequency effects in a pulsed packed column

    International Nuclear Information System (INIS)

    Russell, S.H.

    1954-04-01

    A study has been made of the effect on the efficiency and capacity of applying pulses of varying amplitude and frequency to a packed column. In the efficiency studies, the maximum efficiency was obtained with a pulse having an amplitude of 3/8'' and a frequency of 140 cycles per minute. Under these conditions, the column was about five times as efficient as a simple packed column. Two general types of results were obtained in the capacity studies. Under certain conditions, the capacity increased over that of a simple packed column, but under others, it decreased. Some of the factors causing this were investigated but the fundamental reasons were not determined due to a lack of personnel for the necessary experiments. (author)

  5. Microchip-based monolithic column for high performance liquid chromatography

    Data.gov (United States)

    National Aeronautics and Space Administration — We have developed microchip based monolithic columns that can be used for liquid chromatography of small organic molecules, as well as, macromolecules such as...

  6. Denitrification in the water column of the central Baltic Sea

    DEFF Research Database (Denmark)

    Dalsgaard, Tage; De Brabandere, Loreto; Hall, Per O. J.

    2013-01-01

    Removal of fixed nitrogen in the water column of the eastern Gotland Basin, central Baltic Sea, was studied during two cruises in September 2008 and August 2010. The water column was stratified with anoxic sulfidic bottom water meeting oxic nitrate containing water at the oxic–anoxic interface......3 or sulfide concentrations were converted to in situ rates using the measured water column concentrations of NO3 and sulfide and the actual measured relations between NO3 and sulfide concentrations and enitrification rates. In situ denitrification ranged from 0.24 to 15.9 nM N2 h1. Assuming...... area. Even with an active denitrification layer of 3–6 m thickness the pelagic denitrification per unit area clearly exceeded sediment denitrification rates elsewhere in the Baltic Sea. When extrapolated to the entire Baltic Proper (BP) denitrification in the water column was in the range of 132...

  7. Bubble column fermenter modeling: a comparison for pressure effects

    Energy Technology Data Exchange (ETDEWEB)

    Shioya, S; Dang, N D.P.; Dunn, I J

    1978-01-01

    Two models which describe the oxygen transfer, oxygen uptake, and axial mixing in a bubble column fermenter are described. Model I includes no pressure effects and can be solved analytically. Model II incorporates the influence of hydrostatic pressure on oxygen solubility and gas expansion and must be solved numerically. The liquid phase oxygen concentration profiles from both models are compared to ascertain for what parametric conditions and for what maximum column height Model I is valid. Results show that for many situations Model I can approximate the oxygen profiles in a 10 m column within 20%. As the transfer and uptake rates increase, the deviation of Model I can reach 80% for a 10 m column. 7 figures.

  8. EX0802 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX0802: Operation Halloween Shakedown...

  9. EX1006 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1006: Hawaii to San Francisco Transit to...

  10. EX0801 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX0801: Mapping Operations Shakedown...

  11. EX1603 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1603: Hohonu Moana: Exploring the Deep...

  12. EX1604 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1604: CAPSTONE Wake Island PRIMNM...

  13. Varied overstrain injuries of the vertebral column conditioned by evolution

    Energy Technology Data Exchange (ETDEWEB)

    Kohlbach, W

    1983-08-01

    During physiological growth of the juvenile vertebral column, various stages of stability occur which are characterized by the condition of the marginal rim of the vertebral bodies. If the vertebral juvenile column is overstrained, these variations in stability results in a variety of damage to vertebral bodies and vertebral disks. One of these lesions corresponds to Scheuermann's disease (osteochondrosis of vertebral epiphyses in juveniles). Damage of the vertebral column due to overstrain can occur only if the overstrain is applied in upright position. Since Man alone can damage his vertebral column in upright position (as a result of his evolutionary development), Scheuermann's thesis is confirmed that Scheuermann's disease is confined to Man. Spondylolysis/spondylolisthesis is also a damage caused by overstrain. Here, too, the damage can occur only if the load is exercised in upright position, with the exception of a slanted positioning of the intervertebral components.

  14. Varied overstrain injuries of the vertebral column conditioned by evolution

    International Nuclear Information System (INIS)

    Kohlbach, W.

    1983-01-01

    During physiological growth of the juvenile vertebral column, various stages of stability occur which are characterized by the condition of the marginal rim of the vertebral bodies. If the vertebral juvenile column is overstrained, these variations in stability results in a variety of damage to vertebral bodies and vertebral disks. One of these lesions corresponds to Scheuermann's disease (osteochondrosis of vertebral epiphyses in juveniles). Damage of the vertebral column due to overstrain can occur only if the overstrain is applied in upright position. Since Man alone can damage his vertebral column in upright position (as a result of his evolutionary development), Scheuermann's thesis is confirmed that Scheuermann's disease is confined to Man. Spondylolysis/spondylolisthesis is also a damage caused by overstrain. Here, too, the damage can occur only if the load is exercised in upright position, with the exception of a slanted positioning of the intervertebral components. (orig.) [de

  15. Science Column: Reconstruction: The Experimental Side of Digital Forensics

    Directory of Open Access Journals (Sweden)

    Fred Cohen

    2013-12-01

    Full Text Available Many in digital forensics seem to forget that the science part of digital forensics means experimentation and that implies a whole lot of things that most practitioners never learned.(see PDF for full column

  16. Pulse amplitude and frequency effects in a pulsed packed column

    Energy Technology Data Exchange (ETDEWEB)

    Russell, S H

    1954-04-15

    A study has been made of the effect on the efficiency and capacity of applying pulses of varying amplitude and frequency to a packed column. In the efficiency studies, the maximum efficiency was obtained with a pulse having an amplitude of 3/8'' and a frequency of 140 cycles per minute. Under these conditions, the column was about five times as efficient as a simple packed column. Two general types of results were obtained in the capacity studies. Under certain conditions, the capacity increased over that of a simple packed column, but under others, it decreased. Some of the factors causing this were investigated but the fundamental reasons were not determined due to a lack of personnel for the necessary experiments. (author)

  17. EX1203 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1203: Florida Escarpment and Straits...

  18. EX1602 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1602: Mission System Shakedown/CAPSTONE...

  19. Experimental and numerical investigation of bubble column reactors

    NARCIS (Netherlands)

    Bai, W.

    2010-01-01

    Due to various advantages, such as simple geometry, ease of operation, low operating and maintenance costs, excellent heat and mass transfer characteristics, bubble column reactors are frequently used in chemical, petrochemical, biochemical, pharmaceutical, metallurgical industries for a variety of

  20. EX1704 Water Column Summary Report and Profile Data Collection

    Data.gov (United States)

    National Oceanic and Atmospheric Administration, Department of Commerce — A complete set of water column profile data and CTD Summary Report (if generated) generated by the Okeanos Explorer during EX1704: American Samoa and Cook Islands...