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Sample records for reliable analytical methods

  1. Application of system reliability analytical method, GO-FLOW

    International Nuclear Information System (INIS)

    Matsuoka, Takeshi; Fukuto, Junji; Mitomo, Nobuo; Miyazaki, Keiko; Matsukura, Hiroshi; Kobayashi, Michiyuki

    1999-01-01

    The Ship Research Institute proceed a developmental study on GO-FLOW method with various advancing functionalities for the system reliability analysis method occupying main parts of PSA (Probabilistic Safety Assessment). Here was attempted to intend to upgrade functionality of the GO-FLOW method, to develop an analytical function integrated with dynamic behavior analytical function, physical behavior and probable subject transfer, and to prepare a main accident sequence picking-out function. In 1997 fiscal year, in dynamic event-tree analytical system, an analytical function was developed by adding dependency between headings. In simulation analytical function of the accident sequence, main accident sequence of MRX for improved ship propulsion reactor became possible to be covered perfectly. And, input data for analysis was prepared with a function capable easily to set by an analysis operator. (G.K.)

  2. Precision profiles and analytic reliability of radioimmunologic methods

    International Nuclear Information System (INIS)

    Yaneva, Z.; Popova, Yu.

    1991-01-01

    The aim of the present study is to investigate and compare some methods for creation of 'precision profiles' (PP) and to clarify their possibilities for determining the analytical reliability of RIA. Only methods without complicated mathematical calculations has been used. The reproducibility in serums with a concentration of the determinable hormone in the whole range of the calibration curve has been studied. The radioimmunoassay has been performed with TSH-RIA set (ex East Germany), and comparative evaluations - with commercial sets of HOECHST (Germany) and AMERSHAM (GB). Three methods for obtaining the relationship concentration (IU/l) -reproducibility (C.V.,%) are used and a comparison is made of their corresponding profiles: preliminary rough profile, Rodbard-PP and Ekins-PP. It is concluded that the creation of a precision profile is obligatory and the method of its construction does not influence the relationship's course. PP allows to determine concentration range giving stable results which improves the efficiency of the analitical work. 16 refs., 4 figs

  3. A Comparison of Result Reliability for Investigation of Milk Composition by Alternative Analytical Methods in Czech Republic

    Directory of Open Access Journals (Sweden)

    Oto Hanuš

    2014-01-01

    Full Text Available The milk analyse result reliability is important for assurance of foodstuff chain quality. There are more direct and indirect methods for milk composition measurement (fat (F, protein (P, lactose (L and solids non fat (SNF content. The goal was to evaluate some reference and routine milk analytical procedures on result basis. The direct reference analyses were: F, fat content (Röse–Gottlieb method; P, crude protein content (Kjeldahl method; L, lactose (monohydrate, polarimetric method; SNF, solids non fat (gravimetric method. F, P, L and SNF were determined also by various indirect methods: – MIR (infrared (IR technology with optical filters, 7 instruments in 4 labs; – MIR–FT (IR spectroscopy with Fourier’s transformations, 10 in 6; – ultrasonic method (UM, 3 in 1; – analysis by the blue and red box (BRB, 1 v 1. There were used 10 reference milk samples. Coefficient of determination (R2, correlation coefficient (r and standard deviation of the mean of individual differences (MDsd, for n were evaluated. All correlations (r; for all indirect and alternative methods and all milk components were significant (P ≤ 0.001. MIR and MIR–FT (conventional methods explained considerably higher proportion of the variability in reference results than the UM and BRB methods (alternative. All r average values (x minus 1.64 × sd for 95% confidence interval can be used as standards for calibration quality evaluation (MIR, MIR–FT, UM and BRB: – for F 0.997, 0.997, 0.99 and 0.995; – for P 0.986, 0.981, 0.828 and 0.864; – for L 0.968, 0.871, 0.705 and 0.761; – for SNF 0.992, 0.993, 0.911 and 0.872. Similarly ​MDsd (x plus 1.64 × sd: – for F 0.071, 0.068, 0.132 and 0.101%; – for P 0.051, 0.054, 0.202 and 0.14%; – for L 0.037, 0.074, 0.113 and 0.11%; – for SNF 0.052, 0.068, 0.141 and 0.204.

  4. Basic Concepts in Classical Test Theory: Tests Aren't Reliable, the Nature of Alpha, and Reliability Generalization as a Meta-analytic Method.

    Science.gov (United States)

    Helms, LuAnn Sherbeck

    This paper discusses the fact that reliability is about scores and not tests and how reliability limits effect sizes. The paper also explores the classical reliability coefficients of stability, equivalence, and internal consistency. Stability is concerned with how stable test scores will be over time, while equivalence addresses the relationship…

  5. Bayesian methods in reliability

    Science.gov (United States)

    Sander, P.; Badoux, R.

    1991-11-01

    The present proceedings from a course on Bayesian methods in reliability encompasses Bayesian statistical methods and their computational implementation, models for analyzing censored data from nonrepairable systems, the traits of repairable systems and growth models, the use of expert judgment, and a review of the problem of forecasting software reliability. Specific issues addressed include the use of Bayesian methods to estimate the leak rate of a gas pipeline, approximate analyses under great prior uncertainty, reliability estimation techniques, and a nonhomogeneous Poisson process. Also addressed are the calibration sets and seed variables of expert judgment systems for risk assessment, experimental illustrations of the use of expert judgment for reliability testing, and analyses of the predictive quality of software-reliability growth models such as the Weibull order statistics.

  6. Structural Reliability Methods

    DEFF Research Database (Denmark)

    Ditlevsen, Ove Dalager; Madsen, H. O.

    The structural reliability methods quantitatively treat the uncertainty of predicting the behaviour and properties of a structure given the uncertain properties of its geometry, materials, and the actions it is supposed to withstand. This book addresses the probabilistic methods for evaluation...... of structural reliability, including the theoretical basis for these methods. Partial safety factor codes under current practice are briefly introduced and discussed. A probabilistic code format for obtaining a formal reliability evaluation system that catches the most essential features of the nature...... of the uncertainties and their interplay is the developed, step-by-step. The concepts presented are illustrated by numerous examples throughout the text....

  7. Supercritical fluid analytical methods

    International Nuclear Information System (INIS)

    Smith, R.D.; Kalinoski, H.T.; Wright, B.W.; Udseth, H.R.

    1988-01-01

    Supercritical fluids are providing the basis for new and improved methods across a range of analytical technologies. New methods are being developed to allow the detection and measurement of compounds that are incompatible with conventional analytical methodologies. Characterization of process and effluent streams for synfuel plants requires instruments capable of detecting and measuring high-molecular-weight compounds, polar compounds, or other materials that are generally difficult to analyze. The purpose of this program is to develop and apply new supercritical fluid techniques for extraction, separation, and analysis. These new technologies will be applied to previously intractable synfuel process materials and to complex mixtures resulting from their interaction with environmental and biological systems

  8. Development of reliable analytical method for extraction and separation of thorium(IV) by Cyanex 272 in kerosene

    International Nuclear Information System (INIS)

    Madane, N.S.; Mohite, B.S.

    2011-01-01

    A simple and selective spectrophotometric method has been developed for the extraction and separation of thorium(IV) from sodium salicylate media using Cyanex 272 in kerosene. Thorium(IV) was quantitatively extracted by 5 x 10 -4 M Cyanex 272 in kerosene from 1 x 10 -5 M sodium salicylate medium. The extracted thorium(IV) was stripped out quantitatively from the organic phase with 4.0 M hydrochloric acid and determined spectrophotometrically with arsenazo(III) at 620 nm. The effect of concentrations of sodium salicylate, extractant, diluents, metal ion and strippants has been studied. Separation of thorium(IV) from other elements was achieved from binary as well as multicomponent mixtures such as uranium(VI), strontium(II), rubidium(I), cesium(I), potassium(I), Sodium(I), lithium(I), lead(II), barium(II), beryllium(II) etc. Using this method separation and determination of thorium(IV) in geological and real samples has been carried out. The method is simple, rapid and selective with good reproducibility (approximately ±2%). (author)

  9. Evaluation of structural reliability using simulation methods

    Directory of Open Access Journals (Sweden)

    Baballëku Markel

    2015-01-01

    Full Text Available Eurocode describes the 'index of reliability' as a measure of structural reliability, related to the 'probability of failure'. This paper is focused on the assessment of this index for a reinforced concrete bridge pier. It is rare to explicitly use reliability concepts for design of structures, but the problems of structural engineering are better known through them. Some of the main methods for the estimation of the probability of failure are the exact analytical integration, numerical integration, approximate analytical methods and simulation methods. Monte Carlo Simulation is used in this paper, because it offers a very good tool for the estimation of probability in multivariate functions. Complicated probability and statistics problems are solved through computer aided simulations of a large number of tests. The procedures of structural reliability assessment for the bridge pier and the comparison with the partial factor method of the Eurocodes have been demonstrated in this paper.

  10. Measurement methods to assess diastasis of the rectus abdominis muscle (DRAM): A systematic review of their measurement properties and meta-analytic reliability generalisation.

    Science.gov (United States)

    van de Water, A T M; Benjamin, D R

    2016-02-01

    Systematic literature review. Diastasis of the rectus abdominis muscle (DRAM) has been linked with low back pain, abdominal and pelvic dysfunction. Measurement is used to either screen or to monitor DRAM width. Determining which methods are suitable for screening and monitoring DRAM is of clinical value. To identify the best methods to screen for DRAM presence and monitor DRAM width. AMED, Embase, Medline, PubMed and CINAHL databases were searched for measurement property studies of DRAM measurement methods. Population characteristics, measurement methods/procedures and measurement information were extracted from included studies. Quality of all studies was evaluated using 'quality rating criteria'. When possible, reliability generalisation was conducted to provide combined reliability estimations. Thirteen studies evaluated measurement properties of the 'finger width'-method, tape measure, calipers, ultrasound, CT and MRI. Ultrasound was most evaluated. Methodological quality of these studies varied widely. Pearson's correlations of r = 0.66-0.79 were found between calipers and ultrasound measurements. Calipers and ultrasound had Intraclass Correlation Coefficients (ICC) of 0.78-0.97 for test-retest, inter- and intra-rater reliability. The 'finger width'-method had weighted Kappa's of 0.73-0.77 for test-retest reliability, but moderate agreement (63%; weighted Kappa = 0.53) between raters. Comparing calipers and ultrasound, low measurement error was found (above the umbilicus), and the methods had good agreement (83%; weighted Kappa = 0.66) for discriminative purposes. The available information support ultrasound and calipers as adequate methods to assess DRAM. For other methods limited measurement information of low to moderate quality is available and further evaluation of their measurement properties is required. Copyright © 2015 Elsevier Ltd. All rights reserved.

  11. Application of analytical procedure on system reliability, GO-FLOW

    International Nuclear Information System (INIS)

    Matsuoka, Takeshi; Fukuto, Junji; Mitomo, Nobuo; Miyazaki, Keiko; Matsukura, Hiroshi; Kobayashi, Michiyuki

    2000-01-01

    In the Ship Research Institute, research and development of GO-FLOW procedure with various advanced functions as a system reliability analysis method occupying main part of the probabilistic safety assessment (PSA) were promoted. In this study, as an important evaluation technique on executing PSA with lower than level 3, by intending fundamental upgrading of the GO-FLOW procedure, a safety assessment system using the GO-FLOW as well as an analytical function coupling of dynamic behavior analytical function and physical behavior of the system with stochastic phenomenon change were developed. In 1998 fiscal year, preparation and verification of various functions such as dependence addition between the headings, rearrangement in order of time, positioning of same heading to plural positions, calculation of forming frequency with elapsing time were carried out. And, on a simulation analysis function of accident sequence, confirmation on analysis covering all of main accident sequence in the reactor for improved marine reactor, MRX was carried out. In addition, a function near automatically producible on input data for analysis was also prepared. As a result, the conventional analysis not always easy understanding on analytical results except an expert of PSA was solved, and understanding of the accident phenomenon, verification of validity on analysis, feedback to analysis, and feedback to design could be easily carried out. (G.K.)

  12. Evaluation of the quality of results obtained in institutions participating in interlaboratory experiments and of the reliability characteristics of the analytical methods used on the basis of certification of standard soil samples

    Energy Technology Data Exchange (ETDEWEB)

    Parshin, A.K.; Obol' yaninova, V.G.; Sul' dina, N.P.

    1986-08-20

    Rapid monitoring of the level of pollution of the environment and, especially, of soils necessitates preparation of standard samples (SS) close in properties and material composition to the objects to be analyzed. During 1978-1982 four sets (three types of samples in each) of State Standard Samples of different soils were developed: soddy-podzolic sandy-loamy, typical chernozem, krasnozem, and calcareous sierozem. The certification studies of the SS of the soils were carried out in accordance with the classical scheme of interlab experiment (ILE). More than 100 institutions were involved in the ILE and the total number of independent analytical results was of the order of 10/sup 4/. With such a volume of analytical information at their disposal they were able to find some general characteristics intrinsic to certification studies, to assess the quality of work of the ILE participants with due regard for their specialization, and the reliability characteristics of the analytical methods used.

  13. The analytic Lanczos method

    International Nuclear Information System (INIS)

    Witte, N.S.

    1998-01-01

    The classical formalism of the Moment Problem has been combined with a cumulant approach and applied to the extensive many-body problem. This has yielded many new exact results for many-body systems in the thermodynamic limit - for the ground state energy, for excited state gaps, and for arbitrary ground state averages. The method applies to any extensive Hamiltonian system, for any phase or symmetry arising in the model, whether on a lattice or in the continuum, and for any dimensionality. The theorems are of a nonperturbative nature with respect to any couplings occuring in the model. (Copyright (1998) World Scientific Publishing Co. Pte. Ltd)

  14. Effects of Analytical and Holistic Scoring Patterns on Scorer Reliability in Biology Essay Tests

    Science.gov (United States)

    Ebuoh, Casmir N.

    2018-01-01

    Literature revealed that the patterns/methods of scoring essay tests had been criticized for not being reliable and this unreliability is more likely to be more in internal examinations than in the external examinations. The purpose of this study is to find out the effects of analytical and holistic scoring patterns on scorer reliability in…

  15. Analytical methods under emergency conditions

    International Nuclear Information System (INIS)

    Sedlet, J.

    1983-01-01

    This lecture discusses methods for the radiochemical determination of internal contamination of the body under emergency conditions, here defined as a situation in which results on internal radioactive contamination are needed quickly. The purpose of speed is to determine the necessity for medical treatment to increase the natural elimination rate. Analytical methods discussed include whole-body counting, organ counting, wound monitoring, and excreta analysis. 12 references

  16. Waste minimization in analytical methods

    International Nuclear Information System (INIS)

    Green, D.W.; Smith, L.L.; Crain, J.S.; Boparai, A.S.; Kiely, J.T.; Yaeger, J.S. Schilling, J.B.

    1995-01-01

    The US Department of Energy (DOE) will require a large number of waste characterizations over a multi-year period to accomplish the Department's goals in environmental restoration and waste management. Estimates vary, but two million analyses annually are expected. The waste generated by the analytical procedures used for characterizations is a significant source of new DOE waste. Success in reducing the volume of secondary waste and the costs of handling this waste would significantly decrease the overall cost of this DOE program. Selection of appropriate analytical methods depends on the intended use of the resultant data. It is not always necessary to use a high-powered analytical method, typically at higher cost, to obtain data needed to make decisions about waste management. Indeed, for samples taken from some heterogeneous systems, the meaning of high accuracy becomes clouded if the data generated are intended to measure a property of this system. Among the factors to be considered in selecting the analytical method are the lower limit of detection, accuracy, turnaround time, cost, reproducibility (precision), interferences, and simplicity. Occasionally, there must be tradeoffs among these factors to achieve the multiple goals of a characterization program. The purpose of the work described here is to add waste minimization to the list of characteristics to be considered. In this paper the authors present results of modifying analytical methods for waste characterization to reduce both the cost of analysis and volume of secondary wastes. Although tradeoffs may be required to minimize waste while still generating data of acceptable quality for the decision-making process, they have data demonstrating that wastes can be reduced in some cases without sacrificing accuracy or precision

  17. Jet substructure with analytical methods

    Energy Technology Data Exchange (ETDEWEB)

    Dasgupta, Mrinal [University of Manchester, Consortium for Fundamental Physics, School of Physics and Astronomy, Manchester (United Kingdom); Fregoso, Alessandro; Powling, Alexander [University of Manchester, School of Physics and Astronomy, Manchester (United Kingdom); Marzani, Simone [Durham University, Institute for Particle Physics Phenomenology, Durham (United Kingdom)

    2013-11-15

    We consider the mass distribution of QCD jets after the application of jet-substructure methods, specifically the mass-drop tagger, pruning, trimming and their variants. In contrast to most current studies employing Monte Carlo methods, we carry out analytical calculations at the next-to-leading order level, which are sufficient to extract the dominant logarithmic behaviour for each technique, and compare our findings to exact fixed-order results. Our results should ultimately lead to a better understanding of these jet-substructure methods which in turn will influence the development of future substructure tools for LHC phenomenology. (orig.)

  18. Decision analytic methods in RODOS

    International Nuclear Information System (INIS)

    Borzenko, V.; French, S.

    1996-01-01

    In the event of a nuclear accident, RODOS seeks to provide decision support at all levels ranging from the largely descriptive to providing a detailed evaluation of the benefits and disadvantages of various countermeasure strategies and ranking them according to the societal preferences as perceived by the decision makers. To achieve this, it must draw upon several decision analytic methods and bring them together in a coherent manner so that the guidance offered to decision makers is consistent from one stage of an accident to the next. The methods used draw upon multi-attribute value and utility theories

  19. Analytical approach for confirming the achievement of LMFBR reliability goals

    International Nuclear Information System (INIS)

    Ingram, G.E.; Elerath, J.G.; Wood, A.P.

    1981-01-01

    The approach, recommended by GE-ARSD, for confirming the achievement of LMFBR reliability goals relies upon a comprehensive understanding of the physical and operational characteristics of the system and the environments to which the system will be subjected during its operational life. This kind of understanding is required for an approach based on system hardware testing or analyses, as recommended in this report. However, for a system as complex and expensive as the LMFBR, an approach which relies primarily on system hardware testing would be prohibitive both in cost and time to obtain the required system reliability test information. By using an analytical approach, results of tests (reliability and functional) at a low level within the specific system of interest, as well as results from other similar systems can be used to form the data base for confirming the achievement of the system reliability goals. This data, along with information relating to the design characteristics and operating environments of the specific system, will be used in the assessment of the system's reliability

  20. Design Protocols and Analytical Strategies that Incorporate Structural Reliability Models

    Science.gov (United States)

    Duffy, Stephen F.

    1997-01-01

    Ceramic matrix composites (CMC) and intermetallic materials (e.g., single crystal nickel aluminide) are high performance materials that exhibit attractive mechanical, thermal and chemical properties. These materials are critically important in advancing certain performance aspects of gas turbine engines. From an aerospace engineer's perspective the new generation of ceramic composites and intermetallics offers a significant potential for raising the thrust/weight ratio and reducing NO(x) emissions of gas turbine engines. These aspects have increased interest in utilizing these materials in the hot sections of turbine engines. However, as these materials evolve and their performance characteristics improve a persistent need exists for state-of-the-art analytical methods that predict the response of components fabricated from CMC and intermetallic material systems. This need provided the motivation for the technology developed under this research effort. Continuous ceramic fiber composites exhibit an increase in work of fracture, which allows for "graceful" rather than catastrophic failure. When loaded in the fiber direction, these composites retain substantial strength capacity beyond the initiation of transverse matrix cracking despite the fact that neither of its constituents would exhibit such behavior if tested alone. As additional load is applied beyond first matrix cracking, the matrix tends to break in a series of cracks bridged by the ceramic fibers. Any additional load is born increasingly by the fibers until the ultimate strength of the composite is reached. Thus modeling efforts supported under this research effort have focused on predicting this sort of behavior. For single crystal intermetallics the issues that motivated the technology development involved questions relating to material behavior and component design. Thus the research effort supported by this grant had to determine the statistical nature and source of fracture in a high strength, Ni

  1. 7 CFR 98.4 - Analytical methods.

    Science.gov (United States)

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Analytical methods. 98.4 Section 98.4 Agriculture....4 Analytical methods. (a) The majority of analytical methods used by the USDA laboratories to perform analyses of meat, meat food products and MRE's are listed as follows: (1) Official Methods of...

  2. 7 CFR 93.4 - Analytical methods.

    Science.gov (United States)

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Analytical methods. 93.4 Section 93.4 Agriculture... PROCESSED FRUITS AND VEGETABLES Citrus Juices and Certain Citrus Products § 93.4 Analytical methods. (a) The majority of analytical methods for citrus products are found in the Official Methods of Analysis of AOAC...

  3. 7 CFR 94.303 - Analytical methods.

    Science.gov (United States)

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Analytical methods. 94.303 Section 94.303 Agriculture... POULTRY AND EGG PRODUCTS Processed Poultry Products § 94.303 Analytical methods. The analytical methods... latest edition of the Official Methods of Analysis of AOAC INTERNATIONAL, Suite 500, 481 North Frederick...

  4. Analytical methods in rotor dynamics

    CERN Document Server

    Dimarogonas, Andrew D; Chondros, Thomas G

    2013-01-01

    The design and construction of rotating machinery operating at supercritical speeds was, in the 1920s, an event of revolutionary importance for the then new branch of dynamics known as rotor dynamics. In the 1960s, another revolution occurred: In less than a decade, imposed by operational and economic needs, an increase in the power of turbomachinery by one order of magnitude took place. Dynamic analysis of complex rotor forms became a necessity, while the importance of approximate methods for dynamic analysis was stressed. Finally, the emergence of fracture mechanics, as a new branch of applied mechanics, provided analytical tools to investigate crack influence on the dynamic behavior of rotors. The scope of this book is based on all these developments. No topics related to the well-known classical problems are included, rather the book deals exclusively with modern high-power turbomachinery.

  5. Nuclear analytical methods for platinum group elements

    International Nuclear Information System (INIS)

    2005-04-01

    Platinum group elements (PGE) are of special interest for analytical research due to their economic importance like chemical peculiarities as catalysts, medical applications as anticancer drugs, and possible environmental detrimental impact as exhaust from automobile catalyzers. Natural levels of PGE are so low in concentration that most of the current analytical techniques approach their limit of detection capacity. In addition, Ru, Rh, Pd, Re, Os, Ir, and Pt analyses still constitute a challenge in accuracy and precision of quantification in natural matrices. Nuclear analytical techniques, such as neutron activation analysis, X ray fluorescence, or proton-induced X ray emission (PIXE), which are generally considered as reference methods for many analytical problems, are useful as well. However, due to methodological restrictions, they can, in most cases, only be applied after pre-concentration and under special irradiation conditions. This report was prepared following a coordinated research project and a consultants meeting addressing the subject from different viewpoints. The experts involved suggested to discuss the issue according to the (1) application, hence, the concentration levels encountered, and (2) method applied for analysis. Each of the different fields of application needs special consideration for sample preparation, PGE pre-concentration, and determination. Additionally, each analytical method requires special attention regarding the sensitivity and sample type. Quality assurance/quality control aspects are considered towards the end of the report. It is intended to provide the reader of this publication with state-of-the-art information on the various aspects of PGE analysis and to advise which technique might be most suitable for a particular analytical problem related to platinum group elements. In particular, many case studies described in detail from the authors' laboratory experience might help to decide which way to go. As in many cases

  6. 7 CFR 94.103 - Analytical methods.

    Science.gov (United States)

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Analytical methods. 94.103 Section 94.103 Agriculture... POULTRY AND EGG PRODUCTS Voluntary Analyses of Egg Products § 94.103 Analytical methods. The analytical methods used by the Science and Technology Division laboratories to perform voluntary analyses for egg...

  7. 7 CFR 94.4 - Analytical methods.

    Science.gov (United States)

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Analytical methods. 94.4 Section 94.4 Agriculture... POULTRY AND EGG PRODUCTS Mandatory Analyses of Egg Products § 94.4 Analytical methods. The majority of analytical methods used by the USDA laboratories to perform mandatory analyses for egg products are listed as...

  8. Analytical methods used at model facility

    International Nuclear Information System (INIS)

    Wing, N.S.

    1984-01-01

    A description of analytical methods used at the model LEU Fuel Fabrication Facility is presented. The methods include gravimetric uranium analysis, isotopic analysis, fluorimetric analysis, and emission spectroscopy

  9. Nuclear analytical methods in the life sciences

    NARCIS (Netherlands)

    de Goeij, J.J.M.

    1994-01-01

    A survey is given of various nuclear analytical methods. The type of analytical information obtainable and advantageous features for application in the life sciences are briefly indicated. These features are: physically different basis of the analytical method, isotopic rather than elemental

  10. NUMERICAL AND ANALYTIC METHODS OF ESTIMATION BRIDGES’ CONSTRUCTIONS

    Directory of Open Access Journals (Sweden)

    Y. Y. Luchko

    2010-03-01

    Full Text Available In this article the numerical and analytical methods of calculation of the stressed-and-strained state of bridge constructions are considered. The task on increasing of reliability and accuracy of the numerical method and its solution by means of calculations in two bases are formulated. The analytical solution of the differential equation of deformation of a ferro-concrete plate under the action of local loads is also obtained.

  11. Evidential analytic hierarchy process dependence assessment methodology in human reliability analysis

    International Nuclear Information System (INIS)

    Chen, Lu Yuan; Zhou, Xinyi; Xiao, Fuyuan; Deng, Yong; Mahadevan, Sankaran

    2017-01-01

    In human reliability analysis, dependence assessment is an important issue in risky large complex systems, such as operation of a nuclear power plant. Many existing methods depend on an expert's judgment, which contributes to the subjectivity and restrictions of results. Recently, a computational method, based on the Dempster-Shafer evidence theory and analytic hierarchy process, has been proposed to handle the dependence in human reliability analysis. The model can deal with uncertainty in an analyst's judgment and reduce the subjectivity in the evaluation process. However, the computation is heavy and complicated to some degree. The most important issue is that the existing method is in a positive aspect, which may cause an underestimation of the risk. In this study, a new evidential analytic hierarchy process dependence assessment methodology, based on the improvement of existing methods, has been proposed, which is expected to be easier and more effective

  12. Evidential Analytic Hierarchy Process Dependence Assessment Methodology in Human Reliability Analysis

    Directory of Open Access Journals (Sweden)

    Luyuan Chen

    2017-02-01

    Full Text Available In human reliability analysis, dependence assessment is an important issue in risky large complex systems, such as operation of a nuclear power plant. Many existing methods depend on an expert's judgment, which contributes to the subjectivity and restrictions of results. Recently, a computational method, based on the Dempster–Shafer evidence theory and analytic hierarchy process, has been proposed to handle the dependence in human reliability analysis. The model can deal with uncertainty in an analyst's judgment and reduce the subjectivity in the evaluation process. However, the computation is heavy and complicated to some degree. The most important issue is that the existing method is in a positive aspect, which may cause an underestimation of the risk. In this study, a new evidential analytic hierarchy process dependence assessment methodology, based on the improvement of existing methods, has been proposed, which is expected to be easier and more effective.

  13. Evidential analytic hierarchy process dependence assessment methodology in human reliability analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chen, Lu Yuan; Zhou, Xinyi; Xiao, Fuyuan; Deng, Yong [School of Computer and Information Science, Southwest University, Chongqing (China); Mahadevan, Sankaran [School of Engineering, Vanderbilt University, Nashville (United States)

    2017-02-15

    In human reliability analysis, dependence assessment is an important issue in risky large complex systems, such as operation of a nuclear power plant. Many existing methods depend on an expert's judgment, which contributes to the subjectivity and restrictions of results. Recently, a computational method, based on the Dempster-Shafer evidence theory and analytic hierarchy process, has been proposed to handle the dependence in human reliability analysis. The model can deal with uncertainty in an analyst's judgment and reduce the subjectivity in the evaluation process. However, the computation is heavy and complicated to some degree. The most important issue is that the existing method is in a positive aspect, which may cause an underestimation of the risk. In this study, a new evidential analytic hierarchy process dependence assessment methodology, based on the improvement of existing methods, has been proposed, which is expected to be easier and more effective.

  14. Pre-analytical and analytical aspects affecting clinical reliability of plasma glucose results.

    Science.gov (United States)

    Pasqualetti, Sara; Braga, Federica; Panteghini, Mauro

    2017-07-01

    The measurement of plasma glucose (PG) plays a central role in recognizing disturbances in carbohydrate metabolism, with established decision limits that are globally accepted. This requires that PG results are reliable and unequivocally valid no matter where they are obtained. To control the pre-analytical variability of PG and prevent in vitro glycolysis, the use of citrate as rapidly effective glycolysis inhibitor has been proposed. However, the commercial availability of several tubes with studies showing different performance has created confusion among users. Moreover, and more importantly, studies have shown that tubes promptly inhibiting glycolysis give PG results that are significantly higher than tubes containing sodium fluoride only, used in the majority of studies generating the current PG cut-points, with a different clinical classification of subjects. From the analytical point of view, to be equivalent among different measuring systems, PG results should be traceable to a recognized higher-order reference via the implementation of an unbroken metrological hierarchy. In doing this, it is important that manufacturers of measuring systems consider the uncertainty accumulated through the different steps of the selected traceability chain. In particular, PG results should fulfil analytical performance specifications defined to fit the intended clinical application. Since PG has tight homeostatic control, its biological variability may be used to define these limits. Alternatively, given the central diagnostic role of the analyte, an outcome model showing the impact of analytical performance of test on clinical classifications of subjects can be used. Using these specifications, performance assessment studies employing commutable control materials with values assigned by reference procedure have shown that the quality of PG measurements is often far from desirable and that problems are exacerbated using point-of-care devices. Copyright © 2017 The Canadian

  15. Application of reliability methods in Ontario Hydro

    International Nuclear Information System (INIS)

    Jeppesen, R.; Ravishankar, T.J.

    1985-01-01

    Ontario Hydro have established a reliability program in support of its substantial nuclear program. Application of the reliability program to achieve both production and safety goals is described. The value of such a reliability program is evident in the record of Ontario Hydro's operating nuclear stations. The factors which have contributed to the success of the reliability program are identified as line management's commitment to reliability; selective and judicious application of reliability methods; establishing performance goals and monitoring the in-service performance; and collection, distribution, review and utilization of performance information to facilitate cost-effective achievement of goals and improvements. (orig.)

  16. Reactor Section standard analytical methods. Part 1

    Energy Technology Data Exchange (ETDEWEB)

    Sowden, D.

    1954-07-01

    the Standard Analytical Methods manual was prepared for the purpose of consolidating and standardizing all current analytical methods and procedures used in the Reactor Section for routine chemical analyses. All procedures are established in accordance with accepted practice and the general analytical methods specified by the Engineering Department. These procedures are specifically adapted to the requirements of the water treatment process and related operations. The methods included in this manual are organized alphabetically within the following five sections which correspond to the various phases of the analytical control program in which these analyses are to be used: water analyses, essential material analyses, cotton plug analyses boiler water analyses, and miscellaneous control analyses.

  17. 40 CFR 141.89 - Analytical methods.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 22 2010-07-01 2010-07-01 false Analytical methods. 141.89 Section 141...) NATIONAL PRIMARY DRINKING WATER REGULATIONS Control of Lead and Copper § 141.89 Analytical methods. (a... shall be conducted with the methods in § 141.23(k)(1). (1) Analyses for alkalinity, calcium...

  18. 40 CFR 141.704 - Analytical methods.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 22 2010-07-01 2010-07-01 false Analytical methods. 141.704 Section... Monitoring Requirements § 141.704 Analytical methods. (a) Cryptosporidium. Systems must analyze for Cryptosporidium using Method 1623: Cryptosporidium and Giardia in Water by Filtration/IMS/FA, 2005, United States...

  19. Review of Quantitative Software Reliability Methods

    Energy Technology Data Exchange (ETDEWEB)

    Chu, T.L.; Yue, M.; Martinez-Guridi, M.; Lehner, J.

    2010-09-17

    The current U.S. Nuclear Regulatory Commission (NRC) licensing process for digital systems rests on deterministic engineering criteria. In its 1995 probabilistic risk assessment (PRA) policy statement, the Commission encouraged the use of PRA technology in all regulatory matters to the extent supported by the state-of-the-art in PRA methods and data. Although many activities have been completed in the area of risk-informed regulation, the risk-informed analysis process for digital systems has not yet been satisfactorily developed. Since digital instrumentation and control (I&C) systems are expected to play an increasingly important role in nuclear power plant (NPP) safety, the NRC established a digital system research plan that defines a coherent set of research programs to support its regulatory needs. One of the research programs included in the NRC's digital system research plan addresses risk assessment methods and data for digital systems. Digital I&C systems have some unique characteristics, such as using software, and may have different failure causes and/or modes than analog I&C systems; hence, their incorporation into NPP PRAs entails special challenges. The objective of the NRC's digital system risk research is to identify and develop methods, analytical tools, and regulatory guidance for (1) including models of digital systems into NPP PRAs, and (2) using information on the risks of digital systems to support the NRC's risk-informed licensing and oversight activities. For several years, Brookhaven National Laboratory (BNL) has worked on NRC projects to investigate methods and tools for the probabilistic modeling of digital systems, as documented mainly in NUREG/CR-6962 and NUREG/CR-6997. However, the scope of this research principally focused on hardware failures, with limited reviews of software failure experience and software reliability methods. NRC also sponsored research at the Ohio State University investigating the modeling of

  20. Calculation of the reliability of large complex systems by the relevant path method

    International Nuclear Information System (INIS)

    Richter, G.

    1975-03-01

    In this paper, analytical methods are presented and tested with which the probabilistic reliability data of technical systems can be determined for given fault trees and block diagrams and known reliability data of the components. (orig./AK) [de

  1. HTGR analytical methods and design verification

    International Nuclear Information System (INIS)

    Neylan, A.J.; Northup, T.E.

    1982-05-01

    Analytical methods for the high-temperature gas-cooled reactor (HTGR) include development, update, verification, documentation, and maintenance of all computer codes for HTGR design and analysis. This paper presents selected nuclear, structural mechanics, seismic, and systems analytical methods related to the HTGR core. This paper also reviews design verification tests in the reactor core, reactor internals, steam generator, and thermal barrier

  2. An integrated approach to human reliability analysis -- decision analytic dynamic reliability model

    International Nuclear Information System (INIS)

    Holmberg, J.; Hukki, K.; Norros, L.; Pulkkinen, U.; Pyy, P.

    1999-01-01

    The reliability of human operators in process control is sensitive to the context. In many contemporary human reliability analysis (HRA) methods, this is not sufficiently taken into account. The aim of this article is that integration between probabilistic and psychological approaches in human reliability should be attempted. This is achieved first, by adopting such methods that adequately reflect the essential features of the process control activity, and secondly, by carrying out an interactive HRA process. Description of the activity context, probabilistic modeling, and psychological analysis form an iterative interdisciplinary sequence of analysis in which the results of one sub-task maybe input to another. The analysis of the context is carried out first with the help of a common set of conceptual tools. The resulting descriptions of the context promote the probabilistic modeling, through which new results regarding the probabilistic dynamics can be achieved. These can be incorporated in the context descriptions used as reference in the psychological analysis of actual performance. The results also provide new knowledge of the constraints of activity, by providing information of the premises of the operator's actions. Finally, the stochastic marked point process model gives a tool, by which psychological methodology may be interpreted and utilized for reliability analysis

  3. Nuclear analytical methods: Past, present and future

    International Nuclear Information System (INIS)

    Becker, D.A.

    1996-01-01

    The development of nuclear analytical methods as an analytical tool began in 1936 with the publication of the first paper on neutron activation analysis (NAA). This year, 1996, marks the 60th anniversary of that event. This paper attempts to look back at the nuclear analytical methods of the past, to look around and to see where the technology is right now, and finally, to look ahead to try and see where nuclear methods as an analytical technique (or as a group of analytical techniques) will be going in the future. The general areas which the author focuses on are: neutron activation analysis; prompt gamma neutron activation analysis (PGNAA); photon activation analysis (PAA); charged-particle activation analysis (CPAA)

  4. Analytical methods of radwaste characterization

    International Nuclear Information System (INIS)

    Garcia, C.M.

    1994-10-01

    In view of the need to carry out more extensive studies on the design of newly proposed methods for the treatment of radioactive wastes collected at PNRI, this study is aimed to provide a guide in the characterization of wastes which is a preparatory step for a well-planned waste processing. (auth.). 8 refs

  5. Analytical procedures for determining the impacts of reliability mitigation strategies.

    Science.gov (United States)

    2013-01-01

    Reliability of transport, especially the ability to reach a destination within a certain amount of time, is a regular concern of travelers and shippers. The definition of reliability used in this research is how travel time varies over time. The vari...

  6. Life cycle management of analytical methods.

    Science.gov (United States)

    Parr, Maria Kristina; Schmidt, Alexander H

    2018-01-05

    In modern process management, the life cycle concept gains more and more importance. It focusses on the total costs of the process from invest to operation and finally retirement. Also for analytical procedures an increasing interest for this concept exists in the recent years. The life cycle of an analytical method consists of design, development, validation (including instrumental qualification, continuous method performance verification and method transfer) and finally retirement of the method. It appears, that also regulatory bodies have increased their awareness on life cycle management for analytical methods. Thus, the International Council for Harmonisation of Technical Requirements for Pharmaceuticals for Human Use (ICH), as well as the United States Pharmacopeial Forum discuss the enrollment of new guidelines that include life cycle management of analytical methods. The US Pharmacopeia (USP) Validation and Verification expert panel already proposed a new General Chapter 〈1220〉 "The Analytical Procedure Lifecycle" for integration into USP. Furthermore, also in the non-regulated environment a growing interest on life cycle management is seen. Quality-by-design based method development results in increased method robustness. Thereby a decreased effort is needed for method performance verification, and post-approval changes as well as minimized risk of method related out-of-specification results. This strongly contributes to reduced costs of the method during its life cycle. Copyright © 2017 Elsevier B.V. All rights reserved.

  7. A New Method to Study Analytic Inequalities

    Directory of Open Access Journals (Sweden)

    Xiao-Ming Zhang

    2010-01-01

    Full Text Available We present a new method to study analytic inequalities involving n variables. Regarding its applications, we proved some well-known inequalities and improved Carleman's inequality.

  8. A Method of Nuclear Software Reliability Estimation

    International Nuclear Information System (INIS)

    Park, Gee Yong; Eom, Heung Seop; Cheon, Se Woo; Jang, Seung Cheol

    2011-01-01

    A method on estimating software reliability for nuclear safety software is proposed. This method is based on the software reliability growth model (SRGM) where the behavior of software failure is assumed to follow the non-homogeneous Poisson process. Several modeling schemes are presented in order to estimate and predict more precisely the number of software defects based on a few of software failure data. The Bayesian statistical inference is employed to estimate the model parameters by incorporating the software test cases into the model. It is identified that this method is capable of accurately estimating the remaining number of software defects which are on-demand type directly affecting safety trip functions. The software reliability can be estimated from a model equation and one method of obtaining the software reliability is proposed

  9. Analytical modeling of nuclear power station operator reliability

    International Nuclear Information System (INIS)

    Sabri, Z.A.; Husseiny, A.A.

    1979-01-01

    The operator-plant interface is a critical component of power stations which requires the formulation of mathematical models to be applied in plant reliability analysis. The human model introduced here is based on cybernetic interactions and allows for use of available data from psychological experiments, hot and cold training and normal operation. The operator model is identified and integrated in the control and protection systems. The availability and reliability are given for different segments of the operator task and for specific periods of the operator life: namely, training, operation and vigilance or near retirement periods. The results can be easily and directly incorporated in system reliability analysis. (author)

  10. Measurement of HDO Products Using GC-TCD: Towards Obtaining Reliable Analytical Data

    Directory of Open Access Journals (Sweden)

    Zuas Oman

    2018-03-01

    Full Text Available This paper reported the method development and validation of a gas chromatography with thermal conductivity detector (GC-TCD method for the measurement of the gaseous products of hydrodeoxygenation (HDO. The method validation parameters include selectivity, precision (repeatability and reproducibility, accuracy, linearity, limit of detection (LoD, limit of quantitation (LoQ, and robustness. The results showed that the developed method was able to separate the target components (H2, CO2, CH4 and CO from their mixtures without any special sample treatment. The validated method was selective, precise, accurate, and robust. Application of the developed and validated GC-TCD method to the measurement of by-product components of HDO of bio-oil revealed a good performance with relative standard deviation (RSD less than 1.0% for all target components, implying that the process of method development and validation provides a trustworthy way of obtaining reliable analytical data.

  11. Mathematical methods for physical and analytical chemistry

    CERN Document Server

    Goodson, David Z

    2011-01-01

    Mathematical Methods for Physical and Analytical Chemistry presents mathematical and statistical methods to students of chemistry at the intermediate, post-calculus level. The content includes a review of general calculus; a review of numerical techniques often omitted from calculus courses, such as cubic splines and Newton's method; a detailed treatment of statistical methods for experimental data analysis; complex numbers; extrapolation; linear algebra; and differential equations. With numerous example problems and helpful anecdotes, this text gives chemistry students the mathematical

  12. A Novel Analytic Technique for the Service Station Reliability in a Discrete-Time Repairable Queue

    Directory of Open Access Journals (Sweden)

    Renbin Liu

    2013-01-01

    Full Text Available This paper presents a decomposition technique for the service station reliability in a discrete-time repairable GeomX/G/1 queueing system, in which the server takes exhaustive service and multiple adaptive delayed vacation discipline. Using such a novel analytic technique, some important reliability indices and reliability relation equations of the service station are derived. Furthermore, the structures of the service station indices are also found. Finally, special cases and numerical examples validate the derived results and show that our analytic technique is applicable to reliability analysis of some complex discrete-time repairable bulk arrival queueing systems.

  13. Statistically qualified neuro-analytic failure detection method and system

    Science.gov (United States)

    Vilim, Richard B.; Garcia, Humberto E.; Chen, Frederick W.

    2002-03-02

    An apparatus and method for monitoring a process involve development and application of a statistically qualified neuro-analytic (SQNA) model to accurately and reliably identify process change. The development of the SQNA model is accomplished in two stages: deterministic model adaption and stochastic model modification of the deterministic model adaptation. Deterministic model adaption involves formulating an analytic model of the process representing known process characteristics, augmenting the analytic model with a neural network that captures unknown process characteristics, and training the resulting neuro-analytic model by adjusting the neural network weights according to a unique scaled equation error minimization technique. Stochastic model modification involves qualifying any remaining uncertainty in the trained neuro-analytic model by formulating a likelihood function, given an error propagation equation, for computing the probability that the neuro-analytic model generates measured process output. Preferably, the developed SQNA model is validated using known sequential probability ratio tests and applied to the process as an on-line monitoring system. Illustrative of the method and apparatus, the method is applied to a peristaltic pump system.

  14. A method of predicting the reliability of CDM coil insulation

    International Nuclear Information System (INIS)

    Kytasty, A.; Ogle, C.; Arrendale, H.

    1992-01-01

    This paper presents a method of predicting the reliability of the Collider Dipole Magnet (CDM) coil insulation design. The method proposes a probabilistic treatment of electrical test data, stress analysis, material properties variability and loading uncertainties to give the reliability estimate. The approach taken to predict reliability of design related failure modes of the CDM is to form analytical models of the various possible failure modes and their related mechanisms or causes, and then statistically assess the contributions of the various contributing variables. The probability of the failure mode occurring is interpreted as the number of times one would expect certain extreme situations to combine and randomly occur. One of the more complex failure modes of the CDM will be used to illustrate this methodology

  15. Analytical method for solving radioactive transformations

    International Nuclear Information System (INIS)

    Vudakin, Z.

    1999-01-01

    Analytical method for solving radioactive transformations is presented in this paper. High accuracy series expansion of the depletion function and nonsingular Bateman coefficients are used to overcome numerical difficulties when applying well-known Bateman solution of a simple radioactive decay. Generality and simplicity of the method are found to be useful in evaluating nuclide chains with one hundred or more nuclides in the chain. Method enables evaluation of complete chain, without elimination of short-lives nuclides. It is efficient and accurate

  16. 7 CFR 93.13 - Analytical methods.

    Science.gov (United States)

    2010-01-01

    ... No. 1, USDA, Agricultural Marketing Service, Science and Technology, 3521 South Agriculture Building... 7 Agriculture 3 2010-01-01 2010-01-01 false Analytical methods. 93.13 Section 93.13 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards...

  17. Biodiesel Analytical Methods: August 2002--January 2004

    Energy Technology Data Exchange (ETDEWEB)

    Van Gerpen, J.; Shanks, B.; Pruszko, R.; Clements, D.; Knothe, G.

    2004-07-01

    Biodiesel is an alternative fuel for diesel engines that is receiving great attention worldwide. The material contained in this book is intended to provide the reader with information about biodiesel engines and fuels, analytical methods used to measure fuel properties, and specifications for biodiesel quality control.

  18. Prioritizing pesticide compounds for analytical methods development

    Science.gov (United States)

    Norman, Julia E.; Kuivila, Kathryn; Nowell, Lisa H.

    2012-01-01

    The U.S. Geological Survey (USGS) has a periodic need to re-evaluate pesticide compounds in terms of priorities for inclusion in monitoring and studies and, thus, must also assess the current analytical capabilities for pesticide detection. To meet this need, a strategy has been developed to prioritize pesticides and degradates for analytical methods development. Screening procedures were developed to separately prioritize pesticide compounds in water and sediment. The procedures evaluate pesticide compounds in existing USGS analytical methods for water and sediment and compounds for which recent agricultural-use information was available. Measured occurrence (detection frequency and concentrations) in water and sediment, predicted concentrations in water and predicted likelihood of occurrence in sediment, potential toxicity to aquatic life or humans, and priorities of other agencies or organizations, regulatory or otherwise, were considered. Several existing strategies for prioritizing chemicals for various purposes were reviewed, including those that identify and prioritize persistent, bioaccumulative, and toxic compounds, and those that determine candidates for future regulation of drinking-water contaminants. The systematic procedures developed and used in this study rely on concepts common to many previously established strategies. The evaluation of pesticide compounds resulted in the classification of compounds into three groups: Tier 1 for high priority compounds, Tier 2 for moderate priority compounds, and Tier 3 for low priority compounds. For water, a total of 247 pesticide compounds were classified as Tier 1 and, thus, are high priority for inclusion in analytical methods for monitoring and studies. Of these, about three-quarters are included in some USGS analytical method; however, many of these compounds are included on research methods that are expensive and for which there are few data on environmental samples. The remaining quarter of Tier 1

  19. Analytical detection methods for irradiated foods

    International Nuclear Information System (INIS)

    1991-03-01

    The present publication is a review of scientific literature on the analytical identification of foods treated with ionizing radiation and the quantitative determination of absorbed dose of radiation. Because of the extremely low level of chemical changes resulting from irradiation or because of the lack of specificity to irradiation of any chemical changes, a few methods of quantitative determination of absorbed dose have shown promise until now. On the other hand, the present review has identified several possible methods, which could be used, following further research and testing, for the identification of irradiated foods. An IAEA Co-ordinated Research Programme on Analytical Detection Methods for Irradiation Treatment of Food ('ADMIT'), established in 1990, is currently investigating many of the methods cited in the present document. Refs and tab

  20. Workshop on Analytical Methods in Statistics

    CERN Document Server

    Jurečková, Jana; Maciak, Matúš; Pešta, Michal

    2017-01-01

    This volume collects authoritative contributions on analytical methods and mathematical statistics. The methods presented include resampling techniques; the minimization of divergence; estimation theory and regression, eventually under shape or other constraints or long memory; and iterative approximations when the optimal solution is difficult to achieve. It also investigates probability distributions with respect to their stability, heavy-tailness, Fisher information and other aspects, both asymptotically and non-asymptotically. The book not only presents the latest mathematical and statistical methods and their extensions, but also offers solutions to real-world problems including option pricing. The selected, peer-reviewed contributions were originally presented at the workshop on Analytical Methods in Statistics, AMISTAT 2015, held in Prague, Czech Republic, November 10-13, 2015.

  1. Systems and Methods for Composable Analytics

    Science.gov (United States)

    2014-04-29

    simplistic module that performs a mathematical operation on two numbers. The most important method is the Execute() method. This will get called when it is...addition, an input control is also specified in the example below. In this example, the mathematical operator can only be chosen from a preconfigured...approaches. Some of the industries that could benefit from Composable Analytics include pharmaceuticals, health care, insurance, actuaries , and

  2. Reliability of Estimation Pile Load Capacity Methods

    Directory of Open Access Journals (Sweden)

    Yudhi Lastiasih

    2014-04-01

    Full Text Available None of numerous previous methods for predicting pile capacity is known how accurate any of them are when compared with the actual ultimate capacity of piles tested to failure. The author’s of the present paper have conducted such an analysis, based on 130 data sets of field loading tests. Out of these 130 data sets, only 44 could be analysed, of which 15 were conducted until the piles actually reached failure. The pile prediction methods used were: Brinch Hansen’s method (1963, Chin’s method (1970, Decourt’s Extrapolation Method (1999, Mazurkiewicz’s method (1972, Van der Veen’s method (1953, and the Quadratic Hyperbolic Method proposed by Lastiasih et al. (2012. It was obtained that all the above methods were sufficiently reliable when applied to data from pile loading tests that loaded to reach failure. However, when applied to data from pile loading tests that loaded without reaching failure, the methods that yielded lower values for correction factor N are more recommended. Finally, the empirical method of Reese and O’Neill (1988 was found to be reliable enough to be used to estimate the Qult of a pile foundation based on soil data only.

  3. Reliability of stellar inclination estimated from asteroseismology: analytical criteria, mock simulations and Kepler data analysis

    Science.gov (United States)

    Kamiaka, Shoya; Benomar, Othman; Suto, Yasushi

    2018-05-01

    Advances in asteroseismology of solar-like stars, now provide a unique method to estimate the stellar inclination i⋆. This enables to evaluate the spin-orbit angle of transiting planetary systems, in a complementary fashion to the Rossiter-McLaughlineffect, a well-established method to estimate the projected spin-orbit angle λ. Although the asteroseismic method has been broadly applied to the Kepler data, its reliability has yet to be assessed intensively. In this work, we evaluate the accuracy of i⋆ from asteroseismology of solar-like stars using 3000 simulated power spectra. We find that the low signal-to-noise ratio of the power spectra induces a systematic under-estimate (over-estimate) bias for stars with high (low) inclinations. We derive analytical criteria for the reliable asteroseismic estimate, which indicates that reliable measurements are possible in the range of 20° ≲ i⋆ ≲ 80° only for stars with high signal-to-noise ratio. We also analyse and measure the stellar inclination of 94 Kepler main-sequence solar-like stars, among which 33 are planetary hosts. According to our reliability criteria, a third of them (9 with planets, 22 without) have accurate stellar inclination. Comparison of our asteroseismic estimate of vsin i⋆ against spectroscopic measurements indicates that the latter suffers from a large uncertainty possibly due to the modeling of macro-turbulence, especially for stars with projected rotation speed vsin i⋆ ≲ 5km/s. This reinforces earlier claims, and the stellar inclination estimated from the combination of measurements from spectroscopy and photometric variation for slowly rotating stars needs to be interpreted with caution.

  4. Secondary waste minimization in analytical methods

    International Nuclear Information System (INIS)

    Green, D.W.; Smith, L.L.; Crain, J.S.; Boparai, A.S.; Kiely, J.T.; Yaeger, J.S.; Schilling, J.B.

    1995-01-01

    The characterization phase of site remediation is an important and costly part of the process. Because toxic solvents and other hazardous materials are used in common analytical methods, characterization is also a source of new waste, including mixed waste. Alternative analytical methods can reduce the volume or form of hazardous waste produced either in the sample preparation step or in the measurement step. The authors are examining alternative methods in the areas of inorganic, radiological, and organic analysis. For determining inorganic constituents, alternative methods were studied for sample introduction into inductively coupled plasma spectrometers. Figures of merit for the alternative methods, as well as their associated waste volumes, were compared with the conventional approaches. In the radiological area, the authors are comparing conventional methods for gross α/β measurements of soil samples to an alternative method that uses high-pressure microwave dissolution. For determination of organic constituents, microwave-assisted extraction was studied for RCRA regulated semivolatile organics in a variety of solid matrices, including spiked samples in blank soil; polynuclear aromatic hydrocarbons in soils, sludges, and sediments; and semivolatile organics in soil. Extraction efficiencies were determined under varying conditions of time, temperature, microwave power, moisture content, and extraction solvent. Solvent usage was cut from the 300 mL used in conventional extraction methods to about 30 mL. Extraction results varied from one matrix to another. In most cases, the microwave-assisted extraction technique was as efficient as the more common Soxhlet or sonication extraction techniques

  5. Reliability and risk analysis methods research plan

    International Nuclear Information System (INIS)

    1984-10-01

    This document presents a plan for reliability and risk analysis methods research to be performed mainly by the Reactor Risk Branch (RRB), Division of Risk Analysis and Operations (DRAO), Office of Nuclear Regulatory Research. It includes those activities of other DRAO branches which are very closely related to those of the RRB. Related or interfacing programs of other divisions, offices and organizations are merely indicated. The primary use of this document is envisioned as an NRC working document, covering about a 3-year period, to foster better coordination in reliability and risk analysis methods development between the offices of Nuclear Regulatory Research and Nuclear Reactor Regulation. It will also serve as an information source for contractors and others to more clearly understand the objectives, needs, programmatic activities and interfaces together with the overall logical structure of the program

  6. An analytical framework for reliability growth of one-shot systems

    International Nuclear Information System (INIS)

    Hall, J. Brian; Mosleh, Ali

    2008-01-01

    In this paper, we introduce a new reliability growth methodology for one-shot systems that is applicable to the case where all corrective actions are implemented at the end of the current test phase. The methodology consists of four model equations for assessing: expected reliability, the expected number of failure modes observed in testing, the expected probability of discovering new failure modes, and the expected portion of system unreliability associated with repeat failure modes. These model equations provide an analytical framework for which reliability practitioners can estimate reliability improvement, address goodness-of-fit concerns, quantify programmatic risk, and assess reliability maturity of one-shot systems. A numerical example is given to illustrate the value and utility of the presented approach. This methodology is useful to program managers and reliability practitioners interested in applying the techniques above in their reliability growth program

  7. Comparison of nuclear analytical methods with competitive methods

    International Nuclear Information System (INIS)

    1987-10-01

    The use of nuclear analytical techniques, especially neutron activation analysis, already have a 50 year old history. Today several sensitive and accurate, non-nuclear trace element analytical techniques are available and new methods are continuously developed. The IAEA is supporting the development of nuclear analytical laboratories in its Member States. In order to be able to advise the developing countries which methods to use in different applications, it is important to know the present status and development trends of nuclear analytical methods, what are their benefits, drawbacks and recommended fields of application, compared with other, non-nuclear techniques. In order to get an answer to these questions the IAEA convened this Advisory Group Meeting. This volume is the outcome of the presentations and discussions of the meeting. A separate abstract was prepared for each of the 21 papers. Refs, figs, tabs

  8. An exact method for solving logical loops in reliability analysis

    International Nuclear Information System (INIS)

    Matsuoka, Takeshi

    2009-01-01

    This paper presents an exact method for solving logical loops in reliability analysis. The systems that include logical loops are usually described by simultaneous Boolean equations. First, present a basic rule of solving simultaneous Boolean equations. Next, show the analysis procedures for three-component system with external supports. Third, more detailed discussions are given for the establishment of logical loop relation. Finally, take up two typical structures which include more than one logical loop. Their analysis results and corresponding GO-FLOW charts are given. The proposed analytical method is applicable to loop structures that can be described by simultaneous Boolean equations, and it is very useful in evaluating the reliability of complex engineering systems.

  9. Directory of Analytical Methods, Department 1820

    International Nuclear Information System (INIS)

    Whan, R.E.

    1986-01-01

    The Materials Characterization Department performs chemical, physical, and thermophysical analyses in support of programs throughout the Laboratories. The department has a wide variety of techniques and instruments staffed by experienced personnel available for these analyses, and we strive to maintain near state-of-the-art technology by continued updates. We have prepared this Directory of Analytical Methods in order to acquaint you with our capabilities and to help you identify personnel who can assist with your analytical needs. The descriptions of the various capabilities are requester-oriented and have been limited in length and detail. Emphasis has been placed on applications and limitations with notations of estimated analysis time and alternative or related techniques. A short, simplified discussion of underlying principles is also presented along with references if more detail is desired. The contents of this document have been organized in the order: bulky analysis, microanalysis, surface analysis, optical and thermal property measurements

  10. Modern methods in analytical acoustics lecture notes

    CERN Document Server

    Crighton, D G; Williams, J E Ffowcs; Heckl, M; Leppington, F G

    1992-01-01

    Modern Methods in Analytical Acoustics considers topics fundamental to the understanding of noise, vibration and fluid mechanisms. The series of lectures on which this material is based began by some twenty five years ago and has been developed and expanded ever since. Acknowledged experts in the field have given this course many times in Europe and the USA. Although the scope of the course has widened considerably, the primary aim of teaching analytical techniques of acoustics alongside specific areas of wave motion and unsteady fluid mechanisms remains. The distinguished authors of this volume are drawn from Departments of Acoustics, Engineering of Applied Mathematics in Berlin, Cambridge and London. Their intention is to reach a wider audience of all those concerned with acoustic analysis than has been able to attend the course.

  11. Big data analytics methods and applications

    CERN Document Server

    Rao, BLS; Rao, SB

    2016-01-01

    This book has a collection of articles written by Big Data experts to describe some of the cutting-edge methods and applications from their respective areas of interest, and provides the reader with a detailed overview of the field of Big Data Analytics as it is practiced today. The chapters cover technical aspects of key areas that generate and use Big Data such as management and finance; medicine and healthcare; genome, cytome and microbiome; graphs and networks; Internet of Things; Big Data standards; bench-marking of systems; and others. In addition to different applications, key algorithmic approaches such as graph partitioning, clustering and finite mixture modelling of high-dimensional data are also covered. The varied collection of themes in this volume introduces the reader to the richness of the emerging field of Big Data Analytics.

  12. Analytical chromatography. Methods, instrumentation and applications

    International Nuclear Information System (INIS)

    Yashin, Ya I; Yashin, A Ya

    2006-01-01

    The state-of-the-art and the prospects in the development of main methods of analytical chromatography, viz., gas, high performance liquid and ion chromatographic techniques, are characterised. Achievements of the past 10-15 years in the theory and general methodology of chromatography and also in the development of new sorbents, columns and chromatographic instruments are outlined. The use of chromatography in the environmental control, biology, medicine, pharmaceutics, and also for monitoring the quality of foodstuffs and products of chemical, petrochemical and gas industries, etc. is considered.

  13. The Emergence of the Analytical Method

    DEFF Research Database (Denmark)

    Plum, Maja

    2012-01-01

    accountability, visibility and documentation. It is argued that pedagogy is generated as a sequential and unit-specified way of working on the production of ‘the learning child’, forming a time- and material-optimising approach. Hereby, the nursery teacher, as a daily scientific researcher, comes to serve...... the nation by an ongoing observational intervention, producing the learning foundation for the entrepreneurial citizen, and thus the nation as a knowledge society in a globalised world. This is what this article terms the emergence of the analytical method....

  14. Analytical N beam position monitor method

    Directory of Open Access Journals (Sweden)

    A. Wegscheider

    2017-11-01

    Full Text Available Measurement and correction of focusing errors is of great importance for performance and machine protection of circular accelerators. Furthermore LHC needs to provide equal luminosities to the experiments ATLAS and CMS. High demands are also set on the speed of the optics commissioning, as the foreseen operation with β^{*}-leveling on luminosity will require many operational optics. A fast measurement of the β-function around a storage ring is usually done by using the measured phase advance between three consecutive beam position monitors (BPMs. A recent extension of this established technique, called the N-BPM method, was successfully applied for optics measurements at CERN, ALBA, and ESRF. We present here an improved algorithm that uses analytical calculations for both random and systematic errors and takes into account the presence of quadrupole, sextupole, and BPM misalignments, in addition to quadrupolar field errors. This new scheme, called the analytical N-BPM method, is much faster, further improves the measurement accuracy, and is applicable to very pushed beam optics where the existing numerical N-BPM method tends to fail.

  15. Analytical N beam position monitor method

    Science.gov (United States)

    Wegscheider, A.; Langner, A.; Tomás, R.; Franchi, A.

    2017-11-01

    Measurement and correction of focusing errors is of great importance for performance and machine protection of circular accelerators. Furthermore LHC needs to provide equal luminosities to the experiments ATLAS and CMS. High demands are also set on the speed of the optics commissioning, as the foreseen operation with β*-leveling on luminosity will require many operational optics. A fast measurement of the β -function around a storage ring is usually done by using the measured phase advance between three consecutive beam position monitors (BPMs). A recent extension of this established technique, called the N-BPM method, was successfully applied for optics measurements at CERN, ALBA, and ESRF. We present here an improved algorithm that uses analytical calculations for both random and systematic errors and takes into account the presence of quadrupole, sextupole, and BPM misalignments, in addition to quadrupolar field errors. This new scheme, called the analytical N-BPM method, is much faster, further improves the measurement accuracy, and is applicable to very pushed beam optics where the existing numerical N-BPM method tends to fail.

  16. A Hybrid Approach for Reliability Analysis Based on Analytic Hierarchy Process and Bayesian Network

    International Nuclear Information System (INIS)

    Zubair, Muhammad

    2014-01-01

    By using analytic hierarchy process (AHP) and Bayesian Network (BN) the present research signifies the technical and non-technical issues of nuclear accidents. The study exposed that the technical faults was one major reason of these accidents. Keep an eye on other point of view it becomes clearer that human behavior like dishonesty, insufficient training, and selfishness are also play a key role to cause these accidents. In this study, a hybrid approach for reliability analysis based on AHP and BN to increase nuclear power plant (NPP) safety has been developed. By using AHP, best alternative to improve safety, design, operation, and to allocate budget for all technical and non-technical factors related with nuclear safety has been investigated. We use a special structure of BN based on the method AHP. The graphs of the BN and the probabilities associated with nodes are designed to translate the knowledge of experts on the selection of best alternative. The results show that the improvement in regulatory authorities will decrease failure probabilities and increase safety and reliability in industrial area.

  17. The analytic nodal method in cylindrical geometry

    International Nuclear Information System (INIS)

    Prinsloo, Rian H.; Tomasevic, Djordje I.

    2008-01-01

    Nodal diffusion methods have been used extensively in nuclear reactor calculations, specifically for their performance advantage, but also for their superior accuracy. More specifically, the Analytic Nodal Method (ANM), utilising the transverse integration principle, has been applied to numerous reactor problems with much success. In this work, a nodal diffusion method is developed for cylindrical geometry. Application of this method to three-dimensional (3D) cylindrical geometry has never been satisfactorily addressed and we propose a solution which entails the use of conformal mapping. A set of 1D-equations with an adjusted, geometrically dependent, inhomogeneous source, is obtained. This work describes the development of the method and associated test code, as well as its application to realistic reactor problems. Numerical results are given for the PBMR-400 MW benchmark problem, as well as for a 'cylindrisized' version of the well-known 3D LWR IAEA benchmark. Results highlight the improved accuracy and performance over finite-difference core solutions and investigate the applicability of nodal methods to 3D PBMR type problems. Results indicate that cylindrical nodal methods definitely have a place within PBMR applications, yielding performance advantage factors of 10 and 20 for 2D and 3D calculations, respectively, and advantage factors of the order of 1000 in the case of the LWR problem

  18. FORECASTING PILE SETTLEMENT ON CLAYSTONE USING NUMERICAL AND ANALYTICAL METHODS

    Directory of Open Access Journals (Sweden)

    Ponomarev Andrey Budimirovich

    2016-06-01

    Full Text Available In the article the problem of designing pile foundations on claystones is reviewed. The purpose of this paper is comparative analysis of the analytical and numerical methods for forecasting the settlement of piles on claystones. The following tasks were solved during the study: 1 The existing researches of pile settlement are analyzed; 2 The characteristics of experimental studies and the parameters for numerical modeling are presented, methods of field research of single piles’ operation are described; 3 Calculation of single pile settlement is performed using numerical methods in the software package Plaxis 2D and analytical method according to the requirements SP 24.13330.2011; 4 Experimental data is compared with the results of analytical and numerical calculations; 5 Basing on these results recommendations for forecasting pile settlement on claystone are presented. Much attention is paid to the calculation of pile settlement considering the impacted areas in ground space beside pile and the comparison with the results of field experiments. Basing on the obtained results, for the prediction of settlement of single pile on claystone the authors recommend using the analytical method considered in SP 24.13330.2011 with account for the impacted areas in ground space beside driven pile. In the case of forecasting the settlement of single pile on claystone by numerical methods in Plaxis 2D the authors recommend using the Hardening Soil model considering the impacted areas in ground space beside the driven pile. The analyses of the results and calculations are presented for examination and verification; therefore it is necessary to continue the research work of deep foundation at another experimental sites to improve the reliability of the calculation of pile foundation settlement. The work is of great interest for geotechnical engineers engaged in research, design and construction of pile foundations.

  19. Analytical method for establishing indentation rolling resistance

    Directory of Open Access Journals (Sweden)

    Gładysiewicz Lech

    2018-01-01

    Full Text Available Belt conveyors are highly reliable machines able to work in special operating conditions. Harsh environment, long distance of transporting and great mass of transported martials are cause of high energy usage. That is why research in the field of belt conveyor transportation nowadays focuses on reducing the power consumption without lowering their efficiency. In this paper, previous methods for testing rolling resistance are described, and new method designed by authors was presented. New method of testing rolling resistance is quite simple and inexpensive. Moreover it allows to conduct the experimental tests of the impact of different parameters on the value of indentation rolling resistance such as core design, cover thickness, ambient temperature, idler travel frequency, or load value as well. Finally results of tests of relationship between rolling resistance and idler travel frequency and between rolling resistance and idler travel speed was presented.

  20. Analytical method for establishing indentation rolling resistance

    Science.gov (United States)

    Gładysiewicz, Lech; Konieczna, Martyna

    2018-01-01

    Belt conveyors are highly reliable machines able to work in special operating conditions. Harsh environment, long distance of transporting and great mass of transported martials are cause of high energy usage. That is why research in the field of belt conveyor transportation nowadays focuses on reducing the power consumption without lowering their efficiency. In this paper, previous methods for testing rolling resistance are described, and new method designed by authors was presented. New method of testing rolling resistance is quite simple and inexpensive. Moreover it allows to conduct the experimental tests of the impact of different parameters on the value of indentation rolling resistance such as core design, cover thickness, ambient temperature, idler travel frequency, or load value as well. Finally results of tests of relationship between rolling resistance and idler travel frequency and between rolling resistance and idler travel speed was presented.

  1. Structural reliability methods: Code development status

    Science.gov (United States)

    Millwater, Harry R.; Thacker, Ben H.; Wu, Y.-T.; Cruse, T. A.

    1991-05-01

    The Probabilistic Structures Analysis Method (PSAM) program integrates state of the art probabilistic algorithms with structural analysis methods in order to quantify the behavior of Space Shuttle Main Engine structures subject to uncertain loadings, boundary conditions, material parameters, and geometric conditions. An advanced, efficient probabilistic structural analysis software program, NESSUS (Numerical Evaluation of Stochastic Structures Under Stress) was developed as a deliverable. NESSUS contains a number of integrated software components to perform probabilistic analysis of complex structures. A nonlinear finite element module NESSUS/FEM is used to model the structure and obtain structural sensitivities. Some of the capabilities of NESSUS/FEM are shown. A Fast Probability Integration module NESSUS/FPI estimates the probability given the structural sensitivities. A driver module, PFEM, couples the FEM and FPI. NESSUS, version 5.0, addresses component reliability, resistance, and risk.

  2. Radiochemical methods. Analytical chemistry by open learning

    Energy Technology Data Exchange (ETDEWEB)

    Geary, W.J.; James, A.M. (ed.)

    1986-01-01

    This book presents the analytical uses of radioactive isotopes within the context of radiochemistry as a whole. It is designed for scientists with relatively little background knowledge of the subject. Thus the initial emphasis is on developing the basic concepts of radioactive decay, particularly as they affect the potential usage of radioisotopes. Discussion of the properties of various types of radiation, and of factors such as half-life, is related to practical considerations such as counting and preparation methods, and handling/disposal problems. Practical aspects are then considered in more detail, and the various radioanalytical methods are outlined with particular reference to their applicability. The approach is 'user friendly' and the use of self assessment questions allows the reader to test his/her understanding of individual sections easily. For those who wish to develop their knowledge further, a reading list is provided.

  3. Numerical methods: Analytical benchmarking in transport theory

    International Nuclear Information System (INIS)

    Ganapol, B.D.

    1988-01-01

    Numerical methods applied to reactor technology have reached a high degree of maturity. Certainly one- and two-dimensional neutron transport calculations have become routine, with several programs available on personal computer and the most widely used programs adapted to workstation and minicomputer computational environments. With the introduction of massive parallelism and as experience with multitasking increases, even more improvement in the development of transport algorithms can be expected. Benchmarking an algorithm is usually not a very pleasant experience for the code developer. Proper algorithmic verification by benchmarking involves the following considerations: (1) conservation of particles, (2) confirmation of intuitive physical behavior, and (3) reproduction of analytical benchmark results. By using today's computational advantages, new basic numerical methods have been developed that allow a wider class of benchmark problems to be considered

  4. Detection of food irradiation - two analytical methods

    International Nuclear Information System (INIS)

    1994-01-01

    This publication summarizes the activities of Nordic countries in the field of detection of irradiated food. The National Food Agency of Denmark has coordinated the project. The two analytical methods investigated were: the gas-chromatographic determination of the hydrocarbon/lipid ratio in irradiated chicken meat, and a bioassay based on microelectrophoresis of DNA from single cells. Also a method for determination of o-tyrosine in the irradiated and non-irradiated chicken meat has been tested. The first method based on radiolytical changes in fatty acids, contained in chicken meat, has been tested and compared in the four Nordic countries. Four major hydrocarbons (C16:2, C16:3, C17:1 and C17:2) have been determined and reasonable agreement was observed between the dose level and hydrocarbons concentration. Results of a bioassay, where strand breaks of DNA are demonstrated by microelectrophoresis of single cells, prove a correlation between the dose levels and the pattern of DNA fragments migration. The hydrocarbon method can be applied to detect other irradiated, fat-containing foods, while the DNA method can be used for some animal and some vegetable foods as well.Both methods allow to determine the fact of food irradiation beyond any doubt, thus making them suitable for food control analysis. The detailed determination protocols are given. (EG)

  5. Analytical method for Buddleja colorants in foods.

    Science.gov (United States)

    Aoki, H; Kuze, N; Ichi, T; Koda, T

    2001-04-01

    Buddleja yellow colorant derived from Buddleja officinalis Maxim. has recently been approved for use as a new kind of natural colorant for food additives in China. In order to distinguish Buddleja yellow colorant from other yellow colorants, two known phenylpropanoid glycosides, acteoside (= verbascoside) and poliumoside, were isolated from the colorant as marker substances for Buddleja yellow colorant. Poliumoside has not been detected in B. officinalis Maxim. previously. These phenylpropanoid glycosides were not detected in the fruits of Gardenia jasminoides Ellis or in the stamens of the flowers of Crocus sativus L., which also contain crocetin derivatives as coloring components, using a photodiode array and mass chromatograms. Thus, an analytical HPLC method was developed to distinguish foods that have been colored with yellow colorants containing crocetin derivatives, using phenylpropanoid glycosides as markers.

  6. An Evaluation Method of Equipment Reliability Configuration Management

    Science.gov (United States)

    Wang, Wei; Feng, Weijia; Zhang, Wei; Li, Yuan

    2018-01-01

    At present, many equipment development companies have been aware of the great significance of reliability of the equipment development. But, due to the lack of effective management evaluation method, it is very difficult for the equipment development company to manage its own reliability work. Evaluation method of equipment reliability configuration management is to determine the reliability management capabilities of equipment development company. Reliability is not only designed, but also managed to achieve. This paper evaluates the reliability management capabilities by reliability configuration capability maturity model(RCM-CMM) evaluation method.

  7. Validation of Land Cover Products Using Reliability Evaluation Methods

    Directory of Open Access Journals (Sweden)

    Wenzhong Shi

    2015-06-01

    Full Text Available Validation of land cover products is a fundamental task prior to data applications. Current validation schemes and methods are, however, suited only for assessing classification accuracy and disregard the reliability of land cover products. The reliability evaluation of land cover products should be undertaken to provide reliable land cover information. In addition, the lack of high-quality reference data often constrains validation and affects the reliability results of land cover products. This study proposes a validation schema to evaluate the reliability of land cover products, including two methods, namely, result reliability evaluation and process reliability evaluation. Result reliability evaluation computes the reliability of land cover products using seven reliability indicators. Process reliability evaluation analyzes the reliability propagation in the data production process to obtain the reliability of land cover products. Fuzzy fault tree analysis is introduced and improved in the reliability analysis of a data production process. Research results show that the proposed reliability evaluation scheme is reasonable and can be applied to validate land cover products. Through the analysis of the seven indicators of result reliability evaluation, more information on land cover can be obtained for strategic decision-making and planning, compared with traditional accuracy assessment methods. Process reliability evaluation without the need for reference data can facilitate the validation and reflect the change trends of reliabilities to some extent.

  8. An interactive website for analytical method comparison and bias estimation.

    Science.gov (United States)

    Bahar, Burak; Tuncel, Ayse F; Holmes, Earle W; Holmes, Daniel T

    2017-12-01

    Regulatory standards mandate laboratories to perform studies to ensure accuracy and reliability of their test results. Method comparison and bias estimation are important components of these studies. We developed an interactive website for evaluating the relative performance of two analytical methods using R programming language tools. The website can be accessed at https://bahar.shinyapps.io/method_compare/. The site has an easy-to-use interface that allows both copy-pasting and manual entry of data. It also allows selection of a regression model and creation of regression and difference plots. Available regression models include Ordinary Least Squares, Weighted-Ordinary Least Squares, Deming, Weighted-Deming, Passing-Bablok and Passing-Bablok for large datasets. The server processes the data and generates downloadable reports in PDF or HTML format. Our website provides clinical laboratories a practical way to assess the relative performance of two analytical methods. Copyright © 2017 The Canadian Society of Clinical Chemists. Published by Elsevier Inc. All rights reserved.

  9. Microgenetic Learning Analytics Methods: Workshop Report

    Science.gov (United States)

    Aghababyan, Ani; Martin, Taylor; Janisiewicz, Philip; Close, Kevin

    2016-01-01

    Learning analytics is an emerging discipline and, as such, benefits from new tools and methodological approaches. This work reviews and summarizes our workshop on microgenetic data analysis techniques using R, held at the second annual Learning Analytics Summer Institute in Cambridge, Massachusetts, on 30 June 2014. Specifically, this paper…

  10. Hanford environmental analytical methods: Methods as of March 1990

    International Nuclear Information System (INIS)

    Goheen, S.C.; McCulloch, M.; Daniel, J.L.

    1993-05-01

    This paper from the analytical laboratories at Hanford describes the method used to measure pH of single-shell tank core samples. Sludge or solid samples are mixed with deionized water. The pH electrode used combines both a sensor and reference electrode in one unit. The meter amplifies the input signal from the electrode and displays the pH visually

  11. Big data analytics for the Future Circular Collider reliability and availability studies

    Science.gov (United States)

    Begy, Volodimir; Apollonio, Andrea; Gutleber, Johannes; Martin-Marquez, Manuel; Niemi, Arto; Penttinen, Jussi-Pekka; Rogova, Elena; Romero-Marin, Antonio; Sollander, Peter

    2017-10-01

    Responding to the European Strategy for Particle Physics update 2013, the Future Circular Collider study explores scenarios of circular frontier colliders for the post-LHC era. One branch of the study assesses industrial approaches to model and simulate the reliability and availability of the entire particle collider complex based on the continuous monitoring of CERN’s accelerator complex operation. The modelling is based on an in-depth study of the CERN injector chain and LHC, and is carried out as a cooperative effort with the HL-LHC project. The work so far has revealed that a major challenge is obtaining accelerator monitoring and operational data with sufficient quality, to automate the data quality annotation and calculation of reliability distribution functions for systems, subsystems and components where needed. A flexible data management and analytics environment that permits integrating the heterogeneous data sources, the domain-specific data quality management algorithms and the reliability modelling and simulation suite is a key enabler to complete this accelerator operation study. This paper describes the Big Data infrastructure and analytics ecosystem that has been put in operation at CERN, serving as the foundation on which reliability and availability analysis and simulations can be built. This contribution focuses on data infrastructure and data management aspects and presents case studies chosen for its validation.

  12. Laser induced uranium fluorescence as an analytical method

    International Nuclear Information System (INIS)

    Krutman, I.

    1985-01-01

    A laser induced fluorescence system was developed to measure uranium trace level amounts in aqueous solution with reliable and simple materials and electronics. A nitrogen pulsed laser was built with the storage energy capacitor directly coupled to laser tube electrodes as a transmission line device. This laser operated at 3Hz repetition rate with peak intensity around 21 Kw and temporal width of 4.5 x 10 -9 s. A sample compartment made of rigid PVC and a photomultiplier housing of aluminium were constructed and assembled forming a single integrated device. As a result of this prototype system we made several analytical measurements with U dissolved in nitric acid to obtain a calibration curve. We obtained a straight line from a plot of U concentration versus fluorescence intensity fitted by a least square method that produced a regression coefficient of 0.994. The lower limit of U determination was 30 ppb -+ 3.5%. (Author) [pt

  13. Reliability studies of diagnostic methods in Indian traditional Ayurveda medicine

    DEFF Research Database (Denmark)

    Kurande, Vrinda Hitendra; Waagepetersen, Rasmus; Toft, Egon

    2013-01-01

    as prakriti classification), method development (pulse diagnosis), quality assurance for diagnosis and treatment and in the conduct of clinical studies. Several reliability studies are conducted in western medicine. The investigation of the reliability of traditional Chinese, Japanese and Sasang medicine...

  14. Method for effective usage of Google Analytics tools

    Directory of Open Access Journals (Sweden)

    Ирина Николаевна Егорова

    2016-01-01

    Full Text Available Modern Google Analytics tools have been investigated against effective attraction channels for users and bottlenecks detection. Conducted investigation allowed to suggest modern method for effective usage of Google Analytics tools. The method is based on main traffic indicators analysis, as well as deep analysis of goals and their consecutive tweaking. Method allows to increase website conversion and might be useful for SEO and Web analytics specialists

  15. Nonlinear ordinary differential equations analytical approximation and numerical methods

    CERN Document Server

    Hermann, Martin

    2016-01-01

    The book discusses the solutions to nonlinear ordinary differential equations (ODEs) using analytical and numerical approximation methods. Recently, analytical approximation methods have been largely used in solving linear and nonlinear lower-order ODEs. It also discusses using these methods to solve some strong nonlinear ODEs. There are two chapters devoted to solving nonlinear ODEs using numerical methods, as in practice high-dimensional systems of nonlinear ODEs that cannot be solved by analytical approximate methods are common. Moreover, it studies analytical and numerical techniques for the treatment of parameter-depending ODEs. The book explains various methods for solving nonlinear-oscillator and structural-system problems, including the energy balance method, harmonic balance method, amplitude frequency formulation, variational iteration method, homotopy perturbation method, iteration perturbation method, homotopy analysis method, simple and multiple shooting method, and the nonlinear stabilized march...

  16. Application of Statistical Methods to Activation Analytical Results near the Limit of Detection

    DEFF Research Database (Denmark)

    Heydorn, Kaj; Wanscher, B.

    1978-01-01

    Reporting actual numbers instead of upper limits for analytical results at or below the detection limit may produce reliable data when these numbers are subjected to appropriate statistical processing. Particularly in radiometric methods, such as activation analysis, where individual standard...... deviations of analytical results may be estimated, improved discrimination may be based on the Analysis of Precision. Actual experimental results from a study of the concentrations of arsenic in human skin demonstrate the power of this principle....

  17. 40 CFR 141.25 - Analytical methods for radioactivity.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 22 2010-07-01 2010-07-01 false Analytical methods for radioactivity... § 141.25 Analytical methods for radioactivity. (a) Analysis for the following contaminants shall be conducted to determine compliance with § 141.66 (radioactivity) in accordance with the methods in the...

  18. Improving Wind Turbine Drivetrain Reliability Using a Combined Experimental, Computational, and Analytical Approach

    Energy Technology Data Exchange (ETDEWEB)

    Guo, Y.; van Dam, J.; Bergua, R.; Jove, J.; Campbell, J.

    2015-03-01

    Nontorque loads induced by the wind turbine rotor overhang weight and aerodynamic forces can greatly affect drivetrain loads and responses. If not addressed properly, these loads can result in a decrease in gearbox component life. This work uses analytical modeling, computational modeling, and experimental data to evaluate a unique drivetrain design that minimizes the effects of nontorque loads on gearbox reliability: the Pure Torque(R) drivetrain developed by Alstom. The drivetrain has a hub-support configuration that transmits nontorque loads directly into the tower rather than through the gearbox as in other design approaches. An analytical model of Alstom's Pure Torque drivetrain provides insight into the relationships among turbine component weights, aerodynamic forces, and the resulting drivetrain loads. Main shaft bending loads are orders of magnitude lower than the rated torque and are hardly affected by wind conditions and turbine operations.

  19. Extrapolation Method for System Reliability Assessment

    DEFF Research Database (Denmark)

    Qin, Jianjun; Nishijima, Kazuyoshi; Faber, Michael Havbro

    2012-01-01

    of integrals with scaled domains. The performance of this class of approximation depends on the approach applied for the scaling and the functional form utilized for the extrapolation. A scheme for this task is derived here taking basis in the theory of asymptotic solutions to multinormal probability integrals......The present paper presents a new scheme for probability integral solution for system reliability analysis, which takes basis in the approaches by Naess et al. (2009) and Bucher (2009). The idea is to evaluate the probability integral by extrapolation, based on a sequence of MC approximations...... that the proposed scheme is efficient and adds to generality for this class of approximations for probability integrals....

  20. Analytical methods for heat transfer and fluid flow problems

    CERN Document Server

    Weigand, Bernhard

    2015-01-01

    This book describes useful analytical methods by applying them to real-world problems rather than solving the usual over-simplified classroom problems. The book demonstrates the applicability of analytical methods even for complex problems and guides the reader to a more intuitive understanding of approaches and solutions. Although the solution of Partial Differential Equations by numerical methods is the standard practice in industries, analytical methods are still important for the critical assessment of results derived from advanced computer simulations and the improvement of the underlying numerical techniques. Literature devoted to analytical methods, however, often focuses on theoretical and mathematical aspects and is therefore useless to most engineers. Analytical Methods for Heat Transfer and Fluid Flow Problems addresses engineers and engineering students. The second edition has been updated, the chapters on non-linear problems and on axial heat conduction problems were extended. And worked out exam...

  1. Recent developments in analytical detection methods for radiation processed foods

    International Nuclear Information System (INIS)

    Wu Jilan

    1993-01-01

    A short summary of the programmes of 'ADMIT' (FAO/IAEA) and the developments in analytical detection methods for radiation processed foods has been given. It is suggested that for promoting the commercialization of radiation processed foods and controlling its quality, one must pay more attention to the study of analytical detection methods of irradiated food

  2. Reliability of non-destructive testing methods

    International Nuclear Information System (INIS)

    Broekhoven, M.J.G.

    1988-01-01

    This contribution regards the results of an evaluation of the reliability of radiography (X-rays and gamma-rays), manual-, and mechanized/automated ultrasonic examination by generally accepted codes/rules, with respect to detection, characterization and sizing/localization of defects. The evaluation is based on the results of examinations, by a number of teams, of 30 test plates, 30 and 50 mm thickness, containing V,U, X and K-shaped welds each containing several types of imperfections (211) in total) typical for steel arc fusion welding, such as porosity, inclusions, lack of fusion or penetration and cracks. Besides, some results are presented obtained from research on advanced UT-techniques, viz. the time-of-flight-diffraction and flaw-tip deflection technique. (author)

  3. Reliability of non-destructive testing methods

    Energy Technology Data Exchange (ETDEWEB)

    Broekhoven, M J.G. [Ministry of Social Affairs, (Netherlands)

    1988-12-31

    This contribution regards the results of an evaluation of the reliability of radiography (X-rays and gamma-rays), manual-, and mechanized/automated ultrasonic examination by generally accepted codes/rules, with respect to detection, characterization and sizing/localization of defects. The evaluation is based on the results of examinations, by a number of teams, of 30 test plates, 30 and 50 mm thickness, containing V,U, X and K-shaped welds each containing several types of imperfections (211) in total) typical for steel arc fusion welding, such as porosity, inclusions, lack of fusion or penetration and cracks. Besides, some results are presented obtained from research on advanced UT-techniques, viz. the time-of-flight-diffraction and flaw-tip deflection technique. (author). 4 refs.

  4. A reliability evaluation method for NPP safety DCS application software

    International Nuclear Information System (INIS)

    Li Yunjian; Zhang Lei; Liu Yuan

    2014-01-01

    In the field of nuclear power plant (NPP) digital i and c application, reliability evaluation for safety DCS application software is a key obstacle to be removed. In order to quantitatively evaluate reliability of NPP safety DCS application software, this paper propose a reliability evaluating method based on software development life cycle every stage's v and v defects density characteristics, by which the operating reliability level of the software can be predicted before its delivery, and helps to improve the reliability of NPP safety important software. (authors)

  5. Analytical methods for predicting contaminant transport

    International Nuclear Information System (INIS)

    Pigford, T.H.

    1989-09-01

    This paper summarizes some of the previous and recent work at the University of California on analytical solutions for predicting contaminate transport in porous and fractured geologic media. Emphasis is given here to the theories for predicting near-field transport, needed to derive the time-dependent source term for predicting far-field transport and overall repository performance. New theories summarized include solubility-limited release rate with flow backfill in rock, near-field transport of radioactive decay chains, interactive transport of colloid and solute, transport of carbon-14 as carbon dioxide in unsaturated rock, and flow of gases out of and a waste container through cracks and penetrations. 28 refs., 4 figs

  6. Some analytical methods for explosives: Part 2

    Energy Technology Data Exchange (ETDEWEB)

    Selig, W.

    1965-12-08

    This report is the second compilation of methods for analyzing explosives. All the methods were developed for routine performance by techniques, and an attempt has therefore been made to keep them as simple as possible. Methods are presented for analyzing plastic-bonded explosives based on sym-cyclomethylenetetra-nitramine (HMX), based on viton in addition to HMX, and based on pentraerythritol tetranitrate (PETN).

  7. Examination of fast reactor fuels, FBR analytical quality assurance standards and methods, and analytical methods development: irradiation tests. Progress report, April 1--June 30, 1976, and FY 1976

    International Nuclear Information System (INIS)

    Baker, R.D.

    1976-08-01

    Characterization of unirradiated and irradiated LMFBR fuels by analytical chemistry methods will continue, and additional methods will be modified and mechanized for hot cell application. Macro- and microexaminations will be made on fuel and cladding using the shielded electron microprobe, emission spectrograph, radiochemistry, gamma scanner, mass spectrometers, and other analytical facilities. New capabilities will be developed in gamma scanning, analyses to assess spatial distributions of fuel and fission products, mass spectrometric measurements of burnup and fission gas constituents and other chemical analyses. Microstructural analyses of unirradiated and irradiated materials will continue using optical and electron microscopy and autoradiographic and x-ray techniques. Analytical quality assurance standards tasks are designed to assure the quality of the chemical characterizations necessary to evaluate reactor components relative to specifications. Tasks include: (1) the preparation and distribution of calibration materials and quality control samples for use in quality assurance surveillance programs, (2) the development of and the guidance in the use of quality assurance programs for sampling and analysis, (3) the development of improved methods of analysis, and (4) the preparation of continuously updated analytical method manuals. Reliable analytical methods development for the measurement of burnup, oxygen-to-metal (O/M) ratio, and various gases in irradiated fuels is described

  8. Analytical method for solving radioactive transformations

    International Nuclear Information System (INIS)

    Vukadin, Z.

    1999-01-01

    The exact method of solving radioactive transformations is presented. Nonsingular Bateman coefficients, which can be computed using recurrence formulas, greatly reduce computational time and eliminate singularities that often arise in problems involving nuclide transmutations. Depletion function power series expansion enables high accuracy of the performed calculations, specially in a case of a decay constants with closely spaced values. Generality and simplicity of the method make the method useful for many practical applications. (author)

  9. Determination of aluminum by four analytical methods

    International Nuclear Information System (INIS)

    Hanson, T.J.; Smetana, K.M.

    1975-11-01

    Four procedures have been developed for determining the aluminum concentration in basic matrices. Atomic Absorption Spectroscopy (AAS) was the routine method of analysis. Citrate was required to complex the aluminum and eliminate matrix effects. AAS was the least accurate of the four methods studied and was adversely affected by high aluminum concentrations. The Fluoride Electrode Method was the most accurate and precise of the four methods. A Gran's Plot determination was used to determine the end point and average standard recovery was 100% +- 2%. The Thermometric Titration Method was the fastest method for determining aluminum and could also determine hydroxide concentration at the same time. Standard recoveries were 100% +- 5%. The pH Electrode Method also measures aluminum and hydroxide content simultaneously, but is less accurate and more time consuming that the thermal titration. Samples were analyzed using all four methods and results were compared to determine the strengths and weaknesses of each. On the basis of these comparisons, conclusions were drawn concerning the application of each method to our laboratory needs

  10. Mathematical Methods in Survival Analysis, Reliability and Quality of Life

    CERN Document Server

    Huber, Catherine; Mesbah, Mounir

    2008-01-01

    Reliability and survival analysis are important applications of stochastic mathematics (probability, statistics and stochastic processes) that are usually covered separately in spite of the similarity of the involved mathematical theory. This title aims to redress this situation: it includes 21 chapters divided into four parts: Survival analysis, Reliability, Quality of life, and Related topics. Many of these chapters were presented at the European Seminar on Mathematical Methods for Survival Analysis, Reliability and Quality of Life in 2006.

  11. Extension of the analytic nodal method to four energy groups

    International Nuclear Information System (INIS)

    Parsons, D.K.; Nigg, D.W.

    1985-01-01

    The Analytic Nodal Method is one of several recently-developed coarse mesh numerical methods for efficiently and accurately solving the multidimensional static and transient neutron diffusion equations. This summary describes a mathematically rigorous extension of the Analytic Nodal Method to the frequently more physically realistic four-group case. A few general theoretical considerations are discussed, followed by some calculated results for a typical steady-state two-dimensional PWR quarter core application. 8 refs

  12. An accurate and efficient reliability-based design optimization using the second order reliability method and improved stability transformation method

    Science.gov (United States)

    Meng, Zeng; Yang, Dixiong; Zhou, Huanlin; Yu, Bo

    2018-05-01

    The first order reliability method has been extensively adopted for reliability-based design optimization (RBDO), but it shows inaccuracy in calculating the failure probability with highly nonlinear performance functions. Thus, the second order reliability method is required to evaluate the reliability accurately. However, its application for RBDO is quite challenge owing to the expensive computational cost incurred by the repeated reliability evaluation and Hessian calculation of probabilistic constraints. In this article, a new improved stability transformation method is proposed to search the most probable point efficiently, and the Hessian matrix is calculated by the symmetric rank-one update. The computational capability of the proposed method is illustrated and compared to the existing RBDO approaches through three mathematical and two engineering examples. The comparison results indicate that the proposed method is very efficient and accurate, providing an alternative tool for RBDO of engineering structures.

  13. Analytical methods applied to water pollution

    International Nuclear Information System (INIS)

    Baudin, G.

    1977-01-01

    A comparison of different methods applied to water analysis is given. The discussion is limited to the problems presented by inorganic elements, accessible to nuclear activation analysis methods. The following methods were compared: activation analysis: with gamma-ray spectrometry, atomic absorption spectrometry, fluorimetry, emission spectrometry, colorimetry or spectrophotometry, X-ray fluorescence, mass spectrometry, voltametry, polarography or other electrochemical methods, activation analysis-beta measurements. Drinking-water, irrigation waters, sea waters, industrial wastes and very pure waters are the subjects of the investigations. The comparative evaluation is made on the basis of storage of samples, in situ analysis, treatment and concentration, specificity and interference, monoelement or multielement analysis, analysis time and accuracy. The significance of the neutron analysis is shown. (T.G.)

  14. A novel reliability evaluation method for large engineering systems

    Directory of Open Access Journals (Sweden)

    Reda Farag

    2016-06-01

    Full Text Available A novel reliability evaluation method for large nonlinear engineering systems excited by dynamic loading applied in time domain is presented. For this class of problems, the performance functions are expected to be function of time and implicit in nature. Available first- or second-order reliability method (FORM/SORM will be challenging to estimate reliability of such systems. Because of its inefficiency, the classical Monte Carlo simulation (MCS method also cannot be used for large nonlinear dynamic systems. In the proposed approach, only tens instead of hundreds or thousands of deterministic evaluations at intelligently selected points are used to extract the reliability information. A hybrid approach, consisting of the stochastic finite element method (SFEM developed by the author and his research team using FORM, response surface method (RSM, an interpolation scheme, and advanced factorial schemes, is proposed. The method is clarified with the help of several numerical examples.

  15. Advances in methods and applications of reliability and safety analysis

    International Nuclear Information System (INIS)

    Fieandt, J.; Hossi, H.; Laakso, K.; Lyytikaeinen, A.; Niemelae, I.; Pulkkinen, U.; Pulli, T.

    1986-01-01

    The know-how of the reliability and safety design and analysis techniques of Vtt has been established over several years in analyzing the reliability in the Finnish nuclear power plants Loviisa and Olkiluoto. This experience has been later on applied and developed to be used in the process industry, conventional power industry, automation and electronics. VTT develops and transfers methods and tools for reliability and safety analysis to the private and public sectors. The technology transfer takes place in joint development projects with potential users. Several computer-aided methods, such as RELVEC for reliability modelling and analysis, have been developed. The tool developed are today used by major Finnish companies in the fields of automation, nuclear power, shipbuilding and electronics. Development of computer-aided and other methods needed in analysis of operating experience, reliability or safety is further going on in a number of research and development projects

  16. Analytical methods for the determination of tungsten

    International Nuclear Information System (INIS)

    Topping, J.J.

    1978-01-01

    Methods developed and employed in the recent literature (1969 to 1975) for the detection and determination of tungsten in a wide variety of matrices are reviewed. This paper is a supplement to the books, monographs and review papers which deal with the earlier literature. (author)

  17. Pyrrolizidine alkaloids in honey: comparison of analytical methods

    NARCIS (Netherlands)

    Kempf, M.; Wittig, M.; Reinhard, A.; Ohe, von der K.; Blacquière, T.; Raezke, K.P.; Michel, R.; Schreier, P.; Beuerle, T.

    2011-01-01

    Pyrrolizidine alkaloids (PAs) are a structurally diverse group of toxicologically relevant secondary plant metabolites. Currently, two analytical methods are used to determine PA content in honey. To achieve reasonably high sensitivity and selectivity, mass spectrometry detection is demanded. One

  18. Analytical chemistry methods for boron carbide absorber material. [Standard

    Energy Technology Data Exchange (ETDEWEB)

    DELVIN WL

    1977-07-01

    This standard provides analytical chemistry methods for the analysis of boron carbide powder and pellets for the following: total C and B, B isotopic composition, soluble C and B, fluoride, chloride, metallic impurities, gas content, water, nitrogen, and oxygen. (DLC)

  19. Human Reliability Analysis for Design: Using Reliability Methods for Human Factors Issues

    Energy Technology Data Exchange (ETDEWEB)

    Ronald Laurids Boring

    2010-11-01

    This paper reviews the application of human reliability analysis methods to human factors design issues. An application framework is sketched in which aspects of modeling typically found in human reliability analysis are used in a complementary fashion to the existing human factors phases of design and testing. The paper provides best achievable practices for design, testing, and modeling. Such best achievable practices may be used to evaluate and human system interface in the context of design safety certifications.

  20. Human Reliability Analysis for Design: Using Reliability Methods for Human Factors Issues

    International Nuclear Information System (INIS)

    Boring, Ronald Laurids

    2010-01-01

    This paper reviews the application of human reliability analysis methods to human factors design issues. An application framework is sketched in which aspects of modeling typically found in human reliability analysis are used in a complementary fashion to the existing human factors phases of design and testing. The paper provides best achievable practices for design, testing, and modeling. Such best achievable practices may be used to evaluate and human system interface in the context of design safety certifications.

  1. Analytical techniques for instrument design - matrix methods

    International Nuclear Information System (INIS)

    Robinson, R.A.

    1997-01-01

    We take the traditional Cooper-Nathans approach, as has been applied for many years for steady-state triple-axis spectrometers, and consider its generalisation to other inelastic scattering spectrometers. This involves a number of simple manipulations of exponentials of quadratic forms. In particular, we discuss a toolbox of matrix manipulations that can be performed on the 6- dimensional Cooper-Nathans matrix: diagonalisation (Moller-Nielsen method), coordinate changes e.g. from (Δk I ,Δk F to ΔE, ΔQ ampersand 2 dummy variables), integration of one or more variables (e.g. over such dummy variables), integration subject to linear constraints (e.g. Bragg's Law for analysers), inversion to give the variance-covariance matrix, and so on. We show how these tools can be combined to solve a number of important problems, within the narrow-band limit and the gaussian approximation. We will argue that a generalised program that can handle multiple different spectrometers could (and should) be written in parallel to the Monte-Carlo packages that are becoming available. We will also discuss the complementarity between detailed Monte-Carlo calculations and the approach presented here. In particular, Monte-Carlo methods traditionally simulate the real experiment as performed in practice, given a model scattering law, while the Cooper-Nathans method asks the inverse question: given that a neutron turns up in a particular spectrometer configuration (e.g. angle and time of flight), what is the probability distribution of possible scattering events at the sample? The Monte-Carlo approach could be applied in the same spirit to this question

  2. Surface analytical methods in nuclear technology

    International Nuclear Information System (INIS)

    Baumgaertner, F.

    1985-06-01

    Application of SEM-EDX, AES, XPS are exemplarily demonstrated for highly radioactive materials with ionizing dose rates of about 1 Sv near the surface. The samples studied are aerosols from the high level waste vitrification process, postprecipitation in a pretreated fuel solution and emulsifying sludge from a solvent extraction process. The results of the chemical composition differentiated down to microscopic level reveal much more information about the history of a sample than those available from the integral macro-methods analysing. Elucidication of chemical composition and body structure in micrometer level may give insight into the origin and generation processes of samples under investigation. (orig.)

  3. Analytical techniques for instrument design - Matrix methods

    International Nuclear Information System (INIS)

    Robinson, R.A.

    1997-01-01

    The authors take the traditional Cooper-Nathans approach, as has been applied for many years for steady-state triple-axis spectrometers, and consider its generalization to other inelastic scattering spectrometers. This involves a number of simple manipulations of exponentials of quadratic forms. In particular, they discuss a toolbox of matrix manipulations that can be performed on the 6-dimensional Cooper-Nathans matrix. They show how these tools can be combined to solve a number of important problems, within the narrow-band limit and the gaussian approximation. They will argue that a generalized program that can handle multiple different spectrometers could (and should) be written in parallel to the Monte-Carlo packages that are becoming available. They also discuss the complementarity between detailed Monte-Carlo calculations and the approach presented here. In particular, Monte-Carlo methods traditionally simulate the real experiment as performed in practice, given a model scattering law, while the Cooper-Nathans method asks the inverse question: given that a neutron turns up in a particular spectrometer configuration (e.g. angle and time of flight), what is the probability distribution of possible scattering events at the sample? The Monte-Carlo approach could be applied in the same spirit to this question

  4. Manual of selected physico-chemical analytical methods. IV

    International Nuclear Information System (INIS)

    Beran, M.; Klosova, E.; Krtil, J.; Sus, F.; Kuvik, V.; Vrbova, L.; Hamplova, M.; Lengyel, J.; Kelnar, L.; Zakouril, K.

    1990-11-01

    The Central Testing Laboratory of the Nuclear Research Institute at Rez has for a decade been participating in the development of analytical procedures and has been providing analyses of samples of different types and origin. The analytical procedures developed have been published in special journals and a number of them in the Manuals of analytical methods, in three parts. The 4th part of the Manual contains selected physico-chemical methods developed or modified by the Laboratory in the years 1986-1990 within the project ''Development of physico-chemical analytical methods''. In most cases, techniques are involved for non-nuclear applications. Some can find wider applications, especially in analyses of environmental samples. Others have been developed for specific cases of sample analyses or require special instrumentation (mass spectrometer), which partly restricts their applicability by other institutions. (author)

  5. A method to assign failure rates for piping reliability assessments

    International Nuclear Information System (INIS)

    Gamble, R.M.; Tagart, S.W. Jr.

    1991-01-01

    This paper reports on a simplified method that has been developed to assign failure rates that can be used in reliability and risk studies of piping. The method can be applied on a line-by-line basis by identifying line and location specific attributes that can lead to piping unreliability from in-service degradation mechanisms and random events. A survey of service experience for nuclear piping reliability also was performed. The data from this survey provides a basis for identifying in-service failure attributes and assigning failure rates for risk and reliability studies

  6. Reliability analysis of neutron transport simulation using Monte Carlo method

    International Nuclear Information System (INIS)

    Souza, Bismarck A. de; Borges, Jose C.

    1995-01-01

    This work presents a statistical and reliability analysis covering data obtained by computer simulation of neutron transport process, using the Monte Carlo method. A general description of the method and its applications is presented. Several simulations, corresponding to slowing down and shielding problems have been accomplished. The influence of the physical dimensions of the materials and of the sample size on the reliability level of results was investigated. The objective was to optimize the sample size, in order to obtain reliable results, optimizing computation time. (author). 5 refs, 8 figs

  7. Modifying nodal pricing method considering market participants optimality and reliability

    Directory of Open Access Journals (Sweden)

    A. R. Soofiabadi

    2015-06-01

    Full Text Available This paper develops a method for nodal pricing and market clearing mechanism considering reliability of the system. The effects of components reliability on electricity price, market participants’ profit and system social welfare is considered. This paper considers reliability both for evaluation of market participant’s optimality as well as for fair pricing and market clearing mechanism. To achieve fair pricing, nodal price has been obtained through a two stage optimization problem and to achieve fair market clearing mechanism, comprehensive criteria has been introduced for optimality evaluation of market participant. Social welfare of the system and system efficiency are increased under proposed modified nodal pricing method.

  8. Methods and applications of analytical perturbation theory

    International Nuclear Information System (INIS)

    Kirchgraber, U.; Stiefel, E.

    1978-01-01

    This monograph on perturbation theory is based on various courses and lectures held by the authors at the ETH, Zurich and at the University of Texas, Austin. Its principal intention is to inform application-minded mathematicians, physicists and engineers about recent developments in this field. The reader is not assumed to have mathematical knowledge beyond what is presented in standard courses on analysis and linear algebra. Chapter I treats the transformations of systems of differential equations and the integration of perturbed systems in a formal way. These tools are applied in Chapter II to celestial mechanics and to the theory of tops and gyroscopic motion. Chapter III is devoted to the discussion of Hamiltonian systems of differential equations and exposes the algebraic aspects of perturbation theory showing also the necessary modifications of the theory in case of singularities. The last chapter gives the mathematical justification for the methods developed in the previous chapters and investigates important questions such as error estimations for the solutions and asymptotic stability. Each chapter ends with useful comments and an extensive reference to the original literature. (HJ) [de

  9. Chapter 12. Sampling and analytical methods

    International Nuclear Information System (INIS)

    Busenberg, E.; Plummer, L.N.; Cook, P.G.; Solomon, D.K.; Han, L.F.; Groening, M.; Oster, H.

    2006-01-01

    When water samples are taken for the analysis of CFCs, regardless of the sampling method used, contamination of samples by contact with atmospheric air (with its 'high' CFC concentrations) is a major concern. This is because groundwaters usually have lower CFC concentrations than those waters which have been exposed to the modern air. Some groundwaters might not contain CFCs and, therefore, are most sensitive to trace contamination by atmospheric air. Thus, extreme precautions are needed to obtain uncontaminated samples when groundwaters, particularly those with older ages, are sampled. It is recommended at the start of any CFC investigation that samples from a CFC-free source be collected and analysed, as a check upon the sampling equipment and methodology. The CFC-free source might be a deep monitoring well or, alternatively, CFC-free water could be carefully prepared in the laboratory. It is especially important that all tubing, pumps and connection that will be used in the sampling campaign be checked in this manner

  10. A SOFTWARE RELIABILITY ESTIMATION METHOD TO NUCLEAR SAFETY SOFTWARE

    Directory of Open Access Journals (Sweden)

    GEE-YONG PARK

    2014-02-01

    Full Text Available A method for estimating software reliability for nuclear safety software is proposed in this paper. This method is based on the software reliability growth model (SRGM, where the behavior of software failure is assumed to follow a non-homogeneous Poisson process. Two types of modeling schemes based on a particular underlying method are proposed in order to more precisely estimate and predict the number of software defects based on very rare software failure data. The Bayesian statistical inference is employed to estimate the model parameters by incorporating software test cases as a covariate into the model. It was identified that these models are capable of reasonably estimating the remaining number of software defects which directly affects the reactor trip functions. The software reliability might be estimated from these modeling equations, and one approach of obtaining software reliability value is proposed in this paper.

  11. Analytic Methods Used in Quality Control in a Compounding Pharmacy.

    Science.gov (United States)

    Allen, Loyd V

    2017-01-01

    Analytical testing will no doubt become a more important part of pharmaceutical compounding as the public and regulatory agencies demand increasing documentation of the quality of compounded preparations. Compounding pharmacists must decide what types of testing and what amount of testing to include in their quality-control programs, and whether testing should be done in-house or outsourced. Like pharmaceutical compounding, analytical testing should be performed only by those who are appropriately trained and qualified. This article discusses the analytical methods that are used in quality control in a compounding pharmacy. Copyright© by International Journal of Pharmaceutical Compounding, Inc.

  12. Evaluation of Information Requirements of Reliability Methods in Engineering Design

    DEFF Research Database (Denmark)

    Marini, Vinicius Kaster; Restrepo-Giraldo, John Dairo; Ahmed-Kristensen, Saeema

    2010-01-01

    This paper aims to characterize the information needed to perform methods for robustness and reliability, and verify their applicability to early design stages. Several methods were evaluated on their support to synthesis in engineering design. Of those methods, FMEA, FTA and HAZOP were selected...

  13. Structural hybrid reliability index and its convergent solving method based on random–fuzzy–interval reliability model

    OpenAIRE

    Hai An; Ling Zhou; Hui Sun

    2016-01-01

    Aiming to resolve the problems of a variety of uncertainty variables that coexist in the engineering structure reliability analysis, a new hybrid reliability index to evaluate structural hybrid reliability, based on the random–fuzzy–interval model, is proposed in this article. The convergent solving method is also presented. First, the truncated probability reliability model, the fuzzy random reliability model, and the non-probabilistic interval reliability model are introduced. Then, the new...

  14. Quantifying the measurement uncertainty of results from environmental analytical methods.

    Science.gov (United States)

    Moser, J; Wegscheider, W; Sperka-Gottlieb, C

    2001-07-01

    The Eurachem-CITAC Guide Quantifying Uncertainty in Analytical Measurement was put into practice in a public laboratory devoted to environmental analytical measurements. In doing so due regard was given to the provisions of ISO 17025 and an attempt was made to base the entire estimation of measurement uncertainty on available data from the literature or from previously performed validation studies. Most environmental analytical procedures laid down in national or international standards are the result of cooperative efforts and put into effect as part of a compromise between all parties involved, public and private, that also encompasses environmental standards and statutory limits. Central to many procedures is the focus on the measurement of environmental effects rather than on individual chemical species. In this situation it is particularly important to understand the measurement process well enough to produce a realistic uncertainty statement. Environmental analytical methods will be examined as far as necessary, but reference will also be made to analytical methods in general and to physical measurement methods where appropriate. This paper describes ways and means of quantifying uncertainty for frequently practised methods of environmental analysis. It will be shown that operationally defined measurands are no obstacle to the estimation process as described in the Eurachem/CITAC Guide if it is accepted that the dominating component of uncertainty comes from the actual practice of the method as a reproducibility standard deviation.

  15. Laser: a Tool for Optimization and Enhancement of Analytical Methods

    Energy Technology Data Exchange (ETDEWEB)

    Preisler, Jan [Iowa State Univ., Ames, IA (United States)

    1997-01-01

    In this work, we use lasers to enhance possibilities of laser desorption methods and to optimize coating procedure for capillary electrophoresis (CE). We use several different instrumental arrangements to characterize matrix-assisted laser desorption (MALD) at atmospheric pressure and in vacuum. In imaging mode, 488-nm argon-ion laser beam is deflected by two acousto-optic deflectors to scan plumes desorbed at atmospheric pressure via absorption. All absorbing species, including neutral molecules, are monitored. Interesting features, e.g. differences between the initial plume and subsequent plumes desorbed from the same spot, or the formation of two plumes from one laser shot are observed. Total plume absorbance can be correlated with the acoustic signal generated by the desorption event. A model equation for the plume velocity as a function of time is proposed. Alternatively, the use of a static laser beam for observation enables reliable determination of plume velocities even when they are very high. Static scattering detection reveals negative influence of particle spallation on MS signal. Ion formation during MALD was monitored using 193-nm light to photodissociate a portion of insulin ion plume. These results define the optimal conditions for desorbing analytes from matrices, as opposed to achieving a compromise between efficient desorption and efficient ionization as is practiced in mass spectrometry. In CE experiment, we examined changes in a poly(ethylene oxide) (PEO) coating by continuously monitoring the electroosmotic flow (EOF) in a fused-silica capillary during electrophoresis. An imaging CCD camera was used to follow the motion of a fluorescent neutral marker zone along the length of the capillary excited by 488-nm Ar-ion laser. The PEO coating was shown to reduce the velocity of EOF by more than an order of magnitude compared to a bare capillary at pH 7.0. The coating protocol was important, especially at an intermediate pH of 7.7. The increase of p

  16. Sequential optimization and reliability assessment method for metal forming processes

    International Nuclear Information System (INIS)

    Sahai, Atul; Schramm, Uwe; Buranathiti, Thaweepat; Chen Wei; Cao Jian; Xia, Cedric Z.

    2004-01-01

    Uncertainty is inevitable in any design process. The uncertainty could be due to the variations in geometry of the part, material properties or due to the lack of knowledge about the phenomena being modeled itself. Deterministic design optimization does not take uncertainty into account and worst case scenario assumptions lead to vastly over conservative design. Probabilistic design, such as reliability-based design and robust design, offers tools for making robust and reliable decisions under the presence of uncertainty in the design process. Probabilistic design optimization often involves double-loop procedure for optimization and iterative probabilistic assessment. This results in high computational demand. The high computational demand can be reduced by replacing computationally intensive simulation models with less costly surrogate models and by employing Sequential Optimization and reliability assessment (SORA) method. The SORA method uses a single-loop strategy with a series of cycles of deterministic optimization and reliability assessment. The deterministic optimization and reliability assessment is decoupled in each cycle. This leads to quick improvement of design from one cycle to other and increase in computational efficiency. This paper demonstrates the effectiveness of Sequential Optimization and Reliability Assessment (SORA) method when applied to designing a sheet metal flanging process. Surrogate models are used as less costly approximations to the computationally expensive Finite Element simulations

  17. New Analytical Method for the Determination of Metronidazole in ...

    African Journals Online (AJOL)

    New Analytical Method for the Determination of Metronidazole in Human Plasma: Application to Bioequivalence Study. ... Methods: Metronidazole was extracted from human plasma through one step of ... http://dx.doi.org/10.4314/tjpr.v11i5.14.

  18. Development and Validation of Analytical Method for Losartan ...

    African Journals Online (AJOL)

    Development and Validation of Analytical Method for Losartan-Copper Complex Using UV-Vis Spectrophotometry. ... Tropical Journal of Pharmaceutical Research ... Purpose: To develop a new spectrophotometric method for the analysis of losartan potassium in pharmaceutical formulations by making its complex with ...

  19. Statistical models and methods for reliability and survival analysis

    CERN Document Server

    Couallier, Vincent; Huber-Carol, Catherine; Mesbah, Mounir; Huber -Carol, Catherine; Limnios, Nikolaos; Gerville-Reache, Leo

    2013-01-01

    Statistical Models and Methods for Reliability and Survival Analysis brings together contributions by specialists in statistical theory as they discuss their applications providing up-to-date developments in methods used in survival analysis, statistical goodness of fit, stochastic processes for system reliability, amongst others. Many of these are related to the work of Professor M. Nikulin in statistics over the past 30 years. The authors gather together various contributions with a broad array of techniques and results, divided into three parts - Statistical Models and Methods, Statistical

  20. Analytical Method of Malculation of the Current and Torque a Reluctance Stepper Motor via Fourier Series

    Directory of Open Access Journals (Sweden)

    Pavel Zaskalicky

    2008-01-01

    Full Text Available Reluctance stepper motors are becoming to be very attractive transducer to conversion of electric signal to the mechanical position. Due to its simple construction is reluctance machine considered a very reliable machine which not requiring any maintenance. Present paper proposes a mathematical method of an analytical calculus of a phase current and electromagnetic torque of the motor via Fourier series. Saturation effect and winding reluctance are neglected.

  1. An Investigation to Manufacturing Analytical Services Composition using the Analytical Target Cascading Method.

    Science.gov (United States)

    Tien, Kai-Wen; Kulvatunyou, Boonserm; Jung, Kiwook; Prabhu, Vittaldas

    2017-01-01

    As cloud computing is increasingly adopted, the trend is to offer software functions as modular services and compose them into larger, more meaningful ones. The trend is attractive to analytical problems in the manufacturing system design and performance improvement domain because 1) finding a global optimization for the system is a complex problem; and 2) sub-problems are typically compartmentalized by the organizational structure. However, solving sub-problems by independent services can result in a sub-optimal solution at the system level. This paper investigates the technique called Analytical Target Cascading (ATC) to coordinate the optimization of loosely-coupled sub-problems, each may be modularly formulated by differing departments and be solved by modular analytical services. The result demonstrates that ATC is a promising method in that it offers system-level optimal solutions that can scale up by exploiting distributed and modular executions while allowing easier management of the problem formulation.

  2. Level III Reliability methods feasible for complex structures

    NARCIS (Netherlands)

    Waarts, P.H.; Boer, A. de

    2001-01-01

    The paper describes the comparison between three types of reliability methods: code type level I used by a designer, full level I and a level III method. Two cases that are typical for civil engineering practise, a cable-stayed subjected to traffic load and the installation of a soil retaining sheet

  3. Developing a reliable signal wire attachment method for rail.

    Science.gov (United States)

    2014-11-01

    The goal of this project was to develop a better attachment method for rail signal wires to improve the reliability of signaling : systems. EWI conducted basic research into the failure mode of current attachment methods and developed and tested a ne...

  4. Recent advances in computational structural reliability analysis methods

    Science.gov (United States)

    Thacker, Ben H.; Wu, Y.-T.; Millwater, Harry R.; Torng, Tony Y.; Riha, David S.

    1993-10-01

    The goal of structural reliability analysis is to determine the probability that the structure will adequately perform its intended function when operating under the given environmental conditions. Thus, the notion of reliability admits the possibility of failure. Given the fact that many different modes of failure are usually possible, achievement of this goal is a formidable task, especially for large, complex structural systems. The traditional (deterministic) design methodology attempts to assure reliability by the application of safety factors and conservative assumptions. However, the safety factor approach lacks a quantitative basis in that the level of reliability is never known and usually results in overly conservative designs because of compounding conservatisms. Furthermore, problem parameters that control the reliability are not identified, nor their importance evaluated. A summary of recent advances in computational structural reliability assessment is presented. A significant level of activity in the research and development community was seen recently, much of which was directed towards the prediction of failure probabilities for single mode failures. The focus is to present some early results and demonstrations of advanced reliability methods applied to structural system problems. This includes structures that can fail as a result of multiple component failures (e.g., a redundant truss), or structural components that may fail due to multiple interacting failure modes (e.g., excessive deflection, resonate vibration, or creep rupture). From these results, some observations and recommendations are made with regard to future research needs.

  5. Reliability Estimation of the Pultrusion Process Using the First-Order Reliability Method (FORM)

    DEFF Research Database (Denmark)

    Baran, Ismet; Tutum, Cem Celal; Hattel, Jesper Henri

    2013-01-01

    In the present study the reliability estimation of the pultrusion process of a flat plate is analyzed by using the first order reliability method (FORM). The implementation of the numerical process model is validated by comparing the deterministic temperature and cure degree profiles...... with corresponding analyses in the literature. The centerline degree of cure at the exit (CDOCE) being less than a critical value and the maximum composite temperature (Tmax) during the process being greater than a critical temperature are selected as the limit state functions (LSFs) for the FORM. The cumulative...

  6. Origin Determination and Differentiation of Gelatin Species of Bovine, Porcine, and Piscine through Analytical Methods

    Directory of Open Access Journals (Sweden)

    Hatice Saadiye Eryılmaz

    2017-06-01

    Full Text Available Gelatin origin determination has been a crucial issue with respect to religion and health concerns. It is necessary to analyze the origin of gelatin with reliable methods to ensure not only consumer choices but also safety and legal requirements such as labeling. There are many analytical methods developed for detection and/or quantification of gelatin from different sources including bovine, porcine and piscine. These analytical methods can be divided into physicochemical, chromatographic, immunochemical, spectroscopic and molecular methods. Moreover, computational methods have been used in some cases consecutively to ensure sensitivity of the analytical methods. Every method has different advantages and limitations due to their own principles, applied food matrix and process conditions of material. The present review intends to give insight into novel analytical methods and perspectives that have been developed to differentiate porcine, bovine and piscine gelatins and to establish their authenticity. Almost every method can be succeeded in origin determination; however, it is a matter of sensitivity in that some researches fail to ensure sufficient differentiation.

  7. Reliably detectable flaw size for NDE methods that use calibration

    Science.gov (United States)

    Koshti, Ajay M.

    2017-04-01

    Probability of detection (POD) analysis is used in assessing reliably detectable flaw size in nondestructive evaluation (NDE). MIL-HDBK-1823 and associated mh18232 POD software gives most common methods of POD analysis. In this paper, POD analysis is applied to an NDE method, such as eddy current testing, where calibration is used. NDE calibration standards have known size artificial flaws such as electro-discharge machined (EDM) notches and flat bottom hole (FBH) reflectors which are used to set instrument sensitivity for detection of real flaws. Real flaws such as cracks and crack-like flaws are desired to be detected using these NDE methods. A reliably detectable crack size is required for safe life analysis of fracture critical parts. Therefore, it is important to correlate signal responses from real flaws with signal responses form artificial flaws used in calibration process to determine reliably detectable flaw size.

  8. Evaluating the reliability of multi-body mechanisms: A method considering the uncertainties of dynamic performance

    International Nuclear Information System (INIS)

    Wu, Jianing; Yan, Shaoze; Zuo, Ming J.

    2016-01-01

    Mechanism reliability is defined as the ability of a certain mechanism to maintain output accuracy under specified conditions. Mechanism reliability is generally assessed by the classical direct probability method (DPM) derived from the first order second moment (FOSM) method. The DPM relies strongly on the analytical form of the dynamic solution so it is not applicable to multi-body mechanisms that have only numerical solutions. In this paper, an indirect probability model (IPM) is proposed for mechanism reliability evaluation of multi-body mechanisms. IPM combines the dynamic equation, degradation function and Kaplan–Meier estimator to evaluate mechanism reliability comprehensively. Furthermore, to reduce the amount of computation in practical applications, the IPM is simplified into the indirect probability step model (IPSM). A case study of a crank–slider mechanism with clearance is investigated. Results show that relative errors between the theoretical and experimental results of mechanism reliability are less than 5%, demonstrating the effectiveness of the proposed method. - Highlights: • An indirect probability model (IPM) is proposed for mechanism reliability evaluation. • The dynamic equation, degradation function and Kaplan–Meier estimator are used. • Then the simplified form of indirect probability model is proposed. • The experimental results agree well with the predicted results.

  9. HUMAN RELIABILITY ANALYSIS DENGAN PENDEKATAN COGNITIVE RELIABILITY AND ERROR ANALYSIS METHOD (CREAM

    Directory of Open Access Journals (Sweden)

    Zahirah Alifia Maulida

    2015-01-01

    Full Text Available Kecelakaan kerja pada bidang grinding dan welding menempati urutan tertinggi selama lima tahun terakhir di PT. X. Kecelakaan ini disebabkan oleh human error. Human error terjadi karena pengaruh lingkungan kerja fisik dan non fisik.Penelitian kali menggunakan skenario untuk memprediksi serta mengurangi kemungkinan terjadinya error pada manusia dengan pendekatan CREAM (Cognitive Reliability and Error Analysis Method. CREAM adalah salah satu metode human reliability analysis yang berfungsi untuk mendapatkan nilai Cognitive Failure Probability (CFP yang dapat dilakukan dengan dua cara yaitu basic method dan extended method. Pada basic method hanya akan didapatkan nilai failure probabailty secara umum, sedangkan untuk extended method akan didapatkan CFP untuk setiap task. Hasil penelitian menunjukkan faktor- faktor yang mempengaruhi timbulnya error pada pekerjaan grinding dan welding adalah kecukupan organisasi, kecukupan dari Man Machine Interface (MMI & dukungan operasional, ketersediaan prosedur/ perencanaan, serta kecukupan pelatihan dan pengalaman. Aspek kognitif pada pekerjaan grinding yang memiliki nilai error paling tinggi adalah planning dengan nilai CFP 0.3 dan pada pekerjaan welding yaitu aspek kognitif execution dengan nilai CFP 0.18. Sebagai upaya untuk mengurangi nilai error kognitif pada pekerjaan grinding dan welding rekomendasi yang diberikan adalah memberikan training secara rutin, work instrucstion yang lebih rinci dan memberikan sosialisasi alat. Kata kunci: CREAM (cognitive reliability and error analysis method, HRA (human reliability analysis, cognitive error Abstract The accidents in grinding and welding sectors were the highest cases over the last five years in PT. X and it caused by human error. Human error occurs due to the influence of working environment both physically and non-physically. This study will implement an approaching scenario called CREAM (Cognitive Reliability and Error Analysis Method. CREAM is one of human

  10. Teaching Analytical Method Transfer through Developing and Validating Then Transferring Dissolution Testing Methods for Pharmaceuticals

    Science.gov (United States)

    Kimaru, Irene; Koether, Marina; Chichester, Kimberly; Eaton, Lafayette

    2017-01-01

    Analytical method transfer (AMT) and dissolution testing are important topics required in industry that should be taught in analytical chemistry courses. Undergraduate students in senior level analytical chemistry laboratory courses at Kennesaw State University (KSU) and St. John Fisher College (SJFC) participated in development, validation, and…

  11. Rigid inclusions-Comparison between analytical and numerical methods

    International Nuclear Information System (INIS)

    Gomez Perez, R.; Melentijevic, S.

    2014-01-01

    This paper compares different analytical methods for analysis of rigid inclusions with finite element modeling. First of all, the load transfer in the distribution layer is analyzed for its different thicknesses and different inclusion grids to define the range between results obtained by analytical and numerical methods. The interaction between the soft soil and the inclusion in the estimation of settlements is studied as well. Considering different stiffness of the soft soil, settlements obtained analytical and numerically are compared. The influence of the soft soil modulus of elasticity on the neutral point depth was also performed by finite elements. This depth has a great importance for the definition of the total length of rigid inclusion. (Author)

  12. SPANDOM - source projection analytic nodal discrete ordinates method

    International Nuclear Information System (INIS)

    Kim, Tae Hyeong; Cho, Nam Zin

    1994-01-01

    We describe a new discrete ordinates nodal method for the two-dimensional transport equation. We solve the discrete ordinates equation analytically after the source term is projected and represented in polynomials. The method is applied to two fast reactor benchmark problems and compared with the TWOHEX code. The results indicate that the present method accurately predicts not only multiplication factor but also flux distribution

  13. Comparison of Three Analytical Methods for Separation of Mineral and Chelated Fraction from an Adulterated Zn-EDTA Fertilizer

    International Nuclear Information System (INIS)

    Khan, M.S.; Qazi, M.A.; Khan, N.A.; Mian, S.M.; Ahmed, N.; Ahmed, N.

    2013-01-01

    Summary: Different analytical procedures are being employed in the world to quantify the chelated portion in a Zn-EDTA fertilizer. Agriculture Department, Government of the Punjab is following Shahid's analytical method in this regard. This method is based on Ion-chromatography (IC) that separates the mineral zinc (Zn) from an adulterated Zn-EDTA fertilizer sample i.e. mixture of mineral and chelated Zn fractions. To find out its effectiveness and suitability, this comparative study was carried out by analyzing adulterated, non-adulterated Zn-EDTA standard and Zn-EDTA samples taken from market in thrice following three methods namely Shahid's (IC) analytical method, Atomic Absorption Spectrophotometric (AAS) method based on the principle of precipitating the mineral Zn fraction at high pH value by using alkali solution of suitable concentration and analysis of filtrate containing only chelated fraction and Association of Official Analytical Chemists (AOAC) method FM-841 respectively. Adulterated Zn-EDTA samples were prepared by mixing of known quantity of mineral Zn with chelated Zn-EDTA standard. The results showed that Shahid's analytical method and AAS method, both successfully estimated the chelated fraction. The AOAC FM-841 method was insensitive to put a ceiling on the mineral fraction hence did not furnish the reliable results. The Shahid's analytical method was selected being equallyeffective to produce reliable results both for solid and liquid Zn-EDTA samples. The AAS method was comparable in only liquid samples. (author)

  14. Reliability

    OpenAIRE

    Condon, David; Revelle, William

    2017-01-01

    Separating the signal in a test from the irrelevant noise is a challenge for all measurement. Low test reliability limits test validity, attenuates important relationships, and can lead to regression artifacts. Multiple approaches to the assessment and improvement of reliability are discussed. The advantages and disadvantages of several different approaches to reliability are considered. Practical advice on how to assess reliability using open source software is provided.

  15. An overview of reliability methods in mechanical and structural design

    Science.gov (United States)

    Wirsching, P. H.; Ortiz, K.; Lee, S. J.

    1987-01-01

    An evaluation is made of modern methods of fast probability integration and Monte Carlo treatment for the assessment of structural systems' and components' reliability. Fast probability integration methods are noted to be more efficient than Monte Carlo ones. This is judged to be an important consideration when several point probability estimates must be made in order to construct a distribution function. An example illustrating the relative efficiency of the various methods is included.

  16. Approximate analytical methods for solving ordinary differential equations

    CERN Document Server

    Radhika, TSL; Rani, T Raja

    2015-01-01

    Approximate Analytical Methods for Solving Ordinary Differential Equations (ODEs) is the first book to present all of the available approximate methods for solving ODEs, eliminating the need to wade through multiple books and articles. It covers both well-established techniques and recently developed procedures, including the classical series solution method, diverse perturbation methods, pioneering asymptotic methods, and the latest homotopy methods.The book is suitable not only for mathematicians and engineers but also for biologists, physicists, and economists. It gives a complete descripti

  17. Analytical Evaluation of Beam Deformation Problem Using Approximate Methods

    DEFF Research Database (Denmark)

    Barari, Amin; Kimiaeifar, A.; Domairry, G.

    2010-01-01

    The beam deformation equation has very wide applications in structural engineering. As a differential equation, it has its own problem concerning existence, uniqueness and methods of solutions. Often, original forms of governing differential equations used in engineering problems are simplified......, and this process produces noise in the obtained answers. This paper deals with the solution of second order of differential equation governing beam deformation using four analytical approximate methods, namely the Perturbation, Homotopy Perturbation Method (HPM), Homotopy Analysis Method (HAM) and Variational...... Iteration Method (VIM). The comparisons of the results reveal that these methods are very effective, convenient and quite accurate for systems of non-linear differential equation....

  18. Assessment of the reliability of ultrasonic inspection methods

    International Nuclear Information System (INIS)

    Haines, N.F.; Langston, D.B.; Green, A.J.; Wilson, R.

    1982-01-01

    The reliability of NDT techniques has remained an open question for many years. A reliable technique may be defined as one that, when rigorously applied by a number of inspection teams, consistently finds then correctly sizes all defects of concern. In this paper we report an assessment of the reliability of defect detection by manual ultrasonic methods applied to the inspection of thick section pressure vessel weldments. Initially we consider the available data relating to the inherent physical capabilities of ultrasonic techniques to detect cracks in weldment and then, independently, we assess the likely variability in team to team performance when several teams are asked to follow the same specified test procedure. The two aspects of 'capability' and 'variability' are brought together to provide quantitative estimates of the overall reliability of ultrasonic inspection of thick section pressure vessel weldments based on currently existing data. The final section of the paper considers current research programmes on reliability and presents a view on how these will help to further improve NDT reliability. (author)

  19. Analytic continuation of quantum Monte Carlo data. Stochastic sampling method

    Energy Technology Data Exchange (ETDEWEB)

    Ghanem, Khaldoon; Koch, Erik [Institute for Advanced Simulation, Forschungszentrum Juelich, 52425 Juelich (Germany)

    2016-07-01

    We apply Bayesian inference to the analytic continuation of quantum Monte Carlo (QMC) data from the imaginary axis to the real axis. Demanding a proper functional Bayesian formulation of any analytic continuation method leads naturally to the stochastic sampling method (StochS) as the Bayesian method with the simplest prior, while it excludes the maximum entropy method and Tikhonov regularization. We present a new efficient algorithm for performing StochS that reduces computational times by orders of magnitude in comparison to earlier StochS methods. We apply the new algorithm to a wide variety of typical test cases: spectral functions and susceptibilities from DMFT and lattice QMC calculations. Results show that StochS performs well and is able to resolve sharp features in the spectrum.

  20. Investigation of MLE in nonparametric estimation methods of reliability function

    International Nuclear Information System (INIS)

    Ahn, Kwang Won; Kim, Yoon Ik; Chung, Chang Hyun; Kim, Kil Yoo

    2001-01-01

    There have been lots of trials to estimate a reliability function. In the ESReDA 20 th seminar, a new method in nonparametric way was proposed. The major point of that paper is how to use censored data efficiently. Generally there are three kinds of approach to estimate a reliability function in nonparametric way, i.e., Reduced Sample Method, Actuarial Method and Product-Limit (PL) Method. The above three methods have some limits. So we suggest an advanced method that reflects censored information more efficiently. In many instances there will be a unique maximum likelihood estimator (MLE) of an unknown parameter, and often it may be obtained by the process of differentiation. It is well known that the three methods generally used to estimate a reliability function in nonparametric way have maximum likelihood estimators that are uniquely exist. So, MLE of the new method is derived in this study. The procedure to calculate a MLE is similar just like that of PL-estimator. The difference of the two is that in the new method, the mass (or weight) of each has an influence of the others but the mass in PL-estimator not

  1. Reliability methods in nuclear power plant ageing management

    International Nuclear Information System (INIS)

    Simola, K.

    1999-01-01

    The aim of nuclear power plant ageing management is to maintain an adequate safety level throughout the lifetime of the plant. In ageing studies, the reliability of components, systems and structures is evaluated taking into account the possible time-dependent degradation. The phases of ageing analyses are generally the identification of critical components, identification and evaluation of ageing effects, and development of mitigation methods. This thesis focuses on the use of reliability methods and analyses of plant- specific operating experience in nuclear power plant ageing studies. The presented applications and method development have been related to nuclear power plants, but many of the approaches can also be applied outside the nuclear industry. The thesis consists of a summary and seven publications. The summary provides an overview of ageing management and discusses the role of reliability methods in ageing analyses. In the publications, practical applications and method development are described in more detail. The application areas at component and system level are motor-operated valves and protection automation systems, for which experience-based ageing analyses have been demonstrated. Furthermore, Bayesian ageing models for repairable components have been developed, and the management of ageing by improving maintenance practices is discussed. Recommendations for improvement of plant information management in order to facilitate ageing analyses are also given. The evaluation and mitigation of ageing effects on structural components is addressed by promoting the use of probabilistic modelling of crack growth, and developing models for evaluation of the reliability of inspection results. (orig.)

  2. Reliability methods in nuclear power plant ageing management

    Energy Technology Data Exchange (ETDEWEB)

    Simola, K. [VTT Automation, Espoo (Finland). Industrial Automation

    1999-07-01

    The aim of nuclear power plant ageing management is to maintain an adequate safety level throughout the lifetime of the plant. In ageing studies, the reliability of components, systems and structures is evaluated taking into account the possible time-dependent degradation. The phases of ageing analyses are generally the identification of critical components, identification and evaluation of ageing effects, and development of mitigation methods. This thesis focuses on the use of reliability methods and analyses of plant- specific operating experience in nuclear power plant ageing studies. The presented applications and method development have been related to nuclear power plants, but many of the approaches can also be applied outside the nuclear industry. The thesis consists of a summary and seven publications. The summary provides an overview of ageing management and discusses the role of reliability methods in ageing analyses. In the publications, practical applications and method development are described in more detail. The application areas at component and system level are motor-operated valves and protection automation systems, for which experience-based ageing analyses have been demonstrated. Furthermore, Bayesian ageing models for repairable components have been developed, and the management of ageing by improving maintenance practices is discussed. Recommendations for improvement of plant information management in order to facilitate ageing analyses are also given. The evaluation and mitigation of ageing effects on structural components is addressed by promoting the use of probabilistic modelling of crack growth, and developing models for evaluation of the reliability of inspection results. (orig.)

  3. Selected Methods For Increases Reliability The Of Electronic Systems Security

    Directory of Open Access Journals (Sweden)

    Paś Jacek

    2015-11-01

    Full Text Available The article presents the issues related to the different methods to increase the reliability of electronic security systems (ESS for example, a fire alarm system (SSP. Reliability of the SSP in the descriptive sense is a property preservation capacity to implement the preset function (e.g. protection: fire airport, the port, logistics base, etc., at a certain time and under certain conditions, e.g. Environmental, despite the possible non-compliance by a specific subset of elements this system. Analyzing the available literature on the ESS-SSP is not available studies on methods to increase the reliability (several works similar topics but moving with respect to the burglary and robbery (Intrusion. Based on the analysis of the set of all paths in the system suitability of the SSP for the scenario mentioned elements fire events (device critical because of security.

  4. Comparison of sample preparation methods for reliable plutonium and neptunium urinalysis using automatic extraction chromatography

    DEFF Research Database (Denmark)

    Qiao, Jixin; Xu, Yihong; Hou, Xiaolin

    2014-01-01

    This paper describes improvement and comparison of analytical methods for simultaneous determination of trace-level plutonium and neptunium in urine samples by inductively coupled plasma mass spectrometry (ICP-MS). Four sample pre-concentration techniques, including calcium phosphate, iron......), it endows urinalysis methods with better reliability and repeatability compared with co-precipitation techniques. In view of the applicability of different pre-concentration techniques proposed previously in the literature, the main challenge behind relevant method development is pointed to be the release...

  5. Literature Review on Processing and Analytical Methods for ...

    Science.gov (United States)

    Report The purpose of this report was to survey the open literature to determine the current state of the science regarding the processing and analytical methods currently available for recovery of F. tularensis from water and soil matrices, and to determine what gaps remain in the collective knowledge concerning F. tularensis identification from environmental samples.

  6. 40 CFR 425.03 - Sulfide analytical methods and applicability.

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 29 2010-07-01 2010-07-01 false Sulfide analytical methods and applicability. 425.03 Section 425.03 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) EFFLUENT GUIDELINES AND STANDARDS LEATHER TANNING AND FINISHING POINT SOURCE CATEGORY General Provisions...

  7. THE QuEChERS ANALYTICAL METHOD COMBINED WITH LOW ...

    African Journals Online (AJOL)

    The method has also been applied to different cereal samples and satisfactory average recoveries ... Analysis of multiclass pesticide residues in foods is a challenging task because of the ... compounds set by regulatory bodies. ..... analytes were used to evaluate the influences of the selected factors on performance of the.

  8. Frontier in nanoscale flows fractional calculus and analytical methods

    CERN Document Server

    Lewis, Roland; Liu, Hong-yan

    2014-01-01

    This ebook covers the basic properties of nanoscale flows, and various analytical and numerical methods for nanoscale flows and environmental flows. This ebook is a good reference not only for audience of the journal, but also for various communities in mathematics, nanotechnology and environmental science.

  9. Advances in the Analytical Methods for Determining the Antioxidant ...

    African Journals Online (AJOL)

    Advances in the Analytical Methods for Determining the Antioxidant Properties of Honey: A Review. M Moniruzzaman, MI Khalil, SA Sulaiman, SH Gan. Abstract. Free radicals and reactive oxygen species (ROS) have been implicated in contributing to the processes of aging and disease. In an effort to combat free radical ...

  10. Pilot testing of SHRP 2 reliability data and analytical products: Washington.

    Science.gov (United States)

    2014-07-30

    The second Strategic Highway Research Program (SHRP 2) addresses the challenges of moving people and goods efficiently and safely on the nations highways. In its Reliability focus area, the research emphasizes improving the reliability of highway ...

  11. Analytical difficulties facing today's regulatory laboratories: issues in method validation.

    Science.gov (United States)

    MacNeil, James D

    2012-08-01

    The challenges facing analytical laboratories today are not unlike those faced in the past, although both the degree of complexity and the rate of change have increased. Challenges such as development and maintenance of expertise, maintenance and up-dating of equipment, and the introduction of new test methods have always been familiar themes for analytical laboratories, but international guidelines for laboratories involved in the import and export testing of food require management of such changes in a context which includes quality assurance, accreditation, and method validation considerations. Decisions as to when a change in a method requires re-validation of the method or on the design of a validation scheme for a complex multi-residue method require a well-considered strategy, based on a current knowledge of international guidance documents and regulatory requirements, as well the laboratory's quality system requirements. Validation demonstrates that a method is 'fit for purpose', so the requirement for validation should be assessed in terms of the intended use of a method and, in the case of change or modification of a method, whether that change or modification may affect a previously validated performance characteristic. In general, method validation involves method scope, calibration-related parameters, method precision, and recovery. Any method change which may affect method scope or any performance parameters will require re-validation. Some typical situations involving change in methods are discussed and a decision process proposed for selection of appropriate validation measures. © 2012 John Wiley & Sons, Ltd.

  12. Human reliability analysis methods for probabilistic safety assessment

    International Nuclear Information System (INIS)

    Pyy, P.

    2000-11-01

    Human reliability analysis (HRA) of a probabilistic safety assessment (PSA) includes identifying human actions from safety point of view, modelling the most important of them in PSA models, and assessing their probabilities. As manifested by many incidents and studies, human actions may have both positive and negative effect on safety and economy. Human reliability analysis is one of the areas of probabilistic safety assessment (PSA) that has direct applications outside the nuclear industry. The thesis focuses upon developments in human reliability analysis methods and data. The aim is to support PSA by extending the applicability of HRA. The thesis consists of six publications and a summary. The summary includes general considerations and a discussion about human actions in the nuclear power plant (NPP) environment. A condensed discussion about the results of the attached publications is then given, including new development in methods and data. At the end of the summary part, the contribution of the publications to good practice in HRA is presented. In the publications, studies based on the collection of data on maintenance-related failures, simulator runs and expert judgement are presented in order to extend the human reliability analysis database. Furthermore, methodological frameworks are presented to perform a comprehensive HRA, including shutdown conditions, to study reliability of decision making, and to study the effects of wrong human actions. In the last publication, an interdisciplinary approach to analysing human decision making is presented. The publications also include practical applications of the presented methodological frameworks. (orig.)

  13. A GPU code for analytic continuation through a sampling method

    Directory of Open Access Journals (Sweden)

    Johan Nordström

    2016-01-01

    Full Text Available We here present a code for performing analytic continuation of fermionic Green’s functions and self-energies as well as bosonic susceptibilities on a graphics processing unit (GPU. The code is based on the sampling method introduced by Mishchenko et al. (2000, and is written for the widely used CUDA platform from NVidia. Detailed scaling tests are presented, for two different GPUs, in order to highlight the advantages of this code with respect to standard CPU computations. Finally, as an example of possible applications, we provide the analytic continuation of model Gaussian functions, as well as more realistic test cases from many-body physics.

  14. A reliable method for the stability analysis of structures ...

    African Journals Online (AJOL)

    The detection of structural configurations with singular tangent stiffness matrix is essential because they can be unstable. The secondary paths, especially in unstable buckling, can play the most important role in the loss of stability and collapse of the structure. A new method for reliable detection and accurate computation of ...

  15. Methods to compute reliabilities for genomic predictions of feed intake

    Science.gov (United States)

    For new traits without historical reference data, cross-validation is often the preferred method to validate reliability (REL). Time truncation is less useful because few animals gain substantial REL after the truncation point. Accurate cross-validation requires separating genomic gain from pedigree...

  16. Planning of operation & maintenance using risk and reliability based methods

    DEFF Research Database (Denmark)

    Florian, Mihai; Sørensen, John Dalsgaard

    2015-01-01

    Operation and maintenance (OM) of offshore wind turbines contributes with a substantial part of the total levelized cost of energy (LCOE). The objective of this paper is to present an application of risk- and reliability-based methods for planning of OM. The theoretical basis is presented...

  17. Assessment of reliability of Greulich and Pyle (gp) method for ...

    African Journals Online (AJOL)

    Background: Greulich and Pyle standards are the most widely used age estimation standards all over the world. The applicability of the Greulich and Pyle standards to populations which differ from their reference population is often questioned. This study aimed to assess the reliability of Greulich and Pyle (GP) method for ...

  18. Prediction of polymer flooding performance using an analytical method

    International Nuclear Information System (INIS)

    Tan Czek Hoong; Mariyamni Awang; Foo Kok Wai

    2001-01-01

    The study investigated the applicability of an analytical method developed by El-Khatib in polymer flooding. Results from a simulator UTCHEM and experiments were compared with the El-Khatib prediction method. In general, by assuming a constant viscosity polymer injection, the method gave much higher recovery values than the simulation runs and the experiments. A modification of the method gave better correlation, albeit only oil production. Investigation is continuing on modifying the method so that a better overall fit can be obtained for polymer flooding. (Author)

  19. Use of scientometrics to assess nuclear and other analytical methods

    International Nuclear Information System (INIS)

    Lyon, W.S.

    1986-01-01

    Scientometrics involves the use of quantitative methods to investigate science viewed as an information process. Scientometric studies can be useful in ascertaining which methods have been most employed for various analytical determinations as well as for predicting which methods will continue to be used in the immediate future and which appear to be losing favor with the analytical community. Published papers in the technical literature are the primary source materials for scientometric studies; statistical methods and computer techniques are the tools. Recent studies have included growth and trends in prompt nuclear analysis impact of research published in a technical journal, and institutional and national representation, speakers and topics at several IAEA conferences, at modern trends in activation analysis conferences, and at other non-nuclear oriented conferences. Attempts have also been made to predict future growth of various topics and techniques. 13 refs., 4 figs., 17 tabs

  20. An analytic data analysis method for oscillatory slug tests.

    Science.gov (United States)

    Chen, Chia-Shyun

    2006-01-01

    An analytical data analysis method is developed for slug tests in partially penetrating wells in confined or unconfined aquifers of high hydraulic conductivity. As adapted from the van der Kamp method, the determination of the hydraulic conductivity is based on the occurrence times and the displacements of the extreme points measured from the oscillatory data and their theoretical counterparts available in the literature. This method is applied to two sets of slug test response data presented by Butler et al.: one set shows slow damping with seven discernable extremities, and the other shows rapid damping with three extreme points. The estimates of the hydraulic conductivity obtained by the analytic method are in good agreement with those determined by an available curve-matching technique.

  1. Development and validation of analytical methods for dietary supplements

    International Nuclear Information System (INIS)

    Sullivan, Darryl; Crowley, Richard

    2006-01-01

    The expanding use of innovative botanical ingredients in dietary supplements and foods has resulted in a flurry of research aimed at the development and validation of analytical methods for accurate measurement of active ingredients. The pressing need for these methods is being met through an expansive collaborative initiative involving industry, government, and analytical organizations. This effort has resulted in the validation of several important assays as well as important advances in the method engineering procedures which have improved the efficiency of the process. The initiative has also allowed researchers to hurdle many of the barricades that have hindered accurate analysis such as the lack of reference standards and comparative data. As the availability for nutraceutical products continues to increase these methods will provide consumers and regulators with the scientific information needed to assure safety and dependable labeling

  2. Use of scientometrics to assess nuclear and other analytical methods

    Energy Technology Data Exchange (ETDEWEB)

    Lyon, W.S.

    1986-01-01

    Scientometrics involves the use of quantitative methods to investigate science viewed as an information process. Scientometric studies can be useful in ascertaining which methods have been most employed for various analytical determinations as well as for predicting which methods will continue to be used in the immediate future and which appear to be losing favor with the analytical community. Published papers in the technical literature are the primary source materials for scientometric studies; statistical methods and computer techniques are the tools. Recent studies have included growth and trends in prompt nuclear analysis impact of research published in a technical journal, and institutional and national representation, speakers and topics at several IAEA conferences, at modern trends in activation analysis conferences, and at other non-nuclear oriented conferences. Attempts have also been made to predict future growth of various topics and techniques. 13 refs., 4 figs., 17 tabs.

  3. An analytical optimization method for electric propulsion orbit transfer vehicles

    International Nuclear Information System (INIS)

    Oleson, S.R.

    1993-01-01

    Due to electric propulsion's inherent propellant mass savings over chemical propulsion, electric propulsion orbit transfer vehicles (EPOTVs) are a highly efficient mode of orbit transfer. When selecting an electric propulsion device (ion, MPD, or arcjet) and propellant for a particular mission, it is preferable to use quick, analytical system optimization methods instead of time intensive numerical integration methods. It is also of interest to determine each thruster's optimal operating characteristics for a specific mission. Analytical expressions are derived which determine the optimal specific impulse (Isp) for each type of electric thruster to maximize payload fraction for a desired thrusting time. These expressions take into account the variation of thruster efficiency with specific impulse. Verification of the method is made with representative electric propulsion values on a LEO-to-GEO mission. Application of the method to specific missions is discussed

  4. Procedures for treating common cause failures in safety and reliability studies: Analytical background and techniques

    International Nuclear Information System (INIS)

    Mosleh, A.; Fleming, K.N.; Parry, G.W.; Paula, H.M.; Worledge, D.H.; Rasmuson, D.M.

    1989-01-01

    Volume I of this report presents a framework for the inclusion of the impact of common cause failures in risk and reliability evaluations. Common cause failures are defined as that subset of dependent failures for which causes are not explicitly included in the logic model as basic events. The emphasis here is on providing procedures for a practical, systematic approach that can be used to perform and clearly document the analysis. The framework and the methods discussed for performing the different stages of the analysis integrate insights obtained from engineering assessments of the system and the historical evidence from multiple failure events into a systematic, reproducible, and defensible analysis. This document, Volume 2, contains a series of appendices that provide additional background and methodological detail on several important topics discussed in Volume I

  5. Selection of analytical methods for mixed waste analysis at the Hanford Site

    International Nuclear Information System (INIS)

    Morant, P.M.

    1994-09-01

    This document describes the process that the US Department of Energy (DOE), Richland Operations Office (RL) and contractor laboratories use to select appropriate or develop new or modified analytical methods. These methods are needed to provide reliable mixed waste characterization data that meet project-specific quality assurance (QA) requirements while also meeting health and safety standards for handling radioactive materials. This process will provide the technical basis for DOE's analysis of mixed waste and support requests for regulatory approval of these new methods when they are used to satisfy the regulatory requirements of the Hanford Federal Facility Agreement and Consent Order (Tri-party Agreement) (Ecology et al. 1992)

  6. Long-Term Prediction of Satellite Orbit Using Analytical Method

    Directory of Open Access Journals (Sweden)

    Jae-Cheol Yoon

    1997-12-01

    Full Text Available A long-term prediction algorithm of geostationary orbit was developed using the analytical method. The perturbation force models include geopotential upto fifth order and degree and luni-solar gravitation, and solar radiation pressure. All of the perturbation effects were analyzed by secular variations, short-period variations, and long-period variations for equinoctial elements such as the semi-major axis, eccentricity vector, inclination vector, and mean longitude of the satellite. Result of the analytical orbit propagator was compared with that of the cowell orbit propagator for the KOREASAT. The comparison indicated that the analytical solution could predict the semi-major axis with an accuarcy of better than ~35meters over a period of 3 month.

  7. Statistical Bayesian method for reliability evaluation based on ADT data

    Science.gov (United States)

    Lu, Dawei; Wang, Lizhi; Sun, Yusheng; Wang, Xiaohong

    2018-05-01

    Accelerated degradation testing (ADT) is frequently conducted in the laboratory to predict the products’ reliability under normal operating conditions. Two kinds of methods, degradation path models and stochastic process models, are utilized to analyze degradation data and the latter one is the most popular method. However, some limitations like imprecise solution process and estimation result of degradation ratio still exist, which may affect the accuracy of the acceleration model and the extrapolation value. Moreover, the conducted solution of this problem, Bayesian method, lose key information when unifying the degradation data. In this paper, a new data processing and parameter inference method based on Bayesian method is proposed to handle degradation data and solve the problems above. First, Wiener process and acceleration model is chosen; Second, the initial values of degradation model and parameters of prior and posterior distribution under each level is calculated with updating and iteration of estimation values; Third, the lifetime and reliability values are estimated on the basis of the estimation parameters; Finally, a case study is provided to demonstrate the validity of the proposed method. The results illustrate that the proposed method is quite effective and accuracy in estimating the lifetime and reliability of a product.

  8. Methods of analytical check for highly pure tungsten

    International Nuclear Information System (INIS)

    Miklin, D.G.; Karpov, Yu.A.; Orlova, V.A.

    1993-01-01

    The review is devoted to the methods of high-purity tungsten analysis. Current trends in the development of this branch of analytical chemistry are considered. Application of both instrument mass-spectrometry analysis and optico-spectral, activation methods and mass-spectrometry ones with inductively-bound plasma in combination with preliminary isolation of the basis and impurity concentration is expected to be the most actual

  9. Issues in benchmarking human reliability analysis methods: A literature review

    International Nuclear Information System (INIS)

    Boring, Ronald L.; Hendrickson, Stacey M.L.; Forester, John A.; Tran, Tuan Q.; Lois, Erasmia

    2010-01-01

    There is a diversity of human reliability analysis (HRA) methods available for use in assessing human performance within probabilistic risk assessments (PRA). Due to the significant differences in the methods, including the scope, approach, and underlying models, there is a need for an empirical comparison investigating the validity and reliability of the methods. To accomplish this empirical comparison, a benchmarking study comparing and evaluating HRA methods in assessing operator performance in simulator experiments is currently underway. In order to account for as many effects as possible in the construction of this benchmarking study, a literature review was conducted, reviewing past benchmarking studies in the areas of psychology and risk assessment. A number of lessons learned through these studies is presented in order to aid in the design of future HRA benchmarking endeavors.

  10. Issues in benchmarking human reliability analysis methods : a literature review.

    Energy Technology Data Exchange (ETDEWEB)

    Lois, Erasmia (US Nuclear Regulatory Commission); Forester, John Alan; Tran, Tuan Q. (Idaho National Laboratory, Idaho Falls, ID); Hendrickson, Stacey M. Langfitt; Boring, Ronald L. (Idaho National Laboratory, Idaho Falls, ID)

    2008-04-01

    There is a diversity of human reliability analysis (HRA) methods available for use in assessing human performance within probabilistic risk assessment (PRA). Due to the significant differences in the methods, including the scope, approach, and underlying models, there is a need for an empirical comparison investigating the validity and reliability of the methods. To accomplish this empirical comparison, a benchmarking study is currently underway that compares HRA methods with each other and against operator performance in simulator studies. In order to account for as many effects as possible in the construction of this benchmarking study, a literature review was conducted, reviewing past benchmarking studies in the areas of psychology and risk assessment. A number of lessons learned through these studies are presented in order to aid in the design of future HRA benchmarking endeavors.

  11. Hanford environmental analytical methods (methods as of March 1990)

    International Nuclear Information System (INIS)

    Goheen, S.D.; McCulloch, M.; Daniel, J.L.

    1993-05-01

    Information is provided on the techniques employed towards the chemical analysis of volatile, semi-volatile matter, pesticides and PCB's at the Hanford Reservation. Sample preparation methods are included

  12. An automated method for estimating reliability of grid systems using Bayesian networks

    International Nuclear Information System (INIS)

    Doguc, Ozge; Emmanuel Ramirez-Marquez, Jose

    2012-01-01

    Grid computing has become relevant due to its applications to large-scale resource sharing, wide-area information transfer, and multi-institutional collaborating. In general, in grid computing a service requests the use of a set of resources, available in a grid, to complete certain tasks. Although analysis tools and techniques for these types of systems have been studied, grid reliability analysis is generally computation-intensive to obtain due to the complexity of the system. Moreover, conventional reliability models have some common assumptions that cannot be applied to the grid systems. Therefore, new analytical methods are needed for effective and accurate assessment of grid reliability. This study presents a new method for estimating grid service reliability, which does not require prior knowledge about the grid system structure unlike the previous studies. Moreover, the proposed method does not rely on any assumptions about the link and node failure rates. This approach is based on a data-mining algorithm, the K2, to discover the grid system structure from raw historical system data, that allows to find minimum resource spanning trees (MRST) within the grid then, uses Bayesian networks (BN) to model the MRST and estimate grid service reliability.

  13. Survey of methods used to asses human reliability in the human factors reliability benchmark exercise

    International Nuclear Information System (INIS)

    Poucet, A.

    1988-01-01

    The Joint Research Centre of the European Commission has organised a Human Factors Reliability Benchmark Exercise (HF-RBE) with the aim to assess the state-of-the-art in human reliability modelling and assessment. Fifteen teams from eleven countries, representing industry, utilities, licensing organisations and research institutes, participate in the HF-RBE, which is organised around two study cases: (1) analysis of routine functional test and maintenance procedures, with the aim to assess the probability of test-induced failures, the probability of failures to remain unrevealed, and the potential to initiate transients because of errors performed in the test; and (2) analysis of human actions during an operational transient, with the aim to assess the probability that the operators will correctly diagnose the malfunctions and take proper corrective action. The paper briefly reports how the HF-RBE was structured and gives an overview of the methods that have been used for predicting human reliability in both study cases. The experience in applying these methods is discussed and the results obtained are compared. (author)

  14. Analytical method comparisons for the accurate determination of PCBs in sediments

    Energy Technology Data Exchange (ETDEWEB)

    Numata, M.; Yarita, T.; Aoyagi, Y.; Yamazaki, M.; Takatsu, A. [National Metrology Institute of Japan, Tsukuba (Japan)

    2004-09-15

    National Metrology Institute of Japan in National Institute of Advanced Industrial Science and Technology (NMIJ/AIST) has been developing several matrix reference materials, for example, sediments, water and biological tissues, for the determinations of heavy metals and organometallic compounds. The matrix compositions of those certified reference materials (CRMs) are similar to compositions of actual samples, and those are useful for validating analytical procedures. ''Primary methods of measurements'' are essential to obtain accurate and SI-traceable certified values in the reference materials, because the methods have the highest quality of measurement. However, inappropriate analytical operations, such as incomplete extraction of analytes or crosscontamination during analytical procedures, will cause error of analytical results, even if one of the primary methods, isotope-dilution, is utilized. To avoid possible procedural bias for the certification of reference materials, we employ more than two analytical methods which have been optimized beforehand. Because the accurate determination of trace POPs in the environment is important to evaluate their risk, reliable CRMs are required by environmental chemists. Therefore, we have also been preparing matrix CRMs for the determination of POPs. To establish accurate analytical procedures for the certification of POPs, extraction is one of the critical steps as described above. In general, conventional extraction techniques for the determination of POPs, such as Soxhlet extraction (SOX) and saponification (SAP), have been characterized well, and introduced as official methods for environmental analysis. On the other hand, emerging techniques, such as microwave-assisted extraction (MAE), pressurized fluid extraction (PFE) and supercritical fluid extraction (SFE), give higher recovery yields of analytes with relatively short extraction time and small amount of solvent, by reasons of the high

  15. Nuclear and nuclear related analytical methods applied in environmental research

    International Nuclear Information System (INIS)

    Popescu, Ion V.; Gheboianu, Anca; Bancuta, Iulian; Cimpoca, G. V; Stihi, Claudia; Radulescu, Cristiana; Oros Calin; Frontasyeva, Marina; Petre, Marian; Dulama, Ioana; Vlaicu, G.

    2010-01-01

    Nuclear Analytical Methods can be used for research activities on environmental studies like water quality assessment, pesticide residues, global climatic change (transboundary), pollution and remediation. Heavy metal pollution is a problem associated with areas of intensive industrial activity. In this work the moss bio monitoring technique was employed to study the atmospheric deposition in Dambovita County Romania. Also, there were used complementary nuclear and atomic analytical methods: Neutron Activation Analysis (NAA), Atomic Absorption Spectrometry (AAS) and Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES). These high sensitivity analysis methods were used to determine the chemical composition of some samples of mosses placed in different areas with different pollution industrial sources. The concentrations of Cr, Fe, Mn, Ni and Zn were determined. The concentration of Fe from the same samples was determined using all these methods and we obtained a very good agreement, in statistical limits, which demonstrate the capability of these analytical methods to be applied on a large spectrum of environmental samples with the same results. (authors)

  16. Analytical methods for determination of mycotoxins: a review.

    Science.gov (United States)

    Turner, Nicholas W; Subrahmanyam, Sreenath; Piletsky, Sergey A

    2009-01-26

    Mycotoxins are small (MW approximately 700), toxic chemical products formed as secondary metabolites by a few fungal species that readily colonise crops and contaminate them with toxins in the field or after harvest. Ochratoxins and Aflatoxins are mycotoxins of major significance and hence there has been significant research on broad range of analytical and detection techniques that could be useful and practical. Due to the variety of structures of these toxins, it is impossible to use one standard technique for analysis and/or detection. Practical requirements for high-sensitivity analysis and the need for a specialist laboratory setting create challenges for routine analysis. Several existing analytical techniques, which offer flexible and broad-based methods of analysis and in some cases detection, have been discussed in this manuscript. There are a number of methods used, of which many are lab-based, but to our knowledge there seems to be no single technique that stands out above the rest, although analytical liquid chromatography, commonly linked with mass spectroscopy is likely to be popular. This review manuscript discusses (a) sample pre-treatment methods such as liquid-liquid extraction (LLE), supercritical fluid extraction (SFE), solid phase extraction (SPE), (b) separation methods such as (TLC), high performance liquid chromatography (HPLC), gas chromatography (GC), and capillary electrophoresis (CE) and (c) others such as ELISA. Further currents trends, advantages and disadvantages and future prospects of these methods have been discussed.

  17. Reliability and discriminatory power of methods for dental plaque quantification

    Directory of Open Access Journals (Sweden)

    Daniela Prócida Raggio

    2010-04-01

    Full Text Available OBJECTIVE: This in situ study evaluated the discriminatory power and reliability of methods of dental plaque quantification and the relationship between visual indices (VI and fluorescence camera (FC to detect plaque. MATERIAL AND METHODS: Six volunteers used palatal appliances with six bovine enamel blocks presenting different stages of plaque accumulation. The presence of plaque with and without disclosing was assessed using VI. Images were obtained with FC and digital camera in both conditions. The area covered by plaque was assessed. Examinations were done by two independent examiners. Data were analyzed by Kruskal-Wallis and Kappa tests to compare different conditions of samples and to assess the inter-examiner reproducibility. RESULTS: Some methods presented adequate reproducibility. The Turesky index and the assessment of area covered by disclosed plaque in the FC images presented the highest discriminatory powers. CONCLUSION: The Turesky index and images with FC with disclosing present good reliability and discriminatory power in quantifying dental plaque.

  18. A generic method for estimating system reliability using Bayesian networks

    International Nuclear Information System (INIS)

    Doguc, Ozge; Ramirez-Marquez, Jose Emmanuel

    2009-01-01

    This study presents a holistic method for constructing a Bayesian network (BN) model for estimating system reliability. BN is a probabilistic approach that is used to model and predict the behavior of a system based on observed stochastic events. The BN model is a directed acyclic graph (DAG) where the nodes represent system components and arcs represent relationships among them. Although recent studies on using BN for estimating system reliability have been proposed, they are based on the assumption that a pre-built BN has been designed to represent the system. In these studies, the task of building the BN is typically left to a group of specialists who are BN and domain experts. The BN experts should learn about the domain before building the BN, which is generally very time consuming and may lead to incorrect deductions. As there are no existing studies to eliminate the need for a human expert in the process of system reliability estimation, this paper introduces a method that uses historical data about the system to be modeled as a BN and provides efficient techniques for automated construction of the BN model, and hence estimation of the system reliability. In this respect K2, a data mining algorithm, is used for finding associations between system components, and thus building the BN model. This algorithm uses a heuristic to provide efficient and accurate results while searching for associations. Moreover, no human intervention is necessary during the process of BN construction and reliability estimation. The paper provides a step-by-step illustration of the method and evaluation of the approach with literature case examples

  19. A generic method for estimating system reliability using Bayesian networks

    Energy Technology Data Exchange (ETDEWEB)

    Doguc, Ozge [Stevens Institute of Technology, Hoboken, NJ 07030 (United States); Ramirez-Marquez, Jose Emmanuel [Stevens Institute of Technology, Hoboken, NJ 07030 (United States)], E-mail: jmarquez@stevens.edu

    2009-02-15

    This study presents a holistic method for constructing a Bayesian network (BN) model for estimating system reliability. BN is a probabilistic approach that is used to model and predict the behavior of a system based on observed stochastic events. The BN model is a directed acyclic graph (DAG) where the nodes represent system components and arcs represent relationships among them. Although recent studies on using BN for estimating system reliability have been proposed, they are based on the assumption that a pre-built BN has been designed to represent the system. In these studies, the task of building the BN is typically left to a group of specialists who are BN and domain experts. The BN experts should learn about the domain before building the BN, which is generally very time consuming and may lead to incorrect deductions. As there are no existing studies to eliminate the need for a human expert in the process of system reliability estimation, this paper introduces a method that uses historical data about the system to be modeled as a BN and provides efficient techniques for automated construction of the BN model, and hence estimation of the system reliability. In this respect K2, a data mining algorithm, is used for finding associations between system components, and thus building the BN model. This algorithm uses a heuristic to provide efficient and accurate results while searching for associations. Moreover, no human intervention is necessary during the process of BN construction and reliability estimation. The paper provides a step-by-step illustration of the method and evaluation of the approach with literature case examples.

  20. The application of the analytic hierarchy process (AHP) in uranium mine mining method of the optimal selection

    International Nuclear Information System (INIS)

    Tan Zhongyin; Kuang Zhengping; Qiu Huiyuan

    2014-01-01

    Analytic hierarchy process, AHP, is a combination of qualitative and quantitative, systematic and hierarchical analysis method. Basic decision theory of analytic hierarchy process is applied in this article, with a project example in north Guangdong region as the research object, the in-situ mining method optimization choose hierarchical analysis model is established and the analysis method, The results show that, the AHP model for mining method selecting model was reliable, optimization results were conformity with the actual use of the in-situ mining method, and it has better practicability. (authors)

  1. Limitations in simulator time-based human reliability analysis methods

    International Nuclear Information System (INIS)

    Wreathall, J.

    1989-01-01

    Developments in human reliability analysis (HRA) methods have evolved slowly. Current methods are little changed from those of almost a decade ago, particularly in the use of time-reliability relationships. While these methods were suitable as an interim step, the time (and the need) has come to specify the next evolution of HRA methods. As with any performance-oriented data source, power plant simulator data have no direct connection to HRA models. Errors reported in data are normal deficiencies observed in human performance; failures are events modeled in probabilistic risk assessments (PRAs). Not all errors cause failures; not all failures are caused by errors. Second, the times at which actions are taken provide no measure of the likelihood of failures to act correctly within an accident scenario. Inferences can be made about human reliability, but they must be made with great care. Specific limitations are discussed. Simulator performance data are useful in providing qualitative evidence of the variety of error types and their potential influences on operating systems. More work is required to combine recent developments in the psychology of error with the qualitative data collected at stimulators. Until data become openly available, however, such an advance will not be practical

  2. An analytical method for neutron thermalization calculations in heterogenous reactors

    Energy Technology Data Exchange (ETDEWEB)

    Pop-Jordanov, J [Boris Kidric Institute of Nuclear Sciences, Vinca, Belgrade (Yugoslavia)

    1965-07-01

    It is well known that the use of the diffusion approximation for stumethods are rather laborious and require the use of large digital computers. In this paper, the use of the diffusion approximation in absorbing media has been avoided, but the treatment remained analytical, thus simplifying practical calculations.

  3. Methods for the calculation of uncertainty in analytical chemistry

    Energy Technology Data Exchange (ETDEWEB)

    Suh, M. Y.; Sohn, S. C.; Park, Y. J.; Park, K. K.; Jee, K. Y.; Joe, K. S.; Kim, W. H

    2000-07-01

    This report describes the statistical rules for evaluating and expressing uncertainty in analytical chemistry. The procedures for the evaluation of uncertainty in chemical analysis are illustrated by worked examples. This report, in particular, gives guidance on how uncertainty can be estimated from various chemical analyses. This report can be also used for planning the experiments which will provide the information required to obtain an estimate of uncertainty for the method.

  4. Application of Multi-Analyte Methods for Pesticide Formulations

    Energy Technology Data Exchange (ETDEWEB)

    Lantos, J.; Virtics, I. [Plant Protection & Soil Conservation Service of Szabolcs-Szatmár-Bereg County, Nyíregyháza (Hungary)

    2009-07-15

    The application of multi-analyte methods for pesticide formulations by GC analysis is discussed. HPLC was used to determine active ingredients. HPLC elution sequences were related to individual n-octanol/water partition coefficients. Real laboratory data are presented and evaluated with regard to validation requirements. The retention time data of pesticides on different HPLC columns under gradient and isocratic conditions are compared to illustrate the applicability of the methodologies. (author)

  5. An analytical method for neutron thermalization calculations in heterogenous reactors

    International Nuclear Information System (INIS)

    Pop-Jordanov, J.

    1965-01-01

    It is well known that the use of the diffusion approximation for studying neutron thermalization in heterogeneous reactors may result in considerable errors. On the other hand, more exact numerical methods are rather laborious and require the use of large digital computers. In this paper, the use of the diffusion approximation in absorbing media has been avoided, but the treatment remained analytical, thus simplifying practical calculations

  6. AK-SYS: An adaptation of the AK-MCS method for system reliability

    International Nuclear Information System (INIS)

    Fauriat, W.; Gayton, N.

    2014-01-01

    A lot of research work has been proposed over the last two decades to evaluate the probability of failure of a structure involving a very time-consuming mechanical model. Surrogate model approaches based on Kriging, such as the Efficient Global Reliability Analysis (EGRA) or the Active learning and Kriging-based Monte-Carlo Simulation (AK-MCS) methods, are very efficient and each has advantages of its own. EGRA is well suited to evaluating small probabilities, as the surrogate can be used to classify any population. AK-MCS is built in relation to a given population and requires no optimization program for the active learning procedure to be performed. It is therefore easier to implement and more likely to spend computational effort on areas with a significant probability content. When assessing system reliability, analytical approaches and first-order approximation are widely used in the literature. However, in the present paper we rather focus on sampling techniques and, considering the recent adaptation of the EGRA method for systems, a strategy is presented to adapt the AK-MCS method for system reliability. The AK-SYS method, “Active learning and Kriging-based SYStem reliability method”, is presented. Its high efficiency and accuracy are illustrated via various examples

  7. Analytical Methods for Biomass Characterization during Pretreatment and Bioconversion

    Energy Technology Data Exchange (ETDEWEB)

    Pu, Yunqiao [ORNL; Meng, Xianzhi [University of Tennessee, Knoxville (UTK); Yoo, Chang Geun; Li, Mi; Ragauskas, Arthur J [ORNL

    2016-01-01

    Lignocellulosic biomass has been introduced as a promising resource for alternative fuels and chemicals because of its abundance and complement for petroleum resources. Biomass is a complex biopolymer and its compositional and structural characteristics largely vary depending on its species as well as growth environments. Because of complexity and variety of biomass, understanding its physicochemical characteristics is a key for effective biomass utilization. Characterization of biomass does not only provide critical information of biomass during pretreatment and bioconversion, but also give valuable insights on how to utilize the biomass. For better understanding biomass characteristics, good grasp and proper selection of analytical methods are necessary. This chapter introduces existing analytical approaches that are widely employed for biomass characterization during biomass pretreatment and conversion process. Diverse analytical methods using Fourier transform infrared (FTIR) spectroscopy, gel permeation chromatography (GPC), and nuclear magnetic resonance (NMR) spectroscopy for biomass characterization are reviewed. In addition, biomass accessibility methods by analyzing surface properties of biomass are also summarized in this chapter.

  8. EPA's analytical methods for water: The next generation

    International Nuclear Information System (INIS)

    Hites, R.A.; Budde, W.L.

    1991-01-01

    By the late 1970s, it had become clear to EPA that organic compounds were polluting many of the nation's waters. By 1977, as a result of a lawsuit by several environmentally concerned plaintiffs, EPA had focused on a list of 114 'priority' organic pollutants. Its long-term goal was the regulation of specific compounds that were found to pose significant environmental problems, a daunting task. Tens of thousands of samples needed to be measured by hundreds of different laboratories. Clearly, there were concerns about the comparability of data among laboratories. The result was a series of laboratory-based analytical 'methods.' These EPA methods are detailed, step-by-step directions (recipes) that describe everything the analyst needs to know to complete a satisfactory analysis. During the 1970s the first set of methods was developed; this was the '600 series' for the analysis of organic compounds in wastewater. In 1979 and the 1980s, a set of '500 series' methods, focusing on drinking water, was developed. By now, many of the 500 and 600 series methods are in widespread use, and it is clear that there are considerably overlaps among the methods in terms of both procedures and analytes. Indiana University was asked by EPA to consider the question, 'Is it possible to revise or eliminate some of the 500 and 600 series methods and effect a savings of time and money?' This and related questions were studied and recommendations were developed

  9. Multiplier ideal sheaves and analytic methods in algebraic geometry

    International Nuclear Information System (INIS)

    Demailly, J.-P.

    2001-01-01

    Our main purpose here is to describe a few analytic tools which are useful to study questions such as linear series and vanishing theorems for algebraic vector bundles. One of the early successes of analytic methods in this context is Kodaira's use of the Bochner technique in relation with the theory of harmonic forms, during the decade 1950-60.The idea is to represent cohomology classes by harmonic forms and to prove vanishing theorems by means of suitable a priori curvature estimates. We pursue the study of L2 estimates, in relation with the Nullstellenstatz and with the extension problem. We show how subadditivity can be used to derive an approximation theorem for (almost) plurisubharmonic functions: any such function can be approximated by a sequence of (almost) plurisubharmonic functions which are smooth outside an analytic set, and which define the same multiplier ideal sheaves. From this, we derive a generalized version of the hard Lefschetz theorem for cohomology with values in a pseudo-effective line bundle; namely, the Lefschetz map is surjective when the cohomology groups are twisted by the relevant multiplier ideal sheaves. These notes are essentially written with the idea of serving as an analytic tool- box for algebraic geometers. Although efficient algebraic techniques exist, our feeling is that the analytic techniques are very flexible and offer a large variety of guidelines for more algebraic questions (including applications to number theory which are not discussed here). We made a special effort to use as little prerequisites and to be as self-contained as possible; hence the rather long preliminary sections dealing with basic facts of complex differential geometry

  10. Multiplier ideal sheaves and analytic methods in algebraic geometry

    Energy Technology Data Exchange (ETDEWEB)

    Demailly, J -P [Universite de Grenoble I, Institut Fourier, Saint-Martin d' Heres (France)

    2001-12-15

    Our main purpose here is to describe a few analytic tools which are useful to study questions such as linear series and vanishing theorems for algebraic vector bundles. One of the early successes of analytic methods in this context is Kodaira's use of the Bochner technique in relation with the theory of harmonic forms, during the decade 1950-60.The idea is to represent cohomology classes by harmonic forms and to prove vanishing theorems by means of suitable a priori curvature estimates. We pursue the study of L2 estimates, in relation with the Nullstellenstatz and with the extension problem. We show how subadditivity can be used to derive an approximation theorem for (almost) plurisubharmonic functions: any such function can be approximated by a sequence of (almost) plurisubharmonic functions which are smooth outside an analytic set, and which define the same multiplier ideal sheaves. From this, we derive a generalized version of the hard Lefschetz theorem for cohomology with values in a pseudo-effective line bundle; namely, the Lefschetz map is surjective when the cohomology groups are twisted by the relevant multiplier ideal sheaves. These notes are essentially written with the idea of serving as an analytic tool- box for algebraic geometers. Although efficient algebraic techniques exist, our feeling is that the analytic techniques are very flexible and offer a large variety of guidelines for more algebraic questions (including applications to number theory which are not discussed here). We made a special effort to use as little prerequisites and to be as self-contained as possible; hence the rather long preliminary sections dealing with basic facts of complex differential geometry.

  11. Manual of analytical methods for the Industrial Hygiene Chemistry Laboratory

    Energy Technology Data Exchange (ETDEWEB)

    Greulich, K.A.; Gray, C.E. (comp.)

    1991-08-01

    This Manual is compiled from techniques used in the Industrial Hygiene Chemistry Laboratory of Sandia National Laboratories in Albuquerque, New Mexico. The procedures are similar to those used in other laboratories devoted to industrial hygiene practices. Some of the methods are standard; some, modified to suit our needs; and still others, developed at Sandia. The authors have attempted to present all methods in a simple and concise manner but in sufficient detail to make them readily usable. It is not to be inferred that these methods are universal for any type of sample, but they have been found very reliable for the types of samples mentioned.

  12. Manual of analytical methods for the Industrial Hygiene Chemistry Laboratory

    International Nuclear Information System (INIS)

    Greulich, K.A.; Gray, C.E.

    1991-08-01

    This Manual is compiled from techniques used in the Industrial Hygiene Chemistry Laboratory of Sandia National Laboratories in Albuquerque, New Mexico. The procedures are similar to those used in other laboratories devoted to industrial hygiene practices. Some of the methods are standard; some, modified to suit our needs; and still others, developed at Sandia. The authors have attempted to present all methods in a simple and concise manner but in sufficient detail to make them readily usable. It is not to be inferred that these methods are universal for any type of sample, but they have been found very reliable for the types of samples mentioned

  13. Analytic function expansion nodal method for nuclear reactor core design

    International Nuclear Information System (INIS)

    Noh, Hae Man

    1995-02-01

    In most advanced nodal methods the transverse integration is commonly used to reduce the multi-dimensional diffusion equation into equivalent one- dimensional diffusion equations when derving the nodal coupling equations. But the use of the transverse integration results in some limitations. The first limitation is that the transverse leakage term which appears in the transverse integration procedure must be appropriately approximated. The second limitation is that the one-dimensional flux shapes in each spatial direction resulted from the nodal calculation are not accurate enough to be directly used in reconstructing the pinwise flux distributions. Finally the transverse leakage defined for a non-rectangular node such as a hexagonal node or a triangular node is too complicated to be easily handled and may contain non-physical singular terms of step-function and delta-function types. In this thesis, the Analytic Function Expansion Nodal (AFEN) method and its two variations : the Polynomial Expansion Nodal (PEN) method and the hybrid of the AFEN and PEN methods, have been developed to overcome the limitations of the transverse integration procedure. All of the methods solve the multidimensional diffusion equation without the transverse integration. The AFEN method which we believe is the major contribution of this study to the reactor core analysis expands the homogeneous flux distributions within a node in non-separable analytic basis functions satisfying the neutron diffusion equations at any point of the node and expresses the coefficients of the flux expansion in terms of the nodal unknowns which comprise a node-average flux, node-interface fluxes, and corner-point fluxes. Then, the nodal coupling equations composed of the neutron balance equations, the interface current continuity equations, and the corner-point leakage balance equations are solved iteratively to determine all the nodal unknowns. Since the AFEN method does not use the transverse integration in

  14. Modelling of packet traffic with matrix analytic methods

    DEFF Research Database (Denmark)

    Andersen, Allan T.

    1995-01-01

    BISDN network. The heuristic formula did not seem to yield substantially better results than already available approximations. Finally, some results for the finite capacity BMAP/G/1 queue have been obtained. The steady state probability vector of the embedded chain is found by a direct method where...... process. A heuristic formula for the tail behaviour of a single server queue fed by a superposition of renewal processes has been evaluated. The evaluation was performed by applying Matrix Analytic methods. The heuristic formula has applications in the Call Admission Control (CAC) procedure of the future...

  15. Benchmark Comparison of Cloud Analytics Methods Applied to Earth Observations

    Science.gov (United States)

    Lynnes, Chris; Little, Mike; Huang, Thomas; Jacob, Joseph; Yang, Phil; Kuo, Kwo-Sen

    2016-01-01

    Cloud computing has the potential to bring high performance computing capabilities to the average science researcher. However, in order to take full advantage of cloud capabilities, the science data used in the analysis must often be reorganized. This typically involves sharding the data across multiple nodes to enable relatively fine-grained parallelism. This can be either via cloud-based file systems or cloud-enabled databases such as Cassandra, Rasdaman or SciDB. Since storing an extra copy of data leads to increased cost and data management complexity, NASA is interested in determining the benefits and costs of various cloud analytics methods for real Earth Observation cases. Accordingly, NASA's Earth Science Technology Office and Earth Science Data and Information Systems project have teamed with cloud analytics practitioners to run a benchmark comparison on cloud analytics methods using the same input data and analysis algorithms. We have particularly looked at analysis algorithms that work over long time series, because these are particularly intractable for many Earth Observation datasets which typically store data with one or just a few time steps per file. This post will present side-by-side cost and performance results for several common Earth observation analysis operations.

  16. Benchmark Comparison of Cloud Analytics Methods Applied to Earth Observations

    Science.gov (United States)

    Lynnes, C.; Little, M. M.; Huang, T.; Jacob, J. C.; Yang, C. P.; Kuo, K. S.

    2016-12-01

    Cloud computing has the potential to bring high performance computing capabilities to the average science researcher. However, in order to take full advantage of cloud capabilities, the science data used in the analysis must often be reorganized. This typically involves sharding the data across multiple nodes to enable relatively fine-grained parallelism. This can be either via cloud-based filesystems or cloud-enabled databases such as Cassandra, Rasdaman or SciDB. Since storing an extra copy of data leads to increased cost and data management complexity, NASA is interested in determining the benefits and costs of various cloud analytics methods for real Earth Observation cases. Accordingly, NASA's Earth Science Technology Office and Earth Science Data and Information Systems project have teamed with cloud analytics practitioners to run a benchmark comparison on cloud analytics methods using the same input data and analysis algorithms. We have particularly looked at analysis algorithms that work over long time series, because these are particularly intractable for many Earth Observation datasets which typically store data with one or just a few time steps per file. This post will present side-by-side cost and performance results for several common Earth observation analysis operations.

  17. Pilot testing of SHRP 2 reliability data and analytical products: Southern California.

    Science.gov (United States)

    2015-01-01

    The second Strategic Highway Research Program (SHRP 2) has been investigating the critical subject of travel time reliability for several years. As part of this research, SHRP 2 supported multiple efforts to develop products to evaluate travel time r...

  18. Pilot testing of SHRP 2 reliability data and analytical products: Florida.

    Science.gov (United States)

    2015-01-01

    Transportation agencies have realized the importance of performance estimation, measurement, and management. The Moving Ahead for Progress in the 21st Century Act legislation identifies travel time reliability as one of the goals of the federal highw...

  19. Pilot testing of SHRP 2 reliability data and analytical products: Southern California. [supporting datasets

    Science.gov (United States)

    2014-01-01

    The objective of this project was to develop system designs for programs to monitor travel time reliability and to prepare a guidebook that practitioners and others can use to design, build, operate, and maintain such systems. Generally, such travel ...

  20. An analytical model for computation of reliability of waste management facilities with intermediate storages

    International Nuclear Information System (INIS)

    Kallweit, A.; Schumacher, F.

    1977-01-01

    A high reliability is called for waste management facilities within the fuel cycle of nuclear power stations which can be fulfilled by providing intermediate storage facilities and reserve capacities. In this report a model based on the theory of Markov processes is described which allows computation of reliability characteristics of waste management facilities containing intermediate storage facilities. The application of the model is demonstrated by an example. (orig.) [de

  1. Analytical Methods for Mycotoxin Detection in Southeast Asian Nations (ASEAN).

    Science.gov (United States)

    Lim, Chee Wei; Chung, Gerald; Chan, Sheot Harn

    2017-10-03

    Aflatoxins B 1 (AFB 1 ) and B₂ (AFB₂) and G 1 and G₂ remain the top mycotoxins routinely analyzed and monitored by Association of Southeast Asian Nations (ASEAN) national laboratories primarily for food safety regulation in the major food commodities, nuts and spices. LC tandem fluorescence detection (LC–fluorescence) represents a current mainstream analytical method, with a progressive migration to a primary method by LC tandem MS (MS/MS) for the next half decade. Annual proficiency testing (PT) is conducted by ASEAN Food Reference Laboratories (AFRLs) for mycotoxin testing as part of capability building in national laboratories, with the scope of PT materials spanning from naturally mycotoxin-contaminated spices and nuts in the early 2010s to the recent contamination of corn flour in 2017 for total aflatoxin assay development. The merits of the mainstream LC–fluorescence method are witnessed by a significant improvement ( P < 0.05) in PT z -score passing rates (≤2) from 11.8 to 79.2% for AFB 1 , 23.5 to 83.3% for AFB₂, and 23.5 to 79.2% for total aflatoxins in the last 5 years. This paper discusses the journey of ASEAN national laboratories in analytical testing through AFRLs, and the progressive collective adoption of a multimycotoxin LC-MS/MS method aided by an isotopic dilution assay as a future primary method for safer food commodities.

  2. COMPOSITE METHOD OF RELIABILITY RESEARCH FOR HIERARCHICAL MULTILAYER ROUTING SYSTEMS

    Directory of Open Access Journals (Sweden)

    R. B. Tregubov

    2016-09-01

    Full Text Available The paper deals with the idea of a research method for hierarchical multilayer routing systems. The method represents a composition of methods of graph theories, reliability, probabilities, etc. These methods are applied to the solution of different private analysis and optimization tasks and are systemically connected and coordinated with each other through uniform set-theoretic representation of the object of research. The hierarchical multilayer routing systems are considered as infrastructure facilities (gas and oil pipelines, automobile and railway networks, systems of power supply and communication with distribution of material resources, energy or information with the use of hierarchically nested functions of routing. For descriptive reasons theoretical constructions are considered on the example of task solution of probability determination for up state of specific infocommunication system. The author showed the possibility of constructive combination of graph representation of structure of the object of research and a logic probable analysis method of its reliability indices through uniform set-theoretic representation of its elements and processes proceeding in them.

  3. Structural Reliability Using Probability Density Estimation Methods Within NESSUS

    Science.gov (United States)

    Chamis, Chrisos C. (Technical Monitor); Godines, Cody Ric

    2003-01-01

    A reliability analysis studies a mathematical model of a physical system taking into account uncertainties of design variables and common results are estimations of a response density, which also implies estimations of its parameters. Some common density parameters include the mean value, the standard deviation, and specific percentile(s) of the response, which are measures of central tendency, variation, and probability regions, respectively. Reliability analyses are important since the results can lead to different designs by calculating the probability of observing safe responses in each of the proposed designs. All of this is done at the expense of added computational time as compared to a single deterministic analysis which will result in one value of the response out of many that make up the density of the response. Sampling methods, such as monte carlo (MC) and latin hypercube sampling (LHS), can be used to perform reliability analyses and can compute nonlinear response density parameters even if the response is dependent on many random variables. Hence, both methods are very robust; however, they are computationally expensive to use in the estimation of the response density parameters. Both methods are 2 of 13 stochastic methods that are contained within the Numerical Evaluation of Stochastic Structures Under Stress (NESSUS) program. NESSUS is a probabilistic finite element analysis (FEA) program that was developed through funding from NASA Glenn Research Center (GRC). It has the additional capability of being linked to other analysis programs; therefore, probabilistic fluid dynamics, fracture mechanics, and heat transfer are only a few of what is possible with this software. The LHS method is the newest addition to the stochastic methods within NESSUS. Part of this work was to enhance NESSUS with the LHS method. The new LHS module is complete, has been successfully integrated with NESSUS, and been used to study four different test cases that have been

  4. Applicability of simplified human reliability analysis methods for severe accidents

    Energy Technology Data Exchange (ETDEWEB)

    Boring, R.; St Germain, S. [Idaho National Lab., Idaho Falls, Idaho (United States); Banaseanu, G.; Chatri, H.; Akl, Y. [Canadian Nuclear Safety Commission, Ottawa, Ontario (Canada)

    2016-03-15

    Most contemporary human reliability analysis (HRA) methods were created to analyse design-basis accidents at nuclear power plants. As part of a comprehensive expansion of risk assessments at many plants internationally, HRAs will begin considering severe accident scenarios. Severe accidents, while extremely rare, constitute high consequence events that significantly challenge successful operations and recovery. Challenges during severe accidents include degraded and hazardous operating conditions at the plant, the shift in control from the main control room to the technical support center, the unavailability of plant instrumentation, and the need to use different types of operating procedures. Such shifts in operations may also test key assumptions in existing HRA methods. This paper discusses key differences between design basis and severe accidents, reviews efforts to date to create customized HRA methods suitable for severe accidents, and recommends practices for adapting existing HRA methods that are already being used for HRAs at the plants. (author)

  5. A nonlinear analytic function expansion nodal method for transient calculations

    Energy Technology Data Exchange (ETDEWEB)

    Joo, Han Gyn; Park, Sang Yoon; Cho, Byung Oh; Zee, Sung Quun [Korea Atomic Energy Research Institute, Taejon (Korea, Republic of)

    1998-12-31

    The nonlinear analytic function expansion nodal (AFEN) method is applied to the solution of the time-dependent neutron diffusion equation. Since the AFEN method requires both the particular solution and the homogeneous solution to the transient fixed source problem, the derivation of the solution method is focused on finding the particular solution efficiently. To avoid complicated particular solutions, the source distribution is approximated by quadratic polynomials and the transient source is constructed such that the error due to the quadratic approximation is minimized, In addition, this paper presents a new two-node solution scheme that is derived by imposing the constraint of current continuity at the interface corner points. The method is verified through a series of application to the NEACRP PWR rod ejection benchmark problems. 6 refs., 2 figs., 1 tab. (Author)

  6. Analytical methods for toxic gases from thermal degradation of polymers

    Science.gov (United States)

    Hsu, M.-T. S.

    1977-01-01

    Toxic gases evolved from the thermal oxidative degradation of synthetic or natural polymers in small laboratory chambers or in large scale fire tests are measured by several different analytical methods. Gas detector tubes are used for fast on-site detection of suspect toxic gases. The infrared spectroscopic method is an excellent qualitative and quantitative analysis for some toxic gases. Permanent gases such as carbon monoxide, carbon dioxide, methane and ethylene, can be quantitatively determined by gas chromatography. Highly toxic and corrosive gases such as nitrogen oxides, hydrogen cyanide, hydrogen fluoride, hydrogen chloride and sulfur dioxide should be passed into a scrubbing solution for subsequent analysis by either specific ion electrodes or spectrophotometric methods. Low-concentration toxic organic vapors can be concentrated in a cold trap and then analyzed by gas chromatography and mass spectrometry. The limitations of different methods are discussed.

  7. A nonlinear analytic function expansion nodal method for transient calculations

    Energy Technology Data Exchange (ETDEWEB)

    Joo, Han Gyn; Park, Sang Yoon; Cho, Byung Oh; Zee, Sung Quun [Korea Atomic Energy Research Institute, Taejon (Korea, Republic of)

    1999-12-31

    The nonlinear analytic function expansion nodal (AFEN) method is applied to the solution of the time-dependent neutron diffusion equation. Since the AFEN method requires both the particular solution and the homogeneous solution to the transient fixed source problem, the derivation of the solution method is focused on finding the particular solution efficiently. To avoid complicated particular solutions, the source distribution is approximated by quadratic polynomials and the transient source is constructed such that the error due to the quadratic approximation is minimized, In addition, this paper presents a new two-node solution scheme that is derived by imposing the constraint of current continuity at the interface corner points. The method is verified through a series of application to the NEACRP PWR rod ejection benchmark problems. 6 refs., 2 figs., 1 tab. (Author)

  8. Reducing waste generation and radiation exposure by analytical method modification

    International Nuclear Information System (INIS)

    Ekechukwu, A.A.

    1996-01-01

    The primary goal of an analytical support laboratory has traditionally been to provide accurate data in a timely and cost effective fashion. Added to this goal is now the need to provide the same high quality data while generating as little waste as possible. At the Savannah River Technology Center (SRTC), we have modified and reengineered several methods to decrease generated waste and hence reduce radiation exposure. These method changes involved improving detection limits (which decreased the amount of sample required for analysis), decreasing reaction and analysis time, decreasing the size of experimental set-ups, recycling spent solvent and reagents, and replacing some methods. These changes had the additional benefits of reducing employee radiation exposure and exposure to hazardous chemicals. In all cases, the precision, accuracy, and detection limits were equal to or better than the replaced method. Most of the changes required little or no expenditure of funds. This paper describes these changes and discusses some of their applications

  9. A simple reliability block diagram method for safety integrity verification

    International Nuclear Information System (INIS)

    Guo Haitao; Yang Xianhui

    2007-01-01

    IEC 61508 requires safety integrity verification for safety related systems to be a necessary procedure in safety life cycle. PFD avg must be calculated to verify the safety integrity level (SIL). Since IEC 61508-6 does not give detailed explanations of the definitions and PFD avg calculations for its examples, it is difficult for common reliability or safety engineers to understand when they use the standard as guidance in practice. A method using reliability block diagram is investigated in this study in order to provide a clear and feasible way of PFD avg calculation and help those who take IEC 61508-6 as their guidance. The method finds mean down times (MDTs) of both channel and voted group first and then PFD avg . The calculated results of various voted groups are compared with those in IEC61508 part 6 and Ref. [Zhang T, Long W, Sato Y. Availability of systems with self-diagnostic components-applying Markov model to IEC 61508-6. Reliab Eng System Saf 2003;80(2):133-41]. An interesting outcome can be realized from the comparison. Furthermore, although differences in MDT of voted groups exist between IEC 61508-6 and this paper, PFD avg of voted groups are comparatively close. With detailed description, the method of RBD presented can be applied to the quantitative SIL verification, showing a similarity of the method in IEC 61508-6

  10. Analytical method for thermal stress analysis of plasma facing materials

    Science.gov (United States)

    You, J. H.; Bolt, H.

    2001-10-01

    The thermo-mechanical response of plasma facing materials (PFMs) to heat loads from the fusion plasma is one of the crucial issues in fusion technology. In this work, a fully analytical description of the thermal stress distribution in armour tiles of plasma facing components is presented which is expected to occur under typical high heat flux (HHF) loads. The method of stress superposition is applied considering the temperature gradient and thermal expansion mismatch. Several combinations of PFMs and heat sink metals are analysed and compared. In the framework of the present theoretical model, plastic flow and the effect of residual stress can be quantitatively assessed. Possible failure features are discussed.

  11. Analytical method for thermal stress analysis of plasma facing materials

    International Nuclear Information System (INIS)

    You, J.H.; Bolt, H.

    2001-01-01

    The thermo-mechanical response of plasma facing materials (PFMs) to heat loads from the fusion plasma is one of the crucial issues in fusion technology. In this work, a fully analytical description of the thermal stress distribution in armour tiles of plasma facing components is presented which is expected to occur under typical high heat flux (HHF) loads. The method of stress superposition is applied considering the temperature gradient and thermal expansion mismatch. Several combinations of PFMs and heat sink metals are analysed and compared. In the framework of the present theoretical model, plastic flow and the effect of residual stress can be quantitatively assessed. Possible failure features are discussed

  12. Higher geometry an introduction to advanced methods in analytic geometry

    CERN Document Server

    Woods, Frederick S

    2005-01-01

    For students of mathematics with a sound background in analytic geometry and some knowledge of determinants, this volume has long been among the best available expositions of advanced work on projective and algebraic geometry. Developed from Professor Woods' lectures at the Massachusetts Institute of Technology, it bridges the gap between intermediate studies in the field and highly specialized works.With exceptional thoroughness, it presents the most important general concepts and methods of advanced algebraic geometry (as distinguished from differential geometry). It offers a thorough study

  13. Method of sections in analytical calculations of pneumatic tires

    Science.gov (United States)

    Tarasov, V. N.; Boyarkina, I. V.

    2018-01-01

    Analytical calculations in the pneumatic tire theory are more preferable in comparison with experimental methods. The method of section of a pneumatic tire shell allows to obtain equations of intensities of internal forces in carcass elements and bead rings. Analytical dependencies of intensity of distributed forces have been obtained in tire equator points, on side walls (poles) and pneumatic tire bead rings. Along with planes in the capacity of secant surfaces cylindrical surfaces are used for the first time together with secant planes. The tire capacity equation has been obtained using the method of section, by means of which a contact body is cut off from the tire carcass along the contact perimeter by the surface which is normal to the bearing surface. It has been established that the Laplace equation for the solution of tasks of this class of pneumatic tires contains two unknown values that requires the generation of additional equations. The developed computational schemes of pneumatic tire sections and new equations allow to accelerate the pneumatic tire structure improvement process during engineering.

  14. Performance of analytical methods for tomographic gamma scanning

    International Nuclear Information System (INIS)

    Prettyman, T.H.; Mercer, D.J.

    1997-01-01

    The use of gamma-ray computerized tomography for nondestructive assay of radioactive materials has led to the development of specialized analytical methods. Over the past few years, Los Alamos has developed and implemented a computer code, called ARC-TGS, for the analysis of data obtained by tomographic gamma scanning (TGS). ARC-TGS reduces TGS transmission and emission tomographic data, providing the user with images of the sample contents, the activity or mass of selected radionuclides, and an estimate of the uncertainty in the measured quantities. The results provided by ARC-TGS can be corrected for self-attenuation when the isotope of interest emits more than one gamma-ray. In addition, ARC-TGS provides information needed to estimate TGS quantification limits and to estimate the scan time needed to screen for small amounts of radioactivity. In this report, an overview of the analytical methods used by ARC-TGS is presented along with an assessment of the performance of these methods for TGS

  15. Analytical Method to Estimate the Complex Permittivity of Oil Samples

    Directory of Open Access Journals (Sweden)

    Lijuan Su

    2018-03-01

    Full Text Available In this paper, an analytical method to estimate the complex dielectric constant of liquids is presented. The method is based on the measurement of the transmission coefficient in an embedded microstrip line loaded with a complementary split ring resonator (CSRR, which is etched in the ground plane. From this response, the dielectric constant and loss tangent of the liquid under test (LUT can be extracted, provided that the CSRR is surrounded by such LUT, and the liquid level extends beyond the region where the electromagnetic fields generated by the CSRR are present. For that purpose, a liquid container acting as a pool is added to the structure. The main advantage of this method, which is validated from the measurement of the complex dielectric constant of olive and castor oil, is that reference samples for calibration are not required.

  16. Analytical method of spectra calculations in the Bargmann representation

    International Nuclear Information System (INIS)

    Maciejewski, Andrzej J.; Przybylska, Maria; Stachowiak, Tomasz

    2014-01-01

    We formulate a universal method for solving an arbitrary quantum system which, in the Bargmann representation, is described by a system of linear equations with one independent variable, such as one- and multi-photon Rabi models, or N level systems interacting with a single mode of the electromagnetic field and their various generalizations. We explain three types of conditions that determine the spectrum and show their usage for two deformations of the Rabi model. We prove that the spectra of both models are just zeros of transcendental functions, which in one case are given explicitly in terms of confluent Heun functions. - Highlights: • Analytical method of spectrum determination in Bargmann representation is proposed. • Three types of conditions determining spectrum are identified. • Method to two generalizations of the Rabi system is applied

  17. Analytical method for the isotopic characterization of soils

    International Nuclear Information System (INIS)

    Sibello Hernandez, Rita; Cozzella, Maria Letizia; Mariani, Mario

    2014-01-01

    The aim of this work was to develop an analytical method in order to determine the isotopic composition of different elements in soil samples and to determine the existence of contamination. The method used in the digestion of the samples was the EPA 3050B, and some metal concentration were determined including uranium and thorium. For elements with even lower concentrations such as plutonium and radium a treatment after mineralization by EPA, was necessary. The measurement technique used was mass spectrometry with quadrupole and plasma induced associated (ICP-MS). Results of the analysis performed in two laboratories showed a good correspondence. This method allowed to perform the isotopic characterization of studied soils and results showed that the studied soils do not present any local pollution and that the presence of plutonium-239, is due to global failure

  18. Analytical Methods INAA and PIXE Applied to Characterization of Airborne Particulate Matter in Bandung, Indonesia

    Directory of Open Access Journals (Sweden)

    D.D. Lestiani

    2011-08-01

    Full Text Available Urbanization and industrial growth have deteriorated air quality and are major cause to air pollution. Air pollution through fine and ultra-fine particles is a serious threat to human health. The source of air pollution must be known quantitatively by elemental characterization, in order to design the appropriate air quality management. The suitable methods for analysis the airborne particulate matter such as nuclear analytical techniques are hardly needed to solve the air pollution problem. The objectives of this study are to apply the nuclear analytical techniques to airborne particulate samples collected in Bandung, to assess the accuracy and to ensure the reliable of analytical results through the comparison of instrumental neutron activation analysis (INAA and particles induced X-ray emission (PIXE. Particle samples in the PM2.5 and PM2.5-10 ranges have been collected in Bandung twice a week for 24 hours using a Gent stacked filter unit. The result showed that generally there was a systematic difference between INAA and PIXE results, which the values obtained by PIXE were lower than values determined by INAA. INAA is generally more sensitive and reliable than PIXE for Na, Al, Cl, V, Mn, Fe, Br and I, therefore INAA data are preffered, while PIXE usually gives better precision than INAA for Mg, K, Ca, Ti and Zn. Nevertheless, both techniques provide reliable results and complement to each other. INAA is still a prospective method, while PIXE with the special capabilities is a promising tool that could contribute and complement the lack of NAA in determination of lead, sulphur and silicon. The combination of INAA and PIXE can advantageously be used in air pollution studies to extend the number of important elements measured as key elements in source apportionment.

  19. Analytical Methods INAA and PIXE Applied to Characterization of Airborne Particulate Matter in Bandung, Indonesia

    International Nuclear Information System (INIS)

    Lestiani, D.D.; Santoso, M.

    2011-01-01

    Urbanization and industrial growth have deteriorated air quality and are major cause to air pollution. Air pollution through fine and ultra-fine particles is a serious threat to human health. The source of air pollution must be known quantitatively by elemental characterization, in order to design the appropriate air quality management. The suitable methods for analysis the airborne particulate matter such as nuclear analytical techniques are hardly needed to solve the air pollution problem. The objectives of this study are to apply the nuclear analytical techniques to airborne particulate samples collected in Bandung, to assess the accuracy and to ensure the reliable of analytical results through the comparison of instrumental neutron activation analysis (INAA) and particles induced X-ray emission (PIXE). Particle samples in the PM 2.5 and PM 2.5-10 ranges have been collected in Bandung twice a week for 24 hours using a Gent stacked filter unit. The result showed that generally there was a systematic difference between INAA and PIXE results, which the values obtained by PIXE were lower than values determined by INAA. INAA is generally more sensitive and reliable than PIXE for Na, Al, Cl, V, Mn, Fe, Br and I, therefore INAA data are preferred, while PIXE usually gives better precision than INAA for Mg, K, Ca, Ti and Zn. Nevertheless, both techniques provide reliable results and complement to each other. INAA is still a prospective method, while PIXE with the special capabilities is a promising tool that could contribute and complement the lack of NAA in determination of lead, sulphur and silicon. The combination of INAA and PIXE can advantageously be used in air pollution studies to extend the number of important elements measured as key elements in source apportionment. (author)

  20. Towards reliable multi-hop broadcast in VANETs : An analytical approach

    NARCIS (Netherlands)

    Gholibeigi, M.; Baratchi, M.; Berg, J.L. van den; Heijenk, G.

    2017-01-01

    Intelligent Transportation Systems in the domain of vehicular networking, have recently been subject to rapid development. In vehicular ad hoc networks, data broadcast is one of the main communication types and its reliability is crucial for high performance applications. However, due to the lack of

  1. Towards Reliable Multi-Hop Broadcast in VANETs: An Analytical Approach

    NARCIS (Netherlands)

    Gholibeigi, Mozhdeh; Baratchi, Mitra; van den Berg, Hans Leo; Heijenk, Geert

    2016-01-01

    Intelligent Transportation Systems in the domain of vehicular networking, have recently been subject to rapid development. In vehicular ad hoc networks, data broadcast is one of the main communication types and its reliability is crucial for high performance applications. However, due to the lack of

  2. Vertical equilibrium with sub-scale analytical methods for geological CO2 sequestration

    KAUST Repository

    Gasda, S. E.; Nordbotten, J. M.; Celia, M. A.

    2009-01-01

    equilibrium with sub-scale analytical method (VESA) combines the flexibility of a numerical method, allowing for heterogeneous and geologically complex systems, with the efficiency and accuracy of an analytical method, thereby eliminating expensive grid

  3. Improvement of human reliability analysis method for PRA

    International Nuclear Information System (INIS)

    Tanji, Junichi; Fujimoto, Haruo

    2013-09-01

    It is required to refine human reliability analysis (HRA) method by, for example, incorporating consideration for the cognitive process of operator into the evaluation of diagnosis errors and decision-making errors, as a part of the development and improvement of methods used in probabilistic risk assessments (PRAs). JNES has been developed a HRA method based on ATHENA which is suitable to handle the structured relationship among diagnosis errors, decision-making errors and operator cognition process. This report summarizes outcomes obtained from the improvement of HRA method, in which enhancement to evaluate how the plant degraded condition affects operator cognitive process and to evaluate human error probabilities (HEPs) which correspond to the contents of operator tasks is made. In addition, this report describes the results of case studies on the representative accident sequences to investigate the applicability of HRA method developed. HEPs of the same accident sequences are also estimated using THERP method, which is most popularly used HRA method, and comparisons of the results obtained using these two methods are made to depict the differences of these methods and issues to be solved. Important conclusions obtained are as follows: (1) Improvement of HRA method using operator cognitive action model. Clarification of factors to be considered in the evaluation of human errors, incorporation of degraded plant safety condition into HRA and investigation of HEPs which are affected by the contents of operator tasks were made to improve the HRA method which can integrate operator cognitive action model into ATHENA method. In addition, the detail of procedures of the improved method was delineated in the form of flowchart. (2) Case studies and comparison with the results evaluated by THERP method. Four operator actions modeled in the PRAs of representative BWR5 and 4-loop PWR plants were selected and evaluated as case studies. These cases were also evaluated using

  4. Heat Conduction Analysis Using Semi Analytical Finite Element Method

    International Nuclear Information System (INIS)

    Wargadipura, A. H. S.

    1997-01-01

    Heat conduction problems are very often found in science and engineering fields. It is of accrual importance to determine quantitative descriptions of this important physical phenomena. This paper discusses the development and application of a numerical formulation and computation that can be used to analyze heat conduction problems. The mathematical equation which governs the physical behaviour of heat conduction is in the form of second order partial differential equations. The numerical resolution used in this paper is performed using the finite element method and Fourier series, which is known as semi-analytical finite element methods. The numerical solution results in simultaneous algebraic equations which is solved using the Gauss elimination methodology. The computer implementation is carried out using FORTRAN language. In the final part of the paper, a heat conduction problem in a rectangular plate domain with isothermal boundary conditions in its edge is solved to show the application of the computer program developed and also a comparison with analytical solution is discussed to assess the accuracy of the numerical solution obtained

  5. Structural hybrid reliability index and its convergent solving method based on random–fuzzy–interval reliability model

    Directory of Open Access Journals (Sweden)

    Hai An

    2016-08-01

    Full Text Available Aiming to resolve the problems of a variety of uncertainty variables that coexist in the engineering structure reliability analysis, a new hybrid reliability index to evaluate structural hybrid reliability, based on the random–fuzzy–interval model, is proposed in this article. The convergent solving method is also presented. First, the truncated probability reliability model, the fuzzy random reliability model, and the non-probabilistic interval reliability model are introduced. Then, the new hybrid reliability index definition is presented based on the random–fuzzy–interval model. Furthermore, the calculation flowchart of the hybrid reliability index is presented and it is solved using the modified limit-step length iterative algorithm, which ensures convergence. And the validity of convergent algorithm for the hybrid reliability model is verified through the calculation examples in literature. In the end, a numerical example is demonstrated to show that the hybrid reliability index is applicable for the wear reliability assessment of mechanisms, where truncated random variables, fuzzy random variables, and interval variables coexist. The demonstration also shows the good convergence of the iterative algorithm proposed in this article.

  6. Current Human Reliability Analysis Methods Applied to Computerized Procedures

    Energy Technology Data Exchange (ETDEWEB)

    Ronald L. Boring

    2012-06-01

    Computerized procedures (CPs) are an emerging technology within nuclear power plant control rooms. While CPs have been implemented internationally in advanced control rooms, to date no US nuclear power plant has implemented CPs in its main control room (Fink et al., 2009). Yet, CPs are a reality of new plant builds and are an area of considerable interest to existing plants, which see advantages in terms of enhanced ease of use and easier records management by omitting the need for updating hardcopy procedures. The overall intent of this paper is to provide a characterization of human reliability analysis (HRA) issues for computerized procedures. It is beyond the scope of this document to propose a new HRA approach or to recommend specific methods or refinements to those methods. Rather, this paper serves as a review of current HRA as it may be used for the analysis and review of computerized procedures.

  7. Analytic moment method calculations of the drift wave spectrum

    International Nuclear Information System (INIS)

    Thayer, D.R.; Molvig, K.

    1985-11-01

    A derivation and approximate solution of renormalized mode coupling equations describing the turbulent drift wave spectrum is presented. Arguments are given which indicate that a weak turbulence formulation of the spectrum equations fails for a system with negative dissipation. The inadequacy of the weak turbulence theory is circumvented by utilizing a renormalized formation. An analytic moment method is developed to approximate the solution of the nonlinear spectrum integral equations. The solution method employs trial functions to reduce the integral equations to algebraic equations in basic parameters describing the spectrum. An approximate solution of the spectrum equations is first obtained for a mode dissipation with known solution, and second for an electron dissipation in the NSA

  8. Introduction to Analytical Methods for Internal Combustion Engine Cam Mechanisms

    CERN Document Server

    Williams, J J

    2013-01-01

    Modern design methods of Automotive Cam Design require the computation of a range of parameters. This book provides a logical sequence of steps for the derivation of the relevant equations from first principles, for the more widely used cam mechanisms. Although originally derived for use in high performance engines, this work is equally applicable to the design of mass produced automotive and other internal combustion engines.   Introduction to Analytical Methods for Internal Combustion Engine Cam Mechanisms provides the equations necessary for the design of cam lift curves with an associated smooth acceleration curve. The equations are derived for the kinematics and kinetics of all the mechanisms considered, together with those for cam curvature and oil entrainment velocity. This permits the cam shape, all loads, and contact stresses to be evaluated, and the relevant tribology to be assessed. The effects of asymmetry on the manufacture of cams for finger follower and offset translating curved followers is ...

  9. An analytical method for computing atomic contact areas in biomolecules.

    Science.gov (United States)

    Mach, Paul; Koehl, Patrice

    2013-01-15

    We propose a new analytical method for detecting and computing contacts between atoms in biomolecules. It is based on the alpha shape theory and proceeds in three steps. First, we compute the weighted Delaunay triangulation of the union of spheres representing the molecule. In the second step, the Delaunay complex is filtered to derive the dual complex. Finally, contacts between spheres are collected. In this approach, two atoms i and j are defined to be in contact if their centers are connected by an edge in the dual complex. The contact areas between atom i and its neighbors are computed based on the caps formed by these neighbors on the surface of i; the total area of all these caps is partitioned according to their spherical Laguerre Voronoi diagram on the surface of i. This method is analytical and its implementation in a new program BallContact is fast and robust. We have used BallContact to study contacts in a database of 1551 high resolution protein structures. We show that with this new definition of atomic contacts, we generate realistic representations of the environments of atoms and residues within a protein. In particular, we establish the importance of nonpolar contact areas that complement the information represented by the accessible surface areas. This new method bears similarity to the tessellation methods used to quantify atomic volumes and contacts, with the advantage that it does not require the presence of explicit solvent molecules if the surface of the protein is to be considered. © 2012 Wiley Periodicals, Inc. Copyright © 2012 Wiley Periodicals, Inc.

  10. GenoSets: visual analytic methods for comparative genomics.

    Directory of Open Access Journals (Sweden)

    Aurora A Cain

    Full Text Available Many important questions in biology are, fundamentally, comparative, and this extends to our analysis of a growing number of sequenced genomes. Existing genomic analysis tools are often organized around literal views of genomes as linear strings. Even when information is highly condensed, these views grow cumbersome as larger numbers of genomes are added. Data aggregation and summarization methods from the field of visual analytics can provide abstracted comparative views, suitable for sifting large multi-genome datasets to identify critical similarities and differences. We introduce a software system for visual analysis of comparative genomics data. The system automates the process of data integration, and provides the analysis platform to identify and explore features of interest within these large datasets. GenoSets borrows techniques from business intelligence and visual analytics to provide a rich interface of interactive visualizations supported by a multi-dimensional data warehouse. In GenoSets, visual analytic approaches are used to enable querying based on orthology, functional assignment, and taxonomic or user-defined groupings of genomes. GenoSets links this information together with coordinated, interactive visualizations for both detailed and high-level categorical analysis of summarized data. GenoSets has been designed to simplify the exploration of multiple genome datasets and to facilitate reasoning about genomic comparisons. Case examples are included showing the use of this system in the analysis of 12 Brucella genomes. GenoSets software and the case study dataset are freely available at http://genosets.uncc.edu. We demonstrate that the integration of genomic data using a coordinated multiple view approach can simplify the exploration of large comparative genomic data sets, and facilitate reasoning about comparisons and features of interest.

  11. Structural reliability calculation method based on the dual neural network and direct integration method.

    Science.gov (United States)

    Li, Haibin; He, Yun; Nie, Xiaobo

    2018-01-01

    Structural reliability analysis under uncertainty is paid wide attention by engineers and scholars due to reflecting the structural characteristics and the bearing actual situation. The direct integration method, started from the definition of reliability theory, is easy to be understood, but there are still mathematics difficulties in the calculation of multiple integrals. Therefore, a dual neural network method is proposed for calculating multiple integrals in this paper. Dual neural network consists of two neural networks. The neural network A is used to learn the integrand function, and the neural network B is used to simulate the original function. According to the derivative relationships between the network output and the network input, the neural network B is derived from the neural network A. On this basis, the performance function of normalization is employed in the proposed method to overcome the difficulty of multiple integrations and to improve the accuracy for reliability calculations. The comparisons between the proposed method and Monte Carlo simulation method, Hasofer-Lind method, the mean value first-order second moment method have demonstrated that the proposed method is an efficient and accurate reliability method for structural reliability problems.

  12. Collection of methods for reliability and safety engineering

    International Nuclear Information System (INIS)

    Fussell, J.B.; Rasmuson, D.M.; Wilson, J.R.; Burdick, G.R.; Zipperer, J.C.

    1976-04-01

    The document presented contains five reports each describing a method of reliability and safety engineering. Report I provides a conceptual framework for the study of component malfunctions during system evaluations. Report II provides methods for locating groups of critical component failures such that all the component failures in a given group can be caused to occur by the occurrence of a single separate event. These groups of component failures are called common cause candidates. Report III provides a method for acquiring and storing system-independent component failure logic information. The information stored is influenced by the concepts presented in Report I and also includes information useful in locating common cause candidates. Report IV puts forth methods for analyzing situations that involve systems which change character in a predetermined time sequence. These phased missions techniques are applicable to the hypothetical ''accident chains'' frequently analyzed for nuclear power plants. Report V presents a unified approach to cause-consequence analysis, a method of analysis useful during risk assessments. This approach, as developed by the Danish Atomic Energy Commission, is modified to reflect the format and symbology conventionally used for other types of analysis of nuclear reactor systems

  13. USING ANALYTIC HIERARCHY PROCESS (AHP METHOD IN RURAL DEVELOPMENT

    Directory of Open Access Journals (Sweden)

    Tülay Cengiz

    2003-04-01

    Full Text Available Rural development is a body of economical and social policies towards improving living conditions in rural areas through enabling rural population to utilize economical, social, cultural and technological blessing of city life in place, without migrating. As it is understood from this description, rural development is a very broad concept. Therefore, in development efforts problem should be stated clearly, analyzed and many criterias should be evaluated by experts. Analytic Hierarchy Process (AHP method can be utilized at there stages of development efforts. AHP methods is one of multi-criteria decision method. After degrading a problem in smaller pieces, relative importance and level of importance of two compared elements are determined. It allows evaluation of quality and quantity factors. At the same time, it permits utilization of ideas of many experts and use them in decision process. Because mentioned features of AHP method, it could be used in rural development works. In this article, cultural factors, one of the important components of rural development is often ignored in many studies, were evaluated as an example. As a result of these applications and evaluations, it is concluded that AHP method could be helpful in rural development efforts.

  14. Analytical techniques and method validation for the measurement of selected semivolatile and nonvolatile organofluorochemicals in air.

    Science.gov (United States)

    Reagen, William K; Lindstrom, Kent R; Thompson, Kathy L; Flaherty, John M

    2004-09-01

    The widespread use of semi- and nonvolatile organofluorochemicals in industrial facilities, concern about their persistence, and relatively recent advancements in liquid chromatography/mass spectrometry (LC/MS) technology have led to the development of new analytical methods to assess potential worker exposure to airborne organofluorochemicals. Techniques were evaluated for the determination of 19 organofluorochemicals and for total fluorine in ambient air samples. Due to the potential biphasic nature of most of these fluorochemicals when airborne, Occupational Safety and Health Administration (OSHA) versatile sampler (OVS) tubes were used to simultaneously trap fluorochemical particulates and vapors from workplace air. Analytical methods were developed for OVS air samples to quantitatively analyze for total fluorine using oxygen bomb combustion/ion selective electrode and for 17 organofluorochemicals using LC/MS and gas chromatography/mass spectrometry (GC/MS). The experimental design for this validation was based on the National Institute of Occupational Safety and Health (NIOSH) Guidelines for Air Sampling and Analytical Method Development and Evaluation, with some revisions of the experimental design. The study design incorporated experiments to determine analytical recovery and stability, sampler capacity, the effect of some environmental parameters on recoveries, storage stability, limits of detection, precision, and accuracy. Fluorochemical mixtures were spiked onto each OVS tube over a range of 0.06-6 microg for each of 12 compounds analyzed by LC/MS and 0.3-30 microg for 5 compounds analyzed by GC/MS. These ranges allowed reliable quantitation at 0.001-0.1 mg/m3 in general for LC/MS analytes and 0.005-0.5 mg/m3 for GC/MS analytes when 60 L of air are sampled. The organofluorochemical exposure guideline (EG) is currently 0.1 mg/m3 for many analytes, with one exception being ammonium perfluorooctanoate (EG is 0.01 mg/m3). Total fluorine results may be used

  15. A Reliability-Oriented Design Method for Power Electronic Converters

    DEFF Research Database (Denmark)

    Wang, Huai; Zhou, Dao; Blaabjerg, Frede

    2013-01-01

    Reliability is a crucial performance indicator of power electronic systems in terms of availability, mission accomplishment and life cycle cost. A paradigm shift in the research on reliability of power electronics is going on from simple handbook based calculations (e.g. models in MIL-HDBK-217F h...... and reliability prediction models are provided. A case study on a 2.3 MW wind power converter is discussed with emphasis on the reliability critical component IGBT modules....

  16. [The analytical reliability of clinical laboratory information and role of the standards in its support].

    Science.gov (United States)

    Men'shikov, V V

    2012-12-01

    The article deals with the factors impacting the reliability of clinical laboratory information. The differences of qualities of laboratory analysis tools produced by various manufacturers are discussed. These characteristics are the causes of discrepancy of the results of laboratory analyses of the same analite. The role of the reference system in supporting the comparability of laboratory analysis results is demonstrated. The project of national standard is presented to regulate the requirements to standards and calibrators for analysis of qualitative and non-metrical characteristics of components of biomaterials.

  17. Monte Carlo methods for the reliability analysis of Markov systems

    International Nuclear Information System (INIS)

    Buslik, A.J.

    1985-01-01

    This paper presents Monte Carlo methods for the reliability analysis of Markov systems. Markov models are useful in treating dependencies between components. The present paper shows how the adjoint Monte Carlo method for the continuous time Markov process can be derived from the method for the discrete-time Markov process by a limiting process. The straightforward extensions to the treatment of mean unavailability (over a time interval) are given. System unavailabilities can also be estimated; this is done by making the system failed states absorbing, and not permitting repair from them. A forward Monte Carlo method is presented in which the weighting functions are related to the adjoint function. In particular, if the exact adjoint function is known then weighting factors can be constructed such that the exact answer can be obtained with a single Monte Carlo trial. Of course, if the exact adjoint function is known, there is no need to perform the Monte Carlo calculation. However, the formulation is useful since it gives insight into choices of the weight factors which will reduce the variance of the estimator

  18. Gearbox Reliability Collaborative Analytic Formulation for the Evaluation of Spline Couplings

    Energy Technology Data Exchange (ETDEWEB)

    Guo, Yi [National Renewable Energy Lab. (NREL), Golden, CO (United States); Keller, Jonathan [National Renewable Energy Lab. (NREL), Golden, CO (United States); Errichello, Robert [GEARTECH, Houston, TX (United States); Halse, Chris [Romax Technology, Nottingham (United Kingdom)

    2013-12-01

    Gearboxes in wind turbines have not been achieving their expected design life; however, they commonly meet and exceed the design criteria specified in current standards in the gear, bearing, and wind turbine industry as well as third-party certification criteria. The cost of gearbox replacements and rebuilds, as well as the down time associated with these failures, has elevated the cost of wind energy. The National Renewable Energy Laboratory (NREL) Gearbox Reliability Collaborative (GRC) was established by the U.S. Department of Energy in 2006; its key goal is to understand the root causes of premature gearbox failures and improve their reliability using a combined approach of dynamometer testing, field testing, and modeling. As part of the GRC program, this paper investigates the design of the spline coupling often used in modern wind turbine gearboxes to connect the planetary and helical gear stages. Aside from transmitting the driving torque, another common function of the spline coupling is to allow the sun to float between the planets. The amount the sun can float is determined by the spline design and the sun shaft flexibility subject to the operational loads. Current standards address spline coupling design requirements in varying detail. This report provides additional insight beyond these current standards to quickly evaluate spline coupling designs.

  19. An Analytical Method of Auxiliary Sources Solution for Plane Wave Scattering by Impedance Cylinders

    DEFF Research Database (Denmark)

    Larsen, Niels Vesterdal; Breinbjerg, Olav

    2004-01-01

    Analytical Method of Auxiliary Sources solutions for plane wave scattering by circular impedance cylinders are derived by transformation of the exact eigenfunction series solutions employing the Hankel function wave transformation. The analytical Method of Auxiliary Sources solution thus obtained...

  20. Analytical methods and problems for the diamides type of extractants

    International Nuclear Information System (INIS)

    Cuillerdier, C.; Nigond, L.; Musikas, C.; Vitart, H.; Hoel, P.

    1989-01-01

    Diamides of carboxylic acids and especially malonamides are able to extract alpha emitters (including trivalent ions such as Am and Cm) contained in the wastes solutions of the nuclear industry. As they are completely incinerable and easy to purify, they could be an alternative to the mixture CMPO-TBP which is used in the TRUEX process. A large oxyalkyl radical enhances the distribution coefficients of americium in nitric acid sufficiently to permit the decontamination of wastes solutions in a classical mixers-settlers battery. Now researches are pursued with the aim of optimizing the formula of extractant, the influence of the structure of the extractant on its basicity and stability under radiolysis and hydrolysis is investigated. Analytical methods (potentiometry and NMR of C 13 ) have been developed for solvent titration and to evaluate the percentage of degradation and to identify some of the degradation products

  1. Analytical methods used in plutonium purification cycles by trilaurylamine

    International Nuclear Information System (INIS)

    Perez, J.J.

    1965-01-01

    The utilisation of trilaurylamine as a solvent extractant for the purification of plutonium has entailed to perfect a set of analytical methods which involves, various techniques. The organic impurities of the solvent can be titrated by gas-liquid chromatography. The titration of the main degradation product, the di-laurylamine, can be accomplished also by spectro-colorimetry. Potentiometry is used for the analysis of the different salts of amine-nitrate-sulfate-bisulfate as also the extracted nitric acid. The determination of the nitrate in aqueous phase is carried out by constant current potentiometry. The range of application, the accuracy and the procedure of these analysis are related in the present report. (author) [fr

  2. Nuclear analytical methods for trace element studies in calcified tissues

    International Nuclear Information System (INIS)

    Chaudhry, M.A.; Chaudhry, M.N.

    2001-01-01

    Full text: Various nuclear analytical methods have been developed and applied to determine the elemental composition of calcified tissues (teeth and bones). Fluorine was determined by prompt gamma activation analysis through the 19 F(p,ag) 16 O reaction. Carbon was measured by activation analysis with He-3 ions, and the technique of Proton-Induced X-ray Emission (PIXE) was applied to simultaneously determine Ca, P, and trace elements in well-documented teeth. Dental hard tissues, enamel, dentine, cement, and their junctions, as well as different parts of the same tissue, were examined separately. Furthermore, using a Proton Microprobe, we measured the surface distribution of F and other elements on and around carious lesions on the enamel. The depth profiles of F, and other elements, were also measured right up to the amelodentin junction

  3. Suitability of analytical methods to measure solubility for the purpose of nanoregulation.

    Science.gov (United States)

    Tantra, Ratna; Bouwmeester, Hans; Bolea, Eduardo; Rey-Castro, Carlos; David, Calin A; Dogné, Jean-Michel; Jarman, John; Laborda, Francisco; Laloy, Julie; Robinson, Kenneth N; Undas, Anna K; van der Zande, Meike

    2016-01-01

    Solubility is an important physicochemical parameter in nanoregulation. If nanomaterial is completely soluble, then from a risk assessment point of view, its disposal can be treated much in the same way as "ordinary" chemicals, which will simplify testing and characterisation regimes. This review assesses potential techniques for the measurement of nanomaterial solubility and evaluates the performance against a set of analytical criteria (based on satisfying the requirements as governed by the cosmetic regulation as well as the need to quantify the concentration of free (hydrated) ions). Our findings show that no universal method exists. A complementary approach is thus recommended, to comprise an atomic spectrometry-based method in conjunction with an electrochemical (or colorimetric) method. This article shows that although some techniques are more commonly used than others, a huge research gap remains, related with the need to ensure data reliability.

  4. Development of reliability centered maintenance methods and tools

    International Nuclear Information System (INIS)

    Jacquot, J.P.; Dubreuil-Chambardel, A.; Lannoy, A.; Monnier, B.

    1992-12-01

    This paper recalls the development of the RCM (Reliability Centered Maintenance) approach in the nuclear industry and describes the trial study implemented by EDF in the context of the OMF (RCM) Project. The approach developed is currently being applied to about thirty systems (Industrial Project). On a parallel, R and D efforts are being maintained to improve the selectivity of the analysis methods. These methods use Probabilistic Safety Study models, thereby guaranteeing better selectivity in the identification of safety critical elements and enhancing consistency between Maintenance and Safety studies. They also offer more detailed analysis of operation feedback, invoking for example Bayes' methods combining expert judgement and feedback data. Finally, they propose a functional and material representation of the plant. This dual representation describes both the functions assured by maintenance provisions and the material elements required for their implementation. In the final chapter, the targets of the future OMF workstation are summarized and the latter's insertion in the EDF information system is briefly described. (authors). 5 figs., 2 tabs., 7 refs

  5. Ecological Vulnerability Assessment Based on Fuzzy Analytical Method and Analytic Hierarchy Process in Yellow River Delta.

    Science.gov (United States)

    Wu, Chunsheng; Liu, Gaohuan; Huang, Chong; Liu, Qingsheng; Guan, Xudong

    2018-04-25

    The Yellow River Delta (YRD), located in Yellow River estuary, is characterized by rich ecological system types, and provides habitats or migration stations for wild birds, all of which makes the delta an ecological barrier or ecotone for inland areas. Nevertheless, the abundant natural resources of YRD have brought huge challenges to the area, and frequent human activities and natural disasters have damaged the ecological systems seriously, and certain ecological functions have been threatened. Therefore, it is necessary to determine the status of the ecological environment based on scientific methods, which can provide scientifically robust data for the managers or stakeholders to adopt timely ecological protection measures. The aim of this study was to obtain the spatial distribution of the ecological vulnerability (EV) in YRD based on 21 indicators selected from underwater status, soil condition, land use, landform, vegetation cover, meteorological conditions, ocean influence, and social economy. In addition, the fuzzy analytic hierarchy process (FAHP) method was used to obtain the weights of the selected indicators, and a fuzzy logic model was constructed to obtain the result. The result showed that the spatial distribution of the EV grades was regular, while the fuzzy membership of EV decreased gradually from the coastline to inland area, especially around the river crossing, where it had the lowest EV. Along the coastline, the dikes had an obviously protective effect for the inner area, while the EV was higher in the area where no dikes were built. This result also showed that the soil condition and groundwater status were highly related to the EV spatially, with the correlation coefficients −0.55 and −0.74 respectively, and human activities had exerted considerable pressure on the ecological environment.

  6. CT hepatic perfusion measurement: Comparison of three analytic methods

    International Nuclear Information System (INIS)

    Kanda, Tomonori; Yoshikawa, Takeshi; Ohno, Yoshiharu; Kanata, Naoki; Koyama, Hisanobu; Takenaka, Daisuke; Sugimura, Kazuro

    2012-01-01

    Objectives: To compare the efficacy of three analytic methods, maximum slope (MS), dual-input single-compartment model (CM) and deconvolution (DC), for CT measurements of hepatic perfusion and assess the effects of extra-hepatic systemic factors. Materials and methods: Eighty-eight patients who were suspected of having metastatic liver tumors underwent hepatic CT perfusion. The scans were performed at the hepatic hilum 7–77 s after administration of contrast material. Hepatic arterial and portal perfusions (HAP and HPP, ml/min/100 ml) and arterial perfusion fraction (APF, %) were calculated with the three methods, followed by correlation assessment. Partial correlation analysis was used to assess the effects on hepatic perfusion values by various factors such as age, sex, risk of cardiovascular diseases, arrival time of contrast material at abdominal aorta, transit time from abdominal aorta to hepatic parenchyma, and liver dysfunction. Results: Mean HAP of MS was significantly higher than DC. HPP of CM was significantly higher than MS and CM, and HPP of MS was significantly higher than DC. There was no significant difference in APF. HAP and APF showed significant and moderate correlations among the methods. HPP showed significant and moderate correlations between CM and DC, and poor correlation between MS and CM or DC. All methods showed weak correlations between HAP or APF and age or sex. Finally, MS showed weak correlations between HAP or HPP and arrival time or cardiovascular risks. Conclusions: Hepatic perfusion values arrived at with the three methods are not interchangeable. CM and DC are less susceptible to extra-hepatic systemic factors

  7. Analytical methods associated with the recovery of uranium

    International Nuclear Information System (INIS)

    Dixon, K.

    1983-01-01

    This report summarizes various approaches made to the analysis of materials arising from the processing of Karoo deposits for uranium. These materials include head and residue samples, aqueous solutions and organic solvents and, finally, the precipitated cakes of the elements recovered, i.e. uranium, molybdenum, and arsenic. Analysis was required for these elements and also vanadium, carbon, sulphur, and carbonate in the head and residue samples. The concentration of uranium, molybdenum, and arsenic, other than in the precipitated cakes, ranges from 1 to 2000μg/g, and that of carbon, sulphur, and carbonate from 0,1 to 5 per cent. The analysis of cakes necessitates the determination of silver, arsenic, iron, copper, calcium, magnesium, manganese, molybdenum, lead, tin, titanium, and vanadium within the range 1 to 1000μg/g, and of sodium and silica within the range 10 to 20 000μg/g. The methods used include combustion methods for carbon, sulphur, and carbonate, and atomic-absorption, X-ray-fluorescence, and emission methods for the other analytes. The accuracy of the analysis is within 10 per cent

  8. Groundwater Seepage Estimation into Amirkabir Tunnel Using Analytical Methods and DEM and SGR Method

    OpenAIRE

    Hadi Farhadian; Homayoon Katibeh

    2015-01-01

    In this paper, groundwater seepage into Amirkabir tunnel has been estimated using analytical and numerical methods for 14 different sections of the tunnel. Site Groundwater Rating (SGR) method also has been performed for qualitative and quantitative classification of the tunnel sections. The obtained results of above mentioned methods were compared together. The study shows reasonable accordance with results of the all methods unless for two sections of tunnel. In these t...

  9. Results of a Demonstration Assessment of Passive System Reliability Utilizing the Reliability Method for Passive Systems (RMPS)

    Energy Technology Data Exchange (ETDEWEB)

    Bucknor, Matthew; Grabaskas, David; Brunett, Acacia; Grelle, Austin

    2015-04-26

    Advanced small modular reactor designs include many advantageous design features such as passively driven safety systems that are arguably more reliable and cost effective relative to conventional active systems. Despite their attractiveness, a reliability assessment of passive systems can be difficult using conventional reliability methods due to the nature of passive systems. Simple deviations in boundary conditions can induce functional failures in a passive system, and intermediate or unexpected operating modes can also occur. As part of an ongoing project, Argonne National Laboratory is investigating various methodologies to address passive system reliability. The Reliability Method for Passive Systems (RMPS), a systematic approach for examining reliability, is one technique chosen for this analysis. This methodology is combined with the Risk-Informed Safety Margin Characterization (RISMC) approach to assess the reliability of a passive system and the impact of its associated uncertainties. For this demonstration problem, an integrated plant model of an advanced small modular pool-type sodium fast reactor with a passive reactor cavity cooling system is subjected to a station blackout using RELAP5-3D. This paper discusses important aspects of the reliability assessment, including deployment of the methodology, the uncertainty identification and quantification process, and identification of key risk metrics.

  10. The psychophysiological assessment method for pilot's professional reliability.

    Science.gov (United States)

    Zhang, L M; Yu, L S; Wang, K N; Jing, B S; Fang, C

    1997-05-01

    Previous research has shown that a pilot's professional reliability depends on two relative factors: the pilot's functional state and the demands of task workload. The Psychophysiological Reserve Capacity (PRC) is defined as a pilot's ability to accomplish additive tasks without reducing the performance of the primary task (flight task). We hypothesized that the PRC was a mirror of the pilot's functional state. The purpose of this study was to probe the psychophysiological method for evaluating a pilot's professional reliability on a simulator. The PRC Comprehensive Evaluating System (PRCCES) which was used in the experiment included four subsystems: a) quantitative evaluation system for pilot's performance on simulator; b) secondary task display and quantitative estimating system; c) multiphysiological data monitoring and statistical system; and d) comprehensive evaluation system for pilot PRC. Two studies were performed. In study one, 63 healthy and 13 hospitalized pilots participated. Each pilot performed a double 180 degrees circuit flight program with and without secondary task (three digit operation). The operator performance, score of secondary task and cost of physiological effort were measured and compared by PRCCES in the two conditions. Then, each pilot's flight skill in training was subjectively scored by instructor pilot ratings. In study two, 7 healthy pilots volunteered to take part in the experiment on the effects of sleep deprivation on pilot's PRC. Each participant had PRC tested pre- and post-8 h sleep deprivation. The results show that the PRC values of a healthy pilot was positively correlated with abilities of flexibility, operating and correcting deviation, attention distribution, and accuracy of instrument flight in the air (r = 0.27-0.40, p < 0.05), and negatively correlated with emotional anxiety in flight (r = -0.40, p < 0.05). The values of PRC in healthy pilots (0.61 +/- 0.17) were significantly higher than that of hospitalized pilots

  11. Analytical resource assessment method for continuous (unconventional) oil and gas accumulations - The "ACCESS" Method

    Science.gov (United States)

    Crovelli, Robert A.; revised by Charpentier, Ronald R.

    2012-01-01

    The U.S. Geological Survey (USGS) periodically assesses petroleum resources of areas within the United States and the world. The purpose of this report is to explain the development of an analytic probabilistic method and spreadsheet software system called Analytic Cell-Based Continuous Energy Spreadsheet System (ACCESS). The ACCESS method is based upon mathematical equations derived from probability theory. The ACCESS spreadsheet can be used to calculate estimates of the undeveloped oil, gas, and NGL (natural gas liquids) resources in a continuous-type assessment unit. An assessment unit is a mappable volume of rock in a total petroleum system. In this report, the geologic assessment model is defined first, the analytic probabilistic method is described second, and the spreadsheet ACCESS is described third. In this revised version of Open-File Report 00-044 , the text has been updated to reflect modifications that were made to the ACCESS program. Two versions of the program are added as appendixes.

  12. The fitness for purpose of analytical methods applied to fluorimetric uranium determination in water matrix

    International Nuclear Information System (INIS)

    Grinman, Ana; Giustina, Daniel; Mondini, Julia; Diodat, Jorge

    2008-01-01

    Full text: This paper describes the steps which should be followed by a laboratory in order to validate the fluorimetric method for natural uranium in water matrix. The validation of an analytical method is a necessary requirement prior accreditation under Standard norm ISO/IEC 17025, of a non normalized method. Different analytical techniques differ in a sort of variables to be validated. Depending on the chemical process, measurement technique, matrix type, data fitting and measurement efficiency, a laboratory must set up experiments to verify reliability of data, through the application of several statistical tests and by participating in Quality Programs (QP) organized by reference laboratories such as the National Institute of Standards and Technology (NIST), National Physics Laboratory (NPL), or Environmental Measurements Laboratory (EML). However, the participation in QP not only involves international reference laboratories, but also, the national ones which are able to prove proficiency to the Argentinean Accreditation Board. The parameters that the ARN laboratory had to validate in the fluorimetric method to fit in accordance with Eurachem guide and IUPAC definitions, are: Detection Limit, Quantification Limit, Precision, Intra laboratory Precision, Reproducibility Limit, Repeatability Limit, Linear Range and Robustness. Assays to fit the above parameters were designed on the bases of statistics requirements, and a detailed data treatment is presented together with the respective tests in order to show the parameters validated. As a final conclusion, the uranium determination by fluorimetry is a reliable method for direct measurement to meet radioprotection requirements in water matrix, within its linear range which is fixed every time a calibration is carried out at the beginning of the analysis. The detection limit ( depending on blank standard deviation and slope) varies between 3 ug U and 5 ug U which yields minimum detectable concentrations (MDC) of

  13. Analytic tools for investigating the structure of network reliability measures with regard to observation correlations

    Science.gov (United States)

    Prószyński, W.; Kwaśniak, M.

    2018-03-01

    A global measure of observation correlations in a network is proposed, together with the auxiliary indices related to non-diagonal elements of the correlation matrix. Based on the above global measure, a specific representation of the correlation matrix is presented, being the result of rigorously proven theorem formulated within the present research. According to the theorem, each positive definite correlation matrix can be expressed by a scale factor and a so-called internal weight matrix. Such a representation made it possible to investigate the structure of the basic reliability measures with regard to observation correlations. Numerical examples carried out for two test networks illustrate the structure of those measures that proved to be dependent on global correlation index. Also, the levels of global correlation are proposed. It is shown that one can readily find an approximate value of the global correlation index, and hence the correlation level, for the expected values of auxiliary indices being the only knowledge about a correlation matrix of interest. The paper is an extended continuation of the previous study of authors that was confined to the elementary case termed uniform correlation. The extension covers arbitrary correlation matrices and a structure of correlation effect.

  14. Modern analytic methods applied to the art and archaeology

    International Nuclear Information System (INIS)

    Tenorio C, M. D.; Longoria G, L. C.

    2010-01-01

    The interaction of diverse areas as the analytic chemistry, the history of the art and the archaeology has allowed the development of a variety of techniques used in archaeology, in conservation and restoration. These methods have been used to date objects, to determine the origin of the old materials and to reconstruct their use and to identify the degradation processes that affect the integrity of the art works. The objective of this chapter is to offer a general vision on the researches that have been realized in the Instituto Nacional de Investigaciones Nucleares (ININ) in the field of cultural goods. A series of researches carried out in collaboration with national investigators and of the foreigner is described shortly, as well as with the great support of degree students and master in archaeology of the National School of Anthropology and History, since one of the goals that have is to diffuse the knowledge of the existence of these techniques among the young archaeologists, so that they have a wider vision of what they could use in an in mediate future and they can check hypothesis with scientific methods. (Author)

  15. Analytic-numerical method of determining the freezing front location

    Directory of Open Access Journals (Sweden)

    R. Grzymkowski

    2011-07-01

    Full Text Available Mathematical modeling of thermal processes combined with the reversible phase transitions of type: solid phase – liquid phase leads to formulation of the parabolic boundary problems with the moving boundary. Solution of such defined problem requires, most often, to use sophisticated numerical techniques and far advanced mathematical tools. Excellent illustration of the complexity of considered problems, as well as of the variety of approaches used for finding their solutions, gives the papers [1-4]. In the current paper, the authors present the, especially attractive from the engineer point of view, analytic-numerical method for finding the approximate solution of selected class of problems which can be reduced to the one-phase solidification problem of a plate with the unknown a priori, varying in time boundary of the region in which the solution is sought. Proposed method is based on the known formalism of initial expansion of the sought function describing the temperature field into the power series, some coefficients of which are determined with the aid of boundary conditions, and on the approximation of the function defining the location of freezing front with the broken line, parameters of which are numerically determined.

  16. Analytical method for determining the channel-temperature distribution

    International Nuclear Information System (INIS)

    Kurbatov, I.M.

    1992-01-01

    The distribution of the predicted temperature over the volume or cross section of the active zone is important for thermal calculations of reactors taking into account random deviations. This requires a laborious calculation which includes the following steps: separation of the nominal temperature field, within the temperature range, into intervals, in each of which the temperature is set equal to its average value in the interval; determination of the number of channels whose temperature falls within each interval; construction of the channel-temperature distribution in each interval in accordance with the weighted error function; and summation of the number of channels with the same temperature over all intervals. This procedure can be greatly simplified with the help of methods which eliminate numerous variant calculations when the nominal temperature field is open-quotes refinedclose quotes up to the optimal field according to different criteria. In the present paper a universal analytical method is proposed for determining, by changing the coefficients in the channel-temperature distribution function, the form of this function that reflects all conditions of operation of the elements in the active zone. The problem is solved for the temperature of the coolant at the outlet from the reactor channels

  17. Measurement of company effectiveness using analytic network process method

    Directory of Open Access Journals (Sweden)

    Goran Janjić

    2017-07-01

    Full Text Available The sustainable development of an organisation is monitored through the organisation’s performance, which beforehand incorporates all stakeholders’ requirements in its strategy. The strategic management concept enables organisations to monitor and evaluate their effectiveness along with efficiency by monitoring of the implementation of set strategic goals. In the process of monitoring and measuring effectiveness, an organisation can use multiple-criteria decision-making methods as help. This study uses the method of analytic network process (ANP to define the weight factors of the mutual influences of all the important elements of an organisation’s strategy. The calculation of an organisation’s effectiveness is based on the weight factors and the degree of fulfilment of the goal values of the strategic map measures. New business conditions influence the changes in the importance of certain elements of an organisation’s business in relation to competitive advantage on the market, and on the market, increasing emphasis is given to non-material resources in the process of selection of the organisation’s most important measures.

  18. Measurement of company effectiveness using analytic network process method

    Science.gov (United States)

    Goran, Janjić; Zorana, Tanasić; Borut, Kosec

    2017-07-01

    The sustainable development of an organisation is monitored through the organisation's performance, which beforehand incorporates all stakeholders' requirements in its strategy. The strategic management concept enables organisations to monitor and evaluate their effectiveness along with efficiency by monitoring of the implementation of set strategic goals. In the process of monitoring and measuring effectiveness, an organisation can use multiple-criteria decision-making methods as help. This study uses the method of analytic network process (ANP) to define the weight factors of the mutual influences of all the important elements of an organisation's strategy. The calculation of an organisation's effectiveness is based on the weight factors and the degree of fulfilment of the goal values of the strategic map measures. New business conditions influence the changes in the importance of certain elements of an organisation's business in relation to competitive advantage on the market, and on the market, increasing emphasis is given to non-material resources in the process of selection of the organisation's most important measures.

  19. Analytical methods for study of transmission line lightning protection

    International Nuclear Information System (INIS)

    Pettersson, Per.

    1993-04-01

    Transmission line lightning performance is studied by analytical methods. The elements of shielding failure flashovers and back-flashovers are analysed as functions of incidence, response and insulation. Closed-form approximate expressions are sought to enhance understanding of the phenomena. Probabilistic and wave propagation aspects are particularly studied. The electrogeometric model of lightning attraction to structures is used in combination with the log-normal probability distribution of lightning to ground currents. The log-normality is found to be retained for the currents collected by mast-type as well as line-type structures, but with a change of scale. For both types, exceedingly simple formulas for the number of hits are derived. Simple closed-form expressions for the line outage rates from back- flashovers and shielding failure flashovers are derived in a uniform way as functions of the critical currents. The expressions involve the standardized normal distribution function. System response is analysed by use of Laplace transforms in combination with text-book transmission-line theory. Inversion into time domain is accomplished by an approximate asymptotic method producing closed-form results. The back-flashover problem is analysed in particular. Approximate, image type expressions are derived for shunt admittance of wires above, on and under ground for analyses of fast transients. The derivation parallels that for series impedance, now well-known. 3 refs, 5 figs

  20. Pyrrolizidine alkaloids in honey: comparison of analytical methods.

    Science.gov (United States)

    Kempf, M; Wittig, M; Reinhard, A; von der Ohe, K; Blacquière, T; Raezke, K-P; Michel, R; Schreier, P; Beuerle, T

    2011-03-01

    Pyrrolizidine alkaloids (PAs) are a structurally diverse group of toxicologically relevant secondary plant metabolites. Currently, two analytical methods are used to determine PA content in honey. To achieve reasonably high sensitivity and selectivity, mass spectrometry detection is demanded. One method is an HPLC-ESI-MS-MS approach, the other a sum parameter method utilising HRGC-EI-MS operated in the selected ion monitoring mode (SIM). To date, no fully validated or standardised method exists to measure the PA content in honey. To establish an LC-MS method, several hundred standard pollen analysis results of raw honey were analysed. Possible PA plants were identified and typical commercially available marker PA-N-oxides (PANOs). Three distinct honey sets were analysed with both methods. Set A consisted of pure Echium honey (61-80% Echium pollen). Echium is an attractive bee plant. It is quite common in all temperate zones worldwide and is one of the major reasons for PA contamination in honey. Although only echimidine/echimidine-N-oxide were available as reference for the LC-MS target approach, the results for both analytical techniques matched very well (n = 8; PA content ranging from 311 to 520 µg kg(-1)). The second batch (B) consisted of a set of randomly picked raw honeys, mostly originating from Eupatorium spp. (0-15%), another common PA plant, usually characterised by the occurrence of lycopsamine-type PA. Again, the results showed good consistency in terms of PA-positive samples and quantification results (n = 8; ranging from 0 to 625 µg kg(-1) retronecine equivalents). The last set (C) was obtained by consciously placing beehives in areas with a high abundance of Jacobaea vulgaris (ragwort) from the Veluwe region (the Netherlands). J. vulgaris increasingly invades countrysides in Central Europe, especially areas with reduced farming or sites with natural restorations. Honey from two seasons (2007 and 2008) was sampled. While only trace amounts of

  1. Development of analytical methods for iodine speciation in fresh water

    International Nuclear Information System (INIS)

    Takaku, Yuichi; Ohtsuka, Yoshihito; Hisamatsu, Shun'ichi

    2007-01-01

    Analytical methods for physicochemical speciation of iodine in fresh water samples were developed to elucidate its behavior in the environment. The methods combined inductively coupled plasma mass spectrometry (ICP-MS) with size exclusion high performance liquid chromatography (SEC) or capillary electrophoresis (CE). Freshwater samples were collected from Lake Towada and rivers surrounding the lake. After filtration through a 0.45 μm pore size membrane filter, iodine in the water samples was pre-concentrated with an ultra-filtration filter which had a cut-off size of 10 kDa. The fraction with molecular size over 10 kDa was concentrated to 100 times in the original water, and then introduced into the SEC-ICP-MS. Molecular size chromatograms of all river and lake water samples showed two peaks for iodine concentrations: 40 kDa and 20 kDa. The method for separately determining two valence states of inorganic iodine, I - and IO 3 - , was also developed using the CE-ICP-MS system and it was successfully applied to the fresh water samples. Analysis results of surface water samples in Lake Towada and rivers surrounding the lake indicated that the chemical form of inorganic iodine in all samples was IO 3 - . Additional lake water samples were collected from Lake O-ike-higashi in the Juni-ko area at Shirakami-Sanchi, which is a UNESCO natural world heritage. The lake has a strong thermocline during all seasons; its bottom layer is in a highly reductive state. Depth profiles of I - and IO 3 - clearly showed that I - was not detected in the surface layer, but it was predominant in the bottom layer, and vice versa for IO 3 - . As this separation method is rapid and sensitive, it will be widely used in the future. (author)

  2. Characterization of Catalytic Fast Pyrolysis Oils: The Importance of Solvent Selection for Analytical Method Development

    Energy Technology Data Exchange (ETDEWEB)

    Ferrell, Jack R [National Renewable Energy Laboratory (NREL), Golden, CO (United States); Ware, Anne E [National Renewable Energy Laboratory (NREL), Golden, CO (United States)

    2018-02-25

    Two catalytic fast pyrolysis (CFP) oils (bottom/heavy fraction) were analyzed in various solvents that are used in common analytical methods (nuclear magnetic resonance - NMR, gas chromatography - GC, gel permeation chromatography - GPC, thermogravimetric analysis - TGA) for oil characterization and speciation. A more accurate analysis of the CFP oils can be obtained by identification and exploitation of solvent miscibility characteristics. Acetone and tetrahydrofuran can be used to completely solubilize CFP oils for analysis by GC and tetrahydrofuran can be used for traditional organic GPC analysis of the oils. DMSO-d6 can be used to solubilize CFP oils for analysis by 13C NMR. The fractionation of oils into solvents that did not completely solubilize the whole oils showed that miscibility can be related to the oil properties. This allows for solvent selection based on physico-chemical properties of the oils. However, based on semi-quantitative comparisons of the GC chromatograms, the organic solvent fractionation schemes did not speciate the oils based on specific analyte type. On the other hand, chlorinated solvents did fractionate the oils based on analyte size to a certain degree. Unfortunately, like raw pyrolysis oil, the matrix of the CFP oils is complicated and is not amenable to simple liquid-liquid extraction (LLE) or solvent fractionation to separate the oils based on the chemical and/or physical properties of individual components. For reliable analyses, for each analytical method used, it is critical that the bio-oil sample is both completely soluble and also not likely to react with the chosen solvent. The adoption of the standardized solvent selection protocols presented here will allow for greater reproducibility of analysis across different users and facilities.

  3. Analytical one parameter method for PID motion controller settings

    NARCIS (Netherlands)

    van Dijk, Johannes; Aarts, Ronald G.K.M.

    2012-01-01

    In this paper analytical expressions for PID-controllers settings for electromechanical motion systems are presented. It will be shown that by an adequate frequency domain oriented parametrization, the parameters of a PID-controller are analytically dependent on one variable only, the cross-over

  4. Propulsion and launching analysis of variable-mass rockets by analytical methods

    OpenAIRE

    D.D. Ganji; M. Gorji; M. Hatami; A. Hasanpour; N. Khademzadeh

    2013-01-01

    In this study, applications of some analytical methods on nonlinear equation of the launching of a rocket with variable mass are investigated. Differential transformation method (DTM), homotopy perturbation method (HPM) and least square method (LSM) were applied and their results are compared with numerical solution. An excellent agreement with analytical methods and numerical ones is observed in the results and this reveals that analytical methods are effective and convenient. Also a paramet...

  5. The analytic regularization ζ function method and the cut-off method in Casimir effect

    International Nuclear Information System (INIS)

    Svaiter, N.F.; Svaiter, B.F.

    1990-01-01

    The zero point energy associated to a hermitian massless scalar field in the presence of perfectly reflecting plates in a three dimensional flat space-time is discussed. A new technique to unify two different methods - the ζ function and a variant of the cut-off method - used to obtain the so called Casimir energy is presented, and the proof of the analytic equivalence between both methods is given. (author)

  6. Oxcarbazepine: validation and application of an analytical method

    Directory of Open Access Journals (Sweden)

    Paula Cristina Rezende Enéas

    2010-06-01

    Full Text Available Oxcarbazepine (OXC is an important anticonvulsant and mood stabilizing drug. A pharmacopoeial monograph for OXC is not yet available and therefore the development and validation of a new analytical method for quantification of this drug is essential. In the present study, a UV spectrophotometric method for the determination of OXC was developed. The various parameters, such as linearity, precision, accuracy and specificity, were studied according to International Conference on Harmonization Guidelines. Batches of 150 mg OXC capsules were prepared and analyzed using the validated UV method. The formulations were also evaluated for parameters including drug-excipient compatibility, flowability, uniformity of weight, disintegration time, assay, uniformity of content and the amount of drug dissolved during the first hour.Oxcarbazepina (OXC é um fármaco anticonvulsivante e estabilizante do humor. O desenvolvimento e validação de método analítico para quantificação da OXC são de fundamental importância devido à ausência de monografias farmacopéicas oficiais para esse fármaco. Nesse trabalho, um método espectrofotométrico UV para determinação da OXC foi desenvolvido. O método proposto foi validado seguindo os parâmetros de linearidade, precisão, exatidão e especificidade de acordo com as normas da Conferência Internacional de Harmonização. Cápsulas de OXC 150 mg foram preparadas e analisadas utilizando-se o método analítico validado. As formulações foram avaliadas com relação à compatibilidade fármaco-excipientes, fluidez, determinação de peso, tempo de desintegração, doseamento, uniformidade de conteúdo e quantidade do fármaco dissolvido após 60 minutos.

  7. Development on methods for evaluating structure reliability of piping components

    International Nuclear Information System (INIS)

    Schimpfke, T.; Grebner, H.; Peschke, J.; Sievers, J.

    2003-01-01

    In the frame of the German reactor safety research program of the Federal Ministry of Economics and Labour, GRS has started to develop an analysis code named PROST (PRObabilistic STructure analysis) for estimating the leak and break probabilities of piping systems in nuclear power plants. The development is based on the experience achieved with applications of the public available US code PRAISE 3.10 (Piping Reliability Analysis Including Seismic Events), which was supplemented by additional features regarding the statistical evaluation and the crack orientation. PROST is designed to be more flexible to changes and supplementations. Up to now it can be used for calculating fatigue problems. The paper mentions the main capabilities and theoretical background of the present PROST development and presents a parametric study on the influence by changing the method of stress intensity factor and limit load calculation and the statistical evaluation options on the leak probability of an exemplary pipe with postulated axial crack distribution. Furthermore the resulting leak probability of an exemplary pipe with postulated circumferential crack distribution is compared with the results of the modified PRAISE computer program. The intention of this investigation is to show trends. Therefore the resulting absolute values for probabilities should not be considered as realistic evaluations. (author)

  8. Methods for qualification of highly reliable software - international procedure

    International Nuclear Information System (INIS)

    Kersken, M.

    1997-01-01

    Despite the advantages of computer-assisted safety technology, there still is some uneasyness to be observed with respect to the novel processes, resulting from absence of a body of generally accepted and uncontentious qualification guides (regulatory provisions, standards) for safety evaluation of the computer codes applied. Warranty of adequate protection of the population, operators or plant components is an essential aspect in this context, too - as it is in general with reliability and risk assessment of novel technology - so that, due to appropriate legislation still missing, there currently is a licensing risk involved in the introduction of digital safety systems. Nevertheless, there is some extent of agreement within the international community and utility operators about what standards and measures should be applied for qualification of software of relevance to plant safety. The standard IEC 880/IEC 86/ in particular, in its original version, or national documents based on this standard, are applied in all countries using or planning to install those systems. A novel supplement to this standard, document /IEC 96/, is in the process of finalization and defines the requirements to be met by modern methods of software engineering. (orig./DG) [de

  9. AN ANALYTICAL FRAMEWORK FOR ASSESSING RELIABLE NUCLEAR FUEL SERVICE APPROACHES: ECONOMIC AND NON-PROLIFERATION MERITS OF NUCLEAR FUEL LEASING

    International Nuclear Information System (INIS)

    Kreyling, Sean J.; Brothers, Alan J.; Short, Steven M.; Phillips, Jon R.; Weimar, Mark R.

    2010-01-01

    The goal of international nuclear policy since the dawn of nuclear power has been the peaceful expansion of nuclear energy while controlling the spread of enrichment and reprocessing technology. Numerous initiatives undertaken in the intervening decades to develop international agreements on providing nuclear fuel supply assurances, or reliable nuclear fuel services (RNFS) attempted to control the spread of sensitive nuclear materials and technology. In order to inform the international debate and the development of government policy, PNNL has been developing an analytical framework to holistically evaluate the economics and non-proliferation merits of alternative approaches to managing the nuclear fuel cycle (i.e., cradle-to-grave). This paper provides an overview of the analytical framework and discusses preliminary results of an economic assessment of one RNFS approach: full-service nuclear fuel leasing. The specific focus of this paper is the metrics under development to systematically evaluate the non-proliferation merits of fuel-cycle management alternatives. Also discussed is the utility of an integrated assessment of the economics and non-proliferation merits of nuclear fuel leasing.

  10. Analytical methods for waste minimisation in the convenience food industry.

    Science.gov (United States)

    Darlington, R; Staikos, T; Rahimifard, S

    2009-04-01

    Waste creation in some sectors of the food industry is substantial, and while much of the used material is non-hazardous and biodegradable, it is often poorly dealt with and simply sent to landfill mixed with other types of waste. In this context, overproduction wastes were found in a number of cases to account for 20-40% of the material wastes generated by convenience food manufacturers (such as ready-meals and sandwiches), often simply just to meet the challenging demands placed on the manufacturer due to the short order reaction time provided by the supermarkets. Identifying specific classes of waste helps to minimise their creation, through consideration of what the materials constitute and why they were generated. This paper aims to provide means by which food industry wastes can be identified, and demonstrate these mechanisms through a practical example. The research reported in this paper investigated the various categories of waste and generated three analytical methods for the support of waste minimisation activities by food manufacturers. The waste classifications and analyses are intended to complement existing waste minimisation approaches and are described through consideration of a case study convenience food manufacturer that realised significant financial savings through waste measurement, analysis and reduction.

  11. NIOSH Manual of Analytical Methods (third edition). Fourth supplement

    Energy Technology Data Exchange (ETDEWEB)

    1990-08-15

    The NIOSH Manual of Analytical Methods, 3rd edition, was updated for the following chemicals: allyl-glycidyl-ether, 2-aminopyridine, aspartame, bromine, chlorine, n-butylamine, n-butyl-glycidyl-ether, carbon-dioxide, carbon-monoxide, chlorinated-camphene, chloroacetaldehyde, p-chlorophenol, crotonaldehyde, 1,1-dimethylhydrazine, dinitro-o-cresol, ethyl-acetate, ethyl-formate, ethylenimine, sodium-fluoride, hydrogen-fluoride, cryolite, sodium-hexafluoroaluminate, formic-acid, hexachlorobutadiene, hydrogen-cyanide, hydrogen-sulfide, isopropyl-acetate, isopropyl-ether, isopropyl-glycidyl-ether, lead, lead-oxide, maleic-anhydride, methyl-acetate, methyl-acrylate, methyl-tert-butyl ether, methyl-cellosolve-acetate, methylcyclohexanol, 4,4'-methylenedianiline, monomethylaniline, monomethylhydrazine, nitric-oxide, p-nitroaniline, phenyl-ether, phenyl-ether-biphenyl mixture, phenyl-glycidyl-ether, phenylhydrazine, phosphine, ronnel, sulfuryl-fluoride, talc, tributyl-phosphate, 1,1,2-trichloro-1,2,2-trifluoroethane, trimellitic-anhydride, triorthocresyl-phosphate, triphenyl-phosphate, and vinyl-acetate.

  12. An analytical method for optimal design of MR valve structures

    International Nuclear Information System (INIS)

    Nguyen, Q H; Choi, S B; Lee, Y S; Han, M S

    2009-01-01

    This paper proposes an analytical methodology for the optimal design of a magnetorheological (MR) valve structure. The MR valve structure is constrained in a specific volume and the optimization problem identifies geometric dimensions of the valve structure that maximize the yield stress pressure drop of a MR valve or the yield stress damping force of a MR damper. In this paper, the single-coil and two-coil annular MR valve structures are considered. After describing the schematic configuration and operating principle of a typical MR valve and damper, a quasi-static model is derived based on the Bingham model of a MR fluid. The magnetic circuit of the valve and damper is then analyzed by applying Kirchoff's law and the magnetic flux conservation rule. Based on quasi-static modeling and magnetic circuit analysis, the optimization problem of the MR valve and damper is built. In order to reduce the computation load, the optimization problem is simplified and a procedure to obtain the optimal solution of the simplified optimization problem is presented. The optimal solution of the simplified optimization problem of the MR valve structure constrained in a specific volume is then obtained and compared with the solution of the original optimization problem and the optimal solution obtained from the finite element method

  13. AN ANALYTICAL METHOD FOR CHEMICAL SPECIATION OF SELENIUM IN SOIL

    Directory of Open Access Journals (Sweden)

    Constantin Luca

    2010-10-01

    Full Text Available Selenium is an essential microelement, sometimes redoubtable, through its beneficial role - risk depending on its concentration in the food chain, at low dose is an important nutrient in the life of humans and animals, contrary at high doses, it becomes toxic. Selenium may be find itself in the environment (soil, sediment, water in many forms (oxidized, reduced, organometallic which determine their mobility and toxicity. Determination of chemical speciation (identification of different chemical forms provides much more complete information for a better understanding of the behavior and the potential impact on the environment. In this work we present the results of methodological research on the extraction of sequential forms of selenium in the soil and the coupling of analytical methods capable of identifying very small amounts of selenium in soils An efficient scheme of sequential extractions forms of selenium (SES consisting in atomic absorption spectrometry coupled with hydride generation (HGAAS has been developed into five experimental steps, detailed in the paper. This operational scheme has been applied to the analysis of chemical speciation in the following areas: the Bărăgan Plain and Central Dobrogea of Romania.

  14. Safety and reliability analysis based on nonprobabilistic methods

    International Nuclear Information System (INIS)

    Kozin, I.O.; Petersen, K.E.

    1996-01-01

    Imprecise probabilities, being developed during the last two decades, offer a considerably more general theory having many advantages which make it very promising for reliability and safety analysis. The objective of the paper is to argue that imprecise probabilities are more appropriate tool for reliability and safety analysis, that they allow to model the behavior of nuclear industry objects more comprehensively and give a possibility to solve some problems unsolved in the framework of conventional approach. Furthermore, some specific examples are given from which we can see the usefulness of the tool for solving some reliability tasks

  15. Review of methods for the integration of reliability and design engineering

    International Nuclear Information System (INIS)

    Reilly, J.T.

    1978-03-01

    A review of methods for the integration of reliability and design engineering was carried out to establish a reliability program philosophy, an initial set of methods, and procedures to be used by both the designer and reliability analyst. The report outlines a set of procedures which implements a philosophy that requires increased involvement by the designer in reliability analysis. Discussions of each method reviewed include examples of its application

  16. Method of core thermodynamic reliability determination in pressurized water reactors

    Energy Technology Data Exchange (ETDEWEB)

    Ackermann, G.; Horche, W. (Ingenieurhochschule Zittau (German Democratic Republic). Sektion Kraftwerksanlagenbau und Energieumwandlung)

    1983-01-01

    A statistical model appropriate to determine the thermodynamic reliability and the power-limiting parameter of PWR cores is described for cases of accidental transients. The model is compared with the hot channel model hitherto applied.

  17. Method of core thermodynamic reliability determination in pressurized water reactors

    International Nuclear Information System (INIS)

    Ackermann, G.; Horche, W.

    1983-01-01

    A statistical model appropriate to determine the thermodynamic reliability and the power-limiting parameter of PWR cores is described for cases of accidental transients. The model is compared with the hot channel model hitherto applied. (author)

  18. Intercalibration of analytical methods on marine environmental samples

    International Nuclear Information System (INIS)

    1988-06-01

    The pollution of the seas by various chemical substances constitutes nowadays one of the principal concerns of mankind. The International Atomic Energy Agency has organized in past years several intercomparison exercises in the framework of its Analytical Quality Control Service. The present intercomparison had a double aim: first, to give laboratories participating in this intercomparison an opportunity for checking their analytical performance. Secondly, to produce on the basis of the results of this intercomparison a reference material made of fish tissue which would be accurately certified with respect to many trace elements. Such a material could be used by analytical chemists to check the validity of new analytical procedures. In total, 53 laboratories from 29 countries reported results (585 laboratory means for 48 elements). 5 refs, 52 tabs

  19. Estimating Fuel Cycle Externalities: Analytical Methods and Issues, Report 2

    Energy Technology Data Exchange (ETDEWEB)

    Barnthouse, L.W.; Cada, G.F.; Cheng, M.-D.; Easterly, C.E.; Kroodsma, R.L.; Lee, R.; Shriner, D.S.; Tolbert, V.R.; Turner, R.S.

    1994-07-01

    of complex issues that also have not been fully addressed. This document contains two types of papers that seek to fill part of this void. Some of the papers describe analytical methods that can be applied to one of the five steps of the damage function approach. The other papers discuss some of the complex issues that arise in trying to estimate externalities. This report, the second in a series of eight reports, is part of a joint study by the U.S. Department of Energy (DOE) and the Commission of the European Communities (EC)* on the externalities of fuel cycles. Most of the papers in this report were originally written as working papers during the initial phases of this study. The papers provide descriptions of the (non-radiological) atmospheric dispersion modeling that the study uses; reviews much of the relevant literature on ecological and health effects, and on the economic valuation of those impacts; contains several papers on some of the more complex and contentious issues in estimating externalities; and describes a method for depicting the quality of scientific information that a study uses. The analytical methods and issues that this report discusses generally pertain to more than one of the fuel cycles, though not necessarily to all of them. The report is divided into six parts, each one focusing on a different subject area.

  20. Fuel Cycle Externalities: Analytical Methods and Issues, Report 2

    International Nuclear Information System (INIS)

    Barnthouse, L.W.; Cada, G.F.; Cheng, M.-D.; Easterly, C.E.; Kroodsma, R.L.; Lee, R.; Shriner, D.S.; Tolbert, V.R.; Turner, R.S.

    1994-01-01

    that also have not been fully addressed. This document contains two types of papers that seek to fill part of this void. Some of the papers describe analytical methods that can be applied to one of the five steps of the damage function approach. The other papers discuss some of the complex issues that arise in trying to estimate externalities. This report, the second in a series of eight reports, is part of a joint study by the U.S. Department of Energy (DOE) and the Commission of the European Communities (EC)* on the externalities of fuel cycles. Most of the papers in this report were originally written as working papers during the initial phases of this study. The papers provide descriptions of the (non-radiological) atmospheric dispersion modeling that the study uses; reviews much of the relevant literature on ecological and health effects, and on the economic valuation of those impacts; contains several papers on some of the more complex and contentious issues in estimating externalities; and describes a method for depicting the quality of scientific information that a study uses. The analytical methods and issues that this report discusses generally pertain to more than one of the fuel cycles, though not necessarily to all of them. The report is divided into six parts, each one focusing on a different subject area

  1. Structural Reliability Methods for Wind Power Converter System Component Reliability Assessment

    DEFF Research Database (Denmark)

    Kostandyan, Erik; Sørensen, John Dalsgaard

    2012-01-01

    Wind power converter systems are essential subsystems in both off-shore and on-shore wind turbines. It is the main interface between generator and grid connection. This system is affected by numerous stresses where the main contributors might be defined as vibration and temperature loadings....... The temperature variations induce time-varying stresses and thereby fatigue loads. A probabilistic model is used to model fatigue failure for an electrical component in the power converter system. This model is based on a linear damage accumulation and physics of failure approaches, where a failure criterion...... is defined by the threshold model. The attention is focused on crack propagation in solder joints of electrical components due to the temperature loadings. Structural Reliability approaches are used to incorporate model, physical and statistical uncertainties. Reliability estimation by means of structural...

  2. The effect on reliability and sensitivity to level of training of combining analytic and holistic rating scales for assessing communication skills in an internal medicine resident OSCE.

    Science.gov (United States)

    Daniels, Vijay John; Harley, Dwight

    2017-07-01

    Although previous research has compared checklists to rating scales for assessing communication, the purpose of this study was to compare the effect on reliability and sensitivity to level of training of an analytic, a holistic, and a combined analytic-holistic rating scale in assessing communication skills. The University of Alberta Internal Medicine Residency runs OSCEs for postgraduate year (PGY) 1 and 2 residents and another for PGY-4 residents. Communication stations were scored with an analytic scale (empathy, non-verbal skills, verbal skills, and coherence subscales) and a holistic scale. Authors analyzed reliability of individual and combined scales using generalizability theory and evaluated each scale's sensitivity to level of training. For analytic, holistic, and combined scales, 12, 12, and 11 stations respectively yielded a Phi of 0.8 for the PGY-1,2 cohort, and 16, 16, and 14 stations yielded a Phi of 0.8 for the PGY-4 cohort. PGY-4 residents scored higher on the combined scale, the analytic rating scale, and the non-verbal and coherence subscales. A combined analytic-holistic rating scale increased score reliability and was sensitive to level of training. Given increased validity evidence, OSCE developers should consider combining analytic and holistic scales when assessing communication skills. Copyright © 2017 Elsevier B.V. All rights reserved.

  3. Prepared for the thirtieth annual conference on bioassay analytical and environmental chemistry. Reliable analysis of high resolution gamma spectra

    International Nuclear Information System (INIS)

    Spitz, H.B.; Buschbom, R.; Rieksts, G.A.; Palmer, H.E.

    1985-01-01

    A new method has been developed to reliably analyze pulse height-energy spectra obtained from measurements employing high resolution germanium detectors. The method employs a simple data transformation and smoothing function to calculate background and identify photopeaks and isotopic analysis. This technique is elegant in its simplicity because it avoids dependence upon complex spectrum deconvolution, stripping, or other least-square-fitting techniques which complicate the assessment of measurement reliability. A moving median was chosen for data smoothing because, unlike moving averages, medians are not dominated by extreme data points. Finally, peaks are identified whenever the difference between the background spectrum and the transformed spectrum exceeds a pre-determined number of standard deviations

  4. Studies on analytical method and nondestructive measuring method on the sensitization of austenitic stainless steels

    International Nuclear Information System (INIS)

    Onimura, Kichiro; Arioka, Koji; Horai, Manabu; Noguchi, Shigeru.

    1982-03-01

    Austenitic stainless steels are widely used as structural materials for the machine and equipment of various kinds of plants, such as thermal power, nuclear power, and chemical plants. The machines and equipment using this kind of material, however, have the possibility of suffering corrosion damage while in service, and these damages are considered to be largely due to the sensitization of the material in sometimes. So, it is necessary to develop an analytical method for grasping the sensitization of the material more in detail and a quantitative nondestructive measuring method which is applicable to various kinds of structures in order to prevent the corrosion damage. From the above viewpoint, studies have been made on the analytical method based on the theory of diffusion of chromium in austenitic stainless steels and on Electro-Potentiokinetics Reactivation Method (EPR Method) as a nondestructive measuring method, using 304 and 316 austenitic stainless steels having different carbon contents in base metals. This paper introduces the results of EPR test on the sensitization of austenitic stainless steels and the correlation between analytical and experimental results. (author)

  5. Analytical method of waste allocation in waste management systems: Concept, method and case study

    International Nuclear Information System (INIS)

    Bergeron, Francis C.

    2017-01-01

    Waste is not a rejected item to dispose anymore but increasingly a secondary resource to exploit, influencing waste allocation among treatment operations in a waste management (WM) system. The aim of this methodological paper is to present a new method for the assessment of the WM system, the “analytical method of the waste allocation process” (AMWAP), based on the concept of the “waste allocation process” defined as the aggregation of all processes of apportioning waste among alternative waste treatment operations inside or outside the spatial borders of a WM system. AMWAP contains a conceptual framework and an analytical approach. The conceptual framework includes, firstly, a descriptive model that focuses on the description and classification of the WM system. It includes, secondly, an explanatory model that serves to explain and to predict the operation of the WM system. The analytical approach consists of a step-by-step analysis for the empirical implementation of the conceptual framework. With its multiple purposes, AMWAP provides an innovative and objective modular method to analyse a WM system which may be integrated in the framework of impact assessment methods and environmental systems analysis tools. Its originality comes from the interdisciplinary analysis of the WAP and to develop the conceptual framework. AMWAP is applied in the framework of an illustrative case study on the household WM system of Geneva (Switzerland). It demonstrates that this method provides an in-depth and contextual knowledge of WM. - Highlights: • The study presents a new analytical method based on the waste allocation process. • The method provides an in-depth and contextual knowledge of the waste management system. • The paper provides a reproducible procedure for professionals, experts and academics. • It may be integrated into impact assessment or environmental system analysis tools. • An illustrative case study is provided based on household waste

  6. Analytical method of waste allocation in waste management systems: Concept, method and case study

    Energy Technology Data Exchange (ETDEWEB)

    Bergeron, Francis C., E-mail: francis.b.c@videotron.ca

    2017-01-15

    Waste is not a rejected item to dispose anymore but increasingly a secondary resource to exploit, influencing waste allocation among treatment operations in a waste management (WM) system. The aim of this methodological paper is to present a new method for the assessment of the WM system, the “analytical method of the waste allocation process” (AMWAP), based on the concept of the “waste allocation process” defined as the aggregation of all processes of apportioning waste among alternative waste treatment operations inside or outside the spatial borders of a WM system. AMWAP contains a conceptual framework and an analytical approach. The conceptual framework includes, firstly, a descriptive model that focuses on the description and classification of the WM system. It includes, secondly, an explanatory model that serves to explain and to predict the operation of the WM system. The analytical approach consists of a step-by-step analysis for the empirical implementation of the conceptual framework. With its multiple purposes, AMWAP provides an innovative and objective modular method to analyse a WM system which may be integrated in the framework of impact assessment methods and environmental systems analysis tools. Its originality comes from the interdisciplinary analysis of the WAP and to develop the conceptual framework. AMWAP is applied in the framework of an illustrative case study on the household WM system of Geneva (Switzerland). It demonstrates that this method provides an in-depth and contextual knowledge of WM. - Highlights: • The study presents a new analytical method based on the waste allocation process. • The method provides an in-depth and contextual knowledge of the waste management system. • The paper provides a reproducible procedure for professionals, experts and academics. • It may be integrated into impact assessment or environmental system analysis tools. • An illustrative case study is provided based on household waste

  7. Analytical method of polychlorinated biphenyls(PCBs) in transformer oil

    Energy Technology Data Exchange (ETDEWEB)

    Shin, S.K. [National Institute of Environmental Research, Incheon (Korea); Kim, H.J.; Chung, D.; Kim, K.S.; Kim, J.K.; Chung, Y.H.; Chung, I.R.

    2004-09-15

    Polychlorinated biphenyls (PCBs) is a chlorinated biphenyl compound with the general formula C{sub 12}H{sub 10-n}/Cl{sub n}. PCBs generally occur as mixtures, where n can vary from 1 to 10. The 10 sites available for possible chlorine substitution result in 209 possible PCB congeners. There is now considerable concern regarding; the presence of PCB congeners in insulating oils used within large-scale electrical supply systems. Due to its outstanding chemical and thermal stabilities and electrical insulation properties, the commercial and industrial products of polychlorinated biphenyls (PCBs), such as Aroclors, Kaneclors, Clophens, Phenaclors etc., had been widely used as thermal oil and transformer oil from 1930s until the 1970s. PCBs from a group of persistent organic pollutants of the environment, especially dangerous to living organisms due to high toxicity, persistency, and bio-concentration in adipose tissue. Despite of this fact, PCB-contaminated oils are still commonly encountered partly because PCBs used as dielectric liquids in transformer and condenser. The source of PCBs in environments can range from used transformer oils or dielectric liquids to liquid wastes, and some PCBs contamination is occurred due to the re-use of incompletely reconditioned oil. The current action plan of Republic of Korea dictates that organizations with electrical equipment contaminated with more than 2 mg/L PCBs will need to treat as PCBs-containing wastes, and 50mg/L of PCBs or PCBs equivalent to be treated as a pure PCB preparation. In this study, transformer oils analyzed based on guideline for PCBs analytical method of transformer oil in Korea.

  8. Transport methods: general. 1. The Analytical Monte Carlo Method for Radiation Transport Calculations

    International Nuclear Information System (INIS)

    Martin, William R.; Brown, Forrest B.

    2001-01-01

    We present an alternative Monte Carlo method for solving the coupled equations of radiation transport and material energy. This method is based on incorporating the analytical solution to the material energy equation directly into the Monte Carlo simulation for the radiation intensity. This method, which we call the Analytical Monte Carlo (AMC) method, differs from the well known Implicit Monte Carlo (IMC) method of Fleck and Cummings because there is no discretization of the material energy equation since it is solved as a by-product of the Monte Carlo simulation of the transport equation. Our method also differs from the method recently proposed by Ahrens and Larsen since they use Monte Carlo to solve both equations, while we are solving only the radiation transport equation with Monte Carlo, albeit with effective sources and cross sections to represent the emission sources. Our method bears some similarity to a method developed and implemented by Carter and Forest nearly three decades ago, but there are substantive differences. We have implemented our method in a simple zero-dimensional Monte Carlo code to test the feasibility of the method, and the preliminary results are very promising, justifying further extension to more realistic geometries. (authors)

  9. Characteristics and application study of AP1000 NPPs equipment reliability classification method

    International Nuclear Information System (INIS)

    Guan Gao

    2013-01-01

    AP1000 nuclear power plant applies an integrated approach to establish equipment reliability classification, which includes probabilistic risk assessment technique, maintenance rule administrative, power production reliability classification and functional equipment group bounding method, and eventually classify equipment reliability into 4 levels. This classification process and result are very different from classical RCM and streamlined RCM. It studied the characteristic of AP1000 equipment reliability classification approach, considered that equipment reliability classification should effectively support maintenance strategy development and work process control, recommended to use a combined RCM method to establish the future equipment reliability program of AP1000 nuclear power plants. (authors)

  10. Reliability of a semi-quantitative method for dermal exposure assessment (DREAM)

    NARCIS (Netherlands)

    Wendel de Joode, B. van; Hemmen, J.J. van; Meijster, T.; Major, V.; London, L.; Kromhout, H.

    2005-01-01

    Valid and reliable semi-quantitative dermal exposure assessment methods for epidemiological research and for occupational hygiene practice, applicable for different chemical agents, are practically nonexistent. The aim of this study was to assess the reliability of a recently developed

  11. A Reliability Assessment Method for the VHTR Safety Systems

    International Nuclear Information System (INIS)

    Lee, Hyung Sok; Jae, Moo Sung; Kim, Yong Wan

    2011-01-01

    The Passive safety system by very high temperature reactor which has attracted worldwide attention in the last century is the reliability safety system introduced for the improvement in the safety of the next generation nuclear power plant design. The Passive system functionality does not rely on an external source of energy, but on an intelligent use of the natural phenomena, such as gravity, conduction and radiation, which are always present. Because of these features, it is difficult to evaluate the passive safety on the risk analysis methodology having considered the existing active system failure. Therefore new reliability methodology has to be considered. In this study, the preliminary evaluation and conceptualization are tried, applying the concept of the load and capacity from the reliability physics model, designing the new passive system analysis methodology, and the trial applying to paper plant.

  12. New analytical exact solutions of time fractional KdV-KZK equation by Kudryashov methods

    Science.gov (United States)

    S Saha, Ray

    2016-04-01

    In this paper, new exact solutions of the time fractional KdV-Khokhlov-Zabolotskaya-Kuznetsov (KdV-KZK) equation are obtained by the classical Kudryashov method and modified Kudryashov method respectively. For this purpose, the modified Riemann-Liouville derivative is used to convert the nonlinear time fractional KdV-KZK equation into the nonlinear ordinary differential equation. In the present analysis, the classical Kudryashov method and modified Kudryashov method are both used successively to compute the analytical solutions of the time fractional KdV-KZK equation. As a result, new exact solutions involving the symmetrical Fibonacci function, hyperbolic function and exponential function are obtained for the first time. The methods under consideration are reliable and efficient, and can be used as an alternative to establish new exact solutions of different types of fractional differential equations arising from mathematical physics. The obtained results are exhibited graphically in order to demonstrate the efficiencies and applicabilities of these proposed methods of solving the nonlinear time fractional KdV-KZK equation.

  13. New analytical exact solutions of time fractional KdV–KZK equation by Kudryashov methods

    International Nuclear Information System (INIS)

    Saha Ray, S

    2016-01-01

    In this paper, new exact solutions of the time fractional KdV–Khokhlov–Zabolotskaya–Kuznetsov (KdV–KZK) equation are obtained by the classical Kudryashov method and modified Kudryashov method respectively. For this purpose, the modified Riemann–Liouville derivative is used to convert the nonlinear time fractional KdV–KZK equation into the nonlinear ordinary differential equation. In the present analysis, the classical Kudryashov method and modified Kudryashov method are both used successively to compute the analytical solutions of the time fractional KdV–KZK equation. As a result, new exact solutions involving the symmetrical Fibonacci function, hyperbolic function and exponential function are obtained for the first time. The methods under consideration are reliable and efficient, and can be used as an alternative to establish new exact solutions of different types of fractional differential equations arising from mathematical physics. The obtained results are exhibited graphically in order to demonstrate the efficiencies and applicabilities of these proposed methods of solving the nonlinear time fractional KdV–KZK equation. (paper)

  14. Reliability-Based Shape Optimization using Stochastic Finite Element Methods

    DEFF Research Database (Denmark)

    Enevoldsen, Ib; Sørensen, John Dalsgaard; Sigurdsson, G.

    1991-01-01

    stochastic fields (e.g. loads and material parameters such as Young's modulus and the Poisson ratio). In this case stochastic finite element techniques combined with FORM analysis can be used to obtain measures of the reliability of the structural systems, see Der Kiureghian & Ke (6) and Liu & Der Kiureghian...

  15. Survey of industry methods for producing highly reliable software

    International Nuclear Information System (INIS)

    Lawrence, J.D.; Persons, W.L.

    1994-11-01

    The Nuclear Reactor Regulation Office of the US Nuclear Regulatory Commission is charged with assessing the safety of new instrument and control designs for nuclear power plants which may use computer-based reactor protection systems. Lawrence Livermore National Laboratory has evaluated the latest techniques in software reliability for measurement, estimation, error detection, and prediction that can be used during the software life cycle as a means of risk assessment for reactor protection systems. One aspect of this task has been a survey of the software industry to collect information to help identify the design factors used to improve the reliability and safety of software. The intent was to discover what practices really work in industry and what design factors are used by industry to achieve highly reliable software. The results of the survey are documented in this report. Three companies participated in the survey: Computer Sciences Corporation, International Business Machines (Federal Systems Company), and TRW. Discussions were also held with NASA Software Engineering Lab/University of Maryland/CSC, and the AIAA Software Reliability Project

  16. 40 CFR 136.6 - Method modifications and analytical requirements.

    Science.gov (United States)

    2010-07-01

    ... modifications and analytical requirements. (a) Definitions of terms used in this section. (1) Analyst means the..., oil and grease, total suspended solids, total phenolics, turbidity, chemical oxygen demand, and.... Except as set forth in paragraph (b)(3) of this section, an analyst may modify an approved test procedure...

  17. 77 FR 56176 - Analytical Methods Used in Periodic Reporting

    Science.gov (United States)

    2012-09-12

    ... informal rulemaking proceeding to consider changes in analytical principles (Proposals Six and Seven) used... (Proposals Six and Seven), September 4, 2012 (Petition). Proposal Six: Use of Foreign Postal Settlement System as Sole Source for Reporting of Inbound International Revenue, Pieces, and Weights. The Postal...

  18. Hanford environmental analytical methods: Methods as of March 1990. Volume 3, Appendix A2-I

    Energy Technology Data Exchange (ETDEWEB)

    Goheen, S.C.; McCulloch, M.; Daniel, J.L.

    1993-05-01

    This paper from the analytical laboratories at Hanford describes the method used to measure pH of single-shell tank core samples. Sludge or solid samples are mixed with deionized water. The pH electrode used combines both a sensor and reference electrode in one unit. The meter amplifies the input signal from the electrode and displays the pH visually.

  19. Advancing methods for reliably assessing motivational interviewing fidelity using the motivational interviewing skills code.

    Science.gov (United States)

    Lord, Sarah Peregrine; Can, Doğan; Yi, Michael; Marin, Rebeca; Dunn, Christopher W; Imel, Zac E; Georgiou, Panayiotis; Narayanan, Shrikanth; Steyvers, Mark; Atkins, David C

    2015-02-01

    The current paper presents novel methods for collecting MISC data and accurately assessing reliability of behavior codes at the level of the utterance. The MISC 2.1 was used to rate MI interviews from five randomized trials targeting alcohol and drug use. Sessions were coded at the utterance-level. Utterance-based coding reliability was estimated using three methods and compared to traditional reliability estimates of session tallies. Session-level reliability was generally higher compared to reliability using utterance-based codes, suggesting that typical methods for MISC reliability may be biased. These novel methods in MI fidelity data collection and reliability assessment provided rich data for therapist feedback and further analyses. Beyond implications for fidelity coding, utterance-level coding schemes may elucidate important elements in the counselor-client interaction that could inform theories of change and the practice of MI. Copyright © 2015 Elsevier Inc. All rights reserved.

  20. Usefulness of the Monte Carlo method in reliability calculations

    International Nuclear Information System (INIS)

    Lanore, J.M.; Kalli, H.

    1977-01-01

    Three examples of reliability Monte Carlo programs developed in the LEP (Laboratory for Radiation Shielding Studies in the Nuclear Research Center at Saclay) are presented. First, an uncertainty analysis is given for a simplified spray system; a Monte Carlo program PATREC-MC has been written to solve the problem with the system components given in the fault tree representation. The second program MONARC 2 has been written to solve the problem of complex systems reliability by the Monte Carlo simulation, here again the system (a residual heat removal system) is in the fault tree representation. Third, the Monte Carlo program MONARC was used instead of the Markov diagram to solve the simulation problem of an electric power supply including two nets and two stand-by diesels

  1. Reliability improvement methods for sapphire fiber temperature sensors

    Science.gov (United States)

    Schietinger, C.; Adams, B.

    1991-08-01

    Mechanical, optical, electrical, and software design improvements can be brought to bear in the enhancement of fiber-optic sapphire-fiber temperature measurement tool reliability in harsh environments. The optical fiber thermometry (OFT) equipment discussed is used in numerous process industries and generally involves a sapphire sensor, an optical transmission cable, and a microprocessor-based signal analyzer. OFT technology incorporating sensors for corrosive environments, hybrid sensors, and two-wavelength measurements, are discussed.

  2. A reliable method for ageing of whiting (Merlangius merlangus) for use in stock assessment and management

    DEFF Research Database (Denmark)

    Ross, Stine Dalmann; Hüssy, Karin

    2013-01-01

    Accurate age estimation is important for stock assessment and management. The importance of reliable ageing is emphasized by the impending analytical assessment of whiting (Merlangius merlangus) in the Baltic Sea. Whiting is a top predator in the western Baltic Sea, where it is fished commercially...

  3. Analytical methods of heat transfer compared with numerical methods as related to nuclear waste repositories

    International Nuclear Information System (INIS)

    Estrada-Gasca, C.A.

    1986-01-01

    Analytical methods were applied to the prediction of the far-field thermal impact of a nuclear waste repository. Specifically, the transformation of coordinates and the Kirchhoff transformation were used to solve one-dimensional nonlinear heat conduction problems. Calculations for the HLW and TRU nuclear waste with initial areal thermal loadings of 12 kW/acre and 0.7 kW/acre, respectively, are carried out for various models. Also, finite difference and finite element methods are applied. The last method is used to solve two-dimensional linear and nonlinear heat conduction problems. Results of the analysis are temperature distributions and temperature histories. Explicit analytical expressions of the maximum temperature rise as a function of the system parameters are presented. The theoretical approaches predict maximum temperature increases in the overburden with an error of 10%. When the finite solid one-dimensional NWR thermal problem is solved with generic salt and HLW thermal load as parameters, the maximum temperature rises predicted by the finite difference and finite element methods had maximum errors of 2.6 and 6.7%, respectively. In all the other cases the finite difference method also gave a smaller error than the finite element method

  4. Reliability analysis of reactor systems by applying probability method; Analiza pouzdanosti reaktorskih sistema primenom metoda verovatnoce

    Energy Technology Data Exchange (ETDEWEB)

    Milivojevic, S [Institute of Nuclear Sciences Boris Kidric, Vinca, Beograd (Serbia and Montenegro)

    1974-12-15

    Probability method was chosen for analysing the reactor system reliability is considered realistic since it is based on verified experimental data. In fact this is a statistical method. The probability method developed takes into account the probability distribution of permitted levels of relevant parameters and their particular influence on the reliability of the system as a whole. The proposed method is rather general, and was used for problem of thermal safety analysis of reactor system. This analysis enables to analyze basic properties of the system under different operation conditions, expressed in form of probability they show the reliability of the system on the whole as well as reliability of each component.

  5. Reliability Evaluation of Bridges Based on Nonprobabilistic Response Surface Limit Method

    Directory of Open Access Journals (Sweden)

    Xuyong Chen

    2017-01-01

    Full Text Available Due to many uncertainties in nonprobabilistic reliability assessment of bridges, the limit state function is generally unknown. The traditional nonprobabilistic response surface method is a lengthy and oscillating iteration process and leads to difficultly solving the nonprobabilistic reliability index. This article proposes a nonprobabilistic response surface limit method based on the interval model. The intention of this method is to solve the upper and lower limits of the nonprobabilistic reliability index and to narrow the range of the nonprobabilistic reliability index. If the range of the reliability index reduces to an acceptable accuracy, the solution will be considered convergent, and the nonprobabilistic reliability index will be obtained. The case study indicates that using the proposed method can avoid oscillating iteration process, make iteration process stable and convergent, reduce iteration steps significantly, and improve computational efficiency and precision significantly compared with the traditional nonprobabilistic response surface method. Finally, the nonprobabilistic reliability evaluation process of bridge will be built through evaluating the reliability of one PC continuous rigid frame bridge with three spans using the proposed method, which appears to be more simple and reliable when lack of samples and parameters in the bridge nonprobabilistic reliability evaluation is present.

  6. Analytical methods for the evaluation of melamine contamination.

    Science.gov (United States)

    Cantor, Stuart L; Gupta, Abhay; Khan, Mansoor A

    2014-02-01

    There is an urgent need for the analysis of melamine in the global pharmaceutical supply chain to detect economically motivated adulteration or unintentional contamination using a simple, nondestructive analytical technique that confirms the extent of adulteration in a shorter time period. In this work, different analytical techniques (thermal analysis, X-ray diffraction, Fourier transform infrared (FT-IR), FT-Raman, and near-infrared (NIR) spectroscopy) were evaluated for their ability to detect a range of melamine levels in gelatin. While FT-IR and FT-Raman provided qualitative assessment of melamine contamination or adulteration, powder X-ray diffraction and NIR were able to detect and quantify the presence of melamine at levels as low as 1.0% w/w. Multivariate analysis of the NIR data yielded the most accurate model when three principal components were used. Data were pretreated using standard normal variate transformation to remove multiplicative interferences of scatter and particle size. The model had a root-mean-square error of calibration of 2.4 (R(2) = 0.99) and root-mean square error of prediction of 2.5 (R(2) = 0.96). The value of the paired t test for actual and predicted samples (1%-50% w/w) was 0.448 (p 5), further indicating the robustness of the model. Published 2013. This article is a U.S. Government work and is in the public domain in the USA.

  7. Assessment and Improving Methods of Reliability Indices in Bakhtar Regional Electricity Company

    Directory of Open Access Journals (Sweden)

    Saeed Shahrezaei

    2013-04-01

    Full Text Available Reliability of a system is the ability of a system to do prospected duties in future and the probability of desirable operation for doing predetermined duties. Power system elements failures data are the main data of reliability assessment in the network. Determining antiseptic parameters is the goal of reliability assessment by using system history data. These parameters help to recognize week points of the system. In other words, the goal of reliability assessment is operation improving and decreasing of the failures and power outages. This paper is developed to assess reliability indices of Bakhtar Regional Electricity Company up to 1393 and the improving methods and their effects on the reliability indices in this network. DIgSILENT Power Factory software is employed for simulation. Simulation results show the positive effect of improving methods in reliability indices of Bakhtar Regional Electricity Company.

  8. Reliability studies of diagnostic methods in Indian traditional Ayurveda medicine: An overview

    Science.gov (United States)

    Kurande, Vrinda Hitendra; Waagepetersen, Rasmus; Toft, Egon; Prasad, Ramjee

    2013-01-01

    Recently, a need to develop supportive new scientific evidence for contemporary Ayurveda has emerged. One of the research objectives is an assessment of the reliability of diagnoses and treatment. Reliability is a quantitative measure of consistency. It is a crucial issue in classification (such as prakriti classification), method development (pulse diagnosis), quality assurance for diagnosis and treatment and in the conduct of clinical studies. Several reliability studies are conducted in western medicine. The investigation of the reliability of traditional Chinese, Japanese and Sasang medicine diagnoses is in the formative stage. However, reliability studies in Ayurveda are in the preliminary stage. In this paper, examples are provided to illustrate relevant concepts of reliability studies of diagnostic methods and their implication in practice, education, and training. An introduction to reliability estimates and different study designs and statistical analysis is given for future studies in Ayurveda. PMID:23930037

  9. Method for assessing reliability of a network considering probabilistic safety assessment

    International Nuclear Information System (INIS)

    Cepin, M.

    2005-01-01

    A method for assessment of reliability of the network is developed, which uses the features of the fault tree analysis. The method is developed in a way that the increase of the network under consideration does not require significant increase of the model. The method is applied to small examples of network consisting of a small number of nodes and a small number of their connections. The results give the network reliability. They identify equipment, which is to be carefully maintained in order that the network reliability is not reduced, and equipment, which is a candidate for redundancy, as this would improve network reliability significantly. (author)

  10. Comparison of Model Reliabilities from Single-Step and Bivariate Blending Methods

    DEFF Research Database (Denmark)

    Taskinen, Matti; Mäntysaari, Esa; Lidauer, Martin

    2013-01-01

    Model based reliabilities in genetic evaluation are compared between three methods: animal model BLUP, single-step BLUP, and bivariate blending after genomic BLUP. The original bivariate blending is revised in this work to better account animal models. The study data is extracted from...... be calculated. Model reliabilities by the single-step and the bivariate blending methods were higher than by animal model due to genomic information. Compared to the single-step method, the bivariate blending method reliability estimates were, in general, lower. Computationally bivariate blending method was......, on the other hand, lighter than the single-step method....

  11. A manual of analytical methods used at MINTEK

    International Nuclear Information System (INIS)

    Stoch, H.; Dixon, K.

    1983-01-01

    The manual deals with various methods for a wide range of elemental analysis. Some of the methods that are used, include atomic absorption spectroscopy, optical emission spectroscopy and x-ray fluoresence spectroscopy. The basic charateristics of the method are given and the procedures are recorded step by step. One of the sections deals with methods associated with the recovery of uranium

  12. RELIABILITY ASSESSMENT OF ENTROPY METHOD FOR SYSTEM CONSISTED OF IDENTICAL EXPONENTIAL UNITS

    Institute of Scientific and Technical Information of China (English)

    Sun Youchao; Shi Jun

    2004-01-01

    The reliability assessment of unit-system near two levels is the most important content in the reliability multi-level synthesis of complex systems. Introducing the information theory into system reliability assessment, using the addible characteristic of information quantity and the principle of equivalence of information quantity, an entropy method of data information conversion is presented for the system consisted of identical exponential units. The basic conversion formulae of entropy method of unit test data are derived based on the principle of information quantity equivalence. The general models of entropy method synthesis assessment for system reliability approximate lower limits are established according to the fundamental principle of the unit reliability assessment. The applications of the entropy method are discussed by way of practical examples. Compared with the traditional methods, the entropy method is found to be valid and practicable and the assessment results are very satisfactory.

  13. Survey of Technetium Analytical Production Methods Supporting Hanford Nuclear Materials Processing

    International Nuclear Information System (INIS)

    TROYER, G.L.

    1999-01-01

    This document provides a historical survey of analytical methods used for measuring 99 Tc in nuclear fuel reprocessing materials and wastes at Hanford. Method challenges including special sludge matrices tested are discussed. Special problems and recommendations are presented

  14. Nuclear analytical methods in quality control of microanalysis

    International Nuclear Information System (INIS)

    Tian Weizhi

    2004-01-01

    Quantitative calibration and quality control have been a major bottleneck in microanalysis due to the lack of natural-matrix CRMs certified at sample sizes compatible with those of unknown samples. A solution is described to characterize sampling behavior for individual elements, so as to identify elements homogeneous enough at stated sample size levels in given CRMs/RMs. By using a combination of several nuclear analytical techniques, INAA-EDXRF-μPIXE, sampling behavior for individual elements can be characterized at sample size levels from grams down to pg. Natural-matrix CRMs specifically for QC of microanalysis may thus be created. Additional information in certificates of these new generation CRMs is imagined. (author)

  15. Five-point Element Scheme of Finite Analytic Method for Unsteady Groundwater Flow

    Institute of Scientific and Technical Information of China (English)

    Xiang Bo; Mi Xiao; Ji Changming; Luo Qingsong

    2007-01-01

    In order to improve the finite analytic method's adaptability for irregular unit, by using coordinates rotation technique this paper establishes a five-point element scheme of finite analytic method. It not only solves unsteady groundwater flow equation but also gives the boundary condition. This method can be used to calculate the three typical questions of groundwater. By compared with predecessor's computed result, the result of this method is more satisfactory.

  16. The Reliability, Impact, and Cost-Effectiveness of Value-Added Teacher Assessment Methods

    Science.gov (United States)

    Yeh, Stuart S.

    2012-01-01

    This article reviews evidence regarding the intertemporal reliability of teacher rankings based on value-added methods. Value-added methods exhibit low reliability, yet are broadly supported by prominent educational researchers and are increasingly being used to evaluate and fire teachers. The article then presents a cost-effectiveness analysis…

  17. Reliability testing of tendon disease using two different scanning methods in patients with rheumatoid arthritis

    DEFF Research Database (Denmark)

    Bruyn, George A W; Möller, Ingrid; Garrido, Jesus

    2012-01-01

    To assess the intra- and interobserver reliability of musculoskeletal ultrasonography (US) in detecting inflammatory and destructive tendon abnormalities in patients with RA using two different scanning methods.......To assess the intra- and interobserver reliability of musculoskeletal ultrasonography (US) in detecting inflammatory and destructive tendon abnormalities in patients with RA using two different scanning methods....

  18. Model correction factor method for reliability problems involving integrals of non-Gaussian random fields

    DEFF Research Database (Denmark)

    Franchin, P.; Ditlevsen, Ove Dalager; Kiureghian, Armen Der

    2002-01-01

    The model correction factor method (MCFM) is used in conjunction with the first-order reliability method (FORM) to solve structural reliability problems involving integrals of non-Gaussian random fields. The approach replaces the limit-state function with an idealized one, in which the integrals ...

  19. Fast Reliability Assessing Method for Distribution Network with Distributed Renewable Energy Generation

    Science.gov (United States)

    Chen, Fan; Huang, Shaoxiong; Ding, Jinjin; Ding, Jinjin; Gao, Bo; Xie, Yuguang; Wang, Xiaoming

    2018-01-01

    This paper proposes a fast reliability assessing method for distribution grid with distributed renewable energy generation. First, the Weibull distribution and the Beta distribution are used to describe the probability distribution characteristics of wind speed and solar irradiance respectively, and the models of wind farm, solar park and local load are built for reliability assessment. Then based on power system production cost simulation probability discretization and linearization power flow, a optimal power flow objected with minimum cost of conventional power generation is to be resolved. Thus a reliability assessment for distribution grid is implemented fast and accurately. The Loss Of Load Probability (LOLP) and Expected Energy Not Supplied (EENS) are selected as the reliability index, a simulation for IEEE RBTS BUS6 system in MATLAB indicates that the fast reliability assessing method calculates the reliability index much faster with the accuracy ensured when compared with Monte Carlo method.

  20. A comparative study on the HW reliability assessment methods for digital I and C equipment

    Energy Technology Data Exchange (ETDEWEB)

    Jung, Hoan Sung; Sung, T. Y.; Eom, H. S.; Park, J. K.; Kang, H. G.; Lee, G. Y. [Korea Atomic Energy Research Institute, Taejeon (Korea); Kim, M. C. [Korea Advanced Institute of Science and Technology, Taejeon (Korea); Jun, S. T. [KHNP, Taejeon (Korea)

    2002-03-01

    It is necessary to predict or to evaluate the reliability of electronic equipment for the probabilistic safety analysis of digital instrument and control equipment. But most databases for the reliability prediction have no data for the up-to-date equipment and the failure modes are not classified. The prediction results for the specific component show different values according to the methods and databases. For boards and systems each method shows different values than others also. This study is for reliability prediction of PDC system for Wolsong NPP1 as a digital I and C equipment. Various reliability prediction methods and failure databases are used in calculation of the reliability to compare the effects of sensitivity and accuracy of each model and database. Many considerations for the reliability assessment of digital systems are derived with the results of this study. 14 refs., 19 figs., 15 tabs. (Author)

  1. Development, validation and evaluation of an analytical method for the determination of monomeric and oligomeric procyanidins in apple extracts.

    Science.gov (United States)

    Hollands, Wendy J; Voorspoels, Stefan; Jacobs, Griet; Aaby, Kjersti; Meisland, Ane; Garcia-Villalba, Rocio; Tomas-Barberan, Francisco; Piskula, Mariusz K; Mawson, Deborah; Vovk, Irena; Needs, Paul W; Kroon, Paul A

    2017-04-28

    There is a lack of data for individual oligomeric procyanidins in apples and apple extracts. Our aim was to develop, validate and evaluate an analytical method for the separation, identification and quantification of monomeric and oligomeric flavanols in apple extracts. To achieve this, we prepared two types of flavanol extracts from freeze-dried apples; one was an epicatechin-rich extract containing ∼30% (w/w) monomeric (-)-epicatechin which also contained oligomeric procyanidins (Extract A), the second was an oligomeric procyanidin-rich extract depleted of epicatechin (Extract B). The parameters considered for method optimisation were HPLC columns and conditions, sample heating, mass of extract and dilution volumes. The performance characteristics considered for method validation included standard linearity, method sensitivity, precision and trueness. Eight laboratories participated in the method evaluation. Chromatographic separation of the analytes was best achieved utilizing a Hilic column with a binary mobile phase consisting of acidic acetonitrile and acidic aqueous methanol. The final method showed linearity for epicatechin in the range 5-100μg/mL with a correlation co-efficient >0.999. Intra-day and inter-day precision of the analytes ranged from 2 to 6% and 2 to 13% respectively. Up to dp3, trueness of the method was >95% but decreased with increasing dp. Within laboratory precision showed RSD values <5 and 10% for monomers and oligomers, respectively. Between laboratory precision was 4 and 15% (Extract A) and 7 and 30% (Extract B) for monomers and oligomers, respectively. An analytical method for the separation, identification and quantification of procyanidins in an apple extract was developed, validated and assessed. The results of the inter-laboratory evaluation indicate that the method is reliable and reproducible. Copyright © 2017. Published by Elsevier B.V.

  2. The application of analytical methods to the study of Pareto - optimal control systems

    Directory of Open Access Journals (Sweden)

    I. K. Romanova

    2014-01-01

    ; for Pareto - tasks in the presence touch formed the system of algebraic equations whose solution yields the equation of the line Pareto in the parameter space. Display space criteria provides the required Pareto - border; in the absence touch analyzes the property of monotonicity. Analysis of derivatives enables you to define two borders in the parameter space (abscissa and the ordinate axis or at the borders, their parallel.The obtained analytical results are applied to the problem of parametric synthesis of control systems. In the framework of the given structure of double-circuit system suitable made use of a system of differential equations instead of the traditional structural schemes. The formula that shows the change dynamic coefficients of unmanaged system after applying the correction. The choice of direct quality criteria, calculated according to the transition process, made the decision problem is most visible and effective. As quality criteria selected rise time and overshoot. As parameters used the gains of the sensors of angular velocity and linear accelerations. Isolated in the space of parameters of stability and oscillatory. Given the author's conclusion formulas for gradients of direct quality criteria - and rise time overshoot. Built fields antigradient and the level lines of the criteria. The analysis of the properties of contramonotonicity all of the criteria specified parameters. In accordance with the claims put forward by tradeoff line in the space of parameters and displaying them in the form of lines of Pareto on space criteria. The use of traditional means of sensing space parameters showed the reliability of the obtained analytical manner. The calculation results for the synthesis of double-circuit motion control systems of flying devices can be used for selection of possible directions of improvement of conflicting criteria. The proposed method is able to replace traditional methods of synthesis of the systems under consideration on the

  3. Method of reliability allocation based on fault tree analysis and fuzzy math in nuclear power plants

    International Nuclear Information System (INIS)

    Chen Zhaobing; Deng Jian; Cao Xuewu

    2005-01-01

    Reliability allocation is a kind of a difficult multi-objective optimization problem. It can not only be applied to determine the reliability characteristic of reactor systems, subsystem and main components but also be performed to improve the design, operation and maintenance of nuclear plants. The fuzzy math known as one of the powerful tools for fuzzy optimization and the fault analysis deemed to be one of the effective methods of reliability analysis can be applied to the reliability allocation model so as to work out the problems of fuzzy characteristic of some factors and subsystem's choice respectively in this paper. Thus we develop a failure rate allocation model on the basis of the fault tree analysis and fuzzy math. For the choice of the reliability constraint factors, we choose the six important ones according to practical need for conducting the reliability allocation. The subsystem selected by the top-level fault tree analysis is to avoid allocating reliability for all the equipment and components including the unnecessary parts. During the reliability process, some factors can be calculated or measured quantitatively while others only can be assessed qualitatively by the expert rating method. So we adopt fuzzy decision and dualistic contrast to realize the reliability allocation with the help of fault tree analysis. Finally the example of the emergency diesel generator's reliability allocation is used to illustrate reliability allocation model and improve this model simple and applicable. (authors)

  4. Procedures for treating common cause failures in safety and reliability studies: Volume 2, Analytic background and techniques: Final report

    International Nuclear Information System (INIS)

    Mosleh, A.; Fleming, K.N.; Parry, G.W.; Paula, H.M.; Worledge, D.H.; Rasmuson, D.M.

    1988-12-01

    This report presents a framework for the inclusion of the impact of common cause failures in risk and reliability evaluations. Common cause failures are defined as that subset of dependent failures for which causes are not explicitly included in the logic model as basic events. The emphasis here is on providing procedures for a practical, systematic approach that can be used to perform and clearly document the analysis. The framework and the methods discussed for performing the different stages of the analysis integrate insights obtained from engineering assessments of the system and the historical evidence from multiple failure events into a systematic, reproducible, and defensible analysis. This document, Volume 2, contains a series of appendices that provide additional background and methodological detail on several important topics discussed in Volume 1

  5. Calibration Methods for Reliability-Based Design Codes

    DEFF Research Database (Denmark)

    Gayton, N.; Mohamed, A.; Sørensen, John Dalsgaard

    2004-01-01

    The calibration methods are applied to define the optimal code format according to some target safety levels. The calibration procedure can be seen as a specific optimization process where the control variables are the partial factors of the code. Different methods are available in the literature...

  6. Rapid and Reliable HPLC Method for the Determination of Vitamin ...

    African Journals Online (AJOL)

    Purpose: To develop and validate an accurate, sensitive and reproducible high performance liquid chromatographic (HPLC) method for the quantitation of vitamin C in pharmaceutical samples. Method: The drug and the standard were eluted from Superspher RP-18 (250 mm x 4.6 mm, 10ìm particle size) at 20 0C.

  7. Evaluation and reliability of bone histological age estimation methods

    African Journals Online (AJOL)

    Human age estimation at death plays a vital role in forensic anthropology and bioarchaeology. Researchers used morphological and histological methods to estimate human age from their skeletal remains. This paper discussed different histological methods that used human long bones and ribs to determine age ...

  8. Method matters: Understanding diagnostic reliability in DSM-IV and DSM-5.

    Science.gov (United States)

    Chmielewski, Michael; Clark, Lee Anna; Bagby, R Michael; Watson, David

    2015-08-01

    Diagnostic reliability is essential for the science and practice of psychology, in part because reliability is necessary for validity. Recently, the DSM-5 field trials documented lower diagnostic reliability than past field trials and the general research literature, resulting in substantial criticism of the DSM-5 diagnostic criteria. Rather than indicating specific problems with DSM-5, however, the field trials may have revealed long-standing diagnostic issues that have been hidden due to a reliance on audio/video recordings for estimating reliability. We estimated the reliability of DSM-IV diagnoses using both the standard audio-recording method and the test-retest method used in the DSM-5 field trials, in which different clinicians conduct separate interviews. Psychiatric patients (N = 339) were diagnosed using the SCID-I/P; 218 were diagnosed a second time by an independent interviewer. Diagnostic reliability using the audio-recording method (N = 49) was "good" to "excellent" (M κ = .80) and comparable to the DSM-IV field trials estimates. Reliability using the test-retest method (N = 218) was "poor" to "fair" (M κ = .47) and similar to DSM-5 field-trials' estimates. Despite low test-retest diagnostic reliability, self-reported symptoms were highly stable. Moreover, there was no association between change in self-report and change in diagnostic status. These results demonstrate the influence of method on estimates of diagnostic reliability. (c) 2015 APA, all rights reserved).

  9. Methods for reliability evaluation of trust and reputation systems

    Science.gov (United States)

    Janiszewski, Marek B.

    2016-09-01

    Trust and reputation systems are a systematic approach to build security on the basis of observations of node's behaviour. Exchange of node's opinions about other nodes is very useful to indicate nodes which act selfishly or maliciously. The idea behind trust and reputation systems gets significance because of the fact that conventional security measures (based on cryptography) are often not sufficient. Trust and reputation systems can be used in various types of networks such as WSN, MANET, P2P and also in e-commerce applications. Trust and reputation systems give not only benefits but also could be a thread itself. Many attacks aim at trust and reputation systems exist, but such attacks still have not gain enough attention of research teams. Moreover, joint effects of many of known attacks have been determined as a very interesting field of research. Lack of an acknowledged methodology of evaluation of trust and reputation systems is a serious problem. This paper aims at presenting various approaches of evaluation such systems. This work also contains a description of generalization of many trust and reputation systems which can be used to evaluate reliability of such systems in the context of preventing various attacks.

  10. Application of Dynamic Analysis in Semi-Analytical Finite Element Method.

    Science.gov (United States)

    Liu, Pengfei; Xing, Qinyan; Wang, Dawei; Oeser, Markus

    2017-08-30

    Analyses of dynamic responses are significantly important for the design, maintenance and rehabilitation of asphalt pavement. In order to evaluate the dynamic responses of asphalt pavement under moving loads, a specific computational program, SAFEM, was developed based on a semi-analytical finite element method. This method is three-dimensional and only requires a two-dimensional FE discretization by incorporating Fourier series in the third dimension. In this paper, the algorithm to apply the dynamic analysis to SAFEM was introduced in detail. Asphalt pavement models under moving loads were built in the SAFEM and commercial finite element software ABAQUS to verify the accuracy and efficiency of the SAFEM. The verification shows that the computational accuracy of SAFEM is high enough and its computational time is much shorter than ABAQUS. Moreover, experimental verification was carried out and the prediction derived from SAFEM is consistent with the measurement. Therefore, the SAFEM is feasible to reliably predict the dynamic response of asphalt pavement under moving loads, thus proving beneficial to road administration in assessing the pavement's state.

  11. The development of precisely analytical method for the concentrated boric acid solution in the NPP systems

    Energy Technology Data Exchange (ETDEWEB)

    Sung, G. B.; Jung, K. H.; Kang, D. W. [KEPRI, Taejon (Korea, Republic of); Park, C. S. [KEPCO, Taejon (Korea, Republic of)

    1999-05-01

    Boric acid is used for reactivity control in nuclear reactors, which frequently results in leftover boric acid. This extra boric acid is stored in boric acid storage tank after the concentration process by boric acid evaporator. Apart from this excess, highly concentrated boric acid is stored in safety-related boric acid storage tank. Accordingly, proper maintenance of these boric acid is one of the greatest safety concerns. The solubility of boric acid decreases with decreasing temperature resulting in its precipitation. Consequently, the temperature of boric acid storage tanks is maintained at high temperature. The following analysis should be also performed at the similar temperature to prevent the formation of boric acid precipitation, which is difficult to achieve affecting the accuracy of analytical results. This paper presents a new sampling and measuring technique that makes up for the difficulties mentioned above and shows several advantages including improved reliability and short analysis time. This method is based on gravimetry and dilution method and is expected to be widely used in field application.

  12. Investigation by perturbative and analytical method of electronic properties of square quantum well under electric field

    Directory of Open Access Journals (Sweden)

    Mustafa Kemal BAHAR

    2010-06-01

    Full Text Available In this study, the effects of applied electric field on the isolated square quantum well was investigated by analytic and perturbative method. The energy eigen values and wave functions in quantum well were found by perturbative method. Later, the electric field effects were investigated by analytic method, the results of perturbative and analytic method were compared. As well as both of results fit with each other, it was observed that externally applied electric field changed importantly electronic properties of the system.

  13. Research on Control Method Based on Real-Time Operational Reliability Evaluation for Space Manipulator

    Directory of Open Access Journals (Sweden)

    Yifan Wang

    2014-05-01

    Full Text Available A control method based on real-time operational reliability evaluation for space manipulator is presented for improving the success rate of a manipulator during the execution of a task. In this paper, a method for quantitative analysis of operational reliability is given when manipulator is executing a specified task; then a control model which could control the quantitative operational reliability is built. First, the control process is described by using a state space equation. Second, process parameters are estimated in real time using Bayesian method. Third, the expression of the system's real-time operational reliability is deduced based on the state space equation and process parameters which are estimated using Bayesian method. Finally, a control variable regulation strategy which considers the cost of control is given based on the Theory of Statistical Process Control. It is shown via simulations that this method effectively improves the operational reliability of space manipulator control system.

  14. Reliability research to nuclear power plant operators based on several methods

    International Nuclear Information System (INIS)

    Fang Xiang; Li Fu; Zhao Bingquan

    2009-01-01

    The paper utilizes many kinds of international reliability research methods, and summarizes the review of reliability research of Chinese nuclear power plant operators in past over ten years based on the simulator platform of nuclear power plant. The paper shows the necessity and feasibility of the research to nuclear power plant operators from many angles including human cognition reliability, fuzzy mathematics model and psychological research model, etc. It will be good to the safe operation of nuclear power plant based on many kinds of research methods to the reliability research of nuclear power plant operators. (authors)

  15. Comparison of Methods for Dependency Determination between Human Failure Events within Human Reliability Analysis

    International Nuclear Information System (INIS)

    Cepin, M.

    2008-01-01

    The human reliability analysis (HRA) is a highly subjective evaluation of human performance, which is an input for probabilistic safety assessment, which deals with many parameters of high uncertainty. The objective of this paper is to show that subjectivism can have a large impact on human reliability results and consequently on probabilistic safety assessment results and applications. The objective is to identify the key features, which may decrease subjectivity of human reliability analysis. Human reliability methods are compared with focus on dependency comparison between Institute Jozef Stefan human reliability analysis (IJS-HRA) and standardized plant analysis risk human reliability analysis (SPAR-H). Results show large differences in the calculated human error probabilities for the same events within the same probabilistic safety assessment, which are the consequence of subjectivity. The subjectivity can be reduced by development of more detailed guidelines for human reliability analysis with many practical examples for all steps of the process of evaluation of human performance

  16. Comparison of methods for dependency determination between human failure events within human reliability analysis

    International Nuclear Information System (INIS)

    Cepis, M.

    2007-01-01

    The Human Reliability Analysis (HRA) is a highly subjective evaluation of human performance, which is an input for probabilistic safety assessment, which deals with many parameters of high uncertainty. The objective of this paper is to show that subjectivism can have a large impact on human reliability results and consequently on probabilistic safety assessment results and applications. The objective is to identify the key features, which may decrease of subjectivity of human reliability analysis. Human reliability methods are compared with focus on dependency comparison between Institute Jozef Stefan - Human Reliability Analysis (IJS-HRA) and Standardized Plant Analysis Risk Human Reliability Analysis (SPAR-H). Results show large differences in the calculated human error probabilities for the same events within the same probabilistic safety assessment, which are the consequence of subjectivity. The subjectivity can be reduced by development of more detailed guidelines for human reliability analysis with many practical examples for all steps of the process of evaluation of human performance. (author)

  17. A new, rapid and reliable method for the determination of reduced sulphur (S2-) species in natural water discharges

    International Nuclear Information System (INIS)

    Montegrossi, Giordano; Tassi, Franco; Vaselli, Orlando; Bidini, Eva; Minissale, Angelo

    2006-01-01

    The determination of reduced S species in natural waters is particularly difficult due to their high instability and chemical and physical interferences in the current analytical methods. In this paper a new, rapid and reliable analytical procedure is presented, named the Cd-IC method, for their determination as ΣS 2- via oxidation to SO 4 2- after chemical trapping with an ammonia-cadmium solution that allows precipitation of all the reduced S species as CdS. The S 2- -SO 4 is analysed by ion-chromatography. The main advantages of this method are: low cost, high stability of CdS precipitate, absence of interferences, low detection limit (0.01mg/L as SO 4 for 10mL of water) and low analytical error (about 5%). The proposed method has been applied to more than 100 water samples from different natural systems (water discharges and cold wells from volcanic and geothermal areas, crater lakes) in central-southern Italy

  18. A handbook of decomposition methods in analytical chemistry

    International Nuclear Information System (INIS)

    Bok, R.

    1984-01-01

    Decomposition methods of metals, alloys, fluxes, slags, calcine, inorganic salts, oxides, nitrides, carbides, borides, sulfides, ores, minerals, rocks, concentrates, glasses, ceramics, organic substances, polymers, phyto- and biological materials from the viewpoint of sample preparation for analysis have been described. The methods are systemitized according to decomposition principle: thermal with the use of electricity, irradiation, dissolution with participation of chemical reactions and without it. Special equipment for different decomposition methods is described. Bibliography contains 3420 references

  19. [A reliability growth assessment method and its application in the development of equipment in space cabin].

    Science.gov (United States)

    Chen, J D; Sun, H L

    1999-04-01

    Objective. To assess and predict reliability of an equipment dynamically by making full use of various test informations in the development of products. Method. A new reliability growth assessment method based on army material system analysis activity (AMSAA) model was developed. The method is composed of the AMSAA model and test data conversion technology. Result. The assessment and prediction results of a space-borne equipment conform to its expectations. Conclusion. It is suggested that this method should be further researched and popularized.

  20. Description of JNC's analytical method and its performance for FBR cores

    International Nuclear Information System (INIS)

    Ishikawa, M.

    2000-01-01

    The description of JNC's analytical method and its performance for FBR cores includes: an outline of JNC's Analytical System Compared with ERANOS; a standard data base for FBR Nuclear Design in JNC; JUPITER Critical Experiment; details of Analytical Method and Its Effects on JUPITER; performance of JNC Analytical System (effective multiplication factor k eff , control rod worth, and sodium void reactivity); design accuracy of a 600 MWe-class FBR Core. JNC developed a consistent analytical system for FBR core evaluation, based on JENDL library, f-table method, and three dimensional diffusion/transport theory, which includes comprehensive sensitivity tools to improve the prediction accuracy of core parameters. JNC system was verified by analysis of JUPITER critical experiment, and other facilities. Its performance can be judged quite satisfactory for FBR-core design work, though there is room for further improvement, such as more detailed treatment of cross-section resonance regions

  1. Application of an analytical method for solution of thermal hydraulic conservation equations

    Energy Technology Data Exchange (ETDEWEB)

    Fakory, M.R. [Simulation, Systems & Services Technologies Company (S3 Technologies), Columbia, MD (United States)

    1995-09-01

    An analytical method has been developed and applied for solution of two-phase flow conservation equations. The test results for application of the model for simulation of BWR transients are presented and compared with the results obtained from application of the explicit method for integration of conservation equations. The test results show that with application of the analytical method for integration of conservation equations, the Courant limitation associated with explicit Euler method of integration was eliminated. The results obtained from application of the analytical method (with large time steps) agreed well with the results obtained from application of explicit method of integration (with time steps smaller than the size imposed by Courant limitation). The results demonstrate that application of the analytical approach significantly improves the numerical stability and computational efficiency.

  2. Reliable method for fission source convergence of Monte Carlo criticality calculation with Wielandt's method

    International Nuclear Information System (INIS)

    Yamamoto, Toshihiro; Miyoshi, Yoshinori

    2004-01-01

    A new algorithm of Monte Carlo criticality calculations for implementing Wielandt's method, which is one of acceleration techniques for deterministic source iteration methods, is developed, and the algorithm can be successfully implemented into MCNP code. In this algorithm, part of fission neutrons emitted during random walk processes are tracked within the current cycle, and thus a fission source distribution used in the next cycle spread more widely. Applying this method intensifies a neutron interaction effect even in a loosely-coupled array where conventional Monte Carlo criticality methods have difficulties, and a converged fission source distribution can be obtained with fewer cycles. Computing time spent for one cycle, however, increases because of tracking fission neutrons within the current cycle, which eventually results in an increase of total computing time up to convergence. In addition, statistical fluctuations of a fission source distribution in a cycle are worsened by applying Wielandt's method to Monte Carlo criticality calculations. However, since a fission source convergence is attained with fewer source iterations, a reliable determination of convergence can easily be made even in a system with a slow convergence. This acceleration method is expected to contribute to prevention of incorrect Monte Carlo criticality calculations. (author)

  3. An Analytical Method for Measuring Competence in Project Management

    Science.gov (United States)

    González-Marcos, Ana; Alba-Elías, Fernando; Ordieres-Meré, Joaquín

    2016-01-01

    The goal of this paper is to present a competence assessment method in project management that is based on participants' performance and value creation. It seeks to close an existing gap in competence assessment in higher education. The proposed method relies on information and communication technology (ICT) tools and combines Project Management…

  4. A New Method of Reliability Evaluation Based on Wavelet Information Entropy for Equipment Condition Identification

    International Nuclear Information System (INIS)

    He, Z J; Zhang, X L; Chen, X F

    2012-01-01

    Aiming at reliability evaluation of condition identification of mechanical equipment, it is necessary to analyze condition monitoring information. A new method of reliability evaluation based on wavelet information entropy extracted from vibration signals of mechanical equipment is proposed. The method is quite different from traditional reliability evaluation models that are dependent on probability statistics analysis of large number sample data. The vibration signals of mechanical equipment were analyzed by means of second generation wavelet package (SGWP). We take relative energy in each frequency band of decomposed signal that equals a percentage of the whole signal energy as probability. Normalized information entropy (IE) is obtained based on the relative energy to describe uncertainty of a system instead of probability. The reliability degree is transformed by the normalized wavelet information entropy. A successful application has been achieved to evaluate the assembled quality reliability for a kind of dismountable disk-drum aero-engine. The reliability degree indicates the assembled quality satisfactorily.

  5. Integrated Markov-neural reliability computation method: A case for multiple automated guided vehicle system

    International Nuclear Information System (INIS)

    Fazlollahtabar, Hamed; Saidi-Mehrabad, Mohammad; Balakrishnan, Jaydeep

    2015-01-01

    This paper proposes an integrated Markovian and back propagation neural network approaches to compute reliability of a system. While states of failure occurrences are significant elements for accurate reliability computation, Markovian based reliability assessment method is designed. Due to drawbacks shown by Markovian model for steady state reliability computations and neural network for initial training pattern, integration being called Markov-neural is developed and evaluated. To show efficiency of the proposed approach comparative analyses are performed. Also, for managerial implication purpose an application case for multiple automated guided vehicles (AGVs) in manufacturing networks is conducted. - Highlights: • Integrated Markovian and back propagation neural network approach to compute reliability. • Markovian based reliability assessment method. • Managerial implication is shown in an application case for multiple automated guided vehicles (AGVs) in manufacturing networks

  6. Tank 48H Waste Composition and Results of Investigation of Analytical Methods

    Energy Technology Data Exchange (ETDEWEB)

    Walker , D.D. [Westinghouse Savannah River Company, AIKEN, SC (United States)

    1997-04-02

    This report serves two purposes. First, it documents the analytical results of Tank 48H samples taken between April and August 1996. Second, it describes investigations of the precision of the sampling and analytical methods used on the Tank 48H samples.

  7. A sample preparation method for recovering suppressed analyte ions in MALDI TOF MS

    NARCIS (Netherlands)

    Lou, X.; Waal, de B.F.M.; Milroy, L.G.; Dongen, van J.L.J.

    2015-01-01

    In matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI TOF MS), analyte signals can be substantially suppressed by other compounds in the sample. In this technical note, we describe a modified thin-layer sample preparation method that significantly reduces the analyte

  8. Assessment of modern methods of human factor reliability analysis in PSA studies

    International Nuclear Information System (INIS)

    Holy, J.

    2001-12-01

    The report is structured as follows: Classical terms and objects (Probabilistic safety assessment as a framework for human reliability assessment; Human failure within the PSA model; Basic types of operator failure modelled in a PSA study and analyzed by HRA methods; Qualitative analysis of human reliability; Quantitative analysis of human reliability used; Process of analysis of nuclear reactor operator reliability in a PSA study); New terms and objects (Analysis of dependences; Errors of omission; Errors of commission; Error forcing context); and Overview and brief assessment of human reliability analysis (Basic characteristics of the methods; Assets and drawbacks of the use of each of HRA method; History and prospects of the use of the methods). (P.A.)

  9. Reliable computation of roots in analytical waveguide modeling using an interval-Newton approach and algorithmic differentiation.

    Science.gov (United States)

    Bause, Fabian; Walther, Andrea; Rautenberg, Jens; Henning, Bernd

    2013-12-01

    For the modeling and simulation of wave propagation in geometrically simple waveguides such as plates or rods, one may employ the analytical global matrix method. That is, a certain (global) matrix depending on the two parameters wavenumber and frequency is built. Subsequently, one must calculate all parameter pairs within the domain of interest where the global matrix becomes singular. For this purpose, one could compute all roots of the determinant of the global matrix when the two parameters vary in the given intervals. This requirement to calculate all roots is actually the method's most concerning restriction. Previous approaches are based on so-called mode-tracers, which use the physical phenomenon that solutions, i.e., roots of the determinant of the global matrix, appear in a certain pattern, the waveguide modes, to limit the root-finding algorithm's search space with respect to consecutive solutions. In some cases, these reductions of the search space yield only an incomplete set of solutions, because some roots may be missed as a result of uncertain predictions. Therefore, we propose replacement of the mode-tracer approach with a suitable version of an interval- Newton method. To apply this interval-based method, we extended the interval and derivative computation provided by a numerical computing environment such that corresponding information is also available for Bessel functions used in circular models of acoustic waveguides. We present numerical results for two different scenarios. First, a polymeric cylindrical waveguide is simulated, and second, we show simulation results of a one-sided fluid-loaded plate. For both scenarios, we compare results obtained with the proposed interval-Newton algorithm and commercial software.

  10. Downstream processing and chromatography based analytical methods for production of vaccines, gene therapy vectors, and bacteriophages

    Science.gov (United States)

    Kramberger, Petra; Urbas, Lidija; Štrancar, Aleš

    2015-01-01

    Downstream processing of nanoplexes (viruses, virus-like particles, bacteriophages) is characterized by complexity of the starting material, number of purification methods to choose from, regulations that are setting the frame for the final product and analytical methods for upstream and downstream monitoring. This review gives an overview on the nanoplex downstream challenges and chromatography based analytical methods for efficient monitoring of the nanoplex production. PMID:25751122

  11. Study of Fuze Structure and Reliability Design Based on the Direct Search Method

    Science.gov (United States)

    Lin, Zhang; Ning, Wang

    2017-03-01

    Redundant design is one of the important methods to improve the reliability of the system, but mutual coupling of multiple factors is often involved in the design. In my study, Direct Search Method is introduced into the optimum redundancy configuration for design optimization, in which, the reliability, cost, structural weight and other factors can be taken into account simultaneously, and the redundant allocation and reliability design of aircraft critical system are computed. The results show that this method is convenient and workable, and applicable to the redundancy configurations and optimization of various designs upon appropriate modifications. And this method has a good practical value.

  12. Application of reliability analysis methods to the comparison of two safety circuits

    International Nuclear Information System (INIS)

    Signoret, J.-P.

    1975-01-01

    Two circuits of different design, intended for assuming the ''Low Pressure Safety Injection'' function in PWR reactors are analyzed using reliability methods. The reliability analysis of these circuits allows the failure trees to be established and the failure probability derived. The dependence of these results on test use and maintenance is emphasized as well as critical paths. The great number of results obtained may allow a well-informed choice taking account of the reliability wanted for the type of circuits [fr

  13. The Language Teaching Methods Scale: Reliability and Validity Studies

    Science.gov (United States)

    Okmen, Burcu; Kilic, Abdurrahman

    2016-01-01

    The aim of this research is to develop a scale to determine the language teaching methods used by English teachers. The research sample consisted of 300 English teachers who taught at Duzce University and in primary schools, secondary schools and high schools in the Provincial Management of National Education in the city of Duzce in 2013-2014…

  14. A method to determine validity and reliability of activity sensors

    NARCIS (Netherlands)

    Boerema, Simone Theresa; Hermens, Hermanus J.

    2013-01-01

    METHOD Four sensors were securely fastened to a mechanical oscillator (Vibration Exciter, type 4809, Brüel & Kjær) and moved at various frequencies (6.67Hz; 13.45Hz; 19.88Hz) within the range of human physical activity. For each of the three sensor axes, the sensors were simultaneously moved for

  15. Reliability and Validity of the Research Methods Skills Assessment

    Science.gov (United States)

    Smith, Tamarah; Smith, Samantha

    2018-01-01

    The Research Methods Skills Assessment (RMSA) was created to measure psychology majors' statistics knowledge and skills. The American Psychological Association's Guidelines for the Undergraduate Major in Psychology (APA, 2007, 2013) served as a framework for development. Results from a Rasch analysis with data from n = 330 undergraduates showed…

  16. A platform analytical quality by design (AQbD) approach for multiple UHPLC-UV and UHPLC-MS methods development for protein analysis.

    Science.gov (United States)

    Kochling, Jianmei; Wu, Wei; Hua, Yimin; Guan, Qian; Castaneda-Merced, Juan

    2016-06-05

    A platform analytical quality by design approach for methods development is presented in this paper. This approach is not limited just to method development following the same logical Analytical quality by design (AQbD) process, it is also exploited across a range of applications in methods development with commonality in equipment and procedures. As demonstrated by the development process of 3 methods, the systematic approach strategy offers a thorough understanding of the method scientific strength. The knowledge gained from the UHPLC-UV peptide mapping method can be easily transferred to the UHPLC-MS oxidation method and the UHPLC-UV C-terminal heterogeneity methods of the same protein. In addition, the platform AQbD method development strategy ensures method robustness is built in during development. In early phases, a good method can generate reliable data for product development allowing confident decision making. Methods generated following the AQbD approach have great potential for avoiding extensive post-approval analytical method change. While in the commercial phase, high quality data ensures timely data release, reduced regulatory risk, and lowered lab operational cost. Moreover, large, reliable database and knowledge gained during AQbD method development provide strong justifications during regulatory filling for the selection of important parameters or parameter change needs for method validation, and help to justify for removal of unnecessary tests used for product specifications. Copyright © 2016 Elsevier B.V. All rights reserved.

  17. EVALUATION OF ANALYTICAL METHODS FOR DETERMINING PESTICIDES IN BABY FOOD

    Science.gov (United States)

    Three extraction methods and two detection techniques for determining pesticides in baby food were evaluated. The extraction techniques examined were supercritical fluid extraction (SFE), enhanced solvent extraction (ESE), and solid phase extraction (SPE). The detection techni...

  18. Development of Analytical Method for Detection of Some ...

    African Journals Online (AJOL)

    All rights reserved. ... 3Centre for Water Research and Analysis (ALIR), Faculty of Science and Technology, Universiti Kebangsaan (UKM), ... Purpose: To develop and validate a simple method using solid – phase extraction along with liquid.

  19. Analytical methods for measuring 10Be in marine sediments

    International Nuclear Information System (INIS)

    Graham, I.J.; Ditchburn, R.G.; Sparks, R.J.; Whitehead, N.E.

    1995-01-01

    A suite of marine sediments from the Wanganui Basin (Graham et al. 1995) has provided excellent material to further develop methods for 10 Be analysis at the Institute of Geological and Nuclear Sciences AMS facility. Chemical methods for Be extraction have been streamlined and there has been some reduction of backgrounds and contamination peaks for 1 0Be isotopic analysis. (authors) 12 refs., 5 figs., 1 tab

  20. Reliability and validity of non-radiographic methods of thoracic kyphosis measurement: a systematic review.

    Science.gov (United States)

    Barrett, Eva; McCreesh, Karen; Lewis, Jeremy

    2014-02-01

    A wide array of instruments are available for non-invasive thoracic kyphosis measurement. Guidelines for selecting outcome measures for use in clinical and research practice recommend that properties such as validity and reliability are considered. This systematic review reports on the reliability and validity of non-invasive methods for measuring thoracic kyphosis. A systematic search of 11 electronic databases located studies assessing reliability and/or validity of non-invasive thoracic kyphosis measurement techniques. Two independent reviewers used a critical appraisal tool to assess the quality of retrieved studies. Data was extracted by the primary reviewer. The results were synthesized qualitatively using a level of evidence approach. 27 studies satisfied the eligibility criteria and were included in the review. The reliability, validity and both reliability and validity were investigated by sixteen, two and nine studies respectively. 17/27 studies were deemed to be of high quality. In total, 15 methods of thoracic kyphosis were evaluated in retrieved studies. All investigated methods showed high (ICC ≥ .7) to very high (ICC ≥ .9) levels of reliability. The validity of the methods ranged from low to very high. The strongest levels of evidence for reliability exists in support of the Debrunner kyphometer, Spinal Mouse and Flexicurve index, and for validity supports the arcometer and Flexicurve index. Further reliability and validity studies are required to strengthen the level of evidence for the remaining methods of measurement. This should be addressed by future research. Copyright © 2013 Elsevier Ltd. All rights reserved.

  1. A Generalized Pivotal Quantity Approach to Analytical Method Validation Based on Total Error.

    Science.gov (United States)

    Yang, Harry; Zhang, Jianchun

    2015-01-01

    The primary purpose of method validation is to demonstrate that the method is fit for its intended use. Traditionally, an analytical method is deemed valid if its performance characteristics such as accuracy and precision are shown to meet prespecified acceptance criteria. However, these acceptance criteria are not directly related to the method's intended purpose, which is usually a gurantee that a high percentage of the test results of future samples will be close to their true values. Alternate "fit for purpose" acceptance criteria based on the concept of total error have been increasingly used. Such criteria allow for assessing method validity, taking into account the relationship between accuracy and precision. Although several statistical test methods have been proposed in literature to test the "fit for purpose" hypothesis, the majority of the methods are not designed to protect the risk of accepting unsuitable methods, thus having the potential to cause uncontrolled consumer's risk. In this paper, we propose a test method based on generalized pivotal quantity inference. Through simulation studies, the performance of the method is compared to five existing approaches. The results show that both the new method and the method based on β-content tolerance interval with a confidence level of 90%, hereafter referred to as the β-content (0.9) method, control Type I error and thus consumer's risk, while the other existing methods do not. It is further demonstrated that the generalized pivotal quantity method is less conservative than the β-content (0.9) method when the analytical methods are biased, whereas it is more conservative when the analytical methods are unbiased. Therefore, selection of either the generalized pivotal quantity or β-content (0.9) method for an analytical method validation depends on the accuracy of the analytical method. It is also shown that the generalized pivotal quantity method has better asymptotic properties than all of the current

  2. Radioisotope method potentialities in machine reliability and durability enhancement

    International Nuclear Information System (INIS)

    Postnikov, V.I.

    1975-01-01

    The development of a surface activation method is reviewed with regard to wear of machine parts. Examples demonstrating the highly promising aspects and practical application of the method are cited. The use of high-sensitivity instruments and variation of activation depth from 10 um to 0.5 mm allows to perform the investigations at a sensitivity of 0.05 um and to estimate the linear values of machine wear. Standard diagrams are presented for measuring the wear of different machine parts by means of surface activation. Investigations performed at several Soviet technological institutes afford a set of dependences, which characterize the distribution of radioactive isotopes in depth under different conditions of activation of diverse metals and alloys and permit to study the wear of any metal

  3. TESTING METHODS FOR MECHANICALLY IMPROVED SOILS: RELIABILITY AND VALIDITY

    Directory of Open Access Journals (Sweden)

    Ana Petkovšek

    2017-10-01

    Full Text Available A possibility of in-situ mechanical improvement for reducing the liquefaction potential of silty sands was investigated by using three different techniques: Vibratory Roller Compaction, Rapid Impact Compaction (RIC and Soil Mixing. Material properties at all test sites were investigated before and after improvement with the laboratory and the in situ tests (CPT, SDMT, DPSH B, static and dynamic load plate test, geohydraulic tests. Correlation between the results obtained by different test methods gave inconclusive answers.

  4. reliability reliability

    African Journals Online (AJOL)

    eobe

    Corresponding author, Tel: +234-703. RELIABILITY .... V , , given by the code of practice. However, checks must .... an optimization procedure over the failure domain F corresponding .... of Concrete Members based on Utility Theory,. Technical ...

  5. Reliability and validity of the AutoCAD software method in lumbar lordosis measurement.

    Science.gov (United States)

    Letafatkar, Amir; Amirsasan, Ramin; Abdolvahabi, Zahra; Hadadnezhad, Malihe

    2011-12-01

    The aim of this study was to determine the reliability and validity of the AutoCAD software method in lumbar lordosis measurement. Fifty healthy volunteers with a mean age of 23 ± 1.80 years were enrolled. A lumbar lateral radiograph was taken on all participants, and the lordosis was measured according to the Cobb method. Afterward, the lumbar lordosis degree was measured via AutoCAD software and flexible ruler methods. The current study is accomplished in 2 parts: intratester and intertester evaluations of reliability as well as the validity of the flexible ruler and software methods. Based on the intraclass correlation coefficient, AutoCAD's reliability and validity in measuring lumbar lordosis were 0.984 and 0.962, respectively. AutoCAD showed to be a reliable and valid method to measure lordosis. It is suggested that this method may replace those that are costly and involve health risks, such as radiography, in evaluating lumbar lordosis.

  6. Optimal analytic method for the nonlinear Hasegawa-Mima equation

    Science.gov (United States)

    Baxter, Mathew; Van Gorder, Robert A.; Vajravelu, Kuppalapalle

    2014-05-01

    The Hasegawa-Mima equation is a nonlinear partial differential equation that describes the electric potential due to a drift wave in a plasma. In the present paper, we apply the method of homotopy analysis to a slightly more general Hasegawa-Mima equation, which accounts for hyper-viscous damping or viscous dissipation. First, we outline the method for the general initial/boundary value problem over a compact rectangular spatial domain. We use a two-stage method, where both the convergence control parameter and the auxiliary linear operator are optimally selected to minimize the residual error due to the approximation. To do the latter, we consider a family of operators parameterized by a constant which gives the decay rate of the solutions. After outlining the general method, we consider a number of concrete examples in order to demonstrate the utility of this approach. The results enable us to study properties of the initial/boundary value problem for the generalized Hasegawa-Mima equation. In several cases considered, we are able to obtain solutions with extremely small residual errors after relatively few iterations are computed (residual errors on the order of 10-15 are found in multiple cases after only three iterations). The results demonstrate that selecting a parameterized auxiliary linear operator can be extremely useful for minimizing residual errors when used concurrently with the optimal homotopy analysis method, suggesting that this approach can prove useful for a number of nonlinear partial differential equations arising in physics and nonlinear mechanics.

  7. Analytical methods for quantitative evaluation of the radiocardiagram

    Energy Technology Data Exchange (ETDEWEB)

    Wolberg, J R [Technion-Israel Inst. of Tech., Haifa; Freedman, G S [Yale Univ., New Haven, Conn. (USA). School of Medicine; Dwyer, A [St. Raphael Hospital, New Haven, Conn., U.S.A.

    1975-01-01

    Radiocardiagrams are obtained by monitoring a radioisotope after injection as it passes through the heart and lungs. The purpose of this paper is to discuss several methods used to evaluate cardiac performance from radiocardiagram data. Mathematical models are developed for extracting two parameters of interest to cardiologists: cardiac chamber flow to volume ratio (F/V) and left ventricle ejection fraction (E.F.). The model used to characterize F/V is continuous and provides good agreement with data obtained by other physiological methods for the right heart. A discrete model is used to characterize the left heart and obtain E.F. Comparison has been made with other methods for obtaining E.F. for twelve patients with various types of cardiac disease. An important aspect of the E.F. model is that background interference is taken into consideration. The analyses include calculations of the statistical uncertainties associated with the computed values of both parameters.

  8. Fast analytical method for the addition of random variables

    International Nuclear Information System (INIS)

    Senna, V.; Milidiu, R.L.; Fleming, P.V.; Salles, M.R.; Oliveria, L.F.S.

    1983-01-01

    Using the minimal cut sets representation of a fault tree, a new approach to the method of moments is proposed in order to estimate confidence bounds to the top event probability. The method utilizes two or three moments either to fit a distribution (the normal and lognormal families) or to evaluate bounds from standard inequalities (e.g. Markov, Tchebycheff, etc.) Examples indicate that the results obtained by the log-normal family are in good agreement with those obtained by Monte Carlo simulation

  9. Reliability Evaluation of Bridges Based on Nonprobabilistic Response Surface Limit Method

    OpenAIRE

    Chen, Xuyong; Chen, Qian; Bian, Xiaoya; Fan, Jianping

    2017-01-01

    Due to many uncertainties in nonprobabilistic reliability assessment of bridges, the limit state function is generally unknown. The traditional nonprobabilistic response surface method is a lengthy and oscillating iteration process and leads to difficultly solving the nonprobabilistic reliability index. This article proposes a nonprobabilistic response surface limit method based on the interval model. The intention of this method is to solve the upper and lower limits of the nonprobabilistic ...

  10. Reliable screening of various foodstuffs with respect to their irradiation status: A comparative study of different analytical techniques

    International Nuclear Information System (INIS)

    Ahn, Jae-Jun; Akram, Kashif; Kwak, Ji-Young; Jeong, Mi-Seon; Kwon, Joong-Ho

    2013-01-01

    Cost-effective and time-efficient analytical techniques are required to screen large food lots in accordance to their irradiation status. Gamma-irradiated (0–10 kGy) cinnamon, red pepper, black pepper, and fresh paprika were investigated using photostimulated luminescence (PSL), direct epifluorescent filter technique/the aerobic plate count (DEFT/APC), and electronic-nose (e-nose) analyses. The screening results were also confirmed with thermoluminescence analysis. PSL analysis discriminated between irradiated (positive, >5000 PCs) and non-irradiated (negative, <700 PCs) cinnamon and red peppers. Black pepper had intermediate results (700–5000 PCs), while paprika had low sensitivity (negative results) upon irradiation. The DEFT/APC technique also showed clear screening results through the changes in microbial profiles, where the best results were found in paprika, followed by red pepper and cinnamon. E-nose analysis showed a dose-dependent discrimination in volatile profiles upon irradiation through principal component analysis. These methods can be used considering their potential applications for the screening analysis of irradiated foods. - Highlights: • Detection of irradiated food is important to enforce the applied regulations. • Gamma-irradiated spices were investigated to confirm their irradiation status. • Screening techniques such as PSL, DEFT/APC, and E-nose were tested. • Specificity and potential applications of screening techniques were evaluated. • The screening results were confirmed by promising thermoluminescence technique

  11. An Analytical framework of social learning facilitated by participatory methods

    NARCIS (Netherlands)

    Scholz, G.; Dewulf, A.; Pahl-Wostl, C.

    2014-01-01

    Social learning among different stakeholders is often a goal in problem solving contexts such as environmental management. Participatory methods (e.g., group model-building and role playing games) are frequently assumed to stimulate social learning. Yet understanding if and why this assumption is

  12. Analytic Method for Pressure Recovery in Truncated Diffusers ...

    African Journals Online (AJOL)

    A prediction method is presented for the static pressure recovery in subsonic axisymmetric truncated conical diffusers. In the analysis, a turbulent boundary layer is assumed at the diffuser inlet and a potential core exists throughout the flow. When flow separation occurs, this approach cannot be used to predict the maximum ...

  13. Analytic method for solitary solutions of some partial differential equations

    Energy Technology Data Exchange (ETDEWEB)

    Ugurlu, Yavuz [Firat University, Department of Mathematics, 23119 Elazig (Turkey); Kaya, Dogan [Firat University, Department of Mathematics, 23119 Elazig (Turkey)], E-mail: dkaya@firat.edu.tr

    2007-10-22

    In this Letter by considering an improved tanh function method, we found some exact solutions of the clannish random walker's parabolic equation, the modified Korteweg-de Vries (KdV) equation, and the Sharma-Tasso-Olver (STO) equation with its fission and fusion, the Jaulent-Miodek equation.

  14. Analytic method for solitary solutions of some partial differential equations

    International Nuclear Information System (INIS)

    Ugurlu, Yavuz; Kaya, Dogan

    2007-01-01

    In this Letter by considering an improved tanh function method, we found some exact solutions of the clannish random walker's parabolic equation, the modified Korteweg-de Vries (KdV) equation, and the Sharma-Tasso-Olver (STO) equation with its fission and fusion, the Jaulent-Miodek equation

  15. System reliability with correlated components: Accuracy of the Equivalent Planes method

    NARCIS (Netherlands)

    Roscoe, K.; Diermanse, F.; Vrouwenvelder, A.C.W.M.

    2015-01-01

    Computing system reliability when system components are correlated presents a challenge because it usually requires solving multi-fold integrals numerically, which is generally infeasible due to the computational cost. In Dutch flood defense reliability modeling, an efficient method for computing

  16. System reliability with correlated components : Accuracy of the Equivalent Planes method

    NARCIS (Netherlands)

    Roscoe, K.; Diermanse, F.; Vrouwenvelder, T.

    2015-01-01

    Computing system reliability when system components are correlated presents a challenge because it usually requires solving multi-fold integrals numerically, which is generally infeasible due to the computational cost. In Dutch flood defense reliability modeling, an efficient method for computing

  17. Automated migration analysis based on cell texture: method & reliability

    Directory of Open Access Journals (Sweden)

    Chittenden Thomas W

    2005-03-01

    Full Text Available Abstract Background In this paper, we present and validate a way to measure automatically the extent of cell migration based on automated examination of a series of digital photographs. It was designed specifically to identify the impact of Second Hand Smoke (SHS on endothelial cell migration but has broader applications. The analysis has two stages: (1 preprocessing of image texture, and (2 migration analysis. Results The output is a graphic overlay that indicates the front lines of cell migration superimposed on each original image, with automated reporting of the distance traversed vs. time. Expert preference compares to manual placement of leading edge shows complete equivalence of automated vs. manual leading edge definition for cell migration measurement. Conclusion Our method is indistinguishable from careful manual determinations of cell front lines, with the advantages of full automation, objectivity, and speed.

  18. Approximate Analytic Solutions for the Two-Phase Stefan Problem Using the Adomian Decomposition Method

    Directory of Open Access Journals (Sweden)

    Xiao-Ying Qin

    2014-01-01

    Full Text Available An Adomian decomposition method (ADM is applied to solve a two-phase Stefan problem that describes the pure metal solidification process. In contrast to traditional analytical methods, ADM avoids complex mathematical derivations and does not require coordinate transformation for elimination of the unknown moving boundary. Based on polynomial approximations for some known and unknown boundary functions, approximate analytic solutions for the model with undetermined coefficients are obtained using ADM. Substitution of these expressions into other equations and boundary conditions of the model generates some function identities with the undetermined coefficients. By determining these coefficients, approximate analytic solutions for the model are obtained. A concrete example of the solution shows that this method can easily be implemented in MATLAB and has a fast convergence rate. This is an efficient method for finding approximate analytic solutions for the Stefan and the inverse Stefan problems.

  19. Assessment of Two Analytical Methods in Solving the Linear and Nonlinear Elastic Beam Deformation Problems

    DEFF Research Database (Denmark)

    Barari, Amin; Ganjavi, B.; Jeloudar, M. Ghanbari

    2010-01-01

    and fluid mechanics. Design/methodology/approach – Two new but powerful analytical methods, namely, He's VIM and HPM, are introduced to solve some boundary value problems in structural engineering and fluid mechanics. Findings – Analytical solutions often fit under classical perturbation methods. However......, as with other analytical techniques, certain limitations restrict the wide application of perturbation methods, most important of which is the dependence of these methods on the existence of a small parameter in the equation. Disappointingly, the majority of nonlinear problems have no small parameter at all......Purpose – In the last two decades with the rapid development of nonlinear science, there has appeared ever-increasing interest of scientists and engineers in the analytical techniques for nonlinear problems. This paper considers linear and nonlinear systems that are not only regarded as general...

  20. A new robust method for the treatment of analytical data

    International Nuclear Information System (INIS)

    Pearton, D.C.G.

    1982-01-01

    A new robust method is proposed for the calculation of the median and the relative standard deviation for a set of data containing unsymmetrically placed outliers. Examples of the advantages of the new method are given, the findings being confirmed by Monte Carlo tests. At Mintek mass-spectrometric data are often unsymmetrical, and all outliers are often at one of the extremities, either all high or all low. In some instances the outliers can be seen visually, and would therefore be rejected on sight. However, when large sets of results are processed, such as those from mass-spectrometric, X-ray fluorescence, and neutron-activation analyses, or in fields such as the assignment of values to reference materials, the sets of results are often too large for visual inspection and are processed within the computer

  1. The analytic method for calculating the control rod worth

    International Nuclear Information System (INIS)

    Kim, Han Gon; Lee, Byeong Ho; Chang, Soon Heung

    1989-01-01

    We calculated the control rod worth in this paper. To avoid complexity, we did not consider burnable poisons and soluble boron. The system was localized within one assembly. The control rod was treated as not an absorber but an another boundary. Thus all of the group constants were unchanged before and after control rod insertion. And we discussed the method for calculation of the reactivity of the whole core

  2. Analytical methods applied to diverse types of Brazilian propolis

    Directory of Open Access Journals (Sweden)

    Marcucci Maria

    2011-06-01

    Full Text Available Abstract Propolis is a bee product, composed mainly of plant resins and beeswax, therefore its chemical composition varies due to the geographic and plant origins of these resins, as well as the species of bee. Brazil is an important supplier of propolis on the world market and, although green colored propolis from the southeast is the most known and studied, several other types of propolis from Apis mellifera and native stingless bees (also called cerumen can be found. Propolis is usually consumed as an extract, so the type of solvent and extractive procedures employed further affect its composition. Methods used for the extraction; analysis the percentage of resins, wax and insoluble material in crude propolis; determination of phenolic, flavonoid, amino acid and heavy metal contents are reviewed herein. Different chromatographic methods applied to the separation, identification and quantification of Brazilian propolis components and their relative strengths are discussed; as well as direct insertion mass spectrometry fingerprinting. Propolis has been used as a popular remedy for several centuries for a wide array of ailments. Its antimicrobial properties, present in propolis from different origins, have been extensively studied. But, more recently, anti-parasitic, anti-viral/immune stimulating, healing, anti-tumor, anti-inflammatory, antioxidant and analgesic activities of diverse types of Brazilian propolis have been evaluated. The most common methods employed and overviews of their relative results are presented.

  3. Survey of analytical methods for environmental monitoring of krypton-85

    International Nuclear Information System (INIS)

    Jaquish, R.E.; Moghissi, A.A.

    1973-01-01

    Numerous methods have been developed for measuring krypton-85 in air as krypton ultimately accumulates in air once it is released into the environment. However, krypton-85 can be present in other media such as natural gas from wells stimulated with nuclear devices or in water when krypton-85 is used for aeration studies. Methods for the measurement of ambient levels of krypton-85 require a concentration of krypton from a large air sample of one m 3 or more. If elevated levels are to be measured, carrier krypton may be used provided the contamination of atmospheric krypton with krypton-85 does not interfere with the measurement. In certain cases, such as in the vicinity of nuclear fuel processing plants, direct measurement techniques may be used. A variety of techniques are employed for krypton-85 counting. At low levels, internal gas counting or organic scintillation is used to measure the beta emission of this radionuclide. At higher levels the gamma emission of krypton-85 may be measured using scintillation or solid state gamma spectroscopic methods. Techniques for collection of the sample, concentration of krypton, and radioactivity measurement of krypton-85 are discussed and various processes are critically evaluated and compared

  4. Analytical models approximating individual processes: a validation method.

    Science.gov (United States)

    Favier, C; Degallier, N; Menkès, C E

    2010-12-01

    Upscaling population models from fine to coarse resolutions, in space, time and/or level of description, allows the derivation of fast and tractable models based on a thorough knowledge of individual processes. The validity of such approximations is generally tested only on a limited range of parameter sets. A more general validation test, over a range of parameters, is proposed; this would estimate the error induced by the approximation, using the original model's stochastic variability as a reference. This method is illustrated by three examples taken from the field of epidemics transmitted by vectors that bite in a temporally cyclical pattern, that illustrate the use of the method: to estimate if an approximation over- or under-fits the original model; to invalidate an approximation; to rank possible approximations for their qualities. As a result, the application of the validation method to this field emphasizes the need to account for the vectors' biology in epidemic prediction models and to validate these against finer scale models. Copyright © 2010 Elsevier Inc. All rights reserved.

  5. Analytical method for optimization of maintenance policy based on available system failure data

    International Nuclear Information System (INIS)

    Coria, V.H.; Maximov, S.; Rivas-Dávalos, F.; Melchor, C.L.; Guardado, J.L.

    2015-01-01

    An analytical optimization method for preventive maintenance (PM) policy with minimal repair at failure, periodic maintenance, and replacement is proposed for systems with historical failure time data influenced by a current PM policy. The method includes a new imperfect PM model based on Weibull distribution and incorporates the current maintenance interval T 0 and the optimal maintenance interval T to be found. The Weibull parameters are analytically estimated using maximum likelihood estimation. Based on this model, the optimal number of PM and the optimal maintenance interval for minimizing the expected cost over an infinite time horizon are also analytically determined. A number of examples are presented involving different failure time data and current maintenance intervals to analyze how the proposed analytical optimization method for periodic PM policy performances in response to changes in the distribution of the failure data and the current maintenance interval. - Highlights: • An analytical optimization method for preventive maintenance (PM) policy is proposed. • A new imperfect PM model is developed. • The Weibull parameters are analytically estimated using maximum likelihood. • The optimal maintenance interval and number of PM are also analytically determined. • The model is validated by several numerical examples

  6. [Progress in sample preparation and analytical methods for trace polar small molecules in complex samples].

    Science.gov (United States)

    Zhang, Qianchun; Luo, Xialin; Li, Gongke; Xiao, Xiaohua

    2015-09-01

    Small polar molecules such as nucleosides, amines, amino acids are important analytes in biological, food, environmental, and other fields. It is necessary to develop efficient sample preparation and sensitive analytical methods for rapid analysis of these polar small molecules in complex matrices. Some typical materials in sample preparation, including silica, polymer, carbon, boric acid and so on, are introduced in this paper. Meanwhile, the applications and developments of analytical methods of polar small molecules, such as reversed-phase liquid chromatography, hydrophilic interaction chromatography, etc., are also reviewed.

  7. A Reliable Method for Rhythm Analysis during Cardiopulmonary Resuscitation

    Directory of Open Access Journals (Sweden)

    U. Ayala

    2014-01-01

    Full Text Available Interruptions in cardiopulmonary resuscitation (CPR compromise defibrillation success. However, CPR must be interrupted to analyze the rhythm because although current methods for rhythm analysis during CPR have high sensitivity for shockable rhythms, the specificity for nonshockable rhythms is still too low. This paper introduces a new approach to rhythm analysis during CPR that combines two strategies: a state-of-the-art CPR artifact suppression filter and a shock advice algorithm (SAA designed to optimally classify the filtered signal. Emphasis is on designing an algorithm with high specificity. The SAA includes a detector for low electrical activity rhythms to increase the specificity, and a shock/no-shock decision algorithm based on a support vector machine classifier using slope and frequency features. For this study, 1185 shockable and 6482 nonshockable 9-s segments corrupted by CPR artifacts were obtained from 247 patients suffering out-of-hospital cardiac arrest. The segments were split into a training and a test set. For the test set, the sensitivity and specificity for rhythm analysis during CPR were 91.0% and 96.6%, respectively. This new approach shows an important increase in specificity without compromising the sensitivity when compared to previous studies.

  8. Review and evaluation of spark source mass spectrometry as an analytical method

    International Nuclear Information System (INIS)

    Beske, H.E.

    1981-01-01

    The analytical features and most important fields of application of spark source mass spectrometry are described with respect to the trace analysis of high-purity materials and the multielement analysis of technical alloys, geochemical and cosmochemical, biological and radioactive materials, as well as in environmental analysis. Comparisons are made to other analytical methods. The distribution of the method as well as opportunities for contract analysis are indicated and developmental tendencies discussed. (orig.) [de

  9. Critical node treatment in the analytic function expansion method for Pin Power Reconstruction

    International Nuclear Information System (INIS)

    Gao, Z.; Xu, Y.; Downar, T.

    2013-01-01

    Pin Power Reconstruction (PPR) was implemented in PARCS using the eight term analytic function expansion method (AFEN). This method has been demonstrated to be both accurate and efficient. However, similar to all the methods involving analytic functions, such as the analytic node method (ANM) and AFEN for nodal solution, the use of AFEN for PPR also has potential numerical issue with critical nodes. The conventional analytic functions are trigonometric or hyperbolic sine or cosine functions with an angular frequency proportional to buckling. For a critic al node the buckling is zero and the sine functions becomes zero, and the cosine function become unity. In this case, the eight terms of the analytic functions are no longer distinguishable from ea ch other which makes their corresponding coefficients can no longer be determined uniquely. The mode flux distribution of critical node can be linear while the conventional analytic functions can only express a uniform distribution. If there is critical or near critical node in a plane, the reconstructed pin power distribution is often be shown negative or very large values using the conventional method. In this paper, we propose a new method to avoid the numerical problem wit h critical nodes which uses modified trigonometric or hyperbolic sine functions which are the ratio of trigonometric or hyperbolic sine and its angular frequency. If there are no critical or near critical nodes present, the new pin power reconstruction method with modified analytic functions are equivalent to the conventional analytic functions. The new method is demonstrated using the L336C5 benchmark problem. (authors)

  10. Critical node treatment in the analytic function expansion method for Pin Power Reconstruction

    Energy Technology Data Exchange (ETDEWEB)

    Gao, Z. [Rice University, MS 318, 6100 Main Street, Houston, TX 77005 (United States); Xu, Y. [Argonne National Laboratory, 9700 South Case Ave., Argonne, IL 60439 (United States); Downar, T. [Department of Nuclear Engineering, University of Michigan, 2355 Bonisteel blvd., Ann Arbor, MI 48109 (United States)

    2013-07-01

    Pin Power Reconstruction (PPR) was implemented in PARCS using the eight term analytic function expansion method (AFEN). This method has been demonstrated to be both accurate and efficient. However, similar to all the methods involving analytic functions, such as the analytic node method (ANM) and AFEN for nodal solution, the use of AFEN for PPR also has potential numerical issue with critical nodes. The conventional analytic functions are trigonometric or hyperbolic sine or cosine functions with an angular frequency proportional to buckling. For a critic al node the buckling is zero and the sine functions becomes zero, and the cosine function become unity. In this case, the eight terms of the analytic functions are no longer distinguishable from ea ch other which makes their corresponding coefficients can no longer be determined uniquely. The mode flux distribution of critical node can be linear while the conventional analytic functions can only express a uniform distribution. If there is critical or near critical node in a plane, the reconstructed pin power distribution is often be shown negative or very large values using the conventional method. In this paper, we propose a new method to avoid the numerical problem wit h critical nodes which uses modified trigonometric or hyperbolic sine functions which are the ratio of trigonometric or hyperbolic sine and its angular frequency. If there are no critical or near critical nodes present, the new pin power reconstruction method with modified analytic functions are equivalent to the conventional analytic functions. The new method is demonstrated using the L336C5 benchmark problem. (authors)

  11. A Vocal-Based Analytical Method for Goose Behaviour Recognition

    Directory of Open Access Journals (Sweden)

    Henrik Karstoft

    2012-03-01

    Full Text Available Since human-wildlife conflicts are increasing, the development of cost-effective methods for reducing damage or conflict levels is important in wildlife management. A wide range of devices to detect and deter animals causing conflict are used for this purpose, although their effectiveness is often highly variable, due to habituation to disruptive or disturbing stimuli. Automated recognition of behaviours could form a critical component of a system capable of altering the disruptive stimuli to avoid this. In this paper we present a novel method to automatically recognise goose behaviour based on vocalisations from flocks of free-living barnacle geese (Branta leucopsis. The geese were observed and recorded in a natural environment, using a shielded shotgun microphone. The classification used Support Vector Machines (SVMs, which had been trained with labeled data. Greenwood Function Cepstral Coefficients (GFCC were used as features for the pattern recognition algorithm, as they can be adjusted to the hearing capabilities of different species. Three behaviours are classified based in this approach, and the method achieves a good recognition of foraging behaviour (86–97% sensitivity, 89–98% precision and a reasonable recognition of flushing (79–86%, 66–80% and landing behaviour(73–91%, 79–92%. The Support Vector Machine has proven to be a robust classifier for this kind of classification, as generality and non-linearcapabilities are important. We conclude that vocalisations can be used to automatically detect behaviour of conflict wildlife species, and as such, may be used as an integrated part of awildlife management system.

  12. [Analytic methods for seed models with genotype x environment interactions].

    Science.gov (United States)

    Zhu, J

    1996-01-01

    Genetic models with genotype effect (G) and genotype x environment interaction effect (GE) are proposed for analyzing generation means of seed quantitative traits in crops. The total genetic effect (G) is partitioned into seed direct genetic effect (G0), cytoplasm genetic of effect (C), and maternal plant genetic effect (Gm). Seed direct genetic effect (G0) can be further partitioned into direct additive (A) and direct dominance (D) genetic components. Maternal genetic effect (Gm) can also be partitioned into maternal additive (Am) and maternal dominance (Dm) genetic components. The total genotype x environment interaction effect (GE) can also be partitioned into direct genetic by environment interaction effect (G0E), cytoplasm genetic by environment interaction effect (CE), and maternal genetic by environment interaction effect (GmE). G0E can be partitioned into direct additive by environment interaction (AE) and direct dominance by environment interaction (DE) genetic components. GmE can also be partitioned into maternal additive by environment interaction (AmE) and maternal dominance by environment interaction (DmE) genetic components. Partitions of genetic components are listed for parent, F1, F2 and backcrosses. A set of parents, their reciprocal F1 and F2 seeds is applicable for efficient analysis of seed quantitative traits. MINQUE(0/1) method can be used for estimating variance and covariance components. Unbiased estimation for covariance components between two traits can also be obtained by the MINQUE(0/1) method. Random genetic effects in seed models are predictable by the Adjusted Unbiased Prediction (AUP) approach with MINQUE(0/1) method. The jackknife procedure is suggested for estimation of sampling variances of estimated variance and covariance components and of predicted genetic effects, which can be further used in a t-test for parameter. Unbiasedness and efficiency for estimating variance components and predicting genetic effects are tested by

  13. Selected methods of waste monitoring using modern analytical techniques

    International Nuclear Information System (INIS)

    Hlavacek, I.; Hlavackova, I.

    1993-11-01

    Issues of the inspection and control of bituminized and cemented waste are discussed, and some methods of their nondestructive testing are described. Attention is paid to the inspection techniques, non-nuclear spectral techniques in particular, as employed for quality control of the wastes, waste concentrates, spent waste leaching solutions, as well as for the examination of environmental samples (waters and soils) from the surroundings of nuclear power plants. Some leaching tests used abroad for this purpose and practical analyses by the ICP-AES technique are given by way of example. The ICP-MS technique, which is unavailable in the Czech Republic, is routinely employed abroad for alpha nuclide measurements; examples of such analyses are also given. The next topic discussed includes the monitoring of organic acids and complexants to determine the degree of their thermal decomposition during the bituminization of wastes on an industrial line. All of the methods and procedures highlighted can be used as technical support during the monitoring of radioactive waste properties in industrial conditions, in the chemical and radiochemical analyses of wastes and related matter, in the calibration of nondestructive testing instrumentation, in the monitoring of contamination of the surroundings of nuclear facilities, and in trace analysis. (author). 10 tabs., 1 fig., 14 refs

  14. Applications of Nuclear Analytical Methods for High Tech Industry

    International Nuclear Information System (INIS)

    Hossain, T.

    2013-01-01

    Silicon based semiconductor chip manufacturing is a worldwide high technology industry with numerous measurement issues. One of the major concerns in the semiconductor manufacturing is contamination such as the trace metal impurities. This concern is vividly illustrated by the fact that the manufacturing in this industry is done in ultra clean environment where the entire manufacturing facility or “Fab” is a clean room facility or each and every manufacturing tool is enclosed in a mini-environment Although semiconductor devices are fabricated on the surface of the Si wafers contamination in the bulk material is a major concern. Nuclear methods of analysis are uniquely suited for the contamination analysis in such a matrix. Many opportunities in the semiconductor manufacturing field exist for the nuclear methods to provide support services. Contamination analysis by NAA, depth profiles by NDP and prompt gamma analysis of H in thin films are a few examples. These needs are on-going and require commitment from the lab so that a manufacturing operation can rely on the delivery of these services when required

  15. Using an analytical geometry method to improve tiltmeter data presentation

    Science.gov (United States)

    Su, W.-J.

    2000-01-01

    The tiltmeter is a useful tool for geologic and geotechnical applications. To obtain full benefit from the tiltmeter, easy and accurate data presentations should be used. Unfortunately, the most commonly used method for tilt data reduction now may yield inaccurate and low-resolution results. This article describes a simple, accurate, and high-resolution approach developed at the Illinois State Geological Survey for data reduction and presentation. The orientation of tiltplates is determined first by using a trigonometric relationship, followed by a matrix transformation, to obtain the true amount of rotation change of the tiltplate at any given time. The mathematical derivations used for the determination and transformation are then coded into an integrated PC application by adapting the capabilities of commercial spreadsheet, database, and graphics software. Examples of data presentation from tiltmeter applications in studies of landfill covers, characterizations of mine subsidence, and investigations of slope stability are also discussed.

  16. Manual of analytical methods for the Environmental Health Laboratory

    International Nuclear Information System (INIS)

    Gray, C.E.

    1975-06-01

    The manual contains four sections: absorption spectrophotometry; general radiochemical procedures; instrumental analysis; and calibration of field instruments. Included in the individual analyses using absorption spectrophotometry is one for total iodine in oil. Radiochemical procedures are given for: actinides in urine and water; 137 Cs in soil and vegetation; 137 Cs in soil, urine, vegetation, and water; enriched uranium in urine; gross beta activity in soil, urine, vegetation, and water; plutonium in urine and soil; 210 Po in urine and water; 24 Na in air, blood, urine, and water; 90 Sr in soil, vegetation, and water; tritium in urine, water, and on swipes; and total uranium on fallout trays and in soil, urine, and water. Among the individual instrumental analyses is a spectrographic method for determining beryllium in air samples and swipes. (U.S.)

  17. Analytical Chemistry Laboratory (ACL) procedure compendium. Volume 4, Organic methods

    Energy Technology Data Exchange (ETDEWEB)

    1993-08-01

    This interim notice covers the following: extractable organic halides in solids, total organic halides, analysis by gas chromatography/Fourier transform-infrared spectroscopy, hexadecane extracts for volatile organic compounds, GC/MS analysis of VOCs, GC/MS analysis of methanol extracts of cryogenic vapor samples, screening of semivolatile organic extracts, GPC cleanup for semivolatiles, sample preparation for GC/MS for semi-VOCs, analysis for pesticides/PCBs by GC with electron capture detection, sample preparation for pesticides/PCBs in water and soil sediment, report preparation, Florisil column cleanup for pesticide/PCBs, silica gel and acid-base partition cleanup of samples for semi-VOCs, concentrate acid wash cleanup, carbon determination in solids using Coulometrics` CO{sub 2} coulometer, determination of total carbon/total organic carbon/total inorganic carbon in radioactive liquids/soils/sludges by hot persulfate method, analysis of solids for carbonates using Coulometrics` Model 5011 coulometer, and soxhlet extraction.

  18. An analytical method of estimating Value-at-Risk on the Belgrade Stock Exchange

    Directory of Open Access Journals (Sweden)

    Obadović Milica D.

    2009-01-01

    Full Text Available This paper presents market risk evaluation for a portfolio consisting of shares that are continuously traded on the Belgrade Stock Exchange, by applying the Value-at-Risk model - the analytical method. It describes the manner of analytical method application and compares the results obtained by implementing this method at different confidence levels. Method verification was carried out on the basis of the failure rate that demonstrated the confidence level for which this method was acceptable in view of the given conditions.

  19. Determination of 237Np in environmental and nuclear samples: A review of the analytical method

    International Nuclear Information System (INIS)

    Thakur, P.; Mulholland, G.P.

    2012-01-01

    A number of analytical methods has been developed and used for the determination of neptunium in environmental and nuclear fuel samples using alpha, ICP–MS spectrometry, and other analytical techniques. This review summarizes and discusses development of the radiochemical procedures for separation of neptunium (Np), since the beginning of the nuclear industry, followed by a more detailed discussion on recent trends in the separation of neptunium. This article also highlights the progress in analytical methods and issues associated with the determination of neptunium in environmental samples. - Highlights: ► Determination of Np in environmental and nuclear samples is reviewed. ► Various analytical methods used for the determination of Np are listed. ► Progress and issues associated with the determination of Np are discussed.

  20. Analytical methods for 2,4-D (Dichlorophenoxyacetic acid) determination

    International Nuclear Information System (INIS)

    Martinez G, M.S.M.

    1999-01-01

    The 2,4-D herbicide is one of the main pesticides for controlling the bad grass in crops such as the water undergrowth. In Mexico the allowed bound of this pesticide is 0.05 mg/l in water of 2,4-D so it is required to have methods trusts and exacts, which can used in order to detected low concentration of it. In this work we show some for the conventional techniques and for establishing the 2,4-D concentrations. The UV-Vis spectrometer and liquids chromatography due that they are the most common used nowadays. Beside, we introduce a now developed technique, which is based on the neutronic activation analysis. Though use of the UV-Vis spectrometer technique it was possible target the concentrations interval between 1 and 200 mg/l. In the liquids chromatography interval was between 0.1 and 0.9, and by the neutronic activation analysis the interval was between 0.01 and 200 mg/l. (Author)

  1. Review of Reliability-Based Design Optimization Approach and Its Integration with Bayesian Method

    Science.gov (United States)

    Zhang, Xiangnan

    2018-03-01

    A lot of uncertain factors lie in practical engineering, such as external load environment, material property, geometrical shape, initial condition, boundary condition, etc. Reliability method measures the structural safety condition and determine the optimal design parameter combination based on the probabilistic theory. Reliability-based design optimization (RBDO) is the most commonly used approach to minimize the structural cost or other performance under uncertainty variables which combines the reliability theory and optimization. However, it cannot handle the various incomplete information. The Bayesian approach is utilized to incorporate this kind of incomplete information in its uncertainty quantification. In this paper, the RBDO approach and its integration with Bayesian method are introduced.

  2. Reliability Analysis Of Fire System On The Industry Facility By Use Fameca Method

    International Nuclear Information System (INIS)

    Sony T, D.T.; Situmorang, Johnny; Ismu W, Puradwi; Demon H; Mulyanto, Dwijo; Kusmono, Slamet; Santa, Sigit Asmara

    2000-01-01

    FAMECA is one of the analysis method to determine system reliability on the industry facility. Analysis is done by some procedure that is identification of component function, determination of failure mode, severity level and effect of their failure. Reliability value is determined by three combinations that is severity level, component failure value and critical component. Reliability of analysis has been done for fire system on the industry by FAMECA method. Critical component which identified is pump, air release valve, check valve, manual test valve, isolation valve, control system etc

  3. Verification of practicability of quantitative reliability evaluation method (De-BDA) in nuclear power plants

    International Nuclear Information System (INIS)

    Takahashi, Kinshiro; Yukimachi, Takeo.

    1988-01-01

    A variety of methods have been applied to study of reliability analysis in which human factors are included in order to enhance the safety and availability of nuclear power plants. De-BDA (Detailed Block Diagram Analysis) is one of such mehtods developed with the objective of creating a more comprehensive and understandable tool for quantitative analysis of reliability associated with plant operations. The practicability of this method has been verified by applying it to reliability analysis of various phases of plant operation as well as evaluation of enhanced man-machine interface in the central control room. (author)

  4. Propulsion and launching analysis of variable-mass rockets by analytical methods

    Directory of Open Access Journals (Sweden)

    D.D. Ganji

    2013-09-01

    Full Text Available In this study, applications of some analytical methods on nonlinear equation of the launching of a rocket with variable mass are investigated. Differential transformation method (DTM, homotopy perturbation method (HPM and least square method (LSM were applied and their results are compared with numerical solution. An excellent agreement with analytical methods and numerical ones is observed in the results and this reveals that analytical methods are effective and convenient. Also a parametric study is performed here which includes the effect of exhaust velocity (Ce, burn rate (BR of fuel and diameter of cylindrical rocket (d on the motion of a sample rocket, and contours for showing the sensitivity of these parameters are plotted. The main results indicate that the rocket velocity and altitude are increased with increasing the Ce and BR and decreased with increasing the rocket diameter and drag coefficient.

  5. An introduction to clinical microeconomic analysis: purposes and analytic methods.

    Science.gov (United States)

    Weintraub, W S; Mauldin, P D; Becker, E R

    1994-06-01

    The recent concern with health care economics has fostered the development of a new discipline that is generally called clinical microeconomics. This is a discipline in which microeconomic methods are used to study the economics of specific medical therapies. It is possible to perform stand alone cost analyses, but more profound insight into the medical decision making process may be accomplished by combining cost studies with measures of outcome. This is most often accomplished with cost-effectiveness or cost-utility studies. In cost-effectiveness studies there is one measure of outcome, often death. In cost-utility studies there are multiple measures of outcome, which must be grouped together to give an overall picture of outcome or utility. There are theoretical limitations to the determination of utility that must be accepted to perform this type of analysis. A summary statement of outcome is quality adjusted life years (QALYs), which is utility time socially discounted survival. Discounting is used because people value a year of future life less than a year of present life. Costs are made up of in-hospital direct, professional, follow-up direct, and follow-up indirect costs. Direct costs are for medical services. Indirect costs reflect opportunity costs such as lost time at work. Cost estimates are often based on marginal costs, or the cost for one additional procedure of the same type. Finally an overall statistic may be generated as cost per unit increase in effectiveness, such as dollars per QALY.(ABSTRACT TRUNCATED AT 250 WORDS)

  6. OSS reliability measurement and assessment

    CERN Document Server

    Yamada, Shigeru

    2016-01-01

    This book analyses quantitative open source software (OSS) reliability assessment and its applications, focusing on three major topic areas: the Fundamentals of OSS Quality/Reliability Measurement and Assessment; the Practical Applications of OSS Reliability Modelling; and Recent Developments in OSS Reliability Modelling. Offering an ideal reference guide for graduate students and researchers in reliability for open source software (OSS) and modelling, the book introduces several methods of reliability assessment for OSS including component-oriented reliability analysis based on analytic hierarchy process (AHP), analytic network process (ANP), and non-homogeneous Poisson process (NHPP) models, the stochastic differential equation models and hazard rate models. These measurement and management technologies are essential to producing and maintaining quality/reliable systems using OSS.

  7. A SIMPLE ANALYTICAL METHOD TO DETERMINE SOLAR ENERGETIC PARTICLES' MEAN FREE PATH

    International Nuclear Information System (INIS)

    He, H.-Q.; Qin, G.

    2011-01-01

    To obtain the mean free path of solar energetic particles (SEPs) for a solar event, one usually has to fit time profiles of both flux and anisotropy from spacecraft observations to numerical simulations of SEPs' transport processes. This method can be called a simulation method. But a reasonably good fitting needs a lot of simulations, which demand a large amount of calculation resources. Sometimes, it is necessary to find an easy way to obtain the mean free path of SEPs quickly, for example, in space weather practice. Recently, Shalchi et al. provided an approximate analytical formula of SEPs' anisotropy time profile as a function of particles' mean free path for impulsive events. In this paper, we determine SEPs' mean free path by fitting the anisotropy time profiles from Shalchi et al.'s analytical formula to spacecraft observations. This new method can be called an analytical method. In addition, we obtain SEPs' mean free path with the traditional simulation methods. Finally, we compare the mean free path obtained with the simulation method to that of the analytical method to show that the analytical method, with some minor modifications, can give us a good, quick approximation of SEPs' mean free path for impulsive events.

  8. A study in the reliability analysis method for nuclear power plant structures (I)

    Energy Technology Data Exchange (ETDEWEB)

    Oh, Byung Hwan; Choi, Seong Cheol; Shin, Ho Sang; Yang, In Hwan; Kim, Yi Sung; Yu, Young; Kim, Se Hun [Seoul, Nationl Univ., Seoul (Korea, Republic of)

    1999-03-15

    Nuclear power plant structures may be exposed to aggressive environmental effects that may cause their strength and stiffness to decrease over their service life. Although the physics of these damage mechanisms are reasonably well understood and quantitative evaluation of their effects on time-dependent structural behavior is possible in some instances, such evaluations are generally very difficult and remain novel. The assessment of existing steel containment in nuclear power plants for continued service must provide quantitative evidence that they are able to withstand future extreme loads during a service period with an acceptable level of reliability. Rational methodologies to perform the reliability assessment can be developed from mechanistic models of structural deterioration, using time-dependent structural reliability analysis to take loading and strength uncertainties into account. The final goal of this study is to develop the analysis method for the reliability of containment structures. The cause and mechanism of corrosion is first clarified and the reliability assessment method has been established. By introducing the equivalent normal distribution, the procedure of reliability analysis which can determine the failure probabilities has been established. The influence of design variables to reliability and the relation between the reliability and service life will be continued second year research.

  9. Integrative Mixed Methods Data Analytic Strategies in Research on School Success in Challenging Circumstances

    Science.gov (United States)

    Jang, Eunice E.; McDougall, Douglas E.; Pollon, Dawn; Herbert, Monique; Russell, Pia

    2008-01-01

    There are both conceptual and practical challenges in dealing with data from mixed methods research studies. There is a need for discussion about various integrative strategies for mixed methods data analyses. This article illustrates integrative analytic strategies for a mixed methods study focusing on improving urban schools facing challenging…

  10. A comparison of two analytical evaluation methods for educational computer games for young children

    NARCIS (Netherlands)

    Bekker, M.M.; Baauw, E.; Barendregt, W.

    2008-01-01

    In this paper we describe a comparison of two analytical methods for educational computer games for young children. The methods compared in the study are the Structured Expert Evaluation Method (SEEM) and the Combined Heuristic Evaluation (HE) (based on a combination of Nielsen’s HE and the

  11. Development of reliable analytical tools for evaluating the influence of reductive winemaking on the quality of Lugana wines.

    Science.gov (United States)

    Mattivi, Fulvio; Fedrizzi, Bruno; Zenato, Alberto; Tiefenthaler, Paolo; Tempesta, Silvano; Perenzoni, Daniele; Cantarella, Paolo; Simeoni, Federico; Vrhovsek, Urska

    2012-06-30

    This paper presents methods for the definition of important analytical tools, such as the development of sensitive and rapid methods for analysing reduced and oxidised glutathione (GSH and GSSG), hydroxycinnamic acids (HCA), bound thiols (GSH-3MH and Cys-3MH) and free thiols (3MH and 3MHA), and their first application to evaluate the effect of reductive winemaking on the composition of Lugana juices and wines. Lugana is a traditional white wine from the Lake Garda region (Italy), produced using a local grape variety, Trebbiano di Lugana. An innovative winemaking procedure based on preliminary cooling of grape berries followed by crushing in an inert environment was implemented and explored on a winery scale. The effects of these procedures on hydroxycinnamic acids, GSH, GSSG, free and bound thiols and flavanols content were investigated. The juices and wines produced using different protocols were examined. Moreover, wines aged in tanks for 1, 2 and 3 months were analysed. The high level of GSH found in Lugana grapes, which can act as a natural antioxidant and be preserved in must and young wines, thus reducing the need of exogenous antioxidants, was particularly interesting. Moreover, it was clear that polyphenol concentrations (hydroxycinnamic acids and catechins) were strongly influenced by winemaking and pressing conditions, which required fine tuning of pressing. Above-threshold levels of 3-mercaptohexan-1-ol (3MH) and 3-mercaptohexyl acetate (3MHA) were found in the wines and changed according to the winemaking procedure applied. Interestingly, the evolution during the first three months also varied depending on the procedure adopted. Organic synthesis of cysteine and glutathione conjugates was carried out and juices and wines were subjected to LC-MS/MS analysis. These two molecules appeared to be strongly affected by the winemaking procedure, but did not show any significant change during the first 3 months of post-bottling ageing. This supports the theory

  12. Development of an analytical method for the simultaneous analysis of MCPD esters and glycidyl esters in oil-based foodstuffs.

    Science.gov (United States)

    Ermacora, Alessia; Hrnčiřík, Karel

    2014-01-01

    Substantial progress has been recently made in the development and optimisation of analytical methods for the quantification of 2-MCPD, 3-MCPD and glycidyl esters in oils and fats, and there are a few methods currently available that allow a reliable quantification of these contaminants in bulk oils and fats. On the other hand, no standard method for the analysis of foodstuffs has yet been established. The aim of this study was the development and validation of a new method for the simultaneous quantification of 2-MCPD, 3-MCPD and glycidyl esters in oil-based food products. The developed protocol includes a first step of liquid-liquid extraction and purification of the lipophilic substances of the sample, followed by the application of a previously developed procedure based on acid transesterification, for the indirect quantification of these contaminants in oils and fats. The method validation was carried out on food products (fat-based spreads, creams, margarine, mayonnaise) manufactured in-house, in order to control the manufacturing process and account for any food matrix-analyte interactions (the sample spiking was carried out on the single components used for the formulations rather than the final products). The method showed good accuracy (the recoveries ranged from 97% to 106% for bound 3-MCPD and 2-MCPD and from 88% to 115% for bound glycidol) and sensitivity (the LOD was 0.04 and 0.05 mg kg(-1) for bound MCPD and glycidol, respectively). Repeatability and reproducibility were satisfactory (RSD below 2% and 5%, respectively) for all analytes. The levels of salts and surface-active compounds in the formulation were found to have no impact on the accuracy and the other parameters of the method.

  13. Ernst Equation and Riemann Surfaces: Analytical and Numerical Methods

    International Nuclear Information System (INIS)

    Ernst, Frederick J

    2007-01-01

    metric tensor components. The first two chapters of this book are devoted to some basic ideas: in the introductory chapter 1 the authors discuss the concept of integrability, comparing the integrability of the vacuum Ernst equation with the integrability of nonlinear equations of Korteweg-de Vries (KdV) type, while in chapter 2 they describe various circumstances in which the vacuum Ernst equation has been determined to be relevant, not only in connection with gravitation but also, for example, in the construction of solutions of the self-dual Yang-Mills equations. It is also in this chapter that one of several equivalent linear systems for the Ernst equation is described. The next two chapters are devoted to Dmitry Korotkin's concept of algebro-geometric solutions of a linear system: in chapter 3 the structure of such solutions of the vacuum Ernst equation, which involve Riemann theta functions of hyperelliptic algebraic curves of any genus, is contrasted with the periodic structure of such solutions of the KdV equation. How such solutions can be obtained, for example, by solving a matrix Riemann-Hilbert problem and how the metric tensor of the associated spacetime can be evaluated is described in detail. In chapter 4 the asymptotic behaviour and the similarity structure of the general algebro-geometric solutions of the Ernst equation are described, and the relationship of such solutions to the perhaps more familiar multi-soliton solutions is discussed. The next three chapters are based upon the authors' own published research: in chapter 5 it is shown that a problem involving counter-rotating infinitely thin disks of matter can be solved in terms of genus two Riemann theta functions, while in chapter 6 the authors describe numerical methods that facilitate the construction of such solutions, and in chapter 7 three-dimensional graphs are displayed that depict all metrical fields of the associated spacetime. Finally, in chapter 8, the difficulties associated with

  14. Waste Tank Organic Safety Program: Analytical methods development. Progress report, FY 1994

    International Nuclear Information System (INIS)

    Campbell, J.A.; Clauss, S.A.; Grant, K.E.

    1994-09-01

    The objectives of this task are to develop and document extraction and analysis methods for organics in waste tanks, and to extend these methods to the analysis of actual core samples to support the Waste Tank organic Safety Program. This report documents progress at Pacific Northwest Laboratory (a) during FY 1994 on methods development, the analysis of waste from Tank 241-C-103 (Tank C-103) and T-111, and the transfer of documented, developed analytical methods to personnel in the Analytical Chemistry Laboratory (ACL) and 222-S laboratory. This report is intended as an annual report, not a completed work

  15. Bearing Procurement Analysis Method by Total Cost of Ownership Analysis and Reliability Prediction

    Science.gov (United States)

    Trusaji, Wildan; Akbar, Muhammad; Sukoyo; Irianto, Dradjad

    2018-03-01

    In making bearing procurement analysis, price and its reliability must be considered as decision criteria, since price determines the direct cost as acquisition cost and reliability of bearing determine the indirect cost such as maintenance cost. Despite the indirect cost is hard to identify and measured, it has high contribution to overall cost that will be incurred. So, the indirect cost of reliability must be considered when making bearing procurement analysis. This paper tries to explain bearing evaluation method with the total cost of ownership analysis to consider price and maintenance cost as decision criteria. Furthermore, since there is a lack of failure data when bearing evaluation phase is conducted, reliability prediction method is used to predict bearing reliability from its dynamic load rating parameter. With this method, bearing with a higher price but has higher reliability is preferable for long-term planning. But for short-term planning the cheaper one but has lower reliability is preferable. This contextuality can give rise to conflict between stakeholders. Thus, the planning horizon needs to be agreed by all stakeholder before making a procurement decision.

  16. Application of capability indices and control charts in the analytical method control strategy.

    Science.gov (United States)

    Oliva, Alexis; Llabres Martinez, Matías

    2017-08-01

    In this study, we assessed the usefulness of control charts in combination with the process capability indices, C pm and C pk , in the control strategy of an analytical method. The traditional X-chart and moving range chart were used to monitor the analytical method over a 2-year period. The results confirmed that the analytical method is in-control and stable. Different criteria were used to establish the specifications limits (i.e. analyst requirements) for fixed method performance (i.e. method requirements). If the specification limits and control limits are equal in breadth, the method can be considered "capable" (C pm  = 1), but it does not satisfy the minimum method capability requirements proposed by Pearn and Shu (2003). Similar results were obtained using the C pk index. The method capability was also assessed as a function of method performance for fixed analyst requirements. The results indicate that the method does not meet the requirements of the analytical target approach. A real-example data of a SEC with light-scattering detection method was used as a model whereas previously published data were used to illustrate the applicability of the proposed approach. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  17. Analytical chemistry in semiconductor manufacturing: Techniques, role of nuclear methods and need for quality control

    International Nuclear Information System (INIS)

    1989-06-01

    This report is the result of a consultants meeting held in Gaithersburg, USA, 2-3 October 1987. The meeting was hosted by the National Bureau of Standards and Technology, and it was attended by 18 participants from Denmark, Finland, India, Japan, Norway, People's Republic of China and the USA. The purpose of the meeting was to assess the present status of analytical chemistry in semiconductor manufacturing, the role of nuclear analytical methods and the need for internationally organized quality control of the chemical analysis. The report contains the three presentations in full and a summary report of the discussions. Thus, it gives an overview of the need of analytical chemistry in manufacturing of silicon based devices, the use of nuclear analytical methods, and discusses the need for quality control. Refs, figs and tabs

  18. Assessment of Advanced Life Support competence when combining different test methods--reliability and validity

    DEFF Research Database (Denmark)

    Ringsted, C; Lippert, F; Hesselfeldt, R

    2007-01-01

    Cardiac Arrest Simulation Test (CASTest) scenarios for the assessments according to guidelines 2005. AIMS: To analyse the reliability and validity of the individual sub-tests provided by ERC and to find a combination of MCQ and CASTest that provides a reliable and valid single effect measure of ALS...... that possessed high reliability, equality of test sets, and ability to discriminate between the two groups of supposedly different ALS competence. CONCLUSIONS: ERC sub-tests of ALS competence possess sufficient reliability and validity. A combined ALS score with equal weighting of one MCQ and one CASTest can...... competence. METHODS: Two groups of participants were included in this randomised, controlled experimental study: a group of newly graduated doctors, who had not taken the ALS course (N=17) and a group of students, who had passed the ALS course 9 months before the study (N=16). Reliability in terms of inter...

  19. Optimization of offshore wind turbine support structures using analytical gradient-based method

    OpenAIRE

    Chew, Kok Hon; Tai, Kang; Ng, E.Y.K.; Muskulus, Michael

    2015-01-01

    Design optimization of the offshore wind turbine support structure is an expensive task; due to the highly-constrained, non-convex and non-linear nature of the design problem. This report presents an analytical gradient-based method to solve this problem in an efficient and effective way. The design sensitivities of the objective and constraint functions are evaluated analytically while the optimization of the structure is performed, subject to sizing, eigenfrequency, extreme load an...

  20. Evaluation and selection of in-situ leaching mining method using analytic hierarchy process

    International Nuclear Information System (INIS)

    Zhao Heyong; Tan Kaixuan; Liu Huizhen

    2007-01-01

    According to the complicated conditions and main influence factors of in-situ leaching min- ing, a model and processes of analytic hierarchy are established for evaluation and selection of in-situ leaching mining methods based on analytic hierarchy process. Taking a uranium mine in Xinjiang of China for example, the application of this model is presented. The results of analyses and calculation indicate that the acid leaching is the optimum project. (authors)

  1. Reliability of the k{sub 0}-standardization method using geological sample analysed in a proficiency test

    Energy Technology Data Exchange (ETDEWEB)

    Pelaes, Ana Clara O.; Menezes, Maria Ângela de B.C., E-mail: anacpelaes@gmail.com, E-mail: menezes@cdtn.br [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil)

    2017-11-01

    The Neutron Activation Analysis (NAA) is an analytical technique to determine the elemental chemical composition in samples of several matrices, that has been applied by the Laboratory for Neutron Activation Analysis, located at Centro de Desenvolvimento da Tecnologia Nuclear /Comissão Nacional de Energia Nuclear (Nuclear Technology Development Center/Brazilian Commission for Nuclear Energy), CDTN/CNEN, since the starting up of the TRIGA MARK I IPR-R1 reactor, in 1960. Among the methods of application of the technique, the k{sub 0}-standardization method, which was established at CDTN in 1995, is the most efficient and in 2003 it was reestablished and optimized. In order to verify the reproducibility of the results generated by the application of the k{sub 0}-standardization method at CDTN, aliquots of a geological sample sent by WEPAL (Wageningen Evaluating Programs for Analytical Laboratories) were analysed and its results were compared with the results obtained through the Intercomparison of Results organized by the International Atomic Energy Agency in 2015. WEPAL is an accredited institution for the organisation of interlaboratory studies, preparing and organizing proficiency testing schemes all over the world. Therefore, the comparison with the results provided aims to contribute to the continuous improvement of the quality of the results obtained by the CDTN. The objective of this study was to verify the reliability of the method applied two years after the intercomparison round. (author)

  2. Reliability analysis of idealized tunnel support system using probability-based methods with case studies

    Science.gov (United States)

    Gharouni-Nik, Morteza; Naeimi, Meysam; Ahadi, Sodayf; Alimoradi, Zahra

    2014-06-01

    In order to determine the overall safety of a tunnel support lining, a reliability-based approach is presented in this paper. Support elements in jointed rock tunnels are provided to control the ground movement caused by stress redistribution during the tunnel drive. Main support elements contribute to stability of the tunnel structure are recognized owing to identify various aspects of reliability and sustainability in the system. The selection of efficient support methods for rock tunneling is a key factor in order to reduce the number of problems during construction and maintain the project cost and time within the limited budget and planned schedule. This paper introduces a smart approach by which decision-makers will be able to find the overall reliability of tunnel support system before selecting the final scheme of the lining system. Due to this research focus, engineering reliability which is a branch of statistics and probability is being appropriately applied to the field and much effort has been made to use it in tunneling while investigating the reliability of the lining support system for the tunnel structure. Therefore, reliability analysis for evaluating the tunnel support performance is the main idea used in this research. Decomposition approaches are used for producing system block diagram and determining the failure probability of the whole system. Effectiveness of the proposed reliability model of tunnel lining together with the recommended approaches is examined using several case studies and the final value of reliability obtained for different designing scenarios. Considering the idea of linear correlation between safety factors and reliability parameters, the values of isolated reliabilities determined for different structural components of tunnel support system. In order to determine individual safety factors, finite element modeling is employed for different structural subsystems and the results of numerical analyses are obtained in

  3. Reliability-based design optimization via high order response surface method

    International Nuclear Information System (INIS)

    Li, Hong Shuang

    2013-01-01

    To reduce the computational effort of reliability-based design optimization (RBDO), the response surface method (RSM) has been widely used to evaluate reliability constraints. We propose an efficient methodology for solving RBDO problems based on an improved high order response surface method (HORSM) that takes advantage of an efficient sampling method, Hermite polynomials and uncertainty contribution concept to construct a high order response surface function with cross terms for reliability analysis. The sampling method generates supporting points from Gauss-Hermite quadrature points, which can be used to approximate response surface function without cross terms, to identify the highest order of each random variable and to determine the significant variables connected with point estimate method. The cross terms between two significant random variables are added to the response surface function to improve the approximation accuracy. Integrating the nested strategy, the improved HORSM is explored in solving RBDO problems. Additionally, a sampling based reliability sensitivity analysis method is employed to reduce the computational effort further when design variables are distributional parameters of input random variables. The proposed methodology is applied on two test problems to validate its accuracy and efficiency. The proposed methodology is more efficient than first order reliability method based RBDO and Monte Carlo simulation based RBDO, and enables the use of RBDO as a practical design tool.

  4. Selenium contaminated waters: An overview of analytical methods, treatment options and recent advances in sorption methods.

    Science.gov (United States)

    Santos, Sílvia; Ungureanu, Gabriela; Boaventura, Rui; Botelho, Cidália

    2015-07-15

    Selenium is an essential trace element for many organisms, including humans, but it is bioaccumulative and toxic at higher than homeostatic levels. Both selenium deficiency and toxicity are problems around the world. Mines, coal-fired power plants, oil refineries and agriculture are important examples of anthropogenic sources, generating contaminated waters and wastewaters. For reasons of human health and ecotoxicity, selenium concentration has to be controlled in drinking-water and in wastewater, as it is a potential pollutant of water bodies. This review article provides firstly a general overview about selenium distribution, sources, chemistry, toxicity and environmental impact. Analytical techniques used for Se determination and speciation and water and wastewater treatment options are reviewed. In particular, published works on adsorption as a treatment method for Se removal from aqueous solutions are critically analyzed. Recent published literature has given particular attention to the development and search for effective adsorbents, including low-cost alternative materials. Published works mostly consist in exploratory findings and laboratory-scale experiments. Binary metal oxides and LDHs (layered double hydroxides) have presented excellent adsorption capacities for selenium species. Unconventional sorbents (algae, agricultural wastes and other biomaterials), in raw or modified forms, have also led to very interesting results with the advantage of their availability and low-cost. Some directions to be considered in future works are also suggested. Copyright © 2015 Elsevier B.V. All rights reserved.

  5. MULTIPLE CRITERA METHODS WITH FOCUS ON ANALYTIC HIERARCHY PROCESS AND GROUP DECISION MAKING

    Directory of Open Access Journals (Sweden)

    Lidija Zadnik-Stirn

    2010-12-01

    Full Text Available Managing natural resources is a group multiple criteria decision making problem. In this paper the analytic hierarchy process is the chosen method for handling the natural resource problems. The one decision maker problem is discussed and, three methods: the eigenvector method, data envelopment analysis method, and logarithmic least squares method are presented for the derivation of the priority vector. Further, the group analytic hierarchy process is discussed and six methods for the aggregation of individual judgments or priorities: weighted arithmetic mean method, weighted geometric mean method, and four methods based on data envelopment analysis are compared. The case study on land use in Slovenia is applied. The conclusions review consistency, sensitivity analyses, and some future directions of research.

  6. A Quantitative Analytical Method to Test for Salt Effects on Giant Unilamellar Vesicles

    DEFF Research Database (Denmark)

    Hadorn, Maik; Bönzli, Eva; Eggenberger Hotz, Peter

    2011-01-01

    preparation method with automatic haemocytometry. We found that this new quantitative screening method is highly reliable and consistent with previously reported results. Thus, this method may provide a significant methodological advance in analysis of effects on free-standing model membranes....

  7. Analytical method for reconstruction pin to pin of the nuclear power density distribution

    Energy Technology Data Exchange (ETDEWEB)

    Pessoa, Paulo O.; Silva, Fernando C.; Martinez, Aquilino S., E-mail: ppessoa@con.ufrj.br, E-mail: fernando@con.ufrj.br, E-mail: aquilino@imp.ufrj.br [Coordenacao dos Programas de Pos-Graduacao em Engenharia (COPPE/UFRJ), Rio de Janeiro, RJ (Brazil)

    2013-07-01

    An accurate and efficient method for reconstructing pin to pin of the nuclear power density distribution, involving the analytical solution of the diffusion equation for two-dimensional neutron energy groups in homogeneous nodes, is presented. The boundary conditions used for analytic as solution are the four currents or fluxes on the surface of the node, which are obtained by Nodal Expansion Method (known as NEM) and four fluxes at the vertices of a node calculated using the finite difference method. The analytical solution found is the homogeneous distribution of neutron flux. Detailed distributions pin to pin inside a fuel assembly are estimated by the product of homogeneous flux distribution by local heterogeneous form function. Furthermore, the form functions of flux and power are used. The results obtained with this method have a good accuracy when compared with reference values. (author)

  8. Analytical method for reconstruction pin to pin of the nuclear power density distribution

    International Nuclear Information System (INIS)

    Pessoa, Paulo O.; Silva, Fernando C.; Martinez, Aquilino S.

    2013-01-01

    An accurate and efficient method for reconstructing pin to pin of the nuclear power density distribution, involving the analytical solution of the diffusion equation for two-dimensional neutron energy groups in homogeneous nodes, is presented. The boundary conditions used for analytic as solution are the four currents or fluxes on the surface of the node, which are obtained by Nodal Expansion Method (known as NEM) and four fluxes at the vertices of a node calculated using the finite difference method. The analytical solution found is the homogeneous distribution of neutron flux. Detailed distributions pin to pin inside a fuel assembly are estimated by the product of homogeneous flux distribution by local heterogeneous form function. Furthermore, the form functions of flux and power are used. The results obtained with this method have a good accuracy when compared with reference values. (author)

  9. OPTIMAL METHOD FOR PREPARATION OF SILICATE ROCK SAMPLES FOR ANALYTICAL PURPOSES

    Directory of Open Access Journals (Sweden)

    Maja Vrkljan

    2004-12-01

    Full Text Available The purpose of this study was to determine an optimal dissolution method for silicate rock samples for further analytical purposes. Analytical FAAS method of determining cobalt, chromium, copper, nickel, lead and zinc content in gabbro sample and geochemical standard AGV-1 has been applied for verification. Dissolution in mixtures of various inorganic acids has been tested, as well as Na2CO3 fusion technique. The results obtained by different methods have been compared and dissolution in the mixture of HNO3 + HF has been recommended as optimal.

  10. The auxiliary field method and approximate analytical solutions of the Schroedinger equation with exponential potentials

    Energy Technology Data Exchange (ETDEWEB)

    Silvestre-Brac, Bernard [LPSC Universite Joseph Fourier, Grenoble 1, CNRS/IN2P3, Institut Polytechnique de Grenoble, Avenue des Martyrs 53, F-38026 Grenoble-Cedex (France); Semay, Claude; Buisseret, Fabien [Groupe de Physique Nucleaire Theorique, Universite de Mons-Hainaut, Academie universitaire Wallonie-Bruxelles, Place du Parc 20, B-7000 Mons (Belgium)], E-mail: silvestre@lpsc.in2p3.fr, E-mail: claude.semay@umh.ac.be, E-mail: fabien.buisseret@umh.ac.be

    2009-06-19

    The auxiliary field method is a new and efficient way to compute approximate analytical eigenenergies of the Schroedinger equation. This method has already been successfully applied to the case of central potentials of power-law and logarithmic forms. In the present work, we show that the Schroedinger equation with exponential potentials of the form -{alpha}r{sup {lambda}}exp(-{beta}r) can also be analytically solved by using the auxiliary field method. Closed formulae giving the critical heights and the energy levels of these potentials are presented. Special attention is drawn to the Yukawa potential and the pure exponential potential.

  11. The auxiliary field method and approximate analytical solutions of the Schroedinger equation with exponential potentials

    International Nuclear Information System (INIS)

    Silvestre-Brac, Bernard; Semay, Claude; Buisseret, Fabien

    2009-01-01

    The auxiliary field method is a new and efficient way to compute approximate analytical eigenenergies of the Schroedinger equation. This method has already been successfully applied to the case of central potentials of power-law and logarithmic forms. In the present work, we show that the Schroedinger equation with exponential potentials of the form -αr λ exp(-βr) can also be analytically solved by using the auxiliary field method. Closed formulae giving the critical heights and the energy levels of these potentials are presented. Special attention is drawn to the Yukawa potential and the pure exponential potential

  12. Analytical method for determining colour intensities based on Cherenkov radiation colour quenching

    Energy Technology Data Exchange (ETDEWEB)

    Gonzalez-Gomez, C; Lopez-Gonzalez, J deD; Ferro-Garcia, M A [Univ. of Granada, Granada (Spain). Faculty of Sciences, Dept. of Inorganic Chemistry. Radiochemistry Section; Consejo Superior de Investigaciones Cientificas, Granada (Spain). Dept. of Chemical Research Coordinated Centre)

    1983-01-01

    A study was made for determining color intensities using as luminous non-monochromatic source produced by the Cherenkov emission in the walls of a glass capillary which acts as luminous source itself inside the colored solution to be evaluated. The reproducibility of this method has been compared with the spectrophotometric assay; the relative errors of both analytical methods have been calculated for different concentrations of congo red solution in the range of minimal error, according to Ringbom's criterion. The sensitivity of this analytical method has been studied for the two ..beta..-emitters employed: /sup 90/Sr//sup 90/Y and /sup 204/Tl.

  13. A Novel Reliability Enhanced Handoff Method in Future Wireless Heterogeneous Networks

    Directory of Open Access Journals (Sweden)

    Wang YuPeng

    2016-01-01

    Full Text Available As the demand increases, future networks will follow the trends of network variety and service flexibility, which requires heterogeneous type of network deployment and reliable communication method. In practice, most communication failure happens due to the bad radio link quality, i.e., high-speed users suffers a lot on the problem of radio link failure, which causes the problem of communication interrupt and radio link recovery. To make the communication more reliable, especially for the high mobility users, we propose a novel communication handoff mechanism to reduce the occurrence of service interrupt. Based on computer simulation, we find that the reliability on the service is greatly improved.

  14. Reliability analysis for thermal cutting method based non-explosive separation device

    International Nuclear Information System (INIS)

    Choi, Jun Woo; Hwang, Kuk Ha; Kim, Byung Kyu

    2016-01-01

    In order to increase the reliability of a separation device for a small satellite, a new non-explosive separation device is invented. This device is activated using a thermal cutting method with a Ni-Cr wire. A reliability analysis is carried out for the proposed non-explosive separation device by applying the Fault tree analysis (FTA) method. In the FTA results for the separation device, only ten single-point failure modes are found. The reliability modeling and analysis for the device are performed considering failure of the power supply, the Ni-Cr wire burns failure and unwinds, the holder separation failure, the balls separation failure, and the pin release failure. Ultimately, the reliability of the proposed device is calculated as 0.999989 with five Ni-Cr wire coils

  15. Reliability analysis for thermal cutting method based non-explosive separation device

    Energy Technology Data Exchange (ETDEWEB)

    Choi, Jun Woo; Hwang, Kuk Ha; Kim, Byung Kyu [Korea Aerospace University, Goyang (Korea, Republic of)

    2016-12-15

    In order to increase the reliability of a separation device for a small satellite, a new non-explosive separation device is invented. This device is activated using a thermal cutting method with a Ni-Cr wire. A reliability analysis is carried out for the proposed non-explosive separation device by applying the Fault tree analysis (FTA) method. In the FTA results for the separation device, only ten single-point failure modes are found. The reliability modeling and analysis for the device are performed considering failure of the power supply, the Ni-Cr wire burns failure and unwinds, the holder separation failure, the balls separation failure, and the pin release failure. Ultimately, the reliability of the proposed device is calculated as 0.999989 with five Ni-Cr wire coils.

  16. Case study on the use of PSA methods: Human reliability analysis

    International Nuclear Information System (INIS)

    1991-04-01

    The overall objective of treating human reliability in a probabilistic safety analysis is to ensure that the key human interactions of typical crews are accurately and systematically incorporated into the study in a traceable manner. An additional objective is to make the human reliability analysis (HRA) as realistic as possible, taking into account the emergency procedures, the man-machine interface, the focus of training process, and the knowledge and experience of the crews. Section 3 of the paper describes an overview of this analytical process which leads to three more detailed example problems described in Section 4. Section 5 discusses a peer review process. References are presented that are useful in performing HRAs. In addition appendices are provided for definitions, selected data and a generic list of performance shaping factors. 35 refs, figs and tabs

  17. An attempt to use FMEA method for an approximate reliability assessment of machinery

    Directory of Open Access Journals (Sweden)

    Przystupa Krzysztof

    2017-01-01

    Full Text Available The paper presents a modified FMEA (Failure Mode and Effect Analysis method to assess reliability of the components that make up a wrench type 2145: MAX Impactol TM Driver Ingersoll Rand Company. This case concerns the analysis of reliability in conditions, when full service data is not known. The aim of the study is to determine the weakest element in the design of the tool.

  18. Method of analytic continuation by duality in QCD: Beyond QCD sum rules

    International Nuclear Information System (INIS)

    Kremer, M.; Nasrallah, N.F.; Papadopoulos, N.A.; Schilcher, K.

    1986-01-01

    We present the method of analytic continuation by duality which allows the approximate continuation of QCD amplitudes to small values of the momentum variables where direct perturbative calculations are not possible. This allows a substantial extension of the domain of applications of hadronic QCD phenomenology. The method is illustrated by a simple example which shows its essential features

  19. Flammable gas safety program. Analytical methods development: FY 1994 progress report

    International Nuclear Information System (INIS)

    Campbell, J.A.; Clauss, S.; Grant, K.; Hoopes, V.; Lerner, B.; Lucke, R.; Mong, G.; Rau, J.; Wahl, K.; Steele, R.

    1994-09-01

    This report describes the status of developing analytical methods to account for the organic components in Hanford waste tanks, with particular focus on tanks assigned to the Flammable Gas Watch List. The methods that have been developed are illustrated by their application to samples obtained from Tank 241-SY-101 (Tank 101-SY)

  20. Analytical method for high resolution liquid chromatography for quality control French Macaw

    International Nuclear Information System (INIS)

    Garcia Penna, Caridad M; Torres Amaro, Leonid; Menendez Castillo, Rosa; Sanchez, Esther; Martinez Espinosa, Vivian; Gonzalez, Maria Lidia; Rodriguez, Carlos

    2007-01-01

    Was developed and validated an analytical method for high resolution liquid chromatography applicable to quality control of drugs dry French Macaw (Senna alata L. Roxb.) With ultraviolet detection at 340 nm. The method for high resolution liquid chromatography used to quantify the sennosides A and B, main components, was validated and proved to be specific, linear, precise and accurate. (Author)

  1. Approximate Analytic and Numerical Solutions to Lane-Emden Equation via Fuzzy Modeling Method

    Directory of Open Access Journals (Sweden)

    De-Gang Wang

    2012-01-01

    Full Text Available A novel algorithm, called variable weight fuzzy marginal linearization (VWFML method, is proposed. This method can supply approximate analytic and numerical solutions to Lane-Emden equations. And it is easy to be implemented and extended for solving other nonlinear differential equations. Numerical examples are included to demonstrate the validity and applicability of the developed technique.

  2. Contextual and Analytic Qualities of Research Methods Exemplified in Research on Teaching

    Science.gov (United States)

    Svensson, Lennart; Doumas, Kyriaki

    2013-01-01

    The aim of the present article is to discuss contextual and analytic qualities of research methods. The arguments are specified in relation to research on teaching. A specific investigation is used as an example to illustrate the general methodological approach. It is argued that research methods should be carefully grounded in an understanding of…

  3. An analytical nodal method for time-dependent one-dimensional discrete ordinates problems

    International Nuclear Information System (INIS)

    Barros, R.C. de

    1992-01-01

    In recent years, relatively little work has been done in developing time-dependent discrete ordinates (S N ) computer codes. Therefore, the topic of time integration methods certainly deserves further attention. In this paper, we describe a new coarse-mesh method for time-dependent monoenergetic S N transport problesm in slab geometry. This numerical method preserves the analytic solution of the transverse-integrated S N nodal equations by constants, so we call our method the analytical constant nodal (ACN) method. For time-independent S N problems in finite slab geometry and for time-dependent infinite-medium S N problems, the ACN method generates numerical solutions that are completely free of truncation errors. Bsed on this positive feature, we expect the ACN method to be more accurate than conventional numerical methods for S N transport calculations on coarse space-time grids

  4. Method for assessing software reliability of the document management system using the RFID technology

    Directory of Open Access Journals (Sweden)

    Kiedrowicz Maciej

    2016-01-01

    Full Text Available The deliberations presented in this study refer to the method for assessing software reliability of the docu-ment management system, using the RFID technology. A method for determining the reliability structure of the dis-cussed software, understood as the index vector for assessing reliability of its components, was proposed. The model of the analyzed software is the control transfer graph, in which the probability of activating individual components during the system's operation results from the so-called operational profile, which characterizes the actual working environment. The reliability structure is established as a result of the solution of a specific mathematical software task. The knowledge of the reliability structure of the software makes it possible to properly plan the time and finan-cial expenses necessary to build the software, which would meet the reliability requirements. The application of the presented method is illustrated by the number example, corresponding to the software reality of the RFID document management system.

  5. System and Method for Providing a Climate Data Analytic Services Application Programming Interface Distribution Package

    Science.gov (United States)

    Schnase, John L. (Inventor); Duffy, Daniel Q. (Inventor); Tamkin, Glenn S. (Inventor)

    2016-01-01

    A system, method and computer-readable storage devices for providing a climate data analytic services application programming interface distribution package. The example system can provide various components. The system provides a climate data analytic services application programming interface library that enables software applications running on a client device to invoke the capabilities of a climate data analytic service. The system provides a command-line interface that provides a means of interacting with a climate data analytic service by issuing commands directly to the system's server interface. The system provides sample programs that call on the capabilities of the application programming interface library and can be used as templates for the construction of new client applications. The system can also provide test utilities, build utilities, service integration utilities, and documentation.

  6. Design Optimization Method for Composite Components Based on Moment Reliability-Sensitivity Criteria

    Science.gov (United States)

    Sun, Zhigang; Wang, Changxi; Niu, Xuming; Song, Yingdong

    2017-08-01

    In this paper, a Reliability-Sensitivity Based Design Optimization (RSBDO) methodology for the design of the ceramic matrix composites (CMCs) components has been proposed. A practical and efficient method for reliability analysis and sensitivity analysis of complex components with arbitrary distribution parameters are investigated by using the perturbation method, the respond surface method, the Edgeworth series and the sensitivity analysis approach. The RSBDO methodology is then established by incorporating sensitivity calculation model into RBDO methodology. Finally, the proposed RSBDO methodology is applied to the design of the CMCs components. By comparing with Monte Carlo simulation, the numerical results demonstrate that the proposed methodology provides an accurate, convergent and computationally efficient method for reliability-analysis based finite element modeling engineering practice.

  7. A generic method for assignment of reliability scores applied to solvent accessibility predictions

    DEFF Research Database (Denmark)

    Petersen, Bent; Petersen, Thomas Nordahl; Andersen, Pernille

    2009-01-01

    : The performance of the neural networks was evaluated on a commonly used set of sequences known as the CB513 set. An overall Pearson's correlation coefficient of 0.72 was obtained, which is comparable to the performance of the currently best public available method, Real-SPINE. Both methods associate a reliability...... comparing the Pearson's correlation coefficient for the upper 20% of predictions sorted according to reliability. For this subset, values of 0.79 and 0.74 are obtained using our and the compared method, respectively. This tendency is true for any selected subset....

  8. Predictive ability of the feeding system in Iberian pig by means of several analytical methods

    Directory of Open Access Journals (Sweden)

    González, E.

    2013-04-01

    Full Text Available The reliability of several analytical methods proposed to predict the feeding system received by Iberian pigs during the fattening period has been contrasted. Samples of subcutaneous adipose tissue were analyzed from 38 batches of pigs fattened in three seasons of montanera (acorn and pastures feeding. They corresponded to the four categories described in the Quality Standard for Iberian pig products: 251 samples of bellota, 164 of recebo, 197 of cebo de campo and 137 of cebo. To perform the study, the following analytical methods were used: fatty acid quantification, NIR, alpha and gamma tocopherol, chemical sensor, triacilglycerides, stable isotopes and neophytadiene. The laboratories received the samples without any information about the fattening system to which they belonged and remitted their predictions with respect to the above categories. The results showed a high percentage of accurate predictions of the methods when the fattening type corresponds to the extreme categories (bellota and cebo, however, the methods had difficulty in discerning between samples from a mixed feeding regime with acorn and feed (recebo and problems when pigs are fattened with compound feeds including vegetable fats with high levels of oleic acid. Although a simplification into only two categories (cebo/campo and recebo/bellota results in a success rate higher than 90% for some methods, the combination of two or three techniques with problematic samples allows for differentiating among the four categories with the same accuracy.Se ha contrastado la fiabilidad de varios métodos analíticos para determinar el tipo de alimentación recibida durante el cebo por cerdos Ibéricos a partir de muestras de tejido adiposo subcutáneo, procedentes de 38 partidas de cerdos de tres campañas de montanera. Las muestras correspondieron con las categorías de alimentación contempladas en la Norma de Calidad: 251 fueron de bellota, 164 de recebo, 197 de campo y 137 de cebo

  9. A new analytical method to solve the heat equation for a multi-dimensional composite slab

    International Nuclear Information System (INIS)

    Lu, X; Tervola, P; Viljanen, M

    2005-01-01

    A novel analytical approach has been developed for heat conduction in a multi-dimensional composite slab subject to time-dependent boundary changes of the first kind. Boundary temperatures are represented as Fourier series. Taking advantage of the periodic properties of boundary changes, the analytical solution is obtained and expressed explicitly. Nearly all the published works necessitate searching for associated eigenvalues in solving such a problem even for a one-dimensional composite slab. In this paper, the proposed method involves no iterative computation such as numerically searching for eigenvalues and no residue evaluation. The adopted method is simple which represents an extension of the novel analytical approach derived for the one-dimensional composite slab. Moreover, the method of 'separation of variables' employed in this paper is new. The mathematical formula for solutions is concise and straightforward. The physical parameters are clearly shown in the formula. Further comparison with numerical calculations is presented

  10. A Table Lookup Method for Exact Analytical Solutions of Nonlinear Fractional Partial Differential Equations

    Directory of Open Access Journals (Sweden)

    Ji Juan-Juan

    2017-01-01

    Full Text Available A table lookup method for solving nonlinear fractional partial differential equations (fPDEs is proposed in this paper. Looking up the corresponding tables, we can quickly obtain the exact analytical solutions of fPDEs by using this method. To illustrate the validity of the method, we apply it to construct the exact analytical solutions of four nonlinear fPDEs, namely, the time fractional simplified MCH equation, the space-time fractional combined KdV-mKdV equation, the (2+1-dimensional time fractional Zoomeron equation, and the space-time fractional ZKBBM equation. As a result, many new types of exact analytical solutions are obtained including triangular periodic solution, hyperbolic function solution, singular solution, multiple solitary wave solution, and Jacobi elliptic function solution.

  11. Simplified Analytical Methods to Analyze Lock Gates Submitted to Ship Collisions and Earthquakes

    Directory of Open Access Journals (Sweden)

    Buldgen Loic

    2015-09-01

    Full Text Available This paper presents two simplified analytical methods to analyze lock gates submitted to two different accidental loads. The case of an impact involving a vessel is first investigated. In this situation, the resistance of the struck gate is evaluated by assuming a local and a global deforming mode. The super-element method is used in the first case, while an equivalent beam model is simultaneously introduced to capture the overall bending motion of the structure. The second accidental load considered in this paper is the seismic action, for which an analytical method is presented to evaluate the total hydrodynamic pressure applied on a lock gate during an earthquake, due account being taken of the fluid-structure interaction. For each of these two actions, numerical validations are presented and the analytical results are compared to finite-element solutions.

  12. Development of CAD implementing the algorithm of boundary elements’ numerical analytical method

    Directory of Open Access Journals (Sweden)

    Yulia V. Korniyenko

    2015-03-01

    Full Text Available Up to recent days the algorithms for numerical-analytical boundary elements method had been implemented with programs written in MATLAB environment language. Each program had a local character, i.e. used to solve a particular problem: calculation of beam, frame, arch, etc. Constructing matrices in these programs was carried out “manually” therefore being time-consuming. The research was purposed onto a reasoned choice of programming language for new CAD development, allows to implement algorithm of numerical analytical boundary elements method and to create visualization tools for initial objects and calculation results. Research conducted shows that among wide variety of programming languages the most efficient one for CAD development, employing the numerical analytical boundary elements method algorithm, is the Java language. This language provides tools not only for development of calculating CAD part, but also to build the graphic interface for geometrical models construction and calculated results interpretation.

  13. A method to evaluate performance reliability of individual subjects in laboratory research applied to work settings.

    Science.gov (United States)

    1978-10-01

    This report presents a method that may be used to evaluate the reliability of performance of individual subjects, particularly in applied laboratory research. The method is based on analysis of variance of a tasks-by-subjects data matrix, with all sc...

  14. Progress in analytical methods for the detection of geographical origin and authenticity of tea (Camellia sinensis)

    International Nuclear Information System (INIS)

    Yuan Yuwei; Hu Guixian; Shao Shengzhi; Zhang Yongzhi; Zhang Yu; Zhu Jiahong; Yang Guiling; Zhang Zhiheng

    2013-01-01

    Tea (Camellia sinensis) is one of the important agricultural products with obvious regional characteristics. Analytical methods are very important for the protection of geographical origin and authenticity of tea. The developments of analytical methods including stable isotope determination, multi-elements determination, near infrared reflectance spectroscopy, chemical fingerprint and others were reviewed. Major problems on tea origin and authenticity detection were discussed in this study, and some suggestions were also proposed which would be useful for the protection of geographical origin of tea in China. (authors)

  15. Possibilities of Utilizing the Method of Analytical Hierarchy Process Within the Strategy of Corporate Social Business

    Science.gov (United States)

    Drieniková, Katarína; Hrdinová, Gabriela; Naňo, Tomáš; Sakál, Peter

    2010-01-01

    The paper deals with the analysis of the theory of corporate social responsibility, risk management and the exact method of analytic hierarchic process that is used in the decision-making processes. The Chapters 2 and 3 focus on presentation of the experience with the application of the method in formulating the stakeholders' strategic goals within the Corporate Social Responsibility (CSR) and simultaneously its utilization in minimizing the environmental risks. The major benefit of this paper is the application of Analytical Hierarchy Process (AHP).

  16. Comparison of three analytical methods for the determination of trace elements in whole blood

    International Nuclear Information System (INIS)

    Ward, N.I.; Stephens, R.; Ryan, D.E.

    1979-01-01

    Three different analytical techniques were compared in a study of the role of trace elements in multiple sclerosis. Data for eight elements (Cd, Co, Cr, Cu, Mg, Mn, Pb, Zn) from neutron activation, flame atomic absorption and electrothermal atomic absorption methods were compared and evaluated statistically. No difference (probability less than 0.001) was observed in the elemental values obtained. Comparison of data between suitably different analytical methods gives increased confidence in the results obtained and is of particular value when standard reference materials are not available. (Auth.)

  17. Analytical method and result of radiation exposure for depressurization accident of HTTR

    International Nuclear Information System (INIS)

    Sawa, K.; Shiozawa, S.; Mikami, H.

    1990-01-01

    The Japan Atomic Energy Research Institute (JAERI) is now proceeding with the construction design of the High Temperature Engineering Test Reactor (HTTR). Since the HTTR has some characteristics different from LWRs, analytical method of radiation exposure in accidents provided for LWRs can not be applied directly. This paper describes the analytical method of radiation exposure developed by JAERI for the depressurization accident, which is the severest accident in respect to radiation exposure among the design basis accidents of the HTTR. The result is also described in this paper

  18. Advantages of Analytical Transformations in Monte Carlo Methods for Radiation Transport

    International Nuclear Information System (INIS)

    McKinley, M S; Brooks III, E D; Daffin, F

    2004-01-01

    Monte Carlo methods for radiation transport typically attempt to solve an integral by directly sampling analog or weighted particles, which are treated as physical entities. Improvements to the methods involve better sampling, probability games or physical intuition about the problem. We show that significant improvements can be achieved by recasting the equations with an analytical transform to solve for new, non-physical entities or fields. This paper looks at one such transform, the difference formulation for thermal photon transport, showing a significant advantage for Monte Carlo solution of the equations for time dependent transport. Other related areas are discussed that may also realize significant benefits from similar analytical transformations

  19. A generic method for assignment of reliability scores applied to solvent accessibility predictions

    Directory of Open Access Journals (Sweden)

    Nielsen Morten

    2009-07-01

    Full Text Available Abstract Background Estimation of the reliability of specific real value predictions is nontrivial and the efficacy of this is often questionable. It is important to know if you can trust a given prediction and therefore the best methods associate a prediction with a reliability score or index. For discrete qualitative predictions, the reliability is conventionally estimated as the difference between output scores of selected classes. Such an approach is not feasible for methods that predict a biological feature as a single real value rather than a classification. As a solution to this challenge, we have implemented a method that predicts the relative surface accessibility of an amino acid and simultaneously predicts the reliability for each prediction, in the form of a Z-score. Results An ensemble of artificial neural networks has been trained on a set of experimentally solved protein structures to predict the relative exposure of the amino acids. The method assigns a reliability score to each surface accessibility prediction as an inherent part of the training process. This is in contrast to the most commonly used procedures where reliabilities are obtained by post-processing the output. Conclusion The performance of the neural networks was evaluated on a commonly used set of sequences known as the CB513 set. An overall Pearson's correlation coefficient of 0.72 was obtained, which is comparable to the performance of the currently best public available method, Real-SPINE. Both methods associate a reliability score with the individual predictions. However, our implementation of reliability scores in the form of a Z-score is shown to be the more informative measure for discriminating good predictions from bad ones in the entire range from completely buried to fully exposed amino acids. This is evident when comparing the Pearson's correlation coefficient for the upper 20% of predictions sorted according to reliability. For this subset, values of 0

  20. The Evaluation Method of the Lightning Strike on Transmission Lines Aiming at Power Grid Reliability

    Science.gov (United States)

    Wen, Jianfeng; Wu, Jianwei; Huang, Liandong; Geng, Yinan; Yu, zhanqing

    2018-01-01

    Lightning protection of power system focuses on reducing the flashover rate, only distinguishing by the voltage level, without considering the functional differences between the transmission lines, and being lack of analysis the effect on the reliability of power grid. This will lead lightning protection design of general transmission lines is surplus but insufficient for key lines. In order to solve this problem, the analysis method of lightning striking on transmission lines for power grid reliability is given. Full wave process theory is used to analyze the lightning back striking; the leader propagation model is used to describe the process of shielding failure of transmission lines. The index of power grid reliability is introduced and the effect of transmission line fault on the reliability of power system is discussed in detail.

  1. Investigation of Reliabilities of Bolt Distances for Bolted Structural Steel Connections by Monte Carlo Simulation Method

    Directory of Open Access Journals (Sweden)

    Ertekin Öztekin Öztekin

    2015-12-01

    Full Text Available Design of the distance of bolts to each other and design of the distance of bolts to the edge of connection plates are made based on minimum and maximum boundary values proposed by structural codes. In this study, reliabilities of those distances were investigated. For this purpose, loading types, bolt types and plate thicknesses were taken as variable parameters. Monte Carlo Simulation (MCS method was used in the reliability computations performed for all combination of those parameters. At the end of study, all reliability index values for all those distances were presented in graphics and tables. Results obtained from this study compared with the values proposed by some structural codes and finally some evaluations were made about those comparisons. Finally, It was emphasized in the end of study that, it would be incorrect of the usage of the same bolt distances in the both traditional designs and the higher reliability level designs.

  2. Net Analyte Signal Standard Additions Method for Simultaneous Determination of Sulfamethoxazole and Trimethoprim in Pharmaceutical Formulations and Biological Fluids

    OpenAIRE

    Givianrad, M. H.; Mohagheghian, M.

    2012-01-01

    The applicability of a novel net analyte signal standard addition method (NASSAM) to the resolving of overlapping spectra corresponding to the sulfamethoxazole and trimethoprim was verified by UV-visible spectrophotometry. The results confirmed that the net analyte signal standard additions method with simultaneous addition of both analytes is suitable for the simultaneous determination of sulfamethoxazole and trimethoprim in aqueous media. Moreover, applying the net analyte signal standard a...

  3. An Intelligent Method for Structural Reliability Analysis Based on Response Surface

    Institute of Scientific and Technical Information of China (English)

    桂劲松; 刘红; 康海贵

    2004-01-01

    As water depth increases, the structural safety and reliability of a system become more and more important and challenging. Therefore, the structural reliability method must be applied in ocean engineering design such as offshore platform design. If the performance function is known in structural reliability analysis, the first-order second-moment method is often used. If the performance function could not be definitely expressed, the response surface method is always used because it has a very clear train of thought and simple programming. However, the traditional response surface method fits the response surface of quadratic polynomials where the problem of accuracy could not be solved, because the true limit state surface can be fitted well only in the area near the checking point. In this paper, an intelligent computing method based on the whole response surface is proposed, which can be used for the situation where the performance function could not be definitely expressed in structural reliability analysis. In this method, a response surface of the fuzzy neural network for the whole area should be constructed first, and then the structural reliability can be calculated by the genetic algorithm. In the proposed method, all the sample points for the training network come from the whole area, so the true limit state surface in the whole area can be fitted. Through calculational examples and comparative analysis, it can be known that the proposed method is much better than the traditional response surface method of quadratic polynomials, because, the amount of calculation of finite element analysis is largely reduced, the accuracy of calculation is improved,and the true limit state surface can be fitted very well in the whole area. So, the method proposed in this paper is suitable for engineering application.

  4. A Bayesian reliability evaluation method with integrated accelerated degradation testing and field information

    International Nuclear Information System (INIS)

    Wang, Lizhi; Pan, Rong; Li, Xiaoyang; Jiang, Tongmin

    2013-01-01

    Accelerated degradation testing (ADT) is a common approach in reliability prediction, especially for products with high reliability. However, oftentimes the laboratory condition of ADT is different from the field condition; thus, to predict field failure, one need to calibrate the prediction made by using ADT data. In this paper a Bayesian evaluation method is proposed to integrate the ADT data from laboratory with the failure data from field. Calibration factors are introduced to calibrate the difference between the lab and the field conditions so as to predict a product's actual field reliability more accurately. The information fusion and statistical inference procedure are carried out through a Bayesian approach and Markov chain Monte Carlo methods. The proposed method is demonstrated by two examples and the sensitivity analysis to prior distribution assumption

  5. The Monte Carlo Simulation Method for System Reliability and Risk Analysis

    CERN Document Server

    Zio, Enrico

    2013-01-01

    Monte Carlo simulation is one of the best tools for performing realistic analysis of complex systems as it allows most of the limiting assumptions on system behavior to be relaxed. The Monte Carlo Simulation Method for System Reliability and Risk Analysis comprehensively illustrates the Monte Carlo simulation method and its application to reliability and system engineering. Readers are given a sound understanding of the fundamentals of Monte Carlo sampling and simulation and its application for realistic system modeling.   Whilst many of the topics rely on a high-level understanding of calculus, probability and statistics, simple academic examples will be provided in support to the explanation of the theoretical foundations to facilitate comprehension of the subject matter. Case studies will be introduced to provide the practical value of the most advanced techniques.   This detailed approach makes The Monte Carlo Simulation Method for System Reliability and Risk Analysis a key reference for senior undergra...

  6. Study on reliability analysis based on multilevel flow models and fault tree method

    International Nuclear Information System (INIS)

    Chen Qiang; Yang Ming

    2014-01-01

    Multilevel flow models (MFM) and fault tree method describe the system knowledge in different forms, so the two methods express an equivalent logic of the system reliability under the same boundary conditions and assumptions. Based on this and combined with the characteristics of MFM, a method mapping MFM to fault tree was put forward, thus providing a way to establish fault tree rapidly and realizing qualitative reliability analysis based on MFM. Taking the safety injection system of pressurized water reactor nuclear power plant as an example, its MFM was established and its reliability was analyzed qualitatively. The analysis result shows that the logic of mapping MFM to fault tree is correct. The MFM is easily understood, created and modified. Compared with the traditional fault tree analysis, the workload is greatly reduced and the modeling time is saved. (authors)

  7. An analytical-numerical comprehensive method for optimizing the fringing magnetic field

    International Nuclear Information System (INIS)

    Xiao Meiqin; Mao Naifeng

    1991-01-01

    The criterion of optimizing the fringing magnetic field is discussed, and an analytical-numerical comprehensive method for realizing the optimization is introduced. The method mentioned above consists of two parts, the analytical part calculates the field of the shims, which corrects the fringing magnetic field by using uniform magnetizing method; the numerical part fulfils the whole calculation of the field distribution by solving the equation of magnetic vector potential A within the region covered by arbitrary triangular meshes with the aid of finite difference method and successive over relaxation method. On the basis of the method, the optimization of the fringing magnetic field for a large-scale electromagnetic isotope separator is finished

  8. Introduction on microbiological and biological methods and their possible combination with other analytical techniques for the detection of irradiated food

    International Nuclear Information System (INIS)

    Leonardi, M.

    1991-01-01

    Food irradiation is a physical method of processing and preserving food. One of the main purposes of the application of this technology to food is to obtain specific biological effects on the treated foodstuff. Typical examples of these treatment effects are listed in the article. A whole range of techniques is at disposal of the analyst to assure the Quality Control (QC) of various foodstuffs. They are based on microbiological, organoleptical, chemical, biochemical, immunological and/or physical methods. In the case of irradiation preserved food the opinion of the writer is that very often only a combination of analytical methods can solve the problem of detection of irradiated foodstuffs and in particular in most cases this combination could be formed by a biological or microbiological method + a chemical or physical one. The meaning of these combination of techniques is manifold. Combining the advantages of a rapid screening method with those of a more refined, reliable, even if more time consuming one; offering the possibility to carry out the analysis for the control of irradiated foodstuffs to different kinds of food control laboratories, often equipped in a different way, are some of the most evident advantages. These methods are briefly explained. At present, none method seems promising for the quantitative determination of the irradiation dose. Moreover, some of the proposed methods can only give a good presumption of the irradiation treatment applied to particular foodstuffs. (18 refs)

  9. Experimental design and multiple response optimization. Using the desirability function in analytical methods development.

    Science.gov (United States)

    Candioti, Luciana Vera; De Zan, María M; Cámara, María S; Goicoechea, Héctor C

    2014-06-01

    A review about the application of response surface methodology (RSM) when several responses have to be simultaneously optimized in the field of analytical methods development is presented. Several critical issues like response transformation, multiple response optimization and modeling with least squares and artificial neural networks are discussed. Most recent analytical applications are presented in the context of analytLaboratorio de Control de Calidad de Medicamentos (LCCM), Facultad de Bioquímica y Ciencias Biológicas, Universidad Nacional del Litoral, C.C. 242, S3000ZAA Santa Fe, ArgentinaLaboratorio de Control de Calidad de Medicamentos (LCCM), Facultad de Bioquímica y Ciencias Biológicas, Universidad Nacional del Litoral, C.C. 242, S3000ZAA Santa Fe, Argentinaical methods development, especially in multiple response optimization procedures using the desirability function. Copyright © 2014 Elsevier B.V. All rights reserved.

  10. Comparative analysis of methods for real-time analytical control of chemotherapies preparations.

    Science.gov (United States)

    Bazin, Christophe; Cassard, Bruno; Caudron, Eric; Prognon, Patrice; Havard, Laurent

    2015-10-15

    Control of chemotherapies preparations are now an obligation in France, though analytical control is compulsory. Several methods are available and none of them is presumed as ideal. We wanted to compare them so as to determine which one could be the best choice. We compared non analytical (visual and video-assisted, gravimetric) and analytical (HPLC/FIA, UV/FT-IR, UV/Raman, Raman) methods thanks to our experience and a SWOT analysis. The results of the analysis show great differences between the techniques, but as expected none us them is without defects. However they can probably be used in synergy. Overall for the pharmacist willing to get involved, the implementation of the control for chemotherapies preparations must be widely anticipated, with the listing of every parameter, and remains according to us an analyst's job. Copyright © 2015 Elsevier B.V. All rights reserved.

  11. Analytical methods used at IPR (Instituto de Pesquisas Radioativas - Minas Gerais, Brazil)

    International Nuclear Information System (INIS)

    Murta, C.C.

    The analytical methods available at IPR (MG-Brazil) for the routine determination of uranium are described. These methods are: gravimetric analysis; fluorescence spectroscopy, voltametry, polarography, absorption spectroscopy, beta-and gamma-radiometric analysis, gamma spectroscopy, activation analysis, X-rays fluorescence analysis and delayed neutron analysis. Some additional methods for the study of mineral ores, such as X-rays diffractometry, emmission spectroscopy, thermal analysis, etc, are also discussed [pt

  12. The use of nuclear analytical methods in the investigation of objects of art and historical monuments

    International Nuclear Information System (INIS)

    Janovsky, I.

    2006-01-01

    Special nuclear analytical methods contribute significantly to the identification of the origin, manufacturing technology and/or authenticity of objects of art and historical monuments, Such methods primarily include variants of X-ray fluorescence analysis and activation analysis. The former enables non/destructive testing of materials, the latter features a high sensitivity. The article presents numerous examples of use of such methods especially in the Czech Republic (or former Czechoslovakia). (author)

  13. Structural system reliability calculation using a probabilistic fault tree analysis method

    Science.gov (United States)

    Torng, T. Y.; Wu, Y.-T.; Millwater, H. R.

    1992-01-01

    The development of a new probabilistic fault tree analysis (PFTA) method for calculating structural system reliability is summarized. The proposed PFTA procedure includes: developing a fault tree to represent the complex structural system, constructing an approximation function for each bottom event, determining a dominant sampling sequence for all bottom events, and calculating the system reliability using an adaptive importance sampling method. PFTA is suitable for complicated structural problems that require computer-intensive computer calculations. A computer program has been developed to implement the PFTA.

  14. Analytical Method Development for the Determination of Α-Endosulfan and Bifenthrin Pesticide Residues in Tea

    Directory of Open Access Journals (Sweden)

    Dyah Styarini

    2014-03-01

    Full Text Available The development of analytical method for the determination of α-endosulfan and bifenthrin residues in tea has been done. The complex matrices and also the pigment were the challenge in doing quantification of the pesticide residues in tea matrices. In order to get appropriate analysis method for the determination of pesticide residues in tea, the modification was done in the analytical method for the determination of organochlorine multiresidue in non fat matrices: seasoning and spicy that is published by Directorate General of Food Crops, Directorate of Food Plant Protection. The modification was done particularly in clean-up step to remove the interferences from the extract of tea matrices such as the pigment that usually interfere the measurement with Gas Chromatography (GC. The result showed that the MDL value for both analytes were 0.5 ng/g that were much lower than MRLs. The percent recovery obtained from the method was 78.58 and 90.19% for α-endosulfan and bifenthrin, respectively. The precision of the analysis method for both analytes were good since the % RSD values were below than the Horwitz’s value that was 19.18% at spiking level concentration of 300 ng/g.

  15. Reliability and Validity of the Footprint Assessment Method Using Photoshop CS5 Software.

    Science.gov (United States)

    Gutiérrez-Vilahú, Lourdes; Massó-Ortigosa, Núria; Costa-Tutusaus, Lluís; Guerra-Balic, Myriam

    2015-05-01

    Several sophisticated methods of footprint analysis currently exist. However, it is sometimes useful to apply standard measurement methods of recognized evidence with an easy and quick application. We sought to assess the reliability and validity of a new method of footprint assessment in a healthy population using Photoshop CS5 software (Adobe Systems Inc, San Jose, California). Forty-two footprints, corresponding to 21 healthy individuals (11 men with a mean ± SD age of 20.45 ± 2.16 years and 10 women with a mean ± SD age of 20.00 ± 1.70 years) were analyzed. Footprints were recorded in static bipedal standing position using optical podography and digital photography. Three trials for each participant were performed. The Hernández-Corvo, Chippaux-Smirak, and Staheli indices and the Clarke angle were calculated by manual method and by computerized method using Photoshop CS5 software. Test-retest was used to determine reliability. Validity was obtained by intraclass correlation coefficient (ICC). The reliability test for all of the indices showed high values (ICC, 0.98-0.99). Moreover, the validity test clearly showed no difference between techniques (ICC, 0.99-1). The reliability and validity of a method to measure, assess, and record the podometric indices using Photoshop CS5 software has been demonstrated. This provides a quick and accurate tool useful for the digital recording of morphostatic foot study parameters and their control.

  16. An analytical method for calculating stresses and strains of ATF cladding based on thick walled theory

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Dong Hyun; Kim, Hak Sung [Hanyang University, Seoul (Korea, Republic of); Kim, Hyo Chan; Yang, Yong Sik; In, Wang kee [KAERI, Daejeon (Korea, Republic of)

    2016-05-15

    In this paper, an analytical method based on thick walled theory has been studied to calculate stress and strain of ATF cladding. In order to prescribe boundary conditions of the analytical method, two algorithms were employed which are called subroutine 'Cladf' and 'Couple' of FRACAS, respectively. To evaluate the developed method, equivalent model using finite element method was established and stress components of the method were compared with those of equivalent FE model. One of promising ATF concepts is the coated cladding, which take advantages such as high melting point, a high neutron economy, and low tritium permeation rate. To evaluate the mechanical behavior and performance of the coated cladding, we need to develop the specified model to simulate the ATF behaviors in the reactor. In particular, the model for simulation of stress and strain for the coated cladding should be developed because the previous model, which is 'FRACAS', is for one body model. The FRACAS module employs the analytical method based on thin walled theory. According to thin-walled theory, radial stress is defined as zero but this assumption is not suitable for ATF cladding because value of the radial stress is not negligible in the case of ATF cladding. Recently, a structural model for multi-layered ceramic cylinders based on thick-walled theory was developed. Also, FE-based numerical simulation such as BISON has been developed to evaluate fuel performance. An analytical method that calculates stress components of ATF cladding was developed in this study. Thick-walled theory was used to derive equations for calculating stress and strain. To solve for these equations, boundary and loading conditions were obtained by subroutine 'Cladf' and 'Couple' and applied to the analytical method. To evaluate the developed method, equivalent FE model was established and its results were compared to those of analytical model. Based on the

  17. A human reliability based usability evaluation method for safety-critical software

    International Nuclear Information System (INIS)

    Boring, R. L.; Tran, T. Q.; Gertman, D. I.; Ragsdale, A.

    2006-01-01

    Boring and Gertman (2005) introduced a novel method that augments heuristic usability evaluation methods with that of the human reliability analysis method of SPAR-H. By assigning probabilistic modifiers to individual heuristics, it is possible to arrive at the usability error probability (UEP). Although this UEP is not a literal probability of error, it nonetheless provides a quantitative basis to heuristic evaluation. This method allows one to seamlessly prioritize and identify usability issues (i.e., a higher UEP requires more immediate fixes). However, the original version of this method required the usability evaluator to assign priority weights to the final UEP, thus allowing the priority of a usability issue to differ among usability evaluators. The purpose of this paper is to explore an alternative approach to standardize the priority weighting of the UEP in an effort to improve the method's reliability. (authors)

  18. Inter- and intra- observer reliability of risk assessment of repetitive work without an explicit method.

    Science.gov (United States)

    Eliasson, Kristina; Palm, Peter; Nyman, Teresia; Forsman, Mikael

    2017-07-01

    A common way to conduct practical risk assessments is to observe a job and report the observed long term risks for musculoskeletal disorders. The aim of this study was to evaluate the inter- and intra-observer reliability of ergonomists' risk assessments without the support of an explicit risk assessment method. Twenty-one experienced ergonomists assessed the risk level (low, moderate, high risk) of eight upper body regions, as well as the global risk of 10 video recorded work tasks. Intra-observer reliability was assessed by having nine of the ergonomists repeat the procedure at least three weeks after the first assessment. The ergonomists made their risk assessment based on his/her experience and knowledge. The statistical parameters of reliability included agreement in %, kappa, linearly weighted kappa, intraclass correlation and Kendall's coefficient of concordance. The average inter-observer agreement of the global risk was 53% and the corresponding weighted kappa (K w ) was 0.32, indicating fair reliability. The intra-observer agreement was 61% and 0.41 (K w ). This study indicates that risk assessments of the upper body, without the use of an explicit observational method, have non-acceptable reliability. It is therefore recommended to use systematic risk assessment methods to a higher degree. Copyright © 2017 The Authors. Published by Elsevier Ltd.. All rights reserved.

  19. Solution of the isotopic depletion equation using decomposition method and analytical solution

    Energy Technology Data Exchange (ETDEWEB)

    Prata, Fabiano S.; Silva, Fernando C.; Martinez, Aquilino S., E-mail: fprata@con.ufrj.br, E-mail: fernando@con.ufrj.br, E-mail: aquilino@lmp.ufrj.br [Coordenacao dos Programas de Pos-Graduacao de Engenharia (PEN/COPPE/UFRJ), RJ (Brazil). Programa de Engenharia Nuclear

    2011-07-01

    In this paper an analytical calculation of the isotopic depletion equations is proposed, featuring a chain of major isotopes found in a typical PWR reactor. Part of this chain allows feedback reactions of (n,2n) type. The method is based on decoupling the equations describing feedback from the rest of the chain by using the decomposition method, with analytical solutions for the other isotopes present in the chain. The method was implemented in a PWR reactor simulation code, that makes use of the nodal expansion method (NEM) to solve the neutron diffusion equation, describing the spatial distribution of neutron flux inside the reactor core. Because isotopic depletion calculation module is the most computationally intensive process within simulation systems of nuclear reactor core, it is justified to look for a method that is both efficient and fast, with the objective of evaluating a larger number of core configurations in a short amount of time. (author)

  20. Analytical method used for intermediate products in continuous distillation of furfural

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Z.L.; Jia, M.; Wang, L.J.; Deng, Y.X.

    1981-01-01

    During distillation of furfural, analysis of main components in the crude furfural condensate and intermediate products is very important. Since furfural and methylfurfural are homologous and both furfural and acetone contain a carbonyl group, components in the sample must be separated before analysis. An improved analytical method has been studied, the accuracy and precision of which would meet the requirement of industrial standards. The analytical procedure was provided as follows: to determine the furfural content with gravimetric method of barbituric acid; to determine the methanol content with dichromate method after precipitating furfural and acetone, and distilling the liquid for analysis; and to determine the methylfurfural content with bromide-bromate method, which can be used only in the sample containing higher content of methylfurfural. For the sample in low content, the gas-liquid chromatographic method can be used. 7 references.