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Sample records for polarizing neutron coatings

  1. Precision Polarization of Neutrons

    Science.gov (United States)

    Martin, Elise; Barron-Palos, Libertad; Couture, Aaron; Crawford, Christopher; Chupp, Tim; Danagoulian, Areg; Estes, Mary; Hona, Binita; Jones, Gordon; Klein, Andi; Penttila, Seppo; Sharma, Monisha; Wilburn, Scott

    2009-05-01

    Determining polarization of a cold neutron beam to high precision is required for the next generation neutron decay correlation experiments at the SNS, such as the proposed abBA and PANDA experiments. Precision polarimetry measurements were conducted at Los Alamos National Laboratory with the goal of determining the beam polarization to the level of 10-3 or better. The cold neutrons from FP12 were polarized using optically polarized ^3He gas as a spin filter, which has a highly spin-dependent absorption cross section. A second ^ 3He spin filter was used to analyze the neutron polarization after passing through a resonant RF spin rotator. A discussion of the experiment and results will be given.

  2. POLARIZED NEUTRONS IN RHIC

    Energy Technology Data Exchange (ETDEWEB)

    COURANT,E.D.

    1998-04-27

    There does not appear to be any obvious way to accelerate neutrons, polarized or otherwise, to high energies by themselves. To investigate the behavior of polarized neutrons the authors therefore have to obtain them by accelerating them as components of heavier nuclei, and then sorting out the contribution of the neutrons in the analysis of the reactions produced by the heavy ion beams. The best neutron carriers for this purpose are probably {sup 3}He nuclei and deuterons. A polarized deuteron is primarily a combination of a proton and a neutron with their spins pointing in the same direction; in the {sup 3}He nucleus the spins of the two protons are opposite and the net spin (and magnetic moment) is almost the same as that of a free neutron. Polarized ions other than protons may be accelerated, stored and collided in a ring such as RHIC provided the techniques proposed for polarized proton operation can be adapted (or replaced by other strategies) for these ions. To accelerate polarized particles in a ring, one must make provisions for overcoming the depolarizing resonances that occur at certain energies. These resonances arise when the spin tune (ratio of spin precession frequency to orbit frequency) resonates with a component present in the horizontal field. The horizontal field oscillates with the vertical motion of the particles (due to vertical focusing); its frequency spectrum is dominated by the vertical oscillation frequency and its modulation by the periodic structure of the accelerator ring. In addition, the magnet imperfections that distort the closed orbit vertically contain all integral Fourier harmonics of the orbit frequency.

  3. Imaging with Polarized Neutrons

    Directory of Open Access Journals (Sweden)

    Nikolay Kardjilov

    2018-01-01

    Full Text Available Owing to their zero charge, neutrons are able to pass through thick layers of matter (typically several centimeters while being sensitive to magnetic fields due to their intrinsic magnetic moment. Therefore, in addition to the conventional attenuation contrast image, the magnetic field inside and around a sample can be visualized by detecting changes of polarization in a transmitted beam. The method is based on the spatially resolved measurement of the cumulative precession angles of a collimated, polarized, monochromatic neutron beam that traverses a magnetic field or sample.

  4. A polarizing neutron periscope for neutron imaging

    International Nuclear Information System (INIS)

    Schulz, Michael; Boeni, Peter; Calzada, Elbio; Muehlbauer, Martin; Neubauer, Andreas; Schillinger, Burkhard

    2009-01-01

    Optical neutron polarizers like guides or benders destroy the collimation of a neutron beam due to multiple reflections or scattering. This makes them unsuitable for their use in polarized neutron radiography, because the beam collimation is essential to obtain high spatial resolution. We have developed a neutron polarizer based on the principle of an optical periscope with a zigzag double reflection on two parallel high-m supermirror polarizers. If the supermirrors are perfectly parallel and flat, the beam collimation is left unchanged by such a device. A first proof of concept version of this type of polarizer was built and tested. We expect to achieve a beam polarization of up to 99% with an improved version yet to be built.

  5. A polarizing neutron periscope for neutron imaging

    Energy Technology Data Exchange (ETDEWEB)

    Schulz, Michael [FRM II, Lichtenbergstr. 1, 85748 Garching (Germany); Technische Universitaet Muenchen, Physik Department E21, James Franck Strasse, 85748 Garching (Germany)], E-mail: Michael.Schulz@frm2.tum.de; Boeni, Peter [Technische Universitaet Muenchen, Physik Department E21, James Franck Strasse, 85748 Garching (Germany); Calzada, Elbio; Muehlbauer, Martin [FRM II, Lichtenbergstr. 1, 85748 Garching (Germany); Technische Universitaet Muenchen, Physik Department E21, James Franck Strasse, 85748 Garching (Germany); Neubauer, Andreas [Technische Universitaet Muenchen, Physik Department E21, James Franck Strasse, 85748 Garching (Germany); Schillinger, Burkhard [FRM II, Lichtenbergstr. 1, 85748 Garching (Germany); Technische Universitaet Muenchen, Physik Department E21, James Franck Strasse, 85748 Garching (Germany)

    2009-06-21

    Optical neutron polarizers like guides or benders destroy the collimation of a neutron beam due to multiple reflections or scattering. This makes them unsuitable for their use in polarized neutron radiography, because the beam collimation is essential to obtain high spatial resolution. We have developed a neutron polarizer based on the principle of an optical periscope with a zigzag double reflection on two parallel high-m supermirror polarizers. If the supermirrors are perfectly parallel and flat, the beam collimation is left unchanged by such a device. A first proof of concept version of this type of polarizer was built and tested. We expect to achieve a beam polarization of up to 99% with an improved version yet to be built.

  6. UV Coatings, Polarization, and Coronagraphy

    Science.gov (United States)

    Bolcar, Matthew R.; Quijada, Manuel; West, Garrett; Balasubramanian, Bala; Krist, John; Martin, Stefan; Sabatke, Derek

    2016-01-01

    Presenation for the Large UltraViolet Optical Infrared (LUVOIR) and Habitable Exoplanet Imager (HabEx) Science and Technology Definition Teams (STDT) on technical considerations regarding ultraviolet coatings, polarization, and coronagraphy. The presentations review the state-of-the-art in ultraviolet coatings, how those coatings generate polarization aberrations, and recent study results from both the LUVOIR and HabEx teams.

  7. Corrosion resistant neutron absorbing coatings

    Science.gov (United States)

    Choi, Jor-Shan [El Cerrito, CA; Farmer, Joseph C [Tracy, CA; Lee, Chuck K [Hayward, CA; Walker, Jeffrey [Gaithersburg, MD; Russell, Paige [Las Vegas, NV; Kirkwood, Jon [Saint Leonard, MD; Yang, Nancy [Lafayette, CA; Champagne, Victor [Oxford, PA

    2012-05-29

    A method of forming a corrosion resistant neutron absorbing coating comprising the steps of spray or deposition or sputtering or welding processing to form a composite material made of a spray or deposition or sputtering or welding material, and a neutron absorbing material. Also a corrosion resistant neutron absorbing coating comprising a composite material made of a spray or deposition or sputtering or welding material, and a neutron absorbing material.

  8. Optimization of a solid state polarizing bender for cold neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Shah, V.R.; Washington, A.L.; Stonaha, P.; Ashkar, R.; Kaiser, H. [Center for the Exploration of Energy and Matter, Indiana University, Bloomington IN (United States); Krist, T. [Helmholtz Zentrum Berlin, 14109 Berlin (Germany); Pynn, Roger [Center for the Exploration of Energy and Matter, Indiana University, Bloomington IN (United States); Neutron Science Directorate, Oak Ridge National Laboratory, Oak Ridge TN (United States)

    2014-12-21

    We have designed a solid state bender to polarize cold neutrons for the Spin Echo Scattering Angle Measurement (SESAME) instrument at the Low Energy Neutron Source (LENS) at Indiana University. The design attempts to achieve high neutron polarization across a wide range of neutron wavelengths and divergence angles by optimizing the supermirror coating materials. The transmission and polarizing efficiency of the bender were modeled using the VITESS software, then measured at both continuous-wave and pulsed neutron sources. While the measured peak neutron transmission and polarization agree reasonably well with simulations, neither quantity has been successfully modeled for long wavelength neutrons. These results imply an insufficient understanding of the magnetic microstructure of the supermirror coatings used.

  9. Non-uniform transmission of supermirror devices for neutron polarization

    Energy Technology Data Exchange (ETDEWEB)

    Tong, X., E-mail: tongx@ornl.gov [Instrument and Source Design Division, Oak Ridge National Laboratory, Oak Ridge 37831, TN (United States); Robertson, J.L. [Instrument and Source Design Division, Oak Ridge National Laboratory, Oak Ridge 37831, TN (United States); Pynn, R. [Instrument and Source Design Division, Oak Ridge National Laboratory, Oak Ridge 37831, TN (United States); Indiana University Center for the Exploration of Energy and Matter, Bloomington 47408, IN (United States)

    2014-12-21

    Polarizing supermirrors have been widely used in neutron scattering facilities where they have been employed as neutron spin filters to polarize neutron beams as well as analyze their polarization. In the past, the performance of polarizing supermirrors has been limited by their small acceptance angle, which made them less suitable for use at short wavelengths or with highly divergent beams. Recent advances in supermirror coatings have led to an array of devices designed to, at least partially, overcome this limitation. V-polarizers and multi-channel polarizers have been employed in several different types of neutron scattering instruments. However, our observations in the field where these types of polarizers are in use have raised concerns about their performance. In this paper, we report on detailed Monte-Carlo simulations performed on a multi-channel polarizer used on a prototype Spin-Echo Small Angle Neutron Scattering (SESANS) instrument to better understand its performance. Our results show that careful simulations of polarizers based on mirror reflection are needed to determine whether a particular design is suitable for SESANS applications.

  10. Polarized neutron reflectometry at Dhruva reactor

    Indian Academy of Sciences (India)

    Abstract. Polarized neutron reflectometry (PNR) is an ideal non-destructive tool for chemical and magnetic characterization of thin films and multilayers. We have installed a position sensitive detector-based polarized neutron reflectometer at Dhruva reactor, Trombay. In this paper we will discuss the results obtained from this ...

  11. Layered magnets: polarized neutron reflection studies

    Energy Technology Data Exchange (ETDEWEB)

    Zabel, H.; Schreyer, A. [Ruhr-Univ. Bochum, Lehrstuhl fuer Experimentalphysik/Festkoerperphysik, Bochum (Germany)

    1996-11-01

    Neutron reflectivity measurements from extended surfaces, thin films and superlattices provide information on the chemical profile parallel to the film normal, including film thicknesses, average composition and interfacial roughness parameters. Reflectivity measurements with polarized neutrons are particularly powerful for analyzing the magnetic density profiles in thin films and superlattices in addition to chemical profiles. The basic theory of polarized neutron reflectivity is provided, followed by some examples and more recent applications concerning polarized neutron reflectivity studies from exchange coupled Fe/Cr superlattices. (author) 5 figs., 13 refs.

  12. Polarized neutrons for Australian scientific research

    International Nuclear Information System (INIS)

    Kennedy, Shane J.

    2005-01-01

    Polarized neutron scattering has been a feature at ANSTO's HIFAR research reactor since the first polarization analysis (PA) spectrometer Longpol began operation over 30 years ago. Since that time, we have improved performance of Longpol and added new capabilities in several reincarnations of the instrument. Most of the polarized neutron experiments have been in the fields of magnetism and superconductivity, and most of that research has involved PA. Now as we plan our next generation neutron beam facility, at the Replacement Research Reactor (RRR), we intend to continue the tradition of PA but with a far broader scope in mind. Our new capabilities will combine PA and energy analysis with both cold and thermal neutron source spectra. We will also provide capabilities for research with polarized neutrons in small-angle neutron scattering and in neutron reflectometry. The discussion includes a brief historical account of the technical developments with a summary of past and present applications of polarized neutrons at HIFAR, and an outline of the polarized neutron capabilities that will be included in the first suite of instruments, which will begin operation at the new reactor in 2006

  13. "m=1" coatings for neutron guides

    DEFF Research Database (Denmark)

    Cooper-Jensen, C.P.; Vorobiev, A.; Klinkby, Esben Bryndt

    2014-01-01

    A substantial part of the price for a neutron guide is the shielding needed because of the gamma ray produced when neutrons are absorbed. This absorption occurs in the coating and the substrate of the neutron guides. Traditional m=1 coatings have been made of Ni and if reflectivity over...... the critical angle of Ni is needed one has used Ni58 or Ni/Ti multilayer coatings. Ni has one of the highest neutron scattering density but it also has a fairly high absorption cross section for cold and thermal neutrons and when a neutron is absorbed it emits a lot of gamma rays, some with energies above 9 Me......V. Materials like diamond and Be have higher neutron scattering density than Ni, have smaller absorption cross section and when a neutron is absorbed they emit much less gamma ray and at lower energies. We present results, both theoretically and experimentally, comparing Ni with Be and preliminary results...

  14. Polarized neutron scattering on HYSPEC: the HYbrid SPECtrometer at SNS

    Energy Technology Data Exchange (ETDEWEB)

    Zaliznyak, Igor [Brookhaven National Laboratory (BNL); Savici, Andrei T [ORNL; Garlea, Vasile O [ORNL; Winn, Barry L [ORNL; Schneelock, John [Brookhaven National Laboratory (BNL); Tranquada, John M. [Brookhaven National Laboratory (BNL); Gu, G. D. [Brookhaven National Laboratory (BNL); Wang, Aifeng [Brookhaven National Laboratory (BNL); Petrovic, C [Brookhaven National Laboratory (BNL)

    2017-01-01

    We describe some of the first polarized neutron scattering measurements performed at HYSPEC spectrometer at the Spallation Neutron Source, Oak Ridge National Laboratory. We discuss details of the instrument setup and the experimental procedures in the mode with the full polarization analysis. Examples of the polarized neutron diffraction and the polarized inelastic neutron data obtained on single crystal samples are presented.

  15. High precision neutron polarization for PERC

    International Nuclear Information System (INIS)

    Klauser, C.

    2013-01-01

    The decay of the free neutron into a proton, an electron and an anti-electron neutrino offers a simple system to study the semi-leptonic weak decay. High precision measurements of angular correlation coefficients of this decay provide the opportunity to test the standard model on the low energy frontier. The Proton Electron Radiation Channel PERC is part of a new generation of expriments pushing the accuracy of such an angular correlation coefficient measurement towards 10 -4 . Past experiments have been limited to an accuracy of 10 -3 with uncertainties on the neutron polarization as one of the leading systematic errors. This thesis focuses on the development of a stable, highly precise neutron polarization for a large, divergent cold neutron beam. A diagnostic tool that provides polarization higher than 99.99 % and analyzes with an accuracy of 10 -4 , the Opaque Test Bench, is presented and validated. It consists of two highly opaque polarized helium cells. The Opaque Test Bench reveals depolarizing effects in polarizing supermirrors commonly used for polarization in neutron decay experiments. These effects are investigated in detail. They are due to imperfect lateral magnetization in supermirror layers and can be minimized by significantly increased magnetizing fields and low incidence angle and supermirror factor m. A subsequent test in the crossed (X-SM) geometry demonstrated polarizations up to 99.97% from supermirrors only, improving neutron polarization with supermirrors by an order of magnitude. The thesis also discusses other neutron optical components of the PERC beamline: Monte-Carlo simulations of the beamline under consideration of the primary guide are carried out. In addition, calculation shows that PERC would statistically profit from an installation at the European Spallation source. Furthermore, beamline components were tested. A radio-frequency spin flipper was confirmed to work with an efficiency higher than 0.9999. (author) [de

  16. Maris polarization in neutron-rich nuclei

    Science.gov (United States)

    Shubhchintak; Bertulani, C. A.; Aumann, T.

    2018-03-01

    We present a theoretical study of the Maris polarization effect and its application in quasi-free reactions to assess information on the structure of exotic nuclei. In particular, we explore the dependence of the polarization effect on neutron excess and neutron-skin thickness. We discuss the uncertainties in the calculations of triple differential cross sections and of analyzing powers due the choices of various nucleon-nucleon interactions and optical potentials and the limitations of the method. Our study implies that polarization variables in (p, 2p) reactions in inverse kinematics can be an effective probe of single-particle structure of nuclei in radioactive-beam facilities.

  17. Radiography and tomography with polarized neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Treimer, Wolfgang, E-mail: treimer@helmholtz-berlin.de [University of Applied Sciences, Beuth Hochschule für Technik Berlin, Department Mathematics Physics and Chemistry, Luxemburgerstr. 10, D-13353 Berlin (Germany); Helmholtz Zentrum für Materialien und Energie, Department G – GTOMO, Hahn-Meitner-Platz 1, D-14109 Berlin (Germany)

    2014-01-15

    Neutron imaging became important when, besides providing impressive radiographic and tomographic images of various objects, physical, quantification of chemical, morphological or other parameters could be derived from 2D or 3D images. The spatial resolution of approximately 50 µm (and less) yields real space images of the bulk of specimens with more than some cm{sup 3} in volume. Thus the physics or chemistry of structures in a sample can be compared with scattering functions obtained e.g. from neutron scattering. The advantages of using neutrons become more pronounced when the neutron spin comes into play. The interaction of neutrons with magnetism is unique due to their low attenuation by matter and because their spin is sensitive to magnetic fields. Magnetic fields, domains and quantum effects such as the Meissner effect and flux trapping can only be visualized and quantified in the bulk of matter by imaging with polarized neutrons. This additional experimental tool is gaining more and more importance. There is a large number of new fields that can be investigated by neutron imaging, not only in physics, but also in geology, archeology, cultural heritage, soil culture, applied material research, magnetism, etc. One of the top applications of polarized neutron imaging is the large field of superconductivity where the Meissner effect and flux pinning can be visualized and quantified. Here we will give a short summary of the results achieved by radiography and tomography with polarized neutrons. - Highlights: • Radiography and tomography with polarized neutrons yield new results concerning the suppressed Meissner effect and magnetic flux trapping. • Suppressed Meissner effect was observed in pure lead samples and niobium. • Trapped magnetic fields in cylindrical Pb samples are squeezed around the rod axis. • The shape and the amount of trapped fields could be determined and quantified.

  18. Efficient polarization analysis for focusing neutron instruments

    Science.gov (United States)

    Stahn, Jochen; Glavic, Artur

    2017-06-01

    Polarized neutrons are a powerful probe to investigate magnetism in condensed matter on length scales from single atomic distances to micrometers. With the ongoing advancement of neutron optics, that allow to transport beams with increased divergence, the demands on neutron polarizes and analyzers have grown as well. The situation becomes especially challenging for new instruments at pulsed sources, where a large wavelength band needs to be polarized to make efficient use of the time structure of the beam. Here we present a polarization analysis concept for highly focused neutron beams that is based on transmission supermirrors that are bend in the shape of equiangular spirals. The method allows polarizations above 95% and good transmission, without negative impact on other beam characteristics. An example of a compact polarizing device already tested on the AMOR reflectometer is presented as well as the concept for the next generation implementation of the technique that will be installed on the Estia instrument being build for the European Spallation Source.

  19. Polarized neutron radiography with a periscope

    Energy Technology Data Exchange (ETDEWEB)

    Schulz, Michael; Neubauer, Andreas; Muehlbauer, Martin; Schillinger, Burkhard; Pfleiderer, Christian; Boeni, Peter [Technische Universitaet Muenchen, Physik Department, E21, Garching (Germany); Calzada, Elbio, E-mail: michael.schulz@frm2.tum.d [Technische Universitaet Muenchen, Forschungsneutronenquelle Heinz Maier Leibnitz (FRM II), Garching (Germany)

    2010-01-01

    The interaction of the magnetic moment of the neutron with magnetic fields provides a powerful probe for spatially resolved magnetisation measurements in magnetic materials. We have tested a periscope as a new type of polarizer providing neutron beams with a high polarization and a low divergence. The observed inhomogeneity of the beam caused by the waviness of the glass substrates was quantified by means of Monte-Carlo simulations using the software package McStas. The results show that beams of high homogeneity can be produced if the waviness is reduced to below 1.0{center_dot}10{sup -5} rad. Finally, it is shown that radiography with polarized neutrons is a powerful method for measuring the spatially resolved magnetisation in optically float-zoned samples of the weak itinerant ferromagnet Ni{sub 3}Al, thereby aiding the identification of the appropriate growth parameters.

  20. Polarized neutron radiography with a periscope

    International Nuclear Information System (INIS)

    Schulz, Michael; Neubauer, Andreas; Muehlbauer, Martin; Schillinger, Burkhard; Pfleiderer, Christian; Boeni, Peter; Calzada, Elbio

    2010-01-01

    The interaction of the magnetic moment of the neutron with magnetic fields provides a powerful probe for spatially resolved magnetisation measurements in magnetic materials. We have tested a periscope as a new type of polarizer providing neutron beams with a high polarization and a low divergence. The observed inhomogeneity of the beam caused by the waviness of the glass substrates was quantified by means of Monte-Carlo simulations using the software package McStas. The results show that beams of high homogeneity can be produced if the waviness is reduced to below 1.0·10 -5 rad. Finally, it is shown that radiography with polarized neutrons is a powerful method for measuring the spatially resolved magnetisation in optically float-zoned samples of the weak itinerant ferromagnet Ni 3 Al, thereby aiding the identification of the appropriate growth parameters.

  1. Time reversal invariance in polarized neutron decay

    Energy Technology Data Exchange (ETDEWEB)

    Wasserman, Eric G. [Harvard Univ., Cambridge, MA (United States)

    1994-03-01

    An experiment to measure the time reversal invariance violating (T-violating) triple correlation (D) in the decay of free polarized neutrons has been developed. The detector design incorporates a detector geometry that provides a significant improvement in the sensitivity over that used in the most sensitive of previous experiments. A prototype detector was tested in measurements with a cold neutron beam. Data resulting from the tests are presented. A detailed calculation of systematic effects has been performed and new diagnostic techniques that allow these effects to be measured have been developed. As the result of this work, a new experiment is under way that will improve the sensitivity to D to 3 x 10-4 or better. With higher neutron flux a statistical sensitivity of the order 3 x 10-5 is ultimately expected. The decay of free polarized neutrons (n → p + e + $\\bar{v}$e) is used to search for T-violation by measuring the triple correlation of the neutron spin polarization, and the electron and proton momenta (σn • pp x pe). This correlation changes sign under reversal of the motion. Since final state effects in neutron decay are small, a nonzero coefficient, D, of this correlation indicates the violation of time reversal invariance. D is measured by comparing the numbers of coincidences in electron and proton detectors arranged symmetrically about a longitudinally polarized neutron beam. Particular care must be taken to eliminate residual asymmetries in the detectors or beam as these can lead to significant false effects. The Standard Model predicts negligible T-violating effects in neutron decay. Extensions to the Standard Model include new interactions some of which include CP-violating components. Some of these make first order contributions to D.

  2. Time reversal invariance in polarized neutron decay

    International Nuclear Information System (INIS)

    Wasserman, E.G.

    1994-03-01

    An experiment to measure the time reversal invariance violating (T-violating) triple correlation (D) in the decay of free polarized neutrons has been developed. The detector design incorporates a detector geometry that provides a significant improvement in the sensitivity over that used in the most sensitive of previous experiments. A prototype detector was tested in measurements with a cold neutron beam. Data resulting from the tests are presented. A detailed calculation of systematic effects has been performed and new diagnostic techniques that allow these effects to be measured have been developed. As the result of this work, a new experiment is under way that will improve the sensitivity to D to 3 x 10 -4 or better. With higher neutron flux a statistical sensitivity of the order 3 x 10 -5 is ultimately expected. The decay of free polarized neutrons (n → p + e + bar v e ) is used to search for T-violation by measuring the triple correlation of the neutron spin polarization, and the electron and proton momenta (σ n · p p x p e ). This correlation changes sign under reversal of the motion. Since final state effects in neutron decay are small, a nonzero coefficient, D, of this correlation indicates the violation of time reversal invariance. D is measured by comparing the numbers of coincidences in electron and proton detectors arranged symmetrically about a longitudinally polarized neutron beam. Particular care must be taken to eliminate residual asymmetries in the detectors or beam as these can lead to significant false effects. The Standard Model predicts negligible T-violating effects in neutron decay. Extensions to the Standard Model include new interactions some of which include CP-violating components. Some of these make first order contributions to D

  3. The polarized platypus polarized neutron reflectometry made possible

    International Nuclear Information System (INIS)

    Saerbeck, Thomas

    2009-01-01

    Full text: The magnetic moment of the neutron, together with it's highly penetrating non destructive manner, make polarized neutron reflectometry an excellent tool to study magnetic phenomena across surfaces and interfaces of thin films. Unlike other magnetometry techniques which ordinarily yield only average magnetization values or, in case of probes with higher spatial resolution (e.g. electron microscopy or scanning tunnelling microscopy), show a high surface sensitivity, PNR together with magnetic x-ray scattering provides the ability to spatially resolve vector magnetization well beneath the surface [1] The ability to obtain vector magnetization profiles across interfaces and surfaces of thin films and multilayers offers the intriguing possibility to study systematically magnetic configurations and magnetic exchange interactions through intervening layers. In this paper we present the performance of the new polarization system installed on the time of flight neutron reflectometer PLATYPUS at ANSTO's Bragg Institute. The spin state of the neutrons is polarized and analysed by spatial separation of different neutron spin states using polarizing Fe/Si supermirrors before, and after the sample stage. The supermirrors have a large wavelength acceptance bandwidth of 3 A to 12 A. To control the desired spin direction of the incoming and reflected beam from the sample, two sets of RF spin flippers are installed. In the free space between the spin flippers and the sample stage the neutron spin direction is maintained by two sets of magnetic guide field coils. The new sample environment for studies of magnetic samples includes a 1 T electromagnet and a closed cycle refrigerator which gives access to a temperature range from 4K to 3 50 K .

  4. Grazing incidence polarized neutron scattering in reflection ...

    Indian Academy of Sciences (India)

    During the year 1980, polarized neutron scattering technique came into being as an ana- lytic tool to measure the ... The discovery of antiferromagnetic coupling was critical to the discovery of GMR, pro- viding as it did ..... Here we consider the incident wave vector ki making an angle αi in the x–z plane while the scattered ...

  5. Some applications of polarized inelastic neutron scattering

    Indian Academy of Sciences (India)

    A brief account of applications of polarized inelastic neutron scattering in condensed matter research is given. ... the itinerant antiferromagnet chromium we demonstrate that the dynamics of the longitudinal and transverse excitations are very different, resolving a long standing puzzle concerning the slope of their dispersion.

  6. Polarized neutron reflectometry of magnetic nanostructures

    Science.gov (United States)

    Toperverg, B. P.

    2015-12-01

    Among a number of methods employed to characterize various types of magnetic nano-structures Polarized Neutron Reflectometry (PNR) is shown to be a unique tool providing a scope of quantitative information on magnetization arrangement over relevant scales. Deeply penetrating into materials neutron spins are able to resolve vectorial profile of magnetic induction with accuracy of a fraction of Oersted over a fraction of nano-meters. This property is exploited in measurements of specular PNR which hence constitutes the method of depth resolved vector magnetometry widely used to examine magnetic states in exchange coupled magnetic superlattices, exchange bias systems, spin valves, exchange springs, superconducting/ferromagnetic heterostructure, etc. Off-specular polarized neutron scattering (OS-PNS) measures the in-plane magnetization distribution over scales from hundreds of nanoto hundreds of micrometers providing, in combination with specular PNR, access to lateral long range fluctuations of the magnetization vector and magnetic domains in these systems. OSPNS is especially useful in studies of co-operative magnetization reversal processes in various films and multilayers laterally patterned into periodic arrays of stripes, or islands of various dimentions, shapes, internal structures, etc., representing an interest for e.g. spintronics. Smaller sizes of 10?100 nm are accessed with the method of Polarized Neutrons Grazing Incidence Small Angle Scattering (PN-GISAS), which in a combination with specular PNR and OS-PNS is used to study self-assembling of magnetic nano-particles on flat surfaces, while Polarized Neutron Grazing Incidence Diffraction (PN-GID) complete the scope of magnetic information over wide range of scales in 3D space. The review of recent results obtained employing the methods listed above is preceded by the detailed theoretical consideration and exemplified by new developments addressing with PNR fast magnetic kinetics in nano-systems.

  7. Polarized 3He gas circulating technologies for neutron analyzers

    Energy Technology Data Exchange (ETDEWEB)

    Watt, David W. [Xemed, LLC, Durham, NH (United States)

    2017-10-02

    We outline our project to develop a circulating polarized helium-3 system for developing of large, quasi-continuously operating neutron analyzers. The project consisted of four areas: 1) Development of robust external cavity narrowed diode laser output with spectral line width < 0.17 nm and power of 2000 W. 2) Development of large glass polarizing cells using cell surface treatments to obtain long relaxation lifetimes. 3) Refinements of the circulation system with an emphasis on gas purification and materials testing. 4) Design/fabrication of a new polarizer system. 5) Preliminary testing of the new polarizer. 1. Developed Robust High-Power Narrowed Laser The optical configuration of the laser was discussed in the proposal and will be reviewed in the body of this report. The external cavity is configured to mutually lock the wavelength of five 10-bar laser stacks. All the logistical milestones were been met and critical subsystems- laser stack manifold and power divider, external laser cavity, and output telescope- were assembled and tested at low power. Each individual bar is narrowed to ~0.05 nm; when combined the laser has a cumulative spectral width of 0.17 nm across the entire beam due to variations of the bars central wavelength by +/- 0.1 nm, which is similar to that of Volume Bragg Grating narrowed laser bars. This configuration eliminates the free-running “pedestal” that occurs in other external cavity diode lasers. The full-scale laser was completed in 2016 and was used in both the older and newer helium polarizers. This laser was operated at 75% power for periods of up to 8 hours. Once installed, the spectrum became slightly broader (~.25 nm) at full power; this is likely due to very slight misalignments that occurred during handling. 2. Developed the processes to create uniform sintered sol-gel coatings. Our work on cell development comprised: 1) Production of large GE180 cells and explore different means of cell preparation, and 2) Development of

  8. Neutron stars with spin polarized self-interacting dark matter

    OpenAIRE

    Rezaei, Zeinab

    2018-01-01

    Dark matter, one of the important portion of the universe, could affect the visible matter in neutron stars. An important physical feature of dark matter is due to the spin of dark matter particles. Here, applying the piecewise polytropic equation of state for the neutron star matter and the equation of state of spin polarized self-interacting dark matter, we investigate the structure of neutron stars which are influenced by the spin polarized self-interacting dark matter. The behavior of the...

  9. Polarized Neutron Reflectometry of Nickel Corrosion Inhibitors.

    Science.gov (United States)

    Wood, Mary H; Welbourn, Rebecca J L; Zarbakhsh, Ali; Gutfreund, Philipp; Clarke, Stuart M

    2015-06-30

    Polarized neutron reflectometry has been used to investigate the detailed adsorption behavior and corrosion inhibition mechanism of two surfactants on a nickel surface under acidic conditions. Both the corrosion of the nickel surface and the structure of the adsorbed surfactant layer could be monitored in situ by the use of different solvent contrasts. Layer thicknesses and roughnesses were evaluated over a range of pH values, showing distinctly the superior corrosion inhibition of one negatively charged surfactant (sodium dodecyl sulfate) compared to a positively charged example (dodecyl trimethylammonium bromide) due to its stronger binding interaction with the surface. It was found that adequate corrosion inhibition occurs at significantly less than full surface coverage.

  10. Study and production of polarized monochromatic thermal neutron beams

    International Nuclear Information System (INIS)

    Beiln, H.

    1963-06-01

    Results obtained with a recently built neutron spectrometer producing monochromatic polarized neutron beams,in the energy rang (10 -3 - 10) eV and using a series of artificial (Co: 92 per cent - Fe: 8 per cent) monocrystal as polarizers and analysers, are given. A high precision method for cutting monocrystals is explained. A description of the installation itself as well as some results obtained with Fe 3 O 4 crystals are also given. Experimental result pertaining to various magnetic guide and 'spin flip' system, as required in the handling of such polarized neutron beams, are also discussed. (author) [fr

  11. Development of polarized {sup 3}He filter for polarized neutron experiment

    Energy Technology Data Exchange (ETDEWEB)

    Sakai, K.; Sato, H.; Yoshimi, A.; Asahi, K. [Tokyo Inst. of Tech. (Japan). Faculty of Science; Masuda, Y.; Muto, S.; Ishimoto, S.; Morimoto, K.

    1996-08-01

    A high-pressure polarized {sup 3}He gas cell, pumped with two diode lasers, has been developed at KEK for use as a polarizer and a spin analyzer for low energy neutrons. The polarization attained of {sup 3}He was determined through the measurement of the transmission of the unpolarized neutrons through the {sup 3}He cell. So far we obtained P{sub He}=18% at 10 atm and P{sub He}=12% at 20 atm. (author)

  12. Local magnetic structure determination using polarized neutron holography

    Science.gov (United States)

    Szakál, Alex; Markó, Márton; Cser, László

    2015-05-01

    A unique and important property of the neutron is that it possesses magnetic moment. This property is widely used for determination of magnetic structure of crystalline samples observing the magnetic components of the diffraction peaks. Investigations of diffraction patterns give information only about the averaged structure of a crystal but for discovering of local spin arrangement around a specific (e.g., impurity) nucleus remains still a challenging problem. Neutron holography is a useful tool to investigate the local structure around a specific nucleus embedded in a crystal lattice. The method has been successfully applied experimentally in several cases using non-magnetic short range interaction of the neutron and the nucleus. A mathematical model of the hologram using interaction between magnetic moment of the atom and the neutron spin for polarized neutron holography is provided. Validity of a polarized neutron holographic experiment is demonstrated by applying the proposed method on model systems.

  13. Local magnetic structure determination using polarized neutron holography

    International Nuclear Information System (INIS)

    Szakál, Alex; Markó, Márton; Cser, László

    2015-01-01

    A unique and important property of the neutron is that it possesses magnetic moment. This property is widely used for determination of magnetic structure of crystalline samples observing the magnetic components of the diffraction peaks. Investigations of diffraction patterns give information only about the averaged structure of a crystal but for discovering of local spin arrangement around a specific (e.g., impurity) nucleus remains still a challenging problem. Neutron holography is a useful tool to investigate the local structure around a specific nucleus embedded in a crystal lattice. The method has been successfully applied experimentally in several cases using non-magnetic short range interaction of the neutron and the nucleus. A mathematical model of the hologram using interaction between magnetic moment of the atom and the neutron spin for polarized neutron holography is provided. Validity of a polarized neutron holographic experiment is demonstrated by applying the proposed method on model systems

  14. Invited Article: Polarization ``Down Under'': The polarized time-of-flight neutron reflectometer PLATYPUS

    Science.gov (United States)

    Saerbeck, T.; Klose, F.; Le Brun, A. P.; Füzi, J.; Brule, A.; Nelson, A.; Holt, S. A.; James, M.

    2012-08-01

    This review presents the implementation and full characterization of the polarization equipment of the time-of-flight neutron reflectometer PLATYPUS at the Australian Nuclear Science and Technology Organisation (ANSTO). The functionality and efficiency of individual components are evaluated and found to maintain a high neutron beam polarization with a maximum of 99.3% through polarizing Fe/Si supermirrors. Neutron spin-flippers with efficiencies of 99.7% give full control over the incident and scattered neutron spin direction over the whole wavelength spectrum available in the instrument. The first scientific experiments illustrate data correction mechanisms for finite polarizations and reveal an extraordinarily high reproducibility for measuring magnetic thin film samples. The setup is now fully commissioned and available for users through the neutron beam proposal system of the Bragg Institute at ANSTO.

  15. Dynamically polarized samples for neutron protein crystallography at the Spallation Neutron Source

    Science.gov (United States)

    Zhao, Jinkui; Pierce, Josh; Myles, Dean; Robertson, J. L.; Herwig, Kenneth W.; Standaert, Bob; Cuneo, Matt; Li, Le; Meilleur, Flora

    2016-09-01

    To prepare for the next generation neutron scattering instruments for the planned second target station at the Spallation Neutron Source (SNS) and to broaden the scientific impact of neutron protein crystallography at the Oak Ridge National Laboratory, we have recently ramped up our efforts to develop a dynamically polarized target for neutron protein crystallography at the SNS. Proteins contain a large amount of hydrogen which contributes to incoherent diffraction background and limits the sensitivity of neutron protein crystallography. This incoherent background can be suppressed by using polarized neutron diffraction, which in the same time also improves the coherent diffraction signal. Our plan is to develop a custom Dynamic Nuclear Polarization (DNP) setup tailored to neutron protein diffraction instruments. Protein crystals will be polarized at a magnetic field of 5 T and temperatures of below 1 K. After the dynamic polarization process, the sample will be brought to a frozen-spin mode in a 0.5 T holding field and at temperatures below 100 mK. In a parallel effort, we are also investigating various ways of incorporating polarization agents needed for DNP, such as site specific spin labels, into protein crystals.

  16. A new polarized neutron interferometry facility at the NCNR

    Energy Technology Data Exchange (ETDEWEB)

    Shahi, C.B. [Physics and Engineering Physics Department, Tulane University, New Orleans, LA 70188 (United States); Arif, M. [National Institute of Standards and Technology, Gaithersburg, MD 20899 (United States); Cory, D.G. [Department of Chemistry, University of Waterloo, Waterloo, ON, Canada N2L 3G1 (Canada); Perimeter Institute for Theoretical Physics, Waterloo, ON, Canada N2L 2Y5 (Canada); Institute for Quantum Computing, University of Waterloo, Waterloo, ON, Canada N2L 3G1 (Canada); Canadian Institute for Advanced Research, Toronto, ON, Canada M5G 1Z8 (Canada); Mineeva, T. [Department of Physics and Astronomy, University of Waterloo, Waterloo, ON, Canada N2L 3G1 (Canada); Canadian Institute for Advanced Research, Toronto, ON, Canada M5G 1Z8 (Canada); Nsofini, J.; Sarenac, D. [Institute for Quantum Computing, University of Waterloo, Waterloo, ON, Canada N2L 3G1 (Canada); Department of Physics and Astronomy, University of Waterloo, Waterloo, ON, Canada N2L 3G1 (Canada); Williams, C.J. [National Institute of Standards and Technology, Gaithersburg, MD 20899 (United States); Huber, M.G., E-mail: michael.huber@nist.gov [National Institute of Standards and Technology, Gaithersburg, MD 20899 (United States); Pushin, D.A., E-mail: dmitry.pushin@uwaterloo.ca [Institute for Quantum Computing, University of Waterloo, Waterloo, ON, Canada N2L 3G1 (Canada); Department of Physics and Astronomy, University of Waterloo, Waterloo, ON, Canada N2L 3G1 (Canada)

    2016-03-21

    A new monochromatic beamline and facility has been installed at the National Institute of Standards and Technology (NIST) Center for Neutron Research (NCNR) devoted to neutron interferometry in the research areas of spin control, spin manipulation, quantum mechanics, quantum information science, spintronics, and material science. This facility is possible in part because of advances in decoherence free subspace interferometer designs that have demonstrated consistent contrast in the presence of vibrational noise; a major environmental constraint that has prevented neutron interferometry from being applied at other neutron facilities. Neutron interferometry measures the phase difference between a neutron wave function propagating along two spatially separated paths. It is a practical example of self interference and due to its modest path separation of a few centimeters allows the insertion of samples and macroscopic neutron spin rotators. Phase shifts can be caused by gravitational, magnetic and nuclear interactions as well as purely quantum mechanical effects making interferometer a robust tool in neutron research. This new facility is located in the guide hall of the NCNR upstream of the existing Neutron Interferometry and Optics Facility (NIOF) and has several advantages over the NIOF including higher incident flux, better neutron polarization, and increased accessibility. The long term goal for the new facility is to be a user supported beamline and makes neutron interferometer more generally available to the scientific community. This paper addresses both the capabilities and characteristics of the new facility.

  17. Generation of neutron standing waves at total reflection of polarized neutrons

    International Nuclear Information System (INIS)

    Aksenov, V.L.; Nikitenko, Yu.V.; Kozhevnikov, S.V.; Radu, F.; Kruijs, R.; Rekveldt, M.Th.

    1999-01-01

    The regime of neutron standing waves at reflection of polarized thermal neutrons from the structure glass/Cu (1000 A Angstrom)/Ti (2000 A Angstrom)/Co (60 A Angstrom)/Ti (300 A Angstrom) in a magnetic field directed at an angle to the sample plane is realized. The intensity of neutrons with a particular spin projection on the external magnetic field direction appears to be a periodic function of the neutron wavelength and the glancing angle of the reflected beam. It is shown that the neutron standing wave regime can be a very sensitive method for the determination of changes in the spatial position of magnetic noncollinear layers. (author)

  18. Diamond-like carbon coated ultracold neutron guides

    Energy Technology Data Exchange (ETDEWEB)

    Heule, S. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland) and Physik-Institut der Universitaet Zuerich (Switzerland)]. E-mail: stefan.heule@psi.ch; Atchison, F. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland); Daum, M. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland); Foelske, A. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland); Henneck, R. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland); Kasprzak, M. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland); Stefan Meyer Institut fuer subatomare Physik, Austrian Academy of Sciences, Vienna (Austria); Kirch, K. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland); Knecht, A. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland); Physik-Institut der Universitaet Zuerich (Switzerland); Kuzniak, M. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland); Jagellonian University, Cracow (Poland); Lippert, T. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland); Meier, M. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland); Pichlmaier, A. [Paul Scherrer Institut (PSI), 5232 Villigen PSI (Switzerland); Straumann, U. [Physik-Institut der Universitaet Zuerich (Switzerland)

    2007-07-31

    It has been shown recently that diamond-like carbon (DLC) with a sp{sup 3} fraction above 60% is a better wall coating material for ultracold neutron applications than beryllium. We report on results of Raman spectroscopic and XPS measurements obtained for diamond-like carbon coated neutron guides produced in a new facility, which is based on pulsed laser deposition at 193 nm. For diamond-like carbon coatings on small stainless steel substrates we find sp{sup 3} fractions in the range from 60 to 70% and showing slightly increasing values with laser pulse energy and pulse repetition rate.

  19. A measurement of the absolute neutron beam polarization produced by an optically pumped 3He neutron spin filter

    International Nuclear Information System (INIS)

    Rich, D.R.; Bowman, J.D.; Crawford, B.E.; Delheij, P.P.J.; Espy, M.A.; Haseyama, T.; Jones, G.; Keith, C.D.; Knudson, J.; Leuschner, M.B.; Masaike, A.; Masuda, Y.; Matsuda, Y.; Penttilae, S.I.; Pomeroy, V.R.; Smith, D.A.; Snow, W.M.; Szymanski, J.J.; Stephenson, S.L.; Thompson, A.K.; Yuan, V.

    2002-01-01

    The capability of performing accurate absolute measurements of neutron beam polarization opens a number of exciting opportunities in fundamental neutron physics and in neutron scattering. At the LANSCE pulsed neutron source we have measured the neutron beam polarization with an absolute accuracy of 0.3% in the neutron energy range from 40 meV to 10 eV using an optically pumped polarized 3 He spin filter and a relative transmission measurement technique. 3 He was polarized using the Rb spin-exchange method. We describe the measurement technique, present our results, and discuss some of the systematic effects associated with the method

  20. Limitations on the accuracy of polarized-neutron diffractometry

    International Nuclear Information System (INIS)

    Moon, R.M.; Koehler, W.C.; Shull, C.G.

    1975-01-01

    The magnetic force on a neutron as it enters a high-field magnet can influence the results of polarized-neutron diffraction experiments. The position of the Bragg peak is slightly different for neutrons in the two spin states and the peak intensity is slightly different. The magnitudes of these effects are calculated and experimental evidence confirming the peak shift calculation is presented. Suggestions for experimental procedures to minimize these effects are presented. The discussion is directed toward experiments in which flipping-ratio accuracies approaching 5x10 -5 are desired. (Auth.)

  1. Grazing incidence polarized neutron scattering in reflection ...

    Indian Academy of Sciences (India)

    along with suppression of training effect in exchange coupled system was microscopically identified using neutron ..... reversal mechanism and suppression of training in an exchange-coupled system by Paul et al are worth ...... density functional calculations based on Korringa–Kohn–Rostoker–Coherent potential-.

  2. Measurement of the polarized neutron---polarized {sup 3}He total cross section

    Energy Technology Data Exchange (ETDEWEB)

    Keith, C.D.; Gould, C.R.; Haase, D.G.; Seely, M.L. [North Carolina State University, Raleigh, North Carolina 27695 (United States)]|[Triangle Universities Nuclear Laboratory, Durham, North Carolina 27708 (United States); Huffman, P.R.; Roberson, N.R.; Tornow, W.; Wilburn, W.S. [Duke University, Durham, North Carolina 27708 (United States)]|[Triangle Universities Nuclear Laboratory, Durham, North Carolina 27708 (United States)

    1995-05-10

    The first measurements of polarized neutron--polarized {sup 3}He scattering in the few MeV energy region are reported. The total cross section difference {Delta}{sigma}{sub {ital T}} for transversely polarized target and beam has been measured for neutron energies between 1.9 and 7.5 MeV. Comparison is made to predictions of {Delta}{sigma}{sub {ital T}} using various descriptions of the {sup 4}He continuum. A brute-force polarized target of solid {sup 3}He has been developed for these measurements. The target is 4.3{times}10{sup 22} atoms/cm{sup 2} thick and is polarized to 38% at 7 Telsa and 12 mK. {copyright} {ital 1995} {ital American} {ital Institute} {ital of} {ital Physics}.

  3. Radiography of weakly ferromagnetic metals with polarized neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Schulz, Michael; Calzada, Elbio; Muehlbauer, Martin; Schillinger, Burkhard [FRM II, Garching (Germany); E21, Physik Department TUM, Garching (Germany); Boeni, Peter; Neubauer, Andreas; Pfleiderer, Christian [E21, Physik Department TUM, Garching (Germany)

    2009-07-01

    The depolarization of a neutron beam passing through a ferromagnet crucially depends on the magnetic properties of the sample. Combining neutron depolarisation measurements with neutron radiography allows obtaining spatially resolved information about these properties. For measuring the depolarization, we have installed a longitudinal polarized beam setup at the ANTARES beamline consisting of {sup 3}He polarizers and flat coil spin flippers. With this setup we have performed radiography with polarized neutrons in the weak itinerant ferromagnets Pd{sub 1-x}Ni{sub x} in order to determine the spatial distribution of the Curie temperatures T{sub C} in the samples. The results show that the single crystals are rather inhomogeneous showing large variations in T{sub C}. The data allows firstly to cut out small crystals with improved homogeneity for neutron scattering experiments and secondly to provide feedback for improving the growth techniques for the crystals. In the future we hope to use the potential of this method to map out magnetic domains across large volume samples.

  4. Polarized 3He Gas Circulating Technologies for Neutron Analyzers

    Energy Technology Data Exchange (ETDEWEB)

    Watt, David [Xemed LLC, Durham, NH (United States); Hersman, Bill [Xemed LLC, Durham, NH (United States)

    2014-12-10

    We describe the development of an integrated system for quasi-continuous operation of a large volume neutron analyzer. The system consists of a non-magnetic diaphragm compressor, a prototype large volume helium polarizer, a surrogate neutron analyzer, a non-depolarizing gas storage reservoir, a non-ferrous valve manifold for handling gas distribution, a custom rubidium-vapor gas return purifier, and wire-wound transfer lines, all of which are immersed in a two-meter external magnetic field. Over the Phase II period we focused on three major tasks required for the successful deployment of these types of systems: 1) design and implementation of gas handling hardware, 2) automation for long-term operation, and 3) improvements in polarizer performance, specifically fabrication of aluminosilicate optical pumping cells. In this report we describe the design, implementation, and testing of the gas handling hardware. We describe improved polarizer performance resulting from improved cell materials and fabrication methods. These improvements yielded valved 8.5 liter cells with relaxation times greater than 12 hours. Pumping this cell with 1500W laser power with 1.25nm linewidth yielded peak polarizations of 60%, measured both inside and outside the polarizer. Fully narrowing this laser to 0.25nm, demonstrated separately on one stack of the four, would have allowed 70% polarization with this cell. We demonstrated the removal of 5 liters of polarized helium from the polarizer with no measured loss of polarization. We circulated the gas through a titanium-clad compressor with polarization loss below 3% per pass. We also prepared for the next phase of development by refining the design of the polarizer so that it can be engineer-certified for pressurized operation. The performance of our system far exceeds comparable efforts elsewhere.

  5. Coherence approach to neutron polarization propagation in instruments

    NARCIS (Netherlands)

    De Haan, V.O.; Van Well, A.A.; Plomp, J.

    2008-01-01

    The propagation of the mutual coherence function is a well known method to describe the effects of neutron’s propagation through scattering instruments. This method is extended with the description of the coherence matrix to account for neutron polarization effects and its propagation through an

  6. Polarized 3He Neutron Spin Filters

    Energy Technology Data Exchange (ETDEWEB)

    Sno, William Michael [Indiana Univ., Bloomington, IN (United States)

    2016-01-12

    The goal of this grant to Indiana University and subcontractors at Hamilton College and Wisconsin and the associated Interagency Agreement with NIST was to extend the technique of polarized neutron scattering by the development and application of polarized 3He-based neutron spin filters. This effort was blessed with long-term support from the DOE Office of Science, which started in 2003 and continued until the end of a final no-cost extension of the last 3-year period of support in 2013. The steady support from the DOE Office of Science for this long-term development project was essential to its eventual success. Further 3He neutron spin filter development is now sited at NIST and ORNL.

  7. Data processing workflow for time of flight polarized neutrons inelastic measurements

    Energy Technology Data Exchange (ETDEWEB)

    Savici, Andrei T [ORNL; Zaliznyak, Igor [Brookhaven National Laboratory (BNL); Garlea, Vasile O [ORNL; Winn, Barry L [ORNL

    2017-01-01

    We discuss the data processing workflow for polarized neutron scattering measurements performed at HYSPEC spectrometer at the Spallation Neutron Source, Oak Ridge National Laboratory. The effects of the focusing Heusler crystal polarizer and the wide-angle supermirror transmission polarization analyzer are added to the data processing flow of the non-polarized case. The implementation is done using the Mantid software package.

  8. Ultra-small-angle scattering with polarized neutrons

    International Nuclear Information System (INIS)

    Jericha, E.; Badurek, G.; Trinker, M.

    2007-01-01

    Ultra-small-angle neutron scattering (USANS) has been established as an effective technique for the study of structures in the micrometre range in recent years. Consequentially this method has been extended to magnetic structures of corresponding size. We present the instrument arrangement and first experimental results. The instrument itself is a double crystal diffractometer in Bonse-Hart configuration which takes advantage of the narrow angular width of the perfect crystal reflection to obtain an extremely high angular resolution of the scattering vector. The neutrons are loss-free polarized by permanent magnetic prisms located between the monochromator crystal and the sample. Neutrons with opposite polarization are separated to a large extent and their different scattering behaviour may be studied in a single measurement without additional manipulation of the neutron spin. In this manner we are able to separate the magnetic and nuclear contribution to the scattering. We present first exemplifying measurements on ferromagnetic rods and wires, and on soft-magnetic ribbons. Related experiments were performed at the USANS facility of the TRIGA reactor at the Vienna University of Technology and at the combined neutron interferometer/USANS instrument S18 at the ILL, Grenoble

  9. Ultra-small-angle scattering with polarized neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Jericha, E. [Atominstitut, Vienna University of Technology, Stadionallee 2, 1020 Vienna (Austria)]. E-mail: jericha@ati.ac.at; Badurek, G. [Atominstitut, Vienna University of Technology, Stadionallee 2, 1020 Vienna (Austria); Trinker, M. [Atominstitut, Vienna University of Technology, Stadionallee 2, 1020 Vienna (Austria)

    2007-07-15

    Ultra-small-angle neutron scattering (USANS) has been established as an effective technique for the study of structures in the micrometre range in recent years. Consequentially this method has been extended to magnetic structures of corresponding size. We present the instrument arrangement and first experimental results. The instrument itself is a double crystal diffractometer in Bonse-Hart configuration which takes advantage of the narrow angular width of the perfect crystal reflection to obtain an extremely high angular resolution of the scattering vector. The neutrons are loss-free polarized by permanent magnetic prisms located between the monochromator crystal and the sample. Neutrons with opposite polarization are separated to a large extent and their different scattering behaviour may be studied in a single measurement without additional manipulation of the neutron spin. In this manner we are able to separate the magnetic and nuclear contribution to the scattering. We present first exemplifying measurements on ferromagnetic rods and wires, and on soft-magnetic ribbons. Related experiments were performed at the USANS facility of the TRIGA reactor at the Vienna University of Technology and at the combined neutron interferometer/USANS instrument S18 at the ILL, Grenoble.

  10. The polarized neutron reflectometer 'Reverans'

    Energy Technology Data Exchange (ETDEWEB)

    Radzhabov, A.K. [Petersburg Nuclear Physics Institute, Gatchina, St. Petersburg 188300 (Russian Federation)]. E-mail: akr@pnpi.spb.ru; Gordeev, G.P. [Petersburg Nuclear Physics Institute, Gatchina, St. Petersburg 188300 (Russian Federation); Lazebnik, I.M. [Petersburg Nuclear Physics Institute, Gatchina, St. Petersburg 188300 (Russian Federation); Axelrod, L.A. [Petersburg Nuclear Physics Institute, Gatchina, St. Petersburg 188300 (Russian Federation); Zabenkin, V.N. [Petersburg Nuclear Physics Institute, Gatchina, St. Petersburg 188300 (Russian Federation)

    2007-07-15

    The polarized neutron reflectometer 'Reverans' with a vertical plane of scattering is being installed at the VVR-M reactor (Gatchina, Russia). It will be used for research on phase boundaries, interfaces and free surfaces. Systems under study can be both magnetic and nonmagnetic ones. At present the installation of the reflectometer is at the final stage. The parameters and abilities of the reflectometer are presented.

  11. Radiative capture of polarized neutrons by aluminium and manganese nuclei

    International Nuclear Information System (INIS)

    1979-01-01

    This investigation treats the angular dependence of the intensity and of the circular polarization of gamma-radiation, that is emitted after capture of polarized neutrons by polarized and unpolarized targets. Interference effects between the (n,γ)-reaction amplitudes with different channel spin are discussed and angular distribution coefficients are calculated in case mixing of dipole and quadrupole radiation occurs. It is indicated how the influence of p-wave capture may be taken into account. The nuclear orientation experiments on aluminium yield the values of the angular distribution coefficients of primary and secondary gamma-ray transitions and by a chi 2 -analysis five spin values are assigned uniquely and several α-values are determined. The nuclear orientation experiments on manganese lead to α-values and unique spin assigments for thirteen nuclear states in 56 Mn. (Auth.)

  12. Effect of cathodic polarization on coating doxycycline on titanium surfaces

    Energy Technology Data Exchange (ETDEWEB)

    Geißler, Sebastian; Tiainen, Hanna; Haugen, Håvard J., E-mail: h.j.haugen@odont.uio.no

    2016-06-01

    Cathodic polarization has been reported to enhance the ability of titanium based implant materials to interact with biomolecules by forming titanium hydride at the outermost surface layer. Although this hydride layer has recently been suggested to allow the immobilization of the broad spectrum antibiotic doxycycline on titanium surfaces, the involvement of hydride in binding the biomolecule onto titanium remains poorly understood. To gain better understanding of the influence this immobilization process has on titanium surfaces, mirror-polished commercially pure titanium surfaces were cathodically polarized in the presence of doxycycline and the modified surfaces were thoroughly characterized using atomic force microscopy, electron microscopy, secondary ion mass spectrometry, and angle-resolved X-ray spectroscopy. We demonstrated that no hydride was created during the polarization process. Doxycycline was found to be attached to an oxide layer that was modified during the electrochemical process. A bacterial assay using bioluminescent Staphylococcus epidermidis Xen43 showed the ability of the coating to reduce bacterial colonization and planktonic bacterial growth. - Highlights: • Titanium hydride was found not to be involved in immobilization of doxycycline. • Doxycycline coating was strongly bound to a modified surface oxide layer. • Effect of coatings tested using a dynamic bacteria assay based on bioluminescence. • Topmost layer of adsorbed doxycycline was shown to have strong antibacterial effect.

  13. Macrophage polarization in response to ECM coated polypropylene mesh.

    Science.gov (United States)

    Wolf, Matthew T; Dearth, Christopher L; Ranallo, Christian A; LoPresti, Samuel T; Carey, Lisa E; Daly, Kerry A; Brown, Bryan N; Badylak, Stephen F

    2014-08-01

    The host response to implanted biomaterials is a highly regulated process that influences device functionality and clinical outcome. Non-degradable biomaterials, such as knitted polypropylene mesh, frequently elicit a chronic foreign body reaction with resultant fibrosis. Previous studies have shown that an extracellular matrix (ECM) hydrogel coating of polypropylene mesh reduces the intensity of the foreign body reaction, though the mode of action is unknown. Macrophage participation plays a key role in the development of the foreign body reaction to biomaterials, and therefore the present study investigated macrophage polarization following mesh implantation. Spatiotemporal analysis of macrophage polarization was conducted in response to uncoated polypropylene mesh and mesh coated with hydrated and dry forms of ECM hydrogels derived from either dermis or urinary bladder. Pro-inflammatory M1 macrophages (CD86+/CD68+), alternatively activated M2 macrophages (CD206+/CD68+), and foreign body giant cells were quantified between 3 and 35 days. Uncoated polypropylene mesh elicited a dominant M1 response at the mesh fiber surface, which was decreased by each ECM coating type beginning at 7 days. The diminished M1 response was accompanied by a reduction in the number of foreign body giant cells at 14 and 35 days, though there was a minimal effect upon the number of M2 macrophages at any time. These results show that ECM coatings attenuate the M1 macrophage response and increase the M2/M1 ratio to polypropylene mesh in vivo. Copyright © 2014 Elsevier Ltd. All rights reserved.

  14. Investigation of propagation algorithms for ray-tracing simulation of polarized neutrons

    DEFF Research Database (Denmark)

    Bergbäck Knudsen, Erik; Tranum-Rømer, A.; Willendrup, Peter Kjær

    2014-01-01

    Ray-tracing of polarized neutrons faces a challenge when the neutron propagates through an inhomogeneous magnetic field. This affects simulations of novel instruments using encoding of energy or angle into the neutron spin. We here present a new implementation of propagation of polarized neutrons...... within the McStas simulation package and show that it outperforms the de-facto standard method implemented in the NISP package by Seeger and Daemen. We include simulation of a simplified model of a spin-echo instrument, including a simple virtual experiment.......Ray-tracing of polarized neutrons faces a challenge when the neutron propagates through an inhomogeneous magnetic field. This affects simulations of novel instruments using encoding of energy or angle into the neutron spin. We here present a new implementation of propagation of polarized neutrons...

  15. Polarized neutron reflectivity and scattering studies of magnetic heterostructures

    Science.gov (United States)

    Zabel, H.; Theis-Bröhl, K.

    2003-02-01

    The current interest in the magnetism of ultrathin films and multilayers is driven by their manifold applications in the magneto-and spin-electronic areas, for instance as magnetic field sensors or as information storage devices. In this regard, there is a large interest in exploring spin structures and spin disorder at the interface of magnetic heterostructures, to investigate magnetic domains in thin films and superlattices, and to understand remagnetization processes of various laterally shaped magnetic nanostructures. Traditionally neutron scattering has played a dominant role in the determination of spin structures, phase transitions and magnetic excitations in bulk materials. Today, its potential for the investigation of thin magnetic films has to be redefined. Polarized neutron reflectivity (PNR) at small wavevectors can provide precise information on the magnetic field distribution parallel to the film plane and on layer resolved magnetization vectors. In addition, PNR is not only sensitive to structural interface roughness but also to the magnetic roughness. Furthermore, magnetic hysteresis measurements from polarized small angle Bragg reflections allows us to filter out correlation effects during magnetization reversals of magnetic stripes and islands. An overview is provided on most recent PNR investigations of magnetic heterostructures.

  16. Polarized neutron reflectivity and scattering studies of magnetic heterostructures

    International Nuclear Information System (INIS)

    Zabel, H; Theis-Broehl, K

    2003-01-01

    The current interest in the magnetism of ultrathin films and multilayers is driven by their manifold applications in the magneto-and spin-electronic areas, for instance as magnetic field sensors or as information storage devices. In this regard, there is a large interest in exploring spin structures and spin disorder at the interface of magnetic heterostructures, to investigate magnetic domains in thin films and superlattices, and to understand remagnetization processes of various laterally shaped magnetic nanostructures. Traditionally neutron scattering has played a dominant role in the determination of spin structures, phase transitions and magnetic excitations in bulk materials. Today, its potential for the investigation of thin magnetic films has to be redefined. Polarized neutron reflectivity (PNR) at small wavevectors can provide precise information on the magnetic field distribution parallel to the film plane and on layer resolved magnetization vectors. In addition, PNR is not only sensitive to structural interface roughness but also to the magnetic roughness. Furthermore, magnetic hysteresis measurements from polarized small angle Bragg reflections allows us to filter out correlation effects during magnetization reversals of magnetic stripes and islands. An overview is provided on most recent PNR investigations of magnetic heterostructures

  17. Self-assembled iron oxide nanoparticle multilayer: x-ray and polarized neutron reflectivity.

    Science.gov (United States)

    Mishra, D; Benitez, M J; Petracic, O; Badini Confalonieri, G A; Szary, P; Brüssing, F; Theis-Bröhl, K; Devishvili, A; Vorobiev, A; Konovalov, O; Paulus, M; Sternemann, C; Toperverg, B P; Zabel, H

    2012-02-10

    We have investigated the structure and magnetism of self-assembled, 20 nm diameter iron oxide nanoparticles covered by an oleic acid shell for scrutinizing their structural and magnetic correlations. The nanoparticles were spin-coated on an Si substrate as a single monolayer and as a stack of 5 ML forming a multilayer. X-ray scattering (reflectivity and grazing incidence small-angle scattering) confirms high in-plane hexagonal correlation and a good layering property of the nanoparticles. Using polarized neutron reflectivity we have also determined the long range magnetic correlations parallel and perpendicular to the layers in addition to the structural ones. In a field of 5 kOe we determine a magnetization value of about 80% of the saturation value. At remanence the global magnetization is close to zero. However, polarized neutron reflectivity reveals the existence of regions in which magnetic moments of nanoparticles are well aligned, while losing order over longer distances. These findings confirm that in the nanoparticle assembly the magnetic dipole-dipole interaction is rather strong, dominating the collective magnetic properties at room temperature.

  18. A fan analyzer of neutron beam polarization on the spectrometer REMUR at the pulsed reactor IBR-2

    International Nuclear Information System (INIS)

    Ul'yanov, V.A.; Pusenkov, V.M.; Pleshanov, N.K.

    2004-01-01

    The new spectrometer of polarized neutrons REMUR has been created and put in operation at the Frank Laboratory of Neutron Physics (JINR, Dubna). The spectrometer is dedicated to investigations of multilayer structures and surfaces by registering the reflection of polarized neutrons and of the inhomogeneous state of solid matter by measuring the small-angle scattering of polarized neutrons. The spectrometer's working range of neutron wavelengths is 1.5-10 Angstroem. The spectrometer is equipped with a linear position-sensitive detector and a focused supermirror polarization analyzer (the fan-like polarization analyzer) with a solid angle of polarized neutron detection of 2.2·10 -4 rad. This paper describes the design and the principle of operation of the fan analyzer of neutron polarization together with the results of the fan tests on a polarized neutron beam

  19. Interface alloying in multilayer thin films using polarized neutron reflectometry

    International Nuclear Information System (INIS)

    Basu, Saibal

    2013-01-01

    Polarized Neutron Reflectometry (PNR) is an excellent tool to probe magnetic depth profile in multilayer thin film samples. In case of multilayer films with alternating magnetic and non-magnetic layers, PNR can provide magnetic depth profile at the interfaces with better than nanometer resolution. Using PNR and Xray Reflectometry (XRR) together one can obtain chemical composition and magnetic structure, viz. magnetic moment density at interfaces in multilayer films. We have used these two techniques to obtain kinetics of alloy formation at the interfaces and the magnetic nature of the alloy at the interfaces in several important thin films with magnetic/non-magnetic bilayers. These include Ni/Ti, Ni/Al and Si/Ni pairs. Results obtained from these studies will be presented in this talk. (author)

  20. Measurement of anisotropy constant in US with polarized neutrons

    DEFF Research Database (Denmark)

    Lander, G.H.; Brooks, M.S.S.; Lebech, B.

    1991-01-01

    than found in TbFe2 at 0 K. The method we have used is with polarized neutrons. Because the neutron interaction with the magnetic moment is vectorial in nature we can determine individually the magnitude and direction of the moment in an applied field. In many cases this method has advantages over......Uranium compounds can have an anisotropy that is considerably greater than that found in rare‐earth compounds. Early estimates of K1 in ferromagnetic US (Tc = 178 K), for example, were that K1 ≳ 108 erg/cm3. We have re‐examined this cubic material and determined K1 in the range of reduced moment (μ....../μ0) from 0.1 magnitude. The highest measured K1 is 2 × 108 erg/cm3 at (μ/μ0) = 0.7, but an extrapolation, which we anticipate on arguments of symmetry, to (μ/μ0)=1, (T=0 K) gives K1 ∼ 1010 erg/cm3, some 20 times more...

  1. Small-angle neutron scattering investigations of magnetic nanostructures and interfaces using polarized neutrons

    Science.gov (United States)

    Wiedenmann, Albrecht

    2001-03-01

    Using polarized neutrons, the relative contrasts for small-angle scattering are strongly modified which allows a precise evaluation of magnetization, density and composition profiles at surfaces and interfaces of nanoscaled materials. In Co ferrofluids, the magnetic core behaves as a non-interacting single domain. The core is encapsulated by a shell of surfactant molecules which was found to be impenetrable for the solvent. In soft magnetic Fe-Si-B-(Nb,Cu) and Fe-Nb-B alloys, the presence of a weak magnetic interface between ferromagnetic nanocrystals and amorphous matrix has been demonstrated which breaks the exchange interactions.

  2. The HB-2D Polarized Neutron Development Beamline at the High Flux Isotope Reactor

    Science.gov (United States)

    Crow, Lowell; Hamilton, WA; Zhao, JK; Robertson, JL

    2016-09-01

    The Polarized Neutron Development beamline, recently commissioned at the HB-2D position on the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory, provides a tool for development and testing of polarizers, polarized neutron devices, and prototyping of polarized neutron techniques. With available monochromators including pyrolytic graphite and polarizing enriched Fe-57 (Si), the instrument has operated at 4.25 and 2.6 Å wavelengths, using crystal, supermirror, or He-3 polarizers and analyzers in various configurations. The Neutron Optics and Development Team has used the beamline for testing of He-3 polarizers for use at other HFIR and Spallation Neutron Source (SNS) instruments, as well as a variety of flipper devices. Recently, we have acquired new supermirror polarizers which have improved the instrument performance. The team and collaborators also have continuing demonstration experiments of spin-echo focusing techniques, and plans to conduct polarized diffraction measurements. The beamline is also used to support a growing use of polarization techniques at present and future instruments at SNS and HFIR.

  3. Polarized 3He Neutron Spin Filters at Oak Ridge National Laboratory

    Science.gov (United States)

    Jiang, C. Y.; Tong, X.; Brown, D. R.; Lee, W. T.; Ambaye, H.; Craig, J. W.; Crow, L.; Culbertson, H.; Goyette, R.; Graves-Brook, M. K.; Hagen, M. E.; Kadron, B.; Lauter, V.; McCollum, L. W.; Robertson, J. L.; Winn, B.; Vandegrift, A. E.

    The unique advantages of using polarized 3He as neutron spin filters, such as broadband and wide angular acceptance of neutron beams, have made it widely used in most neutron facilities. Over the last several years, we have developed a polarized 3He program to meet the increasing needs of 3He based neutron spin filters at the Oak Ridge National Laboratory's (ORNL) High Flux Isotope Reactor (HFIR) and Spallation Neutron Source (SNS). At ORNL, polarized 3He is produced using Spin Exchange Optical Pumping (SEOP). We have constructed a 3He cell fabrication station to produce 3He cells of different pressures and dimensions. Two optical pumping stations have been built in the lab to perform ex situ pumping of 3He. A compact in situ3He analyzer has been constructed and installed for the Magnetism Reflectometer (MAGICS) at SNS. A novel polarized 3He filling station for the Hybrid Spectrometer (HYSPEC) at SNS is under development.

  4. Development of a polarized neutron beam line at Algerian research reactors using McStas software

    Energy Technology Data Exchange (ETDEWEB)

    Makhloufi, M., E-mail: makhloufi_8m@yahoo.fr [Centre de Recherche Nucléaire de Birine (Algeria); Salah, H. [Centre de Recherche Nucléaire d' Alger (Algeria)

    2017-02-01

    Unpolarized instrumentation has long been studied and designed using McStas simulation tool. But, only recently new models were developed for McStas to simulate polarized neutron scattering instruments. In the present contribution, we used McStas software to design a polarized neutron beam line, taking advantage of the available spectrometers reflectometer and diffractometer in Algeria. Both thermal and cold neutron was considered. The polarization was made by two types of supermirrors polarizers FeSi and CoCu provided by the HZB institute. For sake of performance and comparison, the polarizers were characterized and their characteristics reproduced. The simulated instruments are reported. Flipper and electromagnets for guide field are developed. Further developments including analyzers and upgrading of the existing spectrometers are underway. - Highlights: • Permit to evaluate the feasibility of a polarized neutron scattering instrument prior to its implementation. • Help to understand the origin of instrumental imperfections and offer an optimized set up configuration. • Provide the possibility to use the FeSi and CoCu supermirrors, designed to polarize spin up cold neutron, to polarize thermal neutron.

  5. Boron carbide coatings for neutron detection probed by x-rays, ions, and neutrons to determine thin film quality

    Science.gov (United States)

    Nowak, G.; Störmer, M.; Becker, H.-W.; Horstmann, C.; Kampmann, R.; Höche, D.; Haese-Seiller, M.; Moulin, J.-F.; Pomm, M.; Randau, C.; Lorenz, U.; Hall-Wilton, R.; Müller, M.; Schreyer, A.

    2015-01-01

    Due to the present shortage of 3He and the associated tremendous increase of its price, the supply of large neutron detection systems with 3He becomes unaffordable. Alternative neutron detection concepts, therefore, have been invented based on solid 10B converters. These concepts require development in thin film deposition technique regarding high adhesion, thickness uniformity and chemical purity of the converter coating on large area substrates. We report on the sputter deposition of highly uniform large-area 10B4C coatings of up to 2 μm thickness with a thickness deviation below 4% using the Helmholtz-Zentrum Geesthacht large area sputtering system. The 10B4C coatings are x-ray amorphous and highly adhesive to the substrate. Material analysis by means of X-ray-Photoelectron Spectroscopy, Secondary-Ion-Mass-Spectrometry, and Rutherford-Back-Scattering (RBS) revealed low impurities concentration in the coatings. The isotope composition determined by Secondary-Ion-Mass-Spectrometry, RBS, and inelastic nuclear reaction analysis of the converter coatings evidences almost identical 10B isotope contents in the sputter target and in the deposited coating. Neutron conversion and detection test measurements with variable irradiation geometry of the converter coating demonstrate an average relative quantum efficiency ranging from 65% to 90% for cold neutrons as compared to a black 3He-monitor. Thus, these converter coatings contribute to the development of 3He-free prototype detectors based on neutron grazing incidence. Transferring the developed coating process to an industrial scale sputtering system can make alternative 3He-free converter elements available for large area neutron detection systems.

  6. Characterization and development of diamond-like carbon coatings for storing ultracold neutrons

    CERN Document Server

    Grinten, M G D; Shiers, D; Baker, C A; Green, K; Harris, P G; Iaydjiev, P S; Ivanov, S N; Geltenbort, P

    1999-01-01

    In order to determine the suitability of diamond-like carbon (DLC) as a material for storing ultracold neutrons to use in neutron electric-dipole moment (EDM) experiments, a number of tests on DLC coatings have been performed. Thin DLC layers deposited on quartz and aluminium substrates by chemical vapour deposition have been characterised by neutron transmission, neutron reflectometry, electron microscopy and neutron and mercury storage and depolarisation lifetime measurements. Two types of DLC have been compared; DLC made by chemical vapour deposition from natural methane and DLC made by chemical vapour deposition from deuterated methane. With these samples we determined the density, hydrogen concentration and Fermi potential of the coatings. DLC coatings made from deuterated methane are now successfully being used in an experiment to measure the EDM of the neutron.

  7. Characterization and development of diamond-like carbon coatings for storing ultracold neutrons

    International Nuclear Information System (INIS)

    Grinten, M.G.D. van der; Pendlebury, J.M.; Shiers, D.; Baker, C.A.; Green, K.; Harris, P.G.; Iaydjiev, P.S.; Ivanov, S.N.; Geltenbort, P.

    1999-01-01

    In order to determine the suitability of diamond-like carbon (DLC) as a material for storing ultracold neutrons to use in neutron electric-dipole moment (EDM) experiments, a number of tests on DLC coatings have been performed. Thin DLC layers deposited on quartz and aluminium substrates by chemical vapour deposition have been characterised by neutron transmission, neutron reflectometry, electron microscopy and neutron and mercury storage and depolarisation lifetime measurements. Two types of DLC have been compared; DLC made by chemical vapour deposition from natural methane and DLC made by chemical vapour deposition from deuterated methane. With these samples we determined the density, hydrogen concentration and Fermi potential of the coatings. DLC coatings made from deuterated methane are now successfully being used in an experiment to measure the EDM of the neutron

  8. The polarized neutron spectrometer REMUR at the pulsed reactor IBR-2

    International Nuclear Information System (INIS)

    Aksenov, V.L.; Zhernenkov, K.N.; Kozhevnikov, S.V.; Nikitenko, Yu.V.; Petrenko, A.V.; Lauter, H.J.; Lauter-Pasyuk, V.

    2004-01-01

    At the Laboratory of Neutron Physics (JINR, Dubna) the new polarized neutron spectrometer REMUR has been constructed and commissioned. The spectrometer REMUR is dedicated to investigations of multilayers and surfaces by polarized neutron reflection and of the inhomogeneous state of solids by diffuse small-angle polarized neutron scattering. The spectrometer operates in the neutron wavelength interval 1-10 Angstroem. In the reflectometry mode it allows one to complete polarization analysis and neutron position-sensitive detection within the solid angle of scattering 2.2·10 -4 rad. The spectrometer ensures good statistics of the reflectometric data in the scattering wave vector interval 3·10 -3 - 5·10 -1 Angstroem -1 . In the small-angle scattering mode the spectrometer allows the investigation of neutron scattering processes without spin-flip over the detector's neutron registration solid angle interval from 4·10 -3 to 10 -1 rad and the scattering wave vector interval from 0.006-0.15 to 0.03-0.7 Angstroem -1 , respectively

  9. The High-Energy Polarization-Limiting Radius of Neutron Star Magnetospheres 1, Slowly Rotating Neutron Stars

    CERN Document Server

    Heyl, J S; Lloyd, D; CERN. Geneva; Heyl, Jeremy S.; Shaviv, Nir J.; Lloyd, Don

    2003-01-01

    In the presence of strong magnetic fields, the vacuum becomes a birefringent medium. We show that this QED effect decouples the polarization modes of photons leaving the NS surface. Both the total intensity and the intensity in each of the two modes is preserved along a ray's path through the neutron-star magnetosphere. We analyze the consequences that this effect has on aligning the observed polarization vectors across the image of the stellar surface to generate large net polarizations. Counter to previous predictions, we show that the thermal radiation of NSs should be highly polarized even in the optical. When detected, this polarization will be the first demonstration of vacuum birefringence. It could be used as a tool to prove the high magnetic field nature of AXPs and it could also be used to constrain physical NS parameters, such as $R/M$, to which the net polarization is sensitive.

  10. Polarized neutron beam properties for measuring parity-violating spin rotation in liquid {sup 4}He

    Energy Technology Data Exchange (ETDEWEB)

    Micherdzinska, A.M., E-mail: amicherd@gwu.ed [Indiana University/IU Center for Exploration of Energy and Matter, Bloomington, IN 47408 (United States); George Washington University, Washington, DC 20052 (United States); Bass, C.D. [Indiana University/IU Center for Exploration of Energy and Matter, Bloomington, IN 47408 (United States); National Institute of Standards and Technology, Gaithersburg, MD 20899 (United States); Bass, T.D. [Indiana University/IU Center for Exploration of Energy and Matter, Bloomington, IN 47408 (United States); Gan, K. [George Washington University, Washington, DC 20052 (United States); Luo, D. [Indiana University/IU Center for Exploration of Energy and Matter, Bloomington, IN 47408 (United States); Markoff, D.M. [North Carolina Central University, Durham, NC 27707 (United States); Mumm, H.P.; Nico, J.S. [National Institute of Standards and Technology, Gaithersburg, MD 20899 (United States); Opper, A.K. [George Washington University, Washington, DC 20052 (United States); Sharapov, E.I. [Joint Institute for Nuclear Research, Dubna 141980 (Russian Federation); Snow, W.M. [Indiana University/IU Center for Exploration of Energy and Matter, Bloomington, IN 47408 (United States); Swanson, H.E. [University of Washington/CENPA, Seattle, WA 98195 (United States); Zhumabekova, V. [Al-Farabi Kazakh National University, Al-Farabi Ave. 71, 050038 Almaty (Kazakhstan)

    2011-03-01

    Measurements of parity-violating neutron spin rotation can provide insight into the poorly understood nucleon-nucleon weak interaction. Because the expected rotation angle per unit length is small (10{sup -7} rad/m), several properties of the polarized cold neutron beam phase space and the neutron optical elements of the polarimeter must be measured to quantify possible systematic effects. This paper presents (1) an analysis of a class of possible systematic uncertainties in neutron spin rotation measurements associated with the neutron polarimetry, and (2) measurements of the relevant neutron beam properties (intensity distribution, energy spectrum, and the product of the neutron beam polarization and the analyzing power as a function of the beam phase space properties) on the NG-6 cold neutron beam-line at the National Institute of Standards and Technology Center for Neutron Research. We conclude that the phase space nonuniformities of the polarimeter in this beam are small enough that a parity-violating neutron spin rotation measurement in n-{sup 4}He with systematic uncertainties at the 10{sup -7} rad/m level is possible.

  11. The Polarized Neutron Spectrometer REMUR at the Pulsed Reactor IBR-2

    CERN Document Server

    Aksenov, V L; Kozhevnikov, S V; Lauter, H; Lauter-Pasyuk, V; Nikitenko, Yu V; Petrenko, A V

    2004-01-01

    A new polarized neutron spectrometer REMUR has been constructed and commissioned. The spectrometer REMUR is dedicated to investigations of multilayers and surfaces by polarized neutron reflection and of the inhomogeneous state of solids by diffuse small-angle polarized neutron scattering. The spectrometer operates in the neutron wavelength interval 1\\div 10 A. In the reflectometry mode it allows one to complete polarization analysis and neutron position-sensitive detection within the solid angle of scattering 2.2\\cdot 10^{-4} rad. The spectrometer ensures good statistics of the reflectometric data in the scattering wave vector interval 3\\cdot 10^{-3}\\div 5\\cdot 10^{-1} A^{-1}. In the small-angle scattering mode the spectrometer allows the investigation of neutron scattering processes without spin-flip over the detector's neutron registration solid angle interval from 4\\cdot 1-^{-3} to 10^{-1} rad and the scattering wave vector interval from 0.006\\div 0.15 to 0.03\\div 0.7 A^{-1}, respectively.

  12. Nanostructures and ordering phenomena in ferrofluids investigated using polarized small angle neutron scattering

    International Nuclear Information System (INIS)

    Wiedenmann, A; Kammel, M; Heinemann, A; Keiderling, U

    2006-01-01

    Polarized small angle neutron scattering (SANSPOL) was used to investigate the microstructure of various ferrofluids (FF) where magnetic materials (Co, Fe magnetite), stabilization mechanisms (electrostatic, monolayers and bilayers of surfactants) and carrier liquids (water, organic solvents) have been systematically varied. Magnetic core-shell particles, non-magnetic micelles and magnetic aggregates were identified and size distributions and density, composition, and magnetization profiles were determined. Partial penetrations of solvent molecules inside the surfactant layer and formation of non-magnetic oxide coatings were established. The magnetic nanostructure in diluted samples consists of non-interacting ferromagnetic single domain particles. In concentrated Co FF a pseudo-crystalline ordering was found to be induced by an external magnetic field where cobalt core-shell particles are arranged in hexagonal planes. The particle ordering and magnetic moment direction followed the direction of the applied field. In addition, segments of uncorrelated dipolar chains were found to be present. The dynamics of the field induced ordering was studied by means of time-resolved SANS. Individual particle moments are stuck by field induced dipolar interactions in domains of local hexagonal ordering which relax by rotational diffusion when the field is switched off, with a characteristic time of a few seconds

  13. Nanostructures and ordering phenomena in ferrofluids investigated using polarized small angle neutron scattering

    Science.gov (United States)

    Wiedenmann, A.; Kammel, M.; Heinemann, A.; Keiderling, U.

    2006-09-01

    Polarized small angle neutron scattering (SANSPOL) was used to investigate the microstructure of various ferrofluids (FF) where magnetic materials (Co, Fe magnetite), stabilization mechanisms (electrostatic, monolayers and bilayers of surfactants) and carrier liquids (water, organic solvents) have been systematically varied. Magnetic core-shell particles, non-magnetic micelles and magnetic aggregates were identified and size distributions and density, composition, and magnetization profiles were determined. Partial penetrations of solvent molecules inside the surfactant layer and formation of non-magnetic oxide coatings were established. The magnetic nanostructure in diluted samples consists of non-interacting ferromagnetic single domain particles. In concentrated Co FF a pseudo-crystalline ordering was found to be induced by an external magnetic field where cobalt core-shell particles are arranged in hexagonal planes. The particle ordering and magnetic moment direction followed the direction of the applied field. In addition, segments of uncorrelated dipolar chains were found to be present. The dynamics of the field induced ordering was studied by means of time-resolved SANS. Individual particle moments are stuck by field induced dipolar interactions in domains of local hexagonal ordering which relax by rotational diffusion when the field is switched off, with a characteristic time of a few seconds.

  14. Wide-angle polarization analysis with 3He for neutron scattering instrumentation at the JCNS

    Science.gov (United States)

    Ioffe, A.; Babcock, E.; Pipich, V.; Radulescu, A.

    2011-06-01

    Polarization analysis is an important technique for polarized neutron scattering as it allows one to obtain the full information about the vector magnetization in the sample that is critically important for detailed understanding of physical properties of molecular magnets, new superconductors, spin electronic and magnetic nanostructures, as well as the self-organization of magnetic nanostructures. In the simplified 1-dimensional version polarization analysis allows for the separation of coherent and incoherent scattering, making it a potentially important technique for studies of non-deuterated biological objects that themselves produce unavoidable background. We compare some of the major considerations between two different methods for the polarization analysis - supermirror based analyzers and polarized 3He neutron spin filters and point out when the latter is beneficial from the point of view of our neutron experiments and instrumentation. We will also discuss some specific requirements to such neutron spin filters and summarize the classes of instrumentation where they will be applied at the JCNS. Finally we will describe a successful application for small-angle neutron scattering from a biological sample.

  15. Wide-angle polarization analysis with 3He for neutron scattering instrumentation at the JCNS

    International Nuclear Information System (INIS)

    Ioffe, A; Babcock, E; Pipich, V; Radulescu, A

    2011-01-01

    Polarization analysis is an important technique for polarized neutron scattering as it allows one to obtain the full information about the vector magnetization in the sample that is critically important for detailed understanding of physical properties of molecular magnets, new superconductors, spin electronic and magnetic nanostructures, as well as the self-organization of magnetic nanostructures. In the simplified 1-dimensional version polarization analysis allows for the separation of coherent and incoherent scattering, making it a potentially important technique for studies of non-deuterated biological objects that themselves produce unavoidable background. We compare some of the major considerations between two different methods for the polarization analysis - supermirror based analyzers and polarized 3 He neutron spin filters and point out when the latter is beneficial from the point of view of our neutron experiments and instrumentation. We will also discuss some specific requirements to such neutron spin filters and summarize the classes of instrumentation where they will be applied at the JCNS. Finally we will describe a successful application for small-angle neutron scattering from a biological sample.

  16. Study and production of polarized monochromatic thermal neutron beams; Etude et production de faisceaux monochromatiques polarises de neutrons lents

    Energy Technology Data Exchange (ETDEWEB)

    Beiln, H. [Commissariat a l' Energie Atomique, Saclay (France). Centre d' Etudes Nucleaires

    1963-06-15

    Results obtained with a recently built neutron spectrometer producing monochromatic polarized neutron beams,in the energy rang (10{sup -3} - 10) eV and using a series of artificial (Co: 92 per cent - Fe: 8 per cent) monocrystal as polarizers and analysers, are given. A high precision method for cutting monocrystals is explained. A description of the installation itself as well as some results obtained with Fe{sub 3}O{sub 4} crystals are also given. Experimental result pertaining to various magnetic guide and 'spin flip' system, as required in the handling of such polarized neutron beams, are also discussed. (author) [French] Nous donnons les resultats obtenus avec un spectrometre produisant des neutrons monochromatiques polarises d'energie comprise entre quelques milliemes d'electronvolts et quelques electronvotts qui utilise une serie de monocristaux artificiels de Co: 92 pour cent - Fe: 8 pour cent, comme polariseurs et analyseurs. Nous discutons egalement une methode de taille de monocristaux a tres haute precision. Le dispositif experimental ainsi que quelques resultats preliminaires obtenus avec des monocristaux de Fe{sub 3}O{sub 4} sont egalement donnes. Nous discutons egalement des resultats experimentaux obtenus avec differents systemes de guidage magnetique et de renversement du spin. (auteur)

  17. Measurement of Angular Correlations in the Decay of Polarized Neutrons

    DEFF Research Database (Denmark)

    Christensen, Carl Jørgen; Krohn, V.E.; Ringo, G.R.

    1970-01-01

    The electron-momentum-neutron-spin correlation coefficient was found to be A=-0.115±0.008, and the antineutrino-momentum-neutron-spin correlation coefficient was found to be B=1.00±0.05. The value of A leads to |GA/GV|=1.26±0.02 for the ratio of Gamow-Teller-to-Fermi coupling constants in β decay...

  18. Magnetic nanostructures studied by polarized small angle neutron scattering

    International Nuclear Information System (INIS)

    Wiedenmann, Albrecht; Kammel, Martin; Heinemann, Andre

    2005-01-01

    Small Angle Neutron Scattering using polarised neutrons is introduced as a contrast variation technique for magnetic systems. The potential of this technique is illustrated on diluted Ferrofluids. Composition, magnetization and size distributions of magnetic core-shell composite particles and magnetic aggregates could be precisely evaluated beside non-magnetic micelles and free surfactants of similar sizes. Structure factors have been extracted which revealed a local pseudo-crystalline ordering of the magnetic particles induced by magnetic fields

  19. Polarized neutron diffraction - a tool for testing extinction models: application to yttrium iron garnet

    International Nuclear Information System (INIS)

    Bonnet, M.; Delapalme, A.; Becker, P.

    1976-01-01

    This paper shows that polarized neutron experiments, which do not depend on any scale factor, are very dependent on extinction and provide original tests for extinction models. Moon, Koehler, Cable and Child (1972) have formulated the problem and proposed a first-order solution applicable only when the extinction is small. In the first part, some analytical derivations of secondary extinction corrections are discussed, using the formalism of Becker and Coppens (1974). In the second part, the main principles governing polarized neutron diffraction are briefly reviewed, with a special discussion of extinction problems. The method is then applied to the case of yttrium iron garnet (YIG). This experiment shows the technique of polarized neutrons to be very powerful for testing extinction models and for deciding whether the crystal behaves dynamically or kinematically (following Kato's criterion). (Auth.)

  20. Fundamental studies for the proton polarization technique in neutron protein crystallography

    International Nuclear Information System (INIS)

    Tanaka, Ichiro; Kusaka, Katsuhiro; Chatake, Toshiyuki; Niimura, Nobuo

    2013-01-01

    Fundamental trials to realise the proton polarization technique for detecting hydrogen with higher sensitivity in neutron protein crystallography are described. The isotope effect in conventional neutron protein crystallography (NPC) can be eliminated by the proton polarization technique (ppt). Furthermore, the ppt can improve detection sensitivity of hydrogen (relative neutron scattering length of hydrogen) by approximately eight times in comparison with conventional NPC. Several technical difficulties, however, should be overcome in order to perform the ppt. In this paper, two fundamental studies to realise ppt are presented: preliminary trials using high-pressure flash freezing has shown the advantage of making bulk water amorphous without destroying the single crystal; and X-ray diffraction and liquid-chromatography/mass-spectrometry analyses of standard proteins after introducing radical molecules into protein crystals have shown that radical molecules could be distributed non-specifically around proteins, which is essential for better proton polarization

  1. Investigation of TbMn2O5 by polarized neutron diffraction.

    Science.gov (United States)

    Zobkalo, Igor Aleksandrovich; Gavrilov, Sergei; Sazonov, Andrew; Hutanu, Vladimir

    2018-04-13

    In order to make a new approach to the elucidation of the microscopic mechanisms of multiferroicity in RMn2O5 family, experiments with different methods of polarized neutrons scattering were performed on a TbMn2O5 single crystal. We employed three different techniques of polarized neutron diffraction: without the analysis after scattering, the XYZ-polarization analysis, and technique of spherical neutron polarimetry (SNP). Measurements with SNP were undertaken both with and without external electric field. A characteristic difference in the population of "right" and "left" helix domains in all magnetically ordered phases of TbMn2O5, was observed. This difference can be controlled by an external electric field in the field-cooled mode. The analysis of the results gives an evidence that antisymmetric Dzyaloshinsky-Moria exchange is effective in all the magnetic phases in TbMn2O5. © 2018 IOP Publishing Ltd.

  2. The production, characterization, and neutronic performance of boron nitride coated uranium dioxide fuel

    International Nuclear Information System (INIS)

    Uslu, I.; Colak, U.; Tombakoglu, M.; Gunduz, G.

    1995-01-01

    The fuel pellets produced by sol-gel technique were coated with boron nitride (BN). This was achieved through chemical vapor deposition (CVD) using boron trichloride and ammonia. Mixing and chemical reaction take place at a temperature around 875 K. The coated samples were then sintered at 1600 K. Thermal reactor physics lattice-cell code WIMS-D/4 was used in the neutronic analysis of CANDU fuel bundle to observe the neutronic performance of the coated fuel. Three types of fuel were considered; fuel made of natural uranium, slightly enriched uranium (SEU, enrichment: 0.82 % U-235), and SEU with various BN coatings. The burnup calculations showed that feasible coating thickness is between 1 to 2 μm. (author)

  3. Development of high-polarization Fe/Ge neutron polarizing supermirror: Possibility of fine-tuning of scattering length density in ion beam sputtering

    Science.gov (United States)

    Maruyama, R.; Yamazaki, D.; Akutsu, K.; Hanashima, T.; Miyata, N.; Aoki, H.; Takeda, M.; Soyama, K.

    2018-04-01

    The multilayer structure of Fe/Si and Fe/Ge systems fabricated by ion beam sputtering (IBS) was investigated using X-ray and polarized neutron reflectivity measurements and scanning transmission electron microscopy with energy-dispersive X-ray analysis. The obtained result revealed that the incorporation of sputtering gas particles (Ar) in the Ge layer gives rise to a marked reduction in the neutron scattering length density (SLD) and contributes to the SLD contrast between the Fe and Ge layers almost vanishing for spin-down neutrons. Bundesmann et al. (2015) have shown that the implantation of primary Ar ions backscattered at the target is responsible for the incorporation of Ar particles and that the fraction increases with increasing ion incidence angle and increasing polar emission angle. This leads to a possibility of fine-tuning of the SLD for the IBS, which is required to realize a high polarization efficiency of a neutron polarizing supermirror. Fe/Ge polarizing supermirror with m = 5 fabricated under the same condition showed a spin-up reflectivity of 0.70 at the critical momentum transfer. The polarization was higher than 0.985 for the qz range where the correction for the polarization inefficiencies of the beamline works properly. The result of the polarized neutron reflectivity measurement suggests that the "magnetically-dead" layers formed at both sides of the Fe layer, together with the SLD contrast, play a critical role in determining the polarization performance of a polarizing supermirror.

  4. Ab initio calculations versus polarized neutron diffraction for the spin density of free radicals

    CERN Document Server

    Ressouche, E

    2003-01-01

    The determination of the magnetization distribution using polarized neutron diffraction has played a key role during the last twenty years in the field of molecular magnetism. This distribution can also be obtained by first principle ab initio calculations. Such calculations always rely on approximations and the question that arises is to know whether the obtained results are reliable enough to represent accurately the properties of these molecules. The comparison between polarized neutron experimental results and ab initio calculations has turned to provide stringent tests for these methods. In the resent article a comparison between experimental and theoretical results is made and is illustrated by examples based on magnetic free radicals. (author)

  5. Recent advancements of wide-angle polarization analysis with 3He neutron spin filters

    International Nuclear Information System (INIS)

    Chen, W.C.; Gentile, T.R.; Ye, Q.; Kirchhoff, A.; Watson, S.M.; Rodriguez-Rivera, J.A.; Qiu, Y.; Broholm, C.

    2016-01-01

    Wide-angle polarization analysis with polarized 3 He based neutron spin filters (NSFs) has recently been employed on the Multi-Axis Crystal Spectrometer (MACS) at the National Institute of Standards and Technology Center for Neutron Research (NCNR). Over the past several years, the apparatus has undergone many upgrades to address the fundamental requirements for wide angle polarization analysis using spin exchange optical pumping based 3 He NSFs. In this paper, we report substantial improvements in the on-beam-line performance of the apparatus and progress toward routine user capability. We discuss new standard samples used for 3 He NSF characterization and the flipping ratio measurement on MACS. We further discuss the management of stray magnetic fields produced by operation of superconducting magnets on the MACS instrument, which can significantly reduce the 3 He polarization relaxation time. Finally, we present the results of recent development of horseshoe-shaped wide angle cells. (paper)

  6. Multi detector input and function generator for polarized neutron experiments

    International Nuclear Information System (INIS)

    De Blois, J.; Beunes, A.J.H.; Ende, P. v.d.; Osterholt, E.A.; Rekveldt, M.T.; Schipper, M.N.; Velthuis, S.G.E. te

    1998-01-01

    In this paper a VME module is described for static or stroboscopic measurements with a neutron scattering instrument, consisting essentially of a series of up to 64 3 He neutron detectors around a sample environment. Each detector is provided with an amplifier and a discriminator to separate the neutrons from noise. To reduce the wiring, the discriminator outputs are connected to the module by coding boxes. Two 16-inputs to one-output coding boxes generate serial output codes on a fiber optic connection. This basically fast connection reduces the dead time introduced by the coding, and the influence of environmental noise. With stroboscopic measurements a periodic function is used to affect the sample surrounded by a field coil. Each detected neutron is labeled with a data label containing the detector number and the time of detection with respect to a time reference. The data time base can be programmed on a linear or a nonlinear scale. An external source or an attribute of the periodic function may generate the time reference pulse. A 12-bit DAC connected to the output of an 8 K, 16-bits memory, where the pattern of the current has been stored before, generates the function. The function memory is scanned by the programmable function time base. Attributes are set by the four remaining bits of the memory. One separate detector input connects a monitor detector in the neutron beam with a 32-bit counter/timer that provides measuring on a preset count, preset time or preset frame. (orig.)

  7. Time reversal in polarized neutron decay: the emiT experiment

    CERN Document Server

    Jones, G L; Anaya, J M; Bowles, T J; Chupp, T E; Coulter, K P; Dewey, M S; Freedman, S J; Fujikawa, B K; García, A; Greene, G L; Hwang, S R; Lising, L J; Mumm, H P; Nico, J S; Robertson, R G H; Steiger, T D; Teasdale, W A; Thompson, A K; Wasserman, E G; Wietfeldt, F E; Wilkerson, J F

    2000-01-01

    The standard electro-weak model predicts negligible violation of time-reversal invariance in light quark processes. We report on an experimental test of time-reversal invariance in the beta decay of polarized neutrons as a search for physics beyond the standard model. The emiT collaboration has measured the time-reversal-violating triple-correlation in neutron beta decay between the neutron spin, electron momentum, and neutrino momentum often referred to as the D coefficient. The first run of the experiment produced 14 million events which are currently being analyzed. However, a second run with improved detectors should provide greater statistical precision and reduced systematic uncertainties.

  8. Influence of an absorbing sublayer on polarizing property of magnetic neutron mirrors

    International Nuclear Information System (INIS)

    Korneev, D.A.; Pasyuk, V.V.; Petrenko, A.V.

    1991-01-01

    Measurements of the neutron reflectivity profile from absorbing thin film mirrors deposited onto glass substrates are presented and the results compared with theoretical predictions. The spectral dependence of the scattering length of natural Gd and GdTi alloy has been determined for the first time for the thermal neutron energy range. The unstable behavior of the neutron scattering length of Gd and consequently the principle impossibility of its compensation in a wide interval of neutron wavelengths is the reason of the strong decreasing of the polarizing properties of neutron guides with ferromagnetic mirrors. The possibility is discussed of producing a new absorbing sublayers with an important decrease of reflection in the neutron wavelength range from 1 to 10 A. The neutron reflectivity was analyzed for absorbing thin BTi, BV and CdV alloys on glass substrates. The calculated reflectivity as a function of neutron wavelength was optimized for concentration and layer thickness. Fist experimental data have been performed at the Laboratory of Neutron Physics (Joint Institute for Nuclear Research, Dubna) and are presented. (author). 7 refs, 7 figs

  9. Periodic magnetic field as a polarized and focusing thermal neutron spectrometer and monochromator

    International Nuclear Information System (INIS)

    Cremer, J. T.; Williams, D. L.; Fuller, M. J.; Gary, C. K.; Piestrup, M. A.; Pantell, R. H.; Feinstein, J.; Flocchini, R. G.; Boussoufi, M.; Egbert, H. P.; Kloh, M. D.; Walker, R. B.

    2010-01-01

    A novel periodic magnetic field (PMF) optic is shown to act as a prism, lens, and polarizer for neutrons and particles with a magnetic dipole moment. The PMF has a two-dimensional field in the axial direction of neutron propagation. The PMF alternating magnetic field polarity provides strong gradients that cause separation of neutrons by wavelength axially and by spin state transversely. The spin-up neutrons exit the PMF with their magnetic spins aligned parallel to the PMF magnetic field, and are deflected upward and line focus at a fixed vertical height, proportional to the PMF period, at a downstream focal distance that increases with neutron energy. The PMF has no attenuation by absorption or scatter, as with material prisms or crystal monochromators. Embodiments of the PMF include neutron spectrometer or monochromator, and applications include neutron small angle scattering, crystallography, residual stress analysis, cross section measurements, and reflectometry. Presented are theory, experimental results, computer simulation, applications of the PMF, and comparison of its performance to Stern-Gerlach gradient devices and compound material and magnetic refractive prisms.

  10. Neutron spin filter based on optically polarized sup 3 He in a near-zero magnetic field

    CERN Document Server

    Skoy, V R; Sorokin, V N; Kolachevsky, N N; Sobelman, I I; Sermyagin, A V

    2003-01-01

    A test of polarization of sup 3 He nuclei via spin-exchange collisions with optically pumped rubidium atoms in an extremely low applied magnetic field was carried out. Permalloy magnetic shields were used to prevent a fast relaxation of sup 3 He polarization owing to the inhomogeneity of a surrounding magnetic field. The whole installation was placed at the neutron beam line of the IBR-30 facility, and used as a neutron spin filter. Thus, a prototype of new design of neutron polarizer was introduced. We intend to apply this experience for the full-scale KaTRIn facility to test the time reversal violation in neutron-nuclear reactions.

  11. Measurements Of Spin Observables In Pseudoscalar-Meson Photo-Production Using Polarized Neutrons In Solid HD

    Energy Technology Data Exchange (ETDEWEB)

    Kageya, Tsuneo

    2014-01-01

    Psuedo-scalar meson photo production measurements have been carried out with longitudinally-polarized neutrons using the circularly and linearly polarized photon beams and the CLAS at Thomas Jefferson National Accelerator Facility (Jlab). The experiment aims to obtain a complete set of spin observables on an efficient neutron target. Preliminary E asymmetries for the exclusive reaction, gamma + n(p)--> pi- + p(p), selecting quasi free neutron kinematics are discussed.

  12. A simple circular-polarized antenna: Circular waveguide horn coated with lossy magnetic material

    Science.gov (United States)

    Lee, Choon S.; Justice, D. W.; Lee, Shung-Wu

    1988-01-01

    It is shown that a circular waveguide horn coated with a lossy material in its interior wall can be used as an alternative to a corrugated waveguide for radiating a circularly polarized (CP) field. To achieve good CP radiation, the diameter of the structure must be larger than the free-space wavelength, and the coating material must be sufficiently lossy and magnetic. The device is cheaper and lighter in weight than the corrugated one.

  13. Spin density measurement of water-bridged Co-dimer using polarized neutrons

    DEFF Research Database (Denmark)

    Damgaard-Møller, Emil; Overgaard, Jacob; Chilton, Nick

    present an experimentally determined spin density using polarized neutron diffraction in a simple water-bridged cobalt dimer [Co2(H2O)(piv)4(Hpiv)2(py)2] which is known to have a small ferromagnetic coupling between the spin centers. Visualizing the SDD could get us one step further in understanding...

  14. Inverse beta decay of arbitrarily polarized neutrons in a magnetic field

    Indian Academy of Sciences (India)

    Home; Journals; Pramana – Journal of Physics; Volume 62; Issue 5. Inverse beta decay of arbitrarily polarized neutrons in a magnetic field. Kaushik Bhattacharya Palash B Pal. Research Articles Volume 62 Issue 5 May 2004 pp 1041-1058. Fulltext. Click here to view fulltext PDF. Permanent link:

  15. Relativistic theory of inverse beta-decay of polarized neutron in ...

    Indian Academy of Sciences (India)

    The relativistic theory of the inverse beta-decay of polarized neutron, + → + -, in strong magnetic field is developed. For the proton wave function we use the exact solution of the Dirac equation in the magnetic filed that enables us to account exactly for effects of the proton momentum quantization in the magnetic ...

  16. Anomalous spin distribution in the superconducting ferromagnet UCoGe studied by polarized neutron diffraction

    NARCIS (Netherlands)

    Prokeš, K.; de Visser, A.; Huang, Y.K.; Fåk, B.; Ressouche, E.

    2010-01-01

    We report a polarized neutron-diffraction study conducted to reveal the nature of the weak ferromagnetic moment in the superconducting ferromagnet UCoGe. We find that the ordered moment in the normal phase in low magnetic fields (B∥c) is predominantly located at the U atom and has a magnitude of

  17. Asymmetry in ternary fission induced by polarized neutrons and fission mechanism

    International Nuclear Information System (INIS)

    Bunakov, V.E.; Gennenvajn, F.; Dzhessinger, P.; Mutterer, M.; Petrov, G.A.

    2003-01-01

    The results of measuring the P-odd, P-even (right-left) and T-odd asymmetries of the charged particles emission in the double and ternary fission, induced by the polarized neutrons, are considered. It is shown, what kind of information on the mechanism of the ternary nuclear fission may be obtained from the theoretical analysis of these data [ru

  18. Through-thickness Residual Stress Measurement by Neutron Diffraction in Cu+W Plasma Spray Coatings

    Czech Academy of Sciences Publication Activity Database

    Luzin, V.; Matějíček, Jiří; Gnäupel-Herold, T.

    2010-01-01

    Roč. 652, č. 652 (2010), s. 50-56 ISSN 1662-9752. [International Conference on Mechanical Stress Evaluation by Neutrons and Synchrotron Radiation/5th./. Mito, 10.11.2009-12.11.2009] R&D Projects: GA MŠk ME 901 Institutional research plan: CEZ:AV0Z20430508 Keywords : fusion materials * plasma sprayed coatings * residual stress * neutron diffraction Subject RIV: JG - Metallurgy http://www.scientific.net/MSF.652.50

  19. Improvements in Boron Plate Coating Technology for Higher Efficiency Neutron Detection and Coincidence Counting Error Reduction

    Energy Technology Data Exchange (ETDEWEB)

    Menlove, Howard Olsen [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Henzlova, Daniela [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-08-25

    This informal report presents the measurement data and information to document the performance of the advanced Precision Data Technology, Inc. (PDT) sealed cell boron-10 plate neutron detector that makes use of the advanced coating materials and procedures. In 2015, PDT changed the boron coating materials and application procedures to significantly increase the efficiency of their basic corrugated plate detector performance. A prototype sealed cell unit was supplied to LANL for testing and comparison with prior detector cells. Also, LANL had reference detector slabs from the original neutron collar (UNCL) and the new Antech UNCL with the removable 3He tubes. The comparison data is presented in this report.

  20. Deep inelastic scattering of polarized electrons by polarized 3 He and the study of the neutron spin structure

    International Nuclear Information System (INIS)

    Arnold, R.G.; Bosted, P.E.; Dunne, J.; Fellbaum, J.; Keppel, C.; Rock, S.E.; Spengos, M.; Szalata, Z.M.; White, J.L.; Breton, V.; Fonvieille, H.; Roblin, Y.; Shapiro, G.; Hughes, E.W.; Borel, H.; Lombard-Nelsen, R.M.; Marroncle, J.; Morgenstern, J.; Staley, F.; Terrien, Y.; Anthony, P.L.; Dietrich, F.S.; Chupp, T.E.; Smith, T.; Thompson, A.K.; Kuhn, S.E.; Cates, G.D.; Middleton, H.; Newbury, N.R.; Anthony, P.L.; Gearhart, R.; Hughes, E.W.; Maruyama, T.; Meyer, W.; Petratos, G.G.; Pitthan, R.; Rokni, S.H.; Stuart, L.M.; White, J.L.; Woods, M.; Young, C.C.; Erbacher, R.; Kawall, D.; Kuhn, S.E.; Meziani, Z.E.; Holmes, R.; Souder, P.A.; Xu, J.; Meziani, Z.E.; Band, H.R.; Johnson, J.R.; Maruyama, T.; Prepost, R.; Zapala, G.

    1996-01-01

    The neutron longitudinal and transverse asymmetries A 1 n and A 2 n have been extracted from deep inelastic scattering of polarized electrons by a polarized 3 He target at incident energies of 19.42, 22.66 and 25.51 GeV. The measurement allows for the determination of the neutron spin structure functions g 1 n (x, Q 2 ) and g 2 n (x, Q 2 ) over the range 0.03 2 of 2 (GeV/c) 2 . The data are used for the evaluation of the Ellis-Jaffe and Bjorken sum rules. The neutron spin structure function g 1 n (x, Q 2 ) is small and negative within the range of our measurement, yielding an integral ∫ 0.03 0.6 g 1 n (x)dx - 0.028 ± 0.006 (stat) ± 0.006 (syst). Assuming Regge behavior at low x, we extract Γ 1 n ∫ 0 1 g 1 n (x)dx = - 0.031 ± 0.006 (stat) ± 0.009 (syst). Combined with previous proton integral results from SLAC experiment E143, we find Γ 1 p - Γ 1 n = 0.160 ± 0.015 in agreement with the Bjorken sum rule prediction Γ 1 p - Γ 1 p 0.176 ± 0.008 at a Q 2 value of 3 (GeV/c) 2 evaluated using α s 0.32 ± 0.05. (authors)

  1. Experimental physics with polarized protons, neutrons and deuterons

    CERN Document Server

    Lehar, František; Wilkin, Colin

    2015-01-01

    The monograph gives a comprehensive overview of the diverse aspects of the experimental study of polarization phenomena in nucleon-nucleon and nucleon-deuteron collisions. The special nature of this volume is that it is based on the original physics results and knowledge gained by one of the authors (F. Lehar), who was a respected researcher in the field for nearly fifty years. The results of these experiments provide valuable information on the spin dependence of the forces acting between nucleons in atomic nuclei, of which all matter is ultimately composed. The fundamental importance of the results means that the subject will remain topical for years to come. The book is designed for teachers and students of natural sciences, espe - cially those with interests in nuclear and particle physics, as well as for ex - perimental physicists who are investigating polarization phenomena using accelerators of charged particles. The writing of the book was initiated by F. Lehar who was the driving force beh...

  2. Diting: A polarized time-of-flight neutron reflectometer at CMRR reactor in China

    Science.gov (United States)

    Li, Xinxi; Huang, Chaoqiang; Wang, Yan; Chen, Bo; Sun, Guang'ai; Liu, Yaoguang; Gong, Jian; Kang, Wu; Liu, Hangang

    2016-11-01

    A new time-of-flight neutron reflectometer with a polarization option is developed and tested at the Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang, China. Its scattering geometry is horizontal. The constructed neutron reflectometer is a multipurpose instrument that can be used for the characterization of a stratified microstructure and hidden interfaces of solid thin films. Diting is designed for both magnetic and nonmagnetic multi-layer thin films. Spin polarization and analysis are achieved by transmission magnetized supermirrors. The sample unit is equipped with an electromagnet, which can provide a vertical magnetic field range of 0-1.2 tesla. The available neutron beam is a white beam with wavelength range of 0.15-1.25 nm, which can be cut into different wavelength resolution neutron pulses by a four-disk chopper. A two-dimensional position-sensitive detector is employed to count the specular and off-specular reflected neutron beam. A minimum reflectivity of 10-6 is measured on this instrument.

  3. Cathodic Polarization Coats Titanium Based Implant Materials with Enamel Matrix Derivate (EMD

    Directory of Open Access Journals (Sweden)

    Matthias J. Frank

    2014-03-01

    Full Text Available The idea of a bioactive surface coating that enhances bone healing and bone growth is a strong focus of on-going research for bone implant materials. Enamel matrix derivate (EMD is well documented to support bone regeneration and activates growth of mesenchymal tissues. Thus, it is a prime candidate for coating of existing implant surfaces. The aim of this study was to show that cathodic polarization can be used for coating commercially available implant surfaces with an immobilized but functional and bio-available surface layer of EMD. After coating, XPS revealed EMD-related bindings on the surface while SIMS showed incorporation of EMD into the surface. The hydride layer of the original surface could be activated for coating in an integrated one-step process that did not require any pre-treatment of the surface. SEM images showed nano-spheres and nano-rods on coated surfaces that were EMD-related. Moreover, the surface roughness remained unchanged after coating, as it was shown by optical profilometry. The mass peaks observed in the matrix-assisted laser desorption/ionization time-of-flight mass spectroscopy (MALDI-TOF MS analysis confirmed the integrity of EMD after coating. Assessment of the bioavailability suggested that the modified surfaces were active for osteoblast like MC3M3-E1 cells in showing enhanced Coll-1 gene expression and ALP activity.

  4. Efficient, High Brightness Sources of Polarized Neutrons and Photons and Their Uses

    Energy Technology Data Exchange (ETDEWEB)

    Spencer, James E.

    2000-05-18

    There are many applications that could benefit from an easily accessible source of monochromatic, high brightness, polarized gammas and neutrons. A compact and comparatively inexpensive system is discussed based on a low-energy, electron storage ring with undulators that is expected to provide 10{sup 11} epithermal n/s and 10{sup 15} {gamma}/s. This method could provide a more efficient, cleaner way to produce epithermal neutrons than conventional means. Technical innovations that make it feasible are described together with some fundamental and practical applications that also take advantage of developments in the field of high power lasers.

  5. Procedures for interface residual stress determination using neutron diffraction: Mo-coated steel gear wheel

    International Nuclear Information System (INIS)

    Bruno, Giovanni; Fanara, Carlo; Hughes, Darren J.; Ratel, Nicolas

    2006-01-01

    Residual stresses were determined in steel gear wheels coated with molybdenum using neutron diffraction. A systematic procedure was developed to assess them in both the molybdenum coating and in the steel substrate. A detailed description of the problems associated with measurements of this type is given, together with a procedure aimed at rationalising their solution. Precise sample positioning was developed using a new experimental method and advanced metrology equipment allowing off-line sample alignment and mounting. This reliably replaces the inefficient use of entrance scans, usually adopted in residual stress analysis by neutron diffraction. Corrections were applied to overcome the presence of pseudo-strains and data reduction was performed to coherently interpret the results, including the determination of the centre-of-mass of the diffracting volume. The full three-dimensional stress profile was determined in the coating and the substrate. The data analysis methodology is fully described and recommendations are given for this kind of measurement

  6. DETECTION OF COATING FAILURES IN A NEUTRONIC REACTOR

    Science.gov (United States)

    Snell, A.H.; Allison, S.K.

    1958-02-11

    This patent relates to water-cooled reactor systems and discloses a means to detect leaks in the jackets of jacketed fuel elements comprising a neutron detector located in the cooling water discharge pipe,the pipe being provided with an enlarged portion for housing the detector so that the latter is completely surrounded by the water in its passage through the pipe, said enlarged portion and detector being shielded from the reactor for the purpose of detecting only those delayed neutrons emitted in the cooling water and due to the latter picking up fission fragments from the defective fuel elements.

  7. Time-of-Flight Polarized Neutron Reflectometry on PLATYPUS: Status and Future Developments

    Science.gov (United States)

    Saerbeck, T.; Cortie, D. L.; Brück, S.; Bertinshaw, J.; Holt, S. A.; Nelson, A.; James, M.; Lee, W. T.; Klose, F.

    Time-of-flight (ToF) polarized neutron reflectometry enables the detailed investigation of depth-resolved magnetic structures in thin film and multilayer magnetic systems. The general advantage of the time-of-flight mode of operation over monochromatic instruments is a decoupling of spectral shape and polarization of the neutron beam with variable resolution. Thus, a wide Q-range can be investigated using a single angle of incidence, with resolution and flux well-adjusted to the experimental requirement. Our paper reviews the current status of the polarization equipment of the ToF reflectometer PLATYPUS and presents first results obtained on stratified Ni80Fe20/α-Fe2O3 films, revealing the distribution of magnetic moments in an exchange bias system. An outlook on the future development of the PLATYPUS polarization system towards the implementation of a polarized 3He cell is presented and discussed with respect to the efficiency and high Q-coverage up to 1 Å-1 and 0.15 Å-1 in the vertical and lateral momentum transfer, respectively.

  8. Accounting for Electronic Polarization Effects in Aqueous Sodium Chloride via Molecular Dynamics Aided by Neutron Scattering.

    Science.gov (United States)

    Kohagen, Miriam; Mason, Philip E; Jungwirth, Pavel

    2016-03-03

    Modeled ions, described by nonpolarizable force fields, can suffer from unphysical ion pairing and clustering in aqueous solutions well below their solubility limit. The electronic continuum correction takes electronic polarization effects of the solvent into account in an effective way by scaling the charges on the ions, resulting in a much better description of the ionic behavior. Here, we present parameters for the sodium ion consistent with this effective polarizability approach and in agreement with experimental data from neutron scattering, which could be used for simulations of complex aqueous systems where polarization effects are important.

  9. Search for Time Reversal Violation in Neutron Decay: A Measurement of the Transverse Polarization of Electrons

    International Nuclear Information System (INIS)

    Bodek, K.; Kaczmarek, A.; Kistryn, St.; Kuzniak, M.; Zejma, J.; Pulut, J.; Kirch, K.; Bialek, A.; Kozela, A.; Ban, G.; Naviliat-Cuncic, O.; Gorel, P.; Beck, M.; Lindroth, A.; Severijns, N.; Stephan, E.; Czarnecki, A.

    2006-01-01

    A non-zero value of the R-correlation coefficient due to the e - polarization component, perpendicular to the plane spanned by the spin of the decaying neutron and the electron momentum, would signal a violation of time reversal symmetry and thus physics beyond the Standard Model. The value of the N-correlation coefficient, given by the transverse e - polarization component within that plane, is expected to be finite. The measurement of N serves as an important systematic check of the apparatus for the R-measurement. The first phase of data taking has been completed. Preliminary results from a limited data sample show no deviations from the Standard Model predictions

  10. Off-specular polarized neutron reflectometry study of magnetic dots with a strong shape anisotropy

    CERN Document Server

    Temst, K; Moshchalkov, V V; Bruynseraede, Y; Fritzsche, H; Jonckheere, R

    2002-01-01

    We have measured the off-specular polarized neutron reflectivity of a regular array of rectangular magnetic polycrystalline Co dots, which were prepared by a combination of electron-beam lithography, molecular beam deposition, and lift-off processes. The dots have a length-to-width ratio of 4:1 imposing a strong shape anisotropy. The intensity of the off-specular satellite reflection was monitored as a function of the magnetic field applied parallel to the rows of dots and in the plane of the sample, allowing us to analyze the magnetization-reversal process using the four spin-polarized cross sections. (orig.)

  11. Neutron imaging with Medipix-2 chip and a coated sensor

    Czech Academy of Sciences Publication Activity Database

    Jakůbek, J.; Holý, T.; Lehmann, E.; Pospíšil, S.; Uher, J.; Vacík, Jiří; Vavřík, D.

    2006-01-01

    Roč. 560, č. 1 (2006), s. 143-147 ISSN 0168-9002 R&D Projects: GA MŠk(CZ) 1P04LA211 Institutional research plan: CEZ:AV0Z10480505 Keywords : neutron radiography * pixel detector * semiconductor detector Subject RIV: JB - Sensors, Measurment, Regulation Impact factor: 1.185, year: 2006

  12. Polarized neutron powder diffraction studies of antiferromagnetic order in bulk and nanoparticle NiO

    DEFF Research Database (Denmark)

    Brok, Erik; Lefmann, Kim; Deen, Pascale P.

    2015-01-01

    In many materials it remains a challenge to reveal the nature of magnetic correlations, including antiferromagnetism and spin disorder. Revealing the spin structure in magnetic nanoparticles is further complicated by the large incoherent neutron scattering cross section from water adsorbed...... surface contribution to the magnetic anisotropy. Here we explore the potential use of polarized neutron diffraction to reveal the magnetic structure in NiO bulk and nanoparticle powders by applying the XYZ-polarization analysis method. Our investigations address in particular the spin orientation in bulk...... at the particle surfaces and by the broadening of diffraction peaks due to the finite crystallite size. Moreover, the spin structure in magnetic nanoparticles may deviate significantly from that of the corresponding bulk material because of the low-symmetry surroundings of surface atoms and the large relative...

  13. Fundamental studies for the proton polarization technique in neutron protein crystallography.

    Science.gov (United States)

    Tanaka, Ichiro; Kusaka, Katsuhiro; Chatake, Toshiyuki; Niimura, Nobuo

    2013-11-01

    The isotope effect in conventional neutron protein crystallography (NPC) can be eliminated by the proton polarization technique (ppt). Furthermore, the ppt can improve detection sensitivity of hydrogen (relative neutron scattering length of hydrogen) by approximately eight times in comparison with conventional NPC. Several technical difficulties, however, should be overcome in order to perform the ppt. In this paper, two fundamental studies to realise ppt are presented: preliminary trials using high-pressure flash freezing has shown the advantage of making bulk water amorphous without destroying the single crystal; and X-ray diffraction and liquid-chromatography/mass-spectrometry analyses of standard proteins after introducing radical molecules into protein crystals have shown that radical molecules could be distributed non-specifically around proteins, which is essential for better proton polarization.

  14. The Spin Structure of the Neutron Determined Using a Polarized He-3 Target

    Energy Technology Data Exchange (ETDEWEB)

    Middleton, H

    2004-01-06

    Described is a study of the internal spin structure of the neutron performed by measuring the asymmetry in spin-dependent deep inelastic scattering of polarized electrons from nuclear polarized {sup 3}He. Stanford Linear Accelerator experiment E142's sample of 400 million scattering events collected at beam energies between 19 and 26 GeV led to the most precise measurement of a nucleon spin structure function to date. The {sup 3}He target represents a major advance in polarized target technology, using the technique of spin exchange with optically pumped rubidium vapor to produce a typical {sup 3}He nuclear polarization of 34% in a 30cm long target cell with a gas density of 2.3 x 10{sup 20} cm{sup -3}. The target polarization was measured to {+-}7% using an Adiabatic Fast Passage NMR system calibrated with the thermal equilibrium polarization of the protons in a sample of water. The relatively high polarization and target thickness were the result of the development of large volume glass target cells which had inherent nuclear spin relaxation times for the {sup 3}He gas of as long as 70 hours. A target cell production procedure is presented which focuses on special glass blowing techniques to minimize surface interactions with the {sup 3}He nuclei and careful gas purification and vacuum system procedures to reduce relaxation inducing impurities.

  15. Stress dependence of the critical currents in neutron irradiated (RE)BCO coated conductors

    Science.gov (United States)

    Emhofer, J.; Eisterer, M.; Weber, H. W.

    2013-03-01

    The application of HTS coated conductors in future fusion or accelerator magnets is currently of increasing interest. High Lorentz forces and therefore high hoop stresses act on the conductors in large coils. The conductor is furthermore exposed to neutron radiation in fusion or accelerator magnets. The expected neutron fluence over the desired lifetime of such magnets can be simulated by irradiation experiments in a fission reactor. The coated conductors were characterized in the pristine state and after irradiation to a fast neutron fluence of 1 × 1022 m-2 (ITER design fluence). The sensitivity of the critical currents to applied stress was measured in liquid nitrogen. The cold part of the setup was positioned within a rotatable split coil electro-magnet to assess the Ic-anisotropy up to 1.4 T under maximum Lorentz force configuration. The Ic-sensitivity to applied stress changed significantly in the GdBCO/IBAD conductor after irradiation, whereas nearly no change was observed in the YBCO/RABiTS conductor. Furthermore, Ic and Tc were strongly reduced in the GdBCO/IBAD sample after irradiation. The angular dependence of Ic changed for both samples in different ways after the irradiation, but no change in the angular dependence was observed upon applying stress. The high neutron capture cross-section of Gd and the resulting strong reduction of Tc seem to be responsible for the different stress dependences of Ic in irradiated Gd-123 coated conductors.

  16. GLE and Sub-GLE Redefinition in the Light of High-Altitude Polar Neutron Monitors

    Science.gov (United States)

    Poluianov, S. V.; Usoskin, I. G.; Mishev, A. L.; Shea, M. A.; Smart, D. F.

    2017-11-01

    The conventional definition of ground-level enhancement (GLE) events requires a detection of solar energetic particles (SEP) by at least two differently located neutron monitors. Some places are exceptionally well suitable for ground-based detection of SEP - high-elevation polar regions with negligible geomagnetic and reduced atmospheric energy/rigidity cutoffs. At present, there are two neutron-monitor stations in such locations on the Antarctic plateau: SOPO/SOPB (at Amundsen-Scott station, 2835 m elevation), and DOMC/DOMB (at Concordia station, 3233 m elevation). Since 2015, when the DOMC/DOMB station started continuous operation, a relatively weak SEP event that was not detected by sea-level neutron-monitor stations was registered by both SOPO/SOPB and DOMC/DOMB, and it was accordingly classified as a GLE. This would lead to a distortion of the homogeneity of the historic GLE list and the corresponding statistics. To address this issue, we propose to modify the GLE definition so that it maintains the homogeneity: A GLE event is registered when there are near-time coincident and statistically significant enhancements of the count rates of at least two differently located neutron monitors, including at least one neutron monitor near sea level and a corresponding enhancement in the proton flux measured by a space-borne instrument(s). Relatively weak SEP events registered only by high-altitude polar neutron monitors, but with no response from cosmic-ray stations at sea level, can be classified as sub-GLEs.

  17. Signatures of field induced spin polarization of neutron star matter in seismic vibrations of paramagnetic neutron star

    International Nuclear Information System (INIS)

    Bastrukov, S I; Yang, J; Podgainy, D V; Weber, F

    2003-01-01

    A macroscopic model of the dissipative magneto-elastic dynamics of viscous spin polarized nuclear matter is discussed in the context of seismic activity of a paramagnetic neutron star. The source of the magnetic field of such a star is attributed to Pauli paramagnetism of baryon matter promoted by a seed magnetic field frozen into the star in the process of gravitational collapse of a massive progenitor. Particular attention is given to the effect of shear viscosity of incompressible stellar material on the timing of non-radial torsional magneto-elastic pulsations of the star triggered by starquakes. By accentuating the fact that this kind of vibration is unique to the seismology of a paramagnetic neutron star we show that the high-frequency modes decay faster than the low-frequency modes. The obtained analytic expressions for the period and relaxation time of this mode, in which the magnetic susceptibility and viscosity enter as input parameters, are then quantified by numerical estimates for these parameters taken from early and current works on transport coefficients of dense matter. It is found that the effect of viscosity is crucial for the lifetime of magneto-torsion vibrations but it does not appreciably affect the periods of this seismic mode which fall in the realm of periods of pulsed emission of soft gamma-ray repeaters and anomalous x-ray pulsars - young super-magnetized neutron stars, radiating, according to the magnetar model, at the expense of the magnetic energy release. Finally, we present arguments that the long periodic pulsed emission of these stars in a quiescent regime of radiation can be interpreted as a manifestation of weakly damped seismic magneto-torsion vibrations exhibiting the field induced spin polarization of baryon matter

  18. New POLDI - project of reincarnation of a polarized neutron diffractometer at the reactor PIK

    Science.gov (United States)

    Zobkalo, I.; Gavrilov, S.; Matveev, V.; Fenske, J.

    2017-06-01

    The project of a considerable modernization of the polarized neutron diffractometer POLDI is discussed. It assumes the adoption of POLDI to a broader range of magnetic investigations such as determination of magnetic structures, detailed investigation of complex magnetic structures, studies of magnetic domains, study of the magnetization density maps, magnetic form-factor particularities, local susceptibility, etc. The flexible construction should permit to use either spherical neutron polarimetry technique or flipping ratio technique. Different types of polarization system were analyzed. Original focusing fan-like bender is proposed as polarizer unit. Our simulations give evidence that for the wavelength range 1.3 - 3 Å and with suitable size, such a device can give much better efficiency than 3He cells, which are often in use. The higher flux at the sample position of a factor of at least 3.3, with lower divergence and good polarization degree from 98% (1.3 Å) to above 94% (3 Å) makes the bender set-up favorable over the layout with a 3He-cell.

  19. Boron-Coated Straw Collar for Uranium Neutron Coincidence Collar Replacement

    International Nuclear Information System (INIS)

    Hu, Jianwei; Croft, Stephen; McElroy, Robert Dennis

    2017-01-01

    The objective of this project was to design and optimize, in simulation space, an active neutron coincidence counter (or collar) using boron-coated straws (BCSs) as a non- 3 He replacement to the Uranium Neutron Coincidence Collar (UNCL). UNCL has been used by the International Atomic Energy Agency (IAEA) and European Atomic Energy Community (Euratom) since the 1980s to verify the 235 U content in fresh light water reactor fuel assemblies for safeguards purposes. This report documents the design and optimization of the BCS collar.

  20. Boron-Coated Straw Collar for Uranium Neutron Coincidence Collar Replacement

    Energy Technology Data Exchange (ETDEWEB)

    Hu, Jianwei [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Croft, Stephen [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); McElroy, Robert Dennis [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2017-01-01

    The objective of this project was to design and optimize, in simulation space, an active neutron coincidence counter (or collar) using boron-coated straws (BCSs) as a non-3He replacement to the Uranium Neutron Coincidence Collar (UNCL). UNCL has been used by the International Atomic Energy Agency (IAEA) and European Atomic Energy Community (Euratom) since the 1980s to verify the 235U content in fresh light water reactor fuel assemblies for safeguards purposes. This report documents the design and optimization of the BCS collar.

  1. First storage of ultracold neutrons using foils coated with diamond-like carbon

    International Nuclear Information System (INIS)

    Atchison, F.; Brys, T.; Daum, M.; Fierlinger, P.; Geltenbort, P.; Henneck, R.; Heule, S.; Kasprzak, M.; Kirch, K.; Pichlmaier, A.; Plonka, C.; Straumann, U.; Wermelinger, C.

    2005-01-01

    For the first time, ultracold neutrons have been stored in a volume formed of foils coated with diamond-like carbon. The coefficients for loss, η, and depolarization, β, per wall collision were determined simultaneously. The results for different samples, η∼10 -4 and β∼10 -5 -10 -6 , are among the best values measured for high Fermi potential materials without elaborate surface pre-treatment. Thin foil storage material will be widely applicable, e.g., in neutron β-decay studies

  2. First storage of ultracold neutrons using foils coated with diamond-like carbon

    Energy Technology Data Exchange (ETDEWEB)

    Atchison, F. [PSI, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); Brys, T. [PSI, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); Daum, M. [PSI, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); Fierlinger, P. [PSI, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); Physik-Institut, Universitaet Zuerich (Switzerland); Geltenbort, P. [ILL, Institut Laue-Langevin, Grenoble (France); Henneck, R. [PSI, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); Heule, S. [PSI, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); Physik-Institut, Universitaet Zuerich (Switzerland); Kasprzak, M. [PSI, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); SMI, Stefan-Meyer-Institut, Vienna (Austria); Kirch, K. [PSI, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); Pichlmaier, A. [PSI, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland)]. E-mail: axel.pichlmaier@psi.ch; Plonka, C. [ILL, Institut Laue-Langevin, Grenoble (France); Straumann, U. [Physik-Institut, Universitaet Zuerich (Switzerland); Wermelinger, C. [PSI, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); ETHZ, Eidgenoessische Technische Hochschule Zuerich (Switzerland)

    2005-10-06

    For the first time, ultracold neutrons have been stored in a volume formed of foils coated with diamond-like carbon. The coefficients for loss, {eta}, and depolarization, {beta}, per wall collision were determined simultaneously. The results for different samples, {eta}{approx}10{sup -4} and {beta}{approx}10{sup -5}-10{sup -6}, are among the best values measured for high Fermi potential materials without elaborate surface pre-treatment. Thin foil storage material will be widely applicable, e.g., in neutron {beta}-decay studies.

  3. Residual stress in sprayed Ni+5%Al coatings determined by neutron diffraction

    CERN Document Server

    Matejicek, J; Gnaeupel-Herold, T; Prask, H J

    2002-01-01

    Coatings of nickel-based alloys are used in numerous high-performance applications. Their properties and lifetimes are influenced by factors such as residual stress. Neutron diffraction is a powerful tool for nondestructive residual stress determination. In this study, through-thickness residual stress profiles in Ni+5%Al coatings on steel substrates were determined. Two examples of significantly different spraying techniques - plasma spraying and cold spraying - are highlighted. Different stress-generation mechanisms are discussed with respect to process parameters and material properties. (orig.)

  4. Neutron imaging with Medipix-2 chip and a coated sensor

    Czech Academy of Sciences Publication Activity Database

    Jakůbek, J.; Holý, T.; Lehmann, E.; Pospíšil, S.; Uher, J.; Vacík, J.; Vavřík, Daniel

    2006-01-01

    Roč. 560, č. 1 (2006), s. 143-147 ISSN 0168-9002. [International Workshop on Vertex Detectors /3./. Como, 13.09.2004-17.09.2004] R&D Projects: GA MŠk(CZ) 1P04LA211 Grant - others:EU(XE) G5RD-CT-2001-00536 Institutional research plan: CEZ:AV0Z20710524 Keywords : neutron radiography * pixel detector * semiconductor detector Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders Impact factor: 1.185, year: 2006

  5. Residual Stress in Sprayed Ni+5% Al Coatings Determined by Neutron Diffraction

    Czech Academy of Sciences Publication Activity Database

    Matějíček, Jiří; Sampath, S.; Gnaupel-Herold, T.; Prask, H. J.

    2002-01-01

    Roč. 74, supplement 8 (2002), s. S1692-S1694 ISSN 0947-8396 R&D Projects: GA ČR GA106/01/0094 Grant - others:NSF DMR(US) 6932570 Institutional research plan: CEZ:AV0Z2043910 Keywords : residual stress, thermal spray coatings, neutron diffraction Subject RIV: JK - Corrosion ; Surface Treatment of Materials Impact factor: 2.231, year: 2002

  6. The Precision Measurement of the Neutron Spin Structure Function Using Polarized HE-3 Target

    Energy Technology Data Exchange (ETDEWEB)

    Wang, X

    2004-01-05

    Using a 48.6 GeV polarized electron beam scattering off a polarized {sup 3}He target at Stanford Linear Accelerator Centre (SLAC), they measured the neutron spin structure function g{sub 1}{sup n} over kinematic(x) ranging 0.014 < x <0.7 and 1 < Q{sup 2} < 17GeV{sup 2}. The measurement gave the integral result over the neutron spin structure function {integral}{sub 0.014}{sup 0.7} g{sub 1}{sup n}(x)dx = -0.036 {+-} 0.004(stat) {+-} 0.005(syst) at an average Q{sup 2} = 5GeV{sup 2}. Along with the proton results from SLAC E143 experiment (0.03 < x) and SMC experiment (0.014 < x < 0.03), they find the Bjorken sum rule appears to be largely saturated by the data integrated down to x of 0.014. However, they observe relatively large values for g{sub 1}{sup n} at low x. The result calls into question the usual methods (Regge theory) for extrapolating to x = 0 to find the full neutron integral {integral}{sub 0}{sup t} g{sub 1}{sup n}(x) dx, needed for testing the Quark-Parton Model (QMP).

  7. Design study of superconducting sextupole magnet using HTS coated conductor for neutron-focusing device

    International Nuclear Information System (INIS)

    Tosaka, T.; Koyanagi, K.; Ono, M.; Kuriyama, T.; Watanabe, I.; Tsuchiya, K.; Suzuki, J.; Adachi, T.; Shimizu, H.M.

    2006-01-01

    We performed a design study of sextupole magnet using high temperature superconducting (HTS) wires. The sextupole magnet is used as a focusing lens for neutron-focusing devices. A neutron-focusing device is desired to have a large aperture and a high magnetic field gradient of G, where G = 2B/r 2 , B is the magnetic field and r is a distance from the sextupole magnet axis. Superconducting magnets offer promising prospects to meet the demands of a neutron-focusing device. Recently NbTi coils of low temperature superconducting (LTS) have been developed for a sextupole magnet with a 46.8 mm aperture. The maximum magnetic field gradient G of this magnet is 9480 T/m 2 at 4.2 K and 12,800 T/m 2 at 1.8 K. On the other hand, rapid progress on second generation HTS wire has been made in increasing the performance of critical current and in demonstrating a long length. The second generation HTS wire is referred to as coated conductor. It consists of tape-shaped base upon which a thin coating of superconductor, usually YBCO, is deposited or grown. This paper describes a design study of sextupole magnet using coated conductors

  8. Neutron-reflectometry study of alcohol adsorption on various DLC coatings

    Energy Technology Data Exchange (ETDEWEB)

    Kalin, M., E-mail: mitjan.kalin@tint.fs.uni-lj.si [University of Ljubljana, Faculty of Mechanical Engineering, Laboratory for Tribology and Interface Nanotechnology, Bogišićeva 8, 1000 Ljubljana (Slovenia); Simič, R. [University of Ljubljana, Faculty of Mechanical Engineering, Laboratory for Tribology and Interface Nanotechnology, Bogišićeva 8, 1000 Ljubljana (Slovenia); Hirayama, T. [Department of Mechanical Engineering, Doshisha University, 1-3 Miyakodani, Tatara, Kyotanabe, Kyoto 610-0394 (Japan); Geue, T.; Korelis, P. [Paul Scherrer Institute, 5232 Villigen – PSI (Switzerland)

    2014-01-01

    Diamond-like carbon (DLC) coatings are notable for their excellent tribological properties. Our understanding of the lubrication of DLC coatings has improved drastically over the past decade. However, only a few details are known about the properties of the adsorbed layers on DLC, which crucially affect their tribological properties under lubricated conditions. In this work we used neutron reflectometry to determine the thickness and the density of adsorbed layers of alcohol molecules on several different types of DLC coatings, i.e., non-hydrogenated (a-C) and hydrogenated, of which both non-doped (a-C:H) and doped (a-C:H:F and a-C:H:Si) coatings were used. The results showed that a 0.9-nm-thick and relatively dense (≈45%) layer of alcohol adsorbed on the a-C coating. In contrast, no adsorption layer was found on the a-C:H, confirming the important role of hydrogen, which predominantly acts as a dangling-bond passivation source and affects the reactivity and tribochemistry of DLC coatings. The incorporation of F into a DLC coating also did not cause an increase in the adsorption ability with respect to alcohol molecules. On the contrary, the incorporation of Si increased the reactivity of the DLC coating so that a 1.3-nm-thick alcohol layer with a 35% bulk density was detected on the surface. We also discuss the very good agreement of the current results with the surface energy of selected coatings found in these experiments.

  9. Measurement of the Spin Structure Function of the Neutron G1(N) from Deep Inelastic Scattering of Polarized Electrons from Polarized Neutrons in He-3

    Energy Technology Data Exchange (ETDEWEB)

    Dunn, J

    2004-01-06

    Polarized electrons of energies 19.42, 22.67, and 25.5 GeV were scattered off a polarized {sup 3}He target at SLAC's End Station A to measure the spin asymmetry of the neutron. From this asymmetry, the spin dependent structure function g{sub 1}{sup n}(x) was determined over a range in x from 0.03 to 0.6 with an average Q{sup 2} of 2 (GeV/C){sup 2}. The value of the integral of g{sub 1}{sup n} over x is {integral}g{sub 1}{sup n}(x)dx = -0.036 {+-} 0.009. The results were interpreted in the frame work of the Quark Parton Model (QPM) and used to test the Ellis-Jaffe and Bjorken sum rules. The value of the integral is 2.6 standard deviations from the Ellis-Jaffe prediction while the Bjorken sum rule was found to be in agreement with this data and proton data from SMC and E-143.

  10. Neutron and X-ray diffraction of plasma-sprayed zirconia-yttria thermal barrier coatings

    Science.gov (United States)

    Shankar, N. R.; Herman, H.; Singhal, S. P.; Berndt, C. C.

    1984-01-01

    ZrO2-7.8mol. pct. YO1.5, a fused powder, and ZrO2-8.7mol. pct. YO1.5, a prereacted powder, were plasma-sprayed onto steel substrates. Neutron diffraction and X-ray diffraction of the as-received powder, the powder plasma sprayed into water, as-sprayed coatings, and coatings heat-treated for 10 and 100 h were carried out to study phase transformations and ordering of the oxygen ions on the oxygen sublattice. The as-received fused powder has a much lower monoclinic percentage than does the pre-reacted powder, this resulting in a much lower monoclinic percentage in the coating. Heat treatment increases the percentages of the cubic and monoclinic phases, while decreasing the tetragonal content. An ordered tetragonal phase is detected by the presence of extra neutron diffraction peaks. These phase transformations and ordering will result in volume changes. The implications of these transformations on the performance of partially stabilized zirconia thermal barrier coatings is discussed.

  11. Measurement of neutrino and proton asymmetry in the decay of polarized neutrons

    International Nuclear Information System (INIS)

    Schumann, M.

    2007-01-01

    The Standard Model of Particle Physics is in excellent agreement with all experimental results. However, it is not believed to be the most fundamental theory. It requires, for example, too many free parameters and is not able to explain the existence of effects such as parity-violation or CP-violation. Thus measurements have to be performed to probe the Standard Model and to search for ''new physics''. An ideal laboratory for this is the decay of the free polarized neutron. In this thesis, we present measurements of the neutrino asymmetry B and the proton asymmetry C in neutron decay. These coefficients describe the correlation between neutron spin and momentum of the respective particle, and provide detailed information on the structure of the underlying theory. The experiment was performed using the electron spectrometer PERKEO II installed at the Institut Laue-Langevin (ILL). It was equipped with a combined electron-proton detector to reconstruct the neutrino in a coincidence measurement. The uncertainty of our neutrino asymmetry result, B=0.9802(50), is comparable to the present best measurement, and, for the first time ever, we obtained a precise value for the proton asymmetry, C=-0.2377(36). Both results are used to analyze neutron decay for hints on ''Physics beyond the Standard Model'' by studying possible admixtures of right-handed currents and of scalar and tensor couplings to the interaction. (orig.)

  12. Measurement of neutrino and proton asymmetry in the decay of polarized neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Schumann, M.

    2007-05-09

    The Standard Model of Particle Physics is in excellent agreement with all experimental results. However, it is not believed to be the most fundamental theory. It requires, for example, too many free parameters and is not able to explain the existence of effects such as parity-violation or CP-violation. Thus measurements have to be performed to probe the Standard Model and to search for ''new physics''. An ideal laboratory for this is the decay of the free polarized neutron. In this thesis, we present measurements of the neutrino asymmetry B and the proton asymmetry C in neutron decay. These coefficients describe the correlation between neutron spin and momentum of the respective particle, and provide detailed information on the structure of the underlying theory. The experiment was performed using the electron spectrometer PERKEO II installed at the Institut Laue-Langevin (ILL). It was equipped with a combined electron-proton detector to reconstruct the neutrino in a coincidence measurement. The uncertainty of our neutrino asymmetry result, B=0.9802(50), is comparable to the present best measurement, and, for the first time ever, we obtained a precise value for the proton asymmetry, C=-0.2377(36). Both results are used to analyze neutron decay for hints on ''Physics beyond the Standard Model'' by studying possible admixtures of right-handed currents and of scalar and tensor couplings to the interaction. (orig.)

  13. Polarized small-angle neutron scattering (SANSPOL) for discrimination of nano sized components in ferro fluids

    International Nuclear Information System (INIS)

    Heinemann, A.; Wiedenmann, A.; Kammel, M.; Hoell, A.

    2003-01-01

    The use of polarized neutron technique in small-angle scattering (SANS) have led to new results in the case of magnetic nanometer-scale structure analysis. Different magnetic cross sections for spin-up and spin-down neutron scattering can be combined with chemical contrast variation methods. We show that the analysis of the interference term of nuclear and magnetic scattering respectively enables the extraction of additional information on the composition and magnetization profiles of the samples. This technique profits by the clear distinction between the magnetic and nonmagnetic scattering contributions and the strong auxiliary conditions for model fitting procedures. Beside general formulas for some special cases of present experimental interest, we apply the approach to cobalt bases ferro fluid scattering data obtained in the HMI-V4 experiment. (authors)

  14. Low-angle polarized neutron and X-ray scattering from magnetic nanolayers and nanostructures

    CERN Document Server

    Paul, Amitesh

    2017-01-01

    This research monograph presents the latest results related to the characterization of low dimensional systems. Low-angle polarized neutron scattering and X-ray scattering at grazing incidence are used as the two main techniques to explore various physical phenomena of these systems. Special focus is put on systems like thin film transition metal and rare-earth layers, oxide heterostructures, hybrid systems, self-assembled nanostructures and self-diffusion.  Readers will gain in-depth knowledge about the usage of specular scattering and off-specular scattering techniques. Investigation of in-plane and out-of-plane structures and magnetism with vector magnetometric information is illustrated comprehensively. The book caters to a wide audience working in the field of nano-dimensional magnetic systems and the neutron and X-ray reflectometry community in particular.

  15. Signatures of field induced spin polarization of neutron star matter in seismic vibrations of paramagnetic neutron star

    CERN Document Server

    Bastrukov, S I; Podgainy, D V; Weber, F

    2003-01-01

    A macroscopic model of the dissipative magneto-elastic dynamics of viscous spin polarized nuclear matter is discussed in the context of seismic activity of a paramagnetic neutron star. The source of the magnetic field of such a star is attributed to Pauli paramagnetism of baryon matter promoted by a seed magnetic field frozen into the star in the process of gravitational collapse of a massive progenitor. Particular attention is given to the effect of shear viscosity of incompressible stellar material on the timing of non-radial torsional magneto-elastic pulsations of the star triggered by starquakes. By accentuating the fact that this kind of vibration is unique to the seismology of a paramagnetic neutron star we show that the high-frequency modes decay faster than the low-frequency modes. The obtained analytic expressions for the period and relaxation time of this mode, in which the magnetic susceptibility and viscosity enter as input parameters, are then quantified by numerical estimates for these parameter...

  16. Model-free polarized neutron diffraction study of an acentric crystal: Metamagnetic UCoAl

    International Nuclear Information System (INIS)

    Papoular, R.J.; Delapalme, A.

    1994-01-01

    For the first time, a model-free procedure is developed to analyze polarized neutron diffraction data pertaining to acentric crystals. It consists of a two-step process, featuring first an effective flipping ratio and second a linear inverse problem. The latter is solved either by a new generalized inverse Fourier transform or by using maximum entropy. Using metamagnetic UCoAl as a test case, we find the following results: (i) the U and Co(2) moments increase with an applied magnetic field whereas the Co(1) moment remains almost constant, (ii) the U and Co(2) magnetic densities are weakly anisotropic

  17. Anomalous spin distribution in the superconducting ferromagnet UCoGe studied by polarized neutron diffraction

    OpenAIRE

    Prokes, K.; de Visser, A.; Huang, Y. K.; Fak, B.; Ressouche, E.

    2010-01-01

    We report a polarized neutron diffraction study conducted to reveal the nature of the weak ferromagnetic moment in the superconducting ferromagnet UCoGe. We find that the ordered moment in the normal phase in low magnetic fields (B // c) is predominantly located at the U atom and has a magnitude of about 0.1 muB at 3 T, in agreement with bulk magnetization data. By increasing the magnetic field the U moment grows to about 0.3 muB in 12 T and most remarkably, induces a substantial moment (abou...

  18. Spin susceptibility of the topological superconductor UPt3 from polarized neutron diffraction

    Science.gov (United States)

    Gannon, W. J.; Halperin, W. P.; Eskildsen, M. R.; Dai, Pengcheng; Hansen, U. B.; Lefmann, K.; Stunault, A.

    2017-07-01

    Experiment and theory indicate that UPt3 is a topological superconductor in an odd-parity state, based in part from the temperature independence of the NMR Knight shift. However, quasiparticle spin-flip scattering near a surface, where the Knight shift is measured, might be responsible. We use polarized neutron scattering to measure the bulk susceptibility with H ∥c , finding consistency with the Knight shift but inconsistency with theory for this field orientation. We infer that neither spin susceptibility nor a Knight shift are a reliable indication of odd parity.

  19. Neutron xyz – polarization analysis at a time-of-flight instrument

    Directory of Open Access Journals (Sweden)

    Ehlers G.

    2015-01-01

    Full Text Available When implementing a dedicated polarization analysis setup at a neutron time-of-flight instrument with a large area detector, one faces enormous challenges. Nevertheless, significant progress has been made towards this goal over the last few years. This paper addresses systematic limitations of the traditional method that is used to make these measurements, and a possible strategy to overcome these limitations. This will be important, for diffraction as well as inelastic experiments, where the scattering occurs mostly out-of-plane.

  20. Magnetization distribution in paramagnetic CoO: a polarized neutron diffraction study

    CERN Document Server

    Kernavanois, N; Brown, P J; Henry, J Y; Lelievre-Berna, E

    2003-01-01

    Unpolarized and polarized neutron diffraction by a single crystal have been used to study the magnetization distribution in the paramagnetic phase of cobalt oxide CoO. Highly accurate magnetic structure factors have been measured using the classical polarized beam method. A detailed description of the magnetization distribution is presented. The magnetization around the cobalt site has a radial distribution which is contracted by approx = 5% with respect to that of the free ion and a symmetry which approximates more closely to e sub g than to the form t sub 2 sub g sup 5 /e sub g sup 2 expected for the Co sup 2 sup + 3d sup 7 configuration. A significant magnetization, corresponding to some 8% of the total moment, is found at the oxygen site.

  1. Boron-coated straws as a replacement for {sup 3}He-based neutron detectors

    Energy Technology Data Exchange (ETDEWEB)

    Lacy, Jeffrey L., E-mail: jlacy@proportionaltech.com [Proportional Technologies, Inc., 8022 El Rio Street, Houston, TX 77054 (United States); Athanasiades, Athanasios; Sun, Liang; Martin, Christopher S.; Lyons, Tom D.; Foss, Michael A.; Haygood, Hal B. [Proportional Technologies, Inc., 8022 El Rio Street, Houston, TX 77054 (United States)

    2011-10-01

    US and international government efforts to equip major seaports with large area neutron detectors, aimed to intercept the smuggling of nuclear materials, have precipitated a critical shortage of {sup 3}He gas. It is estimated that the annual demand of {sup 3}He for US security applications alone is more than the worldwide supply. This is strongly limiting the prospects of neutron science, safeguards, and other applications that rely heavily on {sup 3}He-based detectors. Clearly, alternate neutron detection technologies that can support large sensitive areas, and have low gamma sensitivity and low cost must be developed. We propose a low-cost technology based on long copper tubes (straws), coated on the inside with a thin layer of {sup 10}B-enriched boron carbide ({sup 10}B{sub 4}C). In addition to the high abundance of boron on Earth and low cost of {sup 10}B enrichment, the boron-coated straw (BCS) detector offers distinct advantages over conventional {sup 3}He-based detectors, and alternate technologies such as {sup 10}BF{sub 3} tubes and {sup 10}B-coated rigid tubes. These include better distribution inside moderator assemblies, many-times faster electronic signals, no pressurization, improved gamma-ray rejection, no toxic or flammable gases, and ease of serviceability. We present the performance of BCS detectors dispersed in a solid plastic moderator to address the need for portal monitoring. The design adopts the outer dimensions of currently deployed {sup 3}He-based monitors, but takes advantage of the small BCS diameter to achieve a more uniform distribution of neutron converter throughout the moderating material. We show that approximately 63 BCS detectors, each 205 cm long, distributed inside the moderator, can match or exceed the detection efficiency of typical monitors fitted with a 5 cm diameter {sup 3}He tube, 187 cm long, pressurized to 3 atm.

  2. Boron-coated straws as a replacement for 3He-based neutron detectors

    International Nuclear Information System (INIS)

    Lacy, Jeffrey L.; Athanasiades, Athanasios; Sun, Liang; Martin, Christopher S.; Lyons, Tom D.; Foss, Michael A.; Haygood, Hal B.

    2011-01-01

    US and international government efforts to equip major seaports with large area neutron detectors, aimed to intercept the smuggling of nuclear materials, have precipitated a critical shortage of 3 He gas. It is estimated that the annual demand of 3 He for US security applications alone is more than the worldwide supply. This is strongly limiting the prospects of neutron science, safeguards, and other applications that rely heavily on 3 He-based detectors. Clearly, alternate neutron detection technologies that can support large sensitive areas, and have low gamma sensitivity and low cost must be developed. We propose a low-cost technology based on long copper tubes (straws), coated on the inside with a thin layer of 10 B-enriched boron carbide ( 10 B 4 C). In addition to the high abundance of boron on Earth and low cost of 10 B enrichment, the boron-coated straw (BCS) detector offers distinct advantages over conventional 3 He-based detectors, and alternate technologies such as 10 BF 3 tubes and 10 B-coated rigid tubes. These include better distribution inside moderator assemblies, many-times faster electronic signals, no pressurization, improved gamma-ray rejection, no toxic or flammable gases, and ease of serviceability. We present the performance of BCS detectors dispersed in a solid plastic moderator to address the need for portal monitoring. The design adopts the outer dimensions of currently deployed 3 He-based monitors, but takes advantage of the small BCS diameter to achieve a more uniform distribution of neutron converter throughout the moderating material. We show that approximately 63 BCS detectors, each 205 cm long, distributed inside the moderator, can match or exceed the detection efficiency of typical monitors fitted with a 5 cm diameter 3 He tube, 187 cm long, pressurized to 3 atm.

  3. Boron-coated straws as a replacement for 3He-based neutron detectors

    Science.gov (United States)

    Lacy, Jeffrey L.; Athanasiades, Athanasios; Sun, Liang; Martin, Christopher S.; Lyons, Tom D.; Foss, Michael A.; Haygood, Hal B.

    2011-10-01

    US and international government efforts to equip major seaports with large area neutron detectors, aimed to intercept the smuggling of nuclear materials, have precipitated a critical shortage of 3He gas. It is estimated that the annual demand of 3He for US security applications alone is more than the worldwide supply. This is strongly limiting the prospects of neutron science, safeguards, and other applications that rely heavily on 3He-based detectors. Clearly, alternate neutron detection technologies that can support large sensitive areas, and have low gamma sensitivity and low cost must be developed. We propose a low-cost technology based on long copper tubes (straws), coated on the inside with a thin layer of 10B-enriched boron carbide ( 10B 4C). In addition to the high abundance of boron on Earth and low cost of 10B enrichment, the boron-coated straw (BCS) detector offers distinct advantages over conventional 3He-based detectors, and alternate technologies such as 10BF 3 tubes and 10B-coated rigid tubes. These include better distribution inside moderator assemblies, many-times faster electronic signals, no pressurization, improved gamma-ray rejection, no toxic or flammable gases, and ease of serviceability. We present the performance of BCS detectors dispersed in a solid plastic moderator to address the need for portal monitoring. The design adopts the outer dimensions of currently deployed 3He-based monitors, but takes advantage of the small BCS diameter to achieve a more uniform distribution of neutron converter throughout the moderating material. We show that approximately 63 BCS detectors, each 205 cm long, distributed inside the moderator, can match or exceed the detection efficiency of typical monitors fitted with a 5 cm diameter 3He tube, 187 cm long, pressurized to 3 atm.

  4. Circular polarization of γ-quanta radiated in the capture of polarized neutrons by protons and the quark compound bag model

    International Nuclear Information System (INIS)

    Grach, I.L.; Shmatkov, M.Zh.

    1983-01-01

    The circular polarization Psub(γ) of γ-quanta radiated in the capture of polarized neutrons by protons is calculated The contribution of the M1 and E2 radiation of nucleons to Psub(γ) is found using the accurate wave functions of the continuous spectrum. The contribution of the six-quark bag to the polarization Psub(γ) is determined. The value of Psub(γ) is related to the admixture of the 6q-bag in the deuteron. Experimental value of Psub(γ) corresponds to small (< or approximately 0.7%) admixture of the bag

  5. High-Dose Neutron Detector Development Using 10B Coated Cells

    Energy Technology Data Exchange (ETDEWEB)

    Menlove, Howard Olsen [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Henzlova, Daniela [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-11-08

    During FY16 the boron-lined parallel-plate technology was optimized to fully benefit from its fast timing characteristics in order to enhance its high count rate capability. To facilitate high count rate capability, a novel fast amplifier with timing and operating properties matched to the detector characteristics was developed and implemented in the 8” boron plate detector that was purchased from PDT. Each of the 6 sealed-cells was connected to a fast amplifier with corresponding List mode readout from each amplifier. The FY16 work focused on improvements in the boron-10 coating materials and procedures at PDT to significantly improve the neutron detection efficiency. An improvement in the efficiency of a factor of 1.5 was achieved without increasing the metal backing area for the boron coating. This improvement has allowed us to operate the detector in gamma-ray backgrounds that are four orders of magnitude higher than was previously possible while maintaining a relatively high counting efficiency for neutrons. This improvement in the gamma-ray rejection is a key factor in the development of the high dose neutron detector.

  6. Evaluation of commercial nickel-phosphorus coating for ultracold neutron guides using a pinhole bottling method

    Science.gov (United States)

    Pattie, R. W.; Adamek, E. R.; Brenner, T.; Brandt, A.; Broussard, L. J.; Callahan, N. B.; Clayton, S. M.; Cude-Woods, C.; Currie, S. A.; Geltenbort, P.; Ito, T. M.; Lauer, T.; Liu, C. Y.; Majewski, J.; Makela, M.; Masuda, Y.; Morris, C. L.; Ramsey, J. C.; Salvat, D. J.; Saunders, A.; Schroffenegger, J.; Tang, Z.; Wei, W.; Wang, Z.; Watkins, E.; Young, A. R.; Zeck, B. A.

    2017-11-01

    We report on the evaluation of commercial electroless nickel phosphorus (NiP) coatings for ultracold neutron (UCN) transport and storage. The material potential of 50 μm thick NiP coatings on stainless steel and aluminum substrates was measured to be VF = 213(5 . 2) neV using the time-of-flight spectrometer ASTERIX at the Lujan Center. The loss per bounce probability was measured in pinhole bottling experiments carried out at ultracold neutron sources at Los Alamos Neutron Science Center and the Institut Laue-Langevin. For these tests a new guide coupling design was used to minimize gaps between the guide sections. The observed UCN loss in the bottle was interpreted in terms of an energy independent effective loss per bounce, which is the appropriate model when gaps in the system and upscattering are the dominate loss mechanisms, yielding a loss per bounce of 1 . 3(1) × 10-4. We also present a detailed discussion of the pinhole bottling methodology and an energy dependent analysis of the experimental results.

  7. A simple gold-coated microstructure fiber polarization filter in two communication windows

    Science.gov (United States)

    Feng, Xinxing; Li, Shuguang; Du, Huijing; Zhang, Yinan; Liu, Qiang

    2018-03-01

    A polarization filter is designed at two communication windows of 1310 and 1550 nm based on microstructured optical fiber. The model has four large diameter air holes and two gold-coated air holes. The influence of the geometrical parameters of the photonic crystal fiber on the performance of the polarization filter is analyzed by the finite element method. The numerical simulation shows that when the fiber length is 300 μm, the corresponding extinction ratio is 209.7 dB and 179.8 dB, the bandwidth of extinction ratio (ER) better than 20 dB is 150 nm and 350 nm at the communication wavelength of 1310 nm and 1550 nm.

  8. Accretion dynamics and polarized x-ray emission of magnetized neutron stars

    International Nuclear Information System (INIS)

    Arons, J.

    1991-01-01

    The basic ideas of accretion onto magnetized neutron stars are outlined. These are applied to a simple model of the structure of the plasma mound sitting at the magnetic poles of such as star, in which upward diffusion of photons is balanced by their downward advection. This steady flow model of the plasma's dynamical state is used to compute the emission of polarized X-rays from the optically thick, birefringent medium. The linear polarization of the continuum radiation emerging from the quasi-static mound is found to be as much as 40% at some rotation phases, but is insensitive to the geometry of the accretion flow. The role of the accretion shock, whose detailed polarimetric and spectral characteristics have yet to be calculated, is emphasized as the final determinant of the properties of the emerging X-rays. Some results describing the fully time dependent dynamics of the flow are also presented. In particular, steady flow onto a neutron star is shown to exhibit formation of ''photon bubbles,'' regions of greatly reduced plasma density filled with radiation which form and rise on millisecond time scales. The possible role of these complex structures in the flow for the formation of the emergent spectrum is briefly outlined

  9. Neutronic modeling for a Gas-cooled Fast Reactor assuming coated fuel particles

    International Nuclear Information System (INIS)

    Golfier, H.; Buiron, C.; Poinot, B.; Pothet, J. F.; Salavy, E.; Studer

    2004-01-01

    The modeling of gas cooled fast reactor (GCFR) with the SAPHYR system and in particular APOLLO2 code assuming coated fuel particles, was investigated. It aims to estimate the APOLLO2 code accuracy, solving the neutron transport equation in range of fast neutron reactors. A two level PIJ/SN APOLLO2 scheme is proposed in which the first level is devoted to the self-shielding and the leakage calculation on a cell configuration. The efficiency of a new treatment of adsorption and scattering rates in the self-shielding module of the multigroup transport code APOLLO2 has been evaluated. The results show that two-level scheme provides promising results with 172-group cross section libraries, which confirm the APOLLO2 scheme as a tool for reactor designs. (authors)

  10. In situ Polarized Neutron Reflectometry: Epitaxial Thin-Film Growth of Fe on Cu(001) by dc Magnetron Sputtering

    Science.gov (United States)

    Kreuzpaintner, Wolfgang; Wiedemann, Birgit; Stahn, Jochen; Moulin, Jean-François; Mayr, Sina; Mairoser, Thomas; Schmehl, Andreas; Herrnberger, Alexander; Korelis, Panagiotis; Haese, Martin; Ye, Jingfan; Pomm, Matthias; Böni, Peter; Mannhart, Jochen

    2017-05-01

    The stepwise growth of epitaxial Fe on Cu (001 )/Si (001 ) , investigated by in situ polarized neutron reflectometry is presented. A sputter deposition system was integrated into the neutron reflectometer AMOR at the Swiss neutron spallation source SINQ, which enables the analysis of the microstructure and magnetic moments during all deposition steps of the Fe layer. We report on the progressive evolution of the accessible parameters describing the microstructure and the magnetic properties of the Fe film, which reproduce known features and extend our knowledge on the behavior of ultrathin iron films.

  11. The behavior of a type-II superconductor Nb in a magnetic field as investigated in polarized-neutron transmission experiments

    International Nuclear Information System (INIS)

    Aksenov, V.L.; Dokukin, E.B.; Kozhevnikov, S.V.; Nikitenko, Yu.V.; Petrenko, A.V.

    1995-01-01

    The type-II superconducting polycrystal Nb was investigated on the SPN-1 polarized-neutron spectrometer at the high-intensity pulsed reactor IBR-2 at Dubna. In polarized-neutron transmission experiments the magnetic-field dependence of the neutron beam polarization was measured. Experiments were performed over a wide magnetic-field range from 0 to H c2 at a temperature of 4.8 K. A quasiperiodic variation of the neutron depolarization as a function of magnetic-field strength was observed. (orig.)

  12. A Precision Measurement of the Neutron Spin Structure Functions Using a Polarized HE-3 Target

    Energy Technology Data Exchange (ETDEWEB)

    Smith, T

    2003-11-05

    This thesis describes a precision measurement of the neutron spin dependent structure function, g{sub 1}{sup n}(x). The measurement was made by the E154 collaboration at SLAC using a longitudinally polarized, 48.3 GeV electron beam, and a {sup 3}He target polarized by spin exchange with optically pumped rubidium. A target polarization as high as 50% was achieved. The elements of the experiment which pertain to the polarized {sup 3}He target will be described in detail in this thesis. To achieve a precision measurement, it has been necessary to minimize the systematic error from the uncertainty in the target parameters. All of the parameters of the target have been carefully measured, and the most important parameters of the target have been measured using multiple techniques. The polarization of the target was measured using nuclear magnetic resonance techniques, and has been calibrated using both proton NMR and by measuring the shift of the Rb Zeeman resonance frequency due to the {sup 3}He polarization. The fraction of events which originated in the {sup 3}He, as measured by the spectrometers, has been determined using a physical model of the target and the spectrometers. It was also measured during the experiment using a variable pressure {sup 3}He reference cell in place of the polarized {sup 3}He target. The spin dependent structure function g{sub 1}{sup n}(z) was measured in the Bjorken x range of 0.014 < x < 0.7 with an average Q{sup 2} of 5 (GeV/c){sup 2}. One of the primary motivations for this experiment was to test the Bjorken sum rule. Because the experiment had smaller statistical errors and a broader kinematic coverage than previous experiments, the behavior of the spin structure function g{sub 1}{sup n}(x) could be studied in detail at low values of the Bjorken scaling variable x. It was found that g{sub 1}{sup n}(x) has a strongly divergent behavior at low values of x, calling into question the methods commonly used to extrapolate the value of g

  13. Novel type of neutron polarization analysis using the multianalyzer-equipment of the three-axes spectrometer PUMA

    Science.gov (United States)

    Schwesig, Steffen; Maity, Avishek; Sobolev, Oleg; Ziegler, Fabian; Eckold, Götz

    2018-01-01

    The combination of polarization analysis and multianalyzer system available at the three axes spectrometer PUMA@FRM II allows the simultaneous determination of both spin states of the scattered neutrons and the absolute value of the polarization. The present paper describes the technical details along with the basic formalism used for the precise calibration. Moreover, the performance of this method is illustrated by several test experiments including first polarized inelastic studies of the magnetic excitations of CuO in the multiferroic and the uniaxial antiferromagnetic phases.

  14. Spin-wave dynamics in Invar Fe65Ni35 studied by small-angle polarized neutron scattering

    NARCIS (Netherlands)

    Brück, E.H.; Grigoriev, S.V.; Deriglazov, V.V.; Okorokov, A.I.; Dijk van, N.H.; Klaasse, J.C.P.

    2002-01-01

    Abstract. Spin dynamics in Fe65Ni35 Invar alloy has been studied by left-right asymmetry of small-angle polarized neutron scattering below TC=485 K in external magnetic fields of H=0.05-0.25 T inclined relative to the incident beam. The spin-wave stiffness D and the damping & were obtained by

  15. Spin disorder in maghemite nanoparticles investigated using polarized neutrons and nuclear resonant scattering

    Science.gov (United States)

    Herlitschke, M.; Disch, S.; Sergueev, I.; Schlage, K.; Wetterskog, E.; Bergström, L.; Hermann, R. P.

    2016-04-01

    The manuscript reports the investigation of spin disorder in maghemite nanoparticles of different shape by a combination of polarized small-angle neutron scattering (SANSPOL) and nuclear forward scattering (NFS) techniques. Both methods are sensitive to magnetization on the nanoscale. SANSPOL allows for investigation of the particle morphology and spatial magnetization distribution and NFS extends this nanoscale information to the atomic scale, namely the orientation of the hyperfine field experienced by the iron nuclei. The studied nanospheres and nanocubes with diameters of 7.4 nm and 10.6 nm, respectively, exhibit a significant spin disorder. This effect leads to a reduction of the magnetization to 44% and 58% of the theoretical maghemite bulk value, observed consistently by both techniques.

  16. Polarized neutron diffraction by D sub 2 chemisorbed on a nickel powder

    Energy Technology Data Exchange (ETDEWEB)

    Beaufils, J.P. (Inst. Laue-Langevin, 38 - Grenoble (France))

    1992-02-01

    The theory of surface differential diffraction (SDD) is extended to the case of polarized neutron diffraction. Nuclear and magnetic surface contributions are thus separated. A method for coherent description of the geometry of the grains is proposed. A saturated D layer chemisorbed on Ni carried by silica is studied with the following results: (111) faces represent the majority of the surface; D atoms sit above the centers of surface Ni triangles with no Ni atom in the underlying layer, the Ni-D distance is equal to 0.215(7) nm; the magnetic-moment modification induced by chemisorption is mainly localized in the surface layer of nickel. Two possible interpretations of the magnetic structure factor are discussed: One assumes no magnetic moment on D atoms but Ni displacements; the other is based on opposite assumptions. (orig.).

  17. Experimental evidence for lamellar magnetism in hemo-ilmenite by polarized neutron scattering

    DEFF Research Database (Denmark)

    Brok, Erik; Sales, Morten; Lefmann, Kim

    2014-01-01

    Large local anomalies in the Earth's magnetic field have been observed in Norway, Sweden, and Canada. These anomalies have been attributed to the unusual magnetic properties of naturally occurring hemo-ilmenite, consisting of a paramagnetic ilmenite host (alpha-Fe2O3-bearing FeTiO3) with exsolution...... lamellae (approximate to 3 μm m thick) of canted antiferromagnetic hematite (FeTiO3-bearing α-Fe2O3) and the mutual exsolutions of the same phases on the micron to nanometer scale. The origin of stable natural remanent magnetization (NRM) in this system has been proposed to be uncompensated magnetic...... moments in the contact layers between the exsolution lamellae. This lamellar magnetism hypothesis is tested here by using polarized neutron diffraction to measure the orientation of hematite spins as a function of an applied magnetic field in a natural single crystal of hemo-ilmenite from South Rogaland...

  18. Laser - Polarized HE-3 Target Used for a Precision Measurement of the Neutron Spin Structure

    Energy Technology Data Exchange (ETDEWEB)

    Romalis, M

    2003-11-05

    This thesis describes a precision measurement of the deep inelastic neutron spin structure function g{sub 1}{sup n}(x). The main motivation for the experiment is a test of the Bjorken sum rule. Because of smaller statistical errors and broader kinematic coverage than in previous experiments, we are able to study in detail the behavior of the spin structure function g{sub 1}{sup n}(x) for low values of the Bjorken scaling variable x. We find that it has a strongly divergent behavior, in contradiction to the naive predictions of the Regge theory. This calls into question the methods commonly used for extrapolation of g{sub 1}{sup n}(x) to x = 0. The difference between the proton and the neutron spin structure functions is less divergent at low x, so a test of the Bjorken sum rule is possible. We confirm the sum rule with an accuracy of 8%. The experiment was performed at SLAC using a 50 GeV polarized electron beam and a polarized {sup 3}He target. In this thesis the polarized target is described in detail. We used the technique of Rb optical pumping and Rb-He spin exchange to polarize the {sup 3}He. Because of a novel mechanical design our target had the smallest dilution ever achieved for a high density gas target. Since this is a precision measurement, particular efforts were made to reduce the systematic errors due to the uncertainty in the target parameters. Most important parameters were measured by more than one method. We implemented novel techniques for measuring the thickness of the glass windows of the target, the {sup 3}He density, and the polarization. In particular, one of the methods for measuring the gas density relied on the broadening of the Rb optical absorption lines by collisions with {sup 3}He atoms. The calibration of this technique resulted in the most precise measurements of the pressure broadening parameters for {sup 3}He as well as several other gases, which are described in an Appendix. The polarization of the {sup 3}He was also measured by

  19. LAP-ND: a new instrument for vector polarization analysis and neutron depolarization measurements at FRJ-2

    Energy Technology Data Exchange (ETDEWEB)

    Ioffe, Alexander; Bussmann, Klaus; Dohmen, Ludwig; Axelrod, Leonid; Gordeev, Gennadi; Brueckel, Thomas

    2004-07-15

    The method of vector analysis of the neutron polarization allows for the determination of both the magnitude and the direction of the magnetization vector in the sample. A directional distribution of the magnetization in a sample results in a spread of the direction of the polarization vector in space and thus in the depolarization of the incident beam. A new neutron depolarization set up is installed at the research reactor FRJ-2 of the Forschungszentrum Juelich. The main feature of the set up is the use of rather long wavelength, {lambda}=(4-6.5) A, neutrons thus allowing for a significant increase in the sensitivity of depolarization measurements. The set up uses a non-cryogenic zero-field sample chamber with the residual magnetic field of about 1 mG. It will be used for the determination of the sample magnetization at mesoscopic and macroscopic levels and for the study of magnetic phase transitions, magnetic nanostructures, magnetic glasses, etc.

  20. Study of magnetic thin films by polarized neutron reflectivity. Off-specular diffusion on periodical structures

    International Nuclear Information System (INIS)

    Ott, F.

    1998-01-01

    Theoretical (Zeeman energy effects) and experimental (beam polarisation problems) progress have been made in the understanding of polarized neutron reflectivity with polarisation analysis. It has been shown that modelization and numerical simulations makes it possible to avoid to have to systematically measure a full set of reflectivity curves for each field and temperature condition. It has been possible to determine a magnetic profile as a function of the field in a magnetic bilayer system by using only a few points in the reciprocal space. This technique allows to considerable reduce the experiment time. In single nickel layer systems, we have shown that it is possible to induce magnetic rotation inhomogeneities when these systems are subjects to deformation strains. The effect are related to magneto-elastic constants gradients. In trilayer systems, with a ME constant modulation, we have been able to induce large magnetic rotation gradients. A new magneto-optic technique to measure the magnetization direction without rotating the magnetic field has been developed. The field of neutron reflectivity has been extended to off-specular studies. It has been possible to account quantitatively of the off-specular diffusion on 2-D model systems (prepared by optical lithography). This new technique should make it possible in the future to determine magnetic structures with a in-depth as well as lateral resolution. (author)

  1. Experimental study of boron-coated straws with a neutron source

    Science.gov (United States)

    Xie, Zhaoyang; Zhou, Jianrong; Song, Yushou; Lacy, Jeffrey L.; Sun, Liang; Sun, Zhijia; Hu, Bitao; Chen, Yuanbo

    2018-04-01

    Multiple types of high quality neutron detectors are proposed for the first phase of the China Spallation Neutron Source (CSNS), which will be commissioned in 2018. Considering the shortage of 3He supply, a detector module composed of 49 boron-coated straws (BCS) was developed by Proportional Technologies Inc. (PTI). Each straw has a length of 1000 mm and a diameter of 7.5 mm. Seven straws are tightly packed in a tube, and seven tubes are organized in a row to form a detector module. The charge division method is used for longitudinal positioning. A specific readout system was utilized to output the signal and simultaneously encode each straw. The performance of this detector module was studied using a moderated 252Cf source at the Institute of High Energy Physics (IHEP). The signal amplitude spectrum indicates its n-gamma discrimination capability. Despite the complex readout method, a longitudinal resolution of FWHM=6.1 ± 0.5 mm was obtained. The three-dimensional positioning ability qualifies this BCS detector module as a promising detector for small angle neutron scattering.

  2. Focusing and polarized neutron ultra-small-angle scattering spectrometer (SANS-J-II) at Research Reactor JRR3, Japan

    International Nuclear Information System (INIS)

    Koizumi, Satoshi; Iwase, Hiroki; Suzuki, Jun-ichi; Oku, Takayuki; Motokawa, Ryuhei; Sasao, Hajime; Tanaka, Hirokazu; Yamaguchi, Daisuke; Shimizu, Hirohiko M.; Hashimoto, Takeji

    2006-01-01

    By employing focusing lenses of sextupole permanent magnet and biconcave MgF 2 crystal, and high-resolution photomultiplier, SANS-J (pinhole small-angle neutron scattering spectrometer at research reactor JRR3, Tokai) was reconstructed to focusing and polarized neutron ultra-small-angle scattering spectrometer (SANS-J-II). Consequently, an accessible minimum wave number q min was improved from 3x10 -3 A -1 to 3x10 -4 A -1 . Furthermore, we added 3 He sub-detectors with an analyzer super mirror at a sample position. With this setup, we perform polarization analysis at high q (>0.2 A -1 ) in order to quantitatively discriminate spin incoherent scattering from hydrogen or to perform spin contrast variation, by a dynamic nuclear polarization method (>0.2 A -1 )

  3. Transparent Si–DLC coatings on metals with high repetition bi-polar pulses of a PBII system

    Energy Technology Data Exchange (ETDEWEB)

    Ikeyama, Masami, E-mail: ikeyama3@aist.go.jp; Sonoda, Tsutomu, E-mail: tsutomu.sonoda@aist.go.jp

    2013-07-15

    Diamond-like carbon (DLC) is widely used because of its good properties. However, the color of DLC is usually dark brown or black. Recently, we have made fairly transparent Si contained DLC (Si–DLC) coatings in visible light region. The fairly transparent Si–DLC was made by using our original bi-polar pulse type plasma based ion implantation (PBII) system, with recently introduced high slew rate pulse power supply. The colors of metal sample surface were uniformly changed as subdued red, yellow, subdued green and subdued blue or violet, with the change of Si–DLC coating’s thickness. The colors come from the interference between reflected lights at the surface of the Si–DLC coatings and the surface of the metal samples. The colors were also changed with the angle of glancing. Estimated refractive indexes show well agreements among almost all Si–DLC coatings, instead of the differences of coating conditions. Generally, the longer coating time or slower coating process makes the higher refractive index in near infrared region. Estimated band gap of a Si–DLC coating was about 1.5 eV. The developed Si–DLC coatings must be useful as not only protective but also decorative coatings.

  4. T-odd angular correlations in the emission of prompt gamma rays and neutrons in nuclear fission induced by polarized neutrons

    Science.gov (United States)

    Danilyan, G. V.; Klenke, J.; Krakhotin, V. A.; Kopach, Yu. N.; Novitsky, V. V.; Pavlov, V. S.; Shatalov, P. B.

    2011-05-01

    Study of the T-odd three-vector correlation in the emission of prompt neutrons from 235U fission by polarized cold neutrons has been continued at the facility MEPHISTO of the FRM II reactor (Technical University of Munich). The sought correlation was not found within experimental error of 2.3 × 10-5. The upper limit for the asymmetry coefficient has been set to | D n | fission correlation coefficient D α = (170±20) × 10-5. This limit casts doubt on a model that explains the three-vector correlation in ternary fission by the Coriolis mechanism. At the same time, five-vector correlation in the emission of prompt fission neutrons has been measured, which describes the rotation of the fissioning nucleus at the moment it breaks (ROT effect). At the angle 22.5° to the fission axis, the correlation coefficient was found to be (1.57 ± 0.20) × 10-4, while at the angle of 67.5° it is zero within the experimental uncertainty. The existence of ROT effect in the emission of prompt fission neutrons can be explained by the anisotropy of neutron emission in the rest frame of the fragment (fission fragments are aligned with respect to the axis of deformation of the fissioning nucleus), similar to the mechanism of ROT effect in the emission of prompt γ-rays.

  5. Polarized-neutron-scattering study of the spin-wave excitations in the 3-k ordered phase of uranium antimonide.

    Science.gov (United States)

    Magnani, N; Caciuffo, R; Lander, G H; Hiess, A; Regnault, L-P

    2010-03-24

    The anisotropy of magnetic fluctuations propagating along the [1 1 0] direction in the ordered phase of uranium antimonide has been studied using polarized inelastic neutron scattering. The observed polarization behavior of the spin waves is a natural consequence of the longitudinal 3-k magnetic structure; together with recent results on the 3-k-transverse uranium dioxide, these findings establish this technique as an important tool to study complex magnetic arrangements. Selected details of the magnon excitation spectra of USb have also been reinvestigated, indicating the need to revise the currently accepted theoretical picture for this material.

  6. First measurement of the electric formfactor of the neutron in the exclusive quasielastic scattering of polarized electrons from polarized 3He

    International Nuclear Information System (INIS)

    Meyerhoff, M.; Eyl, D.; Frey, A.; Andresen, H.G.; Annand, J.R.M.; Aulenbacher, K.; Becker, J.; Blume-Werry, J.; Dombo, T.; Drescher, P.; Ducret, J.E.; Fischer, H.; Grabmayr, P.; Hall, S.; Hartmann, P.; Hehl, T.; Heil, W.; Hoffmann, J.; Kellie, J.D.; Klein, F.; Leduc, M.; Moeller, H.; Nachtigall, C.; Ostrick, M.; Otten, E.W.; Owens, R.O.; Pluetzer, S.; Reichert, E.; Rohe, D.; Schaefer, M.; Schearer, L.D.; Schmieden, H.; Steffens, K.; Surkau, R.; Walcher, T.

    1995-01-01

    A first measurement of the asymmetry in quasielastic scattering of longitudinally polarized electrons from a polarized 3 He gas target in coincidence with the knocked out neutron is reported. This measurement was made feasible by the cw beam of the 855 meV Mainz Microtron MAMI. It allows a determination of the electric formfactor of the neutron G n E independent of binding effects to first order. At bar Q 2 =0.31 (GeV/c) 2 two asymmetries bar A parallel (rvec S He parallel rvec q) and bar A perpendicular (rvec S He perpendicular rvec q) have been measured giving bar A parallel =(-7.40±0.73%) and bar A perpendicular =(0.89±0.30)%. The ratio bar A perpendicular /bar A parallel is independent of the absolute value of the electron and target polarization and yields G n E =0.035±0.012±0.005. copyright 1995 American Institute of Physics

  7. Observation of a reorientation of the holmium moments in HoAl2 with polarized neutron diffraction

    International Nuclear Information System (INIS)

    Barbara, B.; Boucherle, J.X.; Rossignol, M.F.; Schweizer, J.

    1976-01-01

    Magnetization measurements performed on a single crystal of HoAl 2 show that the easy axis of magnetization is [110] at low temperature and suggest near 20 0 K a rotation of the easy direction of magnetization. This rotation has been strikingly demonstrated by polarized neutron diffraction experiments including measurements of intensities with both spin states and of depolarization through the sample. This result allows the interpretation of the magnetic properties of HoAl 2 in terms of crystal field

  8. Search for the existence of circulating currents in high-Tc superconductors using the polarized neutron scattering technique

    International Nuclear Information System (INIS)

    Sidis, Y.; Fauque, B.; Aji, V.; Bourges, P.

    2007-01-01

    We review experimental attempts using polarized neutron scattering technique to reveal the existence in high temperature superconductors of a long-range ordered state characterized by the spontaneous appearance of current loops. We draw particular attention to our recent results (B. Fauque et al., Phys. Rev. Lett. 96 (2006) 197001) that, up to now, can be explained only by the theory of circulating currents proposed by Varma

  9. A polarized neutron study of the magnetization distribution in Co2FeSi

    International Nuclear Information System (INIS)

    Brown, P J; Kainuma, R; Kanomata, T; Okubo, A; Neumann, K-U; Umetsu, R Y; Ziebeck, K R A

    2013-01-01

    The magnetization distribution in Co 2 FeSi which has the largest moment per formula unit ∼6 μ B of all Heusler alloys, has been determined using polarized neutron diffraction. The experimentally determined magnetization has been integrated over spheres centred on the three sites of the L1 2 structure giving μ Fe = 3.10(3) μ B and μ Co = 1.43(2) μ B , results which are slightly lower than the moments in atomic spheres of similar radii obtained in recent LDA + U band structure calculations (Li et al 2010 Chin. Phys. B 19 097102). Approximately 50% of the magnetic carriers at the Fe sites were found to be in orbitals with e g symmetry. This was higher, ≃65%, at the Co sites. Both Fe and Co were found to have orbital moments that are larger than those predicted. Comparison with similar results obtained for related alloys suggests that there must be a finite density of states in both spin bands at the Fermi energy indicating that Co 2 FeSi is not a perfect half-metallic ferromagnet. (paper)

  10. Polarized small angle neutron scattering of MnO/Mn3O4 nanocrystals

    Science.gov (United States)

    Dedon, L.; Ijiri, Y.; Booth, R.; Krycka, K.; Borchers, J. A.; Chen, W. C.; Watson, S.; Rhyne, J. J.; Majetich, S. A.

    2012-02-01

    Monodisperse magnetic nanoparticles are of great interest for biomedical and data storage applications, particularly in cases where the core and shell can be carefully controlled to alter properties like magnetic anisotropy. However, it is often difficult to determine the underlying moment arrangements and correlations in these systems. Here, we focus on manganese (II) oxide/manganese (II,III) oxide core/shell nanoparticles, using polarized small angle neutron scattering (SANS) to probe the magnetic intra and interparticle interactions. The 30nm diameter particles with 4-5nm shell were prepared by solution chemistry methods and self-assembled into 3D nanocrystals. SANS measurements were conducted in magnetic fields from remanence-1T and temperatures from 10-300K. Magnetic and structural scattering components were separated using an algorithm previously described in [1]. The magnetic signature depended on the field and temperature history of the sample. Modeling work has been done to further quantify the interparticle length scales and the effects of crystal packing. This work was supported in part by NSF grants DMR-0454672, -0704178, -0804779, -1104489, and DOE grant DE-FG02-08ER40481. [1] K.L. Krycka, et al. Phys. Rev. Lett. 104, 207203 (2010).

  11. Low moment ferrimagnetism in Mn3Al as probed by Polarized Neutron Reflectometry

    Science.gov (United States)

    Jamer, Michelle; Wang, Yung-Jui; Borchers, Julie; Kirby, Brian; Barbiellini, Bernardo; Bansil, Arun; Heiman, Don

    For future spintronic devices, it is paramount to limit stray magnetic interactions which can negatively impact spin injection. A new class of materials called half-metallic antiferromagnets or compensated ferrimagnets have been proposed to remedy this problem. In this work, Mn3Al thin films have shown promising room temperature low-moment ferrimagnetic magnetic properties. Epitaxial Mn3Al thin films (50 nm) were grown on desorbed GaAs(001) substrates via MBE at 200 °C and annealed further to temperatures between 250 - 350 °C. The D03 Heusler-type phase was determined by X-ray diffraction with texturing in the [311] direction. Density functional theory, performed using VASP, indicated that the crystallographic structure of Mn3Al is able to form energetically with a low magnetic moment (0.017 μB/f.u.) despite some epitaxial distortion. SQUID magnetometry confirmed the low magnetic moment and high Curie temperature (610 K) of the structure. Polarized Neutron Reflectometry was used to determine the effect of epitaxy on the magnetic moment of Mn3Al, and analysis confirms a low magnetic moment (0.11 μB/f.u.) for the samples annealed at temperatures between 200-300 °C. This analysis further suggests that the relaxation of the Mn3Al at the interface. National Science Foundation ECCS-1402738.

  12. Test of parity-conserving time-reversal invariance using polarized neutrons and nuclear spin aligned holmium

    International Nuclear Information System (INIS)

    Huffman, P.R.; Roberson, N.R.; Wilburn, W.S.; Gould, C.R.; Haase, D.G.; Keith, C.D.; Raichle, B.W.; Seely, M.L.; Walston, J.R.

    1997-01-01

    A test of parity-conserving, time-reversal noninvariance (PC TRNI) has been performed in 5.9 MeV polarized neutron transmission through nuclear spin aligned holmium. The experiment searches for the T-violating fivefold correlation via a double modulation technique emdash flipping the neutron spin while rotating the alignment axis of the holmium. Relative cross sections for spin-up and spin-down neutrons are found to be equal to within 1.2x10 -5 (80% confidence). This is a two orders of magnitude improvement compared to traditional detailed balance studies of time reversal, and represents the most precise test of PC TRNI in a dynamical process, to our knowledge. copyright 1997 The American Physical Society

  13. Deep UV to NIR Space Telescopes and Exoplanet Coronagraphs: A Trade Study on Throughput, Polarization, Mirror Coating Options and Requirements

    Science.gov (United States)

    Balasubramanian, Kunjithapatham; Shaklan, Stuart; Give'on, Amir; Cady, Eric; Marchen, Luis

    2011-01-01

    The NASA Exoplanet program and the Cosmic Origins program are exploring technical options to combine the visible to NIR performance requirements of a space coronagraph with the general astrophysics requirements of a space telescope covering the deep UV spectrum. Are there compatible options in terms of mirror coatings and telescope architecture to satisfy both goals? In this paper, we address some of the main concerns, particularly relating to polarization in the visible and throughput in the UV. Telescope architectures employing different coating options compatible with current technology are considered in this trade study.

  14. Optimal design and fabrication method for antireflection coatings for P-polarized 193 nm laser beam at large angles of incidence (68°-74°).

    Science.gov (United States)

    Jin, Jingcheng; Jin, Chunshui; Li, Chun; Deng, Wenyuan; Chang, Yanhe

    2013-09-01

    Most of the optical axes in modern systems are bent for optomechanical considerations. Antireflection (AR) coatings for polarized light at oblique incidence are widely used in optical surfaces like prisms or multiform lenses to suppress undesirable reflections. The optimal design and fabrication method for AR coatings with large-angle range (68°-74°) for a P-polarized 193 nm laser beam is discussed in detail. Experimental results showed that after coating, the reflection loss of a P-polarized laser beam at large angles of incidence on the optical surfaces is reduced dramatically, which could greatly improve the output efficiency of the optical components in the deep ultraviolet vacuum range.

  15. Quantifying "Softness" of Organic Coatings on Gold Nanoparticles Using Correlated Small-Angle X-ray and Neutron Scattering.

    Science.gov (United States)

    Diroll, Benjamin T; Weigandt, Katie M; Jishkariani, Davit; Cargnello, Matteo; Murphy, Ryan J; Hough, Lawrence A; Murray, Christopher B; Donnio, Bertrand

    2015-12-09

    Small-angle X-ray and neutron scattering provide powerful tools to selectively characterize the inorganic and organic components of hybrid nanomaterials. Using hydrophobic gold nanoparticles coated with several commercial and dendritic thiols, the size of the organic layer on the gold particles is shown to increase from 1.2 to 4.1 nm. A comparison between solid-state diffraction from self-assembled lattices of nanoparticles and the solution data from neutron scattering suggests that engineering softness/deformability in nanoparticle coatings is less straightforward than simply increasing the organic size. The "dendritic effect" in which higher generations yield increasingly compact molecules explains changes in the deformability of organic ligand shells.

  16. Development and optimisation of a ultracold neutron polarizing system in the framework of a new measurement of the neutron electric dipole moment

    International Nuclear Information System (INIS)

    Pierre, Edgard

    2012-01-01

    The work presented in this thesis has been performed within the framework of an experiment located at the Paul Scherrer Institut (PSI) and dedicated to the measurement of the neutron electric dipole moment (nEDM). The expected sensitivity is 10 -27 e cm at the end of 2013. The experiment requires a polarized ultracold neutron (UCN) beam. A new polarizing system, a spin transport device and a spin reversal system have been developed for this purpose. Their study is detailed in this thesis. These systems are currently installed on the experiment. Thanks to magnetic field mappings done on the spectrometer, to magnetic field simulations using the Radia and Maentouch programs and also to Monte-Carlo simulations using the Geant4 software, the efficiency of the device has been calculated. The measured efficiency is 88.5±0.3%, which is slightly less than the expected value of 95%. Furthermore, this preliminary data taken in October 2011 allows the determination of some fundamental parameters of the experiment such as the filling, storage and longitudinal depolarization time constants of the spectrometer. These parameters are promising for the continuation of the experiment. (author) [fr

  17. Polarized neutron source and detectors for the TUNL parity-even test of time reversal invariance

    International Nuclear Information System (INIS)

    Huffman, P.R.; Roberson, N.R.; Wilburn, W.S.

    1995-01-01

    The development and implementation of a 10 MHz neutron production target and detector system are presented. The system has been used in a test of parity-even time reversal invariance in neutron transmission through an aligned target. Neutrons were produced via the D(d,n) 3 He reaction using a liquid nitrogen cooled deuterium gas cell. The cryogenic cell required temperature stabilization for minimization of systematic effects. Two four-detector arrays of neutron detectors were developed for 0 degrees transmission measurements and flux monitoring. The system allowed transmission asymmetries to be measured to accuracies better than 10 -6 in a parity-conserving test of time reversal invariance

  18. High-Efficiency Thin-Film-Coated Semiconductor Neutron Detectors for Active Dosimetry Monitors

    International Nuclear Information System (INIS)

    Dunn, William L.; McGregor, Douglas

    2009-01-01

    To develop a compact high-detection-efficiency neutron dosimeter capable of discerning between thermal and fast neutron doses in real time. A need exists for portable neutron dosimeters that have greater than 10% thermal neutron detection efficiency and can provide direct readout in the field. To be of widespread use, these dosimeters should have low power requirements. It would be ideal if these dosimeters could differentiate thermal from fast neutrons, as this would allow characterization (at least to some degree) of the source of those neutrons. Such neutron dosimeters could be used either as personnel dosimeters or in area survey instruments. The project has been completed and the objectives of the project were met. Prototype perforated semiconductor neutron detectors have been developed and characterized. Individual detectors have been packaged in small, rugged, battery-powered containers that can be worn as active dosimeters and read in real time. Two prototype neutron dosimeters were constructed and tested.

  19. Polarized neutron tomography of Ni{sub 3}Al and Fe{sub 2}TiSn

    Energy Technology Data Exchange (ETDEWEB)

    Neubauer, Andreas; Schulz, Michael; Pfleiderer, Christian; Boeni, Peter [Physik Department E21, Technische Universitaet Muenchen, Garching (Germany); Koehler, Anke; Wizent, Nadja; Behr, Guenther [Leibniz-Institut fuer Festkoerper- und Werkstoffforschung Dresden (Germany)

    2009-07-01

    The transition metal compounds Ni{sub 3}Al and Fe{sub 2}TiSn are weakly ferromagnetic metals, for which the magnetic properties are extremely sensitive to composition. We have attempted the growth of polycrystalline and single-crystal rods of these compounds with an UHV compatible image furnace. The polycrystalline starting material as well as the floating-zoned rods have been characterized by means of conventional bulk properties and EDX. As a new method we have additionally carried out polarized neutron tomography. The depolarization of the neutron beam proves to be extremely sensitive to tiny variations of the ferromagnetic transition temperature, thus providing key information on the metallurgical phase diagram and the ideal growth conditions. The possible implications of our observations for the nature of quantum criticality in these compounds are discussed.

  20. Optical coating on a corrugated surface to align the polarization of an unpolarized wave without loss

    Science.gov (United States)

    Jen, Yi Jun

    2017-12-01

    A multilayer comprising birefringent thin films is devised to present to function as a polarization beam splitter and waveplate simultaneously. By arranging such a multilayer on a right triangle-shaped corrugated surface, a polarizer is realized to align the randomly oscillating electric field of an unpolarized wave into a linear polarized wave without loss.

  1. Application of neutron activation analysis to the corrosion study of gold coated studs used for piercing ears

    International Nuclear Information System (INIS)

    Saiki, M.; Rogero, S.O.; Costa, I.; Correa, O.V.; Higa, O.Z.

    1998-01-01

    Complete text of publication follows. Gold is known as a metal having little or no toxicity and it has been widely used for coating studs for ear piercing. However, for some people gold coated studs have caused serious allergy and inflammation problems. After piercing, the studs are usually kept in the ear lobes for at least one week, and during this period the stud surfaces in contact with the body fluids have caused swelling, pain and redness of the skin. Consequently, it is of great interest to evaluate if elements from the metallic substrate underneath the gold coatings migrate to the body fluids due to the corrosion and the presence of defects in gold coatings. The solutions for corrosion test were obtained by placing the gold coated studs in contact with the solutions of NaCl and of culture medium. Elemental analyses of these solutions by radioanalytical method of neutron activation analysis indicated the occurrence of substrate corrosion since the elements Cr, Fe, Ni and Zn were found in these solutions. These elements are substrate material components of alloys used to make the studs and they were quantified by X-ray fluorescence analysis. The defects of the coatings were also detected by scanning electron microscopy and energy dispersive spectroscopy analysis of the gold coated studs before and after the corrosion tests. Cytotoxicity studies indicated that after corrosion test the solution used was toxic in the culture cell assay. Among the elements quantified in the test solutions, Ni is considered responsible for most of allergic reactions. Results obtained in this work indicated the necessity to improve quality control of the coating process of studs and in the appropriate choice of material used as substrate

  2. Polarized triple-axis spectrometer TASP

    Energy Technology Data Exchange (ETDEWEB)

    Boeni, P.; Keller, P. [Lab. for Neutron Scattering ETH Zurich, Zurich (Switzerland) and Paul Scherrer Institute, Villigen (Switzerland)

    1996-11-01

    The polarized triple-axis spectrometer TASP at SINQ has been optimized for measuring magnetic cross sections in condensed matter. The neutrons are polarized or analyzed either by means of benders or Heusler monochromators. The beam divergence, i.e. the intensity, and the spectral range of the neutrons is rather large because of the supermirror coatings of the feeding neutron guide. The intensity can be further increased at the sample position by means of a focussing monochromator and a focussing anti-trumpet. The end position of TASP allows the tailoring of the neutron beam already before the monochromator and to scatter neutrons over very wide ranges of angles. (author) 6 figs., 1 tab., 8 refs.

  3. Polarized triple-axis spectrometer TASP

    International Nuclear Information System (INIS)

    Boeni, P.; Keller, P.

    1996-01-01

    The polarized triple-axis spectrometer TASP at SINQ has been optimized for measuring magnetic cross sections in condensed matter. The neutrons are polarized or analyzed either by means of benders or Heusler monochromators. The beam divergence, i.e. the intensity, and the spectral range of the neutrons is rather large because of the supermirror coatings of the feeding neutron guide. The intensity can be further increased at the sample position by means of a focussing monochromator and a focussing anti-trumpet. The end position of TASP allows the tailoring of the neutron beam already before the monochromator and to scatter neutrons over very wide ranges of angles. (author) 6 figs., 1 tab., 8 refs

  4. Residual-Charge Induced Memory Effect of Electric Polarization in Multiferroic CuFe1-xGaxO2 as Seen via Polarized Neutron Diffraction

    Science.gov (United States)

    Nakajima, Taro; Mitsuda, Setsuo; Yamazaki, Hiroe; Matsuura, Masato

    2013-02-01

    We have investigated ferroelectric polarization memory effect in a magneto-electric (ME) multiferroic CuFe1-x GaxO2 (CFGO) with x=0.035, which exhibits a spin-driven ferroelectric phase below TC˜ 7 K in zero magnetic field. In a previous study on CFGO(x=0.035), we have reported that the ferroelectric polarization induced by an applied electric field is retrieved after heating the sample to a non-ferroelectric high-temperature phase and then cooling down to the ferroelectric phase without electric field. [Mitsuda et al. Physica B 404 (2009) 2532] By measuring thermally stimulated electric current in detail, the previous study has elucidated that residual charges trapped in the sample are relevant to the memory effect. In the present study, we have performed polarized neutron diffraction measurements on CFGO(x=0.035) with applied electric fields, in order to investigate the multiferroic domain structure, which can reflect spatial distribution of internal electric fields due to the trapped charges. The present results have shown that the effect of the internal electric fields is significantly different from that of the ``uniform'' electric field applied on the first cooling. To explain the present results, we suggest a model that the residual charges are trapped on boundaries between the three types of magnetic domains originating from the trigonal symmetry of the crystal, implying that the presence of the bound charges of the ferroelectric polarization on the domain boundaries is a key to the memory effect in this system.

  5. Spin observables in charged pion photo-production from polarized neutrons in solid HD at Jefferson Lab

    Energy Technology Data Exchange (ETDEWEB)

    Kageya, Tsuneo [Thomas Jefferson National Accelerator Facility (TJNAF), Newport News, VA (United States); Ho, Dao [Carnegie Mellon Univ., Pittsburgh, PA (United States); Peng, Peng [Univ. of Virginia, Charlottesville, VA (United States); Klein, Franz [George Washington Univ., Washington, DC (United States); Sandorfi, Andrew M. [Thomas Jefferson National Accelerator Facility (TJNAF), Newport News, VA (United States); Schumacher, Reinhard A. [Carnegie Mellon Univ., Pittsburgh, PA (United States)

    2018-04-01

    E asymmetries have been extracted from double-polarizationexperiments in Hall-B of the Thomas Jefferson National Accelerator Facility (JLab). Results have been obtained from the E06-101 (g14) experiment, using circularly polarized photon beams, longitudinally polarized Deuterons in solid HD targets, and the CEBAF Large Acceptance Spectrometer (CLAS). The results cover a range inW from 1.48 to 2.32 GeV. Three independent analyses, using distinctly different methods, have been combined to obtain the final values, which have been published recently. Partial wave analyses (PWA), which have had to rely on a sparse neutron data base, havebeen significantly changed with the inclusion of these g14 asymmetries.

  6. The use of neutron diffraction for the determination of the in-depth residual stresses profile in weld coatings

    International Nuclear Information System (INIS)

    Marques, Maria Jose; Batista, A.C.; Nobre, J.P.; Loureiro, Altino; Kornmeier, Joana R.

    2013-01-01

    The neutron diffraction is a non-destructive technique, particularly suitable for the analysis of residual stress fields in welds. The technique is used in this article to study ferritic samples, coated by submerged arc welding using stainless steel filler metals. This procedure is often used for manufacturing process equipment for chemical and nuclear industries, for ease of implementation and economic reasons. The main disadvantage of that processes is the cracking phenomenon that often occurs at the interface between the base material and coatings, which can be minimized by performing post-weld stress relief heat treatments. The samples analyzed in this study were made of carbon steel plates, coated by submerged arc welding two types of stainless steel filler metals. For the first layer was used one EN 12 072 - S 2 U 23 12 electrode, while for the second and third layers were used an EN 12 072 - 19 12 3 S L electrode. After cladding, the samples were submitted to a post-weld heat treatment for 1 hour at 620 deg C. The residual stress profiles obtained by neutron diffraction evidence the relaxation of residual stress given by the heat treatment. (author)

  7. Polarization-dependent transverse-stress sensing based on photonic crystal fiber with gold-coated air-holes

    Science.gov (United States)

    Liu, Hai; Zhu, Chenghao; Wang, Yan; Tan, Ce; Li, Hongwei; Cheng, Deqiang

    2017-05-01

    A transverse-stress sensor with polarization filtering function based on a specially designed photonic crystal fiber (PCF) is proposed. Four ultralarge side-holes are introduced into the cladding layer, and two of them are gold-coated to enhance the stress sensitivity. The finite element method is applied to study the polarization-dependent wavelength-selective sensing characteristics at the optical communication wavelength. Results reveal that the sensor can achieve a high sensitivity in either direction that can be divided into an x-direction component and a y-direction component. Combining the advantages of side-hole structure and surface plasmon resonance technology, the proposed sensor is believed to be an excellent candidate for the transverse-stress measurement.

  8. Setup for polarized neutron imaging using in situ3He cells at the Oak Ridge National Laboratory High Flux Isotope Reactor CG-1D beamline.

    Science.gov (United States)

    Dhiman, I; Ziesche, Ralf; Wang, Tianhao; Bilheux, Hassina; Santodonato, Lou; Tong, X; Jiang, C Y; Manke, Ingo; Treimer, Wolfgang; Chatterji, Tapan; Kardjilov, Nikolay

    2017-09-01

    In the present study, we report a new setup for polarized neutron imaging at the ORNL High Flux Isotope Reactor CG-1D beamline using an in situ 3 He polarizer and analyzer. This development is very important for extending the capabilities of the imaging instrument at ORNL providing a polarized beam with a large field-of-view, which can be further used in combination with optical devices like Wolter optics, focusing guides, or other lenses for the development of microscope arrangement. Such a setup can be of advantage for the existing and future imaging beamlines at the pulsed neutron sources. The first proof-of-concept experiment is performed to study the ferromagnetic phase transition in the Fe 3 Pt sample. We also demonstrate that the polychromatic neutron beam in combination with in situ 3 He cells can be used as the initial step for the rapid measurement and qualitative analysis of radiographs.

  9. Setup for polarized neutron imaging using in situ 3He cells at the Oak Ridge National Laboratory High Flux Isotope Reactor CG-1D beamline

    Science.gov (United States)

    Dhiman, I.; Ziesche, Ralf; Wang, Tianhao; Bilheux, Hassina; Santodonato, Lou; Tong, X.; Jiang, C. Y.; Manke, Ingo; Treimer, Wolfgang; Chatterji, Tapan; Kardjilov, Nikolay

    2017-09-01

    In the present study, we report a new setup for polarized neutron imaging at the ORNL High Flux Isotope Reactor CG-1D beamline using an in situ 3He polarizer and analyzer. This development is very important for extending the capabilities of the imaging instrument at ORNL providing a polarized beam with a large field-of-view, which can be further used in combination with optical devices like Wolter optics, focusing guides, or other lenses for the development of microscope arrangement. Such a setup can be of advantage for the existing and future imaging beamlines at the pulsed neutron sources. The first proof-of-concept experiment is performed to study the ferromagnetic phase transition in the Fe3Pt sample. We also demonstrate that the polychromatic neutron beam in combination with in situ 3He cells can be used as the initial step for the rapid measurement and qualitative analysis of radiographs.

  10. Interfacial mixing in as-deposited Si/Ni/Si layers analyzed by x-ray and polarized neutron reflectometry

    Energy Technology Data Exchange (ETDEWEB)

    Bhattacharya, Debarati, E-mail: debarati@barc.gov.in [Solid State Physics Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400085 (India); Basu, Saibal; Singh, Surendra [Solid State Physics Division, Bhabha Atomic Research Centre, Trombay, Mumbai 400085 (India); Roy, Sumalay; Dev, Bhupendra Nath [Department of Materials Science, Indian Association for the Cultivation of Science, 2A and 2B Raja S.C. Mullick Road, Jadavpur, Kolkata 700032 (India)

    2012-12-15

    Highlights: Black-Right-Pointing-Pointer Room temperature diffusion in Si/Ni/Si trilayer detected through complementary x-ray and polarized neutron reflectometry. Black-Right-Pointing-Pointer Analyses of XPNR data generated the construction of the layered structure in terms of physical parameters along with alloy layers created by diffusion. Black-Right-Pointing-Pointer Scattering length density information from XPNR provided quantitative assessment of the stoichiometry of alloys formed at the Si/Ni and Ni/Si interfaces. - Abstract: Interdiffusion occurring across the interfaces in a Si/Ni/Si layered system during deposition at room temperature was probed using x-ray reflectivity (XRR) and polarized neutron reflectivity (PNR). Exploiting the complementarity of these techniques, both structural and magnetic characterization with nanometer depth resolution could be achieved. Suitable model fitting of the reflectivity profiles identified the formation of Ni-Si mixed alloy layers at the Si/Ni and Ni/Si interfaces. The physical parameters of the layered structure, including quantitative assessment of the stoichiometry of interfacial alloys, were obtained from the analyses of XRR and PNR patterns. In addition, PNR provided magnetic moment density profile as a function of depth in the stratified medium.

  11. Reconciling the MOLA, TES, and Neutron Observations of the North Polar CO2 Mass Budget on Mars

    Science.gov (United States)

    Haberle, R. M.; Mattingly, B.; Titus, T. N.

    2003-01-01

    There are now three independent observations of the CO2 polar cap mass budget of Mars' north polar cap. The first is based elevation changes detected by the Mars Orbiter Laser Altimeter (MOLA) on the Mars Global Surveyor (MGS). The second is based on MGS Thermal Emission Spectrometer (TES) broadband observations of the solar and infrared radiation fields at the top of the atmosphere. The third is based on neutron counts measured by the neutron spectrometer (NS) on Odyssey. The TES data are based on an energy balance. The net radiative loss (gain) in a column is balanced by latent heating due condensation (sublimation) of CO2. In calculating the mass budget, the other main energy sources, atmospheric heat transport and subsurface conduction, were neglected. At the pole, atmospheric heat transport is indeed a small term. However, subsurface heat conduction can be significant because at the North Pole water ice, which has a high thermal conductivity compared to bare soil, is a dominant component of the subsurface. Thus, heat conducted down into the ice during summer will slowly bleed back out during fall and winter reducing the amount of CO2 that condenses on the pole. We have taken a first cut at quantifying this effect by fitting a curve to Paige's estimates of the conducted energy flux in his analysis of Viking IRTM data.

  12. Interstitial Iron Effects on Magnetic Excitations in Parent Phases Fe1+xTe from Polarized and Inelastic Neutron Scattering

    Science.gov (United States)

    Rodriguez, Efrain

    2012-02-01

    One of the simplest systems of the iron-based superconducting family, Fe1+xCh (where Ch = S, Se, or Te) presents ample opportunity to study the relationship between antiferromagnetism and superconductivity. Several studies have demonstrated how the makeup of the Ch anions changes the electronic properties drastically, but the effect of excess interstitial iron, the x in Fe1+xCh, is not as well understood. Our previous diffraction experiments on samples varying x from 4 % to 16 % demonstrated how the magnetic ordering changes from collinear antiferromagnetic to helical incommensurate via a spin-density wave state at the special composition of x 12%. We present inelastic neutron scattering measurements of the phases Fe1+xTe for two amounts of interstitial iron in the lattice, 5% and 14 %. We have combined data from cold neutron triple-axis, thermal neutron triple-axis, and spallation source time-of-flight to provide a full picture of the magnetic excitations in Fe1+xTe for x=14 % from 0.5 meV to 150 meV. In addition, we present polarized inelastic studies on this particular composition to investigate the nature of the spin waves, i.e. longitudinal vs. transverse. The results are compared with those found in the phase with low amounts of interstitial iron ( 5 %), in order to understand the nature of the exchange interactions in this important parent compound.

  13. First spin-resolved electron distributions in crystals from combined polarized neutron and X-ray diffraction experiments

    Directory of Open Access Journals (Sweden)

    Maxime Deutsch

    2014-05-01

    Full Text Available Since the 1980s it has been possible to probe crystallized matter, thanks to X-ray or neutron scattering techniques, to obtain an accurate charge density or spin distribution at the atomic scale. Despite the description of the same physical quantity (electron density and tremendous development of sources, detectors, data treatment software etc., these different techniques evolved separately with one model per experiment. However, a breakthrough was recently made by the development of a common model in order to combine information coming from all these different experiments. Here we report the first experimental determination of spin-resolved electron density obtained by a combined treatment of X-ray, neutron and polarized neutron diffraction data. These experimental spin up and spin down densities compare very well with density functional theory (DFT calculations and also confirm a theoretical prediction made in 1985 which claims that majority spin electrons should have a more contracted distribution around the nucleus than minority spin electrons. Topological analysis of the resulting experimental spin-resolved electron density is also briefly discussed.

  14. Polarized neutron study of the magnetic mesostructure in (Pd{sub 1-x}Fe{sub x}){sub 1-y}Mn{sub y}

    Energy Technology Data Exchange (ETDEWEB)

    Gordeev, G.P.; Axelrod, L.A.; Lazebnik, I.M.; Zabenkin, V.N. [Petersburg Nuclear Physics Institute, 188300, Gatchina (Russian Federation); Wagner, V. [Physikalisch-Technische Bundesanstalt, 38116, Braunschweig (Germany)

    2002-07-01

    In PdFeMn alloys with different Fe-atom concentrations, the behaviour of both mean magnetization and neutron depolarization in the magnetization/demagnetization process was observed by three-dimensional analysis of neutron-beam polarization. Both magnetization and depolarization have a hysteresis loop for the same values of an applied field. Depolarization loops are sharply distinguished for different alloys. This gives evidence of different magnetic mesostructures in these alloys. (orig.)

  15. Polarized neutron study of the magnetic mesostructure in (Pd sub 1 sub - sub x Fe sub x) sub 1 sub - sub y Mn sub y

    CERN Document Server

    Gordeev, G P; Lazebnik, I M; Zabenkin, V N; Wagner, V

    2002-01-01

    In PdFeMn alloys with different Fe-atom concentrations, the behaviour of both mean magnetization and neutron depolarization in the magnetization/demagnetization process was observed by three-dimensional analysis of neutron-beam polarization. Both magnetization and depolarization have a hysteresis loop for the same values of an applied field. Depolarization loops are sharply distinguished for different alloys. This gives evidence of different magnetic mesostructures in these alloys. (orig.)

  16. Design and construction of a 10B coated ion chamber for the measurement of a thermal neutron flux

    International Nuclear Information System (INIS)

    Vite T, M.

    1979-01-01

    A model of an ionization chamber cover with 10 B, for the measurement of thermal neutron flux is presented, the developed chamber is made of a cylindrical vessel in which interior exist 7 aluminium electrodes which by electrodeposition were covered with a coat of 10 B with a thickness of 0.68 mg/cm 2 . Once the chamber is filled with N 2 to a pressure of 1.33 atm., it was exposed to a flux of thermal neutrons at the order 10 4 n/cm 2 -seg obtaining an ionization current of 10 -11 amp. which can be easily distinguished from the leak current which order is of 10 -12 amp. The conventional electronics associated to the chamber allows to process the ionization current in pulse form. The relation of noise to signal is approximately of 8, for which the pulses can be differentiated from the electronic noise without any problem. (author)

  17. Transverse electron polarization in the neutron decay - Direct search for scalar and tensor couplings in weak interaction

    Science.gov (United States)

    Bodek, Kazimierz

    2012-09-01

    The Standard Model (SM) predictions of T-violation for weak decays of systems built up of u and d quarks are by 7 to 10 orders of magnitude lower than the experimental accuracies attainable at present. It is a general presumption that time reversal phenomena are caused by a tiny admixture of exotic interaction terms. Therefore, weak decays provide a favorable testing ground in a search for such feeble forces. Physics with very slow, polarized neutrons has a great potential in this respect. An experiment seeking for small deviations from the SM in two observables, N and R, that are for the first time addressed experimentally in free neutron decay and that are exclusively sensitive to real and imaginary parts of the same linear combination of the scalar and tensor interaction coupling constants has been completed at the Paul Scherrer Institute, Villigen, Switzerland. The analysis of the experimental data has been completed recently leading to, among others, the best direct constraint for the imaginary part of the R-parity violating MSSM contribution. The success of the applied technique results in a new project devoted to the simultaneous measurement of seven correlation coefficients: H, L, N, R, S, U and V. Five of them (H, L, S, U and V) have never before been measured in weak decays. Such a systematic exploration of the transverse electron polarization will generate from the neutron decay alone a complete set of constraints for the real and imaginary parts of the weak scalar and tensor interactions on the level of 5 × 10-4 or better.

  18. Comparative analysis of the structure of sterically stabilized ferrofluids on polar carriers by small-angle neutron scattering.

    Science.gov (United States)

    Avdeev, M V; Aksenov, V L; Balasoiu, M; Garamus, V M; Schreyer, A; Török, Gy; Rosta, L; Bica, D; Vékás, L

    2006-03-01

    Results of experiments on small-angle neutron scattering from ferrofluids on polar carriers (pentanol, water, methyl-ethyl-ketone), with double-layer sterical stabilization of magnetic nanoparticles, are reported. Several types of spatial structural organization are observed. The structure of highly stable pentanol-based samples is similar to that of stable ferrofluids based on organic non-polar carriers (e.g., benzene) with mono-layer covered magnetic nanoparticles. At the same time, the effect of the interparticle interaction on the scattering is stronger in polar ferrofluids because of the structural difference in the surfactant shell. The structure of the studied methyl-ethyl-ketone- and water-based ferrofluids essentially different from the previous case. The formation of large (>100 nm in size) elongated or fractal aggregates, respectively, is detected even in the absence of external magnetic field, which corresponds to weaker stability of these types of ferrofluids. The structure of the fractal aggregates in water-based ferrofluids does not depend on the particle concentration, but it is sensitive to temperature. A temperature increase results in a decrease in their fractal dimension reflecting destruction of the aggregates. In addition, in water-based ferrofluids these aggregates consist of small (radius approximately 10 nm) and temperature-stable primary aggregates.

  19. Accounting for Electronic Polarization Effects in Aqueous Sodium Chloride via Molecular Dynamics Aided by Neutron Scattering

    Czech Academy of Sciences Publication Activity Database

    Kohagen, Miriam; Mason, Philip E.; Jungwirth, Pavel

    2016-01-01

    Roč. 120, č. 8 (2016), s. 1454-1460 ISSN 1520-6106 R&D Projects: GA ČR GBP208/12/G016 Institutional support: RVO:61388963 Keywords : molecular dynamics * neutron scattering * agueous sodium chloride Subject RIV: CF - Physical ; Theoretical Chemistry Impact factor: 3.177, year: 2016

  20. On the interpretation of flipping ratio measurements on rocking curves in polarized neutron diffraction

    International Nuclear Information System (INIS)

    Dobrzynski, L.

    1980-01-01

    The measurements of the flipping ratio, R, vs crystal misseting angle, σ, from the Bragg position may bring important information on the homogeneity of the mosaic block distribution in ferro or ferrimagnetic crystals. It is shown that even if the sample is free from extinction, a small variation of the flipping ratio may be present if the neutron spin-flipper used in the experiment has efficiency dependence on the neutron wavelength. This effect is rather trivial and may be of importance only if both R and σ are sufficiently large. By far more important effect is due to the multiple Bragg scattering. This phenomenon is also neutron wavelength dependent and depends much on the resolution of the neutron diffractometer. While the differential equations for multiple Bragg scattering are of Zachariassen's type the resolution is treated within the framework of Caglioti et al. theory. It is shown that the multiple scattering, if present, affects seriously the shape of R(σ) and may be a source of errors in the interpretation of e.g. magnetic form factor data. A good example of this is given by the (331) reflection from Cosub(0.92)Fesub(0.08) alloy. (author)

  1. The measurement of g1n polarized structure of the neutron by the E154 experiment at SLAC

    International Nuclear Information System (INIS)

    Incerti, Sebastien

    1998-01-01

    This thesis presents the precision measurement of the neutron polarized structure g 1 n performed by the E154 collaboration at the Standford Linear Accelerator Center, USA, in autumn 1995, using a 48.3 GeV polarized electron beam scattered off a polarized Helium 3 target. The scattered electrons were detected using two spectrometer arms, covering the deep inelastic scattering range: 0.0134 2 2 2 at an average value of Q 2 = 5 GeV 2 . Two electromagnetic calorimeters have been designed by the LPC in Clermont-Ferrand and the SphN-CEA in Saclay to measure the scattered electron energy and to eject the contaminating hadron background using, a cellular automaton and a neural network, widely described in this thesis. The analysis performed in Clermont-Ferrand and presented in this document led us to the integral on the measurement region of g 1 n equaling: - 0.34 ± 0.003 STAT ± 0.004 SYST ± 0.001 EVOL at Q 2 = 5 GeV 2 , where our data have been evolved to Q 2 = 5 GeV 2 using the next-to-leading order DGLAP evolution equations and a world parametrization of the polarized parton distributions. The Ellis and Jaffe sum rule is clearly violated. Using different low x extrapolations, our integral is compatible with the Bjorken sum rule. The quark contribution to the nucleon spin is ΔΣ = 29 ± 6 % in the M S-bar scheme and ΔΣ = 37 ± 7% in the AB scheme, at Q 2 = 5 GeV 2 . The gluon contribution seems to be positive and within the range: 0 < ΔG < 2. (author)

  2. The effect of incremental gamma-ray doses and incremental neutron fluences upon the performance of self-biased sup 1 sup 0 B-coated high-purity epitaxial GaAs thermal neutron detectors

    CERN Document Server

    Gersch, H K; Simpson, P A

    2002-01-01

    High-purity epitaxial GaAs sup 1 sup 0 B-coated thermal neutron detectors advantageously operate at room temperature without externally applied voltage. Sample detectors were systematically irradiated at fixed grid locations near the core of a 2 MW research reactor to determine their operational neutron dose threshold. Reactor pool locations were assigned so that fast and thermal neutron fluxes to the devices were similar. Neutron fluences ranged between 10 sup 1 sup 1 and 10 sup 1 sup 4 n/cm sup 2. GaAs detectors were exposed to exponential fluences of base ten. Ten detector designs were irradiated and studied, differentiated between p-i-n diodes and Schottky barrier diodes. The irradiated sup 1 sup 0 B-coated detectors were tested for neutron detection sensitivity in a thermalized neutron beam. Little damage was observed for detectors irradiated at neutron fluences of 10 sup 1 sup 2 n/cm sup 2 and below, but signals noticeably degraded at fluences of 10 sup 1 sup 3 n/cm sup 2. Catastrophic damage was appare...

  3. Quantitative spatial magnetization distribution in iron oxide nanocubes and nanospheres by polarized small-angle neutron scattering

    International Nuclear Information System (INIS)

    Disch, S; Hermann, R P; Brückel, Th; Wetterskog, E; Salazar-Alvarez, G; Bergström, L; Wiedenmann, A; Vainio, U

    2012-01-01

    By means of polarized small-angle neutron scattering, we have resolved the long-standing challenge of determining the magnetization distribution in magnetic nanoparticles in absolute units. The reduced magnetization, localized in non-interacting nanoparticles, indicates strongly particle shape- dependent surface spin canting with a 0.3(1) and 0.5(1) nm thick surface shell of reduced magnetization found for ∼9 nm nanospheres and ∼8.5 nm nanocubes, respectively. Further, the reduced macroscopic magnetization in nanoparticles results not only from surface spin canting, but also from drastically reduced magnetization inside the uniformly magnetized core as compared to the bulk material. Our microscopic results explain the low macroscopic magnetization commonly found in nanoparticles. (paper)

  4. Amorphous soft-magnetic ribbons studied by ultra-small-angle polarized neutron scattering

    International Nuclear Information System (INIS)

    Badurek, G; Jericha, E; Groessinger, R; Sato-Turtelli, R

    2010-01-01

    When we investigated the magnetic structure of a variety of soft-magnetic amorphous ribbons by means of ultra-small-angle neutron scattering (USANSPOL) we were confronted with one particularly interesting Fe 65.7 Co 18 Si 0.8 B 15.5 ribbon, provided by VAC Hanau. Due to a special thermal treatment during production a field- and stress-induced transverse domain texture was expected. Although the USANSPOL technique encountered its resolution limits during the investigation of this specific sample ribbon, such a texture could indeed be verified.

  5. Study of polar and nonpolar substituted benzenes and aromatic isomers on carbon-coated zirconia and alkyl bonded phases.

    Science.gov (United States)

    Jackson, Paul T; Carr, Peter W

    2002-06-07

    Retention factors of polar and non-polar mono- and di-substituted benzene derivatives were measured on carbon coated zirconia (C/ZrO2) and an alkyl modified silica using water-acetonitrile mobile phases. Published data on porous graphitic carbon phases (PGC) were used to facilitate comparisons between the two types of carbon media. This work showed that retention on both C/ZrO2 and PGC is much more sensitive to the solute polarizability, dipolarity, and shape than on aliphatic phases. For simple disubstituted benzenes there was no general clear cut advantage in terms of chromatographic selectivity to using a carbon-based phase over a bonded phase silica; however, the selectivities towards such isomers are quite different on the two types of media. In contradistinction to their effect on alkyl bonded phase retention, addition of a dipolar substituent and weak hydrogen bond acceptor to a benzene ring almost always increases the solute's retention on C/ZrO2 and PGC.

  6. X-ray and neutron diffraction studies of crystallinity in hydroxyapatite coatings.

    Science.gov (United States)

    Girardin, E; Millet, P; Lodini, A

    2000-02-01

    To standardize industrial implant production and make comparisons between different experimental results, we have to be able to quantify the crystallinity of hydroxyapatite. Methods of measuring crystallinity ratio were developed for various HA samples before and after plasma spraying. The first series of methods uses X-ray diffraction. The advantage of these methods is that X-ray diffraction equipment is used widely in science and industry. In the second series, a neutron diffraction method is developed and the results recorded are similar to those obtained by the modified X-ray diffraction methods. The advantage of neutron diffraction is the ability to obtain measurements deep inside a component. It is a nondestructive method, owing to the very low absorption of neutrons in most materials. Copyright 2000 John Wiley & Sons, Inc.

  7. Neutron scattering. Lectures

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2010-07-01

    The following topics are dealt with: Neutron sources, neutron properties and elastic scattering, correlation functions measured by scattering experiments, symmetry of crystals, applications of neutron scattering, polarized-neutron scattering and polarization analysis, structural analysis, magnetic and lattice excitation studied by inelastic neutron scattering, macromolecules and self-assembly, dynamics of macromolecules, correlated electrons in complex transition-metal oxides, surfaces, interfaces, and thin films investigated by neutron reflectometry, nanomagnetism. (HSI)

  8. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2010-01-01

    The following topics are dealt with: Neutron sources, neutron properties and elastic scattering, correlation functions measured by scattering experiments, symmetry of crystals, applications of neutron scattering, polarized-neutron scattering and polarization analysis, structural analysis, magnetic and lattice excitation studied by inelastic neutron scattering, macromolecules and self-assembly, dynamics of macromolecules, correlated electrons in complex transition-metal oxides, surfaces, interfaces, and thin films investigated by neutron reflectometry, nanomagnetism. (HSI)

  9. Polar hydrogen positions in proteins: empirical energy placement and neutron diffraction comparison.

    Science.gov (United States)

    Brünger, A T; Karplus, M

    1988-01-01

    A method for the prediction of hydrogen positions in proteins is presented. The method is based on the knowledge of the heavy atom positions obtained, for instance, from X-ray crystallography. It employs an energy minimization limited to the environment of the hydrogen atoms bound to a common heavy atom or to a single water molecule. The method is not restricted to proteins and can be applied without modification to nonpolar hydrogens and to nucleic acids. The method has been applied to the neutron diffraction structures of trypsin, ribonuclease A, and bovine pancreatic trypsin inhibitor. A comparison of the constructed and the observed hydrogen positions shows few deviations except in situations in which several energetically similar conformations are possible. Analysis of the potential energy of rotation of Lys amino and Ser, Thr, Tyr hydroxyl groups reveals that the conformations of lowest intrinsic torsion energies are statistically favored in both the crystal and the constructed structures.

  10. High Hydrogen Content Graphene Hydride Compounds & High Cross-Section Cladding Coatings for Fast Neutron Detection

    International Nuclear Information System (INIS)

    Chandrashekhar, MVS

    2017-01-01

    The objective is to develop and implement a superior low-cost, large area (potentially >32in), easily deployable, close proximity, harsh environment innovative neutron sensor needed for next generation fuel cycle monitoring. We will exploit recent breakthroughs at the PI's lab on the electrochemistry of epitaxial graphene (EG) formed on commercial SiC wafers, a transformative nanomaterial system with superior radiation detection and durability properties to develop a new paradigm in detection for fast neutrons, a by-product of fission reactors. There are currently few effective detection/monitoring schemes, especially solid-state ones at present. This is essential for monitoring and control of future fuel cycles to make them more efficient and reliable. By exploiting these novel materials, as well as innovative hybrid SiC/EG/Cladding device architectures conceived by the team, will develop low-cost, high performance solutions to fast-neutron detection. Finally, we will also explore 3-terminal device implementations for neutron detectors with built-in electronic gain to further shrink these devices and improve their sensitivity.

  11. Correlation of Effective Dispersive and Polar Surface Energies in Heterogeneous Self-Assembled Monolayer Coatings

    DEFF Research Database (Denmark)

    Zhuang, Yanxin; Hansen, Ole

    2009-01-01

    grown oil oxidized (100) silicon Surfaces in a vapor phase process using five different precursors. Experimentally, effective surface energy components of the fluorocarbon self-assembled monolayers were determined from measured contact angles using the Owens-Wendt-Rabel-Kaelble method. We show......We show, theoretically, that the measured effective dispersive and polar surface energies of a heterogeneous Surface are correlated; the correlation, however, differs whether a Cassic or an Israelachvili and Gee model is assumed. Fluorocarbon self-assembled monolayers with varying coverage were...

  12. Polarization phenomena in the e-vector d-vector → enp process. Neutron electric form fa>ctor and deuteron structure

    International Nuclear Information System (INIS)

    Rekalo, M.N.; Gakh, G.I.; Rekalo, A.P.

    1987-01-01

    Polarization effects in the e - d→e - np process with longitudinally polarized electrons and vector polarized deuterons have been studied in the relativistic impulse approximation (which takes into account the t-, u-, s-channel pole and contact diagrams). The polarization observables which are most sensitive to the neutron electric form factor G En value have been determined. When calculating both the relativistic Buck-Gross deuteron wave function (DWF) and DWF for the Paris and Reid soft-core potentials are used. In the region of the quasielastic peak (at the nucleon emission angle Θ p =0 deg or 180 deg in c.m.s. of the np-system) the investigated asymmetries are practically independent of the DWF choice. The calculation shows that the asymmetries which are caused by the deuteron spin orientation perpendicular to the momentum transfer are most suitable for the G En determination

  13. The polarized neutron reflectivity and X-ray reflectivity studies of the magnetic profiles of epitaxial Ni80Fe20/Ru multilayers

    International Nuclear Information System (INIS)

    Su, H.-C.; Peir, J.-J.; Lee, C.-H.; Lin, M.-Z.; Wu, P.-T.; Huang, J.C.A.; Tun Zin

    2005-01-01

    The depth profiles of the epitaxial Ni 80 Fe 20 (1 1 1)/Ru(0 0 0 1) multilayers were studied by polarized neutron reflectivity and X-ray reflectivity. At the Ru thickness that the anti-ferromagnetic coupling was found, the magnetic moments between two Ni 80 Fe 20 interlayers show a biquadratic coupling effect with a double unit cell at low applied fields. A magnetic dead layer of about 0.3 nm was also found at the interface boundaries. The maximal polarization effect applied to the Ru layer is less than 0.03μ B

  14. Review on Recent Results from RHIC Polarized Collider; Unexpected Forward Neutron Asymmetry

    Science.gov (United States)

    Nakagawa, Itaru

    The polarized proton-proton collider at RHIC provides an unique opportunity to study the spin structure of the proton. The latest highlights from both transverse and longitudinal RHIC spin program are introduced in this document. For the transverse program, two asymmetry measurements are discussed here which are distinguished by the production mechanism either soft (diffractive) or hard perturbative QCD natures depending on the rapidity region of the hadron production. The former is the very forwardneutron asymmetry measurements which showed unexpectedly drastic dependence on the atomic mass. The latter is the forward pion production whose origin of the large asymmetry has been under debate for theoretical understanding over two decades. For longitudinal program, the latest highlights from the measurements on the gluon and the sea quark spin components of the proton spin are discussed.

  15. Inelastic neutron scattering facilities at the Budapest Neutron Center

    Energy Technology Data Exchange (ETDEWEB)

    Toeroek, Gy.; Nagy, A. [Research Institute for Solid State Physics and Optics, P.O.B.49, 1525 Budapest (Hungary); Lebedev, V.T.; Gordeev, G.P. [Petersburg Nuclear Physics Institute, 188300 Gatchina (Russian Federation); Zsigmond, G. [Hahn Meitner Institute, Glienicker str 100, 14109 Berlin (Germany)

    2004-11-01

    Two Triple Axis spectrometers are commissioned now at the Budapest Neutron Center. The Thermal Triple Axis Spectrometer (TAST) is installed on the 8-th beam (60 mm diameter) and supplied with a 120 mm-long sapphire crystal placed inside the channel (2 m far from monochromator) to filter fast neutrons. The Eulerian cradle can be placed at the sample position to carry out holographic measurements. Otherwise a normal goniometer (carrying up to 100 kg weight for orientation, e.g. Cryostat/magnet/heavy sample) is used. This spectrometer's resolution was modeled by VITESS program package. The second (cold) neutron spectrometer (ATHOS) on a curved (4200 m) neutron guide is mounted at the 19 m-position from the cold source. The neutron guide 1.5{theta}{sub c}, made of boron glass, is coated with NiTi multilayer. This instrument, developed into the RITA-type spectrometer, is supplied with a 190 x 190 mm{sup 2} position sensitive detector and a polarization option (stacked polarizer). In addition it has the optional COMPACT Neutron Spin Echo setup, based on Larmor precession, for energy analysis with the resolution of 10 {mu}eV. The test measurements are presented. (copyright 2004 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  16. Quantum entanglement in manganese(II) hexakisimidazole nitrate: on electronic structure imaging - A polarized neutron diffraction and DFT study

    Science.gov (United States)

    Wallace, Warren A.

    2016-04-01

    Quantum entanglement has been visualized for the first time, in view of the spin density distribution and electronic structure for manganese in manganese(II)hexakisimidazole nitrate. Using polarized neutron diffraction and density functional theory modelling we have found for the complex, which crystallizes in the R3¯ spacegroup, a = b = 12.4898(3) Å, c = 14.5526(4) Å, α = γ = 90°, β = 120°, Z = 3, that spatially antisymmetric and spatially symmetric shaped regions of negative spin density, in the spin density map for manganese, are a result of quantum entanglement of the high spin d5 configuration due to dative imidazole- manganese π- donation and σ-bonding interactions respectively. We have found leakage of the entangled states for manganese observed as regions of positive spin density with spherical (3.758(2) μB) and non-spherical (1.242(3) μB) contributions. Our results, which are supportive of Einstein's theory of general relativity, provide evidence for the existence of a black hole spin density distribution at the origin of an electronic structure and also address the paradoxical views of entanglement and quantum mechanics. We have also found the complex, which is an insulator, to be suitable for spintronic studies.

  17. Design and realization of a sputter deposition system for the in situ- and in operando-use in polarized neutron reflectometry experiments

    Science.gov (United States)

    Schmehl, Andreas; Mairoser, Thomas; Herrnberger, Alexander; Stephanos, Cyril; Meir, Stefan; Förg, Benjamin; Wiedemann, Birgit; Böni, Peter; Mannhart, Jochen; Kreuzpaintner, Wolfgang

    2018-03-01

    We report on the realization of a sputter deposition system for the in situ- and in operando-use in polarized neutron reflectometry experiments. Starting with the scientific requirements, which define the general design considerations, the external limitations and boundaries imposed by the available space at a neutron beamline and by the neutron and vacuum compatibility of the used materials, are assessed. The relevant aspects are then accounted for in the realization of our highly mobile deposition system, which was designed with a focus on a quick and simple installation and removability at the beamline. Apart from the general design, the in-vacuum components, the auxiliary equipment and the remote control via a computer, as well as relevant safety aspects are presented in detail.

  18. Shape coexistence in the N=19 neutron-rich nucleus 31Mg explored by β–γ spectroscopy of spin-polarized 31Na

    Directory of Open Access Journals (Sweden)

    H. Nishibata

    2017-04-01

    Full Text Available The structure of excited states in the neutron-rich nucleus 31Mg, which is in the region of the “island of inversion” associated with the neutron magic number N=20, is studied by β–γ spectroscopy of spin-polarized 31Na. Among the 31Mg levels below the one neutron separation energy of 2.3 MeV, the spin values of all five positive-parity levels are unambiguously determined by observing the anisotropic β decay. Two rotational bands with Kπ=1/2+ and 1/2− are proposed based on the spins and energies of the levels. Comparison on a level-by-level basis is performed between the experimental results and theoretical calculations by the antisymmetrized molecular dynamics (AMD plus generator coordinate method (GCM. It is found that various nuclear structures coexist in the low excitation energy region in 31Mg.

  19. Polarimetric neutron scattering

    International Nuclear Information System (INIS)

    Tasset, F.

    2001-01-01

    Polarimetric Neutron Scattering in introduced, both by, explaining methodological issues and the corresponding instrumental developments. After a short overview of neutron spin polarization and the neutron polarization 3d-vector a pictorial approach of the microscopic theory is used to show how a polarized beam interacts with lattice and magnetic Fourier components in a crystal. Examples are given of using Spherical Neutron Polarimetry (SNP) and the corresponding Cryopad polarimeter for the investigation of non-collinear magnetic structures. (R.P.)

  20. Use of neutron and synchrotron X-ray diffraction for evaluation of residual stresses in a 2024-T351 aluminum alloy variable-polarity plasma-arc weld

    Science.gov (United States)

    Ganguly, S.; Fitzpatrick, M. E.; Edwards, L.

    2006-02-01

    The residual stress fields associated with variable-polarity plasma-arc (VPPA) welds in 2024-T351 aluminum alloy plates have been measured nondestructively using neutron and synchrotron X-ray diffraction. Neutron diffraction allows in-depth measurements of the full strain tensor to be made in thick components; synchrotron X-rays allow for rapid measurements of strains inside components, although their penetration is less than that of the neutrons and constraints arising from the diffraction geometry generally lead to only two strain components being easily measurable. Hence, a combination of the two techniques, applied as described herein, is ideal for a detailed nondestructive evaluation of residual stresses in plates. The residual stresses in a 12-mm-thick VPPA-welded aluminum 2024-T351 alloy plate have been measured using neutron diffraction. The stresses were then remeasured by a combination of neutron and synchrotron X-ray diffraction after the plate had been reduced in thickness (or, skimmed) to 7 mm by machining both sides of the weld, mimicking the likely manufacturing operation, should such welds be used in aerospace structures. A strong tensile residual stress field was measured in the longitudinal direction, parallel to the weld, in both the as-welded and skimmed specimens. There was only a slight modification of the residual stress state on skimming.

  1. Tunable ultra-broadband polarization filter based on three-core resonance of the fluid-infiltrated and gold-coated photonic crystal fiber

    Science.gov (United States)

    Liu, Yingchao; Chen, Hailiang; Ma, Mingjian; Zhang, Wenxun; Wang, Yujun; Li, Shuguang

    2018-03-01

    We propose a tunable ultra-broadband polarization filter based on three-core resonance of the fluid-infiltrated and gold-coated high birefringent photonic crystal fiber (HB-PCF). Gold film was applied to the inner walls of two cladding air holes and surface plasmon polaritons were generated on its surface. The two gold-coated cladding air holes acted as two defective cores. As the phase matching condition was satisfied, light transmitted in the fiber core and coupled to the two defective cores. The three-core PCF supported three super modes in two orthogonal polarization directions. The coupling characteristics among these modes were investigated using the finite-element method. We found that the coupling wavelengths and strength between these guided modes can be tuned by altering the structural parameters of the designed HB-PCF, such as the size of the voids, thickness of the gold-films and liquid infilling pattern. Under the optimized structural parameters, a tunable broadband polarization filter was realized. For one liquid infilling pattern, we obtained a broadband polarization filter which filtered out the light in y-polarization direction at the wavelength of 1550 nm. For another liquid infilling pattern, we filtered out light in the x-polarization direction at the wavelength of 1310 nm. Our studies on the designed HB-PCF made contributions to the further devising of tunable broadband polarization filters, which are extensively used in telecommunication and sensor systems. Project supported by the National Natural Science Foundation of China (Grant Nos. 61505175 and 61475134) and the Natural Science Foundation of Hebei Province (Grant Nos. F2017203110 and F2017203193).

  2. Magnetic properties of the SiO2(Co)/GaAs interface: Polarized neutron reflectometry and SQUID magnetometry

    Science.gov (United States)

    Ukleev, V. A.; Grigoryeva, N. A.; Dyadkina, E. A.; Vorobiev, A. A.; Lott, D.; Lutsev, L. V.; Stognij, A. I.; Novitskiy, N. N.; Mistonov, A. A.; Menzel, D.; Grigoriev, S. V.

    2012-10-01

    The effect of giant injection magnetoresistance (GIMR) was recently observed in a granular SiO2/(54-75 at. % Co) film on a semiconductor GaAs substrate in a temperature range near T=300 K. The magnetoresistance coefficient reaches a value of 105% in a magnetic field of 1.9 T and at a voltage of 90 V. A structural model of the film was proposed based on the results of the grazing-incidence small-angle scattering (GISAXS) and x-ray reflectivity, which showed a specific interface layer 70-75 Å thick separating bulk SiO2(Co) granular film from the semiconductor substrate. This layer is formed by a monolayer of flattened Co particles which are laterally spaced apart much further than the particles in the bulk film. In the present work, using polarized neutron reflectometry (PNR), we study both the structural and magnetic properties of SiO2(Co) film separately in the bulk and in the interface layer, which is possible due to the depth resolution of the method. Temperature-dependent PNR and magnetization measurements performed by Superconducting Quantum Interference Device (SQUID) revealed the occurrence of two types of magnetic nanoparticles with different blocking temperatures and magnetization. The magnetization hysteresis curve demonstrated specific two-loop structure in fields 0.5-2 T. Thus our self-consistent results of PNR, GISAXS, and SQUID measurements emphasize the role of the interface features in the SiO2(Co)/GaAs heterostructures and show a direction for further development of the GIMR theory.

  3. Low Group Delay Dispersion Optical Coating for Broad Bandwidth High Reflection at 45° Incidence, P Polarization of Femtosecond Pulses with 900 nm Center Wavelength

    Directory of Open Access Journals (Sweden)

    John C. Bellum

    2016-03-01

    Full Text Available We describe an optical coating design suitable for broad bandwidth high reflection (BBHR at 45° angle of incidence (AOI, P polarization (Ppol of femtosecond (fs laser pulses whose wavelengths range from 800 to 1000 nm. Our design process is guided by quarter-wave HR coating properties. The design must afford low group delay dispersion (GDD for reflected light over the broad, 200 nm bandwidth in order to minimize temporal broadening of the fs pulses due to dispersive alteration of relative phases between their frequency components. The design should also be favorable to high laser-induced damage threshold (LIDT. We base the coating on TiO2/SiO2 layer pairs produced by means of e-beam evaporation with ion-assisted deposition, and use OptiLayer Thin Film Software to explore designs starting with TiO2/SiO2 layers having thicknesses in a reverse chirped arrangement. This approach led to a design with R > 99% from 800 to 1000 nm and GDD < 20 fs2 from 843 to 949 nm (45° AOI, Ppol. The design’s GDD behaves in a smooth way, suitable for GDD compensation techniques, and its electric field intensities show promise for high LIDTs. Reflectivity and GDD measurements for the initial test coating indicate good performance of the BBHR design. Subsequent coating runs with improved process calibration produced two coatings whose HR bands satisfactorily meet the design goals. For the sake of completeness, we summarize our previously reported transmission spectra and LIDT test results with 800 ps, 8 ps and 675 fs pulses for these two coatings, and present a table of the LIDT results we have for all of our TiO2/SiO2 BBHR coatings, showing the trends with test laser pulse duration from the ns to sub-ps regimes.

  4. Monte Carlo program for the cold neutron beam guide

    International Nuclear Information System (INIS)

    Yoshiki, H.

    1985-02-01

    A Monte Carlo program for the transport of cold neutrons through beam guides has been developed assuming that the neutrons follow the specular reflections. Cold neutron beam guides are normally used to transport cold neutrons (4 ∼ 10 Angstrom) to experimental equipments such as small angle scattering apparatus, TOF measuring devices, polarized neutron spectrometers, and ultra cold neutron generators, etc. The beam guide is about tens of meters in length and is composed from a meter long guide elements made up from four pieces of Ni coated rectangular optical glass. This report describes mathematics and algorithm employed in the Monte Carlo program together with the display of the results. The source program and input data listings are also attached. (Aoki, K.)

  5. Study of the dynamic and magnetic properties of solids using inelastic scattering and polarized neutron techniques. Part of a coordinated programme on the use of neutron scattering techniques in the study of solids

    International Nuclear Information System (INIS)

    Iyengar, P.

    1977-12-01

    Magnetic moment density distributions of several cubic spinel ferrites were obtained by using the neutron diffraction technique. The investigated materials were magnetite, MnFe 2 O 4 , MnAlGe, and Cu 2 MnAl. Information about the static and time-averaged behaviour of the magnetic electrons was deduced. The diffuse scattering technique with polarized neutrons which permits to isolate the magnon-scattering profile from other neutron profiles, was utilized to explore the acoustic magnon branches in ferro and ferrimagnetic materials such as MnFe 2 O 4 . The lattice and molecular dynamics has been studied in a number of condensed systems. Librational motions of water molecules in crystal hydrates were determined by the technique of polarization dependence of incoherent scattering cross section. Librations of amino and methyl groups in amino acids have been studied. Mixed salts of various ammonium and potassium compounds were investigated with a view to elucidate the nature of potential function and reorientational motions of reorienting ions

  6. A Measurement of the neutron electric form factor at very large momentum transfer using polaried electrions scattering from a polarized helium-3 target

    Energy Technology Data Exchange (ETDEWEB)

    Kelleher, Aidan [College of William and Mary, Williamsburg, VA (United States)

    2010-02-01

    Knowledge of the electric and magnetic elastic form factors of the nucleon is essential for an understanding of nucleon structure. Of the form factors, the electric form factor of the neutron has been measured over the smallest range in Q2 and with the lowest precision. Jefferson Lab experiment 02-013 used a novel new polarized 3 He target to nearly double the range of momentum transfer in which the neutron form factor has been studied and to measure it with much higher precision. Polarized electrons were scattered off this target, and both the scattered electron and neutron were detected. Gn E was measured to be 0.0242 ± 0.0020(stat) ± 0.0061(sys) and 0.0247 ± 0.0029(stat) ± 0.0031(sys) at Q2 = 1.7 and 2.5 GeV2 , respectively.

  7. Polarized single crystal neutron diffraction study of the zero-magnetization ferromagnet Sm1 -xGdxAl2 (x =0.024 )

    Science.gov (United States)

    Chatterji, T.; Stunault, A.; Brown, P. J.

    2018-02-01

    We have determined the temperature evolution of the spin and orbital moments in the zero-magnetization ferromagnet Sm1 -xGdxAl2 (x = 0.024) by combining polarized and unpolarized single crystal neutron diffraction data. The sensitivity of the polarized neutron technique has allowed the moment values to be determined with a precision of ≈0.1 μB . Our results clearly demonstrate that, when magnetized by a field of 8 T, the spin and orbital moments in Sm1 -xGdxAl2 are oppositely directed, so that the net magnetization is very small. Below 60 K the contributions from spin and orbital motions are both about 2 μB , with that due to orbital motion being slightly larger than that due to spin. Between 60 and 65 K the contributions of each to the magnetization fall rapidly and change sign at Tcomp ≈67 K , above which the aligned moments recover but with the orbital magnetization still slightly higher than the spin one. These results imply that above Tcomp the small resultant magnetization of the Sm3 + ion is oppositely directed to the magnetizing field. It is suggested that this anomaly is due to polarization of conduction electron spin associated with the doping Gd3 + ions.

  8. When combined X-ray and polarized neutron diffraction data challenge high-level calculations: spin-resolved electron density of an organic radical.

    Science.gov (United States)

    Voufack, Ariste Bolivard; Claiser, Nicolas; Lecomte, Claude; Pillet, Sébastien; Pontillon, Yves; Gillon, Béatrice; Yan, Zeyin; Gillet, Jean Michel; Marazzi, Marco; Genoni, Alessandro; Souhassou, Mohamed

    2017-08-01

    Joint refinement of X-ray and polarized neutron diffraction data has been carried out in order to determine charge and spin density distributions simultaneously in the nitronyl nitroxide (NN) free radical Nit(SMe)Ph. For comparison purposes, density functional theory (DFT) and complete active-space self-consistent field (CASSCF) theoretical calculations were also performed. Experimentally derived charge and spin densities show significant differences between the two NO groups of the NN function that are not observed from DFT theoretical calculations. On the contrary, CASSCF calculations exhibit the same fine details as observed in spin-resolved joint refinement and a clear asymmetry between the two NO groups.

  9. Accessible length scale of the in-plane structure in polarized neutron off-specular and grazing-incidence small-angle scattering measurements

    Science.gov (United States)

    Maruyama, R.; Bigault, T.; Wildes, A. R.; Dewhurst, C. D.; Saerbeck, T.; Honecker, D.; Yamazaki, D.; Soyama, K.; Courtois, P.

    2017-06-01

    Polarized neutron off-specular and grazing-incidence small-angle scattering measurements are useful methods to investigate the in-plane structure and its correlation of layered systems. Although these measurements give information on complementary and overlapping length scale, the different characteristics between them need to be taken into account when performed. In this study, the difference in the accessible length scale of the in-plane structure, which is one of the most important characteristics, was discussed using an Fe/Si multilayer together with simulations based on the distorted wave Born approximation.

  10. Effect of lattice distortion on uranium magnetic moments in U4Ru7Ge6 studied by polarized neutron diffraction

    Science.gov (United States)

    Vališka, Michal; Klicpera, Milan; Doležal, Petr; Fabelo, Oscar; Stunault, Anne; Diviš, Martin; Sechovský, Vladimír

    2018-03-01

    In a cubic ferromagnet, small spontaneous lattice distortions are expected below the Curie temperature, but the phenomenon is usually neglected. This study focuses on such an effect in the U4Ru7Ge6 compound. Based on DFT calculations, we propose a lattice distortion from the cubic I m -3 m space group to a lower, rhombohedral, symmetry described by the R -3 m space group. The strong spin-orbit coupling of the uranium ions plays an essential role in lowering the symmetry, giving rise to two different U sites (U1 and U2). Using polarized neutron diffraction in applied magnetic fields of 1 and 9 T in the ordered state (1.9 K ) and in the paramagnetic state (20 K ), we bring convincing experimental evidence of this splitting of the U sites, with different magnetic moments. The data have been analyzed both by maximum entropy calculations and by a direct fit in the dipolar approximation. In the ordered phase, the μL/μS ratio of the orbital and spin moments on the U2 site is remarkably lower than for the free U3 + or U4 + ion, which points to a strong hybridization of the U 5 f wave functions with the 4 d wave functions of the surrounding Ru. On the U1 site, the μL/μS ratio exhibits an unexpectedly low value: the orbital moment is almost quenched, like in metallic α -uranium. As a further evidence of the 5 f -4 d hybridization in the U4Ru7Ge6 system, we observe the absence of a magnetic moment on the Ru1 site, but a rather large induced moment on the Ru2 site, which is in closer coordination with both U positions. Very similar results are obtained at 20 K in the ferromagnetic regime induced by the magnetic field of 9 T . This shows that applying a strong magnetic field above the Curie temperature also leads to the splitting of the uranium sites, which further demonstrates the intimate coupling of the magnetic ordering and structural distortion. We propose that the difference between the magnetic moment on the U1 and U2 sites results from the strong spin

  11. Contribution to the replacement of cobalt-free hardfacing coating by laser cladding in fast neutron reactors

    International Nuclear Information System (INIS)

    De-Tran, Van

    2014-01-01

    This thesis contributes to the replacement of the coating of Stellite 6 which is used in friction areas for the primary circuit of the fast neutron reactor. It contains three parts: 1) A literature review for selecting the materials and the deposition process 2) A parametric study to get healthy deposits (good adhesion with the substrate, little porosity, no cracks, low dilution) 3) A study wear behavior of deposits obtained, at high temperature (200 C) under an atmosphere inert gas, to determine the wear resistance of materials selected without the influence of an eventual oxidation layer. From the literature review, it appears the following choices implemented in our study: * the method laser cladding with advantages such as: - Good adhesion (metallurgical) - High cooling speed - Low dilution rate - Wide parametric range * two nickel-based alloys: Colmonoy-52 and Tribaloy-700. These alloys have good dry wear behavior and could be deposited by the laser. In the manufacturing part of the healthy deposit, firstly, we characterized the metal powder. Then, a parametric study was performed to look for a good parametric range that makes us getting a healthy deposit of Stellite 6 (reference) of Colmonoy-52 and Tribaloy-700. In this case, relationships among three main process parameters laser cladding (laser beam power, surface scanning speed, rate of powder) with the microstructure and chemical composition of the deposit are studied. In study the wear behavior, a pin-on-disc type of tribological was used and tests were carried out in argon at room temperature and 200 C. We investigated the wear mechanism of the best deposition of Stellite 6, Colmonoy-52 and Tribaloy-700. The wear resistance of these materials were thoroughly compared. (author) [fr

  12. The Electromagnetic Counterpart of the Binary Neutron Star Merger LIGO/Virgo GW170817. III. Optical and UV Spectra of a Blue Kilonova from Fast Polar Ejecta

    Energy Technology Data Exchange (ETDEWEB)

    Nicholl, M.; Berger, E.; Kasen, D.; Metzger, B. D.; Elias, J.; Briceño, C.; Alexander, K. D.; Blanchard, P. K.; Chornock, R.; Cowperthwaite, P. S.; Eftekhari, T.; Fong, W.; Margutti, R.; Villar, V. A.; Williams, P. K. G.; Brown, W.; Annis, J.; Bahramian, A.; Brout, D.; Brown, D. A.; Chen, H. -Y.; Clemens, J. C.; Dennihy, E.; Dunlap, B.; Holz, D. E.; Marchesini, E.; Massaro, F.; Moskowitz, N.; Pelisoli, I.; Rest, A.; Ricci, F.; Sako, M.; Soares-Santos, M.; Strader, J.

    2017-10-16

    We present optical and ultraviolet spectra of the first electromagnetic counterpart to a gravitational wave (GW) source, the binary neutron star merger GW170817. Spectra were obtained nightly between 1.5 and 9.5 days post-merger, using the SOAR and Magellan telescopes; the UV spectrum was obtained with the \\textit{Hubble Space Telescope} at 5.5 days. Our data reveal a rapidly-fading blue component ($T\\approx5500$ K at 1.5 days) that quickly reddens; spectra later than $\\gtrsim 4.5$ days peak beyond the optical regime. The spectra are mostly featureless, although we identify a possible weak emission line at $\\sim 7900$ \\AA\\ at $t\\lesssim 4.5$ days. The colours, rapid evolution and featureless spectrum are consistent with a "blue" kilonova from polar ejecta comprised mainly of light $r$-process nuclei with atomic mass number $A\\lesssim 140$. This indicates a sight-line within $\\theta_{\\rm obs}\\lesssim 45^{\\circ}$ of the orbital axis. Comparison to models suggests $\\sim0.03$ M$_\\odot$ of blue ejecta, with a velocity of $\\sim 0.3c$. The required lanthanide fraction is $\\sim 10^{-4}$, but this drops to $<10^{-5}$ in the outermost ejecta. The large velocities point to a dynamical origin, rather than a disk wind, for this blue component, suggesting that both binary constituents are neutron stars (as opposed to a binary consisting of a neutron star and a black hole). For dynamical ejecta, the high mass favors a small neutron star radius of $\\lesssim 12$ km. This mass also supports the idea that neutron star mergers are a major contributor to $r$-process nucleosynthesis.

  13. A measurement of correlation parameters in the decay of polarized free neutrons: The abBA experiment

    Science.gov (United States)

    Barrón-Palos, L.; Chávez, E.; Crawford, C.; Curiel-García, Q.; Huerta, A.; Juárez-Rosete, M. A.; Marín-Lámbarri, D. J.; Martin, E.; Ortiz, M. E.; Penttilä, S. I.; Rodríguez-Zamora, P.; Salas, A.; Tang, Z.; Wilburn, W. S.

    2010-07-01

    The abBA experiment will measure, in the same apparatus, four correlation parameters in the free neutron β-decay: the electron-antineutrino angular correlation (a), the Fierz interference term (6), and the asymmetries, with respect to the neutron spin direction, of the electron (A)and antineutrino (B).The precise determination of these parameters, together with the neutron lifetime, will provide important information about the Standard Model (SM) and will establish constraints for new physics. In this paper we describe the experimental methodology of abBA as well as some of the advances that have been done so far.

  14. A measurement of correlation parameters in the decay of polarized free neutrons: The abBA experiment

    Energy Technology Data Exchange (ETDEWEB)

    Barron-Palos, L; Chavez, E; Curiel-Garcia, Q; Huerta, A; Juarez-Rosete, M A; Marin-Lambarri, D J; Ortiz, M E [Universidad Nacional Autonoma de Mexico, Mexico, D.F. 04510 (Mexico); Crawford, C; Martin, E [University of Kentucky, Lexington, KY 40506 (United States); Penttilae, S I [Oak Ridge National Laboratory, Oak Ridge, TN 37831 (United States); Salas, A; Wilburn, W S [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); Tang, Z [Indiana University, Bloomington, IN 47405 (United States); RodrIguez-Zamora, P, E-mail: libertad@fisica.unam.m

    2010-07-01

    The abBA experiment will measure, in the same apparatus, four correlation parameters in the free neutron {beta}-decay: the electron-antineutrino angular correlation (a), the Fierz interference term (6), and the asymmetries, with respect to the neutron spin direction, of the electron (A)and antineutrino (B).The precise determination of these parameters, together with the neutron lifetime, will provide important information about the Standard Model (SM) and will establish constraints for new physics. In this paper we describe the experimental methodology of abBA as well as some of the advances that have been done so far.

  15. A measurement of correlation parameters in the decay of polarized free neutrons: The abBA experiment

    International Nuclear Information System (INIS)

    Barron-Palos, L; Chavez, E; Curiel-Garcia, Q; Huerta, A; Juarez-Rosete, M A; Marin-Lambarri, D J; Ortiz, M E; Crawford, C; Martin, E; Penttilae, S I; Salas, A; Wilburn, W S; Tang, Z; RodrIguez-Zamora, P

    2010-01-01

    The abBA experiment will measure, in the same apparatus, four correlation parameters in the free neutron β-decay: the electron-antineutrino angular correlation (a), the Fierz interference term (6), and the asymmetries, with respect to the neutron spin direction, of the electron (A)and antineutrino (B).The precise determination of these parameters, together with the neutron lifetime, will provide important information about the Standard Model (SM) and will establish constraints for new physics. In this paper we describe the experimental methodology of abBA as well as some of the advances that have been done so far.

  16. Quantitative neutron radiography using neutron absorbing honeycomb

    International Nuclear Information System (INIS)

    Tamaki, Masayoshi; Oda, Masahiro; Takahashi, Kenji; Ohkubo, Kohei; Tasaka, Kanji; Tsuruno, Akira; Matsubayashi, Masahito.

    1993-01-01

    This investigation concerns quantitative neutron radiography and computed tomography by using a neutron absorbing honeycomb collimator. By setting the neutron absorbing honeycomb collimator between object and imaging system, neutrons scattered in the object were absorbed by the honeycomb material and eliminated before coming to the imaging system, but the neutrons which were transmitted the object without interaction could reach the imaging system. The image by purely transmitted neutrons gives the quantitative information. Two honeycombs were prepared with coating of boron nitride and gadolinium oxide and evaluated for the quantitative application. The relation between the neutron total cross section and the attenuation coefficient confirmed that they were in a fairly good agreement. Application to quantitative computed tomography was also successfully conducted. The new neutron radiography method using the neutron-absorbing honeycomb collimator for the elimination of the scattered neutrons improved remarkably the quantitativeness of the neutron radiography and computed tomography. (author)

  17. Polarization Studies on Inhibitory Effect of Chromates and Dichromates on Corrosion of Tin Coated Steel in 0.5M Monochloroacetic Acid

    Directory of Open Access Journals (Sweden)

    Sangita Sharma

    2008-01-01

    Full Text Available Chromates and Dichromates have been tested for its inhibitory effects towards tin coated steel in 0.5M monochloroacetic acid. The corrosion behaviour of potassium chromate, sodium chromate, potassium dichromate, sodium dichromate and ammonium dichromate was studied by polarization curves, Tafel parameters like Tafel slopes, extrapolation of cathodic Tafel line and intersection of cathodic and anodic line at open circuit potential in presence of inhibitors have been tabulated along with other electrochemical parameters and corrosion current have been calculated from Tafel lines. The efficiencies are calculated and compared reasonably well with those obtained from loss in weight data. All the inhibitors induce a significant increase of potential positive and direction accounts for cathodic polarization. The Icorr has also been calculated and that accounts well for cathodic reactions in presence of chromates and dichromates as inhibitors.

  18. No evidence for orbital loop currents in charge-ordered YBa2Cu3O6 +x from polarized neutron diffraction

    Science.gov (United States)

    Croft, T. P.; Blackburn, E.; Kulda, J.; Liang, Ruixing; Bonn, D. A.; Hardy, W. N.; Hayden, S. M.

    2017-12-01

    It has been proposed that the pseudogap state of underdoped cuprate superconductors may be due to a transition to a phase which has circulating currents within each unit cell. Here, we use polarized neutron diffraction to search for the corresponding orbital moments in two samples of underdoped YBa2Cu3O6 +x with doping levels p =0.104 and 0.123. In contrast to some other reports using polarized neutrons, but in agreement with nuclear magnetic resonance and muon spin rotation measurements, we find no evidence for the appearance of magnetic order below 300 K. Thus, our experiment suggests that such order is not an intrinsic property of high-quality cuprate superconductor single crystals. Our results provide an upper bound for a possible orbital loop moment which depends on the pattern of currents within the unit cell. For example, for the CC-θI I pattern proposed by Varma, we find that the ordered moment per current loop is less than 0.013 μB for p =0.104 .

  19. Measurement of the ROT effect in the neutron induced fission of 235U in the 0.3 eV resonance at a hot source of polarized neutrons

    Science.gov (United States)

    Kopatch, Yuri; Novitsky, Vadim; Ahmadov, Gadir; Gagarsky, Alexei; Berikov, Daniyar; Danilyan, Gevorg; Hutanu, Vladimir; Klenke, Jens; Masalovich, Sergey

    2018-03-01

    The TRI and ROT asymmetries in fission of heavy nuclei have been extensively studied during more than a decade. The effects were first discovered in the ternary fission in a series of experiments performed at the ILL reactor (Grenoble) by a collaboration of Russian and European institutes, and were carefully measured for a number of fissioning nuclei. Later on, the ROT effect has been observed in the emission of prompt gamma rays and neutrons in fission of 235U and 233U, although its value was an order of magnitude smaller than in the α-particle emission from ternary fission. All experiments performed so far are done with cold polarized neutrons, what assumes a mixture of several spin states, the weights of these states being not well known. The present paper describes the first attempt to get "clean" data by performing the measurement of gamma and neutron asymmetries in an isolated resonance of 235U at the POLI instrument of the FRM2 reactor in Garching.

  20. Investigation of structure and polar domain dynamics of Sr1-xCaxTiO3 compounds by using neutron scattering

    International Nuclear Information System (INIS)

    Tyagi, Shekhar; Sharma, Gaurav; Sathe, V.G.

    2016-01-01

    Sr 1-x Ca x TiO 3 (SCT) compound shows very interesting behaviour. It behaves like a relax or ferroelectric in the concentration range of (0.016polar domains with the application of pressure is reflected in our pressure dependent Raman spectroscopy studies. We probed the effect of high pressure on the local Nano-polar domains phase. We concluded that the rotation of octahedra and shifting of Ti atoms from the centre of unit cell upon doping as well increasing external pressure plays an important role in formation of nano-domains. Therefore, we would like to further extend these studies by using temperature dependent neutron diffraction studies. Unlike x-rays, neutron is more sensitive towards the position of ions in unit cell and hence we expect an accurate information of the displacement of ions and tilt of oxygen octahedral in the two regions i.e. relaxor and anti-ferroelectric regions. We propose to carry out temperature dependent neutron diffraction studies in four compositions, x=0.0, 0.06, 0.25 and 0.35 across the transition temperature. (author)

  1. Investigation of magnetic mesostructure of (Pd{sub 0.984}Fe{sub 0.016}){sub 0.95}Mn{sub 0.05} alloy by polarized neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Gordeev, G. [Petersburg Nuclear Physics Institute RAS, 188300 Gatchina, St. Petersburg (Russian Federation)]. E-mail: ggordev@pnpi.spb.ru; Zabenkin, V. [Petersburg Nuclear Physics Institute RAS, 188300 Gatchina, St. Petersburg (Russian Federation); Axelrod, L. [Petersburg Nuclear Physics Institute RAS, 188300 Gatchina, St. Petersburg (Russian Federation); Lazebnik, I. [Petersburg Nuclear Physics Institute RAS, 188300 Gatchina, St. Petersburg (Russian Federation); Wagner, V. [Physikalish-Technishe Bundesanstalt D-38116, Braunschweig (Germany); Eckerlebe, H. [Forschung Zentrum GKSS, Geesthacht (Germany)

    2007-07-15

    Neutron depolarization measurements and a simple model for depolarization were used to determine the geometrical sizes of magnetic inhomogeneities in the (Pd{sub 0.984}Fe{sub 0.016}){sub 0.95}Mn{sub 0.05} alloy. Polarized small angle scattering shows an asymmetric part, which should be attributed to a chiral ordering of the spins.

  2. Spin-wave dynamics in Invar Fe sub 6 sub 5 Ni sub 3 sub 5 alloy studied by small-angle polarized neutron scattering

    CERN Document Server

    Grigoriev, S V; Deriglazov, V V; Okorokov, A I; Dijk, N H V; Brück, E; Klaasse, J C P; Eckerlebe, H; Kozik, G

    2002-01-01

    Spin dynamics in Fe sub 6 sub 5 Ni sub 3 sub 5 Invar alloy has been studied by left-right asymmetry of small-angle polarized neutron scattering below T sub C =485 K in external magnetic fields of H=0.05-0.25 T inclined relative to the incident beam. The spin-wave stiffness D and the damping GAMMA were obtained by fitting the antisymmetrical contribution to the scattering. The spin-wave stiffness extrapolated by a (T/T sub C) sup 5 sup / sup 2 law to T=0 K is D sub 0 =117+-2 meVA sup 2 , which is somewhat smaller than the spin-wave stiffness obtained by triple-axis spectrometry. (orig.)

  3. Study of magnetic thin films by polarized neutron reflectivity. Off-specular diffusion on periodical structures; Etude de couches minces magnetiques par reflectivite de neutrons polarises. Diffusion non speculaire sur des structures periodiques

    Energy Technology Data Exchange (ETDEWEB)

    Ott, F

    1998-11-26

    Theoretical (Zeeman energy effects) and experimental (beam polarisation problems) progress have been made in the understanding of polarized neutron reflectivity with polarisation analysis. It has been shown that modelization and numerical simulations makes it possible to avoid to have to systematically measure a full set of reflectivity curves for each field and temperature condition. It has been possible to determine a magnetic profile as a function of the field in a magnetic bilayer system by using only a few points in the reciprocal space. This technique allows to considerable reduce the experiment time. In single nickel layer systems, we have shown that it is possible to induce magnetic rotation inhomogeneities when these systems are subjects to deformation strains. The effect are related to magneto-elastic constants gradients. In trilayer systems, with a ME constant modulation, we have been able to induce large magnetic rotation gradients. A new magneto-optic technique to measure the magnetization direction without rotating the magnetic field has been developed. The field of neutron reflectivity has been extended to off-specular studies. It has been possible to account quantitatively of the off-specular diffusion on 2-D model systems (prepared by optical lithography). This new technique should make it possible in the future to determine magnetic structures with a in-depth as well as lateral resolution. (author)

  4. Contrast variation by dynamic nuclear polarization and time-of-flight small-angle neutron scattering. I. Application to industrial multi-component nanocomposites.

    Science.gov (United States)

    Noda, Yohei; Koizumi, Satoshi; Masui, Tomomi; Mashita, Ryo; Kishimoto, Hiroyuki; Yamaguchi, Daisuke; Kumada, Takayuki; Takata, Shin-Ichi; Ohishi, Kazuki; Suzuki, Jun-Ichi

    2016-12-01

    Dynamic nuclear polarization (DNP) at low temperature (1.2 K) and high magnetic field (3.3 T) was applied to a contrast variation study in small-angle neutron scattering (SANS) focusing on industrial rubber materials. By varying the scattering contrast by DNP, time-of-flight SANS profiles were obtained at the pulsed neutron source of the Japan Proton Accelerator Research Complex (J-PARC). The concentration of a small organic molecule, (2,2,6,6-tetramethylpiperidine-1-yl)oxy (TEMPO), was carefully controlled by a doping method using vapour sorption into the rubber specimens. With the assistance of microwave irradiation (94 GHz), almost full polarization of the paramagnetic electronic spin of TEMPO was transferred to the spin state of hydrogen (protons) in the rubber materials to obtain a high proton spin polarization ( P H ). The following samples were prepared: (i) a binary mixture of styrene-butadiene random copolymer (SBR) with silica particles (SBR/SP); and (ii) a ternary mixture of SBR with silica and carbon black particles (SBR/SP/CP). For the binary mixture (SBR/SP), the intensity of SANS significantly increased or decreased while keeping its q dependence for P H = -35% or P H = 40%, respectively. The q behaviour of SANS for the SBR/SP mixture can be reproduced using the form factor of a spherical particle. The intensity at low q (∼0.01 Å -1 ) varied as a quadratic function of P H and indicated a minimum value at P H = 30%, which can be explained by the scattering contrast between SP and SBR. The scattering intensity at high q (∼0.3 Å -1 ) decreased with increasing P H , which is attributed to the incoherent scattering from hydrogen. For the ternary mixture (SBR/SP/CP), the q behaviour of SANS was varied by changing P H . At P H = -35%, the scattering maxima originating from the form factor of SP prevailed, whereas at P H = 29% and P H = 38%, the scattering maxima disappeared. After decomposition of the total SANS according to inverse matrix

  5. Contrast variation by dynamic nuclear polarization and time-of-flight small-angle neutron scattering. I. Application to industrial multi-component nanocomposites1

    Science.gov (United States)

    Noda, Yohei; Koizumi, Satoshi; Masui, Tomomi; Mashita, Ryo; Kishimoto, Hiroyuki; Yamaguchi, Daisuke; Kumada, Takayuki; Takata, Shin-ichi; Ohishi, Kazuki; Suzuki, Jun-ichi

    2016-01-01

    Dynamic nuclear polarization (DNP) at low temperature (1.2 K) and high magnetic field (3.3 T) was applied to a contrast variation study in small-angle neutron scattering (SANS) focusing on industrial rubber materials. By varying the scattering contrast by DNP, time-of-flight SANS profiles were obtained at the pulsed neutron source of the Japan Proton Accelerator Research Complex (J-PARC). The concentration of a small organic molecule, (2,2,6,6-tetramethylpiperidine-1-yl)oxy (TEMPO), was carefully controlled by a doping method using vapour sorption into the rubber specimens. With the assistance of microwave irradiation (94 GHz), almost full polarization of the paramagnetic electronic spin of TEMPO was transferred to the spin state of hydrogen (protons) in the rubber materials to obtain a high proton spin polarization (P H). The following samples were prepared: (i) a binary mixture of styrene–butadiene random copolymer (SBR) with silica particles (SBR/SP); and (ii) a ternary mixture of SBR with silica and carbon black particles (SBR/SP/CP). For the binary mixture (SBR/SP), the intensity of SANS significantly increased or decreased while keeping its q dependence for P H = −35% or P H = 40%, respectively. The q behaviour of SANS for the SBR/SP mixture can be reproduced using the form factor of a spherical particle. The intensity at low q (∼0.01 Å−1) varied as a quadratic function of P H and indicated a minimum value at P H = 30%, which can be explained by the scattering contrast between SP and SBR. The scattering intensity at high q (∼0.3 Å−1) decreased with increasing P H, which is attributed to the incoherent scattering from hydrogen. For the ternary mixture (SBR/SP/CP), the q behaviour of SANS was varied by changing P H. At P H = −35%, the scattering maxima originating from the form factor of SP prevailed, whereas at P H = 29% and P H = 38%, the scattering maxima disappeared. After decomposition of the total SANS according to inverse matrix

  6. Transmission electron microscopy investigation of neutron irradiated Si and ZrN coated UMo particles prepared using FIB

    Science.gov (United States)

    Van Renterghem, W.; Miller, B. D.; Leenaers, A.; Van den Berghe, S.; Gan, J.; Madden, J. W.; Keiser, D. D.

    2018-01-01

    Two fuel plates, containing Si and ZrN coated U-Mo fuel particles dispersed in an Al matrix, were irradiated in the BR2 reactor of SCK•CEN to a burn-up of ∼70% 235U. Five samples were prepared by INL using focused ion beam milling and transported to SCK•CEN for transmission electron microscopy (TEM) investigation. Two samples were taken from the Si coated U-Mo fuel particles at a burn-up of ∼42% and ∼66% 235U and three samples from the ZrN coated U-Mo at a burn-up of ∼42%, ∼52% and ∼66% 235U. The evolution of the coating, fuel structure, fission products and the formation of interaction layers are discussed. Both coatings appear to be an effective barrier against fuel matrix interaction and only on the samples having received the highest burn-up and power, the formation of an interaction between Al and U(Mo) can be observed on those locations where breaches in the coatings were formed during plate fabrication.

  7. Development of a novel neutron detection technique by using a boron layer coating a Charge Coupled Device

    Energy Technology Data Exchange (ETDEWEB)

    Blostein, Juan Jerónimo; Estrada, Juan; Tartaglione, Aureliano; Sofo haro, Miguel; Fernández Moroni, Guillermo; Cancelo, Gustavo

    2015-01-19

    This article describes the design features and the first test measurements obtained during the installation of a novel high resolution 2D neutron detection technique. The technique proposed in this work consists of a boron layer (enriched in ${^{10}}$B) placed on a scientific Charge Coupled Device (CCD). After the nuclear reaction ${^{10}}$B(n,$\\alpha$)${^{7}}$Li, the CCD detects the emitted charge particles thus obtaining information on the neutron absorption position. The above mentioned ionizing particles, with energies in the range 0.5-5.5 MeV, produce a plasma effect in the CCD which is recorded as a circular spot. This characteristic circular shape, as well as the relationship observed between the spot diameter and the charge collected, is used for the event recognition, allowing the discrimination of undesirable gamma events. We present the first results recently obtained with this technique, which has the potential to perform neutron tomography investigations with a spatial resolution better than that previously achieved. Numerical simulations indicate that the spatial resolution of this technique will be about 15 $\\mu$m, and the intrinsic detection efficiency for thermal neutrons will be about 3 %. We compare the proposed technique with other neutron detection techniques and analyze its advantages and disadvantages.

  8. What are the mesoscopic magnetic inhomogeneities in the dilute PdFeMn alloy? Polarized neutron study

    Energy Technology Data Exchange (ETDEWEB)

    Gordeev, G.; Axelrod, L.; Zabenkin, V.; Lazebnik, I.; Grigoriev, S.; Wagner, V.; Eckerlebe, H

    2003-07-01

    The 3D analysis of neutron depolarization was carried out for different thermomagnetic treatment of the dilute PdFeMn alloy versus temperature and magnetic field applied in magnetizing/demagnetizing cycles. Both the macroscopic magnetization and the mean fluctuation of local magnetization behavior were subtracted from experimental data. A complicated behavior of the latter was observed. The hysteresis of local magnetization fluctuations is found out but that of macroscopic magnetization is practically absent. The effort to apply the simple model for the description of magnetic inhomogeneities was made in order to understand the mesostructure of this alloy.

  9. Controllable Release of Interleukin-4 in Double-Layer Sol-Gel Coatings on TiO2 Nanotubes for Modulating Macrophage Polarization.

    Science.gov (United States)

    Li, Mengting; Gao, LIli; Chen, Junhong; Zhang, Yan; Wang, Jianxin; Lu, Xiong; Duan, Ke; Weng, Jie; Feng, Bo

    2017-10-23

    Classically activated M1 macrophages and alternatively activated M2 macrophages play key roles in regulating immune responses. M1 macrophages initiate angiogenesis in the early stages of wound healing or after implantation. However, their prolonged activation can lead to chronic inflammation. We speculated that biomedical implants with specific properties can induce a shift from M1 to M2 macrophages at a specific time point to promote tissue repair and wound healing. To investigate this possibility, drug-loaded double-layer sol-gel coatings were fabricated on TiO2 nanotubes (TNTs), which were used to modulate the switch from the M1 to the M2 phenotype by controlled release of interleukin (IL)-4. The lower sol-gel layer with IL-4 consisted of a carboxymethyl chitosan (CMCS) hydrogel, 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide, and N-hydroxysuccinimide as a crosslinker (IL4/TNT). The upper layer fabricated on the IL4/TNT sample was another type of CMCS hydrogel that used genipin (GP) as a crosslinker (GP/IL4/TNT). We found that IL-4 was released from GP/IL4/TNTs in a controlled manner, with the greatest release occurring after 72 h. GP/IL4/TNT stimulated the polarization of macrophages from the M1 to M2 phenotype after the macrophage polarization from the M0 to M1 phenotype. This provides a template for the fabrication of biomaterials that can direct macrophage polarization and stimulate tissue regeneration following the initial inflammatory response to implants. . © 2017 IOP Publishing Ltd.

  10. High Hydrogen Content Graphene Hydride Compounds & High Cross-­ Section Cladding Coatings for Fast Neutron Detection

    Energy Technology Data Exchange (ETDEWEB)

    Chandrashekhar, MVS [Univ. of South Carolina, Columbia, SC (United States)

    2017-06-21

    The objective is to develop and implement a superior low-cost, large area (potentially >32in), easily deployable, close proximity, harsh environment innovative neutron sensor needed for next generation fuel cycle monitoring. We will exploit recent breakthroughs at the PI’s lab on the electrochemistry of epitaxial graphene (EG) formed on commercial SiC wafers, a transformative nanomaterial system with superior radiation detection and durability properties to develop a new paradigm in detection for fast neutrons, a by-product of fission reactors. There are currently few effective detection/monitoring schemes, especially solid-state ones at present. This is essential for monitoring and control of future fuel cycles to make them more efficient and reliable. By exploiting these novel materials, as well as innovative hybrid SiC/EG/Cladding device architectures conceived by the team, will develop low-cost, high performance solutions to fast-neutron detection. Finally, we will also explore 3-terminal device implementations for neutron detectors with built-in electronic gain to further shrink these devices and improve their sensitivity.

  11. The effect of fast neutron irradiation on the superconducting properties of REBCO coated conductors with and without artificial pinning centers

    Science.gov (United States)

    Fischer, D. X.; Prokopec, R.; Emhofer, J.; Eisterer, M.

    2018-04-01

    Superconductors are essential components of future fusion power plants. The magnet coils responsible for producing the field required for confining the fusion plasma are exposed to considerable neutron radiation. This makes irradiation studies necessary for understanding the radiation response of the superconductor. High temperature superconductors are promising candidates as magnet coil materials. YBCO and GdBCO tapes of several manufacturers were irradiated to fast neutron fluences of up to 3.9 × 1022 m-2 in the research reactor at the Atominstitut. Low energy neutrons contribute to the fission reactor spectrum but not to the expected spectrum at the fusion magnets. Low energy neutrons have to be shielded in irradiation experiments to avoid their substantial effect on the superconducting properties of tapes containing gadolinium. The critical current (I c) of the tapes in this study was examined at fields of up to 15 T and down to a temperature of 30 K. I c first increases upon irradiation and reaches a maximum at a certain fluence, which depends highly on temperature, being highest at low temperature. I c declines at high fluences and eventually degrades with respect to its initial value. Tapes with artificial pinning centers (APCs) degrade at lower fluences than tapes without them. The n-values decrease in all types of tapes after irradiation even when the critical currents are increased. The field dependence of the volume pinning force differs in pristine tapes with and without APCs but shows the same behavior after irradiation.

  12. Development of antireflection coatings with a sup 6 LiF/ sup 6 sup 2 Ni multilayer converter for ultracold neutron detectors

    CERN Document Server

    Maier-Komor, P; Bergmaier, A; Dollinger, G; Paul, S; Schott, W

    2002-01-01

    High efficiency detectors for ultracold neutrons (UCN) are needed at the new high flux neutron source, Forschungsreaktor Muenchen II. In the development described, silicon PIN diodes were chosen to detect the alpha-particles or the tritons created in the reaction sup 6 Li(n,alpha)t. The high reflectance of UCN on sup 6 Li with its positive optical potential must be compensated by a material with negative optical potential. The isotope sup 6 sup 2 Ni was chosen for this. To avoid problems due to chemical reactions of Li with humidity, the compound sup 6 LiF was chosen. One hundred and fifty double layers of sup 6 LiF/ sup 6 sup 2 Ni had to be deposited by physical vapor deposition on silicon PIN diodes which had already been coated with 88 nm approx 77 mu g/cm sup 2 of sup 5 sup 8 Ni for reflection of the UCN. The theoretical optimal thickness of the sup 6 sup 2 Ni layers is 3 nm, and that of sup 6 LiF is 6 nm. Since expensive isotopes were involved, a small source-to-substrate distance had to be used, but wit...

  13. Non-destructive Quantitative Phase Analysis and Microstructural Characterization of Zirconium Coated U-10Mo Fuel Foils via Neutron Diffraction

    Energy Technology Data Exchange (ETDEWEB)

    Cummins, Dustin Ray [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Vogel, Sven C. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Hollis, Kendall Jon [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Brown, Donald William [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Dombrowski, David E. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2016-10-18

    This report uses neutron diffraction to investigate the crystal phase composition of uranium-molybdenum alloy foils (U-10Mo) for the CONVERT MP-1 Reactor Conversion Project, and determines the effect on alpha-uranium contamination following the deposition of a Zr metal diffusion layer by various methods: plasma spray deposition of Zr powders at LANL and hot co-rolling with Zr foils at BWXT. In summary, there is minimal decomposition of the gamma phase U-10Mo foil to alpha phase contamination following both plasma spraying and hot co-rolling. The average unit cell volume, i.e. lattice spacing, of the Zr layer can be mathematically extracted from the diffraction data; co-rolled Zr matches well with literature values of bulk Zr, while plasma sprayed Zr shows a slight increase in the lattice spacing, indicative of interstitial oxygen in the lattice. Neutron diffraction is a beneficial alternative to conventional methods of phase composition, i.e. x ray diffraction (XRD) and destructive metallography. XRD has minimal penetration depth in high atomic number materials, particularly uranium, and can only probe the first few microns of the fuel plate; neutrons pass completely through the foil, allowing for bulk analysis of the foil composition and no issues with addition of cladding layers, as in the final, aluminum-clad reactor fuel plates. Destructive metallography requires skilled technicians, cutting of the foil into small sections, hazardous etching conditions, long polishing and microscopy times, etc.; the neutron diffraction system has an automated sample loader and can fit larger foils, so there is minimal analysis preparation; the total spectrum acquisition time is ~ 1 hour per sample. The neutron diffraction results are limited by spectra refinement/calculation times and the availability of the neutron beam source. In the case of LANSCE at Los Alamos, the beam operates ~50% of the year. Following the lessons learned from these preliminary results, optimizations to

  14. Effect of surfactant excess on the stability of low-polarity ferrofluids probed by small-angle neutron scattering

    Energy Technology Data Exchange (ETDEWEB)

    Petrenko, V. I., E-mail: vip@nf.jinr.ru; Avdeev, M. V. [Joint Institute for Nuclear Research (Russian Federation); Bulavin, L. A. [Taras Shevchenko National University of Kyiv (Ukraine); Almasy, L. [Hungarian Academy of Science, Wigner Research Centre for Physics (Hungary); Grigoryeva, N. A. [St. Petersburg State University (Russian Federation); Aksenov, V. L. [National Research Centre “Kurchatov Institute”, Konstantinov Petersburg Nuclear Physics Institute (Russian Federation)

    2016-01-15

    The structures of ferrofluids (FFs) based on nonpolar solvent decahydronaphthalene, stabilized by saturated monocarboxylic acids with hydrocarbon chains of different lengths, C16 (palmitic acid) and ?12 (lauric acid), with an excess of acid molecules, have been studied by small-angle neutron scattering. It is found that the addition of acid to an initially stable system with optimal composition leads to more significant structural changes (related to aggregation) than those observed previously for this class of FFs. A comparison of the influence of monocarboxylic acids on the stability of nonpolar FFs suggests that the enhancement of aggregation is much more pronounced in the case of palmitic acid excess. This fact confirms the conclusion of previous studies, according to which an increase in the hydrocarbon chain length in a saturated acid reduces the efficiency of the corresponding FF stabilization.

  15. Advances in neutron tomography

    Indian Academy of Sciences (India)

    much improved test experiments using polarized neutrons for radiographic imaging. For this purpose the CONRAD instrument of the HMI was equipped with polarizing and analysing benders very similar to conventional scattering experiments using polarized neu- trons. Magnetic fields in different coils and in samples ...

  16. Study of the nuclear structure far from stability: Coulomb excitation of neutron-rich Rb isotopes around N=60; Production of nuclear spin polarized beams using the tilted foils technique

    International Nuclear Information System (INIS)

    Sotty, C.

    2013-01-01

    The underlying structure in the region A ∼ 100, N ∼ 60 has been under intensive and extensive investigation, mainly by β-decay and γ-ray spectroscopy from fission processes. Around N ∼ 60, by adding just few neutrons, protons a rapid shape change occurs from spherical-like to well deformed g.s. shape. Shape coexistence has been observed in the Sr and Zr nuclei, and is expected to take place in the whole region. The mechanisms involved in the appearance of the deformation is not well understood. The interplay between down-sloping and up-sloping neutron Nilsson orbital is evoked as one of the main reasons for the sudden shape change. However, a clear identification of the active proton and neutron orbitals was still on-going. For that purpose, the neutron rich 93;95;97;99 Rb isotopes have been studied by Coulomb excitation at CERN (ISOLDE) using the REX-ISOLDE post-accelerator and the MINIBALL setup. The completely unknown structures of 97;99 Rb have been populated and observed. Prompt γ-ray coincidences of low-lying states have been observed and time-correlated in order to build level schemes. The associated transition strengths have been extracted with the GOSIA code. The observed matrix elements of the electromagnetic operator constituted new inputs of further theoretical calculations giving new insight on the involved orbitals. The sensitivity of such experiment can be increased using nuclear spin polarized radioactive ion beam. For that purpose the Tilted Foils Technique (TFT) of polarization has been investigated at CERN. This technique consists to spin polarize the ion beam, passing through thin foils tilted at an oblique angle with respect to the beam direction. The initially obtained atomic polarization is transferred to the nucleus by hyperfine interaction. This technique does not depend on the chemical nature of the element. Short lived nuclei can be polarized in-flight without any need to be stopped in a catcher. It opens up the possibility to

  17. Dual-inflammatory cytokines on TiO2nanotube-coated surfaces used for regulating macrophage polarization in bone implants.

    Science.gov (United States)

    Gao, Lili; Li, Mengting; Yin, Lu; Zhao, Chanjuan; Chen, Junhong; Zhou, Jie; Duan, Ke; Feng, Bo

    2018-03-10

    Excessive immune responses following the use of implantable, biomaterial-based medical devices represent a substantial challenge for treatment efficacy and patient well-being. Specifically, after implantation, pro-inflammatory M1 macrophages are activated by cytokines such as interferon-γ (IFN-γ) followed by anti-inflammatory M2 macrophages polarized by cytokines including interleukin-4 (IL-4), leading to healing and long-term stability of implants. Here, we report the loading of an immunomodulatory cytokine,IL-4, into TiO 2 nanotubes (TNTs) followed by hydrogel coating on the TNTs for subsequent release of IL-4. Finally, IFN-γ was added onto the gel layer to effect rapid release. The release rates of both cytokines from the samples were monitored using an immersion test in phosphate-buffered solution. The cytocompatibility of the sample was evaluated using cultures of osteoblasts and macrophages. Macrophage phenotype switching in vitro was examined via cytokine secretion and gene expression analyses. In vitro testing showed that the sample could stimulate macrophage polarization from the M1 to M2 phenotype at the desired period owing to temporal release of IFN-γ and IL-4. Another biomaterial containing only IL-4 in TNTs was also able to modulate the transformation of M1 to M2 although with weaker effect than that containing IFN-γ and IL-4. The biomaterial may be useful as an osteoimplant in vivo owing to the inflammation caused by a wound or implantation. This study provided biomaterials capable of facilitating smooth M1 to M2 macrophages switching, which might be helpful to research immune responses of tissues to implants and will likely contribute to the development of bone substitute materials. © 2018 Wiley Periodicals, Inc. J Biomed Mater Res Part A, 2018. © 2018 Wiley Periodicals, Inc.

  18. Studies on optical pumping cells (OPC) to polarize 3He

    International Nuclear Information System (INIS)

    Hutanu, V.; Rupp, A.

    2004-01-01

    The technique applied at HMI to obtain nuclear-spin-polarized 3 He, used in neutron spin filters (NSFs), is metastability-exchange optical pumping. To prepare efficient NSF, one must highly polarize 3 He nuclei in the optical pumping volume (OPV) and reduce the polarization losses during the compression phase. Great progress has been achieved in reducing of depolarization due to the recent development of both, large polarization preserving piston compressors and long relaxation time filter cells. It is even more important to significantly enhance the 3 He polarization rate during optical pumping in order to increase NSF efficiency. Different cells materials were tested, such as Duran and quartz glass. In order to use the laser light more efficiently and to decrease the risk of 3 He depolarization due to unfavorable reflections, antireflection (AR) coatings were used on cell windows made of quartz glass. They were compared with the ones without coating, made of quartz, Duran and BK7 glass. The comparison of various techniques to mount the windows such as blowing, gluing or molecular diffusion was also conducted. It indicated that the molecular diffusion is the most suitable technique because of a better purity of the gas in the cell and the preservation of the optical flatness of the windows. Cells, for practical reasons each entirely made from the same material (Duran, Quartz glass) with windows mounted using this method, showed the best polarization performance

  19. A novel stir bar sorptive extraction coating based on monolithic material for apolar, polar organic compounds and heavy metal ions.

    Science.gov (United States)

    Huang, Xiaojia; Qiu, Ningning; Yuan, Dongxing; Huang, Benli

    2009-04-15

    In this study, a novel stir bar sorptive extraction (SBSE) based on monolithic material (SBSEM) was prepared. The monolithic material was obtained by in situ copolymerization of vinylpyrrolidone and divinylbenzene in the presence of a porogen solvent containing cyclohexanol and 1-dodecanol with azobisisobutyronitrile as initiator. The influences of polymerization conditions on the extraction efficiencies were investigated, using phenol and p-nitrophenol as detected solutes. The monolithic material was characterized by various techniques, such as elemental analysis, scanning electron microscopy, mercury intrusion porosimetry, infrared spectroscopy. Polycyclic aromatic hydrocarbons were used to investigate the extraction efficiencies of SBSEM for apolar analytes. Hormones, aromatic amines and phenols were selected as test analytes to investigate the extraction efficiencies of SBSEM for weakly and strongly polar compounds. The results showed that the new SBSEM could enrich the above-mentioned organic compounds effectively. It is worthy to mention that the SBSEM can enrich some heavy metal ions, such as Cu(2+), Pb(2+), Cr(3+) and Cd(2+), through coordination adsorption. To our best knowledge, that is the first to use SBSE to enrich heavy metal ions.

  20. Precision neutron polarimetry for neutron beta decay

    Energy Technology Data Exchange (ETDEWEB)

    Penttila, S. I. (Seppo I.); Bowman, J. D. (J. David)

    2004-01-01

    The abBA collaboration is developing a new type of field-expansion spectrometer for measurement of the three correlation coefficients a, A, and B and shape parameter b. The measurement of A and B requires precision neutron polarimetry. We will polarize a pulsed cold neutron beam from SNS using a {sup 3}He neutron spin filter. The well-known polarizing cross section for n-{sup 3}He has 1/v dependence, which is used to determine the absolute beam polarization through a time-of-flight (TOF) measurement. We show that measuring the TOF dependence of A and B, the coefficients and the neutron polarization can be determined with small loss of statistical precision and negligible systematic error. We conclude that it is possible to determine the neutron polarization averaged over a run in the neutron beta decay experiment to better than 10{sup -3}. We discuss various sources of systematic uncertainties in the measurement of A and B and conclude that they are less than 10{sup -4}.

  1. Precision neutron polarimetry for neutron beta decay

    International Nuclear Information System (INIS)

    Penttila, S.I.; Bowman, J.D.

    2004-01-01

    The abBA collaboration is developing a new type of field-expansion spectrometer for measurement of the three correlation coefficients a, A, and B and shape parameter b. The measurement of A and B requires precision neutron polarimetry. We will polarize a pulsed cold neutron beam from SNS using a 3 He neutron spin filter. The well-known polarizing cross section for n- 3 He has 1/v dependence, which is used to determine the absolute beam polarization through a time-of-flight (TOF) measurement. We show that measuring the TOF dependence of A and B, the coefficients and the neutron polarization can be determined with small loss of statistical precision and negligible systematic error. We conclude that it is possible to determine the neutron polarization averaged over a run in the neutron beta decay experiment to better than 10 -3 . We discuss various sources of systematic uncertainties in the measurement of A and B and conclude that they are less than 10 -4 .

  2. NUCLEON POLARIZATION IN 3-BODY MODELS OF POLARIZED LI-6

    NARCIS (Netherlands)

    SCHELLINGERHOUT, NW; KOK, LP; COON, SA; ADAM, RM

    1993-01-01

    Just as He-3 --> can be approximately characterized as a polarized neutron target, polarized Li-6D has been advocated as a good isoscalar nuclear target for the extraction of the polarized gluon content of the nucleon. The original argument rests upon a presumed ''alpha + deuteron'' picture of Li-6,

  3. Measurements of the neutron electric to magnetic form-factor ratio G(En) / G(Mn) via the H-2(polarized-e, e-prime,polarized-n)H-1 reaction to Q**2 = 1.45-(GeV/c)**2

    Energy Technology Data Exchange (ETDEWEB)

    Bradley Plaster; A.Yu. Semenov; A. Aghalaryan; Erick Crouse; Glen MacLachlan; Shigeyuki Tajima; William Tireman; Abdellah Ahmidouch; Brian Anderson; Hartmuth Arenhovel; Razmik Asaturyan; O. Baker; Alan Baldwin; David Barkhuff; Herbert Breuer; Roger Carlini; Michael Christy; Steve Churchwell; Leon Cole; Samuel Danagoulian; Donal Day; T. Eden; Mostafa Elaasar; Rolf Ent; Manouchehr Farkhondeh; Howard Fenker; John Finn; Liping Gan; Ashot Gasparian; Kenneth Garrow; Paul Gueye; Calvin Howell; Bitao Hu; Mark Jones; James Kelly; Cynthia Keppel; Mahbubul Khandaker; Wooyoung Kim; Stanley Kowalski; Allison Lung; David Mack; Richard Madey; D. Manley; Pete Markowitz; Joseph Mitchell; Hamlet Mkrtchyan; Allena Opper; Charles Perdrisat; Vina Punjabi; Brian Raue; Tilmann Reichelt; Joerg Reinhold; Julie Roche; Yoshinori Sato; Nikolai Savvinov; Irina Semenova; Wonick Seo; Neven Simicevic; Gregory Smith; Stepan Stepanyan; Vardan Tadevosyan; Liguang Tang; Shawn Taylor; Paul Ulmer; William Vulcan; John Watson; Steven Wells; Frank Wesselmann; Stephen Wood; Seunghoon Yang; Lulin Yuan; Wei-Ming Zhang; Hong Guo Zhu; Xiaofeng Zhu

    2006-02-01

    We report values for the neutron electric to magnetic form factor ratio, G{sub En}/G{sub Mn}, deduced from measurements of the neutron's recoil polarization in the quasielastic {sup 2}H({rvec e}, e{prime}{rvec n}) {sup 1}H reaction, at three Q{sup 2} values of 0.45, 1.13, and 1.45 (GeV/c){sup 2}. The data at Q{sup 2} = 1.13 and 1.45 (GeV/c){sup 2} are the first direct experimental measurements of GEn employing polarization degrees of freedom in the Q{sup 2} > 1 (GeV/c){sup 2} region and stand as the most precise determinations of GEn for all values of Q{sup 2}.

  4. Neutron scattering. Experiment manuals

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2010-07-01

    The following topics are dealt with: The thermal triple axis spectrometer PUMA, the high-resolution powder diffractometer SPODI, the hot single-crystal diffractometer HEiDi for structure analysis with neutrons, the backscattering spectrometer SPHERES, neutron polarization analysis with tht time-of-flight spectrometer DNS, the neutron spin-echo spectrometer J-NSE, small-angle neutron scattering with the KWS-1 and KWS-2 diffractometers, the very-small-angle neutron scattering diffractrometer with focusing mirror KWS-3, the resonance spin-echo spectrometer RESEDA, the reflectometer TREFF, the time-of-flight spectrometer TOFTOF. (HSI)

  5. Neutron scattering. Experiment manuals

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2010-01-01

    The following topics are dealt with: The thermal triple axis spectrometer PUMA, the high-resolution powder diffractometer SPODI, the hot single-crystal diffractometer HEiDi for structure analysis with neutrons, the backscattering spectrometer SPHERES, neutron polarization analysis with tht time-of-flight spectrometer DNS, the neutron spin-echo spectrometer J-NSE, small-angle neutron scattering with the KWS-1 and KWS-2 diffractometers, the very-small-angle neutron scattering diffractrometer with focusing mirror KWS-3, the resonance spin-echo spectrometer RESEDA, the reflectometer TREFF, the time-of-flight spectrometer TOFTOF. (HSI)

  6. Neutron scattering. Experiment manuals

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2012-01-01

    The following topics are dealt with: The thermal triple-axis spectrometer PUMA, the high-resolution powder diffractometer SPODI, the hot single-crystal diffractometer HEiDi for structure analysis with neutrons, the backscattering spectrometer SPHERES, the neutron polarization analyzer DNS, the neutron spin-echo spectrometer J-NSE, the small-angle neutron diffractometers KWS-1/-2, the very-small-angle neutron diffractometer with focusing mirror KWS-3, the resonance spin-echo spectrometer RESEDA, the reflectometer TREFF, the time-of-flight spectrometer TOFTOF. (HSI)

  7. Gradual Localization of 5f States in Orthorhombic UTX Ferromagnets:Polarized Neutron Diffraction Study of Ru Substituted UCoGe

    Science.gov (United States)

    Vališka, Michal; Pospíšil, Jiří; Stunault, Anne; Takeda, Yukiharu; Gillon, Béatrice; Haga, Yoshinori; Prokeš, Karel; Abd-Elmeguid, Mohsen M.; Nénert, Gwilherm; Okane, Tetsuo; Yamagami, Hiroshi; Chapon, Laurent; Gukasov, Arsene; Cousson, Alain; Yamamoto, Etsuji; Sechovský, Vladimír

    2015-08-01

    We report on a microscopic study of the evolution of ferromagnetism in the Ru substituted ferromagnetic superconductor (FM SC) UCoGe crystallizing in the orthorhombic TiNiSi-type structure. For that purpose, two single crystals with composition UCo0.97Ru0.03Ge and UCo0.88Ru0.12Ge have been prepared and characterized by magnetization, AC susceptibility, specific heat and electrical resistivity measurements. Both compounds have been found to order ferromagnetically below TC = 6.5 and 7.5 K, respectively, which is considerably higher than the TC = 3 K of the parent compound UCoGe. The higher values of TC are accompanied by enhanced values of the spontaneous moment μspont = 0.11 μB/f.u. and μspont = 0.21 μB/f.u., respectively in comparison to the tiny spontaneous moment of UCoGe (about 0.07 μB/f.u.). No sign of superconductivity was detected in either compound. The magnetic moments of the samples were investigated on the microscopic scale using polarized neutron diffraction (PND) and for UCo0.88Ru0.12Ge also by soft X-ray magnetic circular dichroism (XMCD). The analysis of the PND results indicates that the observed enhancement of ferromagnetism is mainly due to the growth of the orbital part of the uranium 5f moment μ LU, reflecting a gradual localization of the 5f electrons with Ru substitution. In addition, the parallel orientation of the U and Co moments has been established in both substituted compounds. The results are discussed and compared with related isostructural ferromagnetic UTX compounds (T: transition metals, X: Si, Ge) in the context of a varying degree of the 5f-ligand hybridization.

  8. Coated ceramic breeder materials

    Science.gov (United States)

    Tam, Shiu-Wing; Johnson, Carl E.

    1987-01-01

    A breeder material for use in a breeder blanket of a nuclear reactor is disclosed. The breeder material comprises a core material of lithium containing ceramic particles which has been coated with a neutron multiplier such as Be or BeO, which coating has a higher thermal conductivity than the core material.

  9. Niobium pentoxide coating replacing zinc phosphate coating

    OpenAIRE

    RODRIGUES, P.R.P.; TERADA, M.; JUNIOR, O.R.A.; LOPES, A.C.; COSTA, I.; BANCZEK, E.P.

    2015-01-01

    A new coating made of niobium pentoxide, obtained through the sol-gel process, was developed for the carbon steel (SAE 1010). The corrosion protection provided by this coating was evaluated through electrochemical tests such as: open circuit potential, electrochemical impedance spectroscopy and anodic potentiodynamic polarization in NaCl 0,5 mol L-1 solution. The morphology and composition of the coatings were analyzed using scanning electronic microscopy, energy dispersive spectroscopy and X...

  10. Probing lateral magnetic nanostructures by polarized GISANS

    International Nuclear Information System (INIS)

    Kentzinger, E.; Frielinghaus, H.; Ruecker, U.; Ioffe, A.; Richter, D.; Brueckel, Th.

    2007-01-01

    While structural and magnetic lateral correlations in thin film materials can be investigated at the μm length scale by neutron off-specular scattering (OSS) with polarization analysis, they can also be investigated at the nm length scale by grazing incidence small-angle scattering of polarized neutrons (polarized GISANS). We exemplify this issue showing a combined OSS and GISANS study of the lateral correlations in a remanent polarizing supermirror

  11. Probing lateral magnetic nanostructures by polarized GISANS

    Science.gov (United States)

    Kentzinger, E.; Frielinghaus, H.; Rücker, U.; Ioffe, A.; Richter, D.; Brückel, Th.

    2007-07-01

    While structural and magnetic lateral correlations in thin film materials can be investigated at the μm length scale by neutron off-specular scattering (OSS) with polarization analysis, they can also be investigated at the nm length scale by grazing incidence small-angle scattering of polarized neutrons (polarized GISANS). We exemplify this issue showing a combined OSS and GISANS study of the lateral correlations in a remanent polarizing supermirror.

  12. Dynamics in γ-Fe2O3 nanoparticles studied by time-of-flight polarized neutron scattering

    DEFF Research Database (Denmark)

    Kuhn, L.T.; Lefmann, K.; Klausen, S.N.

    2004-01-01

    The inelastic neutron-scattering signal from magnetic nanoparticles contains information on magnetic dynamics like superparamagnetic relaxation and collective magnetic excitations. Often another, very broad quasi-elastic component is observed in addition. We have studied this quasi-elastic neutron...

  13. Small-angle neutron scattering studies of mineralization on BSA coated citrate capped gold nanoparticles used as a model surface for membrane scaling in RO wastewater desalination.

    Science.gov (United States)

    Dahdal, Y N; Pipich, V; Rapaport, H; Oren, Y; Kasher, R; Schwahn, D

    2014-12-23

    Bovine serum albumin (BSA) coated on citrate capped gold nanoparticles (BSA-GNPs) was exposed to a simulated wastewater effluent (SSE) in order to study the mineralization and thereby mimic scaling at biofouled membranes of reverse osmosis (RO) wastewater desalination plants. RO is a leading technology of achieving freshwater quality as it has the capability of removing both dissolved inorganic salts and organic contaminants from tertiary wastewater effluents. The aim was to better understand one of the major problems facing this technology which is fouling of the membranes, mainly biofouling and scaling by calcium phosphate. The experiments were performed using the small-angle neutron scattering (SANS) technique. The nanoparticles, GNPs, stabilized by the citrate groups showed 30 Å large particles having a homogeneous distribution of gold and citrate with a gold volume fraction of the order of 1%. On the average two BSA monomers are grafted at 2.4 GNPs. The exposed BSA-GNPs to SSE solution led to immediate mineralization of stable composite particles of the order of 0.2 μm diameter and a mineral volume fraction between 50% and 80%. The volume fraction of the mineral was of the order of 10(-5), which is roughly 3 times larger but an order of magnitude smaller than the maximum possible contents of respectively calcium phosphate and calcium carbonate in the SSE solution. Considering the extreme low solubility product of calcium phosphate, we suggest total calcium phosphate and partially (5-10%) calcium carbonate formation in the presence of BSA-GNPs.

  14. A slow neutron polarimeter for the measurement of parity-odd neutron rotary power

    Energy Technology Data Exchange (ETDEWEB)

    Snow, W. M.; Anderson, E.; Bass, T. D.; Dawkins, J. M.; Fry, J.; Haddock, C.; Horton, J. C.; Luo, D.; Micherdzinska, A. M.; Walbridge, S. B. [Indiana University and Center for the Exploration of Energy and Matter, 2401 Milo B. Sampson Lane, Bloomington, Indiana 47408 (United States); Barrón-Palos, L.; Maldonado-Velázquez, M. [Instituto de Física, Universidad Nacional Autónoma de México, Ciudad de México, D.F. 04510, México (Mexico); Bass, C. D. [LeMoyne College, 1419 Salt Springs Road, Syracuse, New York 13214 (United States); Crawford, B. E. [Gettysburg College, 300 North Washington Street, Gettysburg, Pennsylvania 17325 (United States); Crawford, C. [University of Kentucky, 177 Chem.-Phys. Building, 505 Rose Street, Lexington, Kentucky 40506-0055 (United States); Esposito, D. [University of Dayton, 300 College Park, Dayton, Ohio 45469 (United States); Gardiner, H. [Louisiana State University, Baton Rouge, Louisiana 70803 (United States); Gan, K. [The George Washington University, 2121 I Street N.W., Washington, District of Columbia 20052 (United States); Heckel, B. R.; Swanson, H. E., E-mail: swanson@npl.washington.edu [University of Washington/Center for Experimental Nuclear Physics and Astrophysics, Box 354290, Seattle, Washington 98195 (United States); and others

    2015-05-15

    We present the design, description, calibration procedure, and an analysis of systematic effects for an apparatus designed to measure the rotation of the plane of polarization of a transversely polarized slow neutron beam as it passes through unpolarized matter. This device is the neutron optical equivalent of a crossed polarizer/analyzer pair familiar from light optics. This apparatus has been used to search for parity violation in the interaction of polarized slow neutrons in matter. Given the brightness of existing slow neutron sources, this apparatus is capable of measuring a neutron rotary power of dϕ/dz = 1 × 10{sup −7} rad/m.

  15. Polarized advanced fuel reactors

    International Nuclear Information System (INIS)

    Kulsrud, R.M.

    1987-07-01

    The d- 3 He reaction has the same spin dependence as the d-t reaction. It produces no neutrons, so that if the d-d reactivity could be reduced, it would lead to a neutron-lean reactor. The current understanding of the possible suppression of the d-d reactivity by spin polarization is discussed. The question as to whether a suppression is possible is still unresolved. Other advanced fuel reactions are briefly discussed. 11 refs

  16. The use of neutron diffraction for the determination of the in-depth residual stresses profile in weld coatings; A utilizacao da difracao de neutroes na determinacao do perfil de tensoes residuais em revestimentos por soldadura

    Energy Technology Data Exchange (ETDEWEB)

    Marques, Maria Jose; Batista, A.C.; Nobre, J.P. [Universidade de Coimbra (Portugal). Dept. de Fisica. Centro de Estudos de Materiais por Difraccao de Raios X (CEMDRX); Loureiro, Altino [Universidade de Coimbra (Portugal). Dept. de Engenharia Mecanica. Centro de Engenharia Mecanica (CEMUC); Kornmeier, Joana R., E-mail: mjvaz@fe.up.pt [Technische Universitaet Muenchen, Garching (Germany). FRM II

    2013-04-15

    The neutron diffraction is a non-destructive technique, particularly suitable for the analysis of residual stress fields in welds. The technique is used in this article to study ferritic samples, coated by submerged arc welding using stainless steel filler metals. This procedure is often used for manufacturing process equipment for chemical and nuclear industries, for ease of implementation and economic reasons. The main disadvantage of that processes is the cracking phenomenon that often occurs at the interface between the base material and coatings, which can be minimized by performing post-weld stress relief heat treatments. The samples analyzed in this study were made of carbon steel plates, coated by submerged arc welding two types of stainless steel filler metals. For the first layer was used one EN 12 072 - S 2 U 23 12 electrode, while for the second and third layers were used an EN 12 072 - 19 12 3 S L electrode. After cladding, the samples were submitted to a post-weld heat treatment for 1 hour at 620 deg C. The residual stress profiles obtained by neutron diffraction evidence the relaxation of residual stress given by the heat treatment. (author)

  17. Neutron scattering. Experiment manuals

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2014-01-01

    The following topics are dealt with: The thermal triple-axis spectrometer PUMA, the high-resolution powder diffractometer SPODI, the hot-single-crystal diffractometer HEiDi, the three-axis spectrometer PANDA, the backscattering spectrometer SPHERES, the DNS neutron-polarization analysis, the neutron spin-echo spectrometer J-NSE, small-angle neutron scattering at KWS-1 and KWS-2, a very-small-angle neutron scattering diffractometer with focusing mirror, the reflectometer TREFF, the time-of-flight spectrometer TOFTOF. (HSI)

  18. Neutron scattering. Experiment manuals

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2014-07-01

    The following topics are dealt with: The thermal triple-axis spectrometer PUMA, the high-resolution powder diffractometer SPODI, the hot-single-crystal diffractometer HEiDi, the three-axis spectrometer PANDA, the backscattering spectrometer SPHERES, the DNS neutron-polarization analysis, the neutron spin-echo spectrometer J-NSE, small-angle neutron scattering at KWS-1 and KWS-2, a very-small-angle neutron scattering diffractometer with focusing mirror, the reflectometer TREFF, the time-of-flight spectrometer TOFTOF. (HSI)

  19. Dynamic nuclear spin polarization

    Energy Technology Data Exchange (ETDEWEB)

    Stuhrmann, H.B. [GKSS-Forschungszentrum Geesthacht GmbH (Germany)

    1996-11-01

    Polarized neutron scattering from dynamic polarized targets has been applied to various hydrogenous materials at different laboratories. In situ structures of macromolecular components have been determined by nuclear spin contrast variation with an unprecedented precision. The experiments of selective nuclear spin depolarisation not only opened a new dimension to structural studies but also revealed phenomena related to propagation of nuclear spin polarization and the interplay of nuclear polarisation with the electronic spin system. The observation of electron spin label dependent nuclear spin polarisation domains by NMR and polarized neutron scattering opens a way to generalize the method of nuclear spin contrast variation and most importantly it avoids precontrasting by specific deuteration. It also likely might tell us more about the mechanism of dynamic nuclear spin polarisation. (author) 4 figs., refs.

  20. Neutron physics

    International Nuclear Information System (INIS)

    Beckurts, K.H.; Wirtz, K.

    1974-01-01

    This textbook consists of four sections which deal with the following subjects: 1. Production of neutrons and their interactions with the nuclei; neutron sources; neutron detectors; cross-section measurements. 2. Theory of neutron interactions with macroscopic media; neutron slowing down; space distribution of moderated neutrons; neutron thermalization; neutron scattering. 3. Radioactive probe measurements of thermal neutron fluxes; activation by means of epithermal neutrons; threshold detectors of fast neutrons; neutron calibration. 4. Neutron energy; slowing down kernels; neutron age; diffusion length and absorption of neutrons

  1. Bare and thin-film-coated substrates with null reflection for p- and s-polarized light at the same angle of incidence: reflectance and ellipsometric parameters as functions of substrate refractive index and film thickness.

    Science.gov (United States)

    Azzam, R M A

    2016-10-20

    Intensity reflectances and ellipsometric parameters of a partially clad transparent substrate that suppresses the reflection of incident p- and s-polarized light at the same angle of incidence from uncoated and single-layer-coated areas are determined as functions of normalized film thickness ς and substrate refractive index n2. The common polarizing angle is the Brewster angle of the ambient-substrate interface, and the light beam incident from the ambient (air or vacuum) is refracted in the film at a 45° angle from the normal to the parallel-plane film boundaries. For n2≤2, the differential reflection phase shift Δ=δp-δs≈±90° for all values of ς so that the Brewster angle is also approximately the principal angle of the film-substrate system independent of film thickness. Accurate techniques for monitoring the deposition of such films are also proposed.

  2. Fast neutron spectrometry and dosimetry

    International Nuclear Information System (INIS)

    Blaize, S.; Ailloud, J.; Mariani, J.; Millot, J.P.

    1958-01-01

    We have studied fast neutron spectrometry and dosimetry through the recoil protons they produce in hydrogenated samples. In spectrometric, we used nuclear emulsions, in dosimetric, we used polyethylene coated with zinc sulphide and placed before a photomultiplier. (author) [fr

  3. Hydrogen Distribution in the Lunar Polar Regions

    Science.gov (United States)

    Sanin, A. B.; Mitrofanov, I. G.; Litvak, M. L.; Bakhtin, B. N.; Bodnarik, J. G.; Boynton, W. V.; Chin, G.; Evans, L. G.; Harshmann, K.; Fedosov, F.; hide

    2016-01-01

    We present a method of conversion of the lunar neutron counting rate measured by the Lunar Reconnaissance Orbiter (LRO) Lunar Exploration Neutron Detector (LEND) instrument collimated neutron detectors, to water equivalent hydrogen (WEH) in the top approximately 1 m layer of lunar regolith. Polar maps of the Moon’s inferred hydrogen abundance are presented and discussed.

  4. Measurement of inclusive quasielastic scattering of polarized electrons from polarized 3He

    International Nuclear Information System (INIS)

    Woodward, C.E.; Beise, E.J.; Belz, J.E.; Carr, R.W.; Filippone, B.W.; Lorenzon, W.B.; McKeown, R.D.; Mueller, B.; O'Neill, T.G.; Dodson, G.; Dow, K.; Farkhondeh, M.; Kowalski, S.; Lee, K.; Makins, N.; Milner, R.; Thompson, A.; Tieger, D.; van den Brand, J.; Young, A.; Yu, X.; Zumbro, J.

    1990-01-01

    We report a measurement of the asymmetry in spin-dependent quasielastic scattering of longitudinally polarized electrons from a polarized 3 He gas target. This measurement represents the first demonstration of a new method for studying electromagnetic nuclear structure: the scattering of polarized electrons from a polarized nuclear target. The measured asymmetry is in good agreement with a Faddeev calculation and supports the picture of spin-dependent quasielastic scattering from polarized 3 He as predominantly scattering from a polarized neutron

  5. Parity-nonconserving cold neutron-parahydrogen interactions

    Science.gov (United States)

    Partanen, T. M.

    2012-12-01

    Three pion-dominated observables of the parity-nonconserving interactions between the cold neutrons and parahydrogen are calculated. The transversely polarized neutron spin rotation, unpolarized neutron longitudinal polarization, and photon asymmetry of the radiative polarized neutron capture are considered. For the numerical evaluation of the observables, the strong interactions are taken into account by the Reid93 potential and the parity-nonconserving interactions by the DDH and EFT models including two different EFT parity-nonconserving two-pion exchange potentials.

  6. Optically polarized 3He

    Science.gov (United States)

    Gentile, T. R.; Nacher, P. J.; Saam, B.; Walker, T. G.

    2018-01-01

    This article reviews the physics and technology of producing large quantities of highly spin-polarized 3He nuclei using spin-exchange (SEOP) and metastability-exchange (MEOP) optical pumping. Both technical developments and deeper understanding of the physical processes involved have led to substantial improvements in the capabilities of both methods. For SEOP, the use of spectrally narrowed lasers and K-Rb mixtures has substantially increased the achievable polarization and polarizing rate. For MEOP nearly lossless compression allows for rapid production of polarized 3He and operation in high magnetic fields has likewise significantly increased the pressure at which this method can be performed, and revealed new phenomena. Both methods have benefitted from development of storage methods that allow for spin-relaxation times of hundreds of hours, and specialized precision methods for polarimetry. SEOP and MEOP are now widely applied for spin-polarized targets, neutron spin filters, magnetic resonance imaging, and precision measurements. PMID:29503479

  7. Optically polarized 3He

    Science.gov (United States)

    Gentile, T. R.; Nacher, P. J.; Saam, B.; Walker, T. G.

    2017-10-01

    This article reviews the physics and technology of producing large quantities of highly spin-polarized 3He nuclei using spin-exchange (SEOP) and metastability-exchange (MEOP) optical pumping. Both technical developments and deeper understanding of the physical processes involved have led to substantial improvements in the capabilities of both methods. For SEOP, the use of spectrally narrowed lasers and K-Rb mixtures has substantially increased the achievable polarization and polarizing rate. For MEOP nearly lossless compression allows for rapid production of polarized 3He and operation in high magnetic fields has likewise significantly increased the pressure at which this method can be performed, and revealed new phenomena. Both methods have benefitted from development of storage methods that allow for spin-relaxation times of hundreds of hours, and specialized precision methods for polarimetry. SEOP and MEOP are now widely applied for spin-polarized targets, neutron spin filters, magnetic resonance imaging, and precision measurements.

  8. Magnetic properties of UNi.sub. 2/3./sub. Rh.sub.13./sub. Al single crystal probed by polarized neutron diffraction

    Czech Academy of Sciences Publication Activity Database

    Prokeš, K.; Gukasov, A.; Sechovský, V.; Andreev, Alexander V.

    272-276, - (2004), e67-e69 ISSN 0304-8853 Institutional research plan: CEZ:AV0Z1010914 Keywords : magnetic structure determination * neutron diffraction * fied induced ferromagnetic order * UNi 2/3 Rh 1/3 Al * magnetic frustration Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 1.031, year: 2004

  9. Neutron scattering by Dirac multipoles

    OpenAIRE

    Lovesey, S. W.; Khalyavin, D. D.

    2016-01-01

    Ordered magnetic charge created by Dirac multipoles that are magnetic and polar is examined. It has previously been revealed in the pseudo-gap phase of high-Tc materials by use of the Kerr effect and magnetic neutron Bragg diffraction. There are several forms of the polar operator for magnetic neutron scattering built from spin and electric dipole operators of unpaired electrons. Construction of Dirac quadrupoles that emerge from centrosymmetric sites used by Cu ions in the ceramic supercondu...

  10. Polarized neutron reflectometry study on BiFeO3/Co0.9Fe0.1 heterostructures: enhanced magnetization in BiFeO3 and strong magnetic coupling at interface

    Science.gov (United States)

    Wang, Qiang; Gao, Ya; Ramesh, Ramamoorthy; Fitzsimmons, Michael

    2015-03-01

    Polarized neutron reflectometry (PNR) quantified the uncompensated magnetization occurring throughout the thickness of a BiFeO3 (BFO)/ Co0.9Fe0.1 (CoFe) heterostructures. The net uncompensated magnetization (1.0 μB/Fe) within BFO layer is much larger than that which has been theoretically predicted (0.1 μB/Fe) due to the Dzyaloshinskii-Moriya (DM) type interaction. The field dependent study indicates strong interfacial coupling between BFO and CoFe which extends into CoFe layer within about 1 nm interfacial region. The study also suggests the uncompensated magnetization in the BFO layer has relatively small anisotropy.

  11. Polarization Optics

    OpenAIRE

    Fressengeas, Nicolas

    2010-01-01

    The physics of polarization optics *Polarized light propagation *Partially polarized light; DEA; After a brief introduction to polarization optics, this lecture reviews the basic formalisms for dealing with it: Jones Calculus for totally polarized light and Stokes parameters associated to Mueller Calculus for partially polarized light.

  12. A large angle cold neutron bender using sequential garland reflections for pulsed neutron source

    International Nuclear Information System (INIS)

    Ebisawa, T.; Tasaki, S.; Soyama, K.; Suzuki, J.

    2001-01-01

    We discuss a basic structure and performance of a new cold neutron bender using sequential garland reflections, in order to bend a neutron beam with large divergence by large angle. Using this bender for a pulsed neutron source we could not only avoid the frame overlap for cold neutrons but also install a plural spectrometers at a cold guide and obtain polarized neutron beams if necessary. (author)

  13. Study on the P-odd asymmetry of longitudinally polarized neutron transmission in 117Sn, 233Th, 239Pu isotopes and natural mixture of Cl and Pb isotopes

    International Nuclear Information System (INIS)

    Abov, Yu.G.; Ermakov, O.N.; Karpikhin, I.L.; Krupchitskij, P.A.; Kuznetsov, Yu.Eh.; Perepelitsa, V.F.; Petrushin, V.I.

    1983-01-01

    The results of measurements of P-odd helicity dependence of the total cross-section a=(σsub(tot)sup(+)-σsub(tot)sup(-))/(σsub(tot)sup(+)+σsub(tot)sup(-)) for thermal neutrons on several targets are presented. The result for 117 Sn is a=(11.2+-2.6)x10 -6 . The upper limits for a in the region of several units of 10 -6 are obtained for 232 Th, 239 Pu, Cl (natural) and Pb (natural)

  14. T violating neutron spin rotation asymmetry

    International Nuclear Information System (INIS)

    Masuda, Yasushiro.

    1993-01-01

    A new experiment on T-violation is proposed, where a spin-rotating-neutron transmission through a polarized nuclear target is measuered. The method to control the neutron spin is discussed for the new T-violation experiment. The present method has possibility to provide us more accurate T-violation information than the neutron EDM measurement

  15. Hybrid scintillators for neutron discrimination

    Science.gov (United States)

    Feng, Patrick L; Cordaro, Joseph G; Anstey, Mitchell R; Morales, Alfredo M

    2015-05-12

    A composition capable of producing a unique scintillation response to neutrons and gamma rays, comprising (i) at least one surfactant; (ii) a polar hydrogen-bonding solvent; and (iii) at least one luminophore. A method including combining at least one surfactant, a polar hydrogen-bonding solvent and at least one luminophore in a scintillation cell under vacuum or an inert atmosphere.

  16. Experimental study of time-reversal invariance in neutron-nucleus interactions

    International Nuclear Information System (INIS)

    Shaparov, E.I.; Shimizu, H.M.

    1996-01-01

    Experimental approaches for the test of time-reversal invariance in neutron-nucleus interactions are reviewed. Possible transmission experiments with polarized neutron beams and polarized or aligned targets are discussed as well as neutron capture experiments with unpolarized resonance neutrons. 102 refs., 13 figs., 3 tabs

  17. New techniques in neutron scattering

    International Nuclear Information System (INIS)

    Hayter, J.B.

    1993-01-01

    New neutron sources being planned, such as the Advanced Neutron Source (ANS) or the European Spallation Source (ESS), will provide an order of magnitude flux increase over what is available today, but neutron scattering will still remain a signal-limited technique. At the same time, the development of new materials, such as polymer and ceramic composites or a variety of complex fluids, will increasingly require neutron-based research. This paper will discuss some of the new techniques which will allow us to make better use of the available neutrons, either through improved instrumentation or through sample manipulation. Discussion will center primarily on unpolarized neutron techniques since polarized neutrons will be the subject of the next paper. (author)

  18. Polarization-dependent transverse-stress sensing characters of the gold-coated and liquid crystal filled photonic crystal fiber based on Surface Plasmon Resonance

    Science.gov (United States)

    Liu, Hai; Zhu, Chenghao; Wang, Yan; Tan, Ce; Li, Hongwei

    2018-03-01

    A transverse-stress sensor with enhanced sensitivity based on nematic liquid crystal (NLC) filled photonic crystal fiber (PCF) is proposed and analyzed by using the finite element method (FEM). The central hole of the PCF is infiltrated with NLC material with an adjustable rotation angle to achieve the polarization-dependent wavelength-selective sensing. And the combined use of side-hole structure and Surface Plasmon Resonance (SPR) technology enhanced the transverse-stress sensitivity enormously. Results reveal that the sensor can achieve a high sensitivity based on the polarization filter characteristic at special wavelengths. Besides that, the temperature and the transverse-stress in either direction can be effectively discriminated through dual-parameter demodulation method by adjusting the rotation angle of the NLC to introduce a new degree of freedom for sensing.

  19. High-birefringence photonic crystal fiber polarization filter with gold-coated and liquid-filled air holes based on surface plasmon resonance

    Science.gov (United States)

    Lou, Junbo; Li, Shuguang; Cheng, Tonglei; Yan, Xin; Zhang, Xuenan

    2018-01-01

    A high-birefringence photonic crystal fiber polarization filter is proposed. The coupling theory is used to explain full and incomplete couplings. The resonance point can be adjusted to the communication band by optimizing the fiber structure parameters. Numerical simulation results indicate that the resonance strength can reach 924.96 and 710.28 dB.cm-1 at the communication wavelength of 1.31 and 1.55 μm in x- and y-polarized directions, respectively. By filling liquid analyte, the confinement loss can reach 804.52 dB.cm-1 at the wavelength of 1.55 μm. Furthermore, when the fiber length of L equals 500 μm, the peak value of the cross talk (CT) can reach 389.15 and -280.52 dB, respectively. When the length of the fiber L equals 200 μm, the bandwidth of the CT better than 20 dB is up to 120 nm at the wavelength of 1.31 μm, and the bandwidth of the CT<-20 dB is up to 140 nm at the wavelength of 1.55 μm. These properties make it a good candidate for designing types of polarization filter devices.

  20. Magnetic and chemical nonuniformity in Ga1-xMnxAs films as probed by polarized neutron and x-ray reflectometry

    International Nuclear Information System (INIS)

    Kirby, B. J.; Borchers, J. A.; Rhyne, J. J.; O'Donovan, K. V.; Velthuis, S. G. E. te; Roy, S.; Sanchez-Hanke, Cecilia; Wojtowicz, T.; Liu, X.; Lim, W. L.; Dobrowolska, M.; Furdyna, J. K.

    2006-01-01

    We have used complementary neutron and x-ray reflectivity techniques to examine the depth profiles of a series of as-grown and annealed Ga 1-x Mn x As thin films. A magnetization gradient is observed for two as-grown films and originates from a nonuniformity of Mn at interstitial sites, and not from local variations in Mn at Ga sites. Furthermore, we see that the depth-dependent magnetization can vary drastically among as-grown Ga 1-x Mn x As films despite being deposited under seemingly similar conditions. These results imply that the depth profile of interstitial Mn is dependent not only on annealing, but is also extremely sensitive to initial growth conditions. We observe that annealing improves the magnetization by producing a surface layer that is rich in Mn and O, indicating that the interstitial Mn migrates to the surface. Finally, we expand upon our previous neutron reflectivity study of Ga 1-x Mn x As, by showing how the depth profile of the chemical composition at the surface and through the film thickness is directly responsible for the complex magnetization profiles observed in both as-grown and annealed films

  1. Measurement of the polarized neutron—polarized 3He total cross section

    Science.gov (United States)

    Keith, C. D.; Gould, C. R.; Haase, D. G.; Seely, M. L.; Huffman, P. R.; Roberson, N. R.; Tornow, W.; Wilburn, W. S.

    1995-05-01

    The first measurements of polarized neutron-polarized 3He scattering in the few MeV energy region are reported. The total cross section difference ΔσT for transversely polarized target and beam has been measured for neutron energies between 1.9 and 7.5 MeV. Comparison is made to predictions of ΔσT using various descriptions of the 4He continuum. A brute-force polarized target of solid 3He has been developed for these measurements. The target is 4.3×1022 atoms/cm2 thick and is polarized to 38% at 7 Telsa and 12 mK.

  2. The measurement of g{sub 1}{sup n} polarized structure of the neutron by the E154 experiment at SLAC; Mesure de la fonction de structure polarisee g{sub 1}{sup n} du neutron par l`experience E154 au SLAC

    Energy Technology Data Exchange (ETDEWEB)

    Incerti, Sebastien [Ecole Doctorale des Sciences Fondamentales, Universite Blaise Pascal, U.F.R. de Recherche Scientifique et Technique, F-63177 Aubiere (France)

    1998-01-21

    This thesis presents the precision measurement of the neutron polarized structure g{sub 1}{sup n} performed by the E154 collaboration at the Standford Linear Accelerator Center, USA, in autumn 1995, using a 48.3 GeV polarized electron beam scattered off a polarized Helium 3 target. The scattered electrons were detected using two spectrometer arms, covering the deep inelastic scattering range: 0.0134 < x < 0.7 and 1 GeV{sup 2} < Q{sup 2} < 17 GeV{sup 2} at an average value of Q{sup 2} = 5 GeV{sup 2}. Two electromagnetic calorimeters have been designed by the LPC in Clermont-Ferrand and the SphN-CEA in Saclay to measure the scattered electron energy and to eject the contaminating hadron background using, a cellular automaton and a neural network, widely described in this thesis. The analysis performed in Clermont-Ferrand and presented in this document led us to the integral on the measurement region of g{sub 1}{sup n} equaling: - 0.34 {+-} 0.003{sub STAT} {+-} 0.004{sub SYST} {+-} 0.001{sub EVOL} at Q{sup 2} = 5 GeV{sup 2}, where our data have been evolved to Q{sup 2} = 5 GeV{sup 2} using the next-to-leading order DGLAP evolution equations and a world parametrization of the polarized parton distributions. The Ellis and Jaffe sum rule is clearly violated. Using different low x extrapolations, our integral is compatible with the Bjorken sum rule. The quark contribution to the nucleon spin is {Delta}{Sigma} = 29 {+-} 6 % in the M S-bar scheme and {Delta}{Sigma} = 37 {+-} 7% in the AB scheme, at Q{sup 2} = 5 GeV{sup 2}. The gluon contribution seems to be positive and within the range: 0 < {Delta}G < 2. (author) 245 refs., 170 figs., 60 tabs.

  3. Sensitivity of the neutron crystal diffraction experiment to the neutron EDM and to the nuclear P-,T-violating forces

    OpenAIRE

    Baryshevsky, V. G.; Cherkas, S. L.

    2013-01-01

    We establish a link between an angle of the neutron polarization rotation in a crystal diffraction experiment and constants of the P-,T- violating interactions. The consideration applies to the energy range of thermal and resonance neutrons.

  4. Review of HTGR coated fuel particle stability

    International Nuclear Information System (INIS)

    Morgan, M.T.

    1975-08-01

    The stability of coated fuel particles in high-temperature, gas-cooled reactors as a function of burnup, fast-neutron fluence, irradiation time, and temperature is reviewed; the effect of coating design parameters was not considered. The purpose of the review is to establish limits of coated particle performance and, in particular, to validate diagrams in which coating failure during abnormal temperature excursions is plotted vs previous irradiation time. (U.S.)

  5. Through-the-thickness residual stress analysis by neutron diffraction in inoxidizable martensitic steel samples with and without tungsten carbide coating

    Czech Academy of Sciences Publication Activity Database

    Rogante, M.; Mikula, Pavol; Vrána, Miroslav

    2009-01-01

    Roč. 204, č. 5 (2009), s. 650-656 ISSN 0257-8972 Institutional research plan: CEZ:AV0Z10480505 Keywords : 13Cr4Ni steel * residual stress * Coating Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders Impact factor: 1.793, year: 2009

  6. Neutron emission study after muon capture by nuclei

    International Nuclear Information System (INIS)

    Bouyssy, Alain.

    1974-01-01

    Muon capture by nuclei, used in the beginning for checking the weak interaction, is now a method of investigation of nuclear structure. Study of spectrum, asymmetry and polarization of emitted neutrons after polarized muon capture has been done in three directions: weak coupling constants, final state interaction, nuclear wave functions. The neutron intensity and helicity are very dependent of the neutron - residual nucleus interaction, while the asymmetry is sensitive to the wave functions used for the proton. Moreover if the induced tensor coupling constant is different from zero the asymmetry is increased. Longitudinal polarization experiments, with those for neutron intensity, would be of great interest to give informations on neutron asymmetry [fr

  7. In situ electrochemical small-angle neutron scattering (eSANS) for quantitative structure and redox properties of polymer-coated nanoparticles

    Science.gov (United States)

    Prabhu, Vivek; Reipa, Vytas; Bonnesen, Peter; Rondinone, Adam; Formo, Eric

    2012-02-01

    Rapid growth in nanomaterial applications (energy, cosmetics and healthcare products) highlights limitations of available physicochemical characterization methods. An in situ electrochemical small-angle neutron scattering (eSANS) methodology was devised that enables direct measurements of nano and colloid material dispersion structure while undergoing reduction-oxidation (redox) reactions. By combining the electrochemical signal with contrast variant SANS, the structure of the polymer-nanoparticle complexes can be examined under electrochemical conditions. Specially-synthesized poly(ethyleneglycol)-stabilized zinc oxide nanoparticles were examined by eSANS showing an irreversible change in nanoparticle-complex structure during the potential cycle. We will report on the kinetics of the nanoparticle transformation as measured at BL-6 EQSANS, Spallation Neutron Source, Oak Ridge National Laboratory.

  8. Synthesis and characterization of magnetic nanoparticles coated with a uniform silica shell

    International Nuclear Information System (INIS)

    Bonini, Massimo; Wiedenmann, Albrecht; Baglioni, Piero

    2006-01-01

    Magnetic nanoparticles with a proper surface coating are of outstanding interest for several applications, especially in the biomedical field. In this paper we present the synthesis of CoFe 2 O 4 magnetic nanoparticles covered by a uniform silica shell. These particles were characterized by means of Transmission Electron Microscopy (TEM) and Small Angle Scattering of Polarized Neutrons (SANSPOL). This newly developed technique, taking advantage from the variation of magnetic contrast, allowed us to verify that the thickness of the silica shell can be accurately tailored through a very simple synthetic approach

  9. Boron Activated Neutron Thermometer

    Energy Technology Data Exchange (ETDEWEB)

    Lapsley, A. C. [Argonne National Lab. (ANL), Argonne, IL (United States). Instrument Research & Development

    1952-01-09

    The Brown Instrument Division of Minneapolis-Honeywell Regulator Co. have been making pilot models of boron coated neutron sensitive thermopiles, which show considerable promise of being effective indicators of slow neutron flux. Their loss in sensitivity in a year of operation in the maximum flux of CP-6 calculates to be less than 6 per cent. When used as rooftop indicators, the ratio of the signal of the two units would change by about 2 per cent in a year's time.

  10. Investigations of advanced magnetic materials using neutron scattering

    International Nuclear Information System (INIS)

    Yusuf, S.M.

    2016-01-01

    A wide class of advanced magnetic materials, such as molecular magnets, magnetic nanoparticles, 1-D and 2-D magnetic materials, high magnetocaloric materials, high magnetoresistive materials, and multiferroic materials by using neutron diffraction, neutron depolarization and polarized neutron small angle scattering techniques has been investigated. A detailed understanding of magnetic correlations in mesoscopic and microscopic length scales in such systems has been achieved. The results of some of these recent investigations, and highlight the usefulness of neutron diffraction, neutron depolarization, and polarized neutron small angle scattering techniques for studying advanced magnetic materials have been presented in this talk. The applied aspects of the derived results have been discussed

  11. Physical bases of magnetic neutron diffraction

    International Nuclear Information System (INIS)

    Izyumov, Yu.A.

    1997-01-01

    The paper is a review of the authors work on use of the symmetry theory in neutron diffraction analysis of magnetic structures. A magnetic structure to be describe in terms of mixing coefficients for irreducible representations basis functions of the crystal space group. An algorithm given for determination of the wave vector and the atomic magnetic moments orientations of a crystal via determination of the mixing coefficients. Symmetry aspects of polarized neutrons are studied, particular dependence of magnetic scattering cross section on polarization of the neutron beam and change the polarization vector of the scattering beam

  12. Magnetism and magnetic materials probed with neutron scattering

    Energy Technology Data Exchange (ETDEWEB)

    Velthuis, S.G.E. te, E-mail: tevelthuis@anl.gov [Materials Science Division, Argonne National Laboratory, 9700 S Cass Ave, Argonne, IL 60439 (United States); Pappas, C. [Faculty of Applied Sciences, Delft University of Technology, Mekelweg 15, NL-2629JB Delft (Netherlands)

    2014-01-15

    Neutron scattering techniques are becoming increasingly accessible to a broader range of scientific communities, in part due to the onset of next-generation, high-power spallation sources, high-performance, sophisticated instruments and data analysis tools. These technical advances also advantageously impact research into magnetism and magnetic materials, where neutrons play a major role. In this Current Perspective series, the achievements and future prospects of elastic and inelastic neutron scattering, polarized neutron reflectometry, small angle neutron scattering, and neutron imaging, are highlighted as they apply to research into magnetic frustration, superconductivity and magnetism at the nanoscale. - Highlights: • Introduction to Current Perspective series titled Magnetism and Magnetic Materials probed with Neutron Scattering. • Elastic and inelastic neutron scattering in systems with magnetic frustration and superconductivity. • Small angle neutron scattering and polarized neutron reflectometry in studying magnetism at the nanoscale. • Imaging of magnetic fields and domains.

  13. Magnetism and magnetic materials probed with neutron scattering

    International Nuclear Information System (INIS)

    Velthuis, S.G.E. te; Pappas, C.

    2014-01-01

    Neutron scattering techniques are becoming increasingly accessible to a broader range of scientific communities, in part due to the onset of next-generation, high-power spallation sources, high-performance, sophisticated instruments and data analysis tools. These technical advances also advantageously impact research into magnetism and magnetic materials, where neutrons play a major role. In this Current Perspective series, the achievements and future prospects of elastic and inelastic neutron scattering, polarized neutron reflectometry, small angle neutron scattering, and neutron imaging, are highlighted as they apply to research into magnetic frustration, superconductivity and magnetism at the nanoscale. - Highlights: • Introduction to Current Perspective series titled Magnetism and Magnetic Materials probed with Neutron Scattering. • Elastic and inelastic neutron scattering in systems with magnetic frustration and superconductivity. • Small angle neutron scattering and polarized neutron reflectometry in studying magnetism at the nanoscale. • Imaging of magnetic fields and domains

  14. The neutron reflectometer at `SINQ`

    Energy Technology Data Exchange (ETDEWEB)

    Clemens, D. [Lab. for Neutron Scattering ETH Zurich, Zurich (Switzerland) and Paul Scherrer Institute, Villigen (Switzerland)

    1996-11-01

    SINQ`s dedicated reflectometer will be a flexible instrument in many respect. A `white beam time of flight` as well as a `constant wavelength` setup are possible for reflectometric experiments in a vertical scattering geometry. The phase controlled double chopper at the beginning of the instrument together with properly chosen time channels at the detector allow for the variation of the temporal resolution. Collimation slits serve to determine the angular resolution. In combination, the resolution can be tailored to the experimental needs. Additionally, one can adjust the illumination of the sample by setting the sample table and the detector to an appropriate distance. A mounting for exchangeable mirrors can be used to supply polarized neutrons by a multilayer polarizer or monochromatic neutrons by a multilayer monochromator. When it is equipped with a supermirror as a deflecting unit one can maintain a horizontal sample position which makes reflectometry on liquid samples practicable. Remanent polarizers are assigned for the changing over of the neutron polarization. A 1 T electromagnet installed on the sample manipulation table and polarization analyzers complete the polarized reflectometry setup. Alternately, an x-y-detector and single detectors will be available. By 1997/1998 the neutron reflectometer will be operational as a users` instrument. (author) 9 figs., 2 tabs., 30 refs.

  15. “m=1” coatings

    DEFF Research Database (Denmark)

    Cooper-Jensen, C.; Klinkby, Esben Bryndt; Beaucour, J.

    . For a neutron guide the cost of shielding around the guide is a substantial part of the total cost of the guide. We are therefore looking at other materials than Ni for m=1 coatings. Both Be and diamond have the same or higher neutron scattering density than Ni, and have a much smaller absorption cross section....... Because of the lower absorption cross section, and because of fewer emitted gamma ray photons when a neutron is absorbed, these coatings are producing much less gamma radiation and therefore reduce the shielding costs. Be is frequently used in a wide range of science and technology applications. The only...... chemical hazard after manufacture is Be dust if the sample is destroyed. We have a sample of 276 nm Be coated on a Si wafer for these tests. Diamond Like Carbon (DLC) coatings with 99% sp3 bindings (meaning it is very close to diamond) are made commercially using CVD techniques. In the coating...

  16. Artificial anisotropy and polarizing filters.

    Science.gov (United States)

    Flory, François; Escoubas, Ludovic; Lazaridès, Basile

    2002-06-01

    The calculated spectral transmittance of a multilayer laser mirror is used to determine the effective index of the single layer equivalent to the multilayer stack. We measure the artificial anisotropy of photoresist thin films whose structure is a one-dimensional, subwavelength grating obtained from interference fringes. The limitation of the theory of the first-order effective index homogenization is discussed. We designed normal-incidence, polarizing coating and a polarization rotator by embedding anisotropic films in simple multilayer structures.

  17. Performance of an elliptically tapered neutron guide

    International Nuclear Information System (INIS)

    Muehlbauer, Sebastian; Stadlbauer, Martin; Boeni, Peter; Schanzer, Christan; Stahn, Jochen; Filges, Uwe

    2006-01-01

    Supermirror coated neutron guides are used at all modern neutron sources for transporting neutrons over large distances. In order to reduce the transmission losses due to multiple internal reflection of neutrons, ballistic neutron guides with linear tapering have been proposed and realized. However, these systems suffer from an inhomogeneous illumination of the sample. Moreover, the flux decreases significantly with increasing distance from the exit of the neutron guide. We propose using elliptically tapered guides that provide a more homogeneous phase space at the sample position as well as a focusing at the sample. Moreover, the design of the guide system is simplified because ellipses are simply defined by their long and short axes. In order to prove the concept we have manufactured a doubly focusing guide and investigated its properties with neutrons. The experiments show that the predicted gains using the program package McStas are realized. We discuss several applications of elliptic guides in various fields of neutron physics

  18. Fabrication of boron-phosphide neutron detectors

    International Nuclear Information System (INIS)

    Fitzsimmons, M.; Pynn, R.

    1997-01-01

    Boron phosphide is a potentially viable candidate for high neutron flux neutron detectors. The authors have explored chemical vapor deposition methods to produce such detectors and have not been able to produce good boron phosphide coatings on silicon carbide substrates. However, semi-conducting quality films have been produced. Further testing is required

  19. Experimental technique of neutron reflection

    International Nuclear Information System (INIS)

    Chen Bo; Huang Chaoqiang; Li Xinxi

    2006-12-01

    It is presented that the classifications, structures and components of neutron reflectometer (NR), as well s functions and parameters of each components, detailed characters of NR facility 'PRN-2M'. Based on the practical experiments, the basic experimental techniques, the measurement and the related experimental settings are described, including the choice of experimental conditions, adjustments of polarized neutron beam line, basic experimental technique and approach of measurement. The above can be an instruction for NR experiments and a reference for NR construction. (authors)

  20. Solid State Neutron Detector - A Review of Status

    International Nuclear Information System (INIS)

    Mukhopadhyay, Sanjoy

    2010-01-01

    The PowerPoint presentation was organized into the following areas: Driving forces behind research in semiconductor neutron devices; The (sup 3)He shortage crisis; Alternative detectors for neutron; Semiconductor diodes coated with boron; Perforated semiconductors for neutron detection; and, Three dimensional pillar and trench structured semiconductors.

  1. Small-angle scattering studies on clathrin-coated vesicles

    International Nuclear Information System (INIS)

    Bauer, R.; Hansen, S.; Oegendal, L.; Behan, M.; Jones, G.; Mortensen, K.; Saermark, T.

    1991-01-01

    Structural information of clathrin-coated vesicles has been achieved by small-angle X-ray, neutron and dynamic light scattering studies. A characteristic peak in the X-ray and neutron scattering profile (in D 2 O) from intact coated vesicles is consistent with the polygonic structure of the clathrin coat. Neutron as well as dynamic light scattering gives a coated vesicle size close to 1000A. Dynamic light scattering detects a distribution of sizes for the coated vesicles demonstrating polydispersity of the samples. Quick freezing and slow thawing cause breakdown of the polygonic coat and production of large aggregates, as observed by dynamic light scattering and the reduction of the peak in the X-ray scattering profile as well as an increase in the scattering intensity at the lowest angles in the neutron scattering profile. (orig.)

  2. RPC for thermal neutron detection

    Energy Technology Data Exchange (ETDEWEB)

    Arnaldi, R [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Chiavassa, E [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Colla, A [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Cortese, P [INFN Alessandria and Universita del Piemonte Orientale ' Amedeo Avogadro' , Alessandria (Italy); Dellacasa, G [INFN Alessandria and Universita del Piemonte Orientale ' Amedeo Avogadro' , Alessandria (Italy); Marco, N De [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Ferretti, A [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Gagliardi, M [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Gallio, M [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Gemme, R [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Musso, A [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Oppedisano, C [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Piccotti, A [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Poggio, F [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Scomparin, E [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy); Vercellin, E [INFN Torino and Dip. di Fisica Sperimentale dell' Universita di Torino (Italy)

    2006-05-15

    The possibility to detect thermal neutrons with single gap Resistive Plate Chambers has been investigated. To detect neutrons a {sup 10}B{sub 4}C thin coating on the inner surface of one RPC electrode is used as thermal neutron converter. The RPC detects the charged particles generated by neutrons via the (n, {alpha}) reaction on Boron. Tests on converter samples have been performed with a thermalized {sup 252}Cf source in order to evaluate the conversion efficiency: a good agreement between experimental results and simulation has been achieved. A detector prototype has been developed and tested on a low energy neutron beam at the European laboratories JRC in Belgium. A detailed description of the detector and the experimental test results are presented.

  3. The elements Se, Hg, Cr, Sb, Fe, Zn, Co, and Rb were investigated by neutron activation analysis in blood serum of leukemia patients and workers of metal coating industries

    International Nuclear Information System (INIS)

    Taheriean, Ali Akbar.

    1992-02-01

    Current universal interests in trace element studies are being spurred by our needs to determine trace element requirements and tolerance by organism, including relationships to animal and human health and disease, evaluate the potential bio magnification and bio toxicity of trace elements. The element Se, Hg, Cr, Sb, Fe, Zn, Co, and Rb were investigated in blood serum of 24 leukemia patients and 20 workers of metal coating of industries, using neutron activation analysis and gamma ray counting high purity germanium detector, it was possible to determine the above mentioned trace elements with great accuracy. The result of these investigations are described briefly. In the blood serum of leukemia patients, which were collected from Ali Asghar children Hospital, some increase of Fe and decrease of Se could be found, whereas the amount variation of other trace elements were negligible. The amount of Zn in the blood serum of these workers by comparison with 60 normal man indicates no change. Due to importance of trace elements in the human health we suggest that this investigation must be prolonged using more samples

  4. Neutron diffraction in materials science

    International Nuclear Information System (INIS)

    Howard, C.J.

    1996-01-01

    This article deals with applications of neutron diffraction in materials science. Most of the examples presented here involve the use of powder diffraction, which has been described earlier. In most of these, the Rietveld method has been used for neutron diffraction data, using the Rietveld method. This being an application which was largely pioneered at Lucas Heights. Examples involving single crystal diffraction and neutron polarization analysis are also included. Most of the examples are drawn from studies carried out at Lucas Heights where there is diffraction to the study of ceramics, and this will be reflected in the choice of examples to be considered here. (author)

  5. Measurement of the proton asymmetry (C) in free neutron β-decay with Perkeo III

    Energy Technology Data Exchange (ETDEWEB)

    Raffelt, Lukas Michael

    2016-10-19

    The decay of polarized neutrons can be used to search for Physics Beyond the Standard Model. The non-isotropic angular distributions of the decay particles are parity violating and reveal the true nature of the weak interaction. Many observables are available in the decay of polarized neutrons, but the decay itself is only described by three parameters, which allows searches for new physics in a combined analysis. Measurements of the electron angular correlation coefficient (A) can be used to precisely determine the ratio of the axial to the vector coupling constant. The proton angular correlation coefficient (C) has only been measured once by a predecessor of this experiment. We measured the proton asymmetry with a similar proton detector, but employed a new measuring scheme allowing the collection of the worlds first data on the proton energy dependence of the proton asymmetry. At the current state of the analysis, a statistical uncertainty on the value of C of 0.8 % in each of the two detectors can be reached. For a final value, studies of systematic effects based on field simulations and tracking are still missing. For this measurement I designed and constructed a new detector. For the first time the scintillator was coated with a transparent conductive coating and together with the new CAD milled light-guides in a four-side readout configuration the low energy performance of the detector could be increased. Several systematic effects have been studied, especially the Point Spread Function of the magnetic transport system.

  6. Properties of the TRIUMF neutron beam

    Energy Technology Data Exchange (ETDEWEB)

    Gan, L. [Manitoba Univ., Winnipeg, MB (Canada). Dept. of Physics; Abegg, R. [TRIUMF, 4004 Wesbrook Mall, Vancouver, BC (Canada)]|[University of Alberta, Department of Physics, Edmonton, AB (Canada); Berdoz, A.R. [Manitoba Univ., Winnipeg, MB (Canada). Dept. of Physics; Birchall, J. [Manitoba Univ., Winnipeg, MB (Canada). Dept. of Physics; Campbell, J.R. [Manitoba Univ., Winnipeg, MB (Canada). Dept. of Physics; Davis, C.A. [Manitoba Univ., Winnipeg, MB (Canada). Dept. of Physics]|[TRIUMF, 4004 Wesbrook Mall, Vancouver, BC (Canada); Green, P.W. [TRIUMF, 4004 Wesbrook Mall, Vancouver, BC (Canada)]|[University of Alberta, Department of Physics, Edmonton, AB (Canada); Greeniaus, L.G. [TRIUMF, 4004 Wesbrook Mall, Vancouver, BC (Canada)]|[University of Alberta, Department of Physics, Edmonton, AB (Canada); Helmer, R. [TRIUMF, 4004 Wesbrook Mall, Vancouver, BC (Canada)]|[University of Alberta, Department of Physics, Edmonton, AB (Canada); Korkmaz, E. [University of Alberta, Department of Physics, Edmonton, AB (Canada); Lee, L. [Manitoba Univ., Winnipeg, MB (Canada). Dept. of Physics; Li, J. [University of Alberta, Department of Physics, Edmonton, AB (Canada); Miller, C.A. [TRIUMF, 4004 Wesbrook Mall, Vancouver, BC (Canada)]|[University of Alberta, Department of Physics, Edmonton, AB (Canada); Opper, A.K. [University of Alberta, Department of Physics, Edmonton, AB (Canada); Page, S.A. [Manitoba Univ., Winnipeg, MB (Canada). Dept. of Physics; Ramsay, W.D. [Manitoba Univ., Winnipeg, MB (Canada). Dept. of Physics; Soukup, J. [University of Alberta, Department of Physics, Edmonton, AB (Canada); Van Oers, W.T.H. [Manitoba Univ., Winnipeg, MB (Canada). Dept. of Physics; Zhao, J. [Manitoba Univ., Winnipeg, MB (Canada). Dept. of Physics

    1995-11-01

    Properties of the TRIUMF neutron beam (4A/2) are presented and compared with a Monte Carlo prediction. The beam intensity profile, energy spectrum and polarization are predicted taking into account the beamline geometry, energy losses in the LD{sub 2} production target, the properties of the vector pd{yields} vector npp reaction, and the scattering of neutrons from the collimator walls. The results allow for improved corrections to systematic errors in a number of TRIUMF neutron experiments. (orig.).

  7. Properties of the TRIUMF neutron beam

    International Nuclear Information System (INIS)

    Gan, L.; Berdoz, A.R.; Green, P.W.; Greeniaus, L.G.; Helmer, R.; Korkmaz, E.; Lee, L.; Miller, C.A.; Opper, A.K.; Page, S.A.; Van Oers, W.T.H.; Zhao, J.

    1995-01-01

    Properties of the TRIUMF neutron beam (4A/2) are presented and compared with a Monte Carlo prediction. The beam intensity profile, energy spectrum and polarization are predicted taking into account the beamline geometry, energy losses in the LD 2 production target, the properties of the vector pd→ vector npp reaction, and the scattering of neutrons from the collimator walls. The results allow for improved corrections to systematic errors in a number of TRIUMF neutron experiments. (orig.)

  8. Multi-Wavelength Polarimetry of Isolated Neutron Stars

    Directory of Open Access Journals (Sweden)

    Roberto P. Mignani

    2018-03-01

    Full Text Available Isolated neutron stars are known to be endowed with extreme magnetic fields, whose maximum intensity ranges from 10 12 – 10 15 G, which permeates their magnetospheres. Their surrounding environment is also strongly magnetized, especially in the compact nebulae powered by the relativistic wind from young neutron stars. The radiation from isolated neutron stars and their surrounding nebulae is, thus, supposed to bring a strong polarization signature. Measuring the neutron star polarization brings important information about the properties of their magnetosphere and of their highly magnetized environment. Being the most numerous class of isolated neutron stars, polarization measurements have been traditionally carried out for radio pulsars, hence in the radio band. In this review, I summarize multi-wavelength linear polarization measurements obtained at wavelengths other than radio both for pulsars and other types of isolated neutron stars and outline future perspectives with the upcoming observing facilities.

  9. Current status and future prospect of space and time reversal symmetry violation on low energy neutron reactions

    International Nuclear Information System (INIS)

    Masuda, Yasuhiro

    1993-01-01

    In this report, the papers on symmetry violation under space reflection and time reversal and neutron spin, neutron spin rotation and P-violation, parity nonconservation in neutron capture reaction, some advantage of the search for CP-violation in neutron scattering, dynamic polarization of 139 La target, alexandrite laser for optical pumping, polarized 3 He system for T- and P-violation neutron experiments, control of neutron spin in T-violation neutron experiment, symmetry regarding time and space and angular distribution and angular correlation of radiation and particle beams, T-violation due to low temperature nuclear polarization and axion exploration using nuclear transition are collected. (K.I.)

  10. Instrumentation for PSD-based neutron diffractometers at Dhruva ...

    Indian Academy of Sciences (India)

    positions and data is acquired simultaneously from all the PSDs. Throughput is further improved by using multiple PSDs at each position. Various instruments like the powder diffractometer, high-Q diffractometer, polarized neutron reflectometer, quasi-elastic neutron spectrometer, small-angle neutron spectrometer all use ...

  11. Computational investigations on a catenary-shaped double-reflecting neutron guide

    International Nuclear Information System (INIS)

    Priesmeyer, H.G.

    1983-01-01

    The results of Monte-Carlo calculations of the neutron transmission of a vertical catenary-shaped neutron guide are presented. A two-dimensional problem was considered. Focussing and special coatings are investigated. (orig.) [de

  12. Polarization developments

    International Nuclear Information System (INIS)

    Prescott, C.Y.

    1993-07-01

    Recent developments in laser-driven photoemission sources of polarized electrons have made prospects for highly polarized electron beams in a future linear collider very promising. This talk discusses the experiences with the SLC polarized electron source, the recent progress with research into gallium arsenide and strained gallium arsenide as a photocathode material, and the suitability of these cathode materials for a future linear collider based on the parameters of the several linear collider designs that exist

  13. Neutron guide

    Science.gov (United States)

    Greene, Geoffrey L.

    1999-01-01

    A neutron guide in which lengths of cylindrical glass tubing have rectangular glass plates properly dimensioned to allow insertion into the cylindrical glass tubing so that a sealed geometrically precise polygonal cross-section is formed in the cylindrical glass tubing. The neutron guide provides easier alignment between adjacent sections than do the neutron guides of the prior art.

  14. Few-body experiments with polarized beams and polarized targets

    International Nuclear Information System (INIS)

    Simmons, J.E.

    1983-01-01

    A survey is presented concerning recent polarization experiments in the elastic p-d, p- 3 He, and p- 4 He systems. Mention is made of selected neutron experiments. The nominal energy range is 10 to 1000 MeV. Recent results and interpretations of the p-d system near 10 MeV are discussed. New experiments on the energy dependence of back angle p-d tensor polarization are discussed with respect to resolution of discrepancies and difficulty of theoretical interpretation. Progress is noted concerning multiple scattering interpretation of forward p-d deuteron polarization. Some new results are presented concerning the p- 3 He system and higher energy p- 4 He polarization experiments. 52 references

  15. Optics for Advanced Neutron Imaging and Scattering

    Energy Technology Data Exchange (ETDEWEB)

    Moncton, David E. [Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States); Khaykovich, Boris [Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States)

    2016-03-30

    During the report period, we continued the work as outlined in the original proposal. We have analyzed potential optical designs of Wolter mirrors for the neutron-imaging instrument VENUS, which is under construction at SNS. In parallel, we have conducted the initial polarized imaging experiment at Helmholtz Zentrum, Berlin, one of very few of currently available polarized-imaging facilities worldwide.

  16. Discussion on data correction for Polarization Analysis with a 3He spin filter analyzer

    Science.gov (United States)

    Babcock, Earl; Salhi, Zahir; Kentzinger, Emmanuel; Mattauch, Stefan; Ioffe, Alexander

    2017-06-01

    Fully polarized neutron reflectometry and grazing incidence small angle neutron scattering are effective methods to explore magnetic structures on the nm to μm length scales. This paper is an outline of how to fully correct for the polarization analysis (PA) inefficiencies of such an instrument and to determine the error contributions of the neutron polarizer and analyzer. This discussion considers the exact case of the polarization analysis instrumentation used on the MARIA neutron reflectometer at the MLZ or for a general polarized neutron scattering instrument using at least one 3He neutron spin filter that has the capability for adiabatic fast passage nuclear magnetic resonance flipping of the 3He polarization. This paper will work to build a conceptual understanding of how the inefficiencies of neutron polarization elements affect measured data in order to stress and encourage the application of PA corrections and to help perform successful measurements. Then, using data from a fully polarized neutron reflectometer test measurement we show how it is possible to recover signals on the order of, or even smaller than, the inefficiencies, or bleed-through, of the neutron polarization devices used.

  17. Powder neutron diffractometers HRPT and DMCG

    Energy Technology Data Exchange (ETDEWEB)

    Fischer, P.; Doenni, A.; Staub, U.; Zolliker, M. [Lab. for Neutron Scattering ETH Zurich, Zurich (Switzerland) and Paul Scherrer Institute, Villigen (Switzerland)

    1996-11-01

    Basic properties and applications of SINQ powder neutron diffractometers are described. For optimum use of the continuous neutron beams these instruments are equipped with position sensitive detectors, and both high-intensity and high-resolution modes of operation are possible. HRPT attaining resolutions {delta}d/d{<=}10{sup -3}, d=lattice spacing, at a thermal neutron channel of the target station and DMCG at a cold neutron guide coated with m=2 supermirrors, are complementary concerning the applications: the former will be mainly used for structural studies and the latter to investigate magnetic ordering phenomena. (author) figs., tabs., refs.

  18. Powder neutron diffractometers HRPT and DMCG

    International Nuclear Information System (INIS)

    Fischer, P.; Doenni, A.; Staub, U.; Zolliker, M.

    1996-01-01

    Basic properties and applications of SINQ powder neutron diffractometers are described. For optimum use of the continuous neutron beams these instruments are equipped with position sensitive detectors, and both high-intensity and high-resolution modes of operation are possible. HRPT attaining resolutions δd/d≤10 -3 , d=lattice spacing, at a thermal neutron channel of the target station and DMCG at a cold neutron guide coated with m=2 supermirrors, are complementary concerning the applications: the former will be mainly used for structural studies and the latter to investigate magnetic ordering phenomena. (author) figs., tabs., refs

  19. Specular neutron reflectivity and beyond

    Indian Academy of Sciences (India)

    A polarized neutron reflectometer for vertical samples is available at Dhruva reactor guide hall, Trombay. The reflectometer has been designed for horizontal scattering vector. It uses a position-sensitive detector for obtaining the reflectivity pattern. This arrangement allows one to obtain diffuse or off-specular intensity around ...

  20. Luminosity class of neutron reflectometers

    International Nuclear Information System (INIS)

    Pleshanov, N.K.

    2016-01-01

    The formulas that relate neutron fluxes at reflectometers with differing q-resolutions are derived. The reference luminosity is defined as a maximum flux for measurements with a standard resolution. The methods of assessing the reference luminosity of neutron reflectometers are presented for monochromatic and white beams, which are collimated with either double diaphragm or small angle Soller systems. The values of the reference luminosity for unified parameters define luminosity class of reflectometers. The luminosity class characterizes (each operation mode of) the instrument by one number and can be used to classify operating reflectometers and optimize designed reflectometers. As an example the luminosity class of the neutron reflectometer NR-4M (reactor WWR-M, Gatchina) is found for four operation modes: 2.1 (monochromatic non-polarized beam), 1.9 (monochromatic polarized beam), 1.5 (white non-polarized beam), 1.1 (white polarized beam); it is shown that optimization of measurements may increase the flux at the sample up to two orders of magnitude with monochromatic beams and up to one order of magnitude with white beams. A fan beam reflectometry scheme with monochromatic neutrons is suggested, and the expected increase in luminosity is evaluated. A tuned-phase chopper with a variable TOF resolution is recommended for reflectometry with white beams.

  1. Specular neutron reflectivity and beyond

    Indian Academy of Sciences (India)

    Abstract. A polarized neutron reflectometer for vertical samples is available at Dhruva reactor guide hall, Trombay. The reflectometer has been designed for horizontal scattering vector. It uses a position-sensitive detector for obtaining the reflectivity pattern. This arrangement allows one to obtain diffuse or off-specular ...

  2. Neutron scattering by Dirac multipoles

    Science.gov (United States)

    Lovesey, S. W.; Khalyavin, D. D.

    2017-06-01

    Scattering by magnetic charge formed by Dirac multipoles that are magnetic and polar is examined in the context of materials with properties that challenge conventional concepts. An order parameter composed of Dirac quadrupoles has been revealed in the pseudo-gap phase of ceramic, high-T c superconductors on the basis of Kerr effect and magnetic neutron Bragg diffraction measurements. Construction of Dirac quadrupoles that emerge from centrosymmetric sites used by Cu ions in the ceramic superconductor Hg1201 is illustrated, together with selection rules for excitations that will feature in neutron inelastic scattering, and RIXS experiments. We report magnetic scattering amplitudes for diffraction by polar multipoles that have universal value, because they are not specific to ceramic superconductors. To illustrate this attribute, we consider neutron Bragg diffraction from a magnetically ordered iridate (Sr2IrO4) and discuss shortcomings in published interpretations of diffraction data.

  3. Neutron scattering by Dirac multipoles

    International Nuclear Information System (INIS)

    Lovesey, S W; Khalyavin, D D

    2017-01-01

    Scattering by magnetic charge formed by Dirac multipoles that are magnetic and polar is examined in the context of materials with properties that challenge conventional concepts. An order parameter composed of Dirac quadrupoles has been revealed in the pseudo-gap phase of ceramic, high- T c superconductors on the basis of Kerr effect and magnetic neutron Bragg diffraction measurements. Construction of Dirac quadrupoles that emerge from centrosymmetric sites used by Cu ions in the ceramic superconductor Hg1201 is illustrated, together with selection rules for excitations that will feature in neutron inelastic scattering, and RIXS experiments. We report magnetic scattering amplitudes for diffraction by polar multipoles that have universal value, because they are not specific to ceramic superconductors. To illustrate this attribute, we consider neutron Bragg diffraction from a magnetically ordered iridate (Sr 2 IrO 4 ) and discuss shortcomings in published interpretations of diffraction data. (paper)

  4. Latest developments of neutron scattering instrumentation at the Juelich Centre for Neutron Science

    International Nuclear Information System (INIS)

    Ioffe, Alexander

    2013-01-01

    Jülich Centre for Neutron Science (JCNS) is operating a number of world-class neutron scattering instruments situated at the most powerful and advanced neutron sources (FRM II, ILL and SNS) and is continuously undertaking significant efforts in the development and upgrades to keep this instrumentation in line with the continuously changing scientific request. These developments are mostly based upon the latest progress in neutron optics and polarized neutron techniques. For example, the low-Q limit of the suite of small angle-scattering instruments has been extended to 4·10 -5 Å -1 by the successful use of focusing optics. A new generation of correction elements for the neutron spin-echo spectrometer has allowed for the use of the full field integral available, thus pushing further the instrument resolution. A significant progress has been achieved in the developments of 3 He neutron spin filters for purposes of the wide-angle polarization analysis for off-specular reflectometry and (grazing incidence) small-angle neutron scattering, e.g. the on-beam polarization of 3 He in large cells is allowing to achieve a high neutron beam polarization without any degradation in time. The wide Q-range polarization analysis using 3 He neutron spin filters has been implemented for small-angle neutron scattering that lead to the reduction up to 100 times of the intrinsic incoherent background from non-deuterated biological molecules. Also the work on wide-angle XYZ magnetic cavities (Magic PASTIS) will be presented. (author)

  5. Neutron physics

    CERN Document Server

    Reuss, Paul

    2008-01-01

    Originally just an offshoot of nuclear physics, neutron physics soon became a branch of physics in its own right. It deals with the movement of neutrons in nuclear reactors and ail the nuclear reactions they trigger there, particularly the fission of heavy nuclei which starts a chain reaction to produce energy. Neutron Physics covers the whole range of knowledge of this complex science, discussing the basics of neutron physics and some principles of neutron physics calculations. Because neutron physics is the essential part of reactor physics, it is the main subject taught to students of Nuclear Engineering. This book takes an instructional approach for that purpose. Neutron Physics is also intended for ail physicists and engineers involved in development or operational aspects of nuclear power.

  6. Polarization, political

    NARCIS (Netherlands)

    Wojcieszak, M.; Mazzoleni, G.; Barnhurst, K.G.; Ikeda, K.; Maia, R.C.M.; Wessler, H.

    2015-01-01

    Polarization has been studied in three different forms: on a social, group, and individual level. This entry first focuses on the undisputed phenomenon of elite polarization (i.e., increasing adherence of policy positions among the elites) and also outlines different approaches to assessing mass

  7. Polarization holography

    DEFF Research Database (Denmark)

    Nikolova, L.; Ramanujam, P.S.

    Current research into holography is concerned with applications in optically storing, retrieving, and processing information. Polarization holography has many unique properties compared to conventional holography. It gives results in high efficiency, achromaticity, and special polarization...... properties. This books reviews the research carried out in this field over the last 15 years. The authors provide basic concepts in polarization and the propagation of light through anisotropic materials, before presenting a sound theoretical basis for polarization holography. The fabrication...... and characterization of azobenzene based materials, which remain the most efficient for the purpose, is described in detail. This is followed by a description of other materials that are used in polarization holography. An in-depth description of various applications, including display holography and optical storage...

  8. Interference phenomena and spin rotation of neutrons by magnetic materials

    International Nuclear Information System (INIS)

    Eder, G.; Zeilinger, A.

    1976-01-01

    By the use of a neutron interferometer it is possible to study the transformation properties of spinors. The behaviour of neutrons in homogeneous and helical magnetic fields is studied. Intensity and polarization of the forward neutron beam after the interferometer, which is composed of an unchanged wave and a wave which has passed through a magnetic material, are calculated. Attention is paid to adiabatic helical fields. In all cases the influence of the neutron-nucleus potential is taken into account

  9. Spontaneous growth of polarizing refractory metal ‘nano-fins’

    Science.gov (United States)

    Tai, M. C.; Gentle, A. R.; Arnold, M. D.; Cortie, M. B.

    2018-03-01

    Traditional polymer polarizers degrade in harsh environments and at high temperatures, reducing the polarization effect. In contrast, polarizers produced with refractory metals have vastly improved thermal stability and resistance to harsh environments but are expensive to fabricate. Here we demonstrate prototype refractory metal wire grid polarizers produced by co-sputtering molybdenum and aluminum under specific conditions. Removal of the aluminum through selective dissolution enables the nanostructure array to transmit light. The polarization spans 500–1100 nm and the extinction ratio significantly increases to >100. Possessing broadband polarization and sufficient extinction ratios, the new polarizing film has potential applications in coatings for sunglasses, windows, pyrometers, scientific instruments, and LCD panels.

  10. Grazing incidence polarized neutron scattering in reflection ...

    Indian Academy of Sciences (India)

    Pramana – Journal of Physics. Current Issue : Vol. 90, Issue 1 · Current Issue Volume 90 | Issue 1. January 2018. Home · Volumes & Issues · Special Issues · Forthcoming Articles · Search · Editorial Board · Information for Authors · Subscription ...

  11. Polarized neutron reflectometry at Dhruva reactor

    Indian Academy of Sciences (India)

    beam (divergence ~ few arc minutes) at the air–film interface of a thin film sam- ple. The specular reflection data is collected at grazing incidence to the sample ... 12 Å, averaged over the total number of interfaces. In the present multilayer, the intensity at the Bragg peak is about 70% of the total reflectivity plateau and the.

  12. Magnetic field devices for neutron spin transport and manipulation in precise neutron spin rotation measurements

    Energy Technology Data Exchange (ETDEWEB)

    Maldonado-Velázquez, M. [Posgrado en Ciencias Físicas, Universidad Nacional Autónoma de México, 04510 (Mexico); Barrón-Palos, L., E-mail: libertad@fisica.unam.mx [Instituto de Física, Universidad Nacional Autónoma de México, Apartado Postal 20-364, 01000 (Mexico); Crawford, C. [University of Kentucky, Lexington, KY 40506 (United States); Snow, W.M. [Indiana University, Bloomington, IN 47405 (United States)

    2017-05-11

    The neutron spin is a critical degree of freedom for many precision measurements using low-energy neutrons. Fundamental symmetries and interactions can be studied using polarized neutrons. Parity-violation (PV) in the hadronic weak interaction and the search for exotic forces that depend on the relative spin and velocity, are two questions of fundamental physics that can be studied via the neutron spin rotations that arise from the interaction of polarized cold neutrons and unpolarized matter. The Neutron Spin Rotation (NSR) collaboration developed a neutron polarimeter, capable of determining neutron spin rotations of the order of 10{sup −7} rad per meter of traversed material. This paper describes two key components of the NSR apparatus, responsible for the transport and manipulation of the spin of the neutrons before and after the target region, which is surrounded by magnetic shielding and where residual magnetic fields need to be below 100 μG. These magnetic field devices, called input and output coils, provide the magnetic field for adiabatic transport of the neutron spin in the regions outside the magnetic shielding while producing a sharp nonadiabatic transition of the neutron spin when entering/exiting the low-magnetic-field region. In addition, the coils are self contained, forcing the return magnetic flux into a compact region of space to minimize fringe fields outside. The design of the input and output coils is based on the magnetic scalar potential method.

  13. Neutron stars velocities and magnetic fields

    Science.gov (United States)

    Paret, Daryel Manreza; Martinez, A. Perez; Ayala, Alejandro.; Piccinelli, G.; Sanchez, A.

    2018-01-01

    We study a model that explain neutron stars velocities due to the anisotropic emission of neutrinos. Strong magnetic fields present in neutron stars are the source of the anisotropy in the system. To compute the velocity of the neutron star we model its core as composed by strange quark matter and analice the properties of a magnetized quark gas at finite temperature and density. Specifically we have obtained the electron polarization and the specific heat of magnetized fermions as a functions of the temperature, chemical potential and magnetic field which allow us to study the velocity of the neutron star as a function of these parameters.

  14. Diamondlike carbon can replace beryllium in physics with ultracold neutrons

    International Nuclear Information System (INIS)

    Atchison, F.; Blau, B.; Daum, M.; Fierlinger, P.; Foelske, A.; Geltenbort, P.; Gupta, M.; Henneck, R.; Heule, S.; Kasprzak, M.; Kuzniak, M.; Kirch, K.; Meier, M.; Pichlmaier, A.; Plonka, Ch.; Reiser, R.; Theiler, B.; Zimmer, O.; Zsigmond, G.

    2006-01-01

    To complete our study of ultracold neutron (UCN) storage-vessel coatings, we have measured the Fermi potential for neutrons on diamondlike carbon coatings produced by laser induced vacuum arc deposition. A sample with an sp 3 content of 0.45, measured using, for the first time, neutron transmission had a Fermi potential of (249+/-14)neV. A second sample with an sp 3 fraction of 0.67, measured using cold neutron reflectometry, gave (271+/-13)neV. These values complete the demonstration that there is a viable alternative to Be in UCN physics

  15. Electrochemical behaviour of superhydrophobic coating fabricated ...

    Indian Academy of Sciences (India)

    of Ecorr that confers a better corrosion resistance of the coated samples. Keywords. Al alloy; surface coating; superhydrophobicity; potentiodynamic polarization. 1. Introduction. Aluminium and its alloys exhibit high-specific strength, low density, excellent heat and electric conductivities and low- specific weight.1,2 These ...

  16. Electrochemical behaviour of superhydrophobic coating fabricated ...

    Indian Academy of Sciences (India)

    surface caused by the presence of CNTs. The electrochemical observations indicate the presence of a positive shift of Ecorr that confers a better corrosion resistance of the coated samples. Keywords. Al alloy; surface coating; superhydrophobicity; potentiodynamic polarization. 1. Introduction. Aluminium and its alloys exhibit ...

  17. Neutron radiography

    International Nuclear Information System (INIS)

    Hiraoka, Eiichi

    1988-01-01

    The thermal neutron absorption coefficient is essentially different from the X-ray absorption coefficient. Each substance has a characteristic absorption coefficient regardless of its density. Neutron deams have the following features: (1) neutrons are not transmitted efficiently by low molecular weight substances, (2) they are transmitted efficiently by heavy metals, and (3) the transmittance differs among isotopes. Thus, neutron beams are suitable for cheking for foreign matters in heavy metals and testing of composites consisting of both heavy and light materials. A neutron source generates fast neutrons, which should be converted into thermal neutrons by reducing their energy. Major neutron souces include nuclear reactors, radioisotopes and particle accelerators. Photographic films and television systems are mainly used to observe neutron transmission images. Computers are employed for image processing, computerized tomography and three-dimensional analysis. The major applications of neutron radiography include inspection of neclear fuel; evaluation of material for airplane; observation of fuel in the engine and oil in the hydraulic systems in airplanes; testing of composite materials; etc. (Nogami, K.)

  18. Polar Bears

    Science.gov (United States)

    Amstrup, Steven C.; Douglas, David C.; Reynolds, Patricia E.; Rhode, E.B.

    2002-01-01

    Polar bears (Ursus maritimus) are hunted throughout most of their range. In addition to hunting polar bears of the Beaufort Sea region are exposed to mineral and petroleum extraction and related human activities such as shipping road-building, and seismic testing (Stirling 1990).Little was known at the start of this project about how polar bears move about in their environment, and although it was understood that many bears travel across political borders, the boundaries of populations had not been delineated (Amstrup 1986, Amstrup et al. 1986, Amstrup and DeMaster 1988, Garner et al. 1994, Amstrup 1995, Amstrup et al. 1995, Amstrup 2000).As human populations increase and demands for polar bears and other arctic resources escalate, managers must know the sizes and distributions of the polar bear populations. Resource managers also need reliable estimates of breeding rates, reproductive intervals, litter sizes, and survival of young and adults.Our objectives for this research were 1) to determine the seasonal and annual movements of polar bears in the Beaufort Sea, 2) to define the boundaries of the population(s) using this region, 3) to determine the size and status of the Beaufort Sea polar bear population, and 4) to establish reproduction and survival rates (Amstrup 2000).

  19. FAST NEUTRON SPECTROMETER

    Science.gov (United States)

    Davis, F.J.; Hurst, G.S.; Reinhardt, P.W.

    1959-08-18

    An improved proton recoil spectrometer for determining the energy spectrum of a fast neutron beam is described. Instead of discriminating against and thereby"throwing away" the many recoil protons other than those traveling parallel to the neutron beam axis as do conventional spectrometers, this device utilizes protons scattered over a very wide solid angle. An ovoidal gas-filled recoil chamber is coated on the inside with a scintillator. The ovoidal shape of the sensitive portion of the wall defining the chamber conforms to the envelope of the range of the proton recoils from the radiator disposed within the chamber. A photomultiplier monitors the output of the scintillator, and a counter counts the pulses caused by protons of energy just sufficient to reach the scintillator.

  20. Neutron Diffraction Studies of Nuclear Magnetic Ordering in Copper

    DEFF Research Database (Denmark)

    Jyrkkiö, T.A.; Huiku, M.T.; Siemensmeyer, K.

    1989-01-01

    We have constructed a two-stage nuclear demagnetization cryostat for neutron diffraction studies of nuclear magnetism in copper. The cryostat is combined with a two-axis neutron spectrometer which can use both polarized and unpolarized neutrons. By demagnetizing highly polarized copper nuclear...... spins, the nuclei could be cooled below the ordering temperatureT N≃60 nK, while keeping the lattice at a considerably higher temperature between 50 and 100 µK. The neutron beam increases the lattice temperature in the sample by a factor of two or more, thereby considerably shortening the time...... for measurements in the ordered state; both our calculations and the experiments yield 1 nW beam heating. Polarized neutron experiments show that the scattered intensities from the strong fcc reflections are severely reduced by extinction. This makes the sample not very suitable for further studies with polarized...

  1. Development of a bandwidth limiting neutron chopper for CSNS

    Science.gov (United States)

    Wang, P.; Yang, B.; Cai, W. L.

    2015-08-01

    Bandwidth limiting neutron choppers are indispensable key equipments for the time-of-flight neutron scattering spectrometers of China Spallation Neutron Source (CSNS). The main principle is to chop the neutron beam to limit the neutron wavelength bandwidth at the neutron detector. We have successfully developed a bandwidth limiting neutron chopper for CSNS in the CSNS advance research project II. The transmission rate of the neutron absorbing coating is less than 1×10-4 (for 1 angstrom neutron). The phase control accuracy is ±0.084° (±9.4 μs at 25 Hz). The dynamic balance grade is G1.0. Various experimental technical features have met the design requirements, and it also runs stably and reliably during the long-term tests.

  2. Development of a bandwidth limiting neutron chopper for CSNS

    International Nuclear Information System (INIS)

    Wang, P.; Yang, B.; Cai, W.L.

    2015-01-01

    Bandwidth limiting neutron choppers are indispensable key equipments for the time-of-flight neutron scattering spectrometers of China Spallation Neutron Source (CSNS). The main principle is to chop the neutron beam to limit the neutron wavelength bandwidth at the neutron detector. We have successfully developed a bandwidth limiting neutron chopper for CSNS in the CSNS advance research project II. The transmission rate of the neutron absorbing coating is less than 1×10 −4 (for 1 angstrom neutron). The phase control accuracy is ±0.084° (±9.4 μs at 25 Hz). The dynamic balance grade is G1.0. Various experimental technical features have met the design requirements, and it also runs stably and reliably during the long-term tests

  3. Neutron sensitivity improvement in boron-lined proportional counters

    International Nuclear Information System (INIS)

    Dighe, P.M.; Prasad, K.R.; Kataria, S.K.

    2002-01-01

    Various techniques have been employed to improve the neutron sensitivity of boron-coated proportional counters developed indigenously. A boron-lined proportional counter (67 mm ID x 750 mm length) of 17 cps/nv thermal neutron sensitivity is developed by coating 92% enriched 10 B on the inner wall of the counter. This counter can be used for low thermal neutron flux (∼0.2 nv) at various applications such as neutron area monitoring, reactor start-up instrumentation, assay of fissile materials and detection of fuel failure. An improvement in sensitivity was also achieved by summing the output signals from four 10 B lined counters and two BF 3 proportional counters. The summation did not change the susceptibility of the device to gamma interference. In view of the scarcity of enriched 10 B isotope, indigenously available natural boron coated two prototype proportional counters are developed of 0.8 cps/nv and 1.1 cps/nv thermal neutron sensitivity. Efforts have been made to improve the sensitivity with boron coated 3-dimensional structures introduced into the sensitive volume. Tests in thermal neutron flux showed 50% improvement in the sensitivity due to the introduction of additional boron coated wires. Another counter with 51 boron-coated annular discs (23 mm OD X 10 mm ID X 1 mm thick) mounted perpendicular to the axis of the cathode showed 1.7 cps/nv neutron sensitivity, an improvement by a factor of 2.5. (author)

  4. Neutron detector

    Science.gov (United States)

    Stephan, Andrew C [Knoxville, TN; Jardret,; Vincent, D [Powell, TN

    2011-04-05

    A neutron detector has a volume of neutron moderating material and a plurality of individual neutron sensing elements dispersed at selected locations throughout the moderator, and particularly arranged so that some of the detecting elements are closer to the surface of the moderator assembly and others are more deeply embedded. The arrangement captures some thermalized neutrons that might otherwise be scattered away from a single, centrally located detector element. Different geometrical arrangements may be used while preserving its fundamental characteristics. Different types of neutron sensing elements may be used, which may operate on any of a number of physical principles to perform the function of sensing a neutron, either by a capture or a scattering reaction, and converting that reaction to a detectable signal. High detection efficiency, an ability to acquire spectral information, and directional sensitivity may be obtained.

  5. Fusion neutronics

    CERN Document Server

    Wu, Yican

    2017-01-01

    This book provides a systematic and comprehensive introduction to fusion neutronics, covering all key topics from the fundamental theories and methodologies, as well as a wide range of fusion system designs and experiments. It is the first-ever book focusing on the subject of fusion neutronics research. Compared with other nuclear devices such as fission reactors and accelerators, fusion systems are normally characterized by their complex geometry and nuclear physics, which entail new challenges for neutronics such as complicated modeling, deep penetration, low simulation efficiency, multi-physics coupling, etc. The book focuses on the neutronics characteristics of fusion systems and introduces a series of theories and methodologies that were developed to address the challenges of fusion neutronics, and which have since been widely applied all over the world. Further, it introduces readers to neutronics design’s unique principles and procedures, experimental methodologies and technologies for fusion systems...

  6. Hydrogen dynamics in Na3AlH6: A combined density functional theory and quasielastic neutron scattering study

    DEFF Research Database (Denmark)

    Zsigmond, G.; Manoshin, S.; Lieutenant, K.

    2007-01-01

    Handling of polarization became very important in simulations of neutron scattering. One of the very comprehensive and open-source neutron simulation package, VITESS, has been intensely involved in polarized neutron simulations. Several examples will be shown here. Another similar package NISP also...

  7. Asymmetrically and symmetrically coated tapered optical fiber for sensing applications

    Science.gov (United States)

    Del Villar, Ignacio; Socorro, Abian B.; Corres, Jesus M.; Arregui, Francisco J.; Matias, Ignacio R.

    2015-09-01

    The deposition of a non-metallic thin-film in a symmetrically coated tapered optical fiber leads to the generation of resonances due to guidance of a mode in the thin-film. At certain conditions, the resonances overlap each other, which can be avoided with an asymmetric coated tapered optical fiber, which permits to obtain resonances for TM and TE polarization separately. Numerical results showing the sensitivity to coating thickness and surrounding medium refractive index are also presented for both polarizations.

  8. The neutron

    International Nuclear Information System (INIS)

    Cheetham, A.K.

    1990-01-01

    In 1932, when Chadwick obtained the first unambiguous evidence for the existence of the neutron, his discovery confirmed the widely held belief that there existed a particle with zero charge and a mass similar to that of the proton. Indeed, as early as 1920, Lord Rutherford had suggested such a possibility in a lecture to the Royal Society. The discovery of the neutron had an immediate and dramatic impact in several areas. The nucleus, which had hitherto been regarded, somewhat unsatisfactorily, as a combination of protons and electrons, was now seen as comprising of protons and neutrons. This in turn lead to a proper understanding of the nature of isotopes and provided a fresh basis for nuclear theories. This paper examines the nature and properties of the neutron, and describes some facets of its remarkable role in contemporary science and technology. The aspects covered are its properties, the production and detection of neutrons, the reactions between neutrons and nuclei, fission reactions, neutron scattering, pulsed neutron scattering and neutron spectroscopy. (author)

  9. Atmospheric neutrons

    International Nuclear Information System (INIS)

    Preszler, A.M.; Moon, S.; White, R.S.

    1976-01-01

    Additional calibrations of the University of California double-scatter neutron and additional analysis corrections lead to the slightly changed neutron fluxes reported here. The theoretical angular distributions of Merker (1975) are in general agreement with our experimental fluxes but do not give the peaks for vertical upward and downward moving neutrons. The theoretical neutron escape current J 2 /sub pi/ (Merker, 1972; Armstrong et al., 1973) is in agreement with the experimental values from 10 to 100 MeV. Our experimental fluxes agree with those of the Kanbach et al. (1974) in the overlap region from 70 to 100 MeV

  10. Conducting Polymers for Neutron Detection

    International Nuclear Information System (INIS)

    Clare Kimblin; Kirk Miller; Bob Vogel; Bill Quam; Harry McHugh; Glen Anthony; Steve Jones; Mike Grover

    2007-01-01

    Conjugated polymers have emerged as an attractive technology for large-area electronic applications. As organic semiconductors, they can be used to make large-area arrays of diodes or transistors using fabrication techniques developed for polymer coatings, such as spraying and screen-printing. We have demonstrated both neutron and alpha detection using diodes made from conjugated polymers and have done preliminary work to integrate a boron carbide layer into the conventional polymer device structure to capture thermal neutrons. The polymer devices appear to be insensitive to gamma rays, due to their small physical thickness and low atomic number

  11. Conducting Polymers for Neutron Detection

    Energy Technology Data Exchange (ETDEWEB)

    Kimblin, Clare; Miller, Kirk; Vogel, Bob; Quam, Bill; McHugh, Harry; Anthony, Glen; Mike, Grover

    2007-12-01

    Conjugated polymers have emerged as an attractive technology for large-area electronic applications. As organic semiconductors, they can be used to make large-area arrays of diodes or transistors using fabrication techniques developed for polymer coatings, such as spraying and screen-printing. We have demonstrated both neutron and alpha detection using diodes made from conjugated polymers and have done preliminary work to integrate a boron carbide layer into the conventional polymer device structure to capture thermal neutrons. The polymer devices appear to be insensitive to gamma rays, due to their small physical thickness and low atomic number.

  12. Irradiation performance of thorium oxide based coated particle fuels

    International Nuclear Information System (INIS)

    Shiratori, Tetsuo; Itoh, Akinori; Akabori, Mitsuo; Shiba, Koreyuki; Adachi, Mamoru

    1988-11-01

    BISO coated ThO 2 particles as fertile fuel and BISO or TRISO coated (Th, U)O 2 particles as fissile fuel for a High-temperature Gas-cooled Reactor (HTGR) were irradiated to investigate particle performances in loosely-packed condition of two capsules in JRR-2 and one capsule in JMTR. Irradiation of these coated particles was achieved to a maximum fast neutron fluence of 2.22 x 10 21 neutrons/cm 2 (E > 0.18 MeV) and a maximum thermal neutron fluence of 1.35 x 10 21 neutrons/cm 2 at temperatures of 770 to 1225 deg C. And a maximum burnup of fissile particles was 2.42 % FIMA. It was found in the post-irradiation examinations that the coated particles were intact except a little of the BISO coated fissile particles, and the thorium oxide based coated particles performed well under the irradiation conditions. The data were also taken on the fission product behavior released from the fuel kernels during the irradiation. And density of the outer LTIPyC (OPyC) increased as increasing the fluence of fast neutron. As a result of the densification of the OPyC, the crushing strength of the BISO coated particles increased, otherwise the TRISO coated particles decreased. (author)

  13. A remanent Fe/Si supermirror transmission polarizer

    CERN Document Server

    Stahn, J

    2002-01-01

    In order to develop a neutron spin polarizer on the basis of magnetically remanent supermirrors, we produced a first Fe/Si supermirror (m=2, q=0.044 A sup - sup 1) giving polarizations of 96% to 98%. The addition of the reactive gases O sub 2 and N sub 2 to Si reduced the stress in the supermirror and improved the matching of Si and Fe for spin-down neutrons. (orig.)

  14. J-NSE: Neutron spin echo spectrometer

    Directory of Open Access Journals (Sweden)

    Olaf Holderer

    2015-08-01

    Full Text Available Neutron Spin-Echo (NSE spectroscopy is well known as the only neutron scattering technique that achieves energy resolution of several neV. By using the spin precession of polarized neutrons in magnetic field one can measure tiny velocity changes of the individual neutron during the scattering process. Contrary to other inelastic neutron scattering techniques, NSE measures the intermediate scattering function S(Q,t in reciprocal space and time directly. The Neutron Spin-Echo spectrometer J-NSE, operated by JCNS, Forschungszentrum Jülich at the Heinz Maier-Leibnitz Zentrum (MLZ in Garching, covers a time range (2 ps to 200 ns on length scales accessible by small angle scattering technique. Along with conventional NSE spectroscopy that allows bulk measurements in transmission mode, J-NSE offers a new possibility - gracing incidence spin echo spectroscopy (GINSENS, developed to be used as "push-button" option in order to resolve the depth dependent near surface dynamics.

  15. (International Collaboration on Advanced Neutron Sources)

    Energy Technology Data Exchange (ETDEWEB)

    Hayter, J.B.

    1990-11-08

    The International Collaboration on Advanced Neutron Sources was started about a decade ago with the purpose of sharing information throughout the global neutron community. The collaboration has been extremely successful in optimizing the use of resources, and the discussions are open and detailed, with reasons for failure shared as well as reasons for success. Although the meetings have become increasingly oriented toward pulsed neutron sources, many of the neutron instrumentation techniques, such as the development of better monochromators, fast response detectors and various data analysis methods, are highly relevant to the Advanced Neutron Source (ANS). I presented one paper on the ANS, and another on the neutron optical polarizer design work which won a 1989 R D-100 Award. I also gained some valuable design ideas, in particular for the ANS hot source, in discussions with individual researchers from Canada, Western Europe, and Japan.

  16. Neutron dosimetry; Dosimetria de neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Fratin, Luciano

    1993-12-31

    A neutron irradiation facility was designed and built in order to establish a procedure for calibrating neutron monitors and dosemeters. A 185 GBq {sup 241} Am Be source of known is used as a reference source. The irradiation facility using this source in the air provides neutron dose rates between 9 nSv s{sup -1} and 0,5 {sup {mu}}Sv s{sup -1}. A calibrated 50 nSv s{sup -1} thermal neutron field is obtained by using a specially designed paraffin block in conjunction with the {sup 241} Am Be source. A Bonner multisphere spectrometer was calibrated, using a procedure based on three methods proposed by international standards. The unfold {sup 241} Am Be neutron spectrum was determined from the Bonner spheres data and resulted in a good agreement with expected values for fluence rate, dose rate and mean energy. A dosimetric system based on the electrochemical etching of CR-39 was developed for personal dosimetry. The dosemeter badge using a (n,{alpha}) converter, the etching chamber and high frequency power supply were designed and built specially for this project. The electrochemical etching (ECE) parameters used were: a 6N KOH solution, 59 deg C, 20 kV{sub pp} cm{sup -1}, 2,0 kHz, 3 hours of ECE for thermal and intermediate neutrons and 6 hours for fast neutrons. The calibration factors for thermal, intermediate and fast neutrons were determined for this personal dosemeter. The sensitivities determined for the developed dosimetric system were (1,46{+-} 0,09) 10{sup 4} tracks cm{sup -2} mSv{sup -1} for thermal neutrons, (9{+-}3) 10{sup 2} tracks cm{sup -2} mSV{sup -1} for intermediate neutrons and (26{+-}4) tracks cm{sup -2} mSv{sup -1} for fast neutrons. The lower and upper limits of detection were respectively 0,002 mSv and 0,6 mSv for thermal neutrons, 0,04 mSv and 8 mSv for intermediate neutrons and 1 mSv and 12 mSv for fast neutrons. In view of the 1990`s ICRP recommendations, it is possible to conclude that the personal dosemeter described in this work is

  17. Approaches to ultrafast neutron detectors

    International Nuclear Information System (INIS)

    Wang, C.L.; Kalibjian, R.; Singh, M.S.

    1984-01-01

    We discuss two approaches to obtain detectors of very high temporal resolution. In the first approach, uranium-coated cathode is used in a streak tube configuration. Secondary electrons accompanying the fission fragments from a neutron-uranium reaction are accelerated, focussed and energy analyzed through a pinhole and streaked. Calculations show that 20 ps time-resolution can be obtained. In the second approach, a uranium-coated cathode is integrated into a transmission line. State-of-the-art technology indicates that time resolution of 20 ps can be obtained by gating the cathode with a fast electric pulse

  18. Neutron energy focusing with magnetic fields

    International Nuclear Information System (INIS)

    Schwab, D.E.; Summhammer, J.; Rauch, H.

    2001-01-01

    Full text: For the majority of neutron optics instruments and many neutron scattering techniques the use of a monochromatic neutron beam is vitally important. Most monochromators are passive, and often include an interaction with matter. They cut off certain parts of the spectrum, and as a consequence, large losses of neutron density occur, and the spectral density is depleted as well. On the other hand, active energy focusing systems enrich the beam in a very narrow velocity band without considerable losses. Here, we study the active monochromatization of neutrons, generated at a pulsed neutron source by interaction with magnetic fields. The first proposed set-up consists of magnets which surround the beam-line. They produce traveling magnetic waves with desired velocity to escort a neutron pulse between the source and an instrument. During the interaction, the magnetic field forces the neutrons to accelerate or decelerate to this velocity. Simulations show that a comoving magnetic field, shaped like an harmonic oscillator, or of a sinusoidal form, effectuates an increase of neutron intensity up to an order of magnitude in a small but variable velocity band. Consequently, the precision of related neutron scattering experiments is increased or their measurement time is decreased, accordingly. Another concept arises from static and rf spinflip stages. Thereby, an appropriate number of photons of the rf-field can be transmitted to or extracted from the neutrons. Polarized neutrons entering a static magnetic field which is oriented perpendicularly to the neutrons propagation direction, are subject to acceleration or deceleration depending on their spin orientation (Zeeman shift). Flipping the neutrons spin by on rf coil inside the static field, causes a second acceleration or deceleration of the neutrons when they are leaving the static field. They immediately enter the next stage with another static field, which is much smaller than the one they have just left. Its

  19. Neutron absorbing article and method for manufacture thereof

    International Nuclear Information System (INIS)

    Forsyth, P.F.; Mcmurtry, C.H.; Naum, R.G.

    1980-01-01

    A composite, neutron absorbing, coated article, suitable for installation in storage racks for spent nuclear fuel and for other neutron absorbing applications, includes a backing member, preferably of flexible material such as woven fiberglass cloth, a synthetic organic polymeric coating or a plurality of such coatings on the backing member, preferably of cured phenolic resin, such as phenol formaldehyde or trimethylolphenol formaldehyde and boron carbide particles held to the backing member by the cured coating or a plurality of such coatings. Also within the invention is a method for the manufacture of the neutron absorbing coated article and the use of such an article. In a preferred method the backing member is first coated on both sides thereof with a filling coating of thermosettable liquid phenolic resin, which is then partially cured to solid state, one side of the backing member is then coated with a mixture of thermosettable liquid resin and finely divided boron carbide particles and the resin is partially cured to solid state, the other side is coated with a similar mixture, larger boron carbide particles are applied to it and the resin is partially cured to solid state, such side of the article is coated with thermosettable liquid phenolic resin, the resin is partially cured to solid state and such resin, including previously applied partially cured resins, is cured to final cross-linked and permanently set form

  20. Neutronic reactor

    International Nuclear Information System (INIS)

    Wende, C.W.J.

    1976-01-01

    A safety rod for a nuclear reactor has an inner end portion having a gamma absorption coefficient and neutron capture cross section approximately equal to those of the adjacent shield, a central portion containing materials of high neutron capture cross section and an outer end portion having a gamma absorption coefficient at least equal to that of the adjacent shield

  1. Neutron diffraction

    International Nuclear Information System (INIS)

    Bacon, G.E.

    1983-01-01

    The paper reviews neutron diffraction work from the early studies to the present-day development of the subject. Direct structural investigations were described, including chemical applications associated with single crystal techniques, and magnetic applications identified with powder techniques. The properties of the neutron beams are discussed, as well as the use of polarised beams. (UK)

  2. Neutron holography

    International Nuclear Information System (INIS)

    Beynon, T.D.

    1986-01-01

    the paper concerns neutron holography, which allows an image to be constructed of the surfaces, as well as the interiors, of objects. The technique of neutron holography and its applications are described. Present and future use of the method is briefly outlined. (U.K.)

  3. The University of Texas Cold Neutron Source

    International Nuclear Information System (INIS)

    Uenlue, Kenan; Rios-Martinez, Carlos; Wehring, B.W.

    1994-01-01

    A cold neutron source has been designed, constructed, and tested by the Nuclear Engineering Teaching Laboratory (NETL) at The University of Texas at Austin. The Texas Cold Neutron Source (TCNS) is located in one of the beam ports of the NETL 1-MW TRIGA Mark II research reactor. The main components of the TCNS are a cooled moderator, a heat pipe, a cryogenic refrigerator, and a neutron guide. 80 ml of mesitylene moderator are maintained at about 30 K in a chamber within the reactor graphite reflector by the heat pipe and cryogenic refrigerator. The heat pipe is a 3-m long aluminum tube that contains neon as the working fluid. The cold neutrons obtained from the moderator are transported by a curved 6-m long neutron guide. This neutron guide has a radius of curvature of 300 m, a 50x15 mm cross-section, 58 Ni coating, and is separated into three channels. The TCNS will provide a low-background subthermal neutron beam for neutron capture and scattering research. After the installation of the external portion of the neutron guide, a neutron focusing system and a Prompt Gamma Activation Analysis facility will be set up at the TCNS. ((orig.))

  4. Method to produce a neutron shielding

    International Nuclear Information System (INIS)

    Merkle, H.J.

    1978-01-01

    The neutron shielding for armoured vehicles consists of preshaped plastic plates which are coated on the armoured vehicle walls by conversion of the thermoplast. Suitable plastics or thermoplasts are PVC, PVC acetate, or mixtures of these, into which more than 50% B, B 4 C, or BN is embedded. The colour of the shielding may be determined by the choice of the neutron absorber, e.g. a white colour for BN. The plates are produced using an extruder or calender. (DG) [de

  5. Neutron tubes

    Science.gov (United States)

    Leung, Ka-Ngo [Hercules, CA; Lou, Tak Pui [Berkeley, CA; Reijonen, Jani [Oakland, CA

    2008-03-11

    A neutron tube or generator is based on a RF driven plasma ion source having a quartz or other chamber surrounded by an external RF antenna. A deuterium or mixed deuterium/tritium (or even just a tritium) plasma is generated in the chamber and D or D/T (or T) ions are extracted from the plasma. A neutron generating target is positioned so that the ion beam is incident thereon and loads the target. Incident ions cause D-D or D-T (or T-T) reactions which generate neutrons. Various embodiments differ primarily in size of the chamber and position and shape of the neutron generating target. Some neutron generators are small enough for implantation in the body. The target may be at the end of a catheter-like drift tube. The target may have a tapered or conical surface to increase target surface area.

  6. Neutron source

    Science.gov (United States)

    Cason, J.L. Jr.; Shaw, C.B.

    1975-10-21

    A neutron source which is particularly useful for neutron radiography consists of a vessel containing a moderating media of relatively low moderating ratio, a flux trap including a moderating media of relatively high moderating ratio at the center of the vessel, a shell of depleted uranium dioxide surrounding the moderating media of relatively high moderating ratio, a plurality of guide tubes each containing a movable source of neutrons surrounding the flux trap, a neutron shield surrounding one part of each guide tube, and at least one collimator extending from the flux trap to the exterior of the neutron source. The shell of depleted uranium dioxide has a window provided with depleted uranium dioxide shutters for each collimator. Reflectors are provided above and below the flux trap and on the guide tubes away from the flux trap.

  7. Neutron reflectometry

    DEFF Research Database (Denmark)

    Klösgen-Buchkremer, Beate Maria

    2014-01-01

    Neutron (and X-ray) reflectometry constitute complementary interfacially sensitive techniques that open access to studying the structure within thin films of both soft and hard condensed matter. Film thickness starts oxide surfaces on bulk substrates, proceeding to (pauci-)molecular layers and up...... to hundreds of nanometers. Thickness resolution for flat surfaces is in the range of few Ǻngstrøm, and as a peculiar benefit, the presence and properties of buried interfaces are accessible. Focus here will be on neutron reflectometry, a technique that is unique in applications involving composite organic...... films or films with magnetic properties. The reason is the peculiar property of neutron light since the mass of a neutron is close to the one of a proton, and since it bears a magnetic moment. The optical properties of matter, when interacting with neutrons, are described by a refractive index...

  8. Neutron source

    International Nuclear Information System (INIS)

    Cason, J.L. Jr.; Shaw, C.B.

    1975-01-01

    A neutron source which is particularly useful for neutron radiography consists of a vessel containing a moderating media of relatively low moderating ratio, a flux trap including a moderating media of relatively high moderating ratio at the center of the vessel, a shell of depleted uranium dioxide surrounding the moderating media of relatively high moderating ratio, a plurality of guide tubes each containing a movable source of neutrons surrounding the flux trap, a neutron shield surrounding one part of each guide tube, and at least one collimator extending from the flux trap to the exterior of the neutron source. The shell of depleted uranium dioxide has a window provided with depleted uranium dioxide shutters for each collimator. Reflectors are provided above and below the flux trap and on the guide tubes away from the flux trap

  9. Polarized nuclei in plastic scintillators: a new class of polarized targets

    Science.gov (United States)

    van den Brandt, B.; Bunyatova, E. I.; Hautle, P.; Konter, J. A.; Mango, S.; Nemchonok, I. B.

    2001-06-01

    Polarized scintillating targets are now routinely available: protons, deuterons or other nuclei in blocks of scintillating organic polymer, doped with the free radical TEMPO, are polarized dynamically in a field of 2.5 T in a vertical 3He-4He dilution refrigerator. A 19 mm diameter plastic lightguide transports the scintillation light from the sample in the mixing chamber to a photomultiplier outside the cryostat. Sizeable nuclear polarizations have been achieved newly in boron enriched polystyrene-based scintillating material. A scintillator target with high detection sensitivity for low energy neutrons has been so made available, in which both protons and boron nuclei are polarized. .

  10. T-noninvariant correlations in neutron experiments

    International Nuclear Information System (INIS)

    Belyaev, B.N.

    1999-01-01

    Methods of measuring T-violation effects induced by neutrons passing through a polarized and an aligned nuclear target are analyzed using time-dependent neutron spin wave functions. For the first target the relationships between the polarizations and asymmetries obtained in this analysis are consistent with the structural Kabir relationships which allow one to study the pure effect. It is found that the weak interaction effects, which are background in these experiments, are suppressed when the T-odd and strong effects interfere. It is shown that for the aligned target the polarization-asymmetry relations also exist and allow one to distinguish the pure P-even and T-odd effect. Moreover, in this case the effect can be found making use of the different dependence of the effect and background on the angle formed by the alignment axis and the neutron momentum [ru

  11. Performance of neutron polarimeter SMART-NPOL

    International Nuclear Information System (INIS)

    Noji, S.; Miki, K.; Yako, K.; Kawabata, T.; Kuboki, H.; Sakai, H.; Sekiguchi, K.; Suda, K.

    2007-01-01

    The neutron polarimeter SMART-NPOL has been constructed at the RIKEN Accelerator Research Facility for measuring polarization correlations of proton-neutron systems. The SMART-NPOL system consists of 12 parallel neutron counter planes of two dimensionally position-sensitive plastic scintillators with a size of 60x60x3.0cm 3 . Polarimetry measurements were made using the analyzing power of the H1(n-vector,n)H1 reaction occurring in the plastic scintillators. The effective analyzing power of SMART-NPOL was measured with polarized neutrons from the zero-degree Li6(d-vector,n-vector) reaction with an incident deuteron energy of 135MeV/A. The effective analyzing power thus obtained was 0.26±0.01 stat ±0.03 syst and the double scattering efficiency was 1.1x10 -3

  12. Titanium-Aluminum Oxide Coating on Aluminized Steel

    OpenAIRE

    Fuyan Sun; Guang Wang; Xueyuan Nie

    2014-01-01

    In this study, a plasma electrolytic oxidation (PEO) process was used to form titanium-aluminum oxide coating on aluminized steel. The present work was mainly to study the effects of treatment time of PEO process on properties of the titanium coating. A potentiodynamic polarization corrosion test was employed to investigate the corrosion resistance of the coating. The friction coefficient and wear resistance of the coating were studied by using pin-on-disc test. The thermal transfer behaviors...

  13. Political polarization

    OpenAIRE

    Dixit, Avinash K.; Weibull, Jörgen W.

    2007-01-01

    Failures of government policies often provoke opposite reactions from citizens; some call for a reversal of the policy, whereas others favor its continuation in stronger form. We offer an explanation of such polarization, based on a natural bimodality of preferences in political and economic contexts and consistent with Bayesian rationality.

  14. Political polarization.

    Science.gov (United States)

    Dixit, Avinash K; Weibull, Jörgen W

    2007-05-01

    Failures of government policies often provoke opposite reactions from citizens; some call for a reversal of the policy, whereas others favor its continuation in stronger form. We offer an explanation of such polarization, based on a natural bimodality of preferences in political and economic contexts and consistent with Bayesian rationality.

  15. Neutron diffraction

    International Nuclear Information System (INIS)

    James, M.; Howard, C.J.; Kennedy, S.

    1999-01-01

    Diffraction methods, especially X-ray diffraction, are widely used in materials science. Neutron diffraction is in many ways similar to X-ray diffraction, but is also complementary to the X-ray technique so that in some cases it yields information not accessible using X-rays. Successes of neutron diffraction include the elucidation of the crystal structures of high temperature superconductors and materials that display colossal magnetoresistance, the phase analysis of zirconia engineering ceramics, in depth stress determination in composites, successful determination of the structures of metal hydrides, transition metal polymer complexes and the determination of magnetic structure. A brief description of current studies, using neutron diffraction is given

  16. Neutron diffraction and optics in noncentrosymmetric crystals New feasibility of a search for neutron EDM

    International Nuclear Information System (INIS)

    Fedorov, V.V.; Voronin, V.V.

    2003-01-01

    Recently strong electric fields (up to 10 9 V/cm) have been discovered, which affect the neutrons moving in noncentrosymmetric crystals. Such fields allow for new polarization phenomena in the neutron diffraction and in the optics and provide, for instance, a new method of a search for the neutron electric dipole moment (EDM). A strong interplanar electric field of the crystal and a sufficiently long time for the neutron passage through the crystal for Bragg angle close to π/2 in the case of Laue diffraction make it possible to exceed the sensitivity achieved with the magnetic resonance method using ultra cold neutrons (UCN method). The pilot setup has been created and mounted at the neutron beam at the WWR-M reactor in Gatchina. It allows to study the optics and the dynamical diffraction of polarized neutrons in thick (1-10 cm) crystals, using the direct diffraction beam and Bragg angles close to 90 deg. . The first experimental results are discussed on observing new effects in both the Laue diffraction and the optics of cold neutrons. These results confirm the opportunity to increase more than by an order of magnitude the sensitivity of the method to neutron EDM, using the diffraction angles close to 90 deg. and give a real prospect to exceed the sensitivity of the UCN method

  17. Research using ultracold neutrons at the ILL

    International Nuclear Information System (INIS)

    Steyerl, A.

    1990-01-01

    In this talk I will make no effort to give an exhaustive, detailed description of the well-published results of recent work with ultracold neutrons (UCN) at the ILL. Instead, there will be a biased selection of some topics in which author happens to be most interested, though in some cases as a spectator from a considerable distance than as an actor. The selection includes the recent lifetime experiment using a Fomblin-coated bottle, the continuing search for an electric dipole moment of the neutron and some ideas on high precision neutron optics experiments

  18. Dual neutron flux/temperature measurement sensor

    Science.gov (United States)

    Mihalczo, John T.; Simpson, Marc L.; McElhaney, Stephanie A.

    1994-01-01

    Simultaneous measurement of neutron flux and temperature is provided by a single sensor which includes a phosphor mixture having two principal constituents. The first constituent is a neutron sensitive 6LiF and the second is a rare-earth activated Y203 thermophosphor. The mixture is coated on the end of a fiber optic, while the opposite end of the fiber optic is coupled to a light detector. The detected light scintillations are quantified for neutron flux determination, and the decay is measured for temperature determination.

  19. The UNH polarized 3He program

    International Nuclear Information System (INIS)

    Hersman, F. W.; Carrier, R. H.; Pomeroy, V. R.

    1998-01-01

    The UNH Nuclear Physics Group is developing polarized 3 He cells for use in approved experiments with electron beams and neutron beams. We also have begun to apply our expertise to magnetic resonance imaging experiments I list our projects and review several areas where we have been focusing our efforts

  20. Parity-violation effects in neutron diffraction

    International Nuclear Information System (INIS)

    Zaretskii, D.F.; Sirotkin, V.K.

    1984-01-01

    The effects of parity violation in polarized-neutron diffraction by nuclei are considered. It is shown that the case of dynamical Laue diffraction exhibits significantly enhanced parity-violation effects, and that this enhancement is due to a pendulum-type dependence of the diffracted-beam intensity on the thickness. The effects are estimated for a number of nuclei in the case of thermal neutrons

  1. Circular polarization measurements with a Ge(Li) detector

    DEFF Research Database (Denmark)

    Kopecký, J.; Warming, Inge Elisabeth

    1969-01-01

    This paper presents the results obtained in measurements of the degree of circular polarization of gamma transitions to bound states of 33S, 36Cl, 49Ti, 56Mn, 57Fe, 60Co and 64Cu following the capture of polarized thermal neutrons. Spin values have been determined on the basis of these results....

  2. Superconducting polarizing magnet for a movable polarized target

    International Nuclear Information System (INIS)

    Anishchenko, N.G.; Bartenev, V.D.; Blinov, N.A.

    1998-01-01

    The superconducting polarizing magnet was constructed for the JINR (Dubna) movable polarized target (MPT) with working volume 200 mm long and 30 mm in diameter. The magnet provides a polarizing magnetic field up to 6 T in the centre with the uniformity of 4.5 x 10 -4 in the working volume of the target. The magnet contains a main solenoidal winding 558 mm long and 206/144 mm in diameters, and compensating and correcting winding placed at its ends. The windings are made of a NbTi wire, impregnated with the epoxy resin and placed in the horizontal cryostat. The diameter of the 'warm' aperture of the magnet cryostat is 96 mm. The design and technology of the magnet winding are described. Results of the magnetic field map measurements, using a NMR-magnetometer are given. A similar magnet constructed at DAPNIA, CEA/Saclay (France), represented a model for the present development. The MPT array is installed in the beam line of polarized neutrons produced by break-up of polarized deuterons extracted from the synchrophasotron of the Laboratory of High Energies (LHE), JINR (Dubna)

  3. Neutron scattering

    International Nuclear Information System (INIS)

    Furrer, A.

    1993-01-01

    This report contains the text of 16 lectures given at the Summer School and the report on a panel discussion entitled ''the relative merits and complementarities of x-rays, synchrotron radiation, steady- and pulsed neutron sources''. figs., tabs., refs

  4. Magnetic properties of neutron-star matter

    International Nuclear Information System (INIS)

    Chao, N.C.

    1975-01-01

    An array of qualitative and quantitative evidence is presented to the effect that neutron-star matter in its ground state is antiferromagnetic rather than ferromagnetic. The energy of pure neutron matter is evaluated as a function of spin polarization by a two-body Jastrow procedure, for densities up to five times that of ordinary nuclear matter. The anti-ferromagnetic state is energetically preferred to states with non-zero spin polarization, and lies considerably lower in energy than the ferromagnetic state. The magnetic susceptibility of the material is calculated as a function of density in the same approximation, with results which are in good agreement with independent estimates [pt

  5. REVIEWS OF TOPICAL PROBLEMS Small-angle neutron scattering in structure research of magnetic fluids

    Science.gov (United States)

    Avdeev, Mikhail V.; Aksenov, Viktor L.

    2011-01-01

    A magnetic fluid (MF) is a liquid dispersion of magnetic nanoparticles coated by surfactants for stabilization. The MF research reviewed in this paper is primarily aimed at investigating the atomic and magnetic structure of MF particles and the way they interact under various conditions by means of small-angle neutron scattering (SANS). The presence of a liquid carrier in the structure and the magnetic properties of MFs, which are very close to those of an ideal superparamagnetic system, allow the effective use of the major neutron scattering features: the strong effect of hydrogen-deuterium isotopic substitution and magnetic scattering. An extension of the contrast variation technique to the structure research on polydisperse and superparamagnetic systems is proposed. The cases of noninteracting and interacting particles, the latter with cluster formation taken into account, are considered for non-magnetized and magnetized MFs. The polarized neutron scattering analysis of the structure of magnetized MFs is illustrated by examples. Topical problems in further developing the method to study multiparameter systems are identified.

  6. Small-angle neutron scattering in structure research of magnetic fluids

    International Nuclear Information System (INIS)

    Avdeev, Mikhail V; Aksenov, Viktor L

    2011-01-01

    A magnetic fluid (MF) is a liquid dispersion of magnetic nanoparticles coated by surfactants for stabilization. The MF research reviewed in this paper is primarily aimed at investigating the atomic and magnetic structure of MF particles and the way they interact under various conditions by means of small-angle neutron scattering (SANS). The presence of a liquid carrier in the structure and the magnetic properties of MFs, which are very close to those of an ideal superparamagnetic system, allow the effective use of the major neutron scattering features: the strong effect of hydrogen-deuterium isotopic substitution and magnetic scattering. An extension of the contrast variation technique to the structure research on polydisperse and superparamagnetic systems is proposed. The cases of noninteracting and interacting particles, the latter with cluster formation taken into account, are considered for non-magnetized and magnetized MFs. The polarized neutron scattering analysis of the structure of magnetized MFs is illustrated by examples. Topical problems in further developing the method to study multiparameter systems are identified. (reviews of topical problems)

  7. Neutron Scattering

    International Nuclear Information System (INIS)

    Fayer, Michael J.; Gee, Glendon W.

    2005-01-01

    The neutron probe is a standard tool for measuring soil water content. This article provides an overview of the underlying theory, describes the methodology for its calibration and use, discusses example applications, and identifies the safety issues. Soil water makes land-based life possible by satisfying plant water requirements, serving as a medium for nutrient movement to plant roots and nutrient cycling, and controlling the fate and transport of contaminants in the soil environment. Therefore, a successful understanding of the dynamics of plant growth, nutrient cycling, and contaminant behavior in the soil requires knowledge of the soil water content as well as its spatial and temporal variability. After more than 50 years, neutron probes remain the most reliable tool available for field monitoring of soil water content. Neutron probes provide integrated measurements over relatively large volumes of soil and, with proper access, allow for repeated sampling of the subsurface at the same locations. The limitations of neutron probes include costly and time-consuming manual operation, lack of data automation, and costly regulatory requirements. As more non-radioactive systems for soil water monitoring are developed to provide automated profiling capabilities, neutron-probe usage will likely decrease. Until then, neutron probes will continue to be a standard for reliable measurements of field water contents in soils around the globe

  8. Plasma sprayed alumina coatings for radiation detector development

    Indian Academy of Sciences (India)

    In view of potential applications in neutron-sensitive ion chambers used in reactor control instru- mentation, studies were carried out on alumina 100 μ to 500 μ thick coatings on copper, aluminium and SS components. The electrical insulation varied from 10 ohms to 10. 骄 ohms for coating thick- nesses above 200 μ.

  9. Nuclear reactivity control using laser induced polarization

    International Nuclear Information System (INIS)

    Bowman, C.D.

    1990-01-01

    This patent describes a control element for reactivity control of a fission source provides an atomic density of 3 He in a control volume which is effective to control criticality as the 3 He is spin-polarized. Spin-polarization of the 3 He affects the cross section of the control volume for fission neutrons and hence, the reactivity. An irradiation source is directed within the 3 He for spin-polarizing the 3 He. An alkali-metal vapor may be included with the 3 He where a laser spin-polarizes the alkali-metal atoms which in turn, spin-couple with 3 He to spin-polarize the 3 He atoms

  10. A note on polarized light from magnetars

    Energy Technology Data Exchange (ETDEWEB)

    Capparelli, L.M.; Damiano, A.; Polosa, A.D. [Sapienza Universita di Roma, Dipartimento di Fisica, Rome (Italy); INFN, Rome (Italy); Maiani, L. [CERN, Theory Department, Geneva (Switzerland)

    2017-11-15

    In a recent paper it is claimed that vacuum birefringence has been experimentally observed for the first time by measuring the degree of polarization of visible light from a magnetar candidate, a neutron star with a magnetic field presumably as large as B ∝ 10{sup 13} G. The role of such a strong magnetic field is twofold. First, the surface of the star emits, at each point, polarized light with linear polarization correlated with the orientation of the magnetic field. Depending on the relative orientation of the magnetic axis of the star with the direction to the distant observer, a certain degree of polarization should be visible. Second, the strong magnetic field in the vacuum surrounding the star could enhance the effective degree of polarization observed: vacuum birefringence. We compare experimental data and theoretical expectations concluding that the conditions to support a claim of strong evidence of vacuum birefringence effects are not met. (orig.)

  11. FOREWORD: Neutron metrology Neutron metrology

    Science.gov (United States)

    Thomas, David J.; Nolte, Ralf; Gressier, Vincent

    2011-12-01

    The International Committee for Weights and Measures (CIPM) has consultative committees covering various areas of metrology. The Consultative Committee for Ionizing Radiation (CCRI) differs from the others in having three sections: Section (I) deals with radiation dosimetry, Section (II) with radionuclide metrology and Section (III) with neutron metrology. In 2003 a proposal was made to publish special issues of Metrologia covering the work of the three Sections. Section (II) was the first to complete their task, and their special issue was published in 2007, volume 44(4). This was followed in 2009 by the special issue on radiation dosimetry, volume 46(2). The present issue, volume 48(6), completes the trilogy and attempts to explain neutron metrology, the youngest of the three disciplines, the neutron only having been discovered in 1932, to a wider audience and to highlight the relevance and importance of this field. When originally approached with the idea of this special issue, Section (III) immediately saw the value of a publication specifically on neutron metrology. It is a topic area where papers tend to be scattered throughout the literature in journals covering, for example, nuclear instrumentation, radiation protection or radiation measurements in general. Review articles tend to be few. People new to the field often ask for an introduction to the various topics. There are some excellent older textbooks, but these are now becoming obsolete. More experienced workers in specific areas of neutron metrology can find it difficult to know the latest position in related areas. The papers in this issue attempt, without presenting a purely historical outline, to describe the field in a sufficiently logical way to provide the novice with a clear introduction, while being sufficiently up-to-date to provide the more experienced reader with the latest scientific developments in the different topic areas. Neutron radiation fields obviously occur throughout the nuclear

  12. Layer-by-layer magnetometry of polarizing supermirrors

    CERN Document Server

    Ruecker, U; Toperverg, B; Brueckel, T; Ott, F

    2002-01-01

    We investigate the remagnetization behaviour of remanent polarizing supermirrors by polarized neutron reflectometry. Such a mirror can be remagnetized in a magnetic field of 30 mT. It is shown, that at lower fields, the mirror is not completely remagnetized, but the magnetization of the thinner layers can be flipped more easily than the magnetization of the thicker layers. With polarized neutron reflectometry, we are able to find out exactly how many layers are magnetized parallel and how many are magnetized antiparallel to the external field. Furthermore, information about structural and magnetic imperfections (roughness, domain formation) is available. (orig.)

  13. Diagnostics of transparent polymer coatings of metal items

    Science.gov (United States)

    Varepo, L. G.; Ermakova, I. N.; Nagornova, I. V.; Kondratov, A. P.

    2017-08-01

    The methods of visual and instrumental express diagnostics of safety critical defects and non-uniform thickness of transparent mono- and multilayer polyolefin surface coating of metal items are analyzed in the paper. The instrumental diagnostics method relates to colorimetric measuring based on effects, which appear in the polarized light for extrusion polymer coatings. A color coordinates dependence (in the color system CIE La*b*) on both HDPE / PVC coating thickness fluctuation values (from average ones) and coating interlayer or adhesion layer delaminating is shown. A variation of color characteristics in the polarized light at a liquid penetration into delaminated polymer layers is found. Measuring parameters and critical uncertainties are defined.

  14. Dispersing surface-modified imogolite nanotubes in polar and non-polar solvents

    Science.gov (United States)

    Li, Ming; Brant, Jonathan A.

    2018-02-01

    Furthering the development of nanocomposite structures, namely membranes for water treatment applications, requires that methods be developed to ensure nanoparticle dispersion in polar and non-polar solvents, as both are widely used in associated synthesis techniques. Here, we report on a two-step method to graft polyvinylpyrrolidone (PVP), and a one-step method for octadecylphosphonic acid (OPA), onto the outer surfaces of imogolite nanotubes. The goal of these approaches was to improve and maintain nanotube dispersion in polymer compatible polar and non-polar solvents. The PVP coating modified the imogolite surface charge from positive to weakly negative at pH ≤ 9; the OPA made it weakly positive at acidic pH values to negative at pH ≥ 7. The PVP surface coating stabilized the nanotubes through steric hindrance in polar protic, dipolar aprotic, and chloroform. In difference to the PVP, the OPA surface coating allowed the nanotubes to be dispersed in n-hexane and chloroform, but not in the polar solvents. The lack of miscibility in the polar solvents, as well as the better dispersion in n-hexane, was attributed to the stronger hydrophobicity of the OPA polymer relative to the PVP. [Figure not available: see fulltext.

  15. Neutron diffraction studies of thin film multilayer structures

    Energy Technology Data Exchange (ETDEWEB)

    Majkrzak, C.F.

    1985-01-01

    The application of neutron diffraction methods to the study of the microscopic chemical and magnetic structures of thin film multilayers is reviewed. Multilayer diffraction phenomena are described in general and in particular for the case in which one of the materials of a bilayer is ferromagnetic and the neutron beam polarized. Recent neutron diffraction measurements performed on some interesting multilayer systems are discussed. 70 refs., 5 figs.

  16. Neutron diffraction studies of thin film multilayer structures

    International Nuclear Information System (INIS)

    Majkrzak, C.F.

    1985-01-01

    The application of neutron diffraction methods to the study of the microscopic chemical and magnetic structures of thin film multilayers is reviewed. Multilayer diffraction phenomena are described in general and in particular for the case in which one of the materials of a bilayer is ferromagnetic and the neutron beam polarized. Recent neutron diffraction measurements performed on some interesting multilayer systems are discussed. 70 refs., 5 figs

  17. Neutron spin optics: Fundamentals and verification

    Energy Technology Data Exchange (ETDEWEB)

    Pleshanov, N.K., E-mail: pleshanov_nk@pnpi.nrcki.ru

    2017-05-01

    Neutron spin optics (NSO) based on quantum aspects of the neutron interaction with magnetically anisotropic layers signifies transition in polarized neutron optics from 1D (spin selection) to 3D (spin manipulations). It may essentially widen the functionality of neutron optics. Among the advantages of NSO are compactness, zero-field option (guide fields are optional) and multi-functionality (beam spectrum, beam divergence and spin manipulations can be handled at the same time). Prospects in improving and developing neutron mirror spin turners (incl. flippers) are discussed. Two approaches to measurement of the efficiency of mirror flippers are introduced. The efficiency of a multilayer-backed neutron mirror flipper for monochromatic beams was found to be 97.5±0.5%. Such mirror flippers can combine monochromatization of a polarized beam with flipping spins of the monochromatized neutrons. To improve their performance, account of the spin-dependent refraction in the magnetic layer should be taken. For a monochromatic beam, supermirror-backed flippers are shown to be more advantageous, with a gain in intensity up to 4 times.

  18. Response of electret dosemeter to slow neutrons

    International Nuclear Information System (INIS)

    Ghilardi, A.J.P.; Pela, C.A.; Zimmerman, R.L.

    1987-01-01

    The response of the electret dosemeter to exposition of slow neutrons is studied. Different external coatings are used on the dosemeter (polyethylene, alminium, polyethylene + boron, aluminium + boron) and exposure curves (with and without water) are compared. (M.A.C.) [pt

  19. Neutron residual stress measurements in linepipe

    Science.gov (United States)

    Law, Michael; Gnaëpel-Herold, Thomas; Luzin, Vladimir; Bowie, Graham

    2006-11-01

    Residual stresses in gas pipelines are generated by manufacturing and construction processes and may affect the subsequent pipe integrity. In the present work, the residual stresses in eight samples of linepipe were measured by neutron diffraction. Residual stresses changed with some coating processes. This has special implications in understanding and mitigating stress corrosion cracking, a major safety and economic problem in some gas pipelines.

  20. Neutron residual stress measurements in linepipe

    International Nuclear Information System (INIS)

    Law, Michael; Gnaepel-Herold, Thomas; Luzin, Vladimir; Bowie, Graham

    2006-01-01

    Residual stresses in gas pipelines are generated by manufacturing and construction processes and may affect the subsequent pipe integrity. In the present work, the residual stresses in eight samples of linepipe were measured by neutron diffraction. Residual stresses changed with some coating processes. This has special implications in understanding and mitigating stress corrosion cracking, a major safety and economic problem in some gas pipelines

  1. TOF-SEMSANS—Time-of-flight spin-echo modulated small-angle neutron scattering

    NARCIS (Netherlands)

    Strobl, M.; Tremsin, A.S.; Hilger, A.; Wieder, F.; Kardjilov, N.; Manke, I.; Bouwman, W.G.; Plomp, J.

    2012-01-01

    We report on measurements of spatial beam modulation of a polarized neutron beam induced by triangular precession regions in time-of-flight mode and the application of this novel technique spin-echo modulated small-angle neutron scattering (SEMSANS) to small-angle neutron scattering in the very

  2. Non-Destructive Spent Fuel Characterization with Semi-Conducting Gallium Arsinde Neutron Imaging Arrays

    Energy Technology Data Exchange (ETDEWEB)

    Douglas S. McGregor; Holly K. Gersch; Jeffrey D. Sanders; John C. Lee; Mark D. Hammig; Michael R. Hartman; Yong Hong Yang; Raymond T. Klann; Brian Van Der Elzen; John T. Lindsay; Philip A. Simpson

    2002-01-30

    High resistivity bulk grown GaAs has been used to produce thermal neutron imaging devices for use in neutron radiography and characterizing burnup in spent fuel. The basic scheme utilizes a portable Sb/Be source for monoenergetic (24 keV) neutron radiation source coupled to an Fe filter with a radiation hard B-coated pixellated GaAs detector array as the primary neutron detector. The coated neutron detectors have been tested for efficiency and radiation hardness in order to determine their fitness for the harsh environments imposed by spent fuel. Theoretical and experimental results are presented, showing detector radiation hardness, expected detection efficiency and the spatial resolution from such a scheme. A variety of advanced neutron detector designs have been explored, with experimental results achieving 13% thermal neutron detection efficiency while projecting the possibility of over 30% thermal neutron detection efficiency.

  3. Adhesion and corrosion studies of a lithium based conversion coating film on the 2024 aluminum alloy

    International Nuclear Information System (INIS)

    Castro, M.R.S.; Nogueira, J.C.; Thim, G.P.; Oliveira, M.A.S.

    2004-01-01

    AA2024-T3-aluminum alloy surfaces were coated using non-chromate and chromate conversion coatings. All coatings were painted with the 10P4-2-primer epoxy resin. Independent on the film formation process, films passed on the substrate/conversion coating wet tape adhesion test. However, only the chromate conversion coating passed on the conversion coating/primer epoxy resin adhesion test. Electrochemical corrosion measurements showed that non-chromate conversion coated surfaces present lower corrosion current density, bigger polarization resistance and less negative corrosion potential than chromate conversion coated surfaces

  4. Neutron diffraction

    International Nuclear Information System (INIS)

    Elcomb, M.M.

    2002-01-01

    Full text: Thermal neutrons have a particular combination of properties, which make them the probe of choice for a wide range of scattering applications. They penetrate most materials easily, the wavelength matches interatomic spacings, the energy matches the atomic vibrational energies and the magnetic moment allows them to uniquely interact with magnetic structures. Their widely varying scattering length is also used to advantage. It enables the determination of light atoms in the presence of heavy ones: hydrogen in organic molecules, and oxygen in the high Tc superconductors for example, or solving problems in alloy systems where distinction of atoms, which are neighbours in the periodic table, is required. In the 50 years since thermal neutron beams have been used for research there has been a steady increase in applications as technology has advanced. This also applies to the environments in which the materials are studied. In-situ studies at other than ambient temperatures, pressures and magnetic fields are now routine. By using multiple detector channels in powder instruments the data collection rate has increased by an order of magnitude to some extent compensating for the diffuse nature of the neutron source. The applications of neutron scattering are becoming more industrially oriented. The talk will highlight the complementarity of neutrons to other more readily available techniques, and give examples of recent research and applications. Copyright (2002) Australian X-ray Analytical Association Inc

  5. Neutron diffraction

    International Nuclear Information System (INIS)

    Howard, C.J.; Kennedy, S.J.

    1994-01-01

    A brief account is given of neutron diffraction techniques. Similarities and differences compared with the more familiar X-ray counterparts are discussed. In certain applications, neutron diffraction can be used to obtain information about materials which would be difficult or even impossible to obtain using other techniques. One spectacular success has been the elucidation, from neutron powder diffraction, of the crystal structures of high critical temperature oxide superconductors. There have been substantial contributions in other fields, and these are illustrated by Australian work. The ability of the neutron to penetrate deeply into most materials has been invoked for in-depth determination of stresses in composites and of phase composition in zirconia ceramics. The unique properties of the neutron have been successfully exploited in studies of metal hydrides, to determine where hydrogen is located, and in magnetic structure determination. There is much interest in studying materials under different conditions of temperature and pressure, and kinetic studies under such conditions are now becoming possible. The article includes information on the principles, the instrumentation with particular reference to the instruments installed around the HIFAR reactor at Lucas Heights, and methods for the interpretation of data. 59 refs., 3 tabs., 16 figs

  6. Hydroxyapatite/poly(epsilon-caprolactone) double coating on magnesium for enhanced corrosion resistance and coating flexibility.

    Science.gov (United States)

    Jo, Ji-Hoon; Li, Yuanlong; Kim, Sae-Mi; Kim, Hyoun-Ee; Koh, Young-Hag

    2013-11-01

    Hydroxyapatite was deposited on pure magnesium (Mg) with a flexible poly(ε-caprolactone) interlayer to reduce the corrosion rate of Mg and enhance coating flexibility. The poly(ε-caprolactone) interlayer was uniformly coated on Mg by a spraying method, followed by hydroxyapatite deposition on the poly(ε-caprolactone) using an aerosol deposition method. In scanning electron microscopy observations, inorganic/organic composite-like structure was observed between the hydroxyapatite and poly(ε-caprolactone) layers, resulting from the collisions of hydroxyapatite particles into the poly(ε-caprolactone) matrix at the initial stage of the aerosol deposition. The corrosion resistance of the coated Mg was examined using potentiodynamic polarization tests. The hydroxyapatite/poly(ε-caprolactone) double coating remarkably improved the corrosion resistance of Mg in Hank's solution. In the in vitro cell tests, the coated Mg showed better cell adhesion compared with the bare Mg due to the reduced corrosion rate and enhanced biocompatibility. The stability and flexibility of hydroxyapatite/poly(ε-caprolactone) double coating was investigated by scanning electron microscopy inspections after the coated Mg was deformed. The hydroxyapatite coating on the poly(ε-caprolactone) interlayer revealed enhanced coating stability and flexibility without cracking or delamination during bending and stretching compared with the hydroxyapatite single coating. These results demonstrated that the hydroxyapatite/poly(ε-caprolactone) double coating significantly improved the surface corrosion resistance of Mg and enhanced coating flexibility for use of Mg as a biodegradable implant.

  7. Neutron scattering. Lectures of the JCNS laboratory course held at Forschungszentrum Juelich and the research reactor FRM II of TU Munich

    International Nuclear Information System (INIS)

    Brueckel, T.; Heger, G.; Richter, D.; Zorn, R.

    2007-01-01

    The following topics are dealt with: Fourier transform, basic assumptions of quantum mechanics and the Born approximation, symmtery in crystals, neutron sources, neutron elastic scattering and properties, polarized neutron scattering, correlation functions measured by scattering experiments, grazing incidence neutron scattering, neutron diffractometers, small-angle scattewring inelastic crystal spectrometers, time-of-flight spectrometers using NSE, structure determination, inelastic neutron scattering with phonon and magnon excitations, structure of complex fluids and macromolecules, polymer dynamics, magnetism. (HSI)

  8. Neutron radiography

    International Nuclear Information System (INIS)

    Pugliesi, R.; Freitas, A.G. de; Gammal, A.; Rizzatti, M.R.; Vercelli, P.

    1990-01-01

    The objective was to demonstrate the main characteristics of the neutron radiography technique, which has been developed in the Nuclear Physics Department of the IPEN-CNEN-SP. Its employment, in technology varies enormously and includes among others, the inspection of the hydrogen-rich substances, highly radioactive materials, etc. The indirect conversion method with Dysprosium screen was employed. The experimental arrangement used was a neutron collimator installed in the bottom of the IEA-R1 Nuclear Research Reactor pool. Several samples were analysed which were exposed in a neutron flux ∼ 10 7 n/s.cm 2 during 10 minutes. The obtained results confirm the main characteristics of this technique as well as its viability to be developed in this reactor. (author)

  9. neutron radiography

    International Nuclear Information System (INIS)

    Barton, J.P.

    1993-01-01

    Neutron radiography (or radiology) is a diverse filed that uses neutrons of various energies, subthermal, thermal, epithermal or fast in either steady state or pulsed mode to examine objects for industrial, medical, or other purposes, both microscopic and macroscopic. The applications include engineering design, biological studies, nondestructive inspection and materials evaluation. In the past decade, over 100 different centers in some 30 countries have published reports of pioneering activities using reactors, accelerators and isotopic neutron sources. While film transparency and electronic video are most common imaging methods for static or in motion objects respectively, there are other important data gathering techniques, including track etch, digital gauging and computed tomography. A survey of the world-wide progress shows the field to be gaining steadily in its diversity, its sophistication and its importance. (author)

  10. Neutron diffraction

    International Nuclear Information System (INIS)

    Heger, G.

    1996-01-01

    X-ray diffraction using conventional laboratory equipment and/or synchrotron installations is the most important method for structure analyses. The purpose of this paper is to discuss special cases, for which, in addition to this indispensable part, neutrons are required to solve structural problems. Even though the huge intensity of modern synchrotron sources allows in principle the study of magnetic X-ray scattering the investigation of magnetic structures is still one of the most important applications of neutron diffraction. (author) 15 figs., 1 tab., 10 refs

  11. Neutron diffraction

    Energy Technology Data Exchange (ETDEWEB)

    Heger, G. [Rheinisch-Westfaelische Technische Hochschule Aachen, Inst. fuer Kristallographie, Aachen (Germany)

    1996-12-31

    X-ray diffraction using conventional laboratory equipment and/or synchrotron installations is the most important method for structure analyses. The purpose of this paper is to discuss special cases, for which, in addition to this indispensable part, neutrons are required to solve structural problems. Even though the huge intensity of modern synchrotron sources allows in principle the study of magnetic X-ray scattering the investigation of magnetic structures is still one of the most important applications of neutron diffraction. (author) 15 figs., 1 tab., 10 refs.

  12. Dual-Side Etched Microstructured Semiconductor Neutron Detectors

    Science.gov (United States)

    Fronk, Ryan G.

    Interest in high-efficiency replacements for thin-film-coated thermal neutron detectors led to the development of single-sided microstructured semiconductor neutron detectors (MSNDs). MSNDs are designed with micro-sized trench structures that are etched into a vertically-oriented pvn-junction diode, and backfilled with a neutron converting material, such as 6LiF. Neutrons absorbed by the converting material produce a pair of charged-particle reaction products that can be measured by the diode substrate. MSNDs have higher neutron-absorption and reaction-product counting efficiencies than their thin-film-coated counterparts, resulting in up to a 10x increase in intrinsic thermal neutron detection efficiency. The detection efficiency for a single-sided MSND is reduced by neutron streaming paths between the conversion-material filled regions that consequently allow neutrons to pass undetected through the detector. Previously, the highest reported intrinsic thermal neutron detection efficiency for a single MSND was approximately 30%. Methods for double-stacking and aligning MSNDs to reduce neutron streaming produced devices with an intrinsic thermal neutron detection efficiency of 42%. Presented here is a new type of MSND that features a complementary second set of trenches that are etched into the back-side of the detector substrate. These dual-sided microstructured semiconductor neutron detectors (DS-MSNDs) have the ability to absorb and detect neutrons that stream through the front-side, effectively doubling the detection efficiency of a single-sided device. DS-MSND sensors are theoretically capable of achieving greater than 80% intrinsic thermal neutron detection efficiency for a 1-mm thick device. Prototype DS-MSNDs with diffused pvp-junction operated at 0-V applied bias have achieved 53.54+/-0.61%, exceeding that of the single-sided MSNDs and double-stacked MSNDs to represent a new record for detection efficiency for such solid-state devices.

  13. Neutronics of pulsed spallation neutron sources

    CERN Document Server

    Watanabe, N

    2003-01-01

    Various topics and issues on the neutronics of pulsed spallation neutron sources, mainly for neutron scattering experiments, are reviewed to give a wide circle of readers a better understanding of these sources in order to achieve a high neutronic performance. Starting from what neutrons are needed, what the spallation reaction is and how to produce slow-neutrons more efficiently, the outline of the target and moderator neutronics are explained. Various efforts with some new concepts or ideas have already been devoted to obtaining the highest possible slow-neutron intensity with desired pulse characteristics. This paper also reviews the recent progress of such efforts, mainly focused on moderator neutronics, since moderators are the final devices of a neutron source, which determine the source performance. Various governing parameters for neutron-pulse characteristics such as material issues, geometrical parameters (shape and dimensions), the target-moderator coupling scheme, the ortho-para-hydrogen ratio, po...

  14. Strategic Polarization.

    Science.gov (United States)

    Kalai, Adam; Kalai, Ehud

    2001-08-01

    In joint decision making, similarly minded people may take opposite positions. Consider the example of a marriage in which one spouse gives generously to charity while the other donates nothing. Such "polarization" may misrepresent what is, in actuality, a small discrepancy in preferences. It may be that the donating spouse would like to see 10% of their combined income go to charity each year, while the apparently frugal spouse would like to see 8% donated. A simple game-theoretic analysis suggests that the spouses will end up donating 10% and 0%, respectively. By generalizing this argument to a larger class of games, we provide strategic justification for polarization in many situations such as debates, shared living accommodations, and disciplining children. In some of these examples, an arbitrarily small disagreement in preferences leads to an arbitrarily large loss in utility for all participants. Such small disagreements may also destabilize what, from game-theoretic point of view, is a very stable equilibrium. Copyright 2001 Academic Press.

  15. Radiation Hard Multi-Layer Optical Coatings, Phase II

    Data.gov (United States)

    National Aeronautics and Space Administration — Next-generation space telescopes require advanced optical coatings to provide low-loss polarization-preserving transmission/reflection of light in a variety of...

  16. Tensile properties of polymethyl methacrylate coated natural fabric Sterculia urens

    CSIR Research Space (South Africa)

    Jayaramudu, J

    2009-04-01

    Full Text Available before and after alkali treatment and polymethyl methacrylate coating was studied using the scanning electron microscopy and polarized optical microscopic techniques respectively. The improvement in the tensile properties on polymethyl methacrylate...

  17. Polarization analysis for magnetic field imaging at RADEN in J-PARC/MLF

    Science.gov (United States)

    Shinohara, Takenao; Hiroi, Kosuke; Su, Yuhua; Kai, Tetsuya; Nakatani, Takeshi; Oikawa, Kenichi; Segawa, Mariko; Hayashida, Hirotoshi; Parker, Joseph D.; Matsumoto, Yoshihiro; Zhang, Shuoyuan; Kiyanagi, Yoshiaki

    2017-06-01

    Polarized neutron imaging is an attractive method for visualizing magnetic fields in a bulk object or in free space. In this technique polarization of neutrons transmitted through a sample is analyzed position by position to produce an image of the polarization distribution. In particular, the combination of three-dimensional spin analysis and the use of a pulsed neutron beam is very effective for the quantitative evaluation of both field strength and direction by means of the analysis of the wavelength dependent polarization vector. Recently a new imaging instrument “RADEN” has been constructed at the beam line of BL22 of the Materials and Life Science Experimental Facility (MLF) at J-PARC, which is dedicated to energy-resolved neutron imaging experiments. We have designed a polarization analysis apparatus for magnetic field imaging at the RADEN instrument and have evaluated its performance.

  18. Hard coatings

    International Nuclear Information System (INIS)

    Dan, J.P.; Boving, H.J.; Hintermann, H.E.

    1993-01-01

    Hard, wear resistant and low friction coatings are presently produced on a world-wide basis, by different processes such as electrochemical or electroless methods, spray technologies, thermochemical, CVD and PVD. Some of the most advanced processes, especially those dedicated to thin film depositions, basically belong to CVD or PVD technologies, and will be looked at in more detail. The hard coatings mainly consist of oxides, nitrides, carbides, borides or carbon. Over the years, many processes have been developed which are variations and/or combinations of the basic CVD and PVD methods. The main difference between these two families of deposition techniques is that the CVD is an elevated temperature process (≥ 700 C), while the PVD on the contrary, is rather a low temperature process (≤ 500 C); this of course influences the choice of substrates and properties of the coating/substrate systems. Fundamental aspects of the vapor phase deposition techniques and some of their influences on coating properties will be discussed, as well as the very important interactions between deposit and substrate: diffusions, internal stress, etc. Advantages and limitations of CVD and PVD respectively will briefly be reviewed and examples of applications of the layers will be given. Parallel to the development and permanent updating of surface modification technologies, an effort was made to create novel characterisation methods. A close look will be given to the coating adherence control by means of the scratch test, at the coating hardness measurement by means of nanoindentation, at the coating wear resistance by means of a pin-on-disc tribometer, and at the surface quality evaluation by Atomic Force Microscopy (AFM). Finally, main important trends will be highlighted. (orig.)

  19. Observing SU(2) phases with neutrons

    Indian Academy of Sciences (India)

    A 2.35 ˚A polarized neutron beam illuminated a skew symmetric (220) LLL silicon in- terferometer. Due to the space constraints within the interferometer, the maximum me- chanical rotation of each flipper was limited to ¦22Ж. Larger angles Ж¬ were therefore achieved electrically. A reversal of current in F½ effectively rotates ...

  20. Optical characterization of antirelaxation coatings

    Science.gov (United States)

    Tsvetkov, S.; Gateva, S.; Cartaleva, S.; Mariotti, E.; Nasyrov, K.

    2018-03-01

    Antirelaxation coatings (ARC) are used in optical cells containing alkali metal vapor to reduce the depolarization of alkali atoms after collisions with the cell walls. The long-lived ground state polarization is a basis for development of atomic clocks, magnetometers, quantum memory, slow light experiments, precision measurements of fundamental symmetries etc. In this work, a simple method for measuring the number of collisions of the alkali atoms with the cell walls without atomic spin randomization (Nasyrov et al., Proc. SPIE (2015)) was applied to characterize the AR properties of two PDMS coatings prepared from different solutions in ether (PDMS 2% and PDMS 5%). We observed influence of the light-induced atomic desorption (LIAD) on the AR properties of coatings.

  1. Neutron scattering equipments in JAERI. Current status

    International Nuclear Information System (INIS)

    Hamaguchi, Yoshikazu; Minakawa, Nobuaki

    2003-01-01

    24 neutron scattering instruments are installed in the JRR-3M research reactor. Among them JAERI has 12 neutron scattering instruments. Those instruments are HRPD for high-resolution structural analysis, TAS-1 and TAS-2 for elastic and inelastic scattering and for magnetic scattering measurements by the polarized neutron, LTAS for elastic and inelastic scattering measurement at a low energy region, and for neutron device development, PNO for topography and for very small angle scattering measurement in a small Q range, NRG for neutron radiography, RESA for internal strain measurements, SANS for the molecule and semi-macroscopic magnetic structural analysis, BIX-2 and BIX-3 for the biological structural analysis research, and PGA for the research of prompt gamma-ray analysis. The university groups have 12 neutron scattering instruments. Since those instruments were installed at the period when JRR-3M was completed, about 10 years have passed. In order to match the old control systems with the progress of recent computer technologies, and peripheral equipment, numbers of instruments are being renewed. In the neutron guide hall of JRR-3M, the Ni mirror guide tube was replaced by a super mirror guide tube to increase neutron flux. The intensity of 2A flux was increased by a factor of about two. (J.P.N.)

  2. Neutronic reactor

    International Nuclear Information System (INIS)

    Wende, C.W.J.

    1976-01-01

    The method of operating a water-cooled neutronic reactor having a graphite moderator is described which comprises flowing a gaseous mixture of carbon dioxide and helium, in which the helium comprises 40--60 volume percent of the mixture, in contact with the graphite moderator. 2 claims, 4 figures

  3. Neutronic reactor

    International Nuclear Information System (INIS)

    Carleton, J.T.

    1977-01-01

    A graphite-moderated nuclear reactor includes channels between blocks of graphite and also includes spacer blocks between adjacent channeled blocks with an axis of extension normal to that of the axis of elongation of the channeled blocks to minimize changes in the physical properties of the graphite as a result of prolonged neutron bombardment. 3 claims, 6 figures

  4. Neutron stars as cosmic neutron matter laboratories

    International Nuclear Information System (INIS)

    Pines, D.

    1986-01-01

    Recent developments which have radically changed our understanding of the dynamics of neutron star superfluids and the free precession of neutron stars are summarized, and the extent to which neutron stars are cosmic neutron matter laboratories is discussed. 17 refs., 1 tab

  5. Incorporation of Nicotine into Silicone Coatings for Marine Applications

    Science.gov (United States)

    Jaramillo, Sandy Tuyet

    PDMS-based marine coatings presently used are limited by their inability to mitigate microfouling which limits their application to high speed vessels. PDMS coatings are favored when viable, due to their foul release properties of macrofouling organisms. Natural products have been investigated for antifouling properties for potential use in these marine antifouling coatings but few have incorporated natural products into coatings or coating systems. The purpose of the research was to establish the corrosion inhibiting properties of nicotine and to incorporate nicotine, a biodegradable and readily available natural product, into a PDMS coating to demonstrate the use of a natural product in a coating for marine applications. The corrosion inhibiting properties of nicotine was examined using potentiodynamic polarization scans, material characterization techniques such as scanning electron microscopy, energy dispersive spectroscopy and X-ray diffraction, quartz crystal microbalance and electrochemical impedance spectroscopy. Nicotine was determined to be an anodic corrosion inhibitor for mild steel immersed in simulated seawater with the ability to precipitate a protective calcium carbonate film. Electrochemical impedance spectroscopy was used to evaluate the performance of the developed nicotine incorporated coatings on mild steel immersed in simulated seawater over 21 days of immersion. The coatings with 2 wt.% of nicotine incorporated in the coating with a ratio of 1:30 of additional platinum catalyst to nicotine exhibited the best performance for intact coatings. This coating had the most favorable balance of the amount of nicotine and platinum catalyst of all the coatings evaluated. Overall, all nicotine incorporated coatings had a performance improvement when compared to the control PDMS coating. Of the nicotine incorporated coatings that were tested with an artificial pin-hole defect, the 2PDMS coating also exhibited the best performance with significant

  6. Recent progress on HYSPEC, and its polarization analysis capabilities

    Directory of Open Access Journals (Sweden)

    Winn Barry

    2015-01-01

    Full Text Available HYSPEC is a high-intensity, direct-geometry time-of-flight spectrometer at the Spallation Neutron Source, optimized for measurement of excitations in small single-crystal specimens with optional polarization analysis capabilities. The incident neutron beam is monochromated using a Fermi chopper with short, straight blades, and is then vertically focused by Bragg scattering onto the sample position by either a highly oriented pyrolitic graphite (unpolarized or a Heusler (polarized crystal array. Neutrons are detected by a bank of 3He tubes that can be positioned over a wide range of scattering angles about the sample axis. HYSPEC entered the user program in February 2013 for unpolarized experiments, and is already experiencing a vibrant research program. Polarization analysis will be accomplished by using the Heusler crystal array to polarize the incident beam, and either a 3He spin filter or a supermirror wide-angle polarization analyser to analyse the scattered beam. The 3He spin filter employs the spin-exchange optical pumping technique. A 60∘ wide angle 3He cell that matches the detector coverage will be used for polarization analysis. The polarized gas in the post-sample wide angle cell is designed to be periodically and automatically refreshed with an adjustable pressure of polarized gas, optically pumped in a separate cell and then transferred to the wide angle cell. The supermirror analyser has 960 supermirror polarizers distributed over 60∘, and has been characterized at the Swiss Spallation Neutron Source. The current status of the instrument and the development of its polarization analysis capabilities are presented.

  7. Basic of Neutron NDA

    Energy Technology Data Exchange (ETDEWEB)

    Trahan, Alexis Chanel [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

    2017-09-15

    The objectives of this presentation are to introduce the basic physics of neutron production, interactions and detection; identify the processes that generate neutrons; explain the most common neutron mechanism, spontaneous and induced fission and (a,n) reactions; describe the properties of neutron from different sources; recognize advantages of neutron measurements techniques; recognize common neutrons interactions; explain neutron cross section measurements; describe the fundamental of 3He detector function and designs; and differentiate between passive and active assay techniques.

  8. Polarized targets in high energy physics

    Energy Technology Data Exchange (ETDEWEB)

    Cates, G.D. Jr. [Princeton Univ., NJ (United States)

    1994-12-01

    Various approaches are discussed for producing polarized nuclear targets for high energy physics experiments. As a unifying theme, examples are drawn from experiments to measure spin dependent structure functions of nucleons in deep inelastic scattering. This single physics goal has, over roughly two decades, been a driving force in advances in target technology. Actual or planned approaches have included solid targets polarized by dynamic nuclear polarization (DNP), several types of internal targets for use in storage rings, and gaseous {sup 3}He targets polarized by spin-exchange optical pumping. This last approach is the type of target adopted for SLAC E-142, an experiment to measure the spin structure function of the neutron, and is described in detail.

  9. Protective Coatings

    Science.gov (United States)

    1980-01-01

    General Magnaplate Corporation's pharmaceutical machine is used in the industry for high speed pressing of pills and capsules. Machine is automatic system for molding glycerine suppositories. These machines are typical of many types of drug production and packaging equipment whose metal parts are treated with space spinoff coatings that promote general machine efficiency and contribute to compliance with stringent federal sanitation codes for pharmaceutical manufacture. Collectively known as "synergistic" coatings, these dry lubricants are bonded to a variety of metals to form an extremely hard slippery surface with long lasting self lubrication. The coatings offer multiple advantages; they cannot chip, peel or be rubbed off. They protect machine parts from corrosion and wear longer, lowering maintenance cost and reduce undesired heat caused by power-robbing friction.

  10. Non-dispersive method for measuring longitudinal neutron coherence length using high frequency cold neutron pulser

    International Nuclear Information System (INIS)

    Kawai, T.; Tasaki, S.; Ebisawa, T.; Hino, M.; Yamazaki, D.; Achiwa, N.

    1999-01-01

    Complete text of publication follows. A non-dispersive method is proposed for measuring the longitudinal coherence length of a neutron using a high frequency cold neutron pulser (hf-CNP) placed between two multilayer spin splitters (MSS) which composes the cold neutron spin interferometer. Two spin eigenstates of a neutron polarized x-y plane are split non-dispersively and longitudinally in time by the hf-CNP which could reflect two components alternatively in time. The reduction of the visibility of interference fringes after being superposed by the second MSS is measured as a function of the frequency of the pulser by TOF method. From the zero visibility point obtained by extrapolation one could obtain the longitudinal coherence length of the neutron. (author)

  11. Methods of contrast variation by nuclear polarisation in small-angle neutron scattering: Observation of domains of nuclear polarisation by neutron scattering

    International Nuclear Information System (INIS)

    Leymarie, E.

    2002-11-01

    In this thesis we study the theoretical and experimental aspects of Contrast Variation by Nuclear Polarization (CVNP) applied to small-angle neutron scattering. The basics of neutron scattering theory is developed by highlighting the origin of the CVNP method: the strong spin dependence of thermal neutron scattering, especially on protons. We also present the principles of NMR with a special attention on the method of dynamic nuclear polarization by the solid effect which makes it possible to control the proton polarization and therefore the contrast for neutron scattering. We present a theoretical study of the CVNP method called static which supposes that the nuclear polarization is homogeneous in the sample and constant during the experiment. We show that it allows one to obtain partial structure functions of systems with multiple components, by carrying out several acquisitions with different polarizations on a single sample. For this purpose, we tested a simple device to stabilize the nuclear polarization. We describe finally a new application of the CVNP method called dynamic. In a solution of deuterated glycerol-water containing a small concentration of paramagnetic centres, we showed the existence of domains of polarized protons at the onset of dynamic polarization. This reinforces considerably the coherent scattering of paramagnetic centres. We describe the theoretical reasons explaining the appearance of these domains of polarization, as well as the various techniques used to observe them by neutron scattering. (author)

  12. Precessing deuteron polarization

    International Nuclear Information System (INIS)

    Sitnik, I.M.; Volkov, V.I.; Kirillov, D.A.; Piskunov, N.M.; Plis, Yu.A.

    2002-01-01

    The feasibility of the acceleration in the Nuclotron of deuterons polarized in the horizontal plane is considered. This horizontal polarization is named precessing polarization. The effects of the main magnetic field and synchrotron oscillations are included. The precessing polarization is supposed to be used in studying the polarization parameters of the elastic dp back-scattering and other experiments

  13. Neutron scattering. Lectures

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2012-07-01

    The following topics are dealt with: Neutron scattering in contemporary research, neutron sources, symmetry of crystals, diffraction, nanostructures investigated by small-angle neutron scattering, the structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic scattering, strongly correlated electrons, dynamics of macromolecules, applications of neutron scattering. (HSI)

  14. Neutron scattering. Lectures

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2013-07-01

    The following topics are dealt with: Neutron sources, symmetry of crystals, nanostructures investigated by small-angle neutron scattering, structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic neutron scattering, strongly correlated electrons, polymer dynamics, applications of neutron scattering. (HSI)

  15. Pulsed neutron generator

    International Nuclear Information System (INIS)

    Bespalov, D.F.; Bykovskii, Yu.A.; Vergun, I.I.; Kozlovskii, K.I.; Kozyrev, Yu.P.; Leonov, R.K.; Simagin, B.I.; Tsybin, A.S.; Shikanov, A.Ie.

    1986-03-01

    The paper describes a new device for generating pulsed neutron fields, utilized in nuclear geophysics for carrying out pulsed neutron logging and activation analysis under field conditions. The invention employs a sealed-off neutron tube with a laser ion source which increases neutron yield to the level of 10 neutrons per second or higher. 2 refs., 1 fig

  16. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2012-01-01

    The following topics are dealt with: Neutron scattering in contemporary research, neutron sources, symmetry of crystals, diffraction, nanostructures investigated by small-angle neutron scattering, the structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic scattering, strongly correlated electrons, dynamics of macromolecules, applications of neutron scattering. (HSI)

  17. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2013-01-01

    The following topics are dealt with: Neutron sources, symmetry of crystals, nanostructures investigated by small-angle neutron scattering, structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic neutron scattering, strongly correlated electrons, polymer dynamics, applications of neutron scattering. (HSI)

  18. 16th International Workshop on Polarized Sources, Targets, and Polarimetry (PSTP 2015)

    CERN Document Server

    2015-01-01

    The Workshop on Polarized Sources, Targets and Polarimetry has been a tradition for more than 20 years, moving between Europe, USA and Japan. The XVIth International Workshop on Polarized Sources, Targets and Polarimetry (PSTP 2015) will take place at the Ruhr-University of Bochum, Germany. The workshop addresses the physics and technological challenges related to polarized gas/solid targets, polarized electron/positron/ion/neutron sources, polarimetry and their applications. will be published in Proceedings of Science

  19. A white beam neutron spin splitter

    Energy Technology Data Exchange (ETDEWEB)

    Krist, T. [Hahn Meitner Institute, Berlin (Germany); Klose, F.; Felcher, G.P. [Argonne National Lab., IL (United States)

    1997-07-23

    The polarization of a narrow, highly collimated polychromatic neutron beam is tested by a neutron spin splitter that permits the simultaneous measurement of both spin states. The device consists of a Si-Co{sub 0.11} Fe{sub 0.89} supermirror, which totally reflects one spin state up to a momentum transfer q=0.04 {angstrom}{sup -1}, whilst transmits neutrons of the opposite spin state. The supermirror is sandwitched between two thick silicon wafers and is magnetically saturated by a magnetic field of 400 Oe parallel to its surface. The neutron beam enters through the edge of one of the two silicon wavers, its spin components are split by the supermirror and exit from the opposite edges of the two silicon wafers and are recorded at different channels of a position-sensitive detector. The device is shown to have excellent efficiency over a broad range of wavelengths.

  20. Polare maskuliniteter

    Directory of Open Access Journals (Sweden)

    Marit Anne Hauan

    2012-05-01

    Full Text Available In this paper my aim is to read and understand the journal of Gerrit de Veer from the last journey of William Barents to the Arctic Regions in 1596 and the journal of captain Junge on his hunting trip from Tromsø to Svalbard in 1834.It is nearly 240 years between this to voyages. The first journal is known as the earliest report from the arctic era. Gerrit de Veer adds instructive copper engravings to his text and give us insight in the crews meeting with this new land. Captain Junges journal is found together with his dead crew in a house in a fjord nearby Ny-Ålesund and has no drawings, but word. Both of these journals may be read as sources of the knowledge and understanding of the polar region. They might also unveil the ideas of how to deal with and survive under the challenges that is given. In addition one can ask if the sources can tell us more about how men describe their challenges. Can the way they expressed themselves in the journals give us an understanding of masculinity? And not least help us to create good questions of the change in the ideas of masculinities which is said to follow the change in understanding of the wilderness.

  1. Neutron scattering

    International Nuclear Information System (INIS)

    1991-02-01

    The annual report on hand gives an overview of the research work carried out in the Laboratory for Neutron Scattering (LNS) of the ETH Zuerich in 1990. Using the method of neutron scattering, it is possible to examine in detail the static and dynamic properties of the condensed material. In accordance with the multidisciplined character of the method, the LNS has for years maintained a system of intensive co-operation with numerous institutes in the areas of biology, chemistry, solid-state physics, crystallography and materials research. In 1990 over 100 scientists from more than 40 research groups both at home and abroad took part in the experiments. It was again a pleasure to see the number of graduate students present, who were studying for a doctorate and who could be introduced into the neutron scattering during their stay at the LNS and thus were in the position to touch on central ways of looking at a problem in their dissertation using this modern experimental method of solid-state research. In addition to the numerous and interesting ways of formulating the questions to explain the structure, nowadays the scientific programme increasingly includes particularly topical studies in connection with high temperature-supraconductors and materials research

  2. Spallation Neutron Source (SNS)

    Data.gov (United States)

    Federal Laboratory Consortium — The SNS at Oak Ridge National Laboratory is a next-generation spallation neutron source for neutron scattering that is currently the most powerful neutron source in...

  3. Neutron structure analysis using neutron imaging plate

    International Nuclear Information System (INIS)

    Karasawa, Yuko; Minezaki, Yoshiaki; Niimura, Nobuo

    1997-01-01

    Neutron is complementary against X-ray and is dispensable for structure analysis. However, because of the lack of the neutron intensity, it was not so common as X-ray. In order to overcome the intensity problem, a neutron imaging plate (NIP) has been successfully developed. The NIP has opened the door of neutron structure biology, where all the hydrogen atoms and bound water molecules of protein are determined, and contributed to development of other fields such as neutron powder diffraction and neutron radiography, too. (author)

  4. REFRACTIVE NEUTRON LENS

    OpenAIRE

    Petrov, P. V.; Kolchevsky, N. N.

    2013-01-01

    Compound concave refractive lenses are used for focusing neutron beam. Investigations of spectral and focusing properties of a refractive neutron lens are presented. Resolution of the imaging system on the base of refractive neutron lenses depends on material properties and parameters of neutron source. Model of refractive neutron lens are proposed. Results of calculation diffraction resolution and focal depth of refractive neutron lens are discussed.

  5. High energy neutron radiography

    International Nuclear Information System (INIS)

    Gavron, A.; Morley, K.; Morris, C.; Seestrom, S.; Ullmann, J.; Yates, G.; Zumbro, J.

    1996-01-01

    High-energy spallation neutron sources are now being considered in the US and elsewhere as a replacement for neutron beams produced by reactors. High-energy and high intensity neutron beams, produced by unmoderated spallation sources, open potential new vistas of neutron radiography. The authors discuss the basic advantages and disadvantages of high-energy neutron radiography, and consider some experimental results obtained at the Weapons Neutron Research (WNR) facility at Los Alamos

  6. Neutron Therapy Facility

    Data.gov (United States)

    Federal Laboratory Consortium — The Neutron Therapy Facility provides a moderate intensity, broad energy spectrum neutron beam that can be used for short term irradiations for radiobiology (cells)...

  7. Polarization Measurements on SUMI's TVLS Gratings

    Science.gov (United States)

    Kobayashi, K.; West, E. A.; Davis, J. M.; Gary, G. A.

    2007-01-01

    We present measurements of toroidal variable-line-space (TVLS) gratings for the Solar Ultraviolet Magnetograph Investigation (SUMI), currently being developed at the National Space Science and Technology Center (NSSTC). SUMI is a spectro-polarimeter designed to measure magnetic fields in the solar chromosphere by observing two UV emission lines sensitive to magnetic fields, the CIY line at 155nm and the MgII line at 280nm. The instrument uses a pair of TVLS gratings, to observe both linear polarizations simultaneously. Efficiency measurements were done on bare aluminum gratings and aluminum/MgF2 coated gratings, at both linear polarizations.

  8. Polarization Measurements on SUMI's TVLS Gratings

    Science.gov (United States)

    Kobayashi, K.; West, E. A.; Davis, J. M.; Gary, G. A.

    2007-01-01

    We present measurements of toroidal variable-line-space (TVLS) gratings for the Solar Ultraviolet Magnetograph Investigation (SUMI), currently being developed an the National Space Science and Technology Center (NSSTC). SUMI zs a spectro-polarimeter designed no measure magnetic fields in the solar chromosphere by observing two UV emission lines sensitive to magnetic fields, the C-IV line at 155nm and the Mg-II line at 280nm. The instrument uses a pair of TVLS gratings, to observe both linear polarizations simultaneously. Efficiency measurements were done on bare aluminum gratings and MgF2 coated gratings, at both linear polarizations.

  9. Neutron microdosimetry

    International Nuclear Information System (INIS)

    Kliauga, P.

    1987-01-01

    A major effort was made during the past year to do precision microdosimetry of neutrons at the RARAF facility. By precision microdosimetry the authors mean a special effort to understand, better than previously, some of the factors which go into the limitation of the accuracy and precision of microdosimetric measurements of neutrons. That such factors are still not clearly understood, or at least accounted for, is immediately evident upon examination of published microdosimetric measurements. What becomes immediately apparent upon examination of, say, the dose mean lineal energies reported, is that the spread of reported values for exceeds the reported experimental uncertainty, commonly taken as about 5%. Differences of 50% are not uncommon. It is easy to make the mistake that since classical microdosimetry uses a well-established experimental tool, the proportional counter, that sources of error should also be well understood. However, microdosimetry makes use of the proportional counter in a way which is quite different from its origins as a low-energy photon spectroscopy device. Microdosimetric spectra, particularly of neutrons, span 5 to 6 decades of event sizes. It is by no means certain that proportionality extends over such a range, and in fact it has been pointed out that it probably does not. Data analysis techniques vary from one experimenter to another, and can substantially affect mean values as well as spectral shape. The authors are examining these parameters, as well as others, such as calibration errors, but they are especially concentrating on the effect of counter design and performance on the resultant spectra which the counter measures

  10. Optical enhancing durable anti-reflective coating

    Science.gov (United States)

    Maghsoodi, Sina; Varadarajan, Aravamuthan; Movassat, Meisam

    2016-07-05

    Disclosed herein are polysilsesquioxane based anti-reflective coating (ARC) compositions, methods of preparation, and methods of deposition on a substrate. In embodiments, the polysilsesquioxane of this disclosure is prepared in a two-step process of acid catalyzed hydrolysis of organoalkoxysilane followed by addition of tetralkoxysilane that generates silicone polymers with >40 mol % silanol based on Si-NMR. These high silanol siloxane polymers are stable and have a long shelf-life in the polar organic solvents at room temperature. Also disclosed are low refractive index ARC made from these compositions with and without additives such as porogens, templates, Si--OH condensation catalyst and/or nanofillers. Also disclosed are methods and apparatus for applying coatings to flat substrates including substrate pre-treatment processes, coating processes including flow coating and roll coating, and coating curing processes including skin-curing using hot-air knives. Also disclosed are coating compositions and formulations for highly tunable, durable, highly abrasion-resistant functionalized anti-reflective coatings.

  11. Irradiation behaviors of coated fuel particles, (4)

    International Nuclear Information System (INIS)

    Fukuda, Kousaku; Kashimura, Satoru; Ogawa, Toru; Ikawa, Katsuichi; Iwamoto, Kazumi; Ishimoto, Kiyoshi

    1981-09-01

    Loose coated fuel particles prepared in confirmity to a preliminary design for the multi-purpose VHTR in fiscal 1972 - 1974 were irradiated by 73F - 12A capsule in JMTR. Main purpose for this irradiation experiment was to examine irradiation stability of the candidate TRISO coated fuel particles for the VHTR. Also the coated particles possessing low-density kernel (90%TD), highly anisotropic OLTI-PyC and ZrC coating layer were loaded with the candidate particles in this capsule. The coated particles were irradiated up to 1.5 x 10 21 n/cm 2 of fast neutron fluence (E > 0.18 MeV) and 3.2% FIMA of burnup. In the post irradiation examination it was observed that among three kinds of TRISO particles exposed to irradiation corresponding to the normal operating condition of the VHTR ones possessing poor characteristics of the coating layers did not show a good stability. The particles irradiated under abnormally high temperature condition (> 1800 0 C) revealed 6.7% of max. EOL failure fraction (95% confidence limit). Most of these particles were failed by the ameoba effect. Furthermore, among four kinds of the TRISO particles exposed to irradiation corresponding to the transient condition of the VHTR (--1500 0 C) the two showed a good stability, while the particles possessing highly anisotropic OLTI-PyC or poorly characteristic coating layers were not so good. (author)

  12. Polarized electron sources

    Energy Technology Data Exchange (ETDEWEB)

    Prepost, R. [Univ. of Wisconsin, Madison, WI (United States)

    1994-12-01

    The fundamentals of polarized electron sources are described with particular application to the Stanford Linear Accelerator Center. The SLAC polarized electron source is based on the principle of polarized photoemission from Gallium Arsenide. Recent developments using epitaxially grown, strained Gallium Arsenide cathodes have made it possible to obtain electron polarization significantly in excess of the conventional 50% polarization limit. The basic principles for Gallium and Arsenide polarized photoemitters are reviewed, and the extension of the basic technique to strained cathode structures is described. Results from laboratory measurements of strained photocathodes as well as operational results from the SLAC polarized source are presented.

  13. A Comprehensive Pitting Study of High Velocity Oxygen Fuel Inconel 625 Coating by Using Electrochemical Testing Techniques

    Science.gov (United States)

    Niaz, Akbar; Khan, Sajid Ullah

    2016-01-01

    In the present work, Inconel 625 was coated on a mild steel substrate using a high velocity oxygen fuel coating process. The pitting propensity of the coating was tested by using open circuit potential versus time, potentiodynamic polarization, electrochemical potentiokinetic reactivation, and scanning electrochemical microscopy. The pitting propensity of the coating was compared with bulk Inconel 625 alloy. The results confirmed that there were regions of different electrochemical activities on the coating which have caused pitting corrosion.

  14. Structure of clathrin-coated vesicles from small-angle scattering experiments

    DEFF Research Database (Denmark)

    Pedersen, J.S.

    1993-01-01

    Previously published small-angle neutron and X-ray scattering data from coated vesicles, reassembled coats, and stripped vesicles have been analyzed in terms of one common model. The neutron data sets include contrast variation measurements at three different D2O solvent concentrations. The model....... Thus, the membrane and the high-density protein shell overlap in space, which shows that the lipid membrane contains protein. The molecular mass of the average particle is 27 x 10(6) Da. The coated vesicles consist, on average, of approximately 85% protein and 15% lipids. About 40% of the protein mass...... particles with the barrel structure shows that the accessory polypeptides are incorporated in the lipid membrane. The results from the neutron data for the reassembled coats show that the structure of these particles is very similar to the structure of the native coats. The main difference is a higher...

  15. Corrosion protective poly(o-ethoxyaniline) coatings on copper

    Energy Technology Data Exchange (ETDEWEB)

    Chaudhari, Sudeshna; Patil, P.P. [Department of Physics, North Maharashtra University, Jalgaon 425001, Maharashtra (India)

    2007-12-01

    Poly(o-ethoxyaniline) (POEA) coatings were synthesized on copper (Cu) by electrochemical polymerization of o-ethoxyaniline in aqueous salicylate solution by using cyclic voltammetry. These coatings were characterized by cyclic voltammetry, UV-vis absorption spectroscopy, Fourier transform infrared (FTIR) spectroscopy and scanning electron microscopy (SEM). The performance of POEA as protective coating against corrosion of Cu in aqueous 3% NaCl was assessed by the potentiodynamic polarization technique and electrochemical impedance spectroscopy (EIS). The results of the potentiodynamic polarization and EIS studies demonstrate that the POEA coating has ability to protect the Cu against corrosion. The corrosion potential was about 0.330 V versus SCE more positive in aqueous 3% NaCl for the POEA coated Cu than that of uncoated Cu and reduces the corrosion rate of Cu almost by a factor of 140. (author)

  16. Dielectric relaxation in metal-coated particles: the dramatic role of nano-scale coatings

    International Nuclear Information System (INIS)

    Youngs, I J; Bowler, N; Lymer, K P; Hussain, S

    2005-01-01

    Insulating materials filled with conducting particles permit tailoring of electrical, electromagnetic and thermal properties of the resulting composite. When the filler particles are small and metallic, a dielectric relaxation due to interfacial polarization is commonly observed at optical or smaller wavelengths. Here, experimental results are presented in which the dielectric relaxation is shifted to microwave frequencies as a result of using metal-coated dielectric particles with a nano-scale coating thickness. The results are analysed in the context of effective medium theory adapted for multi-layer particles. Such a large shift in relaxation frequency, compared with that for a similar composite with solid metal filler particles, is shown to be a function of both the coating geometry and a thin-film-related reduction in the conductivity of the metal. The observed broadening of the relaxation peak is attributed to non-uniformity of the coating thickness and a consequent distribution of coating conductivity

  17. Study of materials properties by neutron beam applications

    International Nuclear Information System (INIS)

    Lee, Chang Hee; Kim, H. J.; Kim, B. C.; Jun, B. C.; Lee, J. S.; Seong, B. S.; Shim, H. S.; Choi, B. H.; Ho, J. W.; Kang, S. K.; Kim, J. Y.; Park, D. K.; Kim, C. K.; Kim, C. J.; Cho, Y. S.

    1997-10-01

    Horizontal and vertical beam ports related works for neutron beam experimental facilities in HANARO has been done. And the preparation works of neutron spectrometers, design, manufacture and installation of the high resolution powder diffractometer, the four circle diffractometer, the polarized neutron spectrometer, the small angle neutron spectrometer and the position sensitive detector unit for residual stress measurement have been done. The status for each spectrometer are described. The development of neutron spectroscopy technique for the crystal structure analysis on YBa 2 Cu 3 O 7-x , U 3 Si, Pb(Yb,Nb)O 3 by neutron diffraction, the anisotropic properties of textured orthorhombic polycrystalline materials and the low temperature sample environment facility has been performed and neutron reflectometry has been reviewed. After the design and manufacture of neutron radiography facility, it has been installed at NR beam tube and its' performance evaluation has been done. The image processing technique for real time testing is under development. As for neutron transmutation doping, design of irradiation tube, estimation on neutron flux distribution and flux quality, and study of irradiation damage recovery under annealing have been tried. (author). 11 refs., 40 tabs., 86 figs.

  18. Recent developments in very low energy neutron technology

    International Nuclear Information System (INIS)

    Utsuro, Masahiko; Kawabata, Yuji; Yamaguchi, Akira; Yoshiki, Hajime.

    1993-01-01

    In this report, the recent state of the research and technical development of the neutrons in the energy region below 0.5 meV is introduced. The neutrons in this region are further divided into very cold neutrons (VCN) and ultracold neutrons (UCN). The UCNs are known by such characteristic behavior that they can be confined in a neutron bottle for long time. The attempt to verify the break of T conversion symmetry using neutrons is carried out. The experiment to show the break of T conversion symmetry by grasping the asymmetry of particle emission accompanying the beta decay of polarized neutrons is conceivable. In these cases, the use of UCNs in neutron bottles is effective. The optical properties of VCNs and UCNs are peculiar and resemble to those of light. The only VCN source in Japan is installed in the liquid deuterium CN source in the graphite facility of the KUR. VCNs are taken out from the reactor, and are converted to UCNs using a neutron turbine. The characteristics of an UCN bottle were measured, and the life of neutrons was determined as 887.6 ± 3s. The UCN experiment using superfluid helium was carried out, and the application of gravity to UCN spectrometry was developed as NESSIE. (K.I.)

  19. Neutron matter, symmetry energy and neutron stars

    Energy Technology Data Exchange (ETDEWEB)

    Stefano, Gandolfi [Los Alamos National Laboratory (LANL); Steiner, Andrew W [ORNL

    2016-01-01

    Recent progress in quantum Monte Carlo with modern nucleon-nucleon interactions have enabled the successful description of properties of light nuclei and neutron-rich matter. Of particular interest is the nuclear symmetry energy, the energy cost of creating an isospin asymmetry, and its connection to the structure of neutron stars. Combining these advances with recent observations of neutron star masses and radii gives insight into the equation of state of neutron-rich matter near and above the saturation density. In particular, neutron star radius measurements constrain the derivative of the symmetry energy.

  20. Neutron scattering. Lectures

    Energy Technology Data Exchange (ETDEWEB)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner (eds.)

    2010-07-01

    The following topics are dealt with: Neutron sources, symmetry of crystals, diffraction, nanostructures investigated by small-angle neutron scattering, the structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic scattering, strongly correlated electrons, dynamics of macromolecules, applications of neutron scattering. (HSI)

  1. Neutron generator control system

    International Nuclear Information System (INIS)

    Peelman, H.E.; Bridges, J.R.

    1981-01-01

    A method is described of controlling the neutron output of a neutron generator tube used in neutron well logging. The system operates by monitoring the target beam current and comparing a function of this current with a reference voltage level to develop a control signal used in a series regulator to control the replenisher current of the neutron generator tube. (U.K.)

  2. Neutron scattering. Lectures

    International Nuclear Information System (INIS)

    Brueckel, Thomas; Heger, Gernot; Richter, Dieter; Roth, Georg; Zorn, Reiner

    2010-01-01

    The following topics are dealt with: Neutron sources, symmetry of crystals, diffraction, nanostructures investigated by small-angle neutron scattering, the structure of macromolecules, spin dependent and magnetic scattering, structural analysis, neutron reflectometry, magnetic nanostructures, inelastic scattering, strongly correlated electrons, dynamics of macromolecules, applications of neutron scattering. (HSI)

  3. A compact spin-exchange optical pumping system for 3He polarization based on a solenoid coil, a VBG laser diode, and a cosine theta RF coil

    Science.gov (United States)

    Lee, Sungman; Kim, Jongyul; Moon, Myung Kook; Lee, Kye Hong; Lee, Seung Wook; Ino, Takashi; Skoy, Vadim R.; Lee, Manwoo; Kim, Guinyun

    2013-02-01

    For use as a neutron spin polarizer or analyzer in the neutron beam lines of the HANARO (High-flux Advanced Neutron Application ReactOr) nuclear research reactor, a 3He polarizer was designed based on both a compact solenoid coil and a VBG (volume Bragg grating) diode laser with a narrow spectral linewidth of 25 GHz. The nuclear magnetic resonance (NMR) signal was measured and analyzed using both a built-in cosine radio-frequency (RF) coil and a pick-up coil. Using a neutron transmission measurement, we estimated the polarization ratio of the 3He cell as 18% for an optical pumping time of 8 hours.

  4. Fundamental Problems of Neutron Physics at the Spallation Neutron Source at the ORNL

    International Nuclear Information System (INIS)

    Gudkov, Vladimir

    2008-01-01

    We propose to provide theoretical support for the experimental program in fundamental neutron physics at the SNS. This includes the study of neutron properties, neutron beta-decay, parity violation effects and time reversal violation effects. The main purpose of the proposed research is to work on theoretical problems related to experiments which have a high priority at the SNS. Therefore, we will make a complete analysis of beta-decay process including calculations of radiative corrections and recoil corrections for angular correlations for polarized neutron decay, with an accuracy better that is supposed to be achieved in the planning experiments. Based on the results of the calculations, we will provide analysis of sensitivity of angular correlations to be able to search for the possible extensions of the Standard model. Also we will help to plan other experiments to address significant problems of modern physics and will work on their theoretical support.

  5. Fundamental Problems of Neutron Physics at the Spallation Neutron Source at the ORNL

    Energy Technology Data Exchange (ETDEWEB)

    Vladimir Gudkov

    2008-07-16

    We propose to provide theoretical support for the experimental program in fundamental neutron physics at the SNS. This includes the study of neutron properties, neutron beta-decay, parity violation effects and time reversal violation effects. The main purpose of the proposed research is to work on theoretical problems related to experiments which have a high priority at the SNS. Therefore, we will make a complete analysis of beta-decay process including calculations of radiative corrections and recoil corrections for angular correlations for polarized neutron decay, with an accuracy better that is supposed to be achieved in the planning experiments. Based on the results of the calculations, we will provide analysis of sensitivity of angular correlations to be able to search for the possible extensions of the Standard model. Also we will help to plan other experiments to address significant problems of modern physics and will work on their theoretical support.

  6. The surface properties of biopolymer-coated fruit: A review

    Directory of Open Access Journals (Sweden)

    Diana Cristina Moncayo Martinez

    2013-09-01

    Full Text Available Environmental conservation concerns have led to research and development regarding biodegradable materials from biopolymers, leading to new formulations for edible films and coatings for preserving the quality of fresh fruit and vegetables. Determining fruit skin surface properties for a given coating solution has led to predicting coating efficiency. Wetting was studied by considering spreading, adhesion and cohesion and measuring the contact angle, thus optimising the coating formulation in terms of biopolymer, plasticiser, surfactant, antimicrobial and antioxidant concentration. This work reviews the equations for determining fruit surface properties by using polar and dispersive interaction calculations and by determining the contact angle.

  7. Application of Ketone-Based Resins as Anticorrosive Coating

    Directory of Open Access Journals (Sweden)

    Esma Sezer

    2011-01-01

    Full Text Available Effect of some newly synthesized modified ketonic resins on corrosion inhibition of stainless steel (SS and copper (Cu was investigated in acidic medium. Carboxyl, hydroxyl, and carbonyl functionalized resins have been coated on metal electrode as a thin film by dipping method. Corrosion characteristics of coating on SS (304 L and Cu were investigated by polarization, open-circuit, and impedance measurement. These measurements performed at different time and the stability of polymeric coating were tested with time in acidic medium. The resin coating was able to protect both the SS and copper.

  8. Development of Grazing Incidence Optics for Neutron Imaging and Scattering

    Science.gov (United States)

    Gubarev, M. V.; Khaykovich, B.; Liu, D.; Ramsey, B. D.; Zavlin, V. E.; Kilaru, K.; Romaine, S.; Rosati, R. E.; Bruni, R.; Moncton, D. E.

    2012-01-01

    Because of their wave nature, thermal and cold neutrons can be reflected from smooth surfaces at grazing incidence angles, be reflected by multilayer coatings or be refracted at boundaries of different materials. The optical properties of materials are characterized by their refractive indices which are slightly less than unity for most elements and their isotopes in the case of cold and thermal neutrons as well as for x-rays. The motivation for the optics use for neutrons as well as for x-rays is to increase the signal rate and, by virtue of the optic's angular resolution, to improve the signal-to-noise level by reducing the background so the efficiency of the existing neutron sources use can be significantly enhanced. Both refractive and reflective optical techniques developed for x-ray applications can be applied to focus neutron beams. Typically neutron sources have lower brilliance compared to conventional x-ray sources so in order to increase the beam throughput the neutron optics has to be capable of capturing large solid angles. Because of this, the replicated optics techniques developed for x-ray astronomy applications would be a perfect match for neutron applications, so the electroformed nickel optics under development at the Marshall Space Flight Center (MSFC) can be applied to focus neutron beams. In this technique, nickel mirror shells are electroformed onto a figured and superpolished nickel-plated aluminum cylindrical mandrel from which they are later released by differential thermal contraction. Cylindrical mirrors with different diameters, but the same focal length, can be nested together to increase the system throughput. The throughput can be increased further with the use of the multilayer coatings deposited on the reflectivr surface of the mirror shells. While the electroformed nickel replication technique needs to be adopted for neutron focusing, the technology to coat the inside of cylindrical mirrors with neutron multilayers has to be

  9. Rotating relativistic neutron stars

    Energy Technology Data Exchange (ETDEWEB)

    Weber, F.; Glendenning, N.K.

    1991-07-21

    Models of rotating neutron stars are constructed in the framework of Einstein's theory of general relativity. For this purpose a refined version of Hartle's method is applied. The properties of these objects, e.g. gravitational mass, equatorial and polar radius, eccentricity, red- and blueshift, quadrupole moment, are investigated for Kepler frequencies of 4000 s{sup {minus}1} {le} {Omega}{sub K} {le} 9000 s{sup {minus}1}. Therefore a self-consistency problem inherent in the determination of {Omega}{sub K} must be solved. The investigation is based on neutron star matter equations of state derived from the relativistic Martin-Schwinger hierarch of coupled Green's functions. By means of introducing the Hartree, Hartree-Fock, and ladder ({Lambda}) approximations, models of the equation of state derived. A special feature of the latter approximation scheme is the inclusion of dynamical two-particle correlations. These have been calculated from the relativistic T-matrix applying both the HEA and Bonn meson-exchange potentials of the nucleon-nucleon force. The nuclear forces of the former two treatments are those of the standard scalar-vector-isovector model of quantum hadron dynamics, with parameters adjusted to the nuclear matter data. An important aspect of this work consists in testing the compatibility of different competing models of the nuclear equation of state with data on pulsar periods. By this the fundamental problem of nuclear physics concerning the behavior of the equation of state at supernuclear densities can be treated.

  10. Nuclear reactor neutron shielding

    Science.gov (United States)

    Speaker, Daniel P; Neeley, Gary W; Inman, James B

    2017-09-12

    A nuclear reactor includes a reactor pressure vessel and a nuclear reactor core comprising fissile material disposed in a lower portion of the reactor pressure vessel. The lower portion of the reactor pressure vessel is disposed in a reactor cavity. An annular neutron stop is located at an elevation above the uppermost elevation of the nuclear reactor core. The annular neutron stop comprises neutron absorbing material filling an annular gap between the reactor pressure vessel and the wall of the reactor cavity. The annular neutron stop may comprise an outer neutron stop ring attached to the wall of the reactor cavity, and an inner neutron stop ring attached to the reactor pressure vessel. An excore instrument guide tube penetrates through the annular neutron stop, and a neutron plug comprising neutron absorbing material is disposed in the tube at the penetration through the neutron stop.

  11. Miscellaneous neutron techniques

    International Nuclear Information System (INIS)

    Iddings, F.A.

    1976-01-01

    Attention is brought to the less often uses of neutrons in the areas of neutron radiography, well logging, and neutron gaging. Emphasis on neutron radiography points toward the isotopic sensitivity of the method versus the classical bulk applications. Also recognized is the ability of neutron radiography to produce image changes that correspond to thickness and density changes obtained in photon radiography. Similarly, neutron gaging applications center on the measurement of radiography. Similarly, neutron gaging applications center on the measurement of water, oil, or plastics in industrial samples. Well logging extends the neutron gaging to encompass many neutron properties and reactions besides thermalization and capture. Neutron gaging also gives information on organic structure and concentrations of a variety of elements or specific compounds in selected matrices

  12. A neutron radiography facility on the IRT-2000 reactor

    International Nuclear Information System (INIS)

    Khadduri, I.Y.

    1976-01-01

    A neutron radiography facility has been constructed on the thermal neutron channel of the IRT-2000 reactor. A collimated thermal neutron beam exposure area of 10 cm diameter is obtained with an L/D ratio of 48.8. The film used is cellulose nitrate coated with lithium tetraborate which is insensitive to gamma and beta radiation. Some pictures with good contrast and resolution have been obtained. Pictures of parts of an IRT-2000 reactor fuel pin have also been recorded. (orig) [de

  13. Development of precision elliptic neutron-focusing supermirror.

    Science.gov (United States)

    Hosobata, Takuya; Yamada, Norifumi L; Hino, Masahiro; Yamagata, Yutaka; Kawai, Toshihide; Yoshinaga, Hisao; Hori, Koichiro; Takeda, Masahiro; Takeda, Shin; Morita, Shin-Ya

    2017-08-21

    This paper details methods for the precision design and fabrication of neutron-focusing supermirrors, based on electroless nickel plating. We fabricated an elliptic mirror for neutron reflectometry, which is our second mirror improved from the first. The mirror is a 550-millimeter-long segmented mirror assembled using kinematic couplings, with each segment figured by diamond cutting, polished using colloidal silica, and supermirror coated through ion-beam sputtering. The mirror was evaluated with neutron beams, and the reflectivity was found to be 68-90% at a critical angle. The focusing width was 0.17 mm at the full width at half maximum.

  14. Neutrons in science and technology

    International Nuclear Information System (INIS)

    Bromley, D.A.

    1984-01-01

    Occasionally to the fiftieth anniversy of the discovery of the neutron the author presents a historical review about the impact of this discovery on different fields at physics. Especially considered are nuclear physics, the neutron as an elementary particles, ultracold neutrons, condensed matter physics, radiation damage induced by neutrons, neutron activation analysis, imaging and radiography by neutrons, neutrons in mining operations, track etching, the use of intense gamma sources, gauging systems, neutron holography and neutron stars. (HSI)

  15. Coating materials

    International Nuclear Information System (INIS)

    Ozeki, Takao; Kimura, Tadashi; Kobayashi, Juichi; Maeda, Yutaka; Nakamoto, Hideo.

    1969-01-01

    A non-solvent type coating material composition having properties as good as thermosetting acrylic or amino alkid resins is provided by employing active energy irradiation, particularly electron beams, using a radically polymerizable low molecular compound (A) (hereafter called an oligomer) containing at least two vinyl radicals in one molecule. This oligomer is produced by reacting an epoxy-containing vinyl monomer with alpha-, beta-ethylene unsaturated carboxylic acids or their anhydrides. The composition (I) contains 10% - 100% of this oligomer. In embodiments, an oligomer having a fiberous trivinyl construction is produced by reacting 180 parts by weight of glycidyl methacrylate ester with 130 parts of itaconic acid in the presence of a polymerization-inhibitor and an addition reaction catalyst at 90 0 C for 6 hours. In practice, the coating material compositions (1), consist of the whole oligomer [I-1]; (2), consist of 10-90% of (A) component and 90%-10% of vinyl monomers containing at least 30% (meth) acrylic monomer [I-2]; (3), 10%-90% of component (A) and 90%-10% of other monomers containing at least two vinyl radicals [I-3]; (4), a mixture of (I-2) and (I-3), [I-4]; and (5), consist of 50% or less unsaturated polyester of 500-5,000 molecular weight range or drying oil, or alkyd resin of 500-5,000 molecular weight range modified by drying oil, [I-5]. As a catalyst a tertiary amino vinyl compound is preferred. Five examples are given. (Iwakiri, K.)

  16. Superconducting magnetic Wollaston prism for neutron spin encoding.

    Science.gov (United States)

    Li, F; Parnell, S R; Hamilton, W A; Maranville, B B; Wang, T; Semerad, R; Baxter, D V; Cremer, J T; Pynn, R

    2014-05-01

    A magnetic Wollaston prism can spatially split a polarized neutron beam into two beams with different neutron spin states, in a manner analogous to an optical Wollaston prism. Such a Wollaston prism can be used to encode the trajectory of neutrons into the Larmor phase associated with their spin degree of freedom. This encoding can be used for neutron phase-contrast radiography and in spin echo scattering angle measurement (SESAME). In this paper, we show that magnetic Wollaston prisms with highly uniform magnetic fields and low Larmor phase aberration can be constructed to preserve neutron polarization using high temperature superconducting (HTS) materials. The Meissner effect of HTS films is used to confine magnetic fields produced electromagnetically by current-carrying HTS tape wound on suitably shaped soft iron pole pieces. The device is cooled to ~30 K by a closed cycle refrigerator, eliminating the need to replenish liquid cryogens and greatly simplifying operation and maintenance. A HTS film ensures that the magnetic field transition within the prism is sharp, well-defined, and planar due to the Meissner effect. The spin transport efficiency across the device was measured to be ~98.5% independent of neutron wavelength and energizing current. The position-dependent Larmor phase of neutron spins was measured at the NIST Center for Neutron Research facility and found to agree well with detailed simulations. The phase varies linearly with horizontal position, as required, and the neutron beam shows little depolarization. Consequently, the device has advantages over existing devices with similar functionality and provides the capability for a large neutron beam (20 mm × 30 mm) and an increase in length scales accessible to SESAME to beyond 10 μm. With further improvements of the external coupling guide field in the prototype device, a larger neutron beam could be employed.

  17. Superconducting magnetic Wollaston prism for neutron spin encoding

    Energy Technology Data Exchange (ETDEWEB)

    Li, F., E-mail: fankli@indiana.edu; Parnell, S. R.; Wang, T.; Baxter, D. V. [Center for Exploration of Energy and Matter, Indiana University, Bloomington, Indiana 47408 (United States); Hamilton, W. A. [Neutron Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37830 (United States); Maranville, B. B. [National Institute of Standards and Technology, Gaithersburg, Maryland 20899 (United States); Semerad, R. [Ceraco Ceramic Coating GmbH, Ismaning 85737 (Germany); Cremer, J. T. [Adelphi Technology Inc., Redwood City, California 94063 (United States); Pynn, R. [Center for Exploration of Energy and Matter, Indiana University, Bloomington, Indiana 47408 (United States); Neutron Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37830 (United States)

    2014-05-15

    A magnetic Wollaston prism can spatially split a polarized neutron beam into two beams with different neutron spin states, in a manner analogous to an optical Wollaston prism. Such a Wollaston prism can be used to encode the trajectory of neutrons into the Larmor phase associated with their spin degree of freedom. This encoding can be used for neutron phase-contrast radiography and in spin echo scattering angle measurement (SESAME). In this paper, we show that magnetic Wollaston prisms with highly uniform magnetic fields and low Larmor phase aberration can be constructed to preserve neutron polarization using high temperature superconducting (HTS) materials. The Meissner effect of HTS films is used to confine magnetic fields produced electromagnetically by current-carrying HTS tape wound on suitably shaped soft iron pole pieces. The device is cooled to ∼30 K by a closed cycle refrigerator, eliminating the need to replenish liquid cryogens and greatly simplifying operation and maintenance. A HTS film ensures that the magnetic field transition within the prism is sharp, well-defined, and planar due to the Meissner effect. The spin transport efficiency across the device was measured to be ∼98.5% independent of neutron wavelength and energizing current. The position-dependent Larmor phase of neutron spins was measured at the NIST Center for Neutron Research facility and found to agree well with detailed simulations. The phase varies linearly with horizontal position, as required, and the neutron beam shows little depolarization. Consequently, the device has advantages over existing devices with similar functionality and provides the capability for a large neutron beam (20 mm × 30 mm) and an increase in length scales accessible to SESAME to beyond 10 μm. With further improvements of the external coupling guide field in the prototype device, a larger neutron beam could be employed.

  18. Neutron scattering on magnetic surfaces

    International Nuclear Information System (INIS)

    Ott, F.

    2007-01-01

    During the early eighties, advanced techniques for the deposition of ultra-thin metal films were developed. The combination of different types of materials gave rise to new physical phenomena such as the magnetic exchange coupling in superlattices or the exchange bias between ferro and anti-ferro layers. New types of heterostructures combining magnetic oxides, insulating oxides or magnetic semiconductors are still being developed. Alongside the fabrication of these new meta-materials made of thin films stacking, polarized neutron reflectometry has emerged as a routine tool for the characterization of magnetic hetero-structures. In the recent years, the new developments of polarized reflectivity have been connected to the study of micro- and nano-structures, especially micro-magnetic structures in multilayers. The technique of off-specular scattering has been developed for the study of the roughness or the micro magnetism at a micro metric scale. For the study of nano-metric structures, in the range below 100 nm, grazing incidence Small Angle Scattering is being considered. In thin films, the volume of magnetic matter is very small but nevertheless, diffraction experiments can be performed owing to the good performances of modern neutron spectrometers

  19. Performance Comparison of Steam-Based and Chromate Conversion Coatings on Aluminum Alloy 6060

    DEFF Research Database (Denmark)

    Din, Rameez Ud; Jellesen, Morten Stendahl; Ambat, Rajan

    2015-01-01

    In this study, oxide layers generated on aluminum alloy 6060(UNS A96060) using a steam-based process were compared with conventional chromate and chromate-phosphate conversion coatings. Chemical composition and microstructure of the conversion coatings were investigated and their corrosion...... performance was evaluated using potentio dynamic polarization, acetic acid salt spray, and filiform corrosion testing of powder coated specimens. The steam-based process resulted in homogenous growth of oxide layer and superior coverageover intermetallic particles when compared to chromate-based conversion...... coatings. The coating formed by steam showed improved corrosion resistance, while adhesion to powder coatingand filiform corrosion was comparable with chromate conversion coatings....

  20. Solubilization of a polar oil used in nuclear industry by amphiphilic tri-block copolymers solutions. Relation between structure and behavior by proton nuclear magnetic resonance and small angle neutron scattering

    International Nuclear Information System (INIS)

    Causse, J.

    2005-01-01

    The first step in a decommissioning operation of a nuclear plant concerns the nuclear decontamination of various surfaces. More and more techniques developed for nuclear decontamination use soluble surfactants in aqueous solution with suitable chemical reagents. In most cases decontamination is based on the removal of a surface layer containing most of the activity (grease, organic deposits, paint, oxide layer...). The Tributylphosphate (TBP), a polar oil, is widely used as a complexing agent of Plutonium and Uranium in nuclear industry. This lipophilic compound, containing radioactive residues, strongly sticks on many surfaces. This organic layer is resistant to all classical treatments. Micellar systems proved to be efficient to pull TBP away and solubilize it so as to make easier its draining. In this study, Amphiphilic tri-block copolymers, referred to as Pluronics (polyethylene(oxide) - polypropylene(oxide) - polyethylene(oxide), (EO) n PO) m EO) n ) have been selected as polymeric amphiphiles so as to solubilize TBP in their supramolecular aggregates above the critical aggregation concentration. A first systematic study of the phase behavior of various three components systems (TBP-Water-Pluronic) by turbidity showed the particular behavior of one copolymer (the L64, (EO) 13 PO) 30 EO) 13 ), especially its very high TBP solubilization capacity. Consequently, the main part of this thesis has been devoted to the structural characterization of this micellar system (TBP-Water-L64) using 1 H NMR and SANS measurements. 1 H NMR gave information on the chemical environment of each component in the mixture and especially allowed hypothesis on the TBP location in the copolymer aggregates to be drawn. Direct structural information (size, shape, correlations) were obtained by SANS. Both experimental technique were proved to be very complementary and allowed a structural evolution of the aggregates following addition of TBP in the system to be evidenced. (author)