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Sample records for plasma source mass

  1. Inductively coupled plasma source mass spectrometry

    International Nuclear Information System (INIS)

    Price Russ, G. III

    1993-01-01

    Inductively coupled plasma source mass spectrometry (ICP-MS) is a relatively new (5 y commercial availability) technique for simultaneously determining the concentration and isotopic composition of a large number of elements at trace levels. The principle advantages of ICP-MS are the ability to measure essentially all the metallic elements at concentrations as low as 1 part in 10 12 by weight, to analyse aqueous samples directly, to determine the isotopic composition of essentially all the metallic elements, and to analyse samples rapidly (minutes). The history of the development of ICP-MS and discussions of a variety of applications have been discussed in detail in Date and Gray (1988). Koppenaal (1988, 1990) has reviewed the ICP-MS literature. In that ICP-MS is a relatively new and still evolving technique, this chapter will discuss potential capability more than proven performance. (author). 24 refs

  2. Mass analyzer ``MASHA'' high temperature target and plasma ion source

    Science.gov (United States)

    Semchenkov, A. G.; Rassadov, D. N.; Bekhterev, V. V.; Bystrov, V. A.; Chizov, A. Yu.; Dmitriev, S. N.; Efremov, A. A.; Guljaev, A. V.; Kozulin, E. M.; Oganessian, Yu. Ts.; Starodub, G. Ya.; Voskresensky, V. M.; Bogomolov, S. L.; Paschenko, S. V.; Zelenak, A.; Tikhonov, V. I.

    2004-05-01

    A new separator and mass analyzer of super heavy atoms (MASHA) has been created at the FLNR JINR Dubna to separate and measure masses of nuclei and molecules with precision better than 10-3. First experiments with the FEBIAD plasma ion source have been done and give an efficiency of ionization of up to 20% for Kr with a low flow test leak (6 particle μA). We suppose a magnetic field optimization, using the additional electrode (einzel lens type) in the extracting system, and an improving of the vacuum conditions in order to increase the ion source efficiency.

  3. Mass analyzer 'MASHA' high temperature target and plasma ion source

    International Nuclear Information System (INIS)

    Semchenkov, A.G.; Rassadov, D.N.; Bekhterev, V.V.; Bystrov, V.A.; Chizov, A.Yu.; Dmitriev, S.N.; Efremov, A.A.; Guljaev, A.V.; Kozulin, E.M.; Oganessian, Yu.Ts.; Starodub, G.Ya.; Voskresensky, V.M.; Bogomolov, S.L.; Paschenko, S.V.; Zelenak, A.; Tikhonov, V.I.

    2004-01-01

    A new separator and mass analyzer of super heavy atoms (MASHA) has been created at the FLNR JINR Dubna to separate and measure masses of nuclei and molecules with precision better than 10 -3 . First experiments with the FEBIAD plasma ion source have been done and give an efficiency of ionization of up to 20% for Kr with a low flow test leak (6 particle μA). We suppose a magnetic field optimization, using the additional electrode (einzel lens type) in the extracting system, and an improving of the vacuum conditions in order to increase the ion source efficiency

  4. Indigenous instrumentation for mass spectrometry: Part II - development of plasma source mass spectrometers. PD-5-3

    International Nuclear Information System (INIS)

    Nataraju, V.

    2007-01-01

    The growing demands from analytical community, for a precise isotope ratio and ultra trace concentration measurements, has lead to significant improvement in mass spectrometer instrumentation development with respect to sensitivity, detection limits, precision and accuracy. Among the many analytical techniques available, plasma source mass spectrometers like Inductively Coupled Plasma Mass Spectrometry (ICPMS), multi collector (MC) ICPMS and Glow Discharge Mass Spectrometry (GDMS), have matured into reliable tools for the above applications. Where as ICPMS is by far the most successful method for aqueous solutions, GDMS is being applied for bulk and impurity analysis of conducting as well non-conducting solids. VPID, BARC has been developing mass spectrometers for different inorganic applications of DAE users. Over the years expertise has been developed in all the aspects of mass spectrometry instrumentation. Part 1 of this indigenous instrumentation on mass spectrometry gives details of magnetic sector instruments with either EI or TI source for isotopic ratio analysis. The present paper is a continuation of that on plasma source and quadrupole mass spectrometers. This paper covers i) ICP-QMS, ii) MC-ICPMS, iii) GDMS and iv) QMS

  5. Characterization of a Distributed Plasma Ionization Source (DPIS) for Ion Mobility Spectrometry and Mass Spectrometry

    International Nuclear Information System (INIS)

    Waltman, Melanie J.; Dwivedi, Prabha; Hill, Herbert; Blanchard, William C.; Ewing, Robert G.

    2008-01-01

    A recently developed atmospheric pressure ionization source, a distributed plasma ionization source (DPIS), was characterized and compared to commonly used atmospheric pressure ionization sources with both mass spectrometry and ion mobility spectrometry. The source consisted of two electrodes of different sizes separated by a thin dielectric. Application of a high RF voltage across the electrodes generated plasma in air yielding both positive and negative ions depending on the polarity of the applied potential. These reactant ions subsequently ionized the analyte vapors. The reactant ions generated were similar to those created in a conventional point-to-plane corona discharge ion source. The positive reactant ions generated by the source were mass identified as being solvated protons of general formula (H2O)nH+ with (H2O)2H+ as the most abundant reactant ion. The negative reactant ions produced were mass identified primarily as CO3-, NO3-, NO2-, O3- and O2- of various relative intensities. The predominant ion and relative ion ratios varied depending upon source construction and supporting gas flow rates. A few compounds including drugs, explosives and environmental pollutants were selected to evaluate the new ionization source. The source was operated continuously for several months and although deterioration was observed visually, the source continued to produce ions at a rate similar that of the initial conditions. The results indicated that the DPIS may have a longer operating life than a conventional corona discharge.

  6. An argon–nitrogen–hydrogen mixed-gas plasma as a robust ionization source for inductively coupled plasma mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Makonnen, Yoseif; Beauchemin, Diane, E-mail: diane.beauchemin@chem.queensu.ca

    2014-09-01

    Multivariate optimization of an argon–nitrogen–hydrogen mixed-gas plasma for minimum matrix effects, while maintaining analyte sensitivity as much as possible, was carried out in inductively coupled plasma mass spectrometry. In the presence of 0.1 M Na, the 33.9 ± 3.9% (n = 13 elements) analyte signal suppression on average observed in an all-argon plasma was alleviated with the optimized mixed-gas plasma, the average being − 4.0 ± 8.8%, with enhancement in several cases. An addition of 2.3% v/v N{sub 2} in the outer plasma gas, and 0.50% v/v H{sub 2} to the central channel, as a sheath around the nebulizer gas flow, was sufficient for this drastic increase in robustness. It also reduced the background from ArO{sup +} and Ar{sub 2}{sup +} as well as oxide levels by over an order of magnitude. On the other hand, the background from NO{sup +} and ArN{sup +} increased by up to an order of magnitude while the levels of doubly-charged ions increased to 7% (versus 2.7% in an argon plasma optimized for sensitivity). Furthermore, detection limits were generally degraded by 5 to 15 fold when using the mixed-gas plasma versus the argon plasma for matrix-free solution (although they were better for several elements in 0.1 M Na). Nonetheless, the drastically increased robustness allowed the direct quantitative multielement analysis of certified ore reference materials, as well as the determination of Mo and Cd in seawater, without using any matrix-matching or internal standardization. - Highlights: • Addition of N{sub 2} to the plasma gas and H{sub 2} as a sheath gas results in a very robust ICP. • ArO{sup +} and Ar{sub 2}{sup +} background and oxide levels are reduced by over an order of magnitude. • Multielement analysis of rock digests is possible with a simple external calibration. • No internal standardization or matrix-matching is required for accurate analysis. • Cd and Mo were accurately determined in undiluted seawater.

  7. Development of soft ionization using direct current pulse glow discharge plasma source in mass spectrometry for volatile organic compounds analysis

    Science.gov (United States)

    Nunome, Yoko; Kodama, Kenji; Ueki, Yasuaki; Yoshiie, Ryo; Naruse, Ichiro; Wagatsuma, Kazuaki

    2018-01-01

    This study describes an ionization source for mass analysis, consisting of glow discharge plasma driven by a pulsed direct-current voltage for soft plasma ionization, to detect toxic volatile organic compounds (VOCs) rapidly and easily. The novelty of this work is that a molecular adduct ion, in which the parent molecule attaches with an NO+ radical, [M + NO]+, can be dominantly detected as a base peak with little or no fragmentation of them in an ambient air plasma at a pressure of several kPa. Use of ambient air as the discharge plasma gas is suitable for practical applications. The higher pressure in an ambient air discharge provided a stable glow discharge plasma, contributing to the soft ionization of organic molecules. Typical mass spectra of VOCs toluene, benzene, o-xylene, chlorobenzene and n-hexane were observed as [M + NO]+ adduct ion whose peaks were detected at m/z 122, 108, 136, 142 and 116, respectively. The NO generation was also confirmed by emission bands of NO γ-system. The ionization reactions were suggested, such that NO+ radical formed in an ambient air discharge could attach with the analyte molecule.

  8. Isotopic ratio measurement using a double focusing magnetic sector mass analyser with an inductively coupled plasma as an ion source

    International Nuclear Information System (INIS)

    Walder, A.J.; Freedman, P.A.

    1992-01-01

    An inductively coupled plasma source was coupled to a magnetic sector mass analyser equipped with seven Faraday detectors. An electrostatic filter located between the plasma source and the magnetic sector was used to create a double focusing system. Isotopic ratio measurements of uranium and lead standards revealed levels of internal and external precision comparable to those obtained using thermal inonization mass spectrometry. An external precision of 0.014% was obtained from the 235 U: 238 U measurement of six samples of a National Bureau of Standards (NBS) Standard Reference Material (SRM) U-500, while an RSD of 0.022% was obtained from the 206 Pb: 204 Pb measurement of six samples of NBS SRM Pb-981. Measured isotopic ratios deviated from the NBS value by approximately 0.9% per atomic mass unit. This deviation approximates to a linear function of mass bias and can therefore be corrected for by the analysis of standards. The analysis of NBS SRM Sr-987 revealed superior levels of internal and external precision. The normalization of the 87 Sr: 86 Sr ratio to the 86 Sr: 88 Sr ratio reduced the RSD to approximately 0.008%. The measured ratio was within 0.01% of the NBS value and the day-to-day reproducibility was consistent within one standard deviation. (author)

  9. Characterization of a sealed Americium-Beryllium (AmBe) source by inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Sommers, J.; Jimenez, M.; Adamic, M.; Giglio, J.; Carney, K.

    2009-01-01

    Two Americium-Beryllium neutron sources were dismantled, sampled (sub-sampled) and analyzed via inductively coupled plasma mass spectrometry (ICP-MS). Characteristics such as 'age' since purification, actinide content, trace metal content and inter and intra source composition were determined. The 'age' since purification of the two sources was determined to be 25.0 and 25.4 years, respectively. The systematic uncertainties in the 'age' determination were ±4% 2σ. The amount and isotopic composition of U and Pu varied substantially between the sub-samples of Source 2 (n = 8). This may be due to the physical means of sub-sampling or the way the source was manufactured. Source 1 was much more consistent in terms of content and isotopic composition (n = 3 sub-samples). The Be-Am ratio varied greatly between the two sources. Source 1 had an Am-Be ratio of 6.3 ± 52% (1σ). Source 2 had an Am-Be ratio of 9.81 ± 3.5% (1σ). In addition, the trace element content between the samples varied greatly. Significant differences were determined between Sources 1 and 2 for Sc, Sr, Y, Zr, Mo, Ba and W. (author)

  10. Validation of methods to measure uranium isotopes using magnetic sector mass spectrometry with inductively coupled plasma source

    International Nuclear Information System (INIS)

    Hernandez M, H.; Rios L, M. J.; Romero G, E. T.

    2017-10-01

    The mass spectrometry technique with inductively coupled plasma source (Icp-Ms) has been widely used to measure isotopic ratios of elements toxic to human health. Reason for which, in this work several measurement methods for the analysis of uranium isotopes in different matrices were implemented using magnetic sector mass spectrometry with inductively coupled plasma source (Icp-SFMS). Groundwater, sediment, soil and urine were the matrices analyzed, which were supplied by intercomparison tests conducted by the IAEA and Association for the Promotion of Quality Control of Medical Biology Analysis in Radio-toxicology. The procedures used in the treatment of soil, sediment and water samples were based on US EPA methods. In the case of the urine sample, the preparation was rapid (1:20 dilution). The average of the results obtained in yield of each matrix was 94, 71, 72 and 78% for water, urine, soil and sediment respectively. In addition, the precision in terms of standard relative deviation was less than 5% and the accuracy was less than 4%. In conclusion, the Icp-SFMS is a very sensitive technique for measuring isotopes of U in different matrices. However, careful tuning is necessary, especially in the mass regions of interest 234, 235 and 238 if an external quantification is considered using natural U solutions. (Author)

  11. Ion source with plasma cathode

    International Nuclear Information System (INIS)

    Yabe, E.

    1987-01-01

    A long lifetime ion source with plasma cathode has been developed for use in ion implantation. In this ion source, a plasma of a nonreactive working gas serves as a cathode in place of a thermionic tungsten filament used in the Freeman ion source. In an applied magnetic field, the plasma is convergent, i.e., filamentlike; in zero magnetic field, it turns divergent and spraylike. In the latter case, the plasma exhibits a remarkable ability when the working gas has an ionization potential larger than the feed gas. By any combination of a working gas of either argon or neon and a feed gas of AsF 5 or PF 5 , the lifetime of this ion source was found to be more than 90 h with an extraction voltage of 40 kV and the corresponding ion current density 20 mA/cm 2 . Mass spectrometry results show that this ion source has an ability of generating a considerable amount of As + and P + ions from AsF 5 and PF 5 , and hence will be useful for realizing a fully cryopumped ion implanter system. This ion source is also eminently suitable for use in oxygen ion production

  12. Pulsed Plasma Electron Sources

    Science.gov (United States)

    Krasik, Yakov

    2008-11-01

    Pulsed (˜10-7 s) electron beams with high current density (>10^2 A/cm^2) are generated in diodes with electric field of E > 10^6 V/cm. The source of electrons in these diodes is explosive emission plasma, which limits pulse duration; in the case E Saveliev, J. Appl. Phys. 98, 093308 (2005). Ya. E. Krasik, A. Dunaevsky, and J. Felsteiner, Phys. Plasmas 8, 2466 (2001). D. Yarmolich, V. Vekselman, V. Tz. Gurovich, and Ya. E. Krasik, Phys. Rev. Lett. 100, 075004 (2008). J. Z. Gleizer, Y. Hadas and Ya. E. Krasik, Europhysics Lett. 82, 55001 (2008).

  13. Plasma source ion implantation

    International Nuclear Information System (INIS)

    Conrad, J.R.; Forest, C.

    1986-01-01

    The authors' technique allows the ion implantation to be performed directly within the ion source at higher currents without ion beam extraction and transport. The potential benefits include greatly increased production rates (factors of 10-1000) and the ability to implant non-planar targets without rastering or shadowing. The technique eliminates the ion extractor grid set, beam raster equipment, drift space and target manipulator equipment. The target to be implanted is placed directly within the plasma source and is biased to a large negative potential so that plasma ions gain energy as they accelerate through the potential drop across the sheath that forms at the plasma boundary. Because the sheath surrounds the target on all sides, all surfaces of the target are implanted without the necessity to raster the beam or to rotate the target. The authors have succeeded in implanting nitrogen ions in a silicon target to the depths and concentrations required for surface treatment of materials like stainless steel and titanium alloys. They have performed ESCA measurements of the penetration depth profile of a silicon target that was biased to 30 kV in a nitrogen discharge plasma. Nitrogen ions were implanted to a depth of 700A at a peak concentration of 30% atomic. The measured profile is quite similar to a previously obtained profile in titanium targets with conventional techniques

  14. Microwave plasma ion sources for selected ion flow tube mass spectrometry: Optimizing their performance and detection limits for trace gas analysis

    Czech Academy of Sciences Publication Activity Database

    Španěl, Patrik; Dryahina, Kseniya; Smith, D.

    2007-01-01

    Roč. 267, 1-3 (2007), s. 117-124 ISSN 1387-3806 R&D Projects: GA ČR GA202/06/0776 Institutional research plan: CEZ:AV0Z40400503 Keywords : microwave plasma ion source * selected ion flow tube mass spectrometry * SIFT-MS * breath analysis Subject RIV: CF - Physical ; Theoretical Chemistry Impact factor: 2.411, year: 2007

  15. Use of plasma-source multicollector magnetic-sector mass spectrometry for uranium and plutonium analysis in environmental samples

    International Nuclear Information System (INIS)

    Price Russ, G.; Williams, Ross

    2001-01-01

    Full text: The ability to detect and isotopically characterize uranium and plutonium in environmental samples is of primary importance in the search for nuclear proliferation. The utility of isotope ratio measurements for environmental monitoring is limited by sample preparation costs, measurement precision, and sensitivity. This is particularly true for wide-area monitoring where the number of samples required varies inversely with obtainable precision and sensitivity. Historically isotopic measurements have been made by thermal ionization mass spectrometry (TIMS). While requiring extensive sample preparation, no other technique matched its precision and sensitivity for such measurements. Inductively-coupled-plasma, magnetic-sector, multicollector, mass spectrometry offers the prospect of extending the state-of-the-art to higher precision while increasing sensitivity and reducing costs through more rapid analysis and reduced sample preparation. At LLNL this technique is being implemented in the form of an IsoProbe (Micromass, UK). This paper will present data for both standards and IAEA supplied samples demonstrating the power and limitations of the technique. The precision and sensitivity of the IsoProbe results will be compared to TIMS performance for comparable samples. For 48 determinations of natural uranium, using the double spike to correct for bias, a relative standard deviation of 0.04% (1σ) for 238 U/ 235 U has been obtained in a preliminary study. This is a substantial improvement over the TIMS result of 0.1% reported at the previous conference. Further improvements can be expected as we gain a better understanding of the background peaks occurring in the IsoProbe spectra. (author)

  16. Validation of methods to measure uranium isotopes using magnetic sector mass spectrometry with inductively coupled plasma source; Validacion de metodos para medir isotopos de uranio usando espectrometria de masas de sector magnetico con fuente de plasma acoplado inductivamente

    Energy Technology Data Exchange (ETDEWEB)

    Hernandez M, H. [Universidad del Centro de Mexico, Capitan Caldera 75, Col. Tequixquiapan, 78250 San Luis Potosi, SLP (Mexico); Rios L, M. J. [Universidad Autonoma de San Luis Potosi, Facultad de Enfermeria y Nutricion, Unidad de Posgrado, Av. Nino Artillero 130, 78210 San Luis Potosi, SLP (Mexico); Romero G, E. T., E-mail: hector.hernandez520@gmail.com [ININ, Departamento de Quimica, Laboratorio Forense Nuclear, Carretera Mexico-Toluca s/n, 52750 Ocoyoacac, Estado de Mexico (Mexico)

    2017-10-15

    The mass spectrometry technique with inductively coupled plasma source (Icp-Ms) has been widely used to measure isotopic ratios of elements toxic to human health. Reason for which, in this work several measurement methods for the analysis of uranium isotopes in different matrices were implemented using magnetic sector mass spectrometry with inductively coupled plasma source (Icp-SFMS). Groundwater, sediment, soil and urine were the matrices analyzed, which were supplied by intercomparison tests conducted by the IAEA and Association for the Promotion of Quality Control of Medical Biology Analysis in Radio-toxicology. The procedures used in the treatment of soil, sediment and water samples were based on US EPA methods. In the case of the urine sample, the preparation was rapid (1:20 dilution). The average of the results obtained in yield of each matrix was 94, 71, 72 and 78% for water, urine, soil and sediment respectively. In addition, the precision in terms of standard relative deviation was less than 5% and the accuracy was less than 4%. In conclusion, the Icp-SFMS is a very sensitive technique for measuring isotopes of U in different matrices. However, careful tuning is necessary, especially in the mass regions of interest 234, 235 and 238 if an external quantification is considered using natural U solutions. (Author)

  17. 21 CFR 640.60 - Source Plasma.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 7 2010-04-01 2010-04-01 false Source Plasma. 640.60 Section 640.60 Food and... ADDITIONAL STANDARDS FOR HUMAN BLOOD AND BLOOD PRODUCTS Source Plasma § 640.60 Source Plasma. The proper name of the product shall be Source Plasma. The product is defined as the fluid portion of human blood...

  18. Measurements of total lead concentrations and of lead isotope ratios in whole blood by use of inductively coupled plasma source mass spectrometry

    International Nuclear Information System (INIS)

    Delves, H.T.; Campbell, M.J.

    1988-01-01

    Methods are described for the accurate and precise determination of total lead and its isotopic composition in whole blood using inductively coupled plasma source mass spectrometry (ICP-MS). Sensitivities of up to 3 x 10 6 counts s -1 for 208 Pb at a total lead concentration of 5 μmol l -1 (1 μg ml -1 ) enabled total blood lead levels to be measured in 4 min per sample, with a detection limit of 0.072 μmol l -1 (15 μg l -1 ). The agreement between ICP-MS and atomic absorption spectrometry (AAS) for this analysis was excellent: ICP-MS 0.996 x AAS -0.0165 μmol l -1 ; r 0.994. Isotope ratio measurements required 15 min to achieve the required accuracy and precision both of which were generally better than 0.5% for 206 Pb: 207 Pb and 208 Pb: 206 Pb isotopic lead ratios. The ICP-MS data for these ratios in ten quality control blood specimens has a mean bias relative to isotope dilution mass spectrometry of -0.412% for 206 Pb: 207 Pb ratios and of +0.055% for the 208 Pb: 206 Pb ratios. This level of accuracy and that of the total blood lead measurements is sufficient to permit application of these ICP-MS methods to environmental studies. (author)

  19. Development of a novel low-flow ion source/sampling cone geometry for inductively coupled plasma mass spectrometry and application in hyphenated techniques

    Science.gov (United States)

    Pfeifer, Thorben; Janzen, Rasmus; Steingrobe, Tobias; Sperling, Michael; Franze, Bastian; Engelhard, Carsten; Buscher, Wolfgang

    2012-10-01

    A novel ion source/sampling cone device for inductively coupled plasma mass spectrometry (ICP-MS) especially operated in the hyphenated mode as a detection system coupled with different separation modules is presented. Its technical setup is described in detail. Its main feature is the very low total argon consumption of less than 1.5 L min- 1, leading to significant reduction of operational costs especially when time-consuming speciation analysis is performed. The figures of merit of the new system with respect to sensitivity, detection power, long-term stability and working range were explored. Despite the profound differences of argon consumption of the new system in comparison to the conventional ICP-MS system, many of the characteristic features of the conventional ICP-MS could be maintained to a great extent. To demonstrate the ion source's capabilities, it was used as an element-selective detector for gas (GC) and high performance liquid chromatography (HPLC) where organic compounds of mercury and cobalt, respectively, were separated and detected with the new low-flow ICP-MS detection system. The corresponding chromatograms are shown. The applicability for trace element analysis has been validated with the certified reference material NIST 1643e.

  20. Volumetric plasma source development and characterization

    International Nuclear Information System (INIS)

    Crain, Marlon D.; Maron, Yitzhak; Oliver, Bryan Velten; Starbird, Robert L.; Johnston, Mark D.; Hahn, Kelly Denise; Mehlhorn, Thomas Alan; Droemer, Darryl W.

    2008-01-01

    The development of plasma sources with densities and temperatures in the 10 15 -10 17 cm -3 and 1-10eV ranges which are slowly varying over several hundreds of nanoseconds within several cubic centimeter volumes is of interest for applications such as intense electron beam focusing as part of the x-ray radiography program. In particular, theoretical work (1,2) suggests that replacing neutral gas in electron beam focusing cells with highly conductive, pre-ionized plasma increases the time-averaged e-beam intensity on target, resulting in brighter x-ray sources. This LDRD project was an attempt to generate such a plasma source from fine metal wires. A high voltage (20-60kV), high current (12-45kA) capacitive discharge was sent through a 100 (micro)m diameter aluminum wire forming a plasma. The plasma's expansion was measured in time and space using spectroscopic techniques. Lineshapes and intensities from various plasma species were used to determine electron and ion densities and temperatures. Electron densities from the mid-10 15 to mid-10 16 cm -3 were generated with corresponding electron temperatures of between 1 and 10eV. These parameters were measured at distances of up to 1.85 cm from the wire surface at times in excess of 1 (micro)s from the initial wire breakdown event. In addition, a hydrocarbon plasma from surface contaminants on the wire was also measured. Control of these contaminants by judicious choice of wire material, size, and/or surface coating allows for the ability to generate plasmas with similar density and temperature to those given above, but with lower atomic masses

  1. Metrics for comparing plasma mass filters

    Energy Technology Data Exchange (ETDEWEB)

    Fetterman, Abraham J.; Fisch, Nathaniel J. [Department of Astrophysical Sciences, Princeton University, Princeton, New Jersey 08540 (United States)

    2011-10-15

    High-throughput mass separation of nuclear waste may be useful for optimal storage, disposal, or environmental remediation. The most dangerous part of nuclear waste is the fission product, which produces most of the heat and medium-term radiation. Plasmas are well-suited to separating nuclear waste because they can separate many different species in a single step. A number of plasma devices have been designed for such mass separation, but there has been no standardized comparison between these devices. We define a standard metric, the separative power per unit volume, and derive it for three different plasma mass filters: the plasma centrifuge, Ohkawa filter, and the magnetic centrifugal mass filter.

  2. Metrics for comparing plasma mass filters

    International Nuclear Information System (INIS)

    Fetterman, Abraham J.; Fisch, Nathaniel J.

    2011-01-01

    High-throughput mass separation of nuclear waste may be useful for optimal storage, disposal, or environmental remediation. The most dangerous part of nuclear waste is the fission product, which produces most of the heat and medium-term radiation. Plasmas are well-suited to separating nuclear waste because they can separate many different species in a single step. A number of plasma devices have been designed for such mass separation, but there has been no standardized comparison between these devices. We define a standard metric, the separative power per unit volume, and derive it for three different plasma mass filters: the plasma centrifuge, Ohkawa filter, and the magnetic centrifugal mass filter.

  3. A new large-scale plasma source with plasma cathode

    International Nuclear Information System (INIS)

    Yamauchi, K.; Hirokawa, K.; Suzuki, H.; Satake, T.

    1996-01-01

    A new large-scale plasma source (200 mm diameter) with a plasma cathode has been investigated. The plasma has a good spatial uniformity, operates at low electron temperature, and is highly ionized under relatively low gas pressure of about 10 -4 Torr. The plasma source consists of a plasma chamber and a plasma cathode generator. The plasma chamber has an anode which is 200 mm in diameter, 150 mm in length, is made of 304 stainless steel, and acts as a plasma expansion cup. A filament-cathode-like plasma ''plasma cathode'' is placed on the central axis of this source. To improve the plasma spatial uniformity in the plasma chamber, a disk-shaped, floating electrode is placed between the plasma chamber and the plasma cathode. The 200 mm diameter plasma is measure by using Langmuir probes. As a result, the discharge voltage is relatively low (30-120 V), the plasma space potential is almost equal to the discharge voltage and can be easily controlled, the electron temperature is several electron volts, the plasma density is about 10 10 cm -3 , and the plasma density is about 10% variance in over a 100 mm diameter. (Author)

  4. Simulating Sources of Superstorm Plasmas

    Science.gov (United States)

    Fok, Mei-Ching

    2008-01-01

    We evaluated the contributions to magnetospheric pressure (ring current) of the solar wind, polar wind, auroral wind, and plasmaspheric wind, with the surprising result that the main phase pressure is dominated by plasmaspheric protons. We used global simulation fields from the LFM single fluid ideal MHD model. We embedded the Comprehensive Ring Current Model within it, driven by the LFM transpolar potential, and supplied with plasmas at its boundary including solar wind protons, polar wind protons, auroral wind O+, and plasmaspheric protons. We included auroral outflows and acceleration driven by the LFM ionospheric boundary condition, including parallel ion acceleration driven by upward currents. Our plasmasphere model runs within the CRCM and is driven by it. Ionospheric sources were treated using our Global Ion Kinetics code based on full equations of motion. This treatment neglects inertial loading and pressure exerted by the ionospheric plasmas, and will be superceded by multifluid simulations that include those effects. However, these simulations provide new insights into the respective role of ionospheric sources in storm-time magnetospheric dynamics.

  5. Plasma Mass Filters For Nuclear Waste Reprocessing

    International Nuclear Information System (INIS)

    Fetterman, Abraham J.; Fisch, Nathaniel J.

    2011-01-01

    Practical disposal of nuclear waste requires high-throughput separation techniques. The most dangerous part of nuclear waste is the fission product, which contains the most active and mobile radioisotopes and produces most of the heat. We suggest that the fission products could be separated as a group from nuclear waste using plasma mass filters. Plasmabased processes are well suited to separating nuclear waste, because mass rather than chemical properties are used for separation. A single plasma stage can replace several stages of chemical separation, producing separate streams of bulk elements, fission products, and actinoids. The plasma mass filters may have lower cost and produce less auxiliary waste than chemical processing plants. Three rotating plasma configurations are considered that act as mass filters: the plasma centrifuge, the Ohkawa filter, and the asymmetric centrifugal trap.

  6. Plasma-surface interaction in negative hydrogen ion sources

    Science.gov (United States)

    Wada, Motoi

    2018-05-01

    A negative hydrogen ion source delivers more beam current when Cs is introduced to the discharge, but a continuous operation of the source reduces the beam current until more Cs is added to the source. This behavior can be explained by adsorption and ion induced desorption of Cs atoms on the plasma grid surface of the ion source. The interaction between the ion source plasma and the plasma grid surface of a negative hydrogen ion source is discussed in correlation to the Cs consumption of the ion source. The results show that operation with deuterium instead of hydrogen should require more Cs consumption and the presence of medium mass impurities as well as ions of the source wall materials in the arc discharge enlarges the Cs removal rate during an ion source discharge.

  7. Ion acceleration in the plasma source sheath

    International Nuclear Information System (INIS)

    Birdsall, C.K.

    1986-01-01

    This note is a calculation of the potential drop for a planar plasma source, across the source sheath, into a uniform plasma region defined by vector E = 0 and/or perhaps ∂ 2 PHI/∂ x 2 = 0. The calculation complements that of Bohm who obtained the potential drop at the other end of a plasma, at a planar collector sheath. The result is a relation between the source ion flux and the source sheath potential drop and the accompanying ion acceleration. This planar source sheath ion acceleration mechanism (or that from a distributed source) can provide the pre-collector-sheath ion acceleration as found necessary by Bohm. 3 refs

  8. Large area ion and plasma beam sources

    Energy Technology Data Exchange (ETDEWEB)

    Waldorf, J. [IPT Ionen- und Plasmatech. GmbH, Kaiserslautern (Germany)

    1996-06-01

    In the past a number of ion beam sources utilizing different methods for plasma excitation have been developed. Nevertheless, a widespread use in industrial applications has not happened, since the sources were often not able to fulfill specific demands like: broad homogeneous ion beams, compatibility with reactive gases, low ion energies at high ion current densities or electrical neutrality of the beam. Our contribution wants to demonstrate technical capabilities of rf ion and plasma beam sources, which can overcome the above mentioned disadvantages. The physical principles and features of respective sources are presented. We report on effective low pressure plasma excitation by electron cyclotron wave resonance (ECWR) for the generation of dense homogeneous plasmas and the rf plasma beam extraction method for the generation of broad low energy plasma beams. Some applications like direct plasma beam deposition of a-C:H and ion beam assisted deposition of Al and Cu with tailored thin film properties are discussed. (orig.).

  9. Large area ion and plasma beam sources

    International Nuclear Information System (INIS)

    Waldorf, J.

    1996-01-01

    In the past a number of ion beam sources utilizing different methods for plasma excitation have been developed. Nevertheless, a widespread use in industrial applications has not happened, since the sources were often not able to fulfill specific demands like: broad homogeneous ion beams, compatibility with reactive gases, low ion energies at high ion current densities or electrical neutrality of the beam. Our contribution wants to demonstrate technical capabilities of rf ion and plasma beam sources, which can overcome the above mentioned disadvantages. The physical principles and features of respective sources are presented. We report on effective low pressure plasma excitation by electron cyclotron wave resonance (ECWR) for the generation of dense homogeneous plasmas and the rf plasma beam extraction method for the generation of broad low energy plasma beams. Some applications like direct plasma beam deposition of a-C:H and ion beam assisted deposition of Al and Cu with tailored thin film properties are discussed. (orig.)

  10. Surface plasma source with saddle antenna radio frequency plasma generator.

    Science.gov (United States)

    Dudnikov, V; Johnson, R P; Murray, S; Pennisi, T; Piller, C; Santana, M; Stockli, M; Welton, R

    2012-02-01

    A prototype RF H(-) surface plasma source (SPS) with saddle (SA) RF antenna is developed which will provide better power efficiency for high pulsed and average current, higher brightness with longer lifetime and higher reliability. Several versions of new plasma generators with small AlN discharge chambers and different antennas and magnetic field configurations were tested in the plasma source test stand. A prototype SA SPS was installed in the Spallation Neutron Source (SNS) ion source test stand with a larger, normal-sized SNS AlN chamber that achieved unanalyzed peak currents of up to 67 mA with an apparent efficiency up to 1.6 mA∕kW. Control experiments with H(-) beam produced by SNS SPS with internal and external antennas were conducted. A new version of the RF triggering plasma gun has been designed. A saddle antenna SPS with water cooling is fabricated for high duty factor testing.

  11. Plasma focus - a pulsed radiation source

    International Nuclear Information System (INIS)

    Blagoev, Alexandar; Zapryanov, Stanislav; Gol'tsev, Vasilii; Gemishev, Orlin

    2014-01-01

    The article is devoted to the applications of plasma focus (PF) in radiobiology. Briefly describes the principle of operation of the device and the parameters of the PF type 'Mader' at the Physics Department of the University. Phase pinch discharge zones appear hot and dense plasma, which is a source of X-ray and neutron pulse when the working gas is deuterium. These radiations are essential for biological applications. Besides these bundles are obtained from accelerated charged particles and shock wave of ionized gas. Described are some of the contributions of other authors using PF in radiobiology. Given the results in the exposure of living organisms with soft X-ray emission of PF. We examined the viability of the cells of the two types of yeasts, after irradiation with X-rays at a dose of 65 mSv, where no change was found on the performance. It is shown that soft X-ray radiation doses on the order of tens of mSv, cause a significant change in the productivity of the electronic transport in the photosynthetic apparatus of Chlamydomonas reinhardtii. Trichoderma reesei M7 shows remarkable vitality irradiation with substantial doses of hard X-ray radiation (tens Sv). Appear endoglyukonazata changes in the protein component and the residual mass

  12. Simple microwave plasma source at atmospheric pressure

    International Nuclear Information System (INIS)

    Kim, Jeong H.; Hong, Yong C.; Kim, Hyoung S.; Uhm, Han S.

    2003-01-01

    We have developed a thermal plasma source operating without electrodes. One electrodeless torch is the microwave plasma-torch, which can produce plasmas in large quantities. We can generate plasma at an atmospheric pressure by marking use of the same magnetrons used as commercial microwave ovens. Most of the magnetrons are operated at the frequency of 2.45 GHz; the magnetron power microwave is about 1kW. Electromagnetic waves from the magnetrons propagate through a shorted waveguide. Plasma was generated under a resonant condition, by an auxiliary ignition system. The plasma is stabilized by vortex stabilization. Also, a high-power and high-efficiency microwave plasma-torch has been operated in air by combining two microwave plasma sources with 1kW, 2.45 GHz. They are arranged in series to generate a high-power plasma flame. The second torch adds all its power to the plasma flame of the first torch. Basically, electromagnetic waves in the waveguide were studied by a High Frequency Structure Simulator (HFSS) code and preliminary experiments were conducted

  13. Inductively coupled plasma- mass spectrometry. Chapter 13

    International Nuclear Information System (INIS)

    Mahalingam, T.R.

    1997-01-01

    Inductively Coupled Plasma - Mass Spectrometry (ICP-MS) is a new technique for elemental and isotopic analysis which is currently attracting a great deal of interest. This relatively new technique has found wide applications in different fields of research viz., nuclear, geological, biological and environmental sciences

  14. Plasma x-ray radiation source.

    Science.gov (United States)

    Popkov, N F; Kargin, V I; Ryaslov, E A; Pikar', A S

    1995-01-01

    This paper gives the results of studies on a plasma x-ray source, which enables one to obtain a 2.5-krad radiation dose per pulse over an area of 100 cm2 in the quantum energy range from 20 to 500 keV. Pulse duration is 100 ns. Spectral radiation distributions from a diode under various operation conditions of a plasma are obtained. A Marx generator served as an initial energy source of 120 kJ with a discharge time of T/4 = 10-6 s. A short electromagnetic pulse (10-7 s) was shaped using plasma erosion opening switches.

  15. On plasma ion beam formation in the Advanced Plasma Source

    International Nuclear Information System (INIS)

    Harhausen, J; Foest, R; Hannemann, M; Ohl, A; Brinkmann, R P; Schröder, B

    2012-01-01

    The Advanced Plasma Source (APS) is employed for plasma ion-assisted deposition (PIAD) of optical coatings. The APS is a hot cathode dc glow discharge which emits a plasma ion beam to the deposition chamber at high vacuum (p ≲ 2 × 10 −4 mbar). It is established as an industrial tool but to date no detailed information is available on plasma parameters in the process chamber. As a consequence, the details of the generation of the plasma ion beam and the reasons for variations of the properties of the deposited films are barely understood. In this paper the results obtained from Langmuir probe and retarding field energy analyzer diagnostics operated in the plasma plume of the APS are presented, where the source was operated with argon. With increasing distance to the source exit the electron density (n e ) is found to drop by two orders of magnitude and the effective electron temperature (T e,eff ) drops by a factor of five. The parameters close to the source region read n e ≳ 10 11 cm −3 and T e,eff ≳ 10 eV. The electron distribution function exhibits a concave shape and can be described in the framework of the non-local approximation. It is revealed that an energetic ion population leaves the source region and a cold ion population in the plume is build up by charge exchange collisions with the background neutral gas. Based on the experimental data a scaling law for ion beam power is deduced, which links the control parameters of the source to the plasma parameters in the process chamber. (paper)

  16. Measuring the Plasma Density of a Ferroelectric Plasma Source in an Expanding Plasma

    International Nuclear Information System (INIS)

    Dunaevsky, A.; Fisch, N.J.

    2003-01-01

    The initial density and electron temperature at the surface of a ferroelectric plasma source were deduced from floating probe measurements in an expanding plasma. The method exploits negative charging of the floating probe capacitance by fast flows before the expanding plasma reaches the probe. The temporal profiles of the plasma density can be obtained from the voltage traces of the discharge of the charged probe capacitance by the ion current from the expanding plasma. The temporal profiles of the plasma density, at two different distances from the surface of the ferroelectric plasma source, could be further fitted by using the density profiles for the expanding plasma. This gives the initial values of the plasma density and electron temperature at the surface. The method could be useful for any pulsed discharge, which is accompanied by considerable electromagnetic noise, if the initial plasma parameters might be deduced from measurements in expanding plasma

  17. Construction of a high beta plasma source

    International Nuclear Information System (INIS)

    Naraghi, M.; Torabi-Fard, A.

    1976-02-01

    A high beta plasma source has been designed and constructed. This source will serve as a means of developing and exercising different diagnostic techniques as required for ALVAND I, linear theta pinch experiment. Also, it will serve to acquaint the technicians with some of the techniques and safety rules of high voltage and capacitor discharge experiments. The operating parameters of the theta pinch and Z-pinch preionization is presented and the program of diagnostic measurements on the high beta plasma source is discussed

  18. Consideration of beam plasma ion-source

    International Nuclear Information System (INIS)

    Sano, Fumimichi; Kusano, Norimasa; Ishida, Yoshihiro; Ishikawa, Junzo; Takagi, Toshinori

    1976-01-01

    Theoretical and experimental analyses and their comparison were made on the plasma generation and on the beam extraction for the beam plasma ion-source. The operational principle and the structure of the ion-source are explained in the first part. Considerations are given on the electron beam-plasma interaction and the resulting generation of high frequency or microwaves which in turn increases the plasma density. The flow of energy in this system is also explained in the second part. The relation between plasma density and the imaginary part of frequency is given by taking the magnetic flux density, the electron beam energy, and the electron beam current as parameters. The relations between the potential difference between collector and drift tube and the plasma density or the ion-current are also given. Considerations are also given to the change of the plasma density due to the change of the magnetic flux density at drift tube, the change of the electron beam energy, and the change of the electron beam current. The third part deals with the extraction characteristics of the ion beam. The structure of the multiple-aperture electrode and the relation between plasma density and the extracted ion current are explained. (Aoki, K.)

  19. Moderate pressure plasma source of nonthermal electrons

    Science.gov (United States)

    Gershman, S.; Raitses, Y.

    2018-06-01

    Plasma sources of electrons offer control of gas and surface chemistry without the need for complex vacuum systems. The plasma electron source presented here is based on a cold cathode glow discharge (GD) operating in a dc steady state mode in a moderate pressure range of 2–10 torr. Ion-induced secondary electron emission is the source of electrons accelerated to high energies in the cathode sheath potential. The source geometry is a key to the availability and the extraction of the nonthermal portion of the electron population. The source consists of a flat and a cylindrical electrode, 1 mm apart. Our estimates show that the length of the cathode sheath in the plasma source is commensurate (~0.5–1 mm) with the inter-electrode distance so the GD operates in an obstructed regime without a positive column. Estimations of the electron energy relaxation confirm the non-local nature of this GD, hence the nonthermal portion of the electron population is available for extraction outside of the source. The use of a cylindrical anode presents a simple and promising method of extracting the high energy portion of the electron population. Langmuir probe measurements and optical emission spectroscopy confirm the presence of electrons with energies ~15 eV outside of the source. These electrons become available for surface modification and radical production outside of the source. The extraction of the electrons of specific energies by varying the anode geometry opens exciting opportunities for future exploration.

  20. Resonant power absorption in helicon plasma sources

    International Nuclear Information System (INIS)

    Chen Guangye; Arefiev, Alexey V.; Bengtson, Roger D.; Breizman, Boris N.; Lee, Charles A.; Raja, Laxminarayan L.

    2006-01-01

    Helicon discharges produce plasmas with a density gradient across the confining magnetic field. Such plasmas can create a radial potential well for nonaxisymmetric whistlers, allowing radially localized helicon (RLH) waves. This work presents new evidence that RLH waves play a significant role in helicon plasma sources. An experimentally measured plasma density profile in an argon helicon discharge is used to calculate the rf field structure. The calculations are performed using a two-dimensional field solver under the assumption that the density profile is axisymmetric. It is found that RLH waves with an azimuthal wave number m=1 form a standing wave structure in the axial direction and that the frequency of the RLH eigenmode is close to the driving frequency of the rf antenna. The calculated resonant power absorption, associated with the RLH eigenmode, accounts for most of the rf power deposited into the plasma in the experiment

  1. Plasma-based EUV light source

    Science.gov (United States)

    Shumlak, Uri; Golingo, Raymond; Nelson, Brian A.

    2010-11-02

    Various mechanisms are provided relating to plasma-based light source that may be used for lithography as well as other applications. For example, a device is disclosed for producing extreme ultraviolet (EUV) light based on a sheared plasma flow. The device can produce a plasma pinch that can last several orders of magnitude longer than what is typically sustained in a Z-pinch, thus enabling the device to provide more power output than what has been hitherto predicted in theory or attained in practice. Such power output may be used in a lithography system for manufacturing integrated circuits, enabling the use of EUV wavelengths on the order of about 13.5 nm. Lastly, the process of manufacturing such a plasma pinch is discussed, where the process includes providing a sheared flow of plasma in order to stabilize it for long periods of time.

  2. Microwave interferometry of PEOS plasma sources

    International Nuclear Information System (INIS)

    Weber, B.V.; Commisso, R.J.; Goodrich, P.J.; Hinshelwood, D.D.; Neri, J.M.

    1988-01-01

    A 70 GHz microwave interferometer is used to measure the electron density for various configurations of sources used in plasma erosion opening switch (PEOS) experiments. The interferometer is a phase quadrature system, so the density can be measured as a function of time without ambiguity. Measurements have been made for carbon guns and flashboards driven by a .6 μF. 25 kV capacitor. The plasma density from a gun rises to its peak value in about 10 μs. Then decays in the next 40 μs. A metal screen placed between the gun and the microwave beam attenuates the plasma density by a factor greater than the geometrical transparency of the screen. Density measurements as a function of distance from the gun are analyzed to give the plasma spatial dependence, and the particle flux density and flow velocity are calculated from the continuity equation. Density values used to model previous PEOS experiments are comparable to the values measured here. The flashboard sources produce a denser, faster plasma that is more difficult to diagnose with the interferometer than the gun plasma because of refractive bending of the microwave beam. Reducing the plasma length reduces the refractive bending enough that some measurements are possible. Direct comparison with Gamble II PEOS experiments that used these flashboard sources may not be possible at this frequency because of refraction, but estimates based on measurements at larger distances give reasonable agreement with values used to model these experiments. Other measurements that will be presented include the effects of plasma flow against metal walls, effects of changing the driving current waveform, measurements made in actual experimental configurations and comparisons with Faraday cup and electric probe measurements

  3. Ion deposition by inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Hu, K.; Houk, R.S.

    1996-01-01

    An atmospheric pressure inductively coupled plasma (ICP) is used with a quadrupole mass spectrometer (MS) for ion deposition. The deposited element is introduced as a nebulized aqueous solution. Modifications to the ICP-MS device allow generation and deposition of a mass-resolved beam of 165 Ho + at 5x10 12 ions s -1 . The ICP is a universal, multielement ion source that can potentially be used for applications such as deposition of mixtures of widely varying stoichiometry or of alternating layers of different elements. copyright 1996 American Vacuum Society

  4. Adaptation of metal arc plasma source to plasma source ion implantation

    International Nuclear Information System (INIS)

    Shamim, M.M.; Fetherston, R.P.; Conrad, J.R.

    1995-01-01

    In Plasma Source Ion Implantation (PSII) a target is immersed in a plasma and a train of high negative voltage pulses is applied to accelerate ions into the target and to modify the properties in the near surface region. In PSII, until now the authors have been using gaseous species to generate plasmas. However metal ion plasma may be used to modify the surface properties of material for industrial applications. Conventionally the ion implantation of metal ions is performed using beam line accelerators which have complex engineering and high cost. The employment of a metal arc source to PSII has tremendous potential due to its ability to process the conformal surfaces, simple engineering and cost effectiveness. They have installed metal arc source for generation of titanium plasma. Currently, they are investigating the properties of titanium plasma and material behavior of titanium implanted aluminum and 52100 steel. The recent results of this investigation are presented

  5. High-Current Plasma Electron Sources

    International Nuclear Information System (INIS)

    Gushenets, J.Z.; Krokhmal, V.A.; Krasik, Ya. E.; Felsteiner, J.; Gushenets, V.

    2002-01-01

    In this report we present the design, electrical schemes and preliminary results of a test of 4 different electron plasma cathodes operating under Kg h-voltage pulses in a vacuum diode. The first plasma cathode consists of 6 azimuthally symmetrically distributed arc guns and a hollow anode having an output window covered by a metal grid. Plasma formation is initiated by a surface discharge over a ceramic washer placed between a W-made cathode and an intermediate electrode. Further plasma expansion leads to a redistribution of the discharge between the W-cathode and the hollow anode. An accelerating pulse applied between the output anode grid and the collector extracts electrons from this plasma. The operation of another plasma cathode design is based on Penning discharge for preliminary plasma formation. The main glow discharge occurs between an intermediate electrode of the Penning gun and the hollow anode. To keep the background pressure in the accelerating gap at P S 2.5x10 4 Torr either differential pumping or a pulsed gas puff valve were used. The operation of the latter electron plasma source is based on a hollow cathode discharge. To achieve a sharp pressure gradient between the cathode cavity and the accelerating gap a pulsed gas puff valve was used. A specially designed ferroelectric plasma cathode initiated plasma formation inside the hollow cathode. This type of the hollow cathode discharge ignition allowed to achieve a discharge current of 1.2 kA at a background pressure of 2x10 4 Torr. All these cathodes were developed and initially tested inside a planar diode with a background pressure S 2x10 4 Torr under the same conditions: accelerating voltage 180 - 300 kV, pulse duration 200 - 400 ns, electron beam current - 1 - 1.5 kA, and cross-sectional area of the extracted electron beam 113 cm 2

  6. Characterization of the pulse plasma source

    International Nuclear Information System (INIS)

    Milosavljevic, V; Karkari, S K; Ellingboe, A R

    2007-01-01

    Characterization of the pulse plasma source through the determination of the local thermodynamic equilibrium (LTE) threshold is described. The maximum electron density measured at the peak in discharge current is determined by the width of the He II Paschen alpha spectral line, and the electron temperature is determined from the ratios of the relative intensities of spectral lines emitted from successive ionized stages of atoms. The electron density and temperature maximum values are measured to be 1.3 x 10 17 cm -3 and 19 000 K, respectively. These are typical characteristics for low-pressure, pulsed plasma sources for input energy of 15.8 J at 130 Pa pressure in helium-argon mixture. The use of LTE-based analysis of the emission spectra is justified by measurement of the local plasma electron density at four positions in the discharge tube using a floating hairpin resonance probe. The hairpin resonance probe data are collected during the creation and decay phases of the pulse. From the spatio-temporal profile of the plasma density a 60 μs time-window during which LTE exists throughout the entire plasma source is determined

  7. Development of very large helicon plasma source

    International Nuclear Information System (INIS)

    Shinohara, Shunjiro; Tanikawa, Takao

    2004-01-01

    We have developed a very large volume, high-density helicon plasma source, 75 cm in diameter and 486 cm in axial length; full width at half maximum of the plasma density is up to ∼42 cm with good plasma uniformity along the z axis. By the use of a spiral antenna located just outside the end of the vacuum chamber through a quartz-glass window, plasma can be initiated with a very low value of radio frequency (rf) power ( 12 cm -3 is successfully produced with less than several hundred Watt; achieving excellent discharge efficiency. It is possible to control the radial density profile in this device by changing the magnetic field configurations near the antenna and/or the antenna radiation-field patterns

  8. Plasma sources of solar system magnetospheres

    CERN Document Server

    Blanc, Michel; Chappell, Charles; Krupp, Norbert

    2016-01-01

    This volume reviews what we know of the corresponding plasma source for each intrinsically magnetized planet. Plasma sources fall essentially in three categories: the solar wind, the ionosphere (both prevalent on Earth), and the satellite-related sources. Throughout the text, the case of each planet is described, including the characteristics, chemical composition and intensity of each source. The authors also describe how the plasma generated at the source regions is transported to populate the magnetosphere, and how it is later lost. To summarize, the dominant sources are found to be the solar wind and sputtered surface ions at Mercury, the solar wind and ionosphere at Earth (the relative importance of the two being discussed in a specific introductory chapter), Io at Jupiter and – a big surprise of the Cassini findings – Enceladus at Saturn. The situation for Uranus and Neptune, which were investigated by only one fly-by each, is still open and requires further studies and exploration. In the final cha...

  9. Double plasma system with inductively coupled source plasma and quasi-quiescent target plasma

    International Nuclear Information System (INIS)

    Massi, M.; Maciel, H.S.

    1995-01-01

    Cold plasmas have successfully been used in the plasma-assisted material processing industry. An understanding of the physicochemical mechanisms involved in the plasma-surface interaction is needed for a proper description of deposition and etching processes at material surfaces. Since these mechanisms are dependent on the plasma properties, the development of diagnostic techniques is strongly desirable for determination of the plasma parameters as well as the characterization of the electromagnetic behaviour of the discharge. In this work a dual discharge chamber, was specially designed to study the deposition of thin films via plasma polymerization process. In the Pyrex chamber an inductively coupled plasma can be excited either in the diffuse low density E-mode or in the high density H-mode. This plasma diffuses into the cylindrical stainless steel chamber which is covered with permanent magnets to produce a multidipole magnetic field configuration at the surface. By that means a double plasma is established consisting of a RF source plasma coupled to a quasi-quiescent target plasma. The preliminary results presented here refer to measurements of the profiles of plasma parameters along the central axis of the double plasma apparatus. Additionally a spectrum analysis performed by means of a Rogowski coil probe immersed into the source plasma is also presented. The discharge is made in argon with pressure varying from 10 -2 to 1 torr, and the rf from 10 to 150 W

  10. Burning plasmas in ITER for energy source

    International Nuclear Information System (INIS)

    Inoue, Nobuyuki

    2002-01-01

    Fusion research and development has two aspects. One is an academic research on science and technology, i.e., discovery and understanding of unexpected phenomena and, development of innovative technology, respectively. The other is energy source development to realize fusion as a viable energy future. Fusion research has been made remarkable progress in the past several decades, and ITER will soon realize burning plasma that is essential for both academic research and energy development. With ITER, scientific research on unknown phenomena such as self-organization of the plasma in burning state will become possible and it contributes to create a variety of academic outcome. Fusion researchers will have a responsibility to generate actual energy, and electricity generation immediately after the success of burning plasma control experiment in ITER is the next important step that has to be discussed seriously. (author)

  11. Burning plasmas in ITER for energy source

    Energy Technology Data Exchange (ETDEWEB)

    Inoue, Nobuyuki [Atomic Energy Commission, Tokyo (Japan)

    2002-10-01

    Fusion research and development has two aspects. One is an academic research on science and technology, i.e., discovery and understanding of unexpected phenomena and, development of innovative technology, respectively. The other is energy source development to realize fusion as a viable energy future. Fusion research has been made remarkable progress in the past several decades, and ITER will soon realize burning plasma that is essential for both academic research and energy development. With ITER, scientific research on unknown phenomena such as self-organization of the plasma in burning state will become possible and it contributes to create a variety of academic outcome. Fusion researchers will have a responsibility to generate actual energy, and electricity generation immediately after the success of burning plasma control experiment in ITER is the next important step that has to be discussed seriously. (author)

  12. Note: Possibilities of detecting the trace-level erosion products from an electric propulsion hollow cathode plasma source by the method of time-of-flight mass spectrometry

    Science.gov (United States)

    Ning, Zhong-Xi; Zhang, Hai-Guang; Zhu, Xi-Ming; Jiang, Bin-Hao; Zhou, Zhong-Yue; Yu, Da-Ren; An, Bing-Jian; Wang, Yan-Fei

    2018-02-01

    A hollow cathode produces electrons which neutralize ions from electric propulsion thrusters. After hundreds to thousands of hours of operation in space, the cathode materials can be significantly eroded due to ion bombardment. As a result, the electric propulsion system performance will be obviously changed or even fail. In this work, the erosion products from a LaB6 hollow cathode (widely used presently in electric propulsion systems) are studied by using a specific detection system, which consists of a molecular beam sampler and a time-of-flight mass spectrometer. This system measures trace-level-concentration (10-6-10-3) products. Boron (B), tantalum (Ta), and tungsten (W)—originating from the emitter, keeper, and orifice of the hollow cathode—are measured. It is found that the erosion rate is significantly influenced by the gas flow rate to the cathode.

  13. Microwave Plasma Sources for Gas Processing

    International Nuclear Information System (INIS)

    Mizeraczyk, J.; Jasinski, M.; Dors, M.; Zakrzewski, Z.

    2008-01-01

    In this paper atmospheric pressure microwave discharge methods and devices used for producing the non-thermal plasmas for processing of gases are presented. The main part of the paper concerns the microwave plasma sources (MPSs) for environmental protection applications. A few types of the MPSs, i.e. waveguide-based surface wave sustained MPS, coaxial-line-based and waveguide-based nozzle-type MPSs, waveguide-based nozzleless cylinder-type MPS and MPS for microdischarges are presented. Also, results of the laboratory experiments on the plasma processing of several highly-concentrated (up to several tens percent) volatile organic compounds (VOCs), including Freon-type refrigerants, in the moderate (200-400 W) waveguide-based nozzle-type MPS (2.45 GHz) are presented. The results showed that the microwave discharge plasma fully decomposed the VOCs at relatively low energy cost. The energy efficiency of VOCs decomposition reached 1000 g/kWh. This suggests that the microwave discharge plasma can be a useful tool for environmental protection applications. In this paper also results of the use of the waveguide-based nozzleless cylinder-type MPS to methane reforming into hydrogen are presented

  14. Hall Current Plasma Source Having a Center-Mounted or a Surface-Mounted Cathode

    Science.gov (United States)

    Martinez, Rafael A. (Inventor); Williams, John D. (Inventor); Moritz, Jr., Joel A. (Inventor); Farnell, Casey C. (Inventor)

    2018-01-01

    A miniature Hall current plasma source apparatus having magnetic shielding of the walls from ionized plasma, an integrated discharge channel and gas distributor, an instant-start hollow cathode mounted to the plasma source, and an externally mounted keeper, is described. The apparatus offers advantages over other Hall current plasma sources having similar power levels, including: lower mass, longer lifetime, lower part count including fewer power supplies, and the ability to be continuously adjustable to lower average power levels using pulsed operation and adjustment of the pulse duty cycle. The Hall current plasma source can provide propulsion for small spacecraft that either do not have sufficient power to accommodate a propulsion system or do not have available volume to incorporate the larger propulsion systems currently available. The present low-power Hall current plasma source can be used to provide energetic ions to assist the deposition of thin films in plasma processing applications.

  15. Development and application of helicon plasma sources. Evolution of extensive plasma science

    International Nuclear Information System (INIS)

    Shinohara, Shunjiro

    2009-01-01

    Recent advances in plasma science are remarkable, and are deeply indebted to the development of sophisticated plasma sources. While numerous methods have been proposed for producing the plasma, helicon plasma sources, capable of generating high density (>10 13 cm -3 ) plasma with high ionization degree (>several ten percent) over a wide range of external control parameters, have been utilized in such broad areas as fundamental and processing plasmas, nuclear fusion, gas laser, modeling of space plasma, plasma acceleration/propulsion, among others. On the other hand, a number of important issues are left unsolved, in particular, those relevant to the wave phenomena and efficient plasma production. Solution to these issues are expected to play key roles in taking full advantage of the helicon plasma sources in the next generation. In this article, we overview our current understanding of the helicon plasma production and recent development of characteristic helicon plasma sources, and discuss possible future advancement of extensive plasma science utilizing them. (author)

  16. 21 CFR 640.74 - Modification of Source Plasma.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 7 2010-04-01 2010-04-01 false Modification of Source Plasma. 640.74 Section 640...) BIOLOGICS ADDITIONAL STANDARDS FOR HUMAN BLOOD AND BLOOD PRODUCTS Source Plasma § 640.74 Modification of Source Plasma. (a) Upon approval by the Director, Center for Biologics Evaluation and Research, Food and...

  17. Magnetic plasma confinement for laser ion source

    International Nuclear Information System (INIS)

    Okamura, M.; Adeyemi, A.; Kanesue, T.; Tamura, J.; Kondo, K.; Dabrowski, R.

    2010-01-01

    A laser ion source (LIS) can easily provide a high current beam. However, it has been difficult to obtain a longer beam pulse while keeping a high current. On occasion, longer beam pulses are required by certain applications. For example, more than 10 μs of beam pulse is required for injecting highly charged beams to a large sized synchrotron. To extend beam pulse width, a solenoid field was applied at the drift space of the LIS at Brookhaven National Laboratory. The solenoid field suppressed the diverging angle of the expanding plasma and the beam pulse was widened. Also, it was observed that the plasma state was conserved after passing through a few hundred gauss of the 480 mm length solenoid field.

  18. Magnetic plasma confinement for laser ion source.

    Science.gov (United States)

    Okamura, M; Adeyemi, A; Kanesue, T; Tamura, J; Kondo, K; Dabrowski, R

    2010-02-01

    A laser ion source (LIS) can easily provide a high current beam. However, it has been difficult to obtain a longer beam pulse while keeping a high current. On occasion, longer beam pulses are required by certain applications. For example, more than 10 micros of beam pulse is required for injecting highly charged beams to a large sized synchrotron. To extend beam pulse width, a solenoid field was applied at the drift space of the LIS at Brookhaven National Laboratory. The solenoid field suppressed the diverging angle of the expanding plasma and the beam pulse was widened. Also, it was observed that the plasma state was conserved after passing through a few hundred gauss of the 480 mm length solenoid field.

  19. Mass spectrometer with two ion sources

    International Nuclear Information System (INIS)

    Glickman, L.G.; Mit', A.G.

    2002-01-01

    Static mass spectrometer with mid-plane near which ions are moving is considered in this article. Two ion sources are used, their exit slits are perpendicular to the mid-plane. The simple method of the replacement of source is offered. Two concave two-electrode transaxial mirrors with two-plate electrodes are used for this aim. The mid-plane of these mirrors coincides with the mid-plane of the device. The exit slit of each source is located in the principal plane of the object space. The principal planes of the image space of the both mirrors coincide. The images of the exit slits of the sources are in these planes and coincide too. We used the mirrors making stigmatic images with the magnification one to one, in which the dispersion on energy and spherical aberrations of the second order are equal to zero. These images are the objects on which the ion-optical system of the mass spectrometer is tuned. When you choose one from two ion sources it is enough to switch the corresponding mirror

  20. Atmospheric pressure plasma analysis by modulated molecular beam mass spectrometry

    NARCIS (Netherlands)

    Aranda Gonzalvo, Y.; Whitmore, T.D.; Rees, J.A.; Seymour, D.L.; Stoffels - Adamowicz, E.

    2006-01-01

    Fractional no. d. measurements for a radiofrequency plasma needle operating at atm. pressure were obtained using a mol. beam mass spectrometer (MBMS) system designed for diagnostics of atm. plasmas. The MBMS system comprises three differentially pumped stages and a mass/energy analyzer and includes

  1. Sample preparations for spark source mass spectrography

    International Nuclear Information System (INIS)

    Catlett, C.W.; Rollins, M.B.; Griffin, E.B.; Dorsey, J.G.

    1977-10-01

    Methods have been developed for the preparation of various materials for spark source mass spectrography. The essential features of these preparations (all which can provide adequate precision in a cost-effective manner) consist in obtaining spark-stable electrode sample pieces, a common matrix, a reduction of anomolous effects in the spark, the incorporation of a suitable internal standard for plate response normalization, and a reduction in time

  2. Inertial electro-magnetostatic plasma neutron sources

    International Nuclear Information System (INIS)

    Barnes, D.C.; Nebel, R.A.; Schauer, M.M.; Pickrel, M.M.

    1997-01-01

    Two types of systems are being studied experimentally as D-T plasma neutron sources. In both concepts, spherical convergence of either electrons or ions or both is used to produce a dense central focus within which D-T fusion reactions produce 14 MeV neutrons. One concept uses nonneutral plasma confinement principles in a Penning type trap. In this approach, combined electrostatic and magnetic fields provide a vacuum potential well within which electrons are confined and focused. A small (6 mm radius) spherical machine has demonstrated a focus of 30 microm radius, with a central density of up to 35 times the Brillouin density limit of a static trap. The resulting electron plasma of up to several 10 13 cm -3 provides a multi-kV electrostatic well for confining thermonuclear ions as a neutron source. The second concept (Inertial Electrostatic Confinement, or IEC) uses a high-transparence grid to form a global well for acceleration and confinement of ions. Such a system has demonstrated steady neutron output of 2 x 10 10 s -1 . The present experiment will scale this to >10 11 s -1 . Advanced designs based on each concept have been developed recently. In these proposed approaches, a uniform-density electron sphere forms an electrostatic well for ions. Ions so trapped may be focused by spherical convergence to produce a dense core. An alternative approach produces large amplitude spherical oscillations of a confined ion cloud by a small, resonant modulation of the background electrons. In both the advanced Penning trap approach and the advanced IEC approach, the electrons are magnetically insulated from a large (up to 100 kV) applied electrostatic field. The physics of these devices is discussed, experimental design details are given, present observations are analyzed theoretically, and the performance of future advanced systems are predicted

  3. Plasma Processing of Metallic and Semiconductor Thin Films in the Fisk Plasma Source

    Science.gov (United States)

    Lampkin, Gregory; Thomas, Edward, Jr.; Watson, Michael; Wallace, Kent; Chen, Henry; Burger, Arnold

    1998-01-01

    The use of plasmas to process materials has become widespread throughout the semiconductor industry. Plasmas are used to modify the morphology and chemistry of surfaces. We report on initial plasma processing experiments using the Fisk Plasma Source. Metallic and semiconductor thin films deposited on a silicon substrate have been exposed to argon plasmas. Results of microscopy and chemical analyses of processed materials are presented.

  4. Laboratory Plasma Source as an MHD Model for Astrophysical Jets

    Science.gov (United States)

    Mayo, Robert M.

    1997-01-01

    The significance of the work described herein lies in the demonstration of Magnetized Coaxial Plasma Gun (MCG) devices like CPS-1 to produce energetic laboratory magneto-flows with embedded magnetic fields that can be used as a simulation tool to study flow interaction dynamic of jet flows, to demonstrate the magnetic acceleration and collimation of flows with primarily toroidal fields, and study cross field transport in turbulent accreting flows. Since plasma produced in MCG devices have magnetic topology and MHD flow regime similarity to stellar and extragalactic jets, we expect that careful investigation of these flows in the laboratory will reveal fundamental physical mechanisms influencing astrophysical flows. Discussion in the next section (sec.2) focuses on recent results describing collimation, leading flow surface interaction layers, and turbulent accretion. The primary objectives for a new three year effort would involve the development and deployment of novel electrostatic, magnetic, and visible plasma diagnostic techniques to measure plasma and flow parameters of the CPS-1 device in the flow chamber downstream of the plasma source to study, (1) mass ejection, morphology, and collimation and stability of energetic outflows, (2) the effects of external magnetization on collimation and stability, (3) the interaction of such flows with background neutral gas, the generation of visible emission in such interaction, and effect of neutral clouds on jet flow dynamics, and (4) the cross magnetic field transport of turbulent accreting flows. The applicability of existing laboratory plasma facilities to the study of stellar and extragalactic plasma should be exploited to elucidate underlying physical mechanisms that cannot be ascertained though astrophysical observation, and provide baseline to a wide variety of proposed models, MHD and otherwise. The work proposed herin represents a continued effort on a novel approach in relating laboratory experiments to

  5. Determination of osmium concentrations and (187)Os/(188)Os of crude oils and source rocks by coupling high-pressure, high-temperature digestion with sparging OsO(4) into a multicollector inductively coupled plasma mass spectrometer.

    Science.gov (United States)

    Sen, Indra S; Peucker-Ehrenbrink, Bernhard

    2014-03-18

    The (187)Os/(188)Os ratio that is based on the β(-)-decay of (187)Re to (187)Os (t1/2 = 41.6 billion years) is widely used to investigate petroleum system processes. Despite its broad applicability to studies of hydrocarbon deposits worldwide, a suitable matrix-matched reference material for Os analysis does not exist. In this study, a method that enables Os isotope measurement of crude oil with in-line Os separation and purification from the sample matrix is proposed. The method to analyze Os concentration and (187)Os/(187)Os involves sample digestion under high pressure and high temperature using a high pressure asher (HPA-S, Anton Paar), sparging of volatile osmium tetroxide from the sample solution, and measurements using multicollector inductively coupled plasma mass spectrometry (MC-ICPMS). This methods significantly reduced the total procedural time compared to conventional Carius tube digestion followed by Os separation and purification using solvent extraction, microdistillation and N-TIMS analysis. The method yields Os concentration (28 ± 4 pg g(-1)) and (187)Os/(188)Os (1.62 ± 0.15) of commercially available crude oil reference material NIST 8505 (1 S.D., n = 6). The reference material NIST 8505 is homogeneous with respect to Os concentration at a test portion size of 0.2 g. Therefore, (187)Os/(188)Os composition and Os concentration of NIST 8505 can serve as a matrix-matched reference material for Os analysis. Data quality was assessed by repeated measurements of the USGS shale reference material SCo-1 (sample matrix similar to petroleum source rock) and the widely used Liquid Os Standard solution (LOsSt). The within-laboratory reproducibility of (187)Os/(188)Os for a 5 pg of LOsSt solution, analyzed with this method over a period of 12 months was ∼1.4% (1 S.D., n = 26), respectively.

  6. Dense Plasma Focus - From Alternative Fusion Source to Versatile High Energy Density Plasma Source for Plasma Nanotechnology

    Science.gov (United States)

    Rawat, R. S.

    2015-03-01

    The dense plasma focus (DPF), a coaxial plasma gun, utilizes pulsed high current electrical discharge to heat and compress the plasma to very high density and temperature with energy densities in the range of 1-10 × 1010 J/m3. The DPF device has always been in the company of several alternative magnetic fusion devices as it produces intense fusion neutrons. Several experiments conducted on many different DPF devices ranging over several order of storage energy have demonstrated that at higher storage energy the neutron production does not follow I4 scaling laws and deteriorate significantly raising concern about the device's capability and relevance for fusion energy. On the other hand, the high energy density pinch plasma in DPF device makes it a multiple radiation source of ions, electron, soft and hard x-rays, and neutrons, making it useful for several applications in many different fields such as lithography, radiography, imaging, activation analysis, radioisotopes production etc. Being a source of hot dense plasma, strong shockwave, intense energetic beams and radiation, etc, the DPF device, additionally, shows tremendous potential for applications in plasma nanoscience and plasma nanotechnology. In the present paper, the key features of plasma focus device are critically discussed to understand the novelties and opportunities that this device offers in processing and synthesis of nanophase materials using, both, the top-down and bottom-up approach. The results of recent key experimental investigations performed on (i) the processing and modification of bulk target substrates for phase change, surface reconstruction and nanostructurization, (ii) the nanostructurization of PLD grown magnetic thin films, and (iii) direct synthesis of nanostructured (nanowire, nanosheets and nanoflowers) materials using anode target material ablation, ablated plasma and background reactive gas based synthesis and purely gas phase synthesis of various different types of

  7. Dense Plasma Focus - From Alternative Fusion Source to Versatile High Energy Density Plasma Source for Plasma Nanotechnology

    International Nuclear Information System (INIS)

    Rawat, R S

    2015-01-01

    The dense plasma focus (DPF), a coaxial plasma gun, utilizes pulsed high current electrical discharge to heat and compress the plasma to very high density and temperature with energy densities in the range of 1-10 × 10 10 J/m 3 . The DPF device has always been in the company of several alternative magnetic fusion devices as it produces intense fusion neutrons. Several experiments conducted on many different DPF devices ranging over several order of storage energy have demonstrated that at higher storage energy the neutron production does not follow I 4 scaling laws and deteriorate significantly raising concern about the device's capability and relevance for fusion energy. On the other hand, the high energy density pinch plasma in DPF device makes it a multiple radiation source of ions, electron, soft and hard x-rays, and neutrons, making it useful for several applications in many different fields such as lithography, radiography, imaging, activation analysis, radioisotopes production etc. Being a source of hot dense plasma, strong shockwave, intense energetic beams and radiation, etc, the DPF device, additionally, shows tremendous potential for applications in plasma nanoscience and plasma nanotechnology. In the present paper, the key features of plasma focus device are critically discussed to understand the novelties and opportunities that this device offers in processing and synthesis of nanophase materials using, both, the top-down and bottom-up approach. The results of recent key experimental investigations performed on (i) the processing and modification of bulk target substrates for phase change, surface reconstruction and nanostructurization, (ii) the nanostructurization of PLD grown magnetic thin films, and (iii) direct synthesis of nanostructured (nanowire, nanosheets and nanoflowers) materials using anode target material ablation, ablated plasma and background reactive gas based synthesis and purely gas phase synthesis of various different types of

  8. Plasma sources for EUV lithography exposure tools

    International Nuclear Information System (INIS)

    Banine, Vadim; Moors, Roel

    2004-01-01

    The source is an integral part of an extreme ultraviolet lithography (EUVL) tool. Such a source, as well as the EUVL tool, has to fulfil extremely high demands both technical and cost oriented. The EUVL tool operates at a wavelength in the range 13-14 nm, which requires a major re-thinking of state-of-the-art lithography systems operating in the DUV range. The light production mechanism changes from conventional lamps and lasers to relatively high temperature emitting plasmas. The light transport, mainly refractive for DUV, should become reflective for EUV. The source specifications are derived from the customer requirements for the complete tool, which are: throughput, cost of ownership (CoO) and imaging quality. The EUVL system is considered as a follow up of the existing DUV based lithography technology and, while improving the feature resolution, it has to maintain high wafer throughput performance, which is driven by the overall CoO picture. This in turn puts quite high requirements on the collectable in-band power produced by an EUV source. Increased, due to improved feature resolution, critical dimension (CD) control requirements, together with reflective optics restrictions, necessitate pulse-to-pulse repeatability, spatial stability control and repetition rates, which are substantially better than those of current optical systems. All together the following aspects of the source specification will be addressed: the operating wavelength, the EUV power, the hot spot size, the collectable angle, the repetition rate, the pulse-to-pulse repeatability and the debris induced lifetime of components

  9. Plasma cholesteryl ester transfer protein mass and phospholipid transfer protein activity are associated with leptin in type 2 diabetes mellitus

    NARCIS (Netherlands)

    Dullaart, R. P. F.; de Vries, R.; Dallinga-Thie, G. M.; van Tol, A.; Sluiter, W. J.

    Adipose tissue contributes to plasma levels of lipid transfer proteins and is also the major source of plasma adipokines. We hypothesized that plasma cholesteryl ester transfer protein (CETP) mass, phospholipid transfer protein (PLTP) activity and cholesteryl ester transfer (CET, a measure of CETP

  10. Implosive Thermal Plasma Source for Energy Conversion

    Czech Academy of Sciences Publication Activity Database

    Šonský, Jiří; Tesař, Václav; Gruber, Jan; Mašláni, Alan

    2017-01-01

    Roč. 4, č. 1 (2017), s. 87-90 ISSN 2336-2626 Institutional support: RVO:61388998 ; RVO:61389021 Keywords : implosion * thermal plasma * detonation wave Subject RIV: BL - Plasma and Gas Discharge Physics; BL - Plasma and Gas Discharge Physics (UFP-V) OBOR OECD: Fluids and plasma physics (including surface physics); Fluids and plasma physics (including surface physics) (UFP-V) https://ppt.fel.cvut.cz/ppt2017.html#number1

  11. Measurement of performance parameters of plasma source for plasma opening switch on Qiangguang-Ⅰ generator

    International Nuclear Information System (INIS)

    Luo Weixi; Zeng Zhengzhong; Lei Tianshi; Wang Liangping; Hu Yixiang; Sun Tieping; Huang Tao

    2012-01-01

    The plasma source (cable guns) of the plasma opening switch (POS) on Qiangguang Ⅰ generator was chosen as the study object. The plasma source performance was investigated by using charge collectors. Experimental results show that the plasma ejection density is positively correlated with the structural parameter, the distance between gun core tip and muzzle plane, and the plasma ejection velocity is negatively correlated with the parameter. The increasing rate of plasma ejection density is less than that of drive current. As far as a plasma source with tens of cable plasma guns is concerned, the influence of single cable gun's discharge dispersancy on plasma uniformity is little. Analysis of uncertainty shows that the uncertainty of measurement can be reduced by increasing the number of experiments and averaging the results. The combined standard uncertainty of plasma ejection density is less than 10%. (authors)

  12. Ion sampling and transport in Inductively Coupled Plasma Mass Spectrometry

    Science.gov (United States)

    Farnsworth, Paul B.; Spencer, Ross L.

    2017-08-01

    Quantitative accuracy and high sensitivity in inductively coupled plasma mass spectrometry (ICP-MS) depend on consistent and efficient extraction and transport of analyte ions from an inductively coupled plasma to a mass analyzer, where they are sorted and detected. In this review we examine the fundamental physical processes that control ion sampling and transport in ICP-MS and compare the results of theory and computerized models with experimental efforts to characterize the flow of ions through plasma mass spectrometers' vacuum interfaces. We trace the flow of ions from their generation in the plasma, into the sampling cone, through the supersonic expansion in the first vacuum stage, through the skimmer, and into the ion optics that deliver the ions to the mass analyzer. At each stage we consider idealized behavior and departures from ideal behavior that affect the performance of ICP-MS as an analytical tool.

  13. Experimental facility for determining plasma characteristics in ion sources

    International Nuclear Information System (INIS)

    Abroyan, M.A.; Kagan, Yu.M.; Kolokolov, N.B.; Lavrov, B.P.

    A facility for optical and electrical measurements of the plasma parameters in the arc plasma ion sources is described. The potentialities of the system are demonstrated on the basis of the electron concentration, the electron energy distribution function, and the radial population distribution of the excited states of hydrogen atoms in the arc plasma of the duoplasmatron. (U.S.)

  14. Analysis of the tuning characteristics of microwave plasma source

    Energy Technology Data Exchange (ETDEWEB)

    Miotk, Robert, E-mail: rmiotk@imp.gda.pl; Jasiński, Mariusz [Centre for Plasma and Laser Engineering, The Szewalski Institute of Fluid-Flow Machinery, Polish Academy of Sciences, Fiszera 14, 80-231 Gdańsk (Poland); Mizeraczyk, Jerzy [Department of Marine Electronics, Gdynia Maritime University, Morska 81-87, 81-225 Gdynia (Poland)

    2016-04-15

    In this paper, we present an analysis of the tuning characteristics of waveguide-supplied metal-cylinder-based nozzleless microwave plasma source. This analysis has enabled to estimate the electron concentration n{sub e} and electron frequency collisions ν in the plasma generated in nitrogen and in a mixture of nitrogen and ethanol vapour. The parameters n{sub e} and ν are the basic quantities that characterize the plasma. The presented new plasma diagnostic method is particularly useful, when spectroscopic methods are useless. The presented plasma source is currently used in research of a hydrogen production from liquids.

  15. Analysis of the tuning characteristics of microwave plasma source

    International Nuclear Information System (INIS)

    Miotk, Robert; Jasiński, Mariusz; Mizeraczyk, Jerzy

    2016-01-01

    In this paper, we present an analysis of the tuning characteristics of waveguide-supplied metal-cylinder-based nozzleless microwave plasma source. This analysis has enabled to estimate the electron concentration n_e and electron frequency collisions ν in the plasma generated in nitrogen and in a mixture of nitrogen and ethanol vapour. The parameters n_e and ν are the basic quantities that characterize the plasma. The presented new plasma diagnostic method is particularly useful, when spectroscopic methods are useless. The presented plasma source is currently used in research of a hydrogen production from liquids.

  16. High-efficiency thermal ionization sources for mass spectrometry

    International Nuclear Information System (INIS)

    Olivares, Jose A.

    1996-01-01

    A version of the thermal ionization cavity (TIC) source developed specifically for use in mass spectrometry is presented. The performance of this ion source has been characterized extensively both with the use of an isotope separator and a quadrupole mass spectrometer. A detailed description of the TIC source for mass spectrometry is given along with the performance characteristics observed

  17. Cs+ ion source for secondary ion mass spectrometry

    International Nuclear Information System (INIS)

    Bentz, B.L.; Weiss, H.; Liebl, H.

    1981-12-01

    Various types of cesium ionization sources currently used in secondary ion mass spectrometry are briefly reviewed, followed by a description of the design and performance of a novel, thermal surface ionization Cs + source developed in this laboratory. The source was evaluated for secondary ion mass spectrometry applications using the COALA ion microprobe mass analyzer. (orig.)

  18. Plasma stream transport method (2) Use of charge exchange plasma source

    International Nuclear Information System (INIS)

    Tsuchimoto, T.

    1978-01-01

    The plasma stream transport method using a single plasma source has limitations for practical film deposition. Using a charge exchange phenomenon, a new plasma source is devised and tested by the plasma stream transport machine. Metals, silicon dioxide, and nitride films are deposited by this system. The mechanism of deposition under relatively high vacuum surrounding a silicon wafer is discussed as is the effect of radical atoms

  19. Materials science issues of plasma source ion implantation

    International Nuclear Information System (INIS)

    Nastasi, M.; Faehl, R.J.; Elmoursi, A.A.

    1996-01-01

    Ion beam processing, including ion implantation and ion beam assisted deposition (IBAD), are established surface modification techniques which have been used successfully to synthesize materials for a wide variety of tribological applications. In spite of the flexibility and promise of the technique, ion beam processing has been considered too expensive for mass production applications. However, an emerging technology, Plasma Source Ion Implantation (PSII), has the potential of overcoming these limitations to become an economically viable tool for mass industrial applications. In PSII, targets are placed directly in a plasma and then pulsed-biased to produce a non-line-of-sight process for intricate target geometries without complicated fixturing. If the bias is a relatively high negative potential (20--100 kV) ion implantation will result. At lower voltages (50--1,200 V), deposition occurs. Potential applications for PSII are in low-value-added products such as tools used in manufacturing, orthopedic devices, and the production of wear coatings for hard disk media. This paper will focus on the technology and materials science associated with PSII

  20. The requirements for low-temperature plasma ionization support miniaturization of the ion source.

    Science.gov (United States)

    Kiontke, Andreas; Holzer, Frank; Belder, Detlev; Birkemeyer, Claudia

    2018-06-01

    Ambient ionization mass spectrometry (AI-MS), the ionization of samples under ambient conditions, enables fast and simple analysis of samples without or with little sample preparation. Due to their simple construction and low resource consumption, plasma-based ionization methods in particular are considered ideal for use in mobile analytical devices. However, systematic investigations that have attempted to identify the optimal configuration of a plasma source to achieve the sensitive detection of target molecules are still rare. We therefore used a low-temperature plasma ionization (LTPI) source based on dielectric barrier discharge with helium employed as the process gas to identify the factors that most strongly influence the signal intensity in the mass spectrometry of species formed by plasma ionization. In this study, we investigated several construction-related parameters of the plasma source and found that a low wall thickness of the dielectric, a small outlet spacing, and a short distance between the plasma source and the MS inlet are needed to achieve optimal signal intensity with a process-gas flow rate of as little as 10 mL/min. In conclusion, this type of ion source is especially well suited for downscaling, which is usually required in mobile devices. Our results provide valuable insights into the LTPI mechanism; they reveal the potential to further improve its implementation and standardization for mobile mass spectrometry as well as our understanding of the requirements and selectivity of this technique. Graphical abstract Optimized parameters of a dielectric barrier discharge plasma for ionization in mass spectrometry. The electrode size, shape, and arrangement, the thickness of the dielectric, and distances between the plasma source, sample, and MS inlet are marked in red. The process gas (helium) flow is shown in black.

  1. Matrix effects in inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Chen, Xiaoshan.

    1995-01-01

    The inductively coupled plasma is an electrodeless discharge in a gas (usually Ar) at atmospheric pressure. Radio frequency energy generated by a RF power source is inductively coupled to the plasma gas through a water cooled load coil. In ICP-MS the open-quotes Fasselclose quotes TAX quartz torch commonly used in emission is mounted horizontally. The sample aerosol is introduced into the central flow, where the gas kinetic temperature is about 5000 K. The aerosol is vaporized, atomized, excited and ionized in the plasma, and the ions are subsequently extracted through two metal apertures (sampler and skimmer) into the mass spectrometer. In ICP-MS, the matrix effects, or non-spectroscopic interferences, can be defined as the type of interferences caused by dissolved concomitant salt ions in the solution. Matrix effects can be divided into two categories: (1) signal drift due to the deposition of solids on the sampling apertures; and/or (2) signal suppression or enhancement by the presence of the dissolved salts. The first category is now reasonably understood. The dissolved salts, especially refractory oxides, tend to deposit on the cool tip of the sampling cone. The clogging of the orifices reduces the ion flow into the ICP-MS, lowers the pressure in the first stage of ICP-MS, and enhances the level of metal oxide ions. Because the extent of the clogging increases with the time, the signal drifts down. Even at the very early stage of the development of ICP-MS, matrix effects had been observed. Houk et al. found out that the ICP-MS was not tolerant to solutions containing significant amounts of dissolved solids

  2. Study of electron current extraction from a radio frequency plasma cathode designed as a neutralizer for ion source applications

    Energy Technology Data Exchange (ETDEWEB)

    Jahanbakhsh, Sina, E-mail: sinajahanbakhsh@gmail.com; Satir, Mert; Celik, Murat [Department of Mechanical Engineering, Bogazici University, Istanbul 34342 (Turkey)

    2016-02-15

    Plasma cathodes are insert free devices that are developed to be employed as electron sources in electric propulsion and ion source applications as practical alternatives to more commonly used hollow cathodes. Inductively coupled plasma cathodes, or Radio Frequency (RF) plasma cathodes, are introduced in recent years. Because of its compact geometry, and simple and efficient plasma generation, RF plasma source is considered to be suitable for plasma cathode applications. In this study, numerous RF plasma cathodes have been designed and manufactured. Experimental measurements have been conducted to study the effects of geometric and operational parameters. Experimental results of this study show that the plasma generation and electron extraction characteristics of the RF plasma cathode device strongly depend on the geometric parameters such as chamber diameter, chamber length, orifice diameter, orifice length, as well as the operational parameters such as RF power and gas mass flow rate.

  3. Plasma Waves Associated with Mass-Loaded Comets

    Science.gov (United States)

    Tsurutani, Bruce; Glassmeier, Karl-Heinz

    2015-01-01

    Plasma waves and instabilities are integrally involved with the plasma "pickup" process and the mass loading of the solar wind (thus the formation of ion tails and the magnetic tails). Anisotropic plasmas generated by solar wind-comet interactions (the bow shock, magnetic field pileup) cause the generation of plasma waves which in turn "smooth out" these discontinuities. The plasma waves evolve and form plasma turbulence. Comets are perhaps the best "laboratories" to study waves and turbulence because over time (and distance) one can identify the waves and their evolution. We will argue that comets in some ways are better laboratories than magnetospheres, interplanetary space and fusion devices to study nonlinear waves and their evolution.

  4. Capillary plasma jet: A low volume plasma source for life science applications

    Energy Technology Data Exchange (ETDEWEB)

    Topala, I., E-mail: ionut.topala@uaic.ro, E-mail: tmnagat@ipc.shizuoka.ac.jp [Alexandru Ioan Cuza University of Iasi, Faculty of Physics, Iasi Plasma Advanced Research Center (IPARC), Bd. Carol I No. 11, Iasi 700506 (Romania); Nagatsu, M., E-mail: ionut.topala@uaic.ro, E-mail: tmnagat@ipc.shizuoka.ac.jp [Graduate School of Science and Technology, Shizuoka University, 3-5-1 Johoku, Naka-ku, Hamamatsu 432-8561 (Japan)

    2015-02-02

    In this letter, we present results from multispectroscopic analysis of protein films, after exposure to a peculiar plasma source, i.e., the capillary plasma jet. This plasma source is able to generate very small pulsed plasma volumes, in kilohertz range, with characteristic dimensions smaller than 1 mm. This leads to specific microscale generation and transport of all plasma species. Plasma diagnosis was realized using general electrical and optical methods. Depending on power level and exposure duration, this miniature plasma jet can induce controllable modifications to soft matter targets. Detailed discussions on protein film oxidation and chemical etching are supported by results from absorption, X-ray photoelectron spectroscopy, and microscopy techniques. Further exploitation of principles presented here may consolidate research interests involving plasmas in biotechnologies and plasma medicine, especially in patterning technologies, modified biomolecule arrays, and local chemical functionalization.

  5. Capillary plasma jet: A low volume plasma source for life science applications

    Science.gov (United States)

    Topala, I.; Nagatsu, M.

    2015-02-01

    In this letter, we present results from multispectroscopic analysis of protein films, after exposure to a peculiar plasma source, i.e., the capillary plasma jet. This plasma source is able to generate very small pulsed plasma volumes, in kilohertz range, with characteristic dimensions smaller than 1 mm. This leads to specific microscale generation and transport of all plasma species. Plasma diagnosis was realized using general electrical and optical methods. Depending on power level and exposure duration, this miniature plasma jet can induce controllable modifications to soft matter targets. Detailed discussions on protein film oxidation and chemical etching are supported by results from absorption, X-ray photoelectron spectroscopy, and microscopy techniques. Further exploitation of principles presented here may consolidate research interests involving plasmas in biotechnologies and plasma medicine, especially in patterning technologies, modified biomolecule arrays, and local chemical functionalization.

  6. Determination of iodine at ppt level in a nitric acid medium by inductively coupled plasma sector field mass spectrometry: influence of the chemical forms; Etude de la determination de traces d'iode en solution par spectrometrie de masse a secteur magnetique utilisant un plasma a couplage inductif comme source d'ionisation: influence de la forme chimique

    Energy Technology Data Exchange (ETDEWEB)

    Langlois, B

    2001-07-01

    Inductively Coupled Plasma Sector Field Mass Spectrometry (ICP/SFMS) was used to determine several chemical forms of iodine, at ppt level, in a nitric acid media. Ascorbic acid was added as a reducing agent in order to maintain iodine as iodide. In a preliminary approach, the influence of the chemical form was studied by comparing inorganic iodine (NaI) and organic iodine (CH3I). Different signal responses were observed. With a conventional sample introduction system, sensitivities obtained for iodo-methane could differ by a factor of 5. This was not caused by a problem of atomization or by a change in the ionization efficiency of the iodo-compound into the plasma. The low volatilization temperature of iodo-methane (315.5 K) seemed to be the main explanation of this phenomena. Actually, nebulization resulted in the volatilization of a 2% nitric acid solution containing iodo-methane. As a result, the transport efficiency of iodo-methane between the nebulizer and the torch was approaching 100%. A Direct Injection High Efficiency Nebulizer (DIHEN) allowed us to minimize the behavior difference between the two iodine species, but the sensitivity ratio was inverted and still differed by 20 - 40%. Moreover, the association of a guard electrode and the direct injection system was studied in order to apply these equipments to the determination of iodine. This association allowed us to improve the sensitivity by a factor of 10 and to minimize memory effects, when compared with a conventional system. Further studies indicated that signal responses obtained with different iodine-containing species, except for iodo-methane, were found to be similar. (author)

  7. Inductively-coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Dale, L.

    1990-01-01

    The instrument in operation at the Lucas Heights Research Laboratories is a VG Plasma-quad PQ 2. A schematic diagram of the instrument components is presented along with its applicability to various fields of research and its perceived limitations. Apart from its high sensitivity the capability for rapid multi-element analysis in one of its major advantages over other instrumental method analysis. The necessity to present the sample in the form of a solution is probably its major drawback. 4 tabs, 7 figs

  8. Shunting arc plasma source for pure carbon ion beam

    Energy Technology Data Exchange (ETDEWEB)

    Koguchi, H.; Sakakita, H.; Kiyama, S.; Shimada, T.; Sato, Y.; Hirano, Y. [Energy Technology Research Institute, National Institute of Advanced Industrial Science and Technology (AIST), 1-1-1 Umezono, Tsukuba, Ibaraki 305-8568 (Japan)

    2012-02-15

    A plasma source is developed using a coaxial shunting arc plasma gun to extract a pure carbon ion beam. The pure carbon ion beam is a new type of deposition system for diamond and other carbon materials. Our plasma device generates pure carbon plasma from solid-state carbon material without using a hydrocarbon gas such as methane gas, and the plasma does not contain any hydrogen. The ion saturation current of the discharge measured by a double probe is about 0.2 mA/mm{sup 2} at the peak of the pulse.

  9. Shunting arc plasma source for pure carbon ion beam.

    Science.gov (United States)

    Koguchi, H; Sakakita, H; Kiyama, S; Shimada, T; Sato, Y; Hirano, Y

    2012-02-01

    A plasma source is developed using a coaxial shunting arc plasma gun to extract a pure carbon ion beam. The pure carbon ion beam is a new type of deposition system for diamond and other carbon materials. Our plasma device generates pure carbon plasma from solid-state carbon material without using a hydrocarbon gas such as methane gas, and the plasma does not contain any hydrogen. The ion saturation current of the discharge measured by a double probe is about 0.2 mA∕mm(2) at the peak of the pulse.

  10. Plasma control for efficient extreme ultra-violet source

    International Nuclear Information System (INIS)

    Takahashi, Kensaku; Nakajima, Mitsuo; Kawamura, Tohru; Shiho, Makoto; Hotta, Eiki; Horioka, Kazuhiko

    2008-01-01

    To generate a high efficiency extreme-ultraviolet (EUV) source, effects of plasma shape for controlling radiative plasmas based on xenon capillary discharge are experimentally investigated. The radiation characteristics observed via tapered capillary discharge are compared with those of straight one. From the comparison, the long emission period and different plasma behaviors of tapered capillary discharge are confirmed. This means that control of the plasma geometry is effective for prolonging the EUV emission period. This result also indicates that the plasma shape control seems to have a potential for enhancing the conversion efficiency. (author)

  11. Ferroelectric plasma source for heavy ion beam space charge neutralization

    International Nuclear Information System (INIS)

    Efthimion, Philip C.; Gilson, Erik P.; Davidson, Ronald C.; Grisham, Larry; Grant Logan, B.; Seidl, Peter A.; Waldron, William; Yu, Simon S.

    2007-01-01

    Plasmas are a source of unbound electrons for charge neutralizing intense heavy ion beams to allow them to focus to a small spot size and compress their axial pulse length. The plasma source should be able to operate at low neutral pressures and without strong externally applied electric or magnetic fields. To produce 1 m-long plasma columns, sources based upon ferroelectric ceramics with large dielectric coefficients are being developed. The sources utilize the ferroelectric ceramic BaTiO 3 to form metal plasma. The drift tube inner surface of the Neutralized Drift Compression Experiment (NDCX) will be covered with ceramic material, and high voltage (∼7 kV) will be applied between the drift tube and the front surface of the ceramics. A prototype ferroelectric source, 20 cm in length, has produced plasma densities of 5x10 11 cm -3 . It was integrated into the Neutralized Transport Experiment (NTX), and successfully charge neutralized the K + ion beam. A 1 m-long source comprised of five 20-cm-long sources has been tested. Simply connecting the five sources in parallel to a single pulse forming network power supply yielded non-uniform performance due to the time-dependent nature of the load that each of the five plasma sources experiences. Other circuit combinations have been considered, including powering each source by its own supply. The 1-m-long source has now been successfully characterized, producing relatively uniform plasma over the 1 m length of the source in the mid-10 10 cm -3 density range. This source will be integrated into the NDCX device for charge neutralization and beam compression experiments

  12. Pacific Islands Mass Communications; Selected Information Sources.

    Science.gov (United States)

    Richstad, Jim; McMillan, Michael

    1977-01-01

    Presents a bibliography of materials on such area of mass communications in the Pacific Islands as broadcasting, radio and television, cinema, communication research, mass media in education, Honululu Media Council, newspapers and newspapermen, and printing and satellite communication. (JEG)

  13. Counter-facing plasma guns for efficient extreme ultra-violet plasma light source

    Science.gov (United States)

    Kuroda, Yusuke; Yamamoto, Akiko; Kuwabara, Hajime; Nakajima, Mitsuo; Kawamura, Tohru; Horioka, Kazuhiko

    2013-11-01

    A plasma focus system composed of a pair of counter-facing coaxial guns was proposed as a long-pulse and/or repetitive high energy density plasma source. We applied Li as the source of plasma for improvement of the conversion efficiency, the spectral purity, and the repetition capability. For operation of the system with ideal counter-facing plasma focus mode, we changed the system from simple coaxial geometry to a multi-channel configuration. We applied a laser trigger to make synchronous multi-channel discharges with low jitter. The results indicated that the configuration is promising to make a high energy density plasma with high spectral efficiency.

  14. The coupling of capillary electrophoresis-inductively coupled plasma mass spectrometer as a speciation instrument for actinides at trace level; Le couplage electrophorese capillaire-spectrometre de masse a source plasma en tant qu'instrument de speciation des actinides a l'etat de traces

    Energy Technology Data Exchange (ETDEWEB)

    Delorme, A

    2004-07-01

    An interface between the separation technique (capillary electrophoresis) and the analytical technique (Inductively Coupled Plasma - Mass Spectrometer) was developed. In that sense, bibliographic and parametric studies allowed to define necessary conditions for the good working of both techniques. The results obtained led to the realisation of an interface capillary electrophoresis / ICP-MS (CE / ICP-MS). This one was experimentally validated on classical separations (alkalis / earth-alkalis and lanthanides) and the detection limit of the analytical system was determined equal to 4 x 10{sup -11} mol.L{sup -1} for plutonium. This result exhibits a gain in detection limit of a factor higher than 10{sup 4} compared to the capillary electrophoresis in standard detection (UV). The studies were made in order to check the capacity of the CE / ICP-MS coupling as a speciation instrument for actinides at trace level and to define the associated analytical procedures. The coupling turned out to be a suited instrument for the determination of absolute electrophoretic mobilities at infinite dilution (physico-chemical property which allows to predict the migration time of an ion under an electrical field in a given electrolyte), for the determination of thermodynamic constants and for the separation of different actinide oxidation states in solution. (author)

  15. RF plasma source for heavy ion beam charge neutralization

    International Nuclear Information System (INIS)

    Efthimion, Philip C.; Gilson, Erik; Grisham, Larry; Davidson, Ronald C.; Yu, Simon S.; Logan, B. Grant

    2003-01-01

    Highly ionized plasmas are being used as a medium for charge neutralizing heavy ion beams in order to focus the ion beam to a small spot size. A radio frequency (RF) plasma source has been built at the Princeton Plasma Physics Laboratory (PPPL) in support of the joint Neutralized Transport Experiment (NTX) at the Lawrence Berkeley National Laboratory (LBNL) to study ion beam neutralization with plasma. The goal is to operate the source at pressures ∼ 10 -5 Torr at full ionization. The initial operation of the source has been at pressures of 10 -4 -10 -1 Torr and electron densities in the range of 10 8 -10 11 cm -3 . Recently, pulsed operation of the source has enabled operation at pressures in the 10 -6 Torr range with densities of 10 11 cm -3 . Near 100% ionization has been achieved. The source has been integrated with the NTX facility and experiments have begun

  16. High efficiency nebulization for helium inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Jorabchi, Kaveh; McCormick, Ryan; Levine, Jonathan A.; Liu Huiying; Nam, S.-H.; Montaser, Akbar

    2006-01-01

    A pneumatically-driven, high efficiency nebulizer is explored for helium inductively coupled plasma mass spectrometry. The aerosol characteristics and analyte transport efficiencies of the high efficiency nebulizer for nebulization with helium are measured and compared to the results obtained with argon. Analytical performance indices of the helium inductively coupled plasma mass spectrometry are evaluated in terms of detection limits and precision. The helium inductively coupled plasma mass spectrometry detection limits obtained with the high efficiency nebulizer at 200 μL/min are higher than those achieved with the ultrasonic nebulizer consuming 2 mL/min solution, however, precision is generally better with high efficiency nebulizer (1-4% vs. 3-8% with ultrasonic nebulizer). Detection limits with the high efficiency nebulizer at 200 μL/min solution uptake rate approach those using ultrasonic nebulizer upon efficient desolvation with a heated spray chamber followed by a Peltier-cooled multipass condenser

  17. Handheld low-temperature plasma probe for portable "point-and-shoot" ambient ionization mass spectrometry.

    Science.gov (United States)

    Wiley, Joshua S; Shelley, Jacob T; Cooks, R Graham

    2013-07-16

    We describe a handheld, wireless low-temperature plasma (LTP) ambient ionization source and its performance on a benchtop and a miniature mass spectrometer. The source, which is inexpensive to build and operate, is battery-powered and utilizes miniature helium cylinders or air as the discharge gas. Comparison of a conventional, large-scale LTP source against the handheld LTP source, which uses less helium and power than the large-scale version, revealed that the handheld source had similar or slightly better analytical performance. Another advantage of the handheld LTP source is the ability to quickly interrogate a gaseous, liquid, or solid sample without requiring any setup time. A small, 7.4-V Li-polymer battery is able to sustain plasma for 2 h continuously, while the miniature helium cylinder supplies gas flow for approximately 8 continuous hours. Long-distance ion transfer was achieved for distances up to 1 m.

  18. High electronegativity multi-dipolar electron cyclotron resonance plasma source for etching by negative ions

    DEFF Research Database (Denmark)

    Stamate, Eugen; Draghici, M.

    2012-01-01

    A large area plasma source based on 12 multi-dipolar ECR plasma cells arranged in a 3 x 4 matrix configuration was built and optimized for silicon etching by negative ions. The density ratio of negative ions to electrons has exceeded 300 in Ar/SF6 gas mixture when a magnetic filter was used...... to reduce the electron temperature to about 1.2 eV. Mass spectrometry and electrostatic probe were used for plasma diagnostics. The new source is free of density jumps and instabilities and shows a very good stability for plasma potential, and the dominant negative ion species is F-. The magnetic field...... in plasma volume is negligible and there is no contamination by filaments. The etching rate by negative ions measured in Ar/SF6/O-2 mixtures was almost similar with that by positive ions reaching 700 nm/min. (C) 2012 American Institute of Physics...

  19. Ferroelectric Plasma Source for Heavy Ion Beam Charge Neutralization

    CERN Document Server

    Efthimion, Philip; Gilson, Erik P; Grisham, Larry; Logan, B G; Waldron, William; Yu, Simon

    2005-01-01

    Plasmas are employed as a medium for charge neutralizing heavy ion beams to allow them to focus to a small spot size. Calculations suggest that plasma at a density of 1-100 times the ion beam density and at a length ~ 0.1-1 m would be suitable. To produce 1 meter plasma, large-volume plasma sources based upon ferroelectric ceramics are being considered. These sources have the advantage of being able to increase the length of the plasma and operate at low neutral pressures. The source will utilize the ferroelectric ceramic BaTiO3 to form metal plasma. The drift tube inner surface of the Neutralized Drift Compression Experiment (NDCX) will be covered with ceramic. High voltage (~ 1-5 kV) is applied between the drift tube and the front surface of the ceramic by placing a wire grid on the front surface. A prototype ferroelectric source 20 cm long produced plasma densities ~ 5x1011 cm-3. The source was integrated into the experiment and successfully charge neutralized the K ion beam. Presently, the 1 meter source ...

  20. Modeling of low pressure plasma sources for microelectronics fabrication

    International Nuclear Information System (INIS)

    Agarwal, Ankur; Bera, Kallol; Kenney, Jason; Rauf, Shahid; Likhanskii, Alexandre

    2017-01-01

    Chemically reactive plasmas operating in the 1 mTorr–10 Torr pressure range are widely used for thin film processing in the semiconductor industry. Plasma modeling has come to play an important role in the design of these plasma processing systems. A number of 3-dimensional (3D) fluid and hybrid plasma modeling examples are used to illustrate the role of computational investigations in design of plasma processing hardware for applications such as ion implantation, deposition, and etching. A model for a rectangular inductively coupled plasma (ICP) source is described, which is employed as an ion source for ion implantation. It is shown that gas pressure strongly influences ion flux uniformity, which is determined by the balance between the location of plasma production and diffusion. The effect of chamber dimensions on plasma uniformity in a rectangular capacitively coupled plasma (CCP) is examined using an electromagnetic plasma model. Due to high pressure and small gap in this system, plasma uniformity is found to be primarily determined by the electric field profile in the sheath/pre-sheath region. A 3D model is utilized to investigate the confinement properties of a mesh in a cylindrical CCP. Results highlight the role of hole topology and size on the formation of localized hot-spots. A 3D electromagnetic plasma model for a cylindrical ICP is used to study inductive versus capacitive power coupling and how placement of ground return wires influences it. Finally, a 3D hybrid plasma model for an electron beam generated magnetized plasma is used to understand the role of reactor geometry on plasma uniformity in the presence of E  ×  B drift. (paper)

  1. Modeling of low pressure plasma sources for microelectronics fabrication

    Science.gov (United States)

    Agarwal, Ankur; Bera, Kallol; Kenney, Jason; Likhanskii, Alexandre; Rauf, Shahid

    2017-10-01

    Chemically reactive plasmas operating in the 1 mTorr-10 Torr pressure range are widely used for thin film processing in the semiconductor industry. Plasma modeling has come to play an important role in the design of these plasma processing systems. A number of 3-dimensional (3D) fluid and hybrid plasma modeling examples are used to illustrate the role of computational investigations in design of plasma processing hardware for applications such as ion implantation, deposition, and etching. A model for a rectangular inductively coupled plasma (ICP) source is described, which is employed as an ion source for ion implantation. It is shown that gas pressure strongly influences ion flux uniformity, which is determined by the balance between the location of plasma production and diffusion. The effect of chamber dimensions on plasma uniformity in a rectangular capacitively coupled plasma (CCP) is examined using an electromagnetic plasma model. Due to high pressure and small gap in this system, plasma uniformity is found to be primarily determined by the electric field profile in the sheath/pre-sheath region. A 3D model is utilized to investigate the confinement properties of a mesh in a cylindrical CCP. Results highlight the role of hole topology and size on the formation of localized hot-spots. A 3D electromagnetic plasma model for a cylindrical ICP is used to study inductive versus capacitive power coupling and how placement of ground return wires influences it. Finally, a 3D hybrid plasma model for an electron beam generated magnetized plasma is used to understand the role of reactor geometry on plasma uniformity in the presence of E  ×  B drift.

  2. Fish protein hydrolysate elevates plasma bile acids and reduces visceral adipose tissue mass in rats

    DEFF Research Database (Denmark)

    Liaset, Bjørn; Madsen, Lise; Hao, Qin

    2009-01-01

    levels relative to rats fed soy protein or casein. Concomitantly, the saithe FPH fed rats had reduced liver lipids and fasting plasma TAG levels. Furthermore, visceral adipose tissue mass was reduced and expression of genes involved in fatty acid oxidation and energy expenditure was induced in perirenal....../retroperitoneal adipose tissues of rats fed saithe FPH. Our results provide the first evidence that dietary protein sources with different amino acid compositions can modulate the level of plasma bile acids and our data suggest potential novel mechanisms by which dietary protein sources can affect energy metabolism....

  3. Plasma focus as a pulsed power source

    International Nuclear Information System (INIS)

    Sahlin, H.; McFarland, G.; Barlett, R.; Gullickson, R.

    1975-01-01

    The plasma focus is a remarkable natural phenomena that achieves significant space-time compression of both particle and field energy. Depending on the mode of operation, about 20 percent of the bank energy can be concentrated into the kinetic energy of a thin, dense, cylindrically convergent gas shell, or into a small-diameter, high-ν/γ relativistic electron burst and oppositely directed ion burst. The kinetic energy of the fast ions and electrons can exceed the applied voltage by a factor of greater than 100. The different modes of energy concentration by the plasma focus are presented and discussed both in terms of their role in the direct yield of the focus and for the case of a plasma focus supplemented by various fusionable targets

  4. Spectroscopic measurements of anode plasma with cryogenic pulsed ion sources

    International Nuclear Information System (INIS)

    Yoneda, H.; Urata, T.; Ohbayashi, K.; Kim, Y.; Horioka, K.; Kasuya, K.

    1987-01-01

    In ion beam diodes, electromagnetic wave is coupled to ion beam. Ion is extracted from anode plasma, which is produced early in the power pulse. However, exact mechanism of anode plasma production, expansion and ion extraction process is unknown. In particularly, anode plasma expansion is seemed to be one of the reasons of rapid impedance collapse of the diode, which is serious problem in high power experiments. Some experimental results showed that anode plasma expansion velocity was about 5 times larger than that inferred from simple thermal velocity. Several explanations for these results were proposed; for example, electron collisionarity in anode plasma, fast neutral gas particle, diamagnetism. To solve this question, it is necessary to measure the characteristic of anode plasma with space and time resolution. The authors made spectroscopic measurements to investigate variety of electron temperature, electron density, expansion velocity of anode plasma with various ion sources

  5. Studies of electron cyclotron resonance ion source plasma physics

    International Nuclear Information System (INIS)

    Tarvainen, O.

    2005-01-01

    This thesis consists of an introduction to the plasma physics of electron cyclotron resonance ion sources (ECRIS) and a review of the results obtained by the author and co-workers including discussion of related work by others. The thesis begins with a theoretical discussion dealing with plasma physics relevant for the production of highly charged ions in ECR ion source plasmas. This is followed by an overview of different techniques, such as gas mixing and double frequency heating, that can be used to improve the performance of this type of ion source. The experimental part of the work consists of studies related to ECRIS plasma physics. The effect of the gas mixing technique on the production efficiency of different ion beams was studied with both gaseous and solid materials. It was observed that gas mixing improves the confinement of the heavier element while the confinement of the lighter element is reduced. When the effect of gas mixing on MIVOC-plasmas was studied with several mixing gases it was observed that applying this technique can reduce the inevitable carbon contamination by a significant factor. In order to understand the different plasma processes taking place in ECRIS plasmas, a series of plasma potential and emittance measurements was carried out. An instrument, which can be used to measure the plasma potential in a single measurement without disturbing the plasma, was developed for this work. Studying the plasma potential of ECR ion sources is important not only because it helps to understand different plasma processes, but also because the information can be used as an input parameter for beam transport simulations and ion source extraction design. The experiments performed have revealed clear dependencies of the plasma potential on certain source parameters such as the amount of carbon contamination accumulated on the walls of the plasma chamber during a MIVOC-run. It was also observed that gas mixing affects not only the production efficiency

  6. Long plasma source for heavy ion beam charge neutralization

    International Nuclear Information System (INIS)

    Efthimion, Philip C.; Gilson, Erik P.; Grisham, Larry; Davidson, Ronald C.; Grant Logan, Larry B.; Seidl, Peter A.; Waldron, William

    2009-01-01

    Plasmas are a source of unbound electrons for charge neutralizing intense heavy ion beams to focus them to a small spot size and compress their axial length. The plasma source should operate at low neutral pressures and without strong externally applied fields. To produce long plasma columns, sources based upon ferroelectric ceramics with large dielectric coefficients have been developed. The source utilizes the ferroelectric ceramic BaTiO 3 to form metal plasma. The drift tube inner surface of the Neutralized Drift Compression Experiment (NDCX) is covered with ceramic material. High voltage (∼8 kV) is applied between the drift tube and the front surface of the ceramics. A BaTiO 3 source comprised of five 20-cm-long sources has been tested and characterized, producing relatively uniform plasma in the 5x10 10 cm -3 density range. The source was integrated into the NDCX device for charge neutralization and beam compression experiments, and yielded current compression ratios ∼120. Present research is developing multi-meter-long and higher density sources to support beam compression experiments for high-energy-density physics applications.

  7. Electron Beam Diagnosis and Dynamics using DIADYN Plasma Source

    International Nuclear Information System (INIS)

    Toader, D.; Craciun, G.; Manaila, E.; Oproiu, C.; Marghitu, S.

    2009-01-01

    This paper is presenting results obtained with the DIADYN installation after replacing its vacuum electron source (VES L V) with a plasma electron source (PES L V). DIADYN is a low energy laboratory equipment operating with 10 to 50 keV electron beams and designed to help realize non-destructive diagnosis and dynamics for low energy electron beams but also to be used in future material irradiations. The results presented here regard the beam diagnosis and dynamics made with beams obtained from the newly replaced plasma source. We discuss both results obtained in experimental dynamics and dynamics calculation results for electron beams extracted from the SEP L V source.

  8. Negative ion surface plasma source development for plasma trap injectors in Novosibirsk

    International Nuclear Information System (INIS)

    Bel'chenko, Yu.I.; Dimov, G.I.; Dudnikov, V.G.; Kupriyanov, A.S.

    1989-01-01

    Work on high-current ion sources carried out at the Novosibirsk Institute of Nuclear Physics (INP) is presented. The INP investigations on ''pure plasma'' planotron and ''pure surface'' secondary emission systems of H - generation, which preceded the surface-plasma concept developed in Novosibirsk, are described. The physical basis of the surface-plasma method of negative-ion production is considered. The versions and operating characteristics of different surface-plasma sources including the multi-ampere (approx-gt 10A) source are discussed. Research on efficient large-area (∼10 2 cm 2 ) negative ion surface-plasma emitters is described. The INP long-pulse multiaperture surface- plasma generators, with a current of about 1A, are described. 38 refs., 17 figs

  9. Characterization of an electrothermal plasma source for fusion transient simulations

    Science.gov (United States)

    Gebhart, T. E.; Baylor, L. R.; Rapp, J.; Winfrey, A. L.

    2018-01-01

    The realization of fusion energy requires materials that can withstand high heat and particle fluxes at the plasma material interface. In this work, an electrothermal (ET) plasma source has been designed as a transient heat flux source for a linear plasma material interaction device. An ET plasma source operates in the ablative arc regime driven by a DC capacitive discharge. The current channel width is defined by the 4 mm bore of a boron nitride liner. At large plasma currents, the arc impacts the liner wall, leading to high particle and heat fluxes to the liner material, which subsequently ablates and ionizes. This results in a high density plasma with a large unidirectional bulk flow out of the source exit. The pulse length for the ET source has been optimized using a pulse forming network to have durations of 1 and 2 ms. The peak currents and maximum source energies seen in this system are 1.9 kA and 1.2 kJ for the 2 ms pulse and 3.2 kA and 2.1 kJ for the 1 ms pulse, respectively. This work is a proof of the principal project to show that an ET source produces electron densities and heat fluxes comparable to those anticipated in transient events in large future magnetic confinement fusion devices. Heat flux, plasma temperature, and plasma density were determined for each shot using infrared imaging and optical spectroscopy techniques. This paper will discuss the assumptions, methods, and results of the experiments.

  10. A Penning-assisted subkilovolt coaxial plasma source

    International Nuclear Information System (INIS)

    Wang Zhehui; Beinke, Paul D.; Barnes, Cris W.; Martin, Michael W.; Mignardot, Edward; Wurden, Glen A.; Hsu, Scott C.; Intrator, Thomas P.; Munson, Carter P.

    2005-01-01

    A Penning-assisted 20 MW coaxial plasma source (plasma gun), which can achieve breakdown at sub-kV voltages, is described. The minimum breakdown voltage is about 400 V, significantly lower than previously reported values of 1-5 kV. The Penning region for electrons is created using a permanent magnet assembly, which is mounted to the inside of the cathode of the coaxial plasma source. A theoretical model for the breakdown is given. A 900 V 0.5 F capacitor bank supplies energy for gas breakdown and plasma sustainment from 4 to 6 ms duration. Typical peak gun current is about 100 kA and gun voltage between anode and cathode after breakdown is about 200 V. A circuit model is used to understand the current-voltage characteristics of the coaxial gun plasma. Energy deposited into the plasma accounts for about 60% of the total capacitor bank energy. This plasma source is uniquely suitable for studying multi-MW multi-ms plasmas with sub-MJ capacitor bank energy

  11. Simultaneous electrothermal vaporization and nebulizer sample introduction system for inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Arnquist, Isaac J.; Kreschollek, Thomas E.; Holcombe, James A.

    2011-01-01

    The novel analytical application of the combination of an inline electrothermal vaporization (ETV) and nebulization source for inductively coupled plasma mass spectrometry (ICP-MS) has been studied. Wet plasma conditions are sustained during ETV introduction by 200 mL/min gas flow through the nebulizer, which is merged with the ETV transport line at the torch. The use of a wet plasma with ETV introduction avoided the need to change power settings and torch positions that normally accompany a change from wet to dry plasma operating conditions. This inline-ETV source is shown to have good detection limits for a variety of elements in both HNO 3 and HCl matrices. Using the inline-ETV source, improved limits of detection (LOD) were obtained for elements typically suppressed by polyatomic interferences using a nebulizer. Specifically, improved LODs for 51 V and 53 Cr suffering from Cl interferences ( 51 ClO + and 53 ClO + respectively) in a 1% HCl matrix were obtained using the inline-ETV source. LODs were improved by factors of 65 and 22 for 51 V and 53 Cr, respectively, using the inline-ETV source compared to a conventional concentric glass nebulizer. For elements without polyatomic interferences, LODs from the inline-ETV were comparable to conventional dry plasma ETV-ICP time-of-flight mass spectrometry results. Lastly, the inline-ETV source offers a simple means of changing from nebulizer introduction to inline-ETV introduction without extinguishing the plasma. This permits, for example, the use of the time-resolved ETV-ICP-MS signals to distinguish between an analyte ion and polyatomic isobar.

  12. Fullerene-rare gas mixed plasmas in an electron cyclotron resonance ion source

    Energy Technology Data Exchange (ETDEWEB)

    Asaji, T., E-mail: asaji@oshima-k.ac.jp; Ohba, T. [Oshima National College of Maritime Technology, 1091-1 Komatsu, Suo-oshima, Oshima, Yamaguchi 742-2193 (Japan); Uchida, T.; Yoshida, Y. [Bio-Nano Electronics Research Centre, Toyo University, 2100 Kujirai, Kawagoe, Saitama 350-8585 (Japan); Minezaki, H.; Ishihara, S. [Graduate School of Engineering, Toyo University, 2100 Kujirai, Kawagoe, Saitama 350-8585 (Japan); Racz, R.; Biri, S. [Institute of Nuclear Research (ATOMKI), H-4026 Debrecen, Bem Tér 18/c (Hungary); Muramatsu, M.; Kitagawa, A. [National Institute of Radiological Sciences (NIRS), 4-9-1 Anagawa, Inage-ku, Chiba 263-8555 (Japan); Kato, Y. [Graduate School of Engineering, Osaka University, 2-1 Yamada-oka, Suita, Osaka 565-0871 (Japan)

    2014-02-15

    A synthesis technology of endohedral fullerenes such as Fe@C{sub 60} has developed with an electron cyclotron resonance (ECR) ion source. The production of N@C{sub 60} was reported. However, the yield was quite low, since most fullerene molecules were broken in the ECR plasma. We have adopted gas-mixing techniques in order to cool the plasma and then reduce fullerene dissociation. Mass spectra of ion beams extracted from fullerene-He, Ar or Xe mixed plasmas were observed with a Faraday cup. From the results, the He gas mixing technique is effective against fullerene destruction.

  13. LLNL large-area inductively coupled plasma (ICP) source: Experiments

    International Nuclear Information System (INIS)

    Richardson, R.A.; Egan, P.O.; Benjamin, R.D.

    1995-05-01

    We describe initial experiments with a large (76-cm diameter) plasma source chamber to explore the problems associated with large-area inductively coupled plasma (ICP) sources to produce high density plasmas useful for processing 400-mm semiconductor wafers. Our experiments typically use a 640-nun diameter planar ICP coil driven at 13.56 MHz. Plasma and system data are taken in Ar and N 2 over the pressure range 3-50 mtorr. RF inductive power was run up to 2000W, but typically data were taken over the range 100-1000W. Diagnostics include optical emission spectroscopy, Langmuir probes, and B probes as well as electrical circuit measurements. The B and E-M measurements are compared with models based on commercial E-M codes. Initial indications are that uniform plasmas suitable for 400-mm processing are attainable

  14. Pulsed, atmospheric pressure plasma source for emission spectrometry

    Science.gov (United States)

    Duan, Yixiang; Jin, Zhe; Su, Yongxuan

    2004-05-11

    A low-power, plasma source-based, portable molecular light emission generator/detector employing an atmospheric pressure pulsed-plasma for molecular fragmentation and excitation is described. The average power required for the operation of the plasma is between 0.02 W and 5 W. The features of the optical emission spectra obtained with the pulsed plasma source are significantly different from those obtained with direct current (dc) discharge higher power; for example, strong CH emission at 431.2 nm which is only weakly observed with dc plasma sources was observed, and the intense CN emission observed at 383-388 nm using dc plasma sources was weak in most cases. Strong CN emission was only observed using the present apparatus when compounds containing nitrogen, such as aniline were employed as samples. The present apparatus detects dimethylsulfoxide at 200 ppb using helium as the plasma gas by observing the emission band of the CH radical. When coupled with a gas chromatograph for separating components present in a sample to be analyzed, the present invention provides an apparatus for detecting the arrival of a particular component in the sample at the end of the chromatographic column and the identity thereof.

  15. RF Plasma Source for Heavy Ion Beam Charge Neutralization

    Science.gov (United States)

    Efthimion, P. C.; Gilson, E.; Grisham, L.; Davidson, R. C.

    2003-10-01

    Highly ionized plasmas are being employed as a medium for charge neutralizing heavy ion beams in order to focus to a small spot size. Calculations suggest that plasma at a density of 1 - 100 times the ion beam density and at a length 0.1-0.5 m would be suitable for achieving a high level of charge neutralization. An ECR source has been built at the Princeton Plasma Physics Laboratory (PPPL) in support of the joint Neutralized Transport Experiment (NTX) at the Lawrence Berkeley National Laboratory (LBNL) to study ion beam neutralization with plasma. The ECR source operates at 13.6 MHz and with solenoid magnetic fields of 0-10 gauss. The goal is to operate the source at pressures 10-5 Torr at full ionization. The initial operation of the source has been at pressures of 10-4 - 10-1 Torr. Electron densities in the range of 10^8 - 10^11 cm-3 have been achieved. Recently, pulsed operation of the source has enabled operation at pressures in the 10-6 Torr range with densities of 10^11 cm-3. Near 100% ionization has been achieved. The source has been integrated with NTX and is being used in the experiments. The plasma is approximately 10 cm in length in the direction of the beam propagation. Modifications to the source will be presented that increase its length in the direction of beam propagation.

  16. Development of a long-slot microwave plasma source

    Energy Technology Data Exchange (ETDEWEB)

    Kuwata, Y., E-mail: euo1304@mail4.doshisha.ac.jp; Kasuya, T.; Miyamoto, N.; Wada, M. [Graduate School of Science and Engineering, Doshisha University, Kyotanabe, Kyoto 610-0321 (Japan)

    2016-02-15

    A 20 cm long 10 cm wide microwave plasma source was realized by inserting two 20 cm long 1.5 mm diameter rod antennas into the plasma. Plasma luminous distributions around the antennas were changed by magnetic field arrangement created by permanent magnets attached to the source. The distributions appeared homogeneous in one direction along the antenna when the spacing between the antenna and the source wall was 7.5 mm for the input microwave frequency of 2.45 GHz. Plasma density and temperature at a plane 20 cm downstream from the microwave shield were measured by a Langmuir probe array at 150 W microwave power input. The measured electron density and temperature varied over space from 3.0 × 10{sup 9} cm{sup −3} to 5.8 × 10{sup 9} cm{sup −3}, and from 1.1 eV to 2.1 eV, respectively.

  17. 77 FR 6463 - Revisions to Labeling Requirements for Blood and Blood Components, Including Source Plasma...

    Science.gov (United States)

    2012-02-08

    ... Blood Components, Including Source Plasma; Correction AGENCY: Food and Drug Administration, HHS. ACTION..., Including Source Plasma,'' which provided incorrect publication information regarding a 60-day notice that...

  18. Plasma Ion Source with an Internal Evaporator

    International Nuclear Information System (INIS)

    Turek, M.; Drozdziel, A.; Pyszniak, K.; Prucnal, S.; Maczka, D.

    2011-01-01

    A new construction of a hollow cathode ion source equipped with an internal evaporator heated by a spiral cathode filament and arc discharge is presented. The source is especially suitable for production of ions from solids. The proximity of arc discharge region and extraction opening enables production of intense ion beams even for very low discharge current (I a = 1.2 A). The currents of 50 μA (Al + ) and 70 μA (Bi + ) were obtained using the extraction voltage of 25 kV. The source is able to work for several tens of hours without maintenance breaks, giving possibility of high dose implantations. The paper presents the detailed description of the ion source as well as its experimental characteristics like dependences of extracted currents and anode voltage on anode and cathode currents. (author)

  19. Fundamental studies of the plasma extraction and ion beam formation processes in inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Niu, Hongsen.

    1995-01-01

    The fundamental and practical aspects are described for extracting ions from atmospheric pressure plasma sources into an analytical mass spectrometer. Methodologies and basic concepts of inductively coupled plasma mass spectrometry (ICP-MS) are emphasized in the discussion, including ion source, sampling interface, supersonic expansion, slumming process, ion optics and beam focusing, and vacuum considerations. Some new developments and innovative designs are introduced. The plasma extraction process in ICP-MS was investigated by Langmuir measurements in the region between the skimmer and first ion lens. Electron temperature (T e ) is in the range 2000--11000 K and changes with probe position inside an aerosol gas flow. Electron density (n e ) is in the range 10 8 --10 10 -cm at the skimmer tip and drops abruptly to 10 6 --10 8 cm -3 near the skimmer tip and drops abruptly to 10 6 --10 8 cm -3 downstream further behind the skimmer. Electron density in the beam leaving the skimmer also depends on water loading and on the presence and mass of matrix elements. Axially resolved distributions of electron number-density and electron temperature were obtained to characterize the ion beam at a variety of plasma operating conditions. The electron density dropped by a factor of 101 along the centerline between the sampler and skimmer cones in the first stage and continued to drop by factors of 10 4 --10 5 downstream of skimmer to the entrance of ion lens. The electron density in the beam expansion behind sampler cone exhibited a 1/z 2 intensity fall-off (z is the axial position). An second beam expansion originated from the skimmer entrance, and the beam flow underwent with another 1/z 2 fall-off behind the skimmer. Skimmer interactions play an important role in plasma extraction in the ICP-MS instrument

  20. Comparing Jupiter and Saturn: dimensionless input rates from plasma sources within the magnetosphere

    Directory of Open Access Journals (Sweden)

    V. M. Vasyliūnas

    2008-06-01

    Full Text Available The quantitative significance for a planetary magnetosphere of plasma sources associated with a moon of the planet can be assessed only by expressing the plasma mass input rate in dimensionless form, as the ratio of the actual mass input to some reference value. Traditionally, the solar wind mass flux through an area equal to the cross-section of the magnetosphere has been used. Here I identify another reference value of mass input, independent of the solar wind and constructed from planetary parameters alone, which can be shown to represent a mass input sufficiently large to prevent corotation already at the source location. The source rate from Enceladus at Saturn has been reported to be an order of magnitude smaller (in absolute numbers than that from Io at Jupiter. Both reference values, however, are also smaller at Saturn than at Jupiter, by factors ~40 to 60; expressed in dimensionless form, the estimated mass input from Enceladus may be larger than that from Io by factors ~4 to 6. The magnetosphere of Saturn may thus, despite a lower mass input in kg s−1, intrinsically be more heavily mass-loaded than the magnetosphere of Jupiter.

  1. Comparing Jupiter and Saturn: dimensionless input rates from plasma sources within the magnetosphere

    Directory of Open Access Journals (Sweden)

    V. M. Vasyliūnas

    2008-06-01

    Full Text Available The quantitative significance for a planetary magnetosphere of plasma sources associated with a moon of the planet can be assessed only by expressing the plasma mass input rate in dimensionless form, as the ratio of the actual mass input to some reference value. Traditionally, the solar wind mass flux through an area equal to the cross-section of the magnetosphere has been used. Here I identify another reference value of mass input, independent of the solar wind and constructed from planetary parameters alone, which can be shown to represent a mass input sufficiently large to prevent corotation already at the source location. The source rate from Enceladus at Saturn has been reported to be an order of magnitude smaller (in absolute numbers than that from Io at Jupiter. Both reference values, however, are also smaller at Saturn than at Jupiter, by factors ~40 to 60; expressed in dimensionless form, the estimated mass input from Enceladus may be larger than that from Io by factors ~4 to 6. The magnetosphere of Saturn may thus, despite a lower mass input in kg s−1, intrinsically be more heavily mass-loaded than the magnetosphere of Jupiter.

  2. Plasma source by microwaves: design description

    International Nuclear Information System (INIS)

    Camps, E.; Olea, O.; Andrade, R.; Anguiano, G.

    1992-03-01

    The design of a device for the formation of a plasma with densities of the order of 10 12 cm - 3 and low temperatures (T e ∼ 40 eV) is described. For such purpose it was carried out in the device a microwave discharge (f o = 2.45 GHz) in a resonator of high Q factor, immersed in a static external magnetic field. The device worked in the regime ω ce ≤ ω o /2 (ω ce - cyclotron frequency of the electrons, (ω o = 2 π f o ) where is possible the excitement of non lineal phenomena of waves transformation. (Author)

  3. Honeycomblike large area LaB6 plasma source for Multi-Purpose Plasma facility

    International Nuclear Information System (INIS)

    Woo, Hyun-Jong; Chung, Kyu-Sun; You, Hyun-Jong; Lee, Myoung-Jae; Lho, Taihyeop; Choh, Kwon Kook; Yoon, Jung-Sik; Jung, Yong Ho; Lee, Bongju; Yoo, Suk Jae; Kwon, Myeon

    2007-01-01

    A Multi-Purpose Plasma (MP 2 ) facility has been renovated from Hanbit mirror device [Kwon et al., Nucl. Fusion 43, 686 (2003)] by adopting the same philosophy of diversified plasma simulator (DiPS) [Chung et al., Contrib. Plasma Phys. 46, 354 (2006)] by installing two plasma sources: LaB 6 (dc) and helicon (rf) plasma sources; and making three distinct simulators: divertor plasma simulator, space propulsion simulator, and astrophysics simulator. During the first renovation stage, a honeycomblike large area LaB 6 (HLA-LaB 6 ) cathode was developed for the divertor plasma simulator to improve the resistance against the thermal shock fragility for large and high density plasma generation. A HLA-LaB 6 cathode is composed of the one inner cathode with 4 in. diameter and the six outer cathodes with 2 in. diameter along with separate graphite heaters. The first plasma is generated with Ar gas and its properties are measured by the electric probes with various discharge currents and magnetic field configurations. Plasma density at the middle of central cell reaches up to 2.6x10 12 cm -3 , while the electron temperature remains around 3-3.5 eV at the low discharge current of less than 45 A, and the magnetic field intensity of 870 G. Unique features of electric property of heaters, plasma density profiles, is explained comparing with those of single LaB 6 cathode with 4 in. diameter in DiPS

  4. Ion source for a mass spectrometer

    International Nuclear Information System (INIS)

    Kappus, G.

    1980-01-01

    The ion source is used for electron impact ionisation and chemical ionisation of a gaseous or vapour test substance. In this type of operation, openings of different sizes are provided for the entry of electrons, the exit of ions and sample entry, because of different working pressures. Part of the source is made as a movable case or container floor with the ion exit opening being a shutter. (DG) [de

  5. Study of plasma parameters influencing fractionation in laser ablation-inductively coupled plasma-mass spectrometry

    Science.gov (United States)

    Gäckle, M.; Merten, D.

    2010-12-01

    Methods permitting to test the influence of the matrix as well as of its local and temporal distribution on the plasma conditions in laser ablation-inductively coupled plasma mass spectrometry (LA-ICP-MS) are developed. For this purpose, the MS interface is used as plasma probe allowing to investigate the average plasma condition within the ICP zone observed in terms of temporal and spatial distribution of the matrix. Inserted matrix particles, particularly when being atomized and ionized, can cause considerable changes in both electron density and plasma temperature thus influencing the ionization equilibrium of the individual analytes. In this context, the plasma probe covers a region of the plasma for which no local thermodynamic equilibrium can be assumed. The differences in temperature, identified within the region of the plasma observed, amounted up to 3000 K. While in the central region conditions were detected that would not allow efficient atomization and ionization of the matrix, these conditions improve considerably towards the margin of the area observed. Depending on the nature as well as on the temporally and locally variable density of the matrix, this can lead to varying intensity ratios of the analytes and explain fractionation effects. By means of a derived equation it is shown that the deviation of the intensity ratio from the concentration ratio turns out to be more serious the higher the difference of the ionization potential of the analytes observed, the lower the plasma temperature and the higher the matrix concentration within the area observed.

  6. Industrial application of electron sources with plasma emitters

    CERN Document Server

    Belyuk, S I; Rempe, N G

    2001-01-01

    Paper contains a description, operation, design and parameters of electron sources with plasma emitters. One presents examples of application of these sources as part of automated electron-beam welding lines. Paper describes application of such sources for electron-beam deposition of composite powders. Electron-beam deposition is used to rebuild worn out part and to increase strength of new parts of machines and tools. Paper presents some examples of rebuilding part and the advantages gained in this case

  7. Beam-plasma discharge in a Kyoto beam-plasma-ion source

    International Nuclear Information System (INIS)

    Ishikawa, J.; Takagi, T.

    1983-01-01

    A beam-plasma type ion source employing an original operating principle has been developed by the present authors. The ion source consists of an ion extraction region with an electron gun, a thin long drift tube as the plasma production chamber, and a primary electron beam collector. An electron beam is effectively utilized for the dual purpose of high density plasma production as a result of beam-plasma discharge, and high current ion beam extraction with ion space-charge compensation. A high density plasma of the order of 10 11 --10 13 cm -3 was produced by virtue of the beam-plasma discharge which was caused by the interaction between a space-charge wave on the electron beam and a high frequency plasma wave. The plasma density then produced was 10 2 --10 3 times the density produced only by collisional ionization by the electron beam. In order to obtain a stable beam-plasma discharge, a secondary electron beam emitted from the electron collector should be utilized. The mechanism of the beam-plasma discharge was analyzed by use of a linear theory in the case of the small thermal energy of the electron beam, and by use of a quasilinear theory in the case of the large thermal energy. High current ion beams of more than 0.1 A were extracted even at a low extraction voltage of 1--5 kV

  8. Ion source for a mass spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Kappus, G.

    1980-07-24

    The ion source is used for electron impact ionisation and chemical ionisation of a gaseous or vapour test substance. In this type of operation, openings of different sizes are provided for the entry of electrons, the exit of ions and sample entry, because of different working pressures.

  9. Technical and experimental investigations of a plasma focus neutron source

    International Nuclear Information System (INIS)

    Rapp, H.K.

    The results obtained from two plasma-focus devices of different size allow to report on the technical and physical properties of such neutron flash sources. The results of some diagnostic methods used for the control of the gas discharge and for the measurement of the neutron production are included. The planning of plasma focus devices is illustrated with the aid of snow-plow calculations

  10. Performance evaluation of a permanent ring magnet based helicon plasma source for negative ion source research

    Science.gov (United States)

    Pandey, Arun; Bandyopadhyay, M.; Sudhir, Dass; Chakraborty, A.

    2017-10-01

    Helicon wave heated plasmas are much more efficient in terms of ionization per unit power consumed. A permanent magnet based compact helicon wave heated plasma source is developed in the Institute for Plasma Research, after carefully optimizing the geometry, the frequency of the RF power, and the magnetic field conditions. The HELicon Experiment for Negative ion-I source is the single driver helicon plasma source that is being studied for the development of a large sized, multi-driver negative hydrogen ion source. In this paper, the details about the single driver machine and the results from the characterization of the device are presented. A parametric study at different pressures and magnetic field values using a 13.56 MHz RF source has been carried out in argon plasma, as an initial step towards source characterization. A theoretical model is also presented for the particle and power balance in the plasma. The ambipolar diffusion process taking place in a magnetized helicon plasma is also discussed.

  11. Investigation of radiofrequency plasma sources for space travel

    International Nuclear Information System (INIS)

    Charles, C; Boswell, R W; Takahashi, K

    2012-01-01

    Optimization of radiofrequency (RF) plasma sources for the development of space thrusters differs from other applications such as plasma processing of materials since power efficiency, propellant usage, particle acceleration or heating become driving parameters. The development of two RF (13.56 MHz) plasma sources, the high-pressure (∼1 Torr) capacitively coupled ‘pocket rocket’ plasma micro-thruster and the low-pressure (∼1 mTorr) inductively coupled helicon double layer thruster (HDLT), is discussed within the context of mature and emerging electric propulsion devices. The density gradient in low-pressure expanding RF plasmas creates an electric field that accelerates positive ions out of the plasma. Generally, the total potential drop is similar to that of a wall sheath allowing the plasma electrons to neutralize the ion beam. A high-pressure expansion with no applied magnetic field can result in large dissociation rates and/or a collimated beam of ions of small area and a flowing heated neutral beam (‘pocket rocket’). A low-pressure expansion dominated by a magnetic field can result in the formation of electric double layers which produce a very directed neutralized beam of ions of large area (HDLT). (paper)

  12. Investigation of radiofrequency plasma sources for space travel

    Science.gov (United States)

    Charles, C.; Boswell, R. W.; Takahashi, K.

    2012-12-01

    Optimization of radiofrequency (RF) plasma sources for the development of space thrusters differs from other applications such as plasma processing of materials since power efficiency, propellant usage, particle acceleration or heating become driving parameters. The development of two RF (13.56 MHz) plasma sources, the high-pressure (˜1 Torr) capacitively coupled ‘pocket rocket’ plasma micro-thruster and the low-pressure (˜1 mTorr) inductively coupled helicon double layer thruster (HDLT), is discussed within the context of mature and emerging electric propulsion devices. The density gradient in low-pressure expanding RF plasmas creates an electric field that accelerates positive ions out of the plasma. Generally, the total potential drop is similar to that of a wall sheath allowing the plasma electrons to neutralize the ion beam. A high-pressure expansion with no applied magnetic field can result in large dissociation rates and/or a collimated beam of ions of small area and a flowing heated neutral beam (‘pocket rocket’). A low-pressure expansion dominated by a magnetic field can result in the formation of electric double layers which produce a very directed neutralized beam of ions of large area (HDLT).

  13. Characterization of DBD plasma source for biomedical applications

    Energy Technology Data Exchange (ETDEWEB)

    Kuchenbecker, M; Vioel, W [University of Applied Sciences and Arts, Faculty of Natural Sciences and Technology, Von-Ossietzky-Str. 99, 37085 Goettingen (Germany); Bibinov, N; Awakowicz, P [Institute for Electrical Engineering and Plasma Technology, Ruhr-Universitaet Bochum, Universitaetstr. 150, 44780 Bochum (Germany); Kaemlimg, A; Wandke, D, E-mail: m.kuchenbecker@web.d, E-mail: Nikita.Bibinov@rub.d, E-mail: awakowicz@aept-ruhr-uni-bochum.d, E-mail: vioel@hawk-hhg.d [CINOGY GmbH, Max-Naeder-Str. 15, 37114 Duderstadt (Germany)

    2009-02-21

    The dielectric barrier discharge (DBD) plasma source for biomedical application is characterized using optical emission spectroscopy, plasma-chemical simulation and voltage-current measurements. This plasma source possesses only one electrode covered by ceramic. Human body or some other object with enough high electric capacitance or connected to ground can serve as the opposite electrode. DBD consists of a number of microdischarge channels distributed in the gas gap between the electrodes and on the surface of the dielectric. To characterize the plasma conditions in the DBD source, an aluminium plate is used as an opposite electrode. Electric parameters, the diameter of microdischarge channel and plasma parameters (electron distribution function and electron density) are determined. The gas temperature is measured in the microdischarge channel and calculated in afterglow phase. The heating of the opposite electrode is studied using probe measurement. The gas and plasma parameters in the microdischarge channel are studied at varied distances between electrodes. According to an energy balance study, the input microdischarge electric energy dissipates mainly in heating of electrodes (about 90%) and partially (about 10%) in the production of chemical active species (atoms and metastable molecules).

  14. Measurement of the effective plasma ion mass in large tokamaks

    International Nuclear Information System (INIS)

    Lister, J.B.; Villard, L.; Ridder, G. de

    1997-01-01

    There is not yet a straightforward method for the measurement of the D-T ratio in the centre of a tokamak plasma. One of the simpler measurements put forward in the past is the interpretation of the MHD spectrum in the frequency range of the Global Alfven Eigenmodes (GAE). However, the frequencies of these modes do not only depend on the plasma mass, but are also quite strongly dependent on the details of the current and density profiles, creating a problem of deconvolution of the estimate of the plasma mass from an implicit relationship between several measurable plasma parameters and the detected eigenmode frequencies. This method has been revised to assess its likely precision for the JET tokamak. The low n GAE modes are sometimes too close to the continuum edge to be detectable and the interpretation of the GAE spectrum is rendered less direct than had been hoped. We present a statistical study on the precision with which the D-T ratio could be estimated from the GAE spectrum on JET. (author) 4 figs., 8 refs

  15. Particle flux at the outlet of an Ecr plasma source

    International Nuclear Information System (INIS)

    Gutierrez T, C.; Gonzalez D, J.

    1999-01-01

    The necessity of processing big material areas this has resulted in the development of plasma sources with the important property to be uniform in these areas. Also the continuous diminution in the size of substrates to be processed have stimulated the study of models which allow to predict the control of energy and the density of the ions and neutral particles toward the substrate. On the other hand, there are other applications of the plasma sources where it is very necessary to understand the effects generated by the energetic fluxes of ions and neutrals. These fluxes as well as another beneficial effects can improve the activation energy for the formation and improvement of the diffusion processes in the different materials. In this work, using the drift kinetic approximation is described a model to calculate the azimuthal and radial fluxes in the zone of materials processing of an Ecr plasma source type. The results obtained are compared with experimental results. (Author)

  16. Microwave plasma source having improved switching operation from plasma ignition phase to normal ion extraction phase

    International Nuclear Information System (INIS)

    Sakudo, N.; Abe, K.; Koike, H.; Okada, O.; Tokiguchi, K.

    1985-01-01

    In a microwave plasma source, a discharge space supplied with a microwave electric field is supplied with a DC magnetic field. A material to be ionized is introduced into the discharge space to produce plasma, whereby ions are extracted through an ion extracting system. A switch is provided for effecting through switching operation the change-over of the magnetic field applied to the discharge space from the intensity for the ignition of plasma to the intensity for ion extraction in succession to completion of the plasma ignition

  17. A compact time-of-flight mass spectrometer for ion source characterization

    International Nuclear Information System (INIS)

    Chen, L.; Wan, X.; Jin, D. Z.; Tan, X. H.; Huang, Z. X.; Tan, G. B.

    2015-01-01

    A compact time-of-flight mass spectrometer with overall dimension of about 413 × 250 × 414 mm based on orthogonal injection and angle reflection has been developed for ion source characterization. Configuration and principle of the time-of-flight mass spectrometer are introduced in this paper. The mass resolution is optimized to be about 1690 (FWHM), and the ion energy detection range is tested to be between about 3 and 163 eV with the help of electron impact ion source. High mass resolution and compact configuration make this spectrometer useful to provide a valuable diagnostic for ion spectra fundamental research and study the mass to charge composition of plasma with wide range of parameters

  18. Quantification of "2"3"2Th, "2"3"4U, "2"3"5U and "2"3"8U in river mollusks by magnetic sector mass spectrometry with inductively coupled plasma source (Icp-SFMS)

    International Nuclear Information System (INIS)

    Arevalo R, D. L.; Hernandez M, H.; Romero G, E. T.; Lara A, N.; Alfaro de la T, M. C.

    2016-09-01

    The present work deals with the methodology established for the quantification of "2"3"2Th, "2"3"4U, "2"3"8U and "2"3"5U in the shell of gastropod mollusks collected in the rivers Valles, Coy and Axtla of San Luis Potosi, Mexico, which belong to the Panuco River basin; these rivers have as main source of pollution the discharge of municipal sewage, waste from small industries, agricultural and cattle residues and from natural sources. Conventional methods for measuring radio-nuclides are confronted with certain conditions related to the requirement in measurement, basically in the characterization that is related to the concepts of precision and accuracy. The analysis of the gastropod mollusk shell was performed by the Icp-SFMS technique; the main advantages of this technique lie in the isotope quantification capacity, the high precision and the low limits of detection, in this study are very important because these elements are in concentrations between ppb and ppt. This technique allowed the analysis of the samples having a complex matrix by the presence CaCO_3 minimizing the interferences thanks to the ionization efficiency of the Ar plasma. For the species Pachychilus monachus were found concentrations of "2"3"2Th of 0.16-5.37 μg/g and of total U of 0.101-4.081 μg/g being this species where the highest values of total U were found. For Thiara (melanoids) tuberculata the lowest values were found among the different species ("2"3"2Th 0.61-3.61 μg/g and total U 0.006-0.042 μg/g), for Pachychilus suturalis, values of "2"3"2Th of 0.58-6.4 μg/g and for Pachychilus sp. were found between 0.26-7.62 μg/g and for total U values between 0.28-3.33 μg/g. The method offers several advantages: speed, good precision, low values of quantification limits and high sensitivity in the measurement of radio-nuclides and heavy metals. (Author)

  19. Counter-facing plasma guns for efficient extreme ultra-violet plasma light source

    Directory of Open Access Journals (Sweden)

    Kuroda Yusuke

    2013-11-01

    Full Text Available A plasma focus system composed of a pair of counter-facing coaxial guns was proposed as a long-pulse and/or repetitive high energy density plasma source. We applied Li as the source of plasma for improvement of the conversion efficiency, the spectral purity, and the repetition capability. For operation of the system with ideal counter-facing plasma focus mode, we changed the system from simple coaxial geometry to a multi-channel configuration. We applied a laser trigger to make synchronous multi-channel discharges with low jitter. The results indicated that the configuration is promising to make a high energy density plasma with high spectral efficiency.

  20. Negative-Ion source for mass selective photodetachment photoelectron spectroscopy

    International Nuclear Information System (INIS)

    Kaesmaier, R.; Baemann, C.; Drechsler, G.; Boesl, U.

    1995-01-01

    We have designed and constructed a negative ion source for mass spectrometry and mass selective photodetachement photoelectron spectroscopy. The characteristics of the source are high anion densities and a large variety of accessible systems. Thus, mass spectra and photoelectron spectra of large unvolatile moelcules (biomolecules), of metal-organic compounds and of molecule water clusters, especially mentioned in this article, have been measured. Combining mass spectrometry, photoelectron spectroscopy (PES) and high resolution ZEKE (zero kinetic energy)-PES (1) should make the apparatus to an ideal diagnostic tool for structural assignment

  1. 21 CFR 640.64 - Collection of blood for Source Plasma.

    Science.gov (United States)

    2010-04-01

    ... 21 Food and Drugs 7 2010-04-01 2010-04-01 false Collection of blood for Source Plasma. 640.64... (CONTINUED) BIOLOGICS ADDITIONAL STANDARDS FOR HUMAN BLOOD AND BLOOD PRODUCTS Source Plasma § 640.64 Collection of blood for Source Plasma. (a) Supervision. All blood for the collection of Source Plasma shall...

  2. Development of negative heavy ion sources for plasma potential measurement

    International Nuclear Information System (INIS)

    Sasao, M.; Okabe, Y.; Fujisawa, A.; Iguchi, H.; Fujita, J.; Yamaoka, H.; Wada, M.

    1991-10-01

    A plasma sputter negative ion source was studied for its applicability to the potential measurement of a fusion plasma. Both the beam current density and the beam energy spread are key issues. Energy spectra of a self extracted Au - beam from the source were measured under the condition of a constant work function of the production surface. The full width of half maximum (FWHM) increases from 3 eV to 9 eV monotonically as the target voltage increases from 50 V to 300 V, independently from the target surface work function of 2.2 - 3 eV. (author)

  3. Plasma source ion implantation research at southwestern institute of physics

    International Nuclear Information System (INIS)

    Shang Zhenkui; Geng Man; Tong Honghui

    1997-10-01

    The PSII-EX device and PSII-IM device for research and development of plasma source ion implantation (PSII) technology are described briefly. The functions, main technical specifications and properties of the devices are also discussed. After ion implantation by PSII, the improvements of the surface-mechanical properties (such as microhardness, wear-resistance, friction factor, biological compatibility, etc) for some materials, microanalysis and numerical simulation of modified layers of materials, the technical developments for the practical workpiece treatments and the preliminary experiments for plasma source ion implantation-enhanced deposition are introduced too. As last, the future work about PSII have been proposed

  4. The ionization length in plasmas with finite temperature ion sources

    Science.gov (United States)

    Jelić, N.; Kos, L.; Tskhakaya, D. D.; Duhovnik, J.

    2009-12-01

    The ionization length is an important quantity which up to now has been precisely determined only in plasmas which assume that the ions are born at rest, i.e., in discharges known as "cold ion-source" plasmas. Presented here are the results of our calculations of the ionization lengths in plasmas with an arbitrary ion source temperature. Harrison and Thompson (H&T) [Proc. Phys. Soc. 74, 145 (1959)] found the values of this quantity for the cases of several ion strength potential profiles in the well-known Tonks-Langmuir [Phys. Rev. 34, 876 (1929)] discharge, which is characterized by "cold" ion temperature. This scenario is also known as the "singular" ion-source discharge. The H&T analytic result covers cases of ion sources proportional to exp(βΦ) with Φ the normalized plasma potential and β =0,1,2 values, which correspond to particular physical scenarios. Many years following H&T's work, Bissell and Johnson (B&J) [Phys. Fluids 30, 779 (1987)] developed a model with the so-called "warm" ion-source temperature, i.e., "regular" ion source, under B&J's particular assumption that the ionization strength is proportional to the local electron density. However, it appears that B&J were not interested in determining the ionization length at all. The importance of this quantity to theoretical modeling was recognized by Riemann, who recently answered all the questions of the most advanced up-to-date plasma-sheath boundary theory with cold ions [K.-U. Riemann, Phys. Plasmas 13, 063508 (2006)] but still without the stiff warm ion-source case solution, which is highly resistant to solution via any available analytic method. The present article is an extension of H&T's results obtained for a single point only with ion source temperature Tn=0 to arbitrary finite ion source temperatures. The approach applied in this work is based on the method recently developed by Kos et al. [Phys. Plasmas 16, 093503 (2009)].

  5. Plasma properties of a modified beam-plasma type ion source

    International Nuclear Information System (INIS)

    Ishikawa, Junzo; Sano, Fumimichi; Tsuji, Hiroshi; Ektessabi, A.M.; Takagi, Toshinori

    1978-01-01

    The properties of the plasma produced by beam-plasma discharge were experimentally investigated. The ion source used for this work consists of three parts, that is, the ion-extracting region with an electron gun, the drift space and the collector region. Primary and secondary electron beams are injected in to the drift tube. The interaction between plasma and these electron beams causes production of high density plasma by virtue of the beam-plasma discharge. The gas inlet is located in the middle of the drift tube, so that the gas conductance is high. The energy of the primary and secondary electron beams is transferred to that microwaves through beam-plasma interaction. The microwaves heat the plasma electrons by the cyclotron resonance or other mechanism. The amount of the energetic plasma electrons is much larger than that of the beam electrons, so that neutral gas is ionized. The density of the produced plasma is 10 2 or 10 3 times as large as the plasma produced by impact ionization. With a probe located in the middle of the drift tube, the plasma density and the electron temperature can be measured, and the power and spectra of the microwaves can be detected. The microwave oscillation, the primary electron beam characteristics, and the gas pressure characteristics were studied. Larger current of the high energy primary of secondary electron beam is required for the effective discharge. The ion source has to be operated at the minimum gas pressure. The length of beam-plasma interaction and the magnetic field intensity in the drift tube are also important parameters. (Kato, T.)

  6. Investigation of rf plasma light sources for dye laser excitation

    International Nuclear Information System (INIS)

    Kendall, J.S.; Jaminet, J.F.

    1975-06-01

    Analytical and experimental studies were performed to assess the applicability of radio frequency (rf) induction heated plasma light sources for potential excitation of continuous dye lasers. Experimental efforts were directed toward development of a continuous light source having spectral flux and emission characteristics approaching that required for pumping organic dye lasers. Analytical studies were performed to investigate (1) methods of pulsing the light source to obtain higher radiant intensity and (2) methods of integrating the source with a reflective cavity for pumping a dye cell. (TFD)

  7. Modeling the chemistry of plasma polymerization using mass spectrometry.

    Science.gov (United States)

    Ihrig, D F; Stockhaus, J; Scheide, F; Winkelhake, Oliver; Streuber, Oliver

    2003-04-01

    The goal of the project is a solvent free painting shop. The environmental technologies laboratory is developing processes of plasma etching and polymerization. Polymerized thin films are first-order corrosion protection and primer for painting. Using pure acetylene we get very nice thin films which were not bonded very well. By using air as bulk gas it is possible to polymerize, in an acetylene plasma, well bonded thin films which are stable first-order corrosion protections and good primers. UV/Vis spectroscopy shows nitrogen oxide radicals in the emission spectra of pure nitrogen and air. But nitrogen oxide is fully suppressed in the presence of acetylene. IR spectroscopy shows only C=O, CH(2) and CH(3) groups but no nitrogen species. With the aid of UV/Vis spectra and the chemistry of ozone formation it is possible to define reactive traps and steps, molecule depletion and processes of proton scavenging and proton loss. Using a numerical model it is possible to evaluate these processes and to calculate theoretical mass spectra. Adjustment of theoretical mass spectra to real measurements leads to specific channels of polymerization which are driven by radicals especially the acetyl radical. The estimated theoretical mass spectra show the specific channels of these chemical processes. It is possible to quantify these channels. This quantification represents the mass flow through this chemical system. With respect to these chemical processes it is possible to have an idea of pollutant production processes.

  8. Development of long lifetime-high current plasma cathode ion source

    International Nuclear Information System (INIS)

    Yabe, Eiji; Takayama, Kazuo; Fukui, Ryota.

    1987-01-01

    A long lifetime ion source with plasma cathode has been developed for use in ion implantation. In this ion source, a plasma of a nonreactive working gas serves as a cathode in place of a thermionic tungsten filament used in the Freeman ion source. In an applied magnetic field, the plasma cathode is convergent, i.e. filament-like; in zero magnetic field, it turns divergent and spray-like. In the latter case, the plasma exhibits a remarkable ability when the working gas has an ionization potential larger than the feed gas. By any combination of a working gas of either argon or neon and a feed gas of AsF 5 or PF 5 , the lifetime of this ion source was found to be more than 90 hours with an extraction voltage of 40 kV and the corresponding ion current density 20 mA/cm 2 . Mass spectrometry results show that this ion source has an ability of generating a considerable amount of As + and P + ions from AsF 5 and PF 5 , and hence will be useful for realizing a fully cryopumped ion implanter system. This ion source is eminently suitable for use in oxygen ion production. (author)

  9. Discharge regimes and density jumps in a helicon plasma source

    International Nuclear Information System (INIS)

    Shinohara, S.; Yonekura, K.

    1999-01-01

    A high density plasma source using a helicon wave is becoming very attractive in plasma processing and confinement devices. In the previous work, the characteristics of this wave and plasma performance with diameters of 5 and 45 cm have been studied, and the helicon wave was only observed after the density jump. Recently, density jumps from the low to high electron densities with a level of 10 13 cm -3 were investigated by changing the antenna wavenumber spectrum, and the obtained results were compared with the inductively coupled plasma (ICP). However, the mechanisms of density jumps and plasma production are still open questions to be answered. Here, the authors try to investigate the discharge regimes and density jumps in a helicon plasma source, by changing the antenna wavenumber spectrum. For he case of the parallel current directions in the antenna, where the low wavenumber spectrum part is large, the density jump was observed with the low RF input power of P in < 300 W regardless of the magnetic field. On the other hand, for the case of the opposite directions, where the low wavenumber spectrum part is small, the threshold power to obtain the jump became high with the increase in the magnetic field. This can be understood from the dispersion relation of the helicon wave. The wave structures and the dispersion relations in the discharge modes will be also shown

  10. Plasmas in compact traps: From ion sources to multidisciplinary research

    Science.gov (United States)

    Mascali, D.; Musumarra, A.; Leone, F.; Galatà, A.; Romano, F. P.; Gammino, S.

    2017-09-01

    In linear (minimum-B) magneto-static traps dense and hot plasmas are heated by electromagnetic radiation in the GHz domain via the Electron Cyclotron Resonance (ECR). The values of plasma density, temperature and confinement times ( n_eτ_i>10^{13} cm ^{-3} s; T_e>10 keV) are similar to the ones of thermonuclear plasmas. The research in this field -devoted to heating and confinement optimization- has been supported by numerical modeling and advanced diagnostics, for probing the plasma especially in a non-invasive way. ECR-based systems are nowadays able to produce extremely intense (tens or hundreds of mA) beams of light ions (p, d, He), and relevant currents of heavier elements (C, O, N) up to heavy ions like Xe, Pb, U. Such beams can be extracted from the trap by a proper electrostatic system. The above-mentioned properties make these plasmas very attractive for interdisciplinary researches also, such as i) nuclear decays rates measurements in stellar-like conditions, ii) energy conversion studies, being exceptional sources of short-wavelength electromagnetic radiation (EUV, X-rays, hard X-rays and gammas, useful in material science and archaeometry), iii) environments allowing precise spectroscopical measurements as benchmarks for magnetized astrophysical plasmas. The talk will give an overview about the state-of-the-art in the field of intense ion sources, and some new perspectives for interdisciplinary research, with a special attention to the developments based at INFN-LNS.

  11. Characterization of atomic oxygen from an ECR plasma source

    International Nuclear Information System (INIS)

    Naddaf, M; Bhoraskar, V N; Mandale, A B; Sainkar, S R; Bhoraskar, S V

    2002-01-01

    A low-power microwave-assisted electron cyclotron resonance (ECR) plasma system is shown to be a powerful and effective source of atomic oxygen (AO) useful in material processing. A 2.45 GHz microwave source with maximum power of 600 W was launched into the cavity to generate the ECR plasma. A catalytic nickel probe was used to determine the density of AO. The density of AO is studied as a function of pressure and axial position of the probe in the plasma chamber. It was found to vary from ∼1x10 20 to ∼10x10 20 atom m -3 as the plasma pressure was varied from 0.8 to 10 mTorr. The effect of AO in oxidation of silver is investigated by gravimetric analysis. The stoichiometric properties of the oxide are studied using the x-ray photoelectron spectroscopy as well as energy dispersive x-ray analysis. The degradation of the silver surface due to sputtering effect was viewed by scanning electron spectroscopy. The sputtering yield of oxygen ions in the plasma is calculated using the TRIM code. The effects of plasma pressure and the distance from the ECR zone on the AO density were also investigated. The density of AO measured by oxidation of silver is in good agreement with results obtained from the catalytic nickel probe

  12. Characterization of atomic oxygen from an ECR plasma source

    Science.gov (United States)

    Naddaf, M.; Bhoraskar, V. N.; Mandale, A. B.; Sainkar, S. R.; Bhoraskar, S. V.

    2002-11-01

    A low-power microwave-assisted electron cyclotron resonance (ECR) plasma system is shown to be a powerful and effective source of atomic oxygen (AO) useful in material processing. A 2.45 GHz microwave source with maximum power of 600 W was launched into the cavity to generate the ECR plasma. A catalytic nickel probe was used to determine the density of AO. The density of AO is studied as a function of pressure and axial position of the probe in the plasma chamber. It was found to vary from ~1×1020 to ~10×1020 atom m-3 as the plasma pressure was varied from 0.8 to 10 mTorr. The effect of AO in oxidation of silver is investigated by gravimetric analysis. The stoichiometric properties of the oxide are studied using the x-ray photoelectron spectroscopy as well as energy dispersive x-ray analysis. The degradation of the silver surface due to sputtering effect was viewed by scanning electron spectroscopy. The sputtering yield of oxygen ions in the plasma is calculated using the TRIM code. The effects of plasma pressure and the distance from the ECR zone on the AO density were also investigated. The density of AO measured by oxidation of silver is in good agreement with results obtained from the catalytic nickel probe.

  13. Characterization of atomic oxygen from an ECR plasma source

    Energy Technology Data Exchange (ETDEWEB)

    Naddaf, M [Center for Advanced Studies in Material Science and Solid State Physics, University of Pune, Pune 411 007 (India); Bhoraskar, V N [Center for Advanced Studies in Material Science and Solid State Physics, University of Pune, Pune 411 007 (India); Mandale, A B [National Chemical Laboratory, Pashan, Pune 411008 (India); Sainkar, S R [National Chemical Laboratory, Pashan, Pune 411008 (India); Bhoraskar, S V [Center for Advanced Studies in Material Science and Solid State Physics, University of Pune, Pune 411 007 (India)

    2002-11-01

    A low-power microwave-assisted electron cyclotron resonance (ECR) plasma system is shown to be a powerful and effective source of atomic oxygen (AO) useful in material processing. A 2.45 GHz microwave source with maximum power of 600 W was launched into the cavity to generate the ECR plasma. A catalytic nickel probe was used to determine the density of AO. The density of AO is studied as a function of pressure and axial position of the probe in the plasma chamber. It was found to vary from {approx}1x10{sup 20} to {approx}10x10{sup 20} atom m{sup -3} as the plasma pressure was varied from 0.8 to 10 mTorr. The effect of AO in oxidation of silver is investigated by gravimetric analysis. The stoichiometric properties of the oxide are studied using the x-ray photoelectron spectroscopy as well as energy dispersive x-ray analysis. The degradation of the silver surface due to sputtering effect was viewed by scanning electron spectroscopy. The sputtering yield of oxygen ions in the plasma is calculated using the TRIM code. The effects of plasma pressure and the distance from the ECR zone on the AO density were also investigated. The density of AO measured by oxidation of silver is in good agreement with results obtained from the catalytic nickel probe.

  14. Electron Beam Diagnosis and Dynamics using DIADYN Plasma Source

    Energy Technology Data Exchange (ETDEWEB)

    Toader, D; Craciun, G; Manaila, E; Oproiu, C [National Institute of Research for Laser, Plasma and Radiation Physics Bucuresti (Romania); Marghitu, S [ICPE Electrostatica S.A - Bucuresti (Romania)

    2009-11-15

    This paper is presenting results obtained with the DIADYN installation after replacing its vacuum electron source (VES{sub L}V) with a plasma electron source (PES{sub L}V). DIADYN is a low energy laboratory equipment operating with 10 to 50 keV electron beams and designed to help realize non-destructive diagnosis and dynamics for low energy electron beams but also to be used in future material irradiations. The results presented here regard the beam diagnosis and dynamics made with beams obtained from the newly replaced plasma source. We discuss both results obtained in experimental dynamics and dynamics calculation results for electron beams extracted from the SEP{sub L}V source.

  15. Operation of Ferroelectric Plasma Sources in a Gas Discharge Mode

    International Nuclear Information System (INIS)

    Dunaevsky, A.; Fisch, N.J.

    2004-01-01

    Ferroelectric plasma sources in vacuum are known as sources of ablative plasma, formed due to surface discharge. In this paper, observations of a gas discharge mode of operation of the ferroelectric plasma sources (FPS) are reported. The gas discharge appears at pressures between approximately 20 and approximately 80 Torr. At pressures of 1-20 Torr, there is a transition from vacuum surface discharge to the gas discharge, when both modes coexist and the surface discharges sustain the gas discharge. At pressures between 20 and 80 Torr, the surface discharges are suppressed, and FPS operate in pure gas discharge mode, with the formation of almost uniform plasma along the entire surface of the ceramics between strips. The density of the expanding plasma is estimated to be about 1013 cm-3 at a distance of 5.5 mm from the surface. The power consumption of the discharge is comparatively low, making it useful for various applications. This paper also presents direct measurements of the yield of secondary electron emission from ferroelectric ceramics, which, at low energies of primary electrons, is high and dependent on the polarization of the ferroelectric material

  16. Plasma source ion implantation of ammonia into electroplated chromium

    International Nuclear Information System (INIS)

    Scheuer, J.T.; Walter, K.C.; Rej, D.J.; Nastasi, M.; Blanchard, J.P.

    1995-01-01

    Ammonia gas (NH 3 ) has been used as a nitrogen source for plasma source ion implantation processing of electroplated chromium. No evidence was found of increased hydrogen concentrations in the bulk material, implying that ammonia can be used without risking hydrogen embrittlement. The retained nitrogen dose of 2.1 x 10 17 N-at/cm 2 is sufficient to increase the surface hardness of electroplated Cr by 24% and decrease the wear rate by a factor of 4

  17. RF Plasma modeling of the Linac4 H− ion source

    CERN Document Server

    Mattei, S; Hatayama, A; Lettry, J; Kawamura, Y; Yasumoto, M; Schmitzer, C

    2013-01-01

    This study focuses on the modelling of the ICP RF-plasma in the Linac4 H− ion source currently being constructed at CERN. A self-consistent model of the plasma dynamics with the RF electromagnetic field has been developed by a PIC-MCC method. In this paper, the model is applied to the analysis of a low density plasma discharge initiation, with particular interest on the effect of the external magnetic field on the plasma properties, such as wall loss, electron density and electron energy. The use of a multi-cusp magnetic field effectively limits the wall losses, particularly in the radial direction. Preliminary results however indicate that a reduced heating efficiency results in such a configuration. The effect is possibly due to trapping of electrons in the multi-cusp magnetic field, preventing their continuous acceleration in the azimuthal direction.

  18. Enhanced confinement in electron cyclotron resonance ion source plasma.

    Science.gov (United States)

    Schachter, L; Stiebing, K E; Dobrescu, S

    2010-02-01

    Power loss by plasma-wall interactions may become a limitation for the performance of ECR and fusion plasma devices. Based on our research to optimize the performance of electron cyclotron resonance ion source (ECRIS) devices by the use of metal-dielectric (MD) structures, the development of the method presented here, allows to significantly improve the confinement of plasma electrons and hence to reduce losses. Dedicated measurements were performed at the Frankfurt 14 GHz ECRIS using argon and helium as working gas and high temperature resistive material for the MD structures. The analyzed charge state distributions and bremsstrahlung radiation spectra (corrected for background) also clearly verify the anticipated increase in the plasma-electron density and hence demonstrate the advantage by the MD-method.

  19. Operation of the ORNL High Particle Flux Helicon Plasma Source

    International Nuclear Information System (INIS)

    Goulding, Richard Howell; Biewer, Theodore M.; Caughman, John B.; Chen, Guangye; Owen, Larry W.; Sparks, Dennis O.

    2011-01-01

    A high power, high particle flux rf-based helicon plasma source has been constructed at ORNL and operated at power levels up to 30 kW. High-density hydrogen and helium plasmas have been produced. The source has been designed as the basis for a linear plasma materials interaction (PMI) test facility that will generate particle fluxes Gamma(p) > 10(23) M-3 s(-1), and utilize additional ion and electron cyclotron heating to produce high parallel (to the magnetic field) heat fluxes of similar to 10 MW/m(2). An rf-based source for PMI research is of interest because high plasma densities are generated with no internal electrodes, allowing true steady state operation with minimal impurity generation. The ORNL helicon source has a diameter of 15 cm and to-date has operated at a frequency f = 13.56 MHz, with magnetic field strength vertical bar B vertical bar in the antenna region up to similar to 0.15 T. Maximum densities of 3 x 10(19) M-3 in He and 2.5 x 10(19) m(-3) in H have been achieved. Radial density profiles have been seen to be dependent on the axial vertical bar B vertical bar profile.

  20. Operation of the ORNL High Particle Flux Helicon Plasma Source

    International Nuclear Information System (INIS)

    Goulding, R. H.; Biewer, T. M.; Caughman, J. B. O.; Chen, G. C.; Owen, L. W.; Sparks, D. O.

    2011-01-01

    A high power, high particle flux rf-based helicon plasma source has been constructed at ORNL and operated at power levels up to 30 kW. High-density hydrogen and helium plasmas have been produced. The source has been designed as the basis for a linear plasma materials interaction (PMI) test facility that will generate particle fluxes Γ p 10 23 m -3 s -1 , and utilize additional ion and electron cyclotron heating to produce high parallel (to the magnetic field) heat fluxes of ∼10 MW/m 2 . An rf-based source for PMI research is of interest because high plasma densities are generated with no internal electrodes, allowing true steady state operation with minimal impurity generation. The ORNL helicon source has a diameter of 15 cm and to-date has operated at a frequency f = 13.56 MHz, with magnetic field strength |B| in the antenna region up to ∼0.15 T. Maximum densities of 3x10 19 m -3 in He and 2.5x10 19 m -3 in H have been achieved. Radial density profiles have been seen to be dependent on the axial |B| profile.

  1. RF-Plasma Source Commissioning in Indian Negative Ion Facility

    International Nuclear Information System (INIS)

    Singh, M. J.; Bandyopadhyay, M.; Yadava, Ratnakar; Chakraborty, A. K.; Bansal, G.; Gahlaut, A.; Soni, J.; Kumar, Sunil; Pandya, K.; Parmar, K. G.; Sonara, J.; Kraus, W.; Heinemann, B.; Riedl, R.; Obermayer, S.; Martens, C.; Franzen, P.; Fantz, U.

    2011-01-01

    The Indian program of the RF based negative ion source has started off with the commissioning of ROBIN, the inductively coupled RF based negative ion source facility under establishment at Institute for Plasma research (IPR), India. The facility is being developed under a technology transfer agreement with IPP Garching. It consists of a single RF driver based beam source (BATMAN replica) coupled to a 100 kW, 1 MHz RF generator with a self excited oscillator, through a matching network, for plasma production and ion extraction and acceleration. The delivery of the RF generator and the RF plasma source without the accelerator, has enabled initiation of plasma production experiments. The recent experimental campaign has established the matching circuit parameters that result in plasma production with density in the range of 0.5-1x10 18 /m 3 , at operational gas pressures ranging between 0.4-1 Pa. Various configurations of the matching network have been experimented upon to obtain a stable operation of the set up for RF powers ranging between 25-85 kW and pulse lengths ranging between 4-20 s. It has been observed that the range of the parameters of the matching circuit, over which the frequency of the power supply is stable, is narrow and further experiments with increased number of turns in the coil are in the pipeline to see if the range can be widened. In this paper, the description of the experimental system and the commissioning data related to the optimisation of the various parameters of the matching network, to obtain stable plasma of required density, are presented and discussed.

  2. RF-Plasma Source Commissioning in Indian Negative Ion Facility

    Science.gov (United States)

    Singh, M. J.; Bandyopadhyay, M.; Bansal, G.; Gahlaut, A.; Soni, J.; Kumar, Sunil; Pandya, K.; Parmar, K. G.; Sonara, J.; Yadava, Ratnakar; Chakraborty, A. K.; Kraus, W.; Heinemann, B.; Riedl, R.; Obermayer, S.; Martens, C.; Franzen, P.; Fantz, U.

    2011-09-01

    The Indian program of the RF based negative ion source has started off with the commissioning of ROBIN, the inductively coupled RF based negative ion source facility under establishment at Institute for Plasma research (IPR), India. The facility is being developed under a technology transfer agreement with IPP Garching. It consists of a single RF driver based beam source (BATMAN replica) coupled to a 100 kW, 1 MHz RF generator with a self excited oscillator, through a matching network, for plasma production and ion extraction and acceleration. The delivery of the RF generator and the RF plasma source without the accelerator, has enabled initiation of plasma production experiments. The recent experimental campaign has established the matching circuit parameters that result in plasma production with density in the range of 0.5-1×1018/m3, at operational gas pressures ranging between 0.4-1 Pa. Various configurations of the matching network have been experimented upon to obtain a stable operation of the set up for RF powers ranging between 25-85 kW and pulse lengths ranging between 4-20 s. It has been observed that the range of the parameters of the matching circuit, over which the frequency of the power supply is stable, is narrow and further experiments with increased number of turns in the coil are in the pipeline to see if the range can be widened. In this paper, the description of the experimental system and the commissioning data related to the optimisation of the various parameters of the matching network, to obtain stable plasma of required density, are presented and discussed.

  3. Characteristics of an elongated plasma column produced by magnetically coupled hollow cathode plasma source

    Science.gov (United States)

    Bhuva, M. P.; Karkari, S. K.; Kumar, Sunil

    2018-03-01

    An elongated plasma column in the presence of an axial magnetic field has been formed using a cylindrical hollow cathode (HC) and a constricted anode (CA). The plasma characteristics of the central line have been found to vary with the magnetic field strength and the axial distance from the source. It is believed that the primary electrons constituting the discharge current are steered by the axial magnetic field to undertake ionizing collisions along the plasma column. The current carrying electrons from the HC reach the anode by cross-field diffusion towards the central line. The above observation has been substantiated using a phenomenological model which links the observed characteristics of the source with the plasma column. The experimental results are found to be in qualitative agreement with the model.

  4. Ion source with radiofrequency mass filter for sputtering purposes

    International Nuclear Information System (INIS)

    Sielanko, J.; Sowa, M.

    1990-01-01

    The Kaufman ion source with radiofrequency mass filter is described. The construction as well as operating characteristics of ion source are presented. The arrangement is suitable for range distribution measurements of implanted layers, where the sputtering rate has to be constant over the wide range of sputtering time. 4 figs., 17 refs. (author)

  5. Optical emission spectra of a copper plasma produced by a metal vapour vacuum arc plasma source

    International Nuclear Information System (INIS)

    Yotsombat, B.; Poolcharuansin, P.; Vilaithong, T.; Davydov, S.; Brown, I.G.

    2001-01-01

    Optical emission spectroscopy in the range 200-800 nm was applied for investigation of the copper plasma produced by a metal vapour vacuum arc plasma source. The experiments were conducted for the cases when the plasma was guided by straight and Ω-shaped curved solenoids as well as without solenoids, and also for different vacuum conditions. It was found that, besides singly- and doubly-charged ions, a relatively high concentration of excited neutral copper atoms was present in the plasma. The relative fraction of excited atoms was much higher in the region close to the cathode surface than in the plasma column inside the solenoid. The concentration of excited neutral, singly- and doubly-ionized atoms increased proportionally when the arc current was increased to 400 A. Some weak lines were attributed to more highly ionized copper species and impurities in the cathode material. (author)

  6. Plasma phenomenology in astrophysical systems: Radio-sources and jets

    International Nuclear Information System (INIS)

    Montani, Giovanni; Petitta, Jacopo

    2014-01-01

    We review the plasma phenomenology in the astrophysical sources which show appreciable radio emissions, namely Radio-Jets from Pulsars, Microquasars, Quasars, and Radio-Active Galaxies. A description of their basic features is presented, then we discuss in some details the links between their morphology and the mechanisms that lead to the different radio-emissions, investigating especially the role played by the plasma configurations surrounding compact objects (Neutron Stars, Black Holes). For the sake of completeness, we briefly mention observational techniques and detectors, whose structure set them apart from other astrophysical instruments. The fundamental ideas concerning angular momentum transport across plasma accretion disks—together with the disk-source-jet coupling problem—are discussed, by stressing their successes and their shortcomings. An alternative scenario is then inferred, based on a parallelism between astrophysical and laboratory plasma configurations, where small-scale structures can be found. We will focus our attention on the morphology of the radio-jets, on their coupling with the accretion disks and on the possible triggering phenomena, viewed as profiles of plasma instabilities

  7. Plasma and Ion Sources in Large Area Coatings: A Review

    Energy Technology Data Exchange (ETDEWEB)

    Anders, Andre

    2005-02-28

    Efficient deposition of high-quality coatings often requires controlled application of excited or ionized particles. These particles are either condensing (film-forming) or assisting by providing energy and momentum to the film growth process, resulting in densification, sputtering/etching, modification of stress, roughness, texture, etc. In this review, the technical means are surveyed enabling large area application of ions and plasmas, with ion energies ranging from a few eV to a few keV. Both semiconductortype large area (single wafer or batch processing with {approx} 1000 cm{sup 2}) and in-line web and glass-coating-type large area (> 10{sup 7} m{sup 2} annually) are considered. Characteristics and differences between plasma and ion sources are explained. The latter include gridded and gridless sources. Many examples are given, including sources based on DC, RF, and microwave discharges, some with special geometries like hollow cathodes and E x B configurations.

  8. ECR plasma source for heavy ion beam charge neutralization

    Science.gov (United States)

    Efthimion, Philip C.; Gilson, Erik; Grisham, Larry; Kolchin, Pavel; Davidson, Ronald C.; Yu, Simon; Logan, B. Grant

    2003-01-01

    Highly ionized plasmas are being considered as a medium for charge neutralizing heavy ion beams in order to focus beyond the space-charge limit. Calculations suggest that plasma at a density of 1 100 times the ion beam density and at a length [similar]0.1 2 m would be suitable for achieving a high level of charge neutralization. An Electron Cyclotron Resonance (ECR) source has been built at the Princeton Plasma Physics Laboratory (PPPL) to support a joint Neutralized Transport Experiment (NTX) at the Lawrence Berkeley National Laboratory (LBNL) to study ion beam neutralization with plasma. The ECR source operates at 13.6 MHz and with solenoid magnetic fields of 1 10 gauss. The goal is to operate the source at pressures [similar]10[minus sign]6 Torr at full ionization. The initial operation of the source has been at pressures of 10[minus sign]4 10[minus sign]1 Torr. Electron densities in the range of 108 to 1011 cm[minus sign]3 have been achieved. Low-pressure operation is important to reduce ion beam ionization. A cusp magnetic field has been installed to improve radial confinement and reduce the field strength on the beam axis. In addition, axial confinement is believed to be important to achieve lower-pressure operation. To further improve breakdown at low pressure, a weak electron source will be placed near the end of the ECR source. This article also describes the wave damping mechanisms. At moderate pressures (> 1 mTorr), the wave damping is collisional, and at low pressures (< 1 mTorr) there is a distinct electron cyclotron resonance.

  9. Grid system design on the plasma cathode electron source

    International Nuclear Information System (INIS)

    Agus Purwadi

    2014-01-01

    It has been designed the grid system on the Plasma Cathode Electron Source (PCES). Grid system with the electron emission hole of (15 x 60) cm 2 , the single aperture grid size of (0,5 x O,5) mm 2 and the grid wire diameter of 0,25 mm, will be used on the plasma generator chamber. If the sum of grid holes known and the value of electron emission current through every the grid hole known too then the total value of electron emission Current which emits from the plasma generator chamber can be determined It has been calculated the value of electron emission current I e as function of the grid radius r e =(0.28, 0.40, 0.49, 0.56, 0.63, 0.69) mm on the electron temperature of T e = 5 eV for varying of the value plasma electron densities n e = (10 15 , 10 16 , 10 17 , 10 18 ) m -3 . Also for the value of electron emission current fe as function of the grid radius r e = (0.28, 0.40, 0.49. 0.56, 0.63,0.69) mm on the electron density n e = 10 17 m -3 for varying of the value of plasma electron temperatures T e = (1, 2, 3, 4, 5) eV. electron emission current will be increase by increasing grid radius, electron temperature as well as plasma electron density. (author)

  10. Tailoring of materials by atomic oxygen from ECR plasma source

    International Nuclear Information System (INIS)

    Naddaf, Munzer; Bhoraskar, S.V.

    2002-01-01

    Full text: An intense source of oxygen finds important applications in many areas of science, technology and industry. It has been successfully used for surface activation and cleaning in the electronic, chemical and automotive industries. Atomic oxygen and interaction with materials have also a significant importance in space science and technology. This paper describes the detailed studies related to the surface modification and processing of different materials, which include metals and polymers by atomic oxygen produced in microwave assisted electron cyclotron resonance plasma. The energy distribution of ions was measured as a function of plasma parameters and density measurements were supplemented by catalytic probe using nickel and oxidation of silver surface

  11. Impurity radiation from a beam-plasma neutron source

    International Nuclear Information System (INIS)

    Molvik, A.W.

    1995-01-01

    Impurity radiation, in a worst case evaluation for a beam-plasma neutron source (BPNS), does not limit performance. Impurities originate from four sources: (a) sputtering from walls by charge exchange or alpha particle bombardment, (b) sputtering from limiters, (c) plasma desorption of gas from walls and (d) injection with neutral beams. Sources (c) and (d) are negligible; adsorbed gas on the walls of the confinement chamber and the neutral beam sources is removed by the steady state discharge. Source (b) is negligible for impinging ion energies below the sputtering threshold (T i ≤ 0.025 keV on tungsten) and for power densities to the limiter within the capabilities of water cooling (30-40 MW/m 2 ); both conditions can be satisfied in the BPNS. Source (a) radiates 0.025 MW/m 2 to the neutron irradiation samples, compared with 5 to 10 MW/m 2 of neutrons; and radiates a total of 0.08 MW from the plasma column, compared with 60 MW of injected power. The particle bombardment that yields source (a) deposits an average of 2.7 MW/m 2 on the samples, within the capabilities of helium gas cooling (10 MW/m 2 ). An additional worst case for source (d) is evaluated for present day 2 to 5 s pulsed neutral beams with 0.1% impurity density and is benchmarked against 2XIIB. The total radiation would increase a factor of 1.5 to ≤ 0.12 MW, supporting the conclusion that impurities will not have a significant impact on a BPN. (author). 61 refs, 7 figs, 2 tabs

  12. Design of a helicon plasma source for ion–ion plasma production

    Energy Technology Data Exchange (ETDEWEB)

    Sharma, N., E-mail: narayan.sharma@cppipr.res.in; Chakraborty, M.; Neog, N.K.; Bandyopadhyay, M.

    2017-04-15

    Highlights: • Development of a helicon plasma system to carry out ion–ion plasma studies in electronegative gases such as Hydrogen, Oxygen and Chlorine. • Determination of initial parameters of helicon plasma source for ion–ion plasma by using dispersion relation of bounded helicon waves. • Design and development of solenoid with magnetic field strength production capability of ∼ 600 G along the axis of the chamber. • Optimization of the chamber parameters using Helic codes and estimation of optimum attainable density. • Estimation of RF power requirements for various gases. - Abstract: A helicon plasma system is being designed and developed at CPP-IPR. The design parameters of the system are deduced from the dispersion relation of bounded helicon waves and the required magnetic fields are simulated by using Poisson Superfish code. The Helic code is used to simulate the power deposition profile for various conditions and to investigate the optimum values of chamber parameters for effective coupling of radio frequency (RF) power to plasma. The helicon source system is aimed at carrying out ion–ion plasma studies in electronegative gases such as Hydrogen, Oxygen and Chlorine. The system mainly consists of a source chamber in which helicon plasma will be produced by injecting RF power at a frequency of 13.56 MHz through a right helical antenna in presence of a DC magnetic field followed by an expansion chamber in which it is expected to produce negative ions along with the positive ions. Installation of the various parts of the system is in progress. The details of the design and development of the system is presented in this article.

  13. Plasma shape control by pulsed solenoid on laser ion source

    International Nuclear Information System (INIS)

    Sekine, M.; Ikeda, S.; Romanelli, M.; Kumaki, M.; Fuwa, Y.; Kanesue, T.; Hayashizaki, N.; Lambiase, R.; Okamura, M.

    2015-01-01

    A Laser ion source (LIS) provides high current heavy ion beams with a very simple mechanical structure. Plasma is produced by a pulsed laser ablation of a solid state target and ions are extracted by an electric field. However, it was difficult to manipulate the beam parameters of a LIS, since the plasma condition could only be adjusted by the laser irradiation condition. To enhance flexibility of LIS operation, we employed a pulsed solenoid in the plasma drift section and investigated the effect of the solenoid field on singly charged iron beams. The experimentally obtained current profile was satisfactorily controlled by the pulsed magnetic field. This approach may also be useful to reduce beam emittance of a LIS

  14. Plasma shape control by pulsed solenoid on laser ion source

    Science.gov (United States)

    Sekine, M.; Ikeda, S.; Romanelli, M.; Kumaki, M.; Fuwa, Y.; Kanesue, T.; Hayashizaki, N.; Lambiase, R.; Okamura, M.

    2015-09-01

    A Laser ion source (LIS) provides high current heavy ion beams with a very simple mechanical structure. Plasma is produced by a pulsed laser ablation of a solid state target and ions are extracted by an electric field. However, it was difficult to manipulate the beam parameters of a LIS, since the plasma condition could only be adjusted by the laser irradiation condition. To enhance flexibility of LIS operation, we employed a pulsed solenoid in the plasma drift section and investigated the effect of the solenoid field on singly charged iron beams. The experimentally obtained current profile was satisfactorily controlled by the pulsed magnetic field. This approach may also be useful to reduce beam emittance of a LIS.

  15. Plasma shape control by pulsed solenoid on laser ion source

    Energy Technology Data Exchange (ETDEWEB)

    Sekine, M. [Tokyo Institute of Technology, Meguro-ku, Tokyo 2-12-1 (Japan); RIKEN, Wako, Saitama 351-0198 (Japan); Ikeda, S. [Tokyo Institute of Technology, Yokohama, Kanagawa 226-8502 (Japan); RIKEN, Wako, Saitama 351-0198 (Japan); Romanelli, M. [Cornell University, Ithaca, NY 14850 (United States); Kumaki, M. [RIKEN, Wako, Saitama 351-0198 (Japan); Waseda University, Shinjuku, Tokyo 169-0072 (Japan); Fuwa, Y. [RIKEN, Wako, Saitama 351-0198 (Japan); Kyoto University, Uji, Kyoto 611-0011 (Japan); Kanesue, T. [Brookhaven National Laboratory, Upton, NY 11973 (United States); Hayashizaki, N. [Tokyo Institute of Technology, Meguro-ku, Tokyo 2-12-1 (Japan); Lambiase, R. [Brookhaven National Laboratory, Upton, NY 11973 (United States); Okamura, M. [RIKEN, Wako, Saitama 351-0198 (Japan); Brookhaven National Laboratory, Upton, NY 11973 (United States)

    2015-09-21

    A Laser ion source (LIS) provides high current heavy ion beams with a very simple mechanical structure. Plasma is produced by a pulsed laser ablation of a solid state target and ions are extracted by an electric field. However, it was difficult to manipulate the beam parameters of a LIS, since the plasma condition could only be adjusted by the laser irradiation condition. To enhance flexibility of LIS operation, we employed a pulsed solenoid in the plasma drift section and investigated the effect of the solenoid field on singly charged iron beams. The experimentally obtained current profile was satisfactorily controlled by the pulsed magnetic field. This approach may also be useful to reduce beam emittance of a LIS.

  16. Plasma diagnostic tools for optimizing negative hydrogen ion sources

    International Nuclear Information System (INIS)

    Fantz, U.; Falter, H.D.; Franzen, P.; Speth, E.; Hemsworth, R.; Boilson, D.; Krylov, A.

    2006-01-01

    The powerful diagnostic tool of optical emission spectroscopy is used to measure the plasma parameters in negative hydrogen ion sources based on the surface mechanism. Results for electron temperature, electron density, atomic-to-molecular hydrogen density ratio, and gas temperature are presented for two types of sources, a rf source and an arc source, which are currently under development for a neutral beam heating system of ITER. The amount of cesium in the plasma volume is obtained from cesium radiation: the Cs neutral density is five to ten orders of magnitude lower than the hydrogen density and the Cs ion density is two to three orders of magnitude lower than the electron density in front of the grid. It is shown that monitoring of cesium lines is very useful for monitoring the cesium balance in the source. From a line-ratio method negative ion densities are determined. In a well-conditioned source the negative ion density is of the same order of magnitude as the electron density and correlates with extracted current densities

  17. Aerosol detection efficiency in inductively coupled plasma mass spectrometry

    Science.gov (United States)

    Hubbard, Joshua A.; Zigmond, Joseph A.

    2016-05-01

    An electrostatic size classification technique was used to segregate particles of known composition prior to being injected into an inductively coupled plasma mass spectrometer (ICP-MS). Size-segregated particles were counted with a condensation nuclei counter as well as sampled with an ICP-MS. By injecting particles of known size, composition, and aerosol concentration into the ICP-MS, efficiencies of the order of magnitude aerosol detection were calculated, and the particle size dependencies for volatile and refractory species were quantified. Similar to laser ablation ICP-MS, aerosol detection efficiency was defined as the rate at which atoms were detected in the ICP-MS normalized by the rate at which atoms were injected in the form of particles. This method adds valuable insight into the development of technologies like laser ablation ICP-MS where aerosol particles (of relatively unknown size and gas concentration) are generated during ablation and then transported into the plasma of an ICP-MS. In this study, we characterized aerosol detection efficiencies of volatile species gold and silver along with refractory species aluminum oxide, cerium oxide, and yttrium oxide. Aerosols were generated with electrical mobility diameters ranging from 100 to 1000 nm. In general, it was observed that refractory species had lower aerosol detection efficiencies than volatile species, and there were strong dependencies on particle size and plasma torch residence time. Volatile species showed a distinct transition point at which aerosol detection efficiency began decreasing with increasing particle size. This critical diameter indicated the largest particle size for which complete particle detection should be expected and agreed with theories published in other works. Aerosol detection efficiencies also displayed power law dependencies on particle size. Aerosol detection efficiencies ranged from 10- 5 to 10- 11. Free molecular heat and mass transfer theory was applied, but

  18. Inductively coupled plasma mass spectrometry (ICP-MS)

    International Nuclear Information System (INIS)

    Shimamura, Tadashi

    1997-01-01

    The period of investigation for the previous general remarks on the progress of ICP-MS was from January, 1991 to September, 1993. In the investigation of this time, for the object of the Chemical Abstracts from January, 1994 to September, 1996, retrieval was carried out by using the STN International. As the key words, ICP-MS, Inductively Coupled Plasma Mass Spectrometry or Inductively Coupled Plasma Mass Spectrometer was used. The number of hit was 373 in 1994, 462 in 1995, and 356 as of September, 1996, 1191 in total. The cumulative number of the papers from 1980 to 1996 is shown. It is known how rapidly the ICP-MS has pervaded as the means of analysis. In order to cope with the enormous number of papers, this time, it was decided to do the review by limiting to the papers which were published in the main journals deeply related to analytical chemistry. As to the tendency in the last three years, it is summarized as how to overcome the spectrum interference and matrix effect in the ICP-MS and the trend of using the ICP-MS as the high sensitivity detector for separation techniques. The technical basic research of the ICP-MS on spectrum interference, sample introduction method and others and the analysis of living body samples are reported. (K.I.)

  19. Fissile mass estimation by pulsed neutron source interrogation

    Energy Technology Data Exchange (ETDEWEB)

    Israelashvili, I., E-mail: israelashvili@gmail.com [Nuclear Research Center of the Negev, P.O.B 9001, Beer Sheva 84190 (Israel); Dubi, C.; Ettedgui, H.; Ocherashvili, A. [Nuclear Research Center of the Negev, P.O.B 9001, Beer Sheva 84190 (Israel); Pedersen, B. [Nuclear Security Unit, Institute for Transuranium Elements, Joint Research Centre, Via E. Fermi, 2749, 21027 Ispra (Italy); Beck, A. [Nuclear Research Center of the Negev, P.O.B 9001, Beer Sheva 84190 (Israel); Roesgen, E.; Crochmore, J.M. [Nuclear Security Unit, Institute for Transuranium Elements, Joint Research Centre, Via E. Fermi, 2749, 21027 Ispra (Italy); Ridnik, T.; Yaar, I. [Nuclear Research Center of the Negev, P.O.B 9001, Beer Sheva 84190 (Israel)

    2015-06-11

    Passive methods for detecting correlated neutrons from spontaneous fissions (e.g. multiplicity and SVM) are widely used for fissile mass estimations. These methods can be used for fissile materials that emit a significant amount of fission neutrons (like plutonium). Active interrogation, in which fissions are induced in the tested material by an external continuous source or by a pulsed neutron source, has the potential advantages of fast measurement, alongside independence of the spontaneous fissions of the tested fissile material, thus enabling uranium measurement. Until recently, using the multiplicity method, for uranium mass estimation, was possible only for active interrogation made with continues neutron source. Pulsed active neutron interrogation measurements were analyzed with techniques, e.g. differential die away analysis (DDA), which ignore or implicitly include the multiplicity effect (self-induced fission chains). Recently, both, the multiplicity and the SVM techniques, were theoretically extended for analyzing active fissile mass measurements, made by a pulsed neutron source. In this study the SVM technique for pulsed neutron source is experimentally examined, for the first time. The measurements were conducted at the PUNITA facility of the Joint Research Centre in Ispra, Italy. First promising results, of mass estimation by the SVM technique using a pulsed neutron source, are presented.

  20. A novel plasma source for sterilization of living tissues

    International Nuclear Information System (INIS)

    Martines, E; Zuin, M; Cavazzana, R; Gazza, E; Serianni, G; Spagnolo, S; Spolaore, M; Leonardi, A; Deligianni, V; Brun, P; Aragona, M; Castagliuolo, I; Brun, P

    2009-01-01

    A source for the production of low-power plasmas at atmospheric pressure, to be used for the nondamaging sterilization of living tissues, is presented. The source, powered by radiofrequency and working with a helium flow, has a specific configuration, studied to prevent the formation of electric arcs dangerous to living matter. It is capable of killing different types of bacteria with a decimal reduction time of 1-2 min; on the contrary, human cells such as conjunctival fibroblasts were found to be almost unharmed by the plasma. A high concentration of OH radicals, likely to be the origin of the sterilizing effect, is detected through their UV emission lines. The effect of the UV and the OH radicals on the fibroblasts was analysed and no significant effects were detected.

  1. Dynamics of ion beam charge neutralization by ferroelectric plasma sources

    Energy Technology Data Exchange (ETDEWEB)

    Stepanov, Anton D.; Gilson, Erik P.; Grisham, Larry R.; Kaganovich, Igor D.; Davidson, Ronald C. [Princeton Plasma Physics Laboratory, Princeton University, P.O. Box 451, Princeton, New Jersey 08543 (United States)

    2016-04-15

    Ferroelectric Plasma Sources (FEPSs) can generate plasma that provides effective space-charge neutralization of intense high-perveance ion beams, as has been demonstrated on the Neutralized Drift Compression Experiment NDCX-I and NDCX-II. This article presents experimental results on charge neutralization of a high-perveance 38 keV Ar{sup +} beam by a plasma produced in a FEPS discharge. By comparing the measured beam radius with the envelope model for space-charge expansion, it is shown that a charge neutralization fraction of 98% is attainable with sufficiently dense FEPS plasma. The transverse electrostatic potential of the ion beam is reduced from 15 V before neutralization to 0.3 V, implying that the energy of the neutralizing electrons is below 0.3 eV. Measurements of the time-evolution of beam radius show that near-complete charge neutralization is established ∼5 μs after the driving pulse is applied to the FEPS and can last for 35 μs. It is argued that the duration of neutralization is much longer than a reasonable lifetime of the plasma produced in the sub-μs surface discharge. Measurements of current flow in the driving circuit of the FEPS show the existence of electron emission into vacuum, which lasts for tens of μs after the high voltage pulse is applied. It is argued that the beam is neutralized by the plasma produced by this process and not by a surface discharge plasma that is produced at the instant the high-voltage pulse is applied.

  2. Magnetosphere of Uranus: plasma sources, convection, and field configuration

    International Nuclear Information System (INIS)

    Voigt, G.; Hill, T.W.; Dessler, A.J.

    1983-01-01

    At the time of the Voyager 2 flyby of Uranus, the planetary rotational axis will be roughly antiparallel to the solar wind flow. If Uranus has a magnetic dipole moment that is approximately aligned with its spin axis, and if the heliospheric shock has not been encountered, we will have the rare opportunity to observe a ''pole-on'' magnetosphere as discussed qualitatively by Siscoe. Qualitative arguments based on analogy with Earth, Jupiter, and Saturn suggest that the magnetosphere of Uranus may lack a source of plasma adequate to produce significant internal currents, internal convection, and associated effects. In order to provide a test of this hypothesis with the forthcoming Voyager measurements, we have constructed a class of approximately self-consistent quantitative magnetohydrostatic equilibrium configurations for a pole-on magnetosphere with variable plasma pressure parameters. Given a few simplifying assumptions, the geometries of the magnetic field and of the tail current sheet can be computed for a given distribution of trapped plasma pressure. The configurations have a single funnel-shaped polar cusp that points directly into the solar wind and a cylindrical tail plasma sheet whose currents close within the tail rather than on the tail magnetopause, and whose length depends on the rate of decrease of thermal plasma pressure down the tail. Interconnection between magnetospheric and interplanetary fields results in a highly asymmetric tail-field configuration. These features were predicted qualtitatively by Siscoe; the quantitative models presented here may be useful in the interpretation of Voyager encounter results

  3. High Current, High Density Arc Plasma as a New Source for WiPAL

    Science.gov (United States)

    Waleffe, Roger; Endrizzi, Doug; Myers, Rachel; Wallace, John; Clark, Mike; Forest, Cary; WiPAL Team

    2016-10-01

    The Wisconsin Plasma Astrophysics Lab (WiPAL) has installed a new array of nineteen plasma sources (plasma guns) on its 3 m diameter, spherical vacuum vessel. Each gun is a cylindrical, molybdenum, washer-stabilized, arc plasma source. During discharge, the guns are maintained at 1.2 kA across 100 V for 10 ms by the gun power supply establishing a high density plasma. Each plasma source is fired independently allowing for adjustable plasma parameters, with densities varying between 1018 -1019 m-3 and electron temperatures of 5-15 eV. Measurements were characterized using a 16 tip Langmuir probe. The plasma source will be used as a background plasma for the magnetized coaxial plasma gun (MCPG), the Terrestrial Reconnection Experiment (TREX), and as the plasma source for a magnetic mirror experiment. Temperature, density, and confinement results will be presented. This work is supported by the DoE and the NSF.

  4. Serum/plasma methylmercury determination by isotope dilution gas chromatography-inductively coupled plasma mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Baxter, Douglas C., E-mail: douglas.baxter@alsglobal.com [ALS Scandinavia AB, Aurorum 10, 977 75 Lulea (Sweden); Faarinen, Mikko [ALS Scandinavia AB, Aurorum 10, 977 75 Lulea (Sweden); Osterlund, Helene; Rodushkin, Ilia [ALS Scandinavia AB, Aurorum 10, 977 75 Lulea (Sweden); Division of Geosciences, Lulea University of Technology, 977 87 Lulea (Sweden); Christensen, Morten [ALS Scandinavia AB, Maskinvaegen 2, 183 53 Taeby (Sweden)

    2011-09-09

    Highlights: {center_dot} We determine methylmercury in serum and plasma using isotope dilution calibration. {center_dot} Separation by gas chromatography and detection by inductively coupled plasma mass spectrometry. {center_dot} Data for 50 specimens provides first reference range for methylmercury in serum. {center_dot} Serum samples shown to be stable for 11 months in refrigerator. - Abstract: A method for the determination of methylmercury in plasma and serum samples was developed. The method uses isotope dilution with {sup 198}Hg-labeled methylmercury, extraction into dichloromethane, back-extraction into water, aqueous-phase ethylation, purge and trap collection, thermal desorption, separation by gas chromatography, and mercury isotope specific detection by inductively coupled plasma mass spectrometry. By spiking 2 mL sample with 1.2 ng tracer, measurements in a concentration interval of (0.007-2.9) {mu}g L{sup -1} could be performed with uncertainty amplification factors <2. A limit of quantification of 0.03 {mu}g L{sup -1} was estimated at 10 times the standard deviation of concentrations measured in preparation blanks. Within- and between-run relative standard deviations were <10% at added concentration levels of 0.14 {mu}g L{sup -1}, 0.35 {mu}g L{sup -1} and 2.8 {mu}g L{sup -1}, with recoveries in the range 82-110%. Application of the method to 50 plasma/serum samples yielded a median (mean; range) concentration of methylmercury of 0.081 (0.091; <0.03-0.19) {mu}g L{sup -1}. This is the first time methylmercury has been directly measured in this kind of specimen, and is therefore the first estimate of a reference range.

  5. Efficient cesiation in RF driven surface plasma negative ion source

    Energy Technology Data Exchange (ETDEWEB)

    Belchenko, Yu.; Ivanov, A.; Konstantinov, S.; Sanin, A., E-mail: sanin@inp.nsk.su; Sotnikov, O. [Budker Institute of Nuclear Physics, Siberian Branch of Russian Academy of Sciences, Novosibirsk (Russian Federation)

    2016-02-15

    Experiments on hydrogen negative ions production in the large radio-frequency negative ion source with cesium seed are described. The system of directed cesium deposition to the plasma grid periphery was used. The small cesium seed (∼0.5 G) provides an enhanced H{sup −} production during a 2 month long experimental cycle. The gradual increase of negative ion yield during the long-term source runs was observed after cesium addition to the source. The degraded H{sup −} production was recorded after air filling to the source or after the cesium washing away from the driver and plasma chamber walls. The following source conditioning by beam shots produces the gradual recovery of H{sup −} yield to the high value. The effect of H{sup −} yield recovery after cesium coverage passivation by air fill was studied. The concept of cesium coverage replenishment and of H{sup −} yield recovery due to sputtering of cesium from the deteriorated layers is discussed.

  6. Invited Article: Characterization of background sources in space-based time-of-flight mass spectrometers

    International Nuclear Information System (INIS)

    Gilbert, J. A.; Gershman, D. J.; Gloeckler, G.; Lundgren, R. A.; Zurbuchen, T. H.; Orlando, T. M.; McLain, J.; Steiger, R. von

    2014-01-01

    For instruments that use time-of-flight techniques to measure space plasma, there are common sources of background signals that evidence themselves in the data. The background from these sources may increase the complexity of data analysis and reduce the signal-to-noise response of the instrument, thereby diminishing the science value or usefulness of the data. This paper reviews several sources of background commonly found in time-of-flight mass spectrometers and illustrates their effect in actual data using examples from ACE-SWICS and MESSENGER-FIPS. Sources include penetrating particles and radiation, UV photons, energy straggling and angular scattering, electron stimulated desorption of ions, ion-induced electron emission, accidental coincidence events, and noise signatures from instrument electronics. Data signatures of these sources are shown, as well as mitigation strategies and design considerations for future instruments

  7. A high efficiency thermal ionization source adapted to mass spectrometers

    International Nuclear Information System (INIS)

    Chamberlin, E.P.; Olivares, J.A.

    1996-01-01

    A tungsten crucible thermal ionization source mounted on a quadrupole mass spectrometer is described. The crucible is a disposable rod with a fine hole bored in one end; it is heated by electron bombardment. The schematic design of the assembly, including water cooling, is described and depicted. Historically, the design is derived from that of ion sources used on ion separators at Los Alamos and Dubna, but the crucible is made smaller and simplified. 10 refs., 4 figs

  8. New high temperature plasmas and sample introduction systems for analytical atomic emission and mass spectrometry

    International Nuclear Information System (INIS)

    Montaser, A.

    1993-01-01

    In this research, new high-temperature plasmas and new sample introduction systems are explored for rapid elemental and isotopic analysis of gases, solutions, and solids using mass spectrometry and atomic emission spectrometry. During the period January 1993--December 1993, emphasis was placed on (a) analytical investigations of atmospheric-pressure helium inductively coupled plasma (He ICP) that are suitable for atomization, excitation, and ionization of elements possessing high excitation and ionization energies; (b) simulation and computer modeling of plasma sources to predict their structure and fundamental and analytical properties without incurring the enormous cost of experimental studies; (c) spectrosopic imaging and diagnostic studies of high-temperature plasmas; (d) fundamental studies of He ICP discharges and argon-nitrogen plasma by high-resolution Fourier transform spectrometry; and (e) fundamental and analytical investigation of new, low-cost devices as sample introduction systems for atomic spectrometry and examination of new diagnostic techniques for probing aerosols. Only the most important achievements are included in this report to illustrate progress and obstacles. Detailed descriptions of the authors' investigations are outlined in the reprints and preprints that accompany this report. The technical progress expected next year is briefly described at the end of this report

  9. Capillary filling of miniaturized sources for electrospray mass spectrometry

    International Nuclear Information System (INIS)

    Arscott, Steve; Gaudet, Matthieu; Brinkmann, Martin; Ashcroft, Alison E; Blossey, Ralf

    2006-01-01

    Capillary slot-based emitter tips are a novel tool for use in electrospray ionization-mass spectrometry of large biomolecules. We have performed a combined theoretical and experimental study of capillary filling in micron-sized slots with the aim of developing a rational design procedure for miniaturized electrospray sources, ultimately enabling the integration of ESI into laboratory-on-a-chip devices

  10. 2MASS Extended Source Catalog: Overview and Algorithms

    Science.gov (United States)

    Jarrett, T.; Chester, T.; Cutri, R.; Schneider, S.; Skrutskie, M.; Huchra, J.

    1999-01-01

    The 2 Micron All-Sky Survey (2MASS)will observe over one-million galaxies and extended Galactic sources covering the entire sky at wavelenghts between 1 and 2 m. Most of these galaxies, from 70 to 80%, will be newly catalogued objetcs.

  11. PWFA plasma source - interferometric diagnostics for Li vapor density measurements

    International Nuclear Information System (INIS)

    Sivakumaran, V.; Mohandas, K.K.; Singh, Sneha; Ravi Kumar, A.V.

    2015-01-01

    A prototype (40 cm long) plasma source based on Li heat pipe oven has been developed for the Plasma Wakefield Acceleration (PWFA) experiments at IPR (IPR), Gujarat as a part of the ongoing Accelerator Programme. Li vapor in the oven is produced by heating solid Li in helium buffer gas. A uniform column of Li plasma is generated by UV photo ionization (193 nm) of the Li vapor in the heat pipe oven. In these experiments, an accurate measurement of Li vapor density is important as it has got a direct consequence on the plasma electron density. In the present experiment, the vapor density is measured optically by using Hook method (spectrally resolved white light interferometry). The hook like structure formed near the vicinity of the Li 670.8 nm resonance line was recorded with a white light Mach Zehnder interferometer crossed with an imaging spectrograph to estimate the Li vapor density. The vapor density measurements have been carried out as a function of external oven temperature and the He buffer gas pressure. This technique has the advantage of being insensitive to line broadening and line shape, and its high dynamic range even with optically thick absorption line. Here, we present the line integrated Lithium vapor density measurement using Hook method and also compare the same with other optical diagnostic techniques (White light absorption and UV absorption) for Li vapor density measurements. (author)

  12. Preliminary Calculation for Plasma Chamber Design of Pulsed Electron Source Based on Plasma

    International Nuclear Information System (INIS)

    Widdi Usada

    2009-01-01

    This paper described the characteristics of pulsed electron sources with anode-cathode distance of 5 cm, electrode diameter of 10 cm, driven by capacitor energy of 25 J. The preliminary results showed that if the system is operated with diode resistance is 1.6 Ω, plasma resistance is 0.14 Ω, and β is 0.94, the achieved of plasma voltage is 640 V, its current is 4.395 kA with its pulse width of 0.8 μsecond. According to breakdown voltage based on Paschen empirical formula, with this achieved voltage, this system could be operated for operation pressure of 1 torr. (author)

  13. Modeling of magnetically enhanced capacitively coupled plasma sources: Ar discharges

    International Nuclear Information System (INIS)

    Kushner, Mark J.

    2003-01-01

    Magnetically enhanced capacitively coupled plasma sources use transverse static magnetic fields to modify the performance of low pressure radio frequency discharges. Magnetically enhanced reactive ion etching (MERIE) sources typically use magnetic fields of tens to hundreds of Gauss parallel to the substrate to increase the plasma density at a given pressure or to lower the operating pressure. In this article results from a two-dimensional hybrid-fluid computational investigation of MERIE reactors with plasmas sustained in argon are discussed for an industrially relevant geometry. The reduction in electron cross field mobility as the magnetic field increases produces a systematic decrease in the dc bias (becoming more positive). This decrease is accompanied by a decrease in the energy and increase in angular spread of the ion flux to the substrate. Similar trends are observed when decreasing pressure for a constant magnetic field. Although for constant power the magnitudes of ion fluxes to the substrate increase with moderate magnetic fields, the fluxes decreased at larger magnetic fields. These trends are due, in part, to a reduction in the contributions of more efficient multistep ionization

  14. Quantitative lipidomic analysis of plasma and plasma lipoproteins using MALDI-TOF mass spectrometry.

    Science.gov (United States)

    Serna, Jorge; García-Seisdedos, David; Alcázar, Alberto; Lasunción, Miguel Ángel; Busto, Rebeca; Pastor, Óscar

    2015-07-01

    Knowledge of the plasma lipid composition is essential to clarify the specific roles of different lipid species in various pathophysiological processes. In this study, we developed an analytical strategy combining high-performance liquid chromatography with evaporative light scattering detection (HPLC-ELSD) and off-line coupling with matrix-assisted laser desorption/ionization with time-of-flight mass spectrometry (MALDI-TOF/MS) to determine the composition of plasma and major lipoproteins at two levels, lipid classes and lipid species. We confirmed the suitability of MALDI-TOF/MS as a quantitative measurement tool studying the linearity and repeatability for triglycerides (TG), phosphatidylethanolamine (PE) and phosphatidylcholine (PC). Moreover, data obtained with this method were correlated with other lipid classes and species measurements using currently available technologies. To establish the potential utility of our approach, human plasma very low density- (VLDL), low density- (LDL) and high density- (HDL) lipoproteins from 10 healthy donors were separated using ultracentrifugation, and compositions of nine lipid classes, cholesteryl esters (CE), TG, free cholesterol (FC), PE, phosphatidylinositol (PI), sulfatides (S), PC, lysophosphatidylcholine (LPC) and sphingomyelin (SM), analyzed. In total, 157 lipid species in plasma, 182 in LDL, 171 in HDL, and 148 in VLDL were quantified. The lipidomic profile was consistent with known differences in lipid classes, but also revealed unexpected differences in lipid species distribution of lipoproteins, particularly for LPC and SM. In summary, the methodology developed in this study constitutes a valid approach to determine the lipidomic composition of plasma and lipoproteins. Copyright © 2015 Elsevier Ireland Ltd. All rights reserved.

  15. A compact and continuously driven supersonic plasma and neutral source

    Energy Technology Data Exchange (ETDEWEB)

    Asai, T.; Itagaki, H.; Numasawa, H.; Terashima, Y.; Hirano, Y. [Department of Physics, College of Science and Technology, Nihon University, Tokyo 101-8308 (Japan); Hirose, A. [Plasma Physics Laboratory, University of Saskatchewan, Saskatoon, Saskatchewan S7N 5E2 (Canada)

    2010-10-15

    A compact and repetitively driven plasma source has been developed by utilizing a magnetized coaxial plasma gun (MCPG) for diagnostics requiring deep penetration of a large amount of neutral flux. The system consists of a MCPG 95mm in length with a DN16 ConFlat connection port and an insulated gate bipolar transistor (IGBT) inverter power unit. The power supply consists of an array of eight IGBT units and is able to switch the discharge on and off at up to 10 kV and 600 A with a maximum repetitive frequency of 10 kHz. Multiple short duration discharge pulses maximize acceleration efficiency of the plasmoid. In the case of a 10 kHz operating frequency, helium-plasmoids in the velocity range of 20 km/s can be achieved.

  16. A compact and continuously driven supersonic plasma and neutral source.

    Science.gov (United States)

    Asai, T; Itagaki, H; Numasawa, H; Terashima, Y; Hirano, Y; Hirose, A

    2010-10-01

    A compact and repetitively driven plasma source has been developed by utilizing a magnetized coaxial plasma gun (MCPG) for diagnostics requiring deep penetration of a large amount of neutral flux. The system consists of a MCPG 95mm in length with a DN16 ConFlat connection port and an insulated gate bipolar transistor (IGBT) inverter power unit. The power supply consists of an array of eight IGBT units and is able to switch the discharge on and off at up to 10 kV and 600 A with a maximum repetitive frequency of 10 kHz. Multiple short duration discharge pulses maximize acceleration efficiency of the plasmoid. In the case of a 10 kHz operating frequency, helium-plasmoids in the velocity range of 20 km/s can be achieved.

  17. A Planar Source of Atmospheric-Pressure Plasma Jet

    Science.gov (United States)

    Zhdanova, O. S.; Kuznetsov, V. S.; Panarin, V. A.; Skakun, V. S.; Sosnin, E. A.; Tarasenko, V. F.

    2018-01-01

    In a single-barrier discharge with voltage sharpening and low gas consumption (up to 1 L/min), plane atmospheric pressure plasma jets with a width of up to 3 cm and length of up to 4 cm in air are formed in the slit geometry of the discharge zone. The energy, temperature, and spectral characteristics of the obtained jets have been measured. The radiation spectrum contains intense maxima corresponding to vibrational transitions of the second positive system of molecular nitrogen N2 ( C 3Π u → B 3Π g ) and comparatively weak transition lines of the first positive system of the N 2 + ion ( B 2Σ u + → X 2Σ g ). By an example of inactivation of the Staphylococcus aureus culture (strain ATCC 209), it is shown that plasma is a source of chemically active particles providing the inactivation of microorganisms.

  18. Soft x-ray source by laser produced Xe plasma

    International Nuclear Information System (INIS)

    Amano, Sho; Masuda, Kazuya; Miyamoto, Shuji; Mochizuki, Takayasu

    2010-01-01

    The laser plasma soft X-ray source in the wavelength rage of 5-17 nm was developed, which consisted of the rotating drum system supplying cryogenic Xe target and the high repetition rate pulse Nd:YAG slab laser. We found the maximum conversion efficiency of 30% and it demonstrated the soft X-ray generation with the high repetition rate pulse of 320 pps and the high average power of 20 W. The soft X-ray cylindrical mirror was developed and successfully focused the soft X-ray with an energy intensity of 1.3 mJ/cm 2 . We also succeeded in the plasma debris mitigation with Ar gas. This will allow a long lifetime of the mirror and a focusing power intensity of 400 mW/cm 2 with 320 pps. The high power soft X-ray is useful for various applications. (author)

  19. Modelling RF-plasma interaction in ECR ion sources

    Directory of Open Access Journals (Sweden)

    Mascali David

    2017-01-01

    Full Text Available This paper describes three-dimensional self-consistent numerical simulations of wave propagation in magnetoplasmas of Electron cyclotron resonance ion sources (ECRIS. Numerical results can give useful information on the distribution of the absorbed RF power and/or efficiency of RF heating, especially in the case of alternative schemes such as mode-conversion based heating scenarios. Ray-tracing approximation is allowed only for small wavelength compared to the system scale lengths: as a consequence, full-wave solutions of Maxwell-Vlasov equation must be taken into account in compact and strongly inhomogeneous ECRIS plasmas. This contribution presents a multi-scale temporal domains approach for simultaneously including RF dynamics and plasma kinetics in a “cold-plasma”, and some perspectives for “hot-plasma” implementation. The presented results rely with the attempt to establish a modal-conversion scenario of OXB-type in double frequency heating inside an ECRIS testbench.

  20. Performance of a plasma opening switch in positive polarity on Gamble I using flashboard plasma sources

    International Nuclear Information System (INIS)

    Renk, T.J.

    1995-01-01

    The successful development of the Plasma Opening Switch (POS) for inductive storage applications has been largely confined to negative polarity operation. Some models of POS behavior suggest that this is because in a positive polarity coaxial configuration, the weaker magnetic field at the cathode position retards the switch opening process. This article describes experiments in which both conductor radii in the POS region were significantly reduced. Anode- and cathode-side current monitors indicate that voltages greater than open-circuit are generated at the POS position, but there is a significant amount of electron flow out of the POS, depending upon load impedance. Flow impedance analysis indicates that a relatively small gap appears in the POS plasma after switch opening. Switch performance is also compared between flashboard and carbon gun plasma sources, with the latter operated both in positive and negative polarity

  1. Improvement of a microwave ECR plasma source for the plasma immersion ion implantation and deposition process

    International Nuclear Information System (INIS)

    Wu Hongchen; Zhang Huafang; Peng Liping; Jiang Yanli; Ma Guojia

    2004-01-01

    The Plasma Immersion Ion Implantation and Deposition (PIII and D) process has many advantages over the pure plasma immersion ion implantation or deposition. It can compensate for or eliminate the disadvantages of the shallow modification layer (for PIII) and increase the bond strength of the coating (of deposition). For this purpose, a new type of microwave plasma source used in the PIII and D process was developed, composed of a vacuum bend wave guide and a special magnetic circuit, so that the coupling window was protected from being deposited with a coating and bombarded by high-energy particles. So the life of the window is increased. To enhance the bonding between the coating and substrate a new biasing voltage is applied to the work piece so that the implantation and deposition (or hybrid process) can be completed in one vacuum cycle

  2. Chemical characterization of materials by inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Deb, S.B.; Nagar, B.K.; Saxena, M.K.; Ramakumar, K.L.

    2009-11-01

    An Inductively Coupled Plasma Mass Spectrometer was procured for trace elemental determination in diverse samples. Since its installation a number of analytical measurements have been carried out on different sample matrices. These include chemical quality control measurements of nuclear fuel and other materials such as uranium metal. Uranium peroxide, ADU, ThO 2 , UO 2 ; isotopic composition of B, Li; chemical characterization of simulated ThO 2 + 2%UO 2 fuel; sodium zirconium phosphate and trace metallic elements in zirconium; Antarctica rock samples and wet phosphoric acid. Necessary separation methodologies required for effective removal of matrix were indigenously developed. In addition, a rigorous analytical protocol, which includes various calibration methodologies such as mass calibration, response calibration, detector cross calibration and linearity check over the entire dynamic range of 109 required for quantitative determination of elements at trace and ultra trace level,, has been standardized. This report summarizes efforts of RACD that have been put in this direction for the application of ICP-MS for analytical measurements. (author)

  3. Production of accelerated electrons near an electron source in the plasma resonance region

    International Nuclear Information System (INIS)

    Fedorov, V.A.

    1989-01-01

    Conditions of generation of plasma electrons accelerated and their characteristics in the vicinity of an electron source are determined. The electron source isolated electrically with infinitely conducting surface, being in unrestricted collisionless plasma ω 0 >>ν, where ω 0 - plasma frequency of nonperturbated plasma, ν - frequency of plasma electron collisions with other plasma particles, is considered. Spherically symmetric injection of electrons, which rates are simulated by ω frequency, occurs from the source surface. When describing phenomena in the vicinity of the electron source, one proceeds from the quasihydrodynamic equation set

  4. Humidity Effects on Fragmentation in Plasma-Based Ambient Ionization Sources.

    Science.gov (United States)

    Newsome, G Asher; Ackerman, Luke K; Johnson, Kevin J

    2016-01-01

    Post-plasma ambient desorption/ionization (ADI) sources are fundamentally dependent on surrounding water vapor to produce protonated analyte ions. There are two reports of humidity effects on ADI spectra. However, it is unclear whether humidity will affect all ADI sources and analytes, and by what mechanism humidity affects spectra. Flowing atmospheric pressure afterglow (FAPA) ionization and direct analysis in real time (DART) mass spectra of various surface-deposited and gas-phase analytes were acquired at ambient temperature and pressure across a range of observed humidity values. A controlled humidity enclosure around the ion source and mass spectrometer inlet was used to create programmed humidity and temperatures. The relative abundance and fragmentation of molecular adduct ions for several compounds consistently varied with changing ambient humidity and also were controlled with the humidity enclosure. For several compounds, increasing humidity decreased protonated molecule and other molecular adduct ion fragmentation in both FAPA and DART spectra. For others, humidity increased fragment ion ratios. The effects of humidity on molecular adduct ion fragmentation were caused by changes in the relative abundances of different reagent protonated water clusters and, thus, a change in the average difference in proton affinity between an analyte and the population of water clusters. Control of humidity in ambient post-plasma ion sources is needed to create spectral stability and reproducibility.

  5. The plasma leptin concentration is closely associated with the body fat mass in nondiabetic uremic patients

    DEFF Research Database (Denmark)

    Clausen, P; Nielsen, P K; Olgaard, K

    1999-01-01

    filtration rate seemed to have a limited influence on the plasma leptin concentration in nondiabetic uremic subjects matched by body fat mass to controls. The plasma leptin concentration was closely associated with the body fat mass, and the leptin level might, therefore, be useful as an indicator of the fat......Plasma leptin is associated with the body mass index and, more precisely, with the body fat mass. Plasma leptin has been found to be elevated in uremic patients. This study aimed at investigating the plasma leptin concentration and associations between plasma leptin, body fat mass, and glomerular.......4 (3.1-59.5) ng/ml versus 5.4 (1.6-47.5) ng/ml (median and range in parentheses; p

  6. When API Mass Spectrometry Meets Super Atmospheric Pressure Ion Sources

    Science.gov (United States)

    Chen, Lee Chuin

    2015-01-01

    In a tutorial paper on the application of free-jet technique for API-MS, John Fenn mentioned that “…for a number of years and a number of reasons, it has been found advantageous in many situations to carry out the ionization process in gas at pressures up to 1000 Torr or more” (Int. J. Mass Spectrom. 200: 459–478, 2000). In fact, the first ESI mass spectrometer constructed by Yamashita and Fenn had a counter-flow curtain gas source at 1050 Torr (ca. 1.4 atm) to sweep away the neutral (J. Phys. Chem. 88: 4451–4459, 1984). For gaseous ionization using electrospray plume, theoretical analysis also shows that “super-atmospheric operation would be more preferable in space-charge-limited situations.”(Int. J. Mass Spectrom. 300: 182–193, 2011). However, electrospray and the corona-based chemical ion source (APCI) in most commercial instrument are basically operated under an atmospheric pressure ambient, perhaps out of the concern of safety, convenience and simplicity in maintenance. Running the ion source at pressure much higher than 1 atm is not so common, but had been done by a number of groups as well as in our laboratory. A brief review on these ion sources will be given in this paper. PMID:26819912

  7. Magnetic insulation of secondary electrons in plasma source ion implantation

    International Nuclear Information System (INIS)

    Rej, D.J.; Wood, B.P.; Faehl, R.J.; Fleischmann, H.H.

    1993-01-01

    The uncontrolled loss of accelerated secondary electrons in plasma source ion implantation (PSII) can significantly reduce system efficiency and poses a potential x-ray hazard. This loss might be reduced by a magnetic field applied near the workpiece. The concept of magnetically-insulated PSII is proposed, in which secondary electrons are trapped to form a virtual cathode layer near the workpiece surface where the local electric field is essentially eliminated. Subsequent electrons that are emitted can then be reabsorbed by the workpiece. Estimates of anomalous electron transport from microinstabilities are made. Insight into the process is gained with multi-dimensional particle-in-cell simulations

  8. Engineering high power induction plasma unit at BARC for mass synthesis of refractory nano-ceramics

    International Nuclear Information System (INIS)

    Ghorui, S.; Sahasrabudhe, S.N.; Dhamale, G.; Das, A.K.

    2013-01-01

    Atmospheric pressure RF thermal plasma sources are gaining increasing importance for production of high purity novel nano-materials in different high-end technological applications. Inherent electrode-less features of the discharge together with the large volume and high energy density of the produced plasma ensures contamination free process environment and mass production ability. Reported herewith is the development of an indigenous induction plasma system for mass synthesis of nanopowders of refractory ceramic materials. The system has been tested for continuous synthesis of Al 2 O 3 nano-powder at a rate of more than 600 gm per hour and checked for its viability for bulk production of nano-particles of other refractory ceramics like Yttrium oxide and Neodymium Oxide. From collected evidences, the process of formation of the nano-particles is identified as the evaporation and subsequent homogeneous nucleation. Major features observed for alumina are complete conversion into highly spherical nano-sized particles, small particle sizes, very narrow size distribution, highly crystallite nature and mixed phases depending on the zone of collection. For alumina, the particles are found to exhibit a uni-modal distribution with peak near 15 nm

  9. Energy efficiency of the CTX magnetized coaxial plasma source

    International Nuclear Information System (INIS)

    Fernandez, J.C.; Barnes, C.W.; Jarboe, T.R.; Knox, S.O.; Platts, D.A.; McKenna, K.F.

    1985-01-01

    The energy efficiency of the CTX coaxial plasma source in creating spheromaks is determined experimentally to be in agreement with the theoretical prediction of lambda/sub sp//lambda/sub g/, where del x B = lambda/sub sp/ B in the spheromak, and lambda/sub g/ identical with μ 0 I/sub g//phi/sub g/ with I/sub g/ the source current and phi/sub g/ the magnetic flux through either source electrode. This is shown to be equivalent to magnetic helicity conservation. The spheromak impurity radiation was measured using an absolutely calibrated single chord bolometer system. The theoretical efficiency is within the experimental uncertainty of the ratio of spheromak radiated energy to source input energy in a group of ''dirty'' discharges. But the radiation measurement uncertainty is too large to determine whether a substantial part of the excess source energy not used in the production of spheromak magnetic energy is radiated from the spheromak volume

  10. Similarity analysis for the high-pressure inductively coupled plasma source

    International Nuclear Information System (INIS)

    Vanden-Abeele, D; Degrez, G

    2004-01-01

    It is well known that the optimal operating parameters of an inductively coupled plasma (ICP) torch strongly depend upon its dimensions. To understand this relationship better, we derive a dimensionless form of the equations governing the behaviour of high-pressure ICPs. The requirement of similarity then naturally leads to expressions for the operating parameters as a function of the plasma radius. In addition to the well-known scaling law for frequency, surprising results appear for the dependence of the mass flow rate, dissipated power and operating pressure upon the plasma radius. While the obtained laws do not appear to be in good agreement with empirical results in the literature, their correctness is supported by detailed numerical calculations of ICP sources of varying diameters. The approximations of local thermodynamic equilibrium and negligible radiative losses restrict the validity of our results and can be responsible for the disagreement with empirical data. The derived scaling laws are useful for the design of new plasma torches and may provide explanations for the unsteadiness observed in certain existing ICP sources

  11. Comprehensive Analysis of Low-Molecular-Weight Human Plasma Proteome Using Top-Down Mass Spectrometry.

    Science.gov (United States)

    Cheon, Dong Huey; Nam, Eun Ji; Park, Kyu Hyung; Woo, Se Joon; Lee, Hye Jin; Kim, Hee Cheol; Yang, Eun Gyeong; Lee, Cheolju; Lee, Ji Eun

    2016-01-04

    While human plasma serves as a great source for disease diagnosis, low-molecular-weight (LMW) proteome (mass spectrometry to analyze the LMW proteoforms present in four types of human plasma samples pooled from three healthy controls (HCs) without immunoaffinity depletion and with depletion of the top two, six, and seven high-abundance proteins. The LMW proteoforms were first fractionated based on molecular weight using gel-eluted liquid fraction entrapment electrophoresis (GELFrEE). Then, the GELFrEE fractions containing up to 30 kDa were subjected to nanocapillary-LC-MS/MS, and the high-resolution MS and MS/MS data were processed using ProSightPC 3.0. As a result, a total of 442 LMW proteins and cleaved products, including those with post-translational modifications and single amino acid variations, were identified. From additional comparative analysis of plasma samples without immunoaffinity depletion between HCs and colorectal cancer (CRC) patients via top-down approach, tens of LMW proteoforms, including platelet factor 4, were found to show >1.5-fold changes between the plasma samples of HCs and CRC patients, and six of the LMW proteins were verified by Western blot analysis.

  12. Optimal pulse modulator design criteria for plasma source ion implanters

    International Nuclear Information System (INIS)

    Reass, W.

    1993-01-01

    This paper describes what are believed to be the required characteristics of a high-voltage modulator for efficient and optimal ion deposition from the ''Plasma Source Ion Implantation'' (PSII) process. The PSII process is a method to chemically or physically alter and enhance surface properties of objects by placing them in a weakly ionized plasma and pulsing the object with a high negative voltage. The attracted ions implant themselves and form chemical bonds or are interstitially mixed with the base material. Present industrial uses of implanted objects tends to be for limited-production, high-value-added items. Traditional implanting hardware uses the typical low-current (ma) semiconductor ''raster scan'' implanters. The targets must also be manipulated to maintain a surface normal to the ion beam. The PSII method can provide ''bulk'' equipment processing on a large industrial scale. For the first generation equipment, currents are scaled from milliamps to hundreds of amps, voltages to -175kV, at kilohertz rep-rates, and high plasma ion densities

  13. Honeycomb surface-plasma negative-ion source

    International Nuclear Information System (INIS)

    Bel'chenko, Yu.I.

    1983-01-01

    A honeycomb surface-plasma source (SPS) of negative hydrogen ions the cathode of which consists of a great number of cells with spherical-concave surfaces, is described. Negative ions, knocked off the cathode by cesium-hydrogen discharge fast particles are accelerated in the near-cathode potential drop layer and focused geometrically on small emission apertures in the anode. Due to this, the gas and energy efficiency of the source is increased and the power density on the cathode is decreased. The H - yield is proportional to the number of celts. A pulse beam of negative ions with current up to 4 A is obtained and accelerated to 25 kV from the cathode effective area of 10.6 cm 2 through emission ports of 0.5 cm 2 total area. The honeycomb SPSs with a greater number of cells are promising as regards obtaining negative ion-beams with the current of scores of amperes

  14. Development of neutral beam source using electron beam excited plasma

    International Nuclear Information System (INIS)

    Hara, Yasuhiro; Hamagaki, Manabu; Mise, Takaya; Hara, Tamio

    2011-01-01

    A low-energy neutral beam (NB) source, which consists of an electron-beam-excited plasma (EBEP) source and two carbon electrodes, has been developed for damageless etching of ultra-large-scale integrated (ULSI) devices. It has been confirmed that the Ar ion beam energy was controlled by the acceleration voltage and the beam profile had good uniformity over the diameter of 80 mm. Dry etching of a Si wafer at the floating potential has been carried out by Ar NB. Si sputtering yield by an Ar NB clearly depends on the acceleration voltage. This result shows that the NB has been generated through the charge exchange reaction from the ion beam in the process chamber. (author)

  15. Simulation of a dense plasma focus x-ray source

    International Nuclear Information System (INIS)

    Stark, R.A.

    1994-01-01

    The authors are performing simulations of the magnetohydrodynamics of a Dense Plasma Focus (DPF) x-ray source located at Science Research Laboratory (SRL), Alameda, CA, in order to optimize its performance. The SRL DPF, which was developed as a compact source for x-ray lithography, operates at 20 Hz, giving x-ray power (9--14 Angstroms) of 500 W using neon gas. The simulations are performed with the two dimensional MHD code MACH2, developed by Mission Research Corporation, with a steady state corona model as the equation of state. The results of studies of the sensitivity of x-ray output to charging voltage and current, and to initial gas density will be presented. These studies should indicate ways to optimize x-ray production efficiency. Simulations of various inner electrode configurations will also be presented

  16. Limit of detection in the presence of instrumental and non-instrumental errors: study of the possible sources of error and application to the analysis of 41 elements at trace levels by inductively coupled plasma-mass spectrometry technique

    International Nuclear Information System (INIS)

    Badocco, Denis; Lavagnini, Irma; Mondin, Andrea; Tapparo, Andrea; Pastore, Paolo

    2015-01-01

    In this paper the detection limit was estimated when signals were affected by two error contributions, namely instrumental errors and operational-non-instrumental errors. The detection limit was theoretically obtained following the hypothesis testing schema implemented with the calibration curve methodology. The experimental calibration design was based on J standards measured I times with non-instrumental errors affecting each standard systematically but randomly among the J levels. A two-component variance regression was performed to determine the calibration curve and to define the detection limit in these conditions. The detection limit values obtained from the calibration at trace levels of 41 elements by ICP-MS resulted larger than those obtainable from a one component variance regression. The role of the reagent impurities on the instrumental errors was ascertained and taken into account. Environmental pollution was studied as source of non-instrumental errors. The environmental pollution role was evaluated by Principal Component Analysis technique (PCA) applied to a series of nine calibrations performed in fourteen months. The influence of the seasonality of the environmental pollution on the detection limit was evidenced for many elements usually present in the urban air particulate. The obtained results clearly indicated the need of using the two-component variance regression approach for the calibration of all the elements usually present in the environment at significant concentration levels. - Highlights: • Limit of detection was obtained considering a two variance component regression. • Calibration data may be affected by instrumental and operational conditions errors. • Calibration model was applied to determine 41 elements at trace level by ICP-MS. • Non instrumental errors were evidenced by PCA analysis

  17. Electron backstream to the source plasma region in an ion source

    International Nuclear Information System (INIS)

    Ohara, Y.; Akiba, M.; Arakawa, Y.; Okumura, Y.; Sakuraba, J.

    1980-01-01

    The flux of backstream electrons to the source plasma region increases significantly with the acceleration voltage of an ion beam, so that the back plate in the arc chamber should be broken for quasi-dc operation. The flux of backstream electrons is estimated at the acceleration voltage of 50--100 kV for a proton beam with the aid of ion beam simulation code. The power flux of backstream electrons is up to about 7% of the total beam output at the acceleration voltage of 75 kV. It is pointed out that the conventional ion sources such as the duoPIGatron or the bucket source which use a magnetic field for source plasma production are not suitable for quasi-dc and high-energy ion sources, because the surface heat flux of the back plate is increased by the focusing of backstream electrons and the removal of it is quite difficult. A new ion source which has an electron beam dump in the arc chamber is proposed

  18. Effect of Skimmer Cone Material on the Spectra of Inductively Coupled Plasma Mass Spectrometry

    International Nuclear Information System (INIS)

    Amr, M.A.; Zahran, N.F.; Helal, A.I.

    2002-01-01

    The inductively coupled plasma ion source for mass spectrometry is very sensitive for multielement analysis with detection limits down to sub part per trillion (ppt). Polyatomic ions which could be formed in the mass spectra may interfere in the analysis of some element. Experimental conditions have great influences on the formation of polyatomic ions. The present work demonstrates that the skimmer materials (Au, Ag, Ni, and Cu) are participating in the formation of polyatomic ions, meanwhile the sampler materials have no real effect. The mechanism of formation of polyatomic ions is explained. Heats of formation of polyatomic species formed from the skimmer materials such as: Au X, Ag X, Ni X and Cu X; where X= Ar, O, N, C and H are calculated by Gaussian program (G 94 W)

  19. A high-current pulsed cathodic vacuum arc plasma source

    International Nuclear Information System (INIS)

    Oates, T.W.H.; Pigott, J.; Mckenzie, D.R.; Bilek, M.M.M.

    2003-01-01

    Cathodic vacuum arcs (CVAs) are well established as a method for producing metal plasmas for thin film deposition and as a source of metal ions. Fundamental differences exist between direct current (dc) and pulsed CVAs. We present here results of our investigations into the design and construction of a high-current center-triggered pulsed CVA. Power supply design based on electrolytic capacitors is discussed and optimized based on obtaining the most effective utilization of the cathode material. Anode configuration is also discussed with respect to the optimization of the electron collection capability. Type I and II cathode spots are observed and discussed with respect to cathode surface contamination. An unfiltered deposition rate of 1.7 nm per pulse, at a distance of 100 mm from the source, has been demonstrated. Instantaneous plasma densities in excess of 1x10 19 m -3 are observed after magnetic filtering. Time averaged densities an order of magnitude greater than common dc arc densities have been demonstrated, limited by pulse repetition rate and filter efficiency

  20. The gridless plasma ion source (GIS) for plasma ion assisted optical coating

    International Nuclear Information System (INIS)

    You Dawei; Li Xiaoqian; Wang Yu; Lin Yongchang

    2004-01-01

    High-quality optical coating is a key technology for modern optics. Ion-assisted deposition technology was used to improve the vaporized coating in 1980's. The GIS (gridless ion source), which is an advanced plasma source for producing a high-quality optical coating in large area, can produce a large area uniformity>1000 mm (diameter), a high ion current density ∼0.5 mA/cm 2 , 20 eV-200 eV energetic plasma ions and can activate reactive gas and film atoms. Now we have developed a GIS system. The GIS and the plasma ion-assisted deposition technology are investigated to achieve a high-quality optical coating. The GIS is a high power and high current source with a power of 1 kW-7.5 kW, a current of 10 A- 70 A and an ion density of 200 μA/cm 2 -500 μA/cm 2 . Because of the special magnetic structure, the plasma-ion extraction efficiency has been improved to obtain a maximum ion density of 500 μA/cm 2 in the medium power (∼4 kW) level. The GIS applied is of a special cathode structure, so that the GIS operation can be maintained under a rather low power and the lifetime of cathode will be extended. The GIS has been installed in the LPSX-1200 type box coating system. The coated TiO 2 , SiO 2 films such as antireflective films with the system have the same performance reported by Leybold Co, 1992, along with a controllable refractive index and film structure. (authors)

  1. Abstracts of international symposium on heat and mass transfer under plasma conditions

    International Nuclear Information System (INIS)

    1994-01-01

    The international symposium on heat and mass transfer under plasma conditions was held on 4-8 July 1994 in Cesme, Izmir, Turkey. The spesialists discussed heat and mass transfer in the field of plasma processing at the meeting. More than 70 papers were presented in the meeting

  2. Abstracts of international symposium on heat and mass transfer under plasma conditions

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    1994-12-31

    The international symposium on heat and mass transfer under plasma conditions was held on 4-8 July 1994 in Cesme, Izmir, Turkey. The spesialists discussed heat and mass transfer in the field of plasma processing at the meeting. More than 70 papers were presented in the meeting.

  3. Positive-column plasma studied by fast-flow glow discharge mass spectrometry: Could it be a 'Rydberg gas?'

    International Nuclear Information System (INIS)

    Mason, Rod S.; Miller, Pat D.; Mortimer, Ifor; Mitchell, David J.; Dash, Neil A.

    2003-01-01

    Ions created from the fast-flowing positive column plasma of a glow discharge were monitored using a high voltage magnetic sector mass spectrometer. Since the field gradient and sheath potentials created by the plasma inside the source opposed cation transfer, it is inferred that the ions detected were the field-ionized Rydberg species. This is supported by the mass spectral changes which occurred when a negative bias was applied to the sampling aperture and by the contrasting behavior when attached to a quadrupole analyzer. Reaction with H 2 (titrated into the flowing plasma) quenched not only the ionization of discharge gas Rydberg atoms but also the passage of electric current through the plasma, without significant changes to the field and sheath potentials. Few 'free' ions were present and the lifetimes of the Rydberg atoms detected were much longer than seen in lower pressure experiments, indicating additional stabilization in the plasma environment. The observations support the model of the flowing plasma, given previously [R. S. Mason, P. D. Miller, and I. P. Mortimer, Phys. Rev. E 55, 7462 (1997)] as mainly a neutral Rydberg atom gas, rather than a conventional ion-electron plasma

  4. Theory for beam-plasma millimeter-wave radiation source experiments

    International Nuclear Information System (INIS)

    Rosenberg, M.; Krall, N.A.

    1989-01-01

    This paper reports on theoretical studies for millimeter-wave plasma source experiments. In the device, millimeter-wave radiation is generated in a plasma-filled waveguide driven by counter-streaming electron beams. The beams excite electron plasma waves which couple to produce radiation at twice the plasma frequency. Physics topics relevant to the high electron beam current regime are discussed

  5. Uranium quantification in semen by inductively coupled plasma mass spectrometry

    Science.gov (United States)

    Todorov, Todor I.; Ejnik, John W.; Guandalini, Gustavo S.; Xu, Hanna; Hoover, Dennis; Anderson, Larry W.; Squibb, Katherine; McDiarmid, Melissa A.; Centeno, Jose A.

    2013-01-01

    In this study we report uranium analysis for human semen samples. Uranium quantification was performed by inductively coupled plasma mass spectrometry. No additives, such as chymotrypsin or bovine serum albumin, were used for semen liquefaction, as they showed significant uranium content. For method validation we spiked 2 g aliquots of pooled control semen at three different levels of uranium: low at 5 pg/g, medium at 50 pg/g, and high at 1000 pg/g. The detection limit was determined to be 0.8 pg/g uranium in human semen. The data reproduced within 1.4–7% RSD and spike recoveries were 97–100%. The uranium level of the unspiked, pooled control semen was 2.9 pg/g of semen (n = 10). In addition six semen samples from a cohort of Veterans exposed to depleted uranium (DU) in the 1991 Gulf War were analyzed with no knowledge of their exposure history. Uranium levels in the Veterans’ semen samples ranged from undetectable (<0.8 pg/g) to 3350 pg/g. This wide concentration range for uranium in semen is consistent with known differences in current DU body burdens in these individuals, some of whom have retained embedded DU fragments.

  6. Polyatomic ions in inductively coupled plasma-mass spectrometry

    International Nuclear Information System (INIS)

    Ferguson, Jill Wisnewski; Dudley, Timothy J.; Sears, Kyle C.; McIntyre, Sally M.; Gordon, Mark S.; Houk, R.S.

    2009-01-01

    Several polyatomic ions in inductively coupled plasma-mass spectrometry are studied experimentally and by computational methods. Novel calculations based on spin-restricted open shell second order perturbation theory (ZAPT2) and coupled cluster (CCSD(T)) theory are performed to determine the energies, structures and partition functions of the ions. These values are combined with experimental data to evaluate a dissociation constant and gas kinetic temperature (T gas ) value. In our opinion, the resulting T gas value can sometimes be interpreted to deduce the location where the polyatomic ion of interest is generated. The dissociation of N 2 H + to N 2 + leads to a calculated T gas of 4550 to 4900 K, depending on the computational data used. The COH + to CO + system yields a similar temperature, which is not surprising considering the similar energies and structures of COH + and N 2 H + . The dissociation of H 2 CO + to HCO + leads to a much lower T gas ( 2 COH + to HCOH + generates a T gas value between those from the other H x CO + ions studied here. All of these measured T gas values correspond to formation of extra polyatomic ion in the interface or extraction region. The computations reveal the existence of isomers such as HCO + and COH + , and H 2 CO + and HCOH + , which have virtually the same m/z values and need to be considered in the interpretation of results.

  7. Charge modes of pulsed high energy and high density plasma injection source

    International Nuclear Information System (INIS)

    Cheng, D.Y.

    1974-01-01

    Detonation (snowplow), deflagration and other modes of discharge can be produced in a single coaxial plasma gun. Conservation laws of mass, momentum and energy together with the entropy production condition of the discharge phenomena are used to identify dense discharge modes. The Rankine-Hugoniot relation for a magnetized plasma is derived. Discussions of how to design a deflagration plasma gun to yield a prescribed plasma kinetic energy and plasma beam density are given

  8. Applications of inductively coupled plasma mass spectrometry and laser ablation inductively coupled plasma mass spectrometry in materials science

    International Nuclear Information System (INIS)

    Becker, Johanna Sabine

    2002-01-01

    Inductively coupled plasma mass spectrometry (ICP-MS) and laser ablation ICP-MS (LA-ICP-MS) have been applied as the most important inorganic mass spectrometric techniques having multielemental capability for the characterization of solid samples in materials science. ICP-MS is used for the sensitive determination of trace and ultratrace elements in digested solutions of solid samples or of process chemicals (ultrapure water, acids and organic solutions) for the semiconductor industry with detection limits down to sub-picogram per liter levels. Whereas ICP-MS on solid samples (e.g. high-purity ceramics) sometimes requires time-consuming sample preparation for its application in materials science, and the risk of contamination is a serious drawback, a fast, direct determination of trace elements in solid materials without any sample preparation by LA-ICP-MS is possible. The detection limits for the direct analysis of solid samples by LA-ICP-MS have been determined for many elements down to the nanogram per gram range. A deterioration of detection limits was observed for elements where interferences with polyatomic ions occur. The inherent interference problem can often be solved by applying a double-focusing sector field mass spectrometer at higher mass resolution or by collision-induced reactions of polyatomic ions with a collision gas using an ICP-MS fitted with collision cell. The main problem of LA-ICP-MS is quantification if no suitable standard reference materials with a similar matrix composition are available. The calibration problem in LA-ICP-MS can be solved using on-line solution-based calibration, and different procedures, such as external calibration and standard addition, have been discussed with respect to their application in materials science. The application of isotope dilution in solution-based calibration for trace metal determination in small amounts of noble metals has been developed as a new calibration strategy. This review discusses new

  9. Discharge plasmas as EUV Sources for Future Micro Lithography

    Science.gov (United States)

    Kruecken, Thomas

    2007-08-01

    Future extreme ultraviolet (EUV) lithography will require very high radiation intensities in a narrow wavelength range around 13.5 nm, which is most efficiently emitted as line radiation by highly ionized heavy particles. Currently the most intense EUV sources are based on xenon or tin gas discharges. After having investigated the limits of a hollow cathode triggered xenon pinch discharge Philips Extreme UV favors a laser triggered tin vacuum spark discharge. Plasma and radiation properties of these highly transient discharges will be compared. Besides simple MHD-models the ADAS software package has been used to generate important atomic and spectral data of the relevant ion stages. To compute excitation and radiation properties, collisional radiative equilibria of individual ion stages are computed. For many lines opacity effects cannot be neglected. In the xenon discharges the optical depths allow for a treatment based on escape factors. Due to the rapid change of plasma parameters the abundancies of the different ionization stages must be computed dynamically. This requires effective ionization and recombination rates, which can also be supplied by ADAS. Due to very steep gradients (up to a couple orders of magnitude per mm) the plasma of tin vacuum spark discharges is very complicated. Therefore we shall describe here only some technological aspects of our tin EUV lamp: The electrode system consists of two rotating which are pulled through baths of molten tin such that a tin film remains on their surfaces. With a laser pulse some tin is ablated from one of the wheels and travels rapidly through vacuum towards the other rotating wheel. When the tin plasma reaches the other electrodes it ignites and the high current phase starts, i.e. the capacitor bank is unloaded, the plasma is pinched and EUV is radiated. Besides the good spectral properties of tin this concept has some other advantages: Erosion of electrodes is no severe problem as the tin film is

  10. Dynamic sheath studies in plasma source ion implantation

    International Nuclear Information System (INIS)

    Schever, J.T.; Shamim, M.; Conrad, J.R.

    1990-01-01

    Plasma Source Ion Implantation (PSII) is a non-line-of-sight method for materials processing in which a target is immersed in a plasma and pulse biased to a high negative voltage (∼ 50 kV). A model of the dynamic sheath which forms under these conditions has been developed and applied to planar, cylindrical and spherical geometries. This model assumes that the transient sheath obeys the Child-Langmuir law for space charge limited emission at each instant during the propagation. Ions uncovered by the propagating sheath edge supply the space charge limited current. This yields an equation relating sheath edge velocity to position, which can be integrated to obtain the sheath edge position as a function of time. The same procedure used in cylindrical and spherical geometry results in a similar equation which must be integrated numerically. Comparison of results of experimental measurements, our model and simulation will be presented for the dynamic sheath edge position and target current waveform. Measurements of implanted dose uniformity of wedge shaped targets are also presented

  11. Note: Triggering behavior of a vacuum arc plasma source

    Energy Technology Data Exchange (ETDEWEB)

    Lan, C. H., E-mail: lanchaohui@163.com; Long, J. D.; Zheng, L.; Dong, P.; Yang, Z.; Li, J.; Wang, T.; He, J. L. [Institute of Fluid Physics, China Academy of Engineering Physics, Mianyang 621900 (China)

    2016-08-15

    Axial symmetry of discharge is very important for application of vacuum arc plasma. It is discovered that the triggering method is a significant factor that would influence the symmetry of arc discharge at the final stable stage. Using high-speed multiframe photography, the transition processes from cathode-trigger discharge to cathode-anode discharge were observed. It is shown that the performances of the two triggering methods investigated are quite different. Arc discharge triggered by independent electric source can be stabilized at the center of anode grid, but it is difficult to achieve such good symmetry through resistance triggering. It is also found that the triggering process is highly correlated to the behavior of emitted electrons.

  12. Mass transfer in stellar X-ray sources

    International Nuclear Information System (INIS)

    Verbunt, F.

    1982-01-01

    This thesis deals with mass transfer in the binary stars that emit X-rays. Optical observations on two sources are presented: 2A0311-227 and Cen X-4. The transferred matter will often enter a gaseous disk around the compact star, and spiral inwards slowly through this disk. The conditions for the formation of such a disk are investigated and the equations governing its structure are presented. Different models are discussed and it is concluded that different models lead to very similar results for those regions of the disk where gas pressure is more important than radiative pressure, and that these results agree fairly well with observations. No consistent model has been constructed as yet for the region where radiative pressure is dominant. Theoretically one predicts that the optical light emitted by a disk around a neutron star is mainly caused by X-ray photons from the immediate surroundings of the neutron star that hit the outer disk surface, are absorbed, thermalised, and re-emitted in the optical and ultraviolet regions of the spectrum. This expectation is verified by comparison with the collected observational data of low-mass X-ray binaries. Finally the author investigates which mechanism is responsible for the mass transfer in systems where the mass-losing star is less massive than the sun. (Auth.)

  13. An improved barium plasma source for q-machines

    International Nuclear Information System (INIS)

    Paris, P.J.; Gorgerat, P.; Simik, A.; Rynn, N.; Roe, S.; Schleipen, M.

    1988-06-01

    We have developed a stable q-machine with well determined parameters for long term times, of constant plasma density and temperature. The plasma characteristics and gun behaviour allow research in fundamental plasma physics, especially with the use of non perturbing powerful optical (LIF) diagnostics in the determination of many of the plasma parameters. (author) 17 figs., 2 tabs., 7 refs

  14. Study on surface modification of polymer films by using atmospheric plasma jet source

    International Nuclear Information System (INIS)

    Takemura, Yuichiro; Hara, Tamio; Yamaguchi, Naohiro

    2008-01-01

    Reactive gas plasma treatments of poly(ethylene terephthalate) (PET) and polyimide (Kapton) have been performed using an atmospheric plasmas jet source. Characteristics of surface modification have been examined by changing the distance between the plasma jet source and the treated sample, and by changing the working gas spaces. Simultaneously, each plasma jet source has been investigated by space-resolving spectroscopy in the UV/visible region. Polymer surfaces have been analyzed by X-ray photoelectron spectroscopy (XPS). A marked improvement in the hydrophilicity of the polymer surfaces has been made by using N 2 or O 2 plasma jet source with a very short exposure time of about 0.01 s, whereas the less improvement has been obtained using on air plasma jet source because of NO x compound production. Changes in the chemical states of C of the polymer surfaces have been observed in XPS spectra after N 2 plasma jet spraying. (author)

  15. Plasma focus as an heavy ion source in the problem of heavy ion fusion

    International Nuclear Information System (INIS)

    Gribkov, V.A.; Dubrovskij, A.V.; Kalachev, N.V.; Krokhin, O.N.; Silin, P.V.; Nikulin, V.Ya.; Cheblukov, Yu.N.

    1984-01-01

    Results of experiments on the ion flux formation in a plasma focus (PF) to develop a multicharged ion source for thermonuclear facility driver are presented. In plasma focus accelerating section copper ions were injected. Advantages of the suggested method of ion beam formation are demonstrated. Beam emittance equalling < 0.1 cmxmrad is obtained. Plasma focus ion energy exceeds 1 MeV. Plasma focus in combination with a neodymium laser is thought to be a perspective ion source for heavy ion fusion

  16. Nitrogen capillary plasma as a source of intense monochromatic radiation at 2.88 nm

    Energy Technology Data Exchange (ETDEWEB)

    Vrba, P., E-mail: vrbovmir@fbmi.cvut.cz [Institute of Plasma Physics, Academy of Sciences, Za Slovankou 3, Prague 8 (Czech Republic); Vrbova, M. [Faculty of Biomedical Engineering, CTU in Prague, Sitna 3105, Kladno 2 (Czech Republic); Zakharov, S.V. [EPPRA sas, Villebon/Yvette (France); Zakharov, V.S. [EPPRA sas, Villebon/Yvette (France); KIAM RAS, Moscow (Russian Federation); Jancarek, A.; Nevrkla, M. [Faculty of Nuclear Science and Physical Engineering, CTU in Prague, Brehova 7, Prague 1 (Czech Republic)

    2014-10-15

    Highlights: • Pinching capillary discharge is studied as a source of monochromatic SXR. • Modeling of the laboratory device was performed by RMHD Z* code. • Results of computer and laboratory experiments are presented. - Abstract: Capillary discharge plasma related to our laboratory device is modeled and the results are compared with experimental data. Time dependences of selected plasma quantities (e.g. plasma mass density, electron temperature and density and emission intensities) evaluated by 2D Radiation-Magneto-Hydro-Dynamic code Z* describe plasma evolution. The highest output pulse energy at 2.88 nm wavelength is achieved for nitrogen filling pressure ∼100 Pa. The estimated output energy of monochromatic radiation 5.5 mJ sr{sup −1} (∼10{sup 14} photons sr{sup −1}) corresponds properly to observe experimental value ∼3 × 10{sup 13} photons sr{sup −1}. Ray tracing inspection along the capillary axis proves an influence of radiation self-absorption for the investigated wavelength. The spectra, evaluated using the FLY code, agree to the measured ones.

  17. Real-time breath analysis with active capillary plasma ionization-ambient mass spectrometry.

    Science.gov (United States)

    Bregy, Lukas; Sinues, Pablo Martinez-Lozano; Nudnova, Maryia M; Zenobi, Renato

    2014-06-01

    On-line analysis of exhaled human breath is a growing area in analytical science, for applications such as fast and non-invasive medical diagnosis and monitoring. In this work, we present a novel approach based on ambient ionization of compounds in breath and subsequent real-time mass spectrometric analysis. We introduce a plasma ionization source for this purpose, which has no need for additional gases, is very small, and is easily interfaced with virtually any commercial atmospheric pressure ionization mass spectrometer (API-MS) without major modifications. If an API-MS instrument exists in a laboratory, the cost to implement this technology is only around [Formula: see text]500, far less than the investment for a specialized mass spectrometric system designed for volatile organic compounds (VOCs) analysis. In this proof-of-principle study we were able to measure mass spectra of exhaled human breath and found these to be comparable to spectra obtained with other electrospray-based methods. We detected over 100 VOCs, including relevant metabolites like fatty acids, with molecular weights extending up to 340 Da. In addition, we were able to monitor the time-dependent evolution of the peaks and show the enhancement of the metabolism after a meal. We conclude that this approach may complement current methods to analyze breath or other types of vapors, offering an affordable option to upgrade any pre-existing API-MS to a real-time breath analyzer.

  18. Design of a novel high efficiency antenna for helicon plasma sources

    Science.gov (United States)

    Fazelpour, S.; Chakhmachi, A.; Iraji, D.

    2018-06-01

    A new configuration for an antenna, which increases the absorption power and plasma density, is proposed for helicon plasma sources. The influence of the electromagnetic wave pattern symmetry on the plasma density and absorption power in a helicon plasma source with a common antenna (Nagoya) is analysed by using the standard COMSOL Multiphysics 5.3 software. In contrast to the theoretical model prediction, the electromagnetic wave does not represent a symmetric pattern for the common Nagoya antenna. In this work, a new configuration for an antenna is proposed which refines the asymmetries of the wave pattern in helicon plasma sources. The plasma parameters such as plasma density and absorption rate for a common Nagoya antenna and our proposed antenna under the same conditions are studied using simulations. In addition, the plasma density of seven operational helicon plasma source devices, having a common Nagoya antenna, is compared with the simulation results of our proposed antenna and the common Nagoya antenna. The simulation results show that the density of the plasma, which is produced by using our proposed antenna, is approximately twice in comparison to the plasma density produced by using the common Nagoya antenna. In fact, the simulation results indicate that the electric and magnetic fields symmetry of the helicon wave plays a vital role in increasing wave-particle coupling. As a result, wave-particle energy exchange and the plasma density of helicon plasma sources will be increased.

  19. On the possibility of the multiple inductively coupled plasma and helicon plasma sources for large-area processes

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Jin-Won; Lee, Yun-Seong, E-mail: leeeeys@kaist.ac.kr; Chang, Hong-Young [Low-temperature Plasma Laboratory, Department of Physics, Korea Advanced Institute of Science and Technology, Daejeon 305-701 (Korea, Republic of); An, Sang-Hyuk [Agency of Defense Development, Yuseong-gu, Daejeon 305-151 (Korea, Republic of)

    2014-08-15

    In this study, we attempted to determine the possibility of multiple inductively coupled plasma (ICP) and helicon plasma sources for large-area processes. Experiments were performed with the one and two coils to measure plasma and electrical parameters, and a circuit simulation was performed to measure the current at each coil in the 2-coil experiment. Based on the result, we could determine the possibility of multiple ICP sources due to a direct change of impedance due to current and saturation of impedance due to the skin-depth effect. However, a helicon plasma source is difficult to adapt to the multiple sources due to the consistent change of real impedance due to mode transition and the low uniformity of the B-field confinement. As a result, it is expected that ICP can be adapted to multiple sources for large-area processes.

  20. Ion source memory in {sup 36}Cl accelerator mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Pavetich, Stefan; Akhmadaliev, Shavkat; Merchel, Silke; Rugel, Georg [HZDR, Dresden (Germany); Arnold, Maurice; Aumaitre, Georges; Bourles, Didier; Martschini, Martin [ASTER, Aix-en-Provence (France); Buchriegler, Josef; Golser, Robin; Keddadouche, Karim; Steier, Peter [VERA, Vienna (Austria)

    2013-07-01

    Since the DREAMS (Dresden Accelerator Mass Spectrometry) facility went operational in 2011, constant effort was put into enabling routine measurements of long-lived radionuclides as {sup 10}Be, {sup 26}Al and {sup 41}Ca. For precise AMS-measurements of the volatile element Cl the key issue is the minimization of the long term memory effect. For this purpose one of the two original HVE sources was mechanically modified, allowing the usage of bigger cathodes with individual target apertures. Additionally a more open geometry was used to improve the vacuum level. To evaluate this improvement in comparison to other up-to-date ion sources, a small inter-laboratory comparison had been initiated. The long-term memory effect in the Cs sputter ion sources of the AMS facilities VERA, ASTER and DREAMS had been investigated by running samples of natural {sup 35}Cl/{sup 37}Cl-ratio and samples containing highly enriched {sup 35}Cl({sup 35}Cl/{sup 37}Cl > 500). Primary goals of the research are the time constants of the recovery from the contaminated sample ratio to the initial ratio of the sample and the level of the long-term memory effect in the sources.

  1. Aerosol Vacuum-Assisted Plasma Ionization (Aero-VaPI) Coupled to Ion Mobility-Mass Spectrometry

    Science.gov (United States)

    Blair, Sandra L.; Ng, Nga L.; Zambrzycki, Stephen C.; Li, Anyin; Fernández, Facundo M.

    2018-02-01

    In this communication, we report on the real-time analysis of organic aerosol particles by Vacuum-assisted Plasma Ionization-Mass Spectrometry (Aero-VaPI-MS) using a home-built VaPI ion source coupled to a Synapt G2-S HDMS ion mobility-mass spectrometry (IM-MS) system. Standards of organic molecules of interest in prebiotic chemistry were used to generate aerosols. Monocaprin and decanoic acid aerosol particles were successfully detected in both the positive and negative ion modes, respectively. A complex aerosol mixture of different sizes of polymers of L-malic acid was also examined through ion mobility (IM) separations, resulting in the detection of polymers of up to eight monomeric units. This noncommercial plasma ion source is proposed as a low cost alternative to other plasma ionization platforms used for aerosol analysis, and a higher-performance alternative to more traditional aerosol mass spectrometers. VaPI provides robust online ionization of organics in aerosols without extensive ion activation, with the coupling to IM-MS providing higher peak capacity and excellent mass accuracy. [Figure not available: see fulltext.

  2. An ion source for radiofrequency-pulsed glow discharge time-of-flight mass spectrometry

    International Nuclear Information System (INIS)

    González Gago, C.; Lobo, L.; Pisonero, J.; Bordel, N.; Pereiro, R.; Sanz-Medel, A.

    2012-01-01

    A Grimm-type glow discharge (GD) has been designed and constructed as an ion source for pulsed radiofrequency GD spectrometry when coupled to an orthogonal time of flight mass spectrometer. Pulse shapes of argon species and analytes were studied as a function of the discharge conditions using a new in-house ion source (UNIOVI GD) and results have been compared with a previous design (PROTOTYPE GD). Different behavior and shapes of the pulse profiles have been observed for the two sources evaluated, particularly for the plasma gas ionic species detected. In the more analytically relevant region (afterglow), signals for 40 Ar + with this new design were negligible, while maximum intensity was reached earlier in time for 41 (ArH) + than when using the PROTOTYPE GD. Moreover, while maximum 40 Ar + signals measured along the pulse period were similar in both sources, 41 (ArH) + and 80 (Ar 2 ) + signals tend to be noticeable higher using the PROTOTYPE chamber. The UNIOVI GD design was shown to be adequate for sensitive direct analysis of solid samples, offering linear calibration graphs and good crater shapes. Limits of detection (LODs) are in the same order of magnitude for both sources, although the UNIOVI source provides slightly better LODs for those analytes with masses slightly higher than 41 (ArH) + . - Highlights: ► A new RF-pulsed GD ion source (UNIOVI GD) coupled to TOFMS has been characterized. ► Linear calibration graphs and LODs in the low ppm range are achieved. ► Craters with flat bottoms and vertical walls are obtained. ► UNIOVI source can be easily cleaned as it does not require flow tube. ► UNIOVI GD has a simple design and thus its manufacture is easy and cheap.

  3. Innovative ion sources for accelerators: the benefits of the plasma technology

    Czech Academy of Sciences Publication Activity Database

    Gammino, S.; Ciavola, G.; Celona, L.; Torrisi, L.; Ando, L.; Presti, M.; Láska, Leoš; Krása, Josef; Wolowski, J.

    2004-01-01

    Roč. 54, Suppl. C (2004), s. C883-C888 ISSN 0011-4626. [Symposium on Plasma Physics and Technology /21./. Praha, 14.06.2004-17.06.2004] R&D Projects: GA AV ČR IAA1010405 Institutional research plan: CEZ:AV0Z1010921 Keywords : plasma sources * ion sources * proton sources * ECR Subject RIV: BL - Plasma and Gas Discharge Physics Impact factor: 0.292, year: 2004

  4. Compact tunable Compton x-ray source from laser-plasma accelerator and plasma mirror

    International Nuclear Information System (INIS)

    Tsai, Hai-En; Wang, Xiaoming; Shaw, Joseph M.; Li, Zhengyan; Zgadzaj, Rafal; Henderson, Watson; Downer, M. C.; Arefiev, Alexey V.; Zhang, Xi; Khudik, V.; Shvets, G.

    2015-01-01

    We present an in-depth experimental-computational study of the parameters necessary to optimize a tunable, quasi-monoenergetic, efficient, low-background Compton backscattering (CBS) x-ray source that is based on the self-aligned combination of a laser-plasma accelerator (LPA) and a plasma mirror (PM). The main findings are (1) an LPA driven in the blowout regime by 30 TW, 30 fs laser pulses produce not only a high-quality, tunable, quasi-monoenergetic electron beam, but also a high-quality, relativistically intense (a 0 ∼ 1) spent drive pulse that remains stable in profile and intensity over the LPA tuning range. (2) A thin plastic film near the gas jet exit retro-reflects the spent drive pulse efficiently into oncoming electrons to produce CBS x-rays without detectable bremsstrahlung background. Meanwhile, anomalous far-field divergence of the retro-reflected light demonstrates relativistic “denting” of the PM. Exploiting these optimized LPA and PM conditions, we demonstrate quasi-monoenergetic (50% FWHM energy spread), tunable (75–200 KeV) CBS x-rays, characteristics previously achieved only on more powerful laser systems by CBS of a split-off, counter-propagating pulse. Moreover, laser-to-x-ray photon conversion efficiency (∼6 × 10 −12 ) exceeds that of any previous LPA-based quasi-monoenergetic Compton source. Particle-in-cell simulations agree well with the measurements

  5. Quasi-steady carbon plasma source for neutral beam injector

    International Nuclear Information System (INIS)

    Koguchi, H.; Sakakita, H.; Kiyama, S.; Shimada, T.; Sato, Y.; Hirano, Y.

    2014-01-01

    Carbon plasma is successfully sustained during 1000 s without any carrier gas in the bucket type ionization chamber with cusp magnetic field. Every several seconds, seed plasmas having ∼3 ms duration time are injected into the ionization chamber by a shunting arch plasma gun. The weakly ionized carbon plasma ejected from the shunting arch is also ionized by 2.45 GHz microwave at the electron cyclotron resonance surface and the plasma can be sustained even in the interval of gun discharges. Control of the gun discharge interval allows to keep high pressure and to sustain the plasma for long duration

  6. Quasi-steady carbon plasma source for neutral beam injector.

    Science.gov (United States)

    Koguchi, H; Sakakita, H; Kiyama, S; Shimada, T; Sato, Y; Hirano, Y

    2014-02-01

    Carbon plasma is successfully sustained during 1000 s without any carrier gas in the bucket type ionization chamber with cusp magnetic field. Every several seconds, seed plasmas having ∼3 ms duration time are injected into the ionization chamber by a shunting arch plasma gun. The weakly ionized carbon plasma ejected from the shunting arch is also ionized by 2.45 GHz microwave at the electron cyclotron resonance surface and the plasma can be sustained even in the interval of gun discharges. Control of the gun discharge interval allows to keep high pressure and to sustain the plasma for long duration.

  7. Perspective: The physics, diagnostics, and applications of atmospheric pressure low temperature plasma sources used in plasma medicine

    Science.gov (United States)

    Laroussi, M.; Lu, X.; Keidar, M.

    2017-07-01

    Low temperature plasmas have been used in various plasma processing applications for several decades. But it is only in the last thirty years or so that sources generating such plasmas at atmospheric pressure in reliable and stable ways have become more prevalent. First, in the late 1980s, the dielectric barrier discharge was used to generate relatively large volume diffuse plasmas at atmospheric pressure. Then, in the early 2000s, plasma jets that can launch cold plasma plumes in ambient air were developed. Extensive experimental and modeling work was carried out on both methods and much of the physics governing such sources was elucidated. Starting in the mid-1990s, low temperature plasma discharges have been used as sources of chemically reactive species that can be transported to interact with biological media, cells, and tissues and induce impactful biological effects. However, many of the biochemical pathways whereby plasma affects cells remain not well understood. This situation is changing rather quickly because the field, known today as "plasma medicine," has experienced exponential growth in the last few years thanks to a global research community that engaged in fundamental and applied research involving the use of cold plasma for the inactivation of bacteria, dental applications, wound healing, and the destruction of cancer cells/tumors. In this perspective, the authors first review the physics as well as the diagnostics of the principal plasma sources used in plasma medicine. Then, brief descriptions of their biomedical applications are presented. To conclude, the authors' personal assessment of the present status and future outlook of the field is given.

  8. Reduction of determinate errors in mass bias-corrected isotope ratios measured using a multi-collector plasma mass spectrometer

    International Nuclear Information System (INIS)

    Doherty, W.

    2015-01-01

    A nebulizer-centric instrument response function model of the plasma mass spectrometer was combined with a signal drift model, and the result was used to identify the causes of the non-spectroscopic determinate errors remaining in mass bias-corrected Pb isotope ratios (Tl as internal standard) measured using a multi-collector plasma mass spectrometer. Model calculations, confirmed by measurement, show that the detectable time-dependent errors are a result of the combined effect of signal drift and differences in the coordinates of the Pb and Tl response function maxima (horizontal offset effect). If there are no horizontal offsets, then the mass bias-corrected isotope ratios are approximately constant in time. In the absence of signal drift, the response surface curvature and horizontal offset effects are responsible for proportional errors in the mass bias-corrected isotope ratios. The proportional errors will be different for different analyte isotope ratios and different at every instrument operating point. Consequently, mass bias coefficients calculated using different isotope ratios are not necessarily equal. The error analysis based on the combined model provides strong justification for recommending a three step correction procedure (mass bias correction, drift correction and a proportional error correction, in that order) for isotope ratio measurements using a multi-collector plasma mass spectrometer

  9. Double-layer ion acceleration triggered by ion magnetization in expanding radiofrequency plasma sources

    International Nuclear Information System (INIS)

    Takahashi, Kazunori; Charles, Christine; Boswell, Rod W.; Fujiwara, Tamiya

    2010-01-01

    Ion energy distribution functions downstream of the source exit in magnetically expanding low-pressure plasmas are experimentally investigated for four source tube diameters ranging from about 5 to 15 cm. The magnetic-field threshold corresponding to a transition from a simple expanding plasma to a double layer-containing plasma is observed to increase with a decrease in the source tube diameter. The results demonstrate that for the four geometries, the double layer and the accelerated ion beam form when the ion Larmour radius in the source becomes smaller than the source tube radius, i.e., when the ions become magnetized in the source tube.

  10. Physics-electrical hybrid model for real time impedance matching and remote plasma characterization in RF plasma sources.

    Science.gov (United States)

    Sudhir, Dass; Bandyopadhyay, M; Chakraborty, A

    2016-02-01

    Plasma characterization and impedance matching are an integral part of any radio frequency (RF) based plasma source. In long pulse operation, particularly in high power operation where plasma load may vary due to different reasons (e.g. pressure and power), online tuning of impedance matching circuit and remote plasma density estimation are very useful. In some cases, due to remote interfaces, radio activation and, due to maintenance issues, power probes are not allowed to be incorporated in the ion source design for plasma characterization. Therefore, for characterization and impedance matching, more remote schemes are envisaged. Two such schemes by the same authors are suggested in these regards, which are based on air core transformer model of inductive coupled plasma (ICP) [M. Bandyopadhyay et al., Nucl. Fusion 55, 033017 (2015); D. Sudhir et al., Rev. Sci. Instrum. 85, 013510 (2014)]. However, the influence of the RF field interaction with the plasma to determine its impedance, a physics code HELIC [D. Arnush, Phys. Plasmas 7, 3042 (2000)] is coupled with the transformer model. This model can be useful for both types of RF sources, i.e., ICP and helicon sources.

  11. Improved mass spectrometry assay for plasma hepcidin: detection and characterization of a novel hepcidin isoform.

    Directory of Open Access Journals (Sweden)

    Coby M M Laarakkers

    Full Text Available Mass spectrometry (MS-based assays for the quantification of the iron regulatory hormone hepcidin are pivotal to discriminate between the bioactive 25-amino acid form that can effectively block the sole iron transporter ferroportin and other naturally occurring smaller isoforms without a known role in iron metabolism. Here we describe the design, validation and use of a novel stable hepcidin-25(+40 isotope as internal standard for quantification. Importantly, the relative large mass shift of 40 Da makes this isotope also suitable for easy-to-use medium resolution linear time-of-flight (TOF platforms. As expected, implementation of hepcidin-25(+40 as internal standard in our weak cation exchange (WCX TOF MS method yielded very low inter/intra run coefficients of variation. Surprisingly, however, in samples from kidney disease patients, we detected a novel peak (m/z 2673.9 with low intensity that could be identified as hepcidin-24 and had previously remained unnoticed due to peak interference with the formerly used internal standard. Using a cell-based bioassay it was shown that synthetic hepcidin-24 was, like the -22 and -20 isoforms, a significantly less potent inducer of ferroportin degradation than hepcidin-25. During prolonged storage of plasma at room temperature, we observed that a decrease in plasma hepcidin-25 was paralleled by an increase in the levels of the hepcidin-24, -22 and -20 isoforms. This provides first evidence that all determinants for the conversion of hepcidin-25 to smaller inactive isoforms are present in the circulation, which may contribute to the functional suppression of hepcidin-25, that is significantly elevated in patients with renal impairment. The present update of our hepcidin TOF MS assay together with improved insights in the source and preparation of the internal standard, and sample stability will further improve our understanding of circulating hepcidin and pave the way towards further optimization and

  12. Ferroelectric plasma sources for NDCX-II and heavy ion drivers

    Energy Technology Data Exchange (ETDEWEB)

    Gilson, E.P., E-mail: egilson@pppl.gov [Princeton Plasma Physics Laboratory, Princeton University, P.O. Box 451, Princeton, New Jersey, 08543 (United States); Davidson, R.C.; Efthimion, P.C.; Kaganovich, I.D. [Princeton Plasma Physics Laboratory, Princeton University, P.O. Box 451, Princeton, New Jersey, 08543 (United States); Kwan, J.W.; Lidia, S.M.; Ni, P.A.; Roy, P.K.; Seidl, P.A.; Waldron, W.L. [Lawrence Berkeley National Laboratory, One Cyclotron Road, Berkeley, California, 94720 (United States); Barnard, J.J.; Friedman, A. [Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California, 94550 (United States)

    2014-01-01

    A barium titanate ferroelectric cylindrical plasma source has been developed, tested and delivered for the Neutralized Drift Compression Experiment NDCX-II at Lawrence Berkeley National Laboratory (LBNL). The plasma source design is based on the successful design of the NDCX-I plasma source. A 7 kV pulse applied across the 3.8 mm-thick ceramic cylinder wall produces a large polarization surface charge density that leads to breakdown and plasma formation. The plasma that fills the NDCX-II drift section upstream of the final-focusing solenoid has a plasma number density exceeding 10{sup 10} cm{sup −3} and an electron temperature of several eV. The operating principle of the ferroelectric plasma source are reviewed and a detailed description of the installation plans is presented. The criteria for plasma sources with larger number density will be given, and concepts will be presented for plasma sources for driver applications. Plasma sources for drivers will need to be highly reliable, and operate at several Hz for millions of shots.

  13. Inductively Coupled Plasma: Fundamental Particle Investigations with Laser Ablation and Applications in Magnetic Sector Mass Spectrometry

    International Nuclear Information System (INIS)

    Nathan Joe Saetveit

    2008-01-01

    Particle size effects and elemental fractionation in laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) are investigated with nanosecond and femtosecond laser ablation, differential mobility analysis, and magnetic sector ICP-MS. Laser pulse width was found to have a significant influence on the LA particle size distribution and the elemental composition of the aerosol and thus fractionation. Emission from individual particles from solution nebulization, glass, and a pressed powder pellet are observed with high speed digital photography. The presence of intact particles in an ICP is shown to be a likely source of fractionation. A technique for the online detection of stimulated elemental release from neural tissue using magnetic sector ICP-MS is described. Detection limits of 1 (micro)g L -1 or better were found for P, Mn, Fe, Cu, and Zn in a 60 (micro)L injection in a physiological saline matrix

  14. Rayleigh-Taylor instability in an equal mass plasma

    Energy Technology Data Exchange (ETDEWEB)

    Adak, Ashish, E-mail: ashish-adak@yahoo.com [Department of Instrumentation Science, Jadavpur University, Kolkata 700 032 (India); Ghosh, Samiran, E-mail: sran-g@yahoo.com [Department of Applied Mathematics, University of Calcutta 92, Acharya Prafulla Chandra Road, Kolkata 700 009 (India); Chakrabarti, Nikhil, E-mail: nikhil.chakrabarti@saha.ac.in [Saha Institute of Nuclear Physics, 1/AF Bidhannagar, Kolkata 700 064 (India)

    2014-09-15

    The Rayleigh-Taylor (RT) instability in an inhomogeneous pair-ion plasma has been analyzed. Considering two fluid model for two species of ions (positive and negative), we obtain the possibility of the existence of RT instability. The growth rate of the RT instability as usual depends on gravity and density gradient scale length. The results are discussed in context of pair-ion plasma experiments.

  15. Damping of electron center-of-mass oscillation in ultracold plasmas

    International Nuclear Information System (INIS)

    Chen, Wei-Ting; Witte, Craig; Roberts, Jacob L.

    2016-01-01

    Applying a short electric field pulse to an ultracold plasma induces an electron plasma oscillation. This manifests itself as an oscillation of the electron center of mass around the ion center of mass in the ultracold plasma. In general, the oscillation can damp due to either collisionless or collisional mechanisms, or a combination of the both. To investigate the nature of oscillation damping in ultracold plasmas, we developed a molecular dynamics model of the ultracold plasma electrons. Through this model, we found that depending on the neutrality of the ultracold plasma and the size of an applied DC electric field, there are some parameter ranges where the damping is primarily collisional and some primarily collisionless. We conducted experiments to compare the measured damping rate with theory predictions and found them to be in good agreement. Extension of our measurements to different parameter ranges should enable studies for strong-coupling influence on electron-ion collision rates.

  16. Theory of mass-discrimination effects in ion extraction from a plasma of wide pressure range

    International Nuclear Information System (INIS)

    Chang, J.-S.; Kodera, K.

    1979-01-01

    Mass-discrimination effects in stagnation-point ion extraction are treated for a plasma with a wide range of Knudsen number, i.e. when the charged particle's mean free path 3 , ion Schmidt numbers, from 0 to 10 4 , the effective Knudsen number K from 0 to infinity, and the Debye ratio Rsub(p)/lambdasub(D) from 0 to 10 -1 . Numerical results show that: (1) for a non-flowing plasma, mass-discrimination effects increase with increasing effective Knudsen number (or gas pressure) and decreasing sampling potential; (2) for a non-flowing plasma, no significant effect of the Debye ratio on mass-discrimination was found; (3) for a flowing plasma, mass-discrimination effects decrease with increasing Reynolds number (or flow velocity) and ion Schmidt number, and with decreasing sampling potential and effective Knudsen number. (Auth.)

  17. Determination of trimethyllead reference material using high performance liquid chromatography-inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Lu Hai; Wei Chao; Wang Jun; Chao Jingbo; Zhou Tao; Chen Dazhou

    2005-01-01

    A high-performance liquid chromatography-inductively coupled plasma mass spectrometry (HPLC-ICPMS) was combined, and the chromatography conditions were optimized. The stability and homogeneity of a trimethyllead reference material were determined using this method. (authors)

  18. Screening Samples for Arsenic by Inductively Coupled Plasma-Mass Spectrometry for Treaty Samples

    Science.gov (United States)

    2014-02-01

    quality system in accordance with International Organization for Standardization/International Electrotechnical Commission ( ISO / IEC ) 17025 :2005...plasma-mass spectrometry ISO / IEC International Organization for Standardization/International Electrotechnical Commission L lewisite MDL method

  19. The difference between the metal ion extracted from the R.F. ion source by applying plasma chemistry reaction and by non-plasma range chemistry reaction

    International Nuclear Information System (INIS)

    Bai Gui Bin

    1987-01-01

    The paper introduced the difference between using plasma chemistry reaction draw metal ion and non-plasma range chemistry reaction in the R.F. ion source. By using of the plasma chemistry reaction draw metal ion higher percentage than non-plasma range chemistry reaction in the R.F. ion source. The authors plasma chemistry reaction to R.F. ion source and implanter successfully. The effect is very well, it has its own characteristic

  20. High-precision lead isotope ratio measurement by inductively coupled plasma multiple collector mass spectrometry

    International Nuclear Information System (INIS)

    Walder, A.J.; Furuta, Naoki.

    1993-01-01

    An inductively coupled plasma (ICP) ion source coupled to a magnetic sector mass analyser equipped with seven Faraday detectors has been used to measure the lead isotope ratios in solutions of Sanshiro Pond sediment collected at the University of Tokyo, airborne particulates collected at Shinjuku in Tokyo and Merck multielement standard product number 97279494. A thallium correction technique was utilized to allow a simultaneous correction for mass bias. This work followed an earlier interlaboratory comparison study of the above-mentioned solutions using ICP quadrupole mass spectrometry, and has demonstrated a considerable improvement in analytical precision. The following isotope ratio measurements were recorded. Pond sediment solution containing 82 ng ml -1 lead: 206 Pb/ 204 Pb=17.762±0.014; 206 Pb/ 207 Pb=1.1424±0.0009; 208 Pb/ 204 Pb=37.678±0.034. Airborne particulate solution containing 45 ng ml -1 lead: 206 Pb/ 204 Pb=17.969±0.006; 206 Pb/ 207 Pb=1.1528±0.0003; 208 Pb/ 204 Pb=37.915±0.021. Merck multielement standard solution containing 100 ng ml -1 lead: 206 Pb/ 204 Pb=19.255±0.015; 206 Pb/ 207 Pb=1.2238±0.0004; 208 Pb/ 204 Pb=38.476±0.021 (All errors are given as ±2 standard deviations). (author)

  1. A high-intensity plasma-sputter heavy negative ion source

    International Nuclear Information System (INIS)

    Alton, G.D.; Mori, Y.; Takagi, A.; Ueno, A.; Fukumoto, S.

    1989-01-01

    A multicusp magnetic field plasma surface ion source, normally used for H/sup /minus//ion beam formation, has been modified for the generation of high-intensity, pulsed, heavy negative ion beams suitable for a variety of uses. To date, the source has been utilized to produce mA intensity pulsed beams of more than 24 species. A brief description of the source, and basic pulsed-mode operational data, (e.g., intensity versus cesium oven temperature, sputter probe voltage, and discharge pressure), are given. In addition, illustrative examples of intensity versus time and the mass distributions of ion beams extracted from a number of samples along with emittance data, are also presented. Preliminary results obtained during dc operation of the source under low discharge power conditions suggest that sources of this type may also be used to produce high-intensity (mA) dc beams. The results of these investigations are given, as well, and the technical issues that must be addressed for this mode of operation are discussed. 15 refs., 10 figs., 2 tabs

  2. Operations manual for the plasma source ion implantation economics program

    International Nuclear Information System (INIS)

    Bibeault, M.L.; Thayer, G.R.

    1995-10-01

    Plasma Source Ion Implantation (PSII) is a surface modification technique for metal. PSIICOSTMODEL95 is an EXCEL-based program that estimates the cost for implementing a PSII system in a manufacturing setting where the number of parts to be processed is over 5,000 parts per day and the shape of each part does not change from day to day. Overall, the manufacturing process must be very well defined and should not change. This document is a self-contained manual for PSIICOSTMODEL95. It assumes the reader has some general knowledge of the technical requirements for PSII. Configuration of the PSII process versus design is used as the methodology in PSIICOSTMODEL95. The reason behind this is twofold. First, the design process cannot be programmed into a computer when the relationships between design variables are not understood. Second, the configuration methodology reduces the number of assumptions that must be programmed into our software. Misuse of results are less likely to occur if the user has fewer assumptions to understand

  3. Plasma particle sources due to interactions with neutrals in a turbulent scrape-off layer of a toroidally confined plasma

    DEFF Research Database (Denmark)

    Thrysøe, Alexander Simon; Løiten, M.; Madsen, J.

    2018-01-01

    The conditions in the edge and scrape-off layer (SOL) of magnetically confined plasmas determine the overall performance of the device, and it is of great importance to study and understand the mechanics that drive transport in those regions. If a significant amount of neutral molecules and atoms...... is present in the edge and SOL regions, those will influence the plasma parameters and thus the plasma confinement. In this paper, it is displayed how neutrals, described by a fluid model, introduce source terms in a plasma drift-fluid model due to inelastic collisions. The resulting source terms...... are included in a four-field drift fluid model, and it is shown how an increasing neutral particle density in the edge and SOL regions influences the plasma particle transport across the lastclosed-flux-surface. It is found that an appropriate gas puffing rate allows for the edge density in the simulation...

  4. Improving mass measurement accuracy in mass spectrometry based proteomics by combining open source tools for chromatographic alignment and internal calibration.

    Science.gov (United States)

    Palmblad, Magnus; van der Burgt, Yuri E M; Dalebout, Hans; Derks, Rico J E; Schoenmaker, Bart; Deelder, André M

    2009-05-02

    Accurate mass determination enhances peptide identification in mass spectrometry based proteomics. We here describe the combination of two previously published open source software tools to improve mass measurement accuracy in Fourier transform ion cyclotron resonance mass spectrometry (FTICRMS). The first program, msalign, aligns one MS/MS dataset with one FTICRMS dataset. The second software, recal2, uses peptides identified from the MS/MS data for automated internal calibration of the FTICR spectra, resulting in sub-ppm mass measurement errors.

  5. Study on laser plasma as an ion source for the controlled fasion with heavy ions

    International Nuclear Information System (INIS)

    Barabash, L.Z.; Bykovskij, Yu.A.; Golubev, A.A.; Kozyrev, Yu.P.; Krechet, K.I.; Lapitskij, Yu.Ya.; Sharkov, B.Yu.

    1981-01-01

    The results of experimental investigations of Pb 208 multiply- charged lead ions, obtained in the course of CO 2 laser radiation effect on a solid target are presented. The experimental installation, the basic units of which are CO 2 - laser with transverse discharge, ion source chamber, time- of-flight space, 9-channel electrostatic mirror type mass-analyser with a detection unit, is described. Physical characteristics of a freely spreading laser plasma, ion distribution over energies, velocities and Z charges from Z=+1 to Z=+10 are investigated. Absolute values of ion number of each charge property as well as absolute values of currents are obtained, the laser plasma temperature is estimated. The analysis of time distribution of ion quantity permits to point out the following regularities: with Z increase the ion current duration decreases according to the Δt approximately Z -1 law, with Z increase, the moment of the ion pulse beginning approaches to the moment of target irradiation which testifies that multiply-charged ions have high velocities and energies. The velocity distribution analysis permits to obtain ion velocity dependence in the field of maximum distribution on charge properties. The results presented are obtained at the temperature of hot unspreaded plasma about 60 eV. The data obtained are a basis for development of a real laser forinjector for the problems of the controlled fusion with heavy ions [ru

  6. Technological plasma source equipped with combined system of vacuum-arc discharge initiation

    International Nuclear Information System (INIS)

    Sysoev, Yu.O.

    2013-01-01

    The construction and the operation principle of erosion plasma source with a three-stage system of vacuum-arc discharge excitation is described. As first two step was used the modified contactless start system with plasma injector, which was widely used in standard plasma sources of the ''Bulat'' systems. The operation principle of the third stage was based on the transition of glow discharge to arc discharge. Coordinated operation of three stages during various stages of coating deposition provided significant increasing of service life and reliability of the system of vacuum-arc discharge initiation and extended the functionality of the plasma source

  7. Dependence of the source performance on plasma parameters at the BATMAN test facility

    Science.gov (United States)

    Wimmer, C.; Fantz, U.

    2015-04-01

    The investigation of the dependence of the source performance (high jH-, low je) for optimum Cs conditions on the plasma parameters at the BATMAN (Bavarian Test MAchine for Negative hydrogen ions) test facility is desirable in order to find key parameters for the operation of the source as well as to deepen the physical understanding. The most relevant source physics takes place in the extended boundary layer, which is the plasma layer with a thickness of several cm in front of the plasma grid: the production of H-, its transport through the plasma and its extraction, inevitably accompanied by the co-extraction of electrons. Hence, a link of the source performance with the plasma parameters in the extended boundary layer is expected. In order to characterize electron and negative hydrogen ion fluxes in the extended boundary layer, Cavity Ring-Down Spectroscopy and Langmuir probes have been applied for the measurement of the H- density and the determination of the plasma density, the plasma potential and the electron temperature, respectively. The plasma potential is of particular importance as it determines the sheath potential profile at the plasma grid: depending on the plasma grid bias relative to the plasma potential, a transition in the plasma sheath from an electron repelling to an electron attracting sheath takes place, influencing strongly the electron fraction of the bias current and thus the amount of co-extracted electrons. Dependencies of the source performance on the determined plasma parameters are presented for the comparison of two source pressures (0.6 Pa, 0.45 Pa) in hydrogen operation. The higher source pressure of 0.6 Pa is a standard point of operation at BATMAN with external magnets, whereas the lower pressure of 0.45 Pa is closer to the ITER requirements (p ≤ 0.3 Pa).

  8. Dependence of the source performance on plasma parameters at the BATMAN test facility

    International Nuclear Information System (INIS)

    Wimmer, C.; Fantz, U.

    2015-01-01

    The investigation of the dependence of the source performance (high j H − , low j e ) for optimum Cs conditions on the plasma parameters at the BATMAN (Bavarian Test MAchine for Negative hydrogen ions) test facility is desirable in order to find key parameters for the operation of the source as well as to deepen the physical understanding. The most relevant source physics takes place in the extended boundary layer, which is the plasma layer with a thickness of several cm in front of the plasma grid: the production of H − , its transport through the plasma and its extraction, inevitably accompanied by the co-extraction of electrons. Hence, a link of the source performance with the plasma parameters in the extended boundary layer is expected. In order to characterize electron and negative hydrogen ion fluxes in the extended boundary layer, Cavity Ring-Down Spectroscopy and Langmuir probes have been applied for the measurement of the H − density and the determination of the plasma density, the plasma potential and the electron temperature, respectively. The plasma potential is of particular importance as it determines the sheath potential profile at the plasma grid: depending on the plasma grid bias relative to the plasma potential, a transition in the plasma sheath from an electron repelling to an electron attracting sheath takes place, influencing strongly the electron fraction of the bias current and thus the amount of co-extracted electrons. Dependencies of the source performance on the determined plasma parameters are presented for the comparison of two source pressures (0.6 Pa, 0.45 Pa) in hydrogen operation. The higher source pressure of 0.6 Pa is a standard point of operation at BATMAN with external magnets, whereas the lower pressure of 0.45 Pa is closer to the ITER requirements (p ≤ 0.3 Pa)

  9. [Automatic adjustment control system for DC glow discharge plasma source].

    Science.gov (United States)

    Wan, Zhen-zhen; Wang, Yong-qing; Li, Xiao-jia; Wang, Hai-zhou; Shi, Ning

    2011-03-01

    There are three important parameters in the DC glow discharge process, the discharge current, discharge voltage and argon pressure in discharge source. These parameters influence each other during glow discharge process. This paper presents an automatic control system for DC glow discharge plasma source. This system collects and controls discharge voltage automatically by adjusting discharge source pressure while the discharge current is constant in the glow discharge process. The design concept, circuit principle and control program of this automatic control system are described. The accuracy is improved by this automatic control system with the method of reducing the complex operations and manual control errors. This system enhances the control accuracy of glow discharge voltage, and reduces the time to reach discharge voltage stability. The glow discharge voltage stability test results with automatic control system are provided as well, the accuracy with automatic control system is better than 1% FS which is improved from 4% FS by manual control. Time to reach discharge voltage stability has been shortened to within 30 s by automatic control from more than 90 s by manual control. Standard samples like middle-low alloy steel and tin bronze have been tested by this automatic control system. The concentration analysis precision has been significantly improved. The RSDs of all the test result are better than 3.5%. In middle-low alloy steel standard sample, the RSD range of concentration test result of Ti, Co and Mn elements is reduced from 3.0%-4.3% by manual control to 1.7%-2.4% by automatic control, and that for S and Mo is also reduced from 5.2%-5.9% to 3.3%-3.5%. In tin bronze standard sample, the RSD range of Sn, Zn and Al elements is reduced from 2.6%-4.4% to 1.0%-2.4%, and that for Si, Ni and Fe is reduced from 6.6%-13.9% to 2.6%-3.5%. The test data is also shown in this paper.

  10. Plasma ion sources and ion beam technology in microfabrications

    International Nuclear Information System (INIS)

    Ji, Lili

    2007-01-01

    For over decades, focused ion beam (FIB) has been playing a very important role in microscale technology and research, among which, semiconductor microfabrication is one of its biggest application area. As the dimensions of IC devices are scaled down, it has shown the need for new ion beam tools and new approaches to the fabrication of small-scale devices. In the meanwhile, nanotechnology has also deeply involved in material science research and bioresearch in recent years. The conventional FIB systems which utilize liquid gallium ion sources to achieve nanometer scale resolution can no longer meet the various requirements raised from such a wide application area such as low contamination, high throughput and so on. The drive towards controlling materials properties at nanometer length scales relies on the availability of efficient tools. In this thesis, three novel ion beam tools have been developed and investigated as the alternatives for the conventional FIB systems in some particular applications. An integrated focused ion beam (FIB) and scanning electron microscope (SEM) system has been developed for direct doping or surface modification. This new instrument employs a mini-RF driven plasma source to generate focused ion beam with various ion species, a FEI two-lens electron (2LE) column for SEM imaging, and a five-axis manipulator system for sample positioning. An all-electrostatic two-lens column has been designed to focus the ion beam extracted from the source. Based on the Munro ion optics simulation, beam spot sizes as small as 100 nm can be achieved at beam energies between 5 to 35 keV if a 5 (micro)m-diameter extraction aperture is used. Smaller beam spot sizes can be obtained with smaller apertures at sacrifice of some beam current. The FEI 2LE column, which utilizes Schottky emission, electrostatic focusing optics, and stacked-disk column construction, can provide high-resolution (as small as 20 nm) imaging capability, with fairly long working distance

  11. Coronal mass ejections and disturbances in solar wind plasma parameters in relation with geomagnetic storms

    International Nuclear Information System (INIS)

    Verma, P L; Singh, Puspraj; Singh, Preetam

    2014-01-01

    Coronal Mass Ejections (CMEs) are the drastic solar events in which huge amount of solar plasma materials are ejected into the heliosphere from the sun and are mainly responsible to generate large disturbances in solar wind plasma parameters and geomagnetic storms in geomagnetic field. We have studied geomagnetic storms, (Dst ≤-75 nT) observed during the period of 1997-2007 with Coronal Mass Ejections and disturbances in solar wind plasma parameters (solar wind temperature, velocity, density and interplanetary magnetic field) .We have inferred that most of the geomagnetic storms are associated with halo and partial halo Coronal Mass Ejections (CMEs).The association rate of halo and partial halo coronal mass ejections are found 72.37 % and 27.63 % respectively. Further we have concluded that geomagnetic storms are closely associated with the disturbances in solar wind plasma parameters. We have determined positive co-relation between magnitudes of geomagnetic storms and magnitude of jump in solar wind plasma temperature, jump in solar wind plasma density, jump in solar wind plasma velocity and jump in average interplanetary magnetic field with co-relation co-efficient 0 .35 between magnitude of geomagnetic storms and magnitude of jump in solar wind plasma temperature, 0.19 between magnitude of geomagnetic storms and magnitude of jump in solar wind density, 0.34 between magnitude of geomagnetic storms and magnitude of jump in solar wind plasma velocity, 0.66 between magnitude of geomagnetic storms and magnitude of jump in average interplanetary magnetic field respectively. We have concluded that geomagnetic storms are mainly caused by Coronal Mass Ejections and disturbances in solar wind plasma parameters that they generate.

  12. Development of Langmuir probe diagnostic system for 13.56 MHz plasma sources

    International Nuclear Information System (INIS)

    Ranjini, K.; Nabhiraj, P.Y.; Mallik, C.; Bhandari, R.K.

    2006-01-01

    A work on development of high brightness ion source has been started recently. Plasma parameters are strongly linked to the brightness of the ion beams produced from the ion sources. A self compensated Langmuir probe and related automation system for the measurement of plasma parameters is developed. This paper describes design of the probe, software, hardware and the results. (author)

  13. PIII Plasma Density Enhancement by a New DC Power Source

    International Nuclear Information System (INIS)

    Lopez-Callejas, R.; Godoy-Cabrera, O. G.; Granda-Gutierrez, E. E.; Piedad-Beneitez, A. de la; Munoz-Castro, A. E.; Valencia A, R.; Barocio, S. R.; Mercado-Cabrera, A.; Pena-Eguiluz, R.

    2006-01-01

    In practical terms, those plasmas produced by a DC voltage power supply do not attain densities above the 108 to 109 cm-3 band. Here we present a power supply, controlled in current and voltage, which has been successfully designed and constructed delivering plasma densities in the orders of 109 - 1010 cm-3. Its experimental performance test was conducted within one toroidal and one cylindrical chambers capable of 29 and 35 litres, respectively, using nitrogen gas. The DC plasma was characterized by a double electric probe. Several physical phenomena present in the PIII process have been keenly investigated including plasma sheath dynamics, interaction of plasma and surface, etc. In this paper we analyze the effect of the implantation voltage, plasma density and pulse time in the PIII average heating power and fluence density

  14. Trace metal analysis of road dust by inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Powell, M.J.; Liu, L.; Gnanalingham, N.; Peters, L.

    2000-01-01

    Dust from roads in an air impingement zone close to anthropogenic sources of air pollutants can be a concern for people living in the immediate vicinity. The Ministry of the Environment (MOE) has conducted a case study to monitor the concentration of uranium, strontium, thorium and arsenic in road dust from one such area. A method for the analysis of road dust by inductively coupled plasma mass spectrometry (ICP-MS) has been developed with detection limits in the ng/1 range. A digestion technique has been developed by conducting experiments using single and combinations of acids in open-vessel wet digestions. Accuracy has been determined by the use of matrix representative certified reference materials (CRMs). Digestion precision was determined by elemental concentration measurements of the most representative CRM through replicates. Spike recovery data were from 95% to 110% for all elements, and inter-method comparison studies between hydride generation atomic absorption spectrometry (AAS) inductively coupled plasma atomic emission spectrometry (ICP-AES) and ICP-MS for arsenic and strontium show good agreement. (author)

  15. PLASMA HEATING INSIDE INTERPLANETARY CORONAL MASS EJECTIONS BY ALFVÉNIC FLUCTUATIONS DISSIPATION

    Energy Technology Data Exchange (ETDEWEB)

    Li, Hui; Wang, Chi; Zhang, Lingqian [State Key Laboratory of Space Weather, National Space Science Center, CAS, Beijing, 100190 (China); He, Jiansen [School of Earth and Space Sciences, Peking University, Beijing, 100871 (China); Richardson, John D.; Belcher, John W. [Kavli Institute for Astrophysics and Space Research, Massachusetts Institute of Technology, Cambridge, MA (United States); Tu, Cui, E-mail: hli@spaceweather.ac.cn [Laboratory of Near Space Environment, National Space Science Center, CAS, Beijing, 100190 (China)

    2016-11-10

    Nonlinear cascade of low-frequency Alfvénic fluctuations (AFs) is regarded as one of the candidate energy sources that heat plasma during the non-adiabatic expansion of interplanetary coronal mass ejections (ICMEs). However, AFs inside ICMEs were seldom reported in the literature. In this study, we investigate AFs inside ICMEs using observations from Voyager 2 between 1 and 6 au. It has been found that AFs with a high degree of Alfvénicity frequently occurred inside ICMEs for almost all of the identified ICMEs (30 out of 33 ICMEs) and for 12.6% of the ICME time interval. As ICMEs expand and move outward, the percentage of AF duration decays linearly in general. The occurrence rate of AFs inside ICMEs is much less than that in ambient solar wind, especially within 4.75 au. AFs inside ICMEs are more frequently presented in the center and at the boundaries of ICMEs. In addition, the proton temperature inside ICME has a similar “W”-shaped distribution. These findings suggest significant contribution of AFs on local plasma heating inside ICMEs.

  16. Advanced plasma flow simulations of cathodic-arc and ferroelectric plasma sources for neutralized drift compression experiments

    Directory of Open Access Journals (Sweden)

    Adam B. Sefkow

    2008-07-01

    Full Text Available Large-space-scale and long-time-scale plasma flow simulations are executed in order to study the spatial and temporal evolution of plasma parameters for two types of plasma sources used in the neutralized drift compression experiment (NDCX. The results help assess the charge neutralization conditions for ion beam compression experiments and can be employed in more sophisticated simulations, which previously neglected the dynamical evolution of the plasma. Three-dimensional simulations of a filtered cathodic-arc plasma source show the coupling efficiency of the plasma flow from the source to the drift region depends on geometrical factors. The nonuniform magnetic topology complicates the well-known general analytical considerations for evaluating guiding-center drifts, and particle-in-cell simulations provide a self-consistent evaluation of the physics in an otherwise challenging scenario. Plasma flow profiles of a ferroelectric plasma source demonstrate that the densities required for longitudinal compression experiments involving ion beams are provided over the drift length, and are in good agreement with measurements. Simulations involving azimuthally asymmetric plasma creation conditions show that symmetric profiles are nevertheless achieved at the time of peak on-axis plasma density. Also, the ferroelectric plasma expands upstream on the thermal expansion time scale, and therefore avoids the possibility of penetration into the acceleration gap and transport sections, where partial neutralization would increase the beam emittance. Future experiments on NDCX will investigate the transverse focusing of an axially compressing intense charge bunch to a sub-mm spot size with coincident focal planes using a strong final-focus solenoid. In order to fill a multi-tesla solenoid with the necessary high-density plasma for beam charge neutralization, the simulations predict that supersonically injected plasma from the low-field region will penetrate and

  17. Progress in the Development of a High Power Helicon Plasma Source for the Materials Plasma Exposure Experiment

    Energy Technology Data Exchange (ETDEWEB)

    Goulding, Richard Howell [ORNL; Caughman, John B. [ORNL; Rapp, Juergen [ORNL; Biewer, Theodore M. [ORNL; Bigelow, Tim S. [ORNL; Campbell, Ian H. [ORNL; Caneses Marin, Juan F. [ORNL; Donovan, David C. [ORNL; Kafle, Nischal [ORNL; Martin, Elijah H. [ORNL; Ray, Holly B. [ORNL; Shaw, Guinevere C. [ORNL; Showers, Melissa A. [ORNL

    2017-09-01

    Proto-MPEX is a linear plasma device being used to study a novel RF source concept for the planned Material Plasma Exposure eXperiment (MPEX), which will address plasma-materials interaction (PMI) for nuclear fusion reactors. Plasmas are produced using a large diameter helicon source operating at a frequency of 13.56 MHz at power levels up to 120 kW. In recent experiments the helicon source has produced deuterium plasmas with densities up to ~6 × 1019 m–3 measured at a location 2 m downstream from the antenna and 0.4 m from the target. Previous plasma production experiments on Proto-MPEX have generated lower density plasmas with hollow electron temperature profiles and target power deposition peaked far off axis. The latest experiments have produced flat Te profiles with a large portion of the power deposited on the target near the axis. This and other evidence points to the excitation of a helicon mode in this case.

  18. Radiation sources based on laser-plasma interactions

    NARCIS (Netherlands)

    Jaroszynski, D.A.; Bingham, R.; Brunetti, E.; Ersfeld, B.; Gallacher, J.G.; Geer, van der S.B.; Issac, R.; Jamison, S.P.; Jones, D.; Loos, de M.J.; Lyachev, A.; Pavlov, V.M.; Reitsma, A.J.W.; Saveliev, Y.M.; Vieux, G.; Wiggins, S.M.

    2006-01-01

    Plasma waves excited by intense laser beams can be harnessed to produce femtosecond duration bunches of electrons with relativistic energies. The very large electrostatic forces of plasma density wakes trailing behind an intense laser pulse provide field potentials capable of accelerating charged

  19. Electron attachment mass spectrometry as a diagnostics for electronegative gases and plasmas

    NARCIS (Netherlands)

    Stoffels - Adamowicz, E.; Stoffels, W.W.; Tachibana, K.

    1998-01-01

    Electron attachment mass spectrometry (EAMS) has been developed to study mixtures of electronegative gases and plasmas. A quadrupole mass spectrometer (QMS) has been used to detect negative ions, formed from sampled species by attachment of low energy electrons. Varying the electron energy allows to

  20. On infrared and mass singularities of perturbative QCD in a quark-gluon plasma

    International Nuclear Information System (INIS)

    Altherr, T.; Aurenche, P.; Becherrawy, T.

    1988-07-01

    We discuss the radiative corrections to the production of lepton pairs in a quark-gluon plasma at finite temperature. The real-time formalism is used throughout the calculations. We show that both infrared and mass singularities cancel in the final result. In contrast to the zero-temperature case, no factorization theorem is required to deal with mass singularities

  1. Flux compression generators as plasma compression power sources

    International Nuclear Information System (INIS)

    Fowler, C.M.; Caird, R.S.; Erickson, D.J.; Freeman, B.L.; Thomson, D.B.; Garn, W.B.

    1979-01-01

    A survey is made of applications where explosive-driven magnetic flux compression generators have been or can be used to directly power devices that produce dense plasmas. Representative examples are discussed that are specific to the theta pinch, the plasma gun, the dense plasma focus and the Z pinch. These examples are used to illustrate the high energy and power capabilities of explosive generators. An application employing a rocket-borne, generator-powered plasma gun emphasizes the size and weight potential of flux compression power supplies. Recent results from a local effort to drive a dense plasma focus are provided. Imploding liners ae discussed in the context of both the theta and Z pinches

  2. Comparison in the analytical performance between krypton and argon glow discharge plasmas as the excitation source for atomic emission spectrometry.

    Science.gov (United States)

    Wagatsuma, Kazuaki

    2009-04-01

    The emission characteristics of ionic lines of nickel, cobalt, and vanadium were investigated when argon or krypton was employed as the plasma gas in glow discharge optical emission spectrometry. A dc Grimm-style lamp was employed as the excitation source. Detection limits of the ionic lines in each iron-matrix alloy sample were compared between the krypton and the argon plasmas. Particular intense ionic lines were observed in the emission spectra as a function of the discharge gas (krypton or argon), such as the Co II 258.033 nm for krypton and the Co II 231.707 nm for argon. The explanation for this is that collisions with the plasma gases dominantly populate particular excited levels of cobalt ion, which can receive the internal energy from each gas ion selectively, for example, the 3d(7)4p (3)G(5) (6.0201 eV) for krypton and the 3d(7)4p (3)G(4) (8.0779 eV) for argon. In the determination of nickel as well as cobalt in iron-matrix samples, more sensitive ionic lines could be found in the krypton plasma rather than the argon plasma. Detection limits in the krypton plasma were 0.0039 mass% Ni for the Ni II 230.299-nm line and 0.002 mass% Co for the Co II 258.033-nm line. However, in the determination of vanadium, the argon plasma had better analytical performance, giving a detection limit of 0.0023 mass% V for the V II 309.310-nm line.

  3. Plasma potentials and performance of the advanced electron cyclotron resonance ion source

    International Nuclear Information System (INIS)

    Xie, Z.Q.; Lyneis, C.M.

    1994-01-01

    The mean plasma potential was measured on the LBL advanced electron cyclotron resonance (AECR) ion source for a variety of conditions. The mean potentials for plasmas of oxygen, argon, and argon mixed with oxygen in the AECR were determined. These plasma potentials are positive with respect to the plasma chamber wall and are on the order of tens of volts. Electrons injected into the plasma by an electron gun or from an aluminum oxide wall coating with a very high secondary electron emission reduce the plasma potential as does gas mixing. A lower plasma potential in the AECR source coincides with enhanced production of high charged state ions indicating longer ion confinement times. The effect of the extra electrons from external injection or wall coatings is to lower the average plasma potential and to increase the n e τ i of the ECR plasma. With sufficient extra electrons, the need for gas mixing can be eliminated or reduced to a lower level, so the source can operate at lower neutral pressures. A reduction of the neutral pressure decreases charge exchange between ions and neutrals and enhances the production of high charge state ions. An aluminum oxide coating results in the lowest plasma potential among the three methods discussed and the best source performance

  4. Plasma jet source parameter optimisation and experiments on injection into Globus-M spherical tokamak

    International Nuclear Information System (INIS)

    Gusev, V.K.; Petrov, Yu.V.; Sakharov, N.V.; Semenov, A.A.; Voronin, A.V.

    2005-01-01

    Results of theoretical and experimental research on the plasma sources and injection of plasma and gas jet produced by the modified source into tokamak Globus-M are presented. An experimental test stand was developed for investigation of intense plasma jet generation. Optimisation of pulsed coaxial accelerator parameters by means of analytical calculations is performed with the aim of achieving the highest flow velocity at limited coaxial electrode length and discharge current. The optimal parameters of power supply to generate a plasma jet with minimal impurity contamination and maximum flow velocity were determined. A comparison of experimental and calculation results is made. Plasma jet parameters are measured, such as: impurity species content, pressure distribution across the jet, flow velocity, plasma density, etc. Experiments on the interaction of a higher kinetic energy plasma jet with the magnetic field and plasma of the Globus-M tokamak were performed. Experimental results on plasma and gas jet injection into different Globus-M discharge phases are presented and discussed. Results are presented on the investigation of plasma jet injection as the source for discharge breakdown, plasma current startup and initial density rise. (author)

  5. Field distribution of a source and energy absorption in an inhomogeneous magneto-active plasma

    International Nuclear Information System (INIS)

    Galushko, N.P.; Erokhin, N.S.; Moiseev, S.S.

    1975-01-01

    In the present paper the distribution of source fields in in a magnetoactive plasma is studied from the standpoint of the possibility of an effective SHF heating of an inhomogeneous plasma in both high (ωapproximatelyωsub(pe) and low (ωapproximatelyωsub(pi) frequency ranges, where ωsub(pe) and ωsub(pi) are the electron and ion plasma frequencies. The localization of the HF energy absorption regions in cold and hot plasma and the effect of plasma inhomogeneity and source dimensions on the absorption efficiency are investigated. The linear wave transformation in an inhomogeneous hot plasma is taken into consideration. Attention is paid to the difference between the region localization for collisional and non-collisional absorption. It has been shown that the HF energy dissipation in plasma particle collisions is localized in the region of thin jets going from the source; the radiation field has a sharp peak in this region. At the same time, non-collisional HF energy dissipation is spread over the plasma volume as a result of Cherenkov and cyclotron wave attenuation. The essential contribution to the source field from resonances due to standing wave excitation in an inhomogeneous plasma shell near the source is pointed out

  6. Centrifugal mass separation in rotating plasmas produced by a coaxial plasma gun

    International Nuclear Information System (INIS)

    Ikehata, T.; Suzuki, M.; Tanabe, T.; Mase, H.

    1989-01-01

    Rotating Cu/Zn plasmas produced by a coaxial plasma gun have been applied to plasma centrifuge. A separation factor of up to 10 is measured over a radius of 4 cm when a current of 13 kA and an axial magnetic field of 2.5 kG are applied. Plasma parameters are: rotation frequency ω=1.1x10 6 rad/s, density n∼10 15 cm -3 , and ion temperature T i =10 eV. The separation factor of 2 is attained even in the plasma core where the density is higher than one-half of the peak value. This is attributed to the fact that a strong centrifugal force forms a hollow density profile which gives the density peak at a radius of 2 cm

  7. Mass spectrometric identification of diagnostic markers for chronic prostatitis in seminal plasma by analysis of seminal plasma protein clinical samples.

    Science.gov (United States)

    Rokka, A; Mehik, A; Tonttila, P; Vaarala, M

    2017-08-15

    There are few specific diagnostic markers for chronic prostatitis. Therefore, we used mass spectrometry to evaluate differences in seminal plasma protein expression among patients with prostatitis and young and middle-aged healthy controls. We analysed pooled seminal plasma protein samples from four prostatitis patients (two pools), three young controls (one pool), and three middle-aged controls (one pool). The samples were analysed by liquid chromatography-tandem mass spectrometry. Of the 349 proteins identified, 16 were differentially expressed between the two control pools. Five proteins were up- or down-regulated in both of the prostatitis pools compared to middle-aged controls but not between young and middle-aged pools. Progestagen-associated endometrial protein (PAEP) was over-expressed in prostatitis samples compared to young and middle-aged controls. Our findings and those of previous studies indicate that PAEP is a potential seminal plasma marker for chronic prostatitis. In conclusion, we found age-related changes in seminal plasma protein expression. PAEP expression in seminal plasma should be investigated further to evaluate its potential as a diagnostic marker for chronic prostatitis.

  8. Extractive alkylation of 6-mercaptopurine and determination in plasma by gas chromatography-mass spectrometry.

    Science.gov (United States)

    Floberg, S; Hartvig, P; Lindström, B; Lönner-Holm, G; Odlind, B

    1981-09-11

    An analytical procedure was developed for the determination of 6-mercaptopurine in plasma. Owing to the polar character and low plasma concentration of the compound, extraction and derivatization was carried out directly from the plasma sample by extractive alkylation. Determination was made using gas chromatography-mass spectrometry with multiple-ion detection. Conditions with respect to the rate of formation and the stability of the derivative formed in the extractive alkylation step were evaluated. The selectively of the method to azathioprine and to metabolites was thoroughly investigated. No 6-mercaptopurine was formed from azathioprine added to water or plasma and run through the method. The method enables the detection of 2 ng of 6 mercaptopurine in a 1.0-ml plasma sample. Quantitative determinations were done down to 10 ng/ml 6 mercaptopurine in plasma.

  9. Source formulation for electron-impact ionization for fluid plasma simulations

    DEFF Research Database (Denmark)

    Müller, S.H.; Holland, C.; Tynan, G.R.

    2009-01-01

    The derivation of the correct functional form of source terms in plasma fluid theory is revisited. The relation between the fluid source terms and atomic physics differential cross sections is established for particle-impact ionization. It is shown that the interface between atomic and plasma phy...... electron temperature regimes in a wide variety of basic plasma physics experiments, including the trends across different gases.......The derivation of the correct functional form of source terms in plasma fluid theory is revisited. The relation between the fluid source terms and atomic physics differential cross sections is established for particle-impact ionization. It is shown that the interface between atomic and plasma...... physics is completely described by three scalar functions of the incident particle energy. These are the total cross section and the newly introduced forward momentum and energy functions, which are properties of the differential cross sections only. For electron-impact ionization, the binary...

  10. Material impacts and heat flux characterization of an electrothermal plasma source with an applied magnetic field

    Science.gov (United States)

    Gebhart, T. E.; Martinez-Rodriguez, R. A.; Baylor, L. R.; Rapp, J.; Winfrey, A. L.

    2017-08-01

    To produce a realistic tokamak-like plasma environment in linear plasma device, a transient source is needed to deliver heat and particle fluxes similar to those seen in an edge localized mode (ELM). ELMs in future large tokamaks will deliver heat fluxes of ˜1 GW/m2 to the divertor plasma facing components at a few Hz. An electrothermal plasma source can deliver heat fluxes of this magnitude. These sources operate in an ablative arc regime which is driven by a DC capacitive discharge. An electrothermal source was configured with two pulse lengths and tested under a solenoidal magnetic field to determine the resulting impact on liner ablation, plasma parameters, and delivered heat flux. The arc travels through and ablates a boron nitride liner and strikes a tungsten plate. The tungsten target plate is analyzed for surface damage using a scanning electron microscope.

  11. Plasma ignition and steady state simulations of the Linac4 H$^{-}$ ion source

    CERN Document Server

    Mattei, S; Yasumoto, M; Hatayama, A; Lettry, J; Grudiev, A

    2014-01-01

    The RF heating of the plasma in the Linac4 H- ion source has been simulated using an Particle-in-Cell Monte Carlo Collision method (PIC-MCC). This model is applied to investigate the plasma formation starting from an initial low electron density of 1012 m-3 and its stabilization at 1018 m-3. The plasma discharge at low electron density is driven by the capacitive coupling with the electric field generated by the antenna, and as the electron density increases the capacitive electric field is shielded by the plasma and induction drives the plasma heating process. Plasma properties such as e-/ion densities and energies, sheath formation and shielding effect are presented and provide insight to the plasma properties of the hydrogen plasma.

  12. Development of a 1-m plasma source for heavy ion beam charge neutralization

    Science.gov (United States)

    Efthimion, Philip C.; Gilson, Erik P.; Grisham, Larry; Davidson, Ronald C.; Yu, Simon; Waldron, William; Grant Logan, B.

    2005-05-01

    Highly ionized plasmas are being employed as a medium for charge neutralizing heavy ion beams in order to focus to a small spot size. Calculations suggest that plasma at a density of 1-100 times the ion beam density and at a length ˜0.1-1 m would be suitable for achieving a high level of charge neutralization. A radio frequency (RF) source was constructed at the Princeton Plasma Physics Laboratory (PPPL) in support of the joint Neutralized Transport Experiment (NTX) at the Lawrence Berkeley National Laboratory (LBNL) to study ion beam neutralization. Pulsing the source enabled operation at pressures ˜10 -6 Torr with plasma densities of 10 11 cm -3. Near 100% ionization was achieved. The plasma was 10 cm in length, but future experiments require a source 1 m long. The RF source does not easily scale to the length. Consequently, large-volume plasma sources based upon ferroelectric ceramics are being considered. These sources have the advantage of being able to increase the length of the plasma and operate at low neutral pressures. The source will utilize the ferroelectric ceramic BaTiO 3 to form metal plasma. A 1 m long section of the drift tube inner surface of NTX will be covered with ceramic. A high voltage (˜1-5 kV) is applied between the drift tube and the front surface of the ceramic by placing a wire grid on the front surface. Plasma densities of 10 12 cm -3 and neutral pressures ˜10 -6 Torr are expected. A test stand to produce 20 cm long plasma is being constructed and will be tested before a 1 m long source is developed.

  13. Development of a 1-m plasma source for heavy ion beam charge neutralization

    International Nuclear Information System (INIS)

    Efthimion, Philip C.; Gilson, Erik P.; Grisham, Larry; Davidson, Ronald C.; Yu, Simon; Waldron, William; Grant Logan, B.

    2005-01-01

    Highly ionized plasmas are being employed as a medium for charge neutralizing heavy ion beams in order to focus to a small spot size. Calculations suggest that plasma at a density of 1-100 times the ion beam density and at a length ∼0.1-1 m would be suitable for achieving a high level of charge neutralization. A radio frequency (RF) source was constructed at the Princeton Plasma Physics Laboratory (PPPL) in support of the joint Neutralized Transport Experiment (NTX) at the Lawrence Berkeley National Laboratory (LBNL) to study ion beam neutralization. Pulsing the source enabled operation at pressures ∼10 -6 Torr with plasma densities of 10 11 cm -3 . Near 100% ionization was achieved. The plasma was 10 cm in length, but future experiments require a source 1 m long. The RF source does not easily scale to the length. Consequently, large-volume plasma sources based upon ferroelectric ceramics are being considered. These sources have the advantage of being able to increase the length of the plasma and operate at low neutral pressures. The source will utilize the ferroelectric ceramic BaTiO 3 to form metal plasma. A 1 m long section of the drift tube inner surface of NTX will be covered with ceramic. A high voltage (∼1-5 kV) is applied between the drift tube and the front surface of the ceramic by placing a wire grid on the front surface. Plasma densities of 10 12 cm -3 and neutral pressures ∼10 -6 Torr are expected. A test stand to produce 20 cm long plasma is being constructed and will be tested before a 1 m long source is developed

  14. Determination of nifedipine in dog plasma by high-performance liquid chromatography with tandem mass spectrometric detection.

    Science.gov (United States)

    Pan, Xigui; Zhou, Shunchang; Fu, Qinqin; Hu, Xianming; Wu, Jianhong

    2014-07-01

    Nifedipine is a dihydropyridine calcium channel blocker used widely in the management of hypertension and other cardiovascular disorders. In this work, a simple, rapid and sensitive liquid chromatography/tandem mass spectrometry method was developed and validated to determine nifedipine in dog plasma using nimodipine as the internal standard. Chromatographic separation was carried out on a C₈ column. The mobile phase consisted of a mixture of acetonitrile, water and formic acid (60:40:0.2, v/v/v) at a flow rate of 0.5 mL/min. Detection was performed on a triple quadrupole tandem mass spectrometer in selected reaction monitoring mode via an atmospheric pressure chemical ionization source. The method has a lower limit of quantification of 0.20 ng/mL with consumption of plasma as low as 0.05 mL. The linear calibration curves were obtained in the concentration range of 0.20-50.0 ng/mL (r = 0.9948). The recoveries of the liquid extraction method were 74.5-84.1%. Intra-day and inter-day precisions were 4.1-8.8 and 6.7-7.4%, respectively. The quantification was not interfered with by other plasma components and the method was applied to determine nifedipine in plasma after a single oral administration of two controlled-release nifedipine tablets to beagle dogs. Copyright © 2013 John Wiley & Sons, Ltd.

  15. Plasma Instability Based Compact Coherent Terahertz Radiation Sources

    National Research Council Canada - National Science Library

    Bakshi, P

    2004-01-01

    .... These are in good agreement with experiments carried out at TU Vienna. A sharp emission line was obtained in the most recent structure, suggesting that we are close to the onset of plasma instability...

  16. QSARs for Plasma Protein Binding: Source Data and Predictions

    Data.gov (United States)

    U.S. Environmental Protection Agency — The dataset has all of the information used to create and evaluate 3 independent QSAR models for the fraction of a chemical unbound by plasma protein (Fub) for...

  17. Plasma X-ray sources powered by megajoule magnetocumulative generators

    Energy Technology Data Exchange (ETDEWEB)

    Popkov, N F; Averchenkov, V Ya; Pikar` , A S; Ryaslov, E A; Kargin, V I; Lazarev, S A; Borodkov, V V; Nazarenko, S T; Makartsev, G F [All-Russian Research Inst. of Experimental Physics, Sarov (Russian Federation). Russian Federal Nuclear Center

    1997-12-31

    Experiments using magnetocumulative generators (MCGs) were performed to power three different types of high-energy-density plasma discharges suitable for intense x-ray generation. These included the H-pressed discharge, the capillary z-pinch, and the {theta}-pinch. The MCGs were operated both with and without plasma opening switches. The characteristic currents were approximately 10 MA and characteristic time scales approximately 1 {mu}s. (author). 7 figs., 3 refs.

  18. A 14-MeV beam-plasma neutron source for materials testing

    International Nuclear Information System (INIS)

    Futch, A.H.; Coensgen, F.H.; Damm, C.C.; Molvik, A.W.

    1989-01-01

    The design and performance of 14-MeV beam-plasma neutron sources for accelerated testing of fusion reactor materials are described. Continuous production of 14-MeV neutron fluxes in the range of 5 to 10 MW/m 2 at the plasma surface are produced by D-T reactions in a two-component plasma. In the present designs, 14-MeV neutrons result from collisions of energetic deuterium ions created by transverse injection of 150-keV deuterium atoms on a fully ionized tritium target plasma. The beam energy, which deposited at the center of the tritium column, is transferred to the warm plasma by electron drag, which flows axially to the end regions. Neutral gas at high pressure absorbs the energy in the tritium plasma and transfers the heat to the walls of the vacuum vessel. The plasma parameters of the neutron source, in dimensionless units, have been achieved in the 2XIIB high-β plasma. The larger magnetic field of the present design permits scaling to the higher energy and density of the neutron source design. In the extrapolation, care has been taken to preserve the scaling and plasma attributes that contributed to equilibrium, magnetohydrodynamic (MHD) stability, and microstability in 2XIIB. The performance and scaling characteristics are described for several designs chosen to enhance the thermal isolation of the two-component plasmas. 11 refs., 3 figs., 3 tabs

  19. Radiation from a pulsed dipole source in a moving magnetized plasma

    International Nuclear Information System (INIS)

    Gavrilenko, V. G.; Petrov, E. Yu.; Pikulin, V. D.; Sutyagina, D. A.

    2006-01-01

    The problem of radiation from a pulsed dipole source in a moving magnetized plasma described by a diagonal permittivity tensor is considered. An exact solution describing the spatiotemporal behavior of the excited electromagnetic field is obtained. The shape of an electromagnetic pulse that is generated by the source and propagates at different angles to both the direction of the external magnetic field and the direction of plasma motion is investigated. It is found that even nonrelativistic motion of the plasma medium can substantially influence the parameters of radiation from prescribed unsteady sources

  20. Determination of plasma spot current and arc discharge plasma current on the system of plasma cathode electron sources using Rogowski coil technique

    International Nuclear Information System (INIS)

    Wirjoadi; Bambang Siswanto; Lely Susita RM; Agus Purwadi; Sudjatmoko

    2015-01-01

    It has been done the function test experiments of ignitor electrode system and the plasma generator electrode system to determine the current spot plasma and arc discharge plasma current with Rogowski coil technique. Ignitor electrode system that gets power supply from IDPS system can generate the plasma spot current of 11.68 ampere to the pulse width of about 33 μs, this value is greater than the design probably because of electronic components used in the IDPS system was not as planned. For the plasma generator electrode system that gets power from ADPS system capable of producing an arc discharge plasma current around 103.15 amperes with a pulse width of about 96 μs, and this value as planned. Based on the value of the arc discharge plasma current can be determined plasma electron density, which is about 10.12 10"1"9 electrons/m"3, and with this electron density value, an ignitor electrode system and a plasma generator system is quite good if used as a plasma cathode electron source system. (author)

  1. Determination of clebopride in plasma by capillary gas chromatography-negative-ion chemical ionization mass spectrometry.

    Science.gov (United States)

    Robinson, P R; Jones, M D; Maddock, J

    1988-11-18

    A procedure for the analysis of clebopride in plasma using capillary gas chromatography-negative-ion chemical ionization mass spectrometry has been developed. Employing an ethoxy analogue as internal standard, the two compounds were extracted from basified plasma using dichloromethane. Subsequent reaction with heptafluorobutyryl imidazole produced volatile monoheptafluorobutyryl derivatives whose ammonia negative-ion mass spectra proved ideal for selected-ion monitoring. The recovery of clebopride from plasma at 0.536 nmol/l was found to be 85.5 +/- 0.9% (n = 3) whilst measurement down to 0.268 nmol/l was possible with a coefficient of variation of 7.9%. Plasma levels of the compound are reported in two volunteers following ingestion of 1 mg of clebopride as the malate salt.

  2. The Effects of Muscle Mass on Homocyst(e)ine Levels in Plasma and Urine.

    Science.gov (United States)

    Malinow, M René; Lister, Craig L; DE Crée, Carl

    The present study was designed to examine the relationship between homocyst(e)ine (H[e]) levels and muscle mass. Two experimental groups each of 24 Caucasian males, one consisting of higher-muscle mass subjects (HMM) and the other of lower-muscle mass subjects (LMM) participated in this study. Muscle mass was estimated from 24-hour urine collections of creatinine (Crt). Muscle mass was 40.3 ± 15.9 kg in HMM and 37.2 ± 11.4 kg in LMM (P= 0.002). Mean plasma H(e) levels in HMM were 10.29 ± 2.9 nmol/mL, and in LMM were 10.02 ± 2.4 nmol/L (Not significant, [NS]). Urinary H(e) levels (UH[e]) were 9.95 ± 4.3 nmol/mL and 9.22 ± 2.9 nmol/mL for HMM and LMM, respectively (NS). Plasma H(e) levels correlated well with UH(e) (HMM: r= 0.58, P= 0.009; LMM: r= 0.66, P= 0.004). Muscle mass and was not correlated to either plasma H(e) or UH(e). However, in HMM trends were identified for body mass to be correlated with UH(e) (r= 0.39, P= 0.10) and UCrt (r= 0.41, P= 0.08). Surprisingly, in HMM plasma and UCrt were only weakly correlated (r= 0.44, P= 0.06). Our results do not support a causal relationship between the amount of muscle mass and H(e) levels in plasma or urine.

  3. Development of zeolite ion source for beam probe measurements of high temperature plasma

    International Nuclear Information System (INIS)

    Ohshima, Shinsuke; Fujisawa, Akihide; Shimizu, Akihiro; Nakano, Haruhisa

    2005-10-01

    A zeolite ion source has been developed for plasma diagnostics. Extracted beam current is increased by a factor of ∼10 after redesigning the ion source structure and improving the method to make emitter material (zeolite). The paper introduces an experiment on making desirable ion emitter, together with properties of the newly developed ion source. (author)

  4. Radioimmunoassay and chemical ionization/mass spectrometry compared for plasma cortisol determination

    International Nuclear Information System (INIS)

    Lindberg, C.; Johnson, S.; Hedner, P.; Gustafsson, A.

    1982-01-01

    A method is described for determination of cortisol in plasma and urine, based on chemical ionization/mass spectrometry with deuterium-labeled cortisol as the internal standard. The within-run precision (CV) was 2.5-5.7%, the between-run precision 4.6%. Results by this method were compared with those by a radioimmunological method (RIANEN Cortisol, New England Nuclear) for 395 plasma samples. The latter method gave significantly higher (approx. 25%) cortisol values

  5. Combustion flame-plasma hybrid reactor systems, and chemical reactant sources

    Science.gov (United States)

    Kong, Peter C

    2013-11-26

    Combustion flame-plasma hybrid reactor systems, chemical reactant sources, and related methods are disclosed. In one embodiment, a combustion flame-plasma hybrid reactor system comprising a reaction chamber, a combustion torch positioned to direct a flame into the reaction chamber, and one or more reactant feed assemblies configured to electrically energize at least one electrically conductive solid reactant structure to form a plasma and feed each electrically conductive solid reactant structure into the plasma to form at least one product is disclosed. In an additional embodiment, a chemical reactant source for a combustion flame-plasma hybrid reactor comprising an elongated electrically conductive reactant structure consisting essentially of at least one chemical reactant is disclosed. In further embodiments, methods of forming a chemical reactant source and methods of chemically converting at least one reactant into at least one product are disclosed.

  6. Permanent magnet electron cyclotron resonance plasma source with remote window

    International Nuclear Information System (INIS)

    Berry, L.A.; Gorbatkin, S.M.

    1995-01-01

    An electron cyclotron resonance (ECR) plasma has been used in conjunction with a solid metal sputter target for Cu deposition over 200 mm diameters. The goal is to develop a deposition system and process suitable for filling submicron, high-aspect ratio ULSI features. The system uses a permanent magnet for creation of the magnetic field necessary for ECR, and is significantly more compact than systems equipped with electromagnets. A custom launcher design allows remote microwave injection with the microwave entrance window shielded from the copper flux. When microwaves are introduced at an angle with respect to the plasma, high electron densities can be produced with a plasma frequency significantly greater than the electron cyclotron frequency. Copper deposition rates of 1000 A/min have been achieved

  7. Shaping the electron beams with submicrosecond pulse duration in sources and electron accelerators with plasma emitters

    CERN Document Server

    Gushenets, V I

    2001-01-01

    One studies the techniques in use to shape submicrosecond electron beams and the physical processes associated with extraction of electrons from plasma in plasma emitters. Plasma emitter base sources and accelerators enable to generate pulse beams with currents varying from tens of amperes up to 10 sup 3 A, with current densities up to several amperes per a square centimeter, with pulse duration constituting hundreds of nanoseconds and with high frequencies of repetition

  8. Abnormally large energy spread of electron beams extracted from plasma sources

    Energy Technology Data Exchange (ETDEWEB)

    Winter, H [Technische Univ., Vienna (Austria). Inst. fuer Allgemeine Physik

    1976-07-01

    Intense electron beams extracted from DUOPLASMATRON-plasma cathodes show a high degree of modulation in intensity and an abnormally large energy spread; these facts cannot be explained simply by the temperature of the plasma electrons and the discharge structure. However, an analysis of the discharge stability behaviour and the interaction of source- and extracted beam-plasma leads to an explanation for the observed effects.

  9. Formation of Nitrogen Oxides in an Apokamp-Type Plasma Source

    Science.gov (United States)

    Sosnin, É. A.; Goltsova, P. A.; Panarin, V. A.; Skakun, V. S.; Tarasenko, V. F.; Didenko, M. V.

    2017-08-01

    Using optical and chemical processes, the composition of the products of decay of the atmospheric-pressure non-equilibrium plasma is determined in a pulsed, high-voltage discharge in the modes of apokampic and corona discharges. It is shown that the products of decay primarily contain nitrogen oxides NO x, and in the mode of the corona discharge - ozone. Potential applications of this source of plasma are discussed with respect to plasma processing of the seeds of agricultural crops.

  10. Characterization of an atmospheric pressure air plasma source for polymer surface modification

    Science.gov (United States)

    Yang, Shujun; Tang, Jiansheng

    2013-10-01

    An atmospheric pressure air plasma source was generated through dielectric barrier discharge (DBD). It was used to modify polyethyleneterephthalate (PET) surfaces with very high throughput. An equivalent circuit model was used to calculate the peak average electron density. The emission spectrum from the plasma was taken and the main peaks in the spectrum were identified. The ozone density in the down plasma region was estimated by Absorption Spectroscopy. NSF and ARC-ODU

  11. An Open Source Computational Framework for Uncertainty Quantification of Plasma Chemistry Models

    OpenAIRE

    Zaheri Sarabi, Shadi

    2017-01-01

    The current thesis deals with the development of a computational framework for performing plasma chemistry simulations and their uncertainty quantification analysis by suitably combining and extending existing open source computational tools. A plasma chemistry solver is implemented in the OpenFOAM C++ solver suite. The OpenFOAM plasma chemistry application solves the species conservation equations and the electron energy equation by accounting suitably for various production and loss terms b...

  12. Ion acoustic double layers in the presence of plasma source

    International Nuclear Information System (INIS)

    Okuda, H.; Ashour-Abdalla, M.

    1982-01-01

    Steady-state plasma turbulence and the formation of negative potential spikes and double layers in the presence of ion acoustic instabilities have been studied by means of one-dimensional particle simulations in which the velocities of a small fraction of electrons are replaced by the initial drifting Maxwellian at a constant rate. A steady state is found where negative potential spikes appear randomly in space and time giving rise to an anomalous resistivity much greater than previously found. Comparisons of the simulation results with laboratory and space plasmas are discussed

  13. Atmospheric-pressure solution-cathode glow discharge: A versatile ion source for atomic and molecular mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Schwartz, Andrew J. [Department of Chemistry, Indiana University, Bloomington, IN, 47405 (United States); Williams, Kelsey L. [Department of Chemistry and Biochemistry, Kent State University, Kent, OH, 44242 (United States); Hieftje, Gary M. [Department of Chemistry, Indiana University, Bloomington, IN, 47405 (United States); Shelley, Jacob T., E-mail: shellj@rpi.edu [Department of Chemistry and Biochemistry, Kent State University, Kent, OH, 44242 (United States); Department of Chemistry and Chemical Biology, Rensselaer Polytechnic Institute, Troy, NY, 12180 (United States)

    2017-01-15

    An atmospheric-pressure solution-cathode glow discharge (SCGD) has been evaluated as an ion source for atomic, molecular, and ambient desorption/ionization mass spectrometry. The SCGD consists of a direct-current plasma, supported in the ambient air in the absence of gas flows, and sustained upon the surface of a flowing liquid cathode. Analytes introduced in the flowing liquid, as an ambient gas, or as a solid held near the plasma are vaporized and ionized by interactions within or near the discharge. Introduction of acidic solutions containing metal salts produced bare elemental ions as well as H{sub 2}O, OH{sup −} and NO{sub 3}{sup −} adducts. Detection limits for these elemental species ranged from 0.1 to 4 ppb, working curves spanned more than 4 orders of linear dynamic range, and precision varied between 5 and 16% relative standard deviation. Small organic molecules were also efficiently ionized from solution, and both the intact molecular ion and fragments were observed in the resulting SCGD mass spectra. Fragmentation of molecular species was found to be tunable; high discharge currents led to harder ionization, while low discharge currents produced stronger molecular-ion signals. Ambient gases and solids, desorbed by the plasma from a glass probe, were also readily ionized by the SCGD. Indeed, strong analyte signals were obtained from solid samples placed at least 2 cm from the plasma. These findings indicate that the SCGD might be useful also for ambient desorption/ionization mass spectrometry. Combined with earlier results that showed the SCGD is useful for ionization of labile biomolecules, the results here indicate that the SCGD is a highly versatile ion source capable of providing both elemental and molecular mass-spectral information. - Highlights: • Solution-cathode glow discharge used as an ionization source for mass spectrometry. • SCGD-MS can provide atomic as well as intact molecular mass spectra. • Atomic limits of detection range

  14. Low scale gravity as the source of neutrino masses?

    Energy Technology Data Exchange (ETDEWEB)

    Berezinsky, Veniamin [INFN, Laboratori Nazionali del Gran Sasso, I-67010 Assergi, AQ (Italy); Narayan, Mohan [INFN, Laboratori Nazionali del Gran Sasso, I-67010 Assergi, AQ (Italy); Vissani, Francesco [INFN, Laboratori Nazionali del Gran Sasso, I-67010 Assergi, AQ (Italy)

    2005-04-01

    We address the question whether low-scale gravity alone can generate the neutrino mass matrix needed to accommodate the observed phenomenology. In low-scale gravity the neutrino mass matrix in the flavor basis is characterized by one parameter (the gravity scale M{sub X}) and by an exact or approximate flavor blindness (namely, all elements of the mass matrix are of comparable size). Neutrino masses and mixings are consistent with the observational data for certain values of the matrix elements, but only when the spectrum of mass is inverted or degenerate. For the latter type of spectra the parameter M{sub ee} probed in double beta experiments and the mass parameter probed by cosmology are close to existing upper limits.

  15. Low scale gravity as the source of neutrino masses?

    International Nuclear Information System (INIS)

    Berezinsky, Veniamin; Narayan, Mohan; Vissani, Francesco

    2005-01-01

    We address the question whether low-scale gravity alone can generate the neutrino mass matrix needed to accommodate the observed phenomenology. In low-scale gravity the neutrino mass matrix in the flavor basis is characterized by one parameter (the gravity scale M X ) and by an exact or approximate flavor blindness (namely, all elements of the mass matrix are of comparable size). Neutrino masses and mixings are consistent with the observational data for certain values of the matrix elements, but only when the spectrum of mass is inverted or degenerate. For the latter type of spectra the parameter M ee probed in double beta experiments and the mass parameter probed by cosmology are close to existing upper limits

  16. Inductively coupled plasma as atomization, excitation and ionization sources in analytical atomic spectrometry

    International Nuclear Information System (INIS)

    Kawaguchi, Hiroshi

    1996-01-01

    Studies on inductively coupled plasma (ICP) for atomic emission and mass spectrometry accomplished in our laboratory since 1978 are reviewed. In emission spectrometry, the characteristics of the plasma are studied concerning the spatial profiles of spectral line intensity, axial profiles of gas and excitation temperatures, spectral line widths and matrix effect. The studies are particularly emphasized on the instrumentation such as developments of plasma generator, emission spectrometers, water-cooled torches and sample introduction methods. A slew-scan type spectrometer developed in these works represents a predecessor of the current commercial spectrometers. An ICP mass spectrometer was first developed in Japan in this laboratory in 1984. Non-spectroscopic interference of this method was found to have the correlation with the atomic weight of the matrix element. Plasma gases other than argon such as nitrogen and oxygen were used for the ICP to evaluate their performance in mass spectrometry as for the sensitivity and interferences. (author). 63 refs

  17. Direct analysis of samples by mass spectrometry: From elements to bio-molecules using laser ablation inductively couple plasma mass spectrometry and laser desorption/ionization mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Perdian, David C. [Iowa State Univ., Ames, IA (United States)

    2009-01-01

    Mass spectrometric methods that are able to analyze solid samples or biological materials with little or no sample preparation are invaluable to science as well as society. Fundamental research that has discovered experimental and instrumental parameters that inhibit fractionation effects that occur during the quantification of elemental species in solid samples by laser ablation inductively coupled plasma mass spectrometry is described. Research that determines the effectiveness of novel laser desorption/ionization mass spectrometric methods for the molecular analysis of biological tissues at atmospheric pressure and at high spatial resolution is also described. A spatial resolution is achieved that is able to analyze samples at the single cell level.

  18. Injection of auxiliary electrons for increasing the plasma density in highly charged and high intensity ion sources

    Energy Technology Data Exchange (ETDEWEB)

    Odorici, F., E-mail: fabrizio.odorici@bo.infn.it; Malferrari, L.; Montanari, A. [INFN—Bologna, Viale B. Pichat, 6/2, 40127 Bologna (Italy); Rizzoli, R. [INFN—Bologna, Viale B. Pichat, 6/2, 40127 Bologna (Italy); CNR–Istituto per la Microelettronica ed i Microsistemi, Via Gobetti 101, 40129 Bologna (Italy); Mascali, D.; Castro, G.; Celona, L.; Gammino, S.; Neri, L. [INFN–Laboratori Nazionali del Sud, Via S. Sofia 62, 95125 Catania (Italy)

    2016-02-15

    Different electron guns based on cold- or hot-cathode technologies have been developed since 2009 at INFN for operating within ECR plasma chambers as sources of auxiliary electrons, with the aim of boosting the source performances by means of a higher plasma lifetime and density. Their application to microwave discharge ion sources, where plasma is not confined, has required an improvement of the gun design, in order to “screen” the cathode from the plasma particles. Experimental tests carried out on a plasma reactor show a boost of the plasma density, ranging from 10% to 90% when the electron guns are used, as explained by plasma diffusion models.

  19. Injection of auxiliary electrons for increasing the plasma density in highly charged and high intensity ion sources.

    Science.gov (United States)

    Odorici, F; Malferrari, L; Montanari, A; Rizzoli, R; Mascali, D; Castro, G; Celona, L; Gammino, S; Neri, L

    2016-02-01

    Different electron guns based on cold- or hot-cathode technologies have been developed since 2009 at INFN for operating within ECR plasma chambers as sources of auxiliary electrons, with the aim of boosting the source performances by means of a higher plasma lifetime and density. Their application to microwave discharge ion sources, where plasma is not confined, has required an improvement of the gun design, in order to "screen" the cathode from the plasma particles. Experimental tests carried out on a plasma reactor show a boost of the plasma density, ranging from 10% to 90% when the electron guns are used, as explained by plasma diffusion models.

  20. Electron cyclotron resonance plasmas and electron cyclotron resonance ion sources: Physics and technology (invited)

    International Nuclear Information System (INIS)

    Girard, A.; Hitz, D.; Melin, G.; Serebrennikov, K.

    2004-01-01

    Electron cyclotron resonance (ECR) ion sources are scientific instruments particularly useful for physics: they are extensively used in atomic, nuclear, and high energy physics, for the production of multicharged beams. Moreover, these sources are also of fundamental interest for plasma physics, because of the very particular properties of the ECR plasma. This article describes the state of the art on the physics of the ECR plasma related to multiply charged ion sources. In Sec. I, we describe the general aspects of ECR ion sources. Physics related to the electrons is presented in Sec. II: we discuss there the problems of heating and confinement. In Sec. III, the problem of ion production and confinement is presented. A numerical code is presented, and some particular and important effects, specific to ECR ion sources, are shown in Sec. IV. Eventually, in Sec. V, technological aspects of ECR are presented and different types of sources are shown

  1. Bayesian model comparison using Gauss approximation on multicomponent mass spectra from CH4 plasma

    International Nuclear Information System (INIS)

    Kang, H.D.; Dose, V.

    2004-01-01

    We performed Bayesian model comparison on mass spectra from CH4 rf process plasmas to detect radicals produced in the plasma. The key ingredient for its implementation is the high-dimensional evidence integral. We apply Gauss approximation to evaluate the evidence. The results were compared with those calculated by the thermodynamic integration method using Markov Chain Monte Carlo technique. In spite of very large difference in the computation time between two methods a very good agreement was obtained. Alternatively, a Monte Carlo integration method based on the approximated Gaussian posterior density is presented. Its applicability to the problem of mass spectrometry is discussed

  2. Negative ion mass spectra and particulate formation in rf silane plasma deposition experiments

    International Nuclear Information System (INIS)

    Howling, A.A.; Dorier, J.L.; Hollenstein, C.

    1992-09-01

    Negative ions have been clearly identified in silane rf plasmas used for the deposition of amorphous silicon. Mass spectra were measured for monosilicon up to pentasilicon negative ion radical groups in power-modulated plasmas by means of a mass spectrometer mounted just outside the glow region. Negative ions were only observed over a limited range of power modulation frequency which corresponds to particle-free conditions. The importance of negative ions regarding particulate formation is demonstrated and commented upon. (author) 3 figs., 19 refs

  3. Stationary plasma source of heavy ions for imitating research at the separator

    International Nuclear Information System (INIS)

    Yuferov, V.B.; Sharyj, S.V.; Seroshtanov, V.A.

    2008-01-01

    The imitation gas mix choice for experimenting on the demonstration imitation separator have been grounded. The construction of plasma source is changed. The research of operating conditions and contrastive analysis of received characteristics have been carry out

  4. Facility Effects on a Helicon Plasma Source with a Magnetic Nozzle

    Data.gov (United States)

    National Aeronautics and Space Administration — Proposed here is an analysis of facility effects on a small helicon plasma source with a magnetic nozzle. Backpressure effects will first be recorded and analyzed....

  5. ECR plasma source in a flaring magnetic field

    International Nuclear Information System (INIS)

    Meis, C.; Compant La Fontaine, A.; Louvet, P.

    1992-01-01

    The propagation and absorption of an electromagnetic wave, near the electron cyclotron zone, of a cold plasma (T e ∼ 1-5 eV) confined in a flaring magnetic field is studied. The case of both extraordinary and ordinary modes has been considered. Temperature effects and electron-neutral collisions have been taken account in the dielectric tensor

  6. Air spark-like plasma source for antimicrobial NOx generation

    International Nuclear Information System (INIS)

    Pavlovich, M J; Galleher, C; Curtis, B; Clark, D S; Graves, D B; Ono, T; Machala, Z

    2014-01-01

    We demonstrate and analyse the generation of nitrogen oxides and their antimicrobial efficacy using atmospheric air spark-like plasmas. Spark-like discharges in air in a 1 L confined volume are shown to generate NO x at an initial rate of about 1.5  ×  10 16 NO x molecules/J dissipated in the plasma. Such a discharge operating in this confined volume generates on the order of 6000 ppm NO x in 10 min. Around 90% of the NO x is in the form of NO 2 after several minutes of operation in the confined volume, suggesting that NO 2 is the dominant antimicrobial component. The strong antimicrobial action of the NO x mixture after several minutes of plasma operation is demonstrated by measuring rates of E. coli disinfection on surfaces and in water exposed to the NO x mixture. Some possible applications of plasma generation of NO x (perhaps followed by dissolution in water) include disinfection of surfaces, skin or wound antisepsis, and sterilization of medical instruments at or near room temperature. (paper)

  7. Nuclear Malaysia Plasma Focus Device as a X-ray Source For Radiography Applications

    International Nuclear Information System (INIS)

    Rokiah Mohd Sabri; Abdul Halim Baijan; Siti Aiasah Hashim; Mohd Rizal Mohd Chulan; Wah, L.K.; Mukhlis Mokhtar; Azaman Ahmad; Rosli Che Ros

    2013-01-01

    A 3.375 kJ plasma focus is designed to operate at 13.5 kV for the purpose of studying x-ray source for radiography in Argon discharge. X-rays is detected by using x-ray film from the mammography radiographic plate. The feasibility of the plasma focus as a high intensity flash x-ray source for good contrast in radiography image is presented. (author)

  8. Two new planar coil designs for a high pressure radio frequency plasma source

    Science.gov (United States)

    Munsat, T.; Hooke, W. M.; Bozeman, S. P.; Washburn, S.

    1995-04-01

    Two planar coil designs for a high pressure rf plasma source are investigated using spectroscopic techniques and circuit analysis. In an Ar plasma a truncated version of the commonly used ``spiral'' coil is found to produce improvements in peak electron density of 20% over the full version. A coil with figure-8 geometry is found to move plasma inhomogeneities off of center and produce electron densities comparable to the spiral coils. Both of these characteristics are advantageous in industrial applications. Coil design characteristics for favorable power coupling are also determined, including the necessity of closed hydrodynamic plasma loops and the drawback of closely situated antiparallel coil currents.

  9. Performance of the CERN plasma lens in laboratory and beam tests at the Antiproton Source

    International Nuclear Information System (INIS)

    Kowalewicz, R.; Lubrano di Scampamorte, M.; Milner, S.; Pedersen, F.; Riege, H.; Christiansen, J.; Frank, K.; Stetter, M.; Tkotz, R.; Boggasch, E.

    1991-01-01

    The CERN plasma lens is based on a dynamic z-pinch which creates during 500 ns a cylindrical plasma current conductor of 290 mm length and 38 to 45 mm diameter. The lens is designed for pulsed pinched currents of 400 kA and magnetic field gradients of 200 T/m produced with stored energies of 56 kJ. Life tests of different lens components were carried through at a repetition rate of 4.8 s/pulse. The results of the first beam tests of the plasma lens at the CERN antiproton source are very encouraging in view of other potential plasma lens applications

  10. Ion source plasma parameters measurement based on Langmuir probe with commercial frequency sweep

    International Nuclear Information System (INIS)

    Xie, Y.H.; Hu, C.D.; Liu, S.; Shong, S.H.; Jiang, C.C.; Liu, Z.M.

    2010-01-01

    Langmuir probe is one of the main diagnostic tools to measure the plasma parameters in the ion source. In this article, the commercial frequency power, which is sine wave of 50 Hz, was supplied on the Langmuir probe to measure the plasma parameters. The best feature of this probe sweep voltage is that it does not need extra design. The probe I-V characteristic curve can be got in less than 5 ms and the plasma parameters, the electron temperature and the electron density, varying with the time can be got in one plasma discharge of 400 ms.

  11. Investigations into the origins of polyatomic ions in inductively coupled plasma-mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    McIntyre, Sally M. [Iowa State Univ., Ames, IA (United States)

    2010-01-01

    An inductively coupled plasma-mass spectrometer (ICP-MS) is an elemental analytical instrument capable of determining nearly all elements in the periodic table at limits of detection in the parts per quadrillion and with a linear analytical range over 8-10 orders of magnitude. Three concentric quartz tubes make up the plasma torch. Argon gas is spiraled through the outer tube and generates the plasma powered by a looped load coil operating at 27.1 or 40.6 MHz. The argon flow of the middle channel is used to keep the plasma above the innermost tube through which solid or aqueous sample is carried in a third argon stream. A sample is progressively desolvated, atomized and ionized. The torch is operated at atmospheric pressure. To reach the reduced pressures of mass spectrometers, ions are extracted through a series of two, approximately one millimeter wide, circular apertures set in water cooled metal cones. The space between the cones is evacuated to approximately one torr. The space behind the second cone is pumped down to, or near to, the pressure needed for the mass spectrometer (MS). The first cone, called the sampler, is placed directly in the plasma plume and its position is adjusted to the point where atomic ions are most abundant. The hot plasma gas expands through the sampler orifice and in this expansion is placed the second cone, called the skimmer. After the skimmer traditional MS designs are employed, i.e. quadrupoles, magnetic sectors, time-of-flight. ICP-MS is the leading trace element analysis technique. One of its weaknesses are polyatomic ions. This dissertation has added to the fundamental understanding of some of these polyatomic ions, their origins and behavior. Although mainly continuing the work of others, certain novel approaches have been introduced here. Chapter 2 includes the first reported efforts to include high temperature corrections to the partition functions of the polyatomic ions in ICP-MS. This and other objections to preceeding

  12. X-ray radiation source based on a plasma filled diode

    Energy Technology Data Exchange (ETDEWEB)

    Popkov, N F; Kargin, V I; Ryaslov, E A; Pikar, A S [All-Russian Research Inst. of Experimental Physics, Sarov (Russian Federation). Russian Federal Nuclear Center

    1997-12-31

    The results are given of studies on a plasma X-ray source providing 2.5 krad of radiation dose per pulse over an area of 100 cm{sup 2} in the quantum energy range between 20 and 500 keV. The pulse duration was 100 ns. The spectral radiation distribution was obtained under various operating conditions of plasma and diode. A Marx generator served as the starting power source of 120 kJ with a discharge time of T/4=10{sup -6} s. A short electromagnetic pulse (10{sup -7} s) was shaped using plasma erosion opening switches. (author). 5 figs., 4 refs.

  13. Microwave plasma source for neutral-beam injection systems. Quarterly technical progress report

    International Nuclear Information System (INIS)

    1981-01-01

    The overall program is described and the technical and programmatic reasons for the decision to pursue both the RFI and ECH sources into the current hydrogen test stage is discussed. We consider the general characteristics of plasma sources in the parameter regime of interest for neutral beam applications. The operatonal characteristics, advantages and potential problems of RFI and ECH sources are discussed. In these latter two sections we rely heavily on experience derived from developing RFI and ECH ion engine sources for NASA

  14. Impurities, temperature, and density in a miniature electrostatic plasma and current source

    International Nuclear Information System (INIS)

    Den Hartog, D.J.; Craig, D.J.; Fiksel, G.; Sarff, J.S.

    1996-10-01

    We have spectroscopically investigated the Sterling Scientific miniature electrostatic plasma source-a plasma gun. This gun is a clean source of high density (10 19 - 10 20 m -3 ), low temperature (5 - 15 eV) plasma. A key result of our investigation is that molybdenum from the gun electrodes is largely trapped in the internal gun discharge; only a small amount escapes in the plasma flowing out of the gun. In addition, the gun plasma parameters actually improve (even lower impurity contamination and higher ion temperature) when up to 1 kA of electron current is extracted from the gun via the application of an external bias. This improvement occurs because the internal gun anode no longer acts as the current return for the internal gun discharge. The gun plasma is a virtual plasma electrode capable of sourcing an electron emission current density of 1 kA/cm 2 . The high emission current, small size (3 - 4 cm diameter), and low impurity generation make this gun attractive for a variety of fusion and plasma technology applications

  15. Uses of dense magnetized plasmas as neutron sources

    International Nuclear Information System (INIS)

    Gonzalez, Jose Hector

    2004-01-01

    In this work, a lumped parameter model for Plasma Focus is presented.A fast running computer code was developed, specially focused to the calculation of the neutron production in Deuterium-filled devices.This code is suitable to parameters optimization at the conceptual engineering stage.The kinematics of the current sheet is represented by a plane, 2D snowplow model.It is complemented with sensible estimations for the current sheet characteristics (density n and temperature T).After the radial collapse, a one fluid MHD model with velocity profiles for the particles trapped inside the pinch is proposed.Then, assuming thermal equilibrium in the plasma, the neutron production by termofusion can be estimated.The dynamics equations are coupled with the electrical circuit. A computer code in FORTRAN language was programmed to solve this set of equations.A powerful numerical integrator for first order differential equations is used, and the code can perform an estimation of the neutron production very quickly.The resulting neutron yield and dynamics predictions have been compared against experimental results of Plasma Focus devices from all around the world, for different geometric and energetic conditions.The effective parameters of the model were validated using those experimental measurements. The presented model ultimately calculates the neutron production given the geometric and energetic parameters, and the filling pressure

  16. Quantitative images of metals in plant tissues measured by laser ablation inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Becker, J.S.; Dietrich, R.C.; Matusch, A.; Pozebon, D.; Dressler, V.L.

    2008-01-01

    Laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) was used for quantitative imaging of toxic and essential elements in thin sections (thickness of 30 or 40 μm) of tobacco plant tissues. Two-dimensional images of Mg, Fe, Mn, Zn, Cu, Cd, Rh, Pt and Pb in leaves, shoots and roots of tobacco were produced. Sections of the plant tissues (fixed onto glass slides) were scanned by a focused beam of a Nd:YAG laser in a laser ablation chamber. The ablated material was transported with argon as carrier gas to the ICP ion source at a quadrupole ICP-MS instrument. Ion intensities of the investigated elements were measured together with 13 C + , 33 S + and 34 S + within the entire plant tissue section. Matrix matching standards (prepared using powder of dried tobacco leaves) were used to constitute calibration curves, whereas the regression coefficient of the attained calibration curves was typically 0.99. The variability of LA-ICP-MS process, sample heterogeneity and water content in the sample were corrected by using 13 C + as internal standard. Quantitative imaging of the selected elements revealed their inhomogeneous distribution in leaves, shoots and roots

  17. Levels of Essential Elements in Different Medicinal Plants Determined by Using Inductively Coupled Plasma Mass Spectrometry

    Directory of Open Access Journals (Sweden)

    Eid I. Brima

    2018-01-01

    Full Text Available The objective of this study was to investigate the content of essential elements in medicinal plants in the Kingdom of Saudi Arabia (KSA. Five different medical plants (mahareeb (Cymbopogon schoenanthus, sheeh (Artemisia vulgaris, harjal (Cynanchum argel delile, nabipoot (Equisetum arvense, and cafmariam (Vitex agnus-castus were collected from Madina city in the KSA. Five elements Fe, Mn, Zn, Cu, and Se were determined by using inductively coupled plasma mass spectrometry (ICP-MS. Fe levels were the highest and Se levels were the lowest in all plants. The range levels of all elements in all plants were as follows: Fe 193.4–1757.9, Mn 23.6–143.7, Zn 15.4–32.7, Se 0.13–0.92, and Cu 11.3–21.8 µg/g. Intakes of essential elements from the medical plants in infusion were calculated: Fe 4.6–13.4, Mn 6.7–123.2, Zn 7.0–42.7, Se 0.14–1.5, and Cu 1.5–5.0 µg/dose. The calculated intakes of essential elements for all plants did not exceed the daily intake set by the World Health Organization (WHO and European Food Safety Authority (EFSA. These medicinal plants may be useful sources of essential elements, which are vital for health.

  18. Characterisation of an ion source on the Helix MC Plus noble gas mass spectrometer - pressure dependent mass discrimination

    Science.gov (United States)

    Zhang, X.

    2017-12-01

    Characterisation of an ion source on the Helix MC Plusnoble gas mass spectrometer - pressure dependent mass discrimination Xiaodong Zhang* dong.zhang@anu.edu.au Masahiko Honda Masahiko.honda@anu.edu.au Research School of Earth Sciences, The Australian National University, Canberra, Australia To obtain reliable measurements of noble gas elemental and isotopic abundances in a geological sample it is essential that the mass discrimination (instrument-induced isotope fractionation) of the mass spectrometer remain constant over the working range of noble gas partial pressures. It is known, however, that there are pressure-dependent variations in sensitivity and mass discrimination in conventional noble gas mass spectrometers [1, 2, 3]. In this study, we discuss a practical approach to ensuring that the pressure effect in the Helix MC Plus high resolution, multi-collector noble gas mass spectrometer is minimised. The isotopic composition of atmospheric Ar was measured under a range of operating conditions to test the effects of different parameters on Ar mass discrimination. It was found that the optimised ion source conditions for pressure independent mass discrimination for Ar were different from those for maximised Ar sensitivity. The optimisation can be achieved by mainly adjusting the repeller voltage. It is likely that different ion source settings will be required to minimise pressure-dependent mass discrimination for different noble gases. A recommended procedure for tuning an ion source to reduce pressure dependent mass discrimination will be presented. References: Honda M., et al., Geochim. Cosmochim. Acta, 57, 859 -874, 1993. Burnard P. G., and Farley K. A., Geochemistry Geophysics Geosystems, Volume 1, 2000GC00038, 2000. Mabry J., et al., Journal of Analytical Atomic Spectrometry, 27, 1012 - 1017, 2012.

  19. Ion beam extraction from a matrix ECR plasma source by discrete ion-focusing effect

    DEFF Research Database (Denmark)

    Stamate, Eugen; Draghici, Mihai

    2010-01-01

    -ECR plasma source [3] with transversal magnetic filter for electron temperature control. 12 ECR plasma cells are placed 7.5 cm apart on the top of a cubic chamber 40x40x40 cm3. Each cell can be controlled independently by tuning the injected microwave power. The discharge is operated at pressures below 1 m......Positive or negative ion beams extracted from plasma are used in a large variety of surface functionalization techniques such as implantation, etching, surface activation, passivation or oxidation. Of particular importance is the surface treatment of materials sensitive to direct plasma exposure...... due to high heath fluxes, the controllability of the ion incidence angle, and charge accumulation when treating insulating materials. Despite of a large variety of plasma sources available for ion beam extraction, there is a clear need for new extraction mechanisms that can make available ion beams...

  20. Modeling the influence of coupled mass transfer processes on mass flux downgradient of heterogeneous DNAPL source zones.

    Science.gov (United States)

    Yang, Lurong; Wang, Xinyu; Mendoza-Sanchez, Itza; Abriola, Linda M

    2018-04-01

    Sequestered mass in low permeability zones has been increasingly recognized as an important source of organic chemical contamination that acts to sustain downgradient plume concentrations above regulated levels. However, few modeling studies have investigated the influence of this sequestered mass and associated (coupled) mass transfer processes on plume persistence in complex dense nonaqueous phase liquid (DNAPL) source zones. This paper employs a multiphase flow and transport simulator (a modified version of the modular transport simulator MT3DMS) to explore the two- and three-dimensional evolution of source zone mass distribution and near-source plume persistence for two ensembles of highly heterogeneous DNAPL source zone realizations. Simulations reveal the strong influence of subsurface heterogeneity on the complexity of DNAPL and sequestered (immobile/sorbed) mass distribution. Small zones of entrapped DNAPL are shown to serve as a persistent source of low concentration plumes, difficult to distinguish from other (sorbed and immobile dissolved) sequestered mass sources. Results suggest that the presence of DNAPL tends to control plume longevity in the near-source area; for the examined scenarios, a substantial fraction (43.3-99.2%) of plume life was sustained by DNAPL dissolution processes. The presence of sorptive media and the extent of sorption non-ideality are shown to greatly affect predictions of near-source plume persistence following DNAPL depletion, with plume persistence varying one to two orders of magnitude with the selected sorption model. Results demonstrate the importance of sorption-controlled back diffusion from low permeability zones and reveal the importance of selecting the appropriate sorption model for accurate prediction of plume longevity. Large discrepancies for both DNAPL depletion time and plume longevity were observed between 2-D and 3-D model simulations. Differences between 2- and 3-D predictions increased in the presence of

  1. Modeling the influence of coupled mass transfer processes on mass flux downgradient of heterogeneous DNAPL source zones

    Science.gov (United States)

    Yang, Lurong; Wang, Xinyu; Mendoza-Sanchez, Itza; Abriola, Linda M.

    2018-04-01

    Sequestered mass in low permeability zones has been increasingly recognized as an important source of organic chemical contamination that acts to sustain downgradient plume concentrations above regulated levels. However, few modeling studies have investigated the influence of this sequestered mass and associated (coupled) mass transfer processes on plume persistence in complex dense nonaqueous phase liquid (DNAPL) source zones. This paper employs a multiphase flow and transport simulator (a modified version of the modular transport simulator MT3DMS) to explore the two- and three-dimensional evolution of source zone mass distribution and near-source plume persistence for two ensembles of highly heterogeneous DNAPL source zone realizations. Simulations reveal the strong influence of subsurface heterogeneity on the complexity of DNAPL and sequestered (immobile/sorbed) mass distribution. Small zones of entrapped DNAPL are shown to serve as a persistent source of low concentration plumes, difficult to distinguish from other (sorbed and immobile dissolved) sequestered mass sources. Results suggest that the presence of DNAPL tends to control plume longevity in the near-source area; for the examined scenarios, a substantial fraction (43.3-99.2%) of plume life was sustained by DNAPL dissolution processes. The presence of sorptive media and the extent of sorption non-ideality are shown to greatly affect predictions of near-source plume persistence following DNAPL depletion, with plume persistence varying one to two orders of magnitude with the selected sorption model. Results demonstrate the importance of sorption-controlled back diffusion from low permeability zones and reveal the importance of selecting the appropriate sorption model for accurate prediction of plume longevity. Large discrepancies for both DNAPL depletion time and plume longevity were observed between 2-D and 3-D model simulations. Differences between 2- and 3-D predictions increased in the presence of

  2. Quantitative, multiplexed workflow for deep analysis of human blood plasma and biomarker discovery by mass spectrometry.

    Science.gov (United States)

    Keshishian, Hasmik; Burgess, Michael W; Specht, Harrison; Wallace, Luke; Clauser, Karl R; Gillette, Michael A; Carr, Steven A

    2017-08-01

    Proteomic characterization of blood plasma is of central importance to clinical proteomics and particularly to biomarker discovery studies. The vast dynamic range and high complexity of the plasma proteome have, however, proven to be serious challenges and have often led to unacceptable tradeoffs between depth of coverage and sample throughput. We present an optimized sample-processing pipeline for analysis of the human plasma proteome that provides greatly increased depth of detection, improved quantitative precision and much higher sample analysis throughput as compared with prior methods. The process includes abundant protein depletion, isobaric labeling at the peptide level for multiplexed relative quantification and ultra-high-performance liquid chromatography coupled to accurate-mass, high-resolution tandem mass spectrometry analysis of peptides fractionated off-line by basic pH reversed-phase (bRP) chromatography. The overall reproducibility of the process, including immunoaffinity depletion, is high, with a process replicate coefficient of variation (CV) of 4,500 proteins are detected and quantified per patient sample on average, with two or more peptides per protein and starting from as little as 200 μl of plasma. The approach can be multiplexed up to 10-plex using tandem mass tags (TMT) reagents, further increasing throughput, albeit with some decrease in the number of proteins quantified. In addition, we provide a rapid protocol for analysis of nonfractionated depleted plasma samples analyzed in 10-plex. This provides ∼600 quantified proteins for each of the ten samples in ∼5 h of instrument time.

  3. Characteristics of the Plasma Source for Ground Ionosphere Simulation Surveyed by Disk-Type Langmuir Probe

    Science.gov (United States)

    Ryu, Kwangsun; Lee, Junchan; Kim, Songoo; Chung, Taejin; Shin, Goo-Hwan; Cha, Wonho; Min, Kyoungwook; Kim, Vitaly P.

    2017-12-01

    A space plasma facility has been operated with a back-diffusion-type plasma source installed in a mid-sized vacuum chamber with a diameter of 1.5 m located in Satellite Technology Research Center (SaTReC), Korea Advanced Institute of Science and Technology (KAIST). To generate plasma with a temperature and density similar to the ionospheric plasma, nickel wires coated with carbonate solution were used as filaments that emit thermal electrons, and the accelerated thermal electrons emitted from the heated wires collide with the neutral gas to form plasma inside the chamber. By using a disk-type Langmuir probe installed inside the vacuum chamber, the generation of plasma similar to the space environment was validated. The characteristics of the plasma according to the grid and plate anode voltages were investigated. The grid voltage of the plasma source is realized as a suitable parameter for manipulating the electron density, while the plate voltage is suitable for adjusting the electron temperature. A simple physical model based on the collision cross-section of electron impact on nitrogen molecule was established to explain the plasma generation mechanism.

  4. Plasma particle sources due to interactions with neutrals in a turbulent scrape-off layer of a toroidally confined plasma

    Science.gov (United States)

    Thrysøe, A. S.; Løiten, M.; Madsen, J.; Naulin, V.; Nielsen, A. H.; Rasmussen, J. Juul

    2018-03-01

    The conditions in the edge and scrape-off layer (SOL) of magnetically confined plasmas determine the overall performance of the device, and it is of great importance to study and understand the mechanics that drive transport in those regions. If a significant amount of neutral molecules and atoms is present in the edge and SOL regions, those will influence the plasma parameters and thus the plasma confinement. In this paper, it is displayed how neutrals, described by a fluid model, introduce source terms in a plasma drift-fluid model due to inelastic collisions. The resulting source terms are included in a four-field drift-fluid model, and it is shown how an increasing neutral particle density in the edge and SOL regions influences the plasma particle transport across the last-closed-flux-surface. It is found that an appropriate gas puffing rate allows for the edge density in the simulation to be self-consistently maintained due to ionization of neutrals in the confined region.

  5. Simulations of an ultracold, neutral plasma with equal mass for every charge

    International Nuclear Information System (INIS)

    Robicheaux, F; Bender, B J; Phillips, M A

    2014-01-01

    The results of a theoretical investigation of an ultracold, neutral plasma composed only of equal mass positive and negative charges are reported. In our simulations, the plasma is created by the fast dissociation of a neutral particle; each dissociation leads to one positive ion and one negative ion with the same mass as the positive ion. The temperature of the plasma is controlled by the relative energy of the dissociation. We studied the early time evolution of this system where the initial energy was tuned so that the plasma is formed in the strongly coupled regime. In particular, we present results on the temperature evolution and three body recombination. In the weakly coupled regime, we studied how an expanding plasma thermalizes and how the scattering between ions affects the expansion. Because the expansion causes the density to drop, the velocity distribution only evolves for a finite time with the final distribution depending on the number of particles and initial temperature of the plasma. (paper)

  6. ULTRASONIC NEBULIZATION AND ARSENIC VALENCE STATE CONSIDERATIONS PRIOR TO DETERMINATION VIA INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY

    Science.gov (United States)

    An ultrasonic nebulizer (USN) was utilized as a sample introduction device for an inductively coupled plasma mass spectrometer in an attempt to increase the sensitivity for As. The USN produced a valence state response difference for As. The As response was suppressed approximate...

  7. Independent prognostic value of left ventricular mass, diastolic function, and fasting plasma glucose

    DEFF Research Database (Denmark)

    Pareek, Manan; Nielsen, Mette Lundgren; Leósdóttir, Margrét

    2016-01-01

    OBJECTIVE: To explore the independent prognostic value of left ventricular (LV) mass, diastolic function, and fasting plasma glucose (FPG) for the prediction of incident cardiac events in a random population sample. DESIGN AND METHOD: 415 women and 999 men aged 56-79 years, included between 2002...

  8. Determination of Arsenic in Sinus Wash and Tap Water by Inductively Coupled Plasma-Mass Spectrometry

    Science.gov (United States)

    Donnell, Anna M.; Nahan, Keaton; Holloway, Dawone; Vonderheide, Anne P.

    2016-01-01

    Arsenic is a toxic element to which humans are primarily exposed through food and water; it occurs as a result of human activities and naturally from the earth's crust. An experiment was developed for a senior level analytical laboratory utilizing an Inductively Coupled Plasma-Mass Spectrometer (ICP-MS) for the analysis of arsenic in household…

  9. Evaluation of body mass index and plasma lipid profile in dogs ...

    African Journals Online (AJOL)

    This study evaluated the body mass index (BMI), plasma lipid profile and gait assessment score (GAS) in dogs. Body weights (BW), height (H) at shoulder and waist circumference (WC) were obtained from fifty client-owned dogs of both sexes to determine the BMI. In addition, body condition score (BCS) and GAS were ...

  10. Evaluation of body mass index and plasma lipid profile in Boerboel ...

    African Journals Online (AJOL)

    This study evaluated the body mass index (BMI) and plasma lipid profile in Boerboel dogs. Body weights (BW), height (H) at shoulder and waist circumference (WC) were obtained from fifty-three Boerboels to determine the BMI while, body condition score (BCS) was determined subjectively. Also 5mls of blood was obtained ...

  11. Determination of platinum in human subcellular microsamples by inductively coupled plasma mass spectrometry

    DEFF Research Database (Denmark)

    Björn, Erik; Nygren, Yvonne; Nguyen, Tam T. T. N.

    2007-01-01

    A fast and robust method for the determination of platinum in human subcellular microsamples by inductively coupled plasma mass spectrometry was developed, characterized, and validated. Samples of isolated DNA and exosome fractions from human ovarian (2008) and melanoma (T289) cancer cell lines w...

  12. Interfacing capillary electrophoresis with inductively coupled plasma mass spectrometry by direct injection nebulization for selenium speciation

    DEFF Research Database (Denmark)

    Bendahl, Lars; Gammelgaard, Bente; Jons, O.

    2001-01-01

    A demountable direct injection high efficiency nebulizer operating at low sample uptake rates was developed and used for coupling of capillary electrophoresis (CE) with inductively coupled plasma mass spectrometry (ICP-MS). When the nebulizer was used for continuous sample introduction, detection...

  13. In situ calibration of inductively coupled plasma-atomic emission and mass spectroscopy

    Science.gov (United States)

    Braymen, Steven D.

    1996-06-11

    A method and apparatus for in situ addition calibration of an inductively coupled plasma atomic emission spectrometer or mass spectrometer using a precision gas metering valve to introduce a volatile calibration gas of an element of interest directly into an aerosol particle stream. The present situ calibration technique is suitable for various remote, on-site sampling systems such as laser ablation or nebulization.

  14. Mass spectrometric evidence for suprathermal ionization in an inductively coupled argon plasma

    International Nuclear Information System (INIS)

    Houk, R.S.; Svec, H.J.; Fassel, V.A.

    1981-01-01

    Mass spectra have been obtained of species in the axial channel of an inductively coupled argon plasma by extracting ions from the inductively coupled plasma into a vacuum system housing a quadrupole mass spectrometer. Ionization temperatures (T/sub ion/) are obtained from relative count rates of m/z-resolved ions according to two general types of ionization equilibrium considerations: (a) the radio of doubly/singly charged ions of the same element, and (b) the ratio of singly charged ions from two elements of different ionization energy. The T/sub ion/ values derived from measurement of Ar +2 /Ar + , Ba +2 /Ba + , Sr +2 /Sr + , and Cd + /I + are all greater than those expected from excitation temperatures measured by other workers. The latter three values for T/sub ion/ are in reasonable agreement with values obtained by optical spectrometry for a variety of argon inductively coupled plasmas

  15. Determination of albendazole sulfoxide in human plasma by using liquid chromatography-tandem mass spectrometry.

    Science.gov (United States)

    Saraner, Nihal; Özkan, Güler Yağmur; Güney, Berrak; Alkan, Erkin; Burul-Bozkurt, Nihan; Sağlam, Onursal; Fikirdeşici, Ezgi; Yıldırım, Mevlüt

    2016-06-01

    A rapid, simple and sensitive method was developed and validated using liquid chromatography-tandem mass spectrometry (LC-MS/MS) for determination of albendazole sulfoxide (ABZOX) in human plasma. The plasma samples were extracted by protein precipitation using albendazole sulfoxide-d3 as internal standard (IS). The chromatographic separation was performed on Waters Xbridge C18Column (100×4.6mm, 3.5μm) with a mobile phase consisting of ammonia solution, water and methanol at a flow rate of 0.70mL/min. ABZOX was detected and identified by mass spectrometry with electrospray ionization (ESI) in positive ion and multiple-reaction monitoring (MRM) mode. The method was linear in the range of 3-1500ng/mL for ABZOX. This method was successfully applied to the bioequivalence study in human plasma samples. Copyright © 2016 Elsevier B.V. All rights reserved.

  16. Spectral lines and characteristic of temporal variations in photoionized plasmas induced with laser-produced plasma extreme ultraviolet source

    Science.gov (United States)

    Saber, I.; Bartnik, A.; Wachulak, P.; Skrzeczanowski, W.; Jarocki, R.; Fiedorowicz, H.

    2017-11-01

    Spectral lines for Kr/Ne/H2 photoionized plasma in the ultraviolet and visible (UV/Vis) wavelength ranges have been created using a laser-produced plasma (LPP) EUV source. The source is based on a double-stream gas puff target irradiated with a commercial Nd:YAG laser. The laser pulses were focused onto a gas stream, injected into a vacuum chamber synchronously with the EUV pulses. Spectral lines from photoionization in neutral Kr/Ne/H2 and up to few charged states were observed. The intense emission lines were associated with the Kr transition lines. Experimental and theoretical investigations on intensity variations for some ionic lines are presented. A decrease in the intensity with the delay time between the laser pulse and the spectrum acquisition was revealed. Electron temperature and electron density in the photoionized plasma have been estimated from the characteristic emission lines. Temperature was obtained using Boltzmann plot method, assuming that the population density of atoms and ions are considered in a local thermodynamic equilibrium (LTE). Electron density was calculated from the Stark broadening profile. The temporal evaluation of the plasma and the way of optimizing the radiation intensity of LPP EUV sources is discussed.

  17. Isotopic analysis of calcium in blood plasma and bone from mouse samples by multiple collector-ICP-mass spectrometry

    International Nuclear Information System (INIS)

    Hirata, Takafumi; Tanoshima, Mina; Suga, Akinobu; Tanaka, Yu-ki; Nagata, Yuichi; Shinohara, Atsuko; Chiba, Momoko

    2008-01-01

    The biological processing of Ca produces significant stable isotope fractionation. The level of isotopic fractionation can provide key information about the variation in dietary consumption or Ca metabolism. To investigate this, we measured the 43 Ca/ 42 Ca and 44 Ca/ 42 Ca ratios for bone and blood plasma samples collected from mice of various ages using multiple collector-ICP-mass spectrometry (MC-ICP-MS). The 44 Ca/ 42 Ca ratio in bones was significantly (0.44 - 0.84 per mille) lower than the corresponding ratios in the diet, suggesting that Ca was isotopically fractionated during Ca metabolism for bone formation. The resulting 44 Ca/ 42 Ca ratios for blood plasma showed almost identical, or slightly higher, values (0.03 - 0.2 per mille) than found in a corresponding diet. This indicates that a significant amount of Ca in the blood plasma was from dietary sources. Unlike that discovered for Fe, there were not significant differences in the measured 44 Ca/ 42 Ca ratios between female and male specimens (for either bone or blood plasma samples). Similarity, the 44 Ca/ 42 Ca ratios suggests that there were no significant differences in Ca dietary consumption or Ca metabolism between female and male specimens. In contrast, the 44 Ca/ 42 Ca ratios of blood plasma from mother mice during the lactation period were significantly higher than those for all other adult specimens. This suggests that Ca supplied to infants through lactation was isotopically lighter, and the preferential supply of isotropically lighter Ca resulted in isotopically heavier Ca in blood plasma of mother mice during the lactation period. The data obtained here clearly demonstrate that the Ca isotopic ratio has a potential to become a new tool for evaluating changes in dietary consumption, or Ca metabolism of animals. (author)

  18. Topological sources of soliton mass and supersymmetry breaking

    Science.gov (United States)

    Haas, Patrick A.

    2018-06-01

    We derive the Smarr formulae for two five-dimensional solutions of supergravity, which are asymptotically ; in particular, one has a magnetic ‘bolt’ in its center, and one is a two-center solution. We show for both spacetimes that supersymmetry—and so the BPS-bound—is broken by the holonomy and how each topological feature of a space-like hypersurface enters Smarr’s mass formula, with emphasis on the ones that give rise to the stated violation of the BPS-bound. In this light, we question if any violating extra-mass term in a spacetime with such asymptotics is only evident in the ADM mass while the Komar mass per se ‘tries’ to preserve BPS. Finally, we derive the cohomological fluxes for each situation and examine in a more general fashion how the breaking of supersymmetry—and so the BPS-bound violation—is associated with their topologies. In the second (and more complicated) scenario, we especially focus on the compact cycle linking the centers, and the contribution of non-vanishing bulk terms in the mass formula to the breaking of supersymmetry.

  19. The plasma focus as a large fluence neutron source

    International Nuclear Information System (INIS)

    Zucker, O.; Bostick, W.; Long, J.; Luce, J.; Sahlin, H.

    1977-01-01

    A continuously operated, 1 pps, dense-plasma-focus device capable of delivering a minimum of 10 15 neutrons per pulse for material testing purposes is described. With I 5 scaling, predicted from analysis of existing machines, yields of 10 16 -10 17 neutrons per pulse are postulated. The average power consumption, which has become a major issue as a result of the energy crisis is shown to be highly favorable. A novel approach to the capacitor bank and switch design allowing repetitive operation is discussed. (Auth.)

  20. UV and IR laser ablation for inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Smith, M.R.; Koppenaal, D.W.; Farmer, O.T.

    1993-06-01

    Laser ablation particle plume compositions are characterized using inductively coupled plasma mass spectrometry (ICP/MS). This study evaluates the mass response characteristics peculiar to ICP/MS detection as a function of laser fluence and frequency. Evaluation of the ICP/MS mass response allows deductions to be made concerning how representative the laser ablation produced particle plume composition is relative to the targeted sample. Using a black glass standard, elemental fractionation was observed, primarily for alkalis and other volatile elements. The extent of elemental fractionation between the target sample and the sampled plume varied significantly as a function of laser fluences and IR and UV laser frequency

  1. Investigating the influence of DNAPL spill characteristics on source zone architecture and mass removal in pool-dominated source zones

    Science.gov (United States)

    Wallace, K. A.; Abriola, L.; Chen, M.; Ramsburg, A.; Pennell, K. D.; Christ, J.

    2009-12-01

    Multiphase, compositional simulators were employed to investigate the spill characteristics and subsurface properties that lead to pool-dominated, dense non-aqueous phase liquid (DNAPL) source zone architectures. DNAPL pools commonly form at textural interfaces where low permeability lenses restrict the vertical migration of DNAPL, allowing for DNAPL to accumulate, reaching high saturation. Significant pooling has been observed in bench-scale experiments and field settings. However, commonly employed numerical simulations rarely predict the pooling suspected in the field. Given the importance of pooling on the efficacy of mass recovery and the down-gradient contaminant signal, it is important to understand the predominant factors affecting the creation of pool-dominated source zones and their subsequent mass discharge. In this work, contaminant properties, spill characteristics and subsurface permeability were varied to investigate the factors contributing to the development of a pool-dominated source zone. DNAPL infiltration and entrapment simulations were conducted in two- and three-dimensional domains using the University of Texas Chemical Compositional (UTCHEM) simulator. A modified version of MT3DMS was then used to simulate DNAPL dissolution and mass discharge. Numerical mesh size was varied to investigate the importance of numerical model parameters on simulations results. The temporal evolution of commonly employed source zone architecture metrics, such as the maximum DNAPL saturation, first and second spatial moments, and fraction of DNAPL mass located in pools, was monitored to determine how the source zone architecture evolved with time. Mass discharge was monitored to identify the link between source zone architecture and down-gradient contaminant flux. Contaminant characteristics and the presence of extensive low permeability lenses appeared to have the most influence on the development of a pool-dominated source zone. The link between DNAPL mass

  2. Methods of gas purification and effect on the ion composition in an RF atmospheric pressure plasma jet investigated by mass spectrometry

    International Nuclear Information System (INIS)

    Grosse-Kreul, Simon; Huebner, Simon; Schneider, Simon; Keudell, Achim von; Benedikt, Jan

    2016-01-01

    The analysis of the ion chemistry of atmospheric pressure plasmas is essential to evaluate ionic reaction pathways during plasma-surface or plasma-analyte interactions. In this contribution, the ion chemistry of a radio-frequency atmospheric pressure plasma jet (μ-APPJ) operated in helium is investigated by mass spectrometry (MS). It is found, that the ion composition is extremely sensitive to impurities such as N 2 , O 2 and H 2 O. Without gas purification, protonated water cluster ions of the form H + (H 2 O) n are dominating downstream the positive ion mass spectrum. However, even after careful feed gas purification to the sub-ppm level using a molecular sieve trap and a liquid nitrogen trap as well as operation of the plasma in a controlled atmosphere, the positive ion mass spectrum is strongly influenced by residual trace gases. The observations support the idea that species with a low ionization energy serve as a major source of electrons in atmospheric pressure helium plasmas. Similarly, the neutral density of atomic nitrogen measured by MS in a He/N 2 mixture is varying up to a factor 3, demonstrating the significant influence of impurities on the neutral species chemistry as well. (orig.)

  3. Methods of gas purification and effect on the ion composition in an RF atmospheric pressure plasma jet investigated by mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Grosse-Kreul, Simon; Huebner, Simon; Schneider, Simon; Keudell, Achim von; Benedikt, Jan [Ruhr-Universitaet Bochum, Institute for Experimental Physics II, Bochum (Germany)

    2016-12-15

    The analysis of the ion chemistry of atmospheric pressure plasmas is essential to evaluate ionic reaction pathways during plasma-surface or plasma-analyte interactions. In this contribution, the ion chemistry of a radio-frequency atmospheric pressure plasma jet (μ-APPJ) operated in helium is investigated by mass spectrometry (MS). It is found, that the ion composition is extremely sensitive to impurities such as N{sub 2}, O{sub 2} and H{sub 2}O. Without gas purification, protonated water cluster ions of the form H{sup +}(H{sub 2}O){sub n} are dominating downstream the positive ion mass spectrum. However, even after careful feed gas purification to the sub-ppm level using a molecular sieve trap and a liquid nitrogen trap as well as operation of the plasma in a controlled atmosphere, the positive ion mass spectrum is strongly influenced by residual trace gases. The observations support the idea that species with a low ionization energy serve as a major source of electrons in atmospheric pressure helium plasmas. Similarly, the neutral density of atomic nitrogen measured by MS in a He/N{sub 2} mixture is varying up to a factor 3, demonstrating the significant influence of impurities on the neutral species chemistry as well. (orig.)

  4. New approach to 3-D, high sensitivity, high mass resolution space plasma composition measurements

    International Nuclear Information System (INIS)

    McComas, D.J.; Nordholt, J.E.

    1990-01-01

    This paper describes a new type of 3-D space plasma composition analyzer. The design combines high sensitivity, high mass resolution measurements with somewhat lower mass resolution but even higher sensitivity measurements in a single compact and robust design. While the lower resolution plasma measurements are achieved using conventional straight-through time-of-flight mass spectrometry, the high mass resolution measurements are made by timing ions reflected in a linear electric field (LEF), where the restoring force that an ion experiences is proportional to the depth it travels into the LEF region. Consequently, the ion's equation of motion in that dimension is that of a simple harmonic oscillator and its travel time is simply proportional to the square root of the ion's mass/charge (m/q). While in an ideal LEF, the m/q resolution can be arbitrarily high, in a real device the resolution is limited by the field linearity which can be achieved. In this paper we describe how a nearly linear field can be produced and discuss how the design can be optimized for various different plasma regimes and spacecraft configurations

  5. Characterization of the plasma-switch interaction in the LBL HIF ion source

    International Nuclear Information System (INIS)

    Hewett, D.W.; Rutkowski, H.L.

    1990-01-01

    A new way to characterize the performance of the LBL HIF ion source has been found. In the LBL source, ions are drawn from an arc-generated plasma reservoir in which the electrons are confined by a negative-biased ''switch'' mesh. Stagnation of the plasma is prevented by absorption of the excess ion flow on this mesh. The ion beam is generated by an external negative voltage that provides Child-Langmuir extraction of the ions through the switch mesh. We elucidate the physics requirements of the source and deduce switch mesh parameters needed for successful operation. 2 refs., 2 figs

  6. A common source for neutrino and sparticle masses

    CERN Document Server

    Brignole, Andrea; Rossi, Anna

    2010-01-01

    We discuss supersymmetric scenarios in which neutrino masses arise from effective d=6 operators in the Kahler potential (including SUSY-breaking insertions). Simple explicit realizations of those Kahler operators are presented in the context of the type II seesaw. An appealing scenario emerges upon identifying the seesaw mediators with SUSY-breaking messengers.

  7. A very high yield electron impact ion source for analytical mass spectrometry

    International Nuclear Information System (INIS)

    Koontz, S.L.; Bonner Denton, M.

    1981-01-01

    A novel ion source designed for use in mass spectrometric determination of organic compounds is described. The source is designed around a low pressure, large volume, hot cathode Penning discharge. The source operates in the 10 -4 - 10 -7 torr pressure domain and is capable of producing focusable current densities several orders of magnitude greater than those produced by conventional Nier -type sources. Mass spectra of n-butane and octafluoro-2-butene are presented. An improved signal-to-noise ratio is demonstrated with a General Electric Monopole 300 mass spectrometer. (orig.)

  8. A simple alkali-metal and noble gas ion source for SIMS equipments with mass separation of the primary ions

    International Nuclear Information System (INIS)

    Duesterhoeft, H.; Pippig, R.

    1986-01-01

    An alkali-metal ion source working without a store of alkali-metals is described. The alkali-metal ions are produced by evaporation of alkali salts and ionization in a low-voltage arc discharge stabilized with a noble gas plasma or in the case of small alkali-metal ion currents on the base of the well known thermic ionization at a hot tungsten wire. The source is very simple in construction and produces a stable ion current of 0.3 μA for more than 100 h. It is possible to change the ion species in a short time. This source is applicable to all SIMS equipments using mass separation for primary ions. (author)

  9. Determination of selenoprotein P in human plasma by solid phase extraction and inductively coupled plasma mass spectrometry

    DEFF Research Database (Denmark)

    Bendahl, L.; Sidenius, U.; Gammelgaard, Bente

    2000-01-01

    measured by inductively coupled plasma mass spectrometry (ICP-MS) monitoring the Se-82 isotope. Linear response was observed in the concentration range 0.3-70.8 mu g/l selenium as selenoprotein P with a correlation coefficient of 0.9994. The precision expressed as relative standard deviation was better...... than 2% in this range. The estimated limit of detection was 2 mu g/l and the experimentally verified quantification limit was 5 mu g/l, giving a relative standard deviation less than 2%. (C) 2000 Elsevier Science B.V. All rights reserved...

  10. High power light gas helicon plasma source for VASIMR

    International Nuclear Information System (INIS)

    Squire, Jared P.; Chang-Diaz, Franklin R.; Glover, Timothy W.; Jacobson, Verlin T.; McCaskill, Greg E.; Winter, D. Scott; Baity, F. Wally; Carter, Mark D.; Goulding, Richard H.

    2006-01-01

    In the Advanced Space Propulsion Laboratory (ASPL) helicon experiment (VX-10) we have measured a plasma flux to input gas rate ratio near 100% for both helium and deuterium at power levels up to 10 kW. Recent results at Oak Ridge National Laboratory (ORNL) show enhanced efficiency operation with a high power density, over 5 kW in a 5 cm diameter tube. Our helicon is presently 9 cm in diameter and operates up to 10 kW of input power. The data here uses a Boswell double-saddle antenna design with a magnetic cusp just upstream of the antenna. Similar to ORNL, for deuterium at near 10 kW, we find an enhanced performance of operation at magnetic fields above the lower hybrid matching condition

  11. Environmental friendly high efficient light source plasma lamp - Final report

    Energy Technology Data Exchange (ETDEWEB)

    Courret, G.; Calame, L. [Haute Ecole d' ingenierie et de gestion du canton de Vaud, Institut de micro et nano techniques, Yverdon-les-Bains (Switzerland); Meyer, A. [Solaronix SA, Aubonne (Switzerland)

    2007-07-01

    This illustrated final report for the Swiss Federal Office of Energy (SFOE) takes a look at work done on the development of a sulphur-based plasma lamp. In 2007, the capability of a new modulator has been explored. The most important results are discussed. With the production of a 1.2 cm{sup 3} bulb, the way towards the production of a 100 W lamp has been opened. The authors comment that modulation by impulses increases the luminous efficiency in comparison to modulation using a continuous sinusoidal wave. The report deals with the history of the project, the development of the new modulator, the use of rotational effects and the optimisation of the amount of active substances - tellurium and selenium - in the bulb. The electromagnetic coupling system used is described and discussed.

  12. Confined discharge plasma sources for Z-pinch experiments

    International Nuclear Information System (INIS)

    Hinshelwood, D.D.; Goodrich, P.J.; Mehlman, G.; Scherrer, V.E.; Stephanakis, S.J.; Young, F.C.

    1989-01-01

    The authors report their investigation Z-pinch implosions on the NRL Gamble II generator using metallic sources of sodium and aluminum, and non-metallic source of sodium (NaF), magnesium (MgF 2 ), and aluminum (Al 2 0 3 ). For 1 MA driving currents, peak Κ-shell radiated powers of about 100 GW and energies of about 1.5 kj have been obtained with both pure aluminum and NaF implosions. The aluminum results are comparable to those in previous Gamble II experiments with aluminum wire arrays. Confined discharge sources have been used to generate tens of GW in the Na Heα pump line and flourescence of the neon has been observed. The effects of nozzle shape and size, chamber diameter, amount of fuse material, and confined discharge current have been investigated in Gamble II implosion experiments. These studies indicate that confined discharge sources are capable of supplying significantly more material than required for implosions at the 1 MA level, so that this technique could be extended to higher current generators

  13. Profiling of kidney vascular endothelial cell plasma membrane proteins by liquid chromatography-tandem mass spectrometry.

    Science.gov (United States)

    Liu, Zan; Xu, Bo; Nameta, Masaaki; Zhang, Ying; Magdeldin, Sameh; Yoshida, Yutaka; Yamamoto, Keiko; Fujinaka, Hidehiko; Yaoita, Eishin; Tasaki, Masayuki; Nakagawa, Yuki; Saito, Kazuhide; Takahashi, Kota; Yamamoto, Tadashi

    2013-06-01

    Vascular endothelial cells (VECs) play crucial roles in physiological and pathologic conditions in tissues and organs. Most of these roles are related to VEC plasma membrane proteins. In the kidney, VECs are closely associated with structures and functions; however, plasma membrane proteins in kidney VECs remain to be fully elucidated. Rat kidneys were perfused with cationic colloidal silica nanoparticles (CCSN) to label the VEC plasma membrane. The CCSN-labeled plasma membrane fraction was collected by gradient ultracentrifugation. The VEC plasma membrane or whole-kidney lysate proteins were separated by sodium dodecyl sulfate polyacrylamide gel electrophoresis and digested with trypsin in gels for liquid chromatography-tandem mass spectrometry. Enrichment analysis was then performed. The VEC plasma membrane proteins were purified by the CCSN method with high yield (approximately 20 μg from 1 g of rat kidney). By Mascot search, 582 proteins were identified in the VEC plasma membrane fraction, and 1,205 proteins were identified in the kidney lysate. In addition to 16 VEC marker proteins such as integrin beta-1 and intercellular adhesion molecule-2 (ICAM-2), 8 novel proteins such as Deltex 3-like protein and phosphatidylinositol binding clathrin assembly protein (PICALM) were identified. As expected, many key functions of plasma membranes in general and of endothelial cells in particular (i.e., leukocyte adhesion) were significantly overrepresented in the proteome of CCSN-labeled kidney VEC fraction. The CCSN method is a reliable technique for isolation of VEC plasma membrane from the kidney, and proteomic analysis followed by bioinformatics revealed the characteristics of in vivo VECs in the kidney.

  14. Inductively coupled plasma mass spectrometry in the analysis of biological samples and pharmaceutical drugs

    Science.gov (United States)

    Ossipov, K.; Seregina, I. F.; Bolshov, M. A.

    2016-04-01

    Inductively coupled plasma mass spectrometry (ICP-MS) is widely used in the analysis of biological samples (whole blood, serum, blood plasma, urine, tissues, etc.) and pharmaceutical drugs. The shortcomings of this method related to spectral and non-spectral interferences are manifested in full measure in determination of the target analytes in these complex samples strongly differing in composition. The spectral interferences are caused by similarity of masses of the target component and sample matrix components. Non-spectral interferences are related to the influence of sample matrix components on the physicochemical processes taking place during formation and transportation of liquid sample aerosols into the plasma, on the value and spatial distribution of plasma temperature and on the transmission of the ion beam from the interface to mass spectrometer detector. The review is devoted to analysis of different mechanisms of appearance of non-spectral interferences and to ways for their minimization or elimination. Special attention is paid to the techniques of biological sample preparation, which largely determine the mechanisms of the influence of sample composition on the results of element determination. The ways of lowering non-spectral interferences by instrumental parameter tuning and application of internal standards are considered. The bibliography includes 189 references.

  15. The Sandia laser plasma extreme ultraviolet and soft x-ray (XUV) light source

    International Nuclear Information System (INIS)

    Tooman, T.P.

    1986-01-01

    Laser produced plasmas have been shown to be extremely bright sources of extreme ultraviolet and soft x-ray (XUV) radiation; however, certain practical difficulties have hindered the development of this source as a routinely usable laboratory device. To explore solutions to these difficulties, Sandia has constructed an XUV laser plasma source (LASPS) with the intention of developing an instrument that can be used for experiments requiring intense XUV radiation from 50-300 eV. The driving laser for this source is a KrF excimer with a wavelength of 248 nm, divergence of 200 μrad, pulse width of 23 ns at 20 Hz and typical pulse energy of 500 mJ which allows for good energy coupling to the plasma at moderate (10/sup 12/ W cm/sup 2/) power densities. This source has been pulsed approximately 2 x 10/sup 5/ times, demonstrating good tolerance to plasma debris. The source radiates from the visible to well above 1000 eV, however, to date attention has been concentrated on the 50-300 eV region. In this paper, spectral data and plasma images for both stainless steel and gold targets are presented with the gold target yielding a 200 μm plasma and reradiating 3.9% of the pump energy into 15-73 eV band, a flux of 1.22 x 10/sup 13/ photons/pulse/eV into 2π sr. Further efforts will expand these measurements to rare earth targets and to higher spectral energies. A special high throughput wide angle XUV (50-300 eV) monochromator and associated optics is being concurrently developed to collect the plasma radiation, perform energy dispersion and focus the radiation onto the experimental area

  16. Planned upgrade to the coaxial plasma source facility for high heat flux plasma flows relevant to tokamak disruption simulations

    International Nuclear Information System (INIS)

    Caress, R.W.; Mayo, R.M.; Carter, T.A.

    1995-01-01

    Plasma disruptions in tokamaks remain serious obstacles to the demonstration of economical fusion power. In disruption simulation experiments, some important effects have not been taken into account. Present disruption simulation experimental data do not include effects of the high magnetic fields expected near the PFCs in a tokamak major disruption. In addition, temporal and spatial scales are much too short in present simulation devices to be of direct relevance to tokamak disruptions. To address some of these inadequacies, an experimental program is planned at North Carolina State University employing an upgrade to the Coaxial Plasma Source (CPS-1) magnetized coaxial plasma gun facility. The advantages of the CPS-1 plasma source over present disruption simulation devices include the ability to irradiate large material samples at extremely high areal energy densities, and the ability to perform these material studies in the presence of a high magnetic field. Other tokamak disruption relevant features of CPS-1U include a high ion temperature, high electron temperature, and long pulse length

  17. Model of a source-driven plasma interacting with a wall in an oblique magnetic field

    International Nuclear Information System (INIS)

    Ahedo, E.; Carralero, D.

    2009-01-01

    A fluid model of a magnetized source-driven plasma is discussed for regimes with (Debye length)<<(ion Larmor radius)<<(plasma size and collisional mean-free path). Plasma collection by the wall is determined in terms of angle of incidence, magnetic strength, and plasma collisionality. For nonparallel incidence, a three-scale asymptotic analysis reveals a three-region matched structure consisting of a magnetically aligned bulk region, the Chodura layer, and the Debye sheath. Sonic Chodura and Bohm conditions define the singular region transitions. For near-parallel incidence, a separate analysis demonstrates the presence of a diffusive-collisional bulk region followed by a thin collisionless layer, which differs partially from the Chodura layer. A parametric analysis unveils the presence of four regimes depending on plasma collisionality: (1) a collisionless regime, with the magnetically channeled bulk region governed by plasma production; (2) a resistive semicollisional regime, where collisions retard the plasma transport in the bulk region; (3) a diffusive semicollisional regime, where the ExB drift dominates the ion flux in the bulk region; and (4) a collisional regime, where collisions cancel out magnetic effects. At grazing incidence, plasma collection is found to vary nonmonotonically with plasma collisionality. Nonzero Debye-length effects are discussed briefly.

  18. 2MASS extended sources in the zone of avoidance

    Science.gov (United States)

    Jarrett, T.; Chester, T.; Cutri, R.; Schneider, S.; Rosenberg, J.; Huchra, J.; Mader, J.

    2000-01-01

    A new high-resolution near-infrared mapping effort, the Two Micron All Sky Survey (2MASS), is now underway and will provide a complete census of galaxies as faint as 13.5 mag (3 mJy) at 2.2 mu m for most of the sky, and similar to 12.1 mag (10 mJy) for regions veiled by the Milky Way.

  19. An RF ion source based primary ion gun for secondary ion mass spectroscopy

    International Nuclear Information System (INIS)

    Menon, Ranjini; Nabhiraj, P.Y.; Bhandari, R.K.

    2011-01-01

    In this article we present the design, development and characterization of an RF plasma based ion gun as a primary ion gun for SIMS application. RF ion sources, in particular Inductively Coupled Plasma (ICP) ion sources are superior compared to LMIS and duoplasmtron ion sources since they are filamentless, can produce ions of gaseous elements. At the same time, ICP ion sources offer high angular current density which is an important factor in producing high current in small spot size on the target. These high current microprobes improve the signal to noise ratio by three orders as compared to low current ion sources such as LMIS. In addition, the high current microprobes have higher surface and depth profiling speeds. In this article we describe a simple ion source in its very basic form, two lens optical column and characteristics of microprobe

  20. Mass ablation and magnetic flux losses through a magnetized plasma-liner wall interface

    Science.gov (United States)

    García-Rubio, F.; Sanz, J.

    2017-07-01

    The understanding of energy and magnetic flux losses in a magnetized plasma medium confined by a cold wall is of great interest in the success of magnetized liner inertial fusion (MagLIF). In a MagLIF scheme, the fuel is magnetized and subsonically compressed by a cylindrical liner. Magnetic flux conservation is degraded by the presence of gradient-driven transport processes such as thermoelectric effects (Nernst) and magnetic field diffusion. In previous publications [Velikovich et al., Phys. Plasmas 22, 042702 (2015)], the evolution of a hot magnetized plasma in contact with a cold solid wall (liner) was studied using the classical collisional Braginskii's plasma transport equations in one dimension. The Nernst term degraded the magnetic flux conservation, while both thermal energy and magnetic flux losses were reduced with the electron Hall parameter ωeτe with a power-law asymptotic scaling (ωeτe)-1/2. In the analysis made in the present paper, we consider a similar situation, but with the liner being treated differently. Instead of a cold solid wall acting as a heat sink, we model the liner as a cold dense plasma with low thermal conduction (that could represent the cryogenic fuel layer added on the inner surface of the liner in a high-gain MagLIF configuration). Mass ablation comes into play, which adds notably differences to the previous analysis. The direction of the plasma motion is inverted, but the Nernst term still convects the magnetic field towards the liner. Magnetization suppresses the Nernst velocity and improves the magnetic flux conservation. Thermal energy in the hot plasma is lost in heating the ablated material. When the electron Hall parameter is large, mass ablation scales as (ωeτe)-3/10, while both the energy and magnetic flux losses are reduced with a power-law asymptotic scaling (ωeτe)-7/10.

  1. Quantitative mass fragmentographic determination of unlabeled and deuterium-labeled propoxyphene in plasma

    International Nuclear Information System (INIS)

    Sullivan, H.R.; McMahon, R.E.

    1977-01-01

    A quantitative gas chromatographic-mass spectrometric method for determination of plasma levels of d-propoxyphene has been developed by using d-propoxyphene-benzyl-d 7 as internal standard. Steady-state pharmacokinetics were studied in a dog by orally administering d-propoxyphene-d 0 for 19 days and d-propoxyphene-d 2 on the 20th day, and monitoring the plasma levels of both compounds and the ratio for 48 hours. It was established that the use of propoxyphene-d 2 did not lead to an isotope effect

  2. Plasma volume methodology: Evans blue, hemoglobin-hematocrit, and mass density transformations

    Science.gov (United States)

    Greenleaf, J. E.; Hinghofer-Szalkay, H.

    1985-01-01

    Methods for measuring absolute levels and changes in plasma volume are presented along with derivations of pertinent equations. Reduction in variability of the Evans blue dye dilution technique using chromatographic column purification suggests that the day-to-day variability in the plasma volume in humans is less than + or - 20 m1. Mass density determination using the mechanical-oscillator technique provides a method for measuring vascular fluid shifts continuously for assessing the density of the filtrate, and for quantifying movements of protein across microvascular walls. Equations for the calculation of volume and density of shifted fluid are presented.

  3. Impact of plasma tube wall thickness on power coupling in ICP sources

    International Nuclear Information System (INIS)

    Nawaz, Anuscheh; Herdrich, Georg

    2009-01-01

    The inductively heated plasma source at the Institute of Space Systems was investigated with respect to the wall thickness of the plasma tube using an air plasma. For this, the wall thickness of the quartz tube was reduced in steps from 2.5 to 1.25 mm. The significance of reducing the wall thickness was analyzed with respect to both the maximum allowable tube cooling power and the coupling efficiency. While the former results from thermal stresses in the tube's wall, the latter results from a minimization of magnetic field losses near the coil turns of the inductively coupled plasma (ICP) source. Analysis of the thermal stress could be validated by experimental data, i.e. the measurement of the tube cooling power when the respective tube structure failed. The coupling efficiency could be assessed qualitatively by simplified models, and the experimental data recorded show that coupling was improved far more than predicted.

  4. Diagnostics of microwave assisted electron cyclotron resonance plasma source for surface modification of nylon 6

    Science.gov (United States)

    More, Supriya E.; Das, Partha Sarathi; Bansode, Avinash; Dhamale, Gayatri; Ghorui, S.; Bhoraskar, S. V.; Sahasrabudhe, S. N.; Mathe, Vikas L.

    2018-01-01

    Looking at the increasing scope of plasma processing of materials surface, here we present the development and diagnostics of a microwave assisted Electron Cyclotron Resonance (ECR) plasma system suitable for surface modification of polymers. Prior to the surface-treatment, a detailed diagnostic mapping of the plasma parameters throughout the reactor chamber was carried out by using single and double Langmuir probe measurements in Ar plasma. Conventional analysis of I-V curves as well as the elucidation form of the Electron Energy Distribution Function (EEDF) has become the source of calibration of plasma parameters in the reaction chamber. The high energy tail in the EEDF of electron temperature is seen to extend beyond 60 eV, at much larger distances from the ECR zone. This proves the suitability of the rector for plasma processing, since the electron energy is much beyond the threshold energy of bond breaking in most of the polymers. Nylon 6 is used as a representative candidate for surface processing in the presence of Ar, H2 + N2, and O2 plasma, treated at different locations inside the plasma chamber. In a typical case, the work of adhesion is seen to almost get doubled when treated with oxygen plasma. Morphology of the plasma treated surface and its hydrophilicity are discussed in view of the variation in electron density and electron temperature at these locations. Nano-protrusions arising from plasma treatment are set to be responsible for the hydrophobicity. Chemical sputtering and physical sputtering are seen to influence the surface morphology on account of sufficient electron energies and increased plasma potential.

  5. Identification of phosphorylated butyrylcholinesterase in human plasma using immunoaffinity purification and mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Aryal, Uma K.; Lin, Chiann Tso; Kim, Jong Seo; Heibeck, Tyler H.; Wang, Jun; Qian, Weijun; Lin, Yuehe

    2012-04-20

    Paraoxon (diethyl 4-nitrophenyl phosphate) is an active metabolite of the common insecticide parathion and is acutely toxic due to the inhibition of cholinesterase (ChE) activity in the nervous systems. The Inhibition of butyrylcholinesterase (BChE) activity by paraoxon is due to the formation of phosphorylated BChE adduct, and the detection of the phosphorylated BChE adduct in human plasma can serve as an exposure biomarker of organophosphate pesticides and nerve agents. In this study, we performed immunoaffinity purification and liquid chromatography tandem mass spectrometry (LC-MS/MS) analysis for identifying phosphorylated BChE in human plasma treated by paraoxon. BChE was captured by biotinylated anti-BChE polyclonal antibodies conjugated to streptavidin magnetic beads. Western blot analysis showed that the antibody was effective to recognize both native and modified BChE with high specificity. The exact phosphorylation site of BChE was confirmed on Serine 198 by MS/MS with a 108 Da modification mass and accurately measured parent ion masses. The phosphorylated BChE peptide was also successfully detected in the immunoaffinity purified sample from paraoxon treated human plasma. Thus, immunoaffinity purification combined with mass spectrometry represents a viable approach for the detection of paraoxon-modified BChE and other forms of modified BChE as exposure biomarkers of organophosphates and nerve agents.

  6. Behavior of moving plasma in solenoidal magnetic field in a laser ion source

    International Nuclear Information System (INIS)

    Ikeda, S.; Takahashi, K.; Okamura, M.; Horioka, K.

    2016-01-01

    In a laser ion source, a solenoidal magnetic field is useful to guide the plasma and to control the extracted beam current. However, the behavior of the plasma drifting in the magnetic field has not been well understood. Therefore, to investigate the behavior, we measured the plasma ion current and the total charge within a single pulse in the solenoid by changing the distance from the entrance of the solenoid to a detector. We observed that the decrease of the total charge along the distance became smaller as the magnetic field became larger and then the charge became almost constant with a certain magnetic flux density. The results indicate that the transverse spreading speed of the plasma decreased with increasing the field and the plasma was confined transversely with the magnetic flux density. We found that the reason of the confinement was not magnetization of ions but an influence induced by electrons

  7. Behavior of moving plasma in solenoidal magnetic field in a laser ion source

    Energy Technology Data Exchange (ETDEWEB)

    Ikeda, S., E-mail: ikeda.s.ae@m.titech.ac.jp [Interdisciplinary Graduate School of Science and Engineering, Tokyo Institute of Technology, Yokohama, Kanagawa 226-8502 (Japan); Nishina Center for Accelerator-Based Science, RIKEN, Wako, Saitama 351-0108 (Japan); Takahashi, K. [Department of Electrical Engineering, Nagaoka University of Technology, Nagaoka, Niigata 940-2137 (Japan); Okamura, M. [Collider-Accelerator Department, Brookhaven National Laboratory, Upton, New York 11973-5000 (United States); Horioka, K. [Interdisciplinary Graduate School of Science and Engineering, Tokyo Institute of Technology, Yokohama, Kanagawa 226-8502 (Japan)

    2016-02-15

    In a laser ion source, a solenoidal magnetic field is useful to guide the plasma and to control the extracted beam current. However, the behavior of the plasma drifting in the magnetic field has not been well understood. Therefore, to investigate the behavior, we measured the plasma ion current and the total charge within a single pulse in the solenoid by changing the distance from the entrance of the solenoid to a detector. We observed that the decrease of the total charge along the distance became smaller as the magnetic field became larger and then the charge became almost constant with a certain magnetic flux density. The results indicate that the transverse spreading speed of the plasma decreased with increasing the field and the plasma was confined transversely with the magnetic flux density. We found that the reason of the confinement was not magnetization of ions but an influence induced by electrons.

  8. Behavior of moving plasma in solenoidal magnetic field in a laser ion source

    Science.gov (United States)

    Ikeda, S.; Takahashi, K.; Okamura, M.; Horioka, K.

    2016-02-01

    In a laser ion source, a solenoidal magnetic field is useful to guide the plasma and to control the extracted beam current. However, the behavior of the plasma drifting in the magnetic field has not been well understood. Therefore, to investigate the behavior, we measured the plasma ion current and the total charge within a single pulse in the solenoid by changing the distance from the entrance of the solenoid to a detector. We observed that the decrease of the total charge along the distance became smaller as the magnetic field became larger and then the charge became almost constant with a certain magnetic flux density. The results indicate that the transverse spreading speed of the plasma decreased with increasing the field and the plasma was confined transversely with the magnetic flux density. We found that the reason of the confinement was not magnetization of ions but an influence induced by electrons.

  9. Confinement of laser plasma by solenoidal field for laser ion source

    International Nuclear Information System (INIS)

    Okamura, M.; Kanesue, T.; Kondo, K.; Dabrowski, R.

    2010-01-01

    A laser ion source can provide high current, highly charged ions with a simple structure. However, it was not easy to control the ion pulse width. To provide a longer ion beam pulse, the plasma drift length, which is the distance between laser target and extraction point, has to be extended and as a result the plasma is diluted severely. Previously, we applied a solenoid field to prevent reduction of ion density at the extraction point. Although a current enhancement by a solenoid field was observed, plasma behavior after a solenoid magnet was unclear because plasma behavior can be different from usual ion beam dynamics. We measured a transverse ion distribution along the beam axis to understand plasma motion in the presence of a solenoid field.

  10. A new high-temperature plasma ion source for the TRISTAN ISOL facility

    International Nuclear Information System (INIS)

    Piotrowski, A.; Gill, R.L.; McDonald, D.C.

    1987-01-01

    A vigorous program of ion-source development at TRISTAN has led to several types of ion sources that are especially suited to extended operation at a reactor-based ISOL facility. The latest of these is a high-temperature plasma ion source in which a 5-g /sup 235/U target is located in the cathode and can be heated to 2500 0 C. The ion source has a lifetime of > 1000 h and produces a wide array of elements, including palladium. Off-line investigations indicate that the source functions primarily in an electron impact mode of ionization and exhibits typical ionization efficiencies of > 30% for xenon

  11. A new high-temperature plasma ion source for the TRISTAN ISOL facility

    International Nuclear Information System (INIS)

    Piotrowski, A.; Gill, R.L.; McDonald, D.C.

    1987-01-01

    A vigorous program of ion-source development at TRISTAN has led to several types of ion sources that are especially suited to extended operation at a reactor-based ISOL facility. The latest of these is a high-temperature plasma ion source in which a 5-g 235 U target is located in the cathode and can be heated to 2500 0 C. The ion source has a lifetime of >1000 h and produces a wide array of elements, including palladium. Off-line investigations indicate that the source functions primarily in an electron impact mode of ionization and exhibits typical ionization efficiencies of >30% for xenon. (orig.)

  12. New high temperature plasma ion source for the TRISTAN ISOL facility

    International Nuclear Information System (INIS)

    Piotrowski, A.; Gill, R.L.; McDonald, D.C.

    1986-08-01

    A vigorous program of ion source development at TRISTAN has led to several types of ion sources that are especially suited to extended operation at a reactor-based ISOL facility. The latest of these is a high temperature plasma ion source in which a 5 gm 235 U target is located in the cathode and can be heated to 2500 0 C. The ion source has a lifetime of >1000 hours and produces a wide array of elements, including Pd. Off-line investigations indicate that the source functions primarily in an electron impact mode of ionization and exhibits typical ionzation efficiencies of >30% for Xe

  13. Determining Mass and Persistence of a Reactive Brominated-Solvent DNAPL Source Using Mass Depletion-Mass Flux Reduction Relationships During Pumping

    Science.gov (United States)

    Johnston, C. D.; Davis, G. B.; Bastow, T.; Annable, M. D.; Trefry, M. G.; Furness, A.; Geste, Y.; Woodbury, R.; Rhodes, S.

    2011-12-01

    Measures of the source mass and depletion characteristics of recalcitrant dense non-aqueous phase liquid (DNAPL) contaminants are critical elements for assessing performance of remediation efforts. This is in addition to understanding the relationships between source mass depletion and changes to dissolved contaminant concentration and mass flux in groundwater. Here we present results of applying analytical source-depletion concepts to pumping from within the DNAPL source zone of a 10-m thick heterogeneous layered aquifer to estimate the original source mass and characterise the time trajectory of source depletion and mass flux in groundwater. The multi-component, reactive DNAPL source consisted of the brominated solvent tetrabromoethane (TBA) and its transformation products (mostly tribromoethene - TriBE). Coring and multi-level groundwater sampling indicated the DNAPL to be mainly in lower-permeability layers, suggesting the source had already undergone appreciable depletion. Four simplified source dissolution models (exponential, power function, error function and rational mass) were able to describe the concentration history of the total molar concentration of brominated organics in extracted groundwater during 285 days of pumping. Approximately 152 kg of brominated compounds were extracted. The lack of significant kinetic mass transfer limitations in pumped concentrations was notable. This was despite the heterogeneous layering in the aquifer and distribution of DNAPL. There was little to choose between the model fits to pumped concentration time series. The variance of groundwater velocities in the aquifer determined during a partitioning inter-well tracer test (PITT) were used to parameterise the models. However, the models were found to be relatively insensitive to this parameter. All models indicated an initial source mass around 250 kg which compared favourably to an estimate of 220 kg derived from the PITT. The extrapolated concentrations from the

  14. Inductively coupled plasma and ion sources: History and state-of-the-art

    International Nuclear Information System (INIS)

    Hopwood, J.

    1994-01-01

    Over 100 years ago Hittorf first generated an electrodeless ''ring'' discharge by electromagnetic induction and began a 40 year controversy as to the true physical origin of such a discharge. Even Tesla advocated that these plasmas were merely the result of large electrostatic potential differences rather than electric fields induced by high frequency currents. Through clever experiments using crude spark gaps and leyden jars, the inductive nature of the discharge was confirmed in the late 1920's by MacKinnon, thus supporting the theories and experiments of Sir J.J. Thomson, perhaps the most staunch advocate of the induction mechanism. Today the authors routinely exploit the intense plasmas which are generated by induction. In this talk, the characteristics of inductively coupled plasma (ICP) and ion sources will be reviewed and future applications of intense plasma sources will be discussed. The inductively coupled plasma is Joule heated at moderate gas pressures, but the electromagnetic field penetration of these dense plasmas is limited by the plasma skin depth, typically a few millimeters to a few centimeters. The induction plasma is thus edge heated, a fact that constrains uniformity over large areas if helical induction coils are used. Flat, spiral coils may be used to improve uniformity by driving the plasma using a planar geometry. Issues of dimensional and frequency scaling will be discussed as they apply to large diameter sources. Ion beams extracted from ICPs are used for many applications including space propulsion, high power neutral beams, and materials processing. Broad ion beam (∼10 cm) current densities in excess of 100 mA-cm 2 at 100 keV are obtained in pulsed mode operation. Recently, however, more consumer-oriented applications of less intense ICPs are emerging

  15. Characterization of the seminal plasma proteome in men with prostatitis by mass spectrometry

    Science.gov (United States)

    2012-01-01

    Background Prostatitis is an inflammation of the prostate gland which affects approximately 10% of men. Despite its frequency, diagnosing prostatitis and monitoring patient response to treatment remains frustrating. As the prostate contributes a substantial percentage of proteins to seminal plasma, we hypothesized that a protein biomarker of prostatitis might be found by comparing the seminal plasma proteome of patients with and without prostatitis. Results Using mass spectrometry, we identified 1708 proteins in the pooled seminal plasma of 5 prostatitis patients. Comparing this list to a previously published list of seminal plasma proteins in the pooled seminal plasma of 5 healthy, fertile controls yielded 1464 proteins in common, 413 found only in the control group, and 254 found only in the prostatitis group. Applying a set of criteria to this dataset, we generated a high-confidence list of 59 candidate prostatitis biomarkers, 33 of which were significantly increased in prostatitis as compared to control, and 26 of which were decreased. The candidates were analyzed using Gene Ontology and Ingenuity Pathway analysis to delineate their subcellular localizations and functions. Conclusions Thus, in this study, we identified 59 putative biomarkers in seminal plasma that need further validation for diagnosis and monitoring of prostatitis. PMID:22309592

  16. [Determination of endogenous agmatine in rat plasma by isotope dilution-gas chromatography-mass spectrometry].

    Science.gov (United States)

    Qiu, Zhongli; Lin, Ying; Xiong, Zhili; Xie, Jianwei

    2014-07-01

    A method for the determination of endogenous agmatine in rat plasma was developed by isotope dilution-gas chromatography-negative chemical ionization mass spectrometry (GC-NCI/MS). The plasma samples were analyzed after protein precipitation, evaporation, derivatization by hexafluoroacetone (HFAA), and clean-up on a Florisil SPE column. The GC-MS analysis utilized stable isotope d8-agmatine as internal standard. The samples after treatme were tested by negative chemical ionization with selected ion monitoring (SIM) which was set at m/z 492 (molecular ion of agmatine) and m/z 500 (molecular ion of internal standard). The limit of detection (LOD) of agmatine standard solution was 0.005 7 ng/mL. The calibration curve of the agmatine spiked in rat plasma showed a good linear relationship at the range of 1.14-57.0 ng/mL (r = 0.997). The recoveries of agmatine spiked in rat plasma ranged from 92.3% to 109.8%. Inter-day and intra-day precisions were less than 15%. The average concentration level of agmatine in rat plasma was (22 +/- 9) ng/mL, and there was no significant difference between male and female SD rats (p > 0.05). The method is high sensitive and specific, and can be used for the determination of endogenous agmatine in plasma. It provides a strong support for the subsequent research of agmatine.

  17. Sources plasma RF magnétisées : applications à la propulsion spatiale

    OpenAIRE

    Gerst , Jan Dennis

    2013-01-01

    The PEGASES thruster (Plasma Propulsion with Electronegative Gases) is a novel type of electric thruster for space propulsion. It uses negative and positive ions produced by an inductively coupled radio frequency discharge to create the thrust by electrostatically accelerating the ions through a set of grids. A magnetic filter is used to increase the amount of negative ions in the cavity of the thruster. The PEGASES thruster is not only a source to create a strongly negative ion plasma or eve...

  18. Glovebox enclosed dc plasma source for the determination of metals in plutonium

    International Nuclear Information System (INIS)

    Morris, W.F.

    1986-01-01

    The direct current plasma source of a Beckman Spectraspan IIIB emission spectrometer was enclosed in a glovebox at Lawrence Livermore National Laboratory in December 1982. Since that time, the system has been used for the routine determination of alloy and impurity metals in plutonium. This paper presents the systematic steps involved in developing the glovebox and gives information regarding performance of the plasma in the glovebox and the effectiveness of containment of plutonium. 8 refs., 9 figs., 3 tabs

  19. Sheath physics and materials science results from recent plasma source ion implantation experiments

    International Nuclear Information System (INIS)

    Conrad, J.R.; Radtke, J.L.; Dodd, R.A.; Worzala, F.J.

    1987-01-01

    Plasma Source Ion Implantation (PSII) is a surface modification technique which has been optimized for ion-beam processing of materials. PSII departs radically from conventional implantation by circumventing the line of sight restriction inherent in conventional ion implantation. The authors used PSII to implant cutting tools and dies and have demonstrated substantial improvements in lifetime. Recent results on plasma physics scaling laws, microstructural, mechanical, and tribological properties of PSII-implanted materials are presented

  20. Neutral Beam Source and Target Plasma for Development of a Local Electric Field Fluctuation Diagnostic

    Science.gov (United States)

    Bakken, M. R.; Burke, M. G.; Fonck, R. J.; Lewicki, B. T.; Rhodes, A. T.; Winz, G. R.

    2016-10-01

    A new diagnostic measuring local E-> (r , t) fluctuations is being developed for plasma turbulence studies in tokamaks. This is accomplished by measuring fluctuations in the separation of the π components in the Hα motional Stark spectrum. Fluctuations in this separation are expected to be Ẽ / ẼEMSE 10-3EMSE 10-3 . In addition to a high throughput, high speed spectrometer, the project requires a low divergence (Ω 0 .5°) , 80 keV, 2.5 A H0 beam and a target plasma test stand. The beam employs a washer-stack arc ion source to achieve a high species fraction at full energy. Laboratory tests of the ion source demonstrate repeatable plasmas with Te 10 eV and ne 1.6 ×1017 m-3, sufficient for the beam ion optics requirements. Te and ne scalings of the ion source plasma are presented with respect to operational parameters. A novel three-phase resonant converter power supply will provide 6 mA/cm2 of 80 keV H0 at the focal plane for pulse lengths up to 15 ms, with low ripple δV / 80 keV 0.05 % at 280 kHz. Diagnostic development and validation tests will be performed on a magnetized plasma test stand with 0.5 T field. The test chamber will utilize a washer-stack arc source to produce a target plasma comparable to edge tokamak plasmas. A bias-plate with programmable power supply will be used to impose Ẽ within the target plasma. Work supported by US DOE Grant DE-FG02-89ER53296.

  1. Design and optimization of components and processes for plasma sources in advanced material treatments

    OpenAIRE

    Rotundo, Fabio

    2012-01-01

    The research activities described in the present thesis have been oriented to the design and development of components and technological processes aimed at optimizing the performance of plasma sources in advanced in material treatments. Consumables components for high definition plasma arc cutting (PAC) torches were studied and developed. Experimental activities have in particular focussed on the modifications of the emissive insert with respect to the standard electrode configuration, whi...

  2. Comparison of dielectric barrier discharge, atmospheric pressure radiofrequency-driven glow discharge and direct analysis in real time sources for ambient mass spectrometry of acetaminophen

    Energy Technology Data Exchange (ETDEWEB)

    Kratzer, Jan [Institute for National Measurement Standards, National Research Council of Canada, 1200 Montreal Road, Ottawa, Ontario, K1A 0R6 (Canada); Institute of Analytical Chemistry of the ASCR, v.v.i., Veveri 97, CZ-602 00 Brno (Czech Republic); Mester, Zoltan [Institute for National Measurement Standards, National Research Council of Canada, 1200 Montreal Road, Ottawa, Ontario, K1A 0R6 (Canada); Sturgeon, Ralph E., E-mail: Ralph.Sturgeon@nrc-cnrc.gc.ca [Institute for National Measurement Standards, National Research Council of Canada, 1200 Montreal Road, Ottawa, Ontario, K1A 0R6 (Canada)

    2011-08-15

    Three plasma-based ambient pressure ion sources were investigated; laboratory constructed dielectric barrier and rf glow discharges, as well as a commercial corona discharge (DART source). All were used to desorb and ionize a model analyte, providing sampling techniques for ambient mass spectrometry (MS). Experimental parameters were optimized to achive highest signal for acetaminophen as the analyte. Insight into the mechanisms of analyte desorption and ionization was obtained by means of emission spectrometry and ion current measurements. Desorption and ionization mechanisms for this analyte appear to be identical for all three plasma sources. Emission spectra differ only in the intensities of various lines and bands. Desorption of solid analyte requires transfer of thermal energy from the plasma source to sample surface, in the absence of which complete loss of MS response occurs. For acetaminophen, helium was the best plasma gas, providing 100- to 1000-fold higher analyte response than with argon or nitrogen. The same trend was also evident with background ions (protonated water clusters). MS analyte signal intensity correlates with the ion density (expressed as ion current) in the plasma plume and with emission intensity from excited state species in the plasma. These observations support an ionization process which occurs via proton transfer from protonated water clusters to analyte molecules.

  3. Silicon micromachining using a high-density plasma source

    International Nuclear Information System (INIS)

    McAuley, S.A.; Ashraf, H.; Atabo, L.; Chambers, A.; Hall, S.; Hopkins, J.; Nicholls, G.

    2001-01-01

    Dry etching of Si is critical in satisfying the demands of the micromachining industry. The micro-electro-mechanical systems (MEMS) community requires etches capable of high aspect ratios, vertical profiles, good feature size control and etch uniformity along with high throughput to satisfy production requirements. Surface technology systems' (STS's) high-density inductively coupled plasma (ICP) etch tool enables a wide range of applications to be realized whilst optimizing the above parameters. Components manufactured from Si using an STS ICP include accelerometers and gyroscopes for military, automotive and domestic applications. STS's advanced silicon etch (ASE TM ) has also allowed the first generation of MEMS-based optical switches and attenuators to reach the marketplace. In addition, a specialized application for fabricating the next generation photolithography exposure masks has been optimized for 200 mm diameter wafers, to depths of ∼750 μm. Where the profile is not critical, etch rates of greater than 8 μm min -1 have been realized to replace previous methods such as wet etching. This is also the case for printer applications. Specialized applications that require etching down to pyrex or oxide often result in the loss of feature size control at the interface; this is an industry wide problem. STS have developed a technique to address this. The rapid progression of the industry has led to development of the STS ICP etch tool, as well as the process. (author)

  4. Optical emission spectroscopy of carbon laser plasma ion source

    Science.gov (United States)

    Balki, Oguzhan; Rahman, Md. Mahmudur; Elsayed-Ali, Hani E.

    2018-04-01

    Carbon laser plasma generated by an Nd:YAG laser (wavelength 1064 nm, pulse width 7 ns, fluence 4-52 J cm-2) is studied by optical emission spectroscopy and ion time-of-flight. Up to C4+ ions are detected with the ion flux strongly dependent on the laser fluence. The increase in ion charge with the laser fluence is accompanied by observation of multicharged ion lines in the optical spectra. The time-integrated electron temperature Te is calculated from the Boltzmann plot using the C II lines at 392.0, 426.7, and 588.9 nm. Te is found to increase from ∼0.83 eV for a laser fluence of 22 J cm-2 to ∼0.90 eV for 40 J cm-2. The electron density ne is obtained from the Stark broadened profiles of the C II line at 392 nm and is found to increase from ∼ 2 . 1 × 1017cm-3 for 4 J cm-2 to ∼ 3 . 5 × 1017cm-3 for 40 J cm-2. Applying an external electric field parallel to the expanding plume shows no effect on the line emission intensities. Deconvolution of ion time-of-flight signal with a shifted Maxwell-Boltzmann distribution for each charge state results in an ion temperature Ti ∼4.7 and ∼6.0 eV for 20 and 36 J cm-2, respectively.

  5. Hard X-ray sources from miniature plasma focus devices

    International Nuclear Information System (INIS)

    Raspa, V.; Silva, P.; Moreno, J.; Zambra, M.; Soto, L.

    2004-01-01

    As first stage of a program to design a repetitive pulsed radiation generator for industrial applications, two miniature plasma foci have been designed and constructed at the Chilean commission of nuclear energy. The devices operate at an energy level of the order of tens of joules (PF-50 J, 160 nF capacitor bank, 20-35 kV, 32-100 J, ∼ 150 ns time to peak current) and hundred of joules (PF-400 J, 880 nF, 20-35 kV, 176-539 J, ∼ 300 ns time to peak current). Hard X-rays are being studied in these devices operating with hydrogen. Images of metallic plates with different thickness were obtained on commercial radiographic film, Agfa Curix ST-G2, in order to characterize the energy of the hard X-ray outside of the discharge chamber of PF-400 J. An effective energy of the order of 90 keV was measured under those conditions. X ray images of different metallic objects also have been obtained. (authors)

  6. Hard X-ray sources from miniature plasma focus devices

    Energy Technology Data Exchange (ETDEWEB)

    Raspa, V. [Buenos Aires Univ., PLADEMA, CONICET and INFIP (Argentina); Silva, P.; Moreno, J.; Zambra, M.; Soto, L. [Comision Chilena de Energia Nuclear, Santiago (Chile)

    2004-07-01

    As first stage of a program to design a repetitive pulsed radiation generator for industrial applications, two miniature plasma foci have been designed and constructed at the Chilean commission of nuclear energy. The devices operate at an energy level of the order of tens of joules (PF-50 J, 160 nF capacitor bank, 20-35 kV, 32-100 J, {approx} 150 ns time to peak current) and hundred of joules (PF-400 J, 880 nF, 20-35 kV, 176-539 J, {approx} 300 ns time to peak current). Hard X-rays are being studied in these devices operating with hydrogen. Images of metallic plates with different thickness were obtained on commercial radiographic film, Agfa Curix ST-G2, in order to characterize the energy of the hard X-ray outside of the discharge chamber of PF-400 J. An effective energy of the order of 90 keV was measured under those conditions. X ray images of different metallic objects also have been obtained. (authors)

  7. Deposition of dielectric films on silicon using a fore-vacuum plasma electron source

    Energy Technology Data Exchange (ETDEWEB)

    Zolotukhin, D. B.; Tyunkov, A. V.; Yushkov, Yu. G., E-mail: yuyushkov@gmail.com [Tomsk State University of Control Systems and Radioelectronics, 40 Lenin Ave., Tomsk 634050 (Russian Federation); Oks, E. M. [Tomsk State University of Control Systems and Radioelectronics, 40 Lenin Ave., Tomsk 634050 (Russian Federation); Institute of High Current Electronics SB RAS, 2/3, Akademichesky Ave., Tomsk 634055 (Russian Federation)

    2016-06-15

    We describe an experiment on the use of a fore-vacuum-pressure, plasma-cathode, electron beam source with current up to 100 mA and beam energy up to 15 keV for deposition of Mg and Al oxide films on Si substrates in an oxygen atmosphere at a pressure of 10 Pa. The metals (Al and Mg) were evaporated and ionized using the electron beam with the formation of a gas-metal beam-plasma. The plasma was deposited on the surface of Si substrates. The elemental composition of the deposited films was analyzed.

  8. Mass conservation for instantaneous sources in FEM3 simulations of material dispersion

    International Nuclear Information System (INIS)

    Rodean, H.C.

    1987-11-01

    This report presents the results of a systematic study in which it is shown that the numerical integration errors in determining material mass content are negligible; the material phase-change model by itself is not a cause of material mass variation; and a linear relation between fractional mass change and fractional density change at the source center for given mesh and source geometries exists over a range of values from 10 -5 to 10 -1 . This suggests that the omission of the ∂ rho/∂t term from the mass conservation equation is the cause of the observed non-conservation of mass by FEM3. It is shown that these mass variations can be minimized by minimizing the initial density gradients in the source region. 5 refs., 18 figs., 4 tabs

  9. Effect of dietary protein sources on production performance, egg quality, and plasma parameters of laying hens

    Directory of Open Access Journals (Sweden)

    Xiaocui Wang

    2017-03-01

    Full Text Available Objective This study was conducted to evaluate the effects of dietary protein sources (soybean meal, SBM; low-gossypol cottonseed meal, LCSM; double-zero rapeseed meal, DRM on laying performance, egg quality, and plasma parameters of laying hens. Methods A total of 432 32-wk-old laying hens were randomly divided into 6 treatments with 6 replicates of 12 birds each. The birds were fed diets containing SBM, LCSM100, or DRM100 individually or in combination with an equal amount of crude protein (CP (LCSM50, DRM50, and LCSM50-DRM50. The experimental diets, which were isocaloric (metabolizable energy, 11.11 MJ/kg and isonitrogenous (CP, 16.5%, had similar digestible amino acid profile. The feeding trial lasted 12 weeks. Results The daily egg mass was decreased in the LCSM100 and LCSM50-DRM50 groups (p0.05 and showed increased yolk color at the end of the trial (p0.05. Conclusion Together, our results suggest that the LCSM100 or DRM100 diets may produce the adverse effects on laying performance and egg quality after feeding for 8 more weeks. The 100.0 g/kg LCSM diet or the148.7 g/kg DRM diet has no adverse effects on laying performance and egg quality.

  10. Determining plasma-fueling sources with an end-loss ion spectrometer

    International Nuclear Information System (INIS)

    Grubb, D.P.; Foote, J.H.

    1986-01-01

    To help identify the major sources of fueling gas in Tandem Mirror Experiment-Upgrade (TMX-U), we mounted a mass-sensitive, E parallel to B, end-loss ion spectrometer (ELIS) near the machine's centerline. We set the electric field in the ELIS to simultaneously measure the axial loss currents of both hydrogen and deuterium. We then initiated plasma discharges, where we injected either hydrogen or deuterium gas into the central cell. We also selected and deselected the central-cell neutral beams that were fueled with hydrogen gas. The end-cell neutral beams were always selected and fueled with deuterium. By taking the ratio of the hydrogen end-loss current to the deuterium end-loss current (with a known deuterium-gas feed rate), we were able to infer the effective fueling rates that were due to wall reflux, central-cell beams, and end-cell beams. The results were the following: wall reflux, 6 Torr.l/s; central-cell beams, 15 Torr.l/s; and end-cell beams 1 Torr.l/s. 3 refs., 3 figs., 1 tab

  11. Analysis of the image of pion-emitting sources in the source center-of-mass frame

    Energy Technology Data Exchange (ETDEWEB)

    Ren, Yanyu; Feng, Qichun; Huo, Lei; Zhang, Jingbo; Liu, Jianli; Tang, Guixin [Harbin Institute of Technology, Department of Physics, Harbin, Heilongjiang (China); Zhang, Weining [Harbin Institute of Technology, Department of Physics, Harbin, Heilongjiang (China); Dalian University of Technology, School of Physics and Optoelectronic Technology, Dalian, Liaoning (China)

    2017-08-15

    In this paper, we try a method to extract the image of pion-emitting source function in the center-of-mass frame of the source (CMFS). We choose identical pion pairs according to the difference of their energy and use these pion pairs to build the correlation function. The purpose is to reduce the effect of ΔEΔt, thus the corresponding imaging result can tend to the real source function. We examine the effect of this method by comparing its results with real source functions extracted from models directly. (orig.)

  12. Tungsten transport and sources control in JET ITER-like wall H-mode plasmas

    Energy Technology Data Exchange (ETDEWEB)

    Fedorczak, N., E-mail: nicolas.fedorczak@cea.fr [CEA, IRFM, F-13108 Saint-Paul-Lez-Durance (France); Monier-Garbet, P. [CEA, IRFM, F-13108 Saint-Paul-Lez-Durance (France); Pütterich, T. [MPI für Plasmaphysik, EURATOM Association, Boltzmannstrasse 2, 85748 Garching (Germany); Brezinsek, S. [Institute of Energy and Climate Research, Forschungszentrum Jlich, Assoc EURATOM-FZJ, Jlich (Germany); Devynck, P.; Dumont, R.; Goniche, M.; Joffrin, E. [CEA, IRFM, F-13108 Saint-Paul-Lez-Durance (France); Lerche, E. [Association EURATOM-Belgian State, LPP-ERM-KMS, TEC partner, Brussels (Belgium); Euratom/CCFE Fusion Association, Culham Science Centre, Abingdon OX14 3DB (United Kingdom); Lipschultz, B. [York Plasma Institute, University of York, Heslington, York YO10 5DD (United Kingdom); Luna, E. de la [Laboratorio Nacional de Fusin, Asociacin EURATOM/CIEMAT, 28040 Madrid (Spain); Maddison, G. [Culham Centre for Fusion Energy, EURATOM-CCFE Association, Abingdon (United Kingdom); Maggi, C. [MPI für Plasmaphysik, EURATOM Association, Boltzmannstrasse 2, 85748 Garching (Germany); Matthews, G. [Culham Centre for Fusion Energy, EURATOM-CCFE Association, Abingdon (United Kingdom); Nunes, I. [Istituto de plasmas e fusao nuclear, Lisboa (Portugal); Rimini, F. [Culham Centre for Fusion Energy, EURATOM-CCFE Association, Abingdon (United Kingdom); Solano, E.R. [Laboratorio Nacional de Fusin, Asociacin EURATOM/CIEMAT, 28040 Madrid (Spain); Tamain, P. [CEA, IRFM, F-13108 Saint-Paul-Lez-Durance (France); Tsalas, M. [Association EURATOM-Hellenic Republic, NCSR Demokritos 153 10, Attica (Greece); Vries, P. de [ITER Organization, Route de Vinon sur Verdon, 13115 Saint Paul Lez Durance (France)

    2015-08-15

    A set of discharges performed with the JET ITER-like wall is investigated with respect to control capabilities on tungsten sources and transport. In attached divertor regimes, increasing fueling by gas puff results in higher divertor recycling ion flux, lower divertor tungsten source, higher ELM frequency and lower core plasma radiation, dominated by tungsten ions. Both pedestal flushing by ELMs and divertor screening (including redeposition) are possibly responsible. For specific scenarios, kicks in plasma vertical position can be employed to increase the ELM frequency, which results in slightly lower core radiation. The application of ion cyclotron radio frequency heating at the very center of the plasma is efficient to increase the core electron temperature gradient and flatten electron density profile, resulting in a significantly lower central tungsten peaking. Beryllium evaporation in the main chamber did not reduce the local divertor tungsten source whereas core radiation was reduced by approximately 50%.

  13. A method for studies on interactions between a gold-based drug and plasma proteins based on capillary electrophoresis with inductively coupled plasma mass spectrometry detection

    DEFF Research Database (Denmark)

    Nguyen, Tam T T N; Østergaard, Jesper; Gammelgaard, Bente

    2015-01-01

    An analytical method based on capillary electrophoresis (CE) and inductively coupled plasma mass spectrometry (ICP-MS) detection was developed for studies on the interaction of gold-containing drugs and plasma proteins using auranofin as example. A detection limit of 18 ng/mL of auranofin corresp...

  14. A validated inductively coupled plasma mass spectrometry (ICP-MS) method for the quantification of total platinum content in plasma, plasma ultrafiltrate, urine and peritoneal fluid.

    Science.gov (United States)

    Lemoine, Lieselotte; Thijssen, Elsy; Noben, Jean-Paul; Adriaensens, Peter; Carleer, Robert; Speeten, Kurt Van der

    2018-04-15

    Oxaliplatin is a platinum (Pt) 1 containing antineoplastic agent that is applied in current clinical practice for the treatment of colon and appendiceal neoplasms. A fully validated, highly sensitive, high throughput inductively coupled plasma mass spectrometry (ICP-MS) method is provided to quantify the total Pt content in plasma, plasma ultrafiltrate, urine and peritoneal fluid. In this ICP-MS approach, the only step of sample preparation is a 1000-fold dilution in 0.5% nitric acid, allowing the analysis of 17 samples per hour. Detection of Pt was achieved over a linear range of 0.01-100 ng/mL. The limit of quantification was 18.0 ng/mL Pt in plasma, 8.0 ng/mL in ultrafiltrate and 6.1 ng/mL in urine and peritoneal fluid. The ICP-MS method was further validated for inter-and intraday precision and accuracy (≤15%), recovery, robustness and stability. Short-term storage of the biofluids, for 14 days, can be performed at -4 °C, -24 °C and -80 °C. As to long-term stability, up to 5 months, storage at -80 °C is encouraged. Furthermore, a timeline assessing the total and unbound Pt fraction in plasma and ultrafiltrate over a period of 45 h is provided. Following an incubation period of 5 h at 37 °C, 19-21% of Pt was recovered in the ultrafiltrate, emphasizing the extensive and rapid binding of oxaliplatin-derived Pt to plasma proteins. The described method can easily be implemented in a routine setting for pharmacokinetic studies in patients treated with oxaliplatin-based hyperthermic intraperitoneal perioperative chemotherapy. Copyright © 2018 Elsevier B.V. All rights reserved.

  15. A mass of less than 15 solar masses for the black hole in an ultraluminous X-ray source.

    Science.gov (United States)

    Motch, C; Pakull, M W; Soria, R; Grisé, F; Pietrzyński, G

    2014-10-09

    Most ultraluminous X-ray sources have a typical set of properties not seen in Galactic stellar-mass black holes. They have luminosities of more than 3 × 10(39) ergs per second, unusually soft X-ray components (with a typical temperature of less than about 0.3 kiloelectronvolts) and a characteristic downturn in their spectra above about 5 kiloelectronvolts. Such puzzling properties have been interpreted either as evidence of intermediate-mass black holes or as emission from stellar-mass black holes accreting above their Eddington limit, analogous to some Galactic black holes at peak luminosity. Recently, a very soft X-ray spectrum was observed in a rare and transient stellar-mass black hole. Here we report that the X-ray source P13 in the galaxy NGC 7793 is in a binary system with a period of about 64 days and exhibits all three canonical properties of ultraluminous sources. By modelling the strong optical and ultraviolet modulations arising from X-ray heating of the B9Ia donor star, we constrain the black hole mass to be less than 15 solar masses. Our results demonstrate that in P13, soft thermal emission and spectral curvature are indeed signatures of supercritical accretion. By analogy, ultraluminous X-ray sources with similar X-ray spectra and luminosities of up to a few times 10(40) ergs per second can be explained by supercritical accretion onto massive stellar-mass black holes.

  16. Fast screening of analytes for chemical reactions by reactive low-temperature plasma ionization mass spectrometry.

    Science.gov (United States)

    Zhang, Wei; Huang, Guangming

    2015-11-15

    Approaches for analyte screening have been used to aid in the fine-tuning of chemical reactions. Herein, we present a simple and straightforward analyte screening method for chemical reactions via reactive low-temperature plasma ionization mass spectrometry (reactive LTP-MS). Solution-phase reagents deposited on sample substrates were desorbed into the vapor phase by action of the LTP and by thermal desorption. Treated with LTP, both reagents reacted through a vapor phase ion/molecule reaction to generate the product. Finally, protonated reagents and products were identified by LTP-MS. Reaction products from imine formation reaction, Eschweiler-Clarke methylation and the Eberlin reaction were detected via reactive LTP-MS. Products from the imine formation reaction with reagents substituted with different functional groups (26 out of 28 trials) were successfully screened in a time of 30 s each. Besides, two short-lived reactive intermediates of Eschweiler-Clarke methylation were also detected. LTP in this study serves both as an ambient ionization source for analyte identification (including reagents, intermediates and products) and as a means to produce reagent ions to assist gas-phase ion/molecule reactions. The present reactive LTP-MS method enables fast screening for several analytes from several chemical reactions, which possesses good reagent compatibility and the potential to perform high-throughput analyte screening. In addition, with the detection of various reactive intermediates (intermediates I and II of Eschweiler-Clarke methylation), the present method would also contribute to revealing and elucidating reaction mechanisms. Copyright © 2015 John Wiley & Sons, Ltd.

  17. Standard practice for alternate actinide calibration for inductively coupled plasma-mass spectrometry

    CERN Document Server

    American Society for Testing and Materials. Philadelphia

    2004-01-01

    1.1 This practice provides guidance for an alternate linear calibration for the determination of selected actinide isotopes in appropriately prepared aqueous solutions by Inductively Coupled Plasma-Mass Spectrometry (ICP-MS). This alternate calibration is mass bias adjusted using thorium-232 (232Th) and uranium-238 (238U) standards. One of the benefits of this standard practice is the ability to calibrate for the analysis of highly radioactive actinides using calibration standards at much lower specific activities. Environmental laboratories may find this standard practice useful if facilities are not available to handle the highly radioactive standards of the individual actinides of interest. 1.2 The instrument response for a series of determinations of known concentration of 232Th and 238U defines the mass versus response relationship. For each standard concentration, the slope of the line defined by 232Th and 238U is used to derive linear calibration curves for each mass of interest using interference equ...

  18. Characteristics of cold atmospheric plasma source based on low-current pulsed discharge with coaxial electrodes

    Science.gov (United States)

    Bureyev, O. A.; Surkov, Yu S.; Spirina, A. V.

    2017-05-01

    This work investigates the characteristics of the gas discharge system used to create an atmospheric pressure plasma flow. The plasma jet design with a cylindrical graphite cathode and an anode rod located on the axis of the system allows to realize regularly reproducible spark breakdowns mode with a frequency ∼ 5 kHz and a duration ∼ 40 μs. The device generates a cold atmospheric plasma flame with 1 cm in diameter in the flow of various plasma forming gases including nitrogen and air at about 100 mA average discharge current. In the described construction the cathode spots of individual spark channels randomly move along the inner surface of the graphite electrode creating the secondary plasma stream time-average distributed throughout the whole exit aperture area after the decay of numerous filamentary discharge channels. The results of the spectral diagnostics of plasma in the discharge gap and in the stream coming out of the source are presented. Despite the low temperature of atoms and molecules in plasma stream the cathode spots operation with temperature of ∼ 4000 °C at a graphite electrode inside a discharge system enables to saturate the plasma by CN-radicals and atomic carbon in the case of using nitrogen as the working gas.

  19. Effect of catecholamines and insulin on plasma volume and intravascular mass of albumin in man

    DEFF Research Database (Denmark)

    Hilsted, J; Christensen, N J; Larsen, S

    1989-01-01

    1. The effect of intravenous catecholamine infusions and of intravenous insulin on plasma volume and intravascular mass of albumin was investigated in healthy males. 2. Physiological doses of adrenaline (0.5 microgram/min and 3 microgram/min) increased peripheral venous packed cell volume...... significantly; intravenous noradrenaline at 0.5 microgram/min had no effect on packed cell volume, whereas packed cell volume increased significantly at 3 micrograms of noradrenaline/min. No significant change in packed cell volume was found during saline infusion. 3. During adrenaline infusion at 6 micrograms...... in packed cell volume, plasma volume, intravascular mass of albumin and transcapillary escape rate of albumin during hypoglycaemia may be explained by the combined actions of adrenaline and insulin....

  20. Non-thermal atmospheric pressure HF plasma source: generation of nitric oxide and ozone for bio-medical applications

    Science.gov (United States)

    Kühn, S.; Bibinov, N.; Gesche, R.; Awakowicz, P.

    2010-01-01

    A new miniature high-frequency (HF) plasma source intended for bio-medical applications is studied using nitrogen/oxygen mixture at atmospheric pressure. This plasma source can be used as an element of a plasma source array for applications in dermatology and surgery. Nitric oxide and ozone which are produced in this plasma source are well-known agents for proliferation of the cells, inhalation therapy for newborn infants, disinfection of wounds and blood ozonation. Using optical emission spectroscopy, microphotography and numerical simulation, the gas temperature in the active plasma region and plasma parameters (electron density and electron distribution function) are determined for varied nitrogen/oxygen flows. The influence of the gas flows on the plasma conditions is studied. Ozone and nitric oxide concentrations in the effluent of the plasma source are measured using absorption spectroscopy and electro-chemical NO-detector at variable gas flows. Correlations between plasma parameters and concentrations of the particles in the effluent of the plasma source are discussed. By varying the gas flows, the HF plasma source can be optimized for nitric oxide or ozone production. Maximum concentrations of 2750 ppm and 400 ppm of NO and O3, correspondingly, are generated.

  1. Efficient 'water window' soft x-ray high-Z plasma source

    International Nuclear Information System (INIS)

    Higashiguchi, T; Otsuka, T; Jiang, W; Endo, A; Li, B; Dunne, P; O'Sullivan, G

    2013-01-01

    Unresolved transition array (UTA) is scalable to shorter wavelengths, and we demonstrate a table-top broadband emission 'water window' soft x-ray source based on laser-produced plasmas. Resonance emission from multiply charged ions merges to produce intense UTAs in the 2 to 4 nm region, extending below the carbon K edge (4.37 nm). An outline of a microscope design for single-shot live cell imaging is proposed based on a bismuth (Bi) plasma UTA source, coupled to multilayer mirror optics

  2. Evaluating the accuracy of uranium isotope amount ratio measurements performed by a quadrupole and a multi-collector magnetic sector inductively coupled plasma mass spectrometers for nuclear safeguards

    International Nuclear Information System (INIS)

    Pereira de Oliveira, O. Jr.; Sarkis, J.E.S.; Ponzevera, E.; Alonso, A.; De Bolle, W.; Quetel, C.

    2008-01-01

    The n(U 235 )/n(U 238 ) isotope amount ratio in a set of samples was measured using two modern analytical techniques: quadrupole inductively coupled plasma mass spectrometry (ICP-QMS) and multi-collector magnetic sector inductively coupled plasma mass spectrometry (MC-ICPMS). The measured ratios were compared to the certified ratios provided by the high accuracy gas source mass spectrometry (GSMS). The components of the uncertainty were identified and their contribution to the combined standard uncertainty was estimated using the recommendations of the ISO-GUM guide. The values of the measurement uncertainty and bias were determined and then compared to the International Target Values for Measurement Uncertainties in Safeguarding Nuclear Materials. It appears that only the measurements performed by MC-ICPMS can meet the stringent requirements of international nuclear safeguards. (authors)

  3. Compact radio sources as a plasma turbulent reactor

    International Nuclear Information System (INIS)

    Atoyan, A.M.; Nagapetyan, A.

    1987-01-01

    The electromagnetic raiation spectra of a homogeneous cosmic radio source (CRS) wherein the relativistic electron acceleration on the langmuir waves leads to the formation of Maxwell-like spectra with characteristic value of the Lorentz-factor γ 0 ∼ 10 3 are considered. It has been shown that due to synchrotron radiation of relativistic electrons, usually observed from CRSs flat radiosepctra, gradually steepening at submillimeter wavelengths are naturally formed in the optically thin range of frequencies. The electromagnetic radiation at the scattering of the electron on the turbulence produces significant nonthermal infrared radiation. Inverse compton scattering of the relativistic electrons on the radio-infrared photons leads the production of X-rays. The characteristic of the electromagnetic radiation spectra obtained in the model are compared with the observational ones

  4. Estimation of the quantification uncertainty from flow injection and liquid chromatography transient signals in inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Laborda, Francisco; Medrano, Jesus; Castillo, Juan R.

    2004-01-01

    The quality of the quantitative results obtained from transient signals in high-performance liquid chromatography-inductively coupled plasma mass spectrometry (HPLC-ICPMS) and flow injection-inductively coupled plasma mass spectrometry (FI-ICPMS) was investigated under multielement conditions. Quantification methods were based on multiple-point calibration by simple and weighted linear regression, and double-point calibration (measurement of the baseline and one standard). An uncertainty model, which includes the main sources of uncertainty from FI-ICPMS and HPLC-ICPMS (signal measurement, sample flow rate and injection volume), was developed to estimate peak area uncertainties and statistical weights used in weighted linear regression. The behaviour of the ICPMS instrument was characterized in order to be considered in the model, concluding that the instrument works as a concentration detector when it is used to monitorize transient signals from flow injection or chromatographic separations. Proper quantification by the three calibration methods was achieved when compared to reference materials, although the double-point calibration allowed to obtain results of the same quality as the multiple-point calibration, shortening the calibration time. Relative expanded uncertainties ranged from 10-20% for concentrations around the LOQ to 5% for concentrations higher than 100 times the LOQ

  5. Determination of 90Sr and Pu isotopes in contaminated groundwater samples by inductively coupled plasma mass spectrometry

    Science.gov (United States)

    Zoriy, Miroslav V.; Ostapczuk, Peter; Halicz, Ludwik; Hille, Ralf; Becker, J. Sabine

    2005-04-01

    A sensitive analytical method for determining the artificial radionuclides 90Sr, 239Pu and 240Pu at the ultratrace level in groundwater samples from the Semipalatinsk Test Site area in Kazakhstan by double-focusing sector field inductively coupled plasma mass spectrometry (ICP-SFMS) was developed. In order to avoid possible isobaric interferences at m/z 90 for 90Sr determination (e.g. 90Zr+, 40Ar50Cr+, 36Ar54Fe+, 58Ni16O2+, 180Hf2+, etc.), the measurements were performed at medium mass resolution under cold plasma conditions. Pu was separated from uranium by means of extraction chromatography using Eichrom TEVA resin with a recovery of 83%. The limits of detection for 90Sr, 239Pu and 240Pu in water samples were determined as 11, 0.12 and 0.1 fg ml-1, respectively. Concentrations of 90Sr and 239Pu in contaminated groundwater samples ranged from 18 to 32 and from 28 to 856 fg ml-1, respectively. The 240Pu/239Pu isotopic ratio in groundwater samples was measured as 0.17. This isotope ratio indicates that the most probable source of contamination of the investigated groundwater samples was the nuclear weapons tests at the Semipalatinsk Test Site conducted by the USSR in the 1960s.

  6. Radionuclide determination in environmental samples by inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Lariviere, Dominic; Taylor, Vivien F.; Evans, R. Douglas; Cornett, R. Jack

    2006-01-01

    The determination of naturally occurring and anthropogenic radionuclides in the environment by inductively coupled plasma mass spectrometry has gained recognition over the last fifteen years, relative to radiometric techniques, as the result of improvement in instrumental performance, sample introduction equipment, and sample preparation. With the increase in instrumental sensitivity, it is now possible to measure ultratrace levels (fg range) of many radioisotopes, including those with half-lives between 1 and 1000 years, without requiring very complex sample pre-concentration schemes. However, the identification and quantification of radioisotopes in environmental matrices is still hampered by a variety of analytical issues such as spectral (both atomic and molecular ions) and non-spectral (matrix effect) interferences and instrumental limitations (e.g., abundance sensitivity). The scope of this review is to highlight recent analytical progress and issues associated with the determination of radionuclides by inductively coupled plasma mass spectrometry. The impact of interferences, instrumental limitations (e.g., degree of ionization, abundance sensitivity, detection limits) and low sample-to-plasma transfer efficiency on the measurement of radionuclides by inductively coupled plasma mass spectrometry will be described. Solutions that overcome these issues will be discussed, highlighting their pros and cons and assessing their impact on the measurement of environmental radioactivity. Among the solutions proposed, mass and chemical resolution through the use of sector-field instruments and chemical reactions/collisions in a pressurized cell, respectively, will be described. Other methods, such as unique sample introduction equipment (e.g., laser ablation, electrothermal vaporisation, high efficiency nebulization) and instrumental modifications/optimizations (e.g., instrumental vacuum, radiofrequency power, guard electrode) that improve sensitivity and performance

  7. Reduction of plyatomic ion interferences in indictively coupled plasma mass spectrometry with cryogenic desolvation

    Energy Technology Data Exchange (ETDEWEB)

    Alves, Luis C. [Iowa State Univ., Ames, IA (United States)

    1993-09-01

    A desolvation scheme for introducing aqueous and organic samples into an argon inductively coupled plasma is described; the aerosol generated by nebulizer is heated (+140 C) and cooled (-80 C) repeatedly, and the dried aerosol is then injected into the mass spectrometer. Polyatomic ions are greatly suppressed. This scheme was validated with analysis of seawater and urine reference samples. Finally, the removal of organic solvents by cryogenic desolvation was studied.

  8. Analysis of phosphatidylcholine oxidation products in human plasma using quadrupole time-of flight mass spectrometry

    OpenAIRE

    Adachi, Junko; Asano, Migiwa; Yoshioka, Naoki; Nushida, Hideyuki; Ueno, Yasuhiro

    2006-01-01

    We report here an application of the previous method for the analysis ofphosphatidylcholine (PC) and lysophosphatidylcholine (lysoPC) oxidation products inhuman plasma using quadrupole time of flight (Q-TOF) mass spectrometry withelectrospray ionization. We separated these products using an HPLC C8 column witha gradient of methanol and 10 mM aqueous ammonium acetate. Monohydroperoxides,epoxyhydroxy derivatives, oxo derivatives, and trihydroxides of palmitoyl-linoleoyl(C16:0/C18:2) PC and stea...

  9. On the vanishing electron-mass limit in plasma hydrodynamics in unbounded media

    Czech Academy of Sciences Publication Activity Database

    Donatelli, D.; Feireisl, Eduard; Novotný, A.

    2012-01-01

    Roč. 22, č. 6 (2012), s. 985-1012 ISSN 0938-8974 R&D Projects: GA ČR GA201/09/0917 Institutional research plan: CEZ:AV0Z10190503 Keywords : vanishing electron mass limit * plasma hydrodynamics * compressible fluid Subject RIV: BA - General Mathematics Impact factor: 1.566, year: 2012 http://link.springer.com/article/10.1007%2Fs00332-012-9134-5

  10. Compact quasi-monoenergetic photon sources from laser-plasma accelerators for nuclear detection and characterization

    Energy Technology Data Exchange (ETDEWEB)

    Geddes, Cameron G.R., E-mail: cgrgeddes@lbl.gov; Rykovanov, Sergey; Matlis, Nicholas H.; Steinke, Sven; Vay, Jean-Luc; Esarey, Eric H.; Ludewigt, Bernhard; Nakamura, Kei; Quiter, Brian J.; Schroeder, Carl B.; Toth, Csaba; Leemans, Wim P.

    2015-05-01

    Near-monoenergetic photon sources at MeV energies offer improved sensitivity at greatly reduced dose for active interrogation, and new capabilities in treaty verification, nondestructive assay of spent nuclear fuel and emergency response. Thomson (also referred to as Compton) scattering sources are an established method to produce appropriate photon beams. Applications are however restricted by the size of the required high-energy electron linac, scattering (photon production) system, and shielding for disposal of the high energy electron beam. Laser-plasma accelerators (LPAs) produce GeV electron beams in centimeters, using the plasma wave driven by the radiation pressure of an intense laser. Recent LPA experiments are presented which have greatly improved beam quality and efficiency, rendering them appropriate for compact high-quality photon sources based on Thomson scattering. Designs for MeV photon sources utilizing the unique properties of LPAs are presented. It is shown that control of the scattering laser, including plasma guiding, can increase photon production efficiency. This reduces scattering laser size and/or electron beam current requirements to scale compatible with the LPA. Lastly, the plasma structure can decelerate the electron beam after photon production, reducing the size of shielding required for beam disposal. Together, these techniques provide a path to a compact photon source system.

  11. Study of the matrix specific mass discrimination effects during inductively coupled plasma mass spectrometry isotope ratio measurements

    International Nuclear Information System (INIS)

    Vassileva, E.; Quetel, Ch.R.

    2004-01-01

    Sample matrix related effects on mass discrimination during inductively coupled plasma mass spectrometry (ICP-MS) isotope ratio measurements have only been rarely reported. However, they can lead to errors larger than the uncertainty claimed on the ratio results when not properly taken into account or corrected for. These matrix specific affects were experienced during an Isotope Dilution Mass Spectrometry (IDMS) campaign we carried out for the certification of the Cd amount content in some food digest samples (7% acidity and salts content around 450μg g -1 ). Dilution was not possible for Cd only present at the low ng g -1 level. Up to 1% difference was observed on Cd isotope ratio results between measurements performed directly or after matrix separation. This was a significant difference considering that less than 1.5% relative combined uncertainty was eventually estimated for these IDMS measurements. Similar results could be obtained either way after the implementation of necessary corrections. The direct measurement approach associated to a correction for mass discrimination effects using the food digest sample itself (and the IUPAC table values as reference for the natural Cd isotopic composition) was preferred as it was the easiest. Consequently, the impact of matrix effects on mass discrimination during isotope ratio measurements with two types of ICP- MS (quadrupole and magnetic sector instruments) was studied for 4 elements (Li, Cu, Cd and Tl). Samples of varying salinity (up to 0.25%) and acidity (up to 7%) characteristics were prepared using isotopic certified reference materials of these elements. The long term and short-term stability, respectively reproducibility and repeatability, of the results, as well as the evolution of the difference to certified ratio values were monitored. As expected the 13 investigated isotopic ratios were all sensitive to variations in salt and acid concentrations. Our experiments also showed that simultaneous variation

  12. Sensitive liquid chromatography-tandem mass spectrometry method for quantification of hydrochlorothiazide in human plasma.

    Science.gov (United States)

    Ramakrishna, N V S; Vishwottam, K N; Manoj, S; Koteshwara, M; Wishu, S; Varma, D P

    2005-12-01

    A simple, rapid, sensitive and specific liquid chromatography-tandem mass spectrometry method was developed and validated for quantification of hydrochlorothiazide (I), a common diuretic and anti-hypertensive agent. The analyte and internal standard, tamsulosin (II) were extracted by liquid-liquid extraction with diethyl ether-dichloromethane (70:30, v/v) using a Glas-Col Multi-Pulse Vortexer. The chromatographic separation was performed on a reversed-phase column (Waters symmetry C18) with a mobile phase of 10 mm ammonium acetate-methanol (15:85, v/v). The protonated analyte was quantitated in negative ionization by multiple reaction monitoring with a mass spectrometer. The mass transitions m/z 296.1 solidus in circle 205.0 and m/z 407.2 solidus in circle 184.9 were used to measure I and II, respectively. The assay exhibited a linear dynamic range of 0.5-200 ng/mL for hydrochlorothiazide in human plasma. The lower limit of quantitation was 500 pg/mL, with a relative standard deviation of less than 9%. Acceptable precision and accuracy were obtained for concentrations over the standard curve ranges. A run time of 2.5 min for each sample made it possible to analyze a throughput of more than 400 human plasma samples per day. The validated method has been successfully used to analyze human plasma samples for application in pharmacokinetic, bioavailability or bioequivalence studies. (c) 2005 John Wiley & Sons, Ltd.

  13. Diagnosing impaired glucose tolerance using direct infusion mass spectrometry of blood plasma.

    Directory of Open Access Journals (Sweden)

    Petr G Lokhov

    Full Text Available The goal of this study was to evaluate the capacity for mass spectrometry of blood plasma to diagnose impaired glucose tolerance (IGT. For this study, blood plasma samples from control subjects (n = 30 and patients with IGT (n = 20 were treated with methanol and low molecular weight fraction were then analyzed by direct infusion mass spectrometry. A total of 51 metabolite ions strongly associated with IGT were detected. The area under a receiver operating characteristic (ROC curve (AUC for diagnosing IGT that was based on an analysis of all these metabolites was 0.93 (accuracy 90%, specificity 90%, and sensitivity 90%. The associated reproducibility was 85%. The metabolites identified were also consistent with risk factors previously associated with the development of diabetes. Thus, direct infusion mass spectrometry of blood plasma metabolites represents a rapid, single-step, and reproducible method for the analysis of metabolites. Moreover, this method has the potential to serve as a prototype for clinical analyses that could replace the currently used glucose tolerance test with a more patient-friendly assay.

  14. Atomic processes and equation of state of high Z plasmas for EUV sources and their effects on the spatial and temporal evolution of the plasmas

    Science.gov (United States)

    Sasaki, Akira; Sunahara, Atushi; Furukawa, Hiroyuki; Nishihara, Katsunobu; Nishikawa, Takeshi; Koike, Fumihiro

    2016-03-01

    Laser-produced plasma (LPP) extreme ultraviolet (EUV) light sources have been intensively investigated due to potential application to next-generation semiconductor technology. Current studies focus on the atomic processes and hydrodynamics of plasmas to develop shorter wavelength sources at λ = 6.x nm as well as to improve the conversion efficiency (CE) of λ = 13.5 nm sources. This paper examines the atomic processes of mid-z elements, which are potential candidates for λ = 6.x nm source using n=3-3 transitions. Furthermore, a method to calculate the hydrodynamics of the plasmas in terms of the initial interaction between a relatively weak prepulse laser is presented.

  15. Mass and energy analysis of the ions in a plasma flood system

    International Nuclear Information System (INIS)

    Wooding, A.C.; Armour, D.G.; Berg, J.A. van den; Holmes, A.J.T.; Burgess, C.; Goldberg, R.D.

    2005-01-01

    Plasma flood systems, capable of providing a copious supply of electrons are used in ion implanters to control wafer charging and provide effective space charge neutralisation of the ion beam in the post-analysis/post-deceleration section of the beamline. Under appropriate conditions the plasma from the flood system interacts with the ion beam and this bridging leads to an enhanced beam transport efficiency in the final critical stage of the beamline. The effectiveness of this process depends on the properties of the plasma emanating from the system. In this study, a plasma analyser comprising a double hemi-spherical electrostatic energy analyser and a quadrupole mass spectrometer, was used to measure the energy distributions of all the ion species leaving a magnetically confined argon plasma, generated in the discharge chamber of a conventional flood neutraliser. The energy distributions extended to surprisingly high energies and the peak structures depended strongly on discharge voltage, discharge current and gas pressure. The nature of these dependencies was complex with both the pressure and arc current affecting the way in which the ion energy distributions depended on arc voltage. In all cases, multiply charged ions played a significant role in determining the nature of the ion energy distributions

  16. Ideal stability of cylindrical plasma in the presence of mass flow

    International Nuclear Information System (INIS)

    Bondeson, A.; Iacono, R.

    1988-11-01

    The ideal stability of cylindrical plasma with mass flows is investigated using the guiding centre plasma (GCP) model of Grad. For rotating plasmas, the kinetic treatment of the parallel motion in GCP gives significantly different results than fluid models, where the pressures are obtained from equations of state. In particular, GCP removes the resonance with slow magnetoacoustic waves and the loss of stability that results in magnetohydrodynamics (MHD) for near-soni flows. Because of the strong kinetic damping of the sound waves in an isothermal plasma, the slow waves have little influence on plasma stability in GCP at low β. In the large aspect ratio, low-β tokamak ordering, Alfvenic flows are needed to change the ideal GCP stability significantly. At lowest order in the inverse aspect ratio, flow can be favorable or unfavorable for stability of local modes depending on the profiles, but external kinks are always destilized by flow if the velocity vanishes at the edge. For high-β, reversed field pinch equilibria, numerical computations show that flow can be stabilizing for local modes, but external modes are destabilized by flow. It is shown that in three dimensions, the MHD equilibrium problem becomes hyperbolic for arbitrarily small flows across the magnetic field, whereas in GCP the equilibrium remains elliptic for sub-Alfvenic flows. (author) 7 figs., 1 tab, 32 refs

  17. Myoglobin plasma level related to muscle mass and fiber composition: a clinical marker of muscle wasting?

    Science.gov (United States)

    Weber, Marc-André; Kinscherf, Ralf; Krakowski-Roosen, Holger; Aulmann, Michael; Renk, Hanna; Künkele, Annette; Edler, Lutz; Kauczor, Hans-Ulrich; Hildebrandt, Wulf

    2007-08-01

    Progressive muscle wasting is a central feature of cancer-related cachexia and has been recognized as a determinant of poor prognosis and quality of life. However, until now, no easily assessable clinical marker exists that allows to predict or to track muscle wasting. The present study evaluated the potential of myoglobin (MG) plasma levels to indicate wasting of large locomotor muscles and, moreover, to reflect the loss of MG-rich fiber types, which are most relevant for daily performance. In 17 cancer-cachectic patients (weight loss 22%) and 27 age- and gender-matched healthy controls, we determined plasma levels of MG and creatine kinase (CK), maximal quadriceps muscle cross-sectional area (CSA) by magnetic resonance imaging, muscle morphology and fiber composition in biopsies from the vastus lateralis muscle, body cell mass (BCM) by impedance technique as well as maximal oxygen uptake (VO(2)max). In cachectic patients, plasma MG, muscle CSA, BCM, and VO(2)max were 30-35% below control levels. MG showed a significant positive correlation to total muscle CSA (r = 0.65, p max as an important functional readout. CK plasma levels appear to be less reliable because prolonged increases are observed in even subclinical myopathies or after exercise. Notably, cancer-related muscle wasting was not associated with increases in plasma MG or CK in this study.

  18. Plasma viscosity with mass transport in spherical inertial confinement fusion implosion simulations

    Energy Technology Data Exchange (ETDEWEB)

    Vold, E. L.; Molvig, K. [Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States); Joglekar, A. S. [University of Michigan, Ann Arbor, Michigan 48109 (United States); Ortega, M. I. [University of New Mexico, Albuquerque, New Mexico 87131 (United States); Moll, R. [University of California, Santa Cruz, California 95064 (United States); Fenn, D. [Florida State University, Tallahassee, Florida 32306 (United States)

    2015-11-15

    The effects of viscosity and small-scale atomic-level mixing on plasmas in inertial confinement fusion (ICF) currently represent challenges in ICF research. Many current ICF hydrodynamic codes ignore the effects of viscosity though recent research indicates viscosity and mixing by classical transport processes may have a substantial impact on implosion dynamics. We have implemented a Lagrangian hydrodynamic code in one-dimensional spherical geometry with plasma viscosity and mass transport and including a three temperature model for ions, electrons, and radiation treated in a gray radiation diffusion approximation. The code is used to study ICF implosion differences with and without plasma viscosity and to determine the impacts of viscosity on temperature histories and neutron yield. It was found that plasma viscosity has substantial impacts on ICF shock dynamics characterized by shock burn timing, maximum burn temperatures, convergence ratio, and time history of neutron production rates. Plasma viscosity reduces the need for artificial viscosity to maintain numerical stability in the Lagrangian formulation and also modifies the flux-limiting needed for electron thermal conduction.

  19. Mass and energy analysis of the ions in a plasma flood system

    Energy Technology Data Exchange (ETDEWEB)

    Wooding, A.C. [Institute of Materials Research, University of Salford, Salford M54WT (United Kingdom); Armour, D.G. [Institute of Materials Research, University of Salford, Salford M54WT (United Kingdom); Berg, J.A. van den [Institute of Materials Research, University of Salford, Salford M54WT (United Kingdom)]. E-mail: j.a.vandenberg@salford.ac.uk; Holmes, A.J.T. [Marcham Scientific, Hungerford, Berks RG17 0LH (United Kingdom); Burgess, C. [Applied Materials UK Ltd., Foundry Lane, Horsham, West Sussex RH13 5PX (United Kingdom); Goldberg, R.D. [Applied Materials UK Ltd., Foundry Lane, Horsham, West Sussex RH13 5PX (United Kingdom)

    2005-08-01

    Plasma flood systems, capable of providing a copious supply of electrons are used in ion implanters to control wafer charging and provide effective space charge neutralisation of the ion beam in the post-analysis/post-deceleration section of the beamline. Under appropriate conditions the plasma from the flood system interacts with the ion beam and this bridging leads to an enhanced beam transport efficiency in the final critical stage of the beamline. The effectiveness of this process depends on the properties of the plasma emanating from the system. In this study, a plasma analyser comprising a double hemi-spherical electrostatic energy analyser and a quadrupole mass spectrometer, was used to measure the energy distributions of all the ion species leaving a magnetically confined argon plasma, generated in the discharge chamber of a conventional flood neutraliser. The energy distributions extended to surprisingly high energies and the peak structures depended strongly on discharge voltage, discharge current and gas pressure. The nature of these dependencies was complex with both the pressure and arc current affecting the way in which the ion energy distributions depended on arc voltage. In all cases, multiply charged ions played a significant role in determining the nature of the ion energy distributions.

  20. Enhancement of H{sup -}/D{sup -} volume production in a double plasma type negative ion source

    Energy Technology Data Exchange (ETDEWEB)

    Fukumasa, Osamu; Nishimura, Hideki; Sakiyama, Satoshi [Yamaguchi Univ., Ube (Japan). Faculty of Engineering

    1997-02-01

    H{sup -}/D{sup -} production in a pure volume source has been studied. In our double plasma type negative ion source, both energy and density of fast electrons are well controlled. With the use of this source, the enhancement of H{sup -}/D{sup -} production has been observed. Namely, under the same discharge power, the extracted H{sup -}/D{sup -} current in the double plasma operation is higher than that in the single plasma operation. At the same time, measurements of plasma parameters have been made in the source and the extractor regions for these two cases. (author)

  1. Application of atmospheric plasma sources in growth and differentiation of plant and mammalian stem cells

    Science.gov (United States)

    Puac, Nevena

    2014-10-01

    The expansion of the plasma medicine and its demand for in-vivo treatments resulted in fast development of various plasma devices that operate at atmospheric pressure. These sources have to fulfill all demands for application on biological samples. One of the sources that meet all the requirements needed for treatment of biological material is plasma needle. Previously, we have used this device for sterilization of planctonic samples of bacteria, MRSA biofilm, for improved differentiation of human periodontal stem cells into osteogenic line and for treatment of plant meristematic cells. It is well known that plasma generates reactive oxygen species (ROS) and reactive nitrogen species (RNS) that strongly affect metabolism of living cells. One of the open issues is to correlate external plasma products (electrons, ions, RNS, ROS, photons, strong fields etc.) with the immediate internal response which triggers or induces effects in the living cell. For that purpose we have studied the kinetics of enzymes which are typical indicators of the identity of reactive species from the plasma created environment that can trigger signal transduction in the cell and ensue cell activity. In collaboration with Suzana Zivkovicm, Institute for Biological Research ``Sinisa Stankovic,'' University of Belgrade; Nenad Selakovic, Institute of Physics, University of Belgrade; Milica Milutinovic, Jelena Boljevic, Institute for Biological Research ``Sinisa Stankovic,'' University of Belgrade; and Gordana Malovic, Zoran Lj. Petrovic, Institute of Physics, University of Belgrade. Grants III41011, ON171037 and ON173024, MESTD, Serbia.

  2. Production and transport chemistry of atomic fluorine in remote plasma source and cylindrical reaction chamber

    International Nuclear Information System (INIS)

    Gangoli, S P; Johnson, A D; Fridman, A A; Pearce, R V; Gutsol, A F; Dolgopolsky, A

    2007-01-01

    Increasingly, NF 3 -based plasmas are being used in semiconductor manufacturing to clean chemical vapour deposition (CVD) chambers. With advantages such as faster clean times, substantially lower emissions of gases having high global warming potentials, and reduced chamber damage, NF 3 plasmas are now favoured over fluorocarbon-based processes. Typically, a remote plasma source (RPS) is used to dissociate the NF 3 gas and produce atomic fluorine that etches the CVD residues from the chamber surfaces. However, it is important to efficiently transport F atoms from the plasma source into the process chamber. The current work is aimed at understanding and improving the key processes involved in the production and transport of atomic fluorine atoms. A zero-dimensional model of NF 3 dissociation and F production chemistry in the RPS is developed based on various known and derived plasma parameters. Additionally, a model describing the transport of atomic fluorine is proposed that includes both physical (diffusion, adsorption and desorption) and chemical processes (surface and three-body volume recombination). The kinetic model provides an understanding of the impact of chamber geometry, gas flow rates, pressure and temperature on fluorine recombination. The plasma-kinetic model is validated by comparing model predictions (percentage F atom density) with experimental results (etch rates)

  3. Simulation Study of an Extended Density DC Glow Toroidal Plasma Source

    International Nuclear Information System (INIS)

    Granda-Gutierrez, E. E.; Piedad-Beneitez, A. de la; Lopez-Callejas, R.; Godoy-Cabrera, O. G.; Benitez-Read, J. S.; Pacheco-Sotelo, J. O.; Pena-Eguiluz, R.; Mercado-Cabrera, A.; Valencia A, R.; Barocio, S. R.

    2006-01-01

    Conventional wisdom assigns the DC glow discharge regime to plasma currents below ∼500 mA values, beyond which the discharge falls into the anomalous glow and the turbulent arc regimes. However, we have found evidence that, during toroidal discharges, this barrier can be ostensibly extended up to 800 mA. Thus, a computer simulation has been applied to the evolution of the main electrical characteristics of such a glow discharge plasma in a toroidal vessel in order to design and construct a respective voltage/current controlled source. This should be able to generate a DC plasma in the glow regime with which currents in the range 10-3-100 A can be experimented and 109-1010 cm-3 plasma densities can be achieved to PIII optimization purposes. The plasma is modelled as a voltage-controlled current source able to be turned on whenever the breakdown voltage is reached across the gap between the anode and the vessel wall. The simulation outcome fits well our experimental measurements showing that the plasma current obeys power laws that are dependent on the power current and other control variables such as the gas pressure

  4. Quantitative determination of minor and trace elements in rocks and soils by spark source mass spectrometry

    International Nuclear Information System (INIS)

    Ure, A.M.; Bacon, J.R.

    1978-01-01

    Experimental details are given of the quantitative determination of minor and trace elements in rocks and soils by spark source mass spectrometry. The effects of interfering species, and corrections that can be applied, are discussed. (U.K.)

  5. Beam plasma 14 MeV neutron source for fusion materials development

    International Nuclear Information System (INIS)

    Ravenscroft, D.; Bulmer, D.; Coensgen, F.; Doggett, J.; Molvik, A.; Souza, P.; Summers, L.; Williamson, V.

    1991-09-01

    The conceptual engineering design and expected performance for a 14 MeV DT neutron source is detailed. The source would provide an intense neutron flux for accelerated testing of fusion reactor materials. The 150-keV neutral beams inject energetic deuterium atoms, that ionize, are trapped, then react with a warm (200 eV), dense tritium target plasma. This produces a neutron source strength of 3.6 x 10 17 n/sec for a neutron power density at the plasma edge of 5--10 MW/m 2 . This is several times the ∼2 MW/m 2 anticipated at the first wall of fusion reactors. This high flux provides accelerated end-of-life tests of 1- to 2-year duration, thus making materials development possible. The modular design of the source and the facilities are described

  6. Studies of plasma breakdown and electron heating on a 14 GHz ECR ion source through measurement of plasma bremsstrahlung

    Energy Technology Data Exchange (ETDEWEB)

    Ropponen, T; Machicoane, G; Leitner, D [National Superconducting Cyclotron Laboratory, MSU, East Lansing, MI 48824 (United States); Tarvainen, O; Toivanen, V; Koivisto, H; Kalvas, T; Peura, P; Jones, P [University of Jyvaeskylae, Department of Physics, PO Box 35 (YFL), 40500 Jyvaeskylae (Finland); Izotov, I; Skalyga, V; Zorin, V [Institute of Applied Physics, RAS, 46 Ulyanov St., 603950 Nizhny Novgorod (Russian Federation); Noland, J, E-mail: tommi.ropponen@gmail.com, E-mail: olli.tarvainen@jyu.fi [Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, CA 94720 (United States)

    2011-10-15

    Temporal evolution of plasma bremsstrahlung emitted by a 14 GHz electron cyclotron resonance ion source (ECRIS) operated in pulsed mode is presented in the energy range 1.5-400 keV with 100 {mu}s resolution. Such a high temporal resolution together with this energy range has never been measured before with an ECRIS. Data are presented as a function of microwave power, neutral gas pressure, magnetic field configuration and seed electron density. The saturation time of the bremsstrahlung count rate is almost independent of the photon energy up to 100 keV and exhibits similar characteristics with the neutral gas balance. The average photon energy during the plasma breakdown is significantly higher than that during the steady state and depends strongly on the density of seed electrons. The results are consistent with a theoretical model describing the evolution of the electron energy distribution function during the preglow transient.

  7. Experimental benchmark of the NINJA code for application to the Linac4 H- ion source plasma

    Science.gov (United States)

    Briefi, S.; Mattei, S.; Rauner, D.; Lettry, J.; Tran, M. Q.; Fantz, U.

    2017-10-01

    For a dedicated performance optimization of negative hydrogen ion sources applied at particle accelerators, a detailed assessment of the plasma processes is required. Due to the compact design of these sources, diagnostic access is typically limited to optical emission spectroscopy yielding only line-of-sight integrated results. In order to allow for a spatially resolved investigation, the electromagnetic particle-in-cell Monte Carlo collision code NINJA has been developed for the Linac4 ion source at CERN. This code considers the RF field generated by the ICP coil as well as the external static magnetic fields and calculates self-consistently the resulting discharge properties. NINJA is benchmarked at the diagnostically well accessible lab experiment CHARLIE (Concept studies for Helicon Assisted RF Low pressure Ion sourcEs) at varying RF power and gas pressure. A good general agreement is observed between experiment and simulation although the simulated electron density trends for varying pressure and power as well as the absolute electron temperature values deviate slightly from the measured ones. This can be explained by the assumption of strong inductive coupling in NINJA, whereas the CHARLIE discharges show the characteristics of loosely coupled plasmas. For the Linac4 plasma, this assumption is valid. Accordingly, both the absolute values of the accessible plasma parameters and their trends for varying RF power agree well in measurement and simulation. At varying RF power, the H- current extracted from the Linac4 source peaks at 40 kW. For volume operation, this is perfectly reflected by assessing the processes in front of the extraction aperture based on the simulation results where the highest H- density is obtained for the same power level. In surface operation, the production of negative hydrogen ions at the converter surface can only be considered by specialized beam formation codes, which require plasma parameters as input. It has been demonstrated that

  8. Railguns and plasma accelerators: arc armatures, pulse power sources and US patents

    Energy Technology Data Exchange (ETDEWEB)

    Friedrich, O.M. Jr.

    1980-11-01

    Railguns and plasma accelerators have the potential for use in many basic and applied research projects, such as in creating high-pressures for equation-of-state studies and in impact fusion. A brief review of railguns and plasma accelerators with references is presented. Railgun performance is critically dependent on armature operation. Plasma arc railgun armatures are addressed. Pulsed power supplies for multi-stage railguns are considered. This includes brief comments on the compensated pulsed alternator, or compulsator, rotating machinery, and distributed energy sources for railguns. References are given at the end of each section. Appendix A contains a brief review of the US Patents on multi-staging techniques for electromagnetic accelerators, plasma propulsion devices, and electric guns.

  9. Railguns and plasma accelerators: arc armatures, pulse power sources and US patents

    International Nuclear Information System (INIS)

    Friedrich, O.M. Jr.

    1980-11-01

    Railguns and plasma accelerators have the potential for use in many basic and applied research projects, such as in creating high-pressures for equation-of-state studies and in impact fusion. A brief review of railguns and plasma accelerators with references is presented. Railgun performance is critically dependent on armature operation. Plasma arc railgun armatures are addressed. Pulsed power supplies for multi-stage railguns are considered. This includes brief comments on the compensated pulsed alternator, or compulsator, rotating machinery, and distributed energy sources for railguns. References are given at the end of each section. Appendix A contains a brief review of the US Patents on multi-staging techniques for electromagnetic accelerators, plasma propulsion devices, and electric guns

  10. First results from the Los Alamos plasma source ion implantation experiment

    International Nuclear Information System (INIS)

    Rej, D.J.; Faehl, R.J.; Gribble, R.J.; Henins, I.; Kodali, P.; Nastasi, M.; Reass, W.A.; Tesmer, J.; Walter, K.C.; Wood, B.P.; Conrad, J.R.; Horswill, N.; Shamim, M.; Sridharan, K.

    1993-01-01

    A new facility is operational at Los Alamos to examine plasma source ion implantation on a large scale. Large workpieces can be treated in a 1.5-m-diameter, 4.6-m-long plasma vacuum chamber. Primary emphasis is directed towards improving tribological properties of metal surfaces. First experiments have been performed at 40 kV with nitrogen plasmas. Both coupons and manufactured components, with surface areas up to 4 m 2 , have been processed. Composition and surface hardness of implanted materials are evaluated. Implant conformality and dose uniformity into practical geometries are estimated with multidimensional particle-in-cell computations of plasma electron and ion dynamics, and Monte Carlo simulations of ion transport in solids

  11. On electromagnetic wave propagation through a plasma sheath produced by a moving ionization source

    International Nuclear Information System (INIS)

    Semenova, V.I.

    1977-01-01

    Features of the interaction of electromagnetic waves are considered with a nonstationary plasma layer of a finite thickness, produced in an immovable gas by a movable ionization source. It is shown that a static magnetic field excited on the ionization front in build-up of electrons produced in the incident wave field reemits the energy to the electromagnetic wave during the plasma relaxation caused by recombination processes. As a result the electromagnetic wave of a finite amplitude may propagate behind the nonstationary layer of an ''opaque'' (ωsub(p)sup(2)>>ωsub(urc)sup((0))sup(2)) plasma as distinct from the layer of a movable stationary plasma with the same parameters

  12. Microwave frequency sweep interferometer for plasma density measurements in ECR ion sources: Design and preliminary results

    Energy Technology Data Exchange (ETDEWEB)

    Torrisi, Giuseppe [INFN - Laboratori Nazionali del Sud, Via S. Sofia 62, 95125 Catania (Italy); University Mediterranea of Reggio Calabria, Reggio Calabria (Italy); Mascali, David; Neri, Lorenzo; Leonardi, Ornella; Celona, Luigi; Castro, Giuseppe; Agnello, Riccardo; Caruso, Antonio; Passarello, Santi; Longhitano, Alberto; Gammino, Santo [INFN - Laboratori Nazionali del Sud, Via S. Sofia 62, 95125 Catania (Italy); Sorbello, Gino [INFN - Laboratori Nazionali del Sud, Via S. Sofia 62, 95125 Catania (Italy); University of Catania, Catania, Italy and INFN-LNS, Catania (Italy); Isernia, Tommaso [University Mediterranea of Reggio Calabria, Reggio Calabria (Italy)

    2016-02-15

    The Electron Cyclotron Resonance Ion Sources (ECRISs) development is strictly related to the availability of new diagnostic tools, as the existing ones are not adequate to such compact machines and to their plasma characteristics. Microwave interferometry is a non-invasive method for plasma diagnostics and represents the best candidate for plasma density measurement in hostile environment. Interferometry in ECRISs is a challenging task mainly due to their compact size. The typical density of ECR plasmas is in the range 10{sup 11}–10{sup 13} cm{sup −3} and it needs a probing beam wavelength of the order of few centimetres, comparable to the chamber radius. The paper describes the design of a microwave interferometer developed at the LNS-INFN laboratories based on the so-called “frequency sweep” method to filter out the multipath contribution in the detected signals. The measurement technique and the preliminary results (calibration) obtained during the experimental tests will be presented.

  13. Boundary layer plasmas as a source for high-latitude, early afternoon, auroral arcs

    International Nuclear Information System (INIS)

    Lundin, R.; Evans, D.S.

    1985-02-01

    Simultaneous measurements of hot boundary layer plasma from PROGNOZ-7 and particle precipitation from the TIROS/NOAA satellite in nearly magnetically conjugate regions have been used to study the dynamo process responsible for the formation of high latitude, early afternoon, auroral arcs. Characteristic for the PROGNOZ-7 observations in the dayside boundary layer at high latitudes is the frequent occurrence of regions with injected magnetosheath plasma embedded in a 'halo' of antisunward flowing magnetosphere plasma. The injected magnetosheath plasma have several features which indicate that it also acts as a local source of EMF in the boundary layer. The process resembles that of a local MHD dynamo driven by the excess drift velocity of the injected magnetosheath plasma relative to the background magnetospheric plasma. The dynamo region is capable of driving fielc-aligned currents that couple to the ionosphere, where the upward current is associated with the high latitude auroral arcs. We demonstrate that the large-scale morphology as well as the detailed data intercomparison between PROGNOZ-7 and TIROS-N both agree well with a local injection of magnetosheath plasma into the dayside boundary layer as the main dynamo process powering the high-latitude, early afternoon auroral arcs. (Author)

  14. The inductively coupled plasma as a source for the measurement of fundamental spectroscopic constants

    International Nuclear Information System (INIS)

    Farnsworth, P.B.

    1993-01-01

    Inductively coupled plasmas (ICPs) are stable, robust sources for the generation of spectra from neutral and singly ionized atoms. They are used extensively for analytical spectrometry, but have seen limited use for the measurement of fundamental spectroscopic constants. Several properties of the ICP affect its suitability for such fundamental measurements. They include: spatial structure, spectral background, noise characteristics, electron densities and temperatures, and the state of equilibrium in the plasma. These properties are particularly sensitive to the means by which foreign atoms are introduced into the plasma. With some departures from the operating procedures normally used in analytical measurements, the ICP promise to be a useful source for the measurement of fundamental atomic constants. (orig.)

  15. First plasma of the A-PHOENIX electron cyclotron resonance ion source

    International Nuclear Information System (INIS)

    Thuillier, T.; Lamy, T.; Latrasse, L.; Angot, J.

    2008-01-01

    A-PHOENIX is a new compact hybrid electron cyclotron resonance ion source using a large permanent magnet hexapole (1.92 T at the magnet surface) and high temperature superconducting Solenoids (3 T) to make min-vertical bar B vertical bar structure suitable for 28 GHz cw operation. The final assembly of the source was achieved at the end of June 2007. The first plasma of A-PHOENIX at 18 GHz was done on the 16th of August, 2007. The technological specificities of A-PHOENIX are presented. The large hexapole built is presented and experimental magnetic measurements show that it is nominal with respect to simulation. A fake plasma chamber prototype including thin iron inserts showed that the predicted radial magnetic confinement can be fulfilled up to 2.15 T at the plasma chamber wall. Scheduled planning of experiments until the end of 2008 is presented

  16. Quasi-steady state, low current behaviour of a magnetized coaxial plasma source

    International Nuclear Information System (INIS)

    Gray, Travis K; Mayo, Robert M; Bourham, Mohamed A

    2005-01-01

    The Coaxial Plasma Source-1 facility (Mayo R M et al 1995 Plasma Sources Sci. Technol. 4 47) was modified from a short pulse, high current (SPHC) pulse forming network (PFN) with very low inductance (∼200 nH) to a large inductance ladder circuit. This modification allows for a longer, flat top gun current pulse that eliminates the under-damped, sinusoidal behaviour of the gun current with consequent interruptions in plasma parameters. The new PFN was designed to produce a current waveform for a much longer period (∼1 ms). As a consequence of increasing the pulse length, the magnitude of the gun current was reduced as no additional energy storage was added to the PFN. The characterization of the electrical and plasma behaviour of the experiment operated with the long pulse, low current (LPLC) PFN is presented. The gun currents produced by the LPLC PFN are approximately one-fifth in magnitude of the gun currents produced by the SPHC PFN. Axial plasma parameters were measured near the muzzle of the plasma source, and electron densities were found to range from 1 x 10 19 m -3 to 7 x 10 19 m -3 depending upon the axial location. These values are approximately 1-2 orders of magnitude less than the electron densities produced by the SPHC PFN at the same locations. Electron temperatures range from 30 to 60 eV at these locations and are very similar to those produced by the SPHC PFN. A resistive MHD model was applied as an order estimate of the plasma resistivity and demonstrates reasonable agreement with measured values of the magnetized coaxial gun resistance

  17. Quasi-steady state, low current behaviour of a magnetized coaxial plasma source

    Energy Technology Data Exchange (ETDEWEB)

    Gray, Travis K; Mayo, Robert M; Bourham, Mohamed A [Department of Nuclear Engineering, North Carolina State University, Raleigh, NC 27695-7909 (United States)

    2005-11-15

    The Coaxial Plasma Source-1 facility (Mayo R M et al 1995 Plasma Sources Sci. Technol. 4 47) was modified from a short pulse, high current (SPHC) pulse forming network (PFN) with very low inductance ({approx}200 nH) to a large inductance ladder circuit. This modification allows for a longer, flat top gun current pulse that eliminates the under-damped, sinusoidal behaviour of the gun current with consequent interruptions in plasma parameters. The new PFN was designed to produce a current waveform for a much longer period ({approx}1 ms). As a consequence of increasing the pulse length, the magnitude of the gun current was reduced as no additional energy storage was added to the PFN. The characterization of the electrical and plasma behaviour of the experiment operated with the long pulse, low current (LPLC) PFN is presented. The gun currents produced by the LPLC PFN are approximately one-fifth in magnitude of the gun currents produced by the SPHC PFN. Axial plasma parameters were measured near the muzzle of the plasma source, and electron densities were found to range from 1 x 10{sup 19} m{sup -3} to 7 x 10{sup 19} m{sup -3} depending upon the axial location. These values are approximately 1-2 orders of magnitude less than the electron densities produced by the SPHC PFN at the same locations. Electron temperatures range from 30 to 60 eV at these locations and are very similar to those produced by the SPHC PFN. A resistive MHD model was applied as an order estimate of the plasma resistivity and demonstrates reasonable agreement with measured values of the magnetized coaxial gun resistance.

  18. AutoLens: Automated Modeling of a Strong Lens's Light, Mass and Source

    Science.gov (United States)

    Nightingale, J. W.; Dye, S.; Massey, Richard J.

    2018-05-01

    This work presents AutoLens, the first entirely automated modeling suite for the analysis of galaxy-scale strong gravitational lenses. AutoLens simultaneously models the lens galaxy's light and mass whilst reconstructing the extended source galaxy on an adaptive pixel-grid. The method's approach to source-plane discretization is amorphous, adapting its clustering and regularization to the intrinsic properties of the lensed source. The lens's light is fitted using a superposition of Sersic functions, allowing AutoLens to cleanly deblend its light from the source. Single component mass models representing the lens's total mass density profile are demonstrated, which in conjunction with light modeling can detect central images using a centrally cored profile. Decomposed mass modeling is also shown, which can fully decouple a lens's light and dark matter and determine whether the two component are geometrically aligned. The complexity of the light and mass models are automatically chosen via Bayesian model comparison. These steps form AutoLens's automated analysis pipeline, such that all results in this work are generated without any user-intervention. This is rigorously tested on a large suite of simulated images, assessing its performance on a broad range of lens profiles, source morphologies and lensing geometries. The method's performance is excellent, with accurate light, mass and source profiles inferred for data sets representative of both existing Hubble imaging and future Euclid wide-field observations.

  19. [Experimental investigation of laser plasma soft X-ray source with gas target].

    Science.gov (United States)

    Ni, Qi-liang; Gong, Yan; Lin, Jing-quan; Chen, Bo; Cao, Jian-lin

    2003-02-01

    This paper describes a debris-free laser plasma soft X-ray source with a gas target, which has high operating frequency and can produce strong soft X-ray radiation. The valve of this light source is drived by a piezoelectrical ceramic whose operating frequency is up to 400 Hz. In comparison with laser plasma soft X-ray sources using metal target, the light source is debris-free. And it has higher operating frequency than gas target soft X-ray sources whose nozzle is controlled by a solenoid valve. A channel electron multiplier (CEM) operating in analog mode is used to detect the soft X-ray generated by the laser plasma source, and the CEM's output is fed to to a charge-sensitive preamplifier for further amplification purpose. Output charges from the CEM are proportional to the amplitude of the preamplifier's output voltage. Spectra of CO2, Xe and Kr at 8-14 nm wavelength which can be used for soft X-ray projection lithography are measured. The spectrum for CO2 consists of separate spectral lines originate mainly from the transitions in Li-like and Be-like ions. The Xe spectrum originating mainly from 4d-5f, 4d-4f, 4d-6p and 4d-5p transitions in multiply charged xenon ions. The spectrum for Kr consists of separate spectral lines and continuous broad spectra originating mainly from the transitions in Cu-, Ni-, Co- and Fe-like ions.

  20. Energization of the Ring Current through Convection of Substorm Enhancements of the Plasma Sheet Source.

    Science.gov (United States)

    Menz, A.; Kistler, L. M.; Mouikis, C.; Spence, H. E.; Henderson, M. G.; Matsui, H.

    2017-12-01

    It has been shown that electric field strength and night-side plasma sheet density are the two best predictors of the adiabatic energy gain of the ring current during geomagnetic storms (Liemohn and Khazanov, 2005). While H+ dominates the ring current during quiet times, O+ can contribute substantially during geomagnetic storms. Substorm activity provides a mechanism to enhance the energy density of O+ in the plasma sheet during geomagnetic storms, which is then convected adiabatically into the inner-magnetosphere. Using the Van Allen Probes data in the the plasma sheet source region (defined as L>5.5 during storms) and the inner magnetosphere, along with LANL-GEO data to identify substorm injection times, we show that adiabatic convection of O+ enhancements in the source region can explain the observed enhancements in the inner magnetosphere. We use the UNH-IMEF electric field model to calculate drift times from the source region to the inner magnetosphere to test whether enhancements in the inner-magnetosphere can be explained by dipolarization driven enhancements in the plasma sheet source hours before.

  1. Study of the general plasma characteristics of a high power multifilament ion source

    International Nuclear Information System (INIS)

    Schoenberg, K.F.

    1979-09-01

    A general assessment of the steady state and time dependent plasma properties which characterize a high power multifilament ion source is presented. Steady state measurements, obtained via a pulsed electrostatic probe data acquisition system, are described. Fluctuation measurements, obtained via a broadband digital spectral analysis system, are also given

  2. Increase of plasma ion source efficiency utilizing collisions of the second kind

    International Nuclear Information System (INIS)

    Winkler, H.

    1979-01-01

    It is experimentally found that the efficiency of a plasma ion source for use in an electromagnetic separator can be increased under appropriate operating conditions utilizing collisions of the second kind, of a proper gas is additionally introduced into the arc chamber containing atoms with metastable excited levels. (author)

  3. Mass spectrometer diagnostic technique in the study of stationary afterglow plasmas in helium, argon and krypton

    International Nuclear Information System (INIS)

    Langenwalter, M.

    1979-01-01

    Since some years the method of massspectrometric monitoring has become an important tool in the analysis of time resolved (or stationary) afterglow plasmas. The present thesis reports the construction and testing of a new fully bakeable UHV-stationary-afterglow-apparatus using a hollow cathode discharge as plasma source for the first time. The hollow cathode is moveable perpendicular to its axis relative to the sampling orifice (i.e. a very small hole at the centre of the plasma container's boundary), so that the radical distribution of the charged particle density can be studied. Several specific extraction conditions for ions from the plasma especially the sampling probe potential have been systematically investigated. Results are illustrated and discussed. The new apparatus has been tested by determining the ambipolar diffusion coefficient of the molecular ion He 2 + in a pure Helium-plasma in thermal equilibrium. The present result (Dsub(a2) = 603 +- 38 / P 0 cm 2 s -1 ) is in agreement with results reported by other workers. Finally an example for the radial behaviour of the Ar + -sampling current in an Argon-discharge for several different times in the afterglow period is given. The shown behaviour agrees relatively well with the theoretically predicted radial ion density distribution, i.e. the zero-order Ressel'function. (Author)

  4. An accelerated beam-plasma neutron/proton source and early application of a fusion plasma

    International Nuclear Information System (INIS)

    Ohnishi, M.; Yoshikawa, K.; Yamamoto, Y.; Hoshino, C.; Masuda, K.; Miley, G.; Jurczyk, B.; Stubbers, R.; Gu, Y.

    1999-01-01

    We measured the number of the neutrons and protons produced by D-D reactions in an accelerated beam-plasma fusion and curried out the numerical simulations. The linear dependence of the neutron yield on a discharge current indicates that the fusion reactions occur between the background gas and the fast particles. i.e. charge exchanged neutrals and accelerated ions. The neutron yield divided by (fusion cross section x ion current x neutral gas pressure) still possesses the dependence of the 1.2 power of discharge voltage. which shows the fusion reactions are affected by the electrostatic potential built-up in the center. The measured proton birth profiles suggest the existence of a double potential well, which is supported by the numerical simulations. (author)

  5. Plasma source by microwaves: design description; Fuente de plasma por microondas: descripcion de diseno

    Energy Technology Data Exchange (ETDEWEB)

    Camps, E; Olea, O; Andrade, R; Anguiano, G

    1992-03-15

    The design of a device for the formation of a plasma with densities of the order of 10{sup 12} cm{sup -} {sup 3} and low temperatures (T{sub e} {approx} 40 eV) is described. For such purpose it was carried out in the device a microwave discharge (f{sub o} = 2.45 GHz) in a resonator of high Q factor, immersed in a static external magnetic field. The device worked in the regime {omega}{sub ce} {<=} {omega}{sub o}/2 ({omega}{sub ce}- cyclotron frequency of the electrons, ({omega}{sub o} = 2 {pi} f{sub o}) where is possible the excitement of non lineal phenomena of waves transformation. (Author)

  6. Aluminium content of some processed foods, raw materials and food additives in China by inductively coupled plasma-mass spectrometry.

    Science.gov (United States)

    Deng, Gui-Fang; Li, Ke; Ma, Jing; Liu, Fen; Dai, Jing-Jing; Li, Hua-Bin

    2011-01-01

    The level of aluminium in 178 processed food samples from Shenzhen city in China was evaluated using inductively coupled plasma-mass spectrometry. Some processed foods contained a concentration of up to 1226 mg/kg, which is about 12 times the Chinese food standard. To establish the main source in these foods, Al levels in the raw materials were determined. However, aluminium concentrations in raw materials were low (0.10-451.5 mg/kg). Therefore, aluminium levels in food additives used in these foods was determined and it was found that some food additives contained a high concentration of aluminium (0.005-57.4 g/kg). The results suggested that, in the interest of public health, food additives containing high concentrations of aluminium should be replaced by those containing less. This study has provided new information on aluminium levels in Chinese processed foods, raw materials and a selection of food additives.

  7. Application of isotope dilution for the determination of thorium in biological samples by inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Igarashi, Yasuhito; Shiraishi, Kunio; Takaku, Yuichi; Masuda, Kimihiko; Seki, Riki; Yamamoto, Masayoshi.

    1992-01-01

    The applicability of isotope dilution-inductively coupled plasma mass spectrometry (ID-ICP-MS) was examined for Th in biological samples. A naturally occurring isotope of Th(Th-230) was used as the spiking isotope. The concentration of Th-230 in the final sample solution was about 50 - 60 pg/ml; an isotope ratio of 232/230 could be measured with a relative standard deviation of less than 2%. The error magnification depended on the amount of Th-232 being concomitant with the Th-230. Though it was shown that one ng of Th-232 could be determined with reasonable precision with a tracer of the present purity, more care should be taken to reduce any source of systematic error. (author)

  8. Plasma Desorption Mass Spectrometry using TANDEM accelerator in National Industrial Research Inst. of Nagoya

    Energy Technology Data Exchange (ETDEWEB)

    Mizota, Takeshi; Nakao, Setsuo; Niwa, Hiroaki; Saito, Kazuo [Particle Beam Sceince Laboratory, Multi-Function Material Science Department, National Industrial Research Inst. of Nagoya, Nagoya (Japan)

    2001-02-01

    Plasma Desorption Mass Spectrometry (PDMS) analysis was studied using TANDEM accelerator. The heavy ions of MeV range emit the secondary ions of atoms, molecules, polymers and clusters from the irradiated samples without destruction. The analysis system of PDMS designed and set-up using a mass spectrometer of Time of Flight and the TANDEM accelerator. The system performance was tested for C-60 fullerene on the surface of the samples using 11.2 MeV {sup 28}Si beams produced by the TANDEM accelerator of 1.7MV. The result shows that the hydrogen and hydrocarbons can be analyzed in the range of 1amu unit. The resolution (M/{delta}M) of the Mass Spectrometry system is confirmed to be about 1000 from the separation of the 720 and 721amu peaks, which is attributed to the C-60 fullerene including {sup 13}C atoms. (H. Katsuta)

  9. Design and fabrication of a large rectangular magnetic cusp plasma source for high intensity neutral beam injectors

    International Nuclear Information System (INIS)

    Biagi, L.A.; Berkner, K.H.; Ehlers, K.W.; Paterson, J.A.; Porter, J.R.

    1979-11-01

    The design and fabrication techniques for a large, rectangular magnetic bucket plasma source are described. This source is compatible with the accelerator structures for the TFTR and DIII neutral-beam systems

  10. Plasma injection from the independent SHF-source in the open configuration 2. Magnetic fields of magnetic mirror configurations

    International Nuclear Information System (INIS)

    Beriya, Z.R.; Gogashvili, G.E.; Nanobashvili, S.I.

    1992-01-01

    The investigation was aimed at studying the characteristics and properties of plasma injected from independent stationary SHF source into an open magnetic trap of mirror geometry within a wide range of change in the experimental conditions. The investigations were primarily based on measurements of the distribution of charged particles in a plasma along the trap and on the dependence of the concentration on plasma production conditions in a SHF source. It is shown that the aggregate of the experimental data enables a conclusion that independent of SHF plasma can be succesfully used for filling on open magnetic trap of mirror configuration with plasma

  11. Proteomic Biomarker Discovery in 1000 Human Plasma Samples with Mass Spectrometry.

    Science.gov (United States)

    Cominetti, Ornella; Núñez Galindo, Antonio; Corthésy, John; Oller Moreno, Sergio; Irincheeva, Irina; Valsesia, Armand; Astrup, Arne; Saris, Wim H M; Hager, Jörg; Kussmann, Martin; Dayon, Loïc

    2016-02-05

    The overall impact of proteomics on clinical research and its translation has lagged behind expectations. One recognized caveat is the limited size (subject numbers) of (pre)clinical studies performed at the discovery stage, the findings of which fail to be replicated in larger verification/validation trials. Compromised study designs and insufficient statistical power are consequences of the to-date still limited capacity of mass spectrometry (MS)-based workflows to handle large numbers of samples in a realistic time frame, while delivering comprehensive proteome coverages. We developed a highly automated proteomic biomarker discovery workflow. Herein, we have applied this approach to analyze 1000 plasma samples from the multicentered human dietary intervention study "DiOGenes". Study design, sample randomization, tracking, and logistics were the foundations of our large-scale study. We checked the quality of the MS data and provided descriptive statistics. The data set was interrogated for proteins with most stable expression levels in that set of plasma samples. We evaluated standard clinical variables that typically impact forthcoming results and assessed body mass index-associated and gender-specific proteins at two time points. We demonstrate that analyzing a large number of human plasma samples for biomarker discovery with MS using isobaric tagging is feasible, providing robust and consistent biological results.

  12. Determination of fluspirilene in human plasma by liquid chromatography-tandem mass spectrometry with electrospray ionisation.

    Science.gov (United States)

    Swart, K J; Sutherland, F C; van Essen, G H; Hundt, H K; Hundt, A F

    1998-12-18

    An ultra-sensitive method for the determination of fluspirilene in plasma was established, using high-performance liquid chromatographic separation with tandem mass spectrometric detection. The samples were extracted with hexane/isoamyl alcohol, separated on a Phenomenex Luna C18 5 mu 150 x 2.1 mm column with a mobile phase consisting of methanol-water-acetic acid (600:400:1) at a flow-rate of 0.3 ml/min. Detection was achieved by a Finnigan Matt mass spectrometer (LCQ) at unit resolution in full scan mode scanning the product ion spectrum from m/z 130-500 and monitoring the transition of the protonated molecular ion at m/z 476.2, to the sum of the largest product ions m/z 371, 342 and 274 (MS-MS). Electrospray ionisation was used for ion production. The mean recovery for fluspirilene was 90% with a lower limit of quantification of 21.50 pg/ml using 1 ml plasma for extraction. This is the first chromatographic method described for the determination of fluspirilene in plasma that is accurate and sensitive enough to be used in pharmacokinetic studies.

  13. Multielement determination of rare earth elements in rock sample by liquid chromatography / inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Hamanaka, Tadashi; Itoh, Akihide; Itoh, Shinya; Sawatari, Hideyuki; Haraguchi, Hiroki.

    1995-01-01

    Rare earth elements in geological standard rock sample JG-1 (granodiolite)issued from the Geological Survey of Japan have been determined by a combined system of liquid chromatography and inductively coupled plasma mass spectrometry. (author)

  14. Spring meeting of the scientific associations for atomic physics, high speed physics, mass spectrometry, molecular physics, plasma physics

    International Nuclear Information System (INIS)

    1996-01-01

    The volume contains the abstracts of the contributions to the Spring Meeting in Rostock with aspects of atomic physics, molecular physics, high speed physics, plasma physics and mass spectrometry. (MM)

  15. Suppression of the e- coextracted from a Penning surface-plasma H-source

    International Nuclear Information System (INIS)

    Smith, V.H.; Allison, P.

    1992-01-01

    The ratio of electrons to negative ions extracted from Penning surface-plasma sources (SPS) such as the 8X source is low even before any steps are taken to suppress the electrons. For the 8X source the e - /H - ratio is typically four or five to one for H - operation and nine to one for D - operation. Because the coextracted e - present a power-loading problem to the 8X-source extraction system, methods to dissipate and/or reduce the power in the e - beam must be developed before extracting a dc H - or D - beam. Thus, we conducted this study to determine whether a collar installed in the near-extraction region of the 8X source suppresses the electrons extracted from that source. (Author) 8 refs., 6 figs

  16. High average power, highly brilliant laser-produced plasma source for soft X-ray spectroscopy.

    Science.gov (United States)

    Mantouvalou, Ioanna; Witte, Katharina; Grötzsch, Daniel; Neitzel, Michael; Günther, Sabrina; Baumann, Jonas; Jung, Robert; Stiel, Holger; Kanngiesser, Birgit; Sandner, Wolfgang

    2015-03-01

    In this work, a novel laser-produced plasma source is presented which delivers pulsed broadband soft X-radiation in the range between 100 and 1200 eV. The source was designed in view of long operating hours, high stability, and cost effectiveness. It relies on a rotating and translating metal target and achieves high stability through an on-line monitoring device using a four quadrant extreme ultraviolet diode in a pinhole camera arrangement. The source can be operated with three different laser pulse durations and various target materials and is equipped with two beamlines for simultaneous experiments. Characterization measurements are presented with special emphasis on the source position and emission stability of the source. As a first application, a near edge X-ray absorption fine structure measurement on a thin polyimide foil shows the potential of the source for soft X-ray spectroscopy.

  17. Experimental study of a RF plasma source with helicon configuration in the mix Ar/H_2. Application to the chemical etching of carbon materials surfaces in the framework of the plasma-wall interactions studies of ITER's divertor

    International Nuclear Information System (INIS)

    Bieber, T.

    2012-01-01

    The issue of the interaction wall-plasma is important in thermonuclear devices. The purpose of this work is to design a very low pressure atomic plasma source in order to study chemical etching of carbon surfaces in the same conditions as edge plasma in tokamaks. The experimental work has consisted in 2 stages: first, the characterisation of the new helicon configuration reactor developed for this research and secondly the atomic hydrogen source used for the chemical etching. The first chapter recalls what thermonuclear fusion is. The helicon configuration reactor as well as its diagnostics (optical emission spectroscopy, laser induced fluorescence - LIF, and Langmuir probe) are described in the second chapter. The third chapter deals with the different coupling modes (RF power and plasma) identified in pure argon plasmas and how they are obtained by setting experimental parameters such as injected RF power, magnetic fields or pressure. The fourth chapter is dedicated to the study of the difference in behavior between the electronic density and the relative density of metastable Ar"+ ions. The last chapter presents the results in terms of mass losses of the carbon material surfaces obtained with the atomic hydrogen source. (A.C.)

  18. Biological stimulation of the Human skin applying health promoting light and plasma sources

    Energy Technology Data Exchange (ETDEWEB)

    Awakowicz, P.; Bibinov, N. [Center for Plasma Science and Technology, Ruhr-University, Bochum (Germany); Born, M.; Niemann, U. [Philips Research, Aachen (Germany); Busse, B. [Zell-Kontakt GmbH, Noerten-Hardenberg (Germany); Gesche, R.; Kuehn, S.; Porteanu, H.E. [Ferdinand-Braun-Institut fuer Hoechstfrequenztechnik, Berlin (Germany); Helmke, A. [University of Applied Sciences and Arts, Goettingen (Germany); Kaemling, A.; Wandke, D. [CINOGY GmbH, Duderstadt (Germany); Kolb-Bachofen, V.; Liebmann, J. [Institute for Immunobiology, Heinrich-Heine University, Duesseldorf (Germany); Kovacs, R.; Mertens, N.; Scherer, J. [Aurion Anlagentechnik GmbH, Seligenstadt (Germany); Oplaender, C.; Suschek, C. [Clinic for Plastic Surgery, University Clinic, Aachen (Germany); Vioel, W. [Laser-Laboratorium, Goettingen (Germany); University of Applied Sciences and Arts, Goettingen (Germany)

    2009-10-15

    In the frame of BMBF project ''BioLiP'', new physical treatment techniques aiming at medical treatment of the human skin have been developed. The acronym BioLiP stands for ''Desinfektion, Entkeimung und biologische Stimulation der Haut durch gesundheitsfoerdernde Licht- und Plasmaquellen'' (Disinfection, germ reduction and biological stimulation of the human skin by health promoting light and plasma sources). A source applying a low-temperature dielectric barrier discharge plasma (DBD) has been investigated on its effectiveness for skin disinfection and stimulation of biological material. Alternatively an atmospheric plasma source consisting of a microwave resonator combined with a solid state power oscillator has been examined. This concept which allows for a compact and efficient design avoiding external microwave power supply and matching units has been optimized with respect to nitrogen monoxide (NO) production in high yields. In both cases various application possibilities in the medical and biological domain are opened up. Light sources in the visible spectral range have been investigated with respect to the proliferation of human cell types. Intensive highly selective blue light sources based on LED technology can slow down proliferation rates without inducing toxic effects which offers new opportunities for treatments of so-called hyperproliferative skin conditions (e.g. with psoriasis or in wound healing) using UV-free light. (copyright 2009 WILEY-VCH Verlag GmbH and Co. KGaA, Weinheim) (orig.)

  19. Broadband frequency ECR ion source concepts with large resonant plasma volumes

    International Nuclear Information System (INIS)

    Alton, G.D.

    1995-01-01

    New techniques are proposed for enhancing the performances of ECR ion sources. The techniques are based on the use of high-power, variable-frequency, multiple-discrete-frequency, or broadband microwave radiation, derived from standard TWT technology, to effect large resonant ''volume'' ECR sources. The creation of a large ECR plasma ''volume'' permits coupling of more power into the plasma, resulting in the heating of a much larger electron population to higher energies, the effect of which is to produce higher charge state distributions and much higher intensities within a particular charge state than possible in present forms of the ECR ion source. If successful, these developments could significantly impact future accelerator designs and accelerator-based, heavy-ion-research programs by providing multiply-charged ion beams with the energies and intensities required for nuclear physics research from existing ECR ion sources. The methods described in this article can be used to retrofit any ECR ion source predicated on B-minimum plasma confinement techniques

  20. Study of RF-excited Diethylene Glycol Dimethyl Ether Plasmas by Mass Spectrometry

    International Nuclear Information System (INIS)

    Algatti, M A; Mota, R P; Júnior, P W P Moreira; Honda, R Y; Kayama, M E; Kostov, K G

    2012-01-01

    This paper deals with the study of the fragmentation process of diethylene glycol dimethyl ether (CH 3 O(CH 2 CH 2 O) 2 CH 3 ) (diglyme here in) molecule in low pressure RF excited plasma discharges. The study was carried out using mass spectrometry. The results showed that for a fixed pressure, the increase of the RF power coupled to the plasma chamber from 1 to 35 W produced a plasma environment much more reactive which increases the population of the ionized species like CH 2 + (15 amu), C 2 H 4 + (28 amu), CH 3 O + (31 amu), C 2 H 4 O + (44 amu), CH 3 OCH 2 CH 2 + (59 amu) and CH 3 OCH 2 CH 2 O + (75 amu). This fact may be attributed to the increase of the electronic temperature that makes predominant the occurrence of inelastic processes that promotes molecular fragmentation. For a fixed value of RF power the increase of pressure from 50 mTorr to 100 mTorr produces the decreasing of the above mentioned chemical species due the lower electronic mean free path. These results suggest that if one wants to keep the monomer's functionality within the plasma deposited films resulting from such kind of discharges one must operate in low power conditions.

  1. Quantification of plasma myo-inositol using gas chromatography-mass spectrometry.

    Science.gov (United States)

    Guo, Jin; Shi, Yingfei; Xu, Chengbao; Zhong, Rugang; Zhang, Feng; Zhang, Ting; Niu, Bo; Wang, Jianhua

    2016-09-01

    Myo-inositol (MI) deficiency is associated with an increased risk for neural tube defects (NTDs), mental disorders and metabolic diseases. We developed a gas chromatography-mass spectrometry (GC-MS) method to detect MI in human plasma, which was accurate, relatively efficient and convenient for clinical application. An external standard method was used for determination of plasma MI. Samples were analyzed by GC-MS after derivatization. The stable-isotope labeled internal standard approach was used to validate the method's accuracy. Alpha fetal protein (AFP) was detected by chemiluminescence immunoassay. The method was validated by determining the linearity, sensitivity and recovery rate. There was a good agreement between the internal standard approach and the present method. The NTD-affected pregnancies showed lower plasma MI (P=0.024) and higher AFP levels (P=0.001) than control. Maternal MI level showed a better discrimination in spina bifida subgroup, while AFP level showed a better discrimination in anencephaly subgroup after stratification analysis. We developed a sensitive and reliable method for the detection of clinical plasma MI, which might be a marker for NTDs screening, and established fundamental knowledge for clinical diagnosis and prevention for the diseases related to disturbed MI metabolism. Copyright © 2016 Elsevier B.V. All rights reserved.

  2. Plasma studies of the permanent magnet electron cyclotron resonance ion source at Peking University.

    Science.gov (United States)

    Ren, H T; Peng, S X; Xu, Y; Zhao, J; Lu, P N; Chen, J; Zhang, A L; Zhang, T; Guo, Z Y; Chen, J E

    2014-02-01

    At Peking University (PKU) we have developed several 2.45 GHz Permanent Magnet Electron Cyclotron Resonance ion sources for PKUNIFTY, SFRFQ, Coupled RFQ&SFRFQ, and Dielectric-Wall Accelerator (DWA) projects (respectively, 50 mA of D(+), 10 mA of O(+), 10 mA of He(+), and 50 mA of H(+)). In order to improve performance of these ion sources, it is necessary to better understand the principal factors that influence the plasma density and the atomic ion fraction. Theoretical analysis about microwave transmission and cut-off inside the discharge chamber were carried out to study the influence of the discharge chamber diameters. As a consequence, experimental studies on plasma density and ion fraction with different discharge chamber sizes have been carried out. Due to the difficulties in measuring plasma density inside the discharge chamber, the output beam current was measured to reflect the plasma density. Experimental results show that the plasma density increases to the maximum and then decreases significantly as the diameter changed from 64 mm to 30 mm, and the atomic ion fraction has the same tendency. The maximum beam intensity was obtained with the diameter of 35 mm, but the maximum atomic ion fraction with a diameter of 40 mm. The experimental results are basically accordant with the theoretical calculation. Details are presented in this paper.

  3. Plasma studies of the permanent magnet electron cyclotron resonance ion source at Peking University

    Energy Technology Data Exchange (ETDEWEB)

    Ren, H. T.; Peng, S. X., E-mail: sxpeng@pku.edu.cn; Xu, Y.; Zhao, J.; Lu, P. N.; Chen, J.; Zhang, A. L.; Zhang, T.; Guo, Z. Y.; Chen, J. E. [State Key Laboratory of Nuclear Physics and Technology, Institute of Heavy Ion Physics, Peking University, Beijing 100871 (China)

    2014-02-15

    At Peking University (PKU) we have developed several 2.45 GHz Permanent Magnet Electron Cyclotron Resonance ion sources for PKUNIFTY, SFRFQ, Coupled RFQ and SFRFQ, and Dielectric-Wall Accelerator (DWA) projects (respectively, 50 mA of D{sup +}, 10 mA of O{sup +}, 10 mA of He{sup +}, and 50 mA of H{sup +}). In order to improve performance of these ion sources, it is necessary to better understand the principal factors that influence the plasma density and the atomic ion fraction. Theoretical analysis about microwave transmission and cut-off inside the discharge chamber were carried out to study the influence of the discharge chamber diameters. As a consequence, experimental studies on plasma density and ion fraction with different discharge chamber sizes have been carried out. Due to the difficulties in measuring plasma density inside the discharge chamber, the output beam current was measured to reflect the plasma density. Experimental results show that the plasma density increases to the maximum and then decreases significantly as the diameter changed from 64 mm to 30 mm, and the atomic ion fraction has the same tendency. The maximum beam intensity was obtained with the diameter of 35 mm, but the maximum atomic ion fraction with a diameter of 40 mm. The experimental results are basically accordant with the theoretical calculation. Details are presented in this paper.

  4. The diagnostic neutral beam injector with arc-discharge plasma source on the TCV Tokamak

    Energy Technology Data Exchange (ETDEWEB)

    Karpushov, Alexander N. [Ecole Polytechnique Federale de Lausanne (EPFL), Centre de Recherches en Physique des Plasmas, Association Euratom-Confederation Suisse, CH-1015 Lausanne (Switzerland)], E-mail: alexander.karpushov@epfl.ch; Andrebe, Yanis; Duval, Basil P.; Bortolon, Alessandro [Ecole Polytechnique Federale de Lausanne (EPFL), Centre de Recherches en Physique des Plasmas, Association Euratom-Confederation Suisse, CH-1015 Lausanne (Switzerland)

    2009-06-15

    The diagnostic neutral beam injector (DNBI) together with a charge exchange recombination spectroscopy (CXRS) system has been used on the TCV Tokamak as a diagnostic tool for local measurements of plasma ion temperature, velocity and carbon impurity density based on analysis of the beam induced impurity radiation emission since 2000. To improve the performance of the CXRS diagnostic, several upgrades of both the optical system and the neutral beam were performed. An increase of the plasma source size together with beam optimization in 2003 resulted in a twofold increase the beam current. The RF plasma generator was replaced by an arc-discharge plasma source together with a new ion optical system (IOS) in 2006 and subsequent beam optimization is presented herein. This was designed to increase the line brightness of the beam in the CXRS observation region without increasing of the injected power (to avoid plasma perturbation by the beam). The beam characteristics are measured by a multi-chord scanning of Doppler-shifted H{sub {alpha}} emission, thermal measurements on a movable calorimeter and visible optical measurements inside the Tokamak vessel.

  5. Yosemite conference on ionospheric plasma in the magnetosphere: sources, mechanisms and consequences, meeting report

    International Nuclear Information System (INIS)

    Gallagher, D.L.; Burch, J.L.; Klumpar, D.M.; Moore, T.E.; Waite, J.H. Jr.

    1987-02-01

    The sixth biennial Yosemite topical conference and the first as a Chapman Conference was held on February 3 to 6, 1986. Although the solar wind was once thought to dominate the supply of plasma in the Earth's magnetosphere, it is now thought that the Earth's ionosphere is a significant contributor. Polar wind and other large volume outflows of plasma have been seen at relatively high altitudes over the polar cap and are now being correlated with outflows found in the magnetotail. The auroral ion fountain and cleft ion fountain are examples of ionospheric sources of plasma in the magnetosphere, observed by the Dynamics Explorer 1 (DE 1) spacecraft. The conference was organized into six sessions: four consisting of prepared oral presentations, one poster session, and one session for open forum discussion. The first three oral sessions dealt separately with the three major topics of the conference, i.e., the sources, mechanisms, and consequences of ionospheric plasma in the magnetosphere. A special session of invited oral presentations was held to discuss extraterrestrial ionospheric/magnetospheric plasma processes. The poster session was extended over two evenings during which presenters discussed their papers on a one-on-one basis. The last session of the conferences was reserved for open discussions of those topics or ideas considered most interesting or controversial

  6. Reference masses for precision mass spectrometry design and implementation of a Pierce geometry to the cluster Ion source at ISOLTRAP

    CERN Document Server

    Lommen, Jonathan

    At the mass spectrometer ISOLTRAP carbon clusters ($^{12}$Cn, 1$\\leqslant$n$\\leqslant$25) are provided as reference masses, which are of particular importance in higher mass ranges (m $\\geqslant$ 200u). In this mass range the measurlment uncertainty is increasingly dominated by the difference of the reference mass and the mass of the ion of interest. Using carbon clusters instead of the common $^{133}$Cs ions, this difference decreases. The carbon clusters are produced in a laser ion source which has been improved in the frame of this thesis. The fluctuations of the count rate have been investigated as a function of the laser energy. Furthermore, the energy density at the target has been increased by implementation of a telescope into the laser beam line, which leads to a more narrow energy distribution of the ions. Through the exact adjustment of timing and length of a pulsed cavity an energy range with constant count rate could be selected. In order to provide ideal starting conditions during and after the ...

  7. Laser-produced plasma-extreme ultraviolet light source for next generation lithography

    International Nuclear Information System (INIS)

    Nishihara, Katsunobu; Nishimura, Hiroaki; Gamada, Kouhei; Murakami, Masakatsu; Mochizuki, Takayasu; Sasaki, Akira; Sunahara, Atsushi

    2005-01-01

    Extreme ultraviolet (EUV) lithography is the most promising candidate for the next generation lithography for the 45 nm technology node and below. EUV light sources under consideration use 13.5 nm radiations from multicharged xenon, tin and lithium ions, because Mo/Si multiplayer mirrors have high reflectivity at this wavelength. A review of laser-produced plasma (LPP) EUV light sources is presented with a focus on theoretical and experimental studies under the auspices of the Leading Project promoted by MEXT. We discuss three theoretical topics: atomic processes in the LPP-EUV light source, conversion efficiency from laser light to EUV light at 13.5 nm wave-length with 2% bound width, and fast ion spectra. The properties of EUV emission from tin and xenon plasmas are also shown based on experimental results. (author)

  8. Ultra-Sensitive Elemental Analysis Using Plasmas 4.Application of Inductively Coupled Plasma Mass Spectrometry to the Study of Environmental Radioactivity

    Science.gov (United States)

    Yoshida, Satoshi

    Applications of inductively coupled plasma mass spectrometry (ICP-MS) to the determination of long-lived radionuclides in environmental samples were summarized. In order to predict the long-term behavior of the radionuclides, related stable elements were also determined. Compared with radioactivity measurements, the ICP-MS method has advantages in terms of its simple analytical procedures, prompt measurement time, and capability of determining the isotope ratio such as240Pu/239Pu, which can not be separated by radiation. Concentration of U and Th in Japanese surface soils were determined in order to determine the background level of the natural radionuclides. The 235U/238U ratio was successfully used to detect the release of enriched U from reconversion facilities to the environment and to understand the source term. The 240Pu/239Pu ratios in environmental samples varied widely depending on the Pu sources. Applications of ICP-MS to the measurement of I and Tc isotopes were also described. The ratio between radiocesium and stable Cs is useful for judging the equilibrium of deposited radiocesium in a forest ecosystem.

  9. Comparison of different source calculations in two-nucleon channel at large quark mass

    Science.gov (United States)

    Yamazaki, Takeshi; Ishikawa, Ken-ichi; Kuramashi, Yoshinobu

    2018-03-01

    We investigate a systematic error coming from higher excited state contributions in the energy shift of light nucleus in the two-nucleon channel by comparing two different source calculations with the exponential and wall sources. Since it is hard to obtain a clear signal of the wall source correlation function in a plateau region, we employ a large quark mass as the pion mass is 0.8 GeV in quenched QCD. We discuss the systematic error in the spin-triplet channel of the two-nucleon system, and the volume dependence of the energy shift.

  10. Chemical mass balance source apportionment of fine and PM10 in the Desert Southwest, USA

    Directory of Open Access Journals (Sweden)

    Andrea L. Clements

    2016-03-01

    Full Text Available The Desert Southwest Coarse Particulate Matter Study was undertaken in Pinal County, Arizona, to better understand the origin and impact of sources of fine and coarse particulate matter (PM in rural, arid regions of the U.S. southwestern desert. The desert southwest experiences some of the highest PM10 mass concentrations in the country. To augment previously reported results, 6-week aggregated organic speciation data that included ambient concentrations of n-alkanes, polycyclic aromatic hydrocarbons, organic acids, and saccharides were used in chemical mass balance modeling (CMB. A set of re-suspended soil samples were analyzed for specific marker species to provide locally-appropriate source profiles for the CMB analysis. These profiles, as well as previously collected plant and fungal spore profiles from the region, were combined with published source profiles for other relevant sources and used in the CMB analysis. The six new region-specific source profiles included both organic and inorganic species for four crustal material sources, one plant detritus source, and one fungal spore source.Results indicate that up to half of the ambient PM2.5 was apportioned to motor vehicles with the highest regional contribution observed in the small urban center of Casa Grande. Daily levels of apportioned crustal material accounted for up to 50% of PM2.5 mass with the highest contributions observed at the sites closest to active agricultural areas. Apportioned secondary PM, biomass burning, and road dust typically contributed less than 35% as a group to the apportioned PM2.5 mass. Crustal material was the primary source apportioned to PM10 and accounted for between 50–90% of the apportioned mass. Of the other sources apportioned to PM10, motor vehicles and road dust were the largest contributors at the urban and one of the rural sites, whereas road dust and meat cooking operations were the largest contributors at the other rural site.

  11. Plasma focus sources: Supplement to the neutron resonance radiography workshop proceedings

    International Nuclear Information System (INIS)

    Nardi, V.; Brzosko, J.

    1989-01-01

    Since their discovery, plasma focus discharges have been recognized as very intense pulsed sources of deuterium-deuterium (D-D) or deuterium-tritium (D-T) fusion-reaction neutrons, with outstanding capabilities. Specifically, the total neutron emission/shot, YN, and the rate of neutron emission, Y/sub n/, of an optimized plasma focus (PF) are higher than the corresponding quantities observed in any other type of pinched discharge at the same level of powering energy W 0 . Recent developments have led to the concept and experimental demonstration of an Advanced Plasma Focus System (APF) that consists of a Mather-geometry plasma focus in which field distortion elements (FDEs) are inserted in the inter-electrode gap for increasing the neutron yield/shot, Y/sub n/. The FDE-induced redistribution of the plasma current increases Y/sub n/ by a factor ≅5-10 above the value obtained without FDEs under otherwise identical conditions of operation of the plasma focus. For example, an APF that is fed by a fast capacitor bank with an energy, W 0 = 6kJ, and voltage, V 0 = 16.5 kV provides Y/sub n/ /congruent/ 4 /times/ 10 9 D-D neutrons/shot (pure D 2 filling) and Y/sub n/ = 4 /times/ 10 11 D-T neutrons/shot (filling is 50% deuterium and 50% tritium). The FDE-induced increase of Y/sub n/ for fixed values of (W 0 , V 0 ), the observed scaling law Y/sub n/ /proportional to/ W 0 2 for optimized plasma focus systems, and our experience with neutron scattering in bulk objects lead us to the conclusion that we can use an APF as a source of high-intensity neutron pulses (10 14 n/pulse) in the field off neutron radiography (surface and bulk) with a nanosecond or millisecond time resolution

  12. Development and studies on a compact electron cyclotron resonance plasma source

    Science.gov (United States)

    Ganguli, A.; Tarey, R. D.; Arora, N.; Narayanan, R.

    2016-04-01

    It is well known that electron cyclotron resonance (ECR) produced plasmas are efficient, high-density plasma sources and have many industrial applications. The concept of a portable compact ECR plasma source (CEPS) would thus become important from an application point of view. This paper gives details of such a CEPS that is both portable and easily mountable on a chamber of any size. It uses a fully integrated microwave line operating at 2.45 GHz, up to 800 W, cw. The required magnetic field is produced by a set of suitably designed NdFeB ring magnets; the device has an overall length of  ≈60 cm and weighs  ≈14 kg including the permanent magnets. The CEPS was attached to a small experimental chamber to judge its efficacy for plasma production. In the pressure range of 0.5-10 mTorr and microwave power of  ≈400-500 W the experiments indicate that the CEPS is capable of producing high-density plasma (≈9  ×  1011-1012 cm-3) with bulk electron temperature in the range  ≈2-3 eV. In addition, a warm electron population with density and temperature in the range ≈7  ×  108-109 cm-3 and  ≈45-80 eV, respectively has been detected. This warm population plays an important role at high pressures in maintaining the high-density plasma, when plasma flow from the CEPS into the test chamber is strongly affected.

  13. Generation of plasma X-ray sources via high repetition rate femtosecond laser pulses

    Science.gov (United States)

    Baguckis, Artūras; Plukis, Artūras; Reklaitis, Jonas; Remeikis, Vidmantas; Giniūnas, Linas; Vengris, Mikas

    2017-12-01

    In this study, we present the development and characterization of Cu plasma X-ray source driven by 20 W average power high repetition rate femtosecond laser in ambient atmosphere environment. The peak Cu- Kα photon flux of 2.3 × 109 photons/s into full solid angle is demonstrated (with a process conversion efficiency of 10-7), using pulses with peak intensity of 4.65 × 1014 W/cm2. Such Cu- Kα flux is significantly larger than others found in comparable experiments, performed in air environment. The effects of resonance plasma absorption process, when optimized, are shown to increase measured flux by the factor of 2-3. The relationship between X-ray photon flux and plasma-driving pulse repetition rate is quasi-linear, suggesting that fluxes could further be increased to 1010 photons/s using even higher average powers of driving radiation. These results suggest that to fully utilize the potential of high repetition rate laser sources, novel target material delivery systems (for example, jet-based ones) are required. On the other hand, this study demonstrates that high energy lasers currently used for plasma X-ray sources can be conveniently and efficiently replaced by high average power and repetition rate laser radiation, as a way to increase the brightness of the generated X-rays.

  14. Color Developing Capacity of Plasma-treated Water as a Source of Nitrite for Meat Curing.

    Science.gov (United States)

    Jung, Samooel; Kim, Hyun Joo; Park, Sanghoo; Yong, Hae In; Choe, Jun Ho; Jeon, Hee-Joon; Choe, Wonho; Jo, Cheorun

    2015-01-01

    The interaction of plasma with liquid generates nitrogen species including nitrite (NO(-) 2). Therefore, the color developing capacity of plasma-treated water (PTW) as a nitrite source for meat curing was investigated in this study. PTW, which is generated by surface dielectric barrier discharge in air, and the increase of plasma treatment time resulted in increase of nitrite concentration in PTW. The PTW used in this study contains 46 ppm nitrite after plasma treatment for 30 min. To evaluate the effect of PTW on the cured meat color, meat batters were prepared under three different conditions (control, non-cured meat batter; PTW, meat batter cured with PTW; Sodium nitrite, meat batter cured with sodium nitrite). The meat batters were vacuum-packaged and cooked in a water-bath at 80℃ for 30 min. The typical color of cured meat developed in cooked meat batter treated with sodium nitrite or PTW. The lightness (L*) and yellowness (b*) values were similar in all conditions, whereas, the redness (a*) values of cooked meat batter with PTW and sodium nitrite (pnitrite source in the curing process of meat without addition of other nitrite sources.

  15. L-shell spectroscopic diagnostics of radiation from krypton HED plasma sources

    Energy Technology Data Exchange (ETDEWEB)

    Petkov, E. E., E-mail: emilp@unr.edu; Safronova, A. S.; Kantsyrev, V. L.; Shlyaptseva, V. V. [University of Nevada, Reno, Nevada 89557 (United States); Rawat, R. S.; Tan, K. S. [National Institute of Education, Nanyang Technological University, Singapore 637616 (Singapore); Beiersdorfer, P.; Brown, G. V. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Hell, N. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Dr. Remeis-Sternwarte and ECAP, Universität Erlangen-Nürnberg, 96049 Bamberg (Germany)

    2016-11-15

    X-ray spectroscopy is a useful tool for diagnosing plasma sources due to its non-invasive nature. One such source is the dense plasma focus (DPF). Recent interest has developed to demonstrate its potential application as a soft x-ray source. We present the first spectroscopic studies of krypton high energy density plasmas produced on a 3 kJ DPF device in Singapore. In order to diagnose spectral features, and to obtain a more comprehensive understanding of plasma parameters, a new non-local thermodynamic equilibrium L-shell kinetic model for krypton was developed. It has the capability of incorporating hot electrons, with different electron distribution functions, in order to examine the effects that they have on emission spectra. To further substantiate the validity of this model, it is also benchmarked with data gathered from experiments on the electron beam ion trap (EBIT) at Lawrence Livermore National Laboratory, where data were collected using the high resolution EBIT calorimeter spectrometer.

  16. L-shell spectroscopic diagnostics of radiation from krypton HED plasma sources.

    Science.gov (United States)

    Petkov, E E; Safronova, A S; Kantsyrev, V L; Shlyaptseva, V V; Rawat, R S; Tan, K S; Beiersdorfer, P; Hell, N; Brown, G V

    2016-11-01

    X-ray spectroscopy is a useful tool for diagnosing plasma sources due to its non-invasive nature. One such source is the dense plasma focus (DPF). Recent interest has developed to demonstrate its potential application as a soft x-ray source. We present the first spectroscopic studies of krypton high energy density plasmas produced on a 3 kJ DPF device in Singapore. In order to diagnose spectral features, and to obtain a more comprehensive understanding of plasma parameters, a new non-local thermodynamic equilibrium L-shell kinetic model for krypton was developed. It has the capability of incorporating hot electrons, with different electron distribution functions, in order to examine the effects that they have on emission spectra. To further substantiate the validity of this model, it is also benchmarked with data gathered from experiments on the electron beam ion trap (EBIT) at Lawrence Livermore National Laboratory, where data were collected using the high resolution EBIT calorimeter spectrometer.

  17. Liquid sampling-atmospheric pressure glow discharge as a secondary excitation source: Assessment of plasma characteristics

    Science.gov (United States)

    Manard, Benjamin T.; Gonzalez, Jhanis J.; Sarkar, Arnab; Dong, Meirong; Chirinos, Jose; Mao, Xianglei; Russo, Richard E.; Marcus, R. Kenneth

    The liquid sampling-atmospheric pressure glow discharge (LS-APGD) has been assessed as a secondary excitation source with a parametric evaluation regarding carrier gas flow rate, applied current, and electrode distance. With this parametric evaluation, plasma optical emission was monitored in order to obtain a fundamental understanding with regards to rotational temperature (Trot), excitation temperature (Texc), electron number density (ne), and plasma robustness. Incentive for these studies is not only for a greater overall fundamental knowledge of the APGD, but also in instrumenting a secondary excitation/ionization source following laser ablation (LA). Rotational temperatures were determined through experimentally fitting of the N2 and OH molecular emission bands while atomic excitation temperatures were calculated using a Boltzmann distribution of He and Mg atomic lines. The rotational and excitation temperatures were determined to be ~ 1000 K and ~ 2700 K respectively. Electron number density was calculated to be on the order of ~ 3 × 1015 cm- 3 utilizing Stark broadening effects of the Hα line of the Balmer series and a He I transition. In addition, those diagnostics were performed introducing magnesium (by solution feed and laser ablation) into the plasma in order to determine any perturbation under heavy matrix sampling. The so-called plasma robustness factor, derived by monitoring Mg II/Mg I emission ratios, is also employed as a reflection of potential perturbations in microplasma energetics across the various operation conditions and sample loadings. While truly a miniaturized source (laser ablation sample introduction.

  18. Positron Source from Betatron X-rays Emitted in a Plasma Wiggler

    Energy Technology Data Exchange (ETDEWEB)

    Johnson, D.K.; Clayton, C.E.; Huang, C.; Joshi, C.; Lu, W.; Marsh, K.A.; Mori, W.B.; Zhou, M.; /UCLA; Barnes, C.D.; Decker, F.J.; Hogan, M.J.; Iverson, R.H.; Krejcik, P.; O' Connell, C.L.; Siemann, R.; Walz, D.R.; /SLAC; Deng, S.; Katsouleas, T.C.; Muggli, P.; Oz, E.; /Southern California U.

    2006-04-21

    In the E-167 plasma wakefield accelerator (PWFA) experiments in the Final Focus Test Beam (FFTB) at the Stanford Linear Accelerator Center (SLAC), an ultra-short, 28.5 GeV electron beam field ionizes a neutral column of Lithium vapor. In the underdense regime, all plasma electrons are expelled creating an ion column. The beam electrons undergo multiple betatron oscillations leading to a large flux of broadband synchrotron radiation. With a plasma density of 3 x 10{sup 17}cm{sup -3}, the effective focusing gradient is near 9 MT/m with critical photon energies exceeding 50 MeV for on-axis radiation. A positron source is the initial application being explored for these X-rays, as photo-production of positrons eliminates many of the thermal stress and shock wave issues associated with traditional Bremsstrahlung sources. Photo-production of positrons has been well-studied; however, the brightness of plasma X-ray sources provides certain advantages. In this paper, we present results of the simulated radiation spectra for the E-167 experiments, and compute the expected positron yield.

  19. Impedance of an intense plasma-cathode electron source for tokamak startup

    Science.gov (United States)

    Hinson, E. T.; Barr, J. L.; Bongard, M. W.; Burke, M. G.; Fonck, R. J.; Perry, J. M.

    2016-05-01

    An impedance model is formulated and tested for the ˜1 kV , 1 kA/cm2 , arc-plasma cathode electron source used for local helicity injection tokamak startup. A double layer sheath is established between the high-density arc plasma ( narc≈1021 m-3 ) within the electron source, and the less dense external tokamak edge plasma ( nedge≈1018 m-3 ) into which current is injected at the applied injector voltage, Vinj . Experiments on the Pegasus spherical tokamak show that the injected current, Iinj , increases with Vinj according to the standard double layer scaling Iinj˜Vinj3 /2 at low current and transitions to Iinj˜Vinj1 /2 at high currents. In this high current regime, sheath expansion and/or space charge neutralization impose limits on the beam density nb˜Iinj/Vinj1 /2 . For low tokamak edge density nedge and high Iinj , the inferred beam density nb is consistent with the requirement nb≤nedge imposed by space-charge neutralization of the beam in the tokamak edge plasma. At sufficient edge density, nb˜narc is observed, consistent with a limit to nb imposed by expansion of the double layer sheath. These results suggest that narc is a viable control actuator for the source impedance.

  20. Inductive plasma source for the ion treatment of AISI-304 SS

    International Nuclear Information System (INIS)

    Piedad-Beneitez, A de la; Lopez-Callejas, R; Granda-Gutierrez, E E; Rodriguez-Mendez, B G; Perez-Martinez, J A; Flores-Fuentes, A A; Valencia-Alvarado, R; Barocio, S R; Mercado-Cabrera, A; Pena-Eguiluz, R; Munoz-Castro, A E

    2008-01-01

    The design and construction of a simple inductive plasma source is described as constituted by an evacuated Pyrex glass cylinder reactor with 190 mm inner diameter and 500 mm length. This discharge vessel is coaxially surrounded by a cylindrically wound antenna, 240 mm in diameter, made of 3.2 mm wide copper wire. The antenna is supplied by a 13.56 MHz RF generator whose resulting electric field is able to create the plasma. When nitrogen is admitted to the vessel, the plasma generation takes place within the 0.1-50 Pa work pressure and 300-600 W RF power. The plasma density has been established by double Langmuir probes between 3.2 x 10 15 and 2.4 x 10 18 m -3 . This inductive plasma set up is meant to modify the surface of AISI-304 stainless steel by means of ion deposition, thanks to the sample bias provided by an external - 400 V dc supply, in order to improve the steel hardness without compromising its corrosion resistance. Once accelerated by the negative bias, the plasma ions impinge on the sample nitriding it by diffusion. The treated samples were characterized by x-ray diffraction (XRD) indicating the formation of the expanded gamma phase, by scanning electron microscopy (SEM) providing the atomic percentages of nitrogen, and by microhardness (HV) measurement.