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Sample records for penning-trap mass measurements

  1. Extending Penning trap mass measurements with SHIPTRAP to the heaviest elements

    International Nuclear Information System (INIS)

    Block, M.; Ackermann, D.; Herfurth, F.; Hofmann, S.; Blaum, K.; Droese, C.; Marx, G.; Schweikhard, L.; Düllmann, Ch. E.; Eibach, M.; Eliseev, S.; Haettner, E.; Plaß, W. R.; Scheidenberger, C.; Heßberger, F. P.; Ramirez, E. Minaya; Nesterenko, D.

    2013-01-01

    Penning-trap mass spectrometry of radionuclides provides accurate mass values and absolute binding energies. Such mass measurements are sensitive indicators of the nuclear structure evolution far away from stability. Recently, direct mass measurements have been extended to the heavy elements nobelium (Z=102) and lawrencium (Z=103) with the Penning-trap mass spectrometer SHIPTRAP. The results probe nuclear shell effects at N=152. New developments will pave the way to access even heavier nuclides.

  2. Precise mass measurements of exotic nuclei--the SHIPTRAP Penning trap mass spectrometer

    International Nuclear Information System (INIS)

    Herfurth, F.; Ackermann, D.; Block, M.; Dworschak, M.; Eliseev, S.; Hessberger, F.; Hofmann, S.; Kluge, H.-J.; Maero, G.; Martin, A.; Mazzocco, M.; Rauth, C.; Vorobjev, G.; Blaum, K.; Ferrer, R.; Neidherr, D.; Chaudhuri, A.; Marx, G.; Schweikhard, L.; Neumayr, J.

    2007-01-01

    The SHIPTRAP Penning trap mass spectrometer has been designed and constructed to measure the mass of short-lived, radioactive nuclei. The radioactive nuclei are produced in fusion-evaporation reactions and separated in flight with the velocity filter SHIP at GSI in Darmstadt. They are captured in a gas cell and transfered to a double Penning trap mass spectrometer. There, the cyclotron frequencies of the radioactive ions are determined and yield mass values with uncertainties ≥4.5·10 -8 . More than 50 nuclei have been investigated so far with the present overall efficiency of about 0.5 to 2%

  3. Penning trap mass measurements on nobelium isotopes

    International Nuclear Information System (INIS)

    Dworschak, M.; Block, M.; Ackermann, D.; Herfurth, F.; Hessberger, F. P.; Hofmann, S.; Vorobyev, G. K.; Audi, G.; Blaum, K.; Droese, C.; Marx, G.; Schweikhard, L.; Eliseev, S.; Ketter, J.; Fleckenstein, T.; Haettner, E.; Plass, W. R.; Scheidenberger, C.; Ketelaer, J.; Kluge, H.-J.

    2010-01-01

    The Penning trap mass spectrometer SHIPTRAP at GSI Darmstadt allows accurate mass measurements of radionuclides, produced in fusion-evaporation reactions and separated by the velocity filter SHIP from the primary beam. Recently, the masses of the three nobelium isotopes 252-254 No were determined. These are the first direct mass measurements of transuranium elements, which provide new anchor points in this region. The heavy nuclides were produced in cold-fusion reactions by irradiating a PbS target with a 48 Ca beam, resulting in production rates of the nuclei of interest of about one atom per second. In combination with data from decay spectroscopy our results are used to perform a new atomic-mass evaluation in this region.

  4. PENTATRAP. A novel Penning-trap system for high-precision mass measurements

    Energy Technology Data Exchange (ETDEWEB)

    Doerr, Andreas

    2015-01-21

    The novel Penning-trap mass spectrometer PENTATRAP aims at mass-ratio determinations of medium-heavy to heavy ions with relative uncertainties below 10{sup -11}. From the mass ratios of certain ion species, the corresponding mass differences will be determined with sub-eV/c{sup 2} uncertainties. These mass differences are relevant for neutrino-mass experiments, a test of special relativity and tests of bound-state QED. Means to obtain the required precision are very stable trapping fields, the use of highly-charged ions produced by EBITs, a non-destructive cyclotron-frequency determination scheme employing detectors with single-ion sensitivity and a five-trap tower, that allows for measurement schemes being insensitive to magnetic field drifts. Within this thesis, part of the detection electronics was set up and tested under experimental conditions. A single-trap setup was realized. A Faraday cup in the trap tower enabled the proper adjustment of the settings of the beamline connecting the EBIT and the Penning-trap system, resulting in the first trapping of ions at PENTATRAP. A stabilization of switched voltages in the beamline and detailed studies of ion bunch characteristics allowed for reproducible loading of only a few ions. Detection of the axial oscillation of the trapped ions gave hints that in some cases, even single ions had been trapped. Furthermore, valuable conclusions about necessary modifications of the setup could be drawn.

  5. The construction of TRIGA-TRAP and direct high-precision Penning trap mass measurements on rare-earth elements and americium

    Energy Technology Data Exchange (ETDEWEB)

    Ketelaer, Jens

    2010-06-14

    The construction of TRIGA-TRAP and direct high-precision Penning trap mass measurements on rare-earth elements and americium: Nuclear masses are an important quantity to study nuclear structure since they reflect the sum of all nucleonic interactions. Many experimental possibilities exist to precisely measure masses, out of which the Penning trap is the tool to reach the highest precision. Moreover, absolute mass measurements can be performed using carbon, the atomic-mass standard, as a reference. The new double-Penning trap mass spectrometer TRIGA-TRAP has been installed and commissioned within this thesis work, which is the very first experimental setup of this kind located at a nuclear reactor. New technical developments have been carried out such as a reliable non-resonant laser ablation ion source for the production of carbon cluster ions and are still continued, like a non-destructive ion detection technique for single-ion measurements. Neutron-rich fission products will be available by the reactor that are important for nuclear astrophysics, especially the r-process. Prior to the on-line coupling to the reactor, TRIGA-TRAP already performed off-line mass measurements on stable and long-lived isotopes and will continue this program. The main focus within this thesis was on certain rare-earth nuclides in the well-established region of deformation around N {proportional_to} 90. Another field of interest are mass measurements on actinoids to test mass models and to provide direct links to the mass standard. Within this thesis, the mass of {sup 241}Am could be measured directly for the first time. (orig.)

  6. The construction of TRIGA-TRAP and direct high-precision Penning trap mass measurements on rare-earth elements and americium

    International Nuclear Information System (INIS)

    Ketelaer, Jens

    2010-01-01

    The construction of TRIGA-TRAP and direct high-precision Penning trap mass measurements on rare-earth elements and americium: Nuclear masses are an important quantity to study nuclear structure since they reflect the sum of all nucleonic interactions. Many experimental possibilities exist to precisely measure masses, out of which the Penning trap is the tool to reach the highest precision. Moreover, absolute mass measurements can be performed using carbon, the atomic-mass standard, as a reference. The new double-Penning trap mass spectrometer TRIGA-TRAP has been installed and commissioned within this thesis work, which is the very first experimental setup of this kind located at a nuclear reactor. New technical developments have been carried out such as a reliable non-resonant laser ablation ion source for the production of carbon cluster ions and are still continued, like a non-destructive ion detection technique for single-ion measurements. Neutron-rich fission products will be available by the reactor that are important for nuclear astrophysics, especially the r-process. Prior to the on-line coupling to the reactor, TRIGA-TRAP already performed off-line mass measurements on stable and long-lived isotopes and will continue this program. The main focus within this thesis was on certain rare-earth nuclides in the well-established region of deformation around N ∝ 90. Another field of interest are mass measurements on actinoids to test mass models and to provide direct links to the mass standard. Within this thesis, the mass of 241 Am could be measured directly for the first time. (orig.)

  7. Measurement and simulation of the pressure ratio between the two traps of double Penning trap mass spectrometers

    International Nuclear Information System (INIS)

    Neidherr, D.; Blaum, K.; Block, M.; Ferrer, R.; Herfurth, F.; Ketelaer, J.; Nagy, Sz.; Weber, C.

    2008-01-01

    Penning traps are ideal tools to perform high-precision mass measurements. For this purpose the cyclotron frequency of the stored charged particles is measured. In case of on-line mass measurements of short-lived nuclides produced at radioactive beam facilities the ions get in general first prepared and cooled by buffer-gas collisions in a preparation trap to reduce their motional amplitudes and are then transported to a precision trap for the cyclotron frequency determination. In modern Penning trap mass spectrometers both traps are placed in the homogeneous region of one superconducting magnet to optimize the transport efficiency. Because the gas pressure inside the precision trap has to be very low in order to minimize the damping of the ion motion caused by collisions with rest gas molecules during the frequency determination, a pumping barrier is installed between both traps. To predict the pressure difference between the two traps in the region of molecular gas flow the motion of each particle can be simulated without consideration of the other particles. Thus, it is possible to calculate the transit probability through a tube of a given geometry. The results are compared with experimentally obtained pressure differences.

  8. First direct mass measurements on nobelium and lawrencium with the Penning trap mass spectrometer SHIPTRAP

    Energy Technology Data Exchange (ETDEWEB)

    Dworschak, Michael Gerhard

    2009-12-08

    The Penning trap mass spectrometer SHIPTRAP at GSI Darmstadt was set up for high-precision mass measurements of heavy radionuclides produced in fusion evaporation reactions and separated from the primary beam by the velocity filter SHIP. It consists of a gas stopping cell for the deceleration of the high energetic reaction products, an RFQ cooler and buncher for cooling and accumulation of the ions, and a double Penning trap system to perform mass measurements. The mass is determined by measuring the cyclotron frequency of the ion of interest in a strong homogeneous magnetic field and comparing it to the frequency of a well-known reference ion. With this method relative uncertainties in the order of 10{sup -8} can be achieved. Recently, mass measurements of the three nobelium isotopes {sup 252-254}No (Z=102) and the lawrencium isotope {sup 255}Lr (Z=103) were performed successfully. These were the first direct mass measurements of transuranium elements ever per- formed. The production rate of the atoms of interest was about one per second or less. The results of the measurements on nobelium confirm the previous mass values which were deduced from Q{sub {alpha}} values. In the case of {sup 255}Lr the mass excess value, which was previously only estimated from systematic trends, was for the first time directly measured. These results mark the first step in the exploration of the region of transuranium elements which is planned at SHIPTRAP. The main objective is to fix the endpoints of {alpha} decay chains which are originating from superheavy elements close to the predicted island of stability. (orig.)

  9. Improvements in the injection system of the Canadian Penning trap mass spectrometer

    CERN Document Server

    Clark, J; Boudreau, C; Buchinger, F; Crawford, J E; Gulick, S; Hardy, J C; Heinz, A; Lee, J K P; Moore, R B; Savard, G; Seweryniak, D; Sharma, K S; Sprouse, G; Vaz, J; Wang, J C; Zhou, Z

    2003-01-01

    The Canadian Penning Trap (CPT) mass spectrometer is designed to make precise mass measurements on a variety of stable and short-lived isotopes. Modifications to the injection system of the CPT have been implemented in recent months, the purpose being to more efficiently collect and transfer weakly-produced reaction products from the target to the Penning trap. These include a magnetic triplet situated after the target chamber to increase the acceptance of the Enge spectrograph, a velocity filter to more effectively separate the beam from the reaction products and the replacement of the Paul trap with a linear trap resulting in more efficient capture and accumulation of ions from the ion cooler. This paper will discuss these recent modifications and how they have increased our ability in making mass measurements on isotopes of low abundance, including those from a sup 2 sup 5 sup 2 Cf fission source.

  10. The LEBIT 9.4 T Penning trap system

    Energy Technology Data Exchange (ETDEWEB)

    Ringle, R.; Bollen, G.; Schury, P.; Sun, T. [National Superconducting Cyclotron Laboratory, East Lansing, MI (United States); Michigan State University, Department of Physics and Astronomy, East Lansing, MI (United States); Lawton, D.; Schwarz, S. [National Superconducting Cyclotron Laboratory, East Lansing, MI (United States)

    2005-09-01

    The initial experimental program with the Low-Energy Beam and Ion Trap Facility, or LEBIT, will concentrate on Penning trap mass measurements of rare isotopes, delivered by the Coupled Cyclotron Facility (CCF) of the NSCL. The LEBIT Penning trap system has been optimized for high-accuracy mass measurements of very short-lived isotopes. (orig.)

  11. The LEBIT 9.4 T Penning trap system

    International Nuclear Information System (INIS)

    Ringle, R.; Bollen, G.; Schury, P.; Sun, T.; Lawton, D.; Schwarz, S.

    2005-01-01

    The initial experimental program with the Low-Energy Beam and Ion Trap Facility, or LEBIT, will concentrate on Penning trap mass measurements of rare isotopes, delivered by the Coupled Cyclotron Facility (CCF) of the NSCL. The LEBIT Penning trap system has been optimized for high-accuracy mass measurements of very short-lived isotopes. (orig.)

  12. Penning Trap Experiments with the Most Exotic Nuclei on Earth: Precision Mass Measurements of Halo Nuclei

    Science.gov (United States)

    Brodeur, M.; Brunner, T.; Ettenauer, S.; Lapierre, A.; Ringle, R.; Delheij, P.; Dilling, J.

    2009-05-01

    Exotic nuclei are characterized with an extremely unbalanced protons-neutrons ratio (p/n) where for instance, the halo isotopes of He and Li have up to 3X more n than p (compared to p/n = 1 in ^12C). The properties of these exotic halo nuclei have long been recognized as the most stringent tests of our understanding of the strong force. ^11Li belongs to a special category of halos called Borromean, bound as a three-body family, while the two-body siblings, ^10Li and 2 n, are unbound as separate entities. Last year, a first mass measurement of the radioisotope ^11Li using a Penning trap spectrometer was carried out at the TITAN (Triumf's Ion Trap for Atomic and Nuclear science) facility at TRIUMF-ISAC. Penning traps are proven to be the most precise device to make mass measurements, yet until now they were unable to reach these nuclei. At TRIUMF we managed to measure the mass of ^11Li to an unprecedented precision of dm/m = 60 ppb, which is remarkable since it has a half-life of only 8.8 ms which it the shortest-lived nuclide to be measured with this technique. Furthermore, new and improved masses for the 2 and 4 n halo ^6,8He, as well has the 1 n halo ^11Be have been performed. An overview of the TITAN mass measurement program and its impact in understanding the most exotic nuclei will be given.

  13. Precise mass measurements of astrophysical interest made with the Canadian Penning trap mass spectrometer

    International Nuclear Information System (INIS)

    Clark, J.A.; Barber, R.C.; Blank, B.; Boudreau, C.; Buchinger, F.; Crawford, J.E.; Gulick, S.; Hardy, J.C.; Heinz, A.; Lee, J.K.P.; Levand, A.F.; Moore, R.B.; Savard, G.; Seweryniak, D.; Sharma, K.S.; Sprouse, G.D.; Trimble, W.; Vaz, J.; Wang, J.C.; Zhou, Z.

    2004-01-01

    The processes responsible for the creation of elements more massive than iron are not well understood. Possible production mechanisms involve the rapid capture of protons (rp-process) or the rapid capture of neutrons (r-process), which are thought to occur in explosive astrophysical events such as novae, x-ray bursts, and supernovae. Mass measurements of the nuclides involved with uncertainties on the order of 100 keV or better are critical to determine the process 'paths', the energy output of the events, and the resulting nuclide abundances. Particularly important are the masses of 'waiting-point' nuclides along the rp-process path where the process stalls until the subsequent β decay of the nuclides. This paper will discuss the precise mass measurements made of isotopes along the rp-process and r-process paths using the Canadian Penning Trap mass spectrometer, including the mass of the critical waiting-point nuclide 68 Se

  14. Precision mass measurements at THe-trap and the FSU trap

    Energy Technology Data Exchange (ETDEWEB)

    Hoecker, Martin Juergen

    2016-07-26

    THe-Trap is a Penning-trap mass spectrometer at the Max-Planck-Institute for Nuclear Physics in Heidelberg, Germany, that aims to measure the T/{sup 3}He mass ratio with a relative uncertainty of 10{sup -11}. Improvements of the measurement technique, in particular the measurement of systematic shifts, enabled measurements of mass ratios with relative uncertainties of 7.10{sup -11}, as demonstrated by a cyclotron frequency ratio determination on {sup 12}C{sup 4+}/{sup 16}O{sup 5+}. This uncertainty was limited by the lineshape. An improved theoretical model based on a rotating wave approximation can be used to describe dynamical interactions between the detection system and the ion, in order to better understand the lineshape and to further reduce the uncertainty. The Florida State University trap is a Penning-trap mass spectrometer located in Tallahassee, Florida (USA). In the context of this thesis, three mass ratios were measured, and further 20 mass ratio measurements analyzed, which resulted in the publication of the masses of {sup 82,83}Kr, {sup 131,134}Xe, {sup 86-88}Sr, and {sup 170-174,176}Yb with relative uncertainties between (0.9 - 1.3).10{sup -10}. These masses serve as reference masses for other experiments and have applications in the determination of the fine-structure constant alpha via the photon-recoil method.

  15. Penning-trap mass spectrometry of radioactive, highly charged ions. Measurements of neutron-rich Rb and Sr nuclides for nuclear astrophysics and development of a novel Penning trap for cooling highly charged ions

    International Nuclear Information System (INIS)

    Simon, Vanessa Veronique

    2012-01-01

    High-precision atomic mass measurements are vital for the description of nuclear structure, investigations of nuclear astrophysical processes, and tests of fundamental symmetries. The neutron-rich A ∼ 100 region presents challenges for modeling the astrophysical r-process because of sudden nuclear shape transitions. This thesis reports on high-precision masses of short-lived neutron-rich 94,97,98 Rb and 94,97-99 Sr isotopes using the TITAN Penning-trap mass spectrometer at TRIUMF. The isotopes were charge-bred to q = 15+; uncertainties of less than 4 keV were achieved. Results deviate by up to 11σ compared to earlier measurements and extend the region of nuclear deformation observed in the A∼100 region. A parameterized r-process model network calculation shows that mass uncertainties for the elemental abundances in this region are now negligible. Although beneficial for the measurement precision, the charge breeding process leads to an increased energy spread of the ions on the order of tens of eV/q. To eliminate this drawback, a Cooler Penning Trap (CPET) has been developed as part of this thesis. The novel multi-electrode trap structure of CPET forms nested potentials to cool HCI sympathetically using either electrons or protons to increase the overall efficiency and precision of the mass measurement. The status of the off-line setup and initial commissioning experiments are presented.

  16. Commissioning of the double Penning trap system MLLTRAP and first studies on mass-dependent systematic uncertainties

    Energy Technology Data Exchange (ETDEWEB)

    Krug, Kevin; Weber, Christine; Thirolf, Peter G.; Szerypo, Jerzy; Gartzke, Eva; Habs, Dietrich [Fakultaet fuer Physik, LMU Muenchen (Germany); Kolhinen, Veli [Fakultaet fuer Physik, LMU Muenchen (Germany); Department of Physics, University of Jyvaeskylae (Finland)

    2010-07-01

    The cylindrical double Penning trap system MLLTRAP in its commissioning phase at the Maier-Leibnitz-Laboratory (MLL) Tandem accelerator in Garching is designed to perform high-accuracy mass measurements on fusion-reaction products. As the mass uncertainty is inversely proportional to the ionic charge state, the ions of interest will be charge bred prior to injection into the Penning trap system. In the future setup, both traps are foreseen to be operated as measurement traps with a relative homogeneity of the magnetic field at the trapping sites of {delta}B/B{<=}0.3 ppm. In the commissioning phase, an offline surface ionization source is used for iterative optimization of the apparatus and studies on mass-dependent systematic uncertainties. Mass measurements via the time-of-flight ion cyclotron resonance method (TOF-ICR) of reference ions with well-known masses ({sup 85}Rb, {sup 87}Rb, {sup 39}K, {sup 133}Cs) were carried out to analyze mass-dependent systematic effects. Together with previous studies on the uncertainty due to magnetic-field fluctuations the current status with respect to the limits of mass accuracy of the apparatus is presented.

  17. The Ramsey method in high-precision mass spectrometry with Penning traps Experimental results

    CERN Document Server

    George, S; Herfurth, F; Herlert, A; Kretzschmar, M; Nagy, S; Schwarz, S; Schweikhard, L; Yazidjian, C

    2007-01-01

    The highest precision in direct mass measurements is obtained with Penning trap mass spectrometry. Most experiments use the interconversion of the magnetron and cyclotron motional modes of the stored ion due to excitation by external radiofrequency-quadrupole fields. In this work a new excitation scheme, Ramsey's method of time-separated oscillatory fields, has been successfully tested. It has been shown to reduce significantly the uncertainty in the determination of the cyclotron frequency and thus of the ion mass of interest. The theoretical description of the ion motion excited with Ramsey's method in a Penning trap and subsequently the calculation of the resonance line shapes for different excitation times, pulse structures, and detunings of the quadrupole field has been carried out in a quantum mechanical framework and is discussed in detail in the preceding article in this journal by M. Kretzschmar. Here, the new excitation technique has been applied with the ISOLTRAP mass spectrometer at ISOLDE/CERN fo...

  18. Status and outlook of CHIP-TRAP: The Central Michigan University high precision Penning trap

    Science.gov (United States)

    Redshaw, M.; Bryce, R. A.; Hawks, P.; Gamage, N. D.; Hunt, C.; Kandegedara, R. M. E. B.; Ratnayake, I. S.; Sharp, L.

    2016-06-01

    At Central Michigan University we are developing a high-precision Penning trap mass spectrometer (CHIP-TRAP) that will focus on measurements with long-lived radioactive isotopes. CHIP-TRAP will consist of a pair of hyperbolic precision-measurement Penning traps, and a cylindrical capture/filter trap in a 12 T magnetic field. Ions will be produced by external ion sources, including a laser ablation source, and transported to the capture trap at low energies enabling ions of a given m / q ratio to be selected via their time-of-flight. In the capture trap, contaminant ions will be removed with a mass-selective rf dipole excitation and the ion of interest will be transported to the measurement traps. A phase-sensitive image charge detection technique will be used for simultaneous cyclotron frequency measurements on single ions in the two precision traps, resulting in a reduction in statistical uncertainty due to magnetic field fluctuations.

  19. Preparation of a tritium Q-value measurement in a double penning trap

    Energy Technology Data Exchange (ETDEWEB)

    Diehl, Christoph; Orth, Christoph; Blaum, Klaus [Max-Planck-Institut fuer Kernphysik, Heidelberg (Germany); Physikalisches Institut, Ruprecht-Karls-Universitaet, Heidelberg (Germany); Pinegar, David [Max-Planck-Institut fuer Kernphysik, Heidelberg (Germany); Van Dyck, Robert Jr. [Department of Physics, University of Washington, Seattle (United States)

    2009-07-01

    A precise determination of the Q-value of tritium ({sup 3}H) is of relevance for the determination of the electron anti-neutrino mass as aspired by the Karlsruhe Tritium Neutrino Experiment (KATRIN). In our double Penning trap mass spectrometer we aim to measure the mass ratio of {sup 3}H and its {beta}-decay product {sup 3}He to an accuracy of 10{sup -11}, which would determine the Q-value to an accuracy of 30 meV. The spectrometer we utilize is an enhanced version of the University of Washington Penning trap mass spectrometer (UW-PTMS) and was recently transfered from Seattle to Heidelberg, where it is set up at the moment as the MPIK/UW-PTMS. We present the necessary preparation work at the Max-Planck-Institut fuer Kernphysik. This includes major reconstructions of the building as well as studies and control of environmental parameters in the laboratory, like temperature and magnetic field.

  20. Recent results from the Penning trap mass spectrometer JYFLTRAP

    Energy Technology Data Exchange (ETDEWEB)

    Weber, Christine; Elomaa, Viki-Veikko; Eronen, Tommi; Hakala, Jani; Jokinen, Ari; Kankainen, Anu; Rahaman, Saidur; Rissanen, Juho; Aeystoe, Juha [Department of Physics, (YFL), University of Jyvaeskylae (Finland)

    2009-07-01

    Accurate mass determination employing Penning ion traps has gained increasing importance after the installation of several new on-line facilities at accelerator labs. These setups combine unique production possibilities for rare isotopes with elaborate ion-capture and manipulation techniques. Since the final commissioning of the JYFLTRAP setup at the IGISOL facility in Jyvaeskylae, the masses of more than 200 short-lived nuclides have been measured. Their knowledge applies to studies on nuclear structure, the modeling of nucleosynthesis processes, tests of the conserved vector current (CVC) hypothesis and the unitarity of the CKM matrix, and furthermore, can help to assist in ongoing searches of neutrinoless double-beta decays. This presentation focuses on recent highlights studied at JYFLTRAP.

  1. Penning-trap mass measurements of the neutron-rich K and Ca isotopes: Resurgence of the N=28 shell strength

    Science.gov (United States)

    Lapierre, A.; Brodeur, M.; Brunner, T.; Ettenauer, S.; Finlay, P.; Gallant, A. T.; Simon, V. V.; Delheij, P.; Lunney, D.; Ringle, R.; Savajols, H.; Dilling, J.

    2012-02-01

    We present Penning-trap mass measurements of neutron-rich 44,47-50K and 49,50Ca isotopes carried out at the TITAN facility at TRIUMF-ISAC. The 44K mass measurement was performed with a charge-bred 4+ ion utilizing the TITAN electron beam ion trap and agrees with the literature. The mass excesses obtained for 47K and 49,50Ca are more precise and agree with the values published in the 2003 Atomic Mass Evaluation (AME’03). The 48,49,50K mass excesses are more precise than the AME’03 values by more than 1 order of magnitude. For 48,49K, we find deviations of 7σ and 10σ, respectively. The new 49K mass excess lowers significantly the two-neutron separation energy at the neutron number N=30 compared with the separation energy calculated from the AME’03 mass-excess values and thus increases the N=28 neutron-shell gap energy at Z=19 by approximately 1 MeV.

  2. Commissioning of the double Penning trap system MLLTRAP

    International Nuclear Information System (INIS)

    Kolhinen, V.S.; Bussmann, M.; Gartzke, E.; Habs, D.; Neumayr, J.B.; Schuermann, C.; Szerypo, J.; Thirolf, P.G.

    2009-01-01

    A cylindrical double Penning trap system has been installed and commissioned at the Maier-Leibnitz-Laboratory (MLL) in Garching. This trap system has been designed to isobarically purify low-energy ion beams and perform highly accurate mass measurements. Technical details of the device and the first results of the commissioning measurements will be presented. The mass resolving power achieved in the first trap for 85 Rb ions is R=139(2)x10 3 , while a relative mass uncertainty of δm/m=2.9x10 -8 was reached with the second trap (no analysis of systematic uncertainties included) when using 87 Rb as a reference ion for 85 Rb.

  3. Status of the Penning trap project in Munich

    International Nuclear Information System (INIS)

    Szerypo, J.; Kolhinen, V.S.; Gartzke, E.; Habs, D.; Neumayr, J.; Schuermann, C.; Sewtz, M.; Thirolf, P.G.; Bussmann, M.; Schramm, U.

    2009-01-01

    The MLLTRAP at the Maier-Leibnitz-Laboratory (Garching) is a new Penning trap facility designed to combine several novel technologies to decelerate, charge breed, cool, bunch and purify the reaction products and perform high-accuracy nuclear and atomic mass measurements. It is now in the commissioning phase, achieving a mass-resolving power of about 10 5 in the purification trap for stable ions. (orig.)

  4. Status of the Penning trap project in Munich

    Energy Technology Data Exchange (ETDEWEB)

    Szerypo, J.; Kolhinen, V.S.; Gartzke, E.; Habs, D.; Neumayr, J.; Schuermann, C.; Sewtz, M.; Thirolf, P.G. [University of Munich (LMU) and Maier-Leibnitz-Laboratory (MLL), Faculty of Physics, Garching (Germany); Bussmann, M.; Schramm, U. [University of Munich (LMU) and Maier-Leibnitz-Laboratory (MLL), Faculty of Physics, Garching (Germany); Forschungszentrum Dresden-Rossendorf, Dresden (Germany)

    2009-12-15

    The MLLTRAP at the Maier-Leibnitz-Laboratory (Garching) is a new Penning trap facility designed to combine several novel technologies to decelerate, charge breed, cool, bunch and purify the reaction products and perform high-accuracy nuclear and atomic mass measurements. It is now in the commissioning phase, achieving a mass-resolving power of about 10{sup 5} in the purification trap for stable ions. (orig.)

  5. Precision Comparison of $\\bar{p}$ and $ p $ Masses in a Penning Trap

    CERN Multimedia

    2002-01-01

    PS196 : Precision Comparison of $\\bar{p}$ and p Masses in a Penning Trap For the first time, antiprotons with energies 10$^{10}$ times lower than those in LEAR can be stored and studied over long times in a small apparatus. The first measurement at this new, low energy frontier is a 1000-fold improvement in the measured antiproton mass. The mass dependent cyclotron frequencies, first for antiprotons then for protons orbiting in the same magnetic field, are compared to establish that the antiproton and proton masses are the same to at least 4~parts in 10$^8$. This is the most stringent test of whether a baryon system is invariant under CPT transformations. A special trap geometry and a superconducting solenoid which cancels fluctuations in the magnetic field in the accelerator hall were crucial to this greatly improved measurement. The current objective is to improve the precision by one or two orders of magnitude. Antiprotons from LEAR at 5.9~MeV, slow below 3~keV via collisions in a thin metal window, and ar...

  6. Ion bunch stacking in a Penning trap after purification in an electrostatic mirror trap

    CERN Document Server

    Rosenbusch, M; Blaum, K; Borgmann, Ch; Kreim, S; Lunney, D; Manea, V; Schweikhard, L; Wienholtz, F; Wolf, R N

    2014-01-01

    The success of many measurements in analytical mass spectrometry as well as in precision mass determinations for atomic and nuclear physics is handicapped when the ion sources deliver ``contaminations'', i.e., unwanted ions of masses similar to those of the ions of interest. In particular, in ion-trapping devices, large amounts of contaminant ions result in significant systematic errors-if the measurements are possible at all. We present a solution for such cases: The ions from a quasi-continuous source are bunched in a linear radio-frequency-quadrupole ion trap, separated by a multi-reflection time-of-flight section followed by a Bradbury-Nielsen gate, and then captured in a Penning trap. Buffer-gas cooling is used to damp the ion motion in the latter, which allows a repeated opening of the Penning trap for a stacking of mass-selected ion bunches. Proof-of-principle demonstrations have been performed with the ISOLTRAP setup at ISOLDE/CERN, both with Cs-133(+) ions from an off-line ion source and by applicati...

  7. Commissioning of the double Penning trap system MLLTRAP

    Energy Technology Data Exchange (ETDEWEB)

    Kolhinen, V.S. [Fakultaet fuer Physik, LMU Muenchen and Maier-Leibnitz Laboratory, Am Coulombwall 1, 85748 Garching (Germany)], E-mail: veli.kolhinen@physik.uni-muenchen.de; Bussmann, M. [Fakultaet fuer Physik, LMU Muenchen and Maier-Leibnitz Laboratory, Am Coulombwall 1, 85748 Garching (Germany); Forschungszentrum Dresden-Rossendorf, 01314 Dresden (Germany); Gartzke, E.; Habs, D.; Neumayr, J.B.; Schuermann, C.; Szerypo, J.; Thirolf, P.G. [Fakultaet fuer Physik, LMU Muenchen and Maier-Leibnitz Laboratory, Am Coulombwall 1, 85748 Garching (Germany)

    2009-03-01

    A cylindrical double Penning trap system has been installed and commissioned at the Maier-Leibnitz-Laboratory (MLL) in Garching. This trap system has been designed to isobarically purify low-energy ion beams and perform highly accurate mass measurements. Technical details of the device and the first results of the commissioning measurements will be presented. The mass resolving power achieved in the first trap for {sup 85}Rb ions is R=139(2)x10{sup 3}, while a relative mass uncertainty of {delta}m/m=2.9x10{sup -8} was reached with the second trap (no analysis of systematic uncertainties included) when using {sup 87}Rb as a reference ion for {sup 85}Rb.

  8. High-accuracy mass determination of unstable nuclei with a Penning trap mass spectrometer

    CERN Multimedia

    2002-01-01

    The mass of a nucleus is its most fundamental property. A systematic study of nuclear masses as a function of neutron and proton number allows the observation of collective and single-particle effects in nuclear structure. Accurate mass data are the most basic test of nuclear models and are essential for their improvement. This is especially important for the astrophysical study of nuclear synthesis. In order to achieve the required high accuracy, the mass of ions captured in a Penning trap is determined via their cyclotron frequency $ \

  9. First Penning-trap mass measurement of the electron capture nuclide {sup 163}Ho and its daughter {sup 163}Dy for the ECHO project

    Energy Technology Data Exchange (ETDEWEB)

    Schneider, Fabian [Institut fuer Kernchemie und Institut fuer Physik, Johannes Gutenberg-Universitaet Mainz (Germany); Collaboration: TRIGA-SPEC Collaboration; ECHo-Collaboration

    2015-07-01

    The ECHo (Electron Capture of {sup 163}Ho) project aims to determine the mass of the electron neutrino by measuring the calorimetric spectrum of {sup 163}Ho. To be able to extract the neutrino mass from the spectrum near the endpoint a precise knowledge of the decay Q-value is necessary. The ideal way to measure this in a model independent way is by high-precision Penning-trap mass spectrometry. The ECHo collaboration has {sup 163}Ho samples available, which were produced by reactor neutron irradiation. Such samples are typically highly contaminated with radioactive and stable species. These were efficiently removed by chemical purification. Ionization by laser ablation allows high-precision Penning-trap mass measurements with sample sizes of 10{sup 16} atoms. From the measured cyclotron frequency ratio of {sup 163}Ho{sup 16}O{sup +} to {sup 163}Dy{sup 16}O{sup +} we determined the Q-value to be 2.5(7) keV. In addition absolute mass measurements using carbon cluster ions as reference were performed with an uncertainty two times lower than literature values. Future measurements at SHIPTRAP (GSI, Darmstadt) and PENTATRAP (MPIK, Heidelberg) are planned with the aim to drastically improve the uncertainty of the Q-value down to a few eV and thus providing the required input for the ECHo project.

  10. Technical developments for an upgrade of the LEBIT Penning trap mass spectrometry facility for rare isotopes

    Science.gov (United States)

    Redshaw, M.; Barquest, B. R.; Bollen, G.; Bustabad, S. E.; Campbell, C. M.; Ferrer, R.; Gehring, A.; Kwiatkowski, A. A.; Lincoln, D. L.; Morrissey, D. J.; Pang, G. K.; Ringle, R.; Schwarz, S.

    2011-07-01

    The LEBIT (Low Energy Beam and Ion Trap) facility is the only Penning trap mass spectrometry (PTMS) facility to utilize rare isotopes produced via fast-beam fragmentation. This technique allows access to practically all elements lighter than uranium, and in particular enables the production of isotopes that are not available or that are difficult to obtain at isotope separation on-line facilities. The preparation of the high-energy rare-isotope beam produced by projectile fragmentation for low-energy PTMS experiments is achieved by gas stopping to slow down and thermalize the fast-beam ions, along with an rf quadrupole cooler and buncher and rf quadrupole ion guides to deliver the beam to the Penning trap. During its first phase of operation LEBIT has been very successful, and new developments are now underway to access rare isotopes even farther from stability, which requires dealing with extremely short lifetimes and low production rates. These developments aim at increasing delivery efficiency, minimizing delivery and measurement time, and maximizing use of available beam time. They include an upgrade to the gas-stopping station, active magnetic field monitoring and stabilization by employing a miniature Penning trap as a magnetometer, the use of stored waveform inverse Fourier transform (SWIFT) to most effectively remove unwanted ions, and charge breeding.

  11. Technical developments for an upgrade of the LEBIT Penning trap mass spectrometry facility for rare isotopes

    International Nuclear Information System (INIS)

    Redshaw, M.; Barquest, B. R.; Bollen, G.; Bustabad, S. E.; Campbell, C. M.; Ferrer, R.; Gehring, A.; Kwiatkowski, A. A.; Lincoln, D. L.; Morrissey, D. J.; Pang, G. K.; Ringle, R.; Schwarz, S.

    2011-01-01

    The LEBIT (Low Energy Beam and Ion Trap) facility is the only Penning trap mass spectrometry (PTMS) facility to utilize rare isotopes produced via fast-beam fragmentation. This technique allows access to practically all elements lighter than uranium, and in particular enables the production of isotopes that are not available or that are difficult to obtain at isotope separation on-line facilities. The preparation of the high-energy rare-isotope beam produced by projectile fragmentation for low-energy PTMS experiments is achieved by gas stopping to slow down and thermalize the fast-beam ions, along with an rf quadrupole cooler and buncher and rf quadrupole ion guides to deliver the beam to the Penning trap. During its first phase of operation LEBIT has been very successful, and new developments are now underway to access rare isotopes even farther from stability, which requires dealing with extremely short lifetimes and low production rates. These developments aim at increasing delivery efficiency, minimizing delivery and measurement time, and maximizing use of available beam time. They include an upgrade to the gas-stopping station, active magnetic field monitoring and stabilization by employing a miniature Penning trap as a magnetometer, the use of stored waveform inverse Fourier transform (SWIFT) to most effectively remove unwanted ions, and charge breeding.

  12. Penning trap mass spectrometry Q-value determinations for highly forbidden β-decays

    Science.gov (United States)

    Sandler, Rachel; Bollen, Georg; Eibach, Martin; Gamage, Nadeesha; Gulyuz, Kerim; Hamaker, Alec; Izzo, Chris; Kandegedara, Rathnayake; Redshaw, Matt; Ringle, Ryan; Valverde, Adrian; Yandow, Isaac; Low Energy Beam Ion Trap Team

    2017-09-01

    Over the last several decades, extremely sensitive, ultra-low background beta and gamma detection techniques have been developed. These techniques have enabled the observation of very rare processes, such as highly forbidden beta decays e.g. of 113Cd, 50V and 138La. Half-life measurements of highly forbidden beta decays provide a testing ground for theoretical nuclear models, and the comparison of calculated and measured energy spectra could enable a determination of the values of the weak coupling constants. Precision Q-value measurements also allow for systematic tests of the beta-particle detection techniques. We will present the results and current status of Q value determinations for highly forbidden beta decays. The Q values, the mass difference between parent and daughter nuclides, are measured using the high precision Penning trap mass spectrometer LEBIT at the National Superconducting Cyclotron Laboratory.

  13. Quadrupole deflector of the double Penning trap system MLLTRAP

    Energy Technology Data Exchange (ETDEWEB)

    Gartzke, Eva; Kolhinen, Veli; Habs, Dietrich; Neumayr, Juergen; Schuermann, Christian; Szerypo, Jerzy; Thirolf, Peter [Fakultaet fuer Physik, LMU Muenchen, Garching (Germany); Maier-Leibnitz Laboratory, Garching (Germany)

    2009-07-01

    A cylindrical double Penning trap has been installed and successfully commissioned at the Maier-Leibnitz Laboratory in Garching. This trap system has been designed to isobarically purify low energy ion beams and perform highly accurate mass measurements. An electrostatic quadrupole deflector has been designed and installed at the injection line of the Penning trap system enabling a simultaneous use of an online ion beam with reference ions from an offline ion source. Alternatively two offline sources can be used concurrently e.g. an {alpha} recoil sources providing heavy radioactive species (e.g {sup 240}U) together with reference mass ions (which in the future will be e.g. a carbon cluster ion source). The bender has been designed for beam energies up to 1 keV with q/A ratios 1/1-1/250. This presentation shows the technical design and the operating parameters of the quadrupole beam bender and its implementation at the MLLTRAP system.

  14. A cylindrical Penning trap for capture, mass selective cooling, and bunching of radioactive ion beams

    International Nuclear Information System (INIS)

    Raimbault-Hartmann, H.; Bollen, G.; Beck, D.; Koenig, M.; Kluge, H.-J.; Schwarz, S.; Schark, E.; Stein, J.; Szerypo, J.

    1997-01-01

    A Penning trap ion accumulator, cooler, and buncher for low-energy ion beams has been developed for the ISOLTRAP mass spectrometer at ISOLDE/CERN. A cylindrical electrode configuration is used for the creation of a nested trapping potential. This is required for efficient accumulation of externally produced ions and for high-mass selectivity by buffer gas cooling. The design goal of a mass resolving power of about 1 x 10 5 has been achieved. Isobar separation has been demonstrated for radioactive rare-earth ion beams delivered by the ISOLDE on-line mass separator. (orig.)

  15. A cylindrical Penning trap for capture, mass selective cooling, and bunching of radioactive ion beams

    CERN Document Server

    Raimbault-Hartmann, H; Bollen, G; König, M; Kluge, H J; Schark, E; Stein, J; Schwarz, S; Szerypo, J

    1997-01-01

    A Penning trap ion accumulator, cooler, and buncher for low energy ion beams has been developed for the ISOLTRAP mass spectrometer at ISOLDE/CERN. A cylindrical electrode configuration is used for the creation of a nested trapping potential. This is required for efficient accumulation of externally produced ions and for high mass selectivity by buffer gas cooling. The design goal of a mass resolving power of about $1\\cdot 10^{5}$ has been achieved. Isobar separation has been demonstrated for radioactive rare earth ion beams delivered by the ISOLDE on-line mass separator.

  16. Mass of 17O from Penning-trap mass spectrometry and molecular spectroscopy: A precision test of the Dunham-Watson model in carbon monoxide

    International Nuclear Information System (INIS)

    Mount, Brianna J.; Redshaw, Matthew; Myers, Edmund G.; Mueller, Holger S. P.

    2010-01-01

    By fitting the Dunham-Watson model to extensive rotational and vibrational spectroscopic data of isotopic variants of CO, and by using existing precise masses of 13 C, 16 O, and 18 O from Penning-trap mass spectrometry, we determine the atomic mass of 17 O to be M[ 17 O]=16.999 131 644(30) u, where the uncertainty is purely statistical. Using Penning-trap mass spectrometry, we have also directly determined the atomic mass of 17 O with the more precise result M[ 17 O]=16.999 131 756 6(9) u. The Dunham-Watson model applied to the molecular spectroscopic data hence predicts the mass of 17 O to better than 1 part in 10 8 .

  17. Micro Penning Trap for Continuous Magnetic Field Monitoring in High Radiation Environments

    Science.gov (United States)

    Latorre, Javiera; Bollen, Georg; Gulyuz, Kerim; Ringle, Ryan; Bado, Philippe; Dugan, Mark; Lebit Team; Translume Collaboration

    2016-09-01

    As new facilities for rare isotope beams, like FRIB at MSU, are constructed, there is a need for new instrumentation to monitor magnetic fields in beam magnets that can withstand the higher radiation level. Currently NMR probes, the instruments used extensively to monitor magnetic fields, do not have a long lifespans in radiation-high environments. Therefore, a radiation-hard replacement is needed. We propose to use Penning trap mass spectrometry techniques to make high precision magnetic field measurements. Our Penning microtrap will be radiation resistant as all of the vital electronics will be at a safe distance from the radiation. The trap itself is made from materials not subject to radiation damage. Penning trap mass spectrometers can determine the magnetic field by measuring the cyclotron frequency of an ion with a known mass and charge. This principle is used on the Low Energy Beam Ion Trap (LEBIT) minitrap at NSCL which is the foundation for the microtrap. We have partnered with Translume, who specialize in glass micro-fabrication, to develop a microtrap in fused-silica glass. A microtrap is finished and ready for testing at NSCL with all of the electronic and hardware components setup. DOE Phase II SBIR Award No. DE-SC0011313, NSF Award Number 1062410 REU in Physics, NSF under Grant No. PHY-1102511.

  18. Nuclear structure studies in the xenon and radon region and the discovery of a new radon isotope by Penning-trap mass spectrometry

    CERN Document Server

    Neidherr, Dennis

    2010-01-01

    Nowadays high-precision mass measurements based on Penning traps allow a deep insight into the fundamental properties of nucleonic matter. To this end, the cyclotron frequency of an ion confined in a strong, homogeneous magnetic field B is determined. At the ISOLTRAP mass spectrometer at ISOLDE / CERN the masses of short-lived radioactive nuclei with half-lives down to several ten ms can be measured with an uncertainty in the order of 10$^{-8}$and below. ISOLTRAP consists of an RFQ cooler and buncher to cool and accumulate the ions coming from ISOLDE and a double Penning-trap system to first clean the ion samples and finally perform the mass measurements. Within this thesis the masses of neutron rich xenon and radon isotopes, namely $^{138-146}$Xe and $^{223-229}$Rn were determined, eleven of them for the first time. $^{229}$Rn was even discovered in this experiment and its half-life could be determined to roughly 12$^{+1.2}_{-1.3}$ s. Since the mass reflects all interactions inside the nucleus it is a unique...

  19. The Penning trap system used by the BASE experiment

    CERN Multimedia

    Marcastel, Fabienne

    2015-01-01

    A cut-away schematic of the Penning trap system used by BASE. The experiment receives antiprotons from CERN's AD; negative hydrogen ions are formed during injection into the apparatus. The set-up works with only a pair of particles at a time, while a cloud of a few hundred others are held in the reservoir trap, for future use. Here, an antiproton is in the measurement trap, while the negative hydyrogen ion is in held by the downstream park electrode. When the antiproton has been measured, it is moved to the upstream park electrode and the hydrogen ion is brought in to the measurement trap. This is repeated thousands of times, enabling a high-precision comparison of the charge-to-mass ratios of the two particles.

  20. Space-charge effects in Penning ion traps

    Science.gov (United States)

    Porobić, T.; Beck, M.; Breitenfeldt, M.; Couratin, C.; Finlay, P.; Knecht, A.; Fabian, X.; Friedag, P.; Fléchard, X.; Liénard, E.; Ban, G.; Zákoucký, D.; Soti, G.; Van Gorp, S.; Weinheimer, Ch.; Wursten, E.; Severijns, N.

    2015-06-01

    The influence of space-charge on ion cyclotron resonances and magnetron eigenfrequency in a gas-filled Penning ion trap has been investigated. Off-line measurements with K39+ using the cooling trap of the WITCH retardation spectrometer-based setup at ISOLDE/CERN were performed. Experimental ion cyclotron resonances were compared with ab initio Coulomb simulations and found to be in agreement. As an important systematic effect of the WITCH experiment, the magnetron eigenfrequency of the ion cloud was studied under increasing space-charge conditions. Finally, the helium buffer gas pressure in the Penning trap was determined by comparing experimental cooling rates with simulations.

  1. Developments for the HITRAP cooler trap and mass measurements around A = 96 at SHIPTRAP

    Energy Technology Data Exchange (ETDEWEB)

    Koszudowski, Stephen

    2009-07-08

    The HITRAP (Highly charged Ions Trap) facility is currently being set up and commissioned at GSI in Darmstadt. It will provide bunches of 10{sup 5} heavy highly-charged ions, for example hydrogen-like uranium (U{sup 91+}), to high-precision atomic physics experiments. The ions are produced by the GSI accelerator complex and decelerated to 4 MeV/u in the Experimental Storage Ring. Then the ions are decelerated by a two-step linear decelerator down to 6 keV/u. The first deceleration step down to 500 keV/u was successfully commissioned. The decelerated ions are injected into a Penning trap (the Cooler Trap), where they are cooled to 4 K by electron and resistive cooling. Resonant circuits for non-destructive detection and the resistive cooling of the trapped particles were designed and tested. The time control of the trap-cycle (trapping, cooling, extraction) with a time resolution of 25 ns was implemented into the control system CS. CS is also used at the mass measurement Penning trap SHIPTRAP, where the new time control is successfully operated. SHIPTRAP measures radioactive ions stemming from fusion evaporation reactions at the velocity filter SHIP. The masses of 9 nuclides ({sup 93,94,95}Technetium, {sup 94,96}Ruthenium, {sup 95,96,97,98}Rhodium) near the line of stability were precisely measured and compared with the Atomic Mass Evaluation. The detection of isomeric states with the present SHIPTRAP set-up was studied. (orig.)

  2. Developments for the HITRAP cooler trap and mass measurements around A = 96 at SHIPTRAP

    International Nuclear Information System (INIS)

    Koszudowski, Stephen

    2009-01-01

    The HITRAP (Highly charged Ions Trap) facility is currently being set up and commissioned at GSI in Darmstadt. It will provide bunches of 10 5 heavy highly-charged ions, for example hydrogen-like uranium (U 91+ ), to high-precision atomic physics experiments. The ions are produced by the GSI accelerator complex and decelerated to 4 MeV/u in the Experimental Storage Ring. Then the ions are decelerated by a two-step linear decelerator down to 6 keV/u. The first deceleration step down to 500 keV/u was successfully commissioned. The decelerated ions are injected into a Penning trap (the Cooler Trap), where they are cooled to 4 K by electron and resistive cooling. Resonant circuits for non-destructive detection and the resistive cooling of the trapped particles were designed and tested. The time control of the trap-cycle (trapping, cooling, extraction) with a time resolution of 25 ns was implemented into the control system CS. CS is also used at the mass measurement Penning trap SHIPTRAP, where the new time control is successfully operated. SHIPTRAP measures radioactive ions stemming from fusion evaporation reactions at the velocity filter SHIP. The masses of 9 nuclides ( 93,94,95 Technetium, 94,96 Ruthenium, 95,96,97,98 Rhodium) near the line of stability were precisely measured and compared with the Atomic Mass Evaluation. The detection of isomeric states with the present SHIPTRAP set-up was studied. (orig.)

  3. Penning-trap mass measurements of exotic rubidium and gold isotopes for a mean-field study of pairing and quadrupole correlations

    CERN Document Server

    Manea, Vladimir

    2015-09-14

    The most complex nuclei are situated between the magic and the mid-shell ones, in regions known for sudden changes of the trends of nuclear observables. These are the so-called shape-transition regions, where the nuclear paradigm changes from the vibrational liquid drop to the static rotor. With few exceptions, nuclei in these regions are radioactive, with half-lives dropping into the millisecond range. Complementing the information obtained from the low-lying excitation spectrum, nuclear binding energies and mean-square charge radii are among the observables most sensitive to these changes of nuclear structure. In the present work, a study of the shape- transition phenomenon is performed by measurements of radioactive nuclides produced by the ISOLDE facility at CERN. The masses of the neutron-rich rubidium isotopes $^{98-100}$Rb and of the neutron-deficient gold isotopes $^{180, 185, 188, 190, 191}$Au are determined using the Penning-trap mass spectrometer ISOLTRAP. The mass of $^{100}$Rb is determined for t...

  4. Electrostatic ion trap and Fourier transform measurements for high-resolution mass spectrometry

    International Nuclear Information System (INIS)

    Bhushan, K. G.; Gadkari, S. C.; Yakhmi, J. V.; Sahni, V. C.

    2007-01-01

    We report on the development of an electrostatic ion trap for high-resolution mass spectrometry. The trap works on purely electrostatic fields and hence trapping and storing of ions is not mass restrictive, unlike other techniques based on Penning, Paul, or radio frequency quadrupole ion traps. It allows simultaneous trapping and studying of multiple mass species over a large mass range. Mass spectra were recorded in ''dispersive'' and ''self-bunching'' modes of ions. Storage lifetimes of about 100 ms and mass resolving power of about 20 000 could be achieved from the fifth harmonic Fourier transform spectrum of Xe ions recorded in the self-bunching mode

  5. Cylindrical Penning traps with dynamic orthogonalized anharmonicity compensation for precision experiments

    International Nuclear Information System (INIS)

    Fei Xiang; Snow, W.M.

    1999-01-01

    Harmonic potentials can be produced in cylindrical ion traps by means of dynamic orthogonalized anharmonicity compensation with use of two (or multiple) sets of compensation electrodes. One special example is for traps with multiple identical electrodes which are not only easy to construct and allow access to the center region of the trap for particle loading and releasing, laser beams, and microwaves, but also flexible in forming harmonic potential wells in many locations. The nested trap configuration and the side-by-side trap configuration are readily available in this special scheme. Analytical solutions for cylindrical traps with multiple sets of compensation potentials are presented. This work will be useful for studies involving Penning trap diagnostics, atomic and molecular interactions (including the production of antihydrogen atoms), accurate mass measurements of exotic particles, and precision measurements of the spin precession frequencies of trapped particles

  6. Cylindrical Penning traps with dynamic orthogonalized anharmonicity compensation for precision experiments

    CERN Document Server

    Fei Xiang

    1999-01-01

    Harmonic potentials can be produced in cylindrical ion traps by means of dynamic orthogonalized anharmonicity compensation with use of two (or multiple) sets of compensation electrodes. One special example is for traps with multiple identical electrodes which are not only easy to construct and allow access to the center region of the trap for particle loading and releasing, laser beams, and microwaves, but also flexible in forming harmonic potential wells in many locations. The nested trap configuration and the side-by-side trap configuration are readily available in this special scheme. Analytical solutions for cylindrical traps with multiple sets of compensation potentials are presented. This work will be useful for studies involving Penning trap diagnostics, atomic and molecular interactions (including the production of antihydrogen atoms), accurate mass measurements of exotic particles, and precision measurements of the spin precession frequencies of trapped particles.

  7. Results from the commissioning of the double Penning trap system MLLTRAP

    Energy Technology Data Exchange (ETDEWEB)

    Kolhinen, Veli; Gartzke, Eva; Habs, Dietrich; Neumayr, Juergen; Schuermann, Christian; Szerypo, Jerzy; Thirolf, Peter [Fakultaet fuer Physik, LMU Muenchen, Garching (Germany); Maier-Leibnitz Laboratory, Garching (Germany)

    2009-07-01

    A cylindrical double Penning trap has been installed and successfully commissioned at the Maier-Leibnitz Laboratory (MLL) in Garching. This trap system has been designed to isobarically purify low energy ion beams and perform highly accurate mass measurements. Test measurements were performed by using an offline Rb surface ion source producing singly charged {sup 85}Rb and {sup 87}Rb ions. A mass resolving power of 139(2).10{sup 3} has been reached with the purification trap for {sup 85}Rb ions and a relative mass uncertainty of the order of {delta}m/m=2.9.10{sup -8} with the measurement trap for {sup 85}Rb ions by using {sup 87}Rb as reference ions. This value does not yet include systematic uncertainties. Detailed studies of systematic uncertainties arising from magnetic field changes caused by short term temperature and pressure fluctuations in the experimental area and from the long term decay of the magnetic field strength have been performed and the result of the analysis is presented. Mass measurements with offline actinide alpha recoil ion sources providing heavy radioactive species (e.g. {sup 240}U) are in preparation.

  8. Shedding light on the mercury mass discrepancy by weighing Hg52+ ions in a Penning trap

    International Nuclear Information System (INIS)

    Fritioff, T.; Bluhme, H.; Schuch, R.; Bergstroem, I.; Bjoerkhage, M.

    2003-01-01

    In their nuclear tables Audi and Wapstra have pointed out a serious mass discrepancy between their extrapolated values for the mercury isotopes and those from a direct measurement by the Manitoba group. The values deviate by as much as 85 ppb from each other with claimed uncertainties of about 16 and 7 ppb, respectively. In order to decide which values are correct the masses of the 198 Hg and 204 Hg isotopes have been measured in the Stockholm Penning trap mass spectrometer SMILETRAP using 52+ ions. This charge state corresponds to a filled Ni electron configuration for which the electron binding energy can be accurately calculated. The mass values obtained are 197.966 768 44(43) u for 198 Hg and 203.973 494 10(39) u for 204 Hg. These values agree with those measured by the Manitoba group, with a 3 times lower uncertainty. This measurement was made possible through the implementation of a cooling technique of the highly charged mercury ions during charge breeding in the electron beam ion source used for producing the Hg 52+ ions

  9. Penning-trap mass spectrometry of neutron-rich copper isotopes for probing the Z = 28 and N = 50 shell closures

    CERN Multimedia

    Manea, V

    We propose to perform a Penning-trap mass measurement of $^{79}$Cu. This exotic N = 50 isotone is the last frontier before the doubly-magic $^{78}$Ni and will greatly improve our knowledge of shell evolution. In the same run, we propose $^{77-78}$Cu mass measurements, as well as the search for a possible isomer in $^{76m}$Cu. The data will help to clarify the structure of the odd proton in the Cu isotopes, the influence on the Z = 28 proton core of the νg$_{9/2}$ orbital filling and the impact of the proton-neutron residual interaction on the strength of the N = 50 shell closure.

  10. Mass measurements on radioactive isotopes using the ISOLTRAP spectrometer

    CERN Document Server

    Dilling, J; Kluge, H J; Kohl, A; Lamour, E; Marx, G; Schwarz, S C; Bollen, G; Kellerbauer, A G; Moore, R B; Henry, S

    2000-01-01

    ISOLTRAP is a Penning trap mass spectrometer installed at the on line isotope separator ISOLDE at CERN. Direct measurements of the masses of short lived radio isotopes are performed using the existing triple trap system. This consists of three electromagnetic traps in tandem: a Paul trap to accumulate and bunch the 60 keV dc beam, a Penning trap for cooling and isobar separation, and a precision Penning trap for the determination of the masses by cyclotron resonance. Measurements of masses of unknown mercury isotopes and in the vicinity of doubly magic /sup 208/Pb are presented, all with an accuracy of delta m/m approximately=1*10/sup -7/. Developments to replace the Paul trap by a radiofrequency quadrupole ion guide system to increase the collection efficiency are presently under way and the status is presented. (10 refs).

  11. Coherent states approach to Penning trap

    International Nuclear Information System (INIS)

    Fernandez, David J; Velazquez, Mercedes

    2009-01-01

    By using a matrix technique, which allows us to identify directly the ladder operators, the Penning trap coherent states are derived as eigenstates of the appropriate annihilation operators. These states are compared with those obtained through the displacement operator. The associated wavefunctions and mean values for some relevant operators in these states are also evaluated. It turns out that the Penning trap coherent states minimize the Heisenberg uncertainty relation

  12. Numerical and graphical description on the ion motions in a Penning trap for mass measurements

    International Nuclear Information System (INIS)

    Sun, Y.L.; Tian, Y.L.; Huang, W.X.; Wang, J.Y.; Wang, Y.S.; Zhao, J.M.; Wang, Y.

    2013-01-01

    The ion motions in a Penning trap have been studied in detail in the presence of azimuthal dipolar and quadrupolar radio-frequency excitations and buffer gas cooling. The numerical solutions by using the Runge–Kutta method and thus the pictures of the ion trajectories in the trap have been obtained for different cases and summarized in graphical form. For the recentering of the ion of interest and to perform the purification of the ion species, one has to set a reasonable buffer gas pressure in the trap and apply azimuthal quadrupolar excitation at frequency ω rf =ω c . -- Highlights: • Azimuthal dipolar and quadrupolar rf excitations and buffer gas cooling. • Runge–Kutta method. • Pictures of the ion trajectories obtained and summarized in graphical form. • A reasonable buffer gas pressure should be set for recentering ions

  13. CrossRef Space-charge effects in Penning ion traps

    CERN Document Server

    Porobić, T; Breitenfeldt, M; Couratin, C; Finlay, P; Knecht, A; Fabian, X; Friedag, P; Fléchard, X; Liénard, E; Ban, G; Zákoucký, D; Soti, G; Van Gorp, S; Weinheimer, Ch; Wursten, E; Severijns, N

    2015-01-01

    The influence of space-charge on ion cyclotron resonances and magnetron eigenfrequency in a gas-filled Penning ion trap has been investigated. Off-line measurements with View the MathML source using the cooling trap of the WITCH retardation spectrometer-based setup at ISOLDE/CERN were performed. Experimental ion cyclotron resonances were compared with ab initio Coulomb simulations and found to be in agreement. As an important systematic effect of the WITCH experiment, the magnetron eigenfrequency of the ion cloud was studied under increasing space-charge conditions. Finally, the helium buffer gas pressure in the Penning trap was determined by comparing experimental cooling rates with simulations.

  14. Mass measurement of radioactive isotopes

    CERN Document Server

    Kluge, H J; Scheidenberger, C

    2004-01-01

    The highest precision in mass measurements on short-lived radionuclides is obtained using trapping and cooling techniques. Here, the experimental storage ring (ESR) at GSI/Darmstadt and the tandem Penning trap mass spectrometer ISOLTRAP at ISOLDE/CERN play an important role. Status and recent results on mass measurements of radioactive nuclides with ESR and ISOLTRAP are summarized.

  15. Optimal design of a 7 T highly homogeneous superconducting magnet for a Penning trap

    International Nuclear Information System (INIS)

    Wu Wei; He Yuan; Ma Lizhen; Huang Wenxue; Xia Jiawen

    2010-01-01

    A Penning trap system called Lanzhou Penning Trap (LPT) is now being developed for precise mass measurements at the Institute of Modern Physics(IMP). One of the key components is a 7 T actively shielded superconducting magnet with a clear warm bore of 156 mm. The required field homogeneity is 3 x 10 -7 over two 1 cubic centimeter volumes lying 220 mm apart along the magnet axis. We introduce a two-step method which combines linear programming and a nonlinear optimization algorithm for designing the multi-section superconducting magnet. This method is fast and flexible for handling arbitrary shaped homogeneous volumes and coils. With the help of this method an optimal design for the LPT superconducting magnet has been obtained. (authors)

  16. (Anti)hydrogen recombination studies in a nested Penning trap

    International Nuclear Information System (INIS)

    Quint, W.; Kaiser, R.; Hall, D.; Gabrielse, G.

    1993-01-01

    Extremely cold antiprotons, stored in Penning trap at 4 K, open the way toward the production and study of cold antihydrogen. We have begun experimentally investigating the possibility to recombine cold positrons and antiprotons within nested Penning traps. Trap potentials are adjusted to allow cold trapped protons (and positive helium ions) to pass through cold trapped electrons. Electrons, protons and ions are counted by ejecting them to a cold channel plate and by nondestructive radiofrequency techniques. The effect of the space charge of one trapped species upon another trapped species passing through is clearly observed. (orig.)

  17. First Ramsey-type mass measurements with ISOLTRAP and design studies of the new PENTATRAP project

    International Nuclear Information System (INIS)

    George, Sebastian

    2009-01-01

    The application of Penning traps for mass spectrometry has led to a major step in the mass precision. Consequently, atomic masses became more and more important as input parameters in different research fields. This exploitation is still ongoing in line with a steady development of Penning trap mass spectrometers to even higher accuracies. Penning trap mass spectrometry is based on the determination of the free cyclotron frequency ν c =qB/(2πm) of an ion confined in a homogeneous magnetic field B. In principle two different measurement techniques are available: By applying the destructive time-of-flight detection method (TOF-ICR) the trap content is lost after the measurement. Since it is a fast measurement method it is usually used for mass determinations of short-lived radionuclides, whereas a relative mass uncertainty δm/m of a few parts in 10 -9 is routinely reached even for nuclides with half-lives well below 500 ms. This has been achieved by the implementation of the Ramsey method in Penning trap mass spectrometry within this work. By contrast the non-destructive Fourier Transform-Ion Cyclotron Resonance detection method (FT-ICR) determines the frequency of the image current introduced in the trap electrodes by the ion motion. Thus, the ion remains in the trap and can be used for further measurement cycles. This method is often applied for measurements of stable nuclides reaching a relative mass uncertainty of less than δm/m=10 -11 . One part of this thesis was the application of time-separated oscillatory fields, called Ramsey method, for resonant ion motion excitation in order to improve the time-of-flight detection method. It was used to measure the nuclides 26,27 Al and 38,39 Ca with the Penning trap mass spectrometer ISOLTRAP. The mass values have been included in the ''Atomic Mass Evaluation'' (AME). Furthermore, the nuclides 26 Al and 38 Ca serve as input parameters for stringent tests of the Standard Model. Additionally, damping effects in a

  18. Nuclear structure studies in the xenon and radon region and the discovery of a new radon isotope by Penning trap mass spectrometry

    International Nuclear Information System (INIS)

    Neidherr, Dennis

    2010-01-01

    Nowadays high-precision mass measurements based on Penning traps allow a deep insight into the fundamental properties of nucleonic matter. To this end, the cyclotron frequency ν c =qB=(2πm) of an ion confined in a strong, homogeneous magnetic field B is determined. At the ISOLTRAP mass spectrometer at ISOLDE / CERN the masses of short-lived radioactive nuclei with half-lives down to several ten ms can be measured with an uncertainty in the order of 10 -8 and below. ISOLTRAP consists of an RFQ cooler and buncher to cool and accumulate the ions coming from ISOLDE and a double Penning trap system to first clean the ion samples and finally perform the mass measurements. Within this thesis the masses of neutron rich xenon and radon isotopes, namely 138-146 Xe and 223-229 Rn were determined, eleven of them for the first time. 229 Rn was even discovered in this experiment and its half-life could be determined to 12 -1.3 +1.2 s. Since the mass reflects all interactions inside the nucleus it is a unique fingerprint of the nuclide of interest. One of these interactions, the proton-neutron interaction, leads for example to the onset of deformation. The aim of this thesis is to investigate a possible connection be- tween collective effects in nuclei, like the onset of deformation, and double-differences of binding energies, so called δV pn values. Especially in the here presented areas these δV pn values show a very unusual behavior and can not be explained with simple orbital overlapping arguments. One explanation could be the occurrence of octupolar deformation in these regions, which is usually probed with other experimental techniques. However, a quantitative description of the influence of such type of deformation on δV pn is still not possible with modern theories. (orig.)

  19. First β-ν correlation measurement from the recoil-energy spectrum of Penning trapped Ar35 ions

    Science.gov (United States)

    Van Gorp, S.; Breitenfeldt, M.; Tandecki, M.; Beck, M.; Finlay, P.; Friedag, P.; Glück, F.; Herlert, A.; Kozlov, V.; Porobic, T.; Soti, G.; Traykov, E.; Wauters, F.; Weinheimer, Ch.; Zákoucký, D.; Severijns, N.

    2014-08-01

    We demonstrate a novel method to search for physics beyond the standard model by determining the β-ν angular correlation from the recoil-ion energy distribution after β decay of ions stored in a Penning trap. This recoil-ion energy distribution is measured with a retardation spectrometer. The unique combination of the spectrometer with a Penning trap provides a number of advantages, e.g., a high recoil-ion count rate and low sensitivity to the initial position and velocity distribution of the ions and completely different sources of systematic errors compared to other state-of-the-art experiments. Results of a first measurement with the isotope Ar35 are presented. Although currently at limited precision, we show that a statistical precision of about 0.5% is achievable with this unique method, thereby opening up the possibility of contributing to state-of-the-art searches for exotic currents in weak interactions.

  20. First Ramsey-type mass measurements with ISOLTRAP and design studies of the new PENTATRAP project

    Energy Technology Data Exchange (ETDEWEB)

    George, Sebastian

    2009-07-09

    The application of Penning traps for mass spectrometry has led to a major step in the mass precision. Consequently, atomic masses became more and more important as input parameters in different research fields. This exploitation is still ongoing in line with a steady development of Penning trap mass spectrometers to even higher accuracies. Penning trap mass spectrometry is based on the determination of the free cyclotron frequency {nu}{sub c}=qB/(2{pi}m) of an ion confined in a homogeneous magnetic field B. In principle two different measurement techniques are available: By applying the destructive time-of-flight detection method (TOF-ICR) the trap content is lost after the measurement. Since it is a fast measurement method it is usually used for mass determinations of short-lived radionuclides, whereas a relative mass uncertainty {delta}m/m of a few parts in 10{sup -9} is routinely reached even for nuclides with half-lives well below 500 ms. This has been achieved by the implementation of the Ramsey method in Penning trap mass spectrometry within this work. By contrast the non-destructive Fourier Transform-Ion Cyclotron Resonance detection method (FT-ICR) determines the frequency of the image current introduced in the trap electrodes by the ion motion. Thus, the ion remains in the trap and can be used for further measurement cycles. This method is often applied for measurements of stable nuclides reaching a relative mass uncertainty of less than {delta}m/m=10{sup -11}. One part of this thesis was the application of time-separated oscillatory fields, called Ramsey method, for resonant ion motion excitation in order to improve the time-of-flight detection method. It was used to measure the nuclides {sup 26,27}Al and {sup 38,39}Ca with the Penning trap mass spectrometer ISOLTRAP. The mass values have been included in the ''Atomic Mass Evaluation'' (AME). Furthermore, the nuclides {sup 26}Al and {sup 38}Ca serve as input parameters for stringent

  1. Particle confinement in penning traps an introduction

    CERN Document Server

    Vogel, Manuel

    2018-01-01

    This book provides an introduction to the field of Penning traps and related experimental techniques. It serves both as a primer for those entering the field, and as a quick reference for those working in it. The book is motivated by the observation that often a vast number of different resources have to be explored to gain a good overview of Penning trap principles. This is especially true for students who experience additional difficulty due to the different styles of presentation and notation. This volume provides a broad introductory overview in unified notation.

  2. Asymmetric Penning trap coherent states

    International Nuclear Information System (INIS)

    Contreras-Astorga, Alonso; Fernandez, David J.

    2010-01-01

    By using a matrix technique, which allows to identify directly the ladder operators, the coherent states of the asymmetric Penning trap are derived as eigenstates of the appropriate annihilation operators. They are compared with those obtained through the displacement operator method.

  3. Nuclear structure studies in the xenon and radon region and the discovery of a new radon isotope by Penning trap mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Neidherr, Dennis

    2010-04-28

    Nowadays high-precision mass measurements based on Penning traps allow a deep insight into the fundamental properties of nucleonic matter. To this end, the cyclotron frequency {nu}{sub c}=qB=(2{pi}m) of an ion confined in a strong, homogeneous magnetic field B is determined. At the ISOLTRAP mass spectrometer at ISOLDE / CERN the masses of short-lived radioactive nuclei with half-lives down to several ten ms can be measured with an uncertainty in the order of 10{sup -8} and below. ISOLTRAP consists of an RFQ cooler and buncher to cool and accumulate the ions coming from ISOLDE and a double Penning trap system to first clean the ion samples and finally perform the mass measurements. Within this thesis the masses of neutron rich xenon and radon isotopes, namely {sup 138-146}Xe and {sup 223-229}Rn were determined, eleven of them for the first time. {sup 229}Rn was even discovered in this experiment and its half-life could be determined to 12{sub -1.3}{sup +1.2} s. Since the mass reflects all interactions inside the nucleus it is a unique fingerprint of the nuclide of interest. One of these interactions, the proton-neutron interaction, leads for example to the onset of deformation. The aim of this thesis is to investigate a possible connection be- tween collective effects in nuclei, like the onset of deformation, and double-differences of binding energies, so called {delta}V{sub pn} values. Especially in the here presented areas these {delta}V{sub pn} values show a very unusual behavior and can not be explained with simple orbital overlapping arguments. One explanation could be the occurrence of octupolar deformation in these regions, which is usually probed with other experimental techniques. However, a quantitative description of the influence of such type of deformation on {delta}V{sub pn} is still not possible with modern theories. (orig.)

  4. Space-charge effects in Penning ion traps

    Czech Academy of Sciences Publication Activity Database

    Porobic, T.; Beck, M.; Breitenfeldt, M.; Couratin, C.; Finlay, P.; Knecht, A.; Fabian, X.; Friedag, P.; Flechard, X.; Lienard, E.; Ban, G.; Zákoucký, Dalibor; Soti, G.; Van Gorp, S.; Weinheimer, C.; Wursten, E.; Severijns, N.

    2015-01-01

    Roč. 785, JUN (2015), s. 153-162 ISSN 0168-9002 R&D Projects: GA MŠk LA08015; GA MŠk(CZ) LG13031 Institutional support: RVO:61389005 Keywords : Penning trap * space-charge * magnetron motion * ion trapping * buffer gas cooling * ion cyclotron resonance Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders Impact factor: 1.200, year: 2015

  5. Development of an experiment for ultrahigh-precision g-factor measurements in a Penning-trap setup

    Energy Technology Data Exchange (ETDEWEB)

    Alonso Otamendi, J.

    2007-07-13

    This thesis is concerned with the design and construction of an experimental setup aiming to perform ultrahigh-precision g-factor measurements on a bound electron in highly-charged ions. The g-factor of a particle is a dimensionless constant which determines the strength of its interaction with a magnetic field. In the case of an electron bound to a highly-charged ion, it serves as one of the most stringent tests of bound-state quantum electrodynamics (BS-QED). The measurement is based on a triple-Penning-trap system and the continuous Stern-Gerlach effect. The first part of the thesis is devoted to the current knowledge on magnetic moments and motivates the techniques and experimental setup used during the work described. As a major challenge to overcome, the charge breeding of the ions is dealt with in detail, along with the solution found, based on a field-emission-point array. The tools included allow for the measurement of ionization cross-sections by electron impact. The last part of the thesis is dedicated to the design and operation of the triple-Penning-trap setup and the detection schemes implemented. At present, all the experimental setup for the production of highly-charged ions and the corresponding g-factor measurement is completely finalized, including the control system needed for the first measurement stages, so the ion-creation and charge-breeding processes will be the next steps to be taken. (orig.)

  6. Development of an experiment for ultrahigh-precision g-factor measurements in a Penning-trap setup

    International Nuclear Information System (INIS)

    Alonso Otamendi, J.

    2007-01-01

    This thesis is concerned with the design and construction of an experimental setup aiming to perform ultrahigh-precision g-factor measurements on a bound electron in highly-charged ions. The g-factor of a particle is a dimensionless constant which determines the strength of its interaction with a magnetic field. In the case of an electron bound to a highly-charged ion, it serves as one of the most stringent tests of bound-state quantum electrodynamics (BS-QED). The measurement is based on a triple-Penning-trap system and the continuous Stern-Gerlach effect. The first part of the thesis is devoted to the current knowledge on magnetic moments and motivates the techniques and experimental setup used during the work described. As a major challenge to overcome, the charge breeding of the ions is dealt with in detail, along with the solution found, based on a field-emission-point array. The tools included allow for the measurement of ionization cross-sections by electron impact. The last part of the thesis is dedicated to the design and operation of the triple-Penning-trap setup and the detection schemes implemented. At present, all the experimental setup for the production of highly-charged ions and the corresponding g-factor measurement is completely finalized, including the control system needed for the first measurement stages, so the ion-creation and charge-breeding processes will be the next steps to be taken. (orig.)

  7. Nonlinear PIC simulation in a Penning trap

    International Nuclear Information System (INIS)

    Lapenta, G.; Delzanno, G.L.; Finn, J. M.

    2002-01-01

    We study the nonlinear dynamics of a Penning trap plasma, including the effect of the finite length and end curvature of the plasma column. A new cylindrical PIC code, called KANDINSKY, has been implemented by using a new interpolation scheme. The principal idea is to calculate the volume of each cell from a particle volume, in the same manner as it is done for the cell charge. With this new method, the density is conserved along streamlines and artificial sources of compressibility are avoided. The code has been validated with a reference Eulerian fluid code. We compare the dynamics of three different models: a model with compression effects, the standard Euler model and a geophysical fluid dynamics model. The results of our investigation prove that Penning traps can really be used to simulate geophysical fluids

  8. Experiments with Highly-Ionized Atoms in Unitary Penning Traps

    Directory of Open Access Journals (Sweden)

    Shannon Fogwell Hoogerheide

    2015-08-01

    Full Text Available Highly-ionized atoms with special properties have been proposed for interesting applications, including potential candidates for a new generation of optical atomic clocks at the one part in 1019 level of precision, quantum information processing and tests of fundamental theory. The proposed atomic systems are largely unexplored. Recent developments at NIST are described, including the isolation of highly-ionized atoms at low energy in unitary Penning traps and the use of these traps for the precise measurement of radiative decay lifetimes (demonstrated with a forbidden transition in Kr17+, as well as for studying electron capture processes.

  9. Control of the conformations of ion Coulomb crystals in a Penning trap

    Science.gov (United States)

    Mavadia, Sandeep; Goodwin, Joseph F.; Stutter, Graham; Bharadia, Shailen; Crick, Daniel R.; Segal, Daniel M.; Thompson, Richard C.

    2013-01-01

    Laser-cooled atomic ions form ordered structures in radiofrequency ion traps and in Penning traps. Here we demonstrate in a Penning trap the creation and manipulation of a wide variety of ion Coulomb crystals formed from small numbers of ions. The configuration can be changed from a linear string, through intermediate geometries, to a planar structure. The transition from a linear string to a zigzag geometry is observed for the first time in a Penning trap. The conformations of the crystals are set by the applied trap potential and the laser parameters, and agree with simulations. These simulations indicate that the rotation frequency of a small crystal is mainly determined by the laser parameters, independent of the number of ions and the axial confinement strength. This system has potential applications for quantum simulation, quantum information processing and tests of fundamental physics models from quantum field theory to cosmology. PMID:24096901

  10. Two-species mixing in a nested Penning trap for antihydrogen trapping

    International Nuclear Information System (INIS)

    Ordonez, C. A.; Weathers, D. L.

    2008-01-01

    There exists an international quest to trap neutral antimatter in the form of antihydrogen for scientific study. One method that is being developed for trapping antihydrogen employs a nested Penning trap. Such a trap serves to mix positrons and antiprotons so as to produce low energy antihydrogen atoms. Mixing is achieved when the confinement volumes of the two species overlap one another. In the work presented here, a theoretical understanding of the mixing process is developed by analyzing a mixing scheme that was recently reported [G. Gabrielse et al., Phys. Rev. Lett. 100, 113001 (2008)]. The results indicate that positron space charge or collisions among antiprotons may substantially reduce the fraction of antiprotons that have an energy suitable for antihydrogen trapping

  11. Penning-trap Q-value determination of the 71Ga(ν,e−)71Ge reaction using threshold charge breeding of on-line produced isotopes

    International Nuclear Information System (INIS)

    Frekers, D.; Simon, M.C.; Andreoiu, C.; Bale, J.C.; Brodeur, M.; Brunner, T.; Chaudhuri, A.; Chowdhury, U.; Crespo López-Urrutia, J.R.; Delheij, P.; Ejiri, H.; Ettenauer, S.; Gallant, A.T.; Gavrin, V.; Grossheim, A.; Harakeh, M.N.; Jang, F.; Kwiatkowski, A.A.

    2013-01-01

    We present a first direct Q-value measurement of the 71 Ga(ν,e − ) 71 Ge reaction using the TITAN mass-measurement facility at ISAC/TRIUMF. The measurements were performed in a Penning trap on neon-like 71 Ga 21+ and 71 Ge 22+ using isobar separation of the on-line produced mother and daughter nuclei through threshold charge breeding in an electron-beam ion trap. In addition, isoionic samples of 71 Ga 21+ and 71 Ge 21+ were stored concurrently in the Penning trap and provided a separate Q-value measurement. Both independent measurements result in a combined Q-value of 233.5±1.2 keV, which is in agreement with the previously accepted Q-value for the ν cross-section calculations. Together with a recent measurement of the ν-response from the excited states in 71 Ge, we conclude that there are no further uncertainties in the nuclear structure, which could remove the persistent discrepancy between the SAGE and GALLEX calibration measurements performed with neutrinos from reactor-produced 51 Cr and 37 Ar sources and the theoretical expectation

  12. Possibilities for achieving antihydrogen recombination and trapping using a nested Penning trap and a magnetic well

    International Nuclear Information System (INIS)

    Ordonez, C.A.; Dolliver, D.D.; Chang Yongbin; Correa, J. R.

    2002-01-01

    A theoretical study is presented regarding some possibilities for achieving antihydrogen recombination and trapping using a nested Penning trap and a magnetic well. The work reported consists of a review, an extension, and applications of the relevant knowledge base. A nested Penning trap produces a magnetic field, which provides plasma confinement perpendicular to the magnetic field, and an electric field associated with a nested-well potential profile. The nested-well potential profile provides plasma confinement parallel to the magnetic field for oppositely signed plasma species that can have overlapping confinement regions. A configuration is considered in which the electric field is applied in two regions of uniform magnetic field that reside on opposite sides of a magnetic well region. The electric field confines overlapping positron and antiproton plasmas, which thread the magnetic well region. The magnetic well region would serve to trap a fraction of any antihydrogen atoms that are formed. Two different methods are considered for achieving overlap of positron and antiproton plasmas. For each, a set of conditions is predicted for achieving antihydrogen recombination and trapping. Although the study reported specifically considers simultaneous confinement of positron and antiproton plasmas in nested Penning traps, much of the information presented is also relevant to the prospect of merging other pairs of oppositely signed plasmas (e.g., electron and positron plasmas)

  13. Status of THe-Trap

    Energy Technology Data Exchange (ETDEWEB)

    Streubel, Sebastian; Eronen, Tommi; Hoecker, Martin; Ketter, Jochen; Blaum, Klaus [Max-Planck-Institut fuer Kernphysik, Heidelberg (Germany); Van Dyck, Robert S. Jr. [Department of Physics, University of Washington, Seattle, WA (United States)

    2013-07-01

    THe-Trap (short for Tritium-{sup 3}He Trap) is a Penning-trap setup dedicated to measure the {sup 3}H to {sup 3}He mass-ratio with a relative uncertainty of better than 10{sup -11}. The ratio is of relevance for the KArlsruhe TRItium Neutrino experiment (KATRIN), which aims to measure the electron anti-neutrino mass, by measuring the shape of the β-decay energy spectrum close to its endpoint. An independent measurement of the {sup 3}H to {sup 3}He mass-ratio pins down this endpoint, and thus will help to determine the systematics of KATRIN. The trap setup consists of two Penning-traps: One trap for precision measurements, the other trap for ion storage. Ideally, the trap content will be periodically switched, which reduces the time between the measurements of the two ions' motional frequencies. In 2012, a mass ratio measurement of {sup 12}C{sup 4+} to {sup 14}N{sup 5+} was performed to characterize systematic effects of the traps. This measurement yielded a accuracy of 10{sup -9}. Further investigations revealed that a major reason for the modest accuracy is the large axial amplitude of ∼100 μm, compared to a ideal case of 3 μm at 4 K. In addition, relative magnetic fluctuations at a 3 x 10{sup -10} level on a 10 h timescale need to be significantly improved. In this contribution, the aforementioned findings and further systematic studies will be presented.

  14. Electrostatic modes as a diagnostic in Penning-trap experiments

    International Nuclear Information System (INIS)

    Weimer, C.S.; Bollinger, J.J.; Moore, F.L.; Wineland, D.J.

    1994-01-01

    A subset of the electrostatic modes of a cold cloud of electrons, a non-neutral electron plasma, trapped in a Penning trap has been observed and identified using a recent theoretical model. The detection of these modes is accomplished using electronic techniques which could apply to any ion species. The modes are observed in the low-density, low-rotation limit of the cloud where the cloud approaches a two-dimensional charged disk. We observe both axially symmetric and asymmetric drumhead modes. The shape, rotation frequency, and density of the cloud are found in a real-time nondestructive manner by measuring the frequency of these modes. In addition, it is found that radio-frequency sideband cooling compresses the cloud, increasing its density. The ability to measure and control the density of a trapped ion cloud might be useful for experiments on low-temperature ion--neutral-atom collisions, recombination rates, and studies of the confinement properties of non-neutral plasmas

  15. Status of THe-trap

    Energy Technology Data Exchange (ETDEWEB)

    Ketter, Jochen; Eronen, Tommi; Hoecker, Martin; Streubel, Sebastian; Blaum, Klaus [Max-Planck-Institut fuer Kernphysik, Heidelberg (Germany); Van Dyck, Robert S. Jr. [Department of Physics, University of Washington, Seattle, WA (United States)

    2012-07-01

    Originally developed at the University of Washington and relocated to the Max-Planck-Institut fuer Kernphysik in 2008, the Penning-trap spectrometer THe-Trap is specially tailored for a {sup 3}H/{sup 3}He mass-ratio measurement, from which the Q-value of the beta-decay of {sup 3}H to {sup 3}He can be derived. Improving the current best value by at least an order of magnitude will provide an important independent test parameter for the determination of the electron-antineutrino's mass by the Karlsruhe Tritium Neutrino Experiment (KATRIN). However, Penning-trap mass spectrometry has to be pushed to its limits in a dedicated experiment for a sufficiently accurate mass-ratio measurement with a relative uncertainty of 10{sup -11}. Unlike the closed-envelope, single-trap predecessor, the new spectrometer features an external ion source, owing to the radioactive nature of tritium, and two traps in order to speed up the measurement cycle. While the double-trap technique holds great promise, it also calls for more intricate procedures, such as ion transfer. Details about the recent progress of the experiment are given.

  16. First one-line mass measurements at SHIPTRAP and mass determinations of neutron-rich Fr and Ra isotopes at ISOLTRAP

    International Nuclear Information System (INIS)

    Rahaman, M.S.

    2005-01-01

    SHIPTRAP is an ion trap facility behind the velocity lter SHIP at GSI/Darmstadt. Its aim are precision studies of transuranium nuclides produced in a fusion reaction and separated by SHIP. The current set-up for high-precision mass measurements consists of three main functional parts: (i) a gas cell for stopping the energetic ions from SHIP, (ii) radiofrequency quadrupole structures to cool and to bunch the ions extracted from the gas cell, and (iii) a superconducting magnet with two cylindrical Penning traps at a eld strength of 7 T. In this work the Penning trap system has been installed and extensively characterized. The rst on-line mass measurements of short-lived nuclides were carried out and the masses of 147 Er and 148 Er could be experimentally determined for the rst time. Here a relative mass uncertainty of δm/m of about 1 x 10 -6 was achieved. Furthermore the masses of heavy neutron-rich 229-232 Ra and 230 Fr isotopes have been determined with a relative mass uncertainty of about 1 x 10 -7 with the ISOLTRAP mass spectometer at ISOLDE/CERN. The isotope 232 Ra is the heaviest unstable nuclide ever investigated with a Penning trap. Underlying nuclear structure effects of these nuclides far from β-stability were studied by a comparison of the resulting two-neutron separation energies S 2n with those given by the theoretical Infinite Nuclear Mass model. (orig.)

  17. Direct observation of a single proton in a Penning trap. Towards a direct measurement of the proton g-factor

    Energy Technology Data Exchange (ETDEWEB)

    Kreim, Susanne Waltraud

    2009-08-25

    This PhD thesis presents experiments performed on a single proton stored in a Penning trap. The eigenmotion of an isolated, free proton could be detected electronically via a coupling to a resonance circuit. This represents a non-destructive measurement, i.e. the particle is not lost during the measurement. The free cyclotron frequency emerging from the measured eigenfrequencies is one of the two frequencies required for the determination of the magnetic moment. This enables a direct determination of the g-factor contrary to already existing works. Design, developing, and commissioning of the experimental setup have been accomplished within the scope of this work leading to a measuring accuracy of 10{sup -7}. The technical challenges for the determination of the second frequency (the Larmor frequency) arising from the smallness of the magnetic moment were mastered. Since the spin state required for this measurement is an internal degree of freedom, it can only be accessed through a coupling of the magnetic moment to the eigenmotion. A novel, hybrid penning trap is presented in this work, which imprints the spin information onto the eigenmotion, thus, realizing a quantum jump spectrometer. Therewith, the frequency shift of the two spin states resulting from the magnetic coupling reaches for the first time an electronically detectable range. (orig.)

  18. Direct observation of a single proton in a Penning trap. Towards a direct measurement of the proton g-factor

    International Nuclear Information System (INIS)

    Kreim, Susanne Waltraud

    2009-01-01

    This PhD thesis presents experiments performed on a single proton stored in a Penning trap. The eigenmotion of an isolated, free proton could be detected electronically via a coupling to a resonance circuit. This represents a non-destructive measurement, i.e. the particle is not lost during the measurement. The free cyclotron frequency emerging from the measured eigenfrequencies is one of the two frequencies required for the determination of the magnetic moment. This enables a direct determination of the g-factor contrary to already existing works. Design, developing, and commissioning of the experimental setup have been accomplished within the scope of this work leading to a measuring accuracy of 10 -7 . The technical challenges for the determination of the second frequency (the Larmor frequency) arising from the smallness of the magnetic moment were mastered. Since the spin state required for this measurement is an internal degree of freedom, it can only be accessed through a coupling of the magnetic moment to the eigenmotion. A novel, hybrid penning trap is presented in this work, which imprints the spin information onto the eigenmotion, thus, realizing a quantum jump spectrometer. Therewith, the frequency shift of the two spin states resulting from the magnetic coupling reaches for the first time an electronically detectable range. (orig.)

  19. Precision mass measurements of neutron-rich Co isotopes beyond N =40

    Science.gov (United States)

    Izzo, C.; Bollen, G.; Brodeur, M.; Eibach, M.; Gulyuz, K.; Holt, J. D.; Kelly, J. M.; Redshaw, M.; Ringle, R.; Sandler, R.; Schwarz, S.; Stroberg, S. R.; Sumithrarachchi, C. S.; Valverde, A. A.; Villari, A. C. C.

    2018-01-01

    The region near Z =28 and N =40 is a subject of great interest for nuclear structure studies due to spectroscopic signatures in 68Ni suggesting a subshell closure at N =40 . Trends in nuclear masses and their derivatives provide a complementary approach to shell structure investigations via separation energies. Penning trap mass spectrometry has provided precise measurements for a number of nuclei in this region; however, a complete picture of the mass surfaces has so far been limited by the large uncertainty remaining for nuclei with N >40 along the iron (Z =26 ) and cobalt (Z =27 ) chains because these species are not available from traditional isotope separator online rare isotope facilities. The Low-Energy Beam and Ion Trap Facility at the National Superconducting Cyclotron Laboratory is the first and only Penning trap mass spectrometer coupled to a fragmentation facility and therefore presents the unique opportunity to perform precise mass measurements of these elusive isotopes. Here we present the first Penning trap measurements of Co,6968, carried out at this facility. Some ambiguity remains as to whether the measured values are ground-state or isomeric-state masses. A detailed discussion is presented to evaluate this question and to motivate future work. In addition, we perform ab initio calculations of ground-state and two-neutron separation energies of cobalt isotopes with the valence-space in-medium similarity renormalization group approach based on a particular set of two- and three-nucleon forces that predict saturation in infinite matter. We discuss the importance of these measurements and calculations for understanding the evolution of nuclear structure near 68Ni.

  20. Behavior of many ions in a Penning trap and results of the WITCH experiment

    CERN Document Server

    Porobic, Tomica

    Precision measurements of the beta−neutrino angular correlation in nuclear beta-decay provide a unique window into the physics beyond the Standard model. The WITCH (Weak Interaction Trap for CHarged particles) experiment aims to measure this correlation, a(beta-nu), in order to impose a more stringent constraint on the exotic scalar current admixture in the beta-decay Hamiltonian. The apparatus is situated at CERN/ISOLDE laboratory and consists of a unique combination of a retardation spectrometer and two Penning traps, with one of them serving as a scattering-free source. This configuration is suited for a precise measurement of the energy spectrum of 35Ar recoiled daughter ions. The shape of the spectrum then allows a determination of a(beta-nu) and consequently of the presence or absence of a scalar current. Radioactive 35Ar ions are created at ISOLDE by impinging 1.2 GeV protons on the target material. After being separated by a magnetic separator and bunched by REXTRAP, a high-capacity Penning trap, th...

  1. Penning traps with unitary architecture for storage of highly charged ions.

    Science.gov (United States)

    Tan, Joseph N; Brewer, Samuel M; Guise, Nicholas D

    2012-02-01

    Penning traps are made extremely compact by embedding rare-earth permanent magnets in the electrode structure. Axially-oriented NdFeB magnets are used in unitary architectures that couple the electric and magnetic components into an integrated structure. We have constructed a two-magnet Penning trap with radial access to enable the use of laser or atomic beams, as well as the collection of light. An experimental apparatus equipped with ion optics is installed at the NIST electron beam ion trap (EBIT) facility, constrained to fit within 1 meter at the end of a horizontal beamline for transporting highly charged ions. Highly charged ions of neon and argon, extracted with initial energies up to 4000 eV per unit charge, are captured and stored to study the confinement properties of a one-magnet trap and a two-magnet trap. Design considerations and some test results are discussed.

  2. Penning traps with unitary architecture for storage of highly charged ions

    International Nuclear Information System (INIS)

    Tan, Joseph N.; Guise, Nicholas D.; Brewer, Samuel M.

    2012-01-01

    Penning traps are made extremely compact by embedding rare-earth permanent magnets in the electrode structure. Axially-oriented NdFeB magnets are used in unitary architectures that couple the electric and magnetic components into an integrated structure. We have constructed a two-magnet Penning trap with radial access to enable the use of laser or atomic beams, as well as the collection of light. An experimental apparatus equipped with ion optics is installed at the NIST electron beam ion trap (EBIT) facility, constrained to fit within 1 meter at the end of a horizontal beamline for transporting highly charged ions. Highly charged ions of neon and argon, extracted with initial energies up to 4000 eV per unit charge, are captured and stored to study the confinement properties of a one-magnet trap and a two-magnet trap. Design considerations and some test results are discussed.

  3. Electron Cooling of Protons in a Nested Penning Trap

    International Nuclear Information System (INIS)

    Hall, D.S.; Gabrielse, G.

    1996-01-01

    Trapped protons cool via collisions with trapped electrons at 4 K.This first demonstration of sympathetic cooling by trapped species of opposite sign of charge utilizes a nested Penning trap. The demonstrated interaction of electrons and protons at very low relative velocities, where recombination is predicted to be most rapid, indicates that this may be a route towards the study of low temperature recombination. The production of cold antihydrogen is of particular interest, and electron cooling of highly stripped ions may also be possible. copyright 1996 The American Physical Society

  4. High-precision mass measurements in the realm of the deformed shell closure N=152

    Energy Technology Data Exchange (ETDEWEB)

    Eibach, Martin Andreas

    2013-12-04

    The nuclear masses reflect the sum of all interactions inside a nucleus. Their precise knowledge can be used to benchmark nuclear mass models and to gain nuclear structure information. Penning-trap mass spectrometers have proven their potential to obtain lowest uncertainties. Uniquely located at a nuclear reactor, the double Penning-trap mass spectrometer TRIGA-TRAP is dedicated to measurements in the neutron-rich region. For a gain in sensitivity a non-destructive detection system for single ion mass measurements was adopted. This includes the implementation of a narrow band-pass filter tuned to the heavy ion cyclotron frequency as well as a cryogenic low-noise amplifier. For on-line mass measurements, the laser ablation ion source was equipped with a newly developed miniature radiofrequency quadrupole trap in order to improve the extraction efficiency. A more economic use of the radioactive material enabled mass measurements using only 10{sup 15} atoms of target material. New mass measurements were performed within this work in the realm of the deformed shell closure N=152. Their implementation into the atomic-mass evaluation improved the uncertainty of more than 80 nuclides in the heavy mass region and simultaneously shifted the absolute mass of two α decay chains.

  5. Trapping of positrons in a Penning Malmberg trap in the view of accumulating them with the use of a pulsed beam

    International Nuclear Information System (INIS)

    Dupre, P.

    2011-09-01

    The weak equivalence principle, a fundament of Einstein general relativity, states that gravitational mass and inertial mass are equal whatever the body. This equivalence principle has never been directly tested with antimatter. The GBAR (Gravitational Behaviour of Antimatter at Rest) experiment intends to test it by measuring the acceleration of ultra cold anti-hydrogens in free fall. The production of such anti-atoms requires a pulse of about 10 10 positrons in a few tens of nanoseconds. This thesis focuses on the development of a new accumulation technique of positrons in a Penning-Malmberg trap in order to create this pulse. This new method is an improvement of the accumulation technique of Oshima et al.. This technique requires a non-neutral electron plasma to cool down positrons in the trap in order to confine them. A continuous beam delivers positrons and the trapping efficiency is about 0.4%. The new method needs a positron pulsed beam and the method efficiency is estimated at 80%. A part of this thesis was performed at Riken (Tokyo) on the trap of Oshima et al. to study the behavior of non-neutral plasmas in this type of trap and the first accumulation method. A theoretical model was developed to simulate the positron trapping efficiency. The description and the systematic study of the new accumulation technique with a pulsed positron beam are presented. They includes notably the optimization through simulation of the electromagnetic configuration of the trap and of the parameters of the used non-neutral plasmas. (author)

  6. Precision Mass Measurement of Argon Isotopes

    CERN Multimedia

    Lunney, D

    2002-01-01

    % IS388\\\\ \\\\ A precision mass measurement of the neutron-deficient isotopes $^{32,33,34}$Ar is proposed. Mass values of these isotopes are of importance for: a) a stringent test of the Isobaric-Multiplet- Mass-Equation, b) a verification of the correctness of calculated charge-dependent corrections as used in super-allowed $\\beta$- decay studies aiming at a test of the CVC hypothesis, and c) the determination of the kinematics in electron-neutrino correlation experiments searching for scalar currents in weak interaction. The measurements will be carried out with the ISOLTRAP Penning trap mass spectrometer.

  7. First on-line mass measurements at SHIPTRAP and mass determinations of neutron-rich Fr and Ra isotopes at ISOLTRAP

    CERN Document Server

    Rahaman, Saidu

    SHIPTRAP is an ion trap facility behind the velocity filter SHIP at GSI/Darmstadt. Its aim are precision studies of transuranium nuclides produced in a fusion reaction and separated by SHIP. The current set-up for high-precision mass measurements consists of three main functional parts: (i) a gas cell for stopping the energetic ions from SHIP, (ii) radiofrequency quadrupole structures to cool and to bunch the ions extracted from the gas cell, and (iii) a superconducting magnet with two cylindrical Penning traps at a field strength of 7 T. In this work the Penning trap system has been installed and extensively characterized. The first on-line mass measurements of short-lived nuclides were carried out and the masses of $^{147}$Er and $^{148}$Er could be experimentally determined for the first time. Here a relative mass uncertainty of $\\delta$ m/m of about 1$\\times$ 10$^{-6}$ was achieved. Furthermore the masses of heavy neutron-rich $^{229-232}$Ra and $^{230}$Fr isotopes have been determined with a relative m...

  8. Penning-trap mass spectrometry and mean-field study of nuclear shape coexistence in the neutron-deficient lead region

    Science.gov (United States)

    Manea, V.; Ascher, P.; Atanasov, D.; Barzakh, A. E.; Beck, D.; Blaum, K.; Borgmann, Ch.; Breitenfeldt, M.; Cakirli, R. B.; Cocolios, T. E.; Day Goodacre, T.; Fedorov, D. V.; Fedosseev, V. N.; George, S.; Herfurth, F.; Kowalska, M.; Kreim, S.; Litvinov, Yu. A.; Lunney, D.; Marsh, B.; Neidherr, D.; Rosenbusch, M.; Rossel, R. E.; Rothe, S.; Schweikhard, L.; Wienholtz, F.; Wolf, R. N.; Zuber, K.

    2017-05-01

    We present a study of nuclear shape coexistence in the region of neutron-deficient lead isotopes. The midshell gold isotopes 180,185,188,190Au (Z =79 ), the two long-lived nuclear states in 197At (Z =85 ), and the neutron-rich nuclide 219At were produced by the ISOLDE facility at CERN and their masses were determined with the high-precision Penning-trap mass spectrometer ISOLTRAP. The studied gold isotopes address the trend of binding energies in a region of the nuclear chart where the nuclear charge radii show pronounced discontinuities. Significant deviations from the atomic-mass evaluation were found for Au,190188. The new trend of two-neutron separation energies is smoother, although it does reveal the onset of deformation. The origin of this effect is interpreted in connection to the odd-even staggering of binding energies, as well as theoretically by Hartree-Fock-Bogoliubov calculations including quasiparticle blocking. The role of blocking for reproducing the large odd-even staggering of charge radii in the mercury isotopic chain is illustrated.

  9. Collimated-hole structures as efficient differential pumping barrier, one-way valve and tool for aligning Penning traps

    International Nuclear Information System (INIS)

    Kluge, H.-Jürgen; Block, Michael; Herfurth, Frank

    2011-01-01

    A collimated-hole structure consists of a very large number of parallel channels which have each a very small diameter and are closely packed together. Such devices, installed in vacuum systems allow one to separate regions of very different gas pressures. A collimated-hole structure has high transmission for a directed ion beam with low emittance but a very low conductance for rest gas atoms or molecules exhibiting random walk. Therefore it is proposed to use such a structure as one-way valve and/or efficient differential pumping barrier in set-ups using Penning traps. Furthermore, these devices might be very useful to align the axis of a Penning trap with the direction of the magnetic field lines which is essential to avoid systematic uncertainties in high-accuracy mass spectroscopy.

  10. Mass measurements on neutron-deficient nuclides at SHIPTRAP and commissioning of a cryogenic narrow-band FT-ICR mass spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Ferrer Garcia, R.

    2007-07-01

    The dissertation presented here deals with high-precision Penning trap mass spectrometry on short-lived radionuclides. Owed to the ability of revealing all nucleonic interactions, mass measurements far off the line of {beta}-stability are expected to bring new insight to the current knowledge of nuclear properties and serve to test the predictive power of mass models and formulas. In nuclear astrophysics, atomic masses are fundamental parameters for the understanding of the synthesis of nuclei in the stellar environments. This thesis presents ten mass values of radionuclides around A=90 interspersed in the predicted rp-process pathway. Six of them have been experimentally determined for the first time. The measurements have been carried out at the Penning-trap mass spectrometer SHIPTRAP using the destructive time-of-flight ion-cyclotron-resonance (TOF-ICR) detection technique. Given the limited performance of the TOF-ICR detection when trying to investigate heavy/superheavy species with small production cross sections ({sigma} <1 {mu}b), a new detection system is found to be necessary. Thus, the second part of this thesis deals with the commissioning of a cryogenic double-Penning trap system for the application of a highly-sensitive, narrow-band Fourier-transform ion-cyclotron-resonance (FT-ICR) detection technique. With the non-destructive FT-ICR detection method a single singly-charged trapped ion will provide the required information to determine its mass. First off-line tests of a new detector system based on a channeltron with an attached conversion dynode, of a cryogenic pumping barrier, to guarantee ultra-high vacuum conditions during mass determination, and of the detection electronics for the required single-ion sensitivity are reported. (orig.)

  11. WITCH, a Penning trap for weak interaction studies

    CERN Document Server

    Kozlov, V Yu

    2005-01-01

    This work is the completion of the installation of the WITCH set-up and the first tests and commissioning of it. The first goal of the WITCH experiment is to improve the present limit on a scalar interaction in nuclear $\\beta$-decay by determining the $\\beta$-neutrino angular correlation parameter $a$ via a precise measurement of the shape of the energy spectrum of the recoil ions. The development of the WITCH set-up and its installation at ISOLDE (CERN) were recently completed. The principle of WITCH is based on a combination of a Penning trap to confine the radioactive ions and a retardation spectrometer to probe the energy of the recoil ions resulting from $\\beta$-decays in the trap. Extensive computer simulations show that for a reasonable measurement time a precision on the $a$-parameter of 0.5% can be achieved. This corresponds to an upper limit for the scalar interaction constant Cs/Cv < 9% at 95% C.L. Designing and constructing a set-up as large and complex as the WITCH set-up takes time, several y...

  12. Dynamics of a single ion in a perturbed Penning trap: Octupolar perturbation

    International Nuclear Information System (INIS)

    Lara, Martin; Salas, J. Pablo

    2004-01-01

    Imperfections in the design or implementation of Penning traps may give rise to electrostatic perturbations that introduce nonlinearities in the dynamics. In this paper we investigate, from the point of view of classical mechanics, the dynamics of a single ion trapped in a Penning trap perturbed by an octupolar perturbation. Because of the axial symmetry of the problem, the system has two degrees of freedom. Hence, this model is ideal to be managed by numerical techniques like continuation of families of periodic orbits and Poincare surfaces of section. We find that, through the variation of the two parameters controlling the dynamics, several periodic orbits emanate from two fundamental periodic orbits. This process produces important changes (bifurcations) in the phase space structure leading to chaotic behavior

  13. Direct mass measurements of neutron-deficient xenon isotopes using the ISOLTRAP mass spectrometer

    CERN Document Server

    Dilling, J; Beck, D; Bollen, G; Herfurth, F; Kellerbauer, A G; Kluge, H J; Moore, R B; Scheidenberger, C; Schwarz, S; Sikler, G

    2004-01-01

    The masses of the noble-gas Xe isotopes with 114 $\\leq$ A $\\leq$ 123 have been directly measured for the first time. The experiments were carried out with the ISOLTRAP triple trap spectrometer at the online mass separator ISOLDE/CERN. A mass resolving power of the Penning trap spectrometer of $m/\\Delta m$ of close to a million was chosen resulting in an accuracy of $\\delta m \\leq 13$ keV for all investigated isotopes. Conflicts with existing, indirectly obtained, mass data by several standard deviations were found and are discussed. An atomic mass evaluation has been performed and the results are compared to information from laser spectroscopy experiments and to recent calculations employing an interacting boson model.

  14. Dependence of the confinement time of an electron plasma on the magnetic field in a quadrupole Penning trap

    Energy Technology Data Exchange (ETDEWEB)

    Dyavappa, B.M.; Datar, Durgesh; Prakash; Ananthamurthy, Sharath [Bangalore University, Department of Physics, Bangalore (India)

    2017-12-15

    A quadrupole Penning trap is used to confine electrons in weak magnetic fields. Perturbations due to space charge and imperfections in the trap geometry, as well as collisions with the background gas molecules, lead to loss of the electrons from the trap. We present in this work the results on measurements of the electron confinement time and its dependence on the magnetic field in a quadrupolar Penning trap. We describe a method to measure the confinement time of an electron cloud under weak magnetic fields (0.01 T - 0.1 T). This time is found to scale as τ ∝ B{sup 1.41} in variance with the theoretically expected confinement time that scales as τ ∝ B{sup 2} for trapped electrons that are lost through collisions with the neutrals present in the trap. A measurement of the expansion rate of the electron plasma in the trap through controlled variation of the trap voltage, yields expansion times that depend on the energy of escaping electrons. This is found to vary in our case in the scaling range B{sup 0.32} to B{sup 0.43}. Distorting the geometry of the trap, results in a marked change in the confinement time's dependence on the magnetic field. The results indicate that the confinement time of the electron cloud in the trap is limited by both, effects of collisions and perturbations that result in the plasma loss through expansion in the trap. (orig.)

  15. Time-separated oscillatory fields for high-precision mass measurements on short-lived Al and Ca nuclides

    CERN Document Server

    George, Simon; Blank, B.; Blaum, K.; Breitenfeldt, M.; Hager, U.; Herfurth, F.; Herlert, A.; Kellerbauer, A.; Kluge, H.J.; Kretzschmar, M.; Lunney, D.; Savreux, R.; Schwarz, Andreas S.; Schweikhard, L.; Yazidjian, C.

    2008-01-01

    High-precision Penning trap mass measurements on the stable nuclide $^{27}$Al as well as on the short-lived radionuclides $^{26}$Al and $^{38,39}$Ca have been performed by use of radio-frequency excitation with time-separated oscillatory fields, i.e. Ramsey's method, as recently introduced for the excitation of the ion motion in a Penning trap, was applied. A comparison with the conventional method of a single continuous excitation demonstrates its advantage of up to ten times shorter measurements. The new mass values of $^{26,27}$Al clarify conflicting data in this specific mass region. In addition, the resulting mass values of the superallowed $\\beta$-emitter $^{38}$Ca as well as of the groundstate of the $\\beta$-emitter $^{26}$Al$^{m}$ confirm previous measurements and corresponding theoretical corrections of the ft-values.

  16. Design of a high field uniformity electromagnet for Penning trap

    International Nuclear Information System (INIS)

    Itteera, Janvin; Singh, Kumud; Teotia, Vikas; Ukarde, Priti; Malhotra, Sanjay; Taly, Y.K.; Joshi, Manoj; Rao, Pushpa

    2013-01-01

    An ion trap (Penning trap) facility is being developed at BARC for spectroscopy studies. This requires the design of an iron core electromagnet capable of generating high magnetic fields (∼1.7T) at the centre of an 88 mm long air gap. This electromagnet provides the requisite dipole magnetic field which when superimposed on the electrostatic quadrupoles ensures a stable trapping of ions. To conduct high precision spectroscopy studies, we need to ensure a high degree of magnetic field uniformity ( 3 volume (Trap zone). Various pole shoe profiles were studied and modelled, FEM simulation of the same were conducted to compute the magnetic field intensity and field uniformity. Owing to the large air gap and requirement of high field intensity in the GFR, the exciting coils need to handle high current densities, which require water cooled systems. Double Pan-Cake coil design is selected for powering the magnet. Electrical, thermal and hydraulic designs of the coils are completed and a prototype double pancake coil was fabricated and tested for verifying the electrical and thermal parameter. The spatial field homogeneity is achieved by shimming the pole tip. Temporal stability of magnet requires a highly stable power supply for exciting the coils and its stability class is derived from FEM simulations. This paper discusses the electromagnetic design and development of the penning trap magnet being developed at BARC. (author)

  17. High Precision Atomic Mass Measurements: Tests of CVC and IMME

    International Nuclear Information System (INIS)

    Eronen, Tommi

    2011-01-01

    Atomic mass is one of the key ingredients in testing the Conserved Vector Current (CVC) hypothesis and Isobaric Mass Multiplet Equation (IMME). With JYFLTRAP Penning trap installation at the University of Jyvaeskylae, Finland, several atomic massses related to these studies have been measured. The performed atomic mass measurements for CVC tests cover almost all the nuclei that are relevant for these studies. To test IMME, masses in two isobaric mass chains (A = 23 and A = 32) have been determined.

  18. High Precision Atomic Mass Measurements: Tests of CVC and IMME

    Energy Technology Data Exchange (ETDEWEB)

    Eronen, Tommi [Department of Physics, University of Jyvaeskylae, FI-40014 University of Jyvaeskylae (Finland); Collaboration: JYFLTRAP Collaboration

    2011-11-30

    Atomic mass is one of the key ingredients in testing the Conserved Vector Current (CVC) hypothesis and Isobaric Mass Multiplet Equation (IMME). With JYFLTRAP Penning trap installation at the University of Jyvaeskylae, Finland, several atomic massses related to these studies have been measured. The performed atomic mass measurements for CVC tests cover almost all the nuclei that are relevant for these studies. To test IMME, masses in two isobaric mass chains (A = 23 and A = 32) have been determined.

  19. Precision mass measurements for studies of nucleosynthesis via the rapid neutron-capture process. Penning-trap mass measurements of neutron-rich cadmium and caesium isotopes

    Energy Technology Data Exchange (ETDEWEB)

    Atanasov, Dinko

    2016-07-06

    Although the theory for the rapid neutron-capture process (r-process) was developed more than 55 years ago, the astrophysical site is still under a debate. Theoretical studies predict that the r-process path proceeds through very neutron-rich nuclei with very asymmetric proton-to-neutron ratios. Knowledge about the properties of neutron-rich isotopes found in similar regions of the nuclear chart and furthermore suitable for r-process studies is still little or even not existing. The basic nuclear properties such as binding energies, half-lives, neutron-induced or neutron-capture reaction cross-sections, play an important role in theoretical simulations and can vary or even drastically alternate results of these studies. Therefore, a considerable effort was put forward to access neutron-rich isotopes at radioactive ion-beam facilities like ISOLDE at CERN. The goal of this PhD thesis is to describe the experimental work done for the precision mass measurements of neutron-rich cadmium ({sup 129-131}Cd) and caesium ({sup 132,146-148}Cs) isotopes. Measurements were done at the on-line radioactive ion-beam facility ISOLDE by using the four-trap mass spectrometer ISOLTRAP. The cadmium isotopes are key nuclides for the synthesis of stable isotopes around the mass peak A = 130 in the Solar System abundance.

  20. Accurate mass measurements on neutron-deficient krypton isotopes

    CERN Document Server

    Rodríguez, D.; Äystö, J.; Beck, D.; Blaum, K.; Bollen, G.; Herfurth, F.; Jokinen, A.; Kellerbauer, A.; Kluge, H.-J.; Kolhinen, V.S.; Oinonen, M.; Sauvan, E.; Schwarz, S.

    2006-01-01

    The masses of $^{72–78,80,82,86}$Kr were measured directly with the ISOLTRAP Penning trap mass spectrometer at ISOLDE/CERN. For all these nuclides, the measurements yielded mass uncertainties below 10 keV. The ISOLTRAP mass values for $^{72–75}$Kr being more precise than the previous results obtained by means of other techniques, and thus completely determine the new values in the Atomic-Mass Evaluation. Besides the interest of these masses for nuclear astrophysics, nuclear structure studies, and Standard Model tests, these results constitute a valuable and accurate input to improve mass models. In this paper, we present the mass measurements and discuss the mass evaluation for these Kr isotopes.

  1. Accurate mass measurements of very short-lived nuclei. Prerequisites for high-accuracy investigations of superallowed β-decays

    International Nuclear Information System (INIS)

    Herfurth, F.; Kellerbauer, A.; Sauvan, E.; Ames, F.; Engels, O.; Audi, G.; Lunney, D.; Beck, D.; Blaum, K.; Kluge, H.J.; Scheidenberger, C.; Sikler, G.; Weber, C.; Bollen, G.; Schwarz, S.; Moore, R.B.; Oinonen, M.

    2002-01-01

    Mass measurements of 34 Ar, 73-78 Kr, and 74,76 Rb were performed with the Penning-trap mass spectrometer ISOLTRAP. Very accurate Q EC -values are needed for the investigations of the Ft-value of 0 + → 0 + nuclear β-decays used to test the standard model predictions for weak interactions. The necessary accuracy on the Q EC -value requires the mass of mother and daughter nuclei to be measured with δm/m ≤ 3 . 10 -8 . For most of the measured nuclides presented here this has been reached. The 34 Ar mass has been measured with a relative accuracy of 1.1 .10 -8 . The Q EC -value of the 34 Ar 0 + → 0 + decay can now be determined with an uncertainty of about 0.01%. Furthermore, 74 Rb is the shortest-lived nuclide ever investigated in a Penning trap. (orig.)

  2. High-voltage switching for in-flight capture of keV antiprotons in a Penning trap

    International Nuclear Information System (INIS)

    Fei, X.; Davisson, R.; Gabrielse, G.

    1987-01-01

    The recently observed in-flight capture of keV antiprotons and protons in a Penning trap requires that the -3-kV potentials on electrodes of a Penning trap near 4.2 K be switched on and off with switching times less than 20 ns. These rapidly switched potentials are applied via transmission lines which are not terminated at the trap, thereby avoiding unacceptable heat load on the helium Dewar. Simple high-voltage switching circuits are constructed using krytrons and reed relays. A krytron provides the rapid switching and stays on just long enough for a reed relay to kick in and maintain the switched state indefinitely

  3. Precise atomic mass measurements by deflection mass spectrometry

    CERN Document Server

    Barber, R C

    2003-01-01

    Since its inception nearly 90 years ago by J.J. Thomson, the precise determination of atomic masses by the classical technique of deflecting charged particles in electric and magnetic fields has provided a large body of data on naturally occurring nuclides. Currently, such measurements on stable nuclides have frequently achieved a precision of better than two parts in 10 sup 9 of the mass. A review of the technique, together with a brief summary of the important historical developments in the field of precise atomic mass measurements, will be given. The more recent contributions to this field by the deflection mass spectrometer at the University of Manitoba will be provided as illustrations of the culmination of the techniques used and the applications that have been studied. A brief comparison between this and newer techniques using Penning traps will be presented.

  4. In situ electromagnetic field diagnostics with an electron plasma in a Penning-Malmberg trap

    CERN Document Server

    Amole, C; Baquero-Ruiz, M.; Bertsche, W.; Butler, E.; Capra, A.; Cesar, C.L.; Charlton, M.; Deller, A.; Evetts, N.; Eriksson, S.; Fajans, J.; Friesen, T.; Fujiwara, M.C.; Gill, D.R.; Gutierrez, A.; Hangst, J.S.; Hardy, W.N.; Hayden, M.E.; Isaac, C.A.; Jonsell, S.; Kurchaninov, L.; Little, A.; Madsen, N.; McKenna, J.T.K.; Menary, S.; Napoli, S.C.; Olchanski, K.; Olin, A.; Pusa, P.; Rasmussen, C.; Robicheaux, F.; Sarid, E.; Silveira, D.M.; So, C.; Stracka, S.; Tharp, T.; Thompson, R.I.; van der Werf, D.P.; Wurtele, J.S.

    2014-01-01

    We demonstrate a novel detection method for the cyclotron resonance frequency of an electron plasma in a Penning-Malmberg trap. With this technique, the electron plasma is used as an in situ diagnostic tool for measurement of the static magnetic field and the microwave electric field in the trap. The cyclotron motion of the electron plasma is excited by microwave radiation and the temperature change of the plasma is measured non-destructively by monitoring the plasma's quadrupole mode frequency. The spatially-resolved microwave electric field strength can be inferred from the plasma temperature change and the magnetic field is found through the cyclotron resonance frequency. These measurements were used extensively in the recently reported demonstration of resonant quantum interactions with antihydrogen.

  5. Nested Penning Trap as a Source of Singly Charged Ions

    International Nuclear Information System (INIS)

    Ordonez, C.A.

    2003-01-01

    In the work reported, the possibility of using a nested Penning trap as a high purity source of low-charge-state ions is studied. For the configuration considered, a relatively dense ion plasma is confined by a three-dimensional electric potential well. The three-dimensional well is produced by the electric field generated by both the trap electrodes and a trapped electron plasma. The ion and electron plasmas are each considered to have Maxwellian velocity distributions. However, it is shown that the electron plasma must have a temperature that is higher than that of the ion plasma when the ions have low charge states. The work reported includes a self-consistent prediction of a possible plasma equilibrium

  6. Investigation of the proton-neutron interaction by high-precision nuclear mass measurements

    CERN Multimedia

    Savreux, R P; Akkus, B

    2007-01-01

    We propose to measure the atomic masses of a series of short-lived nuclides, including $^{70}$Ni, $^{122-130}$Cd, $^{134}$Sn, $^{138,140}$Xe, $^{207-210}$Hg, and $^{223-225}$Rn, that contribute to the investigation of the proton-neutron interaction and its role in nuclear structure. The high-precision mass measurements are planned for the Penning trap mass spectrometer ISOLTRAP that reaches the required precision of 10 keV in the nuclear mass determination.

  7. Quantum simulation of the integer factorization problem: Bell states in a Penning trap

    Science.gov (United States)

    Rosales, Jose Luis; Martin, Vicente

    2018-03-01

    The arithmetic problem of factoring an integer N can be translated into the physics of a quantum device, a result that supports Pólya's and Hilbert's conjecture to demonstrate Riemann's hypothesis. The energies of this system, being univocally related to the factors of N , are the eigenvalues of a bounded Hamiltonian. Here we solve the quantum conditions and show that the histogram of the discrete energies, provided by the spectrum of the system, should be interpreted in number theory as the relative probability for a prime to be a factor candidate of N . This is equivalent to a quantum sieve that is shown to require only o (ln√{N}) 3 energy measurements to solve the problem, recovering Shor's complexity result. Hence the outcome can be seen as a probability map that a pair of primes solve the given factorization problem. Furthermore, we show that a possible embodiment of this quantum simulator corresponds to two entangled particles in a Penning trap. The possibility to build the simulator experimentally is studied in detail. The results show that factoring numbers, many orders of magnitude larger than those computed with experimentally available quantum computers, is achievable using typical parameters in Penning traps.

  8. TAMU-TRAP facility - program for the study of fundamental weak interaction

    International Nuclear Information System (INIS)

    Shidling, P.D.; Mehlman, M.; Melconian, Dan; Fenker, Ben; Behling, R.S.

    2012-01-01

    Primary goal of the TAMU-TRAP facility is to test the Standard Model (SM) for a possible admixture of a scalar (S) or tensor (T) type of interaction in T = 2 superallowed β-delayed proton emitters. This information will be inferred from the shape of the proton energy spectrum. The main component of the facility are an RFQ cooler/buncher for cooling and bunching the ions, a Penning trap system with two cylindrical Penning traps. Additional goals for this system are mass measurements, lifetime measurements, and ft-values. A brief overview of the TAMU-TRAP set-up and T-REX upgrade facility will be presented. (author)

  9. First observation of spin flips with a single proton stored in a cryogenic Penning trap

    International Nuclear Information System (INIS)

    Ulmer, Stefan

    2011-01-01

    In this thesis the very first observation of spin transitions of a single proton stored in a cryogenic double-Penning trap is presented. The experimental observation of spin transitions is based on the continuous Stern-Gerlach effect, which couples the spin of the single trapped proton to its axial eigenfrequency, by means of an inhomogeneous magnetic field. A spin transition causes a change of the axial frequency, which can be measured non-destructively. Due to the tiny magnetic moment of the proton, the direct detection of proton spin-flips is an exceeding challenge. To achieve spin-flip resolution, the proton was stored in the largest magnetic field inhomogeneity, which has ever been superimposed to a Penning trap, and its axial frequency was detected non-destructively. Therefore, superconducting detection systems with ultrahigh-sensitivity were developed, allowing the direct observation of the single trapped proton, as well as the high-precision determination of its eigenfrequencies. Based on novel experimental methods, which were developed in the framework of this thesis, the axial frequency of the particle was stabilized to a level, where the observation of single-proton spin-flips is possible, which was demonstrated. This experimental success is one of the most important steps towards the high-precision determination of the magnetic moment of the free proton. With the very first observation of spin transitions with a single trapped proton, a highly exciting perspective opens. All experimental techniques which were developed in this thesis can be directly applied to the antiproton. Thus, the first high-precision measurement of the magnetic moment of the antiproton becomes possible. This will provide a new high-precision test of the matterantimatter symmetry. (orig.)

  10. A measurement of the neutron lifetime by counting trapped protons

    CERN Document Server

    Snow, W M; Dewey, M S; Fei, X; Gilliam, D M; Greene, G L; Nico, J S; Wietfeldt, F E

    2000-01-01

    A measurement of the neutron lifetime tau sub n performed by trapping and counting decay protons from in-beam neutron decays in a Penning trap is in progress at the National Institute of Standards and Technology (NIST). A description of the measurement technique, the status of the data analysis, and prospects for improvements in the measurement are discussed.

  11. High-accuracy mass measurements of neutron-rich Kr isotopes

    CERN Document Server

    Delahaye, P; Blaum, K; Carrel, F; George, S; Herfurth, F; Herlert, A; Kellerbauer, A G; Kluge, H J; Lunney, D; Schweikhard, L; Yazidjian, C

    2006-01-01

    The atomic masses of the neutron-rich krypton isotopes 84,86-95Kr have been determined with the tandem Penning trap mass spectrometer ISOLTRAP with uncertainties ranging from 20 to 220 ppb. The masses of the short-lived isotopes 94Kr and 95Kr were measured for the first time. The masses of the radioactive nuclides 89Kr and 91Kr disagree by 4 and 6 standard deviations, respectively, from the present Atomic-Mass Evaluation database. The resulting modification of the mass surface with respect to the two-neutron separation energies as well as implications for mass models and stellar nucleosynthesis are discussed.

  12. Onsets of nuclear deformation from measurements with the Isoltrap mass spectrometer

    CERN Document Server

    Naimi, Sarah

    Mass measurements provide important information concerning nuclear structure. This work presents results from the pioneering Penning trap spectrometer ISOLTRAP at CERN-ISOLDE. High-precision mass measurements of neutron-rich manganese ($^{58−66}$Mn) and krypton isotopes ($^{96,97}$Kr) are presented, of which the $^{66}$Mn and $^{96,97}$Kr masses are measured for the first time. In particular, the mass of $^{97}$Kr was measured using the preparation trap and required the definition of a new fit function. In the case of the manganese isotopes, the N = 40 shell closure is addressed. The two-neutron-separation energies calculated from the new masses show no shell closure at N = 40 but give an estimation of the proton-neutron interaction (around 0.5 MeV) responsible for the increase of collectivity and nuclear deformation in this mass region. The new krypton masses show behavior in sharp contrast with heavier neighbors where sudden and intense deformation is present, interpreted as the establishment of a nuclea...

  13. Mass measurement on the rp-process waiting point {sup 72}Kr

    Energy Technology Data Exchange (ETDEWEB)

    Rodriguez, D. [Gesellschaft fuer Schwerionenforschung mbH, Darmstadt (Germany); Kolhinen, V.S. [Jyvaeskylae Univ. (Finland); Audi, G. [CSNSM-IN2P3-Centre National de la Recherche Scientifique (CNRS), 91 - Orsay (FR)] [and others

    2004-06-01

    The mass of one of the three major waiting points in the astrophysical rp-process {sup 72}Kr was measured for the first time with the Penning trap mass spectrometer ISOLTRAP. The measurement yielded a relative mass uncertainty of {delta}m/m=1.2 x 10{sup -7} ({delta}m=8 keV). Other Kr isotopes, also needed for astrophysical calculations, were measured with more than one order of magnitude improved accuracy. We use the ISOLTRAP masses of{sup 72-74}Kr to reanalyze the role of the {sup 72}Kr waiting point in the rp-process during X-ray bursts. (orig.)

  14. A Penning trap for advanced studies with particles in extreme laser fields

    International Nuclear Information System (INIS)

    Vogel, M.; Quint, W.; Paulus, G.G.; Stöhlker, Th.

    2012-01-01

    We present a Penning trap as a tool for advanced studies of particles in extreme laser fields. Particularly, trap-specific manipulation techniques allow control over the confined particles’ localization and spatial density by use of trap electrodes as ‘electrostatic tweezers’ and by application of a ‘rotating wall’, respectively. It is thereby possible to select and prepare well-defined ion ensembles and to optimize the laser–particle interaction. Non-destructive detection of reaction educts and products with up to single-ion sensitivity supports advanced studies by maintaining the products for further studies at extended confinement times of minutes and above. The trap features endcaps with conical openings for applications with strongly focused lasers. We show that such a modification of a cylindrical trap is possible while harmonicity and tunability are maintained.

  15. A Penning trap for advanced studies with particles in extreme laser fields

    Science.gov (United States)

    Vogel, M.; Quint, W.; Paulus, G. G.; Stöhlker, Th.

    2012-08-01

    We present a Penning trap as a tool for advanced studies of particles in extreme laser fields. Particularly, trap-specific manipulation techniques allow control over the confined particles' localization and spatial density by use of trap electrodes as 'electrostatic tweezers' and by application of a 'rotating wall', respectively. It is thereby possible to select and prepare well-defined ion ensembles and to optimize the laser-particle interaction. Non-destructive detection of reaction educts and products with up to single-ion sensitivity supports advanced studies by maintaining the products for further studies at extended confinement times of minutes and above. The trap features endcaps with conical openings for applications with strongly focused lasers. We show that such a modification of a cylindrical trap is possible while harmonicity and tunability are maintained.

  16. Mats and LaSpec: High-precision experiments using ion traps and lasers at Fair

    Energy Technology Data Exchange (ETDEWEB)

    Rodriguez, D.; Lallena, A.M.; Blaum, K.; Bohm, C.; Cakirli, R.B.; Crespo Lopez-Urrutia, J.R.; Eliseev, S.; Ketelaer, J.; Kreim, M.S.; Kowalska, M.; Litvinov, Y.A.; Nagy, S.; Neidherr, D.; Repp, J.; Roux, C.; Schabinger, B.; Ullrich, J.; Nortershauser, W.; Eberhardt, K.; Geppert, C.; Kramer, J.; Krieger, A.; Sanchez, R.; Ahammed, M.; Das, P.; Ray, A.; Algora, A.; Rubio, B.; Tain, J.L.; Audi, G.; Lunney, D.; Naimi, S.; Aysto, J.; Jokinen, A.; Kolhinen, V.; Moore, I.; Beck, D.; Block, M.; Geissel, H.; Heinz, S.; Herfurth, F.; Litvinov, Y.A.; Minaya-Ramirez, E.; Plab, W.R.; Quint, W.; Scheidenberger, C.; Winkler, M.; Bender, M.; Billowes, J.; Campbell, P.; Flanagan, K.T.; Schwarz, S.; Bollen, G.; Ferrer, R.; George, S.; Kester, O.; Brodeur, M.; Brunner, T.; Delheij, P.; Dilling, J.; Ettenauer, S.; Lapierre, A.; Bushaw, B.A.; Cano-Ott, D.; Martinez, T.; Cortes, G.; Gomez-Hornillos, M.B.; Dax, A.; Herlert, A.; Yordanov, D.; De, A.; Dickel, T.; Geissel, H.; Jesch, C.; Kuhl, T.; Petrick, M.; PlaB, W.R.; Scheidenberger, C.; Garcia-Ramos, J.E.; Gartzke, E.; Habs, D.; Szerypo, J.; Thirolf, P.G.; Weber, C.; Gusev, Y.; Nesterenko, D.; Novikov, Y.N.; Popov, A.; Seliverstov, M.; Vasiliev, A.; Vorobjev, G.; Heenen, P.H.; Marx, G.; Schweikhard, L.; Ziegler, F.; Hobein, M.; Schuch, R.; Solders, A.; Suhonen, M.; Huber, G.; Wendt, K.; Huyse, M.; Koudriavtsev, I.; Neyens, G.; Van Duppen, P.; Le Blanc, F.; Matos, M.; Reinhard, P.G.; Schneider, D.

    2010-05-15

    Nuclear ground state properties including mass, charge radii, spins and moments can be determined by applying atomic physics techniques such as Penning-trap based mass spectrometry and laser spectroscopy. The MATS and LaSpec setups at the low-energy beamline at FAIR will allow us to extend the knowledge of these properties further into the region far from stability. With MATS (Precision Measurements of very short-lived nuclei using an Advanced Trapping System for highly-charged ions) at FAIR we aim to apply several techniques to very short-lived radionuclides: High-accuracy mass measurements, in-trap conversion electron and alpha spectroscopy, and trap-assisted spectroscopy. The experimental setup of MATS is a unique combination of an electron beam ion trap for charge breeding, ion traps for beam preparation, and a high-precision Penning trap system for mass measurements and decay studies. For the mass measurements, MATS offers both a high accuracy and a high sensitivity. A relative mass uncertainty of 10{sup -9} can be reached by employing highly-charged ions and a non-destructive Fourier-Transform Ion-Cyclotron-Resonance (FT-ICR) detection technique on single stored ions. Decay studies in ion traps will become possible with MATS. Laser spectroscopy of radioactive isotopes and isomers is an efficient and model-independent approach for the determination of nuclear ground and isomeric state properties. Hyperfine structures and isotope shifts in electronic transitions exhibit readily accessible information on the nuclear spin, magnetic dipole and electric quadrupole moments as well as root-mean-square charge radii. The accuracy of laser-spectroscopic-determined nuclear properties is very high while requirements concerning production rates are moderate. This Technical Design Report describes a new Penning trap mass spectrometry setup as well as a number of complementary experimental devices for laser spectroscopy. Since MATS and LaSpec require high-quality low

  17. Mats and LaSpec: High-precision experiments using ion traps and lasers at Fair

    International Nuclear Information System (INIS)

    Rodriguez, D.; Lallena, A.M.; Blaum, K.; Bohm, C.; Cakirli, R.B.; Crespo Lopez-Urrutia, J.R.; Eliseev, S.; Ketelaer, J.; Kreim, M.S.; Kowalska, M.; Litvinov, Y.A.; Nagy, S.; Neidherr, D.; Repp, J.; Roux, C.; Schabinger, B.; Ullrich, J.; Nortershauser, W.; Eberhardt, K.; Geppert, C.; Kramer, J.; Krieger, A.; Sanchez, R.; Ahammed, M.; Das, P.; Ray, A.; Algora, A.; Rubio, B.; Tain, J.L.; Audi, G.; Lunney, D.; Naimi, S.; Aysto, J.; Jokinen, A.; Kolhinen, V.; Moore, I.; Beck, D.; Block, M.; Geissel, H.; Heinz, S.; Herfurth, F.; Litvinov, Y.A.; Minaya-Ramirez, E.; Plab, W.R.; Quint, W.; Scheidenberger, C.; Winkler, M.; Bender, M.; Billowes, J.; Campbell, P.; Flanagan, K.T.; Schwarz, S.; Bollen, G.; Ferrer, R.; George, S.; Kester, O.; Brodeur, M.; Brunner, T.; Delheij, P.; Dilling, J.; Ettenauer, S.; Lapierre, A.; Bushaw, B.A.; Cano-Ott, D.; Martinez, T.; Cortes, G.; Gomez-Hornillos, M.B.; Dax, A.; Herlert, A.; Yordanov, D.; De, A.; Dickel, T.; Geissel, H.; Jesch, C.; Kuhl, T.; Petrick, M.; PlaB, W.R.; Scheidenberger, C.; Garcia-Ramos, J.E.; Gartzke, E.; Habs, D.; Szerypo, J.; Thirolf, P.G.; Weber, C.; Gusev, Y.; Nesterenko, D.; Novikov, Y.N.; Popov, A.; Seliverstov, M.; Vasiliev, A.; Vorobjev, G.; Heenen, P.H.; Marx, G.; Schweikhard, L.; Ziegler, F.; Hobein, M.; Schuch, R.; Solders, A.; Suhonen, M.; Huber, G.; Wendt, K.; Huyse, M.; Koudriavtsev, I.; Neyens, G.; Van Duppen, P.; Le Blanc, F.; Matos, M.; Reinhard, P.G.; Schneider, D.

    2010-01-01

    Nuclear ground state properties including mass, charge radii, spins and moments can be determined by applying atomic physics techniques such as Penning-trap based mass spectrometry and laser spectroscopy. The MATS and LaSpec setups at the low-energy beamline at FAIR will allow us to extend the knowledge of these properties further into the region far from stability. With MATS (Precision Measurements of very short-lived nuclei using an Advanced Trapping System for highly-charged ions) at FAIR we aim to apply several techniques to very short-lived radionuclides: High-accuracy mass measurements, in-trap conversion electron and alpha spectroscopy, and trap-assisted spectroscopy. The experimental setup of MATS is a unique combination of an electron beam ion trap for charge breeding, ion traps for beam preparation, and a high-precision Penning trap system for mass measurements and decay studies. For the mass measurements, MATS offers both a high accuracy and a high sensitivity. A relative mass uncertainty of 10 -9 can be reached by employing highly-charged ions and a non-destructive Fourier-Transform Ion-Cyclotron-Resonance (FT-ICR) detection technique on single stored ions. Decay studies in ion traps will become possible with MATS. Laser spectroscopy of radioactive isotopes and isomers is an efficient and model-independent approach for the determination of nuclear ground and isomeric state properties. Hyperfine structures and isotope shifts in electronic transitions exhibit readily accessible information on the nuclear spin, magnetic dipole and electric quadrupole moments as well as root-mean-square charge radii. The accuracy of laser-spectroscopic-determined nuclear properties is very high while requirements concerning production rates are moderate. This Technical Design Report describes a new Penning trap mass spectrometry setup as well as a number of complementary experimental devices for laser spectroscopy. Since MATS and LaSpec require high-quality low-energy beams

  18. New Beta-delayed Neutron Measurements in the Light-mass Fission Group

    Energy Technology Data Exchange (ETDEWEB)

    Agramunt, J. [Instituto de Física Corpuscular, CSIC-Univ. Valencia, Apdo. Correos 22085, E-46071 Valencia (Spain); García, A.R. [Centro de Investigaciones Energéticas, Medioambientales y Tecnológicas, E-28040 Madrid (Spain); Algora, A. [Instituto de Física Corpuscular, CSIC-Univ. Valencia, Apdo. Correos 22085, E-46071 Valencia (Spain); Äystö, J. [University of Jyväskylä, FI-40014 Jyväskyä (Finland); Caballero-Folch, R.; Calviño, F. [Secció d' Enginyeria Nuclear, Universitat Politécnica de Catalunya, E-08028 Barcelona (Spain); Cano-Ott, D. [Centro de Investigaciones Energéticas, Medioambientales y Tecnológicas, E-28040 Madrid (Spain); Cortés, G. [Secció d' Enginyeria Nuclear, Universitat Politécnica de Catalunya, E-08028 Barcelona (Spain); Domingo-Pardo, C. [Instituto de Física Corpuscular, CSIC-Univ. Valencia, Apdo. Correos 22085, E-46071 Valencia (Spain); Eronen, T. [University of Jyväskylä, FI-40014 Jyväskyä (Finland); Gelletly, W. [Department of Physics, University of Surrey, Guildford GU2 7XH (United Kingdom); Gómez-Hornillos, M.B. [Secció d' Enginyeria Nuclear, Universitat Politécnica de Catalunya, E-08028 Barcelona (Spain); and others

    2014-06-15

    A new accurate determination of beta-delayed neutron emission probabilities from nuclei in the low mass region of the light fission group has been performed. The measurements were carried out using the BELEN 4π neutron counter at the IGISOL-JYFL mass separator in combination with a Penning trap. The new results significantly improve the uncertainties of neutron emission probabilities for {sup 91}Br, {sup 86}As, {sup 85}As, and {sup 85}Ge nuclei.

  19. Progress at THe-trap

    Energy Technology Data Exchange (ETDEWEB)

    Hoecker, Martin; Eronen, Tommi; Ketter, Jochen; Schuh, Marc; Streubel, Sebastian; Blaum, Klaus [Max-Planck-Institut fuer Kernphysik, Heidelberg (Germany); Van Dyck, Robert S. Jr. [Department of Physics, University of Washington, Seattle, WA 98195-1560 (United States)

    2014-07-01

    THe-Trap is a Penning-trap mass spectrometry experiment that is currently being set up to measure the atomic mass ratio of tritium and helium-3 with a relative uncertainty of 10{sup -11}. In 2013, the experiment's first high-precision mass ratio measurement was performed on the ions {sup 12}C{sup 4+} and {sup 16}O{sup 5+}. The carbon-12/oxygen-16 mass ratio is one of the most precisely determined mass ratios and serves as a benchmark for the experiment. This measurement reached a statistical uncertainty of 6.3 . 10{sup -11} and was limited by systematic frequency shifts due to too high motional amplitudes. In the following service cycle, the experiment was modified to address the shortcomings that were discovered in the 2013 ratio measurements. This talk summarizes the results of the 2013 measurements and introduces the upgrades to the experiment, including a new amplifier, a modified ion source, and an improved vacuum system.

  20. Capture, Electron-Cooling and Compression of Antiprotons in a Large Penning-Trap for Physics Experiments with an Ultra-Low Energy Extracted Antiproton Beam

    CERN Multimedia

    2002-01-01

    % PS200 \\\\ \\\\The availability of ultra-low energy antiprotons is a crucial ingredient for the execution of the gravity measurements PS200. We have developed a method to provide such low energy antiprotons based on a large Penning trap (the PS200 catching trap). This system can accept a fast-extracted pulse from LEAR, reduce the energy of the antiprotons in the pulse from 5.9~MeV to several tens of kilovolts using a degrading foil, and then capture the antiprotons in a large Penning trap. These antiprotons are cooled by electrons previously admitted to the trap and are collected in a small region at the center of the trap. We have demonstrated our capability to capture up to 1~million antiprotons from LEAR in a single shot, electron cool these antiprotons, and transfer up to 95\\% of them into the inner, harmonic region. A storage time in excess of 1 hour was observed. These results have been obtained with the cryogenic trap vacuum coupled to a room temperature vacuum at about l0$ ^- ^{1} ^0 $ Torr, which is an...

  1. Multiply-ionized atoms isolated at low energy in a unitary Penning trap

    International Nuclear Information System (INIS)

    Tan, Joseph N.; Hoogerheide, Shannon Fogwell; Guise, Nicholas D.; Brewer, Samuel M.

    2015-01-01

    Ions extracted from the EBIT at NIST are slowed and captured in a Penning trap that is made very compact (< 150 cm 3 ) by a unitary architecture [1]. Measurements after 1 ms of ion storage indicate that the isolated ions are distributed with 5.5(5) eV of energy spread, which is roughly 2 orders of magnitude lower than expected in the ion source, without implementing any active cooling [2]. Some experiments are discussed. One goal is to produce one-electron ions in high angular momentum states for studying optical transitions between Rydberg states that could potentially enable new tests of quantum electrodynamics (QED) and determinations of fundamental constants [3

  2. Conception of PIPERADE: A high-capacity Penning-trap mass separator for high isobaric contamination at DESIR

    Energy Technology Data Exchange (ETDEWEB)

    Minaya Ramirez, E., E-mail: minaya@ipno.in2p3.fr [Max-Planck-Institut für Kernphysik, 69117 Heidelberg (Germany); Alfaurt, P.; Aouadi, M.; Ascher, P.; Blank, B. [Centre d’Etudes Nucléaires de Bordeaux-Gradignan (France); Blaum, K. [Max-Planck-Institut für Kernphysik, 69117 Heidelberg (Germany); Cam, J.-F. [Laboratoire de Physique Corpusculaire, Caen (France); Chauveau, P. [Grand Accélérateur National d’Ions Lourds CEA/DSM-CNRS-IN2P3, Caen (France); Daudin, L. [Centre d’Etudes Nucléaires de Bordeaux-Gradignan (France); Delahaye, P. [Grand Accélérateur National d’Ions Lourds CEA/DSM-CNRS-IN2P3, Caen (France); Delalee, F. [Centre d’Etudes Nucléaires de Bordeaux-Gradignan (France); Dupré, P. [Centre de Sciences Nucléaires et de Sciences de la Matière, Orsay (France); El Abbeir, S.; Gerbaux, M.; Grévy, S.; Guérin, H. [Centre d’Etudes Nucléaires de Bordeaux-Gradignan (France); Lunney, D. [Centre de Sciences Nucléaires et de Sciences de la Matière, Orsay (France); Metz, F. [Max-Planck-Institut für Kernphysik, 69117 Heidelberg (Germany); Naimi, S. [Riken, 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Perrot, L. [Institut de Physique Nucléaire, Orsay (France); and others

    2016-06-01

    The DESIR (decay, excitation and storage of radioactive ions) facility at GANIL-SPIRAL2 will receive a large variety of exotic nuclei at low energy (up to 60 keV) with high intensities. However, the production methods of radioactive beams are non selective, limiting the purity of the beams of interest. Moreover, the high precision needed for nuclear structure and astrophysics studies using beta decay spectroscopy, laser spectroscopy and trap-based experiments at DESIR requires highly pure samples of exotic nuclei. The aim of the double-Pennig-trap mass separator PIPERADE is to deliver large and very pure samples of exotic nuclei to the different experiments in DESIR. New excitation schemes and a large inner diameter of the first trap will mitigate space charge effects to attempt trapping of up to 10{sup 5} ions per pulse. The purification cycle will be performed in a few milliseconds so that short-lived nuclei can be purified. To extract the nuclides of interest from the large amount of isobaric contaminants, a resolving power of 10{sup 5} is mandatory. Afterwards the ions of interest will be accumulated in the second trap until they constitute a sufficiently pure sample for the measurements. The status of the project is presented.

  3. Calcium Atom Trap for Atom Trap Mass Spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Ko, Kwang Hoon; Park, Hyun Min; Han, Jae Min; Kim, Taek Soo; Cha, Yong Ho; Lim, Gwon; Jeong, Do Young [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2012-05-15

    Trace isotope analysis has been an important role in science, archaeological dating, geology, biology and nuclear industry. Artificially produced fission products such as Sr-90, Cs-135 and Kr-85 can be released to the environment when nuclear accident occurs and the reprocessing factory operates. Thus, the analysis of them has been of interest in nuclear industry. But it is difficult to detect them due to low natural abundance less then 10-10. The ultra-trace radio isotopes have been analyzed by the radio-chemical method, accelerator mass spectrometer, and laser based method. The radiochemical method has been used in the nuclear industry. But this method has disadvantages of long measurement time for long lived radioisotopes and toxic chemical process for the purification. The accelerator mass spectrometer has high isotope selectivity, but the system is huge and it has the isobar effects. The laser based method, such as RIMS (Resonance Ionization Mass Spectrometry) is a basically isobar-effect free method. Recently, ATTA (Atom Trap Trace Analysis), one of the laser based method, has been successfully demonstrated sufficient isotope selectivity with small system size. It has been applied for the detection of Kr-81 and Kr-85. However, it is not suitable for real sample detection, because it requires steady atomic beam generation during detection and is not allowed simultaneous detection of other isotopes. Therefore, we proposed the coupled method of Atom Trap and Mass Spectrometer. It consists of three parts, neutral atom trap, ionization and mass spectrometer. In this paper, we present the demonstration of the magneto-optical trap of neutral calcium. We discuss the isotope selective characteristics of the MOT (Magneto Optical Trap) of calcium by the fluorescence measurement. In addition, the frequency stabilization of the trap beam will be presented

  4. Mass measurements of neutron-rich indium isotopes toward the N =82 shell closure

    Science.gov (United States)

    Babcock, C.; Klawitter, R.; Leistenschneider, E.; Lascar, D.; Barquest, B. R.; Finlay, A.; Foster, M.; Gallant, A. T.; Hunt, P.; Kootte, B.; Lan, Y.; Paul, S. F.; Phan, M. L.; Reiter, M. P.; Schultz, B.; Short, D.; Andreoiu, C.; Brodeur, M.; Dillmann, I.; Gwinner, G.; Kwiatkowski, A. A.; Leach, K. G.; Dilling, J.

    2018-02-01

    Precise mass measurements of the neutron-rich In-130125 isotopes have been performed with the TITAN Penning trap mass spectrometer. TITAN's electron beam ion trap was used to charge breed the ions to charge state q =13 + thus providing the necessary resolving power to measure not only the ground states but also isomeric states at each mass number. In this paper, the properties of the ground states are investigated through a series of mass differentials, highlighting trends in the indium isotopic chain as compared to its proton-magic neighbor, tin (Z =50 ). In addition, the energies of the indium isomers are presented. The (8-) level in 128In is found to be 78 keV lower than previously thought and the (21 /2- ) isomer in 127In is shown to be lower than the literature value by more than 150 keV.

  5. Recent improvements of ISOLTRAP Absolute mass measurements of exotic nuclides at $10^{-8}$ precision

    CERN Document Server

    Kellerbauer, A G

    2003-01-01

    In the past three years, the sensitivity and the performance of the Penning trap mass spectrometer ISOLTRAP have been enhanced significantly. These improvements, which range from technical developments to systematic studies of the various factors contributing to the uncertainty of the final mass result, now allow mass measurements of short-lived radionuclides with half-lives of less than 100 ms and with a precision of better than 10$^{-8}$. Using a newly developed carbon cluster ion source, ISOLTRAP can perform absolute mass measurements relative to the microscopic mass standard $^{12}$C. These developments are reviewed as pertaining to the extension of ISOLTRAP mass measurements to higher precision and shorter half-lives and to molecular mass measurements.

  6. Precision measurements with the multi-reflection time-of-flight mass spectrometer of ISOLTRAP at ISOLDE/CERN

    Energy Technology Data Exchange (ETDEWEB)

    Atanasov, Dinko; Ascher, Pauline; Borgmann, Christopher; Boehm, Christine; Eliseev, Sergey; Eronen, Tommi; George, Sebastian; Kisler, Dmitry; Naimi, Sarah [Max-Planck-Institut fuer Kernphysik, Saupfercheckweg 1, 69117 Heidelberg (Germany); Beck, Dietrich; Herfurth, Frank; Litvinov, Yuri; Minaya Ramirez, Enrique; Neidherr, Dennis [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, Planckstr. 1, 64291 Darmstadt (Germany); Breitenfeldt, Martin [Instituut voor Kern- en Stralingsfysica, Celestijnenlaan 200d - bus 2418, 3001 Heverlee (Belgium); Cakirli, Burcu [University of Istanbul, Department of Physics, 34134 Istanbul (Turkey); Cocolios, Thomas Elias [University of Manchester, Manchester (United Kingdom); Herlert, Alexander Josef [FAIR GmbH, Planckstr. 1, D-64291 Darmstadt (Germany); Kowalska, Magdalena [CERN, Geneva 23, 1211 Geneva (Switzerland); Kreim, Susanne [Max-Planck-Institut fuer Kernphysik, Saupfercheckweg 1, 69117 Heidelberg (Germany); CERN, Geneva 23, 1211 Geneva (Switzerland); Lunney, David; Manea, Vladimir [CSNSM-IN2P3-CNRS, 91405 Orsay Campus, Bat. 104, 108 (France); Rosenbusch, Marco; Schweikhard, Lutz; Wienholtz, Frank; Wolf, Robert [Ernst-Moritz-Arndt-Universitaet, Institut fuer Physik, Felix-Hausdorff-Str. 6, 17487 Greifswald (Germany); Stanja, Juliane; Zuber, Kai [Institut fuer Kern- und Teilchenphysik, Technische Universitaet Dresden, Zellescher Weg 19, 01069 Dresden (Germany)

    2014-07-01

    The masses of exotic nuclides are among the most important input parameters for modern nuclear theory and astrophysical models. At the high-precision Penning-trap mass spectrometer ISOLTRAP at ISOLDE/CERN, a multi-reflection time-of-flight mass spectrometer (MR-ToF-MS) in combination with a Bradbury-Nielsen gate (BNG) can be used to achieve high-resolution isobar purification with mass-resolving powers of 105 in a few tens of milliseconds. Furthermore, the MR-ToF device can be used as a spectrometer to determine the masses of nuclides with very low yields and short half-lives, where a Penning-trap mass measurement becomes impractical due to the lower transport efficiency and decay losses during the purification and measurement cycles. Recent cross-check experiments show that the MR-ToF MS allows mass measurements with uncertainties in the sub-ppm range. In a first application the mass measurements of the nuclides 53,54Ca was performed, delivered with production rates as low as 10/s and half-lives of only 90(6) ms. The nuclides serve as important benchmarks for testing modern chiral effective theory with realistic 3-body forces. The contribution presents the on-line mass spectrometer ISOLTRAP focusing on the new applications, which became possible after the implementation of the MR-ToF MS into the current setup. In particular, the mass measurements of the neutron-rich calcium isotopes up to A=54 are discussed. In addition, measurements of the isotonic potassium isotopes are reported.

  7. Measurement of the neutron lifetime by counting trapped protons

    International Nuclear Information System (INIS)

    Byrne, J.; Dawber, P.G.; Spain, J.A.; Williams, A.P.; Dewey, M.S.; Gilliam, D.M.; Greene, G.L.; Lamaze, G.P.; Scott, R.D.; Pauwels, J.; Eykens, R.; Lamberty, A.

    1990-01-01

    The neutron lifetime τ n has been measured by counting decay protons stored in a Penning trap whose magnetic axis coincided with a neutron-beam axis. The result of the measurement is τ n =893.6±5.3 s, which agrees well with the value predicted by precise measurements of the β-decay asymmetry parameter A and the standard model

  8. High-precision mass measurements of neutron-deficient Tl isotopes at ISOLTRAP and the development of an ultra-stable voltage source for the PENTATRAP experiment

    Energy Technology Data Exchange (ETDEWEB)

    Boehm, Christine

    2015-01-14

    Atomic masses and hence binding energies of nuclides are of great importance for studies of nuclear structure since they reflect all effective interactions in a nucleus. Within this thesis the masses of seven nuclides, namely {sup 194}Au, {sup 194}Hg, {sup 190,193,198}Tl and {sup 202,208}Pb, were determined at the Penning-trap mass spectrometer ISOLTRAP at ISOLDE/CERN. The thallium region in the chart of isotopes is of special interest due to the occurrence of nuclear structure effects like low-lying isomers, level inversion, shape coexistence and deformations. These effects are investigated by applying finite-difference mass formulas, such as the two-neutron separation energies or the so-called empirical pairing gaps. The second topic addressed within the present thesis is an ultra-stable voltage source, called StaReP (Stable Reference for Penning Trap Experiments), which was developed at the Max-Planck-Institut fuer Kernphysik. It is one of the key components of the high-precision mass spectrometer PENTATRAP, containing a tower of five Penning traps. A 25-channel voltage source with a relative stability of few 10{sup -8} over a period of 10 minutes in the range of 0 to -100V is mandatory for PENTATRAP aiming for mass measurements with relative mass uncertainties of ≤ 10{sup -11}. Mass values with such a high precision allow for stringent tests of quantum electrodynamics in strong electric fields, testing Einstein's mass-energy relation E = mc{sup 2} as well as measurements of decay energies (Q-values) with applications in neutrino physics.

  9. High-Precision Mass Measurements of Exotic Nuclei with the Triple-Trap Mass Spectrometer Isoltrap

    CERN Multimedia

    Blaum, K; Zuber, K T; Stanja, J

    2002-01-01

    The masses of close to 200 short-lived nuclides have already been measured with the mass spectrometer ISOLTRAP with a relative precision between 1$\\times$10$^{-7}$ and 1$\\times$10^{-8}$. The installatin of a radio-frequency quadrupole trap increased the overall efficiency by two orders of magnitude which is at present about 1%. In a recent upgrade, we installed a carbon cluster laser ion source, which will allow us to use carbon clusters as mass references for absolute mass measurements. Due to these improvements and the high reliability of ISOLTRAP we are now able to perform accurate high-precision mass measurements all over the nuclear chart. We propose therefore mass measurements on light, medium and heavy nuclides on both sides of the valley of stability in the coming four years. ISOLTRAP is presently the only instrument capable of the high precision required for many of the proposed studies.

  10. Mass measurements of 56-57Cr and the question of shell reincarnation at N = 32

    International Nuclear Information System (INIS)

    Guenaut, C; Audi, G; Beck, D

    2005-01-01

    Binding energies determined with high accuracy provide smooth derivatives of the mass surface for analysis of shell and pairing effects. Measurements with the Penning trap mass spectrometer ISOLTRAP at CERN-ISOLDE were made for 56-57 Cr for which an accuracy of 4 x 10 -8 was achieved. Analysis of the mass surface for the supposed new N = 32 shell closure rather indicates a sub-shell closure, but of a different nature than known cases such as 94 Sr

  11. Mass measurements of 56-57Cr and the question of shell reincarnation at N = 32

    Science.gov (United States)

    Guénaut, C.; Audi, G.; Beck, D.; Blaum, K.; Bollen, G.; Delahaye, P.; Herfurth, F.; Kellerbauer, A.; Kluge, H.-J.; Lunney, D.; Schwarz, S.; Schweikhard, L.; Yazidjian, C.

    2005-10-01

    Binding energies determined with high accuracy provide smooth derivatives of the mass surface for analysis of shell and pairing effects. Measurements with the Penning trap mass spectrometer ISOLTRAP at CERN-ISOLDE were made for 56-57Cr for which an accuracy of 4 × 10-8 was achieved. Analysis of the mass surface for the supposed new N = 32 shell closure rather indicates a sub-shell closure, but of a different nature than known cases such as 94Sr.

  12. Mass measurements of $^{56-57}$Cr and the question of shell reincarnation at $N = 32$

    CERN Document Server

    Guenaut, Celine; Beck, D; Blaum, Klaus; Bollen, Georg; Delahaye, P; Herfurth, F; Kellerbauer, A G; Kluge, H J; Lunney, M D; Schwarz, S; Schweikhard, L; Yazidjian, C

    2005-01-01

    Binding energies determined with high accuracy provide smooth derivatives of the mass surface for analysis of shell and pairing effects. Measurements with the Penning trap mass spectrometer ISOLTRAP at CERN-ISOLDE were made for $^{56-57}$Cr for which an accuracy of $4 \\times 10^{-8}$ was achieved. Analysis of the mass surface for the supposed new $N = 32$ shell closure rather indicates a sub-shell closure, but of a different nature than known cases such as $^{94}$Sr.

  13. Preparation and cooling of magnesium ion crystals for sympathetic cooling of highly charged ions in a Penning trap

    Energy Technology Data Exchange (ETDEWEB)

    Murboeck, Tobias

    2017-07-01

    important step towards the sympathetic cooling of highly charged ions (HCI) and paves the way to future investigations of HCI, which will enable a stringent test of bound-state quantum electrodynamics. For supply of HCI to the SpecTrap experiment, the HITRAP low-energy beamline - including the pulsed drift tubes for ion deceleration and the electron beam ion source - were commissioned. Ion bunches containing several tens of thousands of argon ions (Ar{sup 13+}) were transported to the SpecTrap Penning trap. These ion numbers are sufficient for future spectroscopy of the fine structure splitting in boron-like Ar{sup 13+}. In future experiments, the HCI shall be delivered by HITRAP and will possess large kinetic energies immediate after capture into the Penning trap, so that initial sympathetic cooling is not very efficient. Therefore, the SpecTrap Penning trap features axial resonators for pre-cooling of the HCI to the kelvin-regime by means of resistive cooling. An analytical model for resistive cooling of highly charged ions was developed in this work, which for the first time explained the measured resistive cooling signals of HCI given in literature. This model allows for a deeper understanding of the interaction between radial and axial degrees of freedom, it predicts the set of experimental parameters for optimum cooling, and it provides the time evolution of the HCI density and temperature during the cooling process.

  14. The Penning fusion experiment-ions

    International Nuclear Information System (INIS)

    Schauer, M. M.; Umstadter, K. R.; Barnes, D. C.

    1999-01-01

    The Penning fusion experiment (PFX) studies the feasibility of using a Penning trap as a fusion confinement device. Such use would require spatial and/or temporal compression of the plasma to overcome the Brillouin density limit imposed by the nonneutrality of Penning trap plasmas. In an earlier experiment, we achieved enhanced plasma density at the center of a pure, electron plasma confined in a hyperbolic, Penning trap by inducing spherically convergent flow in a nonthermal plasma. The goal of this work is to induce similar flow in a positive ion plasma confined in the virtual cathode provided by a spherical, uniform density electron plasma. This approach promises the greatest flexibility in operating with multi-species plasmas (e.g. D + /T + ) or implementing temporal compression schemes such as the Periodically Oscillating Plasma Sphere of Nebel and Barnes. Here, we report on our work to produce and diagnose the necessary electron plasma

  15. Mass measurements of {sup 56-57}Cr and the question of shell reincarnation at N = 32

    Energy Technology Data Exchange (ETDEWEB)

    Guenaut, C [CSNSM-IN2P3/CNRS, Universite de Paris Sud, 91405 Orsay (France); Audi, G [CSNSM-IN2P3/CNRS, Universite de Paris Sud, 91405 Orsay (France); Beck, D [GSI, Planckstrasse 1, 64291 Darmstadt (Germany)] [and others

    2005-10-01

    Binding energies determined with high accuracy provide smooth derivatives of the mass surface for analysis of shell and pairing effects. Measurements with the Penning trap mass spectrometer ISOLTRAP at CERN-ISOLDE were made for {sup 56-57}Cr for which an accuracy of 4 x 10{sup -8} was achieved. Analysis of the mass surface for the supposed new N = 32 shell closure rather indicates a sub-shell closure, but of a different nature than known cases such as {sup 94}Sr.

  16. Confinement in a cryogenic Penning trap of highest charge state ions from EBIT

    International Nuclear Information System (INIS)

    Schneider, D.

    1994-01-01

    The retrapping of highly charged Xe 44+ and Th 68+,72+ ions extracted from an open-quotes Electron Beam Ion Trapclose quotes (EBIT) is demonstrated after injection of the ions into RETRAP, a cryogenic Penning trap (up to 6 Tesla magnetic field) currently with an open cylinder design. Ion extraction in a short pulse (5-20 μsec) from EBIT, essential for efficient retrapping, is employed. The ions are slowed down upon entering a deceleration tube mounted above the trap within the magnetic field. The potential is then rapidly (100 ns) decreased, enabling low energy ions to enter the trap. Capture efficiencies up to 25% are observed via detection of the delayed ion release pulse with a detector below the trap. Signal voltages induced in a tuned circuit due to single and multiple ions have been observed by tuning the ion resonant axial oscillation frequencies for different ions. Results from transporting and retrapping of the ions, as well as their detection, are described and the trapping efficiency is discussed, The motivation for these studies is to cool the trapped very highly charged ions to low temperatures (< 4 K) in order to perform ultrahigh resolution precision spectroscopy, collision studies at ultra low energies and to observe phase transitions in Coulomb clusters of highly charged ions

  17. Seeking the purported magic number N= 32 with high-precision mass spectrometry

    CERN Multimedia

    Schweikhard, L C; Herfurth, F; Boehm, C; Manea, V; Blaum, K; Beck, D; Kowalska, M; Kreim, K D; Stanja, J; Audi, G; Rosenbusch, M; Wienholtz, F; Litvinov, Y

    Accounting for the appearance of new magic numbers represents an exacting test for nuclear models. Binding energies offer a clear signature for the presence (or disappearance) of shell closures. To determine the strength of the purported N = 32 shell closure, we propose using the Penning-trap spectrometer ISOLTRAP for mass measurements of N = 34 isotones $^{58}$Cr (Z = 24), $^{55}$Sc (Z = 21) and $^{54}$Ca (Z = 20), as well as the N = 32 isotones $^{53}$Sc and $^{52}$Ca. We also propose measuring the mass of $^{60}$Cr to test the shell model prediction of a new magic number at N = 34. In addition to the Penning-trap system at ISOLTRAP, we intend to use the newly commissioned multi-reflection time-of-flight mass separator, which enables direct mass measurements on nuclei with half-lives below 50 ms.

  18. Seeking the purported magic number N= 32 with high-precision mass spectrometry

    CERN Document Server

    Kreim, S; Blaum, K; Bohm, Ch; Borgmann, Ch; Breitenfeldt, M; Cakirli, R B; Herfurth, F; Kowalska, M; Litvinov, Y; Lunney, D; Manea, V; Naimi, S; Neidherr, D; Rosenbusch, M; Schweikhard, L; Stanja, J; Stora, Th; Wienholtz, F; Wolf, R N; Zuber, K

    2011-01-01

    Accounting for the appearance of new magic numbers represents an exacting test for nuclear models. Binding energies o er a clear signature for the presence (or dis- appearance) of shell closures. To determine the strength of the purported N = 32 shell closure, we propose using the Penning-trap spectrometer ISOLTRAP for mass measure- ments of N = 34 isotones 58 Cr ( Z = 24), 55 Sc ( Z = 21) and 54 Ca ( Z = 20), as well as the N = 32 isotones 53 Sc and 52 Ca. We also propose measuring the mass of 60 Cr to test the shell model prediction of a new magic number at N = 34. In addition to the Penning-trap system at ISOLTRAP, we intend to use the newly commissioned multi-re ection time-of- ight mass separator, which enables direct mass measurements on nuclei with half-lives below 50 ms.

  19. Mathematical Descriptions of Axially Varying Penning Traps for the Antimatter Experiment: gravity, Interferometry, and Spectroscopy

    CERN Document Server

    Stephanie, Brown

    2015-01-01

    Antimatter, though proposed in 1933, is still not well understood. AEgIS aims to study the interaction of antihydrogen with the earth's gravitational field. This information will add to our understanding of the matter-antimatter asymmetry present in our universe. This paper discusses a Penning-Malmberg with a magnetic mirror that will hold $C_{2}^{-}$ that will be used for sympathetic cooling of antiprotons before the antihydrogen is created. The trap, which is critical to the cooling process of the antihydrogen, can be characterized by the separatrix between trapped and untrapped particles. This paper applies analytical processes used to define the separatrix of pure electron plasmas to a molecular plasma. Our work is based on the desire conditions (density, particle number, field strength, trap size) of the high field region. The initial application of a semi-analytical method applied to our trap defines the trap potential difference at \\~ 0.6V. The separatrix is defined in both the high and low fiel...

  20. Masses of nuclei close to the dripline

    International Nuclear Information System (INIS)

    Herfurth, F.; Blaum, K.; Audi, G.; Lunney, D.; Beck, D.; Kluge, H.J.; Rodriguez, D.; Sikler, G.; Weber, C.; Bollen, G.; Schwarz, S.; Kellerbauer, A.

    2003-01-01

    Mass measurements of radioactive nuclides are one of the cornerstones of our understanding of the nucleus. The Penning trap spectrometer ISOLTRAP performs direct mass measurements far away from the valley of stability, as well as high-precision measurements of key nuclei to anchor long decay chains. Both schemes provide valuable information on the dripline itself and on nuclei in its close vicinity. (orig.)

  1. Electron cooling of highly charged ions in penning traps; Elektronenkuehlung hochgeladener Ionen in Penningfallen

    Energy Technology Data Exchange (ETDEWEB)

    Moellers, B.

    2007-02-08

    For many high precision experiments with highly charged ions in ion traps it is necessary to work with low energy ions. One possibility to slow ions down to a very low energy in a trap is electron cooling, a method, which is already successfully used in storage rings to produce ion beams with high phase space density. Fast ions and a cold electron plasma are inserted into a Penning trap. The ions lose their energy due to Coulomb interaction with the electrons while they cross the plasma, the electrons are heated. The cooling time is the time, which is needed to cool an ion from a given initial energy to a low final energy. To calculate cooling times it is necessary to solve coupled differential equations for the ion energy and electron temperature. In a Penning trap the strong external magnetic field constitutes a theoretical challenge, as it influences the energy loss of the ions in an electron plasma, which can no longer be calculated analytically. In former estimates of cooling times this influence is neglected. But simulations show a dramatic decrease of the energy loss in the presence of a strong magnetic field, so it is necessary to investigate the effect of the magnetic field on the cooling times. This work presents a model to calculate cooling times, which includes both the magnetic field and the trap geometry. In a first step a simplified model without the external trap potential is developed. The energy loss of the ions in the magnetized electron plasma is calculated by an analytic approximation, which requires a numerical solution of integrals. With this model the dependence of the cooling time on different parameters like electron and ion density, magnetic field and the angle between ion velocity and magnetic field is studied for fully ionized uranium. In addition the influence of the electron heating is discussed. Another important topic in this context is the recombination between ions and electrons. The simplified model for cooling times allows to

  2. Onsets of nuclear deformation from measurements with the Isoltrap mass spectrometer

    International Nuclear Information System (INIS)

    Naimi, S.

    2010-10-01

    Mass measurements provide important information concerning nuclear structure. This work presents results from the pioneering Penning trap spectrometer Isoltrap at CERN-Isolde. High-precision mass measurements of neutron-rich manganese ( 58 - 66 Mn) and krypton isotopes ( 96, 97 Kr) are presented, of which the 66 Mn and 96, 97 Kr masses are measured for the first time. In particular, the mass of 97 Kr was measured using the preparation trap and required the definition of a new fit function. In the case of the manganese isotopes, the N=40 shell closure is addressed. The two-neutron-separation energies calculated from the new masses show no shell closure at N=40 but give an estimation of the proton-neutron interaction (around 0.5 MeV) responsible for the increase of collectivity and nuclear deformation in this mass region. The new krypton masses show behavior in sharp contrast with heavier neighbors where sudden and intense deformation is present, interpreted as the establishment of a nuclear quantum shape/phase transition critical-point boundary. The new masses confirm findings from nuclear mean-square charge-radius measurements up to N=60 but are at variance with conclusions from recent gamma-ray spectroscopy. Another part of this work was the design of new decay spectroscopy system behind the Isoltrap mass spectrometer. The beam purity achievable with Isoltrap will allow decay studies with γ and β detection coupled to a tape-station. This system has been mounted and commissioned with the radioactive beam 80 Rb. (author)

  3. ATRAP - Progress Towards Trapped Antihydrogen

    International Nuclear Information System (INIS)

    Grzonka, D.; Goldenbaum, F.; Oelert, W.; Sefzick, T.; Zhang, Z.; Comeau, D.; Hessels, E.A.; Storry, C.H.; Gabrielse, G.; Larochelle, P.; Lesage, D.; Levitt, B.; Speck, A.; Haensch, T.W.; Pittner, H.; Walz, J.

    2005-01-01

    The ATRAP experiment at the CERN antiproton decelerator AD aims for a test of the CPT invariance by a high precision comparison of the 1s-2s transition in the hydrogen and the antihydrogen atom.Antihydrogen production is routinely operated at ATRAP and detailed studies have been performed in order to optimize the production efficiency of useful antihydrogen.For high precision measurements of atomic transitions cold antihydrogen in the ground state is required which must be trapped due to the low number of available antihydrogen atoms compared to the cold hydrogen beam used for hydrogen spectroscopy. To ensure a reasonable antihydrogen trapping efficiency a magnetic trap has to be superposed the nested Penning trap. First trapping tests of charged particles within a combined magnetic/Penning trap have started at ATRAP

  4. ATRAP Progress Towards Trapped Antihydrogen

    CERN Document Server

    Grzonka, D; Gabrielse, G; Goldenbaum, F; Hänsch, T W; Hessels, E A; Larochelle, P; Le Sage, D; Levitt, B; Oelert, W; Pittner, H; Sefzick, T; Speck, A; Storry, C H; Walz, J; Zhang, Z

    2005-01-01

    The ATRAP experiment at the CERN antiproton decelerator AD aims for a test of the CPT invariance by a high precision comparison of the 1s‐2s transition in the hydrogen and the antihydrogen atom. Antihydrogen production is routinely operated at ATRAP and detailed studies have been performed in order to optimize the production efficiency of useful antihydrogen. For high precision measurements of atomic transitions cold antihydrogen in the ground state is required which must be trapped due to the low number of available antihydrogen atoms compared to the cold hydrogen beam used for hydrogen spectroscopy. To ensure a reasonable antihydrogen trapping efficiency a magnetic trap has to be superposed the nested Penning trap. First trapping tests of charged particles within a combined magnetic/Penning trap have started at ATRAP.

  5. Control of the conformations of ion Coulomb crystals in a Penning trap

    Energy Technology Data Exchange (ETDEWEB)

    Thompson, R. C.; Mavadia, S.; Goodwin, J. F.; Stutter, G.; Bharadia, S.; Crick, D. R.; Segal, D. M. [Blackett Laboratory, Imperial College London, London SW7 2AZ (United Kingdom)

    2015-06-29

    Ion Coulomb crystals containing small numbers of ions have been created and manipulated in a wide range of configurations in a Penning trap, from a linear string, through various three-dimensional conformations, to a planar crystal. We show that the dynamics of the system simplifies enormously in a frame which rotates at half the cyclotron frequency and we discuss the effect of the radial cooling laser beam in this frame. Simulations show that the crystal conformations can be reproduced by finding the minimum energy configuration in a frame whose radial potential is modified by the rotation of the ion crystal. The rotation frequency of the crystal deduced from the simulations is consistent with the known laser parameters. We also show that even though the number of ions in our system is small (typically less than 20), the system still behaves like a plasma and its static properties can be calculated using the standard model for a single-component plasma in a trap.

  6. Control of the conformations of ion Coulomb crystals in a Penning trap

    International Nuclear Information System (INIS)

    Thompson, R. C.; Mavadia, S.; Goodwin, J. F.; Stutter, G.; Bharadia, S.; Crick, D. R.; Segal, D. M.

    2015-01-01

    Ion Coulomb crystals containing small numbers of ions have been created and manipulated in a wide range of configurations in a Penning trap, from a linear string, through various three-dimensional conformations, to a planar crystal. We show that the dynamics of the system simplifies enormously in a frame which rotates at half the cyclotron frequency and we discuss the effect of the radial cooling laser beam in this frame. Simulations show that the crystal conformations can be reproduced by finding the minimum energy configuration in a frame whose radial potential is modified by the rotation of the ion crystal. The rotation frequency of the crystal deduced from the simulations is consistent with the known laser parameters. We also show that even though the number of ions in our system is small (typically less than 20), the system still behaves like a plasma and its static properties can be calculated using the standard model for a single-component plasma in a trap

  7. Coupling an optical trap to a mass separator

    Energy Technology Data Exchange (ETDEWEB)

    Chamberlin, E.P.; Sandberg, V.D.; Tupa, D.; Vieira, D.J.; Zhao, X.X. [Los Alamos National Lab., NM (United States); Guckert, R.; Wollnik, H. [Los Alamos National Lab., NM (United States)]/[Giessen Univ. (Germany); Preston, D.W. [Los Alamos National Lab., NM (United States)]/[California State Univ., Hayward, CA (United States)

    1996-12-31

    The efficient coupling of a magneto-optical trap to a mass separator is being developed to undertake high-precision electroweak interaction measurements in a series of radioisotopes. The use of ion implantation and subsequent heated-foil release is being pursued as a suitable way of introducing radioactive samples into the ultrahigh vacuum region of an optical trap without gas loading. This paper discusses the layout of the mass separator,the coupling to a magneto- optical trap, and the implantation and release scheme.

  8. Coupling an optical trap to a mass separator

    International Nuclear Information System (INIS)

    Chamberlin, E.P.; Sandberg, V.D.; Tupa, D.; Vieira, D.J.; Zhao, X.X.; Guckert, R.; Wollnik, H.; Preston, D.W.

    1996-01-01

    The efficient coupling of a magneto-optical trap to a mass separator is being developed to undertake high-precision electroweak interaction measurements in a series of radioisotopes. The use of ion implantation and subsequent heated-foil release is being pursued as a suitable way of introducing radioactive samples into the ultrahigh vacuum region of an optical trap without gas loading. This paper discusses the layout of the mass separator,the coupling to a magneto- optical trap, and the implantation and release scheme

  9. Trapping radioactive ions

    CERN Document Server

    Kluge, Heinz-Jürgen

    2004-01-01

    Trapping devices for atomic and nuclear physics experiments with radioactive ions are becoming more and more important at accelerator facilities. While about ten years ago only one online Penning trap experiment existed, namely ISOLTRAP at ISOLDE/CERN, meanwhile almost every radioactive beam facility has installed or plans an ion trap setup. This article gives an overview on ion traps in the operation, construction or planing phase which will be used for fundamental studies with short-lived radioactive nuclides such as mass spectrometry, laser spectroscopy and nuclear decay spectroscopy. In addition, this article summarizes the use of gas cells and radiofrequency quadrupole (Paul) traps at different facilities as a versatile tool for ion beam manipulation like retardation, cooling, bunching, and cleaning.

  10. Trapping radioactive ions

    International Nuclear Information System (INIS)

    Kluge, H.-J.; Blaum, K.

    2004-01-01

    Trapping devices for atomic and nuclear physics experiments with radioactive ions are becoming more and more important at accelerator facilities. While about ten years ago only one online Penning trap experiment existed, namely ISOLTRAP at ISOLDE/CERN, meanwhile almost every radioactive beam facility has installed or plans an ion trap setup. This article gives an overview on ion traps in the operation, construction or planing phase which will be used for fundamental studies with short-lived radioactive nuclides such as mass spectrometry, laser spectroscopy and nuclear decay spectroscopy. In addition, this article summarizes the use of gas cells and radiofrequency quadrupole (Paul) traps at different facilities as a versatile tool for ion beam manipulation like retardation, cooling, bunching, and cleaning

  11. Antimatter Plasmas in a Multipole Trap for Antihydrogen

    CERN Document Server

    Andresen, G B; Boston, A; Bowe, P D; Cesar, C L; Chapman, S; Charlton, M; Chartier, M; Deutsch, A; Fajans, J; Fujiwara, M C; Funakoshi, R; Gill, D R; Gomberoff, K; Hangst, J S; Hayano, R S; Hydomako, R; Jenkins, M J; Jørgensen, L V; Kurchaninov, L; Madsen, N; Nolan, P; Olchanski, K; Olin, A; Povilus, A; Robicheaux, F; Sarid, E; Silveira, D M; Storey, J W; Telle, H H; Thompson, R I; van der Werf, D P; Wurtele, J S; Yamazaki, Y

    2007-01-01

    We have demonstrated storage of plasmas of the charged constituents of the antihydrogen atom, antiprotons and positrons, in a Penning trap surrounded by a minimum-B magnetic trap designed for holding neutral antiatoms. The neutral trap comprises a superconducting octupole and two superconducting, solenoidal mirror coils. We have measured the storage lifetimes of antiproton and positron plasmas in the combined Penning-neutral trap, and compared these to lifetimes without the neutral trap fields. The magnetic well depth was 0.6 T, deep enough to trap ground state antihydrogen atoms of up to about 0.4 K in temperature. We have demonstrated that both particle species can be stored for times long enough to permit antihydrogen production and trapping studies.

  12. Antimatter plasmas in a multipole trap for antihydrogen.

    Science.gov (United States)

    Andresen, G; Bertsche, W; Boston, A; Bowe, P D; Cesar, C L; Chapman, S; Charlton, M; Chartier, M; Deutsch, A; Fajans, J; Fujiwara, M C; Funakoshi, R; Gill, D R; Gomberoff, K; Hangst, J S; Hayano, R S; Hydomako, R; Jenkins, M J; Jørgensen, L V; Kurchaninov, L; Madsen, N; Nolan, P; Olchanski, K; Olin, A; Povilus, A; Robicheaux, F; Sarid, E; Silveira, D M; Storey, J W; Telle, H H; Thompson, R I; van der Werf, D P; Wurtele, J S; Yamazaki, Y

    2007-01-12

    We have demonstrated storage of plasmas of the charged constituents of the antihydrogen atom, antiprotons and positrons, in a Penning trap surrounded by a minimum-B magnetic trap designed for holding neutral antiatoms. The neutral trap comprises a superconducting octupole and two superconducting, solenoidal mirror coils. We have measured the storage lifetimes of antiproton and positron plasmas in the combined Penning-neutral trap, and compared these to lifetimes without the neutral trap fields. The magnetic well depth was 0.6 T, deep enough to trap ground state antihydrogen atoms of up to about 0.4 K in temperature. We have demonstrated that both particle species can be stored for times long enough to permit antihydrogen production and trapping studies.

  13. A reservoir trap for antiprotons

    CERN Document Server

    Smorra, Christian; Franke, Kurt; Nagahama, Hiroki; Schneider, Georg; Higuchi, Takashi; Van Gorp, Simon; Blaum, Klaus; Matsuda, Yasuyuki; Quint, Wolfgang; Walz, Jochen; Yamazaki, Yasunori; Ulmer, Stefan

    2015-01-01

    We have developed techniques to extract arbitrary fractions of antiprotons from an accumulated reservoir, and to inject them into a Penning-trap system for high-precision measurements. In our trap-system antiproton storage times > 1.08 years are estimated. The device is fail-safe against power-cuts of up to 10 hours. This makes our planned comparisons of the fundamental properties of protons and antiprotons independent from accelerator cycles, and will enable us to perform experiments during long accelerator shutdown periods when background magnetic noise is low. The demonstrated scheme has the potential to be applied in many other precision Penning trap experiments dealing with exotic particles.

  14. Magnetic field stabilization in THe-Trap

    Energy Technology Data Exchange (ETDEWEB)

    Streubel, Sebastian; Eronen, Tommi; Hoecker, Martin; Ketter, Jochen; Blaum, Klaus [Max-Planck-Institut fuer Kernphysik, Heidelberg (Germany); Van Dyck, Robert S. Jr. [Department of Physics, University of Washington, Seattle, WA (United States)

    2012-07-01

    THe-Trap is a Penning trap mass spectrometer dedicated to measure the {sup 3}H to {sup 3}He mass ratio aiming to a relative mass uncertainty better than 10{sup -11}. The most vital prerequisite for this measurement is a stable magnetic field: The relative temporal fluctuations during a measurement cycle of typically 1 hour, should be better than 10{sup -11}. The 5.26 T field is provided by a superconducting magnet. Unfortunately, the materials within the cryostat have a temperature-dependent susceptibility which necessitates a temperature stabilization. The stabilization is achieved by controlling the liquid helium level above the traps, and by keeping the pressure of the liquid helium constant. An important part of the system is the pressure reference, which is stable at a 0.04 Pa level. In addition to the stabilization of the field fluctuations within the cryostat itself, a system to cancel external fluctuations is set up consisting of a passive coil with a shielding factor of up to 180 build into the cryostat. Furthermore, a Helmholtz coil pair is placed around the cryostat. The compensation signal is provided by a custom-built flux-gate magnetometer. Technical details about the stabilization systems are given.

  15. Development of an in-trap spectroscopy setup at MLLTRAP for the future project MATS at FAIR

    Energy Technology Data Exchange (ETDEWEB)

    Thirolf, Peter; Gartzke, Eva; Habs, Dietrich; Krug, Kevin; Szerypo, Jerzy; Weber, Christine [Fak. fuer Physik, LMU - Muenchen (Germany); Kolhinen, Veli [Dept. of Physics, University of Jyvaeskylae (Sweden); Rodriguez, Daniel [FAMN, Universidad de Granada (Spain)

    2010-07-01

    One of the most important achievements of Penning trap technology is the possibility to manipulate ions of a defined q/m in order to provide purified ion species to dedicated experiments, such as high-precision mass measurements. This feature of ion manipulation and purification is used as well in nuclear decay-spectroscopy experiments with isobarically or even isomerically pure samples, typically installed after the trap. In a further approach, the Penning trap itself is equipped with detectors, since the stored ion clouds represent ideal sources, free from any background or scattering effects in the required backing materials. An in-trap spectroscopy setup is developed at MLLTRAP to be implemented in the future MATS facility at the low-energy branch of FAIR/GSI. Here, the main trapping electrodes will be replaced by position-sensitive Si-strip detectors and emitted electrons are efficiently guided towards detectors by the strong field of the trap magnet. Possible physics experiments are conversion-electron spectroscopy and in-trap {alpha}-decay experiments of heavy actinides. In this presentation, the design of the setup and possible physics applications are presented.

  16. Control of the environmental inluences on THe-Trap on the example of the determination of the mass ratio of carbon-12 to oxygen-16; Kontrolle der Umwelteinfluesse auf THe-Trap am Beispiel der Bestimmung des Massenverhaeltnisses von Kohlenstoff-12 zu Sauerstoff-16

    Energy Technology Data Exchange (ETDEWEB)

    Streubel, Sebastian Dennis

    2014-04-16

    Tritium-Helium-3-Trap (THe-Trap) is a Penning-trap setup dedicated to measure the {sup 3}H to {sup 3}He mass ratio with a relative uncertainty of better than 10{sup -11}. This is 40 times more precise than the currently adopted value and, thus, will help to investigate possible systematic uncertainties of the Karlsruhe Tritium Neutrino experiment (KATRIN). To achieve the desired level of uncertainty, several environmental influences such as atmospheric pressure shifts and magnetic field fluctuations have to be suppressed. With the implemented stabilization system, the relative magnetic field drift could be reduced to a few 10{sup -12}/h for a time span of several weeks. Within the context of this thesis a mass ratio measurement of {sup 12}C{sup 4+} to {sup 16}O{sup 5+} was performed to characterize systematic effects. This measurement yielded a statistical uncertainty of 6.3 x 10{sup -11}, which can easily be improved with more statistics, i.e. a longer measurement time. While the systematic uncertainty for {sup 12}C{sup 4+}-ions were under control at the 10{sup -11} level, the systematic shifts could not be quantified for {sup 16}O{sup 5+} due to poor vacuum conditions. Without these corrections, a systematic uncertainty of 1.2.10{sup -10} could be achieved for the {sup 12}C/{sup 16}O mass ratio measurement.

  17. Mini ion trap mass spectrometer

    Science.gov (United States)

    Dietrich, D.D.; Keville, R.F.

    1995-09-19

    An ion trap is described which operates in the regime between research ion traps which can detect ions with a mass resolution of better than 1:10{sup 9} and commercial mass spectrometers requiring 10{sup 4} ions with resolutions of a few hundred. The power consumption is kept to a minimum by the use of permanent magnets and a novel electron gun design. By Fourier analyzing the ion cyclotron resonance signals induced in the trap electrodes, a complete mass spectra in a single combined structure can be detected. An attribute of the ion trap mass spectrometer is that overall system size is drastically reduced due to combining a unique electron source and mass analyzer/detector in a single device. This enables portable low power mass spectrometers for the detection of environmental pollutants or illicit substances, as well as sensors for on board diagnostics to monitor engine performance or for active feedback in any process involving exhausting waste products. 10 figs.

  18. MATS and LaSpec: High-precision experiments using ion traps and lasers at FAIR

    Science.gov (United States)

    Rodríguez, D.; Blaum, K.; Nörtershäuser, W.; Ahammed, M.; Algora, A.; Audi, G.; Äystö, J.; Beck, D.; Bender, M.; Billowes, J.; Block, M.; Böhm, C.; Bollen, G.; Brodeur, M.; Brunner, T.; Bushaw, B. A.; Cakirli, R. B.; Campbell, P.; Cano-Ott, D.; Cortés, G.; Crespo López-Urrutia, J. R.; Das, P.; Dax, A.; de, A.; Delheij, P.; Dickel, T.; Dilling, J.; Eberhardt, K.; Eliseev, S.; Ettenauer, S.; Flanagan, K. T.; Ferrer, R.; García-Ramos, J.-E.; Gartzke, E.; Geissel, H.; George, S.; Geppert, C.; Gómez-Hornillos, M. B.; Gusev, Y.; Habs, D.; Heenen, P.-H.; Heinz, S.; Herfurth, F.; Herlert, A.; Hobein, M.; Huber, G.; Huyse, M.; Jesch, C.; Jokinen, A.; Kester, O.; Ketelaer, J.; Kolhinen, V.; Koudriavtsev, I.; Kowalska, M.; Krämer, J.; Kreim, S.; Krieger, A.; Kühl, T.; Lallena, A. M.; Lapierre, A.; Le Blanc, F.; Litvinov, Y. A.; Lunney, D.; Martínez, T.; Marx, G.; Matos, M.; Minaya-Ramirez, E.; Moore, I.; Nagy, S.; Naimi, S.; Neidherr, D.; Nesterenko, D.; Neyens, G.; Novikov, Y. N.; Petrick, M.; Plaß, W. R.; Popov, A.; Quint, W.; Ray, A.; Reinhard, P.-G.; Repp, J.; Roux, C.; Rubio, B.; Sánchez, R.; Schabinger, B.; Scheidenberger, C.; Schneider, D.; Schuch, R.; Schwarz, S.; Schweikhard, L.; Seliverstov, M.; Solders, A.; Suhonen, M.; Szerypo, J.; Taín, J. L.; Thirolf, P. G.; Ullrich, J.; van Duppen, P.; Vasiliev, A.; Vorobjev, G.; Weber, C.; Wendt, K.; Winkler, M.; Yordanov, D.; Ziegler, F.

    2010-05-01

    Nuclear ground state properties including mass, charge radii, spins and moments can be determined by applying atomic physics techniques such as Penning-trap based mass spectrometry and laser spectroscopy. The MATS and LaSpec setups at the low-energy beamline at FAIR will allow us to extend the knowledge of these properties further into the region far from stability. The mass and its inherent connection with the nuclear binding energy is a fundamental property of a nuclide, a unique “fingerprint”. Thus, precise mass values are important for a variety of applications, ranging from nuclear-structure studies like the investigation of shell closures and the onset of deformation, tests of nuclear mass models and mass formulas, to tests of the weak interaction and of the Standard Model. The required relative accuracy ranges from 10-5 to below 10-8 for radionuclides, which most often have half-lives well below 1 s. Substantial progress in Penning trap mass spectrometry has made this method a prime choice for precision measurements on rare isotopes. The technique has the potential to provide high accuracy and sensitivity even for very short-lived nuclides. Furthermore, ion traps can be used for precision decay studies and offer advantages over existing methods. With MATS (Precision Measurements of very short-lived nuclei using an A_dvanced Trapping System for highly-charged ions) at FAIR we aim to apply several techniques to very short-lived radionuclides: High-accuracy mass measurements, in-trap conversion electron and alpha spectroscopy, and trap-assisted spectroscopy. The experimental setup of MATS is a unique combination of an electron beam ion trap for charge breeding, ion traps for beam preparation, and a high-precision Penning trap system for mass measurements and decay studies. For the mass measurements, MATS offers both a high accuracy and a high sensitivity. A relative mass uncertainty of 10-9 can be reached by employing highly-charged ions and a non

  19. A 2D Array of 100's of Ions for Quantum Simulation and Many-Body Physics in a Penning Trap

    Science.gov (United States)

    Bohnet, Justin; Sawyer, Brian; Britton, Joseph; Bollinger, John

    2015-05-01

    Quantum simulations promise to reveal new materials and phenomena for experimental study, but few systems have demonstrated the capability to control ensembles in which quantum effects cannot be directly computed. One possible platform for intractable quantum simulations may be a system of 100's of 9Be+ ions in a Penning trap, where the valence electron spins are coupled with an effective Ising interaction in a 2D geometry. Here we report on results from a new Penning trap designed for 2D quantum simulations. We characterize the ion crystal stability and describe progress towards bench-marking quantum effects of the spin-spin coupling using a spin-squeezing witness. We also report on the successful photodissociation of BeH+ contaminant molecular ions that impede the use of such crystals for quantum simulation. This work lays the foundation for future experiments such as the observation of spin dynamics under the quantum Ising Hamiltonian with a transverse field. Supported by a NIST-NRC Research Associateship.

  20. Detection of individual spin transitions of a single proton confined in a cryogenic Penning trap

    Energy Technology Data Exchange (ETDEWEB)

    Kracke, Holger

    2013-02-27

    The presented experiment for the determination of the magnetic moment of the proton is based on the measurement of the ratio of cyclotron frequency and Larmor frequency of a single proton confined in a cryogenic double-Penning trap. In the course of this thesis, the simultaneous non-destructive measurement of two of the three eigenfrequencies of the proton in thermal equilibrium with corresponding detection systems was demonstrated, which reduces the measurement time of the cyclotron frequency by a factor of two. Furthermore, this thesis presents the first detection of individual spin transitions of a single proton, which allows for the determination of the Larmor frequency. The continuous Stern-Gerlach effect is utilized to couple the magnetic moment to the axial mode of the trapped proton by means of a magnetic bottle. Thus, a spin flip causes a jump of the axial frequency, which can be measured non-destructively with highly-sensitive detection systems. However, not only the spin momentum is coupled to the axial motion but also the angular momentum. Thus, the main experimental challenge is the elimination of energy fluctuations in the radial modes in order to maintain spin flip resolution. Due to systematic studies on the stability of the axial frequency and a complete revision of the experimental setup, this goal was achieved. The spin state of the proton can be determined with very high fidelity for the very first time. Thus, this thesis represents an important step towards a high-precision determination of the magnetic moment of the proton.

  1. Precision Mass Measurements of 129-131Cd and Their Impact on Stellar Nucleosynthesis via the Rapid Neutron Capture Process

    CERN Document Server

    Atanasov, D.; Blaum, K.; Cakirli, R.B.; Cocolios, T.E.; George, S.; Herfurth, F.; Kisler, D.; Janka, H.T.; Just, O.; Kowalska, M.; Kreim, S.; Kisler, D.; Litvinov, Yu. A.; Lunney, D.; Manea, V.; Neidherr, D.; Rosenbusch, M.; Schweikhard, L.; Welker, A.; Wienholtz, F.; Wolf, R. N.; Zuber, K.

    2015-01-01

    Masses adjacent to the classical waiting-point nuclide 130Cd have been measured by using the Penning- trap spectrometer ISOLTRAP at ISOLDE/CERN. We find a significant deviation of over 400 keV from earlier values evaluated by using nuclear beta-decay data. The new measurements show the reduction of the N = 82 shell gap below the doubly magic 132Sn. The nucleosynthesis associated with the ejected wind from type-II supernovae as well as from compact object binary mergers is studied, by using state-of-the-art hydrodynamic simulations. We find a consistent and direct impact of the newly measured masses on the calculated abundances in the A = 128 - 132 region and a reduction of the uncertainties from the precision mass input data.

  2. Simulation of the formation of antihydrogen in a nested Penning trap: effect of positron density

    International Nuclear Information System (INIS)

    Jonsell, S; Werf, D P van der; Charlton, M; Robicheaux, F

    2009-01-01

    Detailed simulations of antihydrogen formation have been performed under the conditions of the ATHENA experiment, using several densities of the positron plasma in the range n e = 5 x 10 13 m -3 to 10 15 m -3 . The simulations include only collisional effects, typically resulting in the formation of weakly bound antihydrogen via the three-body process, e + + e + + p-bar → H-bar + e + . (Radiative processes, which are much slower than collisional effects, are neglected.) The properties of these weakly bound anti-atoms are affected not only by further collisions in the plasma but also by the inherent electric fields. The role of field ionization in influencing the distribution of binding energies of the antihydrogen is clarified and the mechanism for this process in the strong B-field nested Penning trap used in the experiment is elucidated. The fate of antihydrogen is explained and the properties of the population detected after having reached the wall of the Penning trap electrodes, as well as those field ionized, are recorded. We find that the yield of detected antihydrogen varies with positron density roughly as n 1.7 e , rather than the n 2 e expected from the underlying formation process. As n e is increased, antihydrogen formation is sufficiently rapid that epithermal effects begin to play an important role. In general, the simulated timescales for antihydrogen formation are much shorter than those found from the experiment.

  3. Precision mass measurements using the Phase-Imaging Ion-Cyclotron-Resonance detection technique

    CERN Document Server

    Karthein, Jonas

    This thesis presents the implementation and improvement of the Phase-Imaging Ion-Cyclotron-Resonance (PI-ICR) detection technique at the ISOLTRAP experiment, located at the ISOLDE / CERN, with the purpose of on-line high-precision and high-resolution mass spectrometry. Extensive simulation studies were performed with the aim of improving the phase-imaging resolution and finding the optimal position for detector placement. Following the outcome of these simulations, the detector was moved out of a region of electric-field distortion and closer to the center of the Penning trap, showing a dramatic improvement in the quality and reproducibility of the phase-imaging measurements. A new image reconstitution and analysis software for the MCP-PS detector was written in Python and ROOT and introduced in the framework of PI-ICR mass measurements. The state of the art in the field of time-of-flight ion-cyclotron-resonance measurements is illustrated through an analysis of on-line measurements of the mirror nuclei $...

  4. High-precision mass measurements for the rp-process at JYFLTRAP

    Directory of Open Access Journals (Sweden)

    Canete Laetitia

    2017-01-01

    Full Text Available The double Penning trap JYFLTRAP at the University of Jyväskylä has been successfully used to achieve high-precision mass measurements of nuclei involved in the rapid proton-capture (rp process. A precise mass measurement of 31Cl is essential to estimate the waiting point condition of 30S in the rp-process occurring in type I x-ray bursts (XRBs. The mass-excess of 31C1 measured at JYFLTRAP, -7034.7(3.4 keV, is 15 more precise than the value given in the Atomic Mass Evaluation 2012. The proton separation energy Sp determined from the new mass-excess value confirmed that 30S is a waiting point, with a lower-temperature limit of 0.44 GK. The mass of 52Co effects both 51Fe(p,γ52Co and 52Co(p,γ53Ni reactions. The mass-excess value measured, - 34 331.6(6.6 keV is 30 times more precise than the value given in AME2012. The Q values for the 51Fe(p,γ52Co and 52Co(p,γ53Ni reactions are now known with a high precision, 1418(11 keV and 2588(26 keV respectively. The results show that 52Co is more proton bound and 53Ni less proton bound than what was expected from the extrapolated value.

  5. Trapped charged particles a graduate textbook with problems and solutions

    CERN Document Server

    Madsen, Niels; Thompson, Richard C

    2016-01-01

    At Les Houches in January 2015, experts in the field of particle trapping came together to discuss the fundamental physics of traps and the different types of applications. This textbook collates the lectures delivered there; the Second Winter School on Physics with Trapped Charged Particles. Taken as a whole, the book gives an overview of why traps for charged particles are important, how they work, their special features and limitations, and their application in areas such as precision measurements, mass spectrometry, optical clocks, plasma physics, antihydrogen creation, quantum simulation and quantum information processing. Chapters from various world experts include those on the basic properties of Penning traps, RF traps and particle accelerators, as well as those covering important practical aspects such as vacuum systems, detection techniques, and different types of particle cooling including laser cooling. Finally, individual chapters deal with the different areas of application listed above. Each ...

  6. Accurate masses of unstable rare earth isotopes by ISOLTRAP

    International Nuclear Information System (INIS)

    Beck, D.; Ames, F.; Audi, G.

    2000-05-01

    Direct mass measurements of neutron-deficient rare earth isotopes in the vicinity of 146 Gd were performed with the Penning trap mass spectrometer ISOLTRAP at ISOLDE/CERN. This paper reports on the measurement of more than 40 isotopes of the elements Pr, Nd, Pm, Sm, Eu, Dy and Ho, that have been measured with a typical accuracy of δm ∼ 14 keV. An atomic mass evaluation has been performed taking into account other experimental mass values via a least-squares adjustment. The results of the adjustment are discussed. (orig.)

  7. Storage ion trap of an 'In-Flight Capture' type for precise mass measurement of radioactive nuclear reaction products and fission fragments

    International Nuclear Information System (INIS)

    Tarantin, N.I.

    2001-01-01

    Data on nuclear masses provide a basis for creating and testing various nuclear models. A tandem system of FLNR comprised of the U-400M cyclotron, the COMBAS magnetic separator and the mass-spectrometric ion trap of an 'in-flight capture' type is considered as a possible complex for producing of the short-lived nuclei in fragmentation reactions by heavy ions and for precise mass measurement of these nuclei. The plan of scientific and technical FLNR research includes a project DRIBs for producing beams of accelerated radioactive nuclear reaction products and photofission fragments. This project proposes also precise mass measurements of the fission fragment with the help of the ion trap. The in-flight entrance of the ions and their capture in the mass-spectrometric ion trap using the monochromatizing degrader, the static electric and magnetic fields and a new invention, a magnetic unidirectional transporting ventil, is considered

  8. First on-line applications of a multi-reflection time-of-flight mass separator at ISOLTRAP and the mass measurement of 82Zn

    International Nuclear Information System (INIS)

    Wolf, Robert

    2013-01-01

    This thesis describes the implementation and first on-line application of a multi-reflection time-of-flight (MR-ToF) mass analyzer for high-resolution mass separation at the ISOLTRAP mass spectrometer at ISOLDE/CERN. On the one hand, the major objective was to improve ISOLTRAPs mass-measurement capabilities with respect to the ratio of delivered contaminating ions to ions of interest. On the other hand, the time necessary to purify wanted from unwanted species should be reduced as much as possible to enable access to even more exotic nuclei. The device has been set up, optimized and tested at the University of Greifswald before its move to ISOLTRAP. The achieved performance comprises mass resolving powers of up to 2 x 10 5 reached at observation times of 30 ms and a contamination suppression of about four orders of magnitude by use of a Bradbury-Nielsen gate. With the characteristics, it outperforms clearly the so far state-of-the-art purification method of a gas-filled Penning trap. To improve the utilization of the MR-ToF mass analyzer, the in-trap lift method has been developed. It simplifies the application and optimization of the device, which is a crucial time factor in an on-line experiment. The device was the first of its kind successfully applied to radioactive ion beams for a mass analysis, for a mass separation (in combination with the Bradbury-Nielsen gate) as a preparatory step for a subsequent Penning-trap mass measurement and as a high-precision mass spectrometer of its own. The later was recently used for the first mass measurement of the neutron-rich calcium isotopes 53 Ca and 54 Ca. The so-far achieved mass-resolving power of 2 x 10 5 belongs to the highest reported for time-of-flight mass analyzers at all. The first successful application of the MR-ToF system as the only mass separator at ISOLTRAP resulted in the mass measurement of 82 Zn. The new mass value has been compared to mass extrapolations of the most recent Hartree-Fock-Bogolyubov (HFB

  9. Higgs boson theory and phenomenology mass measurements and nuclear physics Recent results from ISOLTRAP

    CERN Document Server

    Carena, M S; Herfurth, F; Ames, F; Audi, G; Beck, D; Blaum, K; Bollen, G; Kellerbauer, A G; Kluge, H J; Kuckein, M; Lunney, M D; Moore, R B; Oinonen, M; Rodríguez, D; Sauvan, E; Scheidenberger, C

    2003-01-01

    Precision electroweak data presently-favors a weakly-coupled Higgs sector as the mechanism responsible for electroweak symmetry breaking. Low-energy supersymmetry provides a natural framework for weakly-coupled elementary scalars. In this review, we summarize the theoretical properties of the Standard Model (SM) Higgs boson and the Higgs sector of the minimal super-symmetric extension of the Standard Model (MSSM). We then survey the phenomenology of the SM and MSSM Higgs bosons at the Tevatron, LHC and a future e**+e**- linear collider. We focus on the Higgs discovery potential of present and future colliders and stress the importance of precision measurements of Higgs boson properties. 459 Refs.31 The Penning trap mass spectrometer ISOLTRAP is a facility for high- precision mass measurements of short-lived radioactive nuclei installed at ISOLDE/CERN in Geneva. More than 200 masses have been measured with relative uncertainties of 1 multiplied by 10**-**7 or even close to 1 multiplied by 10**-**8 in special c...

  10. Molecular Dynamics Simulations of Collisional Cooling and Ordering of Multiply Charged Ions in a Penning Trap

    International Nuclear Information System (INIS)

    Holder, J.P.; Church, D.A.; Gruber, L.; DeWitt, H.E.; Beck, B.R.; Schneider, D.

    2000-01-01

    Molecular dynamics simulations are used to help design new experiments by modeling the cooling of small numbers of trapped multiply charged ions by Coulomb interactions with laser-cooled Be + ions. A Verlet algorithm is used to integrate the equations of motion of two species of point ions interacting in an ideal Penning trap. We use a time step short enough to follow the cyclotron motion of the ions. Axial and radial temperatures for each species are saved periodically. Direct heating and cooling of each species in the simulation can be performed by periodically rescaling velocities. Of interest are Fe 11+ due to a EUV-optical double resonance for imaging and manipulating the ions, and Ca 14+ since a ground state fine structure transition has a convenient wavelength in the tunable laser range

  11. Detecting yocto (10-24) newton forces with trapped ions

    CSIR Research Space (South Africa)

    Uys, H

    2010-09-01

    Full Text Available This article reports on a calibrated measurement of 174 Yoctonewton using a cloud of 60 9 Be+ ion confined in a Penning ion trap. These measurements suggest that ion traps may form the basis of a new class of ultrasensitive deployable force sensors....

  12. MATS and LaSpec: High-precision experiments using ion traps and lasers at FAIR

    CERN Document Server

    Rodriguez, D; Scheidenberger, C; Kreim, S; Gomez-Hornillos, M B; Aysto, J; Dickel, T; Geppert, C; Novikov, Y N; Tain, J L; Garcia-Ramos, J E; Bollen, G; Hobein, M; Audi, G; Beck, D; Winkler, M; Jesch, C; Vasiliev, A; Sanchez, R; Neidherr, D; Huber, G; Weber, C; Suhonen, M; Reinhard, P G; Jokinen, A; Lapierre, A; Bender, M; Martinez, T; Solders, A; Huyse, M; Matos, M; Szerypo, J; Seliverstov, M; Cortes, G; Cakirli, R B; Van Duppen, P; George, S; Block, M; Ahammed, M; Herfurth, F; Neyens, G; Habs, D; Thirolf, P G; Flanagan, K T; Roux, C; Schneider, D; Brodeur, M; Yordanov, D; Marx, G; Koudriavtsev, I; De, A; Boehm, C; Noertershaeuser, W; Blaum, K; Schabinger, B; Ettenauer, S; Plass, W R; Wendt, K; Nagy, S; Vorobjev, G; Minaya-Ramirez, E; Heenen, P-H; Quint, W; Kester, O; Le Blanc, F; Ray, A; Billowes, J; Kuehl, T; Kraemer, J; Lunney, D; Kolhinen, V; Rubio, B; Brunner, T; Nesterenko, D; Ferrer, R; Algora, A; Repp, J; Naimi, S; Eberhardt, K; Ziegler, F; Popov, A; Krieger, A; Campbell, P; Gartzke, E; Ketelaer, J; Heinz, S; Delheij, P; Ullrich, J; Dax, A; Crespo Lopez-Urrutia, J R; Eliseev, S; Das, P; Cano-Ott, D; Petrick, M; Moore, I; Litvinov, Y A; Schwarz, S; Dilling, J; Geissel, H; Bushaw, B A; Gusev, Y; Lallena, A M; Schweikhard, L; Schuch, R; Herlert, A

    2010-01-01

    Nuclear ground state properties including mass, charge radii, spins and moments can be determined by applying atomic physics techniques such as Penning-trap based mass spectrometry and laser spectroscopy. The MATS and LaSpec setups at the low-energy beamline at FAIR will allow us to extend the knowledge of these properties further into the region far from stability. The mass and its inherent connection with the nuclear binding energy is a fundamental property of a nuclide, a unique ``fingerprint{''}. Thus, precise mass values are important for a variety of applications, ranging from nuclear-structure studies like the investigation of shell closures and the onset of deformation, tests of nuclear mass models and mass formulas, to tests of the weak interaction and of the Standard Model. The required relative accuracy ranges from 10(-5) to below 10(-8) for radionuclides, which most often have half-lives well below 1 s. Substantial progress in Penning trap mass spectrometry has made this method a prime choice for ...

  13. Developing Antimatter Containment Technology: Modeling Charged Particle Oscillations in a Penning-Malmberg Trap

    Science.gov (United States)

    Chakrabarti, S.; Martin, J. J.; Pearson, J. B.; Lewis, R. A.

    2003-01-01

    The NASA MSFC Propulsion Research Center (PRC) is conducting a research activity examining the storage of low energy antiprotons. The High Performance Antiproton Trap (HiPAT) is an electromagnetic system (Penning-Malmberg design) consisting of a 4 Tesla superconductor, a high voltage confinement electrode system, and an ultra high vacuum test section; designed with an ultimate goal of maintaining charged particles with a half-life of 18 days. Currently, this system is being experimentally evaluated using normal matter ions which are cheap to produce and relatively easy to handle and provide a good indication of overall trap behavior, with the exception of assessing annihilation losses. Computational particle-in-cell plasma modeling using the XOOPIC code is supplementing the experiments. Differing electrode voltage configurations are employed to contain charged particles, typically using flat, modified flat and harmonic potential wells. Ion cloud oscillation frequencies are obtained experimentally by amplification of signals induced on the electrodes by the particle motions. XOOPIC simulations show that for given electrode voltage configurations, the calculated charged particle oscillation frequencies are close to experimental measurements. As a two-dimensional axisymmetric code, XOOPIC cannot model azimuthal plasma variations, such as those induced by radio-frequency (RF) modulation of the central quadrupole electrode in experiments designed to enhance ion cloud containment. However, XOOPIC can model analytically varying electric potential boundary conditions and particle velocity initial conditions. Application of these conditions produces ion cloud axial and radial oscillation frequency modes of interest in achieving the goal of optimizing HiPAT for reliable containment of antiprotons.

  14. In-trap decay spectroscopy for {beta}{beta} decays

    Energy Technology Data Exchange (ETDEWEB)

    Brunner, Thomas

    2011-01-18

    The presented work describes the implementation of a new technique to measure electron-capture (EC) branching ratios (BRs) of intermediate nuclei in {beta}{beta} decays. This technique has been developed at TRIUMF in Vancouver, Canada. It facilitates one of TRIUMF's Ion Traps for Atomic and Nuclear science (TITAN), the Electron Beam Ion Trap (EBIT) that is used as a spectroscopy Penning trap. Radioactive ions, produced at the radioactive isotope facility ISAC, are injected and stored in the spectroscopy Penning trap while their decays are observed. A key feature of this technique is the use of a strong magnetic field, required for trapping. It radially confines electrons from {beta} decays along the trap axis while X-rays, following an EC, are emitted isotropically. This provides spatial separation of X-ray and {beta} detection with almost no {beta}-induced background at the X-ray detector, allowing weak EC branches to be measured. Furthermore, the combination of several traps allows one to isobarically clean the sample prior to the in-trap decay spectroscopy measurement. This technique has been developed to measure ECBRs of transition nuclei in {beta}{beta} decays. Detailed knowledge of these electron capture branches is crucial for a better understanding of the underlying nuclear physics in {beta}{beta} decays. These branches are typically of the order of 10{sup -5} and therefore difficult to measure. Conventional measurements suffer from isobaric contamination and a dominating {beta} background at theX-ray detector. Additionally, X-rays are attenuated by the material where the radioactive sample is implanted. To overcome these limitations, the technique of in-trap decay spectroscopy has been developed. In this work, the EBIT was connected to the TITAN beam line and has been commissioned. Using the developed beam diagnostics, ions were injected into the Penning trap and systematic studies on injection and storage optimization were performed. Furthermore, Ge

  15. In-trap decay spectroscopy for ββ decays

    International Nuclear Information System (INIS)

    Brunner, Thomas

    2011-01-01

    The presented work describes the implementation of a new technique to measure electron-capture (EC) branching ratios (BRs) of intermediate nuclei in ββ decays. This technique has been developed at TRIUMF in Vancouver, Canada. It facilitates one of TRIUMF's Ion Traps for Atomic and Nuclear science (TITAN), the Electron Beam Ion Trap (EBIT) that is used as a spectroscopy Penning trap. Radioactive ions, produced at the radioactive isotope facility ISAC, are injected and stored in the spectroscopy Penning trap while their decays are observed. A key feature of this technique is the use of a strong magnetic field, required for trapping. It radially confines electrons from β decays along the trap axis while X-rays, following an EC, are emitted isotropically. This provides spatial separation of X-ray and β detection with almost no β-induced background at the X-ray detector, allowing weak EC branches to be measured. Furthermore, the combination of several traps allows one to isobarically clean the sample prior to the in-trap decay spectroscopy measurement. This technique has been developed to measure ECBRs of transition nuclei in ββ decays. Detailed knowledge of these electron capture branches is crucial for a better understanding of the underlying nuclear physics in ββ decays. These branches are typically of the order of 10 -5 and therefore difficult to measure. Conventional measurements suffer from isobaric contamination and a dominating β background at theX-ray detector. Additionally, X-rays are attenuated by the material where the radioactive sample is implanted. To overcome these limitations, the technique of in-trap decay spectroscopy has been developed. In this work, the EBIT was connected to the TITAN beam line and has been commissioned. Using the developed beam diagnostics, ions were injected into the Penning trap and systematic studies on injection and storage optimization were performed. Furthermore, Ge detectors, for the detection of X-rays, were

  16. Charged particle traps II applications

    CERN Document Server

    Werth, Günther; Major, Fouad G

    2009-01-01

    This, the second volume of Charged Particle Traps, is devoted to applications, complementing the first volume’s comprehensive treatment of the theory and practice of charged particle traps, their many variants and refinements. In recent years, applications of far reaching importance have emerged ranging from the ultra-precise mass determinations of elementary particles and their antiparticles and short-lived isotopes, to high-resolution Zeeman spectroscopy on multiply-charged ions, to microwave and optical spectroscopy, some involving "forbidden" transitions from metastable states of such high resolution that optical frequency standards are realized by locking lasers to them. Further the potential application of trapped ions to quantum computing is explored, based on the extraordinary quantum state coherence made possible by the particle isolation. Consideration is given to the Paul and Penning traps as potential quantum information processors.

  17. A novel ion cooling trap for multi-reflection time-of-flight mass spectrograph

    Energy Technology Data Exchange (ETDEWEB)

    Ito, Y., E-mail: yito@riken.jp [SLOWRI Team, Nishina Accelerator-Based Research Center, RIKEN, 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); University of Tsukuba, 1-1-1 Tennodai, Tsukuba, Ibaraki 305-8577 (Japan); Schury, P. [SLOWRI Team, Nishina Accelerator-Based Research Center, RIKEN, 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); University of Tsukuba, 1-1-1 Tennodai, Tsukuba, Ibaraki 305-8577 (Japan); New Mexico State University, Department Chemistry and Biochemistry, Las Cruces, NM 88003 (United States); Wada, M.; Naimi, S. [SLOWRI Team, Nishina Accelerator-Based Research Center, RIKEN, 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Smorra, C. [SLOWRI Team, Nishina Accelerator-Based Research Center, RIKEN, 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Max-Planck-Institut für Kernphysik, Saupfercheckweg 1, D-69117 Heidelberg (Germany); Sonoda, T. [SLOWRI Team, Nishina Accelerator-Based Research Center, RIKEN, 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Mita, H. [SLOWRI Team, Nishina Accelerator-Based Research Center, RIKEN, 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); University of Tsukuba, 1-1-1 Tennodai, Tsukuba, Ibaraki 305-8577 (Japan); Takamine, A. [SLOWRI Team, Nishina Accelerator-Based Research Center, RIKEN, 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Aoyama Gakuin University, 4-4-25 Shibuya, Shibuya-ku, Tokyo 150-8366 (Japan); Okada, K. [SLOWRI Team, Nishina Accelerator-Based Research Center, RIKEN, 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Sophia University, 7-1 Kioi-cho, Chiyoda-ku, Tokyo 102-8554 (Japan); Ozawa, A. [University of Tsukuba, 1-1-1 Tennodai, Tsukuba, Ibaraki 305-8577 (Japan); Wollnik, H. [SLOWRI Team, Nishina Accelerator-Based Research Center, RIKEN, 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); New Mexico State University, Department Chemistry and Biochemistry, Las Cruces, NM 88003 (United States)

    2013-12-15

    Highlights: • Fast cooling time: 2 ms. • High efficiency: ≈27% for {sup 23}Na{sup +} and ≈5.1% for {sup 7}Li{sup +}. • 100% Duty cycle with double trap system. -- Abstract: A radiofrequency quadrupole ion trap system for use with a multi-reflection time-of-flight mass spectrograph (MRTOF) for short-lived nuclei has been developed. The trap system consists of two different parts, an asymmetric taper trap and a flat trap. The ions are cooled to a sufficient small bunch for precise mass measurement with MRTOF in only 2 ms cooling time in the flat trap, then orthogonally ejected to the MRTOF for mass analysis. A trapping efficiency of ≈27% for {sup 23}Na{sup +} and ≈5.1% for {sup 7}Li{sup +} has been achieved.

  18. LEBIT - a low-energy beam and ion trap facility at NSCL/MSU

    International Nuclear Information System (INIS)

    Schwarz, S.; Bollen, G.; Davies, D.; Lawton, D.; Lofy, P.; Morrissey, D. J.; Ottarson, J.; Ringle, R.; Schury, P.; Sun, T.; VanWasshenova, D.; Sun, T.; Weissman, L.; Wiggins, D.

    2003-01-01

    The Low Energy Beam and Ion Trap (LEBIT) Project aims to convert the high-energy exotic beams produced at NSCL/MSU into low-energy low-emittance beams. A combination of a high-pressure gas stopping cell and a radiofrequency quadrupole (RFQ) ion accumulator and buncher will be used to manipulate the beam accordingly. High-accuracy mass measurements on very short-lived isotopes with a 9.4 T Penning trap system will be the first experimental program to profit from the low-energy beams. The status of the project is presented with a focus on recent stopping tests of 100-140 MeV/A Ar18+ ions in a gas cell

  19. Background-free beta-decay half-life measurements by in-trap decay and high-resolution MR-ToF mass analysis

    Science.gov (United States)

    Wolf, R. N.; Atanasov, D.; Blaum, K.; Kreim, S.; Lunney, D.; Manea, V.; Rosenbusch, M.; Schweikhard, L.; Welker, A.; Wienholtz, F.; Zuber, K.

    2016-06-01

    In-trap decay in ISOLTRAP's radiofrequency quadrupole (RFQ) ion beam cooler and buncher was used to determine the lifetime of short-lived nuclides. After various storage times, the remaining mother nuclides were mass separated from accompanying isobaric contaminations by the multi-reflection time-of-flight mass separator (MR-ToF MS), allowing for a background-free ion counting. A feasibility study with several online measurements shows that the applications of the ISOLTRAP setup can be further extended by exploiting the high resolving power of the MR-ToF MS in combination with in-trap decay and single-ion counting.

  20. The low-energy-beam and ion-trap facility at NSCL/MSU

    Energy Technology Data Exchange (ETDEWEB)

    Schwarz, S. E-mail: schwarz@nscl.msu.edu; Bollen, G.; Lawton, D.; Lofy, P.; Morrissey, D.J.; Ottarson, J.; Ringle, R.; Schury, P.; Sun, T.; Varentsov, V.; Weissman, L

    2003-05-01

    The goal of the low-energy-beam and ion-trap (LEBIT) project is to convert the high-energy exotic beams produced at NSCL/MSU into low-energy low-emittance beams. This beam manipulation will be done by a combination of a high-pressure gas stopping cell and a radio-frequency quadrupole ion accumulator and buncher. The first experimental program to profit from the low-energy beams produced will be high-accuracy mass measurements on very short-lived isotopes with a 9.4 T Penning trap system. The status of the project is presented with an emphasis on recent stopping tests range of 100 MeV/A {sup 40}Ar{sup 18+} ions in a gas cell.

  1. The low-energy-beam and ion-trap facility at NSCL/MSU

    International Nuclear Information System (INIS)

    Schwarz, S.; Bollen, G.; Lawton, D.; Lofy, P.; Morrissey, D.J.; Ottarson, J.; Ringle, R.; Schury, P.; Sun, T.; Varentsov, V.; Weissman, L.

    2003-01-01

    The goal of the low-energy-beam and ion-trap (LEBIT) project is to convert the high-energy exotic beams produced at NSCL/MSU into low-energy low-emittance beams. This beam manipulation will be done by a combination of a high-pressure gas stopping cell and a radio-frequency quadrupole ion accumulator and buncher. The first experimental program to profit from the low-energy beams produced will be high-accuracy mass measurements on very short-lived isotopes with a 9.4 T Penning trap system. The status of the project is presented with an emphasis on recent stopping tests range of 100 MeV/A 40 Ar 18+ ions in a gas cell

  2. First on-line applications of multi-reflection time-of-flight mass separator at ISOLTRAP and the mass measurement of $^{82}$Zn

    CERN Document Server

    Wolf, Robert

    This thesis describes the implementation and first on-line application of a multi-reflection time-of-flight (MR-ToF) mass analyzer for high-resolution mass separation at the ISOLTRAP mass spectrometer at ISOLDE/CERN. On the one hand, the major objective was to improve ISOLTRAPs mass-measurement capabilities with respect to the ratio of delivered contaminating ions to ions of interest. On the other hand, the time necessary to purify wanted from unwanted species should be reduced as much as possible to enable access to even more exotic nuclei. The device has been set up, optimized and tested at the University of Greifswald before its move to ISOLTRAP. The achieved performance comprises mass resolving powers of up to 200000 reached at observation times of 30ms and a contamination suppression of about four orders of magnitude by use of a Bradbury-Nielsen gate. With the characteristics, it outperforms clearly the so far state-of-the-art purification method of a gas-filled Penning trap. To improve the utilization o...

  3. A phase-imaging ion-cyclotron-resonance technique for mass measurements of short-lived nuclides

    Energy Technology Data Exchange (ETDEWEB)

    Eliseev, Sergey; Blaum, Klaus; Doerr, Andreas; Eronen, Tommi; Goncharov, Mikhail; Hoecker, Martin; Ketter, Jochen; Ramirez, Enrique Minaya; Simon, Vanessa [Max-Planck Institute for Nuclear Physics (Germany); Block, Michael [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH (Germany); Chenmarev, Stanislav; Filjanin, Pavel; Nesterenko, Dmitriy; Novikov, Yuri [Petersburg Nuclear Physics Institute (Russian Federation); Droese, Christian; Schweikhard, Lutz [Institute for Physics, Ernst-Moritz-Arndt-University (Germany)

    2014-07-01

    A novel approach to mass measurements on the sub-ppb level even for short-lived nuclides with half-lives well below one second is presented. It is based on the projection of the radial ion motion in a Penning trap onto a position sensitive detector. Compared to the presently employed time-of-flight ion-cyclotron-resonance technique, the novel approach is 25-times faster and provides a 40-fold gain in resolving power. With the new technique low-lying isomeric states with excitation energy on the 10-keV level can be separated from the ground state. Moreover, the new technique possesses a substantially higher sensitivity since just two ions are sufficient to determine the ion cyclotron frequency. A measurement of the mass difference of singly charged ions of {sup 132}Xe and {sup 131}Xe with an uncertainty of 25 eV has demonstrated the great potential of the new approach.

  4. A radio frequency quadrupole ion beam buncher for ISOLTRAP

    CERN Document Server

    Bollen, G; Dezfuli, A M G; Henry, S; Herfurth, F; Kellerbauer, A G; Kim, T; Kluge, H J; Kohl, A; Lamour, E; Lunney, M D; Moore, R B; Quint, W; Schwarz, S; Varfalvy, P; Vermeeren, L

    1998-01-01

    ISOLTRAP is a Penning trap spectrometer at the on-line mass separator ISOLDE at CERN for the mass determination of radioisotopes. It consists of three electromagnetic traps in tandem; a Paul trap for ISOLDE beam collection, a Penning trap for cooling and purification and a high-precision Penning trap for the measurement of masses by cyclotron resonance. The Paul trap, which collects radionuclide ions using only electric fields and a noble buffer gas, has been essential for the masses of radionuclides that cannot be surface ionized. The success with this system has led to the present program to increase the collection efficiency by replacing the Paul trap by a radiofrequency quadrupole ion guide operating as a buncher. This system would also provide a DC ISOLDE beam of emittance approaching 1$\\pi$ -mm-mrad. (3 refs).

  5. Trap-induced mass declines in small mammals: Mass as a population index

    Science.gov (United States)

    Dean E. Pearson; Yvette K. Ortega; Leonard F. Ruggiero

    2003-01-01

    Body mass is routinely used as an index of physical condition for comparing small-mammal populations. However, trapping effects on animals may undermine the effectiveness of body mass as an index of population health. We examined the effects of live-trapping on body mass of 3 small-mammal species: deer mice (Peromyscus maniculatus), southern red-...

  6. Weak Interaction Measurements with Optically Trapped Radioactive Atoms

    International Nuclear Information System (INIS)

    Vieira, D.J.; Crane, S.G.; Guckert, R.; Zhao, X.; Brice, S.J.; Goldschmidt, A.; Hime, A.; Tupa, D.

    1999-01-01

    This is the final report of a three-year, Laboratory-Directed Research and Development (LDRD) project at the Los Alamos National Laboratory (LANL). The goal of this project is to apply the latest in magneto-optical and pure magnetic trapping technology to concentrate, cool, confine, and polarize radioactive atoms for precise electroweak interaction measurements. In particular, the authors have concentrated their efforts on the trapping of 82 Rb for a parity-violating, beta-asymmetry measurement. Progress has been made in successfully trapping of up to 6 million 82 Rb(t 1/2 =75s) atoms in a magneto-optical trap coupled to a mass separator. This represents a two order of magnitude improvement in the number trapped radioactive atoms over all previous work. They have also measured the atomic hyperfine structure of 82 Rb and demonstrated the MOT-to-MOT transfer and accumulation of atoms in a second trap. Finally, they have constructed and tested a time-orbiting-potential magnetic trap that will serve as a rotating beacon of spin-polarized nuclei and a beta-telescope detection system. Prototype experiments are now underway with the initial goal of making a 1% measurements of the beta-asymmetry parameter A which would match the world's best measurements

  7. The low-energy-beam and ion-trap facility at NSCL/MSU

    CERN Document Server

    Schwarz, S; Lawton, D; Lofy, P; Morrissey, D J; Ottarson, J; Ringle, R; Schury, P; Sun, T; Varentsov, V; Weissman, L

    2003-01-01

    The goal of the low-energy-beam and ion-trap (LEBIT) project is to convert the high-energy exotic beams produced at NSCL/MSU into low-energy low-emittance beams. This beam manipulation will be done by a combination of a high-pressure gas stopping cell and a radio-frequency quadrupole ion accumulator and buncher. The first experimental program to profit from the low-energy beams produced will be high-accuracy mass measurements on very short-lived isotopes with a 9.4 T Penning trap system. The status of the project is presented with an emphasis on recent stopping tests range of 100 MeV/A sup 4 sup 0 Ar sup 1 sup 8 sup + ions in a gas cell.

  8. Nuclear structure studies of neutron-rich heavy nuclei by mass measurements of francium and radium isotopes

    Energy Technology Data Exchange (ETDEWEB)

    Rosenbusch, Marco [Ernst-Moritz-Arndt-Universitaet, Institut fuer Physik, 17487 Greifswald (Germany); Collaboration: ISOLTRAP-Collaboration

    2013-07-01

    The mass is a unique property of an atomic nucleus reflecting its binding energy and thus the sum of all interactions at work. Precise measurements of nuclear masses especially of short-lived exotic nuclides provide important input for nuclear structure, nuclear astrophysics, tests of the Standard Model, and weak interaction studies. The Penning-trap mass spectrometer ISOLTRAP at the on-line isotope separator ISOLDE/CERN has been set up for precision mass measurements and continuously improved for accessing more exotic nuclides. The mass uncertainty is typically δm / m=10{sup -8} and the accessible half-life has been reduced to about 50 ms. In this contribution, the results of a measurement campaign of neutron-rich francium and radium isotopes will be presented, i.e. the masses of the isotopic chain of {sup 224-233}Fr and {sup 233,234}Ra, one of the most neutron-rich ensemble obtainable at ISOL facilities. The mass {sup 234}Ra denotes the heaviest mass ever measured with ISOLTRAP. Experimental data in the neutron-rich, heavy mass region is of great interest for studies of structural evolution far from stability, especially because the knowledge from nuclear mass models is scarce. The impact of the new data on the physics in this mass region as well as recent technical developments of ISOLTRAP are discussed.

  9. Re-measurement of $^{32}$Ar to test the IMME

    CERN Multimedia

    The Isobaric Multiplet Mass Equation (IMME) has been subject to extensive studies in the low-mass region. Especially at the A = 32 quintet, the predicted quadratic form could not be confirmed, possible explanations being the insufficient accuracy of input parameters or higher-order interactions within the nucleon. For this quintet, the uncertainty on the mass-excess values of four of the five T = 2 multiplet members is extremely low: 0.6 keV for $^{32}$Cl, 0.3 keV for $^{32}$S, 0.2 keV for $^{32}$P, and 0.7 keV for $^{32}$Si. In the case of $^{32}$Ar, however, the uncertainty is as large as 1.8 keV. State-of-the-art high-precision Penning-trap mass spectrometry makes it possible to decrease this uncertainty. We propose to remeasure the mass of $^{32}$Ar at the Penning-trap mass spectrometer ISOLTRAP thus decreasing the uncertainty by a factor of 3-5. The proposed measurement is part of an experimental collaboration with JYFLTRAP, where the remaining masses of the T = 2 isospin quintet at A = 32 will be remeas...

  10. Simbuca, using a graphics card to simulate Coulomb interactions in a penning trap

    CERN Document Server

    Van Gorp, S; Friedag, P; De Leebeeck, V; Tandecki, M; Weinheimer, C; Breitenfeldt, M; Traykov, E; Severijn, N; Mader, J; Soti, G; Iitaka, T; Herlert, A; Wauters, F; Zakoucky, D; Kozlov, V; Roccia, S

    2011-01-01

    In almost all cases, N-body simulations are limited by the computation time available. Coulomb interaction calculations scale with O(N(2)) with N the number of particles. Approximation methods exist already to reduce the computation time to O(NlogN) although calculating the interaction still dominates the total simulation time. We present Simbuca, a simulation package for thousands of ions moving in a Penning trap which will be applied for the WITCH experiment. Simbuca uses the output of the Cunbody-1 library, which calculates the gravitational interaction between entities on a graphics card, and adapts it for Coulomb calculations. Furthermore the program incorporates three realistic buffer gas models, the possibility of importing realistic electric and magnetic fieldmaps and different order integrators with adaptive step size and error control. The software is released under the GNU General Public License and free for use. Crown Copyright (C) 2010 Published by Elsevier B.V. All rights reserved.

  11. High-Precision Direct Mass Determination of Unstable Isotopes

    CERN Multimedia

    2002-01-01

    The extension of systematic high-precision measurements of the nuclear mass to nuclei far from the valley of $\\beta$ stability is of great interest in nuclear physics and astrophysics. The mass, or binding energy, is a fundamental gross property and a key input parameter for nuclear matter calculations. It is also a sensitive probe for collective and single-particle effects in nuclear structure. \\\\ \\\\ For such purposes, nuclear masses need to be known to an accuracy of about 10$^{-7}$ (i.e. $\\Delta$M~$\\leq$~10~keV for A~=~100). To resolve a particular mass from its nuclear isomers and isobars, resolving power of 10$^6$ are often required. To achieve this, the ions delivered by the on-line mass separator ISOLDE are confined in a Penning quadrupole trap. This trap is placed in the very homogeneous and stable magnetic field of a superconducting magnet. Here, the cyclotron frequency and hence the mass are determined. \\\\ \\\\ The first measurements using this new technique have been completed for a long chain of Cs ...

  12. Advanced Quadrupole Ion Trap Instrumentation for Low Level Vehicle Emissions Measurements

    International Nuclear Information System (INIS)

    McLuckey, S.A.

    1997-01-01

    Quadrupole ion trap mass spectrometry has been evaluated for its potential use in vehicle emissions measurements in vehicle test facilities as an analyzer for the top 15 compounds contributing to smog generation. A variety of ionization methods were explored including ion trap in situ chemical ionization, atmospheric sampling glow discharge ionization, and nitric oxide chemical ionization in a glow discharge ionization source coupled with anion trap mass spectrometer. Emphasis was placed on the determination of hydrocarbons and oxygenated hydrocarbons at parts per million to parts per billion levels. Ion trap in situ water chemical ionization and atmospheric sampling glow discharge ionization were both shown to be amendable to the analysis of arenes, alcohols, aldehydes and, to some degree, alkenes. Atmospheric sampling glow discharge also generated molecular ions of methy-t-butyl ether (MTBE). Neither of these ionization methods, however, were found to generate diagnostic ions for the alkanes. Nitric oxide chemical ionization, on the other hand, was found to yield diagnostic ions for alkanes, alkenes, arenes, alcohols, aldehydes, and MTBE. The ability to measure a variety of hydrocarbons present at roughly 15 parts per billion at measurement rates of 3 Hz was demonstrated. All of the ions with potential to serve as parent ions in a tandem mass spectrometry experiment were found to yield parent-to-product conversion efficiencies greater than 75%. The flexibility afforded to the ion trap by use of tailored wave-forms applied to the end-caps allows parallel monitoring schemes to be devised that provide many of the advantages of tandem mass spectrometry without major loss in measurement rate. A large loss in measurement rate would ordinarily result from the use of conventional tandem mass spectrometry experiments carried out in series for a large number of targeted components. These results have demonstrated that the ion trap has an excellent combination of

  13. Extending and refining the mass surface around $^{208}$Pb by high-precision Penning-trap mass spectrometry with ISOLTRAP

    CERN Multimedia

    Herfurth, F; Stora, T; Blaum, K; Beck, D; Kowalska, M; Schwarz, S; Stanja, J; Herlert, A J; Yamaguchi, T

    We propose high-precision mass spectrometry of nuclides around the doubly magic $^{208}$Pb. On the neutron-rich side, we aim to extend the knowledge of Fr, At, Hg, and Au masses to study the robustness of the N = 126 shell closure and to provide mass data necessary for modeling the rapid-neutron-capture process. On the proton-rich side, we aim at high-resolution mass spectrometry of selected Au, At, and Fr isotopes to verify the predicted existence of very low-lying isomeric states. The proposal will make use of newly-available laser-ionization schemes for Au and At. Finally, the recently implemented multi-reflection time-of-flight mass separator for auxiliary isobaric purification now allows measurements which were not feasible before.

  14. Extraction of ultra-low-energy antiprotons from the PS200 catching trap for atomic physics experiments

    International Nuclear Information System (INIS)

    Holzscheiter, M.H.

    1996-01-01

    Approximately one million antiprotons have been captured in a large-scale Penning trap at the low energy antiproton ring at CERN. Up to 65% of the captured antiprotons have subsequently been cooled by electron cooling to energies below 1 eV and have been stored up to one hour. This has opened new discussions of the possible use of ultra-low-energy antiprotons for nuclear, atomic, and gravitational physics. For most of these experiments it will be necessary to extract the antiprotons from the trap in the form of either a continuous beam or as a bunched beam, allowing the timing structure to be used for post-acceleration schemes or as a time tag for subsequent measurements. We have designed an extraction scheme to accomplish this and have tested portions of it using a smaller-scale Penning trap loaded with protons. First results in generating a time-correlated beam of particles from a Penning trap are presented. (orig.)

  15. Injection into electron plasma traps

    International Nuclear Information System (INIS)

    Gorgadze, Vladimir; Pasquini, Thomas A.; Fajans, Joel; Wurtele, Jonathan S.

    2003-01-01

    Computational studies and experimental measurements of plasma injection into a Malmberg-Penning trap reveal that the number of trapped particles can be an order of magnitude higher than predicted by a simple estimates based on a ballistic trapping model. Enhanced trapping is associated with a rich nonlinear dynamics generated by the space-charge forces of the evolving trapped electron density. A particle-in-cell simulation is used to identify the physical mechanisms that lead to the increase in trapped electrons. The simulations initially show strong two-stream interactions between the electrons emitted from the cathode and those reflected off the end plug of the trap. This is followed by virtual cathode oscillations near the injection region. As electrons are trapped, the initially hollow longitudinal phase-space is filled, and the transverse radial density profile evolves so that the plasma potential matches that of the cathode. Simple theoretical arguments are given that describe the different dynamical regimes. Good agreement is found between simulation and theory

  16. Precision mass measurements with ISOLTRAP to study the evolution of the $\\textit{N}$=82 shell gap far from stability

    CERN Multimedia

    Shell effects and their evolution across the nuclear chart impose important constraints on the modelling of the nucleon-nucleon interaction. The strength of shell closures in neutron-rich nuclei also influences the path of the $\\textit{r}$-process of nucleo-synthesis and the predicted elemental abundances. We propose to measure the masses of the isotopes $^{132,133}$In, $^{129-132}$Cd, $^{125-129}$Ag with the Penning-trap mass spectrometer ISOLTRAP. The recently developed multi-reflection time-of-flight mass separator of ISOLTRAP will allow, as a beam purifier, to handle higher contamination ratios than before and, for the more exotic cases, to directly determine the mass of the nuclides of interest. The masses of the proposed isotopes will allow the investigation of a possible weakening of the $\\textit{N}$ = 82 shell gap for $\\textit{Z}$ < 50 and corresponding $\\textit{r}$-process waiting point. This in turn enables an exploration of the impact on the $\\textit{A}$ = 130 $\\textit{r}$-process abundances.

  17. Forensic analysis of ballpoint pen inks using paper spray mass spectrometry.

    Science.gov (United States)

    da Silva Ferreira, Priscila; Fernandes de Abreu e Silva, Débora; Augusti, Rodinei; Piccin, Evandro

    2015-02-07

    A novel analytical approach based on paper spray mass spectrometry (PS-MS) is developed for a fast and effective forensic analysis of inks in documents. Ink writings made in ordinary paper with blue ballpoint pens were directly analyzed under ambient conditions without any prior sample preparation. Firstly, the method was explored on a set of distinct pens and the results obtained in the positive ion mode, PS(+)-MS, demonstrated that pens from different brands provide typical profiles. Simple visual inspection of the PS(+)-MS led to the distinction of four different combinations of dyes and additives in the inks. Further discrimination was performed by using the concept of relative ion intensity (RII), owing to the large variability of dyes BV3 and BB26 regarding their demethylated homologues. Following screening and differentiation studies, the composition changes of ink entries subjected to light exposure were also monitored by PS-MS. The results of these tests revealed distinct degradation behaviors which were reflected on the typical chemical profiles of the studied inks, attesting that PS-MS may be also useful to verify the fading of dyes thus allowing the discrimination of entries on a document. As proof of concept experiments, PS-MS was successfully utilized for the analysis of archived documents and characterization of overlapped ink lines made on simulated forged documents.

  18. An integrated ion trap and time-of-flight mass spectrometer for chemical and photo- reaction dynamics studies

    International Nuclear Information System (INIS)

    Schowalter, Steven J.; Chen Kuang; Rellergert, Wade G.; Sullivan, Scott T.; Hudson, Eric R.

    2012-01-01

    We demonstrate the integration of a linear quadrupole trap with a simple time-of-flight mass spectrometer with medium-mass resolution (m/Δm∼ 50) geared towards the demands of atomic, molecular, and chemical physics experiments. By utilizing a novel radial ion extraction scheme from the linear quadrupole trap into the mass analyzer, a device with large trap capacity and high optical access is realized without sacrificing mass resolution. This provides the ability to address trapped ions with laser light and facilitates interactions with neutral background gases prior to analyzing the trapped ions. Here, we describe the construction and implementation of the device as well as present representative ToF spectra. We conclude by demonstrating the flexibility of the device with proof-of-principle experiments that include the observation of molecular-ion photodissociation and the measurement of trapped-ion chemical reaction rates.

  19. Isobar Separation in a Multiple-Reflection Time-of-Flight Mass Spectrometer by Mass-Selective Re-Trapping

    Science.gov (United States)

    Dickel, Timo; Plaß, Wolfgang R.; Lippert, Wayne; Lang, Johannes; Yavor, Mikhail I.; Geissel, Hans; Scheidenberger, Christoph

    2017-06-01

    A novel method for (ultra-)high-resolution spatial mass separation in time-of-flight mass spectrometers is presented. Ions are injected into a time-of-flight analyzer from a radio frequency (rf) trap, dispersed in time-of-flight according to their mass-to-charge ratios and then re-trapped dynamically in the same rf trap. This re-trapping technique is highly mass-selective and after sufficiently long flight times can provide even isobaric separation. A theoretical treatment of the method is presented and the conditions for optimum performance of the method are derived. The method has been implemented in a multiple-reflection time-of-flight mass spectrometer and mass separation powers (FWHM) in excess of 70,000, and re-trapping efficiencies of up to 35% have been obtained for the protonated molecular ion of caffeine. The isobars glutamine and lysine (relative mass difference of 1/4000) have been separated after a flight time of 0.2 ms only. Higher mass separation powers can be achieved using longer flight times. The method will have important applications, including isobar separation in nuclear physics and (ultra-)high-resolution precursor ion selection in multiple-stage tandem mass spectrometry. [Figure not available: see fulltext.

  20. Practical aspects of trapped ion mass spectrometry, 5 applications of ion trapping devices

    CERN Document Server

    March, Raymond E

    2009-01-01

    Examines ion/neutral and ion/ion reactions, ion spectroscopy, and the structural characterization of proteins and peptides using quadropole ion trap mass spectrometry, Fourier transform - ion cyclotron resonance (FT-ICR) mass spectrometry, and traveling wave ion mobility mass spectrometry.

  1. An integrated ion trap and time-of-flight mass spectrometer for chemical and photo- reaction dynamics studies.

    Science.gov (United States)

    Schowalter, Steven J; Chen, Kuang; Rellergert, Wade G; Sullivan, Scott T; Hudson, Eric R

    2012-04-01

    We demonstrate the integration of a linear quadrupole trap with a simple time-of-flight mass spectrometer with medium-mass resolution (m/Δm ∼ 50) geared towards the demands of atomic, molecular, and chemical physics experiments. By utilizing a novel radial ion extraction scheme from the linear quadrupole trap into the mass analyzer, a device with large trap capacity and high optical access is realized without sacrificing mass resolution. This provides the ability to address trapped ions with laser light and facilitates interactions with neutral background gases prior to analyzing the trapped ions. Here, we describe the construction and implementation of the device as well as present representative ToF spectra. We conclude by demonstrating the flexibility of the device with proof-of-principle experiments that include the observation of molecular-ion photodissociation and the measurement of trapped-ion chemical reaction rates. © 2012 American Institute of Physics

  2. Multipole traps for non-neutral plasmas

    International Nuclear Information System (INIS)

    Tiouririne, T.N.; Turner, L.; Lau, A.W.C.

    1994-01-01

    A multipolar generalization of the Penning trap is presented. The case of l=1 is that of standard Penning trap. For the case of a quadrupolar magnetic field, analytic solutions are presented for cold, confined, one-species plasmas with spheroidal or spherical boundaries; for higher l values analytic solutions are given only for spherically bounded plasmas. By virtue of the sheared flow present for solutions with l>1, the classical Brillouin ratio (stored rest energy of particles/stored magnetic energy) of unity is exceeded and attains a global limit of 2 at infinitely high l

  3. Design, construction and commissioning of an ortho-TOF mass spectrometer for investigations of exotic nuclei

    International Nuclear Information System (INIS)

    Eliseev, S.

    2004-01-01

    Precise atomic mass measurements are very important in many disciplines of science, e.g. in physics, biochemistry, medicine, archaeology and environmental research. In nuclear physics, mass measurements of nuclides are essential for testing nuclear mass models. From the knowledge of the mass of a nuclide the nuclear binding energy can be derived. The mass measurements provide a better knowledge of the strong interaction between the constituents in the nucleus. In nuclear astrophysics, mass measurements of exotic nuclides are of great importance for our understanding of the synthesis of the elements. In biochemistry and medicine, mass measurement methods are helpful in a structural analysis of complex biomolecules. Mass measurement techniques are widely used in the trace analysis of poisonous substances in environmental research. Leak searchers and rest gas analysers are also based on the principles of mass measurements. The most precise methods of mass measurements, employed in nuclear physics, are based either on the determination of the time of flight (TOF), the revolution frequency (RF), or cyclotron frequency (CF) of the ion in mass spectrometers. Nowadays, there are several scientific centers such as GSI, CERN, GANIL and ANL employing these techniques. The RF-technique is realized at GSI in the Experimental Storage Ring (ESR) (Schottky Mass Spectrometry SMS and Isochronous Mass Spectrometry IMS) for ions produced in the in-flight FRagment Separator (FRS). At GANIL, the TOF-technique is employed at the Second Separated-Sector Cyclotron (CSS2) and at the Spectrometre a Perte d'Energie du Ganil (SPEG). The CF-technique is implemented in MISTRALand in Penning traps ISOLTRAP at ISOLDE (CERN). The CF- technique is also used at SHIPTRAP at GSI and at the Canadian Penning Trap (CPT), coupled to the Argonne Tandem Linac Accelerating System (ATLAS) at ANL. In the following the relative accuracy of mass determination achieved by the above mentioned techniques and typical

  4. Precision mass measurements for studies of nucleosynthesis via the rapid neutron-capture process Penning-trap mass measurements of neutron-rich cadmium and caesium isotopes

    CERN Document Server

    AUTHOR|(CDS)2085660; Litvinov, Yuri A.; Kreim, Susanne

    Although the theory for the rapid neutron-capture process (r-process) was developed more than 55 years ago, the astrophysical site is still under a debate. Theoretical studies predict that the r-process path proceeds through very neutron-rich nuclei with very asymmetric proton- to-neutron ratios. Knowledge about the properties of neutron-rich isotopes found in similar regions of the nuclear chart and furthermore suitable for r-process studies is still little or even not existing. The basic nuclear properties such as binding energies, half-lives, neutron-induced or neutron-capture reaction cross-sections, play an important role in theoretical simulations and can vary or even drastically alternate results of these studies. Therefore, a considerable effort was put forward to access neutron-rich isotopes at radioactive ion-beam facilities like ISOLDE at CERN. The goal of this PhD thesis is to describe the experimental work done for the precision mass measurements of neutron-rich cadmium (129−131 Cd) and caesium...

  5. Concurrent Mass Measurement and Laser Spectroscopy for Unambiguous Isomeric State Assignment

    Science.gov (United States)

    Lascar, Daniel; Babcock, Carla; Henderson, Jack; Pearson, Matt

    2017-09-01

    Recent work by the TITAN group at TRIUMF on isomeric state mass measurements of odd-A, neutron-rich cadmium nuclei has shown a disconnect between experiment and theory in 127 g , mCd. The spin and parity assignments of the ground and isomeric states are assigned as 3/2+ and 11/2-, respectively, primarily via systematic arguments. Conversely, state of the art shell model and ab initio calculations show a reversal of the states, predicting a ground state of 11/2- and a 3/2+ isomer. Penning Trap Mass Spectrometry (PTMS) can measure the energy separation between the ground state and the isomer without ambiguity but cannot, on its own, comment on the spin and parity. Collinear Laser Spectroscopy (CLS) experiments have been performed on 127Cd and have elegantly demonstrated the existence of both 3/2+ and 11/2- states. What CLS cannot do, on its own, is assign an ordering to those states. If, however, a PTMS and CLS experiment could be performed concurrently using identical beams from the same facility then there exists sufficient information shared between both experiments that a definitive assignment can be made. We present a concept for a new slate of measurements using existing experimental facilities simultaneously, with shared resources, to definitively assign spin and parity for ground and isomeric states in short-lived nuclei.

  6. Search for new candidates for the neutrino-oriented mass determination by electron-capture

    CERN Multimedia

    Herfurth, F; Boehm, C; Blaum, K; Beck, D

    2008-01-01

    This proposal is part of an extended program dedicated to the neutrino-mass determination in the electron-capture sector, which aims at ultra-precise mass measurements by Penning traps in combination with cryogenic micro-calorimetry for atomic de-excitation measurements. Here, precise mass measurements with ISOLTRAP are proposed for the orbital electron-capture nuclides $^{194}$Hg and $^{202}$Pb, as well as their daughters, with the goal to determine accurately their Q-values. These values are expected to be the smallest ones among a great variety of known electron-capture precursors. Therefore, these nuclides are strong candidates for an improved electron-neutrino mass determination. We ask for 8 shifts of on-line beam at ISOLDE for mass measurements of $^{194}$Hg, $^{194}$ Au, $^{202}$Pb, and $^{202}$Tl at ISOLTRAP.

  7. Paper Spray Mass Spectrometry for the Forensic Analysis of Black Ballpoint Pen Inks

    Science.gov (United States)

    Amador, Victoria Silva; Pereira, Hebert Vinicius; Sena, Marcelo Martins; Augusti, Rodinei; Piccin, Evandro

    2017-09-01

    This article describes the use of paper spray mass spectrometry (PS-MS) for the direct analysis of black ink writings made with ballpoint pens. The novel approach was developed in a forensic context by first performing the classification of commercially available ballpoint pens according to their brands. Six of the most commonly worldwide utilized brands (Bic, Paper Mate, Faber Castell, Pentel, Compactor, and Pilot) were differentiated according to their characteristic chemical patterns obtained by PS-MS. MS on the negative ion mode at a mass range of m/ z 100-1000 allowed prompt discrimination just by visual inspection. On the other hand, the concept of relative ion intensity (RII) and the analysis at other mass ranges were necessary for the differentiation using the positive ion mode. PS-MS combined with partial least squares (PLS) was utilized to monitor changes on the ink chemical composition after light exposure (artificial aging studies). The PLS model was optimized by variable selection, which allowed the identification of the most influencing ions on the degradation process. The feasibility of the method on forensic investigations was also demonstrated in three different applications: (1) analysis of overlapped fresh ink lines, (2) analysis of old inks from archived documents, and (3) detection of alterations (simulated forgeries) performed on archived documents. [Figure not available: see fulltext.

  8. An aircraft-borne chemical ionization – ion trap mass spectrometer (CI-ITMS for fast PAN and PPN measurements

    Directory of Open Access Journals (Sweden)

    H. Schlager

    2011-02-01

    Full Text Available An airborne chemical ionization ion trap mass spectrometer instrument (CI-ITMS has been developed for tropospheric and stratospheric fast in-situ measurements of PAN (peroxyacetyl nitrate and PPN (peroxypropionyl nitrate. The first scientific deployment of the FASTPEX instrument (FASTPEX = Fast Measurement of Peroxyacyl nitrates took place in the Arctic during 18 missions aboard the DLR research aircraft Falcon, within the framework of the POLARCAT-GRACE campaign in the summer of 2008. The FASTPEX instrument is described and characteristic properties of the employed ion trap mass spectrometer are discussed. Atmospheric data obtained at altitudes of up to ~12 km are presented, from the boundary layer to the lowermost stratosphere. Data were sampled with a time resolution of 2 s and a 2σ detection limit of 25 pmol mol−1. An isotopically labelled standard was used for a permanent on-line calibration. For this reason the accuracy of the PAN measurements is better than ±10% for mixing ratios greater than 200 pmol mol−1. PAN mixing ratios in the summer Arctic troposphere were in the order of a few hundred pmol mol−1 and generally correlated well with CO. In the Arctic boundary layer and lowermost stratosphere smaller PAN mixing ratios were observed due to a combination of missing local sources of PAN precursor gases and efficient removal processes (thermolysis/photolysis. PPN, the second most abundant PAN homologue, was measured simultaneously. Observed PPN/PAN ratios range between ~0.03 and 0.3.

  9. Radiochemical measurement of mass transport in sodium

    International Nuclear Information System (INIS)

    Cooper, M.H.; Chiang, S.H.

    1976-01-01

    Mass transport processes in the sodium coolant of Liquid Metal Fast Breeder Reactors (LMFBRs) are significant in determining rates of corrosion and deposition of radioactive nuclides from the fuel cladding, deposition and cold trapping of fission products from defect or failed fuel, carbon and nitrogen redistribution in the containment materials, and removal of impurities by cold trapping or hot trapping. Mass transport between rotating, concentric cylinders in molten sodium has been investigated using a unique radiochemical method. Long-lived (33 year) cesium-137, dissolved in the sodium, decays radioactively emitting a beta to barium-137m, which decays with a short half-life (2.6 minutes) emitting a gamma. Cesium is weakly adsorbed and remains in solution, while the barium is strongly adsorbed on the stainless steel surfaces. Hence, by measuring the barium-137m activity on movable stainless steel surfaces, one can calculate the mass transport to that surface. Mass transfer coefficients in sodium measured by this method are in agreement with published heat transfer correlations when the effect of the volumetric mass source is taken into account. Hence, heat transfer correlations can be confidently utilized by analogy in estimating mass transfer in liquid-metal systems

  10. Chemical characterization of microparticles by laser ablation in an ion trap mass spectrometer

    International Nuclear Information System (INIS)

    Dale, J.M.; Whitten, W.B.; Ramsey, J.M.

    1991-01-01

    We are developing a new technique for the chemical characterization of microparticles based upon the use of electrodynamic traps. The electrodynamic trap has achieved widespread use in the mass spectrometry community in the form of the ion trap mass spectrometer or quadrupole ion trap. Small macroscopic particles can be confined or levitated within the electrode structure of a three-dimensional quadrupole electrodynamic trap in the same way as fundamental charges or molecular ions by using a combination of ac and dc potentials. Our concept is to use the same electrode structure to perform both microparticle levitation and ion trapping/mass analysis. The microparticle will first be trapped and spatially stabilized within the trap for characterization by optical probes, i.e., absorption, fluorescence, or Raman spectroscopy. After the particle has been optically characterized, it is further characterized using mass spectrometry. Ions are generated from the particle surface using laser ablation or desorption. The characteristics of the applied voltages are changed to trap the ions formed by the laser with the ions subsequently mass analyzed. The work described in this paper focuses on the ability to perform laser desorption experiments on microparticles contained within the ion trap

  11. Toward sub-Kelvin resistive cooling and non destructive detection of trapped non-neutral electron plasma

    Science.gov (United States)

    Di Domizio, S.; Krasnický, D.; Lagomarsino, V.; Testera, G.; Vaccarone, R.; Zavatarelli, S.

    2015-01-01

    A resonant circuit tuned to a particular frequency of the motion of charged particles stored in a Penning trap and connected to a low noise amplifier allows, at the same time, cooling and non destructive detection of the particles. Its use is widely diffused when single or few particles are stored near the centre of a hyperbolic Penning trap. We present a consistent model that predicts the shape of the induced signal when the tuned circuit is used to detect and cool the axial motion of a cold non neutral plasma stored in an open-ended cylindrical Penning trap. The model correctly accounts for the not negligible axial plasma size. We show that the power spectrum of the signal measured across the tuned circuit provides information about the particle number and insights about the plasma temperature. We report on the design of a HEMT-based cryogenic amplifier working at 14.4 MHz and 4.2 K and the results of the noise measurements. We have measured a drain current noise in the range from 6 to 17 pA/√Hz, which corresponds to an increase of the tuned circuit equivalent temperature of at maximum 0.35 K. The cryogenic amplifier has a very low power consumption from few tens to few hundreds of μW corresponding to a drain current in the range 100-800 μ A. An additional contribution due to the gate noise has been identified when the drain current is below 300 μA above that value an upper limit of the increase of the equivalent tuned circuit temperature due to this contribution of 0.02 K has been obtained. These features make the tuned circuit connected to this amplifier a promising device for detecting and cooling the axial motion of an electron plasma when the Penning trap is mounted inside a dilution refrigerator.

  12. Multi-Reflection Time-of-Flight Mass Separation and Spectrometry

    CERN Document Server

    Kreim, Susanne; Wolf, R N

    2014-01-01

    The mass of a nucleus is one of its most fundamental ground-state properties and reveals the strength of nuclear binding. Investigating the binding energy of nuclei with respect to the number of protons and neutrons in a nucleus is important for advancing nuclear theory and increases our understanding of nucleosynthesis in supernovae and neutron stars. Precision mass measurements on radioactive nuclides belong to the state-of-the-art techniques [1, 2]. Presently, four complementary techniques are applied: isochronous and Schottky mass spectrometry in storage rings (IMS and SMS, respectively), magnetic-rigidity time-of-flight (TOF-ρ) measurements, and Penning-trap mass spectrometry (PTMS). With measurement cycles in the sub-ms range, IMS and TOF-Bρ MS are well suited for very short-lived species while offering moderate relative precision on the level of 10−6. A higher precision is achieved by SMS but with the need for measurement times on the order of several seconds. As soon as masses with a relative prec...

  13. Observation of Spin Flips with a Single Trapped Proton

    CERN Document Server

    Ulmer, S.; Blaum, K.; Kracke, H.; Mooser, A.; Quint, W.; Walz, J.

    2011-01-01

    Spin transitions of an isolated trapped proton are observed for the first time. The spin quantum jumps are detected via the continuous Stern-Gerlach effect which is used in an experiment with a single proton stored in a cryogenic Penning trap. This opens the way for a direct high-precision measurement of the magnetic moment of the proton and a new test of the matter-antimatter symmetry in the baryon sector. This method can also be applied to other light atomic nuclei.

  14. Mass sensors with mechanical traps for weighing single cells in different fluids.

    Science.gov (United States)

    Weng, Yaochung; Delgado, Francisco Feijó; Son, Sungmin; Burg, Thomas P; Wasserman, Steven C; Manalis, Scott R

    2011-12-21

    We present two methods by which single cells can be mechanically trapped and continuously monitored within the suspended microchannel resonator (SMR) mass sensor. Since the fluid surrounding the trapped cell can be quickly and completely replaced on demand, our methods are well suited for measuring changes in cell size and growth in response to drugs or other chemical stimuli. We validate our methods by measuring the density of single polystyrene beads and Saccharomyces cerevisiae yeast cells with a precision of approximately 10(-3) g cm(-3), and by monitoring the growth of single mouse lymphoblast cells before and after drug treatment.

  15. Extending and refining the nuclear mass surface with ISOLTRAP and MISTRAL

    CERN Document Server

    Lunney, M D

    2000-01-01

    Through the nuclear binding energy the atomic mass gives us important information about nuclear structure. Viewing the ensemble of mass data over the nuclear chart, we can examine the hills and valleys that form this surface and make hypotheses about the effects of certain nuclear configurations. To unveil these effects, mass measurements of very high precision (10$^{-6}$) are required. Two experiments at ISOLDE pursue this effort of nuclear cartography the tandem Penning trap spectrometer ISOLTRAP and the radiofrequency transmission spectrometer MISTRAL. Between them, the masses of almost 150 nuclides have been measured from stable isotopes to those with half-lives as short as 30 ms. Both experiments rely on good optical properties of a low energy ion beam and are thus well suited to the ISOLDE facility. (30 refs).

  16. Population Dynamic Observation And Mass Trapping Of Fruit Fly Bactrocera Carambolae (Drew and Hancock)

    International Nuclear Information System (INIS)

    Kuswadi, Achmad Nasroh; Indarwatmi, Murni; Nasution, Indah A.; Darwani; Himawan, Toto

    2000-01-01

    In connection with the control of B. carambolae, major pest of mango fruit in Indonesia using sterile insect technique, population monitoring with methyl eugenol attractant baited traps, absolute population measurement with release and recapture techniques, and mass trapping to reduce population of the pest in mango orchards were conducted. Based on the number of the male fly trapped it was know that the fly population was always low when no mature mango fruit found on the orchard, and it strated to increase in October, the middle time, of mango harvest until some time after the end of harvesting time. In August, when the population was low, about 4000 flies/hectare or 600 flies/hectare were found in the extensive and intensive culture orchards respectively. Mass trapping with 4 trapps per hectare was able to kill about 620 and 240 male flies per hectare of the extensive and intensive culture orchards respectively

  17. Chemical characterization of microparticles by laser ablation in an ion trap mass spectrometer

    International Nuclear Information System (INIS)

    Dale, J.M.; Whitten, W.B.; Ramsey, J.M.

    1991-01-01

    We are developing a new technique for the chemical characterization of microparticles based upon the use of electrodynamic traps. The electrodynamic trap has achieved widespread use in the mass spectrometry community in the form of the ion trap mass spectrometer or quadrupole ion trap. Small macroscopic particles can be confined or leviated within the electrode structure of a three-dimensional quadrupole electrodynamic trap in the same way as fundamental charges or molecular ions by using a combination of ac and dc potentials. Our concept is to use the same electrode structure to perform both microparticle levitation and ion trapping/mass analysis. The microparticle will first be trapped and spatially stabilized within the trap for characterization by optical probes, i.e., absorption, fluorescence, or Raman spectroscopy. After the particle has been optically characterized, it is further characterized using mass spectrometry. Ions are generated from the particle surface using laser ablation or desorption. The characteristics of the applied voltages are changed to trap the ions formed by the laser with the ions subsequently mass analyzed. The work described in this paper focuses on the ability to perform laser desorption experiments on microparticles contained within the ion trap. Laser desorption has previously been demonstrated in ion trap devices by applying the sample to a probe which is inserted so as to place the sample at the surface of the ring electrode. Our technique requires the placement of a microparticle in the center of the trap. Our initial experiments have been performed on falling microparticles rather than levitated particles to eliminate voltage switching requirements when changing from particle to ion trapping modes

  18. A quantum mechanical model of Rabi oscillations between two interacting harmonic oscillator modes and the interconversion of modes in a Penning trap

    International Nuclear Information System (INIS)

    Kretzschmar, Martin

    1999-01-01

    When a Penning trap is operated with an additional quadrupole driving field with a frequency that equals a suitable combination (sum or difference) of the frequencies of the fundamental modes of motion (modified cyclotron, magnetron and axial frequency), then a periodic conversion of the participating modes into each other is observed, strongly resembling the Rabi oscillations in a 2-level atom driven by a laser field tuned to the transition frequency. This investigation attempts to understand on a fundamental level how and why the motion of a classical particle in a macroscopic apparatus can be truely analogous to the oscillations of states of quantum mechanical 2-level systems (2-level atom or magnetic resonance). Ion motion in a Penning trap with an additional quadrupole driving field is described in a quantum mechanical frame work. The Heisenberg equations of motion for the creation and annihilation operators of the interacting oscillators have been explicitly solved, the time development operator of the Schroedinger picture has been determined. The driving field provides for two types of intermode interaction: Type I preserves the total number of excitation quanta present in the two interacting modes, the system oscillates between the modes with a frequency corresponding to the Rabi frequency in two-level systems. Type II preserves the difference of the numbers of excitation quanta present in the two interacting modes, it causes the ion motion to become unbounded. The two types of interaction are associated in a natural way with a SU(2) and a SU(1,1) Lie algebra. The three generators of these algebras form a vector operator that we denote as the Bloch vector operator. The Hilbert space decomposes in a natural way into invariant subspaces, finite dimensional in the case of type I interaction (SU(2)-algebra) and infinite dimensional in the case of type II interaction (SU(1,1)-algebra). The physics of the 2-level atom in the laser field can be described in the 2

  19. Lifetime measurements in an electrostatic ion beam trap using image charge monitoring

    International Nuclear Information System (INIS)

    Rahinov, Igor; Toker, Yoni; Heber, Oded; Rappaport, Michael; Zajfman, Daniel; Strasser, Daniel; Schwalm, Dirk

    2012-01-01

    A technique for mass-selective lifetime measurements of keV ions in a linear electrostatic ion beam trap is presented. The technique is based on bunching the ions using a weak RF potential and non-destructive ion detection by a pick-up electrode. This method has no mass-limitation, possesses the advantage of inherent mass-selectivity, and offers a possibility of measuring simultaneously the lifetimes of different ion species with no need for prior mass-selection.

  20. Direct trace analysis of metals and alloys in a quadrupole ion-trap mass spectrometer

    CERN Document Server

    Song, K S; Yang, M; Cha, H K; Lee, J M; Lee, G H

    1999-01-01

    An ion-trap mass spectrometer adopting a quadrupole ion-trap and laser ablation/ionization method was constructed. The developed system was tested for composition analysis of some metals (Cu, stainless), and alloys (hastalloy C, mumetal) by mass spectrometry. Samples were analyzed by using laser ablation from a sample probe tip followed by a mass analysis with the quadrupole ion-trap. The quadrupole ion-trap was modified to enable laser ablation by a XeCl excimer laser pulse that passed radially through the ring electrode. A mass scan of the produced ions was performed in the mass selective instability mode wherein trapped ions were successively detected by increasing the rf voltage through the ring electrode. Factors affecting the mass resolution, such as pressure of buffer gas and ablation laser power, are discussed.

  1. The mass of $^{22}$Mg and a concept for a novel laser ion source trap

    CERN Document Server

    Mukherjee, Manas

    Clean and high-quality radioactive ion beams can be prepared by combining ion trap and resonance laser ionization techniques. A feasibility study for such a laser ion source trap has been carried out which shows enormous improvement in the beam emittance, purity, and in addition allows for a variation of the ion beam time structure. Direct high-precision mass measurements around mass number A=22 are of utmost importance. First, the masses of the superallowed $\\beta$-emitter $^{22}$Mg and its daughter $^{22}$Na are needed to test the conserved-vector-current(CVC) hypothesis and the Cabibbo-Kobayashi-Maskawa(CKM) matrix unitarity, both being predictions of the Standard Model. Second, to calculate the reaction rate of $^{21}$Na($p,\\gamma$)$^{22}$Mg the involved masses are required very accurately. This rate is needed in order to extract an upper limit on the amount of a characteristic $\\gamma$-radiation emitted from classical nova bursts which has been searched for but not yet detected. At the triple trap mass s...

  2. Practical aspects of trapped ion mass spectrometry, 4 theory and instrumentation

    CERN Document Server

    March, Raymond E

    2010-01-01

    The expansion of the use of ion trapping in different areas of mass spectrometry and different areas of application indicates the value of a single source of information drawing together diverse inputs. This book provides an account of the theory and instrumentation of mass spectrometric applications and an introduction to ion trapping devices.

  3. Mass and QEC value of 26Si

    International Nuclear Information System (INIS)

    Eronen, T.; Elomaa, V.-V.; Hager, U.; Hakala, J.; Jokinen, A.; Kankainen, A.; Kessler, T.; Moore, I. D.; Rahaman, S.; Rissanen, J.; Weber, C.; Aeystoe, J.

    2009-01-01

    The Q EC value of the superallowed β emitter 26 Si has been measured with the JYFLTRAP Penning trap facility to be 4840.85(10) keV which is ten times more precise than any previous measurement. This leaves only the branching ratio to be improved before the Ft value of 26 Si can be used to test the conserved vector current hypothesis. As a consequence, the 25 Al(p,γ) 26 Si reaction Q-value (Q pγ ) was improved to be 5513.7(5) keV, limited now by the mass excess of 25 Al. The new Q pγ value changes the stellar production rate of 26 Si in nova ignition temperatures by about 10%

  4. New Isotope Analysis Method: Atom Trap Mass Spectrometry

    International Nuclear Information System (INIS)

    Ko, Kwang Hoon; Park, Hyun Min; Han, Jae Min; Kim, Taek Soo; Cha, Yong Ho; Lim, Gwon; Jeong, Do Young

    2011-01-01

    Trace isotope analysis has been an important role in science, archaeological dating, geology, biology and nuclear industry. Some fission products such as Sr-90, Cs-135 and Kr-85 can be released to the environment when nuclear accident occurs and the reprocessing factory operates. Thus, the analysis of artificially produced radioactive isotopes has been of interest in nuclear industry. But it is difficult to detect them due to low natural abundance less then 10 -10 . In general, radio-chemical method has been applied to detect ultra-trace radio isotopes. But this method has disadvantages of long measurement time for long lived radioisotopes and toxic chemical process for the purification. The Accelerator Mass Spectrometer has high isotope selectivity, but the system is huge and its selectivity is affected by isobars. The laser based method, such as RIMS (Resonance Ionization Mass Spectrometry) has the advantage of isobar-effect free characteristics. But the system size is still huge for high isotope selective system. Recently, ATTA (Atom Trap Trace Analysis) has been successfully applied to detect ultra-trace isotope, Kr-81 and Kr-85. ATTA is the isobar-effect free detection with high isotope selectivity and the system size is small. However, it requires steady atomic beam source during detection, and is not allowed simultaneous detection of several isotopes. In this presentation, we introduce new isotope detection method which is a coupled method of Atom Trap Mass Spectrometry (ATMS). We expect that it can overcome the disadvantage of ATTA while it has both advantages of ATTA and mass spectrometer. The basic concept and the system design will be presented. In addition, the experimental status of ATMS will also be presented

  5. Production of cold antihydrogen in a nested trap

    International Nuclear Information System (INIS)

    Fujiwara, Makoto

    2004-01-01

    The ATHENA experiment at CERN produced and detected the first cold antihydrogen atoms. Antiprotons and positrons are mixed in a double Penning trap, known as a nested trap. The production of antihydrogen atoms was identified by detecting their annihilations signatures at trap wall. With the ATHENA results subsequently confirmed by another CERN experiment, ATRAP, cold antihydrogen research is entering an exciting era. (author)

  6. Trapping and Evolution Dynamics of Ultracold Two-Component Plasmas

    International Nuclear Information System (INIS)

    Choi, J.-H.; Knuffman, B.; Zhang, X. H.; Povilus, A. P.; Raithel, G.

    2008-01-01

    We demonstrate the trapping of a strongly magnetized, quasineutral ultracold plasma in a nested Penning trap with a background field of 2.9 T. Electrons remain trapped in this system for several milliseconds. Early in the evolution, the dynamics are driven by a breathing-mode oscillation in the ionic charge distribution, which modulates the electron trap depth. Over longer times scales, the electronic component undergoes cooling. Trap loss resulting from ExB drift is characterized

  7. A flexible approach to light pen calibration for a monocular-vision-based coordinate measuring system

    International Nuclear Information System (INIS)

    Fu, Shuai; Zhang, Liyan; Ye, Nan; Liu, Shenglan; Zhang, WeiZhong

    2014-01-01

    A monocular-vision-based coordinate measuring system (MVB-CMS) obtains the 3D coordinates of the probe tip center of a light pen by analyzing the monocular image of the target points on the light pen. The light pen calibration, including the target point calibration and the probe tip center calibration, is critical to guarantee the accuracy of the MVB-CMS. The currently used method resorts to special equipment to calibrate the feature points on the light pen in a separate offsite procedure and uses the system camera to calibrate the probe tip center onsite. Instead, a complete onsite light pen calibration method is proposed in this paper. It needs only several auxiliary target points with the same visual features of the light pen targets and two or more cone holes with known distance(s). The target point calibration and the probe tip center calibration are jointly implemented by simply taking two groups of images of the light pen with the camera of the system. The proposed method requires no extra equipment other than the system camera for the calibration, so it is easier to implement and flexible for use. It has been incorporated in a large field-of-view MVB-CMS, which uses active luminous infrared LEDs as the target points. Experimental results demonstrate the accuracy and effectiveness of the proposed method. (paper)

  8. Precision electron-capture energy in {sup 202}Pb and its relevance for neutrino mass determination

    Energy Technology Data Exchange (ETDEWEB)

    Welker, A. [CERN, Geneva (Switzerland); Technische Universitaet Dresden, Dresden (Germany); Filianin, P. [Max-Planck-Institut fuer Kernphysik, Heidelberg (Germany); Petersburg Nuclear Physics Institute, Gatchina (Russian Federation); Althubiti, N.A.S. [The University of Manchester, School of Physics and Astronomy, Manchester (United Kingdom); Atanasov, D.; Blaum, K.; Eliseev, S.; Kreim, S. [Max-Planck-Institut fuer Kernphysik, Heidelberg (Germany); Cocolios, T.E. [The University of Manchester, School of Physics and Astronomy, Manchester (United Kingdom); KU Leuven, Instituut voor Kern- en Stralingsfysica, Leuven (Belgium); Herfurth, F.; Neidherr, D. [GSI Helmholtzzentrum fuer Schwerionenforschung GmbH, Darmstadt (Germany); Lunney, D. [CSNSM-IN2P3-CNRS, Universite Paris-Sud, Orsay (France); Manea, V. [CERN, Geneva (Switzerland); Novikov, Yu. [Max-Planck-Institut fuer Kernphysik, Heidelberg (Germany); Petersburg Nuclear Physics Institute, Gatchina (Russian Federation); Physics Faculty, St. Petersburg State University (Russian Federation); Rosenbusch, M.; Schweikhard, L.; Wienholtz, F. [Ernst-Moritz-Arndt-Universitaet, Institut fuer Physik, Greifswald (Germany); Wolf, R.N. [Max-Planck-Institut fuer Kernphysik, Heidelberg (Germany); The University of Sydney, ARC Centre of Excellence for Engineered Quantum Systems, Sydney (Australia); Zuber, K. [Technische Universitaet Dresden, Dresden (Germany)

    2017-07-15

    Within the framework of an extensive programme devoted to the search for alternative candidates for the neutrino mass determination, the atomic mass difference between {sup 202}Pb and {sup 202}Tl has been measured with the Penning trap mass spectrometer ISOLTRAP at the ISOLDE facility at CERN. The obtained value Q{sub EC} = 38.8(43) keV is three times more precise than the AME2012 value. While it will probably not lead to a replacement of {sup 163}Ho in modern experiments on the determination of the electron-neutrino mass, the electron capture in {sup 202}Pb would however allow a determination of the electron-neutrino mass on the few-eV level using a cryogenic micro-calorimeter. (orig.)

  9. ATRAP on the way to trapped Antihydrogen

    CERN Document Server

    Grzonka, D; Gabrielse, G; Goldenbaum, F; Hänsch, T W; Hessels, E A; Larochelle, P; Le Sage, D; Levitt, B; Oelert, W; Pittner, H; Sefzick, T; Speck, A; Storry, C H; Walz, J; Zhang, Z

    2005-01-01

    The ATRAP experiment at the CERN antiproton decelerator AD aims for a test of the CPT invariance by a high precision comparison of the 1s‐2s transition in the hydrogen and the antihydrogen atom. Antihydrogen production is routinely operated at ATRAP and detailed studies have been performed in order to optimize the production efficiency of useful antihydrogen. The shape parameters of the antiproton and positron clouds, the n‐state distribution of the produced Rydberg antihydrogen atoms and the antihydrogen velocity have been studied. Furthermore an alternative method of laser controlled antihydrogen production was successfully applied. For high precision measurements of atomic transitions cold antihydrogen in the ground state is required which must be trapped due to the low number of available antihydrogen atoms compared to the cold hydrogen beam used for hydrogen spectroscopy. To ensure a reasonable antihydrogen trapping efficiency a magnetic trap has to be superposed the nested Penning trap. First trappi...

  10. Double-trap measurement of the proton magnetic moment at 0.3 parts per billion precision.

    Science.gov (United States)

    Schneider, Georg; Mooser, Andreas; Bohman, Matthew; Schön, Natalie; Harrington, James; Higuchi, Takashi; Nagahama, Hiroki; Sellner, Stefan; Smorra, Christian; Blaum, Klaus; Matsuda, Yasuyuki; Quint, Wolfgang; Walz, Jochen; Ulmer, Stefan

    2017-11-24

    Precise knowledge of the fundamental properties of the proton is essential for our understanding of atomic structure as well as for precise tests of fundamental symmetries. We report on a direct high-precision measurement of the magnetic moment μ p of the proton in units of the nuclear magneton μ N The result, μ p = 2.79284734462 (±0.00000000082) μ N , has a fractional precision of 0.3 parts per billion, improves the previous best measurement by a factor of 11, and is consistent with the currently accepted value. This was achieved with the use of an optimized double-Penning trap technique. Provided a similar measurement of the antiproton magnetic moment can be performed, this result will enable a test of the fundamental symmetry between matter and antimatter in the baryonic sector at the 10 -10 level. Copyright © 2017, American Association for the Advancement of Science.

  11. Physics with Trapped Antihydrogen

    Science.gov (United States)

    Charlton, Michael

    2017-04-01

    For more than a decade antihydrogen atoms have been formed by mixing antiprotons and positrons held in arrangements of charged particle (Penning) traps. More recently, magnetic minimum neutral atom traps have been superimposed upon the anti-atom production region, promoting the trapping of a small quantity of the antihydrogen yield. We will review these advances, and describe some of the first physics experiments performed on anrtihydrogen including the observation of the two-photon 1S-2S transition, invesigation of the charge neutrailty of the anti-atom and studies of the ground state hyperfine splitting. We will discuss the physics motivations for undertaking these experiments and describe some near-future initiatives.

  12. Winter School on Physics with Trapped Charged Particles - Abstracts and slides

    International Nuclear Information System (INIS)

    Pedersen, T.S.; Thompson, R.C.; Madsen, N.; Champenois, C.; Anderegg, F.; Fajans, J.; Knoop, M.; Scott Hangst, J.; Hilico, L.; Ulmer, S.; Blaum, K.; Drewsen, M.; Roos, C.; Schmidt, P.

    2016-01-01

    This winter school covered various topics of the physics of trapped charged particles. Lectures covered basic trap physics and recent developments in Penning traps, Paul traps..., collective behavior and non-neutral plasmas, as well as applications for fundamental physics, laser cooling, precision spectroscopy and quantum information. This document gathers a booklet of abstracts and the available slides of the presentations

  13. A linear radiofrequency ion trap for accumulation, bunching, and emittance improvement of radioactive ion beams

    International Nuclear Information System (INIS)

    Herfurth, F.; Dilling, J.; Kellerbauer, A.

    2000-05-01

    An ion beam cooler and buncher has been developed for the manipulation of radioactive ion beams. The gas-filled linear radiofrequency ion trap system is installed at the Penning trap mass spectrometer ISOLTRAP at ISOLDE/CERN. Its purpose is to accumulate the 60-keV continuous ISOLDE ion beam with high efficiency and to convert it into low-energy low-emittance ion pulses. The efficiency was found to exceed 10% in agreement with simulations. A more than 10-fold reduction of the ISOLDE beam emittance can be achieved. The system has been used successfully for first on-line experiments. Its principle, setup and performance will be discussed. (orig.)

  14. Formation of Antihydrogen Rydberg atoms in strong magnetic field traps

    International Nuclear Information System (INIS)

    Pohl, T.; Sadeghpour, H. R.

    2008-01-01

    It is shown that several features of antihydrogen production in nested Penning traps can be described with accurate and efficient Monte Carlo simulations. It is found that cold deeply-bound Rydberg states of antihydrogen (H-bar) are produced in three-body capture in the ATRAP experiments and an additional formation mechanism -Rydberg charge transfer-, particular to the nested Penning trap geometry, is responsible for the observed fast (hot) H-bar atoms. Detailed description of the numerical propagation technique for following extreme close encounters is given. An analytic derivation of the power law behavior of the field ionization spectrum is provided

  15. Motion of guiding center drift atoms in the electric and magnetic field of a Penning trap

    International Nuclear Information System (INIS)

    Kuzmin, S.G.; O'Neil, T.M.

    2005-01-01

    The ApparaTus for High precision Experiment on Neutral Antimatter and antihydrogen TRAP collaborations have produced antihydrogen atoms by recombination in a cryogenic antiproton-positron plasma. This paper discusses the motion of the weakly bound atoms in the electric and magnetic field of the plasma and trap. The effective electric field in the moving frame of the atom polarizes the atom, and then gradients in the field exert a force on the atom. An approximate equation of motion for the atom center of mass is obtained by averaging over the rapid internal dynamics of the atom. The only remnant of the atom internal dynamics that enters this equation is the polarizability for the atom. This coefficient is evaluated for the weakly bound and strongly magnetized (guiding center drift) atoms understood to be produced in the antihydrogen experiments. Application of the approximate equation of motion shows that the atoms can be trapped radially in the large space charge field near the edge of the positron column. Also, an example is presented for which there is full three-dimensional trapping, not just radial trapping. Even untrapped atoms follow curved trajectories, and such trajectories are discussed for the important class of atoms that reach a field ionization diagnostic. Finally, the critical field for ionization is determined as an upper bound on the range of applicability of the theory

  16. Frequency-scanning MALDI linear ion trap mass spectrometer for large biomolecular ion detection.

    Science.gov (United States)

    Lu, I-Chung; Lin, Jung Lee; Lai, Szu-Hsueh; Chen, Chung-Hsuan

    2011-11-01

    This study presents the first report on the development of a matrix-assisted laser desorption ionization (MALDI) linear ion trap mass spectrometer for large biomolecular ion detection by frequency scan. We designed, installed, and tested this radio frequency (RF) scan linear ion trap mass spectrometer and its associated electronics to dramatically extend the mass region to be detected. The RF circuit can be adjusted from 300 to 10 kHz with a set of operation amplifiers. To trap the ions produced by MALDI, a high pressure of helium buffer gas was employed to quench extra kinetic energy of the heavy ions produced by MALDI. The successful detection of the singly charged secretory immunoglobulin A ions indicates that the detectable mass-to-charge ratio (m/z) of this system can reach ~385 000 or beyond.

  17. Applicability of hybrid linear ion trap-high resolution mass spectrometry and quadrupole-linear ion trap-mass spectrometry for mycotoxin analysis in baby food.

    Science.gov (United States)

    Rubert, Josep; James, Kevin J; Mañes, Jordi; Soler, Carla

    2012-02-03

    Recent developments in mass spectrometers have created a paradoxical situation; different mass spectrometers are available, each of them with their specific strengths and drawbacks. Hybrid instruments try to unify several advantages in one instrument. In this study two of wide-used hybrid instruments were compared: hybrid quadrupole-linear ion trap-mass spectrometry (QTRAP®) and the hybrid linear ion trap-high resolution mass spectrometry (LTQ-Orbitrap®). Both instruments were applied to detect the presence of 18 selected mycotoxins in baby food. Analytical parameters were validated according to 2002/657/CE. Limits of quantification (LOQs) obtained by QTRAP® instrument ranged from 0.45 to 45 μg kg⁻¹ while lower limits of quantification (LLOQs) values were obtained by LTQ-Orbitrap®: 7-70 μg kg⁻¹. The correlation coefficients (r) in both cases were upper than 0.989. These values highlighted that both instruments were complementary for the analysis of mycotoxin in baby food; while QTRAP® reached best sensitivity and selectivity, LTQ-Orbitrap® allowed the identification of non-target and unknowns compounds. Copyright © 2011 Elsevier B.V. All rights reserved.

  18. MOMA and other next-generation ion trap mass spectrometers for planetary exploration

    Science.gov (United States)

    Arevalo, R. D., Jr.; Brinckerhoff, W. B.; Getty, S.; Mahaffy, P. R.; van Amerom, F. H. W.; Danell, R.; Pinnick, V. T.; Li, X.; Grubisic, A.; Southard, A. E.; Hovmand, L.; Cottin, H.; Makarov, A.

    2016-12-01

    Since the 1970's, quadrupole mass spectrometer (QMS) systems have served as low-risk, cost-efficient means to explore the inner and outer reaches of the solar system. These legacy instruments have interrogated the compositions of the lunar exosphere (LADEE), surface materials on Mars (MSL), and the atmospheres of Venus (Pioneer Venus), Mars (MAVEN) and outer planets (Galileo and Cassini-Huygens). However, the in situ detection of organic compounds on Mars and Titan, coupled with ground-based measurements of amino acids in meteorites and a variety of organics in comets, has underlined the importance of molecular disambiguation in the characterization of high-priority planetary environments. The Mars Organic Molecule Analyzer (MOMA) flight instrument, centered on a linear ion trap, enables the in situ detection of volatile and non-volatile organics, but also the characterization of molecular structures through SWIFT ion isolation/excitation and tandem mass spectrometry (MSn). Like the SAM instrument on MSL, the MOMA investigation also includes a gas chromatograph (GC), thereby enabling the chemical separation of potential isobaric interferences based on retention times. The Linear Ion Trap Mass Spectrometer (LITMS; PI: William Brinckerhoff), developed to TRL 6 via the ROSES MatISSE Program, augments the core MOMA design and adds: expanded mass range (from 20 - 2000 Da); high-temperature evolved gas analysis (up to 1300°C); and, dual polarity detector assemblies (supporting the measurement of negative ions). The LITMS instrument will be tested in the field in 2017 through the Atacama Rover Astrobiology Drilling Studies (ARADS; PI: Brian Glass) ROSES PSTAR award. Following on these advancements, the Advanced Resolution Organic Molecule Analyzer (AROMA; PI: Ricardo Arevalo Jr.), supported through the ROSES PICASSO Program, combines a highly capable MOMA/LITMS-like linear ion trap and the ultrahigh resolution CosmOrbitrap mass analyzer developed by a consortium of five

  19. Extending the applicability of an open-ring trap to perform experiments with a single laser-cooled ion

    Energy Technology Data Exchange (ETDEWEB)

    Cornejo, J. M.; Colombano, M.; Doménech, J.; Rodríguez, D., E-mail: danielrodriguez@ugr.es [Departamento de Física Atómica, Molecular y Nuclear, Universidad de Granada, 18071 Granada (Spain); Block, M. [GSI Helmholtzzentrum für Schwerionenforschung GmbH, 64291 Darmstadt (Germany); Helmholtz-Institut Mainz, 55099 Mainz (Germany); Institut für Kernchemie, University of Mainz, 55099 Mainz (Germany); Delahaye, P. [Grand Accélérateur National d’Ions Lourds, 14000 Caen (France)

    2015-10-15

    A special ion trap was initially built up to perform β-ν correlation experiments with radioactive ions. The trap geometry is also well suited to perform experiments with laser-cooled ions, serving for the development of a new type of Penning trap, in the framework of the project TRAPSENSOR at the University of Granada. The goal of this project is to use a single {sup 40}Ca{sup +} ion as detector for single-ion mass spectrometry. Within this project and without any modification to the initial electrode configuration, it was possible to perform Doppler cooling on {sup 40}Ca{sup +} ions, starting from large clouds and reaching single ion sensitivity. This new feature of the trap might be important also for other experiments with ions produced at radioactive ion beam facilities. In this publication, the trap and the laser system will be described, together with their performance with respect to laser cooling applied to large ion clouds down to a single ion.

  20. 210Pb and Mass Flux Imbalance Between the Settling Particulates and Sediments at a Sediment Trap

    Science.gov (United States)

    Wu, C.; Chung, Y.; Hung, G.

    2005-05-01

    In order to evaluate the mass balance problems between the settling particulates and the underlying sediments, sediment traps were deployed at M1 site (21o32¡¦N, 119o28¡¦E; 2948m) where a box core was taken recently. The sediment trap results were previously published (Chung et al., 2004: Continental Shelf Research). We report here the 210Pb profile measured on this box core by determining its daughter, 210Po, with alpha spectrometry, assuming the paired nuclides are in radioactive equilibrium. The box core (33 cm long, taken in June, 2004) was analyzed for the distributions of its water content, loss on ignition (LOI), and 210Pb. The water content decreases with depth and averages about 55 percent; the LOI as a measure of the total organic matter (TOM) is fairly constant at about 12 percent. The 210Pb profile shows a general exponential decrease with depth, yielding a maximum sedimentation rate of 0.26cm/y, applying a constant flux and constant sedimentation rate model. This rate translates to a mass flux of 0.31g/cm2/y or about 8.5g/m2/d with a dry bulk density of 1.2g/cm3. Based on the excess 210Pb inventory integrated over the core length, the 210Pb flux is estimated at about 19.2dpm/cm2/y or 526dpm/cm2/d assuming at steady state. The 210Pb and mass fluxes obtained from the deepest trap at M1 were only 129dpm/m2/d and 0.55g/m2/d, respectively. The large ¡excess¡" of the 210Pb and mass fluxes in the sediments over those measured from the sediment trap (4 times in 210Pb flux and 14 times in mass flux) suggests either the sedimentation rate was overestimated due to neglect of the mixing effect, and/or large additional particulates, as resuspended sediments which contain less 210Pb, have been transported laterally near the bottom from elsewhere.

  1. Point-Mass Model for Nano-Patterning Using Dip-Pen Nanolithography (DPN

    Directory of Open Access Journals (Sweden)

    Seok-Won Kang

    2011-04-01

    Full Text Available Micro-cantilevers are frequently used as scanning probes and sensors in micro-electromechanical systems (MEMS. Usually micro-cantilever based sensors operate by detecting changes in cantilever vibration modes (e.g., bending or torsional vibration frequency or surface stresses - when a target analyte is adsorbed on the surface. The catalyst for chemical reactions (i.e., for a specific analyte can be deposited on micro-cantilevers by using Dip-Pen Nanolithography (DPN technique. In this study, we simulate the vibration mode in nano-patterning processes by using a Point-Mass Model (or Lumped Parameter Model. The results from the simulations are used to derive the stability of writing and reading mode for a particular driving frequency during the DPN process. In addition, we analyze the sensitivity of the tip-sample interaction forces in fluid (ink solution by utilizing the Derjaguin-Muller-Toporov (DMT contact theory.

  2. A metastable helium trap for atomic collision physics

    International Nuclear Information System (INIS)

    Colla, M.; Gulley, R.; Uhlmann, L.; Hoogerland, M.D.; Baldwin, K.G.H.; Buckman, S.J.

    1999-01-01

    Full text: Metastable helium in the 2 3 S state is an important species for atom optics and atomic collision physics. Because of its large internal energy (20eV), long lifetime (∼8000s) and large collision cross section for a range of processes, metastable helium plays an important role in atmospheric physics, plasma discharges and gas laser physics. We have embarked on a program of studies on atom-atom and electron-atom collision processes involving cold metastable helium. We confine metastable helium atoms in a magneto-optic trap (MOT), which is loaded by a transversely collimated, slowed and 2-D focussed atomic beam. We employ diode laser tuned to the 1083 nm (2 3 S 1 - 2 3 P2 1 ) transition to generate laser cooling forces in both the loading beam and the trap. Approximately 10 million helium atoms are trapped at temperatures of ∼ 1mK. We use phase modulation spectroscopy to measure the trapped atomic density. The cold, trapped atoms can collide to produce either atomic He + or molecular He 2 + ions by Penning Ionisation (PI) or Associative Ionisation (AI). The rate of formation of these ions is dependant upon the detuning of the trapping laser from resonance. A further laser can be used to connect the 2 3 S 1 state to another higher lying excited state, and variation of the probe laser detuning used to measure interatomic collision potential. Electron-atom collision processes are studied using a monochromatic electron beam with a well defined spatial current distribution. The total trap loss due to electron collisions is measured as a function of electron energy. Results will be presented for these atomic collision physics measurements involving cold, trapped metastable helium atoms. Copyright (1999) Australian Optical Society

  3. Management of Cosmopolites sordidus and Metamasius hemipterus in banana by pheromone-based mass trapping.

    Science.gov (United States)

    Alpizar, D; Fallas, M; Oehlschlager, A C; Gonzalez, L M

    2012-03-01

    Mass trapping Cosmopolites sordidus (Coleoptera, Curculionidae) using a pheromone-baited pitfall trap and Metamasius hemipterus (Coleoptera, Curculionidae) using a pheromone-sugarcane-baited open gallon trap was conducted in commercial banana. Four traps for each insect per hectare were placed in each of two 5-hectare plots of banana. Two additional 5-hectare plots were designated as controls and treated according to the plantation protocol. Capture rates of C. sordidus and M. hemipterus declined by >75 % over 10-12 months. In the banana growing region studied, corm damage was due primarily to C. sordidus, while only a minor amount of damage was attributable to M. hemipterus. Corm damage reduction in trapping plots was, thus, attributed primarily to C. sordidus trapping. In trapping plots, corm damage decreased by 61-64 % during the experiment. Banana bunch weights increased 23 % relative to control plots after 11-12 months of trapping. Fruit diameter did not vary between bunches harvested from trapping plots vs. control plots. Plant vigor, however, as determined by stem circumference at one meter above ground increased in plots with traps compared to control plots. Trapping for C. sordidus in two plantations of over 200 hectares each, reduced corm damage 62-86 % relative to pre-trapping levels. Insecticide control measures in place when the experiment commenced resulted in about 20-30 % corm damage, while use of pheromone trapping to manage C. sordidus lowered corm damage to 10 % or less. It is estimated that the increase in value of increased yield obtained in this trial (23 %) is about $4,240 USD per year per hectare, while the cost of pheromone trapping is approximately $185 USD per year per hectare. The trapping program becomes revenue neutral if bunch weights increase by an average of 1 % per year of trapping. Approximately 10 % of all plantation area in Costa Rica use the pheromone trapping system described here. The system also is used in Martinique

  4. Direct neutrino mass measurements

    Energy Technology Data Exchange (ETDEWEB)

    Weinheimer, Christian, E-mail: weinheimer@uni-muenster.de [Westfaelische Wilhelms-Universitaet, Institut fuer Kernphysik (Germany)

    2013-03-15

    Direct neutrino mass experiments are complementary to searches for neutrinoless double {beta}-decay and to analyses of cosmological data. The previous tritium beta decay experiments at Mainz and at Troitsk have achieved upper limits on the neutrino mass of about 2 eV/c{sup 2} . The KATRIN experiment under construction will improve the neutrino mass sensitivity down to 200 meV/c{sup 2} by increasing strongly the statistics and-at the same time-reducing the systematic uncertainties. Huge improvements have been made to operate the system extremely stably and at very low background rate. The latter comprises new methods to reject secondary electrons from the walls as well as to avoid and to eject electrons stored in traps. As an alternative to tritium {beta}-decay experiments cryo-bolometers investigating the endpoint region of {sup 187}Re {beta}-decay or the electron capture of {sup 163}Ho are being developed. This article briefly reviews the current status of the direct neutrino mass measurements.

  5. The kick-out mass selection technique for ions stored in an Electrostatic Ion Beam Trap

    International Nuclear Information System (INIS)

    Toker, Y; Altstein, N; Aviv, O; Rappaport, M L; Heber, O; Schwalm, D; Strasser, D; Zajfman, D

    2009-01-01

    A simple mass selection technique which allows one to clean a keV ion beam of undesirable masses while stored in an Electrostatic Ion Beam Trap (EIBT) is described. The technique is based on the time-of-flight principle and takes advantage of the long storage times and self-bunching that are possible in this type of traps (self bunching being the effect that keeps ions of the same mass bunched in spite of their finite distributions of velocities and trajectories). As the oscillation period is proportional to the square root of the ion mass, bunches containing ions of different masses will separate in space with increasing storage time and can be kicked out by a pulsed deflector mounted inside the trap. A mass selector of this type has been implemented successfully in an EIBT connected to an Even-Lavie supersonic expansion source and is routinely used in ongoing cluster experiments.

  6. In-cylinder pressure resonance analysis for trapped mass estimation in automotive engines

    OpenAIRE

    Bares Moreno, Pau

    2017-01-01

    This thesis presents a new application for in-cylinder pressure sensors in internal combustion engines. The new method takes profit of the high-frequency content of the in-cylinder pressure signal to determine the speed of sound evolution during the expansion stroke and combines this estimation with the low-frequency content of the pressure signal and a volume estimation to obtain a measurement of the trapped mass. The new method is based on the studies of the resonance phenomenon in pent...

  7. The influence of central corneal thickness and age on intraocular pressure measured by pneumotonometry, non-contact tonometry, the Tono-Pen XL, and Goldmann applanation tonometry.

    Science.gov (United States)

    Tonnu, P-A; Ho, T; Newson, T; El Sheikh, A; Sharma, K; White, E; Bunce, C; Garway-Heath, D

    2005-07-01

    To evaluate the influence of central corneal thickness (CCT) on intraocular pressure (IOP) measurements made with the Goldmann applanation tonometer (GAT), Tono-Pen XL, ocular blood flow tonograph (OBF), and Canon TX-10 non-contact tonometer (NCT). CCT was recorded for either eye (randomly selected) of each of 105 untreated patients with ocular hypertension and glaucoma attending the glaucoma research unit at Moorfields Eye Hospital. For each of the selected eyes, IOP was measured with the GAT (two observers), Tono-Pen, OBF, and NCT in a randomised order. The relation of measured IOP and of inter-tonometer differences with CCT and subject age was explored by linear regression analysis. A significant association between measured IOP and CCT was found with each instrument. The change in measured IOP for a 10 mum increase in CCT was 0.28, 0.31, 0.38, and 0.46 for the GAT, Tono-Pen, OBF, and NCT, respectively (all p< or = 0.05). There was a significant association between the NCT/GAT differences and CCT, with a tendency of NCT to overestimate GAT in eyes with thicker corneas. There was a significant association between GAT/Tono-Pen and OBF/Tono-Pen differences and age, with a tendency of GAT and OBF to overestimate the Tono-Pen in eyes of older subjects. IOP measurement by all four methods is affected by CCT. The NCT is affected by CCT significantly more than the GAT. Subject age has a differential effect on the IOP measurements made by the GAT and OBF compared to the Tono-Pen.

  8. Implementation schemes for unsharp measurements with trapped ions

    CSIR Research Space (South Africa)

    Choudhary, SK

    2013-01-01

    Full Text Available trapped ion. The schemes rely on introducing weak entanglement between the state of a target ion and that of an auxiliary ion, using standard ion-trap quantum logic operations, and then realizing an unsharp measurement through projective measurement...

  9. EVOLUTIONARY TRACKS OF TRAPPED, ACCRETING PROTOPLANETS: THE ORIGIN OF THE OBSERVED MASS-PERIOD RELATION

    International Nuclear Information System (INIS)

    Hasegawa, Yasuhiro; Pudritz, Ralph E.

    2012-01-01

    The large number of observed exoplanets (∼>700) provides important constraints on their origin as deduced from the mass-period diagram of planets. The most surprising features in the diagram are (1) the (apparent) pileup of gas giants at a period of ∼500 days (∼1 AU) and (2) the so-called mass-period relation, which indicates that planetary mass is an increasing function of orbital period. We construct the evolutionary tracks of growing planets at planet traps in evolving protoplanetary disks and show that they provide a good physical understanding of how these observational properties arise. The fundamental feature of our model is that inhomogeneities in protoplanetary disks give rise to multiple (up to 3) trapping sites for rapid (type I) planetary migration of planetary cores. The viscous evolution of disks results in the slow radial movement of the traps and their cores from large to small orbital periods. In our model, the slow inward motion of planet traps is coupled with the standard core accretion scenario for planetary growth. As planets grow, type II migration takes over. Planet growth and radial movement are ultimately stalled by the dispersal of gas disks via photoevaporation. Our model makes a number of important predictions: that distinct sub-populations of planets that reflect the properties of planet traps where they have grown result in the mass-period relation, that the presence of these sub-populations naturally explains a pileup of planets at ∼1 AU, and that evolutionary tracks from the ice line do put planets at short periods and fill an earlier claimed p lanet desert — a sparse population of planets in the mass-semimajor axis diagram.

  10. Short communication. Incidence of the OLIPE mass-trapping on olive non-target arthropods

    Energy Technology Data Exchange (ETDEWEB)

    Porcel, M.; Ruano, F.; Sanllorente, O.; Caballero, J. A.; Campos, M.

    2009-07-01

    Due to the widespread of mass-trapping systems for Bactrocera oleae (Gmelin) (Diptera: Tephritidae) control in organic olive cropping, an assessment of the impact on arthropods of the olive agroecosystem was undertaken for the OLIPE trap type. The sampling was carried out in Los Pedroches valley (Cordoba, southern Spain) in three different organic orchard sites. Six OLIPE traps baited with diammonium phosphate were collected from each site (18 in total) from July to November 2002 every 15 days on average. Additionally, in the latest sampling dates, half the traps were reinforced with pheromone to assess its impact on non-target arthropods. From an average of 43.0 catches per trap (cpt) of non-target arthropods during the whole sampling period, the highest number of captures corresponds to the Order Diptera (that represents a 68.5%), followed distantly by the family Formicidae (12.9%) and the Order Lepidoptera (10.4%). Besides the impact on ant populations, other beneficial groups were recorded such as parasitoids (Other Hymenoptera: 2.6%) and predators (Araneae: 1.0%; Neuroptera s.l.: 0.4%). Concerning the temporal distribution of catches, total captures peaked on July and had a slight increase at the beginning of autumn. No significant differences were observed between traps with and without pheromone. The results evidence that a considerable amount of non-specific captures could be prevented by improving the temporal planning of the mass-trapping system. (Author) 25 refs.

  11. Trapping planets in an evolving protoplanetary disk: preferred time, locations and planet mass

    OpenAIRE

    Baillié, Kévin; Charnoz, Sébastien; Pantin, Éric

    2016-01-01

    Planet traps are necessary to prevent forming planets from falling onto their host star by type I migration. Surface mass density and temperature gradient irregularities favor the apparition of traps and deserts. Such features are found at the dust sublimation lines and heat transition barriers. We study how planets may remain trapped or escape as they grow and as the disk evolves. We model the temporal viscous evolution of a protoplanetary disk by coupling its dynamics, thermodynamics, geome...

  12. Dose measurement in periapical radiographic exams using dosemeter pen: a look at the radioprotection

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, Renato; Ferreira, Vanessa, E-mail: vanessamachado@ufmg.br [Curso Superior de Tecnologia em Radiologia. Faculdade de Medicina. Universidade Federal de Minas Gerais, Belo Horizonte, MG (Brazil); Pereira, Claubia; Oliveira, Arno H.; Veloso, M.A.F., E-mail: gbarros@nuclear.ufmg.br, E-mail: claubia@nuclear.ufmg.br, E-mail: heeren@nuclear.ufmg.br, E-mail: Dora@nuclear.ufmg.br [Universidade Federal de Minas Gerais (UFMG), Belo Horizonte, MG (Brazil). Dept. de Engenharia Nuclear

    2011-07-01

    The use of radiology has been a large increase with the crescent accessibility to dental care, orthodontics and aesthetic. Besides the increase in the number of exams, there was an increase in radiation dose during dental exams such as computed tomography. The objective of this work is to evaluate the radiation dose to which the patient is subjected in a peri apical dental radiography. The dose values were measured with a dosimeter pen during radiographs in real exams peri apical with the X-ray equipment Timex 70 C Gnatus. During the exams realization, was maintained, in the holder, the dosimeter pen near to the region of interest. The values collected were recorded in dosimeter pen. These values were compared with the reference doses of the Portaria 453 of ANVISA, this procedure allows to verify if the recommended dose limits for this exam are being respected. These data indicates if the used equipment is calibrated and in good condition of use. It was performed a comparison between the obtained experimental dose values and the values found from computer simulation with the code MCNPX 2.6.0. (author)

  13. Dose measurement in periapical radiographic exams using dosemeter pen: a look at the radioprotection

    International Nuclear Information System (INIS)

    Oliveira, Renato; Ferreira, Vanessa; Pereira, Claubia; Oliveira, Arno H.; Veloso, M.A.F.

    2011-01-01

    The use of radiology has been a large increase with the crescent accessibility to dental care, orthodontics and aesthetic. Besides the increase in the number of exams, there was an increase in radiation dose during dental exams such as computed tomography. The objective of this work is to evaluate the radiation dose to which the patient is subjected in a peri apical dental radiography. The dose values were measured with a dosimeter pen during radiographs in real exams peri apical with the X-ray equipment Timex 70 C Gnatus. During the exams realization, was maintained, in the holder, the dosimeter pen near to the region of interest. The values collected were recorded in dosimeter pen. These values were compared with the reference doses of the Portaria 453 of ANVISA, this procedure allows to verify if the recommended dose limits for this exam are being respected. These data indicates if the used equipment is calibrated and in good condition of use. It was performed a comparison between the obtained experimental dose values and the values found from computer simulation with the code MCNPX 2.6.0. (author)

  14. High-field penning-malmberg trap: confinement properties and use in positron accumulation

    Energy Technology Data Exchange (ETDEWEB)

    Hartley, J.H.

    1997-09-01

    This dissertation reports on the development of the 60 kG cryogenic positron trap at Lawrence Livermore National Laboratory, and compares the trap`s confinement properties with other nonneutral plasma devices. The device is designed for the accumulation of up to 2{times}10{sup 9} positrons from a linear-accelerator source. This positron plasma could then be used in Bhabha scattering experiments. Initial efforts at time-of-flight accumulation of positrons from the accelerator show rapid ({approximately}100 ms) deconfinement, inconsistent with the long electron lifetimes. Several possible deconfinement mechanisms have been explored, including annihilation on residual gas, injection heating, rf noise from the accelerator, magnet field curvature, and stray fields. Detailed studies of electron confinement demonstrate that the empirical scaling law used to design the trap cannot be extrapolated into the parameter regime of this device. Several possible methods for overcoming these limitations are presented.

  15. Highly charged ion trapping and cooling

    International Nuclear Information System (INIS)

    Beck, B. R.; Church, D. A.; Gruber, L.; Holder, J. P.; Schneider, D.; Steiger, J.

    1998-01-01

    In the past few years a cryogenic Penning trap (RETRAP) has been operational at the Electron Beam Ion Trap (EBIT) facility at Lawrence Livermore National Laboratory. The combination of RETRAP and EBIT provides a unique possibility of producing and re-trapping highly charged ions and cooling them to very low temperatures. Due to the high Coulomb potentials in such an ensemble of cold highly charged ions the Coulomb coupling parameter (the ratio of Coulomb potential to the thermal energy) can easily reach values of 172 and more. To study such systems is not only of interest in astrophysics to simulate White Dwarf star interiors but opens up new possibilities in a variety of areas (e.g. laser spectroscopy), cold highly charged ion beams

  16. Chemical Mass Shifts in a Digital Linear Ion Trap as Analytical Identity of o-, m-, and p-Xylene

    Science.gov (United States)

    Sun, Lulu; Xue, Bing; Huang, Zhengxu; Cheng, Ping; Ma, Li; Ding, Li; Zhou, Zhen

    2018-04-01

    Chemical mass shifts between isomeric ions of o-, m-, and p-xylene were measured using a digital linear ion trap, and the directions and values of the shifts were found to be correlated to the collision cross sections of the isomers. Both forward and reverse scans were used and the chemical shifts for each pair of isomers in scans of opposite directions were in opposite signs. Using different voltage settings (namely the voltage dividing ratio-VDR) of the ion trap allows adding high order field components in the quadrupole field and results in larger chemical mass shifts. The differential chemical mass shift which combined the shifts from forward and reverse scans doubled the amount of chemical shift, e.g., 0.077 Th between o- and p-xylene, enough for identification of the type of isomer without using an additional ion mobility spectrometer. The feature of equal and opposite chemical mass shifts also allowed to null out the chemical mass shift by calculating the mean m/z value between the two opposite scans and remove or reduce the mass error caused by chemical mass shift. [Figure not available: see fulltext.

  17. Chemical Mass Shifts in a Digital Linear Ion Trap as Analytical Identity of o-, m-, and p-Xylene.

    Science.gov (United States)

    Sun, Lulu; Xue, Bing; Huang, Zhengxu; Cheng, Ping; Ma, Li; Ding, Li; Zhou, Zhen

    2018-07-01

    Chemical mass shifts between isomeric ions of o-, m-, and p-xylene were measured using a digital linear ion trap, and the directions and values of the shifts were found to be correlated to the collision cross sections of the isomers. Both forward and reverse scans were used and the chemical shifts for each pair of isomers in scans of opposite directions were in opposite signs. Using different voltage settings (namely the voltage dividing ratio-VDR) of the ion trap allows adding high order field components in the quadrupole field and results in larger chemical mass shifts. The differential chemical mass shift which combined the shifts from forward and reverse scans doubled the amount of chemical shift, e.g., 0.077 Th between o- and p-xylene, enough for identification of the type of isomer without using an additional ion mobility spectrometer. The feature of equal and opposite chemical mass shifts also allowed to null out the chemical mass shift by calculating the mean m/z value between the two opposite scans and remove or reduce the mass error caused by chemical mass shift. Graphical Abstract ᅟ.

  18. Penning ionization processes studied by electron spectroscopy

    International Nuclear Information System (INIS)

    Yencha, A.J.

    1978-01-01

    The technique of measuring the kinetic energy of electrons ejected from atomic or molecular species as a result of collisional energy transfer between a metastable excited rare gas atom and an atom or molecule is known as Penning ionization spectroscopy. Like the analogous photoionization process of photoelectron spectroscopy, a considerable amount of information has been gained about the ionization potentials of numerous molecular systems. It is, in fact, through the combined analyses of photoelectron and Penning electron spectra that affords a probe of the particle-particle interactions that occur in the Penning process. In this paper a short survey of the phenomenon of Penning ionization, as studied by electron spectroscopy, will be presented as it pertains to the ionization processes of simple molecules by metastable excited atoms. (author)

  19. The isobaric multiplet mass equation for A≤71 revisited

    Energy Technology Data Exchange (ETDEWEB)

    Lam, Yi Hua, E-mail: lamyihua@gmail.com [CENBG (UMR 5797 — Université Bordeaux 1 — CNRS/IN2P3), Chemin du Solarium, Le Haut Vigneau, BP 120, 33175 Gradignan Cedex (France); Blank, Bertram, E-mail: blank@cenbg.in2p3.fr [CENBG (UMR 5797 — Université Bordeaux 1 — CNRS/IN2P3), Chemin du Solarium, Le Haut Vigneau, BP 120, 33175 Gradignan Cedex (France); Smirnova, Nadezda A. [CENBG (UMR 5797 — Université Bordeaux 1 — CNRS/IN2P3), Chemin du Solarium, Le Haut Vigneau, BP 120, 33175 Gradignan Cedex (France); Bueb, Jean Bernard; Antony, Maria Susai [IPHC, Université de Strasbourg, CNRS/UMR7178, 23 Rue du Loess, 67037 Strasbourg Cedex (France)

    2013-11-15

    Accurate mass determination of short-lived nuclides by Penning-trap spectrometers and progress in the spectroscopy of proton-rich nuclei have triggered renewed interest in the isobaric multiplet mass equation (IMME). The energy levels of the members of T=1/2,1,3/2, and 2 multiplets and the coefficients of the IMME are tabulated for A≤71. The new compilation is based on the most recent mass evaluation (AME2011) and it includes the experimental results on energies of the states evaluated up to end of 2011. Taking into account the error bars, a significant deviation from the quadratic form of the IMME for the A=9,35 quartets and the A=32 quintet is observed.

  20. Final Report - Advanced Ion Trap Mass Spectrometry Program - Oak Ridge National Laboratory - Sandia National Laboratory

    Energy Technology Data Exchange (ETDEWEB)

    Whitten, W.B.

    2002-12-18

    This report covers the three main projects that collectively comprised the Advanced Ion Trap Mass Spectrometry Program. Chapter 1 describes the direct interrogation of individual particles by laser desorption within the ion trap mass spectrometer analyzer. The goals were (1) to develop an ''intelligent trigger'' capable of distinguishing particles of biological origin from those of nonbiological origin in the background and interferent particles and (2) to explore the capability for individual particle identification. Direct interrogation of particles by laser ablation and ion trap mass spectrometry was shown to have good promise for discriminating between particles of biological origin and those of nonbiological origin, although detailed protocols and operating conditions were not worked out. A library of more than 20,000 spectra of various types of biological particles has been assembled. Methods based on multivariate analysis and on neural networks were used to discriminate between particles of biological origin and those of nonbiological origin. It was possible to discriminate between at least some species of bacteria if mass spectra of several hundred similar particles were obtained. Chapter 2 addresses the development of a new ion trap mass analyzer geometry that offers the potential for a significant increase in ion storage capacity for a given set of analyzer operating conditions. This geometry may lead to the development of smaller, lower-power field-portable ion trap mass spectrometers while retaining laboratory-scale analytical performance. A novel ion trap mass spectrometer based on toroidal ion storage geometry has been developed. The analyzer geometry is based on the edge rotation of a quadrupolar ion trap cross section into the shape of a torus. Initial performance of this device was poor, however, due to the significant contribution of nonlinear fields introduced by the rotation of the symmetric ion-trapping geometry. These

  1. Q Value of the Superallowed Decay of 46V and Its Influence on Vud and the Unitarity of the Cabibbo-Kobayashi-Maskawa Matrix

    International Nuclear Information System (INIS)

    Savard, G.; Buchinger, F.; Crawford, J.E.; Gulick, S.; Lee, J.K.P.; Clark, J.A.; Sharma, H.; Sharma, K.S.; Hardy, J.C.; Hecht, A.A.; Levand, A.F.; Scielzo, N.D.; Tanihata, I.; Villari, A.C.C.; Wang, Y.

    2005-01-01

    The masses of the radioactive nuclei 46 V and its decay daughter 46 Ti have been measured with the Canadian Penning Trap on-line Penning trap mass spectrometer to a precision of 1x10 -8 . A Q EC value of 7052.90(40) keV for the superallowed beta decay of 46 V is obtained from the difference of these two masses. With this precise Q value, the Ft value for this decay is determined with improved precision. An investigation of an earlier Q-value measurement for 46 V uncovers a set of 7 measurements that cannot be reconciled with modern data and affects previous evaluations of V ud from superallowed Fermi decays. A new evaluation, adding our new data and removing the discredited subset, yields new values for G V and V ud . When combined with recent results for V us , this yields modified constraints for the unitarity of the Cabibbo-Kobayashi-Maskawa matrix and other extensions of the standard model

  2. Novel control modes to improve the performance of rectilinear ion trap mass spectrometer with dual pressure chambers

    Science.gov (United States)

    Huo, Xinming; Tang, Fei; Zhang, Xiaohua; Chen, Jin; Zhang, Yan; Guo, Cheng'an; Wang, Xiaohao

    2016-10-01

    The rectilinear ion trap (RIT) has gradually become one of the preferred mass analyzers for portable mass spectrometers because of its simple configuration. In order to enhance the performance, including sensitivity, quantitation capability, throughput, and resolution, a novel RIT mass spectrometer with dual pressure chambers was designed and characterized. The studied system constituted a quadrupole linear ion trap (QLIT) in the first chamber and a RIT in the second chamber. Two control modes are hereby proposed: Storage Quadrupole Linear Ion Trap-Rectilinear Ion Trap (SQLIT-RIT) mode, in which the QLIT was used at high pressure for ion storage and isolation, and the RIT was used for analysis; and Analysis Quadrupole Linear Ion Trap-Rectilinear Ion Trap (AQLIT-RIT) mode, in which the QLIT was used for ion storage and cooling. Subsequently, synchronous scanning and analysis were carried out by QLIT and RIT. In SQLIT-RIT mode, signal intensity was improved by a factor of 30; the limit of quantitation was reduced more than tenfold to 50 ng mL-1, and an optimal duty cycle of 96.4% was achieved. In AQLIT-RIT mode, the number of ions coexisting in the RIT was reduced, which weakened the space-charge effect and reduced the mass shift. Furthermore, the mass resolution was enhanced by a factor of 3. The results indicate that the novel control modes achieve satisfactory performance without adding any system complexity, which provides a viable pathway to guarantee good analytical performance in miniaturization of the mass spectrometer.

  3. Resistive cooling circuits for charged particle traps using crystal resonators

    CERN Document Server

    Kaltenbacher, T; Doser, M; Kellerbauer, A; Pribyl, W

    2011-01-01

    The paper addresses a novel method to couple a signal from charged particles in a Penning trap to a high Q resonant circuit using a crystal resonator. Traditionally the trap capacity is converted into a resonator by means of an inductance. When normal conducting wires (e.g. copper) are applied to build up a coil, the unloaded Q value is limited to a value in the order of 1000. The tuned circuit’s Q factor is directly linked to the input impedance “seen” by the trapped particles at resonance frequency. This parallel resonance impedance is a measure of the efficiency of resistive cooling and thus it should be optimized. We propose here a commercially available crystal resonator since it exhibits a very high Q value and a parallel resonance impedance of several MOhm. The possibility to tune the parallel resonance frequency of the quartz results in filter behavior that allows covering a broad range of frequencies.

  4. High-accuracy mass spectrometry for fundamental studies.

    Science.gov (United States)

    Kluge, H-Jürgen

    2010-01-01

    Mass spectrometry for fundamental studies in metrology and atomic, nuclear and particle physics requires extreme sensitivity and efficiency as well as ultimate resolving power and accuracy. An overview will be given on the global status of high-accuracy mass spectrometry for fundamental physics and metrology. Three quite different examples of modern mass spectrometric experiments in physics are presented: (i) the retardation spectrometer KATRIN at the Forschungszentrum Karlsruhe, employing electrostatic filtering in combination with magnetic-adiabatic collimation-the biggest mass spectrometer for determining the smallest mass, i.e. the mass of the electron anti-neutrino, (ii) the Experimental Cooler-Storage Ring at GSI-a mass spectrometer of medium size, relative to other accelerators, for determining medium-heavy masses and (iii) the Penning trap facility, SHIPTRAP, at GSI-the smallest mass spectrometer for determining the heaviest masses, those of super-heavy elements. Finally, a short view into the future will address the GSI project HITRAP at GSI for fundamental studies with highly-charged ions.

  5. Of Papers and Pens: Polysemes and Homophones in Lexical (Mis)Selection

    Science.gov (United States)

    Li, Leon; Slevc, L. Robert

    2017-01-01

    Every word signifies multiple senses. Many studies using comprehension-based measures suggest that polysemes' senses (e.g., "paper" as in "printer paper" or "term paper") share lexical representations, whereas homophones' meanings (e.g., "pen" as in "ballpoint pen" or "pig pen")…

  6. The mass of sup 3 sup 2 Ar and sup 3 sup 3 Ar for fundamental tests

    CERN Document Server

    Blaum, K; Beck, D; Bollen, G; Herfurth, F; Kellerbauer, A G; Kluge, H J; Sauvan, E; Schwarz, S

    2003-01-01

    Masses of the short-lived radionuclides sup 3 sup 2 Ar (T sub 1 sub / sub 2 = 98 ms) sup 3 sup 3 Ar (T sub 1 sub / sub 2 = 173 ms) have been determined with the Penning trap mass spectrometer ISOLTRAP. Relative uncertainties of 6.0 x 10 sup - sup 8 (delta m = 1.8 keV) and 1.4 x 10 sup - sup 8 (delta m = 0.44 keV), respectively, have been achieved. At present, these new mass data serve as the most stringent test of the quadratic form of the isobaricmultiplet mass equation IMME. Furthermore, the improved accuracy for the mass of sup 3 sup 2 Ar yields a better constraint on scalar contributions to the weak interaction. New mass values have also been measured for sup 4 sup 4 Ar and sup 4 sup 5 Ar, and a 20 sigma deviation for sup 4 sup 4 Ar from the literature value was found and interpreted.

  7. Mass Spectrometry Parameters Optimization for the 46 Multiclass Pesticides Determination in Strawberries with Gas Chromatography Ion-Trap Tandem Mass Spectrometry

    Science.gov (United States)

    Fernandes, Virgínia C.; Vera, Jose L.; Domingues, Valentina F.; Silva, Luís M. S.; Mateus, Nuno; Delerue-Matos, Cristina

    2012-12-01

    Multiclass analysis method was optimized in order to analyze pesticides traces by gas chromatography with ion-trap and tandem mass spectrometry (GC-MS/MS). The influence of some analytical parameters on pesticide signal response was explored. Five ion trap mass spectrometry (IT-MS) operating parameters, including isolation time (IT), excitation voltage (EV), excitation time (ET), maximum excitation energy or " q" value (q), and isolation mass window (IMW) were numerically tested in order to maximize the instrument analytical signal response. For this, multiple linear regression was used in data analysis to evaluate the influence of the five parameters on the analytical response in the ion trap mass spectrometer and to predict its response. The assessment of the five parameters based on the regression equations substantially increased the sensitivity of IT-MS/MS in the MS/MS mode. The results obtained show that for most of the pesticides, these parameters have a strong influence on both signal response and detection limit. Using the optimized method, a multiclass pesticide analysis was performed for 46 pesticides in a strawberry matrix. Levels higher than the limit established for strawberries by the European Union were found in some samples.

  8. Production of high stellar-mass primordial black holes in trapped inflation

    Energy Technology Data Exchange (ETDEWEB)

    Cheng, Shu-Lin; Lee, Wolung [Department of Physics, National Taiwan Normal University,Taipei 11677, Taiwan (China); Ng, Kin-Wang [Institute of Physics, Academia Sinica,Taipei 11529, Taiwan (China); Institute of Astronomy and Astrophysics, Academia Sinica,Taipei 11529, Taiwan (China)

    2017-02-01

    Trapped inflation has been proposed to provide a successful inflation with a steep potential. We discuss the formation of primordial black holes in the trapped inflationary scenario. We show that primordial black holes are naturally produced during inflation with a steep trapping potential. In particular, we have given a recipe for an inflaton potential with which particle production can induce large non-Gaussian curvature perturbation that leads to the formation of high stellar-mass primordial black holes. These primordial black holes could be dark matter observed by the LIGO detectors through a binary black-hole merger. At the end, we have given an attempt to realize the required inflaton potential in the axion monodromy inflation, and discussed the gravitational waves sourced by the particle production.

  9. Lifetime measurement of trapped staus using ATLAS

    CERN Document Server

    Sibley, Logan

    I study the creation of long-lived staus at a 14 TeV centre of mass energy in proton-proton collisions at the LHC using both the ATLAS and ACME detectors. The ATLAS overburden or underburden, or even ATLAS itself, may trap the semi-stable staus at that place where they will remain until the time at which they decay, where the stau lifetime ranges between seven days and one year. Using a novel method, one may count the number of muons and pions originating from the stau decay using the standard ATLAS cosmic ray trigger. Using an idealized detector model, I find that this method can lead to measurements of the stau lifetime and SUSY cross-section to within statistical uncertainties of 6% and 1% of their actual values, respectively.

  10. Theoretical Evaluation of the Escape Rate of Charged Particles Trapped in a Potential Energy Well

    International Nuclear Information System (INIS)

    Chang Yongbin; Ordonez, C.A.

    2003-01-01

    In various types of charged particle sources and traps, charged particles are temporarily trapped within a potential energy well. In the work reported, a theoretical evaluation of the escape rate of trapped charged particles is carried out. As a specific example, the loss rate is evaluated for trapped plasma particles that are undergoing both collisions among themselves and collisions with particles of a different plasma species having a different temperature. Conditions are considered in which both species are confined within a nested Penning trap

  11. Improved single ion cyclotron resonance mass spectroscopy

    International Nuclear Information System (INIS)

    Boyce, K.R.

    1993-01-01

    The author has improved the state of the art for precision mass spectroscopy of a mass doublet to below one part in 10 10 . By alternately loading single ions into a Penning trap, the author has determined the mass ratio M(CO + )/M(N + 2 ) = 0.999 598 887 74(11), an accuracy of 1 x 10 -10 . This is a factor of 4 improvement over previous measurements, and a factor of 10 better than the 1985 atomic mass table adjustment [WAA85a]. Much of the author's apparatus has been rebuilt, increasing the signal-to-noise ratio and improving the reliability of the machine. The typical time needed to make and cool a single ion has been reduced from about half an hour to under 5 minutes. This was done by a combination of faster ion-making and a much faster procedure for driving out ions of the wrong species. The improved S/N, in combination with a much better signal processing algorithm to extract the ion phase and frequency from the author's data, has substantially reduced the time required for the actual measurements. This is important now that the measurement time is a substantial fraction of the cycle time (the time to make a new ion and measure it). The improvements allow over 30 comparisons in one night, compared to 2 per night previously. This not only improves the statistics, but eliminates the possibility of large non-Gaussian errors due to sudden magnetic field shifts

  12. Development of a buffer gas trap for the confinement of positrons and study of positronium production in the GBAR experiment

    CERN Document Server

    AUTHOR|(CDS)2101248; van der Werf, Dirk

    The GBAR experiment relies on the production of antihydrogen positive ions to achieve its goal of measuring the gravitational acceleration of antimatter at rest. The ANTION project, included in the GBAR enterprise, is responsible for the production of these antimatter ions. Moreover, it also aims to measure the cross section of antihydrogen production throughout the collision of antiprotons and positronium atoms, as well as the matter cross sections of hydrogen and the hydrogen negative ion. These experiments imply the formation of a very dense positronium cloud, thus a large amount of positrons will be implanted on a positron/positronium converter material. This thesis reports the construction of a three stage buffer gas trap with the goal of trapping and accumulating positrons for the ANTION project. The combination of the Penning-type trap with a LINAC source constitutes a unique experimental setup. The trap was commissioned and optimized and is now fully operational. Trapping protocols were studied and...

  13. Trapped Ion Oscillation Frequencies as Sensors for Spectroscopy

    Directory of Open Access Journals (Sweden)

    Wilfried Nörtershäuser

    2010-03-01

    Full Text Available The oscillation frequencies of charged particles in a Penning trap can serve as sensors for spectroscopy when additional field components are introduced to the magnetic and electric fields used for confinement. The presence of so-called “magnetic bottles” and specific electric anharmonicities creates calculable energy-dependences of the oscillation frequencies in the radiofrequency domain which may be used to detect the absorption or emission of photons both in the microwave and optical frequency domains. The precise electronic measurement of these oscillation frequencies therefore represents an optical sensor for spectroscopy. We discuss possible applications for precision laser and microwave spectroscopy and their role in the determination of magnetic moments and excited state lifetimes. Also, the trap-assisted measurement of radiative nuclear de-excitations in the X-ray domain is discussed. This way, the different applications range over more than 12 orders of magnitude in the detectable photon energies, from below μeV in the microwave domain to beyond MeV in the X-ray domain.

  14. Profile measurements in the plasma edge of mega amp spherical tokamak using a ball pen probe

    International Nuclear Information System (INIS)

    Walkden, N. R.; Adamek, J.; Komm, M.; Allan, S.; Elmore, S.; Fishpool, G.; Harrison, J.; Kirk, A.; Dudson, B. D.

    2015-01-01

    The ball pen probe (BPP) technique is used successfully to make profile measurements of plasma potential, electron temperature, and radial electric field on the Mega Amp Spherical Tokamak. The potential profile measured by the BPP is shown to significantly differ from the floating potential both in polarity and profile shape. By combining the BPP potential and the floating potential, the electron temperature can be measured, which is compared with the Thomson scattering (TS) diagnostic. Excellent agreement between the two diagnostics is obtained when secondary electron emission is accounted for in the floating potential. From the BPP profile, an estimate of the radial electric field is extracted which is shown to be of the order ∼1 kV/m and increases with plasma current. Corrections to the BPP measurement, constrained by the TS comparison, introduce uncertainty into the E R measurements. The uncertainty is most significant in the electric field well inside the separatrix. The electric field is used to estimate toroidal and poloidal rotation velocities from E × B motion. This paper further demonstrates the ability of the ball pen probe to make valuable and important measurements in the boundary plasma of a tokamak

  15. Profile measurements in the plasma edge of mega amp spherical tokamak using a ball pen probe

    Science.gov (United States)

    Walkden, N. R.; Adamek, J.; Allan, S.; Dudson, B. D.; Elmore, S.; Fishpool, G.; Harrison, J.; Kirk, A.; Komm, M.

    2015-02-01

    The ball pen probe (BPP) technique is used successfully to make profile measurements of plasma potential, electron temperature, and radial electric field on the Mega Amp Spherical Tokamak. The potential profile measured by the BPP is shown to significantly differ from the floating potential both in polarity and profile shape. By combining the BPP potential and the floating potential, the electron temperature can be measured, which is compared with the Thomson scattering (TS) diagnostic. Excellent agreement between the two diagnostics is obtained when secondary electron emission is accounted for in the floating potential. From the BPP profile, an estimate of the radial electric field is extracted which is shown to be of the order ˜1 kV/m and increases with plasma current. Corrections to the BPP measurement, constrained by the TS comparison, introduce uncertainty into the ER measurements. The uncertainty is most significant in the electric field well inside the separatrix. The electric field is used to estimate toroidal and poloidal rotation velocities from E × B motion. This paper further demonstrates the ability of the ball pen probe to make valuable and important measurements in the boundary plasma of a tokamak.

  16. Profile measurements in the plasma edge of mega amp spherical tokamak using a ball pen probe

    Energy Technology Data Exchange (ETDEWEB)

    Walkden, N. R., E-mail: nrw504@york.ac.uk [CCFE, Culham Science Centre, Abingdon,Oxon OX14 3DB (United Kingdom); Department of Physics, York Plasma Institute, University of York, Heslington, York YO10 5DD (United Kingdom); Adamek, J.; Komm, M. [Institute of Plasma Physics of AS CR, v. v. i., Za Slovankou 3, 182 00 Praha 8 (Czech Republic); Allan, S.; Elmore, S.; Fishpool, G.; Harrison, J.; Kirk, A. [CCFE, Culham Science Centre, Abingdon,Oxon OX14 3DB (United Kingdom); Dudson, B. D. [Department of Physics, York Plasma Institute, University of York, Heslington, York YO10 5DD (United Kingdom)

    2015-02-15

    The ball pen probe (BPP) technique is used successfully to make profile measurements of plasma potential, electron temperature, and radial electric field on the Mega Amp Spherical Tokamak. The potential profile measured by the BPP is shown to significantly differ from the floating potential both in polarity and profile shape. By combining the BPP potential and the floating potential, the electron temperature can be measured, which is compared with the Thomson scattering (TS) diagnostic. Excellent agreement between the two diagnostics is obtained when secondary electron emission is accounted for in the floating potential. From the BPP profile, an estimate of the radial electric field is extracted which is shown to be of the order ∼1 kV/m and increases with plasma current. Corrections to the BPP measurement, constrained by the TS comparison, introduce uncertainty into the E{sub R} measurements. The uncertainty is most significant in the electric field well inside the separatrix. The electric field is used to estimate toroidal and poloidal rotation velocities from E × B motion. This paper further demonstrates the ability of the ball pen probe to make valuable and important measurements in the boundary plasma of a tokamak.

  17. Trapping of low-mass planets outside the truncated inner edges of protoplanetary discs

    Science.gov (United States)

    Miranda, Ryan; Lai, Dong

    2018-02-01

    We investigate the migration of a low-mass (≲10 M⊕) planet near the inner edge of a protoplanetary disc using two-dimensional viscous hydrodynamics simulations. We employ an inner boundary condition representing the truncation of the disc at the stellar corotation radius. As described by Tsang, wave reflection at the inner disc boundary modifies the Type I migration torque on the planet, allowing migration to be halted before the planet reaches the inner edge of the disc. For low-viscosity discs (α ≲ 10-3), planets may be trapped with semi-major axes as large as three to five times the inner disc radius. In general, planets are trapped closer to the inner edge as either the planet mass or the disc viscosity parameter α increases, and farther from the inner edge as the disc thickness is increased. This planet trapping mechanism may impact the formation and migration history of close-in compact multiplanet systems.

  18. Proposed demonstration of the Einstein-Poldosky-Rosen paradox using trapped electrons

    International Nuclear Information System (INIS)

    Martins, Ana M.

    2002-01-01

    Correlations of the type discussed by Einstein, Poldosky, and Rosen in their original 1935 paradox may be generated between the positions and the momenta of two electrons confined in two spatially separated Penning traps when they are allowed to be coupled for a certain time interval. An experimental demonstration of the paradox could be done using the accurate techniques of manipulation and measurement of confined charged particles. The basic ideas presented in this paper might be extended in order to enable quantum information transfer of continuous variables between massive particles

  19. Factors affecting the transverse force measurements of an optical trap: I

    Science.gov (United States)

    Wood, Tiffany A.; Wright, Amanda; Gleeson, Helen F.; Dickenson, Mark; Mullin, Tom; Murray, Andrew

    2002-03-01

    The transverse force of an optical trap is usually measured by equating the trapping force to the viscous drag force applied to the trapped particle according to Stokes' Law. Under normal conditions, the viscous drag force on a trapped particle is proportional to the fluid velocity of the medium. In this paper we show that an increase of particle concentration within the medium affects force measurements. In order to trap the particle, 1064 nm light from a Nd:YVO4 laser was brought to a focus in a sample slide, of thickness around 380 microns, by using an inverted Zeiss microscope objective, with NA equals 1.3. The slide was filled with distilled water containing 6 micron diameter polystyrene spheres. Measurements were taken at a fluid velocity of 0.75 microns/sec, achieved by moving the sample stage with a piezo-electric transducer whilst a particle was held stationary in the trap. The laser power required to hold a sphere at different trap depths for various concentrations was measured. Significant weakening of the trap was found for concentrations >0.03% solids by weight, becoming weaker for higher trap depths. These results are explained in terms of aberrations, particle-particle interactions and distortion of the beam due to particle-light interactions.

  20. Measurements and characterization of a hole trap in neutron-irradiated silicon

    International Nuclear Information System (INIS)

    Avset, B.S.

    1996-04-01

    The report describes measurements on a hole trap in neutron irradiated silicon diodes made one high resistivity phosphorus doped floatzone silicon. The hole trap was detected by Deep Level Transient Spectroscopy. This measurement gave a trap activation energy of 0.475 MeV. Other measurements showed that the trap has very small capture cross sections for both holes and electrons (10 -18 to 10 -20 cm 2 ) and that the hole capture cross section is temperature dependent. The energy level position of the trap has been estimated to be between 0.25 and 0.29 eV from the valence band. 25 refs., 21 figs., 4 tabs

  1. High-Precision Measurements of the Bound Electron’s Magnetic Moment

    Directory of Open Access Journals (Sweden)

    Sven Sturm

    2017-01-01

    Full Text Available Highly charged ions represent environments that allow to study precisely one or more bound electrons subjected to unsurpassed electromagnetic fields. Under such conditions, the magnetic moment (g-factor of a bound electron changes significantly, to a large extent due to contributions from quantum electrodynamics. We present three Penning-trap experiments, which allow to measure magnetic moments with ppb precision and better, serving as stringent tests of corresponding calculations, and also yielding access to fundamental quantities like the fine structure constant α and the atomic mass of the electron. Additionally, the bound electrons can be used as sensitive probes for properties of the ionic nuclei. We summarize the measurements performed so far, discuss their significance, and give a detailed account of the experimental setups, procedures and the foreseen measurements.

  2. About the measurements systems with pen and thermoluminescent dosemeters

    International Nuclear Information System (INIS)

    Cortes I, M.E.; Ramirez G, F.P.

    1998-01-01

    In this work it is presented dosimetric data obtained with pen and thermoluminescent dosemeters, which are used by the Occupational Exposure Personnel (OEP) of the Mexican Petroleum Institute (IMP)(1). It was marked several great characteristics as for example, the differences among units which use one and another dosemeter type. Likewise, it is given to know diverse problems that were had in the IMP at relating the data obtained with these dosemeters (which utilizes OEP) and the ICRP 60 recommendations 1990. One of the most important difficulties is to satisfy the recommended limits by ICRP, particularly those that are referring to the units and their complex calculations. With respect to the unities, the ICRP makes reference at the concepts 'dose equivalent' and 'effective dose' with the sievert unit, that the General Regulations for Radiological Safety associates with 'dose equivalent' and 'effective dose equivalent'. It was illustrated the type of dosimetric statistics which are obtained with the TLD lectures and a OEP pen dosemeter during 1997. (Author)

  3. Atomic physics measurements in an electron Beam Ion Trap

    International Nuclear Information System (INIS)

    Marrs, R.E.; Beiersdorfer, P.; Bennett, C.

    1989-01-01

    An electron Beam Ion Trap at Lawrence Livermore National Laboratory is being used to produce and trap very-highly-charged ions (q ≤ 70/+/) for x-ray spectroscopy measurements. Recent measurements of transition energies and electron excitation cross sections for x-ray line emission are summarized. 13 refs., 10 figs

  4. Preparing isomerically pure beams of short-lived nuclei at JYFLTRAP

    Energy Technology Data Exchange (ETDEWEB)

    Eronen, T. [Department of Physics, University of Jyvaeskylae, P.O. Box 35 (YFL), FIN-40014 (Finland)], E-mail: tommi.eronen@jyu.fi; Elomaa, V.-V.; Hager, U.; Hakala, J.; Jokinen, A.; Kankainen, A.; Rahaman, S.; Rissanen, J.; Weber, C.; Aystoe, J. [Department of Physics, University of Jyvaeskylae, P.O. Box 35 (YFL), FIN-40014 (Finland)

    2008-10-15

    A new procedure to prepare isomerically clean samples of short-lived ions with a mass resolving power of more than 1 x 10{sup 5} has been developed at the JYFLTRAP tandem Penning trap system. The method utilises a dipolar rf-excitation of the ion motion with separated oscillatory fields in the precision trap. During a subsequent retransfer to the purification trap, the contaminants are rejected and as a consequence, the remaining bunch is isomerically cleaned. This newly-developed method is suitable for very high-resolution cleaning and is at least a factor of five faster than the methods used so far in Penning trap mass spectrometry.

  5. Konzeption eines kryogenen Penningfallenaufbaus für SHIPTRAP und Massenbestimmung von Radionukliden um den Z=82–Schalenabschluss an ISOLTRAP

    CERN Document Server

    Weber, Christine

    Conceptual Design of a Cryogenic Penning Trap Set–Up for SHIPTRAP and Mass Determination of Radionuclides around the Z = 82 – Shell Closure with ISOLTRAP: The Penning trap mass spectrometers SHIPTRAP/GSI and ISOLTRAP/CERN enable precise mass determination of unstable, exotic nuclei. The following detection methods are presented: the destructive time–of–flight method (TOF–ICR) and the non–destructive Fourier Transform–Ion Cyclotron Resonance method (FT–ICR). Planned experiments with SHIPTRAP focus on transuranium elements whose low production limit their experimental investigation. The sensitive FT–ICR– detection allows the identification of stored ions as well as their mass determination. Within this thesis, a cryogenic Penning trap set–up has been designed and constructed, in order to detect and to observe the cyclotron frequency of a single singly-charged heavy ion. It consists of a vacuum system at liquid nitrogen temperature in the bore of a superconducting magnet housing a double tr...

  6. Precision tests of CPT invariance with single trapped antiprotons

    Energy Technology Data Exchange (ETDEWEB)

    Ulmer, Stefan [RIKEN, Ulmer Initiative Research Unit, Wako, Saitama (Japan); Collaboration: BASE-Collaboration

    2015-07-01

    The reason for the striking imbalance of matter and antimatter in our Universe has yet to be understood. This is the motivation and inspiration to conduct high precision experiments comparing the fundamental properties of matter and antimatter equivalents at lowest energies and with greatest precision. According to theory, the most sensitive tests of CPT invariance are measurements of antihydrogen ground-state hyperfine splitting as well as comparisons of proton and antiproton magnetic moments. Within the BASE collaboration we target the latter. By using a double Penning trap we performed very recently the first direct high precision measurement of the proton magnetic moment. The achieved fractional precision of 3.3 ppb improves the currently accepted literature value by a factor of 2.5. Application of the method to a single trapped antiproton will improve precision of the particles magnetic moment by more than a factor of 1000, thus providing one of the most stringent tests of CPT invariance. In my talk I report on the status and future perspectives of our efforts.

  7. ( sup 3 H)(D-PEN sup 2 , D-PEN sup 5 ) enkephalin binding to delta opioid receptors on intact neuroblastoma-glioma (NG 108-15) hybrid cells

    Energy Technology Data Exchange (ETDEWEB)

    Knapp, R.J.; Yamamura, H.I. (Univ. of Arizona College of Medicine, Tucson (USA))

    1990-01-01

    ({sup 3}H)(D-Pen{sup 2}, D-Pen{sup 5})enkephalin binding to intact NG 108-15 cells has been measured under physiological conditions of temperature and medium. The dissociation constant, receptor density, and Hill slope values measured under these conditions are consistent with values obtained by others using membranes prepared from these cells. Kinetic analysis of the radioligand binding to these cells show biphasic association and monophasic dissociation processes suggesting the presence of different receptor affinity states for the agonist. The data show that the binding affinity of ({sup 3}H)(D-Pen{sup 2}, D-Pen{sup 5})enkephalin under physiological conditions is not substantially different to that measured in 50 mM Tris buffer using cell membrane fractions. Unlike DPDPE, the {mu} opioid agonists morphine, normorphine, PL-17, and DAMGO, have much lower affinity for the {delta} receptor measured under these conditions than is observed by studies using 50 mM Tris buffer. The results described here suggest that this assay may serve as a useful model of {delta} opioid receptor binding in vivo.

  8. Trapping cold ground state argon atoms.

    Science.gov (United States)

    Edmunds, P D; Barker, P F

    2014-10-31

    We trap cold, ground state argon atoms in a deep optical dipole trap produced by a buildup cavity. The atoms, which are a general source for the sympathetic cooling of molecules, are loaded in the trap by quenching them from a cloud of laser-cooled metastable argon atoms. Although the ground state atoms cannot be directly probed, we detect them by observing the collisional loss of cotrapped metastable argon atoms and determine an elastic cross section. Using a type of parametric loss spectroscopy we also determine the polarizability of the metastable 4s[3/2](2) state to be (7.3±1.1)×10(-39)  C m(2)/V. Finally, Penning and associative losses of metastable atoms in the absence of light assisted collisions, are determined to be (3.3±0.8)×10(-10)  cm(3) s(-1).

  9. Sodium hydride precipitation in sodium cold traps

    International Nuclear Information System (INIS)

    McPheeters, C.C.; Raue, D.J.

    1980-06-01

    A series of experiments have been performed to test a calculational model for precipitation of NaH in sodium cold traps. The calculational model, called ACTMODEL, is a computer simulation that uses the system geometry and operating conditions as input to calculate a mass-transfer coefficient and the distribution of NaH in a cold trap. The ACTMODEL was tested using an analytical cold trap (ACT) that is simple and essentially one-dimensional. The ACT flow and temperature profile can be controlled at any desired condition. The ACT was analyzed destructively after each test to measure the actual NaH distribution. Excellent agreement was obtained between the ACTMODEL simulations and the experiments. Mass-transfer coefficients ranging upward from 6 x 10 -5 m/s were measured in both packless and packed traps. As much as a fourfold increase in precipitation surface area was observed with increasing amount of NaH deposited. 11 figures, 2 tables

  10. Search for $\\beta$-transitions with the lowest decay energy for a determination of the neutrino mass

    CERN Multimedia

    From a variety of $\\beta$-transitions only those with decay energies of a few keV and smaller are considered suitable for a determination of the neutrino mass on a sub-eV level. The decay energy of a transition can be very small, if, e.g., in an allowed $\\beta$-decay or electron-capture transition, a nuclear excited state of the daughter nuclide is populated whose energy is very close to the mass difference of the transition nuclides. Investigation of these transitions can also be useful for the assessment of a validity of the current $\\beta$-decay theory in the region of vanishingly small decay energies. The authors of this proposal have found several such $\\beta$-transitions whose decay energies are expected to be extremely small. In order to assess the suitability of these $\\beta$-transitions for the determination of the neutrino mass, measurements of the mass differences of the transition nuclides must be carried out with a sub-keV uncertainty. Presently, only high-precision Penning-trap mass spectrometry...

  11. Structural modifications of swift heavy ion irradiated PEN probed by optical and thermal measurements

    International Nuclear Information System (INIS)

    Devgan, Kusum; Singh, Lakhwant; Samra, Kawaljeet Singh

    2013-01-01

    Highlights: • The present paper reports the effect of swift heavy ion irradiation on Polyethylene Naphthalate (PEN). • Swift heavy ion irradiation introduces structural modification and degradation of PEN at different doses. • Lower irradiation doses in PEN result in modification of structural properties and higher doses lead to complete degradation. • Strong correlation between structural, optical, and thermal properties. - Abstract: The effects of swift heavy ion irradiation on the structural characteristics of Polyethylene naphthalate (PEN) were studied. Samples were irradiated in vacuum at room temperature by lithium (50 MeV), carbon (85 MeV), nickel (120 MeV) and silver (120 MeV) ions with the fluence in the range of 1×10 11 –3×10 12 ions cm −2 . Ion induced changes were analyzed using X-ray diffraction (XRD), Fourier transform infra red (FT-IR), UV–visible spectroscopy, thermo-gravimetric analysis (TGA) and differential scanning calorimetry (DSC) techniques. Cross-linking was observed at lower doses resulting in modification of structural properties, however higher doses lead to the degradation of the investigated polymeric samples

  12. Carbon-cluster mass calibration at SHIPTRAP

    International Nuclear Information System (INIS)

    Chaudhuri, Ankur

    2007-01-01

    A carbon-cluster ion source has been installed and tested at SHIPTRAP, the Penning-trap mass spectrometer for mass measurements of heavy elements at GSI/Darmstadt, Germany. A precision mass determination is carried out by measuring the ion cyclotron frequency ω c =qB=m, where q/m is the charge-to-mass ratio of the ion and B is the magnetic field. The mass of the ion of interest is obtained from the comparison of its cyclotron frequency ω c with that of a well-known reference ion. Carbon clusters are the mass reference of choice since the unified atomic mass unit is defined as 1/12 of the mass of the 12 C atom. Thus the masses of carbon clusters 12 C n , n=1,2,3,.. are multiples of the unified atomic mass unit. Carbon-cluster ions 12 C n + , 5≤n≤23, were produced by laser-induced desorption and ionization from a carbon sample. Carbon clusters of various sizes ( 12 C 7 + , 12 C 9 + , 12 C 10 + , 12 C 11 + , 12 C 12 + , 12 C 15 + , 12 C 18 + , 12 C 19 + , 12 C 20 + ) were used for an investigation of the accuracy of SHIPTRAP covering a mass range from 84 u to 240 u. To this end the clusters were used both as ions of interest and reference ions. Hence the true values of the frequency ratios are exactly known. The mass-dependent uncertainty was found to be negligible for the case of (m-m ref ) -8 was revealed. In addition, carbon clusters were employed for the first time as reference ions in an on-line studies of short-lived nuclei. Absolute mass measurements of the radionuclides 144 Dy, 146 Dy and 147 Ho were performed using 12 C 11 + as reference ion. The results agree with measurements during the same run using 85 Rb + as reference ion. The investigated radionuclides were produced in the fusion-evaporation reaction 92 Mo( 58 Ni,xpyn) at SHIP (Separator for Heavy Ion reaction Products) at GSI. Among the measured nuclei 147 Ho has the lowest half life (5.8 s). A relative mass uncertainty of 5 x 10 -8 was obtained from the mass measurements using carbon clusters

  13. An evaluation of prefilled insulin pens: a focus on the Next Generation FlexPen®

    Directory of Open Access Journals (Sweden)

    Estella M Davis

    2010-08-01

    Full Text Available Estella M Davis, Emily L Sexson, Mikayla L Spangler, Pamela A ForalDepartment of Pharmacy Practice, Creighton University School of Pharmacy and Health Professions, Omaha, Nebraska, USAAbstract: Insulin pen delivery systems are preferred by patients over the traditional vial and syringe method for insulin delivery because they are simple and easy to use, improve confidence in dosing insulin, and have less interference with activities and improved discretion with use. Insulin manufacturers have made numerous improvements to their first marketed pen devices and are now introducing their next generation of devices. Design modifications to the newest generation of prefilled insulin pen devices are intended to improve the ease of use and safety and continue to positively impact adherence to insulin. This review focuses on the Next Generation FlexPen® with regard to design considerations to reduce injection force, improve accuracy and ease of use, and evaluate the preference of patient and health-care provider compared with other disposable, prefilled insulin pen devices.Keywords: diabetes, dose accuracy, injection force, patient preference, insulin pen device

  14. Mass-balance measurements in Alaska and suggestions for simplified observation programs

    Science.gov (United States)

    Trabant, D.C.; March, R.S.

    1999-01-01

    US Geological Survey glacier fieldwork in Alaska includes repetitious measurements, corrections for leaning or bending stakes, an ability to reliably measure seasonal snow as deep as 10 m, absolute identification of summer surfaces in the accumulation area, and annual evaluation of internal accumulation, internal ablation, and glacier-thickness changes. Prescribed field measurement and note-taking techniques help eliminate field errors and expedite the interpretative process. In the office, field notes are transferred to computerized spread-sheets for analysis, release on the World Wide Web, and archival storage. The spreadsheets have error traps to help eliminate note-taking and transcription errors. Rigorous error analysis ends when mass-balance measurements are extrapolated and integrated with area to determine glacier and basin mass balances. Unassessable errors in the glacier and basin mass-balance data reduce the value of the data set for correlations with climate change indices. The minimum glacier mass-balance program has at least three measurement sites on a glacier and the measurements must include the seasonal components of mass balance as well as the annual balance.

  15. TASCC newsletter volume 7 no. 10

    International Nuclear Information System (INIS)

    Thomson, L.

    1993-10-01

    A newsletter produced by Chalk River's Tandem Accelerator Superconducting Cyclotron Facility. Included in this October issue of TASCC is an update of the facility report, ECR ion source development, new measurement of Carbon 10, Penning-trap mass spectrometer and a listing of October's experiments. 2 figs

  16. Mass measurement of halo nuclides and beam cooling with the mass spectrometer Mistral

    International Nuclear Information System (INIS)

    Bachelet, C.

    2004-12-01

    Halo nuclides are a spectacular drip-line phenomenon and their description pushes nuclear theories to their limits. The most critical input parameter is the nuclear binding energy; a quantity that requires excellent measurement precision, since the two-neutron separation energy is small at the drip-line by definition. Moreover halo nuclides are typically very short-lived. Thus, a high accuracy instrument using a quick method of measurement is necessary. MISTRAL is such an instrument; it is a radiofrequency transmission mass spectrometer located at ISOLDE/CERN. In July 2003 we measured the mass of the Li 11 , a two-neutron halo nuclide. Our measurement improves the precision by a factor 6, with an error of 5 keV. Moreover the measurement gives a two-neutron separation energy 20% higher than the previous value. This measurement has an impact on the radius of the nucleus, and on the state of the two valence neutrons. At the same time, a measurement of the Be 11 was performed with an uncertainty of 4 keV, in excellent agreement with previous measurements. In order to measure the mass of the two-neutron halo nuclide Be 14 , an ion beam cooling system is presently under development which will increase the sensitivity of the spectrometer. The second part of this work presents the development of this beam cooler using a gas-filled Paul trap. (author)

  17. Review of Plasma Techniques Used to Trap Antihydrogen

    Science.gov (United States)

    Fajans, Joel

    2011-10-01

    Recently, the ALPHA collaboration at CERN trapped antihydrogen atoms. To date, over three hundred antiatoms have been confined, some for as long as 1000s. This was the first time that antiatoms had ever been trapped. The ultimate goal of the ALPHA collaboration is to test CPT invariance by comparing the spectra of hydrogen and antihydrogen, and to measure the gravitational attraction between matter and antimatter. Such studies might resolve the baryogenesis problem: why is there very little antimatter in the Universe? The ALPHA experiment brought together techniques from many different fields of physics, but the crucial breakthroughs were in plasma physics. The essential problem is this: How does one combine two Malmberg-Penning trapped plasmas, one made from antiprotons, and the other positrons, which have opposite electrostatic potentials of nearly one volt, in such a manner that the antiprotons traverse the positrons with kinetic energies of less than 40 μeV, this latter being the depth of the superimposed neutral antihydrogen trap? The plasma techniques ALPHA developed to accomplish this include: Minimizing the effects of the neutral trap multipole fields on the positron and antiproton plasma confinement. Compressing antiprotons down to less than 0.5mm. Using autoresonance to inject antiprotons into the positrons with very little excess energy. Evaporative cooling of the electrons and antiprotons to record low temperatures. Development of charge, radial profile, temperature, and antiproton loss location diagnostics. Careful and lengthy manipulations to finesse the plasmas into the best states for optimal antihydrogen production and trapping. The plasma techniques necessary to trap antihydrogen will be reviewed in this talk. This work was supported by DOE and NSF, and is reported on behalf of the ALPHA collaboration.

  18. Impenetrable Mass-Imbalanced Particles in One-Dimensional Harmonic Traps

    DEFF Research Database (Denmark)

    Salami Dehkharghani, Amin; Volosniev, A. G.; Zinner, N. T.

    2016-01-01

    Strongly interacting particles in one dimension subject to external confinement have become a topic of considerable interest due to recent experimental advances and the development of new theoretical methods to attack such systems. In the case of equal mass fermions or bosons with two or more...... internal degrees of freedom, one can map the problem onto the well-known Heisenberg spin models. However, many interesting physical systems contain mixtures of particles with different masses. Therefore, a generalization of the recent strong-coupling techniques would be highly desirable....... This is particularly important since such problems are generally considered non-integrable and thus the hugely successful Bethe ansatz approach cannot be applied. Here we discuss some initial steps towards this goal by investigating small ensembles of one-dimensional harmonically trapped particles where pairwise...

  19. Chemical composition of felt-tip pen inks.

    Science.gov (United States)

    Germinario, Giulia; Garrappa, Silvia; D'Ambrosio, Valeria; van der Werf, Inez Dorothé; Sabbatini, Luigia

    2018-01-01

    Felt-tip pens are frequently used for the realization of sketches, drawings, architectural projects, and other technical designs. The formulations of these inks are usually rather complex and may be associated to those of modern paint materials where, next to the binding medium and pigments/dyes, solvents, fillers, emulsifiers, antioxidants, plasticizers, light stabilizers, biocides, and so on are commonly added. Felt-tip pen inks are extremely sensitive to degradation and especially exposure to light may cause chromatic changes and fading. In this study, we report on the complete chemical characterization of modern felt-tip pen inks that are commercially available and commonly used for the realization of artworks. Three brands of felt-tip pens (Faber-Castell, Edding, and Stabilo) were investigated with complementary analytical techniques such as thin-layer chromatography (TLC), VIS-reflectance spectroscopy, μ-Raman spectroscopy, surface-enhanced Raman spectroscopy (SERS), pyrolysis-gas chromatography-mass spectrometry (Py-GC-MS), GC-MS, and Fourier transform infrared (FTIR) spectroscopy. The use of TLC proved to be very powerful in the study of complex mixtures of synthetic dyes. First derivatives of the reflectance spectra acquired on the TLC spots were useful in the preliminary identification of the dye, followed by Raman spectroscopy and SERS, which allowed for the unambiguous determination of the chemical composition of the pigments (phthalocyanines, dioxazines, and azo pigments) and dyes (azo dyes, triarylmethanes, xanthenes). FTIR spectroscopy was used especially for the detection of additives, as well as for confirming the nature of solvents and dyes/pigments. Finally, (Py-)GC-MS data provided information on the binders (styrene-acrylic resins, plant gums), solvents, and additives, as well as on pigments and dyes.

  20. Cooling the center-of-mass motion of a diamond nanocrystal in a magneto-gravitational trap

    Science.gov (United States)

    Hsu, Jen-Feng

    A magneto-gravitational trap for micro/nanometer sized diamagnetic particles, such as diamond nanocrystals, is tested and characterized. After exploring various other systems, such as a suspended graphene beam and an optical trap, this magneto-gravitational nanomechanical trapping system for diamond with nitrogen-vacancy (NV) centers presents unique advantages for experiments in fundamental quantum mechanics. Those include, for example, the generation of large quantum superposition states and tests of quantum gravity. Features are demonstrated for this system, such as stable and passive levitation from atmospheric pressure to high vacuum, low resonant frequencies and damping rates, and cooling of the center-of-mass motions to below 1 K. The construction of the trap, vacuum system, optics, and motion detection electronics are described in detail.

  1. Ultrasonic trap for light scattering measurement

    Science.gov (United States)

    Barton, Petr; Pavlu, Jiri

    2017-04-01

    Light scattering is complex phenomenon occurring widely in space environments, including the dense dusty clouds, nebulas or even the upper atmosphere of the Earth. However, when the size of the dust (or of other scattering center) is close to the incident light wavelength, theoretical determination is difficult. In such case, Mie theory is to be used but there is a lack of the material constants for most space-related materials. For experimental measurement of light scattering, we designed unique apparatus, based on ultrasonic trap. Using acoustic levitation we are able to capture the dust grain in midair, irradiate it with laser, and observe scattering directly with goniometer-mounted photodiode. Advantage of this approach is ability to measure directly in the air (thus, no need for the carrier medium) and possibility to study non-spherical particles. Since the trap development is nearly finished and initial experiments are carried out, the paper presents first tests on water droplets.

  2. TASCC newsletter volume 7 no. 10

    Energy Technology Data Exchange (ETDEWEB)

    Thomson, L

    1993-10-01

    A newsletter produced by Chalk River`s Tandem Accelerator Superconducting Cyclotron Facility. Included in this October issue of TASCC is an update of the facility report, ECR ion source development, new measurement of Carbon 10, Penning-trap mass spectrometer and a listing of October`s experiments. 2 figs.

  3. Development of a multiplexed interface for capillary electrophoresis-electrospray ion trap mass spectrometry.

    Science.gov (United States)

    Li, Fu-An; Wu, Ming-Chi; Her, Guor-Rong

    2006-08-01

    A four-channel multiplexed electrospray capillary electrophoresis interface has been developed. This new interface permits up to four capillary electrophoresis columns to be sampled sequentially by means of a stepper motor and a notched rotating plate assembly, which at any instant occludes all but a single sprayer. In this design, four sheath liquid electrospray probes are oriented in a circular array situated 90 degrees relative to one another. The rotating metal disk, which contains a one-quarter notch, is mounted to the stepper motor assembly and is located between the sprayers and the entrance aperture of an ion trap mass spectrometer. By using the data acquisition signal from the ion trap mass spectrometer, the scan event is synchronized with the rotation of the metal disk. With this device, four discrete sample streams can be simultaneously analyzed, resulting in a 4-fold increase in analytical throughput.

  4. Vegetation survey of PEN Branch wetlands

    Energy Technology Data Exchange (ETDEWEB)

    1991-01-01

    A survey was conducted of vegetation along Pen Branch Creek at Savannah River Site (SRS) in support of K-Reactor restart. Plants were identified to species by overstory, understory, shrub, and groundcover strata. Abundance was also characterized and richness and diversity calculated. Based on woody species basal area, the Pen Branch delta was the most impacted, followed by the sections between the reactor and the delta. Species richness for shrub and groundcover strata were also lowest in the delta. No endangered plant species were found. Three upland pine areas were also sampled. In support of K Reactor restart, this report summarizes a study of the wetland vegetation along Pen Branch. Reactor effluent enters Indian Grove Branch and then flows into Pen Branch and the Pen Branch Delta.

  5. Trapped field measurements on MgB{sub 2} bulk samples

    Energy Technology Data Exchange (ETDEWEB)

    Koblischka, Michael; Karwoth, Thomas; Zeng, XianLin; Hartmann, Uwe [Institute of Experimental Physics, Saarland University, P. O. Box 151150, D-66041 Saarbruecken (Germany); Berger, Kevin; Douine, Bruno [University of Lorraine, GREEN, 54506 Vandoeuvre-les-Nancy (France)

    2016-07-01

    Trapped field measurements were performed on bulk, polycrystalline MgB{sub 2} samples stemming from different sources with the emphasis to develop applications like superconducting permanent magnets ('supermagnets') and electric motors. We describe the setup for the trapped field measurements and the experimental procedure (field cooling, zero-field cooling, field sweep rates). The trapped field measurements were conducted using a cryocooling system to cool the bulk samples to the desired temperatures, and a low-loss cryostat equipped with a room-temperature bore and a maximum field of ±5 T was employed to provide the external magnetic field. The superconducting coil of this cryostat is operated using a bidirectional power supply. Various sweep rates of the external magnetic field ranging between 1 mT/s and 40 mT/s were used to generate the applied field. The measurements were performed with one sample and two samples stacked together. A maximum trapped field of 7 T was recorded. We discuss the results obtained and the problems arising due to flux jumping, which is often seen for the MgB{sub 2} samples cooled to temperatures below 10 K.

  6. A method of measurement of lifetimes of excited ion levels, using orientation transfer by Penning collisions

    International Nuclear Information System (INIS)

    Hamel, J.; Barrat, J.-P.

    1978-01-01

    A method for measuring the lifetimes of ionic excited levels is described. This method uses the transfer of coherence in a Penning collision using metastable optically oriented He 2 3 S 1 atoms. If R.F. transitions are induced in the (2 3 S 1 )He level, a transverse component of the magnetic moment of this level is created, which precesses coherently at the angular frequency ω of the R.F. field. The helium transverse orientation is partially transferred to the ions produced by Penning collisions. After the collision, the orientation transferred precesses around the external magnetic field at the Larmor frequency ω 0 ' of the ion excited level. The degree of orientation of the excited ion level depends, in the stationary state, on the average phase shift, during the lifetime tau prime of this level, between the Larmor precession at angular frequency ω 0 ' and the forced precession of helium (at angular frequency ω). The orientation of the ions is monitored by the modulation of the light emitted during their radiative decay. It is possible to determine the lifetime tau prime by measuring the degree of modulation of the reemitted light as a function of ω [fr

  7. Planetary populations in the mass-period diagram: A statistical treatment of exoplanet formation and the role of planet traps

    International Nuclear Information System (INIS)

    Hasegawa, Yasuhiro; Pudritz, Ralph E.

    2013-01-01

    The rapid growth of observed exoplanets has revealed the existence of several distinct planetary populations in the mass-period diagram. Two of the most surprising are (1) the concentration of gas giants around 1 AU and (2) the accumulation of a large number of low-mass planets with tight orbits, also known as super-Earths and hot Neptunes. We have recently shown that protoplanetary disks have multiple planet traps that are characterized by orbital radii in the disks and halt rapid type I planetary migration. By coupling planet traps with the standard core accretion scenario, we showed that one can account for the positions of planets in the mass-period diagram. In this paper, we demonstrate quantitatively that most gas giants formed at planet traps tend to end up around 1 AU, with most of these being contributed by dead zones and ice lines. We also show that a large fraction of super-Earths and hot Neptunes are formed as 'failed' cores of gas giants—this population being constituted by comparable contributions from dead zone and heat transition traps. Our results are based on the evolution of forming planets in an ensemble of disks where we vary only the lifetimes of disks and their mass accretion rates onto the host star. We show that a statistical treatment of the evolution of a large population of planetary cores caught in planet traps accounts for the existence of three distinct exoplanetary populations—the hot Jupiters, the more massive planets around r = 1 AU, and the short-period super-Earths and hot Neptunes. There are very few populations that feed into the large orbital radii characteristic of the imaged Jovian planet, which agrees with recent surveys. Finally, we find that low-mass planets in tight orbits become the dominant planetary population for low-mass stars (M * ≤ 0.7 M ☉ ).

  8. A comb-sampling method for enhanced mass analysis in linear electrostatic ion traps

    Energy Technology Data Exchange (ETDEWEB)

    Greenwood, J. B.; Kelly, O.; Calvert, C. R.; Duffy, M. J.; King, R. B.; Belshaw, L.; Graham, L.; Alexander, J. D.; Williams, I. D. [Centre for Plasma Physics, School of Mathematics and Physics, Queen' s University Belfast, Belfast BT7 1NN (United Kingdom); Bryan, W. A. [Department of Physics, Swansea University, Swansea SA2 8PP (United Kingdom); Turcu, I. C. E.; Cacho, C. M.; Springate, E. [Central Laser Facility, STFC Rutherford Appleton Laboratory, Didcot, Oxfordshire OX11 0QX (United Kingdom)

    2011-04-15

    In this paper an algorithm for extracting spectral information from signals containing a series of narrow periodic impulses is presented. Such signals can typically be acquired by pickup detectors from the image-charge of ion bunches oscillating in a linear electrostatic ion trap, where frequency analysis provides a scheme for high-resolution mass spectrometry. To provide an improved technique for such frequency analysis, we introduce the CHIMERA algorithm (Comb-sampling for High-resolution IMpulse-train frequency ExtRAaction). This algorithm utilizes a comb function to generate frequency coefficients, rather than using sinusoids via a Fourier transform, since the comb provides a superior match to the data. This new technique is developed theoretically, applied to synthetic data, and then used to perform high resolution mass spectrometry on real data from an ion trap. If the ions are generated at a localized point in time and space, and the data is simultaneously acquired with multiple pickup rings, the method is shown to be a significant improvement on Fourier analysis. The mass spectra generated typically have an order of magnitude higher resolution compared with that obtained from fundamental Fourier frequencies, and are absent of large contributions from harmonic frequency components.

  9. Neutron lifetime measurements with a large gravitational trap for ultracold neutrons

    Science.gov (United States)

    Serebrov, A. P.; Kolomensky, E. A.; Fomin, A. K.; Krasnoshchekova, I. A.; Vassiljev, A. V.; Prudnikov, D. M.; Shoka, I. V.; Chechkin, A. V.; Chaikovskiy, M. E.; Varlamov, V. E.; Ivanov, S. N.; Pirozhkov, A. N.; Geltenbort, P.; Zimmer, O.; Jenke, T.; Van der Grinten, M.; Tucker, M.

    2018-05-01

    Neutron lifetime is one of the most important physical constants: it determines parameters of the weak interaction and predictions of primordial nucleosynthesis theory. There remains the unsolved problem of a 3.9σ discrepancy between measurements of this lifetime using neutrons in beams and those with stored ultracold neutrons (UCN). In our experiment we measure the lifetime of neutrons trapped by Earth's gravity in an open-topped vessel. Two configurations of the trap geometry are used to change the mean frequency of UCN collisions with the surfaces; this is achieved by plunging an additional surface into the trap without breaking the vacuum. The trap walls are coated with a hydrogen-less fluorine-containing polymer to reduce losses of UCN. The stability of this coating over multiple thermal cycles between 80 and 300 K was tested. At 80 K, the probability of UCN loss due to collisions with the trap walls is just 1.5% of the probability of β decay. The free neutron lifetime is determined by extrapolation to an infinitely large trap with zero collision frequency. The result of these measurements is τn=881.5 ±0 .7stat ±0 .6syst s which is consistent with the conventional value of 880.2 ± 1.0 s presented by the Particle Data Group. Future prospects for this experiment are in further cooling to 10 K, which will lead to an improved accuracy of measurement. In conclusion we present an analysis of currently available data on various measurements of the neutron lifetime.

  10. Measurement of plasma potential and electron temperature by ball-pen probes in RFX-MOD

    International Nuclear Information System (INIS)

    Brotankova, J.; Adamek, J.; Stockel, J.; Martines, E.; Spolaore, M.; Cavazzana, R.; Serianni, G.; Vianello, N.; Zuin, M.

    2009-01-01

    The ball-pen probe (BPP) is an innovative electric probe for direct measurements of the plasma potential. This probe was developed in IPP Prague and it is based on the Katsumata probe concept. Combined measurements of the plasma potential by a BPP and floating potential by a Langmuir probe provide also the value of the electron temperature. First test of the BPP on the RFX-mod reversed field pinch in Padova has been performed in November 2006. The BPP head, made of boron nitride, is equipped with four graphite collectors, which are positioned at four different radial positions h inside four shafts hollow into the probe head. The radial profile of the plasma potential and also the electron temperature were measured

  11. Utilization of the ion traps by SPIRAL

    International Nuclear Information System (INIS)

    Le Brun, C.; Lienard, E.; Mauger, F.; Tamain, B.

    1997-01-01

    An ion trap is a device capable of confine particles, ions or atoms in a well-controlled environment isolated from any exterior perturbations. There are different traps. They are utilized to collect or stock ions, to cool them after in order to subject them to high precision measurement of masses, magnetic moments, hyperfine properties, beta decay properties, etc. Some dozen of traps are currently used all over the world to study stable or radioactive ions.. SPIRAL has been designed and built to produce radioactive ions starting from various heavy ion beams. SPIRAL has the advantage that the projectile parameters, the target and the energy can be chosen to optimize the production in various regions of the nuclear chart. Also, in SPIRAL it is possible to extract more rapidly the radioactive ions formed in the targets. In addition, in SPIRAL the multicharged ion production in a ECR source is possible. The utilization of multicharged ions is indeed very useful for fast mass measurements or for the study of the interaction between the nucleus and the electronic cloud. Finally, utilization of a ion trap on SPIRAL can be designed first at the level of production target by installing a low energy output line. Than, the trap system could be up-graded and brought to its full utilization behind of the recoil spectrometer. It must be capable of selecting and slowing down the ions produced in the reactions (fusion transfer, very inelastic collisions, etc.) induced by the radioactive ions accelerated in CIME. At present, the collaboration is debating on the most favored subject to study and the most suited experimental setups. The following subjects were selected: ion capture, purification and manipulation; isomers (separation and utilization); mass measurements; hyperfine interactions; lifetimes, nuclear electric cloud; β decays; study of the N = Z nuclei close to the proton drip line; physical and chemical properties of transuranium systems

  12. Pen dosimeters

    CERN Multimedia

    SC/RP Group

    2006-01-01

    The Radiation Protection Group has decided to withdraw all pen dosimeters from the main PS and SPS access points. This will be effective as of January 2006. The following changes will be implemented: All persons working in a limited-stay controlled radiation area must wear an operational dosimeter in addition to their personal DIS dosimeter. Any persons not equipped with this additional dosimeter must contact the SC/RP Group, which will make this type of dosimeter available for temporary loan. A notice giving the phone numbers of the SC/RP Group members to contact will be displayed at the former distribution points for the pen dosimeters. Thank you for your cooperation. The SC/RP Group

  13. Optical trapping of carbon nanotubes and graphene

    Directory of Open Access Journals (Sweden)

    S. Vasi

    2011-09-01

    Full Text Available We study optical trapping of nanotubes and graphene. We extract the distribution of both centre-of-mass and angular fluctuations from three-dimensional tracking of these optically trapped carbon nanostructures. The optical force and torque constants are measured from auto and cross-correlation of the tracking signals. We demonstrate that nanotubes enable nanometer spatial, and femto-Newton force resolution in photonic force microscopy by accurately measuring the radiation pressure in a double frequency optical tweezers. Finally, we integrate optical trapping with Raman and photoluminescence spectroscopy demonstrating the use of a Raman and photoluminescence tweezers by investigating the spectroscopy of nanotubes and graphene flakes in solution. Experimental results are compared with calculations based on electromagnetic scattering theory.

  14. Cytotoxicity of Pd nanostructures supported on PEN: Influence of sterilization on Pd/PEN interface

    Energy Technology Data Exchange (ETDEWEB)

    Polívková, M., E-mail: polivkoa@vscht.cz [Department of Solid State Engineering, University of Chemistry and Technology Prague, 166 28 Prague (Czech Republic); Siegel, J. [Department of Solid State Engineering, University of Chemistry and Technology Prague, 166 28 Prague (Czech Republic); Rimpelová, S. [Department of Biochemistry and Microbiology, University of Chemistry and Technology Prague, 166 28 Prague (Czech Republic); Hubáček, T. [Institute of Hydrobiology, Biology Centre of the AS CR, 370 05 Ceske Budejovice (Czech Republic); Kolská, Z. [Materials Centre of Usti n. L., J.E. Purkyne University, 400 96 Usti nad Labem (Czech Republic); Švorčík, V. [Department of Solid State Engineering, University of Chemistry and Technology Prague, 166 28 Prague (Czech Republic)

    2017-01-01

    Non-conventional antimicrobial agents, such as palladium nanostructures, have been increasingly used in the medicinal technology. However, experiences uncovering their harmful and damaging effects to human health have begun to appear. In this study, we have focused on in vitro cytotoxicity assessment of Pd nanostructures supported on a biocompatible polymer. Pd nanolayers of variable thicknesses (ranging from 1.1 to 22.4 nm) were sputtered on polyethylene naphthalate (PEN). These nanolayers were transformed by low-temperature post-deposition annealing into discrete nanoislands. Samples were characterized by AFM, XPS, ICP-MS and electrokinetic analysis before and after annealing. Sterilization of samples prior to cytotoxicity testing was done by UV irradiation, autoclave and/or ethanol. Among the listed sterilization techniques, we have chosen the gentlest one which had minimal impact on sample morphology, Pd dissolution and overall Pd/PEN interface quality. Cytotoxic response of Pd nanostructures was determined by WST-1 cell viability assay in vitro using three model cell lines: mouse macrophages (RAW 264.7) and two types of mouse embryonic fibroblasts (L929 and NIH 3T3). Finally, cell morphology in response to Pd/PEN was evaluated by means of fluorescence microscopy. - Highlights: • Annealing of Pd nanolayers on PEN resulted to Pd aggregation and formation of discrete nanoislands. • UV treatment was found as the gentlest sterilization method in term of physicochemical properties of Pd/PEN interface. • Autoclaving and chemical sterilization by ethanol resulted into remarkable changes of Pd/PEN interface. • Cytotoxicity of Pd samples was insignificant. • Pd nanostructures are potentially applicable as health-unobjectionable antibacterial coatings of medical devices.

  15. NovoPen Echo® insulin delivery device

    Directory of Open Access Journals (Sweden)

    Hyllested-Winge J

    2016-01-01

    Full Text Available Jacob Hyllested-Winge,1 Thomas Sparre,2 Line Kynemund Pedersen2 1Novo Nordisk Pharma Ltd, Tokyo, Japan; 2Novo Nordisk A/S, Søborg, Denmark Abstract: The introduction of insulin pen devices has provided easier, well-tolerated, and more convenient treatment regimens for patients with diabetes mellitus. When compared with vial and syringe regimens, insulin pens offer a greater clinical efficacy, improved quality of life, and increased dosing accuracy, particularly at low doses. The portable and discreet nature of pen devices reduces the burden on the patient, facilitates adherence, and subsequently contributes to the improvement in glycemic control. NovoPen Echo® is one of the latest members of the NovoPen® family that has been specifically designed for the pediatric population and is the first to combine half-unit increment (=0.5 U of insulin dosing with a simple memory function. The half-unit increment dosing amendments and accurate injection of 0.5 U of insulin are particularly beneficial for children (and insulin-sensitive adults/elders, who often require small insulin doses. The memory function can be used to record the time and amount of the last dose, reducing the fear of double dosing or missing a dose. The memory function also provides parents with extra confidence and security that their child is taking insulin at the correct doses and times. NovoPen Echo is a lightweight, durable insulin delivery pen; it is available in two different colors, which may help to distinguish between different types of insulin, providing more confidence for both users and caregivers. Studies have demonstrated a high level of patient satisfaction, with 80% of users preferring NovoPen Echo to other pediatric insulin pens. Keywords: NovoPen Echo®, memory function, half-unit increment dosing, adherence, children, adolescents 

  16. Caution on the use of liquid nitrogen traps in stable hydrogen isotope-ratio mass spectrometry

    Science.gov (United States)

    Coplen, Tyler B.; Qi, Haiping

    2010-01-01

    An anomalous stable hydrogen isotopic fractionation of 4 ‰ in gaseous hydrogen has been correlated with the process of adding liquid nitrogen (LN2) to top off the dewar of a stainless-steel water trap on a gaseous hydrogen-water platinum equilibration system. Although the cause of this isotopic fractionation is unknown, its effect can be mitigated by (1) increasing the capacity of any dewars so that they do not need to be filled during a daily analytic run, (2) interspersing isotopic reference waters among unknowns, and (3) applying a linear drift correction and linear normalization to isotopic results with a program such as Laboratory Information Management System (LIMS) for Light Stable Isotopes. With adoption of the above guidelines, measurement uncertainty can be substantially improved. For example, the long-term (months to years) δ2H reproducibility (1& sigma; standard deviation) of nine local isotopic reference waters analyzed daily improved substantially from about 1‰ to 0.58 ‰. This isotopically fractionating mechanism might affect other isotope-ratio mass spectrometers in which LN2 is used as a moisture trap for gaseous hydrogen

  17. Area-wide mass trapping by pheromone-based attractants for the control of sugar beet weevil (Bothynoderes punctiventris Germar, Coleoptera: Curculionidae).

    Science.gov (United States)

    Drmić, Zrinka; Tóth, Miklós; Lemić, Darija; Grubišić, Dinka; Pospišil, Milan; Bažok, Renata

    2017-10-01

    Owing to the changing climate, narrow crop rotation, and changes in insecticide application practice, sugar beet weevil (SBW) (Bothynoderes punctiventris Germar) has become the most important economic pest in sugar beet. To develop alternative control methods, an area-wide (AW) control program using aggregation pheromones was implemented over 4 years on an area of 6 and 14.8 km 2 in east Croatia. The mass trapping of SBW on the 'old' sugar beet fields reduced the population from 0.73% to 11.59%. Owing to the strong attack, mass trapping was not effective enough to avoid an insecticide application. However, it significantly reduced the number of insecticide applications, the amount of insecticide used, and the damage compared to the fields outside the mass trapping area. This is the first study to implement an AW program for SBW. It may not be possible to state from this study that trapping alone can reduce the SBW population below the economic threshold level. However, the data do suggest that trapping can play an important role in the reduction of insecticide applications and in creating an integrated pest management plan for dealing with SBW under similar circumstances. © 2017 Society of Chemical Industry. © 2017 Society of Chemical Industry.

  18. In-depth study of in-trap high-resolution mass separation by transversal ion ejection from a multi-reflection time-of-flight device.

    Science.gov (United States)

    Fischer, Paul; Knauer, Stefan; Marx, Gerrit; Schweikhard, Lutz

    2018-01-01

    The recently introduced method of ion separation by transversal ejection of unwanted species in electrostatic ion-beam traps and multi-reflection time-of-flight devices has been further studied in detail. As this separation is performed during the ion storage itself, there is no need for additional external devices such as ion gates or traps for either pre- or postselection of the ions of interest. The ejection of unwanted contaminant ions is performed by appropriate pulses of the potentials of deflector electrodes. These segmented ring electrodes are located off-center in the trap, i.e., between one of the two ion mirrors and the central drift tube, which also serves as a potential lift for capturing incoming ions and axially ejecting ions of interest after their selection. The various parameters affecting the selection effectivity and resolving power are illustrated with tin-cluster measurements, where isotopologue ion species provide mass differences down to a single atomic mass unit at ion masses of several hundred. Symmetric deflection voltages of only 10 V were found sufficient for the transversal ejection of ion species with as few as three deflection pulses. The duty cycle, i.e., the pulse duration with respect to the period of ion revolution, has been varied, resulting in resolving powers of up to several tens of thousands for this selection technique.

  19. Planetary populations in the mass-period diagram: A statistical treatment of exoplanet formation and the role of planet traps

    Energy Technology Data Exchange (ETDEWEB)

    Hasegawa, Yasuhiro [Currently EACOA Fellow at Institute of Astronomy and Astrophysics, Academia Sinica (ASIAA), Taipei 10641, Taiwan. (China); Pudritz, Ralph E., E-mail: yasu@asiaa.sinica.edu.tw, E-mail: pudritz@physics.mcmaster.ca [Also at Origins Institute, McMaster University, Hamilton, ON L8S 4M1, Canada. (Canada)

    2013-11-20

    The rapid growth of observed exoplanets has revealed the existence of several distinct planetary populations in the mass-period diagram. Two of the most surprising are (1) the concentration of gas giants around 1 AU and (2) the accumulation of a large number of low-mass planets with tight orbits, also known as super-Earths and hot Neptunes. We have recently shown that protoplanetary disks have multiple planet traps that are characterized by orbital radii in the disks and halt rapid type I planetary migration. By coupling planet traps with the standard core accretion scenario, we showed that one can account for the positions of planets in the mass-period diagram. In this paper, we demonstrate quantitatively that most gas giants formed at planet traps tend to end up around 1 AU, with most of these being contributed by dead zones and ice lines. We also show that a large fraction of super-Earths and hot Neptunes are formed as 'failed' cores of gas giants—this population being constituted by comparable contributions from dead zone and heat transition traps. Our results are based on the evolution of forming planets in an ensemble of disks where we vary only the lifetimes of disks and their mass accretion rates onto the host star. We show that a statistical treatment of the evolution of a large population of planetary cores caught in planet traps accounts for the existence of three distinct exoplanetary populations—the hot Jupiters, the more massive planets around r = 1 AU, and the short-period super-Earths and hot Neptunes. There are very few populations that feed into the large orbital radii characteristic of the imaged Jovian planet, which agrees with recent surveys. Finally, we find that low-mass planets in tight orbits become the dominant planetary population for low-mass stars (M {sub *} ≤ 0.7 M {sub ☉}).

  20. From handwriting analysis to pen-computer applications

    NARCIS (Netherlands)

    Schomaker, L

    1998-01-01

    In this paper, pen computing, i.e. the use of computers and applications in which the pen is the main input device, will be described from four different viewpoints. Firstly a brief overview of the hardware developments in pen systems is given, leading to the conclusion that the technological

  1. Utility of Higher Harmonics in Electrospray Ionization Fourier Transform Electrostatic Linear Ion Trap Mass Spectrometry.

    Science.gov (United States)

    Dziekonski, Eric T; Johnson, Joshua T; McLuckey, Scott A

    2017-04-18

    Mass resolution (M/ΔM fwhm) is observed to linearly increase with harmonic order in a Fourier transform electrostatic linear ion trap (ELIT) mass spectrometer. This behavior was predicted by Grosshans and Marshall for frequency-multiple detection in a Fourier transform ion cyclotron resonance mass spectrometer only for situations when the prominent mechanism for signal decay is ion ejection from the trap. As the analyzer pressure in our ELIT chamber is relatively high, such that collisional scattering and collision-induced dissociation are expected to underlie much of the ion loss, we sought to explore the relationship between harmonic order and mass resolution. Mass resolutions of 36 900 (fundamental), 75 850 (2nd harmonic), and 108 200 (3rd harmonic) were obtained for GdO + (avg. m/z 173.919) with a transient length of 300 ms. To demonstrate that the mass resolution was truly increasing with harmonic order, the unresolved isotopes at the fundamental distribution of cytochrome c +8 (m/z ∼ 1549) were nearly baseline, resolved at the third harmonic (mass resolution ≈ 23 000) with a transient length of only 200 ms. This experiment demonstrates that, when the ion density is sufficiently low, ions with frequency differences of less than 4 Hz remain uncoalesced. Higher harmonics can be used to increase the effective mass resolution for a fixed transient length and thereby may enable the resolution of closely spaced masses, determination of a protein ion's charge state, and study of the onset of peak coalescence when the resolution at the fundamental frequency is insufficient.

  2. Evaluation of Commercial and Field-Expedient Baited Traps for House Flies, Musca domestica L. (Diptera: Muscidae)

    Science.gov (United States)

    2009-01-09

    32212, U.S.A. Received 7 September 2008; Accepted 9 January 2009 ABSTRACT: A comparison of nine commercial baited fly traps on Florida dairy farms...baits relied on natural products such as fermented egg slurries (Willson and Mulla 1973) or combinations of such items as molasses, milk, yeast, grain...2006 on four dairy farms in Gilchrist and Alachua counties, FL. Traps were placed near the calf pens on three of the farms and by the commodity

  3. The Influence of Trapped Particles on the Parametric Decay Instability of Near-Acoustic Waves

    Science.gov (United States)

    Affolter, M.; Anderegg, F.; Dubin, D. H. E.; Driscoll, C. F.

    2017-10-01

    We present quantitative measurements of a decay instability to lower frequencies of near-acoustic waves. These experiments are conducted on pure ion plasmas confined in a cylindrical Penning-Malmberg trap. The axisymmetric, standing plasma waves have near-acoustic dispersion, discretized by the axial wave number kz =mz(π /Lp) . The nonlinear coupling rates are measured between large amplitude mz = 2 (pump) waves and small amplitude mz = 1 (daughter) waves, which have a small frequency detuning Δω = 2ω1 -ω2 . Classical 3-wave parametric coupling rates are proportional to pump wave amplitude as Γ (δn2 /n0) , with oscillatory energy exchange for Γ Δω / 2 . Experiments on cold plasmas agree quantitatively for oscillatory energy exchange, and agree within a factor-of-two for decay instability rates. However, nascent theory suggest that this latter agreement is merely fortuitous, and that the instability mechanism is trapped particles. Experiments at higher temperatures show that trapped particles reduce the instability threshold below classical 3-wave theory predictions. Supported by NSF Grant PHY-1414570, and DOE Grants DE-SC0002451 and DE-SC0008693. M. Affolter is supported by the DOE FES Postdoctoral Research Program administered by ORISE for the DOE. ORISE is managed by ORAU under DOE Contract Number DE-SC0014664.

  4. Electrical shielding box measurement of the negative hydrogen beam from Penning ion gauge ion source.

    Science.gov (United States)

    Wang, T; Yang, Z; Dong, P; long, J D; He, X Z; Wang, X; Zhang, K Z; Zhang, L W

    2012-06-01

    The cold-cathode Penning ion gauge (PIG) type ion source has been used for generation of negative hydrogen (H(-)) ions as the internal ion source of a compact cyclotron. A novel method called electrical shielding box dc beam measurement is described in this paper, and the beam intensity was measured under dc extraction inside an electrical shielding box. The results of the trajectory simulation and dc H(-) beam extraction measurement were presented. The effect of gas flow rate, magnetic field strength, arc current, and extraction voltage were also discussed. In conclusion, the dc H(-) beam current of about 4 mA from the PIG ion source with the puller voltage of 40 kV and arc current of 1.31 A was extrapolated from the measurement at low extraction dc voltages.

  5. Ballpoint pen ingestion in a 2-year-old child.

    Science.gov (United States)

    Rameau, Anaïs; Anand, Sumeet M; Nguyen, Lily H

    2011-07-01

    A 2-year-old girl ingested a ballpoint pen, which was found on chest x-ray to have lodged in the lower esophagus and stomach. The pen, which measured nearly 15 cm in length, was removed via rigid esophagoscopy without complication. To the best of our knowledge, this is the longest nonflexible foreign body ingested by a young child ever reported in the English-language literature. We describe the presentation of this case and the current guidelines for safety as enumerated in the Small Parts Regulations established by the U.S. Consumer Product Safety Commission.

  6. Detection of lysergic acid diethylamide (LSD) in urine by gas chromatography-ion trap tandem mass spectrometry.

    Science.gov (United States)

    Sklerov, J H; Kalasinsky, K S; Ehorn, C A

    1999-10-01

    A confirmatory method for the detection and quantitation of lysergic acid diethylamide (LSD) is presented. The method employs gas chromatography-tandem mass spectrometry (GC-MS-MS) using an internal ionization ion trap detector for sensitive MS-MS-in-time measurements of LSD extracted from urine. Following a single-step solid-phase extraction of 5 mL of urine, underivatized LSD can be measured with limits of quantitation and detection of 80 and 20 pg/mL, respectively. Temperature-programmed on-column injections of urine extracts were linear over the concentration range 20-2000 pg/mL (r2 = 0.999). Intraday and interday coefficients of variation were LSD-positive samples in this laboratory. Comparisons with alternate GC-MS methods and extraction procedures are discussed.

  7. Use of Early Ripening Cultivars to Avoid Infestation and Mass Trapping to Manage Drosophila suzukii (Diptera: Drosophilidae) in Vaccinium corymbosum (Ericales: Ericaceae).

    Science.gov (United States)

    Hampton, Emily; Koski, Carissa; Barsoian, Olivia; Faubert, Heather; Cowles, Richard S; Alm, Steven R

    2014-10-01

    Use of early ripening highbush blueberry cultivars to avoid infestation and mass trapping were evaluated for managing spotted wing drosophila, Drosophila suzukii (Matsumura). Fourteen highbush blueberry cultivars were sampled for spotted wing drosophila infestation. Most 'Earliblue', 'Bluetta', and 'Collins' fruit were harvested before spotted wing drosophila oviposition commenced, and so escaped injury. Most fruit from 'Bluejay', 'Blueray', and 'Bluehaven' were also harvested before the first week of August, after which spotted wing drosophila activity led to high levels of blueberry infestation. In a separate experiment, damage to cultivars was related to the week in which fruit were harvested, with greater damage to fruit observed as the season progressed. Attractant traps placed within blueberry bushes increased nearby berry infestation by 5%, irrespective of cultivar and harvest date. The significant linear reduction in infestation with increasing distance from the attractant trap suggests that traps are influencing fly behavior to at least 5.5 m. Insecticides applied to the exterior of traps, compared with untreated traps, revealed that only 10-30% of flies visiting traps enter the traps and drown. Low trap efficiency may jeopardize surrounding fruits by increasing local spotted wing drosophila activity. To protect crops, traps for mass trapping should be placed in a perimeter outside fruit fields and insecticides need to be applied to the surface of traps or on nearby fruit to function as an attract-and-kill strategy. © 2014 Entomological Society of America.

  8. Sensitive and comprehensive detection of chemical warfare agents in air by atmospheric pressure chemical ionization ion trap tandem mass spectrometry with counterflow introduction.

    Science.gov (United States)

    Seto, Yasuo; Sekiguchi, Hiroshi; Maruko, Hisashi; Yamashiro, Shigeharu; Sano, Yasuhiro; Takayama, Yasuo; Sekioka, Ryoji; Yamaguchi, Shintaro; Kishi, Shintaro; Satoh, Takafumi; Sekiguchi, Hiroyuki; Iura, Kazumitsu; Nagashima, Hisayuki; Nagoya, Tomoki; Tsuge, Kouichiro; Ohsawa, Isaac; Okumura, Akihiko; Takada, Yasuaki; Ezawa, Naoya; Watanabe, Susumu; Hashimoto, Hiroaki

    2014-05-06

    A highly sensitive and specific real-time field-deployable detection technology, based on counterflow air introduction atmospheric pressure chemical ionization, has been developed for a wide range of chemical warfare agents (CWAs) comprising gaseous (two blood agents, three choking agents), volatile (six nerve gases and one precursor agent, five blister agents), and nonvolatile (three lachrymators, three vomiting agents) agents in air. The approach can afford effective chemical ionization, in both positive and negative ion modes, for ion trap multiple-stage mass spectrometry (MS(n)). The volatile and nonvolatile CWAs tested provided characteristic ions, which were fragmented into MS(3) product ions in positive and negative ion modes. Portions of the fragment ions were assigned by laboratory hybrid mass spectrometry (MS) composed of linear ion trap and high-resolution mass spectrometers. Gaseous agents were detected by MS or MS(2) in negative ion mode. The limits of detection for a 1 s measurement were typically at or below the microgram per cubic meter level except for chloropicrin (submilligram per cubic meter). Matrix effects by gasoline vapor resulted in minimal false-positive signals for all the CWAs and some signal suppression in the case of mustard gas. The moisture level did influence the measurement of the CWAs.

  9. Increasing viscosity and inertia using a robotically-controlled pen improves handwriting in children

    Science.gov (United States)

    Ben-Pazi, Hilla; Ishihara, Abraham; Kukke, Sahana; Sanger, Terence D

    2010-01-01

    The aim of this study was to determine the effect of mechanical properties of the pen on the quality of handwriting in children. Twenty two school aged children, ages 8–14 years wrote in cursive using a pen attached to a robot. The robot was programmed to increase the effective weight (inertia) and stiffness (viscosity) of the pen. Speed, frequency, variability, and quality of the two handwriting samples were compared. Increased inertia and viscosity improved handwriting quality in 85% of children (pHandwriting quality did not correlate with changes in speed, suggesting that improvement was not due to reduced speed. Measures of movement variability remained unchanged, suggesting that improvement was not due to mechanical smoothing of pen movement by the robot. Since improvement was not explained by reduced speed or mechanical smoothing, we conclude that children alter handwriting movements in response to pen mechanics. Altered movement could be caused by changes in proprioceptive sensory feedback. PMID:19794098

  10. Plasma manipulation techniques for positron storage in a multicell trap

    International Nuclear Information System (INIS)

    Danielson, J. R.; Weber, T. R.; Surko, C. M.

    2006-01-01

    New plasma manipulation techniques are described that are central to the development of a multicell Penning trap designed to increase positron storage by orders of magnitude (e.g., to particle numbers N≥10 12 ). The experiments are done using test electron plasmas. A technique is described to move plasmas across the confining magnetic field and to deposit them at specific radial and azimuthal positions. Techniques to fill and operate two in-line plasma cells simultaneously, and the use of 1 kV confinement potentials are demonstrated. These experiments establish the capabilities to create, confine, and manipulate plasmas with the parameters required for a multicell trap; namely, particle numbers >10 10 in a single cell with plasma temperature ≤0.2 eV for plasma lengths ∼10 cm and radii ≤0.2 cm. The updated design of a multicell positron trap for 10 12 particles is described

  11. Negative Ion Sources: Magnetron and Penning

    CERN Document Server

    Faircloth, D.C.

    2013-12-16

    The history of the magnetron and Penning electrode geometry is briefly outlined. Plasma generation by electrical discharge-driven electron impact ionization is described and the basic physics of plasma and electrodes relevant to magnetron and Penning discharges are explained. Negative ions and their applications are introduced, along with their production mechanisms. Caesium and surface production of negative ions are detailed. Technical details of how to build magnetron and Penning surface plasma sources are given, along with examples of specific sources from around the world. Failure modes are listed and lifetimes compared.

  12. Negative Ion Sources: Magnetron and Penning

    International Nuclear Information System (INIS)

    Faircloth, D C

    2013-01-01

    The history of the magnetron and Penning electrode geometry is briefly outlined. Plasma generation by electrical discharge-driven electron impact ionization is described and the basic physics of plasma and electrodes relevant to magnetron and Penning discharges are explained. Negative ions and their applications are introduced, along with their production mechanisms. Caesium and surface production of negative ions are detailed. Technical details of how to build magnetron and Penning surface plasma sources are given, along with examples of specific sources from around the world. Failure modes are listed and lifetimes compared. (author)

  13. Weighing halo nuclides

    International Nuclear Information System (INIS)

    Lunney, D.

    2009-01-01

    Weak binding energy is one of the fundamental criteria characterizing the unique properties of nuclear halos. As such, it must be known with great accuracy and is best obtained through direct mass measurements. The global mass market is now a competitive one. Of the many investment vehicles, the Penning trap has emerged as providing the best rate of return and reliability. We examine mass-market trends, highlighting the recent cases of interest. We also hazard a prediction for the halo futures market. (author)

  14. Optimization and simulation of MEMS rectilinear ion trap

    Directory of Open Access Journals (Sweden)

    Huang Gang

    2015-04-01

    Full Text Available In this paper, the design of a MEMS rectilinear ion trap was optimized under simulated conditions. The size range of the MEMS rectilinear ion trap’s electrodes studied in this paper is measured at micron scale. SIMION software was used to simulate the MEMS rectilinear ion trap with different sizes and different radio-frequency signals. The ion-trapping efficiencies of the ion trap under these different simulation conditions were obtained. The ion-trapping efficiencies were compared to determine the performance of the MEMS rectilinear ion trap in different conditions and to find the optimum conditions. The simulation results show that for the ion trap at micron scale or smaller, the optimized length–width ratio was 0.8, and a higher frequency of radio-frequency signal is necessary to obtain a higher ion-trapping efficiency. These results have a guiding role in the process of developing MEMS rectilinear ion traps, and great application prospects in the research fields of the MEMS rectilinear ion trap and the MEMS mass spectrometer.

  15. 40 CFR 75.15 - Special provisions for measuring Hg mass emissions using the excepted sorbent trap monitoring...

    Science.gov (United States)

    2010-07-01

    ... 40 Protection of Environment 16 2010-07-01 2010-07-01 false Special provisions for measuring Hg... EMISSION MONITORING Monitoring Provisions § 75.15 Special provisions for measuring Hg mass emissions using... Federal Hg mass emission reduction program that adopts the provisions of subpart I of this part, if the...

  16. III. Penning ionization, associative ionization and chemi-ionization processes

    International Nuclear Information System (INIS)

    Cermak, V.

    1975-01-01

    Physical mechanisms of three important ionization processes in a cold plasma and the methods of their experimental study are discussed. An apparatus for the investigation of the Penning ionization using ionization processes of long lived metastable rare gas atoms is described. Methods of determining interaction energies and ionization rates from the measured energy spectra of the originating electrons are described and illustrated by several examples. Typical associative ionization processes are listed and the ionization rates are compared with those of the Penning ionization. Interactions with short-lived excited particles and the transfer of excitation without ionization are discussed. (J.U.)

  17. Isodose plotting for pen plotters

    International Nuclear Information System (INIS)

    Rosen, I.I.

    1985-01-01

    A general algorithm for treatment plan isodose line plotting is described which is particularly useful for pen plotters. Unlike other methods of plotting isodose lines, this algorithm is designed specifically to reduce pen motion, thereby reducing plotting time and wear on the transport mechanism. Points with the desired dose value are extracted from the dose matrix and stored, sorted into continuous contours, and then plotted. This algorithm has been implemented on DEC PDP-11/60 and VAX-11/780 computers for use with two models of Houston Instrument pen plotters, two models of Tektronix vector graphics terminals, a DEC VT125 raster graphics terminal, and a DEC VS11 color raster graphics terminal. Its execution time is similar to simpler direct-plotting methods

  18. Carbon-cluster mass calibration at SHIPTRAP

    Energy Technology Data Exchange (ETDEWEB)

    Chaudhuri, Ankur

    2007-12-10

    A carbon-cluster ion source has been installed and tested at SHIPTRAP, the Penning-trap mass spectrometer for mass measurements of heavy elements at GSI/Darmstadt, Germany. A precision mass determination is carried out by measuring the ion cyclotron frequency {omega}{sub c}=qB=m, where q/m is the charge-to-mass ratio of the ion and B is the magnetic field. The mass of the ion of interest is obtained from the comparison of its cyclotron frequency {omega}{sub c} with that of a well-known reference ion. Carbon clusters are the mass reference of choice since the unified atomic mass unit is defined as 1/12 of the mass of the {sup 12}C atom. Thus the masses of carbon clusters {sup 12}C{sub n}, n=1,2,3,.. are multiples of the unified atomic mass unit. Carbon-cluster ions {sup 12}C{sub n}{sup +}, 5{<=}n{<=}23, were produced by laser-induced desorption and ionization from a carbon sample. Carbon clusters of various sizes ({sup 12}C{sub 7}{sup +}, {sup 12}C{sub 9}{sup +}, {sup 12}C{sub 10}{sup +}, {sup 12}C{sub 11}{sup +}, {sup 12}C{sub 12}{sup +}, {sup 12}C{sub 15}{sup +}, {sup 12}C{sub 18}{sup +}, {sup 12}C{sub 19}{sup +}, {sup 12}C{sub 20}{sup +}) were used for an investigation of the accuracy of SHIPTRAP covering a mass range from 84 u to 240 u. To this end the clusters were used both as ions of interest and reference ions. Hence the true values of the frequency ratios are exactly known. The mass-dependent uncertainty was found to be negligible for the case of (m-m{sub ref})<100 u. However, a systematic uncertainty of 4.5 x 10{sup -8} was revealed. In addition, carbon clusters were employed for the first time as reference ions in an on-line studies of short-lived nuclei. Absolute mass measurements of the radionuclides {sup 144}Dy, {sup 146}Dy and {sup 147}Ho were performed using {sup 12}C{sub 11}{sup +} as reference ion. The results agree with measurements during the same run using {sup 85}Rb{sup +} as reference ion. The investigated radionuclides were produced in the

  19. Online trapping and enrichment ultra performance liquid chromatography–tandem mass spectrometry method for sensitive measurement of “arginine-asymmetric dimethylarginine cycle” biomarkers in human exhaled breath condensate

    International Nuclear Information System (INIS)

    Di Gangi, Iole Maria; Pirillo, Paola; Carraro, Silvia; Gucciardi, Antonina; Naturale, Mauro; Baraldi, Eugenio; Giordano, Giuseppe

    2012-01-01

    Highlights: ► Simultaneous quantification of “arginine-ADMA cycle” metabolites developed in EBC. ► EBC is a non-invasive matrix highly useful in patients with respiratory diseases. ► Method, fast, precise and accurate, is suitable in the pediatric clinical studies. ► Sensitivity is increased using on-line trapping and enrichment-UPLC–MS/MS method. ► EBC measurements in asthmatic adolescents confirm that ADMA is increased in asthma. - Abstract: Background: Exhaled breath condensate (EBC) is a biofluid collected non invasively that, enabling the measurement of several biomarkers, has proven useful in the study of airway inflammatory diseases, including asthma, COPD and cystic fibrosis. To the best of our knowledge, there is no previous report of any analytical method to detect ADMA in EBC. Objectives: Aim of this work was to develop an online sample trapping and enrichment system, coupled with an UPLC–MS/MS method, for simultaneous quantification of seven metabolites related to “Arginine-ADMA cycle”, using the isotopic dilution. Methods: Butylated EBC samples were trapped in an online cartridge, washed before and after each injection with cleanup solution to remove matrix components and switched inline into the high pressure analytical column. Multiple reaction monitoring in positive mode was used for analyte quantification by tandem mass spectrometry. Results: Validation studies were performed in EBC to examine accuracy, precision and robustness of the method. For each compound, the calibration curves showed a coefficient of correlation (r 2 ) greater than 0.992. Accuracy (%Bias) was −1 ), measured in EBC samples of asthmatic adolescents are significantly increased (p < 0.0001) than in normal controls (0.0040 ± 0.0021 vs. 0.0012 ± 0.0005 and 0.0020 ± 0.0015 vs. 0.0002 ± 0.0001, respectively), as well the ADMA/Tyr (0.34 ± 0.09 vs. 0.12 ± 0.02, p < 0.0001) and the SDMA/Tyr ratio (0.10 ± 0.04 vs. 0.015 ± 0.004, p < 0.0001). Conclusions

  20. The LongPen--the world's first original remote signing device.

    Science.gov (United States)

    Kruger, Diane M

    2010-05-01

    The LongPen is a remote-controlled pen and videoconferencing device conceived by Canadian author Margaret Atwood in 2004 and initially intended to bring "live" author signings to far away locations. The LongPen allows for individually inscribed long distance signatures and writing while maintaining an original record, written with pen and ink. LongPen specimens were compared with control specimens using different speeds, pen pressures, and types of pens. Preliminary indications are that LongPen inscriptions can be identified or associated with their author. Size and form are maintained and artifacts are subtle. Some limitations with respect to the capture of long tapered strokes, delicate connecting strokes, and differences in line width were noted. Factors which may impact forensic handwriting examinations include limited amounts of writing, light pen pressure, date of the writing, type of writing instrument, dimensions of the writing, and failure to consider that the device has been used.

  1. Precision measurements on trapped antihydrogen in the ALPHA experiment

    Science.gov (United States)

    Eriksson, S.

    2018-03-01

    Both the 1S-2S transition and the ground state hyperfine spectrum have been observed in trapped antihydrogen. The former constitutes the first observation of resonant interaction of light with an anti-atom, and the latter is the first detailed measurement of a spectral feature in antihydrogen. Owing to the narrow intrinsic linewidth of the 1S-2S transition and use of two-photon laser excitation, the transition energy can be precisely determined in both hydrogen and antihydrogen, allowing a direct comparison as a test of fundamental symmetry. The result is consistent with CPT invariance at a relative precision of around 2×10-10. This constitutes the most precise measurement of a property of antihydrogen. The hyperfine spectrum of antihydrogen is determined to a relative uncertainty of 4×10-4. The excited state and the hyperfine spectroscopy techniques currently both show sensitivity at the few 100 kHz level on the absolute scale. Here, the most recent work of the ALPHA collaboration on precision spectroscopy of antihydrogen is presented together with an outlook on improving the precision of measurements involving lasers and microwave radiation. Prospects of measuring the Lamb shift and determining the antiproton charge radius in trapped antihydrogen in the ALPHA apparatus are presented. Future perspectives of precision measurements of trapped antihydrogen in the ALPHA apparatus when the ELENA facility becomes available to experiments at CERN are discussed. This article is part of the Theo Murphy meeting issue `Antiproton physics in the ELENA era'.

  2. Synergy of decay spectroscopy and mass spectrometry for the study of exotic nuclides

    CERN Document Server

    Stanja, Juliane

    With only two ingredients, atomic nuclei exhibit a rich structure depending on the ordering of the different proton- and neutron-occupied states. This ordering can give rise to excited states with exceptionally long half-lives, also known as isomers, especially near shell closures. On-line mass spectrometry can often be compromised by the existence of such states that may even be produced in higher proportion than the ground state. This thesis presents the first results obtained from a nuclear spectroscopy setup coupled with the high-resolution Penning-trap mass spectrometer ISOLTRAP, at CERN’s radioactive ion beam facility ISOLDE. The isomerism in the neutron-deficient thallium isotopes was investigated. The data on $^{184,190,193−195}$Tl allow an improvement of existing mass values as well as a mass-spin- state assignment in $^{ 190,193,194}$Tl. Due to the presence of the ground and isomeric state for $^{ 194}$Tl the excitation energy of the latter was determined for the first time experimentally. Syste...

  3. Results from a Test Fixture for button BPM Trapped Mode Measurements

    Energy Technology Data Exchange (ETDEWEB)

    Cameron,P.; Bacha, B.; Blednykh, A.; Pinayev, I.; Singh, O.

    2009-05-04

    A variety of measures have been suggested to mitigate the problem of button BPM trapped mode heating. A test fixture, using a combination of commercial-off-the-shelf and custom machined components, was assembled to validate the simulations. We present details of the fixture design, measurement results, and a comparison of the results with the simulations. A brief history of the trapped mode button heating problem and a set of design rules for BPM button optimization are presented elsewhere in these proceedings. Here we present measurements on a test fixture that was assembled to confirm, if possible, a subset of those rules: (1) Minimize the trapped mode impedance and the resulting power deposited in this mode by the beam. (2) Maximize the power re-radiated back into the beampipe. (3) Maximize electrical conductivity of the outer circumference of the button and minimize conductivity of the inner circumference of the shell, to shift power deposition from the button to the shell. The problem is then how to extract useful and relevant information from S-parameter measurements of the test fixture.

  4. Pen of Health Care Worker as Vector of Infection

    Directory of Open Access Journals (Sweden)

    Prashant Patil

    2010-10-01

    Full Text Available Nosocomial infections are the major concern in tertiary hospitals. Health care workers and their belonging are known to act as vector in transmission of infections. In present study, the writing pen of health care workers was worked out for carrying infection. The swab from writing pen of health care workers were cultured for any growth of microorganism and compared with swab from pen of the non health care workers. It was found that the rate of growth of microorganism were more in pen of health care workers. Similarly the organism attributed to the nosocomial infection was grown from the pens of health care workers. These organisms might be transmitted from the hands of health care workers. The writing pen which health care worker are using became the vectors of transmission of infection. So to prevent it, the most important way is to wash the hands and pen properly after examining the patients.

  5. Towards accurate T-3He Q-value

    Energy Technology Data Exchange (ETDEWEB)

    Eronen, Tommi; Hoecker, Martin; Ketter, Jochen; Streubel, Sebastian; Blaum, Klaus [Max-Planck Institut fuer Kernphysik, Heidelberg (Germany); Van Dyck, Robert S. Jr. [Department of Physics, University of Washington, Seattle, WA (United States)

    2013-07-01

    Great efforts have been put forward to determine the neutrino mass from tritium β decay. The most prominent experimental setup, KATRIN, is expected to deliver an upper limit to the neutrino mass that is one order of magnitude more stringent than the current value by measuring the endpoint and the shape of the β spectrum of the tritium decay. The endpoint energy (assuming zero neutrino mass) can also be deduced from the Q-value of the decay by measuring the mass difference of tritium and the daughter {sup 3}He using high-resolution mass spectrometry. Such a measurement would give an excellent, independent calibration point for the KATRIN experiment to deduce its systematics. Our mass-difference measurement utilizes the Tritium- Helium double Penning trap (THe-Trap) setup. Based on the anharmonic cyclotron frequency determination method pioneered at the University of Washington, Seattle, precision at the level of 1 part in 10{sup 11} in the T/{sup 3}He mass ratio is expected. In this contribution, I describe the motivation, the principle, current status, and expectations of the experiment.

  6. Air trapping on computed tomography images of healthy individuals: effects of respiration and body mass index

    International Nuclear Information System (INIS)

    Hashimoto, M.; Tate, E.; Watarai, J.; Sasaki, M.

    2006-01-01

    Aim: To evaluate the relationships of changes in the lung area during respiration and of individual body mass index (BMI) to air trapping on expiratory computed tomography (CT) in young non-smoking adults of either gender. Methods: The volunteers were 10 women and 10 men (mean age 25.7 years) who were healthy lifelong non-smokers. We obtained both end-inspiratory and end-expiratory CT images at three levels: the upper, middle and lower lung. The ratio of cross-sectional lung area upon expiration to cross-sectional lung area upon inspiration (lung area ratio) was determined for each lung at each of the three levels. In cases showing air trapping, we calculated the percentage of area of air in relation to the total lung area in each section. BMI was calculated for each participant. Results: Air trapping was present in dependent areas of the lungs of 6 women and 5 men. The mean percentage of area of air trapped was statistically greater for men (9.8 ± 9.2%) than for women (4.9 ± 5.2%). The mean lung area ratio was 0.52 ± 0 14 among volunteers with air trapping (66 sections) and 0.69 ± 0.12 among those without air trapping (54 sections) (p < 0.001). At each lung level, the mean lung area ratio was greater in individuals with air trapping than in those without. Mean BMI was also greater in these people (p = 0.009). Conclusion: Change in the respiratory lung area and BMI contribute to development of air trapping

  7. Self-consistent static analysis of using nested-well plasma traps for achieving antihydrogen recombination

    International Nuclear Information System (INIS)

    Dolliver, D. D.; Ordonez, C. A.

    1999-01-01

    The use of a Malmberg-Penning type trap with nested electric potential wells to confine overlapping antiproton and positron plasmas for the purpose of producing low temperature antihydrogen is studied. Two approaches for confining antiproton and positron plasmas with a region of overlap are considered. In one approach the two components have a large temperature difference. In the other, one of the components is in a nonequilibrium 'antishielding' plasma state. A finite differences algorithm is used to solve Poisson's equation based on a simultaneous overrelaxation numerical approach. Self-consistent numerical results for required trap potentials and possible particle density profiles are presented

  8. Spectral measurements of few-electron uranium ions produced and trapped in a high-energy electron beam ion trap

    International Nuclear Information System (INIS)

    Beiersdorfer, P.

    1994-01-01

    Measurements of 2s l/2 -2p 3/2 electric dipole and 2p 1/2 -2p 3/2 magnetic dipole and electric quadrupole transitions in U 82+ through U 89+ have been made with a high-resolution crystal spectrometer that recorded the line radiation from stationary ions produced and trapped in a high-energy electron beam ion trap. From the measurements we infer -39.21 ± 0.23 eV for the QED contribution to the 2s 1/2 -2p 3/2 transition energy of lithiumlike U 89+ . A comparison between our measurements and various computations illustrates the need for continued improvements in theoretical approaches for calculating the atomic structure of ions with two or more electrons in the L shell

  9. Particle fluxes in the Bay of Bengal measurEd. by sediment traps

    Digital Repository Service at National Institute of Oceanography (India)

    Ramaswamy, V.; Parthiban, G.

    Particle fluxes were measured between October, 1987 and March, 1988 using six automated time series sediment traps at three locations in the northern, central and southern Bay of Bengal. Particle fluxes varied between 16.8 and 345 mg m/2 day/1...

  10. A lethal ovitrap-based mass trapping scheme for dengue control in Australia: I. Public acceptability and performance of lethal ovitraps.

    Science.gov (United States)

    Ritchie, S A; Rapley, L P; Williams, C; Johnson, P H; Larkman, M; Silcock, R M; Long, S A; Russell, R C

    2009-12-01

    We report on the first field evaluation of the public acceptability and performance of two types of lethal ovitrap (LO) in three separate trials in Cairns, Australia. Health workers were able to set standard lethal ovitraps (SLOs) in 75 and 71% of premise yards in the wet and dry season, respectively, and biodegradable lethal ovitraps (BLOs) in 93% of yards. Public acceptance, measured as retention of traps by residents, was high for both trap types, with porous (grass, soil and mulch) versus solid (tiles, concrete, wood and stone) substrates. The SLOs and the BLOs were readily acceptable to ovipositing Aedes aegypti L. (Diptera: Culicidae); the mean number of eggs/trap was 6 and 15, for the dry season and wet season SLO trial, respectively, and 15 for the BLO wet season trial. Indeed, 84-94% of premise yards had egg positive SLOs or BLOs. A high percentage of both wet and dry season SLOs (29 and 70%, respectively) and BLOs (62%) that were dry after 4 weeks were egg positive, indicating the traps had functioned. Lethal strips from SLOs and BLOs that had been exposed for 4 weeks killed 83 and 74%, respectively, of gravid Ae. aegypti in laboratory assays. These results indicate that mass trapping schemes using SLOs and BLOs are not rejected by the public and effectively target gravid Ae. aegypti. The impact of the interventions on mosquito populations is described in a companion paper.

  11. Measurement of Secular Motion Frequency in Miniature Paul Trap to Ascertain the Stability Parameters

    International Nuclear Information System (INIS)

    Bin, Guo; Hua, Guan; Qu, Liu; Yao, Huang; Xue-Ren, Huang; Ke-Lin, Gao

    2010-01-01

    40 Ca + ions are trapped and laser cooled in a miniature Paul trap. The secular motion was observed by the radio-frequency resonance of the ion cloud and Zeeman profile sidebands of a single ion experimentally. The trap stability parameters a and q are determined with an uncertainty under 1 % by the secular motion frequency measurement. The trap efficiency is 0.75. A practicable suggestion is given for the benefits of a new trap design. (atomic and molecular physics)

  12. The effects of zonation of the pen and grouping in intact litters on use of pen, immune competence and health of pigs

    DEFF Research Database (Denmark)

    Damgaard, B.M.; Studnitz, M.; Nielsen, Jens

    2006-01-01

    The effects of pen design and group composition were examined with respect to activity, use of pen, floor conditions, health condition and immune competence for groups of 60 pigs. The experiment was designed with the two factors with zones/without zones and divided litters/intact litters....... The experiment included a total of 1440 pigs from weaning at the age of 4 weeks to the age of 18 weeks after weaning. In pens with zones, the selection of different areas for different activities was improved. Pens with zones were more dirty in the elimination and open areas than pens without zones. In pens...... with zones, the number of lymphocytes was decreased, the ability to respond to an additional challenge by a model infection was decreased and the number of neutrophils was increased in intact litters. In week 9, the health condition was better with a group composition consisting of intact litters compared...

  13. Stable Trapping of Multielectron Helium Bubbles in a Paul Trap

    Science.gov (United States)

    Joseph, E. M.; Vadakkumbatt, V.; Pal, A.; Ghosh, A.

    2017-06-01

    In a recent experiment, we have used a linear Paul trap to store and study multielectron bubbles (MEBs) in liquid helium. MEBs have a charge-to-mass ratio (between 10^{-4} and 10^{-2} C/kg) which is several orders of magnitude smaller than ions (between 10^6 and 10^8 C/kg) studied in traditional ion traps. In addition, MEBs experience significant drag force while moving through the liquid. As a result, the experimental parameters for stable trapping of MEBs, such as magnitude and frequency of the applied electric fields, are very different from those used in typical ion trap experiments. The purpose of this paper is to model the motion of MEBs inside a linear Paul trap in liquid helium, determine the range of working parameters of the trap, and compare the results with experiments.

  14. Pen- Name in Persian and Arabic Poetry

    Directory of Open Access Journals (Sweden)

    Ebrahim Khodayar

    2012-03-01

    Full Text Available  Abstract Pen-name (Takhalloss is one of the main features of Persian poetry. It has been a matter of concern among many of Persian language geography poets in the orient at least up to the Mashrouteh era. Pen-name has been promoted among the other Muslim nations throuph Persian poetry. Although it is not as famous in the Arab nations as in the Persian speaking nations, it is known as “Alqab-o-shoara” among the Arab nations and, through this way, it has affected the poetrical wealth of the Arabic poets.   The Present paper, using description-analystic approach, compares the pen-names of Persian and Arabic poets under the title of “pen-names” and investigates their features in both cultures. The main research question is: What are the similarities and differences of poetic-names, in Persian and Arabic poets in terms of the type of name, position and importance? The results showed that Pseudonym by its amazing expansion in Persian poetry has also influenced Arabic poetry. In addition to the factors affecting in the choice of pen-names (like pseudonym, pen-name, nickname..., sometimes such external factors as events, commends, community benefactors and climate, as well as internal factors including the poets’ inner beliefs are associated too. .

  15. Uncertainty quantification for nuclear density functional theory and information content of new measurements.

    Science.gov (United States)

    McDonnell, J D; Schunck, N; Higdon, D; Sarich, J; Wild, S M; Nazarewicz, W

    2015-03-27

    Statistical tools of uncertainty quantification can be used to assess the information content of measured observables with respect to present-day theoretical models, to estimate model errors and thereby improve predictive capability, to extrapolate beyond the regions reached by experiment, and to provide meaningful input to applications and planned measurements. To showcase new opportunities offered by such tools, we make a rigorous analysis of theoretical statistical uncertainties in nuclear density functional theory using Bayesian inference methods. By considering the recent mass measurements from the Canadian Penning Trap at Argonne National Laboratory, we demonstrate how the Bayesian analysis and a direct least-squares optimization, combined with high-performance computing, can be used to assess the information content of the new data with respect to a model based on the Skyrme energy density functional approach. Employing the posterior probability distribution computed with a Gaussian process emulator, we apply the Bayesian framework to propagate theoretical statistical uncertainties in predictions of nuclear masses, two-neutron dripline, and fission barriers. Overall, we find that the new mass measurements do not impose a constraint that is strong enough to lead to significant changes in the model parameters. The example discussed in this study sets the stage for quantifying and maximizing the impact of new measurements with respect to current modeling and guiding future experimental efforts, thus enhancing the experiment-theory cycle in the scientific method.

  16. Sodium hydride precipitation in sodium cold traps

    International Nuclear Information System (INIS)

    McPheeters, C.C.; Raue, D.J.

    1979-10-01

    A series of experiments have been performed to test a calculational model for precipitation of NaH in sodium cold traps. The calculational model, called ACTMODEL, is a computer simulation that uses the system geometry and operating conditions as input to calculate a mass transfer coefficient and the distribution of NaH in a cold trap. The ACTMODEL was tested using an analytical cold trap (ACT) that is simple and essentially one-dimensional. The ACT flow and temperature profile may be controlled at any desired condition. The ACT was analyzed destructively after each test to measure the actual NaH distribution. Excellent agreement was obtained between the ACTMODEL simulations and the experiments

  17. Fundamental tests of nature with cooled and stored exotic ions

    CERN Multimedia

    CERN. Geneva

    2014-01-01

    The presentation will concentrate on recent applications with exciting results of Penning traps in atomic and nuclear physics with cooled and stored exotic ions. These are high-accuracy mass measurements of short-lived radionuclides, g-factor determinations of the bound-electron in highly-charged, hydrogen-like ions and g-factor measurements of the proton and antiproton. The experiments are dedicated, e.g., to astrophysics studies and to tests of fundamental symmetries in the case of mass measurements on radionuclides, and to the determination of fundamental constants and a CPT test in the case of the g-factor measurements.

  18. Positrons in gas filled traps and their transport in molecular gases

    Energy Technology Data Exchange (ETDEWEB)

    Petrovic, Z Lj; Bankovic, A; Marjanovic, S; Suvakov, M; Dujko, S; Malovic, G [Institute of Physics, University of Belgrade, Pregrevica 118, POB 68, Zemun (Serbia); White, R D [ARC Centre for Antimatter-Matter Studies, James Cook University, Townsville 4810, QLD (Australia); Buckman, S J, E-mail: zoran@ipb.ac.rs [ARC Centre for Antimatter-Matter Studies, Australian National University, Canberra, ACT, 0200 (Australia)

    2011-01-01

    In this paper we give a review of two recent developments in positron transport, calculation of transport coefficients for a relatively complete set of collision cross sections for water vapour and for application of they Monte Carlo technique to model gas filled subexcitation positron traps such as Penning Malmberg Surko (Surko) trap. Calculated transport coefficients, very much like those for argon and other molecular gases show several new kinetic phenomena. The most important is the negative differential conductivity (NDC) for the bulk drift velocity when the flux drift velocity shows no sign of NDC. These results in water vapour are similar to the results in argon or hydrogen. The same technique that has been used for positron (and previously electron) transport may be applied to model development of particles in a Surko trap. We have provided calculation of the ensemble of positrons in the trap from an initial beam like distribution to the fully thermalised distribution. This model, however, does not include plasma effects (interaction between charged particles) and may be applied for lower positron densities.

  19. The masses of nobelium and lawrencium isotopes, the mass difference between {sup 180}W and {sup 180}Hf, and a characterization of the future cryogenic stopping cell of the online mass spectrometer SHIPTRAP

    Energy Technology Data Exchange (ETDEWEB)

    Droese, Christian

    2015-01-29

    This work describes the recent scientific and technical achievements obtained at the high-precision Penning trap mass spectrometer SHIPTRAP. The scientific focus of the SHIPTRAP experiment are mass measurements of short-lived nuclides with proton number larger than 100. The masses of these isotopes are usually determined via extrapolations, systematic trends, predictions based on theoretical models or alpha-decay spectroscopy. In several experiments the masses of the isotopes {sup 252-255}No and {sup 255,256}Lr have been measured directly. With the obtained results the region of enhanced nuclear stability at the deformed shell closure at the neutron number 152 was investigated. Furthermore, the masses have been used to benchmark theoretical mass models. The measured masses were compared selected mass models which revealed differences between few keV/c² up to several MeV/c² depending on the investigated nuclide and model. In order to perform mass measurements on superheavy nuclei with lower production rates, the efficiency of the SHIPTRAP setup needs to be increased. Currently, the efficiency is 2% and mainly limited by the stopping- and extraction efficiency of the buffer gas cell. The stopping and extraction efficiency of the current buffer gas cell is 12%. To this end, a modified version of the buffer gas cell was developed and characterized with {sup 223}Ra ion source. Besides a larger stopping volume and a coaxial injection the new buffer gas cell is operated at a temperature of 40 K. The operation at cryogenic temperatures increases the cleanliness of the buffer gas. From extraction measurements and simulations an overall efficiency of 62(3)% was determined which results in an increase by a factor of 5 in comparison to the current buffer gas cell. Aside from high-precision mass measurements of heavy radionuclides the mass differences of metastable isobars was measured to identify candidates for the neutrinoless double-electron capture. Neutrinoless double

  20. Mass-manufacturable polymer microfluidic device for dual fiber optical trapping.

    Science.gov (United States)

    De Coster, Diane; Ottevaere, Heidi; Vervaeke, Michael; Van Erps, Jürgen; Callewaert, Manly; Wuytens, Pieter; Simpson, Stephen H; Hanna, Simon; De Malsche, Wim; Thienpont, Hugo

    2015-11-30

    We present a microfluidic chip in Polymethyl methacrylate (PMMA) for optical trapping of particles in an 80µm wide microchannel using two counterpropagating single-mode beams. The trapping fibers are separated from the sample fluid by 70µm thick polymer walls. We calculate the optical forces that act on particles flowing in the microchannel using wave optics in combination with non-sequential ray-tracing and further mathematical processing. Our results are compared with a theoretical model and the Mie theory. We use a novel fabrication process that consists of a premilling step and ultraprecision diamond tooling for the manufacturing of the molds and double-sided hot embossing for replication, resulting in a robust microfluidic chip for optical trapping. In a proof-of-concept demonstration, we show the trapping capabilities of the hot embossed chip by trapping spherical beads with a diameter of 6µm, 8µm and 10µm and use the power spectrum analysis of the trapped particle displacements to characterize the trap strength.

  1. Energy of the 2p1h intruder state in $^{34}$Al

    CERN Multimedia

    The second 0$^{+}$ state in $^{34}$Si, of high importance for the understanding of the island of inversion at N=20, has been recently observed through the $\\beta$- decay of a predicted long-lived low-lying isomeric 1$^{+}$ state in $^{34}$Al. We intend to measure the unknown excitation energy of this isomer using the ISOLTRAP Penning-trap mass spectrometer. Since a recent experiment at ISOLDE (IS-530) showed that the full $\\beta$- strength in the decay of $^{34}$Mg goes through this 1$^{+}$ state in $^{34}$Al, we propose to perform a direct mass measurement of the daughter $^{34}$Al ions trapped after the decay of $^{34}$Mg. Mass measurements indicate that the 4$^{−}$ ground state in $^{34}$Al may be an excited state, the ground state being therefore the intruder 1$^{+}$ state. In another run, we propose to perform a remeasurement of the mass of the 4$^{−}$ ground state.

  2. Real-time measurement of plutonium in air by direct-inlet surface ionization mass spectrometry. Status report

    International Nuclear Information System (INIS)

    Stoffels, J.J.

    1980-04-01

    A new technique is being developed for monitoring low-level airborne plutonium on a real-time basis. The technique is based on surface ionization mass spectrometry of airborne particles. It will be capable of measuring plutonium concentrations below the maximum permissible concentration (MPC) level. A complete mass spectrometer was designed and constructed for this purpose. Major components which were developed and made operational for the instrument include an efficient inlet for directly sampling particles in air, a wide dynamic range ion detector and a minicomputer-based ion-burst measurement system. Calibration of the direct-inlet mass spectrometer (DIMS) was initiated to establish the instrument's response to plutonium dioxide as a function of concentration and particle size. This work revealed an important problem - bouncing of particles upon impact with the ionizing filament. Particle bounce results in a significant loss of measurement sensitivity. The feasibility of using an oven ionizer to overcome the particle bounce problem has been demonstrated. A rhenium oven ionizer was designed and constructed for the purpose of trapping particles which enter via the direct inlet. High-speed particles were trapped in the oven yielding a measurement sensitivity comparable to that for particles which are preloaded. Development of the Pu DIMS can now be completed by optimizing the oven design and calibrating the instrument's performance with UO 2 and CeO 2 particles as analogs to PuO 2 particles

  3. CRESU studies of electron attachment and Penning ionization at temperatures down to 48 K

    International Nuclear Information System (INIS)

    Le Garrec, J.L.; Mitchell, J.B.A.; Rowe, B.R.

    1996-01-01

    The object of the present report is to present results obtained for electron attachment and Penning ionization, obtained with the addition of a Langmuir probe to the measurement apparatus. Measurements of the rate coefficients for electron attachment and Penning ionization are performed using the standard techniques for the flow reactors. Rate coefficients for the Penning ionisation of argon, nitrogen molecule, oxygen molecule by helium metastable are presented. The results obtained concerning the attachment of electrons to SF 6 (non-dissociative), CCl 2 F 2 (producing Cl - ), and CF 3 Br as a function of temperature are presented. The differences observed, and the variation of the value of β below 100 K, provides evidence of the strong influence of the internal state (probably vibrational) of the CF 3 Br molecule on its dissociative attachment

  4. Experimental comparison of particle interaction measurement techniques using optical traps

    International Nuclear Information System (INIS)

    Koehler, Timothy P.; Grillet, Anne Mary; Brotherton, Christopher M.; Molecke, Ryan A.

    2008-01-01

    Optical tweezers has become a powerful and common tool for sensitive determination of electrostatic interactions between colloidal particles. Recently, two techniques, 'blinking' tweezers and direct force measurements, have become increasingly prevalent in investigations of inter-particle potentials. The 'blinking' tweezers method acquires physical statistics of particle trajectories to determine drift velocities, diffusion coefficients, and ultimately colloidal forces as a function of the center-center separation of two particles. Direct force measurements monitor the position of a particle relative to the center of an optical trap as the separation distance between two continuously trapped particles is gradually decreased. As the particles near each other, the displacement from the trap center for each particle increases proportional to the inter-particle force. Although commonly employed in the investigation of interactions of colloidal particles, there exists no direct comparison of these experimental methods in the literature. In this study, an experimental apparatus was developed capable of performing both methods and is used to quantify electrostatic potentials between particles in several particle/solvent systems. Comparisons are drawn between the experiments conducted using the two measurement techniques, theory, and existing literature. Forces are quantified on the femto-Newton scale and results agree well with literature values

  5. Fission yield measurements at IGISOL

    Science.gov (United States)

    Lantz, M.; Al-Adili, A.; Gorelov, D.; Jokinen, A.; Kolhinen, V. S.; Mattera, A.; Moore, I.; Penttilä, H.; Pomp, S.; Prokofiev, A. V.; Rakopoulos, V.; Rinta-Antila, S.; Simutkin, V.; Solders, A.

    2016-06-01

    The fission product yields are an important characteristic of the fission process. In fundamental physics, knowledge of the yield distributions is needed to better understand the fission process. For nuclear energy applications good knowledge of neutroninduced fission-product yields is important for the safe and efficient operation of nuclear power plants. With the Ion Guide Isotope Separator On-Line (IGISOL) technique, products of nuclear reactions are stopped in a buffer gas and then extracted and separated by mass. Thanks to the high resolving power of the JYFLTRAP Penning trap, at University of Jyväskylä, fission products can be isobarically separated, making it possible to measure relative independent fission yields. In some cases it is even possible to resolve isomeric states from the ground state, permitting measurements of isomeric yield ratios. So far the reactions U(p,f) and Th(p,f) have been studied using the IGISOL-JYFLTRAP facility. Recently, a neutron converter target has been developed utilizing the Be(p,xn) reaction. We here present the IGISOL-technique for fission yield measurements and some of the results from the measurements on proton induced fission. We also present the development of the neutron converter target, the characterization of the neutron field and the first tests with neutron-induced fission.

  6. Fission yield measurements at IGISOL

    Directory of Open Access Journals (Sweden)

    Lantz M.

    2016-01-01

    Full Text Available The fission product yields are an important characteristic of the fission process. In fundamental physics, knowledge of the yield distributions is needed to better understand the fission process. For nuclear energy applications good knowledge of neutroninduced fission-product yields is important for the safe and efficient operation of nuclear power plants. With the Ion Guide Isotope Separator On-Line (IGISOL technique, products of nuclear reactions are stopped in a buffer gas and then extracted and separated by mass. Thanks to the high resolving power of the JYFLTRAP Penning trap, at University of Jyväskylä, fission products can be isobarically separated, making it possible to measure relative independent fission yields. In some cases it is even possible to resolve isomeric states from the ground state, permitting measurements of isomeric yield ratios. So far the reactions U(p,f and Th(p,f have been studied using the IGISOL-JYFLTRAP facility. Recently, a neutron converter target has been developed utilizing the Be(p,xn reaction. We here present the IGISOL-technique for fission yield measurements and some of the results from the measurements on proton induced fission. We also present the development of the neutron converter target, the characterization of the neutron field and the first tests with neutron-induced fission.

  7. Quantum limits to center-of-mass measurements

    International Nuclear Information System (INIS)

    Vaughan, Timothy; Drummond, Peter; Leuchs, Gerd

    2007-01-01

    We discuss the issue of measuring the mean position (center of mass) of a group of bosonic or fermionic quantum particles, including particle number fluctuations. We introduce a standard quantum limit for these measurements at ultralow temperatures, and discuss this limit in the context of both photons and ultracold atoms. In the case of non-interacting harmonically trapped fermions, we present evidence that the Pauli exclusion principle has a strongly beneficial effect, giving rise to a 1/N scaling in the position standard deviation--as opposed to a 1/√(N) scaling for bosons. The difference between the actual mean-position fluctuation and this limit is evidence for quantum wave-packet spreading in the center of mass. This macroscopic quantum effect cannot be readily observed for noninteracting particles, due to classical pulse broadening. For this reason, we also study the evolution of photonic and matter-wave solitons, where classical dispersion is suppressed. In the photonic case, we show that the intrinsic quantum diffusion of the mean position can contribute significantly to uncertainties in soliton pulse arrival times. We also discuss ways in which the relatively long lifetimes of attractive bosons in matter-wave solitons may be used to demonstrate quantum interference between massive objects composed of thousands of particles

  8. Mass Spectrometric Analysis of Eight Common Chemical Explosives Using Ion Trap Mass Spectrometer

    Energy Technology Data Exchange (ETDEWEB)

    Park, Sehwan; Lee, Jihyeon; KIm, Jeongkwon [Chungnam National Univ., Daejeon (Korea, Republic of); Cho, Soo Gyeong; Goh, Eun Mee [Agency for Defense Development, Daejeon (Korea, Republic of); Lee, Sungman; Koh, Sungsuk [Sensor Tech Inc., Seoul (Korea, Republic of)

    2013-12-15

    Eight representative explosives (ammonium perchlorate (AP), ammonium nitrate (AN), trinitrotoluene (TNT), 2,4-dinitrotoluene (DNT), cyclonite (RDX), cyclotetramethylenetetranitramine (HMX), pentaerythritol tetranitrate (PETN), and hexanitrostilbene (HNS)) were comprehensively analyzed with an ion trap mass spectrometer in negative ion mode using direct infusion electrospray ionization. MS/MS experiments were performed to generate fragment ions from the major parent ion of each explosive. Explosives in salt forms such as AP or AN provided cluster parent ions with their own anions. Explosives with an aromatic ring were observed as either [M.H]{sup -} for TNT and DNT or [M]{sup ·-}. for HNS, while explosives without an aromatic ring such as RDX, HMX, and PETN were detected as an adduct ion with a formate anion, i. e., [M+HCOO]{sup -}. These findings provide a guideline for the rapid and accurate detection of explosives once portable MS instruments become more readily available.

  9. Mass Spectrometric Analysis of Eight Common Chemical Explosives Using Ion Trap Mass Spectrometer

    International Nuclear Information System (INIS)

    Park, Sehwan; Lee, Jihyeon; KIm, Jeongkwon; Cho, Soo Gyeong; Goh, Eun Mee; Lee, Sungman; Koh, Sungsuk

    2013-01-01

    Eight representative explosives (ammonium perchlorate (AP), ammonium nitrate (AN), trinitrotoluene (TNT), 2,4-dinitrotoluene (DNT), cyclonite (RDX), cyclotetramethylenetetranitramine (HMX), pentaerythritol tetranitrate (PETN), and hexanitrostilbene (HNS)) were comprehensively analyzed with an ion trap mass spectrometer in negative ion mode using direct infusion electrospray ionization. MS/MS experiments were performed to generate fragment ions from the major parent ion of each explosive. Explosives in salt forms such as AP or AN provided cluster parent ions with their own anions. Explosives with an aromatic ring were observed as either [M.H] - for TNT and DNT or [M] ·- . for HNS, while explosives without an aromatic ring such as RDX, HMX, and PETN were detected as an adduct ion with a formate anion, i. e., [M+HCOO] - . These findings provide a guideline for the rapid and accurate detection of explosives once portable MS instruments become more readily available

  10. Deuterium trapping in tungsten

    Science.gov (United States)

    Poon, Michael

    Tungsten is one of the primary material candidates being investigated for use in the first-wall of a magnetic confinement fusion reactor. An ion accelerator was used to simulate the type of ion interaction that may occur at a plasma-facing material. Thermal desorption spectroscopy (TDS) was the primary tool used to analyze the effects of the irradiation. Secondary ion mass spectroscopy (SIMS) was used to determine the distribution of trapped D in the tungsten specimen. The tritium migration analysis program (TMAP) was used to simulate thermal desorption profiles from the D depth distributions. Fitting of the simulated thermal desorption profiles with the measured TDS results provided values of the D trap energies. Deuterium trapping in single crystal tungsten was studied as a function of the incident ion fluence, ion flux, irradiation temperature, irradiation history, and surface impurity levels during irradiation. The results show that deuterium was trapped at vacancies and voids. Two deuterium atoms could be trapped at a tungsten vacancy, with trapping energies of 1.4 eV and 1.2 eV for the first and second D atoms, respectively. In a tungsten void, D is trapped as atoms adsorbed on the inner walls of the void with a trap energy of 2.1 eV, or as D2 molecules inside the void with a trap energy of 1.2 eV. Deuterium trapping in polycrystalline tungsten was also studied as a function of the incident fluence, irradiation temperature, and irradiation history. Deuterium trapping in polycrystalline tungsten also occurs primarily at vacancies and voids with the same trap energies as in single crystal tungsten; however, the presence of grain boundaries promotes the formation of large surface blisters with high fluence irradiations at 500 K. In general, D trapping is greater in polycrystalline tungsten than in single crystal tungsten. To simulate mixed materials comprising of carbon (C) and tungsten, tungsten specimens were pre-irradiated with carbon ions prior to D

  11. Deuterium trapping in tungsten

    International Nuclear Information System (INIS)

    Poon, M.

    2004-01-01

    Tungsten is one of the primary material candidates being investigated for use in the first-wall of a magnetic confinement fusion reactor. An ion accelerator was used to simulate the type of ion interaction that may occur at a plasma-facing material. Thermal desorption spectroscopy (TDS) was the primary tool used to analyze the effects of the irradiation Secondary ion mass spectroscopy (SIMS) was used to determine the distribution of trapped D in the tungsten specimen. The tritium migration analysis program (TMAP) was used to simulate thermal desorption profiles from the D depth distributions. Fitting of the simulated thermal desorption profiles with the measured TDS results provided values of the D trap energies. . Deuterium trapping in single crystal tungsten was studied as a function of the incident ion fluence, ion flux, irradiation temperature, irradiation history, and surface impurity levels during irradiation The results show that deuterium was trapped at vacancies and voids. Two deuterium atoms could be trapped at a tungsten vacancy, with trapping energies of 1.4 eV and 1.2 eV for the first and second D atoms, respectively. In a tungsten void, D is trapped as atoms adsorbed on the inner walls of the void with a trap energy of 2.1 eV, or as D 2 molecules inside the void with a trap energy of 1.2 eV. . Deuterium trapping in polycrystalline tungsten was also studied as a function of the incident fluence, irradiation temperature, and irradiation history. Deuterium trapping in polycrystalline tungsten also occurs primarily at vacancies and voids with the same trap energies as in single crystal tungsten; however, the presence of grain boundaries promotes the formation of large surface blisters with high fluence irradiations at 500 K. In general, D trapping is greater in polycrystalline tungsten than in single crystal tungsten. To simulate mixed materials comprising of carbon (C) and tungsten, tungsten specimens were pre-irradiated with carbon ions prior to D

  12. Deuterium trapping in tungsten

    Energy Technology Data Exchange (ETDEWEB)

    Poon, M

    2004-07-01

    Tungsten is one of the primary material candidates being investigated for use in the first-wall of a magnetic confinement fusion reactor. An ion accelerator was used to simulate the type of ion interaction that may occur at a plasma-facing material. Thermal desorption spectroscopy (TDS) was the primary tool used to analyze the effects of the irradiation Secondary ion mass spectroscopy (SIMS) was used to determine the distribution of trapped D in the tungsten specimen. The tritium migration analysis program (TMAP) was used to simulate thermal desorption profiles from the D depth distributions. Fitting of the simulated thermal desorption profiles with the measured TDS results provided values of the D trap energies. . Deuterium trapping in single crystal tungsten was studied as a function of the incident ion fluence, ion flux, irradiation temperature, irradiation history, and surface impurity levels during irradiation The results show that deuterium was trapped at vacancies and voids. Two deuterium atoms could be trapped at a tungsten vacancy, with trapping energies of 1.4 eV and 1.2 eV for the first and second D atoms, respectively. In a tungsten void, D is trapped as atoms adsorbed on the inner walls of the void with a trap energy of 2.1 eV, or as D{sub 2} molecules inside the void with a trap energy of 1.2 eV. . Deuterium trapping in polycrystalline tungsten was also studied as a function of the incident fluence, irradiation temperature, and irradiation history. Deuterium trapping in polycrystalline tungsten also occurs primarily at vacancies and voids with the same trap energies as in single crystal tungsten; however, the presence of grain boundaries promotes the formation of large surface blisters with high fluence irradiations at 500 K. In general, D trapping is greater in polycrystalline tungsten than in single crystal tungsten. To simulate mixed materials comprising of carbon (C) and tungsten, tungsten specimens were pre-irradiated with carbon ions prior to D

  13. Quantification of Tissue Trauma following Insulin Pen Needle Insertions in Skin

    DEFF Research Database (Denmark)

    Jensen, Casper Bo; Larsen, Rasmus; Vestergaard, Jacob Schack

    Objective: Within the field of pen needle development, most research on needle design revolves around mechanical tensile testing and patient statements. Only little has been published on the actual biological skin response to needle insertions. The objective of this study was to develop a computa......Objective: Within the field of pen needle development, most research on needle design revolves around mechanical tensile testing and patient statements. Only little has been published on the actual biological skin response to needle insertions. The objective of this study was to develop...... a computational method to quantify tissue trauma based on skin bleeding and immune response. Method: Two common sized pen needles of 28G (0.36mm) and 32G (0.23mm) were inserted into skin of sedated LYD pigs prior to termination. Four pigs were included and a total of 32 randomized needle insertions were conducted...... diameter. Conclusion: A computational and quantitative method has been developed to assess tissue trauma following insulin pen needle insertions. Application of the method is tested by conduction of a needle diameter study. The obtained quantitative measures of tissue trauma correlate positively to needle...

  14. De innemende verteller Louwrens Penning

    OpenAIRE

    Ester, Hans

    2012-01-01

    Dutch author Louwrens Penning (1854 – 1927) indisputably contributed more than any other novelist in the Netherlands to the high degree of solidarity with the Boers before, during and after the Anglo- Boer War 1899 – 1902. Penning, being a believer in the Calvinist tradition, had a profound trust in God’s guidance of history. He identified the war of the Boer soldiers against the British imperialists with the rebellion of the Dutch out of their true religious convictions against t...

  15. Dual-stage trapped-flux magnet cryostat for measurements at high magnetic fields

    Science.gov (United States)

    Islam, Zahirul; Das, Ritesh K.; Weinstein, Roy

    2015-04-14

    A method and a dual-stage trapped-flux magnet cryostat apparatus are provided for implementing enhanced measurements at high magnetic fields. The dual-stage trapped-flux magnet cryostat system includes a trapped-flux magnet (TFM). A sample, for example, a single crystal, is adjustably positioned proximate to the surface of the TFM, using a translation stage such that the distance between the sample and the surface is selectively adjusted. A cryostat is provided with a first separate thermal stage provided for cooling the TFM and with a second separate thermal stage provided for cooling sample.

  16. Particle-in-cell simulations of anomalous transport in a Penning discharge

    Science.gov (United States)

    Carlsson, Johan; Kaganovich, Igor; Powis, Andrew; Raitses, Yevgeny; Romadanov, Ivan; Smolyakov, Andrei

    2018-06-01

    Electrostatic particle-in-cell simulations of a Penning discharge are performed in order to investigate azimuthally asymmetric, spoke-like structures previously observed in experiments. Two-dimensional simulations show that for Penning-discharge conditions, a persistent nonlinear spoke-like structure forms readily and rotates in the direction of E × B and electron diamagnetic drifts. The azimuthal velocity is within about a factor of 2 of the ion acoustic speed. The spoke frequency follows the experimentally observed scaling with ion mass, which indicates the importance of ion inertia in spoke formation. The spoke provides enhanced (anomalous) radial electron transport, and the effective cross-field conductivity is several times larger than the classical (collisional) value. The level of anomalous current obtained in the simulations is in good agreement with the experimental data. The rotating spoke channels most of the radial current, observable by an edge probe as short pulses.

  17. 9 CFR 313.1 - Livestock pens, driveways and ramps.

    Science.gov (United States)

    2010-01-01

    ... 9 Animals and Animal Products 2 2010-01-01 2010-01-01 false Livestock pens, driveways and ramps... INSPECTION AND CERTIFICATION HUMANE SLAUGHTER OF LIVESTOCK § 313.1 Livestock pens, driveways and ramps. (a) Livestock pens, driveways and ramps shall be maintained in good repair. They shall be free from sharp or...

  18. Preliminary study for the National Energy Plan (PEN) uses the Community market as a reference base. El ante-proyecto del Plan Energetico Nacional (PEN) toma referencia basica del mercado comunitario

    Energy Technology Data Exchange (ETDEWEB)

    1991-11-01

    The National Energy Plan (PEN) for the period 1991 to 2000 lays down basic guidelines for a Spanish energy policy. This includes a wide range of economic measures. The PEN is divided into five main sections with two appendices. The sections are: the international situation; energy demand; energy supply; energy and the environment; and R D policy. The appendices are: Energy-saving and energy-efficiency plan; and General plan for radioactive waste. The PEN provides for 4-year research programmes which aim to reduce the environmental impact of energy production and use. General demand for energy during this period will increase by2.4% and investment in power installations and in the gas sector will be some 1.5 thousand million pesetas. 4 figs., 3 tabs.

  19. Comprehensive lipidomic analysis of human plasma using multidimensional liquid- and gas-phase separations: Two-dimensional liquid chromatography-mass spectrometry vs. liquid chromatography-trapped-ion-mobility-mass spectrometry.

    Science.gov (United States)

    Baglai, Anna; Gargano, Andrea F G; Jordens, Jan; Mengerink, Ynze; Honing, Maarten; van der Wal, Sjoerd; Schoenmakers, Peter J

    2017-12-29

    Recent advancements in separation science have resulted in the commercialization of multidimensional separation systems that provide higher peak capacities and, hence, enable a more-detailed characterization of complex mixtures. In particular, two powerful analytical tools are increasingly used by analytical scientists, namely online comprehensive two-dimensional liquid chromatography (LC×LC, having a second-dimension separation in the liquid phase) and liquid chromatography-ion mobility-spectrometry (LC-IMS, second dimension separation in the gas phase). The goal of the current study was a general assessment of the liquid-chromatography-trapped-ion-mobility-mass spectrometry (LC-TIMS-MS) and comprehensive two-dimensional liquid chromatography-mass spectrometry (LC×LC-MS) platforms for untargeted lipid mapping in human plasma. For the first time trapped-ion-mobility spectrometry (TIMS) was employed for the separation of the major lipid classes and ion-mobility-derived collision-cross-section values were determined for a number of lipid standards. The general effects of a number of influencing parameters have been inspected and possible directions for improvements are discussed. We aimed to provide a general indication and practical guidelines for the analyst to choose an efficient multidimensional separation platform according to the particular requirements of the application. Analysis time, orthogonality, peak capacity, and an indicative measure for the resolving power are discussed as main characteristics for multidimensional separation systems. Copyright © 2017 Elsevier B.V. All rights reserved.

  20. Application of a trap-free two-dimensional liquid chromatography combined with ion trap/time-of-flight mass spectrometry for separation and characterization of impurities and isomers in cefpiramide.

    Science.gov (United States)

    Wang, Jian; Xu, Yu; Wen, Chunmei; Wang, Zhijian

    2017-11-01

    High-resolution mass spectrometry had been routinely used for structure identification of impurity. However, all LC-MS methods were based on a volatile mobile phase, and a non-volatile system is used in the official analytical method of United States Pharmacopoeia for cefpiramide which limited the use of mass spectrometry for structure characterization of the impurities. Here we presented the utilization of a trap-free two-dimensional liquid chromatography coupled to high resolution ion trap/time-of-flight mass spectrometry (2D LC-IT-TOF MS) with positive and negative modes of electrospray ionization for characterization of eight impurities in cefpiramide. Trap-free two-dimensional liquid chromatography and online desalting technique made it possible to characterize the impurity in cefpiramide in the condition of official standard, and the TIC chromatogram of LC-MS was in conformity with the LC chromatogram of the official analytical method in the peak sequence of impurities, which could further improve the method of official monographs in pharmacopoeias. Each peak separated by the non-volatile mobile phase was trapped by a 20 μL quantitative loop then transferred into a system with a volatile mobile phase connected to a MS detector. In the first dimension, the column was Kromasil C 8 analytical column (250 mm × 4.6 mm, 5 μm) with a non-volatile salt mobile phase at the flow rate of 0.8 mL min -1 . In the second dimension, the column was Shimadzu Shim-pack GISS C 18 (50 mm × 2.1 mm, 1.9 μm) with a volatile salt mobile phase at the flow rate of 0.3 mL min -1 . Through the multiple heart-cutting 2D-LC approach and online desalting technique, the problem of incompatibility between non-volatile salt mobile phase and mass spectrometry was solved completely. The fragmentation behavior of cefpiramide and its eight impurities were studied. The structures of eight impurities in cefpiramide drug substance were deduced based on the HPLC-MS n data, in

  1. Microfabricated linear Paul-Straubel ion trap

    Science.gov (United States)

    Mangan, Michael A [Albuquerque, NM; Blain, Matthew G [Albuquerque, NM; Tigges, Chris P [Albuquerque, NM; Linker, Kevin L [Albuquerque, NM

    2011-04-19

    An array of microfabricated linear Paul-Straubel ion traps can be used for mass spectrometric applications. Each ion trap comprises two parallel inner RF electrodes and two parallel outer DC control electrodes symmetric about a central trap axis and suspended over an opening in a substrate. Neighboring ion traps in the array can share a common outer DC control electrode. The ions confined transversely by an RF quadrupole electric field potential well on the ion trap axis. The array can trap a wide array of ions.

  2. Effects of oxide traps, interface traps, and ''border traps'' on metal-oxide-semiconductor devices

    International Nuclear Information System (INIS)

    Fleetwood, D.M.; Winokur, P.S.; Reber, R.A. Jr.; Meisenheimer, T.L.; Schwank, J.R.; Shaneyfelt, M.R.; Riewe, L.C.

    1993-01-01

    We have identified several features of the 1/f noise and radiation response of metal-oxide-semiconductor (MOS) devices that are difficult to explain with standard defect models. To address this issue, and in response to ambiguities in the literature, we have developed a revised nomenclature for defects in MOS devices that clearly distinguishes the language used to describe the physical location of defects from that used to describe their electrical response. In this nomenclature, ''oxide traps'' are simply defects in the SiO 2 layer of the MOS structure, and ''interface traps'' are defects at the Si/SiO 2 interface. Nothing is presumed about how either type of defect communicates with the underlying Si. Electrically, ''fixed states'' are defined as trap levels that do not communicate with the Si on the time scale of the measurements, but ''switching states'' can exchange charge with the Si. Fixed states presumably are oxide traps in most types of measurements, but switching states can either be interface traps or near-interfacial oxide traps that can communicate with the Si, i.e., ''border traps'' [D. M. Fleetwood, IEEE Trans. Nucl. Sci. NS-39, 269 (1992)]. The effective density of border traps depends on the time scale and bias conditions of the measurements. We show the revised nomenclature can provide focus to discussions of the buildup and annealing of radiation-induced charge in non-radiation-hardened MOS transistors, and to changes in the 1/f noise of MOS devices through irradiation and elevated-temperature annealing

  3. Evaluation of drop versus trickle-feeding systems for crated or group-penned gestating sows.

    Science.gov (United States)

    Hulbert, L E; McGlone, J J

    2006-04-01

    A total of 160 gilts were used to evaluate the effects of pen vs. crated housing systems and drop- vs. trickle-fed feeding systems on sow productivity, occurrence of lesions during farrowing and weaning, immune measures, and behavioral responses during 2 consecutive gestation periods. Of the 160 eligible gilts, 117 farrowed in parity 1, and of those, 72 farrowed in parity 2. The gilts were randomly assigned to represent 1 of 4 factorially arranged treatment groups: pen drop-fed, crate drop-fed, pen trickle-fed, or crate trickle-fed. Replicate blocks were used for each parity with 5 sows per block initially in each treatment. At weaning, sows housed in pens had greater (P trickle-feeding system. Lesions scores and all other productivity measures did not differ among treatments. An interaction was observed for percentage of neutrophil phagocytosis (P trickle-fed sows, but in crates, drop-fed sows had a tendency for lower phagocytosis than trickle-fed sows. All other immune measures were not different among treatments. The occurrence of oral-nasal-facial (ONF) behaviors (chewing, rooting, and rubbing) and active behaviors increased, and lying behavior decreased (P trickle-feeding systems. None of the environments evaluated were associated with significant physiological stress responses among the sows. Thus, sows were able to adapt within each environment through behavioral mechanisms without the need to invoke major physiological adjustments.

  4. Precision polarization measurements of atoms in a far-off-resonance optical dipole trap

    International Nuclear Information System (INIS)

    Fang, F.; Vieira, D. J.; Zhao, X.

    2011-01-01

    Precision measurement of atomic and nuclear polarization is an essential step for beta-asymmetry measurement of radioactive atoms. In this paper, we report the polarization measurement of Rb atoms in an yttrium-aluminum-garnet (YAG) far-off-resonance optical dipole trap. We have prepared a cold cloud of polarized Rb atoms in the YAG dipole trap by optical pumping and achieved an initial nuclear polarization of up to 97.2(5)%. The initial atom distribution in different Zeeman levels is measured by using a combination of microwave excitation, laser pushing, and atomic retrap techniques. The nuclear-spin polarization is further purified to 99.2(2)% in 10 s and maintained above 99% because the two-body collision loss rate between atoms in mixed spin states is greater than the one-body trap loss rate. Systematic effects on the nuclear polarization, including the off-resonance Raman scattering, magnetic field gradient, and background gas collisions, are discussed.

  5. Pitch angle distribution of trapped energetic protons and helium isotope nuclei measured along the Resurs-01 No. 4 LEO satellite

    Directory of Open Access Journals (Sweden)

    A. Leonov

    2005-11-01

    Full Text Available The NINA detector on board the Resurs-01 No. 4 satellite (835 km, 98° inclination is equipped with particle trackers based on silicon strip detectors. From the energy deposited in each of its silicon layers the mass, the momentum direction and energy of incident particles have been determined. The resolutions in mass and energy allow identification of H and He isotopes over the 10-50 MeV/n energy range. The angular resolution is about 2.5°. We present the direct measurements of proton and helium isotopes pitch angle distributions derived from Resurs-01 No.4/NINA observations and their variations as functions of (B, L coordinates and energy. The measurements of trapped helium isotopes spectrum are also presented.

  6. Measurement of elastic light scattering from two optically trapped microspheres and red blood cells in a transparent medium.

    Science.gov (United States)

    Kinnunen, Matti; Kauppila, Antti; Karmenyan, Artashes; Myllylä, Risto

    2011-09-15

    Optical tweezers can be used to manipulate small objects and cells. A trap can be used to fix the position of a particle during light scattering measurements. The places of two separately trapped particles can also be changed. In this Letter we present elastic light scattering measurements as a function of scattering angle when two trapped spheres are illuminated with a He-Ne laser. This setup is suitable for trapping noncharged homogeneous spheres. We also demonstrate measurement of light scattering patterns from two separately trapped red blood cells. Two different illumination schemes are used for both samples.

  7. Ballpoint pen inks: characterization by positive and negative ion-electrospray ionization mass spectrometry for the forensic examination of writing inks.

    Science.gov (United States)

    Ng, Lay-Keow; Lafontaine, Pierre; Brazeau, Luc

    2002-11-01

    A method based on profiling of dye components by electrospray ionization mass spectrometry (ESI/MS) is described for the characterization of ballpoint pen inks. The method involves benzyl alcohol (30 microL) extraction of ink from paper. The extracts of ink lines 1 and 5 mm in length are used for direct ESI/MS analysis in positive and negative modes, respectively. The instrumental analysis takes 3 min. Basic and acid dyes in the inks are detected in the positive and negative modes, respectively, with each dye yielding one or two characteristic ion peaks. The mass spectrum, which is mainly a compositional signature of the dyes in the ink, was not affected by the type of paper from which the ink was extracted, or by natural ageing of the ink on document in the absence of light. However, exposure to fluorescent illumination caused dealkylation of polyalkylated basic dyes and resulted in changes in the homologous distribution of the dyes. In this study, a total of 44 blue inks, 23 black inks, and 10 red inks have been analyzed, and the mass spectra were used to establish a searchable library. ESI/MS analysis provides a simple and fast way to compare ink specimens and in combination with on-line library search permits rapid screening of inks for forensic document investigations.

  8. A Dual Source Ion Trap Mass Spectrometer for the Mars Organic Molecule Analyzer of ExoMars 2018

    Science.gov (United States)

    Brickerhoff, William B.; vanAmerom, F. H. W.; Danell, R. M.; Arevalo, R.; Atanassova, M.; Hovmand, L.; Mahaffy, P. R.; Cotter, R. J.

    2011-01-01

    We present details on the objectives, requirements, design and operational approach of the core mass spectrometer of the Mars Organic Molecule Analyzer (MOMA) investigation on the 2018 ExoMars mission. The MOMA mass spectrometer enables the investigation to fulfill its objective of analyzing the chemical composition of organic compounds in solid samples obtained from the near surface of Mars. Two methods of ionization are realized, associated with different modes of MOMA operation, in a single compact ion trap mass spectrometer. The stringent mass and power constraints of the mission have led to features such as low voltage and low frequency RF operation [1] and pulse counting detection.

  9. Synergy of decay spectroscopy and mass spectrometry for the study of exotic nuclides

    Energy Technology Data Exchange (ETDEWEB)

    Stanja, Juliane

    2013-04-12

    With only two ingredients, atomic nuclei exhibit a rich structure depending on the ordering of the different proton- and neutron-occupied states. This ordering can give rise to excited states with exceptionally long half-lives, also known as isomers, especially near shell closures. On-line mass spectrometry can often be compromised by the existence of such states that may even be produced in higher proportion than the ground state. This thesis presents the first results obtained from a nuclear spectroscopy setup coupled with the high-resolution Penning-trap mass spectrometer ISOLTRAP, at CERN's radioactive ion beam facility ISOLDE. The isomerism in the neutron-deficient thallium isotopes was investigated. The data on {sup 184,190,193-195}Tl allow an improvement of existing mass values as well as a mass-spin-state assignment in {sup 190,193,194}Tl. Due to the presence of the ground and isomeric state for {sup 194}Tl the excitation energy of the latter was determined for the first time experimentally. Systematic trends in the vicinity of the Z = 82 shell closure have been discussed.

  10. Chlorine by-products in sea water at the Penly nuclear power plant. Measurement survey in May 1993; Residus de chloration en mer a Penly. Campagne de mesures de Mai 1993

    Energy Technology Data Exchange (ETDEWEB)

    Khalanski, M.; Delesmont, R.

    1994-09-01

    The objective of the measurement survey conducted at the Penly nuclear power plant on May 27 and 28, 1993, was to determine the distribution of residual oxidants and volatile organo-halogenated compounds (THM) concentrations in the discharge plume when both units of the plants are carrying out chlorination. The data collected provide a mapping of the chemical types analyzed and will serve in calibration of a numerical model to simulate the evolution of these compounds in the discharge plume. During the two days of measurements, quantitative analyses were performed on samples taken by helicopter, once at high tide and twice at low tide with mean tidal coefficients. The chlorine injection level ranged from 0.84 to 0.92 mg/l (ppm) in unit 1 and from 0.64 to 0.70 mg/l in unit 2. Residual oxidants were measured as Total Chlorine equivalents using the colorimetric DPD method. Bromoform accounted for 97.8 % of the THM generated by chlorination. Three minutes after injection of hypochlorite, in the discharge basin, bromoform reached 60 % of its maximum concentration (29.23 {mu}g/l). The maximum reaction yield of bromoform formation is 2,9 %. Three zones were defined according to their proximity to releases. In each zone, given the lake of precision in measurements, the concentration of residual oxidants found did not reach significant levels ({<=}0.03 mg/l). The bromoform concentration, on the contrary, reached measurable levels in each of the samples. Its distribution differs significantly from one zone to another: -release zone : 1.66{+-}0.40{mu}g/l -nearby zone: 0.44{+-}0.13{mu}g/l - distant zone : 0.26{+-}0.10{mu}g/l. Our analysis, which indicates a background level of the order of 0.1 {mu}g/l for the entire studied area, raises the question of possible other sources of bromoform, independent of discharge from Penly. (authors). 15 refs., 11 figs., 5 tabs., 4 annexes.

  11. Effect of the trapped mass and its composition on the heat transfer in the compression cycle of a reciprocating engine

    International Nuclear Information System (INIS)

    Armas, Octavio; Rodriguez, Jose; Payri, Francisco; Martin, Jaime; Agudelo, John R.

    2005-01-01

    The use of the polytropic coefficient calculation during the compression process in the thermodynamic cycle of a reciprocating internal combustion engine is an interesting tool to minimize errors in the synchronization of pressure and volume signals, and to determine heat flux transferred to the cylinder walls. The accuracy of this calculation depends on the instantaneous values for pressure, volume, trapped mass and its composition, as well as on their variations. In this work the effect of the errors in blow-by, trapped mass and its composition have been studied in detail, specially the effect of errors in the composition estimation, owing to the use of exhaust gas recirculation in typical diesel engines

  12. Uncertainty quantification for nuclear density functional theory and information content of new measurements

    Energy Technology Data Exchange (ETDEWEB)

    McDonnell, J. D. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Schunck, N. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Higdon, D. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Sarich, J. [Argonne National Lab. (ANL), Argonne, IL (United States); Wild, S. M. [Argonne National Lab. (ANL), Argonne, IL (United States); Nazarewicz, W. [Michigan State Univ., East Lansing, MI (United States); Oak Ridge National Lab., Oak Ridge, TN (United States); Univ. of Warsaw, Warsaw (Poland)

    2015-03-24

    Statistical tools of uncertainty quantification can be used to assess the information content of measured observables with respect to present-day theoretical models, to estimate model errors and thereby improve predictive capability, to extrapolate beyond the regions reached by experiment, and to provide meaningful input to applications and planned measurements. To showcase new opportunities offered by such tools, we make a rigorous analysis of theoretical statistical uncertainties in nuclear density functional theory using Bayesian inference methods. By considering the recent mass measurements from the Canadian Penning Trap at Argonne National Laboratory, we demonstrate how the Bayesian analysis and a direct least-squares optimization, combined with high-performance computing, can be used to assess the information content of the new data with respect to a model based on the Skyrme energy density functional approach. Employing the posterior probability distribution computed with a Gaussian process emulator, we apply the Bayesian framework to propagate theoretical statistical uncertainties in predictions of nuclear masses, two-neutron dripline, and fission barriers. Overall, we find that the new mass measurements do not impose a constraint that is strong enough to lead to significant changes in the model parameters. As a result, the example discussed in this study sets the stage for quantifying and maximizing the impact of new measurements with respect to current modeling and guiding future experimental efforts, thus enhancing the experiment-theory cycle in the scientific method.

  13. The influence of central corneal thickness and age on intraocular pressure measured by pneumotonometry, non-contact tonometry, the Tono-Pen XL, and Goldmann applanation tonometry

    OpenAIRE

    Tonnu, P-A; Ho, T; Newson, T; El Sheikh, A; Sharma, K; White, E; Bunce, C; Garway-Heath, D

    2005-01-01

    Aims: To evaluate the influence of central corneal thickness (CCT) on intraocular pressure (IOP) measurements made with the Goldmann applanation tonometer (GAT), Tono-Pen XL, ocular blood flow tonograph (OBF), and Canon TX-10 non-contact tonometer (NCT).

  14. Administration technique and storage of disposable insulin pens reported by patients with diabetes.

    Science.gov (United States)

    Mitchell, Virginia D; Porter, Kyle; Beatty, Stuart J

    2012-01-01

    The purpose of the study was to evaluate insulin injection technique and storage of insulin pens as reported by patients with diabetes and to compare correct pen use to initial education on injection technique, hemoglobin A1C, duration of insulin therapy, and duration of insulin pen. Cross-sectional questionnaire orally administered to patients at a university-affiliated primary care practice. Subjects were patients with diabetes who were 18 years or older and prescribed a disposable insulin pen for at least 4 weeks. A correct usage score was calculated for each patient based on manufacturer recommendations for disposable insulin pen use. Associations were made between the correct usage score and certainty in technique, initial education, years of insulin therapy, duration of pen use, and hemoglobin A1C. Sixty-seven patients completed the questionnaire, reporting total use of 94 insulin pens. The 3 components most often neglected by patients were priming pen needle, holding for specific count time before withdrawal of pen needle from skin, and storing an in-use pen. For three-fourths of the insulin pens being used, users did not follow the manufacturer's instructions for proper administration and storage of insulin pens. Correct usage scores were significantly higher if initial education on insulin pens was performed by a pharmacist or nurse. The majority of patients may be ignoring or unaware of key components for consistent insulin dosing using disposable insulin pens; therefore, initial education and reeducation on correct use of disposable insulin pens by health care professionals are needed.

  15. Chlorine by-products in sea water at the Penly nuclear power plant. Measurement survey in May 1993

    International Nuclear Information System (INIS)

    Khalanski, M.; Delesmont, R.

    1994-09-01

    The objective of the measurement survey conducted at the Penly nuclear power plant on May 27 and 28, 1993, was to determine the distribution of residual oxidants and volatile organo-halogenated compounds (THM) concentrations in the discharge plume when both units of the plants are carrying out chlorination. The data collected provide a mapping of the chemical types analyzed and will serve in calibration of a numerical model to simulate the evolution of these compounds in the discharge plume. During the two days of measurements, quantitative analyses were performed on samples taken by helicopter, once at high tide and twice at low tide with mean tidal coefficients. The chlorine injection level ranged from 0.84 to 0.92 mg/l (ppm) in unit 1 and from 0.64 to 0.70 mg/l in unit 2. Residual oxidants were measured as Total Chlorine equivalents using the colorimetric DPD method. Bromoform accounted for 97.8 % of the THM generated by chlorination. Three minutes after injection of hypochlorite, in the discharge basin, bromoform reached 60 % of its maximum concentration (29.23 μg/l). The maximum reaction yield of bromoform formation is 2,9 %. Three zones were defined according to their proximity to releases. In each zone, given the lake of precision in measurements, the concentration of residual oxidants found did not reach significant levels (≤0.03 mg/l). The bromoform concentration, on the contrary, reached measurable levels in each of the samples. Its distribution differs significantly from one zone to another: -release zone : 1.66±0.40μg/l -nearby zone: 0.44±0.13μg/l - distant zone : 0.26±0.10μg/l. Our analysis, which indicates a background level of the order of 0.1 μg/l for the entire studied area, raises the question of possible other sources of bromoform, independent of discharge from Penly. (authors). 15 refs., 11 figs., 5 tabs., 4 annexes

  16. Pen-and-Paper User Interfaces

    CERN Document Server

    Steimle, Jurgen

    2012-01-01

    Even at the beginning of the 21st century, we are far from becoming paperless. Pen and paper is still the only truly ubiquitous information processing technology. Pen-and-paper user interfaces bridge the gap between paper and the digital world. Rather than replacing paper with electronic media, they seamlessly integrate both worlds in a hybrid user interface. Classical paper documents become interactive. This opens up a huge field of novel computer applications at our workplaces and in our homes. This book provides readers with a broad and extensive overview of the field, so as to provide a fu

  17. Using a Computer Module to Teach Use of the EpiPen®

    Directory of Open Access Journals (Sweden)

    Amandeep Singh Rai

    2011-11-01

    Full Text Available Background: The medical literature suggests that patients and physicians are deficient in their ability to use a self-injectable epinephrine device (EpiPen® for management of anaphylaxis. This study aims to determine whether a computer module is an effective tool for the instruction of a technical skill to medical trainees. Methods: We conducted a two group comparison study of 35 Post-Graduate Year 1 and 2 Family Medicine residents. Participants were instructed on use of the EpiPen® using either a written module or a computer module. Participants were evaluated on use of the EpiPen® using standardized objective outcome measures by a blinded assessor. Assessments took place prior to and following instruction, using the assigned learning modality. Results: There were 34 participants who completed the study. Both groups demonstrated significant improvement in demonstrating use of the EpiPen® following training (p <0.001 for both. A significant post-training difference favouring the computer module learners over the written module learners was observed (p = 0.035. However, only 53% and 18% of candidates (computer module and written module, respectively were able to correctly perform all of the checklist steps. Conclusion: While our findings suggest computer modules represent an effective modality for teaching use of the EpiPen® to medical trainees, the low number of candidates who were able to perform all the checklist items regardless of modality needs to be addressed.

  18. Laser Cooling and Trapping of Neutral Strontium for Spectroscopic Measurements of Casimir-Polder Potentials

    Science.gov (United States)

    Cook, Eryn C.

    Casimir and Casimir-Polder effects are forces between electrically neutral bodies and particles in vacuum, arising entirely from quantum fluctuations. The modification to the vacuum electromagnetic-field modes imposed by the presence of any particle or surface can result in these mechanical forces, which are often the dominant interaction at small separations. These effects play an increasingly critical role in the operation of micro- and nano-mechanical systems as well as miniaturized atomic traps for precision sensors and quantum-information devices. Despite their fundamental importance, calculations present theoretical and numeric challenges, and precise atom-surface potential measurements are lacking in many geometric and distance regimes. The spectroscopic measurement of Casimir-Polder-induced energy level shifts in optical-lattice trapped atoms offers a new experimental method to probe atom-surface interactions. Strontium, the current front-runner among optical frequency metrology systems, has demonstrated characteristics ideal for such precision measurements. An alkaline earth atom possessing ultra-narrow intercombination transitions, strontium can be loaded into an optical lattice at the "magic" wavelength where the probe transition is unperturbed by the trap light. Translation of the lattice will permit controlled transport of tightly-confined atomic samples to well-calibrated atom-surface separations, while optical transition shifts serve as a direct probe of the Casimir-Polder potential. We have constructed a strontium magneto-optical trap (MOT) for future Casimir-Polder experiments. This thesis will describe the strontium apparatus, initial trap performance, and some details of the proposed measurement procedure.

  19. Measurement of few-electron uranium ions on a high-energy electron beam ion trap

    International Nuclear Information System (INIS)

    Beiersdorfer, P.

    1994-01-01

    The high-energy electron beam ion trap, dubbed Super-EBIT, was used to produce, trap, and excite uranium ions as highly charged as fully stripped U 92+ . The production of such highly charged ions was indicated by the x-ray emission observed with high-purity Ge detectors. Moreover, high-resolution Bragg crystal spectromters were used to analyze the x-ray emission, including a detailed measurement of both the 2s 1/2 -2p 3/2 electric dipole and 2p 1/2 -2p 3/2 magnetic dipole transitions. Unlike in ion accelerators, where the uranium ions move at relativistic speeds, the ions in this trap are stationary. Thus very precise measurements of the transition energies could be made, and the QED contribution to the transition energies could be measured within less than 1 %. Details of the production of these highly charged ions and their measurement is given

  20. In situ measurements of krypton in xenon gas with a quadrupole mass spectrometer following a cold-trap at a temporarily reduced pumping speed

    Energy Technology Data Exchange (ETDEWEB)

    Brown, Ethan; Rosendahl, Stephan; Huhmann, Christian; Kettling, Hans; Schlak, Martin; Weinheimer, Christian [Muenster Univ. (Germany). Inst. fuer Kernphysik

    2013-07-01

    Liquid xenon detectors have risen to be extremely competitive for dark matter and neutrinoless double-beta decay searches. In order to achieve the required sensitivity, backgrounds must be reduced substantially. One important background is the beta-decay of {sup 85}Kr, which constitutes a uniform internal background in liquid xenon detectors. Cryogenic distillation can be used to reduce the krypton concentration to acceptable levels, but gas diagnostics become incredibly difficult at these ultra-pure levels. A new method for measuring the concentration of krypton in xenon has been developed, expanding on the existing technique of a cold trap and a Residual Gas Analyzer (RGA). By using a liquid nitrogen cold trap, one can take advantage of the difference in vapor pressures of krypton in xenon to freeze most of the xenon gas while allowing the krypton to pass to the measurement chamber. Here, only a few milliliters of xenon is expended in the measurement, while achieving a sensitivity of sub ppb (parts per billion). The key change is the use of a butterfly valve to partially close the opening in front of the turbomolecular pump, thereby reducing the effective pumping speed and enhancing the RGA signal.

  1. Early warning of diarrhea and pen fouling in growing pigs using sensor-based monitoring

    DEFF Research Database (Denmark)

    Jensen, D. B.; Toft, Nils; Kristensen, A. R.

    2016-01-01

    then identify specific pens in need of extra attention. Here we evaluate the value of monitoring live weight, feed usage, humidity, drinking behavior and pen temperature in relation to early warnings of diarrhea and pen fouling in slaughter pigs. Materials and methods: We used data collected in 16 pens (8...... double-pens) between November 2013 and December 2014 at a commercial Danish farm. During this time, three new batches were inserted. We monitored the mean live weight of the pigs per pen (weekly, only in 4 pens), feed usage per double-pen (daily), humidity per section (daily), temperature at two...... positions per pen (hourly), water flow per double-pen (liters/hour/pig) and drinking frequency per pen (activations/hour/pig). Staff registrations of diarrhea and pen fouling were the events of interest. The data were divided into a learning set (15 events) and a test set (18 events). The data were modeled...

  2. Tail posture predicts tail biting outbreaks at pen level in weaner pigs

    DEFF Research Database (Denmark)

    Lahrmann, Helle Pelant; Hansen, Christian Fink; D'Eath, Rick

    2018-01-01

    posture and behaviour could be detected at pen level between upcoming tail biting pens (T-pens) and control pens (C-pens). The study included 2301 undocked weaner pigs in 74 pens (mean 31.1 pigs/pen; SD 1.5). Tails were scored three times weekly (wound freshness, wound severity and tail length) between 07......Detecting a tail biting outbreak early is essential to reduce the risk of pigs getting severe tail damage. A few previous studies suggest that tail posture and behavioural differences can predict an upcoming outbreak. The aim of the present study was therefore to investigate if differences in tail......:00 h-14:00 h from weaning until a tail biting outbreak. An outbreak (day 0) occurred when at least four pigs had a tail damage, regardless of wound freshness. On average 7.6 (SD 4.3) pigs had a damaged tail (scratches + wound) in T-pens on day 0. Tail posture and behaviour (activity, eating...

  3. Dip-Pen Nanolithography on (Bio)Reactive Monolayer and Block-Copolymer Platforms: Deposition of Lines of Single Macromolecules

    NARCIS (Netherlands)

    Salazar, Ramon B.; Shovsky, A.; Schönherr, Holger; Vancso, Gyula J.

    2006-01-01

    The application of atomic force microscopy (AFM) tip-mediated molecular transfer (dip-pen nanolithography or DPN) to fabricate nanopatterned (bio)reactive platforms based on dendrimers on reactive self-assembled monolayer (SAM) and polymer thin films is discussed. The transfer of high-molar-mass

  4. Humalog(®) KwikPen™: an insulin-injecting pen designed for ease of use.

    Science.gov (United States)

    Schwartz, Sherwyn L; Ignaut, Debra A; Bodie, Jennifer N

    2010-11-01

    Insulin pens offer significant benefits over vial and syringe injections for patients with diabetes who require insulin therapy. Insulin pens are more discreet, easier for patients to hold and inject, and provide better dosing accuracy than vial and syringe injections. The Humalog(®) KwikPen™ (prefilled insulin lispro [Humalog] pen, Eli Lilly and Company, Indianapolis, IN, USA) is a prefilled insulin pen highly rated by patients for ease of use in injections, and has been preferred by patients to both a comparable insulin pen and to vial and syringe injections in comparator studies. Together with an engineering study demonstrating smoother injections and reduced dosing error versus a comparator pen, recent evidence demonstrates the Humalog KwikPen device is an accurate, easy-to-use, patient-preferred insulin pen.

  5. Subthreshold slope as a measure of interfacial trap density in pentacene films

    International Nuclear Information System (INIS)

    Kwon, Yongwoo; Park, Byoungnam

    2016-01-01

    Electrical properties in organic field effect transistors (FETs) are dominated by charge transport in the accumulation layer, few molecular layers close to the gate dielectric. Through comparison of the subthreshold slope between monolayer (ML) and thick pentacene FETs, formation of the second layer islands on top of the complete first layer is found to be crucial in determining the charge transport in ML pentacene FETs. It is demonstrated that a pentacene ML field effect transistor (FET) is an excellent probe that can detect electronic states of organic semiconductors interfacing with the gate dielectric at nanometer scale. Far higher sub-threshold slope in ML FETs, as a measure of interfacial charge trap density, than that in thick pentacene FETs is translated that the path of the induced carriers in ML FETs is limited into the molecular layer interfacing with the gate dielectric with a high density of charge traps, while carriers in thicker films have alternative pathways through more electrically conductive layer above the first layer with much less trap density. - Highlights: • Sub-threshold slope is demonstrated to be a measure of interface traps. • For application to sensors, effective charge transport layer should be chosen. • Monolayer transistors can be used as a platform for probing localized states.

  6. Subthreshold slope as a measure of interfacial trap density in pentacene films

    Energy Technology Data Exchange (ETDEWEB)

    Kwon, Yongwoo; Park, Byoungnam, E-mail: metalpbn@hongik.ac.kr

    2016-01-29

    Electrical properties in organic field effect transistors (FETs) are dominated by charge transport in the accumulation layer, few molecular layers close to the gate dielectric. Through comparison of the subthreshold slope between monolayer (ML) and thick pentacene FETs, formation of the second layer islands on top of the complete first layer is found to be crucial in determining the charge transport in ML pentacene FETs. It is demonstrated that a pentacene ML field effect transistor (FET) is an excellent probe that can detect electronic states of organic semiconductors interfacing with the gate dielectric at nanometer scale. Far higher sub-threshold slope in ML FETs, as a measure of interfacial charge trap density, than that in thick pentacene FETs is translated that the path of the induced carriers in ML FETs is limited into the molecular layer interfacing with the gate dielectric with a high density of charge traps, while carriers in thicker films have alternative pathways through more electrically conductive layer above the first layer with much less trap density. - Highlights: • Sub-threshold slope is demonstrated to be a measure of interface traps. • For application to sensors, effective charge transport layer should be chosen. • Monolayer transistors can be used as a platform for probing localized states.

  7. A multi-passage spectrometer for charge-state separation at MLLTRAP

    Energy Technology Data Exchange (ETDEWEB)

    Weber, Christine; Gartzke, Eva; Habs, Dietrich; Krug, Kevin; Szerypo, Jerzy; Thirolf, Peter [Fakultaet fuer Physik, LMU - Muenchen (Germany); Kolhinen, Veli [Department of Physics, University of Jyvaeskylae (Finland)

    2010-07-01

    MLLTRAP is a Penning trap mass spectrometer facility which is currently being commissioned at the Maier-Leibnitz Tandem Accelerator Laboratory in Garching. Here, atomic mass values are determined by comparison of cyclotron frequencies, {omega}{sub c}=qB/m, of stored ions with mass m and charge q in a strong magnetic field B, relative to those of well-known ion species. One of the future goals of MLLTRAP is to utilize highly-charged ions for an improvement in the achievable mass accuracy {delta}m/m. For this purpose, singly-charged ions will have to be injected into a charge-breeding device, such as an EBIT, and transferred back towards the Penning traps, while being q/A selected. A multi-passage-spectrometer (MPS) is being built to fulfill these tasks. It consists of a fast-ramping, round-pole dipole magnet with a four-way electrostatic mirror system. In this presentation, the planned MLLTRAP setup focussing on the q/A-selection with the MPS system is presented.

  8. Trace detection of organic compounds in complex sample matrixes by single photon ionization ion trap mass spectrometry: real-time detection of security-relevant compounds and online analysis of the coffee-roasting process.

    Science.gov (United States)

    Schramm, Elisabeth; Kürten, Andreas; Hölzer, Jasper; Mitschke, Stefan; Mühlberger, Fabian; Sklorz, Martin; Wieser, Jochen; Ulrich, Andreas; Pütz, Michael; Schulte-Ladbeck, Rasmus; Schultze, Rainer; Curtius, Joachim; Borrmann, Stephan; Zimmermann, Ralf

    2009-06-01

    An in-house-built ion trap mass spectrometer combined with a soft ionization source has been set up and tested. As ionization source, an electron beam pumped vacuum UV (VUV) excimer lamp (EBEL) was used for single-photon ionization. It was shown that soft ionization allows the reduction of fragmentation of the target analytes and the suppression of most matrix components. Therefore, the combination of photon ionization with the tandem mass spectrometry (MS/MS) capability of an ion trap yields a powerful tool for molecular ion peak detection and identification of organic trace compounds in complex matrixes. This setup was successfully tested for two different applications. The first one is the detection of security-relevant substances like explosives, narcotics, and chemical warfare agents. One test substance from each of these groups was chosen and detected successfully with single photon ionization ion trap mass spectrometry (SPI-ITMS) MS/MS measurements. Additionally, first tests were performed, demonstrating that this method is not influenced by matrix compounds. The second field of application is the detection of process gases. Here, exhaust gas from coffee roasting was analyzed in real time, and some of its compounds were identified using MS/MS studies.

  9. (D-Pen2,4 prime -125I-Phe4,D-Pen5)enkephalin: A selective high affinity radioligand for delta opioid receptors with exceptional specific activity

    Energy Technology Data Exchange (ETDEWEB)

    Knapp, R.J.; Sharma, S.D.; Toth, G.; Duong, M.T.; Fang, L.; Bogert, C.L.; Weber, S.J.; Hunt, M.; Davis, T.P.; Wamsley, J.K. (Department of Pharmacology, University of Arizona, College of Medicine, Tucson (United States))

    1991-09-01

    (D-Pen2,4{prime}-125I-Phe4,D-Pen5)enkephalin ((125I)DPDPE) is a highly selective radioligand for the delta opioid receptor with a specific activity (2200 Ci/mmol) that is over 50-fold greater than that of tritium-labeled DPDPE analogs. (125I)DPDPE binds to a single site in rat brain membranes with an equilibrium dissociation constant (Kd) value of 421 {plus minus} 67 pM and a receptor density (Bmax) value of 36.4 {plus minus} 2.7 fmol/mg protein. The high affinity of this site for delta opioid receptor ligands and its low affinity for mu or kappa receptor-selective ligands are consistent with its being a delta opioid receptor. The distribution of these sites in rat brain, observed by receptor autoradiography, is also consistent with that of delta opioid receptors. Association and dissociation binding kinetics of 1.0 nM (125I) DPDPE are monophasic at 25 degrees C. The association rate (k + 1 = 5.80 {plus minus} 0.88 {times} 10(7) M-1 min-1) is about 20- and 7-fold greater than that measured for 1.0 nM (3H) DPDPE and 0.8 nM (3H) (D-Pen2,4{prime}-Cl-Phe4, D-Pen5)enkephalin, respectively. The dissociation rate of (125I)DPDPE (0.917 {plus minus} 0.117 {times} 10(-2) min-1) measured at 1.0 nM is about 3-fold faster than is observed for either of the other DPDPE analogs. The rapid binding kinetics of (125I)DPDPE is advantageous because binding equilibrium is achieved with much shorter incubation times than are required for other cyclic enkephalin analogs. This, in addition to its much higher specific activity, makes (125I)DPDPE a valuable new radioligand for studies of delta opioid receptors.

  10. TRAPPED PROTON FLUXES AT LOW EARTH ORBITS MEASURED BY THE PAMELA EXPERIMENT

    Energy Technology Data Exchange (ETDEWEB)

    Adriani, O.; Bongi, M. [Department of Physics and Astronomy, University of Florence, I-50019 Sesto Fiorentino, Florence (Italy); Barbarino, G. C. [Department of Physics, University of Naples " Federico II," I-80126 Naples (Italy); Bazilevskaya, G. A. [Lebedev Physical Institute, RU-119991 Moscow (Russian Federation); Bellotti, R.; Bruno, A. [Department of Physics, University of Bari, I-70126 Bari (Italy); Boezio, M.; Bonvicini, V.; Carbone, R. [INFN, Sezione di Trieste, I-34149 Trieste (Italy); Bogomolov, E. A. [Ioffe Physical Technical Institute, RU-194021 St. Petersburg (Russian Federation); Bottai, S. [INFN, Sezione di Florence, I-50019 Sesto Fiorentino, Florence (Italy); Cafagna, F. [INFN, Sezione di Bari, I-70126 Bari (Italy); Campana, D. [INFN, Sezione di Naples, I-80126 Naples (Italy); Carlson, P. [KTH, Department of Physics, and the Oskar Klein Centre for Cosmoparticle Physics, AlbaNova University Centre, SE-10691 Stockholm (Sweden); Casolino, M.; De Donato, C.; De Santis, C.; De Simone, N.; Felice, V. Di [INFN, Sezione di Rome " Tor Vergata," I-00133 Rome (Italy); Castellini, G., E-mail: alessandro.bruno@ba.infn.it [IFAC, I-50019 Sesto Fiorentino, Florence (Italy); and others

    2015-01-20

    We report an accurate measurement of the geomagnetically trapped proton fluxes for kinetic energy above ∼70 MeV performed by the PAMELA mission at low Earth orbits (350 ÷ 610 km). Data were analyzed in the frame of the adiabatic theory of charged particle motion in the geomagnetic field. Flux properties were investigated in detail, providing a full characterization of the particle radiation in the South Atlantic Anomaly region, including locations, energy spectra, and pitch angle distributions. PAMELA results significantly improve the description of the Earth's radiation environment at low altitudes, placing important constraints on the trapping and interaction processes, and can be used to validate current trapped particle radiation models.

  11. Beta Neutrino Correlation Measurement with Trapped Radioactive Ions

    International Nuclear Information System (INIS)

    Velten, Ph.; Ban, G.; Durand, D.; Flechard, X.; Lienard, E.; Mauger, F.; Naviliat-Cuncic, O.; Mery, A.; Rodriguez, D.; Thomas, J.-C.

    2010-01-01

    The beta-neutrino angular correlation coefficient provides a sensitive observable to search for physics beyond the standard electroweak model in nuclear beta decay. We address here the measurement of this parameter in the pure Gamow-Teller transition of 6 He. A deviation from the standard model prediction would indicate the existence of tensor like couplings, possibly mediated by new bosons like leptoquarks. The aim of the LPCTrap experiment is to measure this coefficient with a statistical uncertainty of 0.5% using a novel transparent Paul trap. The status of the experiment is briefly presented along with the work in progress.

  12. Trapping volumetric measurement by multidetector CT in chronic obstructive pulmonary disease: Effect of CT threshold

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Xiaohua; Yuan, Huishu [Department of Radiology, Peking University Third Hospital, Beijing 100191 (China); Duan, Jianghui [Medical School, Peking University, Beijing 100191 (China); Du, Yipeng; Shen, Ning; He, Bei [Department of Respiration Internal Medicine, Peking University Third Hospital, Beijing 100191 (China)

    2013-08-15

    Purpose: The purpose of this study was to evaluate the effect of various computed tomography (CT) thresholds on trapping volumetric measurements by multidetector CT in chronic obstructive pulmonary disease (COPD).Methods: Twenty-three COPD patients were scanned with a 64-slice CT scanner in both the inspiratory and expiratory phase. CT thresholds of −950 Hu in inspiration and −950 to −890 Hu in expiration were used, after which trapping volumetric measurements were made using computer software. Trapping volume percentage (Vtrap%) under the different CT thresholds in the expiratory phase and below −950 Hu in the inspiratory phase was compared and correlated with lung function.Results: Mean Vtrap% was similar under −930 Hu in the expiratory phase and below −950 Hu in the inspiratory phase, being 13.18 ± 9.66 and 13.95 ± 6.72 (both lungs), respectively; this difference was not significant (P= 0.240). Vtrap% under −950 Hu in the inspiratory phase and below the −950 to −890 Hu threshold in the expiratory phase was moderately negatively correlated with the ratio of forced expiratory volume in one second to forced vital capacity and the measured value of forced expiratory volume in one second as a percentage of the predicted value.Conclusions: Trapping volumetric measurement with multidetector CT is a promising method for the quantification of COPD. It is important to know the effect of various CT thresholds on trapping volumetric measurements.

  13. Temperature measurement of {sup 6}He{sup + } ions confined in a transparent Paul trap

    Energy Technology Data Exchange (ETDEWEB)

    Flechard, X., E-mail: flechard@lpccaen.in2p3.fr; Ban, G.; Durand, D.; Lienard, E.; Mauger, F. [Universite de Caen, LPC Caen, ENSICAEN (France); Mery, A. [Universite de Caen, CIMAP, CEA/CNRS/ENSICAEN (France); Naviliat-Cuncic, O. [Universite de Caen, LPC Caen, ENSICAEN (France); Rodriguez, D. [Universitad de Granada, Departamento de Fisica Atomica, Molecular y Nuclear (Spain); Velten, P. [Universite de Caen, LPC Caen, ENSICAEN (France)

    2011-07-15

    The LPCTrap setup is a transparent Paul trap dedicated to the measurement of the {beta}-{nu} correlation coefficient a{sub {beta}{nu}} in the {beta} decay of trapped radioactive nuclides. In a first experiment, the system has been used to record {approx}10{sup 5} coincidences between the {beta} particles and recoiling ions emitted from the decay of {sup 6}He{sup + } ions. The analysis of the collected data has already shown that the size of the {sup 6}He{sup + } ion cloud confined in the Paul trap is a critical parameter, potentially limiting the accuracy on the a{sub {beta}{nu}} measurement. We report here the precise determination of the trapped ion cloud temperature and size. This was performed by extracting the trapped ions toward a position sensitive micro channel plate detector at different phases of the RF driving field. We find a temperature T{sub exp} = 0.107(7) eV, consistent with the temperature values inferred using two other observables but 20% higher than the temperature T{sub sim} = 0.09 eV predicted by realistic simulations of the ions interacting with the H{sub 2} buffer gas.

  14. Double-β decay Q value of 150Nd

    International Nuclear Information System (INIS)

    Kolhinen, V. S.; Eronen, T.; Gorelov, D.; Hakala, J.; Jokinen, A.; Kankainen, A.; Moore, I. D.; Rissanen, J.; Saastamoinen, A.; Suhonen, J.; Aeystoe, J.

    2010-01-01

    The double-β decay Q value of 150 Nd was determined by using the JYFLTRAP Penning trap mass spectrometer. The measured mass difference between 150 Nd and 150 Sm is 3371.38(20) keV. This new value deviates by 3.7 keV from the previously adopted value of 3367.7(22) keV and is a factor of 10 more precise. Accurate knowledge of this Q value is important because 150 Nd is a primary candidate to be used in the search for neutrinoless double-β decay modes in several experiments.

  15. Single Ion Trapping for the Enriched Xenon Observatory

    Energy Technology Data Exchange (ETDEWEB)

    Waldman, Samuel J.; /Stanford U., Phys. Dept. /SLAC

    2006-03-28

    In the last decade, a variety of neutrino oscillation experiments have established that there is a mass difference between neutrino flavors, without determining the absolute neutrino mass scale. The Enriched Xenon Observatory for neutrinoless double beta decay (EXO) will search for the rare decays of xenon to determine the absolute value of the neutrino mass. The experiment uses a novel technique to minimize backgrounds, identifying the decay daughter product in real time using single ion spectroscopy. Here, we describe single ion trapping and spectroscopy compatible with the EXO detector. We extend the technique of single ion trapping in ultrahigh vacuum to trapping in xenon gas. With this technique, EXO will achieve a neutrino mass sensitivity of {approx_equal} .010 eV.

  16. Online trapping and enrichment ultra performance liquid chromatography-tandem mass spectrometry method for sensitive measurement of 'arginine-asymmetric dimethylarginine cycle' biomarkers in human exhaled breath condensate

    Energy Technology Data Exchange (ETDEWEB)

    Di Gangi, Iole Maria, E-mail: giordano@pediatria.unipd.it [Chromatography and Mass Spectrometry Laboratory, Department of Women' s and Children' s Health, University of Padova (Italy); Pirillo, Paola [Chromatography and Mass Spectrometry Laboratory, Department of Women' s and Children' s Health, University of Padova (Italy); Carraro, Silvia [Unit of Allergy and Respiratory Diseases, Department of Women' s and Children' s Health, University of Padova (Italy); Gucciardi, Antonina; Naturale, Mauro [Chromatography and Mass Spectrometry Laboratory, Department of Women' s and Children' s Health, University of Padova (Italy); Baraldi, Eugenio [Unit of Allergy and Respiratory Diseases, Department of Women' s and Children' s Health, University of Padova (Italy); Giordano, Giuseppe [Chromatography and Mass Spectrometry Laboratory, Department of Women' s and Children' s Health, University of Padova (Italy)

    2012-11-19

    Highlights: Black-Right-Pointing-Pointer Simultaneous quantification of 'arginine-ADMA cycle' metabolites developed in EBC. Black-Right-Pointing-Pointer EBC is a non-invasive matrix highly useful in patients with respiratory diseases. Black-Right-Pointing-Pointer Method, fast, precise and accurate, is suitable in the pediatric clinical studies. Black-Right-Pointing-Pointer Sensitivity is increased using on-line trapping and enrichment-UPLC-MS/MS method. Black-Right-Pointing-Pointer EBC measurements in asthmatic adolescents confirm that ADMA is increased in asthma. - Abstract: Background: Exhaled breath condensate (EBC) is a biofluid collected non invasively that, enabling the measurement of several biomarkers, has proven useful in the study of airway inflammatory diseases, including asthma, COPD and cystic fibrosis. To the best of our knowledge, there is no previous report of any analytical method to detect ADMA in EBC. Objectives: Aim of this work was to develop an online sample trapping and enrichment system, coupled with an UPLC-MS/MS method, for simultaneous quantification of seven metabolites related to 'Arginine-ADMA cycle', using the isotopic dilution. Methods: Butylated EBC samples were trapped in an online cartridge, washed before and after each injection with cleanup solution to remove matrix components and switched inline into the high pressure analytical column. Multiple reaction monitoring in positive mode was used for analyte quantification by tandem mass spectrometry. Results: Validation studies were performed in EBC to examine accuracy, precision and robustness of the method. For each compound, the calibration curves showed a coefficient of correlation (r{sup 2}) greater than 0.992. Accuracy (%Bias) was <3% except for NMMA and H-Arg (<20%), intra- and inter-assay precision (expressed as CV%) were within {+-}20% and recovery ranged from 97.1 to 102.8% for all analytes. Inter-day variability analysis on 20 EBC of adult subjects did

  17. Essential Characteristics of Plasma Antennas Filled with He-Ar Penning Gases

    International Nuclear Information System (INIS)

    Sun Naifeng; Li Wenzhong; Wang Shiqing; Li Jian; Ci Jiaxiang

    2012-01-01

    Based on the essential theory of Penning gases, the discharge characteristics of He-Ar Penning gases in insulating tubes were analyzed qualitatively. The relation between the effective length of an antenna column filled with He-Ar Penning gases and the applied radio frequency (RF) power was investigated both theoretically and experimentally. The distribution of the plasma density along the antenna column in different conditions was studied. The receiving characteristics of local frequency modulated (FM) electromagnetic waves by the plasma antenna filled with He-Ar Penning gases were compared with those by an aluminum antenna with the same dimensions. Results show that it is feasible to take plasma antennas filled with He-Ar Penning gases as receiving antennas.

  18. Ease of use and patient preference injection simulation study comparing two prefilled insulin pens.

    Science.gov (United States)

    Clark, Paula E; Valentine, Virginia; Bodie, Jennifer N; Sarwat, Samiha

    2010-07-01

    To determine patient ease of use and preference for the Humalog KwikPen* (prefilled insulin lispro [Humalog dagger] pen, Eli Lilly and Company, Indianapolis, IN, USA) (insulin lispro pen) versus the Next Generation FlexPen double dagger (prefilled insulin aspart [NovoRapid section sign ] pen, Novo Nordisk A/S, Bagsvaerd, Denmark) (insulin aspart pen). This was a randomized, open-label, 2-period, 8-sequence crossover study in insulin pen-naïve patients with diabetes. Randomized patients (N = 367) received device training, then simulated low- (15 U) and high- (60 U) dose insulin injections with an appliance. Patients rated pens using an ease of use questionnaire and were asked separately for final pen preferences. The Insulin Device 'Ease of Use' Battery is a 10-item questionnaire with a 7-point scale (higher scores reflect greater ease of use). The primary objective was to determine pen preference for 'easy to press to inject my dose' (by comparing composite scores [low- plus high-dose]). Secondary objectives were to determine pen preference on select questionnaire items (from composite scores), final pen preference, and summary responses for all questionnaire items. On the primary endpoint, 'easy to press to inject my dose,' a statistically significant majority of patients with a preference chose the insulin lispro pen over the insulin aspart pen (68.4%, 95% CI = 62.7-73.6%). Statistically significant majorities of patients with a preference also favored the insulin lispro pen on secondary items: 'easy to hold in my hand when I inject' (64.9%, 95% CI = 58.8-70.7%), 'easy to use when I am in a public place' (67.5%, 95% CI = 61.0-73.6%), and 'overall easy to use' (69.9%, 95% CI = 63.9-75.4%). A statistically significant majority of patients had a final preference for the insulin lispro pen (67.3%, 95% CI = 62.2-72.1%). Among pen-naïve patients with diabetes who had a preference, the majority preferred the insulin lispro pen over the insulin aspart pen with regard

  19. Properties of H- and D- beams from magnetron and Penning sources

    International Nuclear Information System (INIS)

    Sluyters, T.; Kovarik, V.

    1979-01-01

    The quality of negative hydrogen isotope beams are evaluated after extraction from magnetron and Penning sources. The general conclusions of these measurements are that: (a) the beam quality from these plasma sources are adequate for the transport of high current negative ion beams in bending magnets; (b) there is evidence of practically complete space charge neutralization in the drift space beyond the extractor; (c) the beam performance from the Penning source appears to be better compared with the magnetron source; and (d) it is likely that the high electric field gradient and a concave ion emission boundary are responsible for a beam cross-over near the anode aperture, which causes beam divergence practically independent of the extraction geometry

  20. Mass measurement of halo nuclides and beam cooling with the mass spectrometer Mistral; Mesure de masse de noyaux a halo et refroidissement de faisceaux avec l'experience MISTRAL

    Energy Technology Data Exchange (ETDEWEB)

    Bachelet, C

    2004-12-01

    Halo nuclides are a spectacular drip-line phenomenon and their description pushes nuclear theories to their limits. The most critical input parameter is the nuclear binding energy; a quantity that requires excellent measurement precision, since the two-neutron separation energy is small at the drip-line by definition. Moreover halo nuclides are typically very short-lived. Thus, a high accuracy instrument using a quick method of measurement is necessary. MISTRAL is such an instrument; it is a radiofrequency transmission mass spectrometer located at ISOLDE/CERN. In July 2003 we measured the mass of the Li{sup 11}, a two-neutron halo nuclide. Our measurement improves the precision by a factor 6, with an error of 5 keV. Moreover the measurement gives a two-neutron separation energy 20% higher than the previous value. This measurement has an impact on the radius of the nucleus, and on the state of the two valence neutrons. At the same time, a measurement of the Be{sup 11} was performed with an uncertainty of 4 keV, in excellent agreement with previous measurements. In order to measure the mass of the two-neutron halo nuclide Be{sup 14}, an ion beam cooling system is presently under development which will increase the sensitivity of the spectrometer. The second part of this work presents the development of this beam cooler using a gas-filled Paul trap. (author)

  1. Quadrature detection for the separation of the signals of positive and negative ions in fourier transform ion cyclotron resonance mass spectrometry

    International Nuclear Information System (INIS)

    Schweikhard, Lutz; Drader, Jared J.; Shi, Stone D.-H.; Hendrickson, Christopher L.; Marshall, Alan G.

    2002-01-01

    Positive and negative ions may be confined simultaneously in a nested open cylindrical Malmberg-Penning trap. However, ion charge sign cannot be distinguished by conventional dipolar (linearly-polarized) detection with a single pair of opposed electrodes. Here, the signals from each of two orthogonal pairs of opposed detection electrodes are acquired simultaneously and stored as real and imaginary parts of mathematically complex data. Complex Fourier transformation yields separate spectra for positive and negative ions. For a fullerene sample, experimental quadrature detection yields C 60 + and C 60 - signals separated by ∼1440 u rather than by the mass of two electrons, ∼0.001 u in conventional dipolar detection

  2. Ultrafast state detection and 2D ion crystals in a Paul trap

    Science.gov (United States)

    Ip, Michael; Ransford, Anthony; Campbell, Wesley

    2016-05-01

    Projective readout of quantum information stored in atomic qubits typically uses state-dependent CW laser-induced fluorescence. This method requires an often sophisticated imaging system to spatially filter out the background CW laser light. We present an alternative approach that instead uses simple pulse sequences from a mode-locked laser to affect the same state-dependent excitations in less than 1 ns. The resulting atomic fluorescence occurs in the dark, allowing the placement of non-imaging detectors right next to the atom to improve the qubit state detection efficiency and speed. We also study 2D Coulomb crystals of atomic ions in an oblate Paul trap. We find that crystals with hundreds of ions can be held in the trap, potentially offering an alternative to the use of Penning traps for the quantum simulation of 2D lattice spin models. We discuss the classical physics of these crystals and the metastable states that are supported in 2D. This work is supported by the US Army Research Office.

  3. Pen-based Interfaces for Engineering and Education

    Science.gov (United States)

    Stahovich, Thomas F.

    Sketches are an important problem-solving tool in many fields. This is particularly true of engineering design, where sketches facilitate creativity by providing an efficient medium for expressing ideas. However, despite the importance of sketches in engineering practice, current engineering software still relies on traditional mouse and keyboard interfaces, with little or no capabilities to handle free-form sketch input. With recent advances in machine-interpretation techniques, it is now becoming possible to create practical interpretation-based interfaces for such software. In this chapter, we report on our efforts to create interpretation techniques to enable pen-based engineering applications. We describe work on two fundamental sketch understanding problems. The first is sketch parsing, the task of clustering pen strokes or geometric primitives into individual symbols. The second is symbol recognition, the task of classifying symbols once they have been located by a parser. We have used the techniques that we have developed to construct several pen-based engineering analysis tools. These are used here as examples to illustrate our methods. We have also begun to use our techniques to create pen-based tutoring systems that scaffold students in solving problems in the same way they would ordinarily solve them with paper and pencil. The chapter concludes with a brief discussion of these systems.

  4. The W Boson Mass Measurement

    CERN Document Server

    Kotwal, Ashutosh V

    2016-01-01

    The measurement of the W boson mass has been growing in importance as its precision has improved, along with the precision of other electroweak observables and the top quark mass. Over the last decade, the measurement of the W boson mass has been led at hadron colliders. Combined with the precise measurement of the top quark mass at hadron colliders, the W boson mass helped to pin down the mass of the Standard Model Higgs boson through its induced radiative correction on the W boson mass. With the discovery of the Higgs boson and the measurement of its mass, the electroweak sector of the Standard Model is over-constrained. Increasing the precision of the W boson mass probes new physics at the TeV-scale. We summarize an extensive Tevatron (1984–2011) program to measure the W boson mass at the CDF and Dø experiments. We highlight the recent Tevatron measurements and prospects for the final Tevatron measurements.

  5. Trapping, self-trapping and the polaron family

    International Nuclear Information System (INIS)

    Stoneham, A M; Gavartin, J; Shluger, A L; Kimmel, A V; Ramo, D Munoz; Roennow, H M; Aeppli, G; Renner, C

    2007-01-01

    The earliest ideas of the polaron recognized that the coupling of an electron to ionic vibrations would affect its apparent mass and could effectively immobilize the carrier (self-trapping). We discuss how these basic ideas have been generalized to recognize new materials and new phenomena. First, there is an interplay between self-trapping and trapping associated with defects or with fluctuations in an amorphous solid. In high dielectric constant oxides, like HfO 2 , this leads to oxygen vacancies having as many as five charge states. In colossal magnetoresistance manganites, this interplay makes possible the scanning tunnelling microscopy (STM) observation of polarons. Second, excitons can self-trap and, by doing so, localize energy in ways that can modify the material properties. Third, new materials introduce new features, with polaron-related ideas emerging for uranium dioxide, gate dielectric oxides, Jahn-Teller systems, semiconducting polymers and biological systems. The phonon modes that initiate self-trapping can be quite different from the longitudinal optic modes usually assumed to dominate. Fourth, there are new phenomena, like possible magnetism in simple oxides, or with the evolution of short-lived polarons, like muons or excitons. The central idea remains that of a particle whose properties are modified by polarizing or deforming its host solid, sometimes profoundly. However, some of the simpler standard assumptions can give a limited, indeed misleading, description of real systems, with qualitative inconsistencies. We discuss representative cases for which theory and experiment can be compared in detail

  6. Criticality experiments to provide benchmark data on neutron flux traps

    International Nuclear Information System (INIS)

    Bierman, S.R.

    1988-06-01

    The experimental measurements covered by this report were designed to provide benchmark type data on water moderated LWR type fuel arrays containing neutron flux traps. The experiments were performed at the US Department of Energy Hanford Critical Mass Laboratory, operated by Pacific Northwest Laboratory. The experimental assemblies consisted of 2 /times/ 2 arrays of 4.31 wt % 235 U enriched UO 2 fuel rods, uniformly arranged in water on a 1.891 cm square center-to-center spacing. Neutron flux traps were created between the fuel units using metal plates containing varying amounts of boron. Measurements were made to determine the effect that boron loading and distance between the fuel and flux trap had on the amount of fuel required for criticality. Also, measurements were made, using the pulse neutron source technique, to determine the effect of boron loading on the effective neutron multiplications constant. On two assemblies, reaction rate measurements were made using solid state track recorders to determine absolute fission rates in 235 U and 238 U. 14 refs., 12 figs., 7 tabs

  7. Loading of mass spectrometry ion trap with Th ions by laser ablation for nuclear frequency standard application.

    Science.gov (United States)

    Borisyuk, Petr V; Derevyashkin, Sergey P; Khabarova, Ksenia Y; Kolachevsky, Nikolay N; Lebedinsky, Yury Y; Poteshin, Sergey S; Sysoev, Alexey A; Tkalya, Evgeny V; Tregubov, Dmitry O; Troyan, Viktor I; Vasiliev, Oleg S; Yakovlev, Valery P; Yudin, Valery I

    2017-08-01

    We describe an original multisectional quadrupole ion trap aimed to realize nuclear frequency standard based on the unique isomer transition in thorium nucleus. It is shown that the system effectively operates on Th + , Th 2+ and Th 3+ ions produced by laser ablation of metallic thorium-232 target. Laser intensity used for ablation is about 6 GW/cm 2 . Via applying a bias potential to every control voltage including the RF one, we are able not only to manipulate ions within the energy range as wide as 1-500 eV but to specially adjust trap potentials in order to work mainly with ions that belong to energy distribution maximum and therefore to effectively enhance the number of trapped ions. Measurement of energy distributions of 232 Th + , 232 Th 2+ , 232 Th 3+ ions obtained by laser ablation allows us to define optimal potential values for trapping process. Observed number of ions inside trap in dependence on trapping time is found to obey an unusually slow - logarithmic decay law that needs more careful study.

  8. Direct measurements of the plasma potential in ELMy H-mode plasma with ball-pen probes on ASDEX Upgrade tokamak

    Energy Technology Data Exchange (ETDEWEB)

    Adamek, J., E-mail: adamek@ipp.cas.c [Institute of Plasma Physics, Association EURATOM/IPP.CR, Prague, Za Slovankou 3, 182 00, Prague 8 (Czech Republic); Rohde, V.; Mueller, H.W.; Herrmann, A. [Institute of Plasma Physics, Association EURATOM/IPP, Garching (Germany); Ionita, C.; Schrittwieser, R.; Mehlmann, F. [Institute for Ion Physics and Applied Physics, University of Innsbruck, Association EURATOM/OAW (Austria); Stoeckel, J.; Horacek, J.; Brotankova, J. [Institute of Plasma Physics, Association EURATOM/IPP.CR, Prague, Za Slovankou 3, 182 00, Prague 8 (Czech Republic)

    2009-06-15

    Experimental investigations of the plasma potential and electric field were performed for ELMy H-mode plasmas in the vicinity of the limiter shadow of ASDEX Upgrade. A fast reciprocating probe with a probe head containing four ball-pen probes (BPPs) [J. Adamek et al., Czech. J. Phys. 54 (2004) C95 - C99.] was used on the midplane manipulator. Different gradients of the plasma potential were observed during ELMs and in between them. The temporal resolution of the direct plasma potential measurements with BPP was determined by using power-spectra analysis.

  9. First simultaneous measurements of Reynolds stress with ball-pen and Langmuir probes

    Czech Academy of Sciences Publication Activity Database

    Grover, Ondřej; Adámek, Jiří; Seidl, Jakub; Devitre, A.; Šos, Miroslav; Vondráček, Petr; Bílková, Petra; Hron, Martin

    2017-01-01

    Roč. 88, č. 6 (2017), č. článku 063501. ISSN 0034-6748 R&D Projects: GA ČR(CZ) GA15-10723S; GA ČR(CZ) GA16-25074S; GA MŠk(CZ) LM2015045 Institutional support: RVO:61389021 Keywords : COMPASS tokamak * Electric field effects * Electric fields * Langmuir probes * Magnetoplasma * Ball-pen probes Subject RIV: BL - Plasma and Gas Discharge Physics OBOR OECD: 2.11 Other engineering and technologies Impact factor: 1.515, year: 2016 http://aip.scitation.org/doi/full/10.1063/1.4984240

  10. Pen-on-paper strategy for point-of-care testing: Rapid prototyping of fully written microfluidic biosensor.

    Science.gov (United States)

    Li, Zedong; Li, Fei; Xing, Yue; Liu, Zhi; You, Minli; Li, Yingchun; Wen, Ting; Qu, Zhiguo; Ling Li, Xiao; Xu, Feng

    2017-12-15

    Paper-based microfluidic biosensors have recently attracted increasing attentions in point-of-care testing (POCT) territories benefiting from their affordable, accessible and eco-friendly features, where technologies for fabricating such biosensors are preferred to be equipment free, easy-to-operate and capable of rapid prototyping. In this work, we developed a pen-on-paper (PoP) strategy based on two custom-made pens, i.e., a wax pen and a conductive-ink pen, to fully write paper-based microfluidic biosensors through directly writing both microfluidic channels and electrodes. Particularly, the proposed wax pen is competent to realize one-step fabrication of wax channels on paper, as the melted wax penetrates into paper during writing process without any post-treatments. The practical applications of the fabricated paper-based microfluidic biosensors are demonstrated by both colorimetric detection of Salmonella typhimurium DNA with detection limit of 1nM and electrochemical measurement of glucose with detection limit of 1mM. The developed PoP strategy for making microfluidic biosensors on paper characterized by true simplicity, prominent portability and excellent capability for rapid prototyping shows promising prospect in POCT applications. Copyright © 2017 Elsevier B.V. All rights reserved.

  11. A quadrupole ion trap as low-energy cluster ion beam source

    CERN Document Server

    Uchida, N; Kanayama, T

    2003-01-01

    Kinetic energy distribution of ion beams was measured by a retarding field energy analyzer for a mass-selective cluster ion beam deposition system that uses a quadrupole ion trap as a cluster ion beam source. The results indicated that the system delivers a cluster-ion beam with energy distribution of approx 2 eV, which corresponded well to the calculation results of the trapping potentials in the ion trap. Using this deposition system, mass-selected hydrogenated Si cluster ions Si sub n H sub x sup + were actually deposited on Si(111)-(7x7) surfaces at impact kinetic energy E sub d of 3-30 eV. Observation by using a scanning tunneling microscope (STM) demonstrated that Si sub 6 H sub x sup + cluster ions landed on the surface without decomposition at E sub d =3 eV, while the deposition was destructive at E sub d>=18 eV. (author)

  12. The analysis of dyes in ball point pen inks on single paper fibres using laser desorption ionisation time of flight mass spectrometry (LDI-TOFMS).

    Science.gov (United States)

    Matthews, Broderick; Walker, G Stewart; Kobus, Hilton; Pigou, Paul; Bird, Carolyne; Smith, Glyn

    2011-06-15

    An important requisite for the forensic analysis of inks on documents is that damage to the document is avoided or minimised. This paper describes a technique for dye identification in ballpoint pen inks using LDI-TOFMS on single ink bearing paper fibres and its application to a case. A single ink bearing paper fibre can be prised from the surface of the document under a stereo microscope and presented to the instrument for analysis without further treatment. This sampling process causes imperceptible damage to the surface of the document. Clear mass spectrometric identification of the ink dyes is obtained. A case example is provided to illustrate the practical application of the technique. Copyright © 2011 Elsevier Ireland Ltd. All rights reserved.

  13. Measurement Of The β-ν Correlation In 6He Using A Transparent Paul Trap

    International Nuclear Information System (INIS)

    Lienard, E.; Ban, G.; Darius, G.; Durand, D.; Flechard, X.; Herbane, M.; Labalme, M.; Mauger, F.; Mery, A.; Naviliat-Cuncic, O.; Rodriguez, D.

    2006-01-01

    The angular correlation between the electron and the neutrino in nuclear β-decay constitutes a sensitive observable to search for the existence of exotic couplings in the weak interaction. In this contribution, we describe the progress of the LPCTrap experiment, devoted to measure the β-ν angular correlation in the pure Gamow-Teller (GT) decay of 6He using a transparent Paul trap. We present a first coincidence spectrum, obtained during the commissioning run, which is the first β-recoil coincidence measurement obtained from any ion trap

  14. Comparative measurements of plasma potential with ball-pen and Langmuir probe in low-temperature magnetized plasma

    Science.gov (United States)

    Zanáška, M.; Adámek, J.; Peterka, M.; Kudrna, P.; Tichý, M.

    2015-03-01

    The ball-pen probe (BPP) is used for direct plasma potential measurements in magnetized plasma. The probe can adjust the ratio of the electron and ion saturation currents Isat-/Isat+ to be close to one and therefore its I-V characteristic becomes nearly symmetric. If this is achieved, the floating potential of the BPP is close to the plasma potential. Because of its rather simple construction, it offers an attractive probe for measurements in magnetized plasma. Comparative measurements of plasma potential by BPPs of different dimensions as well as one Langmuir probe (LP) in an argon discharge plasma of a cylindrical magnetron were performed at various experimental conditions. An additional comparison by an emissive probe was also performed. All these types of probes provide similar values of plasma potential in a wide range of plasma parameters. Our results for three different BPP dimensions indicate that the BPP can be operated in a cylindrical magnetron DC argon discharge if the value of the ratio of the magnetic field and neutral gas pressure, B/p, is greater than approximately 10 mT/Pa.

  15. Correlates of cannabis vape-pen use and knowledge among U.S. college students

    Directory of Open Access Journals (Sweden)

    Tessa Frohe

    2018-06-01

    Full Text Available Introduction: The proliferation of electronic devices, such as vape-pens, has provided alternative means for cannabis use. Research has found cannabis-vaping (i.e., vape-pen use is associated with lower perceived risks and higher cannabis use. Knowledge of these products may increase likelihood of subsequent use. As policies for cannabis shift, beliefs that peers and family approve of this substance use (injunctive norms increase and there has been an increase in vape-pen use among young adults (18–35year olds; however, correlates thereof remain unknown. Young adults often engage in cross-substance use with cannabis and alcohol, making alcohol a potential correlate of cannabis vape-pen use and knowledge. Therefore, we examined alcohol use and other potential correlates of vape-pen use and knowledge among a sample of university students. Methods: This secondary data analysis utilized surveys at multiple colleges in the U.S. (N=270. Alcohol use, social anxiety, cannabis expectancies, injunctive and descriptive norms and facets of impulsivity were examined as correlates of vape-pen use and knowledge using bivariate correlations and logistic regressions. Results: Alcohol use was correlated with cannabis vape-pen use and knowledge. Frequency of cannabis use, peer injunctive norms, and positive expectancies were associated with increased likelihood of vape-pen use. Lack of premeditation, a facet of impulsivity, was associated with cannabis vape-pen knowledge. Conclusions: Given the unknown nature and consequences of cannabis vape-pens, the present findings offer valuable information on correlates of this behavior. Further, correlates of knowledge of vape-pens may point to areas for education and clinical intervention to prevent heavy cannabis vape-pen use. Keywords: Marijuana, Vaporizer, College students, Substance use, Attitudes, Cannabis

  16. High-precision mass measurements of nickel, copper, and gallium isotopes and the purported shell closure at N=40

    International Nuclear Information System (INIS)

    Guenaut, C.; Audi, G.; Beck, D.

    2007-01-01

    High-precision mass measurement of more than thirty neutron-rich nuclides around the Z=28 closed proton shell were performed with the triple-trap mass spectrometer ISOLTRAP at ISOLDE/CERN to address the question of a possible neutron shell closure at N=40. The results for 57,60,64-69 Ni, 65-74,76 Cu (Z=29), and 63-65,68-78 Ga (Z=31), have a relative uncertainty of the order of 10 -8 . In particular, the masses of 72-74,76 Cu have been measured for the first time. We analyse the resulting mass surface for signs of magicity, comparing the behavior of N=40 to that of known magic numbers and to mid-shell behavior. Contrary to nuclear spectroscopy studies, no indications of a shell or sub-shell closure are found for N=40. (authors)

  17. Differential fragmentation patterns of pectin oligogalacturonides observed by nanoelectrospray quadrupole ion-trap mass spectrometry using automated spectra interpretation

    DEFF Research Database (Denmark)

    Mutenda, Kudzai E; Matthiesen, Rune; Roepstorff, Peter

    2007-01-01

    Oligogalacturonides of different degrees of polymerization (DP) and methyl esterification (DE) were structurally analyzed by nanoESI quadrupole ion-trap mass spectrometry. The fragmentation patterns of the oligogalacturonides were compared using the program 'Virtual Expert Mass Spectrometrist...... with free carboxylic acid groups underwent higher water loss compared to fully methyl-esterified oligogalacturonides under the same fragmentation conditions. Cross-ring cleavage, in which fragmentation occurs across the ring system of the galacturonate residue and signified by unique mass losses...... water loss than methyl-esterified ones will be postulated. In addition, the VEMS program was extended to automatically interpret and assign the fragment ions peaks generated in this study....

  18. Effects of neutrino trapping on supernova explosions

    International Nuclear Information System (INIS)

    Takahara, Mariko; Sato, Katsuhiko

    1982-01-01

    Effects of neutrino trapping on the mass ejection from the stellar cores are investigated with the aid of a simplified equation of state under the assumption of adiabatic collapse. It is found that mass ejection becomes violent only if the ratio of the trapped leptons to baryons, Y sub(L), lies in an appropriate range. If the value of Y sub(L) lies out of this range, mass ejection is difficult. It is also shown that as the thermal stiffness of the shocked matter increases, the range necessary for the violent mass ejection becomes wider. Possibilities of supernova explosion are discussed on the basis of these results. (author)

  19. Research with stored ions produced using synchrotron radiation

    International Nuclear Information System (INIS)

    Church, D.A.; Kravis, S.D.; Meron, M.; Johnson, B.M.; Jones, K.W.; Sellin, I.A.; O, C.S.; Levin, J.C.; Short, R.T.

    1987-01-01

    A distribution of argon ion charge states has been produced by inner shell photoionization of argon atoms using x-ray synchrotron radiation. These ions were stored in a Penning ion trap at moderate to very low well depths, and analog-detected yielding narrow charge-to-mass spectrum linewidths. Estimates of ion densities indicated that ion-ion collisional energy transfer should be rapid, leading to thermalization. Measurements using variants of this novel stored, multi-charged ion gas are considered

  20. In situ measurements of krypton in xenon gas with a quadrupole mass spectrometer following a cold-trap at a temporarily reduced pumping speed

    International Nuclear Information System (INIS)

    Brown, E; Rosendahl, S; Huhmann, C; Weinheimer, C; Kettling, H

    2013-01-01

    A new method for measuring trace amounts of krypton in xenon using a cold trap with a residual gas analyzer has been developed, which achieves an increased sensitivity by temporarily reducing the pumping speed while expending a minimal amount of xenon. By partially closing a custom built butterfly valve between the measurement chamber and the turbomolecular pump, a sensitivity of 40 ppt has been reached. This method has been tested on an ultra-pure gas sample from Air Liquide with an unknown intrinsic krypton concentration, yielding a krypton concentration of 330±200 ppt.

  1. Development of a Linear Ion Trap Mass Spectrometer (LITMS) Investigation for Future Planetary Surface Missions

    Science.gov (United States)

    Brinckerhoff, W.; Danell, R.; Van Ameron, F.; Pinnick, V.; Li, X.; Arevalo, R.; Glavin, D.; Getty, S.; Mahaffy, P.; Chu, P.; hide

    2014-01-01

    Future surface missions to Mars and other planetary bodies will benefit from continued advances in miniature sensor and sample handling technologies that enable high-performance chemical analyses of natural samples. Fine-scale (approx.1 mm and below) analyses of rock surfaces and interiors, such as exposed on a drill core, will permit (1) the detection of habitability markers including complex organics in association with their original depositional environment, and (2) the characterization of successive layers and gradients that can reveal the time-evolution of those environments. In particular, if broad-based and highly-sensitive mass spectrometry techniques could be brought to such scales, the resulting planetary science capability would be truly powerful. The Linear Ion Trap Mass Spectrometer (LITMS) investigation is designed to conduct fine-scale organic and inorganic analyses of short (approx.5-10 cm) rock cores such as could be acquired by a planetary lander or rover arm-based drill. LITMS combines both pyrolysis/gas chromatograph mass spectrometry (GCMS) of sub-sampled core fines, and laser desorption mass spectrometry (LDMS) of the intact core surface, using a common mass analyzer, enhanced from the design used in the Mars Organic Molecule Analyzer (MOMA) instrument on the 2018 ExoMars rover. LITMS additionally features developments based on the Sample Analysis at Mars (SAM) investigation on MSL and recent NASA-funded prototype efforts in laser mass spectrometry, pyrolysis, and precision subsampling. LITMS brings these combined capabilities to achieve its four measurement objectives: (1) Organics: Broad Survey Detect organic molecules over a wide range of molecular weight, volatility, electronegativity, concentration, and host mineralogy. (2) Organic: Molecular Structure Characterize internal molecular structure to identify individual compounds, and reveal functionalization and processing. (3) Inorganic Host Environment Assess the local chemical

  2. Overview of the mass measurements

    International Nuclear Information System (INIS)

    Shull, L.M.

    1991-01-01

    a three-day mass measurement workshop conference sponsored by the INMM was held April 22-24, 1991, in Atlanta, Georgia. DOE Order 5633.3 requires mass measurement control programs for the measurements of nuclear materials but provides little guidance on details for these programs. Measurement principles used for mass are often applicable to other physical property measurements. Westinghouse Savannah River Site (WSRS) personnel organized the workshop conference to facilitate the transfer of mass measurement technology and establish better communications between the calibration laboratories, manufactures, regulators, and scale and balance users in the mass measurement community. Three different formats were used to present the information: a seminar, individual papers, and workshops. The seminar topic was the Process Measurement Assurance Program (PMAP), developed by EG and G Mound Applied Technologies, for determining and controlling measurement errors in manufacturing processes. Paper and workshop topics included: Mass Measurement Techniques and Programs, Selection of equipment and Standards, Standards and Traceability, and Automation in Mass Measurement. The paper gives an overview of the workshop conference, including purpose, participants, and summaries of the seminar, paper, and workshops

  3. [Comparative study of intraocular pressure measurements by Goldmann applanation tonometer, noncontact tonometer and TonoPen].

    Science.gov (United States)

    Ceská, Burdová M; Ferrová, K; Filous, A; Oskorypová, K; Lezatková, P; Sedlácková, P

    2012-02-01

    The purpose of the study was to compare the levels of the intraocular pressure (NOT) measured in one eye at the same moment by three different methods: by Goldmann applanation tonometer (AT), non-contact tonometer (BT) and Tono-Pen (TP). It was further set the average variability of the performed measurements for particular tonometric methods. NOT was assessed in 106 eyes of 106 subjects aged 7-77 years (average 34.3 +/- 17.1 years). NOT was measured at the same moment with BT, TP and AT. The obtained data were statistically analyzed. The average NOT was 16.55 +/- 2.95, 17.95 +/- 4.47 and 16.13 +/- 3.4 mmHg when AT, BT and TP were applied. Average variability of three measurements for AT, BT and TP was 1.51 +/- 0.96, 1.78 +/- 1.08 and 1.47 +/- 0.9 mmHg. Average NOT levels of the measured AT and TP were almost identical with a difference of 0.42 mmHg (p = 0.236). Average level of the intraocular pressure measured by BT was higher by 1.40 mmHg and 1.82 mmHg in comparison with AT and TP (p = 0.00002), respectively. NOT measurement produced almost identical average levels at AT and TP, whereas at BT the levels were much higher. Average variability of the three subsequent NOT measurements was the highest at BT, whereas at AT and TP the average variability was lower and nearly identical.

  4. Review of the High Performance Antiproton Trap (HiPAT) Experiment at the Marshall Space Flight Center

    Science.gov (United States)

    Pearson, J. B.; Sims, Herb; Martin, James; Chakrabarti, Suman; Lewis, Raymond; Fant, Wallace

    2003-01-01

    The significant energy density of matter-antimatter annihilation is attractive to the designers of future space propulsion systems, with the potential to offer a highly compact source of power. Many propulsion concepts exist that could take advantage of matter-antimatter reactions, and current antiproton production rates are sufficient to support basic proof-of-principle evaluation of technology associated with antimatter- derived propulsion. One enabling technology for such experiments is portable storage of low energy antiprotons, allowing antiprotons to be trapped, stored, and transported for use at an experimental facility. To address this need, the Marshall Space Flight Center's Propulsion Research Center is developing a storage system referred to as the High Performance Antiproton Trap (HiPAT) with a design goal of containing 10(exp 12) particles for up to 18 days. The HiPAT makes use of an electromagnetic system (Penning- Malmberg design) consisting of a 4 Telsa superconductor, high voltage electrode structure, radio frequency (RF) network, and ultra high vacuum system. To evaluate the system normal matter sources (both electron guns and ion sources) are used to generate charged particles. The electron beams ionize gas within the trapping region producing ions in situ, whereas the ion sources produce the particles external to the trapping region and required dynamic capture. A wide range of experiments has been performed examining factors such as ion storage lifetimes, effect of RF energy on storage lifetime, and ability to routinely perform dynamic ion capture. Current efforts have been focused on improving the FW rotating wall system to permit longer storage times and non-destructive diagnostics of stored ions. Typical particle detection is performed by extracting trapped ions from HiPAT and destructively colliding them with a micro-channel plate detector (providing number and energy information). This improved RF system has been used to detect various

  5. Challenging the standard model by high-precision comparisons of the fundamental properties of protons and antiprotons

    Science.gov (United States)

    Ulmer, S.; Mooser, A.; Nagahama, H.; Sellner, S.; Smorra, C.

    2018-03-01

    The BASE collaboration investigates the fundamental properties of protons and antiprotons, such as charge-to-mass ratios and magnetic moments, using advanced cryogenic Penning trap systems. In recent years, we performed the most precise measurement of the magnetic moments of both the proton and the antiproton, and conducted the most precise comparison of the proton-to-antiproton charge-to-mass ratio. In addition, we have set the most stringent constraint on directly measured antiproton lifetime, based on a unique reservoir trap technique. Our matter/antimatter comparison experiments provide stringent tests of the fundamental charge-parity-time invariance, which is one of the fundamental symmetries of the standard model of particle physics. This article reviews the recent achievements of BASE and gives an outlook to our physics programme in the ELENA era. This article is part of the Theo Murphy meeting issue `Antiproton physics in the ELENA era'.

  6. Challenging the standard model by high-precision comparisons of the fundamental properties of protons and antiprotons.

    Science.gov (United States)

    Ulmer, S; Mooser, A; Nagahama, H; Sellner, S; Smorra, C

    2018-03-28

    The BASE collaboration investigates the fundamental properties of protons and antiprotons, such as charge-to-mass ratios and magnetic moments, using advanced cryogenic Penning trap systems. In recent years, we performed the most precise measurement of the magnetic moments of both the proton and the antiproton, and conducted the most precise comparison of the proton-to-antiproton charge-to-mass ratio. In addition, we have set the most stringent constraint on directly measured antiproton lifetime, based on a unique reservoir trap technique. Our matter/antimatter comparison experiments provide stringent tests of the fundamental charge-parity-time invariance, which is one of the fundamental symmetries of the standard model of particle physics. This article reviews the recent achievements of BASE and gives an outlook to our physics programme in the ELENA era.This article is part of the Theo Murphy meeting issue 'Antiproton physics in the ELENA era'. © 2018 The Authors.

  7. Magnetic monopole search with the MoEDAL test trapping detector

    Directory of Open Access Journals (Sweden)

    Katre Akshay

    2016-01-01

    Full Text Available IMoEDAL is designed to search for monopoles produced in high-energy Large Hadron Collider (LHC collisions, based on two complementary techniques: nucleartrack detectors for high-ionisation signatures and other highly ionising avatars of new physics, and trapping volumes for direct magnetic charge measurements with a superconducting magnetometer. The MoEDAL test trapping detector array deployed in 2012, consisting of over 600 aluminium samples, was analysed and found to be consistent with zero trapped magnetic charge. Stopping acceptances are obtained from a simulation of monopole propagation in matter for a range of charges and masses, allowing to set modelindependent and model-dependent limits on monopole production cross sections. Multiples of the fundamental Dirac magnetic charge are probed for the first time at the LHC.

  8. Magnetic monopole search with the MoEDAL test trapping detector

    Science.gov (United States)

    Katre, Akshay

    2016-11-01

    IMoEDAL is designed to search for monopoles produced in high-energy Large Hadron Collider (LHC) collisions, based on two complementary techniques: nucleartrack detectors for high-ionisation signatures and other highly ionising avatars of new physics, and trapping volumes for direct magnetic charge measurements with a superconducting magnetometer. The MoEDAL test trapping detector array deployed in 2012, consisting of over 600 aluminium samples, was analysed and found to be consistent with zero trapped magnetic charge. Stopping acceptances are obtained from a simulation of monopole propagation in matter for a range of charges and masses, allowing to set modelindependent and model-dependent limits on monopole production cross sections. Multiples of the fundamental Dirac magnetic charge are probed for the first time at the LHC.

  9. Measurements of β - ν angular correlations using a transparent Paul trap

    International Nuclear Information System (INIS)

    Ban, G.; Delahaye, P.; Le Brun, Ch.; Lienard, E.; Mauger, F.; Naviliat-Cuncic, O.; Szerypo, J.; Tamain, B.

    1999-06-01

    The potentiality to search for physics beyond the Standard Model by means of precision measurements of β - ν angular correlations in nuclear β-decay is discussed. The possibility to reveal unexpected time reversal invariant tensor type contributions is investigated and the pure Gamow-Teller decay of 6 He is considered as a possible candidate. A new experimental method is proposed which is based on the use of a transparent Paul trap surrounded by detectors to directly record β-ion coincidences in an event-by-event mode. The experiment requires intense beams of radioactive nuclei like those which will become available at the Low Energy Facility near SPIRAL at GANIL. Such beams should preferably be efficiently cooled and bunched prior to their injection into the Paul trap. Estimates of the transmission figure required for the cooling and bunching system and of the measuring time to achieve a first step are presented. (author)

  10. New experiment to gain unparalleled insight into antimatter

    CERN Multimedia

    Katarina Anthony

    2013-01-01

    At last week’s Research Board meeting, the Baryon Antibaryon Symmetry Experiment (BASE) was approved for installation at CERN. The experiment will be diving into the search for matter-antimatter asymmetry, as it aims to take ultra-high precision measurements of the antiproton magnetic moment.   CERN's AD Hall: the new home of the BASE double Penning trap set-up. The BASE collaboration will be setting up shop in the AD Hall this September with its first CERN-based experimental set-up. Using the novel double-Penning trap set-up developed at the University of Mainz, GSI Darmstadt and the Max Plank Institute for Nuclear Physics (Germany), the BASE team will be able to measure the antiproton magnetic moment with hitherto unreachable part-per-billion precision. “We constructed the first double-Penning trap at our companion facility in Germany, and made the first ever direct observations of single spin flips of a single proton,” explains Stefan Ulmer from RIKE...

  11. Fundamental physics in particle traps

    International Nuclear Information System (INIS)

    Quint, Wolfgang; Vogel, Manuel

    2014-01-01

    The individual topics are covered by leading experts in the respective fields of research. Provides readers with present theory and experiments in this field. A useful reference for researchers. This volume provides detailed insight into the field of precision spectroscopy and fundamental physics with particles confined in traps. It comprises experiments with electrons and positrons, protons and antiprotons, antimatter and highly charged ions, together with corresponding theoretical background. Such investigations represent stringent tests of quantum electrodynamics and the Standard model, antiparticle and antimatter research, test of fundamental symmetries, constants, and their possible variations with time and space. They are key to various aspects within metrology such as mass measurements and time standards, as well as promising to further developments in quantum information processing. The reader obtains a valuable source of information suited for beginners and experts with an interest in fundamental studies using particle traps.

  12. Determination of vanillin, ethyl vanillin, and coumarin in infant formula by liquid chromatography-quadrupole linear ion trap mass spectrometry.

    Science.gov (United States)

    Shen, Yan; Han, Chao; Liu, Bin; Lin, Zhengfeng; Zhou, Xiujin; Wang, Chengjun; Zhu, Zhenou

    2014-02-01

    A simple, precise, accurate, and validated liquid chromatography-quadrupole linear ion trap mass spectrometry method was developed for the determination of vanillin, ethyl vanillin, and coumarin in infant formula samples. Following ultrasonic extraction with methanol/water (1:1, vol/vol), and clean-up on an HLB solid-phase extraction cartridge (Waters Corp., Milford, MA), samples were separated on a Waters XSelect HSS T3 column (150 × 2.1-mm i.d., 5-μm film thickness; Waters Corp.), with 0.1% formic acid solution-acetonitrile as mobile phase at a flow rate of 0.25 mL/min. Quantification of the target was performed by the internal standard approach, using isotopically labeled compounds for each chemical group, to correct matrix effects. Data acquisition was carried out in multiple reaction monitoring transitions mode, monitoring 2 multiple reaction monitoring transitions to ensure an accurate identification of target compounds in the samples. Additional identification and confirmation of target compounds were performed using the enhanced product ion modus of the linear ion trap. The novel liquid chromatography-quadrupole linear ion trap mass spectrometry platform offers the best sensitivity and specificity for characterization and quantitative determination of vanillin, ethyl vanillin, and coumarin in infant formula and fulfills the quality criteria for routine laboratory application. Copyright © 2014 American Dairy Science Association. Published by Elsevier Inc. All rights reserved.

  13. An ex situ evaluation of TBA- and MTBE-baited bio-traps.

    Science.gov (United States)

    North, Katharine P; Mackay, Douglas M; Annable, Michael D; Sublette, Kerry L; Davis, Greg; Holland, Reef B; Petersen, Daniel; Scow, Kate M

    2012-08-01

    Aquifer microbial communities can be investigated using Bio-traps(®) ("bio-traps"), passive samplers containing Bio-Sep(®) beads ("bio-beads") that are deployed in monitoring wells to be colonized by bacteria delivered via groundwater flow through the well. When bio-beads are "baited" with organic contaminants enriched in (13)C, stable isotope probing allows assessment of the composition and activity of the microbial community. This study used an ex situ system fed by groundwater continuously extracted from an adjacent monitoring well within an experimentally-created aerobic zone treating a tert-butyl alcohol (TBA) plume. The goal was to evaluate aspects of bio-trap performance that cannot be studied quantitatively in situ. The measured groundwater flow through a bio-trap housing suggests that such traps might typically "sample" about 1.8 L per month. The desorption of TBA or methyl tert-butyl ether (MTBE) bait from bio-traps during a typical deployment duration of 6 weeks was approximately 90% and 45%, respectively, of the total initial bait load, with initially high rate of mass loss that decreased markedly after a few days. The concentration of TBA in groundwater flowing by the TBA-baited bio-beads was estimated to be as high as 3400 mg/L during the first few days, which would be expected to inhibit growth of TBA-degrading microbes. Initial inhibition was also implied for the MTBE-baited bio-trap, but at lower concentrations and for a shorter time. After a few days, concentrations in groundwater flowing through the bio-traps dropped below inhibitory concentrations but remained 4-5 orders of magnitude higher than TBA or MTBE concentrations within the aquifer at the experimental site. Desorption from the bio-beads during ex situ deployment occurred at first as predicted by prior sorption analyses of bio-beads but with apparent hysteresis thereafter, possibly due to mass transfer limitations caused by colonizing microbes. These results suggest that TBA- or MTBE

  14. Digital assist: A comparison of two note-taking methods (traditional vs. digital pen) for students with emotional behavioral disorders

    Science.gov (United States)

    Rody, Carlotta A.

    High school biology classes traditionally follow a lecture format to disseminate content and new terminology. With the inclusive practices of No Child Left Behind, the Common Core State Standards, and end-of-course exam requirement for high school diplomas, classes include a large range of achievement levels and abilities. Teachers assume, often incorrectly, that students come to class prepared to listen and take notes. In a standard diploma, high school biology class in a separate school for students with emotional and behavioral disorders, five students participated in a single-subject, alternating treatment design study that compared the use of regular pens and digital pens to take notes during 21 lecture sessions. Behavior measures were threefold between the two interventions: (a) quantity of notes taken per minute during lectures, (b) quantity of notes or notations taken during review pauses, and (c) percent of correct responses on the daily comprehension quizzes. The study's data indicated that two students were inclined to take more lecture notes when using the digital pen. Two students took more notes with the regular pen. One student demonstrated no difference in her performance with either pen type. Both female students took more notes per minute, on average, than the three males regardless of pen type. During the review pause, three of the five students only added notes or notations to their notes when using the regular pen. The remaining two students did not add to their notes. Quiz scores differed in favor of the regular pen. All five participants earned higher scores on quizzes given during regular pen sessions. However, the differences were minor, and recommendations are made for specific training in note-taking, the pause strategy, and digital pen fluency which may produce different results for both note-taking and quiz scores.

  15. Effects of lignite application on ammonia and nitrous oxide emissions from cattle pens

    Energy Technology Data Exchange (ETDEWEB)

    Sun, Jianlei, E-mail: su@unimelb.edu.au [Faculty of Veterinary and Agricultural Sciences, The University of Melbourne, VIC 3010 (Australia); Bai, Mei [Faculty of Veterinary and Agricultural Sciences, The University of Melbourne, VIC 3010 (Australia); Shen, Jianlin [Institute of Subtropical Agriculture, Chinese Academy of Sciences, Changsha 410125 (China); Griffith, David W.T. [Department of Chemistry, University of Wollongong, NSW 2522 (Australia); Denmead, Owen T. [Faculty of Veterinary and Agricultural Sciences, The University of Melbourne, VIC 3010 (Australia); Hill, Julian [Ternes Agricultural Consulting Pty Ltd, Upwey, VIC 3158 (Australia); Lam, Shu Kee; Mosier, Arvin R. [Faculty of Veterinary and Agricultural Sciences, The University of Melbourne, VIC 3010 (Australia); Chen, Deli, E-mail: delichen@unimelb.edu.au [Faculty of Veterinary and Agricultural Sciences, The University of Melbourne, VIC 3010 (Australia)

    2016-09-15

    Beef cattle feedlots are a major source of ammonia (NH{sub 3}) emissions from livestock industries. We investigated the effects of lignite surface applications on NH{sub 3} and nitrous oxide (N{sub 2}O) emissions from beef cattle feedlot pens. Two rates of lignite, 3 and 6 kg m{sup −2}, were tested in the treatment pen. No lignite was applied in the control pen. Twenty-four Black Angus steers were fed identical commercial rations in each pen. We measured NH{sub 3} and N{sub 2}O concentrations continuously from 4th Sep to 13th Nov 2014 using Quantum Cascade Laser (QCL) NH{sub 3} analysers and a closed-path Fourier Transform Infrared Spectroscopy analyser (CP-FTIR) in conjunction with the integrated horizontal flux method to calculate NH{sub 3} and N{sub 2}O fluxes. During the feeding period, 16 and 26% of the excreted nitrogen (N) (240 g N head{sup −1} day{sup −1}) was lost via NH{sub 3} volatilization from the control pen, while lignite application decreased NH{sub 3} volatilization to 12 and 18% of the excreted N, for Phase 1 and Phase 2, respectively. Compared to the control pen, lignite application decreased NH{sub 3} emissions by approximately 30%. Nitrous oxide emissions from the cattle pens were small, 0.10 and 0.14 g N{sub 2}O-N head{sup −1} day{sup −1} (< 0.1% of excreted N) for the control pen, for Phase 1 and Phase 2, respectively. Lignite application increased direct N{sub 2}O emissions by 40 and 57%, to 0.14 and 0.22 g N{sub 2}O-N head{sup −1} day{sup −1}, for Phase 1 and Phase 2, respectively. The increase in N{sub 2}O emissions resulting from lignite application was counteracted by the lower indirect N{sub 2}O emission due to decreased NH{sub 3} volatilization. Using 1% as a default emission factor of deposited NH{sub 3} for indirect N{sub 2}O emissions, the application of lignite decreased total N{sub 2}O emissions. - Graphical abstract: Lignite application substantially decreased NH{sub 3} emissions from cattle feedlots and increased

  16. Photoacoustic measurements of photokinetics in single optically trapped aerosol droplets

    Science.gov (United States)

    Covert, Paul; Cremer, Johannes; Signorell, Ruth; Thaler, Klemens; Haisch, Christoph

    2017-04-01

    It is well established that interaction of light with atmospheric aerosols has a large impact on the Earth's climate. However, uncertainties in the magnitude of this impact remain large, due in part to broad distributions of aerosol size, composition, and chemical reactivity. In this context, photoacoustic spectroscopy is commonly used to measure light absorption by aerosols. Here, we present photoacoustic measurements of single, optically-trapped nanodroplets to reveal droplet size-depencies of photochemical and physical processes. Theoretical considerations have pointed to a size-dependence in the magnitude and phase of the photoacoustic response from aerosol droplets. This dependence is thought to originate from heat transfer processes that are slow compared to the acoustic excitation frequency. In the case of a model aerosol, our measurements of single particle absorption cross-section versus droplet size confirm these theoretical predictions. In a related study, using the same model aerosol, we also demonstrate a droplet size-dependence of photochemical reaction rates [1]. Within sub-micron sized particles, photolysis rates were observed to be an order of magnitude greater than those observed in larger droplets. [1] J. W. Cremer, K. M. Thaler, C. Haisch, and R. Signorell. Photoacoustics of single laser-trapped nanodroplets for the direct observation of nanofocusing in aerosol photokinetics. Nat. Commun., 7:10941, 2016.

  17. Counter-Propagating Optical Trapping System for Size and Refractive Index Measurement of Microparticles

    National Research Council Canada - National Science Library

    Flynn, Richard A; Shao, Bing; Chachisvilis, Mirianas; Ozkan, Mihrimah; Esener, Sadik C

    2005-01-01

    .... Different from the current best technique for microparticles refractive index measurement, refractometry, a bulk technique requiring changing the fluid composition of the sample, our optical trap...

  18. Tilting-Twisting-Rolling: a pen-based technique for compass geometric construction

    Institute of Scientific and Technical Information of China (English)

    Fei LYU; Feng TIAN; Guozhong DAI; Hongan WANG

    2017-01-01

    This paper presents a new pen-based technique,Tilting-Twisting-Rolling,to support compass geometric construction.By leveraging the 3D orientation information and 3D rotation information of a pen,this technique allows smooth pen action to complete multi-step geometric construction without switching task states.Results from a user study show this Tilting-Twisting-Rolling technique can improve user performance and user experience in compass geometric construction.

  19. Direct Analysis of Organic Compounds in Liquid Using a Miniature Photoionization Ion Trap Mass Spectrometer with Pulsed Carrier-Gas Capillary Inlet.

    Science.gov (United States)

    Lu, Xinqiong; Yu, Quan; Zhang, Qian; Ni, Kai; Qian, Xiang; Tang, Fei; Wang, Xiaohao

    2017-08-01

    A miniature ion trap mass spectrometer with capillary direct sampling and vacuum ultraviolet photoionization source was developed to conduct trace analysis of organic compounds in liquids. Self-aspiration sampling is available where the samples are drawn into the vacuum chamber through a capillary with an extremely low flow rate (less than 1 μL/min), which minimizes sample consumption in each analysis to tens of micrograms. A pulsed gas-assisted inlet was designed and optimized to promote sample transmission in the tube and facilitate the cooling of ions, thereby improving instrument sensitivity. A limit of detection of 2 ppb could be achieved for 2,4-dimethylaniline in a methanol solution. The sampling system described in the present study is specifically suitable for a miniature photoionization ion trap mass spectrometer that can perform rapid and online analysis for liquid samples. Graphical Abstract ᅟ.

  20. Penning transfer in argon-based gas mixtures

    CERN Document Server

    Sahin, O; Tapan, I; Ozmutlu, E N

    2010-01-01

    Penning transfers, a group of processes by which excitation energy is used to ionise the gas, increase the gas gain in some detectors. Both the probability that such transfers occur and the mechanism by which the transfer takes place, vary with the gas composition and pressure. With a view to developing a microscopic electron transport model that takes Penning transfers into account, we use this dependence to identify the transfer mechanisms at play. We do this for a number of argon-based gas mixtures, using gain curves from the literature.

  1. Theoretical study of the mode of the mass-selective nonstable axial output ions from the nonlinear trap

    International Nuclear Information System (INIS)

    Sudakov, M.Yu.

    2000-01-01

    One studied theoretically the mode of mass-selective unstable output of ions from three-dimensional quadrupole ion trap. One developed a method represent coordinates of ions per one period of supplying HF voltage with regard to nonlinear distortions of quadrupole potential. One derived equation for an envelope of ion oscillations in the form of motion equation of mass point in the efficient force field. One explained the effect of output delay of ions at presence of the field negative even harmonics. One proved that the positive even distortions of quadrupole potential favored realization of that mode and studied the dynamics of ions in the course of output [ru

  2. Human factors engineering and design validation for the redesigned follitropin alfa pen injection device.

    Science.gov (United States)

    Mahony, Mary C; Patterson, Patricia; Hayward, Brooke; North, Robert; Green, Dawne

    2015-05-01

    To demonstrate, using human factors engineering (HFE), that a redesigned, pre-filled, ready-to-use, pre-asembled follitropin alfa pen can be used to administer prescribed follitropin alfa doses safely and accurately. A failure modes and effects analysis identified hazards and harms potentially caused by use errors; risk-control measures were implemented to ensure acceptable device use risk management. Participants were women with infertility, their significant others, and fertility nurse (FN) professionals. Preliminary testing included 'Instructions for Use' (IFU) and pre-validation studies. Validation studies used simulated injections in a representative use environment; participants received prior training on pen use. User performance in preliminary testing led to IFU revisions and a change to outer needle cap design to mitigate needle stick potential. In the first validation study (49 users, 343 simulated injections), in the FN group, one observed critical use error resulted in a device design modification and another in an IFU change. A second validation study tested the mitigation strategies; previously reported use errors were not repeated. Through an iterative process involving a series of studies, modifications were made to the pen design and IFU. Simulated-use testing demonstrated that the redesigned pen can be used to administer follitropin alfa effectively and safely.

  3. Active stabilization of ion trap radiofrequency potentials

    Energy Technology Data Exchange (ETDEWEB)

    Johnson, K. G.; Wong-Campos, J. D.; Restelli, A.; Landsman, K. A.; Neyenhuis, B.; Mizrahi, J.; Monroe, C. [Joint Quantum Institute and University of Maryland Department of Physics, College Park, Maryland 20742 (United States)

    2016-05-15

    We actively stabilize the harmonic oscillation frequency of a laser-cooled atomic ion confined in a radiofrequency (rf) Paul trap by sampling and rectifying the high voltage rf applied to the trap electrodes. We are able to stabilize the 1 MHz atomic oscillation frequency to be better than 10 Hz or 10 ppm. This represents a suppression of ambient noise on the rf circuit by 34 dB. This technique could impact the sensitivity of ion trap mass spectrometry and the fidelity of quantum operations in ion trap quantum information applications.

  4. Laser induced fluorescence of trapped molecular ions

    Energy Technology Data Exchange (ETDEWEB)

    Grieman, F.J.

    1979-10-01

    An experimental apparatus for obtaining the optical spectra of molecular ions is described. The experimental technique includes the use of three dimensional ion trapping, laser induced fluorescence, and gated photon counting methods. The ions, which are produced by electron impact, are confined in a radio-frequency quadrupole ion trap of cylindrical design. Because the quadrupole ion trap allows mass selection of the molecular ion desired for study, the analysis of the spectra obtained is greatly simplified. The ion trap also confines the ions to a region easily probed by a laser beam. 18 references.

  5. Laser induced fluorescence of trapped molecular ions

    International Nuclear Information System (INIS)

    Grieman, F.J.

    1979-10-01

    An experimental apparatus for obtaining the optical spectra of molecular ions is described. The experimental technique includes the use of three dimensional ion trapping, laser induced fluorescence, and gated photon counting methods. The ions, which are produced by electron impact, are confined in a radio-frequency quadrupole ion trap of cylindrical design. Because the quadrupole ion trap allows mass selection of the molecular ion desired for study, the analysis of the spectra obtained is greatly simplified. The ion trap also confines the ions to a region easily probed by a laser beam. 18 references

  6. An ex situ evaluation of TBA- and MTBE-baited bio-traps

    Science.gov (United States)

    North, Katharine P.; Mackay, Douglas M.; Annable, Michael D.; Sublette, Kerry L.; Davis, Greg; Holland, Reef B.; Petersen, Daniel; Scow, Kate M.

    2013-01-01

    Aquifer microbial communities can be investigated using Bio-traps® (“bio-traps”), passive samplers containing Bio-Sep® beads (“bio-beads”) that are deployed in monitoring wells to be colonized by bacteria delivered via groundwater flow through the well. When bio-beads are “baited” with organic contaminants enriched in 13C, stable isotope probing allows assessment of the composition and activity of the microbial community. This study used an ex situ system fed by groundwater continuously extracted from an adjacent monitoring well within an experimentally-created aerobic zone treating a tert-butyl alcohol (TBA) plume. The goal was to evaluate aspects of bio-trap performance that cannot be studied quantitatively in situ. The measured groundwater flow through a bio-trap housing suggests that such traps might typically “sample” about 1.8 L per month. The desorption of TBA or methyl tert-butyl ether (MTBE) bait from bio-traps during a typical deployment duration of 6 weeks was approximately 90% and 45%, respectively, of the total initial bait load, with initially high rate of mass loss that decreased markedly after a few days. The concentration of TBA in groundwater flowing by the TBA-baited bio-beads was estimated to be as high as 3400 mg/L during the first few days, which would be expected to inhibit growth of TBA-degrading microbes. Initial inhibition was also implied for the MTBE-baited bio-trap, but at lower concentrations and for a shorter time. After a few days, concentrations in groundwater flowing through the bio-traps dropped below inhibitory concentrations but remained 4–5 orders of magnitude higher than TBA or MTBE concentrations within the aquifer at the experimental site. Desorption from the bio-beads during ex situ deployment occurred at first as predicted by prior sorption analyses of bio-beads but with apparent hysteresis thereafter, possibly due to mass transfer limitations caused by colonizing microbes. These results suggest that

  7. Lithogenic fluxes to the deep Arabian Sea measurEd. by sediment traps

    Digital Repository Service at National Institute of Oceanography (India)

    Ramaswamy, V.; Nair, R.R; Manganini, S.J.; Haake, B.; Ittekkot, V.

    . 38. No. 2. pp 1~g-\\[~44 It,lqt. fllC~g...4)i49tql $31~) 4- 0.till Pnnted m Great Britain. ~ lg~t Pergamon Press pie Lithogenic fluxes to the deep Arabian Sea measured by sediment traps V. RAMASWAMY,* R. R. NAIR,* S. MANGANINI,# B. HAAKE~. and V... (MIct, lrdAN et al., 1984). Most of the present suspended sediment discharge is in July and August, during the peak of the southwest monsoon period, with negligible discharge during other times (I'rrEKKO'r and ARAIN, 1986). The Narmada and Tapti...

  8. Q value of the superallowed decay of 22Mg and the calibration of the 21Na(p,γ) experiment

    International Nuclear Information System (INIS)

    Savard, G.; Clark, J.A.; Wang, J.C.; Buchinger, F.; Crawford, J.E.; Gulick, S.; Lee, J.K.P.; Hardy, J.C.; Iacob, V.E.; Hecht, A.A.; Levand, A.F.; Lundgren, B.F.; Scielzo, N.D.; Tanihata, I.; Trimble, W.; Zhou, Z.; Sharma, K.S.; Wang, Y.; Towner, I.S.

    2004-01-01

    The masses of the radioactive nuclei 22 Mg and 22 Na have been measured with the Canadian Penning trap on-line mass spectrometer to a precision of 3x10 -8 and 1x10 -8 , respectively. A Q EC value of 4124.39(73) keV for the superallowed β decay of 22 Mg is obtained from the difference of these two masses. With this precise Q value, the Ft value for this decay is determined with improved precision and is found to be consistent with the existing precision data set of superallowed Fermi emitters. This provides an important test of the isospin symmetry-breaking corrections. If the mass of 22 Mg determined here is used in the calibration of a recent 21 Na(p,γ) 22 Mg measurement, part of the discrepancy observed in that measurement is removed

  9. Accurate absolute measurement of trapped Cs atoms in a MOT

    International Nuclear Information System (INIS)

    Talavera O, M.; Lopez R, M.; Carlos L, E. de; Jimenez S, S.

    2007-01-01

    A Cs-133 Magneto-Optical Trap (MOT) has been developed at the Time and Frequency Division of the Centro Nacional de Metrologia, CENAM, in Mexico. This MOT is part of a primary frequency standard based on ultra-cold Cs atoms, called CsF-1 clock, under development at CENAM. In this Cs MOT, we use the standard configuration (σ + - σ - ) 4-horizontal 2-vertical laser beams 1.9 cm in diameter, with 5 mW each. We use a 852 nm, 5 mW, DBR laser as a master laser which is stabilized by saturation spectroscopy. Emission linewidth of the master laser is l MHz. In order to amplify the light of the master laser, a 50 mW, 852 nm AlGaAs laser is used as slave laser. This slave laser is stabilized by light injection technique. A 12 MHz red shift of the light is performed by two double passes through two Acusto-Optic Modulators (AOMs). The optical part of the CENAMs MOT is very robust against mechanical vibration, acoustic noise and temperature changes in our laboratory, because none of our diode lasers use an extended cavity to reduce the linewidth. In this paper, we report results of our MOT characterization as a function of several operation parameters such as the intensity of laser beams, the laser beam diameter, the red shift of light, and the gradient of the magnetic field. We also report accurate absolute measurement of the number of Cs atoms trapped in our Cs MOT. We found up to 6 x 10 7 Cs atoms trapped in our MOT measured with an uncertainty no greater than 6.4%. (Author)

  10. Compensation and trapping in CdZnTe radiation detectors studied by thermoelectric emission spectroscopy, thermally stimulated conductivity, and current-voltage measurements

    International Nuclear Information System (INIS)

    James, Ralph B.

    2000-01-01

    In today's commercially available counter-select-grade CdZnTe crystals for radiation detector applications, the thermal ionization energies of the traps and their types, whether electron or hole traps, were measured. The measurements were successfully done using thermoelectric emission spectroscopy (TEES) and thermally stimulated conductivity (TSC). For reliability, the electrical contacts to the sample were found to be very important and, instead of Au Schottky contacts, In Ohmic contacts had to be used. For the filling of the traps, photoexcitation was done at zero bias, at 20K and at wavelengths which gave the maximum bulk photoexcitation for the sample. Between the temperature range from 20 to 400 K, the TSC current was found to be on the order of ∼ 10,000 times or even larger than the TEES current, in agreement with theory, but only TEES could resolve the trap type and was sensitive to the deep traps. Large concentration of hole traps at 0.1 and 0.6 eV were observed and smaller contraction of electron traps at 0.4 eV was seen. These deep traps cause compensation in the material and also cause trapping that degrades the radiation detection measurement

  11. Ultracold molecules for the masses: Evaporative cooling and magneto-optical trapping

    Science.gov (United States)

    Stuhl, B. K.

    While cold molecule experiments are rapidly moving towards their promised benefits of precision spectroscopy, controllable chemistry, and novel condensed phases, heretofore the field has been greatly limited by a lack of methods to cool and compress chemically diverse species to temperatures below ten millikelvin. While in atomic physics these needs are fulfilled by laser cooling, magneto-optical trapping, and evaporative cooling, until now none of these techniques have been applicable to molecules. In this thesis, two major breakthroughs are reported. The first is the observation of evaporative cooling in magnetically trapped hydroxyl (OH) radicals, which potentially opens a path all the way to Bose-Einstein condensation of dipolar radicals, as well as allowing cold- and ultracold-chemistry studies of fundamental reaction mechanisms. Through the combination of an extremely high gradient magnetic quadrupole trap and the use of the OH Λ-doublet transition to enable highly selective forced evaporation, cooling by an order of magnitude in temperature was achieved and yielded a final temperature no higher than 5mK. The second breakthrough is the successful application of laser cooling and magneto-optical trapping to molecules. Motivated by a proposal in this thesis, laser cooling of molecules is now known to be technically feasible in a select but substantial pool of diatomic molecules. The demonstration of not only Doppler cooling but also two-dimensional magneto-optical trapping in yttrium (II) oxide, YO, is expected to enable rapid growth in the availability of ultracold molecules—just as the invention of the atomic magneto-optical trap stimulated atomic physics twenty-five years ago.

  12. Comparative measurements of plasma potential with ball-pen and Langmuir probe in low-temperature magnetized plasma

    International Nuclear Information System (INIS)

    Zanáška, M.; Kudrna, P.; Tichý, M.; Adámek, J.; Peterka, M.

    2015-01-01

    The ball-pen probe (BPP) is used for direct plasma potential measurements in magnetized plasma. The probe can adjust the ratio of the electron and ion saturation currents I sat − /I sat + to be close to one and therefore its I-V characteristic becomes nearly symmetric. If this is achieved, the floating potential of the BPP is close to the plasma potential. Because of its rather simple construction, it offers an attractive probe for measurements in magnetized plasma. Comparative measurements of plasma potential by BPPs of different dimensions as well as one Langmuir probe (LP) in an argon discharge plasma of a cylindrical magnetron were performed at various experimental conditions. An additional comparison by an emissive probe was also performed. All these types of probes provide similar values of plasma potential in a wide range of plasma parameters. Our results for three different BPP dimensions indicate that the BPP can be operated in a cylindrical magnetron DC argon discharge if the value of the ratio of the magnetic field and neutral gas pressure, B/p, is greater than approximately 10 mT/Pa

  13. Comparative measurements of plasma potential with ball-pen and Langmuir probe in low-temperature magnetized plasma

    Energy Technology Data Exchange (ETDEWEB)

    Zanáška, M.; Kudrna, P.; Tichý, M. [Faculty of Mathematics and Physics, Charles University in Prague, Ke Karlovu 3, 12116 Prague 2 (Czech Republic); Adámek, J. [Institute of Plasma Physics AS CR, v.v.i., Za Slovankou 3, 18200 Prague 8 (Czech Republic); Peterka, M. [Faculty of Mathematics and Physics, Charles University in Prague, Ke Karlovu 3, 12116 Prague 2 (Czech Republic); Institute of Plasma Physics AS CR, v.v.i., Za Slovankou 3, 18200 Prague 8 (Czech Republic)

    2015-03-15

    The ball-pen probe (BPP) is used for direct plasma potential measurements in magnetized plasma. The probe can adjust the ratio of the electron and ion saturation currents I{sub sat}{sup −}/I{sub sat}{sup +} to be close to one and therefore its I-V characteristic becomes nearly symmetric. If this is achieved, the floating potential of the BPP is close to the plasma potential. Because of its rather simple construction, it offers an attractive probe for measurements in magnetized plasma. Comparative measurements of plasma potential by BPPs of different dimensions as well as one Langmuir probe (LP) in an argon discharge plasma of a cylindrical magnetron were performed at various experimental conditions. An additional comparison by an emissive probe was also performed. All these types of probes provide similar values of plasma potential in a wide range of plasma parameters. Our results for three different BPP dimensions indicate that the BPP can be operated in a cylindrical magnetron DC argon discharge if the value of the ratio of the magnetic field and neutral gas pressure, B/p, is greater than approximately 10 mT/Pa.

  14. Some mass measurement problems

    International Nuclear Information System (INIS)

    Merritt, J.S.

    1976-01-01

    Concerning the problem of determining the thickness of a target, an uncomplicated approach is to measure its mass and area and take the quotient. This paper examines the mass measurement aspect of such an approach. (author)

  15. Performance of the linear ion trap Orbitrap mass analyzer for qualitative and quantitative analysis of drugs of abuse and relevant metabolites in sewage water.

    Science.gov (United States)

    Bijlsma, Lubertus; Emke, Erik; Hernández, Félix; de Voogt, Pim

    2013-03-20

    This work illustrates the potential of liquid chromatography coupled to a hybrid linear ion trap Fourier Transform Orbitrap mass spectrometer for the simultaneous identification and quantification of 24 drugs of abuse and relevant metabolites in sewage water. The developed methodology consisted of automatic solid-phase extraction using Oasis HLB cartridges, chromatographic separation of the targeted drugs, full-scan accurate mass data acquisition under positive electrospray ionization mode over an m/z range of 50-600Da at a resolution of 30,000 FWHM and simultaneous MS(n) measurements to obtain information of fragment ions generated in the linear ion trap. Accurate mass of the protonated molecule, together with at least one nominal mass product ion and retention time allowed the confident identification of the compounds detected in these complex matrices. In addition to the highly reliable qualitative analysis, Orbitrap analyzer also proved to have satisfactory potential for quantification at sub-ppb analyte levels, a possibility that has been very little explored in the literature until now. The limits of quantification ranged from 4 to 68ngL(-1) in influent sewage water, and from 2 to 35ngL(-1) in effluent, with the exception of MDA, morphine and THC that presented higher values as a consequence of the high ionization suppression in this type of samples. Satisfactory recoveries (70-120%) and precision (abuse could be identified and quantified, mainly MDMA, benzoylecgonine, codeine, oxazepam and temazepam. Orbitrap also showed potential for retrospective investigation of ketamine metabolites in the samples without the need of additional analysis. Copyright © 2013 Elsevier B.V. All rights reserved.

  16. Ball-Pen Probe Measurements in L-Mode and H-Mode on ASDEX Upgrade

    Czech Academy of Sciences Publication Activity Database

    Adámek, Jiří; Horáček, Jan; Müller, H. W.; Rohde, V.; Ionita, C.; Schrittwieser, R.; Mehlmann, F.; Kurzan, B.; Stöckel, Jan; Dejarnac, Renaud; Weinzettl, Vladimír; Seidl, Jakub; Peterka, M.

    2010-01-01

    Roč. 50, č. 9 (2010), s. 854-859 ISSN 0863-1042. [International Workshop on Electric Probes in Magnetized Plasmas/8th./. Innsbruck, 21.09.2009-24.09.2009] R&D Projects: GA AV ČR KJB100430901; GA ČR GA202/09/1467 Institutional research plan: CEZ:AV0Z20430508 Keywords : Tokamak * ball- pen probe * electron temperature * L-mode * H-mode * ELMs Subject RIV: BL - Plasma and Gas Discharge Physics Impact factor: 1.006, year: 2010 http://onlinelibrary.wiley.com/doi/10.1002/ctpp.201010145/pdf

  17. Technical note: whole-pen assessments of nutrient excretion and digestibility from dairy replacement heifers housed in sand-bedded freestalls.

    Science.gov (United States)

    Coblentz, W K; Hoffman, P C; Esser, N M; Bertram, M G

    2013-10-01

    Our objectives were to describe and test refined procedures for quantifying excreta produced from whole pens of dairy heifers. Previous research efforts attempting to make whole-pen measurements of excreta output have been complicated by the use of organic bedding, which requires cumbersome analytical techniques to quantify excreta apart from the bedding. Research pens equipped with sand-bedded freestalls offer a unique opportunity for refinement of whole-pen fecal collection methods, primarily because sand-bedded freestall systems contain no organic bedding; therefore, concentrations of ash within the manure, sand, and feces can be used to correct for contamination of manure by sand bedding. This study was conducted on a subset of heifers from a larger production-scale feeding trial evaluating ensiled eastern gamagrass [Tripsacum dactyloides (L.) L.] haylage (EGG) that was incorporated into a corn silage/alfalfa haylage-based blended diet at rates of 0, 9.1, 18.3, or 27.4% of total DM. The diet without EGG also was offered on a limit-fed basis. Eighty Holstein dairy heifers were blocked (heavy weight, 424 ± 15.9 kg; light weight, 324 ± 22.4 kg) and then assigned to 10 individual pens containing 8 heifers/pen. One pen per block was assigned to each of the 5 research diets, and whole-pen fecal collections were conducted twice for each pen. Grab fecal samples also were gathered from individual heifers within each pen, and subsequent analysis of these whole-pen composites allowed reasonable estimates of OM and NDF excreta output. Under the conditions of our experimental design, pooled SEM for the excreta DM, OM, NDF, and NDF (ash corrected) output were 0.113, 0.085, 0.093, and 0.075 kg·heifer(-1)·d(-1), respectively. For DM excretion, this represented about one-third of the SEM reported for previous whole-pen collections from bedded-pack housing systems. Subsequent calculations of apparent DM and OM digestibilities indicated that the technique was sensitive, and

  18. Towards trapped antihydrogen

    CERN Document Server

    Jorgensen, L V; Bertsche, W; Boston, A; Bowe, P D; Cesar, C L; Chapman, S; Charlton, M; Fajans, J; Fujiwara, M C; Funakoshi, R; Gill, D R; Hangst, J S; Hayano, R S; Hydomako, R; Jenkins, M J; Kurchaninov, L; Madsen, N; Nolan, P; Olchanski, K; Olin, A; Page, R D; Povilus, A; Robicheaux, F; Sarid, E; Silveira, D M; Storey, J W; Thompson, R I; van der Werf, D P; Wurtele, J S; Yamazaki, Y

    2008-01-01

    Substantial progress has been made in the last few years in the nascent field of antihydrogen physics. The next big step forward is expected to be the trapping of the formed antihydrogen atoms using a magnetic multipole trap. ALPHA is a new international project that started to take data in 2006 at CERN’s Antiproton Decelerator facility. The primary goal of ALPHA is stable trapping of cold antihydrogen atoms to facilitate measurements of its properties. We discuss the status of the ALPHA project and the prospects for antihydrogen trapping.

  19. Measurement of radical scavenging activity of irradiated Kampo extracts using ESR spin-trap method

    International Nuclear Information System (INIS)

    Ohta, Yui; Kawamura, Shoei; Ukai, Mitsuko; Nakamura, Hideo; Kikuchi, Masahiro; Kobayashi, Yasuhiko

    2014-01-01

    The radical scavenging activity (RSA) of 13 kinds of γ-ray irradiated Kampo extracts were studied by ESR spin-trap method. The RSA against alkoxy radical and hydroxyl radical were measured using new spin trapping reagent CYPMPO. The RSA against these two radicals were evaluated using GSH for alkoxy RSA and L-ascorbic acid for hydroxy RSA as a standard antioxidant reagent. We revealed that a few Kampo extracts showed high RSA against alkoxy radical and also hydroxy radical. This RSA of Kampo extracts was changed by γ-ray irradiation treatment. Using ESR spin-trap method, it is concluded that the effect of radiation treatment on RSA of Kampo extracts were able to detect. (author)

  20. Thermoregulation of the bovine scrotum 1: measurements of free-range animals in a paddock and pen

    Science.gov (United States)

    Wallage, Andrea L.; Johnston, S. D.; Lisle, A. T.; Beard, L.; Lees, A. M.; Collins, C. W.; Gaughan, J. B.

    2017-08-01

    The bull's scrotum and scrotal cord vasculature has traditionally been regarded as a thermoregulatory device for maintaining optimal testicular temperature for normal spermatogenesis. This assumption has mostly been derived from discrete measurements using thermocouples with limited data correlating continuous scrotal temperature (ST) to body temperature (BT). From mid-summer to early autumn, four Wagyu bulls (9-18 months) were surgically implanted with two data loggers (DL) logging at 30 min intervals: one on the right hand side flank and the other was attached to the visceral vaginal tunic of the mid-testis. Bulls were firstly housed in a paddock (PK) for 13 days and then moved to individual pens (IP), again for 13 days. Repeated measures analysis modelled the long-term and diurnal trends in BT and ST. While both day and time of day (TOD) were significant effects for ST at both housing locations ( P behavioural changes. Reporting concurrent and continuous BT and ST will allow further investigation into factors influencing bovine ST and should be useful in selecting bulls with high degrees of thermoregulation capacity.

  1. A Quantum Non-Demolition Parity measurement in a mixed-species trapped-ion quantum processor

    Science.gov (United States)

    Marinelli, Matteo; Negnevitsky, Vlad; Lo, Hsiang-Yu; Flühmann, Christa; Mehta, Karan; Home, Jonathan

    2017-04-01

    Quantum non-demolition measurements of multi-qubit systems are an important tool in quantum information processing, in particular for syndrome extraction in quantum error correction. We have recently demonstrated a protocol for quantum non-demolition measurement of the parity of two beryllium ions by detection of a co-trapped calcium ion. The measurement requires a sequence of quantum gates between the three ions, using mixed-species gates between beryllium hyperfine qubits and a calcium optical qubit. Our work takes place in a multi-zone segmented trap setup in which we have demonstrated high fidelity control of both species and multi-well ion shuttling. The advantage of using two species of ion is that we can individually manipulate and read out the state of each ion species without disturbing the internal state of the other. The methods demonstrated here can be used for quantum error correcting codes as well as quantum metrology and are key ingredients for realizing a hybrid universal quantum computer based on trapped ions. Mixed-species control may also enable the investigation of new avenues in quantum simulation and quantum state control. left the group and working in a company now.

  2. RESEARCHES REGARDING THE MAIN REPRODUCTION INDICATORS DETERMINATED IN SOWS, STAND GESTATION PEN TIPE

    Directory of Open Access Journals (Sweden)

    RAMONA UNTARU

    2007-05-01

    Full Text Available Current researches were carried out with the goal to quantisize the lost from the weaning to early gestation at the sows housed in open pen gestation. In this trail we tested two pen types, different not only by size, but also by feeders’ emplacement. The main reproduction indicators that we calculated until the 28 gestation day were the proportion of sows in heat after weaning, the weaning to estrus interval and the gestation rates. The weaning to estrus interval was about 4 to 7 days, most sows were in heat in the day 5 and 6 days after weaning. The percent of heat detection after weaning was 71.42% for the small pens and 70.71% for the big pens (differences statistically non significant, chi test value was 0.983. The gestation rate at 28 days after insemination was 91.62% for the small pens and 94.72% for the large pens (chi test value 0,959, statistically non significant differences. The overpopulation for heat induction and after that chipping animals together in those pens, show that the lost are up to 40.47%, between weaning – day 28 of gestation.

  3. Cryogenic surface ion traps

    International Nuclear Information System (INIS)

    Niedermayr, M.

    2015-01-01

    Microfabricated surface traps are a promising architecture to realize a scalable quantum computer based on trapped ions. In principle, hundreds or thousands of surface traps can be located on a single substrate in order to provide large arrays of interacting ions. To this end, trap designs and fabrication methods are required that provide scalable, stable and reproducible ion traps. This work presents a novel surface-trap design developed for cryogenic applications. Intrinsic silicon is used as the substrate material of the traps. The well-developed microfabrication and structuring methods of silicon are utilized to create simple and reproducible traps. The traps were tested and characterized in a cryogenic setup. Ions could be trapped and their life time and motional heating were investigated. Long ion lifetimes of several hours were observed and the measured heating rates were reproducibly low at around 1 phonon per second at a trap frequency of 1 MHz. (author) [de

  4. Global nickel anomaly links Siberian Traps eruptions and the latest Permian mass extinction.

    Science.gov (United States)

    Rampino, Michael R; Rodriguez, Sedelia; Baransky, Eva; Cai, Yue

    2017-09-29

    Anomalous peaks of nickel abundance have been reported in Permian-Triassic boundary sections in China, Israel, Eastern Europe, Spitzbergen, and the Austrian Carnic Alps. New solution ICP-MS results of enhanced nickel from P-T boundary sections in Hungary, Japan, and Spiti, India suggest that the nickel anomalies at the end of the Permian were a worldwide phenomenon. We propose that the source of the nickel anomalies at the P-T boundary were Ni-rich volatiles released by the Siberian volcanism, and by coeval Ni-rich magma intrusions. The peaks in nickel abundance correlate with negative δ 13 C and δ 18 O anomalies, suggesting that explosive reactions between magma and coal during the Siberian flood-basalt eruptions released large amounts of CO 2 and CH 4 into the atmosphere, causing severe global warming and subsequent mass extinction. The nickel anomalies may provide a timeline in P-T boundary sections, and the timing of the peaks supports the Siberian Traps as a contributor to the latest Permian mass extinction.

  5. Dynamic-compliance and viscosity of PET and PEN

    International Nuclear Information System (INIS)

    Weick, Brian L.

    2016-01-01

    Complex dynamic-compliance and in-phase dynamic-viscosity data are presented and analyzed for PET and PEN advanced polyester substrates used for magnetic tapes. Frequency-temperature superposition is used to predict long-term behavior. Temperature and frequency ranges for the primary glass transition and secondary transitions are discussed and compared for PET and PEN. Shift factors from frequency-temperature superposition are used to determine activation energies for the transitions, and WLF parameters are determined for the polyester substrates.

  6. Dynamic-compliance and viscosity of PET and PEN

    Energy Technology Data Exchange (ETDEWEB)

    Weick, Brian L. [School of Engineering and Computer Science, University of the Pacific, Stockton, California, 95211 (United States)

    2016-05-18

    Complex dynamic-compliance and in-phase dynamic-viscosity data are presented and analyzed for PET and PEN advanced polyester substrates used for magnetic tapes. Frequency-temperature superposition is used to predict long-term behavior. Temperature and frequency ranges for the primary glass transition and secondary transitions are discussed and compared for PET and PEN. Shift factors from frequency-temperature superposition are used to determine activation energies for the transitions, and WLF parameters are determined for the polyester substrates.

  7. Dynamic-compliance and viscosity of PET and PEN

    Science.gov (United States)

    Weick, Brian L.

    2016-05-01

    Complex dynamic-compliance and in-phase dynamic-viscosity data are presented and analyzed for PET and PEN advanced polyester substrates used for magnetic tapes. Frequency-temperature superposition is used to predict long-term behavior. Temperature and frequency ranges for the primary glass transition and secondary transitions are discussed and compared for PET and PEN. Shift factors from frequency-temperature superposition are used to determine activation energies for the transitions, and WLF parameters are determined for the polyester substrates.

  8. Spin polarized atom traps and fundamental symmetries

    International Nuclear Information System (INIS)

    Haeusser, O.

    1994-10-01

    Plans are described to couple a neutral atom trap to an upgraded version of TRIUMF's TISOL on-line mass separator. The unique properties of trapped and cooled atoms promise improvements of some symmetry tests of the Standard Model of the electroweak and strong interactions. (author). 33 refs., 3 figs

  9. Analysis of iodinated quorum sensing peptides by LC–UV/ESI ion trap mass spectrometry

    Directory of Open Access Journals (Sweden)

    Yorick Janssens

    2018-02-01

    Full Text Available Five different quorum sensing peptides (QSP were iodinated using different iodination techniques. These iodinated peptides were analyzed using a C18 reversed phase HPLC system, applying a linear gradient of water and acetonitrile containing 0.1% (m/v formic acid as mobile phase. Electrospray ionization (ESI ion trap mass spectrometry was used for the identification of the modified peptides, while semi-quantification was performed using total ion current (TIC spectra. Non-iodinated peptides and mono- and di-iodinated peptides (NIP, MIP and DIP respectively were well separated and eluted in that order. Depending on the used iodination method, iodination yields varied from low (2% to high (57%.

  10. Development of the Pirani and penning vacuum gauges

    International Nuclear Information System (INIS)

    Oh, B. H.; In, S. R.; Yoon, B. J.; Yoon, J. S.

    2000-02-01

    The Pirani and penning gauges developed during this study had made good characteristics compared with the measured results of customized other gauges, and this results show the possibility of developing the gauges by ourselves in Korea. In order to make a competition with the customized gauges of other countries, it is necessary to upgrade several points to have good characteristics over the large range of the pressure. The new efforts will be made in developing the full scale gauge in the next year. (author)

  11. Effect of radiative trapping on measurement of the spectroscopic properties of Yb sup 3 sup + :phosphate glasses

    CERN Document Server

    Dai Shi Xun; Wen Lei; Hu Li Li; Jiang Zhong Hon

    2003-01-01

    The effect of radiative trapping on measurement of the spectroscopic properties of Yb sup 3 sup + -doped phosphate glasses was investigated as a function of Yb sup 3 sup + concentration at different thicknesses. It was found that radiative trapping exists generally in Yb sup 3 sup + :phosphate glasses, even at low concentration. As a result, the measured lifetime of Yb sup 3 sup + in phosphate glasses is usually larger than the calculated one. The maximum discrepancies between them at high concentration are found to be <42%. The calculated lifetime should be used as a reference in determining the true value of the measured lifetime because of it being lengthened largely by radiative trapping. On the other hand, the shape of fluorescence spectrum exhibits remarkable changes due to the radiative trapping. What is more, the intensity increase of DELTA lambda sub e sub f sub f at high concentration is greater than that of low doping. The DELTA lambda sub e sub f sub f increases 36% from 53 to 72 nm with thickn...

  12. The magnetic moments of the proton and the antiproton

    CERN Document Server

    Ulmer, S.; Blaum, K.; Braeuninger, S.; Franke, K.; Kracke, H.; Leiteritz, C.; Matsuda, Y.; Nagahama, H.; Ospelkaus, C.; Rodegheri, C.C.; Quint, W.; Schneider, G.; Smorra, C.; Van Gorp, S.; Walz, J.; Yamazaki, Y.

    2014-01-01

    Recent exciting progress in the preparation and manipulation of the motional quantum states of a single trapped proton enabled the first direct detection of the particle's spin state. Based on this success the proton magnetic moment $\\mu_p$ was measured with ppm precision in a Penning trap with a superimposed magnetic field inhomogeneity. An improvement by an additional factor of 1000 in precision is possible by application of the so-called double Penning trap technique. In a recent paper we reported the first demonstration of this method with a single trapped proton, which is a major step towards the first direct high-precision measurement of $\\mu_p$. The techniques required for the proton can be directly applied to measure the antiproton magnetic moment $\\mu_{\\bar{p}}$. An improvement in precision of $\\mu_{\\bar{p}}$ by more than three orders of magnitude becomes possible, which will provide one of the most sensitive tests of CPT invariance. To achieve this research goal we are currently setting up the Baryo...

  13. Black-Hole Mass Measurements

    DEFF Research Database (Denmark)

    Vestergaard, Marianne

    2004-01-01

    The applicability and apparent uncertainties of the techniques currently available for measuring or estimating black-hole masses in AGNs are briefly summarized.......The applicability and apparent uncertainties of the techniques currently available for measuring or estimating black-hole masses in AGNs are briefly summarized....

  14. Influence of lucite phantoms on calibration of dosimetric pens

    International Nuclear Information System (INIS)

    Oliveira, E.C.; Xavier, M.; Caldas, L.E.V.

    1992-01-01

    Dosimetrical pens were studied for the answer repetition and were tested in gamma radiation fields ( 60 Co and 137 Cs) in air and in front of a lucite phantom, obtaining a backscattering contribution. The medium backscattering factors were 1,053 and 1,108 for respectively 60 Co and 137 Cs. The pens were placed behind the phantom for verifying the radiation attenuation. (C.G.C.)

  15. Pulsed laser manipulation of an optically trapped bead: Averaging thermal noise and measuring the pulsed force amplitude

    DEFF Research Database (Denmark)

    Lindballe, Thue Bjerring; Kristensen, Martin V. G.; Keiding, Søren Rud

    2013-01-01

    An experimental strategy for post-eliminating thermal noise on position measurements of optically trapped particles is presented. Using a nanosecond pulsed laser, synchronized to the detection system, to exert a periodic driving force on an optically trapped 10 polystyrene bead, the laser pulse-bead...... interaction is repeated hundreds of times. Traces with the bead position following the prompt displacement from equilibrium, induced by each laser pulse, are averaged and reveal the underlying deterministic motion of the bead, which is not visible in a single trace due to thermal noise. The motion of the bead...... is analyzed from the direct time-dependent position measurements and from the power spectrum. The results show that the bead is on average displaced 208 nm from the trap center and exposed to a force amplitude of 71 nanoNewton, more than five orders of magnitude larger than the trapping forces. Our...

  16. Production and properties of the heaviest elements. Status and perspectives

    International Nuclear Information System (INIS)

    Backe, H.; Hebberger, F.P.; Sewtz, M.; Turler, A.

    2007-01-01

    This article reviews the following topics which were discussed at the Workshop on the Atomic Properties of the Heaviest Elements held from September 25-27, 2006 in Chiemsee, Germany: (i) the recent progress in the production of the heaviest elements, the investigation of their nuclear structure, and prospects for direct mass measurements in Penning traps; (ii) recent studies of their chemical properties with the aid of volatile species and single-atom aqueous-phase chemistry; (iii) the current status and future prospects for the investigation of atomic and ionic properties such as optical spectroscopy in gas cells and ion traps, including fully relativistic calculations of the atomic level structure with predictions for the element nobelium; and (iv) ionic charge radii measurements in buffer gas filled drift cells, and ion chemical reactions in the gas phase. (authors)

  17. Investigation of two-frequency Paul traps for antihydrogen production

    Energy Technology Data Exchange (ETDEWEB)

    Leefer, Nathan; Krimmel, Kai, E-mail: kkrimmel@students.uni-mainz.de [Helmholtz-Institut Mainz (Germany); Bertsche, William [University of Manchester (United Kingdom); Budker, Dmitry [Helmholtz-Institut Mainz (Germany); Fajans, Joel [University of California at Berkeley, Department of Physics (United States); Folman, Ron [Ben-Gurion University of the Negev, Department of Physics (Israel); Häffner, Hartmut [University of California at Berkeley, Department of Physics (United States); Schmidt-Kaler, Ferdinand [Helmholtz-Institut Mainz (Germany)

    2017-11-15

    Radio-frequency (rf) Paul traps operated with multifrequency rf trapping potentials provide the ability to independently confine charged particle species with widely different charge-to-mass ratios. In particular, these traps may find use in the field of antihydrogen recombination, allowing antiproton and positron clouds to be trapped and confined in the same volume without the use of large superconducting magnets. We explore the stability regions of two-frequency Paul traps and perform numerical simulations of small samples of multispecies charged-particle mixtures of up to twelve particles that indicate the promise of these traps for antihydrogen recombination.

  18. Characteristics of Handwriting of People With Cerebellar Ataxia: Three-Dimensional Movement Analysis of the Pen Tip, Finger, and Wrist.

    Science.gov (United States)

    Fujisawa, Yuhki; Okajima, Yasutomo

    2015-11-01

    There are several functional tests for evaluating manual performance; however, quantitative manual tests for ataxia, especially those for evaluating handwriting, are limited. This study aimed to investigate the characteristics of cerebellar ataxia by analyzing handwriting, with a special emphasis on correlation between the movement of the pen tip and the movement of the finger or wrist. This was an observational study. Eleven people who were right-handed and had cerebellar ataxia and 17 people to serve as controls were recruited. The Scale for the Assessment and Rating of Ataxia was used to grade the severity of ataxia. Handwriting movements of both hands were analyzed. The time required for writing a character, the variability of individual handwriting, and the correlation between the movement of the pen tip and the movement of the finger or wrist were evaluated for participants with ataxia and control participants. The writing time was longer and the velocity profile and shape of the track of movement of the pen tip were more variable in participants with ataxia than in control participants. For participants with ataxia, the direction of movement of the pen tip deviated more from that of the finger or wrist, and the shape of the track of movement of the pen tip differed more from that of the finger or wrist. The severity of upper extremity ataxia measured with the Scale for the Assessment and Rating of Ataxia was mostly correlated with the variability parameters. Furthermore, it was correlated with the directional deviation of the trajectory of movement of the pen tip from that of the finger and with increased dissimilarity of the shapes of the tracks. The results may have been influenced by the scale and parameters used to measure movement. Ataxic handwriting with increased movement noise is characterized by irregular pen tip movements unconstrained by the finger or wrist. The severity of ataxia is correlated with these unconstrained movements. © 2015 American

  19. Phase II Practice-based Evidence in Nutrition (PEN) evaluation: interviews with key informants.

    Science.gov (United States)

    Bowden, Fran Martin; Lordly, Daphne; Thirsk, Jayne; Corby, Lynda

    2012-01-01

    Dietitians of Canada has collaborated with experts in knowledge translation and transfer, technology, and dietetic practice to develop and implement an innovative online decision-support system called Practice-based Evidence in Nutrition (PEN). A study was conducted to evaluate the perceived facilitators and barriers that enable dietitians to use or prevent them from using PEN. As part of the overall evaluation framework of PEN, a qualitative descriptive research design was used to address the research purpose. Individual, semi-structured telephone interviews with 17 key informants were completed, and the interview transcripts underwent qualitative content analysis. Respondents identified several facilitators of and barriers to PEN use. Facilitators included specificity to dietetics, rigorous/expert review, easy accessibility, current content, credible/secure material, well-organized/easy-to-use material, material that is valuable to practice, and good value for money. Barriers included perceived high cost, fee structuring/cost to students, certain organizational aspects, and a perceived lack of training for pathway contributors. This formative evaluation has indicated areas in which PEN could be improved and strategies to make PEN the standard for dietetic education and practice. Ensuring that PEN is meeting users' knowledge needs is of the utmost importance if dietitians are to remain on the cutting edge of scientific inquiry.

  20. Counter-Propagating Optical Trapping System for Size and Refractive Index Measurement of Microparticles

    National Research Council Canada - National Science Library

    Flynn, Richard A; Shao, Bing; Chachisvilis, Mirianas; Ozkan, Mihrimah; Esener, Sadik C

    2005-01-01

    We propose and demonstrate a novel approach to measure the size and refractive index of microparticles based on two beam optical trapping, where forward scattered light is detected to give information about the particle...