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Sample records for particle-induced x-ray emission analysis

  1. Qualitative analysis of a powdered diamond sample by particle induced X-ray emission (PIXE)

    International Nuclear Information System (INIS)

    Mabida, C.; Annegarn, H.J.; Renan, M.J.; Sellschop, J.P.F.

    The main purpose of this analysis was to determine whether nickel is present in diamond powder as a trace element. Particle induced X-ray emission (PIXE) showed unambiguously that nickel was present. Due to the convenience of PIXE in multielemental analysis, the investigations also include a number of other trace elements in the sample

  2. Particle induced X-ray emission for quantitative trace-element analysis using the Eindhoven cyclotron

    International Nuclear Information System (INIS)

    Kivits, H.

    1980-01-01

    Development of a multi-elemental trace analysis technique using PIXE (Particle Induced X-ray Emission), was started almost five years ago at the Eindhoven University of Technology, in the Cyclotron Applications Group of the Physics Department. The aim of the work presented is to improve the quantitative aspects of trace-element analysis with PIXE, as well as versatility, speed and simplicity. (Auth.)

  3. Particle induced X-ray emission

    International Nuclear Information System (INIS)

    Cohen, D.D.

    1991-08-01

    The accelerator based ion beam technique of Particle Induced X-ray Emission (PIXE) is discussed in some detail. This report pulls together all major reviews and references over the last ten years and reports on PIXE in vacuum and using external beams. The advantages, limitations, costs and types of studies that may be undertaken using an accelerator based ion beam technique such as PIXE, are also discussed. 25 refs., 7 tabs., 40 figs

  4. Particle induced X-ray emission: a valuable tool for the analysis of metalpoint drawings

    International Nuclear Information System (INIS)

    Duval, A.; Guicharnaud, H.; Dran, J.C.

    2004-01-01

    For several years, we carry out a research on metalpoint drawings, a graphic technique mainly employed by European artists during the 15th and 16th centuries. As a non-destructive and very sensitive analytical technique is required, particle induced X-ray emission (PIXE) analysis with an external beam has been used for this purpose. More than 70 artworks drawn by Italian, Flemish and German artists have been analysed, including leadpoint and silverpoint drawings. Following a short description of the metalpoint technique, the results are compared with the recipes written by Cennino Cennini at the beginning of the 15th century and specific examples are presented

  5. Determination of impurities in silicon nitride by particle induced x-ray emission analysis

    International Nuclear Information System (INIS)

    Miyagawa, Yoshiko; Saito, Kazuo; Niwa, Hiroaki; Ishizuka, Toshio; Miyagawa, Soji

    1985-01-01

    A method is presented for quantitative particle induced X-ray emission (PIXE) analysis of impurities in the thick samples of silicon nitride. In the analysis of ceramic materials such as silicon nitride, chemical treatments are required to prepare thin enough samples. However, the chemical treatments are undesirable for the PIXE analysis, because another complications are brought about. Our method does not need any chemical treatments and thick samples can be subjected to the measurements. The determination of impurities were made by on-line use of a personal computer in which standard X-ray intensity data were stored. The method and procedures are as follows: After subtracting a buckground spectrum from an observed PIXE spectrum, the resultant peaks are assigned to individual elements. Then, in order to determine the contents of the impurities, the intensity of each peak is compared with a Gaussian curve which is generated from the standard X-ray intensity data. The latter data were determined theoretically. The results were in satisfactory agreement with those obtained by ICP emission spectrometry. (author)

  6. Forensic analysis of tempered sheet glass by particle induced X-ray emission (PIXE)

    Energy Technology Data Exchange (ETDEWEB)

    Jisonna, L.J. [Department of Chemistry and Department of Physics, Hope College, Holland, MI 49422-9000 (United States); DeYoung, P.A., E-mail: deyoung@hope.ed [Department of Chemistry and Department of Physics, Hope College, Holland, MI 49422-9000 (United States); Ferens, J.; Hall, C.; Lunderberg, J.M.; Mears, P. [Department of Chemistry and Department of Physics, Hope College, Holland, MI 49422-9000 (United States); Padilla, D. [Department of Physics, San Diego State University, San Diego, CA 92182-1233 (United States); Peaslee, G.F. [Department of Chemistry and Department of Physics, Hope College, Holland, MI 49422-9000 (United States); Sampson, R. [Department of Physics, Columbia University, New York, NY 10027 (United States)

    2011-05-15

    Highlights: {yields} PIXE was found to give the same results for trace elements in glass as ICP. {yields} PIXE can non-destructively determine trace element concentrations in auto glass. {yields} Measured Ca, Fe, Ti, Mn, and Sr in auto glass with PIXE. -- Abstract: The elemental concentrations of five trace elements in tempered sheet glass fragments were determined using particle-induced X-ray emission (PIXE) spectrometry. The trace element concentrations for calcium, iron, manganese, strontium, and titanium are compared to those obtained by inductively-coupled plasma-atomic emission spectrometry (ICP-AES) following complete digestion by hydrofluoric acid. For these five elements, the absolute concentrations obtained by both methods are shown to agree well over a wide range of concentrations. The limits of detection for trace elements are typically lower for the ICP-AES method. However, we show that the concentrations of these five elements can be accurately measured by the PIXE method. Since PIXE is an entirely non-destructive method, there exists a niche for this technique to be used as a complement to the more sensitive ICP-AES technique in the forensic analysis of sheet glass.

  7. Applications of particle induced X-ray emission analysis to ambient aerosol studies

    International Nuclear Information System (INIS)

    Lannefors, H.

    1982-01-01

    The characteristics of Particle Induced X-ray Emission (PIXE) analysis in conjunction with different ambient aerosol samplers have been studied. Correction factors have been calculated for homogeneous and inhomogeneous rural and urban aerosol samples. The Nuclepore two stage filter sampler provided the most useful combination of the resolution and particle size fractionation in urban, rural and remote environments. The PIXE-analysis technique in combination with different samplers was employed in aerosol composition studies in rural and remote environments. Particular emphasis was laid on studies of aerosol long range transport. Based on air mass trajectory analysis and aerosol composition measurements the foreign contribution in southern Sweden was estimated to be 70 - 80% for S and Pb but only 30 - 50% for V and Ni. The spatial and temporal extension of a long range transport episode was studied using high time resolution continuous filter samplers in a network in southern Sweden. The variation in the concentration levels of sulphur agreed well with changes in the air mass history. Arctic summer elemental concentration levels as measured during the Swedish YMER-80 icebreaker expedition were typically one order of magnitude lower than Arctic winter levels. The combination of chemical information, optical properties and size distribution data supports the hypothesis of long range transport of air pollution into the Arctic especially during the winter. This takes place during the winter season because the Polar front is further south making conditions for long range transport up to the Arctic more favourable. (Auth.)

  8. Development of a PIXE (Particle Induced X-ray Emission) analysis device using an extracted proton beam

    International Nuclear Information System (INIS)

    Saidi, A.

    1989-01-01

    The experimental device described allows the extention of the PIXE (Particle Induced X-ray Emission) method to the analysis, by means of proton beams, of solid or liquid samples, which can not be analyzed under vacuum conditions. The homogeneity of the surfaces to be analysed and elements (in the atmosphere) which absorb X-rays must be taken into account. Liquid samples do not need special care. The results show that: at high energies, the extracted beam sensibility is of the same order of magnitude as those obtained under vacuum; at low energies, the performance under vacuum conditions is better. The particles energy losses, at the exit membrane and in the outer atmosphere, decrease the X-rays production efficiency [fr

  9. Applications of particle induced X-ray emission

    International Nuclear Information System (INIS)

    Akselsson, K. R.

    1978-01-01

    In Particle Induced X-ray Emission (PIXE) analysis samples are bombarded by protons or α-particles of a few MeV/u. The induced characteristic x-rays are detected with a x-ray detector e.g. a Si(Li)-detector. The energies of the x-ray peaks are characteristic for the elements in the samples and the intensities of the x-ray transitions are proportional to the abundances of the elements. The research area which first attracted those of us working with PIXE was the study of sources, transport and deposition of airborne particulates. Sources, transport, wet deposition, other applications where PIXE is already known to be competitive are trace elemental analysis of water below the ppb-level and analyses requiring a space resolution of 1-10μ. However, there is still much to do for physicists in developing the full potential of low-energy accelerators as analytical tools in multidisciplinary teams. (JIW)

  10. Material analysis with the aid of particle induced X-ray emission

    International Nuclear Information System (INIS)

    Stadler, E.

    1984-12-01

    Material analysis are discussed on the basis of PIXE and Rutherford scattering spectroscopy. Various problems including cross-section changes, energy changes, count rate and deadtime, background, escape peaks and perturbations and overlap are discussed in relation to PIXE, while the influence of the energy loss of the projectile, the mass of the projectile, the cinematic factor, projectile energy, the scattering angle and the solid angle are discussed in terms of Rutherford scattering spectroscopy. X-ray production theory and x-ray detectors are also briefly discussed. The effect of elastically scattered protons on the energy resolution of the x-ray detector is discussed. The application of PIXE and Rutherford scattering spectroscopy to the analysis of air particle samples, and to the determination of the efficiency of the filters used for the collection of air-particle samples is also discussed

  11. Particle-induced X-ray emission: thick-target analysis of inorganic materials in the determination of light elements

    International Nuclear Information System (INIS)

    Perez-Arantegui, J.; Castillo, J.R.; Querre, G.

    1994-01-01

    Particle-induced X-ray emission (PIXE) has been applied to the analysis of inorganic materials to determine some elements with Z < 27: Na, Mg, Al, Si, K, Ca, Ti, Mn and Fe, in thick-target analysis. A PIXE method has been developed for the analysis of geological materials, ceramics and pottery. Work has been carried out with an ion beam analytical system, using a low particle beam energy. Relative sensitivity, detection limits, reproducibility and accuracy of the method were calculated based on the analysis of geological standard materials (river sediments, argillaceous limestone, basalt, diorite and granite). Analysis using PIXE offers a number of advantages, such as short analysis time, multi-elemental and nondestructive determinations, and the results are similar to those obtained with other instrumental techniques of analysis. (Author)

  12. Statistics associated with an elemental analysis system of particles induced by X-ray emission

    International Nuclear Information System (INIS)

    Romo K, C.M.

    1987-01-01

    In the quantitative elemental analysis by X-ray techniques one has to use data spectra which present fluctuations of statistical nature both from the energy and from the number of counts accumulated. While processing the results for the obtainment of a quantitative result, a detailed knowledge of the associated statistics distributions is needed. In this work, l) the statistics associated with the system photon's counting as well as 2) the distribution of the results as a function of the energy are analyzed. The first one is important for the definition of the expected values and uncertainties and for the spectra simulation (Mukoyama, 1975). The second one is fundamental for the determination of the contribution for each spectral line. (M.R.) [es

  13. Trace metal analysis in sea grasses from Mexican Caribbean Coast by particle induced X-ray emission (PIXE)

    International Nuclear Information System (INIS)

    Solis, C.; Issac O, K.; Martinez, A.; Lavoisier, E.; Martinez, M. A.

    2008-01-01

    The growing urban and tourist activity in the Mexican Caribbean coasts has resulted in an increase of chemical substances, metals in particular, discharged to the coastal waters. In order to reach an adequate management and conservation of these marine ecosystems it is necessary to perform an inventory of the actual conditions that reflect the vulnerability and the level of damage. Sea-grasses are considered good biological indicators of heavy metal contamination in marine systems. The goal of this preliminary work is to evaluate the concentrations of trace metals such as Cr, Mn, Fe, Co, Cu, Zn, and Pb in Thalassia testudinum, a very common sea-grass in the Mexican Caribbean Sea. Samples were collected from several locations in the coasts of the Yucatan Peninsula: Holbox, Blanquizal and Punta Allen, areas virtually uninfluenced by anthropogenic activities. Trace elements in different part plants were determined by particle induced X-ray emission (PIXE). This is a very suitable technique since it offers a fast, accurate and multi-element analysis. Also, the analysis by PIXE can be performed directly on powdered leaves without a laborious sample preparation. The trace metal concentration determined in sea-grasses growing in Caribbean generally fall in the range of the lowest valuables reported for sea grasses from the Gulf of Mexico. The results indicate that the studied areas do not present contamination by heavy metals. (Author)

  14. Elemental analysis of gold coins by particle induced X-ray emission (PIXE)

    International Nuclear Information System (INIS)

    Ferreira, G.P.; Gil, F.B.

    1981-01-01

    A Van de Graaff accelerator of 2 MeV energy was used for quantitative analysis of gold coins of the eighteenth and nineteenth centuries by the PIXE method. The results reproduce well the known legal title of the coins. However, for confirmation, a small set of Au-Ag-Cu and Au-Cu standards was also analysed. Again, the known composition of the standards was reasonably reproduced. In this way the authors think that the PIXE method is quite adequate for absolutely non-destructive analysis of gold alloy artifacts with no need of standards. (author)

  15. Element analysis of the eutardigrades Richtersius coronifer and Milnesium cf. asiaticum using Particle Induced X-ray Emission (PIXE

    Directory of Open Access Journals (Sweden)

    Charlotta Nilsson

    2013-05-01

    Full Text Available Semi-terrestrial tardigrades are well-known for their tolerance to a variety of environmental extremes, including desiccation, freezing and radiation. Despite several attempts to reveal the genetic and molecular mechanisms behind the resilience of tardigrades, it is still unknown how these animals are able to maintain the integrity of their cellular components under severe stress. Quantitative or qualitative changes in molecular compounds (e.g., carbohydrates, proteins are expected, and have been the main line of research towards understanding the tolerance of tardigrades. In radiation tolerant bacteria, a tolerance mechanism based on manganese has been proposed. We evaluate this hypothesis in tardigrades and provide the first data on element composition in desiccated and non-desiccated specimens of two eutardigrade species, Richtersius coronifer and Milnesium cf. asiaticum. A focused 2 MeV proton microbeam was utilised to determine the elemental content, distributions and concentrations, using the ion beam analytical technique particle induced X-ray emission (PIXE. The presence of six elements – phosphorus, sulphur, chlorine, potassium, calcium and iron – were confirmed in all tardigrade specimens, at levels up to a few mg g–1. However, manganese was found in less than 10% of the analysed specimens, and in low amounts, thus our study provides no evidence for the manganese hypothesis. We also show that the distributions and/or concentrations of some elements differ between the two species as well as between the dehydrated and hydrated state. In particular, very low levels of iron were found in dehydrated M. cf. asiaticum. Our analysis shows that the PIXE technique is a useful tool for investigating questions on the distribution of elements both in dehydrated and hydrated tardigrades.

  16. Characterization of nuclear physics targets using Rutherford backscattering and particle induced X-ray emission

    International Nuclear Information System (INIS)

    Rubehn, T.; Wozniak, G.J.; Phair, L.; Moretto, L.G.; Yu, K.M.

    1997-01-01

    Rutherford backscattering and particle induced X-ray emission have been utilized to precisely characterize targets used in nuclear fission experiments. The method allows for a fast and non-destructive determination of target thickness, homogeneity and element composition. (orig.)

  17. Trace element analysis in geochemistry using a nuclear microprobe. Ionoluminescence and particle induced X-ray emission

    International Nuclear Information System (INIS)

    Homman, P.

    1994-01-01

    In PIXE analysis of geological specimens based on X-ray detection with Si(Li) detectors, effects of detector tailing, pulse pileup, and gamma-ray production are pronounced. In this work the tailing effect has been addressed through characterization of the response function of a Si(Li) detector using an absorber technique. The pileup interval, in the pulse forming electronics of a PIXE detection system, has been improved to 100 ns X-ray energies above 8 keV by means of pulse shape analysis. Pulses due to tailing effects were also isolated but no major improvement was obtained. A means of reducing the increased background in the PIXE spectrum due to Compton scattering of high energetic gamma-rays in the Si(Li) crystal has been investigated by installation of an anti-Compton shield consisting of an organic scintillator mounted inside the detector cryostat and read out by a photomultiplier. Ionoluminescence, a new analytical technique for the nuclear microprobe, has shown to be a technique that can be employed as a fast diagnostic tool in imaging applications. The technique is based on analysis of the light that often can be observed when an ion beam impinges on a geological specimen. This light, luminescence, can often be associated with impurities in the crystal lattice or other structural defects. It can therefore be employed for revealing some chemical information about the specimens in contradiction to PIXE which is rather insensitive to chemical variations. The potential of the method is demonstrated and discussed both as an imaging tool and for spectroscopic studies. 19 refs, 10 figs

  18. Particle induced X-ray emission and complementary nuclear methods for trace element determination; Plenary lecture

    Energy Technology Data Exchange (ETDEWEB)

    Johansson, S A.E. [Lund Univ. (Sweden). Dept. of Nuclear Physics

    1992-03-01

    In this review the state-of-the-art of particle induced X-ray emission (PIXE) methods for the determination of trace elements is described. The developmental work has mostly been carried out in nuclear physics laboratories, where accelerators are available, but now the increased interest has led to the establishment of other dedicated PIXE facilities. The reason for this interest is the versatility, high sensitivity and multi-element capability of PIXE analysis. A further very important advantage is that PIXE can be combined with the microbeam technique, which makes elemental mapping with a spatial resolution of about 1 {mu}m possible. As a technique, PIXE can also be combined with other nuclear reactions such as elastic scattering and particle-induced gamma emission, so that light elements can be determined. The usefulness of PIXE is illustrated by a number of typical applications in biology, medicine, geology, air pollution research, archaeology and the arts. (author).

  19. Alpha Particle Induced X-ray Emission in the Classroom

    International Nuclear Information System (INIS)

    Lopez, Jorge A.; Borunda, Mario F.; Morales, Jaime

    2003-01-01

    We report on an experimental demonstration in an introductory modern physics course to elucidate the X-ray line spectra, and how they arise from transitions of electrons to inner shells. We seek to determine the effect of limited use of an interactive component as a supplement to a traditional lecture, and how it would improve the student achievement. In this preliminary study the students were exposed to traditional lectures on X-ray production and Bohr's model, they then were given a homework on the abc of X-ray spectra, after which they were given a pre-test on the materials, followed by an in-class demonstration, and a final post-exam. The gain, as measured from pre- to post-exams appears to remark the differences in how students approached the subject before and after the use of the demonstration. This initial study shows the validity of in-class demonstrations as teaching tools and opens a wide new area of research in modern physics teaching

  20. Charged particle induced energy dispersive X-ray analysis

    International Nuclear Information System (INIS)

    Johansson, S.A.E.

    1979-01-01

    This review article deals with the X-ray emission induced by heavy, charged particles and the use of this process as an analytical method (PIXE). The physical processes involved, X-ray emission and the various reactions contributing to the background, are described in some detail. The sensitivity is calculated theoretically and the results compared with practical experience. A discussion is given on how the sensitivity can be optimized. The experimental arrangements are described and the various technical problems discussed. The analytical procedure, especially the sample preparation, is described in considerable detail. A number of typical practical applications are discussed. (author)

  1. Particle induced x-ray emission (PIXE) measurement of the Cd content in animal tissues

    International Nuclear Information System (INIS)

    Le Huong Quynh; Demeter, I.; Hollos-Nagy, K.; Szoekefalvi-Nagy, Z.

    1989-12-01

    Particle induced x-ray emission (PIXE) measurements were performed on thin samples prepared from different rabbit tissues, using 3 MeV proton beam for inducing x-rays from the animal tissues. This method is very sensitive and very small amounts of trace elements can be detected. Cadmium, one of the most toxic elements which can be concentrated in animal and human tissues due to environmental pollution, was detected with a limit of 0.7 ppm. The trace element concentrations obtained by PIXE were compared to those measured by atomic absorption spectrometry. PIXE method is proposed for routine analysis at the Veterinary and Food Investigating Service, Budapest, Hungary. (D.Gy.) 6 refs.; 3 figs

  2. 14th International Conference on Particle Induced X-ray Emission ("PIXE 2015")

    Science.gov (United States)

    Przybyłowicz, Wojciech Józef; Pineda-Vargas, Carlos

    2015-11-01

    This special issue of Nuclear Instruments and Methods in Physics Research B contains the proceedings of the 14th International Conference on Particle Induced X-ray Emission ("PIXE 2015") that was held in Somerset West (South Africa) from 25th February to 3rd March 2015.

  3. The quantitative determination of trace elements in giant unicellular plants by particle-induced X-ray emission

    International Nuclear Information System (INIS)

    Navarrete-Dominguez, V.R.; Yoshihara, K.; Tanaka, N.

    1982-01-01

    Particle-induced X-ray emission (PIXE) was applied for the determination of trace elements in biologically interesting materials, giant unicellular plants. It was found that the PIXE method had advantages in multi-element trace analysis of a single cell of the sample plant. (author)

  4. Detection of halogenated flame retardants in polyurethane foam by particle induced X-ray emission

    International Nuclear Information System (INIS)

    Maley, Adam M.; Falk, Kyle A.; Hoover, Luke; Earlywine, Elly B.; Seymour, Michael D.; DeYoung, Paul A.; Blum, Arlene; Stapleton, Heather M.; Peaslee, Graham F.

    2015-01-01

    A novel application of particle-induced X-ray emission (PIXE) has been developed to detect the presence of chlorinated and brominated flame retardant chemicals in polyurethane foams. Traditional Gas Chromatography–Mass Spectrometry (GC–MS) methods for the detection and identification of halogenated flame retardants in foams require extensive sample preparation and data acquisition time. The elemental analysis of the halogens in polyurethane foam performed by PIXE offers the opportunity to identify the presence of halogenated flame retardants in a fraction of the time and sample preparation cost. Through comparative GC–MS and PIXE analysis of 215 foam samples, excellent agreement between the two methods was obtained. These results suggest that PIXE could be an ideal rapid screening method for the presence of chlorinated and brominated flame retardants in polyurethane foams

  5. Quantification of arsenic in activated carbon using particle induced X-ray emission

    International Nuclear Information System (INIS)

    Yadav, Nirbhay N.; Maheswaran, Saravanamuthu; Shutthanandan, Vaithiyalingam; Thevuthasan, Suntharampillai; Ngo, Huu H.; Vigneswaran, Saravanamuth

    2006-01-01

    To date, the trace elemental analysis of solids with inhomogeneous internal structure has been limited, particularly in the case of adsorbents. High-energy ion beam based particle induced X-ray emission (PIXE) is an ideal analytical tool suitable for simultaneous quantification of trace elements with high accuracy. In this study, PIXE was used to quantify arsenic in the adsorbents, granular activated carbon (GAC) and powder activated carbon (PAC). Pelletized and unmodified GAC and PAC samples were analyzed along with powder samples deposited on thin teflon filters. These sample preparation methods resulted in samples of various thicknesses and densities. PIXE measurements taken from these samples were compared to results from neutron activation analysis (NAA) and atomic absorption spectroscopy (AAS). There is a good agreement between the values from the NAA and pelletized PIXE measurements and some AAS measurements

  6. Detection of halogenated flame retardants in polyurethane foam by particle induced X-ray emission

    Energy Technology Data Exchange (ETDEWEB)

    Maley, Adam M.; Falk, Kyle A.; Hoover, Luke; Earlywine, Elly B.; Seymour, Michael D. [Department of Chemistry, Hope College, 35 E. 12th Street, Holland, MI 49423 (United States); DeYoung, Paul A. [Department of Physics, Hope College, 27 Graves Place, Holland, MI 49423 (United States); Blum, Arlene [Green Science Policy Institute, Box 5455, Berkeley, CA 94705 (United States); Stapleton, Heather M. [Nicholas School of the Environment, Duke University, LSRC Box 90328, Durham, NC 27708 (United States); Peaslee, Graham F., E-mail: peaslee@hope.edu [Department of Chemistry, Hope College, 35 E. 12th Street, Holland, MI 49423 (United States)

    2015-09-01

    A novel application of particle-induced X-ray emission (PIXE) has been developed to detect the presence of chlorinated and brominated flame retardant chemicals in polyurethane foams. Traditional Gas Chromatography–Mass Spectrometry (GC–MS) methods for the detection and identification of halogenated flame retardants in foams require extensive sample preparation and data acquisition time. The elemental analysis of the halogens in polyurethane foam performed by PIXE offers the opportunity to identify the presence of halogenated flame retardants in a fraction of the time and sample preparation cost. Through comparative GC–MS and PIXE analysis of 215 foam samples, excellent agreement between the two methods was obtained. These results suggest that PIXE could be an ideal rapid screening method for the presence of chlorinated and brominated flame retardants in polyurethane foams.

  7. An optimised set-up for total reflection particle induced X-ray emission

    International Nuclear Information System (INIS)

    Kan, J.A. van; Vis, R.D.

    1997-01-01

    MeV proton beams at small angles of incidence (0-35 mrad) are used to analyse trace elements on flat surfaces such as Si wafers or quartz substrates. In these experiments, the particle induced X-ray emission (PIXE) signal is used in a new optimized set-up. This set-up is constructed in such a way that the X-ray detector can reach very large solid angles, larger than 1 sr. Use of these large detector solid angles, combined with the reduction of bremsstrahlung background, affords limits of detection (LOD) of the order of 10 10 at cm -2 using total reflection particle induced X-ray emission (TPIXE). The LODs from earlier TPIXE measurements in a non-optimized set-up are used to estimate LODs in the new TPIXE set-up. Si wafers with low surface concentrations of V, Ni, Cu and Ag are used as standards to calibrate the LODs found with this set-up. The metal concentrations are determined by total reflection X-ray fluorescence (TXRF). The TPIXE measurements are compared with TXRF measurements on the same wafers. (Author)

  8. Proton induced X-ray emission analysis

    International Nuclear Information System (INIS)

    Khan, Rashiduzzman

    1976-09-01

    The developments in proton induced X-ray emission analysis are reviewed. Techniques for analyzing thick and thin samples of different origin are described. Discussions on the application of proton induced X-ray emission analysis in different fields, comparison of the sensitivity of this method with other analytical techniques, its limitations and possible improvements are presented

  9. Composition of Renaissance paint layers: simultaneous particle induced X-ray emission and backscattering spectrometry.

    Science.gov (United States)

    de Viguerie, L; Beck, L; Salomon, J; Pichon, L; Walter, Ph

    2009-10-01

    Particle induced X-ray emission spectroscopy (PIXE) is now routinely used in the field of cultural heritage. Various setups have been developed to investigate the elemental composition of wood/canvas paintings or of cross-section samples. However, it is not possible to obtain information concerning the quantity of organic binder. Backscattering spectrometry (BS) can be a useful complementary method to overcome this limitation. In the case of paint layers, PIXE brings the elemental composition (major elements to traces) and the BS spectrum can give access to the proportion of pigment and binder. With the use of 3 MeV protons for PIXE and BS simultaneously, it was possible to perform quantitative analysis including C and O for which the non-Rutherford cross sections are intense. Furthermore, with the use of the same conditions for PIXE and BS, the experiment time and the potential damage by the ion beam were reduced. The results obtained with the external beam of the Accélérateur Grand Louvre pour l'Analyse Elementaire (AGLAE) facility on various test painting samples and on cross sections from Italian Renaissance masterpieces are shown. Simultaneous combination of PIXE and BS leads to a complete characterization of the paint layers: elemental composition and proportion of the organic binder have been determined and thus provide useful information about ancient oil painting recipes.

  10. Trace element determination in tomato puree using particle induced X-ray emission and Rutherford backscattering

    International Nuclear Information System (INIS)

    Romero-Davila, E.; Miranda, J.

    2004-01-01

    Particle induced X-ray emission (PIXE) and Rutherford backscattering spectrometry (RBS) were used to determine the concentrations of trace elements in samples of 12 tomato puree brands sold in the Mexican market. While RBS offered information about the main elements present in the matrix, PIXE gave results on trace elements. As a whole, data for 17 elements (C, N, O, Na, Mg, S, Cl, K, Ca, Ti, V, Cr, Mn, Fe, Ni, Cu, and Zn) were obtained. To evaluate the results, a comparison with brands from USA, Japan, Colombia, and Chile was carried out, using tomato purees produced following the domestic technology recipe. Additionally, the results were considered in the light of the Codex Alimentarius and the Mexican standard. It was found that all of the brands fall within the limits established by these standards, being of the same order of magnitude as the foreign brands. (author)

  11. Particle induced x-ray emission studies of some Indian medicinal plants

    International Nuclear Information System (INIS)

    Nomita Devi, K.; Nandakumar Sarma, H.; Kumar, Sanjiv

    2007-01-01

    Medicinal herbs have been used from antiquity by humanity. This paper discusses the elemental composition and concentration of ten Indian medicinal plants investigated by particle induced X-ray emission (PIXE) technique. The accuracy and precision of the technique were assured by analyzing three Certified Standard Reference Materials -cabbage- (GBW 08504, China), wheat flour (NIST-8436) and bovine liver (NIST-1577b). The element K, Ca, Mn, Fe, Cu and Zn were found to be present in all the samples in varying concentrations. No toxic heavy metals such as As, Pb and Hg were detected in the studied plants. The range of the elemental concentrations in dry weight has been found to vary from 4.69x10 4 mg/kg to 1.81 mg/kg in the plants. The results also show that these plants contain elements of vital importance in man's metabolism and that are needed for growth and developments, prevention and heating of diseases. (author)

  12. Particle Induced X-ray Emission (PIXE) Approach for the Quantification of Thin Al Films

    International Nuclear Information System (INIS)

    Younes, G; Zahraman, K; Nsouli, B; Soueidan, M; Ferro, G

    2008-01-01

    Particle Induced X-ray Emission (PIXE) has been used as a fast and non-destructive technique for sensitive characterization of ultra thin Al films deposited by evaporation onto Si substrate. In this work the PIXE technique was optimized, using proton beam at different energies and different angles of incidence, for the characterization of ultra thin Al films (few nanometers) deposited onto Si substrate. The PIXE results showed that a proton beam of 300 keV under tilting angle of 80 degree permits an accurate determination of Al with high sensitivity within few minutes of acquisition time and a LOD of less than 0.2 nm. The LOD versus energy and tilting angle will be presented and discussed. (author)

  13. Applications of charged particle induced x-ray analysis to forensic and biological studies

    International Nuclear Information System (INIS)

    Barnes, B.K.; Beghian, L.E.; Kegel, G.H.R.; Mathur, S.C.; Mittler, A.; Quinn, P.W.

    1974-01-01

    X-ray emission analysis was applied to the analysis of firearm discharge residues on hands for trace elements. It was also applied to the determination of trace element concentrations in the blood of malaria-infected and healthy mice

  14. Therapeutic application of metallic nanoparticles combined with particle-induced x-ray emission effect

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Jong-Ki; Seo, Seung-Jun [Biomedical Engineering and Radiology, School of Medicine, Catholic University of Daegu, Daegu 705-034 (Korea, Republic of); Kim, Ki-Hong [Department of Optometry and Visual Sciences, Catholic University of Daegu, Kyungsan 712-702 (Korea, Republic of); Kim, Tae-Jeong [Applied Chemical Engineering, College of Engineering, Kyungpuk National University, Daegu 702-701 (Korea, Republic of); Chung, Myung-Hwan; Kim, Kye-Ryung [Proton Engineering Frontier Project, Korea Atomic Energy Research Institute, Daejeon 305-353 (Korea, Republic of); Yang, Tae-Keun, E-mail: jkkim@cu.ac.kr [Korea Institute of Radiological and Medical Sciences, Seoul 139-706 (Korea, Republic of)

    2010-10-22

    Metallic nanoparticles (MNP) are able to release localized x-rays when activated with a high energy proton beam by the particle-induced x-ray emission (PIXE) effect. The exploitation of this phenomenon in the therapeutic irradiation of tumors has been investigated. PIXE-based x-ray emission directed at CT26 tumor cells in vitro, when administered with either gold (average diameter 2 and 13 nm) or iron (average diameter 14 nm) nanoparticles (GNP or SNP), increased with MNP solution concentration over the range of 0.1-2 mg ml{sup -1}. With irradiation by a 45 MeV proton therapy (PT) beam, higher concentrations had a decreased cell survival fraction. An in vivo study in CT26 mouse tumor models with tumor regression assay demonstrated significant tumor dose enhancement, thought to be a result of the PIXE effect when compared to conventional PT without MNP (radiation-only group) using a 45 MeV proton beam (p < 0.02). Those receiving GNP or SNP injection doses of 300 mg kg{sup -1} body weight before proton beam therapy demonstrated 90% or 75% tumor volume reduction (TVR) in 20 days post-PT while the radiation-only group showed only 18% TVR and re-growth of tumor volume after 20 days. Higher complete tumor regression (CTR) was observed in 14-24 days after a single treatment of PT with an average rate of 33-65% for those receiving MNP compared with 25% for the radiation-only group. A lower bound of therapeutic effective MNP concentration range, in vivo, was estimated as 30-79 {mu}g g{sup -1} tissue for both gold and iron nanoparticles. The tumor dose enhancement may compensate for an increase in entrance dose associated with conventional PT when treating large, solid tumors with a spread-out Bragg peak (SOBP) technique. The use of a combined high energy Bragg peak PT with PIXE generated by MNP, or PIXE alone, may result in new treatment options for infiltrative metastatic tumors and other diffuse inflammatory diseases.

  15. Elemental and mineralogical study of earth-based pigments using particle induced X-ray emission and X-ray diffraction

    International Nuclear Information System (INIS)

    Nel, P.; Lynch, P.A.; Laird, J.S.; Casey, H.M.; Goodall, L.J.; Ryan, C.G.; Sloggett, R.J.

    2010-01-01

    Artwork and precious artefacts demand non-destructive analytical methodologies for art authentication, attribution and provenance assessment. However, structural and chemical characterisation represents a challenging problem with existing analytical techniques. A recent authentication case based on an Australian Aboriginal artwork, indicate there is substantial benefit in the ability of particle induced X-ray emission (PIXE), coupled with dynamic analysis (DA) to characterise pigments through trace element analysis. However, this information alone is insufficient for characterising the mineralogical residence of trace elements. For this reason a combined methodology based on PIXE and X-ray diffraction (XRD) has been performed to explore the benefits of a more comprehensive data set. Many Aboriginal paintings and artefacts are predominantly earth pigment based. This makes these cultural heritage materials an ideal case study for testing the above combined methodological approach on earth-based pigments. Samples of synthetic and naturally occurring earth-based pigments were obtained from a range of sources, which include Indigenous communities within Australia's Kimberley region. PIXE analyses using a 3 MeV focussed proton beam at the CSIRO nuclear microprobe, as well as laboratory-based XRD was carried out on the above samples. Elemental signature spectra as well as mineralogical data were used to assess issues regarding synthetic and naturally occurring earth pigments with the ultimate aim of establishing provenance.

  16. The Importance of Particle Induced X-Ray Emission (PIXE) Analysis and Imaging to the Search for Life on the Ocean Worlds

    Science.gov (United States)

    Blake, D. F.; Sarrazin, P.; Thompson, Kathleen

    2017-01-01

    The MapX imaging X-ray spectrometer is described and Monte Carlo modeling is used to show the efficacy of 244-Cm radioisotope sources in detecting and quantifying the biogenic elements in ices on Ocean Worlds such as Europa.

  17. Charged particle induced delayed X-rays (DEX) for the analysis of intermediate and heavy elements

    Science.gov (United States)

    Pillay, A. E.; Erasmus, C. S.; Andeweg, A. H.; Sellschop, J. P. F.; Annegarn, H. J.; Dunn, J.

    1988-12-01

    The emission of K X-rays from proton-rich and metastable radionuclides, following proton activation of the stable isotopes of the elements of interest, has not been widely used as a means of analysis. The thrust of this paper proposes a nuclear technique using delayed X-rays for the analysis of low concentrations of intermediate and heavy elements. The method is similar to the delayed gamma-ray technique. Proton bombardment induces mainly (p, n) reactions whereas the delayed X-rays originate largely from e --capture and isomeric transition. Samples of rare earth and platinum group elements (PGE), in the form of compacted powders, were irradiated with an 11 MeV proton beam and delayed X-rays detected with a 100 mm 2 Ge detector. Single element spectra for a range of rare earths and PGEs are presented. Analytical conditions are demonstrated for Pd in the range 0.1-5%. Spectra from actual geological samples of a PGE ore, preconcentrated by fire-assay, and monazite are presented. All six platinum group elements are visible and interference-free in a single spectrum, a marked advance on other nuclear techniques for these elements, including PIXE and neutron activation analysis (NAA).

  18. PIXE in 1980: Summary of the second international conference on particle induced x-ray emission and its analytical applications

    International Nuclear Information System (INIS)

    Akselsson, K.R.

    1981-01-01

    The Second International Conference on Particle Induced X-ray Emission (PIXE) and its analytical applications was held in Lund, Sweden, June 9-12, 1980. About a hundred papers were presented, including seven invited talks (PIXE and particle scattering, microbeam analysis, applications to aerosols and biological samples). The main impression left by the conference was that both the PIXE method and its applications are in a phase of fast development. Considerable effort has successfully been devoted to optimizing the basic PIXE technique. Also the great advantage of simultaneously getting information about lighter elements and sample mass was reported to have been successfully employed in routine analyses. PIXE, which was initially considered to be a method mainly for thin samples, has also been shown to be competitive for a variety of thick samples. Data from aerosol studies was presented. With the PIXE-method, it is feasible to perform series of measurements over a long period of time, many samples in parallel and/or samples from sites of poor accessibility. However, the advantages of PIXE may be further exploited in aerosol investigations and some promising lines of sampler development were reported. Sample preparation techniques are crucial for applications to biological samples and several laboratories are engaged in such developmental work. However, it was also evident that PIXE is already giving significant contributions to research in biology and medicine

  19. Analysis of HgI2 and PbI2 crystals and detectors by particle-induced x-ray emission (PIXE) and ion backscattering spectroscopy (IBS)

    International Nuclear Information System (INIS)

    Bench, G.S.; Heikkinen, D.W.; Antolak, A.J.; Morse, D.H.; Pontau, A.E.; James, R.B.; David, D.C.; Burger, A.; Van Den Berg, L.

    1993-03-01

    The Ion Micro-Analysis Group (IMAG) in Livermore conducts quantitative trace elemental analysis with PIXE and depth profiling with IBS using an MeV ion microbeam. The system has the capability to produce two-dimensional trace element and IBS images. PIXE analyses have been conducted on HgI 2 and PbI 2 crystals and detector materials in order to identify and quantify near surface trace contaminants. IBS measurements have been conducted to investigate elemental depth distributions in various materials. The results of measurements on several different samples are reported and a discussion of factors affecting quantitative in vacuo microanalysis of these materials is presented

  20. Improvement in limit of detection in particle induced X-ray emission by means of rise time and pulse shape discrimination

    Energy Technology Data Exchange (ETDEWEB)

    Papp, Tibor E-mail: tibpapp@netscape.nettibpapp@yahoo.ca; Lakatos, Tamas; Nejedly, Zdenek; Campbell, John L

    2002-04-01

    A digital signal processor, based upon high-rate sampling of the preamplifier output, and equipped with rise time and pulse shape discrimination, has been tested in three situations. This processor provided significant improvement of particle induced X-ray emission and X-ray fluorescence detection limits over the state of the art analog processors, depending on the energy and intensity distribution of the X-ray spectra. Additionally it had a superior performance when measurements were performed in an environment of large electronic noise and in large nuclear background environment. It has also improved the reduction of several artifacts in X-ray spectra.

  1. Increased sensitivity in thick-target particle induced X-ray emission analyses using dry ashing for preconcentration

    International Nuclear Information System (INIS)

    Lill, J.-O.; Harju, L.; Saarela, K.-E.; Lindroos, A.; Heselius, S.-J.

    1999-01-01

    The sensitivity in thick-target particle induced X-ray emission (PIXE) analyses of biological materials can be enhanced by dry ashing. The gain depends mainly on the mass reduction factor and the composition of the residual ash. The enhancement factor was 7 for the certified reference material Pine Needles and the limits of detection (LODs) were below 0.2 μg/g for Zn, Cu, Rb and Sr. When ashing biological materials with low ash contents such as wood of pine or spruce (0.3% of dry weight) and honey (0.1% of wet weight) the gain was far greater. The LODs for these materials were 30 ng/g for wood and below 10 ng/g for honey. In addition, the ashed samples were more homogenous and more resistant to changes during the irradiation than the original biological samples. (Copyright (c) 1999 Elsevier Science B.V., Amsterdam. All rights reserved.)

  2. Contribution to depth profiling by particle induced X-ray emission application to the study of zinc diffusion in AgZn alloy

    International Nuclear Information System (INIS)

    Frontier, J.P.

    1987-08-01

    A contribution of the study of the capacities of Particle Induced X-ray Emission (P.I.X.E.) for depth profiling, in the range of 1 to 10 micrometers and over, is presented here. It is shown that, in a non destructuve way, the concentration profile of a given element can be obtained, in principle, by deconvoluting the X-ray yields of this element, measured in a set of experiments in which the energy of the impinging protons, hence their range, is systematically varied. Direct deconvolution procedure, which leads to the inversion of an ill-conditionned matrix is unsuitable. So we generalized the iterative procedure previously used by Vegh to solve a similar problem. Alternatively we also used a fitting procedure of several parameters which gave us somewhat better than those of the iterative procedure. Both algorithms where applied to a set of X-ray yields induced by protons of energy between 0.45 to 2 MeV, corresponding to the first 6 micrometers of various depletion profiles of zinc in an initially homogeneous Ag-3 at % Zn annealed under vacuum. For investigation of deeper layers, a sectionning technique which consists in analysing thin film hydroxide targets by specific chemistry of tiny turning, was developped with success. Cross-reference of all the obtained profiles was made with electron microprobe determination on transverse section, and with the predictions of the theory of atomic diffusion. In addition, the possibilities of increasing the depth resolution by developping techniques either of controled sanding of the surface, or analysis of the sample is discussed [fr

  3. Trends in grazing emission x-ray analysis techniques

    International Nuclear Information System (INIS)

    Grieken, R. van; Tsuji, K.; Injuk, J.

    2000-01-01

    then, the detection limits imposed by the semiconductor industry roadmap can probably not be obtained by tube-excited GEXRF. Th perspectives for tube-excited GE-XRF are thus rather poor. Future developments imply the combination of GEXRF with synchrotron radiation excitation. Grazing-emission particle-induced X-ray emission (GE-PIXE) suffers of similar quantification Problems for material deposited on a carrier, but it makes PIXE a surface-sensitive technique, while normally the protons penetrate some tens of μm in the sample. Similarly, grazing-emission electron probe micro-analysis (GE-EPNIA) allows to selectively analyze particles on a flat carrier, allows surface sensitivities in the nm rather than μ range, and yields, in principle, a spatial resolution for chemical analysis similar to the size of the impinging electron beam, rather than of the electron-excited volume. Both GE-PIXE and GE-EPMA need to be explored more fully in the near future. (author)

  4. Ion induced x-ray emission

    International Nuclear Information System (INIS)

    Cohen, D.D.; Clayton, E.

    1989-01-01

    This paper discusses particle induced x-ray emission (PIXE). Its use as a tool for multi-element non-destructive trace element analysis of small samples is addressed. Concepts and details needed for the construction of a PIXE system are offered

  5. Comparison of laser microprobe mass spectrometry (LMMS) and micro particle induced x-ray emission (micro-PIXE) for the analysis of senile plaques in Alzheimer`s disease. A preliminary study

    Energy Technology Data Exchange (ETDEWEB)

    Lovell, M A; Robertson, J D; Ehmann, W D [Kentucky Univ., Lexington, KY (United States). Dept. of Chemistry; Markesbery, W R [Kentucky Univ., Lexington, KY (United States); Teesdale, W J; Campbell, J L [Guelph Univ., ON (Canada). Dept. of Physics

    1995-08-01

    Results of micro-PIXE analysis of senile plaques (SP) in Alzheimer`s disease (AD) brain have been utilized to independently confirm levels of iron (Fe) as measured by LMMS in adjacent brain sections. LMMS concentrations were calculated based on the preparation and analysis of an iron calibration curve prepared in our laboratory. The LMMS standards consist of iron cis-dicylclohexano-18-crown-6 ether coordination complexes dissolved in Spurr`s low viscosity embedding medium. To our knowledge, this is the first report of the use of micro-PIXE, with its spatial resolution and detection limits comparable to that of LMMS, in the validation of LMMS results. The agreement observed between results obtained for Fe by micro-PIXE and LMMS indicates that the use of our LMMS standards, at least in the case of Fe, yields accurate results. (author). 6 refs., 1 fig., 1 tab.

  6. Particle induced X-ray emission (PIXE) present and future. Ryushisen reiki X sen bunsekiho (PIXE) no genjo to shorai

    Energy Technology Data Exchange (ETDEWEB)

    Uda, M. (Waseda Univ., Tokyo (Japan). Science and Engineering)

    1992-07-10

    The principle of measurement of PIXE are explained. It has in comparison with SEM and EPM, the following characteristics such as; very short measurement and analysis time, developed detection sensitivity for more than 100 elements, no need of pretreatment, undestructive analysis method in the air, possibility of trace element analysis by using micro specimen and information input of chemical bonding condition. Bio-medical applications have been, the microanalysis of multi elements in light element matrix forming living body and the diagnosis of kidney cancer and other diseases. Environmental applications have been, detection of the composition of sea water and the detection of the pollutants of the rivers by elements concentration distribution. It is also applied for managing the amount of impurities in electronic materials and monitoring the emitted elements from fusion reactor. It is used for archaeological analysis such as, analysis of gold fixing in ancient Rome and earthernware analysis of ancient China. As for the chemical bonding condition, the small difference of chemical bonding has been able to be observed clearly as a difference of strength over the multiple spectra, and PIXE has prospects in multiple fields. 24 refs., 21 figs.

  7. Swift Quantification of Fenofibrate and Tiemonium methylsulfate Active Ingredients in Solid Drugs Using Particle Induced X-Ray Emission

    International Nuclear Information System (INIS)

    Bejjani, A.; Nsouli, B.; Zahraman, K.; Assi, S.; Younes, Gh.; Yazbi, F.

    2011-01-01

    The quantification of active ingredients (AI) in drugs is a crucial and important step in the drug quality control process. This is usually performed by using wet chemical techniques like LC-MS, UV spectrophotometry and other appropriate organic analytical methods. However, if the active ingredient contains specific heteroatoms (F, S, Cl), elemental IBA like PIXE and PIGE techniques, using small tandem accelerator of 1-2 MV, can be explored for molecular quantification. IBA techniques permit the analysis of the sample under solid form, without any laborious sample preparations. In this work, we demonstrate the ability of the Thick Target PIXE technique for rapid and accurate quantification of both low and high concentrations of active ingredients in different commercial drugs. Fenofibrate, a chlorinated active ingredient, is present in high amounts in two different commercial drugs, its quantification was done using the relative approach to an external standard. On the other hand, Tiemonium methylsulfate which exists in relatively low amount in commercial drugs, its quantification was done using GUPIX simulation code (absolute quantification). The experimental aspects related to the quantification validity (use of external standards, absolute quantification, matrix effect,...) are presented and discussed. (author)

  8. Analysis of sludge using Proton induced X-ray emission

    International Nuclear Information System (INIS)

    Aspiazu, J.; Moreno, E.; Andrade, E.; Miranda, J.; Citalan, S.; Moeller, G.; Soler, F.

    1996-01-01

    Regulations to control the huge amounts of sludge produced by wastewater are needed. Sludge generated in conventional sedimentators or anaerobic digesters were characterized by Proton Induced X-ray Emission (PIXE). It was possible to determine the presence of macro nutrient elements, such as P and K, and secondary nutrients like Ca, S, and Mg. Moreover, heavy elements like Cu, Zn, and Pb were also found. The sludge treatment in anaerobic digesters increased the amount of certain elements Al, Si, S, Cl, and K; decrease in Ca, Ti, and Cu, and no change in V, Cr, and Zn. Possible uses of this sludge are also suggested

  9. Spectral analysis of K-shell X-ray emission of magnesium plasma

    Indian Academy of Sciences (India)

    2014-02-06

    Feb 6, 2014 ... Spectral analysis of K-shell X-ray emission of magnesium plasma, produced by laser pulses of 45 fs duration, focussed up to an intensity of ∼1018 W cm-2, is carried out. The plasma conditions prevalent during the emission of X-ray spectrum were identified by comparing the experimental spectra with the ...

  10. X-ray emission spectroscopy. X-ray fluorescence

    International Nuclear Information System (INIS)

    Despujols, J.

    1992-01-01

    Principles of X-ray emission spectrometry are first recalled, then wave-length dispersive and energy dispersive X-ray fluorescence spectrometer are described. They are essentially designed for qualitative and quantitative analysis of elements (Z>10). Sample preparation, calibration, corrections, interferences, accuracy are reviewed. Examples of use in different industries are given. (71 refs.)

  11. Proton-induced X-ray emission analysis of marine particulates

    International Nuclear Information System (INIS)

    Burnett, W.C.; Mitchum, G.T.

    1981-01-01

    We report a methodology used to analyze suspended marine particulates by particle induced X-ray emission (PIXE). Water samples from an estuary in Brazil were filtered soon after collection onto pre-weighed Nuclepore filters, washed with deionized water, dried to constant weight and analyzed as thin targets. Because of the relatively high mass loadings (0.1-1.0 mg/cm 2 ) on the filters, proton bombardment times of a few minutes were adequate for maintaining good counting statistics. Precision and accuary were determined by replicate analysis and intercomparison to geochemical standards. Suspensions of standards in deionized water were filtered dried, weighed and analyzed in a similar fashion as our samples of marine particulates. Net X-ray intensities were related to mass by calibration against pure elemental standards. Initial experiments showed systematically low concentrations for all elements determined by PIXE relative to known values. Further experiments verified that this systematic errors was due to an uneven distribution of mass on the surface of the filters. Improvements in the filtration technique have eliminated the topographic effect on our samples and the PIXE resultes were substantially improved. Variations in matrix and particle size of the samples analyzed did not cause any measureable analytical effect. PIXE thus seems well suited for providing rapid, multi-element data on samples of marine particulates if suitable precautions are made during the sample preparation process. (orig.)

  12. Elemental analysis of coal by proton-induced x-ray emission analysis

    International Nuclear Information System (INIS)

    Cronch, S.M.; Ehmann, W.D.; Laumer, H.W.; Gabbard, F.

    1976-01-01

    Proton-induced x-ray emission was used to determine elemental concentrations in solid coal samples. The coal samples were irradiated with 2.5 to 5.5 MeV protons. Concentrations were determined from characteristic x-ray yields taking into account matrix absorption. The precision is shown by replicate analysis and the accuracy by comparison with results obtained by other laboratories using different techniques

  13. Application of X-ray emission techniques for monitoring environmental pollution

    International Nuclear Information System (INIS)

    Bernasconi, G.; Danesi, P.R.; Dargie, M.; Haselberger, N.; Markowicz, A.; Tajani, A.

    1997-01-01

    X-ray emission techniques are versatile and powerful methods used for multielement non-destructive analysis. They include X-ray fluorescence (XRF), particle induced X-ray emission (PIXE), scanning electron microscopy combined with X-ray spectrometry and electron probe microanalysis (EPMA). Since many years the IAEA has utilised and promoted these techniques for the analysis of environmental, biological and geological samples. In this paper recent progress at our laboratory in selected aspects related to the application of X-ray emission techniques is briefly overviewed. (authors)

  14. PIXE (proton induced X-ray emission) analysis of caatinger

    International Nuclear Information System (INIS)

    Nakanishi, T.M.; Futatsugawa, Shoji; Sera, Kouichiro.

    1995-01-01

    Caatinger (Mimosa acutistipula Benth), which has been a popular wood among the people in north east part of Brazil, was analyzed using PIXE (proton induced X-ray emission). The wood sample was divided into three parts, center, inner and outer side of the wood. Using the wood slice of each part, Na, Mg, Al, Si, P, S, Cl, K, Ca, Ti, Mn, Fe, Cu, Zn, As, Se, Br, Rb, Sr, Y, Ru and Pb were detected. When the wood slices were decomposed with nitric acid, Co and Ni were able to be determined. Two samples, non-destructive and chemically treated sample, of heartwood and sapwood showed the similar concentration of the elements. There was a discrete change of the accumulated elements between heartwood and sapwood. Most of the elements detected tended to be concentrated at sapwood, whereas Ca, Cu and Sr were concentrated at heartwood. At center part, especially, Na, Mg, Fe and Sr were accumulated. Since most of the heartwood and sapwood is dead, discrete change of the element concentration suggests some element movement across the annual ring at heartwood formation. (author)

  15. Application of particle-induced X-ray emission, backscattering spectrometry and scanning electron microscopy in the evaluation of orthodontic materials

    International Nuclear Information System (INIS)

    Gihwala, D.; Mars, J.A.; Pineda-Vargas, C.

    2013-01-01

    The focus of this investigation was on orthodontic materials used in the manufacture of dental brackets. The properties of these dental materials are subjected to various physical parameters such as elongation, yield strength and elasticity that justify their application. In turn, these parameters depend on the quantitative elemental concentration distribution (QECD) in the materials used in the manufacture. For compositional analysis, proton-induced X-ray emission (PIXE), backscatter spectrometry (BS) and scanning electron microscopy (SEM) were applied. QECD analysis was performed to correlate the physical parameters with the composition and to quantify imperfections in the materials. PIXE and BS analyses were performed simultaneously with a 3 MeV proton beam while electrons accelerated at 25 keV were used for the SEM analysis. From the QECDs it was observed that: (1) the major elements Cr, Fe and Ni were homogeneously distributed in the orthodontic plate; (2) the distribution of Mo and O correlated with one another; (3) there was a spread of Cr around regions of high C concentration; and, (4) areas of high concentrations of Mo and O corresponded to a decrease in C concentrations. Elemental concentration correlations are shown to indicate the similarities and differences in the ease of formation of phases, based on the tangent of linearity. (author)

  16. Multielement proton-induced x-ray emission analysis of Bangladeshi tobacco

    International Nuclear Information System (INIS)

    Hadi, D.A.; Ali, M.; Biswas, S.K.; Islam, M.M.; Khan, A.H.

    1984-01-01

    The concentration of 12 different elements in cigarette tobacco of different brands, commercially made in Bangladesh, was determined using the proton particle-induced x-ray emission (proton PIXE) method. In all the present experiments, proton beams of 2.0 MeV (on the target in air) and about 30 nA current were used for characteristic x-ray excitation. The concentration of the elements (K, Ca, Ti, Cr, Mn, Fe, Ni, Cu, Zn, Br, Rb and Sr) was determined by comparison with a calibration obtained from the NBS orchard leaf standard SRM 1571. The results have been compared with available data on some foreign brands of tobacco and the probable reasons for the difference in the contents of some of the elements found in the Bangladeshi brands are discussed. (author)

  17. Proton induced X-ray emission (PIXE) analysis at Lucas Heights

    International Nuclear Information System (INIS)

    Cohen, D.; Duerden, P.

    1979-02-01

    The state of the proton induced X-ray emission (PIXE) work at Lucas Heights is reported together with a full description of the experimental arrangement and its use for analysis of trace elements (Z >or= 14). The fundamentals of PIXE are examined in detail with a view to understanding not only the background continuum but also the X-ray production mechanisms. Quantitative predictions for the number of X-rays detected after proton bombardment of the target have been made and these compare well with experiments

  18. X-ray fluorescence analysis and optical emission spectrometry of an roman mirror from Tomis, Romania

    International Nuclear Information System (INIS)

    Belc, M.; Bogoi, M.; Ionescu, D.; Guita, D.; Caiteanu, S.; Caiteanu, D.

    2000-01-01

    The miscellaneous population of Roman Empire, their diverse cultural tradition, their ability to assimilate the roman civilization spirits, had determined a permanent reassessment superimposed upon the roman contribution. Analysis was undertaken using optical emission spectrometry and non-destructive X-ray fluorescence. X-ray fluorescence analysis is a well-established method and is often used in archaeometry and other work dealing with valuable objects pertaining to the history of art and civilization. Roman mirror analysed has been found not to be made of speculum (a high tin bronze). (authors)

  19. Trace element analysis in liquids by proton induced x-ray emission

    International Nuclear Information System (INIS)

    Deconninck, G.

    Proton induced x-ray emission (PIXE) from liquid has been developed for quantitative and simultaneous analysis of trace elements. Liquid drops and trickles are bombarded at atmospheric pressure, x-rays are detected in a non dispersive Si(Li) solid state detector. Absolute determinations are made by comparison with standard solutions. Detection limits in a 5 minutes run are in the ppm range for a single drop (0.05 ml). The application of this technique to the determination of trace elements in biological liquids is investigated (Cr, Mn, Fe, Co, Ni, Cu, Zn, in plant extracts, haemocyanine, albumins...). (author)

  20. Proton-Induced X-Ray Emission Analysis of Crematorium Emissions

    Science.gov (United States)

    Ali, Salina; Nadareski, Benjamin; Yoskowitz, Joshua; Labrake, Scott; Vineyard, Michael

    2014-09-01

    There has been considerable debate in recent years about possible mercury emissions from crematoria due to amalgam tooth restorations. We have performed a proton-induced X-ray emission (PIXE) analysis of aerosol and soil samples taken near the Vale Cemetery Crematorium in Schenectady, NY, to address this concern. The aerosol samples were collected on the roof of the crematorium using a nine-stage, cascade impactor that separates the particulate matter by aerodynamic diameter and deposits it onto thin Kapton foils. The soil samples were collected at several different distances from the crematorium and compressed into pellets with a hydraulic press. The Kapton foils containing the aerosol samples and the soil pellets were bombarded with 2.2-MeV protons from the 1.1-MV tandem Pelletron accelerator in the Union College Ion-Beam Analysis Laboratory. We measured significant concentrations of sulfur, phosphorus, potassium, calcium, and iron, but essentially no mercury in the aerosol samples. The lower limit of detection for airborne mercury in this experiment was approximately 0.2 ng / m3. The PIXE analysis of the soil samples showed the presence of elements commonly found in soil (Si, K, Ca, Ti, Mn, Fe), but no trace of mercury. There has been considerable debate in recent years about possible mercury emissions from crematoria due to amalgam tooth restorations. We have performed a proton-induced X-ray emission (PIXE) analysis of aerosol and soil samples taken near the Vale Cemetery Crematorium in Schenectady, NY, to address this concern. The aerosol samples were collected on the roof of the crematorium using a nine-stage, cascade impactor that separates the particulate matter by aerodynamic diameter and deposits it onto thin Kapton foils. The soil samples were collected at several different distances from the crematorium and compressed into pellets with a hydraulic press. The Kapton foils containing the aerosol samples and the soil pellets were bombarded with 2.2-Me

  1. L X-ray emission induced by heavy ions

    Energy Technology Data Exchange (ETDEWEB)

    Pajek, M. [Institute of Physics, Jan Kochanowski University, 25-406 Kielce (Poland); Banaś, D., E-mail: d.banas@ujk.edu.pl [Institute of Physics, Jan Kochanowski University, 25-406 Kielce (Poland); Braziewicz, J.; Majewska, U.; Semaniak, J. [Institute of Physics, Jan Kochanowski University, 25-406 Kielce (Poland); Fijał-Kirejczyk, I. [The Institute of Atomic Energy, 05-400 Otwock-Świerk (Poland); Jaskóła, M.; Czarnacki, W.; Korman, A. [The National Centre for Nuclear Research, 05-400 Otwock-Świerk (Poland); Kretschmer, W. [Physikalisches Institut, Universität Erlangen-Nürnberg, D-91058 Erlangen (Germany); Mukoyama, T. [Institute for Nuclear Research, Hungarian Academy of Sciences (ATOMKI), H-4026 Debrecen (Hungary); Trautmann, D. [Institut für Physik, Universität Basel, Basel (Switzerland)

    2015-11-15

    Particle-induced X-ray emission (PIXE) technique is usually applied using typically 1 MeV to 3 MeV protons or helium ions, for which the ion-atom interaction is dominated by the single ionization process. For heavier ions the multiple ionization plays an increasingly important role and this process can influence substantially both the X-ray spectra and atomic decay rates. Additionally, the subshell coupling effects are important for the L- and M-shells ionized by heavy ions. Here we discuss the main features of the X-ray emission induced by heavy ions which are important for PIXE applications, namely, the effects of X-ray line shifts and broadening, vacancy rearrangement and change of the fluorescence and Coster–Kronig yields in multiple ionized atoms. These effects are illustrated here by the results of the measurements of L X-ray emission from heavy atoms bombarded by 6 MeV to 36 MeV Si ions, which were reported earlier. The strong L-subshell coupling effects are observed, in particular L{sub 2}-subshell, which can be accounted for within the coupling subshell model (CSM) developed within the semiclassical approximation. Finally, the prospects to use heavy ions in PIXE analysis are discussed.

  2. Method and multichannel equipment for chemical analysis by X-ray emission

    International Nuclear Information System (INIS)

    Bacso, J.; Horkay, Gy.; Kalinka, G.; Kertesz, Zs.; Kiss Varga, M.; Lakatos, T.; Mathe, Gy.; Paal, A.; Sulik, B.

    1978-01-01

    In the patent a simple method and an apparatus are described for chemical analysis based on X-ray emission generated by irradiation. The concentrations of pre-selected elements can be determined easily by this method using an equipment containing microprocessor. The number of channels and the elements to be determined can be modified by a simple change in the program. (Sz.J.)

  3. Sample analysis using gamma ray induced fluorescent X-ray emission

    Energy Technology Data Exchange (ETDEWEB)

    Sood, B S; Allawadhi, K L; Gandhi, R; Batra, O P; Singh, N [Punjabi Univ., Patiala (India). Nuclear Science Labs.

    1983-01-01

    A non-destructive method for the analysis of materials using gamma ray-induced fluorescent x-ray emission has been developed. In this method, special preparation of very thin samples in which the absorption of the incident gamma rays and the emitted fluorescent x-rays is negligible, is not needed, and the absorption correction is determined experimentally. A suitable choice of the incident gamma ray energies is made to minimise enhancement effects through selective photoionization of the elements in the sample. The method is applied to the analysis of a typical sample of the soldering material using 279 keV and 59.5 keV gamma rays from /sup 203/Hg and /sup 241/Am radioactive sources respectively. The results of the analysis are found to agree well with those obtained from the chemical analysis.

  4. Proton induced x-ray emission analysis of trace elements in thick bread samples

    International Nuclear Information System (INIS)

    Mohamed Baker Al-bedri; Ikram Jameel Abdul Ghani; Ibrahim Abdul Rahman Al-aghil

    2009-01-01

    Proton induced X-ray emission (PIXE) technique has been used for identification and quantitative analysis of the elemental concentration in thick bread samples. Bread samples were air-oven dried at 60degC and milled in a clean agate mortar to homogenize the sample and pressed into a pellet. PIXE technique relies on the analysis of the energy spectra of the characteristic X-ray emitted from the thick bread sample and the orchard leaf standard (NIST-SRM-1571) bombarded with 2.0 MeV protons. The concentration of the elements (Cl, K, Ca, Mn, Fe, Cu, and Zn) in the bread samples was determined by comparison with NIST orchard leaf standard. The accuracy of the measurements ranged between ±2% and ±10% for the most elements detected in this method. The aim of this study is to establish the reference concentration of trace elements in the Iraqi bread using PIXE technique. (author)

  5. X-ray Emission from Solar Flares

    Indian Academy of Sciences (India)

    2016-01-27

    Jan 27, 2016 ... Solar flares; X-ray detectors; X-ray line emission and continuum; break energy; microflares. Abstract. Solar X-ray Spectrometer (SOXS), the first space-borne solar astronomy experiment of India was designed to improve our current understanding of X-ray emission from the Sun in general and solar flares in ...

  6. SU-E-T-231: Measurements of Gold Nanoparticle-Mediated Proton Dose Enhancement Due to Particle-Induced X-Ray Emission and Activation Products Using Radiochromic Films and CdTe Detector

    International Nuclear Information System (INIS)

    Cho, J; Cho, S; Manohar, N; Krishnan, S

    2014-01-01

    Purpose: There have been several reports of enhanced cell-killing and tumor regression when tumor cells and mouse tumors were loaded with gold nanoparticles (GNPs) prior to proton irradiation. While particle-induced xray emission (PIXE), Auger electrons, secondary electrons, free radicals, and biological effects have been suggested as potential mechanisms responsible for the observed GNP-mediated dose enhancement/radiosensitization, there is a lack of quantitative analysis regarding the contribution from each mechanism. Here, we report our experimental effort to quantify some of these effects. Methods: 5-cm-long cylindrical plastic vials were filled with 1.8 mL of either water or water mixed with cylindrical GNPs at the same gold concentration (0.3 mg Au/g) as used in previous animal studies. A piece of EBT2 radiochromic film (30-µm active-layer sandwiched between 80/175-µm outer-layers) was inserted along the long axis of each vial and used to measure dose enhancement due to PIXE from GNPs. Vials were placed at center-of-modulation (COM) and 3-cm up-/down-stream from COM and irradiated with 5 different doses (2–10 Gy) using 10-cm-SOBP 160-MeV protons. After irradiation, films were cleaned and read to determine the delivered dose. A vial containing spherical GNPs (20 mg Au/g) was also irradiated, and gamma-rays from activation products were measured using a cadmium-telluride (CdTe) detector. Results: Film measurements showed no significant dose enhancement beyond the experimental uncertainty (∼2%). There was a detectable activation product from GNPs, but it appeared to contribute to dose enhancement minimally (<0.01%). Conclusion: Considering the composition of EBT2 film, it can be inferred that gold characteristic x-rays from PIXE and their secondary electrons make insignificant contribution to dose enhancement. The current investigation also suggests negligible dose enhancement due to activation products. Thus, previously-reported GNP-mediated proton dose

  7. Spectral analysis of K-shell X-ray emission of magnesium plasma ...

    Indian Academy of Sciences (India)

    2014-02-06

    Feb 6, 2014 ... the experimental spectra with the synthetic spectra generated using .... user to specify the time duration over which the ionic populations ... ied the dependence of X-ray emission spectrum as a function of laser intensity in the.

  8. Inorganic Profiling of Amoxicillin Drugs in Ghana Using Proton Induced X-Ray Emission (Pixe) Analysis

    International Nuclear Information System (INIS)

    Abdul-Wahab, Zurika

    2017-07-01

    Induced X-ray Emission (PIXE) analysis of the amoxicillin standard reference material revealed ten (10 ) elements which include Al, S, K, Ca, V, Cr, Mn, Fe, Ni, and Zn. Sulphur was identified as the major element in the standard reference material and recorded concentration value of 396,805 ppm. Samples from Kwame Nkrumah Circle, a locally manufactured brand recorded the lowest sulphur concentrations of 251,745 ppm, compared to all drugs analysed using PIXE; imported amoxicillin (395,753 ppm) and Okaishi locally manufactured (384,710 ppm). Additionally, the elements Cr, Mn and Fe were found to be relatively higher in the Kwame Nkrumah Circle sample hence raising concerns over the quality of the Kwame Nkrumah Circle brand. When a physical parameter test was performed on all samples, all brands with the exception of Kwame Nkrumah Circle passed the disintegration and dissolution test deeming the Kwame Nkrumah Circle brand substandard. After an HPLC test was performed for all samples, it was discovered that all the drugs analysed passed the acceptance criteria (90-120%) for drugs set by the British Pharmacopoeia; with the Kwame Nkrumah Circle brand recording a value of 97% relatively lower than all the other samples which range from 113 to 117%. Sulphur as an active principle ingredient was correlated with the other identified elements. Strong correlations with correlation coefficients within the range 0.9936 – 0.9978 were found with the elements Cr, Mn, and Fe. Hence the elements S, Cr, Mn, and Fe lend themselves as element signature for amoxicillin medical drug. This was done to discover element signatures that will facilitate differentiating between genuine and counterfeit amoxicillin drugs. Considering the simplicity in sample preparation, the non-distractive nature of PIXE analysis, and also fast turn out in producing results. PIXE offers a considerable advantage when analysing antibiotic drugs on a large scale. (author)

  9. Analysis of memory consolidation and evocation in rats by proton induced X-ray emission

    Energy Technology Data Exchange (ETDEWEB)

    Jobim, P.F.C., E-mail: pjobim@uol.com.br [Ion Implantation Laboratory, Physics Institute, Federal University of Rio Grande do Sul, Av. Bento Gonçalves 9500, CP 15051, CEP 91501-970, Porto Alegre (Brazil); Laboratory of Neuropharmacology and Neural Tumor Biology, Department of Pharmacology, Institute for Basic Health Sciences, Federal University of Rio Grande do Sul, Av. Paulo Gama 90050-170, Porto Alegre (Brazil); University Hospital Research Center (HCPA), Federal University of Rio Grande do Sul, 90035-003, Rua Ramiro Barcelos, Porto Alegre (Brazil); Santos, C.E.I. dos [Ion Implantation Laboratory, Physics Institute, Federal University of Rio Grande do Sul, Av. Bento Gonçalves 9500, CP 15051, CEP 91501-970, Porto Alegre (Brazil); Maurmann, N.; Reolon, G.K. [Laboratory of Neuropharmacology and Neural Tumor Biology, Department of Pharmacology, Institute for Basic Health Sciences, Federal University of Rio Grande do Sul, Av. Paulo Gama 90050-170, Porto Alegre (Brazil); University Hospital Research Center (HCPA), Federal University of Rio Grande do Sul, 90035-003, Rua Ramiro Barcelos, Porto Alegre (Brazil); Debastiani, R. [Ion Implantation Laboratory, Physics Institute, Federal University of Rio Grande do Sul, Av. Bento Gonçalves 9500, CP 15051, CEP 91501-970, Porto Alegre (Brazil); Pedroso, T.R.; Carvalho, L.M. [Laboratory of Neuropharmacology and Neural Tumor Biology, Department of Pharmacology, Institute for Basic Health Sciences, Federal University of Rio Grande do Sul, Av. Paulo Gama 90050-170, Porto Alegre (Brazil); University Hospital Research Center (HCPA), Federal University of Rio Grande do Sul, 90035-003, Rua Ramiro Barcelos, Porto Alegre (Brazil); Dias, J.F. [Ion Implantation Laboratory, Physics Institute, Federal University of Rio Grande do Sul, Av. Bento Gonçalves 9500, CP 15051, CEP 91501-970, Porto Alegre (Brazil)

    2014-08-01

    It is well known that trace elements such as Mg, Ca, Fe, Cu and Zn have a key role in synapse plasticity and learning. Learning process is conventionally divided in three distinct and complementary stages: memory acquisition, consolidation and evocation. Consolidation is the stabilization of the synaptic trace formed by acquisition, while evocation is the recall of this trace. Ion-based techniques capable of providing information concerning the elemental composition of organic tissues may be helpful to improve our understanding on memory consolidation and evocation processes. In particular, the Particle-Induced X-ray Emission (PIXE) technique can be used to analyze different biological tissues with good accuracy. In this work we explore the versatility of PIXE to measure the elemental concentrations in rat brain tissues in order to establish any possible correlation between them and the memory consolidation and evocation processes. To this end, six groups of middle-age male Wistar rats were trained and tested in a step-down Inhibitory Avoidance conditioning. After the behavior tests, the animals were decapitated in accordance with the legal procedures and their brains were removed and dissected for the PIXE analyses. The results demonstrated that there are differences in the elemental concentration among the groups and such variations may be associated with their availability to the learning processes (by memory consolidation and evocation). Moreover, the control groups circumvent the possibility that a non-specific event involved in learning tasks cause such variations. Our results suggest that PIXE may be a useful tool to investigate memory consolidation and evocation in animal models.

  10. Analysis of memory consolidation and evocation in rats by proton induced X-ray emission

    International Nuclear Information System (INIS)

    Jobim, P.F.C.; Santos, C.E.I. dos; Maurmann, N.; Reolon, G.K.; Debastiani, R.; Pedroso, T.R.; Carvalho, L.M.; Dias, J.F.

    2014-01-01

    It is well known that trace elements such as Mg, Ca, Fe, Cu and Zn have a key role in synapse plasticity and learning. Learning process is conventionally divided in three distinct and complementary stages: memory acquisition, consolidation and evocation. Consolidation is the stabilization of the synaptic trace formed by acquisition, while evocation is the recall of this trace. Ion-based techniques capable of providing information concerning the elemental composition of organic tissues may be helpful to improve our understanding on memory consolidation and evocation processes. In particular, the Particle-Induced X-ray Emission (PIXE) technique can be used to analyze different biological tissues with good accuracy. In this work we explore the versatility of PIXE to measure the elemental concentrations in rat brain tissues in order to establish any possible correlation between them and the memory consolidation and evocation processes. To this end, six groups of middle-age male Wistar rats were trained and tested in a step-down Inhibitory Avoidance conditioning. After the behavior tests, the animals were decapitated in accordance with the legal procedures and their brains were removed and dissected for the PIXE analyses. The results demonstrated that there are differences in the elemental concentration among the groups and such variations may be associated with their availability to the learning processes (by memory consolidation and evocation). Moreover, the control groups circumvent the possibility that a non-specific event involved in learning tasks cause such variations. Our results suggest that PIXE may be a useful tool to investigate memory consolidation and evocation in animal models

  11. Elemental concentrations in kidney and liver of mice fed with cafeteria or standard diet determined by particle induced X-ray emission

    Energy Technology Data Exchange (ETDEWEB)

    Dimer Leffa, Daniela [Graduate Program in Health Sciences, Health Sciences Unit, University of Southern Santa Catarina, 88806-000 Criciúma, SC (Brazil); Iochims dos Santos, Carla Eliete; Debastiani, Rafaela; Amaral, Livio; Yoneama, Maria Lucia; Ferraz Dias, Johnny [Ion Implantation Laboratory, Physics Institute, Federal University of Rio Grande do Sul, Porto Alegre (Brazil); Moraes Andrade, Vanessa, E-mail: vmoraesdeandrade@yahoo.com.br [Graduate Program in Health Sciences, Health Sciences Unit, University of Southern Santa Catarina, 88806-000 Criciúma, SC (Brazil)

    2014-01-01

    The importance of trace elements in human health is well known and their main source is daily diet. Nowadays, one of the biggest issues is the presence of these micronutrients in levels much higher than required, leading to potential toxic effects. The aim of this work was to investigate the elemental content in organs of mice fed with cafeteria or standard diet using PIXE. Twelve male Swiss mice were divided into two groups: control group (standard chow) and cafeteria group (high-caloric diet). After 17 weeks, samples of different organs (kidney and liver) were collected and prepared for PIXE analysis. The Fe concentration in kidney and liver was statistically higher in animals that received the cafeteria diet (p < 0.001). The Al and Si kidney contents were significantly higher for cafeteria diet in relation to standard diet (p < 0.05). Moreover, the standard diet showed significant differences for Cl and K (p < 0.05) in comparison to cafeteria diet in kidney, and for P, S and Zn (p < 0.005) in liver.

  12. Elemental concentrations in kidney and liver of mice fed with cafeteria or standard diet determined by particle induced X-ray emission

    International Nuclear Information System (INIS)

    Dimer Leffa, Daniela; Iochims dos Santos, Carla Eliete; Debastiani, Rafaela; Amaral, Livio; Yoneama, Maria Lucia; Ferraz Dias, Johnny; Moraes Andrade, Vanessa

    2014-01-01

    The importance of trace elements in human health is well known and their main source is daily diet. Nowadays, one of the biggest issues is the presence of these micronutrients in levels much higher than required, leading to potential toxic effects. The aim of this work was to investigate the elemental content in organs of mice fed with cafeteria or standard diet using PIXE. Twelve male Swiss mice were divided into two groups: control group (standard chow) and cafeteria group (high-caloric diet). After 17 weeks, samples of different organs (kidney and liver) were collected and prepared for PIXE analysis. The Fe concentration in kidney and liver was statistically higher in animals that received the cafeteria diet (p < 0.001). The Al and Si kidney contents were significantly higher for cafeteria diet in relation to standard diet (p < 0.05). Moreover, the standard diet showed significant differences for Cl and K (p < 0.05) in comparison to cafeteria diet in kidney, and for P, S and Zn (p < 0.005) in liver

  13. Applications of X-ray emission to elemental analysis of foods

    International Nuclear Information System (INIS)

    Flocchini, R.G.; Lagunas-Solar, M.C.; Perley, B.P.

    1996-01-01

    Trace element analysis via X-Ray Fluorescence (XRF) and Proton-Induced X-Ray Emission (PIXE) techniques were applied to several samples of fresh and processed foods. Thin samples of fresh fruits and vegetables, processed dry foods, and spices were included in these analyses. The results indicate that XRF and/or PIXE analysis is applicable to these types of samples but require special and simple modifications in sample preparation techniques, and the inclusion of new matrix type corrections for data analysis. However, the non-destructive nature, reproducibility, efficiency and high sensitivity that characterize these multi-element analytical procedures can provide new potential methods for detecting trace elements in foods and in many agricultural commodities. Toxic metals such as Hg, Pb, and As were detected in some foods. In addition, other essential or neutral trace elements such as Na, K, Mg, Ca, Cu, Cr, V, Zn, Mo, Fe, Mn, Ni, Se, Cl, S, and P were also detected. These and other elements can be analyzed rapidly and with high sensitivity for applications in process control and for certification of food quality. Developing these techniques and procedures specifically for food and for various agricultural products may provide new analytical options and help mitigate the expected impact of forthcoming regulations intended to establish limits and tolerance levels for micro toxicants and other essential nutrients in foods and agricultural products. (author)

  14. Trace analysis in cadmium telluride by heavy ion induced X-ray emission and by SIMS

    International Nuclear Information System (INIS)

    Scharager, C.; Stuck, R.; Siffert, P.; Cailleret, J.; Heitz, Ch.; Lagarde, G.; Tenorio, D.

    1979-01-01

    The possibilities of using both selective heavy ion induced X-ray emission and secondary ion mass spectroscopy (SIMS), for the identification of impurities present at low concentrations in cadmium telluride are examined. The relative concentrations of the impurities along CdTe crystals have been determined by exciting the X-ray emission of the elements in several slices with Ar and Kr ions and by comparing the relative characteristic X-ray emission yields. As a consequence of the quasimolecular inner shell ionization mechanism in heavy ion-atom collisions, Ar and Kr ions allow a strong excitation of the main impurities seen by SIMS namely Si, Cl and Ge, As, with only a minor contribution of Cd and Te. From the changes of the concentrations of the various impurities along the crystal, informations about segregation coefficients and compensation can be obtained

  15. Sample preparation techniques in trace element analysis by X-ray emission spectroscopy

    International Nuclear Information System (INIS)

    Valkovic, V.

    1983-11-01

    The report, written under a research contract with the IAEA, contains a detailed presentation of the most difficult problem encountered in the trace element analysis by methods of the X-ray emission spectroscopy, namely the sample preparation techniques. The following items are covered. Sampling - with specific consideration of aerosols, water, soil, biological materials, petroleum and its products, storage of samples and their handling. Pretreatment of samples - preconcentration, ashing, solvent extraction, ion exchange and electrodeposition. Sample preparations for PIXE - analysis - backings, target uniformity and homogeneity, effects of irradiation, internal standards and specific examples of preparation (aqueous, biological, blood serum and solid samples). Sample preparations for radioactive sources or tube excitation - with specific examples (water, liquid and solid samples, soil, geological, plants and tissue samples). Finally, the problem of standards and reference materials, as well as that of interlaboratory comparisons, is discussed

  16. Capacity of X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Wobrauschek, P.; Kregsamer, P.

    1997-01-01

    X-Ray fluorescence analysis (XRF) is a powerful analytical tool for the qualitative and quantitative determination of chemical elements in a sample. Two different detection principles are accepted widely: wavelength dispersive and energy dispersive. Various sources for XRF are discussed: X-ray tubes, accelerators for particle induced XRF, radioactive isotopes, and the use of synchrotron radiation. Applications include environmental, technical, medical, fine art, and forensic studies. Due to the demands of research and application special techniques like total reflection XRF (TXRF) were developed with ultimately achievable detection limits in the femtogram region. The elements detectable by XRF range from Be to U. (author)

  17. Proton induced X-ray emission analysis of trace elements in human blood serum

    International Nuclear Information System (INIS)

    Cheek, D.B.; Hay, H.J.; Newton, C.S.

    1979-01-01

    Proton induced x-ray emission has been used for quantitative analyses of trace elements in blood serum samples. This work is part of a survey concerned with Zn, Cu, Fe, Cr, Mn and Se in Australian Aboriginal people not receiving optimal diet. Special attention is being directed to Cr because of the high incidence of diabetes mellitus in these people

  18. Proton-induced X-ray emission analysis of Jordanian cigarettes

    International Nuclear Information System (INIS)

    Hallak, A.B.

    1981-01-01

    Proton-induced X-ray emission spectroscopy was applied to determine the concentration of 11 elements in cigaretta tobacco of four brands commercially made in Jordan, and one foreign brand. The results are expressed in absolute amount per cigarette. Cigarette wrapping paper and cigarette smoke were also anlayzed. The significance of some of the elements found in the samples are discussed. (author)

  19. Analysis of the electronic structure of human hemoglobin from soft X-ray emission

    International Nuclear Information System (INIS)

    Soldatov, A.V.; Kravtsova, A.N.; Fedorovich, E.N.; Ankudinov, A.; Moewes, A.; Kurmaev, E.Z.

    2005-01-01

    We present X-ray emission spectra (XES) of human hemoglobin excited near the iron L 2,3 threshold and the nitrogen and carbon K-edges. The experiment is compared with our calculations of the corresponding spectra and gives good agreement. We find that the Fe L 3 emission is affected by the nearest nitrogen atoms located in the heme plane around the central iron atom. The distribution of the partial electronic densities of states of hemoglobin is determined

  20. High-Resolution X-ray Emission and X-ray Absorption Spectroscopy

    NARCIS (Netherlands)

    Groot, F.M.F. de

    2000-01-01

    In this review, high-resolution X-ray emission and X-ray absorption spectroscopy will be discussed. The focus is on the 3d transition-metal systems. To understand high-resolution X-ray emission and reso-nant X-ray emission, it is first necessary to spend some time discussing the X-ray absorption

  1. Observing Solvation Dynamics with Simultaneous Femtosecond X-ray Emission Spectroscopy and X-ray Scattering

    DEFF Research Database (Denmark)

    Haldrup, Kristoffer; Gawelda, Wojciech; Abela, Rafael

    2016-01-01

    and structural changes, and local solvent structural changes are desired. We have studied the intra- and intermolecular dynamics of a model chromophore, aqueous [Fe(bpy)3]2+, with complementary X-ray tools in a single experiment exploiting intense XFEL radiation as a probe. We monitored the ultrafast structural...... rearrangement of the solute with X-ray emission spectroscopy, thus establishing time zero for the ensuing X-ray diffuse scattering analysis. The simultaneously recorded X-ray diffuse scattering atterns reveal slower subpicosecond dynamics triggered by the intramolecular structural dynamics of the photoexcited...

  2. Standardization of proton-induced x-ray emission technique for analysis of thick samples

    Science.gov (United States)

    Ali, Shad; Zeb, Johar; Ahad, Abdul; Ahmad, Ishfaq; Haneef, M.; Akbar, Jehan

    2015-09-01

    This paper describes the standardization of the proton-induced x-ray emission (PIXE) technique for finding the elemental composition of thick samples. For the standardization, three different samples of standard reference materials (SRMs) were analyzed using this technique and the data were compared with the already known data of these certified SRMs. These samples were selected in order to cover the maximum range of elements in the periodic table. Each sample was irradiated for three different values of collected beam charges at three different times. A proton beam of 2.57 MeV obtained using 5UDH-II Pelletron accelerator was used for excitation of x-rays from the sample. The acquired experimental data were analyzed using the GUPIXWIN software. The results show that the SRM data and the data obtained using the PIXE technique are in good agreement.

  3. Chemical Analysis of Impurity Boron Atoms in Diamond Using Soft X-ray Emission Spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Muramatsu, Yasuji; Iihara, Junji; Takebe, Toshihiko; Denlinger, Jonathan D.

    2008-03-29

    To analyze the local structure and/or chemical states of boron atoms in boron-doped diamond, which can be synthesized by the microwave plasma-assisted chemical vapor deposition method (CVD-B-diamond) and the temperature gradient method at high pressure and high temperature (HPT-B-diamond), we measured the soft X-ray emission spectra in the CK and BK regions of B-diamonds using synchrotron radiation at the Advanced Light Source (ALS). X-ray spectral analyses using the fingerprint method and molecular orbital calculations confirm that boron atoms in CVD-B-diamond substitute for carbon atoms in the diamond lattice to form covalent B-C bonds, while boron atoms in HPT-B-diamond react with the impurity nitrogen atoms to form hexagonal boron nitride. This suggests that the high purity diamond without nitrogen impurities is necessary to synthesize p-type B-diamond semiconductors.

  4. Detection and Analysis of X Ray Emission from the Princeton-Field-Reversed Configuration (PFRC-2)

    Science.gov (United States)

    Bosh, Alexandra; Swanson, Charles; Jandovitz, Peter; Cohen, Samuel

    2016-10-01

    The PFRC is an odd-parity rotating-magnetic-field-driven field-reversed-configuration magnetic confinement experiment. Studying X rays produced via electron Bremsstrahlung with neutral particles is crucial to the further understanding of the energy and particle confinement of the PFRC. The data on the x rays are collected using a detector system comprised of two, spatially scannable Amptek XR-100 CR detectors and a Amptek XR-100 SDD detector that view the plasma column at two axial locations, one in the divertor and one near the axial midplane. These provide X-ray energy and arrival-time information. (Data analysis requires measurement of each detector's efficiency, a parameter that is modified by window transmission. Detector calibrations were performed with a custom-made X-ray tube that impinged 1-microamp 1-5 kV electron beams onto a carbon target.) From the analyzed data, the average electron energy, effective temperature, and electron density can be extracted. Spatial scans then allow the FRC's internal energy to be measured. We present recent measurements of the Bremsstrahlung spectrum from 0.8 to 6 keV and the inferred electron temperature in the PFRC device as functions of heating power, magnetic field and fill gas pressure. This work was supported, in part, by DOE Contract Number DE-AC02-09CH11466.

  5. Multielement analysis of minerals from Madagascar by X-ray emission induced by protons and gamma rays

    International Nuclear Information System (INIS)

    Rakotoarisoa, C.

    1990-12-01

    This study is a part of a large multidisciplinary program for the study of soil formation in the south east of Madagascar near the uranothorianite deposit of Tranomaro explaining the particular interest for rare earths, uranium and thorium. X-ray emission principles and physical processes of a X-ray spectra are briefly recalled. The choice of analysis method depends upon sensitivity simplicity and rapidity. Experimental techniques are described and results obtained are discussed. Methods used for qualitative and quantitative interpretation of spectra are exposed. In conclusion performance and limits of the method are examined [fr

  6. Environmental aspects of ion-induced x-ray emission by infinitely thick targets

    International Nuclear Information System (INIS)

    Van Rinsvelt, H.A.; Dunnam, F.E.; Russell, J.P.; Bolch, W.E.

    1974-01-01

    Elemental analysis through proton and alpha particle induced x-ray emission by infinitely thick samples of environmental interest was found to be feasible. A quantization technique using internal standards and the optimization of the beam energy for optimal sensitivity were investigated. The average limit of detection ranges from about 0.1 ppM for calcium to 1 ppM for strontium

  7. Metrology and X-rays emissions

    International Nuclear Information System (INIS)

    Chancel, C.; Schirmann, D.

    1993-01-01

    This scientific journal explains different technologies used to study X-rays emissions hot dense plasmas created by laser at the Dam center of Limeil-Valenton (CEL-V) or created by nuclear fire in the Pacific

  8. Proton exciting X ray analysis

    International Nuclear Information System (INIS)

    Ma Xinpei

    1986-04-01

    The analyzing capability of proton exciting X ray analysis for different elements in organisms was discussed, and dealing with examples of trace element analysis in the human body and animal organisms, such as blood serum, urine, and hair. The sensitivity, accuracy, and capability of multielement analysis were discussed. Its strong points for the trace element analysis in biomedicine were explained

  9. X-ray emission from comets

    International Nuclear Information System (INIS)

    Dennerl, Konrad

    1999-01-01

    When comet Hyakutake (C/1996 B2) encountered Earth in March 1996 at a minimum distance of only 15 million kilometers (40 times the distance of the moon), x-ray and extreme ultraviolet emission was discovered for the first time from a comet. The observations were performed with the astronomy satellites ROSAT and EUVE. A systematic search for x-rays from comets in archival data, obtained during the ROSAT all-sky survey in 1990/91, resulted in the discovery of x-ray emission from four additional comets. They were detected at seven occasions in total, when they were optically 300 to 30 000 times fainter than Hyakutake. These findings indicated that comets represent a new class of celestial x-ray sources. Subsequent detections of x-ray emission from additional comets with the satellites ROSAT, EUVE, and BeppoSAX confirmed this conclusion. The x-ray observations have obviously revealed the presence of a process in comets which had escaped attention until recently. This process is most likely charge exchange between highly charged heavy ions in the solar wind and cometary neutrals. The solar wind, a stream of particles continuously emitted from the sun with ≅ 400 km s -1 , consists predominantly of protons, electrons, and alpha particles, but contains also a small fraction (≅0.1%) of highly charged heavier ions, such as C 6+ ,O 6+ ,Ne 8+ ,Si 9+ ,Fe 11+ . When these ions capture electrons from the cometary gas, they attain highly excited states and radiate a large fraction of their excitation energy in the extreme ultraviolet and x-ray part of the spectrum. Charge exchange reproduces the intensity, the morphology and the spectrum of the observed x-ray emission from comets very well

  10. Repeated pulsed x-ray emission equipment

    International Nuclear Information System (INIS)

    Terauchi, Hikaru; Iida, Satoshi

    1982-01-01

    X-ray diffraction technique has been applied to determine the spatial positions of atoms which compose a material, and it is needless to say that the technique is a fundamental means regardless of the fields of research. However, the application of X-ray diffraction to the research on physical properties has been so far limited to know the spatial positions of atoms or molecules under thermal equilibrium condition. The addition of time element to the conventional technique, that is, the analysis of material structure including the time-varying processes under non-equilibrium conditions, is considered to approach the elucidation of the essence of materials. The authors call this dynamic structural analysis. The authors have planned to analyze X-ray diffraction intensity which has the resolution of about 10 -8 s in the real time which is conjugate with energy. However, present pulsed X-ray sources are not suitable for diffraction experiment because the pulse width is too long or X-ray wavelength is too short. Accordingly, the authors have made for trial a pulsed X-ray source for diffraction experiment. Its specifications are: diode voltage (X-ray tube voltage) from 200 to 300 kV, diode current from 2 to 5 kA, pulse width of about 30ns, maximum repetition frequency 10 pps, and X-ray focus size of 2 mm diameter. One of the features of this source is the repeated generation of pulsed X-ray. This is the first trial in the world, and is indispensable to the dynamic structural analysis described above. The quality of the emitted X-ray is also written. (Wakatsuki, Y.)

  11. Trace determination of heavy metal concentrations in fauna, flora and salt samples from Black Sea waters by charged particles - induced X-rays

    International Nuclear Information System (INIS)

    Badica, T.; Ciortea, C.; Dima, S.; Petrovici, A.; Popescu, I.; Serbanescu, O.

    1977-01-01

    Studies were performed on Black Sea pollution by charged particles induced X-rays spectra analysis, using alpha and 16 O beams. Fauna, flora and salt samples were analysed. We found some of the concentrations of pollutant elements to be below the accepted levels. (author)

  12. X-ray system analysis

    International Nuclear Information System (INIS)

    Shapiro, J.S.

    1985-01-01

    An X-ray system tester for measuring anode voltage, cathode voltage, anode current, filament current and line voltage in an X-ray system has a selector which couples one of these analog signals or one of a plurality of processing control signals entered by an operator from a control panel to a digitizing section selectively in accordance with control signals provided to the selector by a computing section. The digitizing section converts the selected signal into a train of pulses having a frequency proportional to the value of the selected signal. These pulses are counted, the counts being used by the computing section to determine the value of the selected signal. This computed value is stored in a computing memory section of the computing section. The computing section is adapted to store a plurality of the sets of signals produced during a corresponding sequence of operational intervals of the X-ray system and determines a measure of the deviation of any selected one of the stored electrical signals over the sequence of operating intervals. Each signal produced during the sequential operational intervals can be recalled to aid analysis of the operation of the X-ray system. (author)

  13. Analysis of the X-ray emission spectra of copper, germanium and rubidium plasmas produced at the Phelix laser facility

    Science.gov (United States)

    Comet, M.; Pain, J.-C.; Gilleron, F.; Piron, R.; Denis-Petit, D.; Méot, V.; Gosselin, G.; Morel, P.; Hannachi, F.; Gobet, F.; Tarisien, M.; Versteegen, M.

    2017-03-01

    We present the analysis of X-ray emission spectra of copper, germanium and rubidium plasmas measured at the Phelix laser facility. The laser intensity was around 6×1014 W.cm-2. The analysis is based on the hypothesis of an homogeneous plasma in local thermodynamic equilibrium using an effective temperature. This temperature is deduced from hydrodynamic simulations and collisional-radiative computations. Spectra are then calculated using the LTE opacity codes OPAMCDF and SCO-RCG and compared to experimental data.

  14. Analysis of borophosphosilicate glass layers on silicon wafers by X-ray emission from photon and electron excitation

    International Nuclear Information System (INIS)

    Elgersma, O.; Borstrok, J.J.M.

    1989-01-01

    Phosphorus and oxygen concentrations in the homogeneous layer of borosilicate glass (BPSG) deposited on Si-integrated circuits are determined by X-ray fluorescence from photon excitation. The X-ray emission from electron excitation in an open X-ray tube instrument yields a sufficiently precise determination of the boron content. The thickness of the layer can be derived from silicon Kα-fluorescence. A calibration model is proposed for photon as well as for electron excitation. The experimentally determined parameters in this model well agree with those derived from fundamental parameters for X-ray absorption and emission. The chemical surrounding of silicon affects strongly the peak profile of the silicon Kβ-emission. This enables to distinguish emission from the silicon atoms in the wafer and from the silicon atoms in the silicon oxide complexes of the BPSG-layer. (author)

  15. A moving target for accelerated charged particle induced X-ray measurement

    International Nuclear Information System (INIS)

    Chuang, L.S.; Shima, K.; Ebihara, H.; Seki, R.; Mikumo, T.

    1980-01-01

    To attain good reproducibility as well as to enable an absolute determination in the measurement of X-ray fluorescences, resulting from bombardment of a heterogeneous sample by accelerated charged particles, a moving-target mechanism incorporating an electronic remote control system has been devised. The system is designed to scan the whole sample area with a chosen constant linear speed, by a fixed particle beam with a cross-sectional area a small fraction of that of the sample. Using 16 MeV protons and 40 MeV oxygen-ion beams, test runs of this system showed that the attempted objectives are attainable with good accuracies: reproducibility of the data for a given target is better than 3%, the linearity of the calibration curve is in good agreement, within the weighing errors of the standard elements and the uncertainty due to beam current fluctuation, with the expected values, and the results of absolute determinations using both metal foils and heterogeneous powder samples are in good agreement with accepted results using different methods. Detailed accounts of the moving-target system, and the test for reproducibility and linearity are presented. An absolute determination of the quantities related to accelerated charged-particle induced X-ray fluorescence (PIXE) using the moving target is presented for samples in different forms. (orig./HP)

  16. Boron analysis for neutron capture therapy using particle-induced gamma-ray emission

    International Nuclear Information System (INIS)

    Nakai, Kei; Yamamoto, Yohei; Okamoto, Emiko; Yamamoto, Tetsuya; Yoshida, Fumiyo; Matsumura, Akira; Yamada, Naoto; Kitamura, Akane; Koka, Masashi; Satoh, Takahiro

    2015-01-01

    The neutron source of BNCT is currently changing from reactor to accelerator, but peripheral facilities such as a dose-planning system and blood boron analysis have still not been established. To evaluate the potential application of particle-induced gamma-ray emission (PIGE) for boron measurement in clinical boron neutron capture therapy, boronophenylalanine dissolved within a cell culture medium was measured using PIGE. PIGE detected 18 μgB/mL f-BPA in the culture medium, and all measurements of any given sample were taken within 20 min. Two hours of f-BPA exposure was required to create a boron distribution image. However, even though boron remained in the cells, the boron on the cell membrane could not be distinguished from the boron in the cytoplasm. - Highlights: • PIGE was evaluated for measuring blood boron concentration during clinical BNCT. • PIGE detected 18 μgB/mL f-BPA in culture medium. • All measurements of any given sample were taken within 20 min. • Two hours of f-BPA exposure is required to create boron distribution image by PIGE. • Boron on the cell membrane could not be distinguished from boron in the cytoplasm.

  17. X-ray emission from hot plasma

    International Nuclear Information System (INIS)

    Hayakawa, Satio; Kato, Takako.

    1979-01-01

    X-ray emission from hot plasmas is discussed with a critical review of different theories. The results given in the present paper are complementary to those given by Kato in the sense that the present paper is introductory to the paper by Kato. The contents of the present paper are; 1. Introduction 2. Ionization and Recombination Rate Coefficients 3. Relative Abundances of Ions 4. Intensity and Spectra of Radiation 5. Comparison with Earlier Results 6. Emission and Absorption Lines (author)

  18. New applications of elemental analysis methods using X-rays at the INPE Cyclotron

    International Nuclear Information System (INIS)

    Constantinescu, B.; Constantin, F.; Dima, S.; Plostinaru, D.; Popa-Simil, L.

    1990-01-01

    Some results in various samples elemental analysis using PIXE(Particle Induced X-ray Emission) method at INPE U-120 Cyclotron are presented. The main purpose of the research was the determination of metal concentration (Ca,Cr,Mn,Fe,Ni,Cu,Zn) in drug industry materials and products, some tree seeds as environmental pollution indicator, mineral oil and gasoline used in mechanical engineering, cooling water for oil industry equipment. (Author)

  19. X-ray photoelectron emission spectromicroscopic analysis of arborescent lycopsid cell wall composition and Carboniferous coal ball preservation

    Energy Technology Data Exchange (ETDEWEB)

    Boyce, C. Kevin [Department of the Geophysical Sciences, University of Chicago, Chicago, IL 60637 (United States); Abrecht, Mike; Zhou, Dong; Gilbert, P.U.P.A. [Department of Physics, University of Wisconsin, Madison, WI 53706 (United States)

    2010-08-01

    Two alternative processes complicate understanding of the biochemical origins and geochemical alteration of organic matter over geologic time: selective preservation of original biopolymers and in situ generation of new geopolymers. One of the best constrained potential sources of bio- and geochemical information about extinct fossil plants is frequently overlooked. Permineralized anatomically preserved plant fossils allow analysis of individual cell and tissue types that have an original biochemical composition already known from living plants. The original composition of more enigmatic fossils can be constrained by geochemical comparisons to tissues of better understood fossils from the same locality. This strategy is possible using synchrotron-based techniques for submicron-scale imaging with X-rays over a range of frequencies in order to provide information concerning the relative abundance of different organic bonds with X-ray Absorption Near Edge Spectroscopy. In this study, X-ray PhotoElectron Emission spectroMicroscopy (X-PEEM) was used to analyze the tissues of Lepidodendron, one of the lycopsid trees that were canopy dominants of many Pennsylvanian coal swamp forests. Its periderm or bark - the single greatest biomass contributor to many Late Paleozoic coals - is found to have a greater aliphatic content and an overall greater density of organic matter than lignified wood. Because X-PEEM allows simultaneous analysis of organic matter and matrix calcite in fully mineralized fossils, this technique also has great potential for analysis of fossil preservation, including documentation of significant traces of organic matter entrained in the calcite crystal fabric that fills the cell lumens. (author)

  20. Stimulated X-Ray Emission Spectroscopy in Transition Metal Complexes

    Science.gov (United States)

    Kroll, Thomas; Weninger, Clemens; Alonso-Mori, Roberto; Sokaras, Dimosthenis; Zhu, Diling; Mercadier, Laurent; Majety, Vinay P.; Marinelli, Agostino; Lutman, Alberto; Guetg, Marc W.; Decker, Franz-Josef; Boutet, Sébastien; Aquila, Andy; Koglin, Jason; Koralek, Jake; DePonte, Daniel P.; Kern, Jan; Fuller, Franklin D.; Pastor, Ernest; Fransson, Thomas; Zhang, Yu; Yano, Junko; Yachandra, Vittal K.; Rohringer, Nina; Bergmann, Uwe

    2018-03-01

    We report the observation and analysis of the gain curve of amplified K α x-ray emission from solutions of Mn(II) and Mn(VII) complexes using an x-ray free electron laser to create the 1 s core-hole population inversion. We find spectra at amplification levels extending over 4 orders of magnitude until saturation. We observe bandwidths below the Mn 1 s core-hole lifetime broadening in the onset of the stimulated emission. In the exponential amplification regime the resolution corrected spectral width of ˜1.7 eV FWHM is constant over 3 orders of magnitude, pointing to the buildup of transform limited pulses of ˜1 fs duration. Driving the amplification into saturation leads to broadening and a shift of the line. Importantly, the chemical sensitivity of the stimulated x-ray emission to the Mn oxidation state is preserved at power densities of ˜1020 W /cm2 for the incoming x-ray pulses. Differences in signal sensitivity and spectral information compared to conventional (spontaneous) x-ray emission spectroscopy are discussed. Our findings build a baseline for nonlinear x-ray spectroscopy for a wide range of transition metal complexes in inorganic chemistry, catalysis, and materials science.

  1. X-Ray Emission Properties of Supernova Remnants

    NARCIS (Netherlands)

    Vink, J.; Alsabti, A.W.; Murdin, P.

    2016-01-01

    X-ray emission from supernova remnants can be broadly divided into thermal X-ray emission from the shock-heated plasmas and in nonthermal (synchrotron) emission caused by very high-energy (10–100 TeV) electrons moving in the magnetic fields of the hot plasmas. The thermal X-ray emission of young

  2. The determination of trace elements in commercial human serum albumin solutions by proton-induced X-ray emission spectrometry and neutron activation analysis

    International Nuclear Information System (INIS)

    Maenhaut, W.; De Reu, L.; Tomza, U.; Versieck, J.

    1982-01-01

    Particle induced X-ray emission (p.i.x.e.) and neutron activation analysis (n.a.a.) are proposed for determining the trace element content of human serum albumin. Application of these methods to some commercial albumin solutions provided concentration data for up to 19 elements, most of which were present at a level below a few μg ml -1 . The precision of the p.i.x.e. technique, as determined by irradiating up to 20 targets from one sample, was about 3% for those elements where counting statistics were good. A comparison between the p.i.x.e. and n.a.a. results showed close agreement, indicating that p.i.x.e. can yield data which are accurate to within 10%. Neutron activation showed very good sensitivity for the elements producing long-lived nuclides (tsub(1/2) >= 3 days), but had rather high detection limits for the other elements, unless radiochemical separations were used. (Auth.)

  3. Analysis of hard X-ray emission from selected very high energy {gamma}-ray sources observed with INTEGRAL

    Energy Technology Data Exchange (ETDEWEB)

    Hoffmann, Agnes Irene Dorothee

    2009-11-13

    A few years ago, the era of very high energy {gamma}-ray astronomy started, when the latest generation of Imaging Atmospheric Cherenkov Telescopes (IACT) like H.E.S.S. began to operate and to resolve the sources of TeV emission. Identifications via multi-wavelength studies reveal that the detected sources are supernova remnants and active galactic nuclei, but also pulsar wind nebulae and a few binaries. One widely discussed open question is, how these sources are able to accelerate particles to such high energies. The understanding of the underlying particle distribution, the acceleration processes taking place, and the knowledge of the radiation processes which produce the observed emission, is, therefore, of crucial interest. Observations in the hard X-ray domain can be a key to get information on these particle distributions and processes. Important for this thesis are the TeV and the hard X-ray range. The two instruments, H.E.S.S. and INTEGRAL, whose data were used, are, therefore, described in detail. The main part of this thesis is focused on the X-ray binary system LS 5039/RX J1826.2-1450. It was observed in several energy ranges. The nature of the compact object is still not known, and it was proposed either to be a microquasar system or a non-accreting pulsar system. The observed TeV emission is modulated with the orbital cycle. Several explanations for this variability have been discussed in recent years. The observations with INTEGRAL presented in this thesis have provided new information to solve this question. Therefore, a search for a detection in the hard X-ray range and for its orbital dependence was worthwhile. Since LS 5039 is a faint source and the sky region where it is located is crowded, a very careful, non-standard handling of the INTEGRAL data was necessary, and a cross-checking with other analysis methods was essential to provide reliable results. We found that LS 5039 is emitting in the hard X-ray energy range. A flux rate and an upper

  4. Analysis of hard X-ray emission from selected very high energy γ-ray sources observed with INTEGRAL

    International Nuclear Information System (INIS)

    Hoffmann, Agnes Irene Dorothee

    2009-01-01

    A few years ago, the era of very high energy γ-ray astronomy started, when the latest generation of Imaging Atmospheric Cherenkov Telescopes (IACT) like H.E.S.S. began to operate and to resolve the sources of TeV emission. Identifications via multi-wavelength studies reveal that the detected sources are supernova remnants and active galactic nuclei, but also pulsar wind nebulae and a few binaries. One widely discussed open question is, how these sources are able to accelerate particles to such high energies. The understanding of the underlying particle distribution, the acceleration processes taking place, and the knowledge of the radiation processes which produce the observed emission, is, therefore, of crucial interest. Observations in the hard X-ray domain can be a key to get information on these particle distributions and processes. Important for this thesis are the TeV and the hard X-ray range. The two instruments, H.E.S.S. and INTEGRAL, whose data were used, are, therefore, described in detail. The main part of this thesis is focused on the X-ray binary system LS 5039/RX J1826.2-1450. It was observed in several energy ranges. The nature of the compact object is still not known, and it was proposed either to be a microquasar system or a non-accreting pulsar system. The observed TeV emission is modulated with the orbital cycle. Several explanations for this variability have been discussed in recent years. The observations with INTEGRAL presented in this thesis have provided new information to solve this question. Therefore, a search for a detection in the hard X-ray range and for its orbital dependence was worthwhile. Since LS 5039 is a faint source and the sky region where it is located is crowded, a very careful, non-standard handling of the INTEGRAL data was necessary, and a cross-checking with other analysis methods was essential to provide reliable results. We found that LS 5039 is emitting in the hard X-ray energy range. A flux rate and an upper flux

  5. X-ray fluorescence spectrometric and optical emission spectographic analysis of thoria in thoriated copper metal powder

    International Nuclear Information System (INIS)

    Chandola, L.C.; Khanna, P.P.

    1984-01-01

    Two methods, one using the X-ray fluorescence (XRF) spectrometric technique and another using optical emission spectrographic (OES) technique are described for the determination of thoria in the concentration range 0.5-10% in thoriated copper metal powder. The precision of XRF method is superior to OES method but when sample quantity is very small, the OES method is useful. For XRF method, 500 mg sample is mixed with boric acid binding material and converted to a tablet for analysis. For OES method, only 200 mg sample is needed which is glued to the flat ends of two graphite electrodes for excitation by AC arc. The precision obtained in XRF is better than +-1% and in OES it is +-23%. (author)

  6. Synchrotron-Radiation Induced X-Ray Emission (SRIXE)

    Energy Technology Data Exchange (ETDEWEB)

    Jones, Keith W.

    1999-09-01

    Elemental analysis using emission of characteristic x rays is a well-established scientific method. The success of this analytical method is highly dependent on the properties of the source used to produce the x rays. X-ray tubes have long existed as a principal excitation source, but electron and proton beams have also been employed extensively. The development of the synchrotron radiation x-ray source that has taken place during the past 40 years has had a major impact on the general field of x-ray analysis. Even tier 40 years, science of x-ray analysis with synchrotron x-ray beams is by no means mature. Improvements being made to existing synchrotron facilities and the design and construction of new facilities promise to accelerate the development of the general scientific use of synchrotron x-ray sources for at least the next ten years. The effective use of the synchrotron source technology depends heavily on the use of high-performance computers for analysis and theoretical interpretation of the experimental data. Fortunately, computer technology has advanced at least as rapidly as the x-ray technology during the past 40 years and should continue to do so during the next decade. The combination of these technologies should bring about dramatic advances in many fields where synchrotron x-ray science is applied. It is interesting also to compare the growth and rate of acceptance of this particular research endeavor to the rates for other technological endeavors. Griibler [1997] cataloged the time required for introduction, diffusion,and acceptance of technological, economic, and social change and found mean values of 40 to 50 years. The introduction of the synchrotron source depends on both technical and non-technical factors, and the time scale at which this seems to be occurring is quite compatible with what is seen for other major innovations such as the railroad or the telegraph. It will be interesting to see how long the present rate of technological change

  7. Synchrotron-Radiation Induced X-Ray Emission (SRIXE)

    International Nuclear Information System (INIS)

    Jones, Keith W.

    1999-01-01

    Elemental analysis using emission of characteristic x rays is a well-established scientific method. The success of this analytical method is highly dependent on the properties of the source used to produce the x rays. X-ray tubes have long existed as a principal excitation source, but electron and proton beams have also been employed extensively. The development of the synchrotron radiation x-ray source that has taken place during the past 40 years has had a major impact on the general field of x-ray analysis. Even tier 40 years, science of x-ray analysis with synchrotron x-ray beams is by no means mature. Improvements being made to existing synchrotron facilities and the design and construction of new facilities promise to accelerate the development of the general scientific use of synchrotron x-ray sources for at least the next ten years. The effective use of the synchrotron source technology depends heavily on the use of high-performance computers for analysis and theoretical interpretation of the experimental data. Fortunately, computer technology has advanced at least as rapidly as the x-ray technology during the past 40 years and should continue to do so during the next decade. The combination of these technologies should bring about dramatic advances in many fields where synchrotron x-ray science is applied. It is interesting also to compare the growth and rate of acceptance of this particular research endeavor to the rates for other technological endeavors. Griibler [1997] cataloged the time required for introduction, diffusion,and acceptance of technological, economic, and social change and found mean values of 40 to 50 years. The introduction of the synchrotron source depends on both technical and non-technical factors, and the time scale at which this seems to be occurring is quite compatible with what is seen for other major innovations such as the railroad or the telegraph. It will be interesting to see how long the present rate of technological change

  8. X-ray Emission Line Spectroscopy of Nearby Galaxies

    Science.gov (United States)

    Wang, Daniel

    What are the origins of the diffuse soft X-ray emission from non-AGN galaxies? Preliminary analysis of XMM-Newton RGS spectra shows that a substantial fraction of the emission cannot arise from optically-thin thermal plasma, as commonly assumed, and may originate in charge exchange at the interface with neutral gas. We request the support for a comprehensive observing, data analysis, and modeling program to spectroscopically determine the origins of the emission. First, we will use our scheduled XMM-Newton AO-10 368 ks observations of the nearest compact elliptical galaxy M32 to obtain the first spectroscopic calibration of the cumulative soft X-ray emission from the old stellar population and will develop a spectral model for the charge exchange, as well as analysis tools to measure the spatial and kinematic properties of the X-ray line- emitting plasma. Second, we will characterize the truly diffuse emission from the hot plasma and/or its interplay with the neutral gas in a sample of galactic spheroids and active star forming/starburst regions in nearby galaxies observed by XMM-Newton. In particular, we will map out the spatial distributions of key emission lines and measure (or tightly constrain) the kinematics of hot plasma outflows for a few X-ray-emitting regions with high-quality RGS data. For galaxies with insufficient counting statistics in individual emission lines, we will conduct a spectral stacking analysis to constrain the average properties of the X-ray-emitting plasma. We will use the results of these X-ray spectroscopic analyses, together with complementary X-ray CCD imaging/spectral data and observations in other wavelength bands, to test the models of the emission. In addition to the charge exchange, alternative scenarios such as resonance scattering and relic AGN photo-ionization will also be examined for suitable regions. These studies are important to the understanding of the relationship between the diffuse soft X-ray emission and various

  9. Utilization of synchrotron radiation in analytical chemistry. Soft X-ray emission and absorption spectroscopy

    International Nuclear Information System (INIS)

    Muramatsu, Yasuji

    2015-01-01

    Synchrotron soft X-ray spectroscopy includes three major types of spectroscopy such as X-ray absorption spectroscopy (XAS), X-ray emission spectroscopy (XES), and X-ray photoelectron spectroscopy (XPS). This paper takes up XAS and XES of soft X-rays, and briefly describes the principle. XAS is roughly classified into XANES (X-ray absorption near-edge structure) and EXAFS (extended X-ray absorption fine structure), and XANES is mainly used in the analysis based on XAS of soft X-rays. As the examples of the latest soft X-ray analyses, the following are introduced: (1) bandgap of boron implantation diamond and the local structure of boron, (2) catalytic sites in solid fuel cell carbon electrode, and (3) soft X-ray analysis under atmospheric pressure. (A.O.)

  10. Elemental trace analysis of hepatomas and normal tissues by proton induced x-ray emission spectroscopy

    International Nuclear Information System (INIS)

    Matsuzawa, Taiju; Shishido, Fumio; Sera, Koichiro; Sato, Tachio; Morita, Tasuku.

    1977-01-01

    Specimens taken from liver, brain, serum and ascites hepatoma 130 in rats, were bombarded with 3.5 MeV protons accelerated by a Van de graaff generator, and the induced x-ray fluorescence was analysed with a Si(Li) detector. Absolute concentrations were determined with reference to a known concentration of uranium in the specimen. Small amounts of Ga, Yb and Tl which are known as metals having tumor affinity were injected into rats implanted with ascites hepatoma and several of its derivatives. Twenty-four hours after injection, liver, brain, serum and hepatoma were removed from the rats and these specimens were analysed by the same method. Relative concentrations of Fe, Cu, Zn and Br in liver, brain, serum and hepatoma specimens showed characteristic patterns. Patterns of liver and ascites hepatoma were quite similar, but the total amount of metals in liver was greater. The serum contained a large quantity of Br. Each AH 130 tumor cell line and its derivatives showed a different accumulation rate for Ga, Yb and Tl. Tl accumulated peculiarly in the brain. There was excellent co-relation between the concentrations of the elements and the biological characteristics of the tumor. (Evans, J.)

  11. Detailed analysis of hollow ions spectra from dense matter pumped by X-ray emission of relativistic laser plasma

    International Nuclear Information System (INIS)

    Hansen, S. B.; Colgan, J.; Abdallah, J.; Faenov, A. Ya.; Pikuz, S. A.; Skobelev, I. Yu.; Wagenaars, E.; Culfa, O.; Dance, R. J.; Tallents, G. J.; Rossall, A. K.; Woolsey, N. C.; Booth, N.; Lancaster, K. L.; Evans, R. G.; Gray, R. J.; McKenna, P.; Kaempfer, T.; Schulze, K. S.; Uschmann, I.

    2014-01-01

    X-ray emission from hollow ions offers new diagnostic opportunities for dense, strongly coupled plasma. We present extended modeling of the x-ray emission spectrum reported by Colgan et al. [Phys. Rev. Lett. 110, 125001 (2013)] based on two collisional-radiative codes: the hybrid-structure Spectroscopic Collisional-Radiative Atomic Model (SCRAM) and the mixed-unresolved transition arrays (MUTA) ATOMIC model. We show that both accuracy and completeness in the modeled energy level structure are critical for reliable diagnostics, investigate how emission changes with different treatments of ionization potential depression, and discuss two approaches to handling the extensive structure required for hollow-ion models with many multiply excited configurations

  12. X-Ray-Driven Gamma Emission

    International Nuclear Information System (INIS)

    Carroll, J. J.; Karamian, S. A.; Rivlin, L. A.; Zadernovsky, A. A.

    2001-01-01

    X-ray-driven gamma emission describes processes that may release nuclear energy in a 'clean' way, as bursts of incoherent or coherent gamma rays without the production of radioactive by-products. Over the past decade, studies in this area, as a part of the larger field of quantum nucleonics, have gained tremendous momentum. Since 1987 it has been established that photons could trigger gamma emission from a long-lived metastable nuclear excited state of one nuclide and it appears likely that triggering in other isotopes will be demonstrated conclusively in the near future. With these experimental results have come new proposals for the creation of collective and avalanche-like incoherent gamma-ray bursts and even for the ultimate light source, a gamma-ray laser. Obviously, many applications would benefit from controlled bursts of gamma radiation, whether coherent or not. This paper reviews the experimental results and concepts for the production of gamma rays, driven by externally produced X-rays

  13. Radionuclide X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Cechak, T.

    1994-01-01

    The author's achievements in the title field are summarized and discussed. The following topics are dealt with: (i) principles of radionuclide X-ray fluorescence analysis; (ii) mathematical methods in X-ray fluorescence analysis; (iii) Ross differential filters; (iv) application of radionuclide X-ray fluorescence analysis in the coal industry (with emphasis on the determination of the ash content, sulfur content, and arsenic content of coal); and (v) evaluation of the X-ray fluorescence analyzer from the radiological safety point of view. (P.A.)

  14. The X-ray emission spectrum of gaseous acetylene

    International Nuclear Information System (INIS)

    Brammer, R.; Rubensson, J.E.; Wassdahl, N.; Nordgren, J.

    1987-01-01

    The X-ray emission spectrum of acetylene in the gas phase has been recorded using a 10 m grazing incidence spectrometer. Analysis of the spectrum is made based on calculations of total energies, potential curves and Franck-Condon vibrational intensities. Four emission bands are seen with the 1 π u band exhibiting vibrational structure. Analysis of the vibrations gives the CIs ionization energy. High energy satellite structure is observed and interpreted. (orig.)

  15. The trace element analysis of ancient Indian coins using proton induced x-ray emission (PIXE) technique

    International Nuclear Information System (INIS)

    PURI, N.K.; HAJIVALIEI, M.; BEDI, S.C.; SINGH, N.; GOVIL, I.M.; GARG, M.L.; HANDA, D.K.; GOVIL, K.L.; ROUT, B.; VIJAYAN, V.

    2004-01-01

    Elemental analysis of ancient Indian coins viz. thirty-three punched marked coins (6 th century B.C.), fifty-nine coins belonging to Kusanas (78-250 A.D) and twenty-five coins belonging to medieval period (11 th -14 th century A.D), from India have been analysed using Proton Induced X-ray Emission (PIXE) technique. The elements namely S, Ca, Fe, Ag, Cu, Ni and Pb were detected in most of the punch-marked coins while elements namely S, Cl, K, Ca, Ti, Cr, Mn, Fe, Ni, Cu, As and Zn were detected in most of the Kusanas coins and the S, Ca, Fe, Cu, Ag, Sn, Pb were detected in 11 th -14 th century A.D. coins. Based on the elemental analysis different hypotheses put forward in the earlier literature were examined. This is the first attempt where reasonable number of ancient coins belonging to different periods were analysed by modern non destructive multi-elemental technique such as PIXE and has put the importance of the elemental analysis of ancient Indian coins in the proper perspective

  16. X-ray trace element analysis with positive ion beams

    International Nuclear Information System (INIS)

    Davis, R.H.

    1973-01-01

    A new trace element analysis having the advantage that many elements may be detected in a single measurement, based on positive charged particle induced X-ray florescence and on the production of X-rays by heavy ions, is described. Because of the large cross-sections for the production of discrete X-ray and the low yield of continuum radiation, positive charged particle X-ray florescence is a competitive, fast, analytic tool. In the experiment a beam of positive charged particles from an accelerator was directed toward a target. X-rays induced by the bombardment were detected by a Si(Li) detector the ouput from which was amplified and sorted in a multichannel analyzer. For rapid data handling and analysis, the multichannel analyzer or ADC unit was connected to an on-line computer. A large variety of targets prepared in collaboration with the oceanographers have been studied and spectra obtained for different particles having the same velocity are presented to show that the yield of discrete X-rays increases at least as rapidly as Z 2 . While protons of several MeV appear to be already competitive further advantage may be gained by heavy ions at lower energies since the continuum is reduced while the peak ''signals'' retain strength due to the Z 2 dependence. (S.B.)

  17. Exploratory study using proton induced X-ray emission analysis and histopathological techniques to determine the toxic burden of environmental pollutants

    International Nuclear Information System (INIS)

    Ejaz, Sohail; Ashraf, Muhammad; Shakir, Lubna; Ahmad, Nisar

    2012-01-01

    The aim of this novel research was to determine the toxic burden of increased elements in water resources on the inhabitant wild animals (squirrels, turtles, bats), using particle induced x-ray emission (PIXE) and histopathological approaches. PIXE analysis of skin, muscle, lung, liver and kidney revealed significant increase in Al, Cl, Fe, Mg, Mn, Si and V. Moreover, data clearly reflect a significant (P < 0.001) deposition of toxic elements (Al, Cl, Fe and K) in the lung producing interstitial/proliferative pneumonitis, intra-alveolar hemorrhages, and thickening of alveolar capillary walls. The results obtained from the liver samples emphasized that majority of the animals were intoxicated with Cl, Mg, S, Si and V, which have produced profound deterioration and swelling of the hepatocytes. Likewise, histopathology of the kidney sections spotlighted severe nephritis and degenerative changes, which could be associated with the elevated amount of Al, Cl and Mg. This data undoubtedly provide relevant information on the heavy burden of toxic elements and their pathological outcomes in wild animals and highlight their potential risks for human exposure. Thus, the information provided is critical for developing effective strategies in dealing with health hazards associated with elemental exposures. Highlights: ► The aim of this study was to determine environmental burden on wild animals. ► Elemental load was determined by PIXE and histological techniques. ► Lungs and liver were most affected organs. ► Environmental pollution is the main cause of different degenerative changes. - Toxic burden of environmental pollutants on wild animals

  18. Automated x-ray fluorescence analysis

    International Nuclear Information System (INIS)

    O'Connell, A.M.

    1977-01-01

    A fully automated x-ray fluorescence analytical system is described. The hardware is based on a Philips PW1220 sequential x-ray spectrometer. Software for on-line analysis of a wide range of sample types has been developed for the Hewlett-Packard 9810A programmable calculator. Routines to test the system hardware are also described. (Author)

  19. Image analysis in x-ray cinefluorography

    Energy Technology Data Exchange (ETDEWEB)

    Ikuse, J; Yasuhara, H; Sugimoto, H [Toshiba Corp., Kawasaki, Kanagawa (Japan)

    1979-02-01

    For the cinefluorographic image in the cardiovascular diagnostic system, the image quality is evaluated by means of MTF (Modulation Transfer Function), and object contrast by introducing the concept of x-ray spectrum analysis. On the basis of these results, further investigation is made of optimum X-ray exposure factors set for cinefluorography and the cardiovascular diagnostic system.

  20. X-ray emission lines from photoionized plasmas

    International Nuclear Information System (INIS)

    Liedahl, D.A.

    1992-11-01

    Plasma emission codes have become a standard tool for the analysis of spectroscopic data from cosmic X-ray sources. However, the assumption of collisional equilibrium, typically invoked in these codes, renders them inapplicable to many important astrophysical situations, particularly those involving X-ray photoionized nebulae, which are likely to exist in the circumsource environments of compact X-ray sources. X-ray line production in a photoionized plasma is primarily the result of radiative cascades following recombination. Through the development of atomic models of several highly-charged ions, this work extends the range of applicability of discrete spectral models to plasmas dominated by recombination. Assuming that ambient plasma conditions lie in the temperature range 10 5 --10 6 K and the density range 10 11 --10 16 cm -3 , X-ray line spectra are calculated over the wavelength range 5--45 angstrom using the HULLAC atomic physics package. Most of the work focuses on the Fe L-shell ions. Line ratios of the form (3s-2p)/(3d-2p) are shown to characterize the principal mode of line excitation, thereby providing a simple signature of photoionization. At electron densities exceeding 10 12 cm -3 , metastable state populations in the ground configurations approach their LTE value, resulting in the enrichment of the Fe L-shell recombination spectrum and a set of density-sensitive X-ray line ratios. Radiative recombination continua and emission lines produced selectively by Δn = 0 dielectronic recombination are shown to provide two classes of temperature diagnostics. Because of the extreme overionization, the recombination continua are expected to be narrow (ΔE/E much-lt 1), with ΔE = kT. Dielectronic recombination selectively drives radiative transitions that originate on states with vacancies in the 2s subshell, states that are inaccessible under pure RR population kinetics

  1. Analysis of powdered milk by PIXE (Proton Induced X-ray Emission)

    International Nuclear Information System (INIS)

    Desales Galeana, G.

    1990-01-01

    The purpose of this work was to establish the conditions to analyze elements of Z>15 in powdered milk samples using the PIXE technique. Ten different commercial samples were analyzed: 2 full-cream, 3 half-cream and 5 for infant feeding. They were all purchased in Toluca City, Mexico. Thick targets were prepared and irradiated with 1.5 and 3 MeV protons beam in Mexico's Nuclear Center Tandem Van de Graff Accelerator. The obtained data were analyzed by two computers programs. Iron, the reference element was analyzed by atomic absorption spectrometry. Concentrations of the following elements: phosphorus, chlorine, potassium, calcium, chrome, iron, cobalt, nickel, copper, zinc, bromine, rubidium, molybdenum and cadmium were evaluated. The concentrations of the first four elements were usually high, whereas those of the other elements remained in some ppm. The experimental conditions set up in this work were suitable for the analysis of powdered milk and can be applied to other organic samples (Author)

  2. Damage evolution analysis in mortar, during compressive loading using acoustic emission and X-ray tomography: Effects of the sand/cement ratio

    International Nuclear Information System (INIS)

    Elaqra, H.; Godin, N.; Peix, G.; R'Mili, M.; Fantozzi, G.

    2007-01-01

    This paper explores the use of acoustic emission (AE) and X-ray tomography to identify the mechanisms of damage and the fracture process during compressive loading on concrete specimens. Three-dimensional (3D) X-ray tomography image analysis was used to observe defects of virgin mortar specimen under different compressive loads. Cumulative AE events were used to evaluate damage process in real time according to the sand/cement ratio. This work shows that AE and X-ray tomography are complementary nondestructive methods to measure, characterise and locate damage sites in mortar. The effect of the sand proportion on damage and fracture behaviour is studied, in relation with the microstructure of the material

  3. Theory of X-ray absorption and emission spectra

    International Nuclear Information System (INIS)

    Mukoyama, Takeshi

    2004-01-01

    Theoretical studies on X-ray absorption and emission spectroscopy are discussed. Simple expressions for X-ray emission rate and X-ray absorption cross section are presented in the dipole approximation. Various atomic models to obtain realistic wave functions and theoretical calculations for X-ray absorption cross sections and X-ray emission rates are described. In the case of molecules and solids, molecular orbital methods for electronic structures and molecular wave functions are discussed. The emphasis is on the procedures to obtain the excited-state and continuum wave functions for molecules and to calculate the multi-center dipole matrix elements. The examples of the calculated X-ray absorption and emission spectra are shown and compared with the experimental results

  4. Synchrotron x-ray microbeam characteristics for x-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Iida, Atsuo; Noma, Takashi

    1995-01-01

    X-ray fluorescence analysis using a synchrotron x-ray microprobe has become an indispensable technique for non-destructive micro-analysis. One of the most important parameters that characterize the x-ray microbeam system for x-ray fluorescence analysis is the beam size. For practical analysis, however, the photon flux, the energy resolution and the available energy range are also crucial. Three types of x-ray microbeam systems, including monochromatic and continuum excitation systems, were compared with reference to the sensitivity, the minimum detection limit and the applicability to various types of x-ray spectroscopic analysis. 16 refs., 5 figs

  5. Chemical effects in x-ray emission spectra

    International Nuclear Information System (INIS)

    Fernandes, N.G.

    1982-01-01

    The chemical bond influence in X-ray emission spectra of hafnium, iodine, iron, sulphur, aluminium and magnesium is detected. The position of one X-ray emission line is determined by three methods: parabolic profile; Gaussian distribution and extra-heavy maximum. (author)

  6. X-Ray Emission from Compact Sources

    Energy Technology Data Exchange (ETDEWEB)

    Cominsky, L

    2004-03-23

    This paper presents a review of the physical parameters of neutron stars and black holes that have been derived from X-ray observations. I then explain how these physical parameters can be used to learn about the extreme conditions occurring in regions of strong gravity, and present some recent evidence for relativistic effects seen in these systems. A glossary of commonly used terms and a short tutorial on the names of X-ray sources are also included.

  7. Preparation and characterization of a new set of IAEA reference air filters using instrumental neutron activation analysis, proton-induced X-ray emission and Rutherford backscattering

    Czech Academy of Sciences Publication Activity Database

    Kučera, Jan; Havránek, Vladimír; Krausová, Ivana

    2009-01-01

    Roč. 281, č. 1 (2009), s. 123-129 ISSN 0236-5731. [9th International Conference on Nuclear Analytical Methods in the Life Sciences. Lisbon, 07.09.2008-12.09.2008] Institutional research plan: CEZ:AV0Z10480505 Keywords : Reference air filters * instrumental neutron activation analysis * Proton induced X-ray emission Subject RIV: BG - Nuclear, Atomic and Molecular Physics, Colliders Impact factor: 0.631, year: 2009

  8. Multielement analysis of Picea rubens Sarg. Three-rings by proton-induced x-ray emission

    International Nuclear Information System (INIS)

    Hall, G.S.

    1984-01-01

    A 3.7 MeV external proton beam was employed to produce X-rays in Picea rubens Sarg. (red spruce). Intra-annual growth rings and several elements were quantitatively determined (P, S, Cl, K, Ca, Ti, Cr, Mn, Fe, Ni, Cu, Zn, Pb, Sr). The PIXE experimental set-up, rapid sample preparation methods, and some interesting observations are discussed. In addition, statistical analysis of the tree-ring element concentrations revealed that K, Cl, and Ca were slightly translocated whereas the other elements detected were not. 15 references, 1 figure, 1 table

  9. VETA-I x ray test analysis

    Science.gov (United States)

    Brissenden, R. J. V.; Chartas, G.; Freeman, M. D.; Hughes, J. P.; Kellogg, E. M.; Podgorski, W. A.; Schwartz, D. A.; Zhao, P.

    1992-01-01

    This interim report presents some definitive results from our analysis of the VETA-I x-ray testing data. It also provides a description of the hardware and software used in the conduct of the VETA-I x-ray test program performed at the MSFC x-ray Calibration Facility (XRCF). These test results also serve to supply data and information to include in the TRW final report required by DPD 692, DR XC04. To provide an authoritative compendium of results, we have taken nine papers as published in the SPIE Symposium, 'Grazing Incidence X-ray/EUV Optics for Astronomy and Projection Lithography' and have reproduced them as the content of this report.

  10. The analysis and the three-dimensional, forward-fit modeling of the X-ray and the microwave emissions of major solar flares

    Science.gov (United States)

    Kuroda, Natsuha; Wang, Haimin; Gary, Dale E.

    2017-08-01

    It is well known that the time profiles of the hard X-ray (HXR) emission and the microwave (MW) emission during the impulsive phase of the solar flare are well correlated, and that their analysis can lead to the understandings of the flare-accelerated electrons. In this work, we first studied the source locations of seven distinct temporal peaks observed in HXR and MW lightcurves of the 2011-02-15 X2.2 flare using the Reuven Ramaty High Energy Solar Spectroscopic Imager (RHESSI) and Nobeyama Radioheliograph. We found that the seven emission peaks did not come from seven spatially distinct sites in HXR and MW, but rather in HXR we observed a sudden change in location only between the second and the third peak, with the same pattern occurring, but evolving more slowly in MW, which is consistent with the tether-cutting model of solar flares. Next, we closely examine the widely-used notion of a "common population" of the accelerated electrons producing the HXR and the MW, which has been challenged by some studies suggesting the differences in the inferred energy spectral index and emitting energies of the HXR- and MW- producing electrons. We use the Non-linear Force Free Field model extrapolated from the observed photospheric magnetogram in the three-dimensional, multi-wavelength modeling platform GX Simulator, and attempt to create a unified electron population model that can simultaneously reproduce the observed X-ray and MW observations of the 2015-06-22 M6.5 flare. We constrain the model parameters by the observations made by the highest-resolving instruments currently available in two wavelengths, the RHESSI for X-ray and the Expanded Owens Valley Solar Array for MW. The results suggest that the X-ray emitting electron population model fits to the standard flare model with the broken, hardening power-law spectrum at ~300 keV that simultaneously produces the HXR footpoint emission and the MW high frequency emission, and also reveals that there could be a “X-ray

  11. Radio and X-ray emission from supernova remnants

    International Nuclear Information System (INIS)

    Asvarova, A.I.; Novruzova, H.I.; Ahmedova, S.I.

    2010-01-01

    In this paper it was studied the statistical correlation between radio and X-ray emissions from shell-type supernova remnants (SNR). The primary aim of this study is to test the model of radio emission of shell-type SNRs presented by one of the authors. Based on this model of radio emission, by using the Monte Carlo techniques we have simulated statistical relations radio - X-ray luminosities (not surface brightnesses) which then were compared with the observations. X-ray emission is assumed to be thermal. To have a uniform statistical material it was used observational data on the SNRs in Magellanic Clouds

  12. Proton Induced X-Rays Emission (PIXE) and Atomic Absorption Spectrometry (AAS) applied in the environmental sample analysis

    International Nuclear Information System (INIS)

    Popescu, Ion V.; Iordan, M.; Stihi, C.; Bancuta, A.; Dima, G.; Busuioc, G.; Ciupina, V.; Belc, M.; Badica, T.

    2003-01-01

    The aim of this work is to determine the elemental composition of tree leaves using Proton-Induced X-Rays Emission (PIXE) and Atomic Absorption Spectrophotometry (AAS) methods. By PIXE Spectrometry we identified and determined the concentration of S, Cl, K, Ca, Ti, Cr, Mn, Fe, Co, Ni, Cu Zn, As, Br, Sr and by AAS method the concentration of elements: Cr, Mn, Fe, Co, Cu, Zn, Se, Cd. Pb was identified in only 2 samples from 29. For tree leave samples collected at a large distance to the polluting source the Sr concentration decreased and the Mg, Ca, Se, Zn and Fe concentrations increased. Also, we can observe a small affinity of these leaves for the environmental Pb which was detected for two samples at a small distance to polluting source. (authors)

  13. X-ray and extreme ultraviolet emission from comets

    Science.gov (United States)

    Lisse, C. M.; Cravens, T. E.; Dennerl, K.

    The discovery of high energy X-ray emission in 1996 from C/1996 B2 (Hyakutake) has created a surprising new class of X-ray emitting objects. The original discovery (Lisse et al., 1996) and subsequent detection of X-rays from 17 other comets (Table 1) have shown that the very soft (E < 1 keV) emission is due to an interaction between the solar wind and the comet's atmosphere, and that X-ray emission is a fundamental property of comets. Theoretical and observational work has demonstrated that charge exchange collisions of highly charged solar wind ions with cometary neutral species is the best explanation for the emission. Now a rapidly changing and expanding field, the study of cometary X-ray emission appears to be able to lead us to a better understanding of a number of physical phenomena: the nature of the cometary coma, other sources of X-ray emission in the solar system, the structure of the solar wind in the heliosphere, and the source of the local soft X-ray background.

  14. Quantitative X ray analysis system. User's manual and guide to X ray fluorescence technique

    International Nuclear Information System (INIS)

    2009-01-01

    This guide covers trimmed and re-arranged version 3.6 of the Quantitative X ray Analysis System (QXAS) software package that includes the most frequently used methods of quantitative analysis. QXAS is a comprehensive quantitative analysis package that has been developed by the IAEA through research and technical contracts. Additional development has also been carried out in the IAEA Laboratories in Seibersdorf where QXAS was extensively tested. New in this version of the manual are the descriptions of the Voigt-profile peak fitting, the backscatter fundamental parameters' and emission-transmission methods of chemical composition analysis, an expanded chapter on the X ray fluorescence physics, and completely revised and increased number of practical examples of utilization of the QXAS software package. The analytical data accompanying this manual were collected in the IAEA Seibersdorf Laboratories in the years 2006/2007

  15. Investigation of drug-release polymers using nuclear reaction analysis and particle induced X-ray emission

    International Nuclear Information System (INIS)

    Smith, R.W.; Massingham, Gary; Clough, A.S.

    2003-01-01

    The diffusion of water into the developmental drug-release polymer addition cured silicone has been investigated using 3 He ion scanning micro-beam techniques developed at the University of Surrey. Polymer samples loaded with 15% by weight of the drug chlorohexidine diacetate were immersed in a water based phosphate buffered saline solution for times of 1 hour, 1 day, 1 week and 1 month. The results showed that as the water diffused into the polymer it associated with the drug allowing its release by diffusion through the network formed by water filled pores. Future improvements to the techniques are discussed including the use of an array of CdZnTe detectors

  16. Weak hard X-ray emission from broad absorption line quasars: evidence for intrinsic X-ray weakness

    International Nuclear Information System (INIS)

    Luo, B.; Brandt, W. N.; Scott, A. E.; Alexander, D. M.; Gandhi, P.; Stern, D.; Teng, S. H.; Arévalo, P.; Bauer, F. E.; Boggs, S. E.; Craig, W. W.; Christensen, F. E.; Comastri, A.; Farrah, D.; Hailey, C. J.; Harrison, F. A.; Koss, M.; Ogle, P.; Puccetti, S.; Saez, C.

    2014-01-01

    We report NuSTAR observations of a sample of six X-ray weak broad absorption line (BAL) quasars. These targets, at z = 0.148-1.223, are among the optically brightest and most luminous BAL quasars known at z < 1.3. However, their rest-frame ≈2 keV luminosities are 14 to >330 times weaker than expected for typical quasars. Our results from a pilot NuSTAR study of two low-redshift BAL quasars, a Chandra stacking analysis of a sample of high-redshift BAL quasars, and a NuSTAR spectral analysis of the local BAL quasar Mrk 231 have already suggested the existence of intrinsically X-ray weak BAL quasars, i.e., quasars not emitting X-rays at the level expected from their optical/UV emission. The aim of the current program is to extend the search for such extraordinary objects. Three of the six new targets are weakly detected by NuSTAR with ≲ 45 counts in the 3-24 keV band, and the other three are not detected. The hard X-ray (8-24 keV) weakness observed by NuSTAR requires Compton-thick absorption if these objects have nominal underlying X-ray emission. However, a soft stacked effective photon index (Γ eff ≈ 1.8) for this sample disfavors Compton-thick absorption in general. The uniform hard X-ray weakness observed by NuSTAR for this and the pilot samples selected with <10 keV weakness also suggests that the X-ray weakness is intrinsic in at least some of the targets. We conclude that the NuSTAR observations have likely discovered a significant population (≳ 33%) of intrinsically X-ray weak objects among the BAL quasars with significantly weak <10 keV emission. We suggest that intrinsically X-ray weak quasars might be preferentially observed as BAL quasars.

  17. X-ray emission from Centaurus A

    International Nuclear Information System (INIS)

    Terrell, J.

    1984-01-01

    The X-ray strength of Cen A (NGC 5128) was monitored for 10 years by Vela 5B, beginning in 1979. The 1973 to 1975 period of exceptional activity and strength was especially well covered, and was characterized by numerous rapid changes in intensity, in agreement with other data, indicating that the nucleus of Cen A is small but massive. 16 references, 3 figures

  18. Quality assurance challenges in x-ray emission based analyses

    International Nuclear Information System (INIS)

    Papp, T.

    2005-01-01

    Complete text of publication follows. There is a large scatter in the results of X-ray analysis with solid-state detectors suggesting methodological origin. Although the PIXE (proton induced X-ray emission) analytical technique can work without relation to any physics, as was commented at the recent PIXE conference, one could argue that if the same technique is used for measuring physical quantities reveals problems, then perhaps potential methodological issues can not apriory be excluded. We present a simple example which could be interpreted as indications for methodological considerations. Recently an inter-comparison was made of analysis of the spectra measured at the laboratory of the International Atomic Energy Agency (IAEA). Four participating analytical software packages were used to evaluate the X-ray spectra. There are several thin metal samples spectra, for which common energy scale could not be established. The quality of the spectrum can be judged from the line shape. The line shape is parametrized by the full widths at half maximum (FWHM) of a peak and the so-called low energy tailing. Fitting the spectra individually we obtained FWHM squared values at different energies and determined the linear regression parameters. The parameters suggest a rather poor detector performance. It is generally assumed that the (FWHM) 2 values have a first order polynomial form as a function of X-ray energy. Having done a linear regression analysis, we can plot the standard residual, presented in Fig. 1, which clearly shows a three-sigma deviation. The probability to having a three-sigma deviation is 1%. In other words, the probability that these spectra are in accordance with the expected FWHM functional form is less than 1%. The main problem is that, although the composite spectra were analyzed using four different programs, the difficulty in interpreting the spectra was not commented upon by any of the participants in the inter-comparison. (author)

  19. X-ray Emission from the Guitar Nebula

    OpenAIRE

    Romani, Roger W.; Cordes, James M.; Yadigaroglu, I. -A.

    1997-01-01

    We have detected weak soft X-ray emission from the Pulsar Wind Nebula trailing the high velocity star PSR 2224+65 (the `Guitar Nebula'). This X-ray flux gives evidence of \\gamma~10^7 eV particles in the pulsar wind and constrains the properties of the post-shock flow. The X-ray emission is most easily understood if the shocked pulsar wind is partly confined in the nebula and if magnetic fields in this zone can grow to near equipartition values.

  20. X-Ray Emission from the Guitar Nebula

    Science.gov (United States)

    Romani, Roger W.; Cordes, James M.; Yadigaroglu, I.-A.

    1997-01-01

    We have detected weak soft X-ray emission from the pulsar wind nebula trailing the high-velocity star PSR 2224+65 (the "Guitar Nebula"). This X-ray flux gives evidence of gamma approximately 10(exp 7) eV particles in the pulsar wind and constrains the properties of the postshock flow. The X-ray emission is most easily understood if the shocked pulsar wind is partly confined in the nebula and if magnetic fields in this zone can grow to near-equipartition values.

  1. Space- and time-resolved diagnostics of soft x-ray emission from laser plasmas

    International Nuclear Information System (INIS)

    Richardson, M.C.; Jaanimagi, P.A.; Chen, H.

    1988-01-01

    The analysis of soft x-ray emission from plasmas created by intense short-wavelength laser radiation can provide much useful information on the density, temperature and ionization distribution of the plasma. Until recently, limitations of sensitivity and the availability of suitable x-ray optical elements have restricted studies of soft x-ray emission from laser plasmas. In this paper, the authors describe novel instrumentation which provides high sensitivity in the soft x-ray spectrum with spatial and temporal resolution in the micron and picosecond ranges respectively. These systems exploit advances made in soft x-ray optic and electro-optic technology. Their application in current studies of laser fusion, x-ray lasers, and high density atomic physics are discussed

  2. Multi-element analysis of the rat hippocampus by proton induced x-ray emission spectroscopy (phosphorus, sulfur, chlorine, potassium, calcium, iron, zinc, copper, lead, bromine, and rubidium)

    Energy Technology Data Exchange (ETDEWEB)

    Kemp, K.; Danscher, G.

    1979-01-22

    A technique for multi-element analysis of brain tissue by proton induced x-ray emission spectroscopy (PIXE) is described and data from analysis of fixed and unfixed samples from rat hippocampus, neocortex, amygdala, and spinal cord are presented and commented on. The atoms present in the tissue are bombarded with protons which cause the ejection of electrons from the inner shells. When the holes are refilled with electrons from outer shells, x-ray quanta characteristic for each element are emitted. Using a high resolution energy dispersive detector, a complete x-ray spectrum of the specimen can be recorded in a single measurement. Detection limits less than or approximately 5 ppM of dry matter are obtained for most elements with atomic number greater than 14 (silicon). Around 13 elements were found in concentrations above the detection limits. The grand means for non-fixed hippocampi were e.g., for Zn-120 ppM; Rb-20 ppM; Fe-150 ppM; Pb-3 ppM; Ni-5 ppM.

  3. Data processing for the Active Particle-induced X-ray Spectrometer and initial scientific results from Chang'e-3 mission

    Science.gov (United States)

    Fu, Xiao-Hui; Li, Chun-Lai; Zhang, Guang-Liang; Zou, Yong-Liao; Liu, Jian-Jun; Ren, Xin; Tan, Xu; Zhang, Xiao-Xia; Zuo, Wei; Wen, Wei-Bin; Peng, Wen-Xi; Cui, Xing-Zhu; Zhang, Cheng-Mo; Wang, Huan-Yu

    2014-12-01

    The Active Particle-induced X-ray Spectrometer (APXS) is an important payload mounted on the Yutu rover, which is part of the Chang'e-3 mission. The scientific objective of APXS is to perform in-situ analysis of the chemical composition of lunar soil and rock samples. The radioactive sources, 55Fe and 109Cd, decay and produce α-particles and X-rays. When X-rays and α-particles interact with atoms in the surface material, they knock electrons out of their orbits, which release energy by emitting X-rays that can be measured by a silicon drift detector (SDD). The elements and their concentrations can be determined by analyzing their peak energies and intensities. APXS has analyzed both the calibration target and lunar soil once during the first lunar day and again during the second lunar day. The total detection time lasted about 266 min and more than 2000 frames of data records have been acquired. APXS has three operating modes: calibration mode, distance sensing mode and detection mode. In detection mode, work distance can be calculated from the X-ray counting rate collected by SDD. Correction for the effect of temperature has been performed to convert the channel number for each spectrum to X-ray energy. Dead time correction is used to eliminate the systematic error in quantifying the activity of an X-ray pulse in a sample and derive the real count rate. We report APXS data and initial results during the first and second lunar days for the Yutu rover. In this study, we analyze the data from the calibration target and lunar soil on the first lunar day. Seven major elements, including Mg, Al, Si, K, Ca, Ti and Fe, have been identified. Comparing the peak areas and ratios of calibration basalt and lunar soil the landing site was found to be depleted in K, and have lower Mg and Al but higher Ca, Ti, and Fe. In the future, we will obtain the elemental concentrations of lunar soil at the Chang'e-3 landing site using APXS data.

  4. A comparative study of neutron activation analysis and proton-induced X-ray emission analysis for the determination of heavy metals in estuarine sediments

    Science.gov (United States)

    Randle, K.; Al-Jundi, J.; Mamas, C. J. V.; Sokhi, R. S.; Earwaker, L. G.

    1993-06-01

    Our work on heavy metals in the estuarine environment has involved the use of two multielement techniques: neutron activation analysis (NAA) and proton-induced X-ray emission (PIXE) analysis. As PIXE is essentially a surface analytical technique problems may arise due to sample inhomogeneity and surface roughness. In order to assess the contribution of these effects we have compared the results from PIXE analysis with those from a technique which analyzes a larger bulk sample rather than just the surface. An obvious method was NAA. A series of sediment samples containing particles of variable diameter were compared. Pellets containing a few mg of sediment were prepared from each sample and analyzed by the PIXE technique using both an absolute and a comparitive method. For INAA the rest of the sample was then irradiated with thermal neutrons and element concentrations determined from analyses of the subsequent gamma-ray spectrum. Results from the two methods are discussed.

  5. Kinematic X-Ray Analysis Apparatus

    NARCIS (Netherlands)

    Koningsberger, D.C.; Brinkgreve, P.

    1983-01-01

    In an X-ray analysis apparatus, a moving mechanism is provided by a main guide member along which a main slide device can be displaced. Rotatably connected with the main slide device is a detector guide member along which a detection slide device is displaced. The main slide device, as well as the

  6. Quantitative X-ray analysis of pigments

    International Nuclear Information System (INIS)

    Araujo, M. Marrocos de

    1987-01-01

    The 'matrix-flushing' and the 'adiabatic principle' methods have been applied for the quantitative analysis through X-ray diffraction patterns of pigments and extenders mixtures, frequently used in paint industry. The results obtained have shown the usefulness of these methods, but still ask for improving their accuracy. (Author) [pt

  7. Chandra X-ray Observations of Jovian Low-latitude Emissions: Morphological, Temporal, and Spectral Characteristics

    Science.gov (United States)

    Bhardwaj, Anil; Elsner, Ronald F.; Gladstone, G. Randall; Cravens, Thomas E.; Waiate J. Hunter, Jr.; Branduardi-Raymont, Graziella; Ford, Peter

    2004-01-01

    Chandra observed X-rays from Jupiter during 24-26 February 2003 for about 40 hours with the ACIS-S and HRC-I instruments. The analysis of Jovian low-latitude "disk" Xray emissions are presented and compared with the high-latitude "auroral" emissions. We report the first Chandra ACIS-S measured X-ray spectrum (0.3-2 keV) of Jupiter's low-latitude disk The disk X-ray emission is harder and extends to higher energies than the auroral spectrum. The temporal variation in the Jovian disk X-rays is on an average consistent with those in the solar X-rays observed by GOES, and TIMED/SSE. Contrary to the auroral X-rays, the disk emissions are uniformly distributed over Jupiter; no indication of longitudinal dependence or correlation with surface magneh field strength is visible. Also, unlike the approx. 40 +/- 20 min periodic oscillations seen in the auroral X-ray emissions, the disk emissions do not show any periodic oscillations. The disk spectrum seems to be consistent with resonant and fluorescent scattering of solar X-rays by the Jovian upper atmosphere. Jupiter's disk is found to be about 50% dimmer in soft X-rays in February 2003 compared that in December 2000, which is consistent with the decrease in solar activity. No evidence of lightning-induced X-rays is seen in the Chandra X-ray data. The Jovian disk spectra observed with Chandra-ACIS is stronger than that observed with XMM-Newton two months later during April 28-29, 2003. The XMM-Newton Xray image of Jupiter shows evidence of limb darkening on the anti-sunward side as seen from Earth, as well as an asymmetry with respect to the subsolar point: suggesting a solar driven process.

  8. Signatures of Synchrotron: Low-cutoff X-ray emission and the hard X-ray spectrum of Cas A

    Science.gov (United States)

    Stage, Michael D.; Fedor, Emily Elizabeth; Martina-Hood, Hyourin

    2018-06-01

    In soft X-rays, bright, young Galactic remnants (Cas A, Kepler, Tycho, etc.) present thermal line emission and bremsstrahlung from ejecta, and synchrotron radiation from the shocks. Their hard X-ray spectra tend to be dominated by power-law sources. However, it can be non-trivial to discriminate between contributions from processes such as synchrotron and bremsstrahlung from nonthermally accelerated electrons, even though the energies of the electrons producing this radiation may be very different. Spatially-resolved spectroscopic analysis of 0.5-10 keV observations with, e.g., Chandracan provide leverage in identifying the processes and their locations. Previously, Stage & Allen (2006), Allen & Stage (2007) and Stage & Allen (2011) identified regions characterized by high-cutoff synchrotron radiation. Extrapolating synchrotron model fits to the emission in the Chandra band, they estimated the synchrotron contribution to the hard X-ray spectrum at about one-third the observed flux, fitting the balance with nonthermal bremsstrahlung emission produced by nonthermal electrons in the ejecta. Although it is unlikely this analysis missed regions of the highest-cutoff synchrotron emission, which supplies the bulk of the synchrotron above 15 keV, it may have missed regions of lower-cutoff emission, especially if they are near bright ejecta and the reverse shock. These regions cannot explain the emission at the highest energies (~50 keV), but may make significant contributions to the hard spectrum at lower energies (~10 keV). Using the technique described in Fedor, Martina-Hood & Stage (this meeting), we revisit the analysis to include regions that may be dominated by low-cutoff synchrotron, located in the interior of the remnant, and/or correlated with the reverse shock. Identifying X-ray emission from accelerated electrons associated with the reverse-shock would have important implications for synchrotron and non-thermal bremsstrahlung radiation above the 10 keV.

  9. Studies of soft x-ray emission during solar flares

    International Nuclear Information System (INIS)

    Anandaram, M.N.

    1973-01-01

    Solar flare soft x-ray emission from 0.5 A to 8.5 A was observed during 1967-68 by Bragg crystal (LiF and EDDT) spectrometers aboard the OSO-4 satellite and also by NRL broad-band ionization detectors aboard the OGO-4 satellite. In this work, instrumental parameters for the LiF crystal spectrometer based on experimental values have been determined and used in the data analysis. The total continuum emission in the 0.5 to 3 A and the 1 to 8 A broad band segments has been determined from OGO-4 data for 21 flares. In doing this, a simple and approximate method of converting the total emission based on the gray body approximation (in which the OGO-4 data are reported) to one based on the thermal continuum spectrum has been developed. (author)

  10. Characterization of X-ray emission from laser generated plasma

    Science.gov (United States)

    Cannavò, Antonino; Torrisi, Lorenzo; Ceccio, Giovanni; Cutroneo, Mariapompea; Calcagno, Lucia; Sciuto, Antonella; Mazzillo, Massimo

    2018-01-01

    X-ray emission from laser generated plasma was studied at low (1010 W/cm2) and high (1018 W/cm2) intensity using ns and fs laser, respectively. Plasma characteristics were controlled trough the laser parameters, the irradiation conditions and the target properties. The X-ray spectra were acquired using fast detection technique based on SiC diodes with different active regions. The X-ray yield increases with the atomic number of the target, both at low and high intensity, and a similar empirical law has been obtained. The X-ray emission mechanisms from plasma are correlated to the plasma temperature and density and to the Coulomb charge particle acceleration, due to the charge separation effects produced in the non-equilibrium plasma. Functional dependences, theoretical approaches and interpretation of possible mechanism will be presented and discussed.

  11. Characterization of X-ray emission from laser generated plasma

    Directory of Open Access Journals (Sweden)

    Cannavò Antonino

    2018-01-01

    Full Text Available X-ray emission from laser generated plasma was studied at low (1010 W/cm2 and high (1018 W/cm2 intensity using ns and fs laser, respectively. Plasma characteristics were controlled trough the laser parameters, the irradiation conditions and the target properties. The X-ray spectra were acquired using fast detection technique based on SiC diodes with different active regions. The X-ray yield increases with the atomic number of the target, both at low and high intensity, and a similar empirical law has been obtained. The X-ray emission mechanisms from plasma are correlated to the plasma temperature and density and to the Coulomb charge particle acceleration, due to the charge separation effects produced in the non-equilibrium plasma. Functional dependences, theoretical approaches and interpretation of possible mechanism will be presented and discussed.

  12. Circumstellar X-ray Emission from SN1978K

    Science.gov (United States)

    Schlegel, Eric M.; Colbert, E.; Petre, R.

    1995-02-01

    We present the X-ray light curve in the 0.2 2.4 keV band based on fiveROSAT observations of SN1978K in NGC 1313. The X-ray emission is believed to arise from the interaction of the reverse shock and the expanding debris from the supernova. The reverse shock becomes established after the outgoing shock runs into circumstellar matter.

  13. Analyais of solar X-ray emission line profiles

    International Nuclear Information System (INIS)

    Burek, A.J.; Marrus, D.M.; Blake, R.L.; Fenimore, E.E.

    1981-01-01

    We report results of the analysis of the X-ray emission line profiles for the Ne X La and Fe XVII 4d 1 P 1 lines produced in an active region that was undergoing a radio and X-ray gradual rise and fall (GRF) in intensity. The spectra were obtained with collimated Bragg spectrometers launched on a rocket from White Sands Missile Range on 1976 March 26. Using a crystal of ammonium acid phthalate, we have fully resolved the Ne X La and Fe XVII 4d 1 P 1 lines, permitting an accurate determinination of the Ne X La intensity and allowing Doppler broadened profiles for lines formed from ions having greatly different atomic mass and charge to be measured. An isothermal model derived from the Ne IX/Ne X resonance line intensity ratio gives an electron temperature of 3.4 x 10 6 K. An isothermal model, however, fails to account for the intensities of all lines and continuum observed. All multitemperature models that do reproduce the observed relative line intensities require the presence of a hot plasma component with an electron temperature in excess of 5 x 10 6 K. The presence of a high temperature component is also suggested by the measured line to continuum ratio of 3.6 in the 12--15 A wavelength interval. Interpretation of the line profiles in terms of a multitemperature model requires an rms turbulence velocity of 48 +- 15 km s -1 for Fe XVII 1 P 1 and 74 +- 54 km s - 2exclamation for Ne X La at the 95% confidence level. Collimated scans across the active region show the presence of a compact source of intense X-ray emission close to the magnetic neutral line, which is very probably the GRF plasma

  14. Handbook on simultaneous x-ray and γ-ray ion beam methods for fine particle analysis

    International Nuclear Information System (INIS)

    Cohen, D.D.

    2000-01-01

    Sampling, measurement, characterisation and source appointment of fine atmospheric particles has become increasingly important in recent times. This is due in part to the realisation that the fine particle pollution caused by anthropogenic activities plays a key role in certain aspects of human health, pollution transport and global climate change. This publication discusses accelerator based ion beam analysis (IBA) methods of particle induced X-ray emission (PIXE) and particle induced γ-ray emission (PIGE) as applied to aerosol analysis. These techniques are sensitive, multielemental, mainly non-destructive, require no sample preparation, have short analysis times and can be used to analyse hundreds of filter samples a day in batch processing with minimum operator interaction. The aspects discussed in the publication include: the basics of the techniques; spectrum analysis; system calibration and blank subtraction; quantification; sensitivity; measurement errors

  15. Preparation of specimens for analysis by: X-ray diffraction and X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Banos L, L.

    2004-01-01

    Specimen preparation is one of the most important requirements in the analysis of samples by X-ray Diffraction and X-ray Fluorescence. This statement is especially true for samples containing different types of materials. There are many forms of specimen suitable for X-ray analysis and the type of the sample as received will generally determine the method of pretreatment. It is convenient to refer to the material received for analysis as the sample, and that, which is actually analyzed as the specimen. The powder Diffraction method assumes that the particles in the specimen are ideally random orientation and that there are enough crystallites in the specimen to achieve a representative intensity distribution for these crystallites. X ray Fluorescence is essentially a comparative method of analysis, it is vital that all standards and unknowns be presented to the spectrometer in a reproducible and identical manner. (Author) 3 refs., 6 figs

  16. Total reflection X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Michaelis, W.; Prange, A.

    1987-01-01

    In the past few years, total reflection X-ray flourescence analysis (TXRF) has found an increasing number of assignments and applications. Experience of trace element analysis using TXRF and examples of applications are already widespread. Therefore, users of TXRF had the opportunity of an intensive exchange of their experience at the 1st workshop on total reflection X-ray fluorescence analysis which took place on May 27th and 28th 1986 at the GKSS Research Centre at Geesthacht. In a series of lectures and discussions dealing with the analytical principle itself, sample preparation techniques and applications as well as comuter programs for spectrum evaluation, the present state of development and the range of applications were outlined. 3 studies out of a total of 14 were included separately in the INIS and ENERGY databases. With 61 figs., 12 tabs [de

  17. Ultrafast secondary emission x-ray imaging detectors

    International Nuclear Information System (INIS)

    Akkerman, A.; Gibrekhterman, A.; Majewski, S.

    1991-07-01

    Fast high accuracy, x-ray imaging at high photon flux can be achieved when coupling thin solid convertors to gaseous electron multipliers, operating at low gas pressures. Secondary electron emitted from the convertor foil are multiplied in several successive amplification elements. The obvious advantage of solid x-ray detectors, as compared to gaseous conversion, are the production of parallax-free images and the fast (subnanoseconds) response. These x-ray detectors have many potential applications in basic and applied research. Of particular interest is the possibility of an efficient and ultrafast high resolution imaging of transition radiation,with a reduced dE/dx background. We present experimental results on the operation of the secondary emission x-ray (SEX) detectors, their detection efficiency, localization and time resolution. The experimental work is accompanied by mathematical modelling and computer simulation of transition radiation detectors based on CsI transition radiation convertors. (author)

  18. Is X-ray emissivity constant on magnetic flux surfaces?

    International Nuclear Information System (INIS)

    Granetz, R.S.; Borras, M.C.

    1997-01-01

    Knowledge of the elongations and shifts of internal magnetic flux surfaces can be used to determine the q profile in elongated tokamak plasmas. X-ray tomography is thought to be a reasonable technique for independently measuring internal flux surface shapes, because it is widely believed that X-ray emissivity should be constant on a magnetic flux surface. In the Alcator C-Mod tokamak, the X-ray tomography diagnostic system consists of four arrays of 38 chords each. A comparison of reconstructed X-ray contours with magnetic flux surfaces shows a small but consistent discrepancy in the radial profile of elongation. Numerous computational tests have been performed to verify these findings, including tests of the sensitivity to calibration and viewing geometry errors, the accuracy of the tomography reconstruction algorithms, and other subtler effects. We conclude that the discrepancy between the X-ray contours and the magnetic flux surfaces is real, leading to the conclusion that X-ray emissivity is not exactly constant on a flux surface. (orig.)

  19. Observations of EUV and X-ray Emission from Comets

    Science.gov (United States)

    Lisse, C.

    The unexpected discovery of x-ray emission from Comet Hyakutake in March 1996 (Lisse et al. 1996) produced a number of questions about the physical mechanism producing the radiation. The original detection and subsequent observations have shown that the very soft (best fit thermal bremsstrahlung model kT0.2 keV) emission is due to an interaction between the solar wind and the comet's atmosphere. Using the results from the more than 15 comets detected to date in x-rays, I report here on the latest results on cometary x-ray emission, including new results from Chandra, and show that charge exchange between highly ionized minor ions in the solar wind and neutral gases in the cometary coma is the most likely operative mechanism. I then use this result to study a number of problems of astrophysical interest: the nature of the cometary coma, other possible sources of x-ray emission in the solar system, the structure of the solar wind in the heliosphere, and the source of the local x-ray background.

  20. Quantitative reconstruction of PIXE-tomography data for thin samples using GUPIX X-ray emission yields

    Energy Technology Data Exchange (ETDEWEB)

    Michelet, C., E-mail: michelet@cenbg.in2p3.fr [Univ. Bordeaux, CENBG, UMR 5797, F-33170 Gradignan (France); CNRS, IN2P3, CENBG, UMR 5797, F-33170 Gradignan (France); Barberet, Ph., E-mail: barberet@cenbg.in2p3.fr [Univ. Bordeaux, CENBG, UMR 5797, F-33170 Gradignan (France); CNRS, IN2P3, CENBG, UMR 5797, F-33170 Gradignan (France); Devès, G., E-mail: deves@cenbg.in2p3.fr [Univ. Bordeaux, CENBG, UMR 5797, F-33170 Gradignan (France); CNRS, IN2P3, CENBG, UMR 5797, F-33170 Gradignan (France); Bouguelmouna, B., E-mail: bbouguel@gmail.com [Univ. Bordeaux, CENBG, UMR 5797, F-33170 Gradignan (France); CNRS, IN2P3, CENBG, UMR 5797, F-33170 Gradignan (France); Bourret, S., E-mail: bourret@cenbg.in2p3.fr [Univ. Bordeaux, CENBG, UMR 5797, F-33170 Gradignan (France); CNRS, IN2P3, CENBG, UMR 5797, F-33170 Gradignan (France); Delville, M.-H., E-mail: delville@icmcb-bordeaux.cnrs.fr [Institut de Chimie de la Matière Condensée de Bordeaux (ICMCB, UPR9048) CNRS, Université de Bordeaux, 87 avenue du Dr. A. Schweitzer, Pessac F-33608 (France); Le Trequesser, Q., E-mail: letreque@cenbg.in2p3.fr [Univ. Bordeaux, CENBG, UMR 5797, F-33170 Gradignan (France); CNRS, IN2P3, CENBG, UMR 5797, F-33170 Gradignan (France); Institut de Chimie de la Matière Condensée de Bordeaux (ICMCB, UPR9048) CNRS, Université de Bordeaux, 87 avenue du Dr. A. Schweitzer, Pessac F-33608 (France); Gordillo, N., E-mail: nuri.gordillo@gmail.com [Univ. Bordeaux, CENBG, UMR 5797, F-33170 Gradignan (France); CNRS, IN2P3, CENBG, UMR 5797, F-33170 Gradignan (France); Beasley, D.G., E-mail: d.beasley@ucl.ac.uk [Center of Medical Imaging Computing (CMIC), Department of Medical Physics & Bioengineering, University College London, Gower Street, London WC1E 6BT (United Kingdom); and others

    2015-04-01

    We present here a new development of the TomoRebuild software package, to perform quantitative Particle Induced X-ray Emission Tomography (PIXET) reconstruction. X-ray yields are obtained from the GUPIX code. The GUPIX data base is available for protons up to 5 MeV and also in the 20–100 MeV energy range, deuterons up to 6 MeV, {sup 3}He and alphas up to 12 MeV. In this version, X-ray yields are calculated for thin samples, i.e. without simulating X-ray attenuation. PIXET data reconstruction is kept as long as possible independent from Scanning Transmission Ion Microscopy Tomography (STIMT). In this way, the local mass distribution (in g/cm{sup 3}) of each X-ray emitting element is reconstructed in all voxels of the analyzed volume, only from PIXET data, without the need of associated STIMT data. Only the very last step of data analysis requires STIMT data, in order to normalize PIXET data to obtain concentration distributions, in terms of normalized mass fractions (in μg/g). For this, a noise correction procedure has been designed in ImageJ. Moreover sinogram or image misalignment can be corrected, as well as the difference in beam size between the two experiments. The main features of the TomoRebuild code, user friendly design and modular C++ implementation, were kept. The software package is portable and can run on Windows and Linux operating systems. An optional user-friendly graphic interface was designed in Java, as a plugin for the ImageJ graphic software package. Reconstruction examples are presented from biological specimens of Caenorhabditis elegans – a small nematode constituting a reference model for biology studies. The reconstruction results are compared between the different codes TomoRebuild, DISRA and JPIXET, and different reconstruction methods: Filtered BackProjection (FBP) and Maximum Likelihood Expectation Maximization (MLEM)

  1. Atmospheric NLTE models for the spectroscopic analysis of blue stars with winds. III. X-ray emission from wind-embedded shocks

    Science.gov (United States)

    Carneiro, L. P.; Puls, J.; Sundqvist, J. O.; Hoffmann, T. L.

    2016-05-01

    Context. Extreme ultraviolet (EUV) and X-ray radiation emitted from wind-embedded shocks in hot, massive stars can affect the ionization balance in their outer atmospheres and can be the mechanism responsible for producing highly ionized atomic species detected in stellar wind UV spectra. Aims: To allow for these processes in the context of spectral analysis, we have implemented the emission from wind-embedded shocks and related physics into our unified, NLTE model atmosphere/spectrum synthesis code FASTWIND. Methods: The shock structure and corresponding emission is calculated as a function of user-supplied parameters (volume filling factor, radial stratification of shock strength, and radial onset of emission). We account for a temperature and density stratification inside the postshock cooling zones, calculated for radiative and adiabatic cooling in the inner and outer wind, respectively. The high-energy absorption of the cool wind is considered by adding important K-shell opacities, and corresponding Auger ionization rates have been included in the NLTE network. To test our implementation and to check the resulting effects, we calculated a comprehensive model grid with a variety of X-ray emission parameters. Results: We tested and verified our implementation carefully against corresponding results from various alternative model atmosphere codes, and studied the effects from shock emission for important ions from He, C, N, O, Si, and P. Surprisingly, dielectronic recombination turned out to play an essential role for the ionization balance of O iv/O v (particularly in dwarfs with Teff~ 45 000 K). Finally, we investigated the frequency dependence and radial behavior of the mass absorption coefficient, κν(r), which is important in the context of X-ray line formation in massive star winds. Conclusions: In almost all of the cases considered, direct ionization is of major influence because of the enhanced EUV radiation field, and Auger ionization only affects N vi

  2. X-Ray and Near-Infrared Spectroscopy of Dim X-Ray Point Sources Constituting the Galactic Ridge X-Ray Emission

    Directory of Open Access Journals (Sweden)

    Kumiko Morihana

    2014-12-01

    Full Text Available We present the results of X-ray and Near-Infrared observations of the Galactic Ridge X-ray Emission (GRXE. We extracted 2,002 X-ray point sources in the Chandra Bulge Field (l =0°.113, b = 1°.424 down to ~10-14.8 ergscm-2s-1 in 2-8 keV band with the longest observation (900 ks of the GRXE. Based on X-ray brightness and hardness, we classied the X-ray point sources into three groups: A (hard, B (soft and broad spectrum, and C (soft and peaked spectrum. In order to know populations of the X-ray point sources, we carried out NIR imaging and spectroscopy observation. We identied 11% of X-ray point sources with NIR and extracted NIR spectra for some of them. Based on X-ray and NIR properties, we concluded that non-thermal sources in the group A are mostly active galactic nuclei and the thermal sources are mostly white dwarf binaries such as cataclysmic variables (CVs and Pre-CVs. We concluded that the group B and C sources are X-ray active stars in flare and quiescence, respectively.

  3. Resonant X-ray emission spectroscopy in Dy compounds

    International Nuclear Information System (INIS)

    Tanaka, Satoshi; Okada, Kozo; Kotani, Akio.

    1994-01-01

    The excitation spectrum of the L 3 -M 5 X-ray emission of Dy compounds in the pre-edge region of Dy L 3 X-ray absorption near edge structure (L 3 -XANES) is theoretically investigated based upon the coherent second order optical formula with multiplet coupling effects. The spectral broadening of the excitation spectrum is determined by the M 5 core hole lifetime, being free from the L 3 core hole lifetime. The fine pre-edge structure of the L 3 edge due to the 2p→4f quadrupole transition can be seen in the excitation spectrum, while this structure is invisible in the conventional XANES, in agreement with the recent experimental results. We clarify the conditions for the excitation spectrum to be regarded as the absorption spectrum with a smaller width. The resonant X-ray emission spectra for various incident photon energies around the L 3 edge are also calculated. (author)

  4. The determination of light elements in heavy matrix using proton induced X-ray emission

    International Nuclear Information System (INIS)

    Levenets, V.V.; Omel'nik, A.P.; Shchur, A.A.; Chernov, A.E.; Usikov, N.P.; Zats, A.V.

    2007-01-01

    In this report the possibility of determination of light impurities in heavy matrixes is studied using proton induced X-Ray emission. The wide-band X-ray emission filter made from pyrolytic graphite was used in spectrometric scheme of experiment. The results of studying of filter features in energy range of X-ray emission from 4 to 12 keV were presented. The possibilities were examined of application of pyrolytic graphite filter to modify the X-rays spectrum for determination of iron, using characteristic emission of K-series, and hafnium, using L-series, in substances on base of zirconium (glasses, alloys etc.). It was shown, that the using of similar filter allows to reach the significant improving of metrological characteristics of analysis of mentioned impurities: the limits of detection of iron and hafnium were lowered single-order of magnitude. (authors)

  5. Potpourri of proton induced x-ray emission analyses

    International Nuclear Information System (INIS)

    Mangelson, N.F.; Nielson, K.K.; Eatough, D.J.; Hansen, L.D.

    1974-01-01

    A proton-induced x-ray emission analysis (PIXE) system using 2-MeV protons was developed. Measurements are being made in connection with several research projects. A study is being conducted to provide ecological baseline information in the region of the Navajo and the proposed Kaiparowits coal-fired electric generating stations. Trace-element measurements in this study are reported on air-particulate samples, small rodent tissues, soils, and plants. In another study air particulates collected near a source of SO 2 are extracted from the collection filter with an HCl solution and sulfate and sulfite ions are determined by calorimetric methods. The extraction solution is also analyzed by PIXE to determine the elemental composition. The latter information is necessary for an understanding of possible interferences with the calorimetric method and also indicates the heavy metals emitted by the source. Studies on human autopsy tissues, archeological artifacts, and in regular graduate and undergraduate laboratory classes are mentioned briefly

  6. Sawtooth-like X-ray emission observed in EBIT

    International Nuclear Information System (INIS)

    Radtke, R.; Biedermann, C.; Bachmann, P.

    2003-01-01

    The evolution of a mixture of highly charged Ar and Ba ions was measured in an electron beam ion trap (EBIT) by recording the characteristic X-ray emission from trapped ions. A special feature in the spectra are sawtooth-like intensity variations caused by a periodic collapse of the ion inventory in the trap. The effect requires favorable conditions to become present and is very sensitive to the trapping conditions. Analysis of the measurements is based on a time-dependent calculation of the trapping process. Simulations show that sawtooth activity results from the feedback between the low-Z Ar and high-Z Ba ions (Hopf bifurcation). Sawtooth spectra open up a spectroscopic method to test theoretical EBIT models and probe the dynamics in ion traps and sources

  7. Investigations of mode I crack propagation in fibre-reinforced plastics with real time X-ray tests and simultaneous sound emission analysis

    International Nuclear Information System (INIS)

    Brunner, A.; Nordstrom, R.; Flueeler, P.

    1992-01-01

    The described investigation of crack formation and crack propagation in mode I (tensile stress) in fibre-reinforced plastic samples, especially uni-directional carbon fibre reinforced polyether-ether ketone (PEEK) has several aims. On the one hand, the phenomena of crack formation and crack propagation in these materials are to be studied, and on the other hand, the draft standards for these tests are to be checked. It was found that the combination of real time X-ray tests and simultaneous sound emission analysis is excellently suited for the basic examination of crack formation and crack propagation in DCB samples. With the aid of picture processing and analysis of the video representation, consistent crack lengths and resulting G IC values can be determined. (orig./RHM) [de

  8. Observational Trends of Cometary X-ray Emission

    Science.gov (United States)

    Lisse, C. M.

    2001-05-01

    The unexpected discovery of x-ray emission from Comet Hyakutake in March 1996 (Lisse et al. 1996) has produced a number of questions about the physical mechanism producing the radiation. The original detection and subsequent observations (Dennerl et al. 1997, Mumma et al. 1997, Krasnopolsky et al. 1998, Owens et al. 1998, Lisse et al. 1999, Lisse et a. 2001, Dennerl et al. 2001) have shown that the very soft (best fit thermal bremsstrahlung model kT = 0.23 keV) emission is due to an interaction between the solar wind and the comet's atmosphere. Using the results from the more than 15 comets detected to date in x-rays, we report on the latest results on cometary x-ray emission. Our emphasis will be on understanding the physical mechanism producing the emission, and using this to determine the nature of the cometary coma and solar wind flux. As-observed morphologies, spectra, and light curves will be discussed. We also report on the status of current cometary observations using the new powerful x-ray observatories Chandra and XMM. This work has been graciously supported by grants from the NASA Planetary Astronomy and Astrophysical Data Programs.

  9. Radio search for pulsed emission from X-ray pulsars

    Energy Technology Data Exchange (ETDEWEB)

    delli Santi, F S; Delpino, F [Bologna Univ. (Italy). Ist. di Astronomia; Inzani, P; Sironi, G [Consiglio Nazionale delle Ricerche, Milan (Italy). Lab. di Fisica Cosmica e Tecnologie Relative; Mandolesi, N; Morigi, G [Consiglio Nazionale delle Ricerche, Bologna (Italy). Lab. TESRE

    1981-05-01

    An experiment has been performed at 325 MHz, with a 10 m tracking dish, for the search of pulsed radio emission associated with X-ray pulsars. No evidence of radio pulses has been found in the four sources investigated, although the radio pulsar PSR 0329 + 54, used a testing object, has been detected successfully.

  10. CHANDRA DETECTION OF X-RAY EMISSION FROM ULTRACOMPACT DWARF GALAXIES AND EXTENDED STAR CLUSTERS

    Energy Technology Data Exchange (ETDEWEB)

    Hou, Meicun; Li, Zhiyuan, E-mail: lizy@nju.edu.cn [School of Astronomy and Space Science, Nanjing University, Nanjing 210046 (China)

    2016-03-10

    We have conducted a systematic study of X-ray emission from ultracompact dwarf (UCD) galaxies and extended star clusters (ESCs), based on archival Chandra observations. Among a sample of 511 UCDs and ESCs complied from the literature, 17 X-ray counterparts with 0.5–8 keV luminosities above ∼5 × 10{sup 36} erg s{sup −1} are identified, which are distributed in eight early-type host galaxies. To facilitate comparison, we also identify X-ray counterparts of 360 globular clusters (GCs) distributed in four of the eight galaxies. The X-ray properties of the UCDs and ESCs are found to be broadly similar to those of the GCs. The incidence rate of X-ray-detected UCDs and ESCs, 3.3% ± 0.8%, while lower than that of the X-ray-detected GCs (7.0% ± 0.4%), is substantially higher than expected from the field populations of external galaxies. A stacking analysis of the individually undetected UCDs/ESCs further reveals significant X-ray signals, which corresponds to an equivalent 0.5–8 keV luminosity of ∼4 × 10{sup 35} erg s{sup −1} per source. Taken together, these provide strong evidence that the X-ray emission from UCDs and ESCs is dominated by low-mass X-ray binaries having formed from stellar dynamical interactions, consistent with the stellar populations in these dense systems being predominantly old. For the most massive UCDs, there remains the possibility that a putative central massive black hole gives rise to the observed X-ray emission.

  11. CHANDRA DETECTION OF X-RAY EMISSION FROM ULTRACOMPACT DWARF GALAXIES AND EXTENDED STAR CLUSTERS

    International Nuclear Information System (INIS)

    Hou, Meicun; Li, Zhiyuan

    2016-01-01

    We have conducted a systematic study of X-ray emission from ultracompact dwarf (UCD) galaxies and extended star clusters (ESCs), based on archival Chandra observations. Among a sample of 511 UCDs and ESCs complied from the literature, 17 X-ray counterparts with 0.5–8 keV luminosities above ∼5 × 10 36 erg s −1 are identified, which are distributed in eight early-type host galaxies. To facilitate comparison, we also identify X-ray counterparts of 360 globular clusters (GCs) distributed in four of the eight galaxies. The X-ray properties of the UCDs and ESCs are found to be broadly similar to those of the GCs. The incidence rate of X-ray-detected UCDs and ESCs, 3.3% ± 0.8%, while lower than that of the X-ray-detected GCs (7.0% ± 0.4%), is substantially higher than expected from the field populations of external galaxies. A stacking analysis of the individually undetected UCDs/ESCs further reveals significant X-ray signals, which corresponds to an equivalent 0.5–8 keV luminosity of ∼4 × 10 35 erg s −1 per source. Taken together, these provide strong evidence that the X-ray emission from UCDs and ESCs is dominated by low-mass X-ray binaries having formed from stellar dynamical interactions, consistent with the stellar populations in these dense systems being predominantly old. For the most massive UCDs, there remains the possibility that a putative central massive black hole gives rise to the observed X-ray emission

  12. Analysis of nickel-base alloys by Grimm-type glow discharge emission and x-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Ferreira, N.P.; Strauss, J.A.; Van Maarseveen, I.; Ivanfy, A.B.

    1985-01-01

    Nickel-base alloys can be analysed as satisfactorily as steels by XRF as well as by the Grimm-type source, in spite of problems caused by element combinations, spectral line overlap and the influence of the structure and heat conduction properties on sputtering in the glow discharge source. This extended abstract briefly discusses the use of Grimm-type glow discharge emission and XRF as techniques for the analysis of nickel-base alloys

  13. X-ray emission from hot subdwarfs with compact companions

    Directory of Open Access Journals (Sweden)

    Esposito P.

    2013-03-01

    Full Text Available We review the X-ray observations of hot subdwarf stars. While no X-ray emission has been detected yet from binaries containing B-type subdwarfs, interesting results have been obtained in the case of the two luminous O-type subdwarfs HD 49798 and BD + 37° 442. Both of them are members of binary systems in which the X-ray luminosity is powered by accretion onto a compact object: a rapidly spinning (13.2 s and massive (1.28  M⊙ white dwarf in the case of HD 49798 and most likely a neutron star, spinning at 19.2 s, in the case of BD + 37° 442. Their study can shed light on the poorly known processes taking place during common envelope evolutionary phases and on the properties of wind mass loss from hot subdwarfs.

  14. X-ray emission from the Pleiades cluster

    Science.gov (United States)

    Agrawal, P. C.; Singh, K. P.; Riegler, G. R.

    1983-01-01

    The detection and identification of H0344+24, a new X-ray source located in the Pleiades cluster, is reported, based on observations made with HEAO A-2 low-energy detector 1 in the 0.15-3.0-keV energy band in August, 1977. The 90-percent-confidence error box for the new source is centered at 03 h 44.1 min right ascension (1950), near the center star of the 500-star Pleiades cluster, 25-eta-Tau. Since no likely galactic or extragalactic source of X-rays was found in a catalog search of the error-box region, identification of the source with the Pleiades cluster is considered secure. X-ray luminosity of the source is calculated to be about 10 to the 32nd ergs/sec, based on a distance of 125 pc. The X-ray characteristics of the Pleiades stars are discussed, and it is concluded that H0344+24 can best be explained as the integrated X-ray emission of all the B and F stars in the cluster.

  15. A laboratory-based hard x-ray monochromator for high-resolution x-ray emission spectroscopy and x-ray absorption near edge structure measurements

    Energy Technology Data Exchange (ETDEWEB)

    Seidler, G. T., E-mail: seidler@uw.edu; Mortensen, D. R.; Remesnik, A. J.; Pacold, J. I.; Ball, N. A.; Barry, N.; Styczinski, M.; Hoidn, O. R. [Physics Department, University of Washington, Seattle, Washington 98195-1560 (United States)

    2014-11-15

    We report the development of a laboratory-based Rowland-circle monochromator that incorporates a low power x-ray (bremsstrahlung) tube source, a spherically bent crystal analyzer, and an energy-resolving solid-state detector. This relatively inexpensive, introductory level instrument achieves 1-eV energy resolution for photon energies of ∼5 keV to ∼10 keV while also demonstrating a net efficiency previously seen only in laboratory monochromators having much coarser energy resolution. Despite the use of only a compact, air-cooled 10 W x-ray tube, we find count rates for nonresonant x-ray emission spectroscopy comparable to those achieved at monochromatized spectroscopy beamlines at synchrotron light sources. For x-ray absorption near edge structure, the monochromatized flux is small (due to the use of a low-powered x-ray generator) but still useful for routine transmission-mode studies of concentrated samples. These results indicate that upgrading to a standard commercial high-power line-focused x-ray tube or rotating anode x-ray generator would result in monochromatized fluxes of order 10{sup 6}–10{sup 7} photons/s with no loss in energy resolution. This work establishes core technical capabilities for a rejuvenation of laboratory-based hard x-ray spectroscopies that could have special relevance for contemporary research on catalytic or electrical energy storage systems using transition-metal, lanthanide, or noble-metal active species.

  16. Proton Induced X-ray Emission Analysis of Sources of Raw for Blue-and-White Porcelain From Jingdezhen and Dehua Area

    International Nuclear Information System (INIS)

    Liu Shunmin; Yang Dawei; Li Rongwu; Li Guoxia; Cheng Huansheng; Zheng Jongxin; Chen Lifang

    2010-01-01

    In order to find out sources of raw, ingredients and classification relationship for Blue-and-White porcelain from Jingdezhen and Dehua area in different time, 34 Blue-and-White porcelain samples were selected. The chemical ingredients of every sample were determined by proton induced X-ray emission. The chemical ingredients data of all samples were further analyzed using fuzzy cluster analysis. The results indicate that the sources of raw and classification relationship of majority bodies from Blue-and-White porcelain of Dehua and Jingdezhen area are commendably differentiated. The sources of raw and batch formulas of eight transparent enamel samples from Jingdezhen area in Ming Dynasty and majority transparent enamel samples from Dehua area are commendably differentiated. Except one or two samples, majority Blue-and-White glaze samples from two areas are obviously different, and it might be an important path for non-destructive discrimination among Blue-and-White porcelains from two areas. (authors)

  17. Synchrotron x-ray fluorescence and extended x-ray absorption fine structure analysis

    International Nuclear Information System (INIS)

    Chen, J.R.; Gordon, B.M.; Hanson, A.L.; Jones, K.W.; Kraner, H.W.; Chao, E.C.T.; Minkin, J.A.

    1984-01-01

    The advent of dedicated synchrotron radiation sources has led to a significant increase in activity in many areas of science dealing with the interaction of x-rays with matter. Synchrotron radiation provides intense, linearly polarized, naturally collimated, continuously tunable photon beams, which are used to determine not only the elemental composition of a complex, polyatomic, dilute material but also the chemical form of the elements with improved accuracy. Examples of the application of synchrotron radiation include experiments in synchrotron x-ray fluorescence (SXRF) analysis and extended x-ray absorption fine structure (EXAFS) analysis. New synchrotron radiation x-ray microprobes for elemental analysis in the parts per billion range are under construction at several laboratories. 76 references, 24 figures

  18. Weak Hard X-Ray Emission from Broad Absorption Line Quasars: Evidence for Intrinsic X-Ray Weakness

    DEFF Research Database (Denmark)

    Luo, B.; Brandt, W. N.; Alexander, D. M.

    2014-01-01

    We report NuSTAR observations of a sample of six X-ray weak broad absorption line (BAL) quasars. These targets, at z = 0.148-1.223, are among the optically brightest and most luminous BAL quasars known at z 330 times weaker than...... expected for typical quasars. Our results from a pilot NuSTAR study of two low-redshift BAL quasars, a Chandra stacking analysis of a sample of high-redshift BAL quasars, and a NuSTAR spectral analysis of the local BAL quasar Mrk 231 have already suggested the existence of intrinsically X-ray weak BAL...... quasars, i.e., quasars not emitting X-rays at the level expected from their optical/UV emission. The aim of the current program is to extend the search for such extraordinary objects. Three of the six new targets are weakly detected by NuSTAR with ≲ 45 counts in the 3-24 keV band, and the other three...

  19. Multielement analysis of environmental samples by total-reflection X-ray fluorescence sprectrometry, neutron activation analysis and inductively coupled plasma optical emission spectroscopy

    International Nuclear Information System (INIS)

    Michaelis, W.

    1986-01-01

    In environmental research and protection trace elements have to be determined over a wide range of atomic number, down to very low concentrations, and in quite different matrices. This challenge requires the availability of complementary analytical methods characterized by a high detection power and few sources of systematic errors. Besides, the capacity of multielement detection is often desired since it facilitates the talking of many problems in which numerous trace elements are of direct concern. Total-reflection X-ray fluorescence, neutron activation analysis and inductively coupled plasma optical emission spectroscopy, in principle fulfill these requirements quite well. However, each method has its domain, and the application to certain sample species may be less promising. Under this aspect, the paper summarizes some recent developments and investigations, including intercomparisons as far as possible. Various matrices are considered : rainwater and airborne particulates, soil samples, river sediments and suspended particulate matter, river water filtrates, ozean water, and organic matrices. Capabilities and limitations are discussed. Sample preparation techniques are described if they are new or essential for achieving the results given. (orig.) [de

  20. X-ray emission and the winds of cataclysmic variables

    International Nuclear Information System (INIS)

    Cordova, F.A.

    1985-01-01

    X-ray and ultraviolet observations of cataclysmic variable stars reveal a variety of exotic behavior - pulsations, winds, and episodic outbursts - are these related, what do they tell us about the nature of the outburst, about the environment of the accreting white dwarf. The author summarizes the observed changes in the x-ray and uv continuum and spectral features through the outbursts of the dwarf novae. The author then discusses how the modeling of these data have refined our ideas about the location and nature of the emissions, and the source of the outbursts. The author shows how comparisons of the x-ray and uv properties of cataclysmic variables with similar phenomena in other astronomical systems - the solar corona, OB stars, and Be stars - suggest ways in which the x-ray and uv emissions in CVs may be related, and point to further, specific observations that would elucidate our understanding of the behavior and role of the white dwarf in the outburst. 26 references

  1. Variability of X-ray emission from OB stars

    International Nuclear Information System (INIS)

    Collura, A.; Sciortino, S.; Serio, S.; Vaiana, G. S.; Harnden, F.R. JR.; Osservatorio Astronomico, Palermo, Italy; Harvard-Smithsonian Center for Astrophysics, Cambridge, MA)

    1989-01-01

    The variability in soft X-ray emission of 12 OB stars is studied. Two different methods of analysis, one more suitable for detecting short-term variations, the other aimed at detecting long time-scale variations, are applied to all stars in the sample. The long-term variability analysis shows that Cyg-OB2 8A Zeta Pup and Delta Ori exhibit significant count rate variations between different data sections. Similar variations are marginally detected in 15 Mon; the count rate variations for the other eight stars are consistent with statistical fluctuations. The light curve of Cyg-OB2 8A suggests the existence of two different emission levels. The short-term variability analysis detects marginal variability in Tau Sco with an effective amplitude of about 30 percent and a time scale of about 50 s. The upper limits to the effective short-term variability amplitude for all other sample stars are in the 10-30 percent range. 30 refs

  2. In vivo X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Ahlgren, L.

    1980-02-01

    Measurements on five occupationally exposed persons have shown that it is possible to use X-ray fluorescence analysis for in vivo measurements of lead in the skeleton. The technique for calibrating in vivo X-ray fluorescence measurements of lead in bone tissue has been studied in detail and a two-component phantom simulating the bone and the soft tissue parts of the finger constructed. The technique has been used for in vivo measurements on 22 occupationally exposed persons. The minimum detectable concentration of lead in fingerbones was found to be around 20 μg x g -1 . The lead concentrations in their skeletons and blood were compared: the correlation was poor. The variations in lead concentrations in the skeleton have been studied in occupationally exposed persons and in samples from archaeological skeletons. The sensitivity and the minimum detectable concentration of cadmium in the kidney cortex in in vivo measurements has been studied by measurements on kidney models. The minimum detectable concentration was 20 μg x g -1 at a skin-kidney distance of 30 mm and 40 μg x g -1 at 40 mm. Five persons occupationally exposed were studied. (Author)

  3. INTEGRAL hard X-ray spectra of the cosmic X-ray background and Galactic ridge emission

    Science.gov (United States)

    Türler, M.; Chernyakova, M.; Courvoisier, T. J.-L.; Lubiński, P.; Neronov, A.; Produit, N.; Walter, R.

    2010-03-01

    Aims: We derive the spectra of the cosmic X-ray background (CXB) and of the Galactic ridge X-ray emission (GRXE) in the ~20-200 keV range from the data of the IBIS instrument aboard the INTEGRAL satellite obtained during the four dedicated Earth-occultation observations in early 2006. Methods: We analyze the modulation of the IBIS/ISGRI detector counts induced by the passage of the Earth through the field of view of the instrument. Unlike previous studies, we do not fix the spectral shape of the various contributions, but model instead their spatial distribution and derive for each of them the expected modulation of the detector counts. The spectra of the diffuse emission components are obtained by fitting the normalizations of the model lightcurves to the observed modulation in different energy bins. Because of degeneracy, we guide the fits with a realistic choice of the input parameters and a constraint for spectral smoothness. Results: The obtained CXB spectrum is consistent with the historic HEAO-1 results and falls slightly below the spectrum derived with Swift/BAT. A 10% higher normalization of the CXB cannot be completely excluded, but it would imply an unrealistically high albedo of the Earth. The derived spectrum of the GRXE confirms the presence of a minimum around 80 keV with improved statistics and yields an estimate of ~0.6 M⊙ for the average mass of white dwarfs in the Galaxy. The analysis also provides updated normalizations for the spectra of the Earth's albedo and the cosmic-ray induced atmospheric emission. Conclusions: This study demonstrates the potential of INTEGRAL Earth-occultation observations to derive the hard X-ray spectra of three fundamental components: the CXB, the GRXE and the Earth emission. Further observations would be extremely valuable to confirm our results with improved statistics.

  4. Cosmological analysis of galaxy clusters surveys in X-rays

    International Nuclear Information System (INIS)

    Clerc, N.

    2012-01-01

    Clusters of galaxies are the most massive objects in equilibrium in our Universe. Their study allows to test cosmological scenarios of structure formation with precision, bringing constraints complementary to those stemming from the cosmological background radiation, supernovae or galaxies. They are identified through the X-ray emission of their heated gas, thus facilitating their mapping at different epochs of the Universe. This report presents two surveys of galaxy clusters detected in X-rays and puts forward a method for their cosmological interpretation. Thanks to its multi-wavelength coverage extending over 10 sq. deg. and after one decade of expertise, the XMM-LSS allows a systematic census of clusters in a large volume of the Universe. In the framework of this survey, the first part of this report describes the techniques developed to the purpose of characterizing the detected objects. A particular emphasis is placed on the most distant ones (z ≥ 1) through the complementarity of observations in X-ray, optical and infrared bands. Then the X-CLASS survey is fully described. Based on XMM archival data, it provides a new catalogue of 800 clusters detected in X-rays. A cosmological analysis of this survey is performed thanks to 'CR-HR' diagrams. This new method self-consistently includes selection effects and scaling relations and provides a means to bypass the computation of individual cluster masses. Propositions are made for applying this method to future surveys as XMM-XXL and eRosita. (author) [fr

  5. Fundamentals of energy dispersive X-ray analysis

    CERN Document Server

    Russ, John C; Kiessling, R; Charles, J

    1984-01-01

    Fundamentals of Energy Dispersive X-ray Analysis provides an introduction to the fundamental principles of dispersive X-ray analysis. It presents descriptions, equations, and graphs to enable the users of these techniques to develop an intuitive and conceptual image of the physical processes involved in the generation and detection of X-rays. The book begins with a discussion of X-ray detection and measurement, which is accomplished by one of two types of X-ray spectrometer: energy dispersive or wavelength dispersive. The emphasis is on energy dispersive spectrometers, given their rather wid

  6. X-ray fluorescence method for trace analysis and imaging

    International Nuclear Information System (INIS)

    Hayakawa, Shinjiro

    2000-01-01

    X-ray fluorescence analysis has a long history as conventional bulk elemental analysis with medium sensitivity. However, with the use of synchrotron radiation x-ray fluorescence method has become a unique analytical technique which can provide tace elemental information with the spatial resolution. To obtain quantitative information of trace elemental distribution by using the x-ray fluorescence method, theoretical description of x-ray fluorescence yield is described. Moreover, methods and instruments for trace characterization with a scanning x-ray microprobe are described. (author)

  7. X-ray Microprobe for Fluorescence and Diffraction Analysis

    International Nuclear Information System (INIS)

    Ice, G.E.

    2005-01-01

    X-ray diffraction (see unit 1.1) and x-ray excited fluorescence analysis are powerful techniques for the nondestructive measurement of crystal structure and chemical composition. X-ray fluorescence analysis is inherently nondestructive with orders of magnitude lower power deposited for the same detectable limit as with fluorescence excited by charged particle probes (Sparks, 1980). X-ray diffraction analysis is sensitive to crystal structure with orders-of-magnitude greater sensitivity to crystallographic strain than electron probes (Rebonato, et al. 1989). When a small-area x-ray microbeam is used as the probe, chemical composition (Z>14), crystal structure, crystalline texture, and crystalline strain distributions can be determined. These distributions can be studied both at the surface of the sample and deep within the sample (Fig. 1). Current state-of-the-art can achieve an ∼1 mm-D x-ray microprobe and an ∼0.1 mm-D x-ray microprobe has been demonstrated (Bilderback, et al., 1994). Despite their great chemical and crystallographic sensitivities, x-ray microprobe techniques have until recently been restricted by inefficient x-ray focusing optics and weak x-ray sources; x-ray microbeam analysis was largely superseded by electron techniques in the 50's. However, interest in x-ray microprobe techniques has now been revived (Howells, et al., 1983; Ice and Sparks, 1984; Chevallier, et al., 1997; Riekel 1992; Thompson, el al., 1992; and Making and Using... 1997) by the development of efficient x-ray focusing optics and ultra-high intensity synchrotron x-ray sources (Buras and Tazzari, 1984; Shenoy, et al., 1988). These advances have increased the achievable microbeam flux by more than 11 orders of magnitude (Fig. 2) (Ice, 1997); the flux in a tunable 1 mm-D beam on a 'so called' 3rd-generation synchrotron source such as the APS can exceed the flux in a fixed-energy mm2 beam on a conventional source. These advances make x-ray microfluorescence and x-ray

  8. X-ray emission characteristics of foam target plasmas

    International Nuclear Information System (INIS)

    Fronya, A.A.; Borisenko, N.G.; Chernodub, M.L.; Merkuliev, Yu.A.; Osipov, M.V.; Puzyrev, V.N.; Sahakyan, A.T.; Starodub, A.N.; Vasin, B.L.; Yakushev, O.F.

    2010-01-01

    Complete text of publication follows. Experimental results of laser radiation interaction with a foam targets are presented. The spatial, temporal and energy characteristics of x-ray plasma radiation have been investigated. The pinhole-camera and Schwarzschild objective have been used for the plasma image formation in different spectral ranges. The plasma image is registered by the Schwarzschild objective in a narrow spectral range 180 - 200 A. Spectral characteristics of x-ray radiation registered by pinhole-camera have been defined by means outer filters. The use of the filters with different transmission curves allowed one the determine the localization of x-ray radiation with fixed wavelength. Spatial resolution accounts 16 μm in the pinhole-camera diagnostic channel and 2.5 μm in the Schwarzschild objective diagnostic channel. The plasma images in the intrinsic x-ray radiation show that the emission area in the transverse direction with respect to the direction of the propagating heating radiation exceeds the focal spot size. This fact indicates that the target heating in the transverse direction is due to internal energy of the created plasma. The average value of plasma electron temperature is ∼ 0.4 - 1.4 keV. Acknowledgements. The work is partly supported by the Russian Foundation for Basic Researches, grant no. 10-02-00113 and by Federal Target Program 'Research and scientific-pedagogical cadres of Innovative Russia' (grant 2009-1.1-122-052-025).

  9. Electron emission regulator for an x-ray tube filament

    International Nuclear Information System (INIS)

    Daniels, H.E.; Randall, H.G.

    1982-01-01

    An x-ray tube ma regulator has an scr phase shift voltage regulator supplying the primary winding of a transformer whose secondary is coupled to the x-ray tube filament. Prior to initiation of an x-ray exposure, the filament is preheated to a temperature corresponding substantially to the electron emissivity needed for obtaining the desired tube ma during an exposure. During the preexposure interval, the phase shift regulator is controlled by a signal corresponding to the sum of signals representative of the voltage applied to the filament transformer, the desired filament voltage and the space charge compensation needed for the selected x-ray tube anode to cathode voltage. When an exposure is initiated, control of the voltage regulator is switched to a circuit that responds to the tube current by controlling the amount of phase shift and, hence, the voltage supplied to the transformer. Transformer leakage current compensation is provided during the exposure interval with a circuit that includes an element whose impedance is varied in accordance with the anode-to-cathode voltage setting so the element drains off tube current as required to cancel the effect of leakage current variations

  10. Hard X-ray emission spectroscopy with pink beam

    Energy Technology Data Exchange (ETDEWEB)

    Kvashnina, Kristina O.; Rossberg, Andre; Exner, Joerg; Scheinost, Andreas C. [Helmholtz-Zentrum Dresden-Rossendorf e.V., Dresden (Germany). Molecular Structures

    2017-06-01

    Valence-band X-ray emission spectroscopy (XES) with a ''pink beam'', i.e. a beam with large energy bandwidth produced by a double-multilayer monochromator, is introduced here to overcome the weak count rate of monochromatic beams produced by conventional double-crystal monochromators. Our results demonstrate that - in spite of the large bandwidth in the order of 100 eV - the high spectral resolution of the Johann-type spectrometer is maintained, while the two orders of magnitude higher flux greatly reduces the required counting time. The short working distance Johann-type X-ray emission spectrometer and multilayer monochromator is available at ROBL.

  11. Quantifying the Exospheric Component of Soft X-ray Emission

    Science.gov (United States)

    Kuntz, Kip; Collier, Michael R.; Snowden, Steven L.; Robertson, Ina; Hansen, Kenneth; Cravens, Thomas

    2007-01-01

    High charge state heavy ions in the solar wind exchange charge with ambient neutral gas. This process creates a product ion in an excited state. During the radiative cascade process, EUV and X-ray photons are emitted with energies in the range of about 100 eV to 1 keV. Because the terrestrial exospheric density at the nominal magnetopause location is relatively high, approx. 10 cu cm, solar wind charge exchange, or SWCX, can be observed by Earth-orbiting soft X-ray instruments such as the ROSAT Position Sensitive Proportional Counters (PSPC). In this presentation, we will compare simulated and observed soft Xray emission during an event on August 18-19, 1991 and discuss the role of exospheric SWCX emission for this and other events.

  12. NuSTAR HARD X-RAY SURVEY OF THE GALACTIC CENTER REGION. I. HARD X-RAY MORPHOLOGY AND SPECTROSCOPY OF THE DIFFUSE EMISSION

    Energy Technology Data Exchange (ETDEWEB)

    Mori, Kaya; Hailey, Charles J.; Perez, Kerstin; Nynka, Melania; Zhang, Shuo; Canipe, Alicia M. [Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Krivonos, Roman; Tomsick, John A.; Barrière, Nicolas; Boggs, Steven E.; Craig, William W. [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Hong, Jaesub [Harvard-Smithsonian Center for Astrophysics, Cambridge, MA 02138 (United States); Ponti, Gabriele [Max-Planck-Institut f. extraterrestrische Physik, HEG, Garching (Germany); Bauer, Franz [Instituto de Astrofísica, Facultad de Física, Pontificia Universidad Católica de Chile, 306, Santiago 22 (Chile); Alexander, David M. [Department of Physics, Durham University, Durham DH1 3LE (United Kingdom); Baganoff, Frederick K. [Kavli Institute for Astrophysics and Space Research, Massachusets Institute of Technology, Cambridge, MA 02139 (United States); Barret, Didier [Université de Toulouse, UPS-OMP, IRAP, Toulouse (France); Christensen, Finn E. [DTU Space—National Space Institute, Technical University of Denmark, Elektrovej 327, DK-2800 Lyngby (Denmark); Forster, Karl [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, Pasadena, CA 91125 (United States); Giommi, Paolo, E-mail: kaya@astro.columbia.edu [ASI Science Data Center, Via del Politecnico snc I-00133, Roma (Italy); and others

    2015-12-01

    We present the first sub-arcminute images of the Galactic Center above 10 keV, obtained with NuSTAR. NuSTAR resolves the hard X-ray source IGR J17456–2901 into non-thermal X-ray filaments, molecular clouds, point sources, and a previously unknown central component of hard X-ray emission (CHXE). NuSTAR detects four non-thermal X-ray filaments, extending the detection of their power-law spectra with Γ ∼ 1.3–2.3 up to ∼50 keV. A morphological and spectral study of the filaments suggests that their origin may be heterogeneous, where previous studies suggested a common origin in young pulsar wind nebulae (PWNe). NuSTAR detects non-thermal X-ray continuum emission spatially correlated with the 6.4 keV Fe Kα fluorescence line emission associated with two Sgr A molecular clouds: MC1 and the Bridge. Broadband X-ray spectral analysis with a Monte-Carlo based X-ray reflection model self-consistently determined their intrinsic column density (∼10{sup 23} cm{sup −2}), primary X-ray spectra (power-laws with Γ ∼ 2) and set a lower limit of the X-ray luminosity of Sgr A* flare illuminating the Sgr A clouds to L{sub X} ≳ 10{sup 38} erg s{sup −1}. Above ∼20 keV, hard X-ray emission in the central 10 pc region around Sgr A* consists of the candidate PWN G359.95–0.04 and the CHXE, possibly resulting from an unresolved population of massive CVs with white dwarf masses M{sub WD} ∼ 0.9 M{sub ⊙}. Spectral energy distribution analysis suggests that G359.95–0.04 is likely the hard X-ray counterpart of the ultra-high gamma-ray source HESS J1745–290, strongly favoring a leptonic origin of the GC TeV emission.

  13. Scaling of x-ray emission and ion velocity in laser produced Cu ...

    Indian Academy of Sciences (India)

    Laser plasma; x-ray emission; conversion efficiency; ion velocities. ... fits from this kind of optimization studies are in the fields of x-ray lithography, x-ray lasers etc. .... formula between the x-ray conversion rate versus different parameters of the ...

  14. A deep view in cultural heritage - confocal micro X-ray spectroscopy for depth resolved elemental analysis

    International Nuclear Information System (INIS)

    Kanngiesser, B.; Malzer, W.; Mantouvalou, I.; Sokaras, D.; Karydas, A.G.

    2012-01-01

    Quantitative X-ray fluorescence (XRF) and particle induced X-ray emission (PIXE) techniques have been developed mostly for the elemental analysis of homogeneous bulk or very simple layered materials. Further on, the microprobe version of both techniques is applied for 2D elemental mapping of surface heterogeneities. At typical XRF/PIXE fixed geometries and exciting energies (15-25 keV and 2-3 MeV, respectively), the analytical signal (characteristic X-ray radiation) emanates from a variable but rather extended depth within the analyzed material, according to the exciting probe energy, set-up geometry, specimen matrix composition and analyte. Consequently, the in-depth resolution offered by XRF and PIXE techniques is rather limited for the characterization of materials with micrometer-scale stratigraphy or 3D heterogeneous structures. This difficulty has been over-passed to some extent in the case of an X-ray or charged particle microprobe by creating the so-called confocal geometry. The field of view of the X-ray spectrometer is spatially restricted by a polycapillary X-ray lens within a sensitive microvolume formed by the two inter-sectioned focal regions. The precise scanning of the analyzed specimen through the confocal microvolume results in depth-sensitive measurements, whereas the additional 2D scanning microprobe possibilities render to element-specific 3D spatial resolution (3D micro-XRF and 3D micro-PIXE). These developments have contributed since 2003 to a variety of fields of applications in environmental, material and life sciences. In contrast to other elemental imaging methods, no size restriction of the objects investigated and the non-destructive character of analysis have been found indispensable for cultural heritage (CH) related applications. The review presents a summary of the experimental set-up developments at synchrotron radiation beamlines, particle accelerators and desktop spectrometers that have driven methodological developments and

  15. Relative probabilities of the uranium isotopes for thorium x-ray emission and fluorescence of uranium x-rays

    International Nuclear Information System (INIS)

    Parker, J.L.

    1991-01-01

    Both thorium x-rays from decaying uranium isotopes and self-fluoresced uranium x-rays are prominent in high-resolution gamma-ray spectra of uranium-bearing materials. Useful application of the information carried by those x-rays has been curtailed because the probabilities of the uranium isotopes for thorium x-ray emission and for uranium x-ray fluorescence have not been known. By analyzing enrichment-meter geometry spectra from uranium oxide standards whose enrichments ranged from 0.7% to 91%, relative values, primarily, have been obtained for the probabilities of both processes. Thorium x-ray emission is very heavily dominated by 235 U. In all ordinarily occurring uranium isotopic distributions, thorium x-rays may be used as a valid 235 U signature. The probability for a thorium K α1 x-ray to be emitted in the decay of a 235 U atom is 0.048 ±0.002. In infinitely thick uranium oxide materials, the relative ratios of effectiveness for self-fluorescence, on a per unit mass basis, are approximately 234 U : 235 U : 236 U : 238 U = 1.13 : 1.00 : 0.52 : 0.028. on a per decay basis, the approximate ratios are 0.00039 : 1.00 : 0.017 : 0.18. These results imply that, contrary to what has often been stated, gamma rays are far more important than alpha particles in the self-fluorescence of uranium. Because of the importance of gamma-ray self-fluorescence, the uranium x-ray yield will be somewhat influenced by the size, shape, and composition of the materials. 4 refs., 1 fig

  16. Colliding Stellar Winds Structure and X-ray Emission

    Science.gov (United States)

    Pittard, J. M.; Dawson, B.

    2018-04-01

    We investigate the structure and X-ray emission from the colliding stellar winds in massive star binaries. We find that the opening angle of the contact discontinuity (CD) is overestimated by several formulae in the literature at very small values of the wind momentum ratio, η. We find also that the shocks in the primary (dominant) and secondary winds flare by ≈20° compared to the CD, and that the entire secondary wind is shocked when η ≲ 0.02. Analytical expressions for the opening angles of the shocks, and the fraction of each wind that is shocked, are provided. We find that the X-ray luminosity Lx∝η, and that the spectrum softens slightly as η decreases.

  17. X-Rays from NGC 3256: High-Energy Emission in Starburst Galaxies and Their Contribution to the Cosmic X-Ray Background

    International Nuclear Information System (INIS)

    Moran, Edward C.; Lehnert, Matthew D.; Helfand, David J.

    1999-01-01

    The infrared-luminous galaxy NGC 3256 is a classic example of a merger-induced nuclear starburst system. We find here that it is the most X-ray-luminous star-forming galaxy yet detected (L 0.5-10keV =1.6x10 42 ergs s-1). Long-slit optical spectroscopy and a deep, high-resolution ROSAT X-ray image show that the starburst is driving a ''superwind'' which accounts for ∼20% of the observed soft X-ray emission. Analysis of X-ray spectral data from ASCA indicates this gas has a characteristic temperature of kT≅0.3 keV. Our model for the broadband X-ray emission of NGC 3256 contains two additional components: a warm thermal plasma (kT≅0.8 keV) associated with the central starburst, and a hard power-law component with an energy index of α X ≅0.7. We discuss the energy budget for the two thermal plasmas and find that the input of mechanical energy from the starburst is more than sufficient to sustain the observed level of emission. We also examine possible origins for the power-law component, concluding that neither a buried AGN nor the expected population of high-mass X-ray binaries can account for this emission. Inverse Compton scattering, involving the galaxy's copious flux of infrared photons and the relativistic electrons produced by supernovae, is likely to make a substantial contribution to the hard X-ray flux. Such a model is consistent with the observed radio and IR fluxes and the radio and X-ray spectral indices. We explore the role of X-ray-luminous starbursts in the production of the cosmic X-ray background radiation. The number counts and spectral index distribution of the faint radio source population, thought to be dominated by star-forming galaxies, suggest that a significant fraction of the hard X-ray background could arise from starbursts at moderate redshift. (c) (c) 1999. The American Astronomical Society

  18. X-Ray analysis and methods for nondestructive control (On the 100-anniversary of X-ray foundation)

    International Nuclear Information System (INIS)

    Sosnin, F.R.

    1995-01-01

    Brief consideration is given to the history of X-ray discovery, formation of domestic X-ray industry. Principles of operation and potentialities of X-ray diffraction analysis, gammagraphy, radioscopy, radiometric analysis are described briefly. Domestic and foreign scientists, institutes and companies who contributed much to development of methods for nondestructive control are listed

  19. X-ray/UV variability and the origin of soft X-ray excess emission from II Zw 177

    Science.gov (United States)

    Pal, Main

    We study a detailed broad-band X-ray/UV emission from the narrow line Seyfert 1 galaxy II Zw 177 based on two XMM-Newton and single Swift/XRT observations. Both XMM-Newton observations show the soft X-ray excess emission below 2 keV when the best-fit 2 - 10 keV power law is extrapolated down to 0.3 keV. We find the blurred reflection from an ionized accretion disc and Comptonized disc emission both describe the observed soft excess well. We find a remarkable trend of decreasing UV flux with increasing soft X-ray excess and power law emission. We suggest that this could be due to that the external edge of corona hide a fraction of accretion disk. Co-Author: Prof. Gulab C. Dewangan (IUCAA), Prof. Ranjeev Misra (IUCAA), Pramod Kumar (Nanded university)

  20. A Non-thermal Pulsed X-Ray Emission of AR Scorpii

    Science.gov (United States)

    Takata, J.; Hu, C.-P.; Lin, L. C. C.; Tam, P. H. T.; Pal, P. S.; Hui, C. Y.; Kong, A. K. H.; Cheng, K. S.

    2018-02-01

    We report the analysis result of UV/X-ray emission from AR Scorpii, which is an intermediate polar (IP) composed of a magnetic white dwarf and an M-type star, with the XMM-Newton data. The X-ray/UV emission clearly shows a large variation over the orbit, and their intensity maximum (or minimum) is located at the superior conjunction (or inferior conjunction) of the M star orbit. The hardness ratio of the X-ray emission shows a small variation over the orbital phase and shows no indication of the absorption by an accretion column. These properties are naturally explained by the emission from the M star surface rather than that from the accretion column on the white dwarf’s (WD) star, which is similar to usual IPs. Additionally, the observed X-ray emission also modulates with the WD’s spin with a pulse fraction of ∼14%. The peak position is aligned in the optical/UV/X-ray band. This supports the hypothesis that the electrons in AR Scorpii are accelerated to a relativistic speed and emit non-thermal photons via the synchrotron radiation. In the X-ray bands, evidence of the power-law spectrum is found in the pulsed component, although the observed emission is dominated by the optically thin thermal plasma emissions with several different temperatures. It is considered that the magnetic dissipation/reconnection process on the M star surface heats up the plasma to a temperature of several keV and also accelerates the electrons to the relativistic speed. The relativistic electrons are trapped in the WD’s closed magnetic field lines by the magnetic mirror effect. In this model, the observed pulsed component is explained by the emissions from the first magnetic mirror point.

  1. Application of X-ray spectroscopy in nondestructive photon activation analysis

    International Nuclear Information System (INIS)

    Weise, H.-P.; Segebade, Chr.

    1977-01-01

    The use of X-ray spectroscopy for the qualitative and quantitative analysis of samples activated by 30 MeV bremsstrahlung from an electron linear accelerator. Detection limits are calculated from the measured X-ray spectra and compared with those for γ-ray spectroscopy. In general, the detection limits for γ-ray and X-ray spectroscopy are comparable. Higher sensitivities for X-ray spectroscopy are observed when only low intensity γ-rays are emitted by the activation products. X-ray spectroscopy should be applied in three cases: (a) low γ-ray emission probability, (b) extremely complicated γ-ray spectrum, (c) overlapping of γ-ray lines from different elements. γ-ray spectroscopy should be preferred for the analysis of light elements for two reasons: very strong absorption of low energy X-rays (low Z) within the sample, low X-ray emission probability for the activation products of light elements. Therefore no attempt was made to use X-ray spectroscopy for the analysis of elements below Ti. Some practical applications of X-ray spectroscopy in nondestructive multielement analysis are quoted. (T.G.)

  2. Absorption correction factor in X-ray fluorescent quantitative analysis

    International Nuclear Information System (INIS)

    Pimjun, S.

    1994-01-01

    An experiment on absorption correction factor in X-ray fluorescent quantitative analysis were carried out. Standard samples were prepared from the mixture of Fe 2 O 3 and tapioca flour at various concentration of Fe 2 O 3 ranging from 5% to 25%. Unknown samples were kaolin containing 3.5% to-50% of Fe 2 O 3 Kaolin samples were diluted with tapioca flour in order to reduce the absorption of FeK α and make them easy to prepare. Pressed samples with 0.150 /cm 2 and 2.76 cm in diameter, were used in the experiment. Absorption correction factor is related to total mass absorption coefficient (χ) which varied with sample composition. In known sample, χ can be calculated by conveniently the formula. However in unknown sample, χ can be determined by Emission-Transmission method. It was found that the relationship between corrected FeK α intensity and contents of Fe 2 O 3 in these samples was linear. This result indicate that this correction factor can be used to adjust the accuracy of X-ray intensity. Therefore, this correction factor is essential in quantitative analysis of elements comprising in any sample by X-ray fluorescent technique

  3. Discovery of Diffuse Hard X-ray Emission associated with Jupiter

    Science.gov (United States)

    Ezoe, Y.; Miyoshi, Y.; Ishikawa, K.; Ohashi, T.; Terada, N.; Uchiyama, Y.; Negoro, H.

    2009-12-01

    Our discovery of diffuse hard (1-5 keV) X-ray emission around Jupiter is reported. Recent Chandra and XMM-Newton observations revealed several types of X-rays in the vicinity of Jupiter such as auroral and disk emission from Jupiter and faint diffuse X-rays from the Io Plasma Torus (see Bhardwaj et al. 2007 for review). To investigate possible diffuse hard X-ray emission around Jupiter with the highest sensitivity, we conducted data analysis of Suzaku XIS observations of Jupiter on Feb 2006. After removing satellite and planetary orbital motions, we detected a significant diffuse X-ray emission extending to ~6 x 3 arcmin with the 1-5 keV X-ray luminosity of ~3e15 erg/s. The emitting region very well coincided with the Jupiter's radiation belts. The 1-5 keV X-ray spectrum was represented by a simple power law model with a photon index of 1.4. Such a flat continuum strongly suggests non-thermal origin. Although such an emission can be originated from multiple background point sources, its possibility is quite low. We hence examined three mechanisms, assuming that the emission is truly diffuse: bremsstrahlung by keV electrons, synchrotron emission by TeV electrons, and inverse Compton scattering of solar photons by MeV electrons. The former two can be rejected because of the X-ray spectral shape and implausible existence of TeV electrons around Jupiter, respectively. The last possibility was found to be possible because tens MeV electrons, which have been confirmed in inner radiation belts (Bolton et al. 2002), can kick solar photons to the keV energy range and provide a simple power-law continuum. We estimated an average electron density from the X-ray luminosity assuming the oblate spheroid shaped emitting region with 8 x 8 x 4 Jovian radii. The necessary density was 0.02 1/cm3 for 50 MeV electrons. Hence, our results may suggest a new particle acceleration phenomenon around Jupiter.

  4. Effect of Electric Voltage and Current of X-ray Chamber on the Element inthe Zirconium Alloy Analysis X-ray by X-ray Fluorescence

    International Nuclear Information System (INIS)

    Yusuf-Nampira; Narko-Wibowo, L; Rosika-Krisnawati; Nudia-Barenzani

    2000-01-01

    The using of x-ray fluorescence in the chemical analysis depend heavilyon the parameters of x-ray chamber, for examples : electric voltage andelectric current. That parameter give effect in the result of determine ofSn, Cr, Fe and Ni in the zirconium alloy. 20 kV electric voltages are used onthe Mo x-ray chamber shall product x-ray of zirconium in the sample materialcan give effect in the stability of the analysis result (deviation more than5%). The result of analysis of elements in the zirconium alloy shall givedeviation less than 5% when using of electric voltage of the x-ray chamberless than 19 kV. The sensitivity of analysis can be reached by step upelectric current of x-ray chamber. (author)

  5. AGN X-Ray emission and black holes (Kelly+, 2008)

    DEFF Research Database (Denmark)

    Kelly, B. C.; Bechtold, J.; Trump, J. R.

    2009-01-01

    In this analysis we combine 169 RQQs from Kelly et al. (2007ApJ...665.1489K) with 149 RQQs from the main SDSS sample of Strateva et al. (2005, Cat. J/AJ/130/387) to create a sample of 318 RQQs. Out of these 318 sources, 276 (86.8%) are detected in the X-ray. (1 data file)....

  6. X-ray analysis in lung leptospira disease

    International Nuclear Information System (INIS)

    Deng Shiyong; Peng Shi; He Guoman

    2006-01-01

    Objective: To analysis the X-ray signs and subtype of the lung leptospira disease, and improve the undersdand, reduce the error diagnosis of this diseases. Methods: 40 cases of lung leptospira disease were evaluated about the check X-ray sings and clinical data, the check X-ray sings were dynamic observated and typed, and 40 cases had a diagnostic treatment. Results: There were various X-ray changes of lung leptospira disease. in 40 cases, 12 cases (30%) pulmonary marking, 21 cases (52%) little lesions, and 7 cases(18%) lager lesions, respectively. The patients who were correctly diagnosed made a recovery after effective treatment, the patients who were error diagnosed died because of multiple system organ damage. Conclusion: The check X-ray signs in lung leptospira disease have some characteristics. It may play an important role in improving this disease' diagnosis combining the dynamic observation of check X-ray sings with clinical data. (authors)

  7. Comparison of a portable micro-X-ray fluorescence spectrometry with inductively coupled plasma atomic emission spectrometry for the ancient ceramics analysis

    International Nuclear Information System (INIS)

    Papadopoulou, D.N.; Zachariadis, G.A.; Anthemidis, A.N.; Tsirliganis, N.C.; Stratis, J.A.

    2004-01-01

    Two multielement instrumental methods of analysis, micro X-ray fluorescence spectrometry (micro-XRF) and inductively coupled plasma atomic emission spectrometry (ICP-AES) were applied for the analysis of 7th and 5th century B.C. ancient ceramic sherds in order to evaluate the above two methods and to assess the potential to use the current compact and portable micro-XRF instrument for the in situ analysis of ancient ceramics. The distinguishing factor of interest is that micro-XRF spectrometry offers the possibility of a nondestructive analysis, an aspect of primary importance in the compositional analysis of cultural objects. Micro-XRF measurements were performed firstly directly on the ceramic sherds with no special pretreatment apart from surface cleaning (micro-XRF on sherds) and secondly on pressed pellet disks which were prepared for each ceramic sherd (micro-XRF on pellet). For the ICP-AES determination of elements, test solutions were prepared by the application of a microwave-assisted decomposition procedure in closed high-pressure PFA vessels. Also, the standard reference material SARM 69 was used for the efficiency calibration of the micro-XRF instrument and was analysed by both methods. In order to verify the calibration, the standard reference materials NCS DC 73332 and SRM620 as well as the reference materials AWI-1 and PRI-1 were analysed by micro-XRF. Elemental concentrations determined by the three analytical procedures (ICP-AES, micro-XRF on sherds and micro-XRF on pellets) were statistically treated by correlation analysis and Student's t-test (at the 95% confidence level)

  8. Comparison of a portable micro-X-ray fluorescence spectrometry with inductively coupled plasma atomic emission spectrometry for the ancient ceramics analysis

    Energy Technology Data Exchange (ETDEWEB)

    Papadopoulou, D.N. [Laboratory of Analytical Chemistry, Faculty of Chemistry, Aristotle University, GR-54124, Thessaloniki (Greece); Zachariadis, G.A. [Laboratory of Analytical Chemistry, Faculty of Chemistry, Aristotle University, GR-54124, Thessaloniki (Greece); Anthemidis, A.N. [Laboratory of Analytical Chemistry, Faculty of Chemistry, Aristotle University, GR-54124, Thessaloniki (Greece); Tsirliganis, N.C. [Archaeometry Laboratory, Cultural and Educational Technology Institute, Tsimiski 58, GR-67100, Xanthi (Greece); Stratis, J.A. [Laboratory of Analytical Chemistry, Faculty of Chemistry, Aristotle University, GR-54124, Thessaloniki (Greece)]. E-mail: jstratis@chem.auth.gr

    2004-12-01

    Two multielement instrumental methods of analysis, micro X-ray fluorescence spectrometry (micro-XRF) and inductively coupled plasma atomic emission spectrometry (ICP-AES) were applied for the analysis of 7th and 5th century B.C. ancient ceramic sherds in order to evaluate the above two methods and to assess the potential to use the current compact and portable micro-XRF instrument for the in situ analysis of ancient ceramics. The distinguishing factor of interest is that micro-XRF spectrometry offers the possibility of a nondestructive analysis, an aspect of primary importance in the compositional analysis of cultural objects. Micro-XRF measurements were performed firstly directly on the ceramic sherds with no special pretreatment apart from surface cleaning (micro-XRF on sherds) and secondly on pressed pellet disks which were prepared for each ceramic sherd (micro-XRF on pellet). For the ICP-AES determination of elements, test solutions were prepared by the application of a microwave-assisted decomposition procedure in closed high-pressure PFA vessels. Also, the standard reference material SARM 69 was used for the efficiency calibration of the micro-XRF instrument and was analysed by both methods. In order to verify the calibration, the standard reference materials NCS DC 73332 and SRM620 as well as the reference materials AWI-1 and PRI-1 were analysed by micro-XRF. Elemental concentrations determined by the three analytical procedures (ICP-AES, micro-XRF on sherds and micro-XRF on pellets) were statistically treated by correlation analysis and Student's t-test (at the 95% confidence level)

  9. Quantitative analysis with energy dispersive X-ray fluorescence analyser

    International Nuclear Information System (INIS)

    Kataria, S.K.; Kapoor, S.S.; Lal, M.; Rao, B.V.N.

    1977-01-01

    Quantitative analysis of samples using radioisotope excited energy dispersive x-ray fluorescence system is described. The complete set-up is built around a locally made Si(Li) detector x-ray spectrometer with an energy resolution of 220 eV at 5.94 KeV. The photopeaks observed in the x-ray fluorescence spectra are fitted with a Gaussian function and the intensities of the characteristic x-ray lines are extracted, which in turn are used for calculating the elemental concentrations. The results for a few typical cases are presented. (author)

  10. Weak Hard X-Ray Emission from Two Broad Absorption Line Quasars Observed with NuStar: Compton-Thick Absorption or Intrinsic X-Ray Weakness?

    Science.gov (United States)

    Luo, B.; Brandt, W. N.; Alexander, D. M.; Harrison, F. A.; Stern, D.; Bauer, F. E.; Boggs, S. E.; Christensen, F. E.; Comastri, A.; Craig, W. W..; hide

    2013-01-01

    We present Nuclear Spectroscopic Telescope Array (NuSTAR) hard X-ray observations of two X-ray weak broad absorption line (BAL) quasars, PG 1004+130 (radio loud) and PG 1700+518 (radio quiet). Many BAL quasars appear X-ray weak, probably due to absorption by the shielding gas between the nucleus and the accretion-disk wind. The two targets are among the optically brightest BAL quasars, yet they are known to be significantly X-ray weak at rest-frame 2-10 keV (16-120 times fainter than typical quasars). We would expect to obtain approx. or equal to 400-600 hard X-ray (is greater than or equal to 10 keV) photons with NuSTAR, provided that these photons are not significantly absorbed N(sub H) is less than or equal to 10(exp24) cm(exp-2). However, both BAL quasars are only detected in the softer NuSTAR bands (e.g., 4-20 keV) but not in its harder bands (e.g., 20-30 keV), suggesting that either the shielding gas is highly Compton-thick or the two targets are intrinsically X-ray weak. We constrain the column densities for both to be N(sub H) 7 × 10(exp 24) cm(exp-2) if the weak hard X-ray emission is caused by obscuration from the shielding gas. We discuss a few possibilities for how PG 1004+130 could have Compton-thick shielding gas without strong Fe Ka line emission; dilution from jet-linked X-ray emission is one likely explanation. We also discuss the intrinsic X-ray weakness scenario based on a coronal-quenching model relevant to the shielding gas and disk wind of BAL quasars. Motivated by our NuSTAR results, we perform a Chandra stacking analysis with the Large Bright Quasar Survey BAL quasar sample and place statistical constraints upon the fraction of intrinsically X-ray weak BAL quasars; this fraction is likely 17%-40%.

  11. WEAK HARD X-RAY EMISSION FROM TWO BROAD ABSORPTION LINE QUASARS OBSERVED WITH NuSTAR: COMPTON-THICK ABSORPTION OR INTRINSIC X-RAY WEAKNESS?

    Energy Technology Data Exchange (ETDEWEB)

    Luo, B.; Brandt, W. N. [Department of Astronomy and Astrophysics, 525 Davey Lab, The Pennsylvania State University, University Park, PA 16802 (United States); Alexander, D. M.; Hickox, R. [Department of Physics, Durham University, South Road, Durham DH1 3LE (United Kingdom); Harrison, F. A.; Fuerst, F.; Grefenstette, B. W.; Madsen, K. K. [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, Pasadena, CA 91125 (United States); Stern, D. [Jet Propulsion Laboratory, California Institute of Technology, Pasadena, CA 91109 (United States); Bauer, F. E. [Departamento de Astronomia y Astrofisica, Pontificia Universidad Catolica de Chile, Casilla 306, Santiago 22 (Chile); Boggs, S. E.; Craig, W. W. [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Christensen, F. E. [DTU Space-National Space Institute, Technical University of Denmark, Elektrovej 327, DK-2800 Lyngby (Denmark); Comastri, A. [INAF-Osservatorio Astronomico di Bologna, Via Ranzani 1, I-40127 Bologna (Italy); Fabian, A. C. [Institute of Astronomy, Madingley Road, Cambridge CB3 0HA (United Kingdom); Farrah, D. [Department of Physics, Virginia Tech, Blacksburg, VA 24061 (United States); Fiore, F. [Osservatorio Astronomico di Roma, via Frascati 33, I-00040 Monteporzio Catone (Italy); Hailey, C. J. [Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Matt, G. [Dipartimento di Matematica e Fisica, Universita degli Studi Roma Tre, via della Vasca Navale 84, I-00146 Roma (Italy); Ogle, P. [IPAC, California Institute of Technology, Mail Code 220-6, Pasadena, CA 91125 (United States); and others

    2013-08-01

    We present Nuclear Spectroscopic Telescope Array (NuSTAR) hard X-ray observations of two X-ray weak broad absorption line (BAL) quasars, PG 1004+130 (radio loud) and PG 1700+518 (radio quiet). Many BAL quasars appear X-ray weak, probably due to absorption by the shielding gas between the nucleus and the accretion-disk wind. The two targets are among the optically brightest BAL quasars, yet they are known to be significantly X-ray weak at rest-frame 2-10 keV (16-120 times fainter than typical quasars). We would expect to obtain Almost-Equal-To 400-600 hard X-ray ({approx}> 10 keV) photons with NuSTAR, provided that these photons are not significantly absorbed (N{sub H} {approx}< 10{sup 24} cm{sup -2}). However, both BAL quasars are only detected in the softer NuSTAR bands (e.g., 4-20 keV) but not in its harder bands (e.g., 20-30 keV), suggesting that either the shielding gas is highly Compton-thick or the two targets are intrinsically X-ray weak. We constrain the column densities for both to be N{sub H} Almost-Equal-To 7 Multiplication-Sign 10{sup 24} cm{sup -2} if the weak hard X-ray emission is caused by obscuration from the shielding gas. We discuss a few possibilities for how PG 1004+130 could have Compton-thick shielding gas without strong Fe K{alpha} line emission; dilution from jet-linked X-ray emission is one likely explanation. We also discuss the intrinsic X-ray weakness scenario based on a coronal-quenching model relevant to the shielding gas and disk wind of BAL quasars. Motivated by our NuSTAR results, we perform a Chandra stacking analysis with the Large Bright Quasar Survey BAL quasar sample and place statistical constraints upon the fraction of intrinsically X-ray weak BAL quasars; this fraction is likely 17%-40%.

  12. The application of proton induced X-ray emission in criminalistics

    International Nuclear Information System (INIS)

    Li Zhenyuan; Xie Shuxian

    1993-01-01

    The determination method of trace elements in high pure gold by proton induced X-ray emission is reported. The target preparation, design of physical experiment, data proceeding and the analysis of gold samples by the internal standard of single-standard are discussed. Using this determination method, the identification of a sample of high pure gold is performed

  13. X-ray spectrometry and X-ray microtomography techniques for soil and geological samples analysis

    Energy Technology Data Exchange (ETDEWEB)

    Kubala-Kukuś, A.; Banaś, D.; Braziewicz, J. [Institute of Physics, Jan Kochanowski University, ul. Świetokrzyska 15, 25-406 Kielce (Poland); Holycross Cancer Center, ul. Artwińskiego 3, 25-734 Kielce (Poland); Dziadowicz, M.; Kopeć, E. [Institute of Physics, Jan Kochanowski University, ul. Świetokrzyska 15, 25-406 Kielce (Poland); Majewska, U. [Institute of Physics, Jan Kochanowski University, ul. Świetokrzyska 15, 25-406 Kielce (Poland); Holycross Cancer Center, ul. Artwińskiego 3, 25-734 Kielce (Poland); Mazurek, M.; Pajek, M.; Sobisz, M.; Stabrawa, I. [Institute of Physics, Jan Kochanowski University, ul. Świetokrzyska 15, 25-406 Kielce (Poland); Wudarczyk-Moćko, J. [Holycross Cancer Center, ul. Artwińskiego 3, 25-734 Kielce (Poland); Góźdź, S. [Holycross Cancer Center, ul. Artwińskiego 3, 25-734 Kielce (Poland); Institute of Public Health, Jan Kochanowski University, IX Wieków Kielc 19, 25-317 Kielce (Poland)

    2015-12-01

    A particular subject of X-ray fluorescence analysis is its application in studies of the multielemental sample of composition in a wide range of concentrations, samples with different matrices, also inhomogeneous ones and those characterized with different grain size. Typical examples of these kinds of samples are soil or geological samples for which XRF elemental analysis may be difficult due to XRF disturbing effects. In this paper the WDXRF technique was applied in elemental analysis concerning different soil and geological samples (therapeutic mud, floral soil, brown soil, sandy soil, calcium aluminum cement). The sample morphology was analyzed using X-ray microtomography technique. The paper discusses the differences between the composition of samples, the influence of procedures with respect to the preparation of samples as regards their morphology and, finally, a quantitative analysis. The results of the studies were statistically tested (one-way ANOVA and correlation coefficients). For lead concentration determination in samples of sandy soil and cement-like matrix, the WDXRF spectrometer calibration was performed. The elemental analysis of the samples was complemented with knowledge of chemical composition obtained by X-ray powder diffraction.

  14. X-ray spectrometry and X-ray microtomography techniques for soil and geological samples analysis

    International Nuclear Information System (INIS)

    Kubala-Kukuś, A.; Banaś, D.; Braziewicz, J.; Dziadowicz, M.; Kopeć, E.; Majewska, U.; Mazurek, M.; Pajek, M.; Sobisz, M.; Stabrawa, I.; Wudarczyk-Moćko, J.; Góźdź, S.

    2015-01-01

    A particular subject of X-ray fluorescence analysis is its application in studies of the multielemental sample of composition in a wide range of concentrations, samples with different matrices, also inhomogeneous ones and those characterized with different grain size. Typical examples of these kinds of samples are soil or geological samples for which XRF elemental analysis may be difficult due to XRF disturbing effects. In this paper the WDXRF technique was applied in elemental analysis concerning different soil and geological samples (therapeutic mud, floral soil, brown soil, sandy soil, calcium aluminum cement). The sample morphology was analyzed using X-ray microtomography technique. The paper discusses the differences between the composition of samples, the influence of procedures with respect to the preparation of samples as regards their morphology and, finally, a quantitative analysis. The results of the studies were statistically tested (one-way ANOVA and correlation coefficients). For lead concentration determination in samples of sandy soil and cement-like matrix, the WDXRF spectrometer calibration was performed. The elemental analysis of the samples was complemented with knowledge of chemical composition obtained by X-ray powder diffraction.

  15. Temporal characteristic analysis of laser-modulated pulsed X-ray source for space X-ray communication

    Science.gov (United States)

    Hang, Shuang; Liu, Yunpeng; Li, Huan; Tang, Xiaobin; Chen, Da

    2018-04-01

    X-ray communication (XCOM) is a new communication type and is expected to realize high-speed data transmission in some special communication scenarios, such as deep space communication and blackout communication. This study proposes a high-speed modulated X-ray source scheme based on the laser-to-X-ray conversion. The temporal characteristics of the essential components of the proposed laser-modulated pulsed X-ray source (LMPXS) were analyzed to evaluate its pulse emission performance. Results show that the LMPXS can provide a maximum modulation rate up to 100 Mbps which is expected to significantly improve the data rate of XCOM.

  16. Characterizing X-Ray and Radio Emission in the Black Hole X-Ray Binary V404 Cygni During Quiescence

    Science.gov (United States)

    Rana, Vikram; Loh, Alan; Corbel, Stephane; Tomsick, John A.; Chakrabarty, Deepto; Walton, Dominic J.; Barret, Didier; Boggs, Steven E.; Christensen, Finn E.; Craig, William; hide

    2016-01-01

    We present results from multi-wavelength simultaneous X-ray and radio observations of the black hole X-ray binary V404 Cyg in quiescence. Our coverage with NuSTAR provides the very first opportunity to study the X-ray spectrum of V404 Cyg at energies above 10 keV. The unabsorbed broadband (0.3-30 keV) quiescent luminosity of the source is 8.9 x 10(exp 32) erg per sec for a distance of 2.4 kpc. The source shows clear variability on short timescales (an hour to a couple of hours) in the radio, soft X-ray, and hard X-ray bands in the form of multiple flares. The broadband X-ray spectra obtained from XMM-Newton and NuSTAR can be characterized with a power-law model having a photon index of gamma = 2.12 +/- 0.07 (90% confidence errors); however, residuals at high energies indicate spectral curvature significant at a 3 sigma confidence level with the e-folding energy of the cutoff as 20(sub -7)(sup +20) keV. Such curvature can be explained using synchrotron emission from the base of a jet outflow. Radio observations using the VLA reveal that the spectral index evolves on very fast timescales (as short as 10 minutes), switching between optically thick and thin synchrotron emission, possibly due to instabilities in the compact jet or stochastic instabilities in the accretion rate. We explore different scenarios to explain this very fast variability.

  17. X-ray emission as a diagnostic from pseudospark-sourced electron beams

    Energy Technology Data Exchange (ETDEWEB)

    Bowes, D., E-mail: david.bowes@strath.ac.uk [Department of Physics, SUPA, University of Strathclyde, Glasgow G4 0NG (United Kingdom); Yin, H.; He, W.; Zhang, L.; Cross, A.W.; Ronald, K.; Phelps, A.D.R. [Department of Physics, SUPA, University of Strathclyde, Glasgow G4 0NG (United Kingdom); Chen, D.; Zhang, P. [Computed Tomography Lab, School of Mathematical Sciences, Capital Normal University, Beijing 100048 (China); Chen, X.; Li, D. [Department of Electronic Engineering, Queen Mary University of London, London E1 4NS (United Kingdom)

    2014-09-15

    X-ray emission has been achieved using an electron beam generated by a pseudospark low-pressure discharge and utilised as a diagnostic for beam detection. A 300 A, 34 kV PS-sourced electron beam pulse of 3 mm diameter impacting on a 0.1 mm-thick molybdenum target generated X-rays which were detected via the use of a small, portable X-ray detector. Clear X-ray images of a micro-sized object were captured using an X-ray photodetector. This demonstrates the inducement of proton induced X-ray emission (PIXE) not only as an indicator of beam presence but also as a future X-ray source for small-spot X-ray imaging of materials.

  18. Neutron and X-ray emission studies in a low energy plasma focus

    Energy Technology Data Exchange (ETDEWEB)

    Zakaullah, M. [Quaid-i-Azam Univ., Islamabad (Pakistan). Dept. of Physics; Murtaza, G. [Quaid-i-Azam Univ., Islamabad (Pakistan). Dept. of Physics; Qamar, S. [Quaid-i-Azam Univ., Islamabad (Pakistan). Dept. of Physics; Ahmad, I. [Quaid-i-Azam Univ., Islamabad (Pakistan). Dept. of Physics; Beg, M.M. [Quaid-i-Azam Univ., Islamabad (Pakistan). Dept. of Physics

    1996-03-01

    In a low energy Mather-type plasma focus energized by a single 32 {mu}F capacitor, the X-ray and neutron emission is investigated using time-integrated and time-resolved detectors. The X-ray emission profile has a width (FWHM) of 40-50 ns. The neutron emission profile is broader compared to the X-ray emission profile and also delayed by 30-40 ns. To identify different regimes of X-ray emission, an X-ray pin-hole camera along with different absorption filters is employed. While the X-ray emission is high within a narrow pressure range of 2.0-2.5 mbar, the neutron emission is intense for a wider range of 1.0-4.5 mbar. The intense X-ray emission seems to originate from the axially moving shock wave. These results also indicate rather different production mechanisms for X-ray and neutron emission. Also on comparing the X-ray images with Al(2 {mu}m), Al(5 {mu}m), Al(9 {mu}m) filters, we find that the bulk of X-rays from the focus filament have energies less than 2 keV. (orig.).

  19. NuSTAR Hard X-ray Survey of the Galactic Center Region. I. Hard X-ray Morphology and Spectroscopy of the Diffuse Emission

    DEFF Research Database (Denmark)

    Mori, Kaya; Hailey, Charles J.; Krivonos, Roman

    2015-01-01

    We present the first sub-arcminute images of the Galactic Center above 10 keV, obtained with NuSTAR. NuSTAR resolves the hard X-ray source IGR J17456-2901 into non-thermal X-ray filaments, molecular clouds, point sources, and a previously unknown central component of hard X-ray emission (CHXE). Nu...

  20. Soft X-ray emission studies of biomaterials

    Energy Technology Data Exchange (ETDEWEB)

    Kurmaev, E.Z. E-mail: kurmaev@ifmlrs.uran.ru; Werner, J.P.; Moewes, A.; Chiuzbaian, S.; Bach, M.; Ching, W.-Y.; Motozaki, W.; Otsuka, T.; Matsuya, S.; Endo, K.; Neumann, M

    2004-07-01

    Soft X-ray fluorescence measurements are used to characterize three groups of biomaterials: Vitamin B{sub 12} and derivatives, antioxidants (aspirin and paracetamol), and human teeth. We show that the chemical bonding in Vitamin B{sub 12} is characterized by the strong Co-C bond and the relatively weak Co-N bond. The Co-C bond in cyanocobalamin is found to be stronger than that of methylcobalamin leading to their different biological activity. The chemical bonding of paracetamol and aspirin is characterized by the formation of oxygen lone-pair {pi}-orbitals, which can neutralize free radicals and therefore be related to antioxidant activity of these compounds. Carbon K{alpha} emission spectra of a caries lesion suggest that the CaCO{sub 3} like phase exists in sound enamel and that a selective loss of carbonate occurs during the early stages of a caries attack.

  1. Soft X-ray emission studies of biomaterials

    International Nuclear Information System (INIS)

    Kurmaev, E.Z.; Werner, J.P.; Moewes, A.; Chiuzbaian, S.; Bach, M.; Ching, W.-Y.; Motozaki, W.; Otsuka, T.; Matsuya, S.; Endo, K.; Neumann, M.

    2004-01-01

    Soft X-ray fluorescence measurements are used to characterize three groups of biomaterials: Vitamin B 12 and derivatives, antioxidants (aspirin and paracetamol), and human teeth. We show that the chemical bonding in Vitamin B 12 is characterized by the strong Co-C bond and the relatively weak Co-N bond. The Co-C bond in cyanocobalamin is found to be stronger than that of methylcobalamin leading to their different biological activity. The chemical bonding of paracetamol and aspirin is characterized by the formation of oxygen lone-pair π-orbitals, which can neutralize free radicals and therefore be related to antioxidant activity of these compounds. Carbon Kα emission spectra of a caries lesion suggest that the CaCO 3 like phase exists in sound enamel and that a selective loss of carbonate occurs during the early stages of a caries attack

  2. X-ray emission in heavy ion collisions. Final report

    International Nuclear Information System (INIS)

    Watson, R.L.

    1984-01-01

    A detailed accounting of the yearly activities of the research program entitled X-ray Emission in Heavy Ion Collisions may be found in the annual progress reports submitted in accordance with the terms of the contract. The principal goals of the program to be summarized herein were (a) to delineate the mechanisms whereby highly ionized atoms in the condensed phase deexcite and return to charge neutrality, (b) to investigate the charge quenching processes acting to reduce the charge states of highly ionized projectiles, and (c) to attain a better understanding of the interactions occurring between highly charged ions and solid surfaces. These projects all relate to problems associated with the ultimate application of controlled thermonuclear reactions as a practical energy source

  3. Limestone rocks analysis by X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Izquierdo M, G.; Ponce R, R.; Vazquez J, J.

    1996-01-01

    By request of a private company, employing basically X-ray fluorescence analysis (X RF), was established a fast and accurate method for the analysis of the major elements in limestone rocks. Additionally, for complementing analysis was determined by ion chromatography, the chlorides appearance and by atomic absorption of sodium. By gravimetry, was determined the losses by ignition and the alpha quartz. (Author)

  4. Discovery of Hard Nonthermal Pulsed X-Ray Emission from the Anomalous X-Ray Pulsar 1E 1841-045

    NARCIS (Netherlands)

    Kuiper, L.; Hermsen, W.; Méndez, R.M.

    2004-01-01

    We report the discovery of nonthermal pulsed X-ray/soft gamma-ray emission up to ~150 keV from the anomalous 11.8 s X-ray pulsar AXP 1E 1841-045 located near the center of supernova remnant Kes 73 using Rossi X-Ray Timing Explorer (RXTE) Proportional Counter Array and High Energy X-Ray Timing

  5. X-ray absorption and emission studies of diamond nanoparticles

    International Nuclear Information System (INIS)

    Van Buuren, T.; Willey, T.; Raty, J.Y.; Galli, G.; Terminello, L.J.; Bostedt, C.

    2004-01-01

    Full text: A new family of carbon nanopaticles produced in detonations, are found to have a core of diamond with a coating fullerene- like carbon. X-ray diffraction and TEM show that the nanodiamond powder is crystalline and approximately 4 nm in diameter. These nano-sized diamonds do not display the characteristic property of other group IV nanoparticles: a strong widening of the energy gap between the conduction and valence bands owing to quantum-confinement effects. For nano-sized diamond with a size distribution of 4 nm, there is no shift of the band energies relative to bulk diamond. Although the C1s core exciton feature clearly observed in the K-edge absorption edge of bulk diamond is shifted and broadening due to increased overlap of the excited electron with the core holein the small particle. Also the depth of the second gap in the nanodiamond spectra is shallower than that of bulk diamond. A feature at lower energy in the X-ray absorption spectra that is not present in the bulk samples is consistent with a fullerene like surface reconstruction. By exposing the diamond nanoparticles to an Argon /Oxygen plasma then annealing in a UHV environment we have obtained a hydrogen free surface. The nanodiamonds processed in this manner show an increase fullerene type contribution in the carbon x-ray absorption pre-edge. High spatial resolution EELS measurements of the empty states of a single nanodiamond particle acquired with a ld emission TEM also show the core of the particle is bulk diamond like where as the surface has a fullerene like structure. Standard density-functional calculations on clusters in which the diamond surface bonds are terminated with hydrogen atoms, show that the bandgap begins to increase above the bulk value only for clusters smaller than 1 nm. Surface hydrogen atoms are found to be about as close as they do in molecular hydrogen and can escape as H 2 , forcing the respective carbon atoms to rearrange. A series of such rearrangements can

  6. Plasma Emission Profile Recreation using Soft X-Ray Tomography

    Science.gov (United States)

    Page, J. W.; Mauel, M. E.; Levesque, J. P.

    2015-11-01

    With sufficient views from multiple diode arrays, soft X-ray tomography is an invaluable plasma diagnostic because it is a non-perturbing method to reconstruct the emission within the interior of the plasma. In preparation for the installation of new SXR arrays in HBT-EP, we compute high-resolution tomographic reconstructions of discharges having kink-like structures that rotate nearly rigidly. By assuming a uniform angular mapping from the kink mode rotation, Δϕ ~ ωΔ t, a temporal sequence from a single 16-diode fan array represents as many as 16 x 100 independent views. We follow the procedure described by Wang and Granetz and use Bessel basis functions to take the inverse Radon transform. This transform is fit to our data using a least-squares method to estimate the internal SXR emissivity as a sum of polar functions. By varying different parameters of the transformation, we optimize the quality of our recreation of the emission profile and quantify how the reconstruction changes with the azimuthal order of the transform. Supported by U.S. DOE Grant DE-FG02-86ER53222.

  7. Tissue chemical analysis with muonic X-rays

    International Nuclear Information System (INIS)

    Hutson, R.L.; Reidy, J.J.; Springer, K.; Daniel, H.; Knowles, H.B.

    1976-01-01

    The stopped muon channel at the Clinton P. Anderson Meson Physics Facility (LAMPF) was used as a source of muons for studying the elemental composition of tissue with muonic X rays. The X ray spectra from several types of tissue were used to determine the amounts of carbon, nitrogen, and oxygen present. These determinations agree with the results of more conventional chemical analysis. The results show that muonic X rays offer a non-invasive technique for determining the amounts of the more abundant elements present in selected regions of the body. (orig.) [de

  8. Working gas effects on the X-ray emission of a plasma focus device

    Energy Technology Data Exchange (ETDEWEB)

    Cengher, M; Presura, R; Zoita, V [Inst. of Physics and Technology of Radiation Devices, Bucharest (Romania)

    1997-12-31

    Experiments on the plasma focus device IPF-2/20 operating with argon, neon and mixtures of argon with deuterium were performed and some X-ray emission parameters measured. The time evolution of the X-ray emission and dependence of the X-ray yield on the working gas composition was analyzed. The softer X radiation was measured with time resolution in the energy bands from 4 to 40 keV, and the hard X-rays for energies above 200 keV. In deuterium-argon mixtures the soft X-ray yield increases both with pressure (for the same ratio of argon) and with the quantity of argon added to deuterium at the same total pressure. For argon or neon the hard X-ray yield is lower than for deuterium-heavy gas mixtures. The softer X-ray yield decreases with pressure both for neon and for argon. (author). 4 figs., 5 refs.

  9. 0.5 to 6 MeV Ar ion induced X-ray emission in view to analytical application

    International Nuclear Information System (INIS)

    Tenorio Castilleros, M.D.

    1979-01-01

    A study of the X-ray emission induced by 0.5 to 6 MeV Ar ions has been realized in view of multielemental analytical applications. The historical development of the use of heavy ion induced X-ray emission in analysis and the theoretical background of inner-shell ionization in heavy ion-atom collisions are described. The emission of non characteristic X-rays and the effects related to the penetration of heavy ions in matter are also related. The experimental part contains a description of the experimental devices and of the X-ray spectra fitting method. Thick target yields as a function of the target Z and the Ar ion energy are reported. The analytical possibilities are examined and an application to the analysis of Si and Cl in cadmium telluride crystals is given [fr

  10. X-ray structure analysis of soil compositions

    International Nuclear Information System (INIS)

    Tillaev, T.; Kalonov, M.; Kuziev, Sh.; Khatamov, Sh.; Suvanov, M.

    1998-01-01

    The analytic characteristics of techniques developed to analyse soil structure by means of X-ray diffraction method are presented. Presence of 8 minerals in Fergana valley soils have been established. It is shown that X-ray structure analysis of soils gives rise to new original possibilities to determine not only their structure but also quantative content and type of chemical compound of element in soil. (author)

  11. X-ray fluorescent elemental analysis. Ch. 16

    International Nuclear Information System (INIS)

    Baryshev, V.; Kulipanov, G.; Skrinsky, A.

    1991-01-01

    X-ray fluorescence analysis (XFA) is used worldwide to define a quantitative content of the elements as well as to visualize the distribution of elements in different regions (element mapping). Utilization of synchrotron radiation (SR) to excite X-ray fluorescence enables the XFA method to be qualitatively improved. This chapter reviews the experimental work in especially the last decade (author). 71 refs.; 24 figs.; 3 tabs

  12. X-ray absorption and X-ray emission spectroscopy theory and applications

    CERN Document Server

    Lamberti, Carlo

    2016-01-01

    During the last two decades, remarkable and often spectacular progress has been made in the methodological and instrumental aspects of x–ray absorption and emission spectroscopy. This progress includes considerable technological improvements in the design and production of detectors especially with the development and expansion of large-scale synchrotron reactors All this has resulted in improved analytical performance and new applications, as well as in the perspective of a dramatic enhancement in the potential of x–ray based analysis techniques for the near future. This comprehensive two-volume treatise features articles that explain the phenomena and describe examples of X–ray absorption and emission applications in several fields, including chemistry, biochemistry, catalysis, amorphous and liquid systems, synchrotron radiation, and surface phenomena. Contributors explain the underlying theory, how to set up X–ray absorption experiments, and how to analyze the details of the resulting spectra. X-R...

  13. SphinX MEASUREMENTS OF THE 2009 SOLAR MINIMUM X-RAY EMISSION

    OpenAIRE

    Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Kuzin, S.; Farnik, F.; Reale, F.; Phillips, K. J. H.; Bakala, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B.

    2012-01-01

    The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 x 10^47 cm^-3 and 1.1 x 10^48 cm^-3. Comparing Sph...

  14. X-ray emission from National Ignition Facility indirect drive targets

    International Nuclear Information System (INIS)

    Anderson, A.T.; Managan, R.A.; Tobin, M.T.; Peterson, P.F.

    1996-01-01

    We have performed a series of 1-D numerical simulations of the x-ray emission from National Ignition Facility (NIF) targets. Results are presented in terms of total x-ray energy, pulse length, and spectrum. Scaling of x-ray emissions is presented for variations in both target yield and hohlraum thickness. Experiments conducted on the Nova facility provide some validation of the computational tools and methods

  15. Analysis of magnetohydrodynamic modes in tokamaks by x-ray techniques

    International Nuclear Information System (INIS)

    Sauthoff, N.R.

    1977-01-01

    A brief review of recent studies of fluctuations in x-ray emission from tokamak plasmas of controlled thermonuclear fusion interest is given. The origin of the x-rays, the nature of the oscillations, and measurement and analysis techniques are discussed, with emphasis on the work performed on the ST and PLT tokamaks. Areas for future research, particularly in the region of reconstruction, are stressed

  16. Theoretical concepts of X-ray nanoscale analysis theory and applications

    CERN Document Server

    Benediktovitch, Andrei; Ulyanenkov, Alexander

    2013-01-01

    This book provides a concise survey of modern theoretical concepts of X-ray materials analysis. The principle features of the book are: basics of X-ray scattering, interaction between X-rays and matter and new theoretical concepts of X-ray scattering. The various X-ray techniques are considered in detail: high-resolution X-ray diffraction, X-ray reflectivity, grazing-incidence small-angle X-ray scattering and X-ray residual stress analysis. All the theoretical methods presented use the unified physical approach. This makes the book especially useful for readers learning and performing data ana

  17. Simultaneous analysis of Grazing Incidence X-Ray reflectivity and X-ray standing waves from periodic multilayer systems

    NARCIS (Netherlands)

    Yakunin, S.N.; Makhotkin, Igor Alexandrovich; Chuyev, M.A.; Seregin, A.Y.; Pashayev, E.M.; Louis, Eric; van de Kruijs, Robbert Wilhelmus Elisabeth; Bijkerk, Frederik; Kovalchuk, M.V.

    2012-01-01

    Structural analysis of periodic multilayers with small period thickness (~4 nm) is a challenging task, especially when thicknesses of intermixed interfaces become comparable to individual layer thicknesses. In general, angular dependent X-ray fluorescence measurements, excited by the X-ray standing

  18. Einstein Observatory survey of X-ray emission from solar-type stars - the late F and G dwarf stars

    Energy Technology Data Exchange (ETDEWEB)

    Maggio, A.; Sciortino, S.; Vaiana, G.S.; Majer, P.; Bookbinder, J.

    1987-04-01

    Results of a volume-limited X-ray survey of stars of luminosity classes IV and V in the spectral range F7-G9 observed with the Einstein Observatory are presented. Using survival analysis techniques, the stellar X-ray luminosity function in the 0.15-4.0 keV energy band for both single and multiple sources. It is shown that the difference in X-ray luminosity between these two classes of sources is consistent with the superposition of individual components in multiple-component systems, whose X-ray properties are similar to those of the single-component sources. The X-ray emission of the stars in our sample is well correlated with their chromospheric CA II H-K line emission and with their projected equatorial rotational velocity. Comparison of the X-ray luminosity function constructed for the sample of the dG stars of the local population with the corresponding functions derived elsewhere for the Hyades, the Pleiades, and the Orion Ic open cluster confirms that the level of X-ray emission decreases with stellar age. 62 references.

  19. Einstein Observatory survey of X-ray emission from solar-type stars - The late F and G dwarf stars

    Science.gov (United States)

    Maggio, A.; Sciortino, S.; Vaiana, G. S.; Majer, P.; Bookbinder, J.

    1987-01-01

    Results of a volume-limited X-ray survey of stars of luminosity classes IV and V in the spectral range F7-G9 observed with the Einstein Observatory are presented. Using survival analysis techniques, the stellar X-ray luminosity function in the 0.15-4.0 keV energy band for both single and multiple sources. It is shown that the difference in X-ray luminosity between these two classes of sources is consistent with the superposition of individual components in multiple-component systems, whose X-ray properties are similar to those of the single-component sources. The X-ray emission of the stars in our sample is well correlated with their chromospheric CA II H-K line emission and with their projected equatorial rotational velocity. Comparison of the X-ray luminosity function constructed for the sample of the dG stars of the local population with the corresponding functions derived elsewhere for the Hyades, the Pleiades, and the Orion Ic open cluster confirms that the level of X-ray emission decreases with stellar age.

  20. Luminosity dependence in the ratio of X-ray to infrared emission of QSOs

    International Nuclear Information System (INIS)

    Worrall, D.M.

    1987-01-01

    The correlation of X-ray and near-infrared luminosity is studied for a sample of radio-quiet QSOs. The X-ray to infrared ratio is found to decrease as the infrared luminosity increases. No preference is found between the correlations of X-ray luminosity with optical or infrared luminosity. This implies that optical and infrared emission are equally good predictors of X-ray emission. Source models which directly link infrared and X-ray emission are discussed, and a preference is found for a specific synchrotron self-Compton model. This model predicts the correct luminosity dependence of the X-ray to infrared ratio if certain conditions apply. 55 references

  1. Study of X-ray emission in aluminium z-pinches

    International Nuclear Information System (INIS)

    Rosch, R.

    1999-01-01

    Previous experiments, at 0.1. TX level, have shown that stability and x-ray emission of fast Z-pinches, could be strongly increased by imploding an aluminium vapor jet onto a very thin coaxial wire. We present here first results of an aluminium Z-pinch, using a similar liner, but at mega-ampere level. The pinch is driven by AMBIORIX high-power facility, a 2 TW, 0.5 Ω, 2 MA, 50 ns pulse-line generator. We study the effect of an aluminium wire and its diameter (20-50 μm) on the implosion dynamics, on x-ray yield on MHD stability of the column at stagnation. Analysis of A1 jet on A1 wire shots demonstrates that x-ray yield due to emission processes in the H- and He- like ionization stages (i.e. the K-shell) is significantly enhanced, relative to that of A1 jet only ones. The wire also leads to better symmetry of the implosion, and to better reproducibility of shots. X-ray signals exhibit two similar pulses, 10 ns in width, 15 ns spaced. To discern spectral origin of both pulses, experiments are realized with stainless steel wire (25 μm in diameter). Results show that liner and wire radial simultaneously and contribute to both pulses. Analysis of a typical A1 jet on A1 wire shot, using detailed collisional-radiative equilibrium (CRE) model is also given in this thesis. View o the pinch at stagnation as a cola-dense core surrounded by a hot-low density corona reproduces all features of the X-ray data. (author)

  2. Charge Exchange of Ne^9+ for X-ray Emission

    Science.gov (United States)

    Lyons, David

    2016-01-01

    Using the molecular-orbital close-coupling (MOCC) method, single electron capture (SEC) cross sections were computed for Ne^9+ colliding with H.Potential energies and nonadiabatic couplings were calculated and used to obtain the MOCC cross sections which are final-quantum-state-resolved including a separation of singlet and triplet states. Atomic-orbital close-coupling, classical trajectory Monte Carlo, and multichannel Landau-Zener (MCLZ) calculations are also performed. Cross sections for more complicated targets including He, H2, N2, H2O, CO, and CO2, were obtained with the MCLZ method. The SEC results are compared with experimental and other theoretical data, where available. The SEC cross sections are being used in cascade models to predict X-ray emission spectra relevant to solar systemand astrophysical environments.D. Lyons, R. S. Cumbee, P. D. Mullen, P. C. Stancil (UGA), D. R. Schultz (UNT), P. Liebermann (Wuppertal Univ.),R. Buenker (NCSU).This work was partially supported by NASA grant NNX09AC46G.

  3. Soft x-ray emission studies of several aluminum alloys

    International Nuclear Information System (INIS)

    Tsang, K.L.; Zhang, C.H.; Callcott, T.A.; Arakawa, E.T.; Ederer, D.L.; Biancaniello, F.; Curelaru, I.

    1986-01-01

    During the first few months of operation of our soft x-ray spectrometer at the NSLS, we have measured the L emission spectrum for three classes of aluminum alloys: dilute aluminum-magnesium alloys to extend the Al-Mg system to the impurity limit; a 50-50 alloy of aluminum-lithium to characterize the band structure of bulk samples of this potential battery electrolite; and the icosahedral and normal Al-Mn alloys to see if the two phases had measurably different density of states which have been predicted. All spectra shown are produced when core holes generated by energetic electrons or photons are filled by radiative transitions from conduction band states. Dipole selection rules govern the transitions. Thus, K spectra provide a measure of the p-symmetic partial density of states (DOS) near the atom. Similarly, L spectra produced by transitions to p-core holes map the s and d symmetric DOS in the vicinity of the atom with the core hole

  4. Soft x-ray emission studies of several aluminum alloys

    Energy Technology Data Exchange (ETDEWEB)

    Tsang, K.L.; Zhang, C.H.; Callcott, T.A.; Arakawa, E.T.; Ederer, D.L.; Biancaniello, F.; Curelaru, I.

    1986-09-23

    During the first few months of operation of our soft x-ray spectrometer at the NSLS, we have measured the L emission spectrum for three classes of aluminum alloys: dilute aluminum-magnesium alloys to extend the Al-Mg system to the impurity limit; a 50-50 alloy of aluminum-lithium to characterize the band structure of bulk samples of this potential battery electrolite; and the icosahedral and normal Al-Mn alloys to see if the two phases had measurably different density of states which have been predicted. All spectra shown are produced when core holes generated by energetic electrons or photons are filled by radiative transitions from conduction band states. Dipole selection rules govern the transitions. Thus, K spectra provide a measure of the p-symmetic partial density of states (DOS) near the atom. Similarly, L spectra produced by transitions to p-core holes map the s and d symmetric DOS in the vicinity of the atom with the core hole.

  5. Soft X-ray Emission from Large-Scale Galactic Outflows in Seyfert Galaxies

    Science.gov (United States)

    Colbert, E. J. M.; Baum, S.; O'Dea, C.; Veilleux, S.

    1998-01-01

    Kiloparsec-scale soft X-ray nebulae extend along the galaxy minor axes in several Seyfert galaxies, including NGC 2992, NGC 4388 and NGC 5506. In these three galaxies, the extended X-ray emission observed in ROSAT HRI images has 0.2-2.4 keV X-ray luminosities of 0.4-3.5 x 10(40) erg s(-1) . The X-ray nebulae are roughly co-spatial with the large-scale radio emission, suggesting that both are produced by large-scale galactic outflows. Assuming pressure balance between the radio and X-ray plasmas, the X-ray filling factor is >~ 10(4) times as large as the radio plasma filling factor, suggesting that large-scale outflows in Seyfert galaxies are predominantly winds of thermal X-ray emitting gas. We favor an interpretation in which large-scale outflows originate as AGN-driven jets that entrain and heat gas on kpc scales as they make their way out of the galaxy. AGN- and starburst-driven winds are also possible explanations if the winds are oriented along the rotation axis of the galaxy disk. Since large-scale outflows are present in at least 50 percent of Seyfert galaxies, the soft X-ray emission from the outflowing gas may, in many cases, explain the ``soft excess" X-ray feature observed below 2 keV in X-ray spectra of many Seyfert 2 galaxies.

  6. Measurements of laser generated soft X-ray emission from irradiated gold foils

    Energy Technology Data Exchange (ETDEWEB)

    Davis, J. S.; Keiter, P. A.; Klein, S. R.; Drake, R. P.; Shvarts, D. [University of Michigan, 2455 Hayward St., Ann Arbor, Michigan 48109 (United States); Frank, Y.; Raicher, E.; Fraenkel, M. [Soreq Nuclear Research Center, Yavne (Israel)

    2016-11-15

    Soft x-ray emission from laser irradiated gold foils was measured at the Omega-60 laser system using the Dante photodiode array. The foils were heated with 2 kJ, 6 ns laser pulses and foil thicknesses were varied between 0.5, 1.0, and 2.0 μm. Initial Dante analysis indicates peak emission temperatures of roughly 100 eV and 80 eV for the 0.5 μm and 1.0 μm thick foils, respectively, with little measurable emission from the 2.0 μm foils.

  7. A ROTSE-I/ROSAT Survey of X-ray Emission from Contact Binary Stars

    Science.gov (United States)

    Geske, M.; McKay, T.

    2005-05-01

    Using public data from the ROSAT All Sky Survey (RASS) and the ROTSE-I Sky Patrols, the incidence of strong x-ray emissions from contact binary systems was examined. The RASS data was matched to an expanded catalog of contact binary systems from the ROTSE-I data, using a 35 arc second radius. X-ray luminosities for matching objects were then determined. This information was then used to evaluate the total x-ray emissions from all such objects, in order to determine their contribution to the galactic x-ray background.

  8. Hard X-Ray Emission from Partially Occulted Solar Flares: RHESSI Observations in Two Solar Cycles

    Energy Technology Data Exchange (ETDEWEB)

    Effenberger, Frederic; Costa, Fatima Rubio da; Petrosian, Vahé [Department of Physics and KIPAC, Stanford University, Stanford, CA 94305 (United States); Oka, Mitsuo; Saint-Hilaire, Pascal; Krucker, Säm [Space Sciences Laboratory, University of California, Berkeley, CA 94720-7450 (United States); Liu, Wei [Bay Area Environmental Research Institute, 625 2nd Street, Suite 209, Petaluma, CA 94952 (United States); Glesener, Lindsay, E-mail: feffen@stanford.edu, E-mail: frubio@stanford.edu [School of Physics and Astronomy, University of Minnesota, Minneapolis, MN 55455 (United States)

    2017-02-01

    Flares close to the solar limb, where the footpoints are occulted, can reveal the spectrum and structure of the coronal looptop source in X-rays. We aim at studying the properties of the corresponding energetic electrons near their acceleration site, without footpoint contamination. To this end, a statistical study of partially occulted flares observed with Reuven Ramaty High-Energy Solar Spectroscopic Imager is presented here, covering a large part of solar cycles 23 and 24. We perform detailed spectra, imaging, and light curve analyses for 116 flares and include contextual observations from SDO and STEREO when available, providing further insights into flare emission that were previously not accessible. We find that most spectra are fitted well with a thermal component plus a broken power-law, non-thermal component. A thin-target kappa distribution model gives satisfactory fits after the addition of a thermal component. X-ray imaging reveals small spatial separation between the thermal and non-thermal components, except for a few flares with a richer coronal source structure. A comprehensive light curve analysis shows a very good correlation between the derivative of the soft X-ray flux (from GOES ) and the hard X-rays for a substantial number of flares, indicative of the Neupert effect. The results confirm that non-thermal particles are accelerated in the corona and estimated timescales support the validity of a thin-target scenario with similar magnitudes of thermal and non-thermal energy fluxes.

  9. Extracting chemical information from high-resolution Kβ X-ray emission spectroscopy

    Science.gov (United States)

    Limandri, S.; Robledo, J.; Tirao, G.

    2018-06-01

    High-resolution X-ray emission spectroscopy allows studying the chemical environment of a wide variety of materials. Chemical information can be obtained by fitting the X-ray spectra and observing the behavior of some spectral features. Spectral changes can also be quantified by means of statistical parameters calculated by considering the spectrum as a probability distribution. Another possibility is to perform statistical multivariate analysis, such as principal component analysis. In this work the performance of these procedures for extracting chemical information in X-ray emission spectroscopy spectra for mixtures of Mn2+ and Mn4+ oxides are studied. A detail analysis of the parameters obtained, as well as the associated uncertainties is shown. The methodologies are also applied for Mn oxidation state characterization of double perovskite oxides Ba1+xLa1-xMnSbO6 (with 0 ≤ x ≤ 0.7). The results show that statistical parameters and multivariate analysis are the most suitable for the analysis of this kind of spectra.

  10. Spin-polarized x-ray emission of 3d transition-metal ions : A comparison via K alpha and K beta detection

    NARCIS (Netherlands)

    Wang, Xin; deGroot, F.M.F.; Cramer, SP

    1997-01-01

    This paper demonstrates that spin-polarized x-ray-excitation spectra can be obtained using K alpha emission as well as K beta lines. A spin-polarized analysis of K alpha x-ray emission and the excitation spectra by K alpha detection on a Ni compound is reported. A systematic analysis of the

  11. X-RAY EMISSION FROM MAGNETIC MASSIVE STARS

    International Nuclear Information System (INIS)

    Nazé, Yaël; Petit, Véronique; Rinbrand, Melanie; Owocki, Stan; Cohen, David; Ud-Doula, Asif; Wade, Gregg A.

    2014-01-01

    Magnetically confined winds of early-type stars are expected to be sources of bright and hard X-rays. To clarify the systematics of the observed X-ray properties, we have analyzed a large series of Chandra and XMM-Newton observations, corresponding to all available exposures of known massive magnetic stars (over 100 exposures covering ∼60% of stars compiled in the catalog of Petit et al.). We show that the X-ray luminosity is strongly correlated with the stellar wind mass-loss rate, with a power-law form that is slightly steeper than linear for the majority of the less luminous, lower- M-dot B stars and flattens for the more luminous, higher- M-dot O stars. As the winds are radiatively driven, these scalings can be equivalently written as relations with the bolometric luminosity. The observed X-ray luminosities, and their trend with mass-loss rates, are well reproduced by new MHD models, although a few overluminous stars (mostly rapidly rotating objects) exist. No relation is found between other X-ray properties (plasma temperature, absorption) and stellar or magnetic parameters, contrary to expectations (e.g., higher temperature for stronger mass-loss rate). This suggests that the main driver for the plasma properties is different from the main determinant of the X-ray luminosity. Finally, variations of the X-ray hardnesses and luminosities, in phase with the stellar rotation period, are detected for some objects and they suggest that some temperature stratification exists in massive stars' magnetospheres

  12. Image Analysis for X-ray Imaging of Food

    DEFF Research Database (Denmark)

    Einarsdottir, Hildur

    for quality and safety evaluation of food products. In this effort the fields of statistics, image analysis and statistical learning are combined, to provide analytical tools for determining the aforementioned food traits. The work demonstrated includes a quantitative analysis of heat induced changes......X-ray imaging systems are increasingly used for quality and safety evaluation both within food science and production. They offer non-invasive and nondestructive penetration capabilities to image the inside of food. This thesis presents applications of a novel grating-based X-ray imaging technique...... and defect detection in food. Compared to the complex three dimensional analysis of microstructure, here two dimensional images are considered, making the method applicable for an industrial setting. The advantages obtained by grating-based imaging are compared to conventional X-ray imaging, for both foreign...

  13. X-ray emission from stainless steel foils irradiated by femtosecond petawatt laser pulses

    Science.gov (United States)

    Alkhimova, M. A.; Faenov, A. Ya; Pikuz, T. A.; Skobelev, I. Yu; Pikuz, S. A.; Nishiuchi, M.; Sakaki, H.; Pirozhkov, A. S.; Sagisaka, S.; Dover, N. P.; Kondo, Ko; Ogura, K.; Fukuda, Y.; Kiriyama, H.; Esirkepov, T.; Bulanov, S. V.; Andreev, A.; Kando, M.; Zhidkov, A.; Nishitani, K.; Miyahara, T.; Watanabe, Y.; Kodama, R.; Kondo, K.

    2018-01-01

    We report about nonlinear growth of x-ray emission intensity emitted from plasma generated by femtosecond petawatt laser pulses irradiating stainless steel foils. X-ray emission intensity increases as ˜ I 4.5 with laser intensity I on a target. High spectrally resolved x-ray emission from front and rear surfaces of 5 μm thickness stainless steel targets were obtained at the wavelength range 1.7-2.1 Å, for the first time in experiments at femtosecond petawatt laser facility J-KAREN-P. Total intensity of front x-ray spectra three times dominates to rear side spectra for maximum laser intensity I ≈ 3.2×1021 W/cm2. Growth of x-ray emission is mostly determined by contribution of bremsstrahlung radiation that allowed estimating bulk electron plasma temperature for various magnitude of laser intensity on target.

  14. Highly ionized copper contribution to the soft X-ray emission in a plasma focus device

    Energy Technology Data Exchange (ETDEWEB)

    Zoita, V; Patran, A [Inst. of Physics and Technology of Radiation Devices, Bucharest (Romania); Larour, J [Ecole Polytechnique, Palaiseau (France). Lab. de Physique des Milieux Ionises

    1997-12-31

    In order to discriminate between the contributions of the gas plasma and of the anode (solid or plasma) to the soft X-ray emission in a plasma focus device, a series of experiments was carried out using the following combinations of experimental conditions: various gases, different absorption filters and viewing different regions in front of the centre electrode. The experiments were performed on the IPF-2/20 plasma focus device using the following working gases: helium, neon and helium-argon mixtures. The diagnostics used: magnetic probe for current derivative, PIN diode for the minimum pinch radius detection, PIN diodes for the soft X-ray emission, scintillator-photomultiplier detector for the hard X-ray emission. From the analysis of the various diagnostics data recorded with very good time correlation, it followed that the soft K-ray signals had a strong contribution from optical transitions of the highly ionised Cu (Cu XX to XXII) emitting in the range 0.8-1.3 nm. (author). 7 figs., 9 refs.

  15. A low power x-ray tube for use in energy dispersive x-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Kataria, S.K.; Govil, Rekha; Lal, M.

    1980-01-01

    A low power X-ray tube with thin molybdenum transmission target for use in energy dispersive X-ray fluorescence (ENDXRF) element analysis has been indigenously built, along with its power supply. The X-ray tube has been in operation since August 1979, and it has been operated upto maximum target voltage of 35 KV and tube current upto 200 μA which is more than sufficient for trace element analysis. This X-ray tube has been used alongwith the indigenously built Si(Li) detector X-ray spectrometer with an energy resolution of 200 eV at 5.9 Kev MnKsub(α) X-ray peak for ENDXRF analysis. A simple procedure of calibration has been developed for thin samples based on the cellulose diluted, thin multielement standard pellets. Analytical sensitivities of the order of a few p.p.m. have been obtained with the experimental setup for elements with 20 < = Z < = 38 and 60 < = Z < = 90. A number of X-ray spectra for samples of environmental, biological, agricultural, industrial and metallurgical interest are presented to demonstrate the salient features of the experimental sep up. (auth.)

  16. Application of X-ray fluorescence analysis in environmental research

    International Nuclear Information System (INIS)

    Kliment, V.; Kliman, J.; Turzo, I.

    1978-01-01

    A description is presented of the X-ray fluorescence analysis principles and of its possibilities in the study of environmental pollution impact. Experiments with X-ray fluorescence analysis using 241-Am and a Ge(Li) semiconductor detector are discussed. The reproducibility of determinations in dependence on the sample preparation and the evaluation of peak surfaces of characteristic radiation is shown. The dependence of the peak surface on the elemental contents in the sample was linear. Detection limits of the investigated elements ranged in tenths of μg for 300 s measurement. (author)

  17. Energy dispersive X-ray analysis in the electron microscope

    CERN Document Server

    Bell, DC

    2003-01-01

    This book provides an in-depth description of x-ray microanalysis in the electron microscope. It is sufficiently detailed to ensure that novices will understand the nuances of high-quality EDX analysis. Includes information about hardware design as well as the physics of x-ray generation, absorption and detection, and most post-detection data processing. Details on electron optics and electron probe formation allow the novice to make sensible adjustments to the electron microscope in order to set up a system which optimises analysis. It also helps the reader determine which microanalytical me

  18. Theoretical estimation of proton induced X-ray emission yield of the trace elements present in the lung and breast cancer

    International Nuclear Information System (INIS)

    Manjunatha, H.C.; Sowmya, N.

    2013-01-01

    X-rays may be produced following the excitation of target atoms induced by an energetic incident ion beam of protons. Proton induced X-ray emission (PIXE) analysis has been used for many years for the determination of elemental composition of materials using X-rays. Recent interest in the proton induced X-ray emission cross section has arisen due to their importance in the rapidly expanding field of PIXE analysis. One of the steps in the analysis is to fit the measured X-ray spectrum with theoretical spectrum. The theoretical cross section and yields are essential for the evaluation of spectrum. We have theoretically evaluated the PIXE cross sections for trace elements in the lung and breast cancer tissues such as Cl, K, Ca,Ti, Cr, Mn, Fe, Ni, Cu, Zn, As, Se, Br, Rb, P, S, Sr, Hg and Pb. The estimated cross section is used in the evaluation of Proton induced X-ray emission spectrum for the given trace elements.We have also evaluated the Proton induced X-ray emission yields in the thin and thick target of the given trace elements. The evaluated Proton induced X-ray emission cross-section, spectrum and yields are graphically represented. Some of these values are also tabulated. Proton induced X-ray emission cross sections and a yield for the given trace elements varies with the energy. PIXE yield depends on a real density and does not on thickness of the target. (author)

  19. Clustering of germanium atoms in silica glass responsible for the 3.1 eV emission band studied by optical absorption and X-ray absorption fine structure analysis

    International Nuclear Information System (INIS)

    Yoshida, Tomoko; Muto, Shunsuke; Yuliati, Leny; Yoshida, Hisao; Inada, Yasuhiro

    2009-01-01

    Correlation between the 3.1 eV emission band and local atomic configuration was systematically examined for Ge + implanted silica glass by UV-vis optical absorption spectroscopy and X-ray absorption fine structure (XAFS) analysis. The 2.7 eV emission band, commonly observed in defective silica, was replaced by the sharp and intense 3.1 eV emission band for the Ge + fluence > 2 x 10 16 cm -2 , in which UV-vis absorption spectra suggested clustering of Ge atoms with the size ∼1 nm. XAFS spectroscopy indicated that the Ge atoms were under coordinated with oxygen atoms nearly at a neutral valence state on average. The present results are consistent with the previous ESR study but imply that the small Ge clusters rather than the O=Ge: complexes (point defects) are responsible for the 3.1 eV emission band.

  20. The Origin of the Extra-nuclear X-ray Emission in the Seyfert Galaxy NGC 2992

    Science.gov (United States)

    Colbert, E. J. M.; Strickland, D. K.; Veilleux, S.; Weaver, K. A.

    2004-12-01

    We present an analysis of a Chandra ACIS observation of the edge-on Seyfert galaxy NGC 2992. We find extended X-ray emission with Lx(total) in excess of 10**40 erg/s. The brightest nebula is positioned a few 100 pc from the X-ray core, and is spatially coincident with optical line and radio emission. This emission nebula may be energized by the AGN, as opposed to a nuclear starburst. The expected kpc-scale X-ray emission due to a starburst-driven wind is larger than a few 10**39 erg/s, and we present large-scale X-ray emission that may be associated with such an outflow. The extra-nuclear emission has a very soft spectrum. Chandra and XMM spectra of the total nuclear region show a very prominent ``soft excess'' below 2-3 keV. We shall discuss the spectral properties of this soft excess, and will compare with the results from the spatial analysis, and with AGN and starburst models for extranuclear X-ray nebulae.

  1. X-ray Peltier cooled detectors for X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Loupilov, A.; Sokolov, A.; Gostilo, V.

    2001-01-01

    The recent results on development of X-ray Si(Li), Si-planar and CdTe p-i-n detectors cooled by Peltier coolers for fabrication of laboratory and portable XRF analysers for different applications are discussed. Low detection limits of XRF analysers are provided by increasing of detectors sensitive surface; improvement of their spectrometrical characteristics; decreasing of front-end-electronics noise level; Peltier coolers and vacuum chambers cooling modes optimization. Solution of all mentioned tasks allowed to develop Peltier cooled detectors with the following performances: (1.) Si(Li) detectors: S=20 mm 2 , thickness=3.5 mm, 175 eV (5.9 keV), 430 eV (59.6 keV); S=100 mm 2 ; thickness=4.5 mm, 270 eV (5.9 keV), 485 eV (59.6 keV). (2.) Si-planar detector: S=10 mm 2 , thickness=0.4 mm, 230 eV (5.9 keV), 460 eV (59.6 keV). (3.) CdTe p-i-n detectors: S=16 mm 2 , thickness=0.5 mm, 350 eV (5.9 keV), 585 eV (59.6 keV). S=16 mm 2 , thickness=1.2 mm, 310 eV (5.9 keV), 600 eV (59.6 keV). Advantages and disadvantages of all types of detectors for X-ray fluorescence analysis are compared. Spectra are presented. Application of different XRF analysers based on developed detectors in medicine, environmental science, industry, cryminalistics and history of art are demonstrated

  2. X-ray Peltier cooled detectors for X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Loupilov, A.; Sokolov, A.; Gostilo, V.

    2000-01-01

    The recent results on development of X-ray Si(Li), Si-planar and CdTe p-i- n detectors cooled by Peltier coolers for fabrication of laboratory and portable XRF analysers for different applications are discussed. Low detection limits of XRF analysers are provided by increasing of detectors sensitive surface; improvement of their spectrometrical characteristics; decreasing of front-end-electronics noise level; Peltier coolers and vacuum chambers cooling modes optimization. Solution of all mentioned tasks allowed to develop Peltier cooled detectors with the following performances: (1) Si(Li) detectors: S = 20 mm 2 , thickness = 3.5 mm, 175 eV (5.9 keV), 430 eV (59.6 keV); S = 100 mm 2 ; thickness = 4.5 mm, 270 eV (5.9 keV), 485 eV (59,6 keV). (2) Si-planar detector: S = 10 mm 2 , thickness = 0.4 mm, 230 eV (5.9 keV), 460 eV (59.6 keV). (3) CdTe p-i-n detectors: S = 16 mm 2 , thickness 0.5 mm, 350 eV (5.9 keV), 585 eV (59.6 keV). S = 16 mm 2 , thickness = 1.2 mm, 310 eV (5.9 keV), 600 eV (59.6 keV). Advantages and disadvantages of all types of detectors for X-ray fluorescence analysis are compared. Spectra are presented. Application of different XRF analysers based on developed detectors in medicine, environmental science, industry, criminalistics and history of art are demonstrated. (author)

  3. Discovery of Spatial and Spectral Structure in the X-Ray Emission from the Crab Nebula

    Science.gov (United States)

    Weisskopf, Martin C.; Hester, J. Jeff; Tennant, Allyn F.; Elsner, Ronald F.; Schulz, Norbert S.; Marshall, Herman L.; Karovska, Margarita; Nichols, Joy S.; Swartz, Douglas A.; Kolodziejczak, Jeffery J.

    2000-01-01

    The Chandra X-Ray Observatory observed the Crab Nebula and pulsar during orbital calibration. Zeroth-order images with the High-Energy Transmission Grating (HETG) readout by the Advanced Charge Coupled Devices (CCD) Imaging Spectrometer spectroscopy array (ACIS-S) show a striking richness of X-ray structure at a resolution comparable to that of the best ground-based visible-light observations. The HETG-ACIS-S images reveal, for the first time, an X-ray inner ring within the X-ray torus, the suggestion of a hollow-tube structure for the torus, and X-ray knots along the inner ring and (perhaps) along the inward extension of the X-ray jet. Although complicated by instrumental effects and the brightness of the Crab Nebula, the spectrometric analysis shows systematic variations of the X-ray spectrum throughout the nebula.

  4. Discovery of Spatial and Spectral Structure in the X-Ray Emission from the Crab Nebula.

    Science.gov (United States)

    Weisskopf; Hester; Tennant; Elsner; Schulz; Marshall; Karovska; Nichols; Swartz; Kolodziejczak; O'Dell

    2000-06-20

    The Chandra X-Ray Observatory observed the Crab Nebula and pulsar during orbital calibration. Zeroth-order images with the High-Energy Transmission Grating (HETG) readout by the Advanced CCD Imaging Spectrometer spectroscopy array (ACIS-S) show a striking richness of X-ray structure at a resolution comparable to that of the best ground-based visible-light observations. The HETG-ACIS-S images reveal, for the first time, an X-ray inner ring within the X-ray torus, the suggestion of a hollow-tube structure for the torus, and X-ray knots along the inner ring and (perhaps) along the inward extension of the X-ray jet. Although complicated by instrumental effects and the brightness of the Crab Nebula, the spectrometric analysis shows systematic variations of the X-ray spectrum throughout the nebula.

  5. Resonant soft X-ray emission spectroscopy of liquids

    International Nuclear Information System (INIS)

    Guo, J.-H.; Augustsson, A.; Englund, C.-J.; Nordgren, J.

    2004-01-01

    We present now a possible way to carry out soft-x-ray fluorescence spectroscopy of liquids. The liquid cell has a window to attain compatibility with UHV conditions of the spectrometer and beamline. The synchrotron radiation enters the liquid cell through a 100nm-thick silicon nitride window and the emitted x-rays exit through the same window. This allows in particular liquid solid interfaces to be studied. Such a liquid cell has been used to study the electronic structure of a variety of systems ranging from water solutions of inorganic salts and inertial drugs to nano materials and actinide compounds in their wet conditions

  6. X-ray emission from open star clusters with Spectrum-Rontgen-Gamma

    DEFF Research Database (Denmark)

    Singh, K.P.; Ojha, D.K.; Schnopper, H.W.

    1998-01-01

    The study of X-ray emission from co-evolving populations of stars in open dusters is extremely important for understanding the dynamo activity among the stars. With this objective, we propose to observe a number of open clusters in the X-ray and UV bands using SPECTRUM-Rontgen-Gamma. The high...... throughput of SPECTRUM-Rontgen-Gamma will help detect main sequence stars like Sun in middle-aged and old clusters. We will study the relationships between various parameters - age, rotation, abundance, UBV colors, X-ray luminosity, coronal temperature etc. X-ray spectra of younger and brighter populations...

  7. Exploring the Hard and Soft X-ray Emission of Magnetic Cataclysmic Variables

    Science.gov (United States)

    de Martino, D.; Anzolin, G.; Bonnet-Bidaud, J.-M.; Falanga, M.; Matt, G.; Mouchet, M.; Mukai, K.; Masetti, N.

    2009-05-01

    A non-negligible fraction of galactic hard (>20 keV) X-ray sources were identified as CVs of the magnetic Intermediate Polar type in INTEGRAL, SWIFT and RXTE surveys, that suggests a still hidden but potentially important population of faint hard X-ray sources. Simbol-X has the unique potential to simultaneously characterize their variable and complex soft and hard X-ray emission thus allowing to understand their putative role in galactic populations of X-ray sources.

  8. DISCOVERY OF X-RAY EMISSION FROM YOUNG SUNS IN THE SMALL MAGELLANIC CLOUD

    International Nuclear Information System (INIS)

    Oskinova, L. M.; Hainich, R.; Sun, W.; Chen, Y.; Evans, C. J.; Hénault-Brunet, V.; Chu, Y.-H.; Gruendl, R. A.; Gallagher, J. S. III; Guerrero, M. A.; Güdel, M.; Silich, S.; Nazé, Y.; Reyes-Iturbide, J.

    2013-01-01

    We report the discovery of extended X-ray emission within the young star cluster NGC 602a in the Wing of the Small Magellanic Cloud (SMC) based on observations obtained with the Chandra X-Ray Observatory. X-ray emission is detected from the cluster core area with the highest stellar density and from a dusty ridge surrounding the H II region. We use a census of massive stars in the cluster to demonstrate that a cluster wind or wind-blown bubble is unlikely to provide a significant contribution to the X-ray emission detected from the central area of the cluster. We therefore suggest that X-ray emission at the cluster core originates from an ensemble of low- and solar-mass pre-main-sequence (PMS) stars, each of which would be too weak in X-rays to be detected individually. We attribute the X-ray emission from the dusty ridge to the embedded tight cluster of the newborn stars known in this area from infrared studies. Assuming that the levels of X-ray activity in young stars in the low-metallicity environment of NGC 602a are comparable to their Galactic counterparts, then the detected spatial distribution, spectral properties, and level of X-ray emission are largely consistent with those expected from low- and solar-mass PMS stars and young stellar objects (YSOs). This is the first discovery of X-ray emission attributable to PMS stars and YSOs in the SMC, which suggests that the accretion and dynamo processes in young, low-mass objects in the SMC resemble those in the Galaxy.

  9. A PILOT DEEP SURVEY FOR X-RAY EMISSION FROM fuvAGB STARS

    Energy Technology Data Exchange (ETDEWEB)

    Sahai, R. [Jet Propulsion Laboratory, MS 183-900, California Institute of Technology, Pasadena, CA 91109 (United States); Sanz-Forcada, J.; Sánchez Contreras, C. [Astrobiology Center (CSIC-INTA), ESAC campus, E-28691 Villanueva de la Canada, Madrid (Spain); Stute, M. [Institute for Astronomy and Astrophysics, Eberhard Karls Universität Tübingen, Auf der Morgenstelle 10, D-72076, Tübingen (Germany)

    2015-09-01

    We report the results of a pilot survey for X-ray emission from a newly discovered class of AGB stars with far-ultraviolet excesses (fuvAGB stars) using XMM-Newton and Chandra. We detected X-ray emission in three of six fuvAGB stars observed—the X-ray fluxes are found to vary in a stochastic or quasi-periodic manner on roughly hour-long timescales, and simultaneous UV observations using the Optical Monitor on XMM for these sources show similar variations in the UV flux. These data, together with previous studies, show that X-ray emission is found only in fuvAGB stars. From modeling the spectra, we find that the observed X-ray luminosities are ∼(0.002–0.2) L{sub ⊙} and the X-ray-emitting plasma temperatures are ∼(35–160) × 10{sup 6} K. The high X-ray temperatures argue against the emission arising in stellar coronae, or directly in an accretion shock, unless it occurs on a WD companion. However, none of the detected objects is a known WD-symbiotic star, suggesting that if WD companions are present, they are relatively cool (<20,000 K). In addition, the high X-ray luminosities specifically argue against emission originating in the coronae of main-sequence companions. We discuss several models for the X-ray emission and its variability and find that the most likely scenario for the origin of the X-ray (and FUV) emission involves accretion activity around a companion star, with confinement by strong magnetic fields associated with the companion and/or an accretion disk around it.

  10. DISCOVERY OF X-RAY EMISSION FROM THE FIRST Be/BLACK HOLE SYSTEM

    Energy Technology Data Exchange (ETDEWEB)

    Munar-Adrover, P.; Paredes, J. M.; Ribó, M. [Departament d' Astronomia i Meteorologia, Institut de Ciències del Cosmos, Universitat de Barcelona, IEEC-UB, Martí i Franquès 1, E-08028 Barcelona (Spain); Iwasawa, K. [ICREA, Institut de Ciències del Cosmos, Universitat de Barcelona, IEEC-UB, Martí i Franquès 1, E-08028 Barcelona (Spain); Zabalza, V. [Department of Physics and Astronomy, University of Leicester, University Road, Leicester LE1 7RH (United Kingdom); Casares, J. [Instituto de Astrofísica de Canarias, E-38200 La Laguna, Tenerife (Spain)

    2014-05-10

    MWC 656 (=HD 215227) was recently discovered to be the first binary system composed of a Be star and a black hole (BH). We observed it with XMM-Newton, and detected a faint X-ray source compatible with the position of the optical star, thus proving it to be the first Be/BH X-ray binary. The spectrum analysis requires a model fit with two components, a blackbody plus a power law, with k{sub B}T=0.07{sub −0.03}{sup +0.04} keV and a photon index Γ = 1.0 ± 0.8, respectively. The non-thermal component dominates above ≅0.8 keV. The obtained total flux is F(0.3-5.5 keV)=(4.6{sub −1.1}{sup +1.3})×10{sup −14} erg cm{sup –2} s{sup –1}. At a distance of 2.6 ± 0.6 kpc the total flux translates into a luminosity L {sub X} = (3.7 ± 1.7) × 10{sup 31} erg s{sup –1}. Considering the estimated range of BH masses to be 3.8-6.9 M {sub ☉}, this luminosity represents (6.7 ± 4.4) × 10{sup –8} L {sub Edd}, which is typical of stellar-mass BHs in quiescence. We discuss the origin of the two spectral components: the thermal component is associated with the hot wind of the Be star, whereas the power-law component is associated with emission from the vicinity of the BH. We also find that the position of MWC 656 in the radio versus X-ray luminosity diagram may be consistent with the radio/X-ray correlation observed in BH low-mass X-ray binaries. This suggests that this correlation might also be valid for BH high-mass X-ray binaries (HMXBs) with X-ray luminosities down to ∼10{sup –8} L {sub Edd}. MWC 656 will allow the accretion processes and the accretion/ejection coupling at very low luminosities for BH HMXBs to be studied.

  11. Research Note: Energy dispersive x-ray fluorescence analysis ...

    African Journals Online (AJOL)

    Energy Dispersive X-Ray fluorescence (EDXRF) technique for the analysis of geological, biological and environmental samples is described. The technique has been applied in the analysis of 10 (geological, biological, environmental) standard reference materials. The accuracy and precision of the technique were attested ...

  12. X-ray emission from supernova remnants with particular reference to the Cygnus Loop

    International Nuclear Information System (INIS)

    Gronenschild, E.H.B.M.

    1979-01-01

    Observational or theoretical results related to the study of supernova remnants (SNRs) are described. Some background information is given by reviewing the present status of our knowledge of supernovae and supernova remnants, both from theory and observations. Also the distribution of all known radio, optical, and X-ray SNRs in the Galaxy is shown and a comparison is made. The X-ray observations of the well-known X-ray SNR the Cygnus Loop are discussed in detail and the discovery of a new X-ray emitting SNR W44 is described. Other radio sources are investigated, and the observed X-ray emission of SNRs are analysed using thermal spectra like exponential or bremsstrahlung spectra. The X-ray line spectrum that emerges from SNRs is described in detail. (Auth.)

  13. Astrophysical extended X-ray absorption fine-structure analysis

    International Nuclear Information System (INIS)

    Woo, J.W.; Forrey, R.C.; Cho, K.; Department of Physics and Division of Applied Sciences, Harvard University)

    1997-01-01

    We present an astrophysical extended X-ray absorption fine-structure (EXAFS) analysis (AEA) tool. The AEA tool is designed to generate a numerical model of the modification to the X-ray absorption coefficient due to the EXAFS phenomenon. We have constructed a complete database (elements up to the atomic number 92) of EXAFS parameters: central atom phase shift (2δ 1 ), backscattering phase shift (φ b ), and backscattering amplitude (F). Using the EXAFS parameter data base, the AEA tool can generate a numerical model of any compound when the atomic numbers of neighboring atoms and their distances to the central X-ray-absorbing atom are given. copyright 1997 The American Astronomical Society

  14. Spectral properties of X-ray selected narrow emission line galaxies

    Science.gov (United States)

    Romero-Colmenero, E.

    1998-03-01

    This thesis reports a study of the X-ray and optical properties of two samples of X-ray selected Narrow Emission Line Galaxies (NELGs), and their comparison with the properties of broad line Active Galactic Nuclei (AGN). One sample (18 NELGs) is drawn from the ROSAT International X-ray Optical Survey (RIXOS), the other (19 NELGs and 33 AGN) from the ROSAT UK Deep Survey. ROSAT multi-channel X-ray spectra have been extracted and fitted with power-law, bremsstrahlung and black body models for the brighter RIXOS sources. In most cases, power-law and bremsstrahlung models provide the best results. The average spectral energy index, alpha, of the RIXOS NELGs is 0.96 +/- 0.07, similar to that of AGN (alpha~1). For the fainter RIXOS NELGs, as well as for all the UK Deep Survey sources, counts in three spectral bands have been extracted and fitted with a power-law model, assuming the Galactic value for N_H. The brighter RIXOS sources demonstrated that the results obtained by these two different extraction and fitting procedures provide consistent results. Two average X-ray spectra, one for the NELGs and another for the AGN, were created from the UK Deep Survey sources. The power-law slope of the average NELG is alpha = 0.45 +/- 0.09, whilst that of the AGN is alpha = 0.96 +/- 0.03. ROSAT X-ray surveys have shown that the fractional surface density of NELGs increases with respect to AGN at faint fluxes (case for NELGs to be major contributors to the XRB at the fainter fluxes. The analysis of optical spectroscopy, obtained on La Palma and Hawaii, shows that NELGs form a very heterogeneous group, made up of a mixture of Seyfert 2, LINER and HII-region like galaxies. Seyfert 2 galaxies are found to possess in general the steepest X-ray slopes. Ways to explain this in the context of the unified model of AGN are discussed. The FWHM of some emission lines (Halpha, Hbeta, [NII]) in the NELGs appears to increase with steepening X-ray spectral slope. In the case of the Balmer lines

  15. Analysis of X-Ray (L) spectra of heavy elements

    International Nuclear Information System (INIS)

    Souza Coelho, L.F. de.

    1976-08-01

    The general problem of obtaining and analysing spectra is presented, with emphasis in the comparison of methods for the analysis of gamma rays and X rays. The method proposed to obtain a standard and later the intensities of lines of an X-ray (L) spectrum is discussed. The good eesults obtained by the program RAIOXL, when simulated spectra are used, and by the program RAIXL1, when doublets are decomposed, are shown. In annex A, the listings of the programs used are presented, and in annex B a review is made of the analytical formulae used for adjustment of the pulses. (I.C.R.) [pt

  16. Multilayer optics for x-ray analysis: design - fabrication - application

    International Nuclear Information System (INIS)

    Dietsch, R.; Holz, Th.; Bruegemann, L.

    2002-01-01

    Full text: The use of multilayer optics induced a decisive extension of opportunities in laboratory based X-ray analysis. With the growing number of different applications, more and more dedicated X-ray optics are required, optimized for the spectral range they are intended to be used for. Both the characteristic of the used X-ray source and the design of the multilayer optics finally define the performance of the conditioned incident beam for the application. In any case, qualified spacer and absorber materials have to be selected for the deposition of the multilayer in respect to the designated X-ray wavelength. X-ray optical devices based on uniform multilayers have the advantage of a wide acceptance angle but show chromatic aberrations. This effect can be avoided by synthesizing a multilayer with a lateral thickness gradient. The gradient ensures that any beam of a certain wavelength emitted from an infinite narrow X-ray source impinging the multilayer optics fulfills the Bragg condition. Three different types of curvature of laterally graded multilayer mirrors are used for X-ray analysis experiments: parabolic, elliptic and planar, which result in parallel, focusing and divergent beam conditions, respectively. Furthermore, the X-ray beam characteristics: intensity, monochromasy, divergence, beam width and brilliance can be additionally conditioned by combining one multilayer optics with either a different optic and/or with a crystal monochromator. The deposition of nanometer-multilayers, used as X-ray optical components, result in extraordinary requirements of the deposition process concerning precision, reproducibility and long term stability. Across a stack of more than 150 individual layers with thicknesses in the range between 1 to 10 nm, a variation of single layer thickness considerably lower than σ D = 0.1 nm and an interface roughness below σ R = 0.25 nm have to be achieved. Thickness homogeneity Δd/d -8 have to be guaranteed across macroscopic

  17. Changes of soft X-ray emission spectra of oxygen and copper in high Tc superconductors

    International Nuclear Information System (INIS)

    Fukushima, Sei; Gohshi, Yohichi; Kohiki, Shigemi; Saitoh, Naoki

    1989-01-01

    X-ray induced soft X-ray emission spectroscopy is one of the bulk analysis methods used to characterize high-Tc superconductor. In this report, some observations on the changes in O Kα and Cu L spectra of thin layer LnBa 2 Cu 3 O 7-δ (Ln=Er,Gd) samples are presented. From the measurement of O Kα, no discernible difference was found between those of Gd compounds which were composed single phase or not. It may be said that the electronic structure of p state localized on the O is not sensitive to the change of Tc or zero-resistance temperature. From the measurement of Cu L spectra, it was found that Cu Lα of only Gd containing compounds has a low energy shoulder

  18. Characterization of offset printing ink tagged with rare-earth taggants by X-ray emission techniques

    International Nuclear Information System (INIS)

    Joseph, D.; Saxena, A.; Choudhury, R.K.; Maind, S.D.

    2007-01-01

    Proton Induced X-ray Emission (PIXE) and Energy Dispersive X-ray Fluorescence (EDXRF) techniques have been used for elemental characterization of offset printing ink tagged with rare-earth taggants. The offset printing ink was tagged with rare-earth (La, Pr, Nd, Sm, Eu and Gd) thenoyltrifluoroacetonate chelates at about 1000-ppm level for each element separately. Small aliquots (approximately 20 mg) of tagged inks were coated on paper supports in the form of small circles having diameter 10-15 mm each and then analyzed. In the case of PIXE, a proton beam of energy 4 MeV and in the case of EDXRF a radioisotope source of 241 Am (100 mCi) was used to excite the samples. The PIXE analysis showed well-resolved rare-earth L X-rays and EDXRF analysis showed the K X-rays of rare earths. Satisfactory results to identify and quantify the taggants were achieved. (author)

  19. X-Ray Emission of Cataclysmic Variables Observed by Integral

    Czech Academy of Sciences Publication Activity Database

    Gális, R.; Eckert, D.; Paltani, S.; Münz, F.; Kocka, Matúš

    2009-01-01

    Roč. 18, 3-4 (2009), s. 321-326 ISSN 1392-0049 Grant - others:ESA(XE) ESA- PECS project No. 98023; VEGA(SK) 2/0078/10 Institutional research plan: CEZ:AV0Z10030501 Keywords : binaries starss * cataclysmic * X-rays Subject RIV: BN - Astronomy, Celestial Mechanics, Astrophysics Impact factor: 1.032, year: 2009

  20. X-ray Emission Characteristics of Flares Associated with CMEs ...

    Indian Academy of Sciences (India)

    tics of solar flares and their relationship with the dynamics of CMEs have ... lation between X-ray peak intensity of the flares with linear speed as well ... shear angle (θ1, measured at the flare onset), the final shear angle (θ2, measured at the.

  1. Energetic electron processes fluorescence effects for structured nanoparticles X-ray analysis and nuclear medicine applications

    Energy Technology Data Exchange (ETDEWEB)

    Taborda, A.; Desbrée, A. [Institut de Radioprotection et de Sûreté Nucléaire (IRSN), PRP-HOM/SDI/LEDI, BP-17, 31, Avenue de la Division Leclerc, 92262 Fontenay-aux-Roses (France); Carvalho, A. [IEQUALTECS, Lda, Rua Dr. Francisco Sá Carneiro, 36, 2500-065 S. Gregório CLD (Portugal); Chaves, P.C. [C" 2TN, Campus Tecnológico e Nuclear, Instituto Superior Técnico, Universidade de Lisboa, EN10 km 139.7, 2685-066 Bobadela LRS (Portugal); Reis, M.A., E-mail: mareis@ctn.tecnico.ulisboa.pt [IEQUALTECS, Lda, Rua Dr. Francisco Sá Carneiro, 36, 2500-065 S. Gregório CLD (Portugal); C" 2TN, Campus Tecnológico e Nuclear, Instituto Superior Técnico, Universidade de Lisboa, EN10 km 139.7, 2685-066 Bobadela LRS (Portugal)

    2016-08-15

    Superparamagnetic iron oxide (SPIO) nanoparticles are widely used as contrast agents for nuclear magnetic resonance imaging (MRI), and can be modified for improved imaging or to become tissue-specific or even protein-specific. The knowledge of their detailed elemental composition characterisation and potential use in nuclear medicine applications, is, therefore, an important issue. X-ray fluorescence techniques such as particle induced X-ray emission (PIXE) or X-ray fluorescence spectrometry (XRF), can be used for elemental characterisation even in problematic situations where very little sample volume is available. Still, the fluorescence coefficient of Fe is such that, during the decay of the inner-shell ionised atomic structure, keV Auger electrons are produced in excess to X-rays. Since cross-sections for ionisation induced by keV electrons, for low atomic number atoms, are of the order of 10{sup 3} barn, care should be taken to account for possible fluorescence effects caused by Auger electrons, which may lead to the wrong quantification of elements having atomic number lower than the atomic number of Fe. Furthermore, the same electron processes will occur in iron oxide nanoparticles containing {sup 57}Co, which may be used for nuclear medicine therapy purposes. In the present work, simple approximation algorithms are proposed for the quantitative description of radiative and non-radiative processes associated with Auger electrons cascades. The effects on analytical processes and nuclear medicine applications are quantified for the case of iron oxide nanoparticles, by calculating both electron fluorescence emissions and energy deposition on cell tissues where the nanoparticles may be embedded.

  2. Laboratory manual on sample preparation procedures for x-ray micro-analysis

    International Nuclear Information System (INIS)

    1997-01-01

    X-ray micro fluorescence is a non-destructive and sensitive method for studying the microscopic distribution of different elements in almost all kinds of samples. Since the beginning of this century, x-rays and electrons have been used for the analysis of many different kinds of material. Techniques which rely on electrons are mainly developed for microscopic studies, and are used in conventional Electron Microscopy (EM) or Scanning Electron Microscopy (SEM), while x-rays are widely used for chemical analysis at the microscopic level. The first chemical analysis by fluorescence spectroscopy using small x-ray beams was conducted in 1928 by Glockner and Schreiber. Since then much work has been devoted to developing different types of optical systems for focusing an x-ray beam, but the efficiency of these systems is still inferior to the conventional electron optical systems. However, even with a poor optical efficiency, the x-ray microbeam has many advantages compared with electron or proton induced x-ray emission methods. These include: The analyses are non-destructive, losses of mass are negligible, and due to the low thermal loading of x-rays, materials which may be thermally degraded can be analysed; Samples can be analysed in air, and no vacuum is required, therefore specimens with volatile components such as water in biological samples, can be imaged at normal pressure and temperature; No charging occurs during analysis and therefore coating of the sample with a conductive layer is not necessary; With these advantages, simpler sample preparation procedures including mounting and preservation can be used

  3. X-ray fluorescence spectrometry applied to soil analysis

    International Nuclear Information System (INIS)

    Salvador, Vera Lucia Ribeiro; Sato, Ivone Mulako; Scapin Junior, Wilson Santo; Scapin, Marcos Antonio; Imakima, Kengo

    1997-01-01

    This paper studies the X-ray fluorescence spectrometry applied to the soil analysis. A comparative study of the WD-XRFS and ED-XRFS techniques was carried out by using the following soil samples: SL-1, SOIL-7 and marine sediment SD-M-2/TM, from IAEA, and clay, JG-1a from Geological Survey of Japan (GSJ)

  4. A portable tube exciting X-ray fluorescence analysis system

    International Nuclear Information System (INIS)

    Yang Qiang; Lai Wanchang; Ge Liangquan

    2009-01-01

    Article introduced a portable tube exciting X-ray fluorescence analysis system which is based on arm architecture. Also, we designed Tube control circuit and finished preliminary application. The energy and the intensity of the photon can be adjusted continuously by using the tube. Experiments show that high excitation efficiency obtained by setting the appropriate parameters of the tube for the various elements. (authors)

  5. X-ray analysis in the steel industry

    International Nuclear Information System (INIS)

    Bourke, T.; Turner, K.

    1999-01-01

    Full text: The steel industry makes extensive use of X-ray analysis at all stages of the steelmaking process. XRF and XRD techniques, together with the associated techniques of electron probe microanalysis and electron microscopy are key tools for exploration and mine site and process development where detailed grade and mineralogical data is required. In production X-ray analysis is used to monitor and control: mine product grade (eg iron ore, coal and other raw materials), steel making production processes (eg iron ore sinter, incoming raw materials), waste products (eg coal watery refuse, slags) and final products (eg paint coatings, customer complaints). The demands put on X-ray analysis by the Steel Industry are severe. Iron ore mining and steelmaking is a continuous process, hence instrumentation has to be robust and reliable. In addition, with ever tightening environmental controls there is an increasing demand for trace heavy element analysis in both raw and waste materials. Copyright (1999) Australian X-ray Analytical Association Inc

  6. Hard X-ray Emission and Efficient Particle Acceleration by Supernova Remnants

    International Nuclear Information System (INIS)

    Vink, Jacco

    2009-01-01

    I discuss the non-thermal X-ray emission from young supernova remnants. Over the last decade it has become clear from both X-ray and γ-ray observations that young supernovae accelerate particles up to 100 TeV. In soft X-rays the accelerated >10 TeV electrons produce synchrotron radiation, coming from narrow filaments located at the shock fronts. The width of these filaments shows that the magnetic fields are relatively high, thus providing evidence for magnetic field amplification.The synchrotron radiation of several remnants is known to extend into the hard X-ray regime. In particular Cas A, has a spectrum that appears as a power law up to almost 100 TeV. This is very surprising, as a steepening is expected going from the soft to the hard X-ray band. The spectrum is likely a result of many superimposed individual spectra, each steepening at different energies. This implies considerable spatial variation in hard X-rays, an obvious target for Simbol-X. The variations will be important to infer local shock acceleration properties, but also magnetic field fluctuations may cause spatial and temporal variations.Finally, I draw the attention to super bubbles and supernovae as sources of cosmic rays. As such they may be sources of hard X-ray emission. In particular, supernovae exploding inside the dense red supergiants winds of their progenitors ares promising candidates for hard X-ray emission.

  7. Hard X-ray Emission and Efficient Particle Acceleration by Supernova Remnants

    Science.gov (United States)

    Vink, Jacco

    2009-05-01

    I discuss the non-thermal X-ray emission from young supernova remnants. Over the last decade it has become clear from both X-ray and γ-ray observations that young supernovae accelerate particles up to 100 TeV. In soft X-rays the accelerated >10 TeV electrons produce synchrotron radiation, coming from narrow filaments located at the shock fronts. The width of these filaments shows that the magnetic fields are relatively high, thus providing evidence for magnetic field amplification. The synchrotron radiation of several remnants is known to extend into the hard X-ray regime. In particular Cas A, has a spectrum that appears as a power law up to almost 100 TeV. This is very surprising, as a steepening is expected going from the soft to the hard X-ray band. The spectrum is likely a result of many superimposed individual spectra, each steepening at different energies. This implies considerable spatial variation in hard X-rays, an obvious target for Simbol-X. The variations will be important to infer local shock acceleration properties, but also magnetic field fluctuations may cause spatial and temporal variations. Finally, I draw the attention to super bubbles and supernovae as sources of cosmic rays. As such they may be sources of hard X-ray emission. In particular, supernovae exploding inside the dense red supergiants winds of their progenitors ares promising candidates for hard X-ray emission.

  8. News on the X-ray emission from hot subdwarf stars

    Directory of Open Access Journals (Sweden)

    Palombara Nicola La

    2017-12-01

    Full Text Available In latest years, the high sensitivity of the instruments on-board the XMM-Newton and Chandra satellites allowed us to explore the properties of the X-ray emission from hot subdwarf stars. The small but growing sample of X-ray detected hot subdwarfs includes binary systems, in which the X-ray emission is due to wind accretion onto a compact companion (white dwarf or neutron star, as well as isolated sdO stars, in which X-rays are probably due to shock instabilities in the wind. X-ray observations of these low-mass stars provide information which can be useful for our understanding of the weak winds of this type of stars and can lead to the discovery of particularly interesting binary systems. Here we report the most recent results we have recently obtained in this research area.

  9. RAMI analysis for ITER radial X-ray camera system

    Energy Technology Data Exchange (ETDEWEB)

    Qin, Shijun, E-mail: sjqin@ipp.ac.cn [Institute of Plasma Physics, Chinese Academy of Sciences, Hefei 230031 (China); Hu, Liqun; Chen, Kaiyun [Institute of Plasma Physics, Chinese Academy of Sciences, Hefei 230031 (China); Barnsley, Robin; Sirinelli, Antoine [ITER Organization, Route Vinon sur Verdon, CS 90046, 13067, St. Paul lez Durance, Cedex (France); Song, Yuntao; Lu, Kun; Yao, Damao; Chen, Yebin; Li, Shi; Cao, Hongrui; Yu, Hong; Sheng, Xiuli [Institute of Plasma Physics, Chinese Academy of Sciences, Hefei 230031 (China)

    2016-11-15

    Highlights: • The functional analysis of the ITER RXC system was performed. • A failure modes, effects and criticality analysis of the ITER RXC system was performed. • The reliability and availability of the ITER RXC system and its main functions were calculated. • The ITER RAMI approach was applied to the ITER RXC system for technical risk control in the preliminary design phase. - Abstract: ITER is the first international experimental nuclear fusion device. In the project, the RAMI approach (reliability, availability, maintainability and inspectability) has been adopted for technical risk control to mitigate all the possible failure of components in preparation for operation and maintenance. RAMI analysis of the ITER Radial X-ray Camera diagnostic (RXC) system during preliminary design phase was required, which insures the system with a very high performance to measure the X-ray emission and research the MHD of plasma with high accuracy on the ITER machine. A functional breakdown was prepared in a bottom-up approach, resulting in the system being divided into 3 main functions, 6 intermediate functions and 28 basic functions which are described using the IDEFØ method. Reliability block diagrams (RBDs) were prepared to calculate the reliability and availability of each function under assumption of operating conditions and failure data. Initial and expected scenarios were analyzed to define risk-mitigation actions. The initial availability of RXC system was 92.93%, while after optimization the expected availability was 95.23% over 11,520 h (approx. 16 months) which corresponds to ITER typical operation cycle. A Failure Modes, Effects and Criticality Analysis (FMECA) was performed to the system initial risk. Criticality charts highlight the risks of the different failure modes with regard to the probability of their occurrence and impact on operations. There are 28 risks for the initial state, including 8 major risks. No major risk remains after taking into

  10. Laboratory verification of the Active Particle-induced X-ray Spectrometer (APXS) on the Chang'e-3 mission

    International Nuclear Information System (INIS)

    Zhang, Guang-Liang; Li, Chun-Lai; Fu, Xiao-Hui; Zhang, Li-Yan; Ban, Cao; Li, Han; Zou, Yong-Liao; Peng, Wen-Xi; Cui, Xing-Zhu; Zhang, Cheng-Mo; Wang, Huan-Yu

    2015-01-01

    In the Chang'e-3 mission, the Active Particle-induced X-ray Spectrometer (APXS) on the Yutu rover is used to analyze the chemical composition of lunar soil and rock samples. APXS data are only valid are only if the sensor head gets close to the target and integration time lasts long enough. Therefore, working distance and integration time are the dominant factors that affect APXS results. This study confirms the ability of APXS to detect elements and investigates the effects of distance and time on the measurements. We make use of a backup APXS instrument to determine the chemical composition of both powder and bulk samples under the conditions of different working distances and integration times. The results indicate that APXS can detect seven major elements, including Mg, Al, Si, K, Ca, Ti and Fe under the condition that the working distance is less than 30 mm and having an integration time of 30 min. The statistical deviation is smaller than 15%. This demonstrates the instrument's ability to detect major elements in the sample. Our measurements also indicate the increase of integration time could reduce the measurement error of peak area, which is useful for detecting the elements Mg, Al and Si. However, an increase in working distance can result in larger errors in measurement, which significantly affects the detection of the element Mg. (paper)

  11. Characterizing X-Ray and Radio Emission in the Black Hole X-Ray Binary V404 Cygni During Quiescence

    DEFF Research Database (Denmark)

    Rana, Vikram; Loh, Alan; Corbel, Stephane

    2016-01-01

    We present results from multi-wavelength simultaneous X-ray and radio observations of the black hole X-ray binary V404 Cyg in quiescence. Our coverage with NuSTAR provides the very first opportunity to study the X-ray spectrum of V404 Cyg at energies above 10 keV. The unabsorbed broadband (0...

  12. Soft x-ray emission from classical novae in outburst

    International Nuclear Information System (INIS)

    Starrfield, S.; Krautter, J.; MacDonald, J.

    1989-01-01

    Theoretical modeling of novae in outburst predicts that they should be active emitters of radiation at soft x-ray wavelengths twice during their outburst. The first time occurs very early in the outburst when only a very sensitive all sky survey will be able to detect them. This period lasts only a few hours for the very fastest novae. They again become bright in x-rays late in the outburst when the remnant object becomes very hot and is still luminous. Both simulations and observations show that novae can remain very hot for months to years. It is important to observe them at these late times because a measurement both of the flux and temperature can provide information about the mass of the white dwarf, the turn-off time scale, and the energy budget of the outburst. 8 refs., 2 figs

  13. Coaxial gun parameters and X-ray emission

    International Nuclear Information System (INIS)

    Soliman, H.M.; El-Aragi, G.M.; Saudy, A.H.; Masoud, M.M.

    1994-01-01

    The paper presents the results of investigation with 3 kJ coaxial plasma gun, which operated with argon gas at pressure 0.8 torr. The coaxial plasma gun parameters are investigated by pick up coils, double electric probe, and x-ray probe. The mean electron temperature and density of the ejected plasma are 25 eV and 10 15 cm -3 respectively. The maximum kinetic pressure of the ejected plasma in the expansion chamber appears after 10 μs from the start of the discharge current. The energetic electrons is detected by an x-ray probe which showed a single pulse of electrons with energy ≅ 3 Kev. (orig.)

  14. Nonlinear QED effects in X-ray emission of pulsars

    Energy Technology Data Exchange (ETDEWEB)

    Shakeri, Soroush [Department of Physics, Isfahan University of Technology, Isfahan 84156-83111 (Iran, Islamic Republic of); Haghighat, Mansour [Department of Physics, Shiraz University, Shiraz 71946-84795 (Iran, Islamic Republic of); Xue, She-Sheng, E-mail: Soroush.Shakeri@ph.iut.ac.ir, E-mail: m.haghighat@shirazu.ac.ir, E-mail: xue@icra.it [ICRANet, Piazzale della Repubblica 10, 65122, Pescara (Italy)

    2017-10-01

    In the presence of strong magnetic fields near pulsars, the QED vacuum becomes a birefringent medium due to nonlinear QED interactions. Here, we explore the impact of the effective photon-photon interaction on the polarization evolution of photons propagating through the magnetized QED vacuum of a pulsar. We solve the quantum Boltzmann equation within the framework of the Euler-Heisenberg Lagrangian to find the evolution of the Stokes parameters. We find that linearly polarized X-ray photons propagating outward in the magnetosphere of a rotating neutron star can acquire high values for the circular polarization parameter. Meanwhile, it is shown that the polarization characteristics of photons besides photon energy depend strongly on parameters of the pulsars such as magnetic field strength, inclination angle and rotational period. Our results are clear predictions of QED vacuum polarization effects in the near vicinity of magnetic stars which can be tested with the upcoming X-ray polarimetric observations.

  15. Multielemental X-ray radiometric analysis of ferromanganese concretions

    International Nuclear Information System (INIS)

    Metelev, A.Yu.; Grigor'ev, A.I.; Rakita, K.A.; Mamaenko, M.V.; Ivanenko, V.V.

    1994-01-01

    Ferromanganese concretions are promising mineral resources of the ocean. Most often, they are analyzed by atomic-absorption, spectra, X-ray spectral, neutron-activation, and X-ray radiometric methods. Note that X-ray radiometric analysis (XRRA) allows the sufficiently rapid determination of a great number of elements in ferromanganese concretions. The possibility of using XRRA with saturated and thin layers was shown; however, the data on the precision and accuracy of the technique was not given. The purpose of this study is to evaluate the basic performance characteristics of the multielemental X-ray radiometric analysis of ferromanganese concretions (Pacific Ocean). Determinations for K,Ca and Ti content were made using a 55 Fe source and for Mn, Fe, Ni, Cu, Zn, Pb, Sr, Y, Zr, Nb, and Mo contents by using a 109 Cd source. The precision and accuracy of the method was investigated by using reference concretions; it was found the confidence intervals overlap for all of the elements except Ca and Pb. The relative standard deviation was 1-5%, indicating the high precision of the method. The described technique is successfully used on research vessels of the Far East Division of the Russian Academy of Sciences and in South Pacific Ocean geological expeditions of PO open-quotes Dal'morgeologiyaclose quotes

  16. X-ray emission from clusters and groups of galaxies

    Science.gov (United States)

    Mushotzky, R.

    1998-01-01

    Recent major advances in x-ray imaging and spectroscopy of clusters have allowed the determination of their mass and mass profile out to approximately 1/2 the virial radius. In rich clusters, most of the baryonic mass is in the gas phase, and the ratio of mass in gas/stars varies by a factor of 2-4. The baryonic fractions vary by a factor of approximately 3 from cluster to cluster and almost always exceed 0.09 h50-[3/2] and thus are in fundamental conflict with the assumption of Omega = 1 and the results of big bang nucleosynthesis. The derived Fe abundances are 0.2-0.45 solar, and the abundances of O and Si for low redshift systems are 0.6-1.0 solar. This distribution is consistent with an origin in pure type II supernova. The amount of light and energy produced by these supernovae is very large, indicating their importance in influencing the formation of clusters and galaxies. The lack of evolution of Fe to a redshift of z approximately 0.4 argues for very early enrichment of the cluster gas. Groups show a wide range of abundances, 0.1-0.5 solar. The results of an x-ray survey indicate that the contribution of groups to the mass density of the universe is likely to be larger than 0.1 h50-2. Many of the very poor groups have large x-ray halos and are filled with small galaxies whose velocity dispersion is a good match to the x-ray temperatures.

  17. Correlated X-ray/UV/optical emission and short-term variability in a Seyfert 1 galaxy NGC 4593

    Science.gov (United States)

    Pal, Main; Naik, Sachindra

    2018-03-01

    We present a detailed multifrequency analysis of an intense monitoring programme of Seyfert 1 galaxy NGC 4593 over a duration of nearly for a month with Swift observatory. We used 185 pointings to study the variability in six ultraviolet/optical and two soft (0.3-1.5 keV) and hard X-ray (1.5-10 keV) bands. The amplitude of the observed variability is found to decrease from high energy to low energy (X-ray to optical) bands. Count-count plots of ultraviolet/optical bands with hard X-rays clearly suggest the presence of a mixture of two major components: (i) highly variable component such as hard X-ray emission, and (ii) slowly varying disc-like component. The variations observed in the ultraviolet/optical emission are strongly correlated with the hard X-ray band. Cross-correlation analysis provides the lags for the longer wavelengths compared to the hard X-rays. Such lags clearly suggest that the changes in the ultraviolet/optical bands follow the variations in the hard X-ray band. This implies that the observed variation in longer wavelengths is due to X-ray reprocessing. Though, the measured lag spectrum (lag versus wavelength) is well described by λ4/3 as expected from the standard disc model, the observed lags are found to be longer than the predicted values from standard disc model. This implies that the actual size of the disc of NGC 4593 is larger than the estimated size of standard thin disc as reported in active galactic nuclei such as NGC 5548 and Fairall 9.

  18. A SEARCH FOR X-RAY EMISSION FROM COLLIDING MAGNETOSPHERES IN YOUNG ECCENTRIC STELLAR BINARIES

    Energy Technology Data Exchange (ETDEWEB)

    Getman, Konstantin V.; Broos, Patrick S. [Department of Astronomy and Astrophysics, 525 Davey Laboratory, Pennsylvania State University, University Park, PA 16802 (United States); Kóspál, Ágnes [Konkoly Observatory, Research Center for Astronomy and Earth Sciences, Hungarian Academy of Sciences, P.O. Box 67, 1525 Budapest (Hungary); Salter, Demerese M. [Department of Astronomy and Laboratory for Millimeter-Wave Astronomy, University of Maryland, College Park, MD 20742 (United States); Garmire, Gordon P. [Huntingdon Institute for X-ray Astronomy, LLC, 10677 Franks Road, Huntingdon, PA 16652 (United States)

    2016-12-01

    Among young binary stars whose magnetospheres are expected to collide, only two systems have been observed near periastron in the X-ray band: the low-mass DQ Tau and the older and more massive HD 152404. Both exhibit elevated levels of X-ray emission at periastron. Our goal is to determine whether colliding magnetospheres in young high-eccentricity binaries commonly produce elevated average levels of X-ray activity. This work is based on Chandra snapshots of multiple periastron and non-periastron passages in four nearby young eccentric binaries (Parenago 523, RX J1622.7-2325 Nw, UZ Tau E, and HD 152404). We find that for the merged sample of all four binaries the current X-ray data show an increasing average X-ray flux near periastron (at a ∼2.5-sigma level). Further comparison of these data with the X-ray properties of hundreds of young stars in the Orion Nebula Cluster, produced by the Chandra Orion Ultradeep Project (COUP), indicates that the X-ray emission from the merged sample of our binaries cannot be explained within the framework of the COUP-like X-ray activity. However, due to the inhomogeneities of the merged binary sample and the relatively low statistical significance of the detected flux increase, these findings are regarded as tentative only. More data are needed to prove that the flux increase is real and is related to the processes of colliding magnetospheres.

  19. Thermal analysis on x-ray tube for exhaust process

    Science.gov (United States)

    Kumar, Rakesh; Rao Ratnala, Srinivas; Veeresh Kumar, G. B.; Shivakumar Gouda, P. S.

    2018-02-01

    It is great importance in the use of X-rays for medical purposes that the dose given to both the patient and the operator is carefully controlled. There are many types of the X- ray tubes used for different applications based on their capacity and power supplied. In present thesis maxi ray 165 tube is analysed for thermal exhaust processes with ±5% accuracy. Exhaust process is usually done to remove all the air particles and to degasify the insert under high vacuum at 2e-05Torr. The tube glass is made up of Pyrex material, 95%Tungsten and 5%rhenium is used as target material for which the melting point temperature is 3350°C. Various materials are used for various parts; during the operation of X- ray tube these waste gases are released due to high temperature which in turn disturbs the flow of electrons. Thus, before using the X-ray tube for practical applications it has to undergo exhaust processes. Initially we build MX 165 model to carry out thermal analysis, and then we simulate the bearing temperature profiles with FE model to match with test results with ±5%accuracy. At last implement the critical protocols required for manufacturing processes like MF Heating, E-beam, Seasoning and FT.

  20. The Elusive Soft Emission from Hard X-ray Symbiotic System RT Cru

    Science.gov (United States)

    Karovska, Margarita

    2014-09-01

    RT Cru is a fascinating member of a new class of hard X-ray emitting symbiotic binaries showing X-ray emission extending to over 50keV. While its hard X-ray emission has been studied in detail, the soft component of the spectrum, including flares, remains elusive, since previous observations have focused on the high-energy regime. We propose Chandra HRC-S/LETG observations to determine the spatial, spectral, and temporal characteristics of the source of the soft X-ray emission with a goal to establish the origin of the soft component, and determine whether and how it is tied to the hard component. Determining the origin of the soft emission is a crucial piece of the puzzle to understanding the geometry, energetics, and the environment of WD accretion in this class of symbiotic systems.

  1. Laboratory simulation of charge exchange-produced X-ray emission from comets.

    Science.gov (United States)

    Beiersdorfer, P; Boyce, K R; Brown, G V; Chen, H; Kahn, S M; Kelley, R L; May, M; Olson, R E; Porter, F S; Stahle, C K; Tillotson, W A

    2003-06-06

    In laboratory experiments using the engineering spare microcalorimeter detector from the ASTRO-E satellite mission, we recorded the x-ray emission of highly charged ions of carbon, nitrogen, and oxygen, which simulates charge exchange reactions between heavy ions in the solar wind and neutral gases in cometary comae. The spectra are complex and do not readily match predictions. We developed a charge exchange emission model that successfully reproduces the soft x-ray spectrum of comet Linear C/1999 S4, observed with the Chandra X-ray Observatory.

  2. X-ray Imaging and preliminary studies of the X-ray self-emission from an innovative plasma-trap based on the Bernstein waves heating mechanism

    Science.gov (United States)

    Caliri, C.; Romano, F. P.; Mascali, D.; Gammino, S.; Musumarra, A.; Castro, G.; Celona, L.; Neri, L.; Altana, C.

    2013-10-01

    Electron Cyclotron Resonance Ion Sources (ECRIS) are based on ECR heated plasmas emitting high fluxes of X-rays. Here we illustrate a pilot study of the X-ray emission from a compact plasma-trap in which an off-resonance microwave-plasma interaction has been attempted, highlighting a possible Bernstein-Waves based heating mechanism. EBWs-heating is obtained via the inner plasma EM-to-ES wave conversion and enables to reach densities much larger than the cut-off ones. At LNS-INFN, an innovative diagnostic technique based on the design of a Pinhole Camera (PHC) coupled to a CCD device for X-ray Imaging of the plasma (XRI) has been developed, in order to integrate X-ray traditional diagnostics (XRS). The complementary use of electrostatic probes measurements and X-ray diagnostics enabled us to gain knowledge about the high energy electrons density and temperature and about the spatial structure of the source. The combination of the experimental data with appropriate modeling of the plasma-source allowed to estimate the X-ray emission intensity in different energy domains (ranging from EUV up to Hard X-rays). The use of ECRIS as X-ray source for multidisciplinary applications, is now a concrete perspective due to the intense fluxes produced by the new plasma heating mechanism.

  3. Intravenous coronary angiography utilizing K-emission and bremsstrahlung X-rays produced by electron bombardment

    International Nuclear Information System (INIS)

    1992-01-01

    The screening of the general population for coronary artery disease would be practical if a method existed for visualizing the extent of occlusion after an intravenous injection of contrast agent. Measurements performed with synchrotron radiation at SSRL and NSLS have shown that such an intravenous angiography procedure would be possible with an intense source of monochromatic X-rays. Because of the high cost of an electron synchrotron, theoretical analysis and experiments using inanimate phantoms has been undertaken to demonstrate the feasibility of using the spectrum produced by two appropriately chosen anode materials when bombarded with electrons in the 100--500 keV energy range for angiography. By using the X-rays emitted at 120 degree to the incident electron direction, about 20--30% of the X-ray intensity would be due to K-emission lines. Calculations using the TIGERP Monte Carlo Code, have shown that high quality angiograms of human coronary arteries should be possible with a contrast agent containing ytterbium, if an electron beam pulses of 16 kJ were used for each anode target. The experimental program supported in part by the DOE has consisted of these theoretical calculations and experiments at the Dynamitron Electron Accelerator Facility at BNL

  4. Modeling of X-ray emissions produced by stepping lightning leaders

    OpenAIRE

    Xu , Wei; Celestin , Sebastien; Pasko , Victor P.

    2014-01-01

    International audience; Intense and brief bursts of X-ray emissions have been measured during the stepping processof both natural cloud-to-ground (CG) and rocket-triggered lightning flashes. In this paper, we investigatetheoretically the energy spectra of X-rays produced by the bremsstrahlung emission of thermal runawayelectrons accelerated in the inhomogeneous electric field produced around lightning leader tips. The X-rayenergy spectrum depends on the physical properties of the associated l...

  5. DISCOVERY OF X-RAY EMISSION FROM THE GALACTIC SUPERNOVA REMNANT G32.8-0.1 WITH SUZAKU

    Energy Technology Data Exchange (ETDEWEB)

    Bamba, Aya; Sawada, Makoto [Department of Physics and Mathematics, Aoyama Gakuin University 5-10-1 Fuchinobe Chuo-ku, Sagamihara, Kanagawa 252-5258 (Japan); Terada, Yukikatsu [Department of Physics, Science, Saitama University, Sakura, Saitama 338-8570 (Japan); Hewitt, John; Petre, Robert; Angelini, Lorella [NASA Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Safi-Harb, Samar [Department of Physics and Astronomy, University of Manitoba, Winnipeg MB R3T 2N2 (Canada); Zhou, Ping [Department of Astronomy, Nanjing University, Nanjing 210093 (China); Bocchino, Fabrizio [INAF—Osservatorio Astronomico di Palermo, Piazza del Parlamento 1, I-90134, Palermo (Italy)

    2016-02-10

    We present the first dedicated X-ray study of the supernova remnant (SNR) G32.8−0.1 (Kes 78) with Suzaku. X-ray emission from the whole SNR shell has been detected for the first time. The X-ray morphology is well correlated with the emission from the radio shell, while anti-correlated with the molecular cloud found in the SNR field. The X-ray spectrum shows not only conventional low-temperature (kT ∼ 0.6 keV) thermal emission in a non-equilibrium ionization state, but also a very high-temperature (kT ∼ 3.4 keV) component with a very low ionization timescale (∼2.7 × 10{sup 9} cm{sup −3} s), or a hard nonthermal component with a photon index Γ ∼ 2.3. The average density of the low-temperature plasma is rather low, of the order of 10{sup −3}–10{sup −2} cm{sup −3}, implying that this SNR is expanding into a low-density cavity. We discuss the X-ray emission of the SNR, also detected in TeV with H.E.S.S., together with multi-wavelength studies of the remnant and other gamma-ray emitting SNRs, such as W28 and RCW 86. Analysis of a time-variable source, 2XMM J185114.3−000004, found in the northern part of the SNR, is also reported for the first time. Rapid time variability and a heavily absorbed hard-X-ray spectrum suggest that this source could be a new supergiant fast X-ray transient.

  6. Discovery of X-Ray Emission from the Galactic Supernova Remnant G32.8-0.1 with Suzaku

    Science.gov (United States)

    Bamba, Aya; Terada, Yukikatsu; Hewitt, John; Petre, Robert; Angelini, Lorella; Safi-Harb, Samar; Zhou, Ping; Bocchino, Fabrizio; Sawada, Makoto

    2016-01-01

    We present the first dedicated X-ray study of the supernova remnant (SNR) G32.8-0.1 (Kes 78) with Suzaku. X-ray emission from the whole SNR shell has been detected for the first time. The X-ray morphology is well correlated with the emission from the radio shell, while anti-correlated with the molecular cloud found in the SNR field. The X-ray spectrum shows not only conventional low-temperature (kT approximately 0.6 kiloelectronvolts) thermal emission in a nonequilibrium ionization state, but also a very high-temperature (approximately 3.4 kiloelectronvolts) component with a very low ionization timescale (approximately 2.7 times 10 (sup 9) per cubic centimeter per second), or a hard nonthermal component with a photon index Gamma approximately equal to 2.3. The average density of the low-temperature plasma is rather low, of the order of 10 (sup -3) - 10 (sup -2) per cubic centimeter, implying that this SNR is expanding into a low-density cavity. We discuss the X-ray emission of the SNR, also detected in teraelectronvolts with H.E.S.S. (High Energy Stereoscopic System), together with multi-wavelength studies of the remnant and other gamma-ray emitting SNRs, such as W28 and RCW 86. Analysis of a time-variable source, 2XMM J185114.3-000004, found in the northern part of the SNR, is also reported for the first time. Rapid time variability and a heavily absorbed hard-X-ray spectrum suggest that this source could be a new supergiant fast X-ray transient.

  7. Chemical analysis by X-ray fluorescence, of niobium in high-strength plate steels

    International Nuclear Information System (INIS)

    Iozzi, F.B.; Dias, M.J.P.

    1981-01-01

    The use of X-ray fluorescence spectrometry in quantitative analysis of niobium in steels, as an alternative solution for optical emission spectrometry, in the rapid chemical control of steel fabrication by LD type converters, is presented. (M.C.K.) [pt

  8. X-ray emission of the hot gas and of accelerated particles in supernova remnants

    International Nuclear Information System (INIS)

    Acero, F.

    2008-09-01

    The current observations seem to support the theory that the shock wave of supernova remnants accelerate electrons (representing about 1% of cosmic rays) of the interstellar medium up to energies of about 10 15 eV. However there is still no solid evidence that supernova remnants also accelerate protons (major component of cosmic rays). The X-ray observations of those supernova remnants with the satellite XMM-Newton can provide crucial information on the acceleration mechanisms and on this population of accelerated particles. This thesis presents the X-ray analysis of the supernova remnants RX J1713.7-3946 and SN 1006 for which it has been shown that they accelerate electrons efficiently. As a result, these objects are very good targets to compare the theoretical models of acceleration to the observation. For the first object, I constructed through new XMM-Newton observations, the first high-angular resolution mosaic of the entire supernova remnant. I then compared the X- and gamma-ray emission of this object in order to understand the nature of the gamma-ray emission. This spectral and morphological comparison allowed me to discuss the two possible origins of the gamma-ray radiation (issued by electrons or by protons). For SN 1006, I studied the density of the ambient medium in which the shock wave propagates. This density is a key parameter for the hydrodynamical evolution of the remnant and for studying a future gamma-ray emission. The study of X-ray emission of the gas heated by the shock wave allowed me to better estimate of the value of the density so far poorly constrained for this object. (author)

  9. C IV EMISSION AND THE ULTRAVIOLET THROUGH X-RAY SPECTRAL ENERGY DISTRIBUTION OF RADIO-QUIET QUASARS

    International Nuclear Information System (INIS)

    Kruczek, Nicholas E.; Richards, Gordon T.; Deo, Rajesh P.; Krawczyk, Coleman M.; Gallagher, S. C.; Hall, Patrick B.; Hewett, Paul C.; Leighly, Karen M.; Proga, Daniel

    2011-01-01

    In the rest-frame ultraviolet (UV), two of the parameters that best characterize the range of emission-line properties in quasar broad emission-line regions are the equivalent width and the blueshift of the C IV λ1549 line relative to the quasar rest frame. We explore the connection between these emission-line properties and the UV through X-ray spectral energy distribution (SED) for radio-quiet (RQ) quasars. Our sample consists of a heterogeneous compilation of 406 quasars from the Sloan Digital Sky Survey (at z > 1.54) and Palomar-Green survey (at z < 0.4) that have well-measured C IV emission-line and X-ray properties (including 164 objects with measured Γ). We find that RQ quasars with both strong C IV emission and small C IV blueshifts can be classified as 'hard-spectrum' sources that are (relatively) strong in the X-ray as compared to the UV. On the other hand, RQ quasars with both weak C IV emission and large C IV blueshifts are instead 'soft-spectrum' sources that are (relatively) weak in the X-ray as compared to the UV. This work helps to further bridge optical/soft X-ray 'eigenvector 1' relationships to the UV and hard X-ray. Based on these findings, we argue that future work should consider systematic errors in bolometric corrections (and thus accretion rates) that are derived from a single mean SED. Detailed analysis of the C IV emission line may allow for SED-dependent corrections to these quantities.

  10. X-ray emission as a potential hazard during ultrashort pulse laser material processing

    Science.gov (United States)

    Legall, Herbert; Schwanke, Christoph; Pentzien, Simone; Dittmar, Günter; Bonse, Jörn; Krüger, Jörg

    2018-06-01

    In laser machining with ultrashort laser pulses unwanted X-ray radiation in the keV range can be generated when a critical laser intensity is exceeded. Even if the emitted X-ray dose per pulse is low, high laser repetition rates can lead to an accumulation of X-ray doses beyond exposure safety limits. For 925 fs pulse duration at a center wavelength of 1030 nm, the X-ray emission was investigated up to an intensity of 2.6 × 1014 W/cm2. The experiments were performed in air with a thin disk laser at a repetition rate of 400 kHz. X-ray spectra and doses were measured for various planar target materials covering a wide range of the periodic table from aluminum to tungsten. Without radiation shielding, the measured radiation doses at this high repetition rate clearly exceed the regulatory limits. Estimations for an adequate radiation shielding are provided.

  11. On the Absence of Non-thermal X-Ray Emission around Runaway O Stars

    Energy Technology Data Exchange (ETDEWEB)

    Toalá, J. A. [Institute of Astronomy and Astrophysics, Academia Sinica (ASIAA), Taipei 10617, Taiwan (China); Oskinova, L. M. [Institute for Physics and Astronomy, University of Potsdam, D-14476 Potsdam (Germany); Ignace, R. [Department of Physics and Astronomy, East Tennessee State University, Johnson City, TN 37614 (United States)

    2017-04-01

    Theoretical models predict that the compressed interstellar medium around runaway O stars can produce high-energy non-thermal diffuse emission, in particular, non-thermal X-ray and γ -ray emission. So far, detection of non-thermal X-ray emission was claimed for only one runaway star, AE Aur. We present a search for non-thermal diffuse X-ray emission from bow shocks using archived XMM-Newton observations for a clean sample of six well-determined runaway O stars. We find that none of these objects present diffuse X-ray emission associated with their bow shocks, similarly to previous X-ray studies toward ζ Oph and BD+43°3654. We carefully investigated multi-wavelength observations of AE Aur and could not confirm previous findings of non-thermal X-rays. We conclude that so far there is no clear evidence of non-thermal extended emission in bow shocks around runaway O stars.

  12. Exotic x-ray emission from dense plasmas

    Czech Academy of Sciences Publication Activity Database

    Rosmej, F.B.; Dachicourt, R.; Deschaud, B.; Khaghani, D.; Dozières, M.; Šmíd, Michal; Renner, Oldřich

    2015-01-01

    Roč. 48, č. 22 (2015), s. 224005 ISSN 0953-4075 R&D Projects: GA MŠk ED1.1.00/02.0061 EU Projects: European Commission(XE) 284464 - LASERLAB-EUROPE Grant - others:ELI Beamlines(XE) CZ.1.05/1.1.00/02.0061; AVČR(CZ) M100101208 Institutional support: RVO:68378271 Keywords : hollow ions * x-ray spectroscopy * atomic physics Subject RIV: BL - Plasma and Gas Discharge Physics Impact factor: 1.833, year: 2015

  13. Radio and X-ray emission from newly born remnants

    International Nuclear Information System (INIS)

    Salvati, M.

    1983-01-01

    Radio and X-ray observations of SN 1979c and SN 1980k offer a unique opportunity of monitoring the transition from supernovae to remnants. By means of the two-frequency radio light curves, the hypothesis that these objects are surrounded by circumstellar matter, originated in a presupernova wind, is tested, and the relevant parameters are derived. Then the absorption-corrected light curves are used to test the various proposed models. SN 1980k appears to be powered by a canonical shock, while SN 1979c is a good plerion candidate. An optical pulsar could still be detected at its location. (Auth.)

  14. Analysis of Atmospheric Aerosols Collected in an Urban Area in Upstate NY Using Proton Induced X-ray Emission (PIXE) Spectroscopy

    Science.gov (United States)

    Smith, Jeremy; Ali, Salina; Nadareski, Benjamin; Safiq, Alexandrea; Yoskowitz, Joshua; Labrake, Scott; Vineyard, Michael

    2013-10-01

    We examined atmospheric aerosol samples collected in Schenectady NY for evidence of pollution. We collected aerosol samples using a nine stage cascade impactor which distributes the particulate matter by aerodynamic size onto 7.5 μm Kapton foils. We then used a 1MV electrostatic Pelletron accelerator to produce a 2.2 MeV proton beam to hit the impacted foils. X-ray intensity versus energy spectra were collected using an Amptek x-ray detector where the x-rays are produced from the proton beam interacting with the sample. This is called PIXE. The elemental composition and concentrations of the elements present in the aerosol samples were determined using a software package called GUPIX. We have found elements ranging from Al to Pb and in particular have found significant amounts of Pb and Br on some of our impacted foils, with a Br/Pb ratio of 0.6 +/- 0.2 which agrees with previous studies. This result suggests the presence of leaded aviation fuel perhaps due to the proximity of the collection site to a small airport with a significant amount of general aviation traffic. Union College.

  15. Bayesian Multiscale Analysis of X-Ray Jet Features in High Redshift Quasars

    Science.gov (United States)

    McKeough, Kathryn; Siemiginowska, A.; Kashyap, V.; Stein, N.

    2014-01-01

    X-ray emission of powerful quasar jets may be a result of the inverse Compton (IC) process in which the Cosmic Microwave Background (CMB) photons gain energy by interactions with the jet’s relativistic electrons. However, there is no definite evidence that IC/CMB process is responsible for the observed X-ray emission of large scale jets. A step toward understanding the X-ray emission process is to study the Radio and X-ray morphologies of the jet. We implement a sophisticated Bayesian image analysis program, Low-count Image Reconstruction and Analysis (LIRA) (Esch et al. 2004; Conners & van Dyk 2007), to analyze jet features in 11 Chandra images of high redshift quasars (z ~ 2 - 4.8). Out of the 36 regions where knots are visible in the radio jets, nine showed detectable X-ray emission. We measured the ratios of the X-ray and radio luminosities of the detected features and found that they are consistent with the CMB radiation relationship. We derived a range of the bulk lorentz factor (Γ) for detected jet features under the CMB jet emission model. There is no discernible trend of Γ with redshift within the sample. The efficiency of the X-ray emission between the detected jet feature and the corresponding quasar also shows no correlation with redshift. This work is supported in part by the National Science Foundation REU and the Department of Defense ASSURE programs under NSF Grant no.1262851 and by the Smithsonian Institution, and by NASA Contract NAS8-39073 to the Chandra X-ray Center (CXC). This research has made use of data obtained from the Chandra Data Archive and Chandra Source Catalog, and software provided by the CXC in the application packages CIAO, ChIPS, and Sherpa. We thank Teddy Cheung for providing the VLA radio images. Connors, A., & van Dyk, D. A. 2007, Statistical Challenges in Modern Astronomy IV, 371, 101 Esch, D. N., Connors, A., Karovska, M., & van Dyk, D. A. 2004, ApJ, 610, 1213

  16. Non-thermal Hard X-Ray Emission from Coma and Several Abell Clusters

    International Nuclear Information System (INIS)

    Correa, C

    2004-01-01

    We report results of hard X-Ray observations of the clusters Coma, Abell 496, Abell754, Abell 1060, Abell 1367, Abell2256 and Abell3558 using RXTE data from the NASA HEASARC public archive. Specifically we searched for clusters with hard x-ray emission that can be fitted by a power law because this would indicate that the cluster is a source of non-thermal emission. We are assuming the emission mechanism proposed by Vahk Petrosian where the inter cluster space contains clouds of relativistic electrons that by themselves create a magnetic field and emit radio synchrotron radiation. These relativistic electrons Inverse-Compton scatter Microwave Background photons up to hard x-ray energies. The clusters that were found to be sources of non-thermal hard x-rays are Coma, Abell496, Abell754 and Abell 1060

  17. Quantitative analysis by computer controlled X-ray fluorescence spectrometer

    International Nuclear Information System (INIS)

    Balasubramanian, T.V.; Angelo, P.C.

    1981-01-01

    X-ray fluorescence spectroscopy has become a widely accepted method in the metallurgical field for analysis of both minor and major elements. As encountered in many other analytical techniques, the problem of matrix effect generally known as the interelemental effects is to be dealt with effectively in order to make the analysis accurate. There are several methods by which the effects of matrix on the analyte are minimised or corrected for and the mathematical correction is one among them. In this method the characteristic secondary X-ray intensities are measured from standard samples and correction coefficients. If any, for interelemental effects are evaluated by mathematical calculations. This paper describes attempts to evaluate the correction coefficients for interelemental effects by multiple linear regression programmes using a computer for the quantitative analysis of stainless steel and a nickel base cast alloy. The quantitative results obtained using this method for a standard stainless steel sample are compared with the given certified values. (author)

  18. X-RAY EMISSION FROM J1446–4701, J1311–3430, AND OTHER BLACK WIDOW PULSARS

    Energy Technology Data Exchange (ETDEWEB)

    Arumugasamy, Prakash; Pavlov, George G. [Department of Astronomy and Astrophysics, 525 Davey Lab, The Pennsylvania State University, University Park, PA 16802 (United States); Garmire, Gordon P., E-mail: pxa151@ucs.psu.edu [Huntingdon Institute for X-ray Astronomy, LLC, 10677 Franks Road, Huntingdon, PA 16652 (United States)

    2015-12-01

    We present the results of detailed X-ray analysis of two black-widow pulsars (BWPs), J1446–4701 and J1311–3430. PSR J1446–4701 is a BWP with orbital parameters near the median values of the sample of known BWPs. Its X-ray emission that was detected by XMM-Newton is well characterized by a soft power-law (PL) spectrum (photon index Γ ≈ 3), and it shows no significant orbital modulations. In view of a lack of radio eclipses and an optical non-detection, the system most likely has a low orbital inclination. PSR J1311–3430 is an extreme BWP with a very compact orbit and the lowest minimum mass companion. Our Chandra data confirm the hard Γ ≈ 1.3 emission seen in previous observations. Through phase-restricted spectral analysis, we found a hint (∼2.6σ) of spectral hardening around pulsar inferior conjunction. We also provide a uniform analysis of the 12 BWPs observed with Chandra and compare their X-ray properties. Pulsars with soft, Γ > 2.5 emission seem to have lower than average X-ray and γ-ray luminosities. We do not, however, see any other prominent correlation between the pulsar’s X-ray emission characteristics and any of its other properties. The contribution of the intra-binary shock to the total X-ray emission, if any, is not discernible in this sample of pulsars with shallow observations.

  19. X-ray qualitative analysis of low concentration phases

    International Nuclear Information System (INIS)

    Brusilovskii, B.A.; Khaet, L.G.

    1993-01-01

    The identification of low concentration phases (LCP) situated at the detection limit of x-ray analysis have not been examined sufficiently. The authors have developed a method of qualitative x-ray analysis of LCPs of the first order (carbides and certain intermetallic compounds) in a multiphase system. X-ray examination of the LCPs consists of analysis of a priori information and formation of the information data on the basis of the profile of the diffraction line with subsequent processing using the F-criterion (Fischer's criterion). If the phase is not detected, consecutive analysis with build up of information is pursued. Results are presented of a successive qualitative phase analysis of a region of quenched layer of a roll situated 10 mm from the surface. Carbide phases were identified in the quenched layer of the roll up to 15 mm deep and in the transition zone 15-35 mm. The proposed method was justified physically and statistically, recommendations for practice were given, and the method was tested and is regarded as promising for detecting weak lines in qualitative diffractometric analysis. 12 refs., 3 tabs

  20. Proton induced X-Ray fluorescence study as a tool trace element analysis

    International Nuclear Information System (INIS)

    El-Kady, Ahmed A.

    1978-01-01

    Usefulness and limitations of trace elemental analysis by high energy charged particles and photon induced X-ray have been discussed. Comparison with the well established neutron activation analysis technique is also given. Back-ground radiation due to bremsstrahlung from secondary electrons and due to charged particle bremsstrahlung have been reviewed for different projectiles. The sensitivity of elemental analysis by proton induced X-ray fluorescence have been examined by measuring the characteristic X-ray emission cross section for K and L transitions of many elements and for different proton energies and compared with theroretical values. The discussion given in this report show that with suitable proton generator and a high resolution X-ray detector, proton X-ray fluorescence technique is capable of analyzing many elements simultaneously at the part per million level and offers a rapid and reliable method for trace element analysis. Data on water, blood and tissue samples given in this report are few examples of many possible applications

  1. Nuclear X-ray emission after fusion of heavy ions

    Energy Technology Data Exchange (ETDEWEB)

    Berner, Christian; Muecher, Dennis; Gernhaeuser, Roman; Faestermann, Thomas [Technische Universitaet Muenchen, Lehrstuhl E12 (Germany); Henning, Walter [Technische Universitaet Muenchen, Lehrstuhl E12 (Germany); Argonne National Laboratory (United States); Morita, Kosuke; Morimoto, Kouji; Kaji, Daija [RIKEN, Research Group for Superheavy Elements (Japan)

    2015-07-01

    The goal is to establish in-beam K-X-ray spectroscopy as a sensitive tool to identify super heavy elements (SHEs) produced in fusion reactions via their proton number. SHEs, formed after cold or hot fusion, are usually identified via the alpha-decay products, which have to be connected to well-known elements. In case of hot fusion, the daughter nuclei quickly undergo spontaneous fission, so that the identification of the produced SHEs is difficult. Using the hot fusion approach in our first test experiments, the resultant products will be analysed by the gas-filled GARIS separator at the RILAC facility at RIKEN. As the X-ray detector is required to have superior energy and timing resolution to best identify the rare events at highest masses and to supress random coincidences as sufficient as possible, we chose a thin and planar geometry, which also reduces the damage caused by fast neutrons. We show first measurements using the MINIBALL Ge array at Munich. Additionally we report on our feasibility studies and on first tests using the new detector at high count rates together with a powerful DAQ system and transistor reset preamplifiers.

  2. SphinX MEASUREMENTS OF THE 2009 SOLAR MINIMUM X-RAY EMISSION

    International Nuclear Information System (INIS)

    Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Bakała, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B.; Kuzin, S.; Farnik, F.; Reale, F.; Phillips, K. J. H.

    2012-01-01

    The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 × 10 47 cm –3 and 1.1 × 10 48 cm –3 . Comparing SphinX emission with that from the Hinode X-ray Telescope, we deduce that most of the emission is from general coronal structures rather than confined features like bright points. For one of 27 intervals of exceptionally low activity identified in the SphinX data, the Sun's X-ray luminosity in an energy range roughly extrapolated to that of ROSAT (0.1-2.4 keV) was less than most nearby K and M dwarfs.

  3. SphinX Measurements of the 2009 Solar Minimum X-Ray Emission

    Science.gov (United States)

    Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Kuzin, S.; Farnik, F.; Reale, F.; Phillips, K. J. H.; Bakała, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B.

    2012-06-01

    The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 × 1047 cm-3 and 1.1 × 1048 cm-3. Comparing SphinX emission with that from the Hinode X-ray Telescope, we deduce that most of the emission is from general coronal structures rather than confined features like bright points. For one of 27 intervals of exceptionally low activity identified in the SphinX data, the Sun's X-ray luminosity in an energy range roughly extrapolated to that of ROSAT (0.1-2.4 keV) was less than most nearby K and M dwarfs.

  4. SphinX MEASUREMENTS OF THE 2009 SOLAR MINIMUM X-RAY EMISSION

    Energy Technology Data Exchange (ETDEWEB)

    Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Bakala, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B. [Space Research Centre, Polish Academy of Sciences, 51-622, Kopernika 11, Wroclaw (Poland); Kuzin, S. [P. N. Lebedev Physical Institute (FIAN), Russian Academy of Sciences, Leninsky Prospect 53, Moscow 119991 (Russian Federation); Farnik, F. [Astronomical Institute, Ondrejov Observatory (Czech Republic); Reale, F. [Dipartimento di Fisica, Universita di Palermo, Palermo, Italy, and INAF, Osservatorio Astronomico di Palermo, Palermo (Italy); Phillips, K. J. H., E-mail: js@cbk.pan.wroc.pl [Mullard Space Science Laboratory, University College London, Holmbury St. Mary, Dorking, Surrey RH5 6NT (United Kingdom)

    2012-06-01

    The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 Multiplication-Sign 10{sup 47} cm{sup -3} and 1.1 Multiplication-Sign 10{sup 48} cm{sup -3}. Comparing SphinX emission with that from the Hinode X-ray Telescope, we deduce that most of the emission is from general coronal structures rather than confined features like bright points. For one of 27 intervals of exceptionally low activity identified in the SphinX data, the Sun's X-ray luminosity in an energy range roughly extrapolated to that of ROSAT (0.1-2.4 keV) was less than most nearby K and M dwarfs.

  5. Analysis of neon soft x-ray spectra from short-pulse laser-produced plasmas

    International Nuclear Information System (INIS)

    Abare, A.C.; Keane, C.J.; Crane, J.K.; DaSilva, L.B.; Lee, R.W.; Perry, M.D.; Falcone, R.W.

    1993-04-01

    We report preliminary results from the analysis of streaked soft x-ray neon spectra a gas jet target. In obtained from the interaction of a picosecond Nd:glass laser with these experiments streaked spectra show prompt harmonic emission followed by longer time duration soft x-ray line emission. The majority of the line emission observed was found to originate from Li- and Be-like Ne and the major transitions in the observed spectra have been identified. Li-like emission lines were observed to decay faster in time than Be-like transitions, suggesting that recombination is taking place. Line ratios of n=4-2 and n=3-2 transitions supported the view that these lines were optically thin and thick, respectively. The time history of Li-like Ne 2p-4d and 2p-3d lines is in good agreement with a simple adiabatic expansion model coupled to a time dependent collisional-radiative code. Further x-ray spectroscopic analysis is underway which is aimed at diagnosing plasma conditions and assessing the potential of this recombining neon plasma as a quasi-steady-state recombination x-ray laser medium

  6. Parallelization for X-ray crystal structural analysis program

    Energy Technology Data Exchange (ETDEWEB)

    Watanabe, Hiroshi [Japan Atomic Energy Research Inst., Tokyo (Japan); Minami, Masayuki; Yamamoto, Akiji

    1997-10-01

    In this report we study vectorization and parallelization for X-ray crystal structural analysis program. The target machine is NEC SX-4 which is a distributed/shared memory type vector parallel supercomputer. X-ray crystal structural analysis is surveyed, and a new multi-dimensional discrete Fourier transform method is proposed. The new method is designed to have a very long vector length, so that it enables to obtain the 12.0 times higher performance result that the original code. Besides the above-mentioned vectorization, the parallelization by micro-task functions on SX-4 reaches 13.7 times acceleration in the part of multi-dimensional discrete Fourier transform with 14 CPUs, and 3.0 times acceleration in the whole program. Totally 35.9 times acceleration to the original 1CPU scalar version is achieved with vectorization and parallelization on SX-4. (author)

  7. Infrared X-ray and thermal analysis of terbium soaps

    International Nuclear Information System (INIS)

    Mehrotra, K.N.; Sharma, N.

    1996-01-01

    Terbium sops (laureate, myristate and palmitate) were synthesized by direct metathesis of corresponding potassium soap with an aqueous solution of terbium nitrate. The physico-chemical characteristics of soaps in solid state were investigated by IR spectra, X-ray diffraction patterns and TGA measurements. The IR results revealed that the fatty acids exist in dimeric state through hydrogen bonding while the soaps possess partial ionic character. The X-ray analysis showed that the soaps have double layer structure with molecular axes slightly inclined to the basal plane. The thermal analysis suggested that the decomposition of soaps occur in two steps. The energy of activation, order of reaction and various kinetic parameters (i.e. frequency factor, entropy of activation and free energy) for the thermal decomposition of soaps were evaluated. (author). 26 refs, 4 figs, 4 tabs

  8. ORIGIN OF THE GALACTIC DIFFUSE X-RAY EMISSION: IRON K-SHELL LINE DIAGNOSTICS

    Energy Technology Data Exchange (ETDEWEB)

    Nobukawa, Masayoshi [Department of Teacher Training and School Education, Nara University of Education, Takabatake-cho, Nara, 630-8528 (Japan); Uchiyama, Hideki [Faculty of Education, Shizuoka University, 836 Ohya, Suruga-ku, Shizuoka, 422-8529 (Japan); Nobukawa, Kumiko K.; Koyama, Katsuji [Department of Physics, Graduate School of Science, Kyoto University, Kitashirakawa-oiwake-cho, Sakyo-ku, Kyoto, 606-8502 (Japan); Yamauchi, Shigeo, E-mail: nobukawa@nara-edu.ac.jp [Department of Physics, Nara Women’s University, Kitauoyanishimachi, Nara, 630-8506 (Japan)

    2016-12-20

    This paper reports detailed K-shell line profiles of iron (Fe) and nickel (Ni) of the Galactic Center X-ray Emission (GCXE), Galactic Bulge X-ray Emission (GBXE), Galactic Ridge X-ray Emission (GRXE), magnetic Cataclysmic Variables (mCVs), non-magnetic Cataclysmic Variables (non-mCVs), and coronally Active Binaries (ABs). For the study of the origin of the GCXE, GBXE, and GRXE, the spectral analysis is focused on equivalent widths of the Fe i-K α , Fe xxv-He α , and Fe xxvi-Ly α  lines. The global spectrum of the GBXE is reproduced by a combination of the mCVs, non-mCVs, and ABs spectra. On the other hand, the GRXE spectrum shows significant data excesses at the Fe i-K α and Fe xxv-He α  line energies. This means that additional components other than mCVs, non-mCVs, and ABs are required, which have symbiotic phenomena of cold gas and very high-temperature plasma. The GCXE spectrum shows larger excesses than those found in the GRXE spectrum at all the K-shell lines of iron and nickel. Among them the largest ones are the Fe i-K α , Fe xxv-He α , Fe xxvi-Ly α , and Fe xxvi-Ly β  lines. Together with the fact that the scale heights of the Fe i-K α , Fe xxv-He α , and Fe xxvi-Ly α lines are similar to that of the central molecular zone (CMZ), the excess components would be related to high-energy activity in the extreme envelopment of the CMZ.

  9. Radiometric dating and quantitative analysis of elements in depth profiles of sediments by means of nuclear physical as well as X-ray fluorescence and atomic emission spectroscopic methods

    International Nuclear Information System (INIS)

    Schoenburg, M.

    1987-01-01

    The measurement of heavy metal concentration in sediments is of great importance for the assessment of water quality. If dating of the different layers of sediment cores is possible, informations about the history of pollution can be inferred. This paper describes the development and practical test of a procedure suitable for the investigation of sediment cores. Both the element analysis and the dating are based on physical methods. For element concentration determination inductively coupled plasma atomic emission spectrometry (ICP), total-reflection X-ray fluorescence analysis (TXRF) and neutron activation analysis (NAA) are used. The techniques are described and compared. For dating radiometric measurements of 210 Pb and 137 Cs are carried out with a coaxial well-type germanium γ-ray detector in a special low-level arrangement. Results of the systematic investigations are presented and a few individual depth profiles are discussed. (orig.) With 34 figs., 20 tabs [de

  10. Analysis of sculptures using XRF and X-ray radiography

    Science.gov (United States)

    Calza, C.; Oliveira, D. F.; Freitas, R. P.; Rocha, H. S.; Nascimento, J. R.; Lopes, R. T.

    2015-11-01

    This work reports the analysis of two sacred images on polychrome wood using X-ray Radiography and Energy Dispersive X-Ray Fluorescence. The first case is the analysis of a sculpture portraying Saint Sebastian, the patron saint of Rio de Janeiro, which is considered the second most ancient sacred image of Brazil. This sculpture was made in Portugal and was transported to Brazil by Estácio Sá, founder of the city of Rio de Janeiro, in 1565. Nowadays, it is located on the main altar of the Church of Capuchin Friars. The second case is the analysis of a sculpture representing Our Lady of Conception, which is located in the D. João VI Museum (EBA/UFRJ, Rio de Janeiro). The objective of these analyses was to evaluate the general conditions of the sculptures, identifying possible problems and internal damages, areas that revealed signs of previous retouchings and the materials and pigments employed by the artists, in order to assist its restoration procedures. EDXRF measurements were carried out with a portable system, developed at the Nuclear Instrumentation Laboratory, consisting of a Si-PIN XR-100CR detector from Amptek and an Oxford TF3005 X-ray tube with W anode. An X-ray source, a CR System GE CR50P and IP detectors were used to perform the radiographs. The XRF analysis of the sculptures identified the original pigments in both cases and the radiographic images revealed details of the manufacture; restored regions; extensive use of lead white; presence of cracks on the wood; use of nails and spikes, etc.

  11. Structure of polysaccharide and structural analysis by x-ray

    International Nuclear Information System (INIS)

    Yuguchi, Yoshiaki

    2010-01-01

    Polysaccharides occur in plants and the living body in the solid, gel, or liquid. They have a highly structural diversity and possess the potential to be used for development of new materials and energy sources. So it is very important to understand their molecular structure under various conditions. This review introduces the structural characteristics of polysaccharides and the examples of their analysis by the X-ray scattering method. (author)

  12. Scoria analysis by X-ray fluorescence with briquet

    International Nuclear Information System (INIS)

    Silva, G.R. da; Albert, P.E.

    1987-01-01

    The sample of scoria is triturated, using boric acid as agglomerative. The briquets are analyzed by X-ray quantometry, establishing the proportions of SiO 2 , P 2 O 5 , S, Cr 2 O 3 , V 2 O 5 , TiO 2 , Al 2 O 3 , Mg O, Ca O, FeO and their basicity. The calibration curves are prepared with standard scoria samples, by chemical analysis. (C.G.C.) [pt

  13. X-ray powder microdiffraction for routine analysis of paintings

    Czech Academy of Sciences Publication Activity Database

    Šímová, Veronika; Bezdička, Petr; Hradilová, J.; Hradil, David; Grygar, Tomáš

    2005-01-01

    Roč. 20, č. 3 (2005), s. 224-229 ISSN 0885-7156 R&D Projects: GA MŠk(CZ) LN00A028; GA ČR GA203/04/2091; GA AV ČR KJB1032401 Institutional research plan: CEZ:AV0Z40320502 Keywords : powder X-ray microdiffraction * artwork analysis Subject RIV: CA - Inorganic Chemistry Impact factor: 0.483, year: 2005

  14. Plasma heating in solar flares and their soft and hard X-ray emissions

    International Nuclear Information System (INIS)

    Falewicz, R.

    2014-01-01

    In this paper, the energy budgets of two single-loop-like flares observed in X-ray are analyzed under the assumption that nonthermal electrons (NTEs) are the only source of plasma heating during all phases of both events. The flares were observed by RHESSI and GOES on 2002 February 20 and June 2, respectively. Using a one-dimensional (1D) hydrodynamic code for both flares, the energy deposited in the chromosphere was derived applying RHESSI observational data. The use of the Fokker-Planck formalism permits the calculation of distributions of the NTEs in flaring loops and thus spatial distributions of the X-ray nonthermal emissions and integral fluxes for the selected energy ranges that were compared with the observed ones. Additionally, a comparative analysis of the spatial distributions of the signals in the RHESSI images was conducted for the footpoints and for all the flare loops in selected energy ranges with these quantities' fluxes obtained from the models. The best compatibility of the model and observations was obtained for the 2002 June 2 event in the 0.5-4 Å GOES range and total fluxes in the 6-12 keV, 12-25 keV, 20-25 keV, and 50-100 keV energy bands. Results of photometry of the individual flaring structures in a high energy range show that the best compliance occurred for the 2002 June 2 flare, where the synthesized emissions were at least 30% higher than the observed emissions. For the 2002 February 20 flare, synthesized emission is about four times lower than the observed one. However, in the low energy range the best conformity was obtained for the 2002 February 20 flare, where emission from the model is about 11% lower than the observed one. The larger inconsistency occurs for the 2002 June 2 solar flare, where synthesized emission is about 12 times greater or even more than the observed emission. Some part of these differences may be caused by inevitable flaws of the applied methodology, like by an assumption that the model of the flare is

  15. Plasma Heating in Solar Flares and their Soft and Hard X-Ray Emissions

    Science.gov (United States)

    Falewicz, R.

    2014-07-01

    In this paper, the energy budgets of two single-loop-like flares observed in X-ray are analyzed under the assumption that nonthermal electrons (NTEs) are the only source of plasma heating during all phases of both events. The flares were observed by RHESSI and GOES on 2002 February 20 and June 2, respectively. Using a one-dimensional (1D) hydrodynamic code for both flares, the energy deposited in the chromosphere was derived applying RHESSI observational data. The use of the Fokker-Planck formalism permits the calculation of distributions of the NTEs in flaring loops and thus spatial distributions of the X-ray nonthermal emissions and integral fluxes for the selected energy ranges that were compared with the observed ones. Additionally, a comparative analysis of the spatial distributions of the signals in the RHESSI images was conducted for the footpoints and for all the flare loops in selected energy ranges with these quantities' fluxes obtained from the models. The best compatibility of the model and observations was obtained for the 2002 June 2 event in the 0.5-4 Å GOES range and total fluxes in the 6-12 keV, 12-25 keV, 20-25 keV, and 50-100 keV energy bands. Results of photometry of the individual flaring structures in a high energy range show that the best compliance occurred for the 2002 June 2 flare, where the synthesized emissions were at least 30% higher than the observed emissions. For the 2002 February 20 flare, synthesized emission is about four times lower than the observed one. However, in the low energy range the best conformity was obtained for the 2002 February 20 flare, where emission from the model is about 11% lower than the observed one. The larger inconsistency occurs for the 2002 June 2 solar flare, where synthesized emission is about 12 times greater or even more than the observed emission. Some part of these differences may be caused by inevitable flaws of the applied methodology, like by an assumption that the model of the flare is

  16. AN XMM-NEWTON SURVEY OF THE SOFT X-RAY BACKGROUND. III. THE GALACTIC HALO X-RAY EMISSION

    International Nuclear Information System (INIS)

    Henley, David B.; Shelton, Robin L.

    2013-01-01

    We present measurements of the Galactic halo's X-ray emission for 110 XMM-Newton sight lines selected to minimize contamination from solar wind charge exchange emission. We detect emission from few million degree gas on ∼4/5 of our sight lines. The temperature is fairly uniform (median = 2.22 × 10 6 K, interquartile range = 0.63 × 10 6 K), while the emission measure and intrinsic 0.5-2.0 keV surface brightness vary by over an order of magnitude (∼(0.4-7) × 10 –3 cm –6 pc and ∼(0.5-7) × 10 –12 erg cm –2 s –1 deg –2 , respectively, with median detections of 1.9 × 10 –3 cm –6 pc and 1.5 × 10 –12 erg cm –2 s –1 deg –2 , respectively). The high-latitude sky contains a patchy distribution of few million degree gas. This gas exhibits a general increase in emission measure toward the inner Galaxy in the southern Galactic hemisphere. However, there is no tendency for our observed emission measures to decrease with increasing Galactic latitude, contrary to what is expected for a disk-like halo morphology. The measured temperatures, brightnesses, and spatial distributions of the gas can be used to place constraints on models for the dominant heating sources of the halo. We provide some discussion of such heating sources, but defer comparisons between the observations and detailed models to a later paper

  17. Globular clusters as a source of X-ray emission from the neighbourhood of M87

    International Nuclear Information System (INIS)

    Fabian, A.C.; Pringle, J.E.; Rees, M.J.

    1976-01-01

    It is stated that the X-ray emission from globular clusters may be attributable to accretion on to compact objects, the accreting material being supplied from binary companions, or gas trapped in the potential well of the cluster. Counts of objects in the vicinity of the M87 have revealed that it has an extensive halo of globular clusters, the number of which may exceed 10,000 within a radius of 23 arc min. Most of these clusters may be explicable as a population effect, and the similarity of their optical properties to those of cluster in our own Galaxy suggests that they may also contain X-ray sources. The brighter globular clusters in M87 may, however, be substantially more X-ray luminous, and there may be proportionally more gas available in globular clusters in M87 compared with our Galaxy. The average X-ray luminosity of individual globular clusters may be of the order of 10 38 erg/sec., which raises the possibility that the integrated globular cluster emission may account for a substantial fraction of the X-ray emission observed from the region of M87. In support of this it is noted that the extended X-ray emission from the Virgo cluster is centered on M87, which lies approximately 45 arc min from the cluster centroid, and it is expected that the general X-ray emission from the globular cluster will appear to be smoothly and symmetrically distributed about M87 at moderate spatial resolution. A similar situation may apply to the elliptical galaxy NGC 3311 in Abell 1060 which, as a cluster, has been suggested as the identification for the X-ray source 3 U 1044-40, and it seems possible that that galaxy is surrounded by a similar globular cluster population to that of M87. (U.K.)

  18. CIAO: CHANDRA/X-RAY DATA ANALYSIS FOR EVERYONE

    Science.gov (United States)

    McDowell, Jonathan; CIAO Team

    2018-01-01

    Eighteen years after the launch of Chandra, the archive is full of scientifically rich data and new observations continue. Improvements in recent years to the data analysis package CIAO (Chandra Interactive Analysis of Observations) and its extensive accompanying documentation make it easier for astronomers without a specialist background in high energy astrophysics to take advantage of this resource.The CXC supports hundreds of CIAO users around the world at all levels of training from high school and undergraduate students to the most experienced X-ray astronomers. In general, we strive to provide a software system which is easy for beginners, yet powerful for advanced users.Chandra data cover a range of instrument configurations and types of target (pointlike, extended and moving), requiring a flexible data analysis system. In addition to CIAO tools using the familiar FTOOLS/IRAF-style parameter interface, CIAO includes applications such as the Sherpa fitting engine which provide access to the data via Python scripting.In this poster we point prospective (and existing!) users to the high level Python scripts now provided to reprocess Chandra or other X-ray mission data, determine source fluxes and upper limits, and estimate backgrounds; and to the latest documentation including the CIAO Gallery, a new entry point featuring the system's different capabilities.This work has been supported by NASA under contract NAS 8-03060 to the Smithsonian Astrophysical Observatory for operation of the Chandra X-ray Center.

  19. Electronic structure of human hemoglobin: ultrasoft X-ray emission study

    International Nuclear Information System (INIS)

    Soldatov, A.V.; Kravtsova, A.N.; Fedorovich, E.N.; Kurmaev, E.Z.; Moewes, A.

    2004-01-01

    Full text: The iron L 2,3 and carbon, nitrogen and oxygen Kα X-ray emission spectra (XES) of human hemoglobin have been recorded at the soft X-ray spectroscopy endstation on Undulator Beam line 8.0 at Advanced Light Source (ALS) located at the Lawrence Berkeley National Laboratory. The theoretical calculations of Fe L 3 -XES have been performed using ab initio code FEFF8.2. The calculations have been carried out for the structure of hemoglobin presented in PDB (entry 3HHB) as well as for the molecule with symmetrical heme plane. It was found that the Fe L 3 emission spectrum calculated for the ideal molecule agrees slightly better with the experiment as compared with those calculated for the real molecule. Thus, one can use the structure of the ideal molecule for theoretical Fe L 3 -XES simulations. The theoretical analysis has shown that the fist peak of experimental Fe L 3 - emission spectrum is enhanced by the nearest nitrogen atoms lying in heme plane around the central iron atom. The theoretical C K- and N K-XES spectra of hemoglobin have been calculated. A good agreement between theoretical and experimental spectra has been obtained. The distribution of the partial electronic densities of states in the valence and conduction bands of hemoglobin has been determined

  20. Measurement of X-ray emission efficiency for K-lines.

    Science.gov (United States)

    Procop, M

    2004-08-01

    Results for the X-ray emission efficiency (counts per C per sr) of K-lines for selected elements (C, Al, Si, Ti, Cu, Ge) and for the first time also for compounds and alloys (SiC, GaP, AlCu, TiAlC) are presented. An energy dispersive X-ray spectrometer (EDS) of known detection efficiency (counts per photon) has been used to record the spectra at a takeoff angle of 25 degrees determined by the geometry of the secondary electron microscope's specimen chamber. Overall uncertainty in measurement could be reduced to 5 to 10% in dependence on the line intensity and energy. Measured emission efficiencies have been compared with calculated efficiencies based on models applied in standardless analysis. The widespread XPP and PROZA models give somewhat too low emission efficiencies. The best agreement between measured and calculated efficiencies could be achieved by replacing in the modular PROZA96 model the original expression for the ionization cross section by the formula given by Casnati et al. (1982) A discrepancy remains for carbon, probably due to the high overvoltage ratio.

  1. Ultra fast atomic process in X-ray emission by inner-shell ionization

    Energy Technology Data Exchange (ETDEWEB)

    Moribayashi, Kengo; Sasaki, Akira [Japan Atomic Energy Research Inst., Neyagawa, Osaka (Japan). Kansai Research Establishment; Tajima, T

    1998-03-01

    An ultra-fast atomic process together with X-ray emission by inner-shell ionization using high intensity (10{sup 18} W/cm{sup 2}) short pulse (20fs) X-ray is studied. A new class of experiment is proposed and a useful pumping source is suggested. In this method, it is found that the gain value of X-ray laser amounts to larger than 1000(1/cm) with use of the density of 10{sup 22}/cm{sup 3} of carbon atom. Electron impact ionization effect and initial density effect as well as intensity of pumping source effect are also discussed. (author)

  2. Time correlation between plasma behaviour and soft x-ray emission in a plasma focus

    International Nuclear Information System (INIS)

    Hirano, Katsumi; Tagaya, Yutaka; Shimoda, Katsuji; Okabe, Yushiro; Yamamoto, Toshikazu

    1986-01-01

    Soft X-rays emitted from a plasma focus are investigated experimentally. In contrast to single-pulsive burst of neutron, hard X-rays, ion- and electron beams, the soft X-rays are observed from the collapse phase to the decay phase of the plasma column, and have typically three successive peaks in its signal. Each peak corresponds to the maximum compression, the disruption and the decay phase of plasma column. It is revealed that the first and the second peaks are radiated by plasma itself, whereas the third peak is caused by emission from the inner electrode face. (author)

  3. Analysis of fresco paintings by X-ray fluorescence method

    International Nuclear Information System (INIS)

    Cechak, T.; Gerndt, J.; Musilek, L.; Kopecka, I.

    2000-01-01

    In this work we present the application of X-ray fluorescence analysis (XRFA) to examine fresco paintings from the Karlstejn castle. The X-ray fluorescence apparatus built and operated in the Laboratory of Quantitative Methods in Research of Ancient Monuments was used for the purpose of fresco paintings measurements. The X-ray sources (radionuclides) generate the characteristic X-ray photons from the sample. The Si(Li) detector measures numbers and energies of photons emitted from the specimen. The energy and number of photons detected can be converted into kind and amount of measured atoms. These results give data for qualitative and quantitative analysis of samples. XRFA is relatively simple and non-destructive method. Capability of in-situ measurement is one of big advantages of this method. The radionuclide sources of exciting radiation (e.g. 55 Fe enables the excitation of elements with Z up to 23, 238 Pu is used in interval of Z from 20 to 39 etc.) were used. An Si(Li) semiconductor detector with a 5 l Dewar vessel and portable spectroscopy system enable the in situ measurement. Narrow collimation of the exciting beam makes it possible to select the measured area of fresco painting. The valuable fresco paintings from the Karlstejn castle were investigated in this way. The measurements were carried out in collaboration with the Analytical Laboratory of the State Institute for the Preservation of Historic Monuments. A suitable analysis of paintings makes it possible to detect the kind of colours and evaluate changes in the surface colour of paintings and suggest useful and timely procedures for their conservation and restoration. (author)

  4. X-ray emission in collisions of highly charged I, Pr, Ho, and Bi ions with a W surface

    International Nuclear Information System (INIS)

    Watanabe, H.; Tona, M.; Ohtani, S.; Sun, J.; Nakamura, N.; Yamada, C.; Yoshiyasu, N.; Sakurai, M.

    2007-01-01

    X-ray emission yields, which are defined as the total number of emitted x-ray photons per incident ion, and dissipated fractions of potential energies through x-ray emission have been measured for slow highly charged ions of I, Pr, Ho, and Bi colliding with a W surface. A larger amount of potential energy was consumed for the x-ray emission with increasing the atomic number and the charge state. The present measurements show that x-ray emission is one of the main decay channels of hollow atoms produced in collisions of very highly charged ions of heavy elements

  5. Gaseous detectors for energy dispersive X-ray fluorescence analysis

    Science.gov (United States)

    Veloso, J. F. C. A.; Silva, A. L. M.

    2018-01-01

    The energy resolution capability of gaseous detectors is being used in the last years to perform studies on the detection of characteristic X-ray lines emitted by elements when excited by external radiation sources. One of the most successful techniques is the Energy Dispersive X-ray Fluorescence (EDXRF) analysis. Recent developments in the new generation of micropatterned gaseous detectors (MPGDs), triggered the possibility not only of recording the photon energy, but also of providing position information, extending their application to EDXRF imaging. The relevant features and strategies to be applied in gaseous detectors in order to better fit the requirements for EDXRF imaging will be reviewed and discussed, and some application examples will be presented.

  6. Crystal quality analysis and improvement using x-ray topography

    International Nuclear Information System (INIS)

    Maj, J.; Goetze, K.; Macrander, A.; Zhong, Y.; Huang, X.; Maj, L.

    2008-01-01

    The Topography X-ray Laboratory of the Advanced Photon Source (APS) at Argonne National Laboratory operates as a collaborative effort with APS users to produce high performance crystals for APS X-ray beamline experiments. For many years the topography laboratory has worked closely with an on-site optics shop to help ensure the production of crystals with the highest quality, most stress-free surface finish possible. It has been instrumental in evaluating and refining methods used to produce high quality crystals. Topographical analysis has shown to be an effective method to quantify and determine the distribution of stresses, to help identify methods that would mitigate the stresses and improve the Rocking curve, and to create CCD images of the crystal. This paper describes the topography process and offers methods for reducing crystal stresses in order to substantially improve the crystal optics.

  7. Microbeam X-ray analysis in Poland - past and future

    International Nuclear Information System (INIS)

    Kusinski, J

    2010-01-01

    The article provides an overview of the development of electron beam X-ray microanalysis (EPMA) in Poland. Since the introduction by Prof. Bojarski of EMPA over 45 years ago, tremendous advances in methodologies and in instrumentation have been made in order to improve the precision of quantitative compositional analysis, spatial resolution and analytical sensitivity. This was possible due to the activity of Applied Crystallography Committee at the Polish Academy of Sciences, as well as the groups of researches working in the Institute for Ferrous Metallurgy (Gliwice), the Technical University of Warsaw, the Silesian Technical University (Katowice), the AGH-University of Sciences and Technology (Krakow), and the Institute of Materials Science and Metallurgy Polish Academy of Sciences (Krakow). Based on the research examples realized by these teams, conferences, seminars and congresses organized, as well as books and academic textbooks issued, the evolution of electron beam X-ray microanalysis in Poland is demonstrated.

  8. Extended hard-X-ray emission in the inner few parsecs of the Galaxy

    DEFF Research Database (Denmark)

    Perez, Kerstin; Hailey, Charles J.; Bauer, Franz E.

    2015-01-01

    of objects emitting soft X-rays (less than 10 kiloelectronvolts) within the surrounding hundreds of parsecs, as well as the population responsible for unresolved X-ray emission extending along the Galactic plane, is dominated by accreting white dwarf systems. Observations of diffuse hard-X-ray (more than 10...... kiloelectronvolts) emission in the inner 10 parsecs, however, have been hampered by the limited spatial resolution of previous instruments. Here we report the presence of a distinct hard-X-ray component within the central 4 × 8 parsecs, as revealed by subarcminute-resolution images in the 20-40 kiloelectronvolt...... outflows interacting with the surrounding radiation field, dense molecular material or magnetic fields. However, all these interpretations pose significant challenges to our understanding of stellar evolution, binary formation, and cosmic-ray production in the Galactic Centre....

  9. Electron and photon emissions from gold nanoparticles irradiated by X-ray photons

    Energy Technology Data Exchange (ETDEWEB)

    Casta, R., E-mail: castaromain@gmail.com, E-mail: romain.casta@irsamc.ups-tlse.fr; Champeaux, J.-P.; Moretto-Capelle, P.; Sence, M.; Cafarelli, P. [Université de Toulouse, UPS, Laboratoire Collisions Agrégats Réactivité, IRSAMC, CNRS, UMR 5589 (France)

    2015-01-15

    In this paper, we develop a totally new probabilistic model for the electron and photon emission of gold nanoparticles irradiated by X-ray photons. This model allows direct applications to recent researches about the radiotherapy enhancement by gold nanoparticles in the context of cancer treatment. Our model uses, in a complete original way, simulated Auger cascade and stopping power to compute electron emission spectra, photon emission spectra and released energy inside the material of gold nanoparticles. It allows us to present new results about the electron and photon emission of gold nanoparticle irradiated by hard X-rays.

  10. THERMAL X-RAY EMISSION FROM THE SHOCKED STELLAR WIND OF PULSAR GAMMA-RAY BINARIES

    Energy Technology Data Exchange (ETDEWEB)

    Zabalza, V.; Paredes, J. M. [Departament d' Astronomia i Meteorologia, Institut de Ciencies del Cosmos (ICC), Universitat de Barcelona (IEEC-UB), Marti i Franques 1, E08028 Barcelona (Spain); Bosch-Ramon, V., E-mail: vzabalza@am.ub.es [Dublin Institute for Advanced Studies, 31 Fitzwilliam Place, Dublin 2 (Ireland)

    2011-12-10

    Gamma-ray-loud X-ray binaries are binary systems that show non-thermal broadband emission from radio to gamma rays. If the system comprises a massive star and a young non-accreting pulsar, their winds will collide producing broadband non-thermal emission, most likely originated in the shocked pulsar wind. Thermal X-ray emission is expected from the shocked stellar wind, but until now it has neither been detected nor studied in the context of gamma-ray binaries. We present a semi-analytic model of the thermal X-ray emission from the shocked stellar wind in pulsar gamma-ray binaries, and find that the thermal X-ray emission increases monotonically with the pulsar spin-down luminosity, reaching luminosities of the order of 10{sup 33} erg s{sup -1}. The lack of thermal features in the X-ray spectrum of gamma-ray binaries can then be used to constrain the properties of the pulsar and stellar winds. By fitting the observed X-ray spectra of gamma-ray binaries with a source model composed of an absorbed non-thermal power law and the computed thermal X-ray emission, we are able to derive upper limits on the spin-down luminosity of the putative pulsar. We applied this method to LS 5039, the only gamma-ray binary with a radial, powerful wind, and obtain an upper limit on the pulsar spin-down luminosity of {approx}6 Multiplication-Sign 10{sup 36} erg s{sup -1}. Given the energetic constraints from its high-energy gamma-ray emission, a non-thermal to spin-down luminosity ratio very close to unity may be required.

  11. Some implications of excess soft X-ray emission from Seyfert 1 galaxies

    International Nuclear Information System (INIS)

    Fabian, A.C.; Guilbert, P.W.; Arnaud, K.A.; Shafer, R.A.; Tennant, A.F.; Ward, M.J.

    1986-01-01

    The X-ray spectrum of Seyfert 1 galaxies is characterized by a hard power-law spectrum. It is often postulated that this maintains a Compton-heated two-phase Broad-Line Region (BLR) around the central source. It is shown here that the strong excess soft X-ray emission observed in MKN 841 and other Seyfert galaxies invalidates this model if the BLR is spherically symmetric. Alternatives are proposed. (author)

  12. X-Ray Emission from Active Galactic Nuclei with Intermediate-Mass Black Holes

    Science.gov (United States)

    Dewangan, G. C.; Mathur, S.; Griffiths, R. E.; Rao, A. R.

    2008-12-01

    We present a systematic X-ray study of eight active galactic nuclei (AGNs) with intermediate-mass black holes (MBH ~ 8-95 × 104 M⊙) based on 12 XMM-Newton observations. The sample includes the two prototype AGNs in this class—NGC 4395 and POX 52 and six other AGNs discovered with the Sloan Digitized Sky Survey. These AGNs show some of the strongest X-ray variability, with the normalized excess variances being the largest and the power density break timescales being the shortest observed among radio-quiet AGNs. The excess-variance-luminosity correlation appears to depend on both the BH mass and the Eddington luminosity ratio. The break timescale-black hole mass relations for AGN with IMBHs are consistent with that observed for massive AGNs. We find that the FWHM of the Hβ/Hα line is uncorrelated with the BH mass, but shows strong anticorrelation with the Eddington luminosity ratio. Four AGNs show clear evidence for soft X-ray excess emission (kTin ~ 150-200 eV). X-ray spectra of three other AGNs are consistent with the presence of the soft excess emission. NGC 4395 with lowest L/LEdd lacks the soft excess emission. Evidently small black mass is not the primary driver of strong soft X-ray excess emission from AGNs. The X-ray spectral properties and optical-to-X-ray spectral energy distributions of these AGNs are similar to those of Seyfert 1 galaxies. The observed X-ray/UV properties of AGNs with IMBHs are consistent with these AGNs being low-mass extensions of more massive AGNs, those with high Eddington luminosity ratio looking more like narrow-line Seyfert 1 s and those with low L/LEdd looking more like broad-line Seyfert 1 galaxies.

  13. X-ray analysis and mapping by wavelength dispersive X-ray spectroscopy in an electron microscope

    International Nuclear Information System (INIS)

    Tanaka, Miyoko; Takeguchi, Masaki; Furuya, Kazuo

    2008-01-01

    A compact and easy-to-use wavelength dispersive X-ray spectrometer using a multi-capillary X-ray lens attached to a scanning (transmission) electron microscope has been tested for thin-film analysis. B-K spectra from thin-film boron compounds (B 4 C, h-BN, and B 2 O 3 ) samples showed prominent peak shifts and detailed structural differences. Mapping images of a thin W/Si double-layer sample resolved each element clearly. Additionally, a thin SiO 2 film grown on a Si substrate was imaged with O-K X-rays. Energy and spatial resolution of the system is also discussed

  14. OSO-8 soft X-ray wheel experiment: Data analysis

    Science.gov (United States)

    Kraushaar, W. L.

    1982-01-01

    The soft X-ray experiment hardware and its operation are described. The device included six X-ray proportional counters, two of which, numbers 1 and 4, were pressurized with on-board methane gas supplies. Number 4 developed an excessive leak rate early in the mission and was turned off on 1975 day number 282 except for brief (typically 2-hour) periods up to day 585 after which it as left off. Counter 1 worked satisfactorily until 1975 day number 1095 (January 1, 1978) at which time the on-board methane supply was depleted. The other four counters were sealed and all except number 3 worked satisfactorily throughout the mission which terminated with permanent satellie shut-down on day 1369. This was the first large area thin-window, gas-flow X-ray detector to be flown in orbit. The background problems were severe and consumed a very large portion of the data analysis effort. These background problems were associated with the Earth's trapped electron belts.

  15. Spectral modeling of the charge-exchange X-ray emission from M82

    Energy Technology Data Exchange (ETDEWEB)

    Zhang, Shuinai; Ji, Li; Zhou, Xin [Purple Mountain Observatory, CAS, Nanjing 210008 (China); Wang, Q. Daniel [Astronomy Department, University of Massachusetts, Amherst, MA 01003 (United States); Smith, Randall K.; Foster, Adam R., E-mail: snzhang@pmo.ac.cn [Harvard-Smithsonian Center for Astrophysics, Cambridge, MA 02138 (United States)

    2014-10-10

    It has been proposed that the charge-exchange (CX) process at the interface between hot and cool interstellar gases could contribute significantly to the observed soft X-ray emission in star-forming galaxies. We analyze the XMM-Newton/reflection grating spectrometer (RGS) spectrum of M82 using a newly developed CX model combined with a single-temperature thermal plasma to characterize the volume-filling hot gas. The CX process is largely responsible for not only the strongly enhanced forbidden lines of the Kα triplets of various He-like ions but also good fractions of the Lyα transitions of C VI (∼87%), O VIII, and N VII (≳50%) as well. In total about a quarter of the X-ray flux in the RGS 6-30 Å band originates in the CX. We infer an ion incident rate of 3 × 10{sup 51} s{sup –1} undergoing CX at the hot and cool gas interface and an effective area of the interface of ∼2 × 10{sup 45} cm{sup 2} that is one order of magnitude larger than the cross section of the global biconic outflow. With the CX contribution accounted for, the best-fit temperature of the hot gas is 0.6 keV, and the metal abundances are approximately solar. We further show that the same CX/thermal plasma model also gives an excellent description of the EPIC-pn spectrum of the outflow Cap, projected at 11.6 kpc away from the galactic disk of M82. This analysis demonstrates that the CX is potentially an important contributor to the X-ray emission from starburst galaxies and also an invaluable tool to probe the interface astrophysics.

  16. X-Ray Emission from a Merger Remnant, NGC 7252 (the ``Atoms-for-Peace'' Galaxy)

    Science.gov (United States)

    Awaki, Hisamitsu; Matsumoto, Hironori; Tomida, Hiroshi

    2002-03-01

    We observed a nearby merger remnant NGC 7252 with the X-ray satellite ASCA and detected X-ray emission with the X-ray flux of (1.8+/-0.3)×10-13 ergs s-1 cm-2 in the 0.5-10 keV band. This corresponds to the X-ray luminosity of 8.1×1040 ergs s-1. The X-ray emission is well described with a two-component model: a soft component with kT=0.72+/-0.13 keV and a hard component with kT>5.1 keV. Although NGC 7252 is referred to as a dynamically young protoelliptical, the 0.5-4 keV luminosity of the soft component is about 2×1040 ergs s-1, which is low for an early-type galaxy. The ratio of LX/LFIR suggests that the soft component originated from the hot gas due to star formation. Its low luminosity can be explained by the gas ejection from the galaxy as galaxy winds. Our observation reveals the existence of hard X-ray emission with the 2-10 keV luminosity of 5.6×1040 ergs s-1. This may indicate the existence of nuclear activity or an intermediate-mass black hole in NGC 7252.

  17. Application of energy dispersive x-ray techniques for water analysis

    International Nuclear Information System (INIS)

    Funtua, I. I.

    2000-07-01

    Energy dispersive x-ray fluorescence (EDXRF) is a class of emission spectroscopic techniques that depends upon the emission of characteristic x-rays following excitation of the atomic electron energy levels by tube or isotopic source x-rays. The technique has found wide range of applications that include determination of chemical elements of water and water pollutants. Three EDXRF systems, the isotopic source, secondary target and total reflection (TXRF) are available at the Centre for Energy research and Training. These systems have been applied for the analysis of sediments, suspensions, ground water, river and rainwater. The isotopic source is based on 55 Fe, 109 Cd and 241 Am excitations while the secondary target and the total reflection are utilizing a Mo x-ray tube. Sample preparation requirements for water analysis range from physical and chemical pre-concentration steps to direct analysis and elements from Al to U can be determined with these systems. The EDXRF techniques, TXRF in particular with its multielement capability, low detection limit and possibility of direct analysis for water have competitive edge over the traditional methods of atomic absorption and flame photometry

  18. X-ray emission on hybird stars: ROSAT observations of alpha Trianguli Australis and iota Aurigae

    Science.gov (United States)

    Kashyap, V.; Rosner, R.; Harnden, F. R., Jr.; Maggio, A.; Micela, G.; Sciortino, S.

    1994-01-01

    We report on deep ROSAT observations of two Hybrid atmosphere stars, alpha TrA and iota Aur, and our analysis of these observations. We detect high-energy transient phenomena on alpha TrA and consider the implications of this discovery to the atmospheres of Hybrid stars. We detect iota Aur in the high-energy passband of ROSAT, implying the existence of multimillion degree plasma on the star. Our major results include the following: discovery of two large flare events, detected during pointed observations of alpha TrA; the demonstration that the flare emission most likely comes from the giant itself, rather than from a previously unseen low-mass companion star; the demonstration that the plasma characteristics associated with the flares and with the 'quiescent' component are essentially indistinguishable; and that the geometric dimensions of the emitting plasma are considerably smaller than the critical dimension characterizing stable 'hot' coronal loop structures. Our results suggest that alpha TrA does not have any steady X-ray emission consistent with theoretical expectations, and support the argument that Hybrid stars constitute a transitional type of object in which large-scale magnetic dynamo activity ceases, and the dominant spatial scales characterizing coronal structure rapidly decline as such stars evolve across the X-ray 'Dividing Line' in the H-R diagram.

  19. Applications of X-ray Computed Tomography and Emission Computed Tomography

    International Nuclear Information System (INIS)

    Seletchi, Emilia Dana; Sutac, Victor

    2005-01-01

    Computed Tomography is a non-destructive imaging method that allows visualization of internal features within non-transparent objects such as sedimentary rocks. Filtering techniques have been applied to circumvent the artifacts and achieve high-quality images for quantitative analysis. High-resolution X-ray computed tomography (HRXCT) can be used to identify the position of the growth axis in speleothems by detecting subtle changes in calcite density between growth bands. HRXCT imagery reveals the three-dimensional variability of coral banding providing information on coral growth and climate over the past several centuries. The Nuclear Medicine imaging technique uses a radioactive tracer, several radiation detectors, and sophisticated computer technologies to understand the biochemical basis of normal and abnormal functions within the brain. The goal of Emission Computed Tomography (ECT) is to accurately determine the three-dimensional radioactivity distribution resulting from the radiopharmaceutical uptake inside the patient instead of the attenuation coefficient distribution from different tissues as obtained from X-ray Computer Tomography. ECT is a very useful tool for investigating the cognitive functions. Because of the low radiation doses associated with Positron Emission Tomography (PET), this technique has been applied in clinical research, allowing the direct study of human neurological diseases. (authors)

  20. Cross section for induced L X-ray emission by protons of energy <400 keV

    International Nuclear Information System (INIS)

    Mohan, Harsh; Jain, Arvind Kumar; Kaur, Mandeep; Singh, Parjit S.; Sharma, Sunita

    2014-01-01

    In performing ion beam analysis, cross section for induced L X-ray emission plays a crucial role. There are different approaches by which these can be found experimentally or can be calculated theoretically based on various models. L X-ray production cross sections for Bi with protons in the energy range 260–400 keV at the interval of 20 keV are measured. These are compared with calculations obtained on the basis of current prevailing theories ECPSSR and ECPSSR-UA. Their importance in understanding this phenomenon and existing arguments in this regard will be highlighted

  1. Microwave and X-Ray emission during a isentropic expansion and its application to solar bursts

    International Nuclear Information System (INIS)

    Piazza, L.R.

    1983-01-01

    The gyro-synchrotron emission in microwaves and the free-free emission in X-rays of a plasma enclosed in a cylinder coincident with a magnetic force tube were calculated for an isentropic self-similar expansion, with plane and cylindrical symmetries. This expansion model was applied to a region of the low solar corona, and the results were compared to the emission observed in some simple solar events of low intensity. The calculations show satisfactory coincidence with the events in X-rays for energies around 10 29 ergs. The solar events analyzed in microwaves, which are not the same that were studied in X-rays, in general do not fit the theoretical results. The origin of the discrepancy is probably the formulation of the processes of emission applied to the expansion. (Author) [pt

  2. Spectral and Temporal Properties of the Ultra-Luminous X-Ray Pulsar in M82 from 15 Years of Chandra Observations and Analysis of the Pulsed Emission Using NuSTAR

    Science.gov (United States)

    Brightman, Murray; Harrison, Fiona; Walton, Dominic J.; Fuerst, Felis; Zezas, Andreas; Bachetti, Matteo; Grefenstette, Brian; Ptak, Andrew; Tendulkar, Shriharsh; Yukita, Mihoko

    2016-01-01

    The recent discovery by Bachetti et al. of a pulsar in M82 that can reach luminosities of up to 10(exp 40) erg s(exp -1), a factor of approximately 100 times the Eddington luminosity for a 1.4 solar mass compact object, poses a challenge for accretion physics. In order to better understand the nature of this source and its duty cycle, and in light of several physical models that have been subsequently published, we conduct a spectral and temporal analysis of the 0.58 keV X-ray emission from this source from 15 years of Chandra observations. We analyze 19 ACIS observations where the point-spread function (PSF) of the pulsar is not contaminated by nearby sources. We fit the Chandra spectra of the pulsar with a power-law model and a disk blackbody model, subjected to interstellar absorption in M82. We carefully assess for the effect of pile-up in our observations, where four observations have a pile-up fraction of 10, which we account for during spectral modeling with a convolution model. When fitted with a power-law model, the average photon index when the source is at high luminosity (LX greater than 10(exp 39) erg s(exp -1) is equal to gamma 1.33 +/-.0.15. For the disk blackbody model, the average temperature is T(sub in) 3.24 +/- 0.65 keV, the spectral shape being consistent with other luminous X-ray pulsars. We also investigated the inclusion of a soft excess component and spectral break, finding that the spectra are also consistent with these features common to luminous X-ray pulsars. In addition, we present spectral analysis from NuSTAR over the 3-50 keV range where we have isolated the pulsed component. We find that the pulsed emission in this band is best fit by a power-law with a high-energy cutoff, where gamma is equal to 0.6 +/- 0.3 and E(sub C) is equal to 14(exp +5) (sub -3)) keV. While the pulsar has previously been identified as a transient, we find from our longer-baseline study that it has been remarkably active over the 15-year period, where for 9

  3. Hard x ray imaging and the relative contribution of thermal and nonthermal emission in flares

    International Nuclear Information System (INIS)

    Holman, G.D.

    1986-01-01

    The question of whether the impulsive 25 to 100 keV x ray emission from solar flares is thermal or nonthermal has been a long-standing controversy. Both thermal and nonthermal (beam) models have been developed and applied to the hard x ray data. It now seems likely that both thermal and nonthermal emission have been observed at hard x ray energies. The Hinotori classification scheme, for example, is an attempt to associate the thermal-nonthermal characteristics of flare hard x ray emission with other flare properties. From a theoretical point of view, it is difficult to generate energetic, nonthermal electrons without dumping an equal or greater amount of energy into plasma heating. On the other hand, any impulsive heating process will invariably generate at least some nonthermal particles. Hence, strictly speaking, although thermal or nonthermal emission may dominate the hard x ray emission in a given energy range for a given flare, there is no such thing as a purely thermal or nonthermal flare mechanism

  4. Lifetime-vibrational interference effects in resonantly excited x-ray emission spectra of CO

    Energy Technology Data Exchange (ETDEWEB)

    Skytt, P.; Glans, P.; Gunnelin, K. [Uppsala Univ. (Sweden)] [and others

    1997-04-01

    The parity selection rule for resonant X-ray emission as demonstrated for O{sub 2} and N{sub 2} can be seen as an effect of interference between coherently excited degenerate localized core states. One system where the core state degeneracy is not exact but somewhat lifted was previously studied at ALS, namely the resonant X-ray emission of amino-substituted benzene (aniline). It was shown that the X-ray fluorescence spectrum resulting from excitation of the C1s at the site of the {open_quotes}aminocarbon{close_quotes} could be described in a picture separating the excitation and the emission processes, whereas the spectrum corresponding to the quasi-degenerate carbons could not. Thus, in this case it was necessary to take interference effects between the quasi-degenerate intermediate core excited states into account in order to obtain agreement between calculations and experiment. The different vibrational levels of core excited states in molecules have energy splittings which are of the same order of magnitude as the natural lifetime broadening of core excitations in the soft X-ray range. Therefore, lifetime-vibrational interference effects are likely to appear and influence the band shapes in resonant X-ray emission spectra. Lifetime-vibrational interference has been studied in non-resonant X-ray emission, and in Auger spectra. In this report the authors discuss results of selectively excited soft X-ray fluorescence spectra of molecules, where they focus on lifetime-interference effects appearing in the band shapes.

  5. X-ray-based attenuation correction for positron emission tomography/computed tomography scanners.

    Science.gov (United States)

    Kinahan, Paul E; Hasegawa, Bruce H; Beyer, Thomas

    2003-07-01

    A synergy of positron emission tomography (PET)/computed tomography (CT) scanners is the use of the CT data for x-ray-based attenuation correction of the PET emission data. Current methods of measuring transmission use positron sources, gamma-ray sources, or x-ray sources. Each of the types of transmission scans involves different trade-offs of noise versus bias, with positron transmission scans having the highest noise but lowest bias, whereas x-ray scans have negligible noise but the potential for increased quantitative errors. The use of x-ray-based attenuation correction, however, has other advantages, including a lack of bias introduced from post-injection transmission scanning, which is an important practical consideration for clinical scanners, as well as reduced scan times. The sensitivity of x-ray-based attenuation correction to artifacts and quantitative errors depends on the method of translating the CT image from the effective x-ray energy of approximately 70 keV to attenuation coefficients at the PET energy of 511 keV. These translation methods are usually based on segmentation and/or scaling techniques. Errors in the PET emission image arise from positional mismatches caused by patient motion or respiration differences between the PET and CT scans; incorrect calculation of attenuation coefficients for CT contrast agents or metallic implants; or keeping the patient's arms in the field of view, which leads to truncation and/or beam-hardening (or x-ray scatter) artifacts. Proper interpretation of PET emission images corrected for attenuation by using the CT image relies on an understanding of the potential artifacts. In cases where an artifact or bias is suspected, careful inspection of all three available images (CT and PET emission with and without attenuation correction) is recommended. Copyright 2003 Elsevier Inc. All rights reserved.

  6. THE CHANDRA SURVEY OF EXTRAGALACTIC SOURCES IN THE 3CR CATALOG: X-RAY EMISSION FROM NUCLEI, JETS, AND HOTSPOTS IN THE CHANDRA ARCHIVAL OBSERVATIONS

    Energy Technology Data Exchange (ETDEWEB)

    Massaro, F. [Dipartimento di Fisica, Università degli Studi di Torino, via Pietro Giuria 1, I-10125 Torino (Italy); Harris, D. E.; Paggi, A.; Wilkes, B. J.; Kuraszkiewicz, J. [Smithsonian Astrophysical Observatory, 60 Garden Street, Cambridge, MA 02138 (United States); Liuzzo, E.; Orienti, M.; Paladino, R. [Istituto di Radioastronomia, INAF, via Gobetti 101, I-40129, Bologna (Italy); Tremblay, G. R. [Yale Center for Astronomy and Astrophysics, Physics Department, Yale University, P.O. Box 208120, New Haven, CT 06520-8120 (United States); Baum, S. A.; O’Dea, C. P. [University of Manitoba, Dept of Physics and Astronomy, Winnipeg, MB R3T 2N2 (Canada)

    2015-09-15

    As part of our program to build a complete radio and X-ray database of all Third Cambridge catalog extragalactic radio sources, we present an analysis of 93 sources for which Chandra archival data are available. Most of these sources have already been published. Here we provide a uniform re-analysis and present nuclear X-ray fluxes and X-ray emission associated with radio jet knots and hotspots using both publicly available radio images and new radio images that have been constructed from data available in the Very Large Array archive. For about 1/3 of the sources in the selected sample, a comparison between the Chandra and radio observations was not reported in the literature: we find X-ray detections of 2 new radio jet knots and 17 hotspots. We also report the X-ray detection of extended emission from the intergalactic medium for 15 galaxy clusters.

  7. X ray emission: a tool and a probe for laser - clusters interaction

    International Nuclear Information System (INIS)

    Prigent, Ch.

    2004-12-01

    In intense laser-cluster interaction, the experimental results show a strong energetic coupling between radiation and matter. We have measured absolute X-ray yields and charge state distributions under well control conditions as a function of physical parameters governing the interaction; namely laser intensity, pulse duration, wavelength or polarization state of the laser light, the size and the species of the clusters (Ar, Kr, Xe). We have highlighted, for the first time, an intensity threshold in the X-ray production very low (∼ 2.10 14 W/cm 2 for a pulse duration of 300 fs) which can results from an effect of the dynamical polarisation of clusters in an intense electric field. A weak dependence with the wavelength (400 nm / 800 nm) on the absolute X-ray yields has been found. Moreover, we have observed a saturation of the X-ray emission probability below a critical cluster size. (author)

  8. Magnetar-like X-Ray Bursts Suppress Pulsar Radio Emission

    Energy Technology Data Exchange (ETDEWEB)

    Archibald, R. F.; Lyutikov, M.; Kaspi, V. M.; Tendulkar, S. P. [Department of Physics and McGill Space Institute, McGill University, 3600 University Street, Montreal, QC H3A 2T8 (Canada); Burgay, M.; Possenti, A. [INAF–Osservatorio Astronomico di Cagliari, Via della Scienza 5, I-09047 Selargius (Italy); Esposito, P.; Rea, N. [Anton Pannekoek Institute for Astronomy, University of Amsterdam, Postbus 94249, 1090 GE Amsterdam (Netherlands); Israel, G. [INAF–Osservatorio Astronomico di Roma, via Frascati 33, I-00040 Monteporzio Catone, Roma (Italy); Kerr, M. [Space Science Division, Naval Research Laboratory, Washington, DC 20375-5352 (United States); Sarkissian, J. [CSIRO Astronomy and Space Science, Parkes Observatory, P.O. Box 276, Parkes, NSW 2870 (Australia); Scholz, P., E-mail: archibald@astro.utoronto.ca [National Research Council of Canada, Herzberg Astronomy and Astrophysics, Dominion Radio Astrophysical Observatory, P.O. Box 248, Penticton, BC V2A 6J9 (Canada)

    2017-11-10

    Rotation-powered pulsars and magnetars are two different observational manifestations of neutron stars: rotation-powered pulsars are rapidly spinning objects that are mostly observed as pulsating radio sources, while magnetars, neutron stars with the highest known magnetic fields, often emit short-duration X-ray bursts. Here, we report simultaneous observations of the high-magnetic-field radio pulsar PSR J1119−6127 at X-ray, with XMM-Newton and NuSTAR , and at radio energies with the Parkes radio telescope, during a period of magnetar-like bursts. The rotationally powered radio emission shuts off coincident with the occurrence of multiple X-ray bursts and recovers on a timescale of ∼70 s. These observations of related radio and X-ray phenomena further solidify the connection between radio pulsars and magnetars and suggest that the pair plasma produced in bursts can disrupt the acceleration mechanism of radio-emitting particles.

  9. Specific features of thermocouple calorimeter application for measurements of pulsed X-ray emission from plasma

    International Nuclear Information System (INIS)

    Gavrilov, V. V.; Fasakhov, I. K.

    2012-01-01

    It is shown that the accuracy of time-integrated measurements of pulsed X-ray emission from hot plasma with calibrated thermocouple calorimeters is mainly determined by two factors. The first and the most important factor is heating of the filter by the absorbed X-rays; as a result, the calorimeter measures the thermal radiation of the filter, which causes appreciable distortion of the temporal profile and amplitude of the recorded signal. The second factor is the dependence of the effective depth of X-ray absorption in the dielectric that covers the entrance window of the calorimeter on the energy of X-ray photons, i.e., on the recorded radiation spectrum. The results of model calculations of the calorimeter signal are compared with the experimental data.

  10. Time Variabilities of Solar Wind Ion Fluxes and of X-ray and EUV Emissions from Comet Hyakutake

    Science.gov (United States)

    Neugebauer, M.; Cravens, T.; Lisse, C.; Ipavich, F.; von Steiger, R.; Shah, P.; Armstrong, T.

    1999-01-01

    Observations of X-ray and extreme ultraviolet (EUV) emissions from comet C/Hyakutake 1996 B2 made by the Rontgen X-ray satellite (ROSAT) and the Extreme Ultraviolet Explorer (EUVE) revealed a total X-ray luminosity of about 500 MW.

  11. Determination of molybdenite leaching degree by x-ray radiometric analysis

    International Nuclear Information System (INIS)

    Bibinov, S.A.; Gladyshev, V.P.; Yarmolik, A.S.; Kim, A.Ch.; Sokur, N.P.

    1984-01-01

    A express chemical X-ray radiometric method for determination of leaching degree and analysis of molybdenite products is developed. The method comprises chemical preparation and the following X-ray radiometric determination of molyb bdenum. Total duration of the analysis is 1-1.5 h. The best reproductivity is btained at X-ray radiometric analysis as compared with the chemical one

  12. Electron and X-ray emission in collisions of multiply charged ions and atoms

    International Nuclear Information System (INIS)

    Woerlee, P.H.

    1979-01-01

    The author presents experimental results of electron and X-ray emission following slow collisions of multiply charged ions and atoms. The aim of the investigation was to study the mechanisms which are responsible for the emission. (G.T.H.)

  13. X-RAY EMISSION FROM SN 2004dj: A TALE OF TWO SHOCKS

    Energy Technology Data Exchange (ETDEWEB)

    Chakraborti, Sayan; Yadav, Naveen; Ray, Alak [Tata Institute of Fundamental Research, 1 Homi Bhabha Road, Colaba, Mumbai 400 005 (India); Smith, Randall [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States); Chandra, Poonam [Department of Physics, Royal Military College of Canada, Kingston, ON K7K 7B4 (Canada); Pooley, David, E-mail: schakraborti@fas.harvard.edu [Department of Physics, Sam Houston State University, Huntsville, TX (United States)

    2012-12-20

    Type IIP (Plateau) supernovae are the most commonly observed variety of core-collapse events. They have been detected in a wide range of wavelengths from radio, through optical to X-rays. The standard picture of a Type IIP supernova has the blastwave interacting with the progenitor's circumstellar matter to produce a hot region bounded by a forward and a reverse shock. This region is thought to be responsible for most of the X-ray and radio emission from these objects. Yet the origin of X-rays from these supernovae is not well understood quantitatively. The relative contributions of particle acceleration and magnetic field amplification in generating the X-ray and radio emission need to be determined. In this work, we analyze archival Chandra observations of SN 2004dj, one of the nearest supernovae since SN 1987A, along with published radio and optical information. We determine the pre-explosion mass-loss rate, blastwave velocity, electron acceleration, and magnetic field amplification efficiencies. We find that a greater fraction of the thermal energy goes into accelerating electrons than into amplifying magnetic fields. We conclude that the X-ray emission arises out of a combination of inverse Compton scattering by non-thermal electrons accelerated in the forward shock and thermal emission from supernova ejecta heated by the reverse shock.

  14. Modelling of X-ray emission supernova remnants observed by the European satellite XMM-Newton

    International Nuclear Information System (INIS)

    Cassam-Chenai, G.

    2004-01-01

    This thesis deals with the X-ray emission of supernova remnants (SNRs) observed by the European satellite XMM-Newton. In SNRs, the matter heated to millions of degrees shines brightly in X-rays. This emission depends on the hydrodynamical evolution of the SNR, on the chemical composition of the ejected matter and on the ambient medium. Moreover, the blast-wave is considered to be the prime site of the production and the acceleration of cosmic-rays in our Galaxy. XMM-Newton is one of the first to allow the investigation of these different aspects thanks to its spatially-resolved spectroscopy and its very good sensitivity. l first studied Kepler's SNR (SN 1604) whose X-ray emission is dominated by the ejecta. Its observation has allowed to obtain information on the nucleosynthesis products, on their spatial distribution and on the temperature structure in the shocked ejecta. This gives strong constraints on the physics of the explosion and on the progenitor's type. l have shown also that the X-ray emission at the shock is likely to be non-thermal. Then, l studied the SNR G347.3-0.5 whose X-ray emission is entirely due to the synchrotron radiation of relativistic (TeV) electrons accelerated at the shock. From five pointing, l made a full mapping of the X-ray emission characteristics (brightness, absorption and spectral index) at small scale. Combined to radio observations, these results have indicated a clear interaction between the SNR and molecular clouds located at 1 kpc and not at 6 kpc as previously estimated. Lastly, in the framework of a self-similar hydrodynamical model coupled with non-linear particle acceleration, l have obtained the synchrotron emission profile in SNRs, including the adiabatic and radiative losses of the accelerated electrons. (author) [fr

  15. The Chandra planetary nebula survey (CHANPLANS). II. X-ray emission from compact planetary nebulae

    Energy Technology Data Exchange (ETDEWEB)

    Freeman, M.; Kastner, J. H. [Center for Imaging Science and Laboratory for Multiwavelength Astrophysics, Rochester Institute of Technology, 54 Lomb Memorial Drive, Rochester, NY 14623 (United States); Montez, R. Jr. [Department of Physics and Astronomy, Vanderbilt University, Nashville, TN (United States); Balick, B. [Department of Astronomy, University of Washington, Seattle, WA (United States); Frew, D. J.; De Marco, O.; Parker, Q. A. [Department of Physics and Astronomy and Macquarie Research Centre for Astronomy, Astrophysics and Astrophotonics, Macquarie University, Sydney, NSW 2109 (Australia); Jones, D. [Departamento de Física, Universidad de Atacama, Copayapu 485, Copiapó (Chile); Miszalski, B. [South African Astronomical Observatory, P.O. Box 9, Observatory, 7935 (South Africa); Sahai, R. [Jet Propulsion Laboratory, MS 183-900, California Institute of Technology, Pasadena, CA 91109 (United States); Blackman, E.; Frank, A. [Department of Physics and Astronomy, University of Rochester, Rochester, NY (United States); Chu, Y.-H. [Department of Astronomy, University of Illinois at Urbana-Champaign, Urbana, IL (United States); Guerrero, M. A. [Instituto de Astrofísica de Andalucía, IAA-CSIC, Glorieta de la Astronomía s/n, Granada, E-18008 (Spain); Lopez, J. A. [Instituto de Astronomía, Universidad Nacional Autonoma de Mexico, Campus Ensenada, Apdo. Postal 22860, Ensenada, B. C. (Mexico); Zijlstra, A. [School of Physics and Astronomy, University of Manchester, Manchester M13 9PL (United Kingdom); Bujarrabal, V. [Instituto de Astrofísica de Canarias, E-38200 La Laguna, Tenerife (Spain); Corradi, R. L. M. [Departamento de Astrofísica, Universidad de La Laguna, E-38206 La Laguna, Tenerife (Spain); Nordhaus, J. [NSF Astronomy and Astrophysics Fellow, Center for Computational Relativity and Gravitation, Rochester Institute of Technology, Rochester, NY 14623 (United States); and others

    2014-10-20

    We present results from the most recent set of observations obtained as part of the Chandra X-ray observatory Planetary Nebula Survey (CHANPLANS), the first comprehensive X-ray survey of planetary nebulae (PNe) in the solar neighborhood (i.e., within ∼1.5 kpc of the Sun). The survey is designed to place constraints on the frequency of appearance and range of X-ray spectral characteristics of X-ray-emitting PN central stars and the evolutionary timescales of wind-shock-heated bubbles within PNe. CHANPLANS began with a combined Cycle 12 and archive Chandra survey of 35 PNe. CHANPLANS continued via a Chandra Cycle 14 Large Program which targeted all (24) remaining known compact (R {sub neb} ≲ 0.4 pc), young PNe that lie within ∼1.5 kpc. Results from these Cycle 14 observations include first-time X-ray detections of hot bubbles within NGC 1501, 3918, 6153, and 6369, and point sources in HbDs 1, NGC 6337, and Sp 1. The addition of the Cycle 14 results brings the overall CHANPLANS diffuse X-ray detection rate to ∼27% and the point source detection rate to ∼36%. It has become clearer that diffuse X-ray emission is associated with young (≲ 5 × 10{sup 3} yr), and likewise compact (R {sub neb} ≲ 0.15 pc), PNe with closed structures and high central electron densities (n{sub e} ≳ 1000 cm{sup –3}), and is rarely associated with PNe that show H{sub 2} emission and/or pronounced butterfly structures. Hb 5 is one such exception of a PN with a butterfly structure that hosts diffuse X-ray emission. Additionally, two of the five new diffuse X-ray detections (NGC 1501 and NGC 6369) host [WR]-type central stars, supporting the hypothesis that PNe with central stars of [WR]-type are likely to display diffuse X-ray emission.

  16. X-Ray Diffraction and Fluorescence Instrument for Mineralogical Analysis at the Lunar Surface, Phase II

    Data.gov (United States)

    National Aeronautics and Space Administration — We propose to develop LUNA, a compact and lightweight X-Ray Diffraction (XRD) / X-Ray Fluorescence (XRF) instrument for mineralogical analysis of regolith, rock...

  17. X-Ray Diffraction and Fluorescence Instrument for Mineralogical Analysis at the Lunar Surface, Phase I

    Data.gov (United States)

    National Aeronautics and Space Administration — We propose to develop a compact and lightweight X-Ray Diffraction (XRD) / X-Ray Fluorescence (XRF) instrument for analysis of mineralogical composition of regolith,...

  18. Plan for PLEX X-Ray Ablation Experiments and Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Latkowski, J F; Reyes, S

    2001-09-27

    PLEX is a Z-pinch based x-ray source that can produce x-rays with fluences (0.3-18 J/cm{sup 2}), pulselengths (10-30 ns), repetition rates (<10 Hz), and energies (50-500 eV) of interest for IFE chambers and optics. It provides an affordable, dedicated method to advance our understanding of x-ray damage to materials. The PLEX x-ray source will be used to experimentally validate and further develop the ABLATOR x-ray ablation code for use in inertial fusion energy (IFE) studies.

  19. A study of x-ray emission from the anode region in a plasma focus device

    International Nuclear Information System (INIS)

    Jia Wang; Tsinchi Yang

    1988-01-01

    The physical process of x-ray emission from the anode region in a plasma focus device due to the interaction of a powerful electron beam with the metal anode and with ionised metallic vapour from the anode is investigated. The influence of the magnetic field of the beam is taken into consideration. A MC-PIC model (Monte Carlo-particle in cell) is proposed for the process, in which an electron-photon collision cascade is simulated by the MC approach and the time-dependent state of metallic vapour is determined by PIC computation. The time-resolved energy spectra and angular distributions of x-ray emission from the extending anode region are calculated. The time-integrated characteristics of the x-ray emission can be compared with the results of experiments as far as they are available. (author)

  20. High resolution krypton M/sub 4,5/ x-ray emission spectra

    International Nuclear Information System (INIS)

    Perera, R.C.C.; Hettrick, M.C.; Lindle, D.W.

    1987-10-01

    High resolution M/sub 4,5/ (3d → 4p) x-ray emission spectra from a krypton plasma were measured using a recently developed grazing-incidence reflection-grating monochromator/spectrometer with very high flux rates at extreme ultraviolet and soft x-ray wave lengths. The nominal resolving power of the instrument, E/ΔE, is about 300 in this energy range (∼80 eV). Three dipole-allowed 3d → 4p emission lines were observed at 80.98 eV, 80.35 eV and 79.73 eV. A broad peak at about 82.3 eV is tentatively assigned to transitions resulting from Kr 2+ , and effects of excitation energy on M/sub 4,5/ x-ray emission were observed. 9 refs., 3 figs., 1 tab

  1. X-ray fluorescence analysis of welding fume particles

    International Nuclear Information System (INIS)

    Carsey, T.P.

    1982-01-01

    A commercial standard filter set and two laboratory-made standard filter sets are compared via the analysis of generated welding fume samples by X-ray fluorescence. The latter standards are made by (1) hydrophobic-edge membrane filters spiked with prepared metal ion solutions, and (2) filters through which a dispersion of metal oxide powder in isopropanol has been drawn. The results are presented in table form. Precision (Pre) is the relative standard deviation of the six samples. Four main conclusions are enumerated

  2. Quantitative x-ray fluorescent analysis using fundamental parameters

    International Nuclear Information System (INIS)

    Sparks, C.J. Jr.

    1976-01-01

    A monochromatic source of x-rays for sample excitation permits the use of pure elemental standards and relatively simple calculations to convert the measured fluorescent intensities to an absolute basis of weight per unit weight of sample. Only the mass absorption coefficients of the sample for the exciting and the fluorescent radiation need be determined. Besides the direct measurement of these absorption coefficients in the sample, other techniques are considered which require fewer sample manipulations and measurements. These fundamental parameters methods permit quantitative analysis without recourse to the time-consuming process of preparing nearly identical standards

  3. Quantification procedures in micro X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Kanngiesser, Birgit

    2003-01-01

    For the quantification in micro X-ray fluorescence analysis standardfree quantification procedures have become especially important. An introduction to the basic concepts of these quantification procedures is given, followed by a short survey of the procedures which are available now and what kind of experimental situations and analytical problems are addressed. The last point is extended by the description of an own development for the fundamental parameter method, which renders the inclusion of nonparallel beam geometries possible. Finally, open problems for the quantification procedures are discussed

  4. Towards adaptive, streaming analysis of x-ray tomography data

    Energy Technology Data Exchange (ETDEWEB)

    Thomas, Mathew; Kleese van Dam, Kerstin; Marshall, Matthew J.; Kuprat, Andrew P.; Carson, James P.; Lansing, Carina S.; Guillen, Zoe C.; Miller, Erin A.; Lanekoff, Ingela; Laskin, Julia

    2015-03-04

    Temporal and spatial resolution of chemical imaging methodologies such as x-ray tomography are rapidly increasing, leading to more complex experimental procedures and fast growing data volumes. Automated analysis pipelines and big data analytics are becoming essential to effectively evaluate the results of such experiments. Offering those data techniques in an adaptive, streaming environment can further substantially improve the scientific discovery process, by enabling experimental control and steering based on the evaluation of emerging phenomena as they are observed by the experiment. Pacific Northwest National Laboratory (PNNL)’ Chemical Imaging Initiative (CII - http://imaging.pnnl.gov/ ) has worked since 2011 towards developing a framework that allows users to rapidly compose and customize high throughput experimental analysis pipelines for multiple instrument types. The framework, named ‘Rapid Experimental Analysis’ (REXAN) Framework [1], is based on the idea of reusable component libraries and utilizes the PNNL developed collaborative data management and analysis environment ‘Velo’, to provide a user friendly analysis and data management environment for experimental facilities. This article will, discuss the capabilities established for X-Ray tomography, discuss lessons learned, and provide an overview of our more recent work in the Analysis in Motion Initiative (AIM - http://aim.pnnl.gov/ ) at PNNL to provide REXAN capabilities in a streaming environment.

  5. Elemental analysis techniques using proton microbeam

    International Nuclear Information System (INIS)

    Sakai, Takuro; Oikawa, Masakazu; Sato, Takahiro

    2005-01-01

    Proton microbeam is a powerful tool for two-dimensional elemental analysis. The analysis is based on Particle Induced X-ray Emission (PIXE) and Particle Induced Gamma-ray Emission (PIGE) techniques. The paper outlines the principles and instruments, and describes the dental application has been done in JAERI Takasaki. (author)

  6. Ultrafast atomic process in X-ray emission by using inner-shell ionization method for sodium and carbon atoms

    Energy Technology Data Exchange (ETDEWEB)

    Moribayashi, Kengo; Sasaki, Akira; Tajima, Toshiki [Japan Atomic Energy Research Inst., Neyagawa, Osaka (Japan). Kansai Research Establishment

    1998-07-01

    An ultrafast inner-shell ionization process with X-ray emission stimulated by high-intensity short-pulse X-ray is studied. Carbon and sodium atoms are treated as target matter. It is shown that atomic processes of the target determine the necessary X-ray intensity for X-ray laser emission as well as the features of X-ray laser such as wavelength and duration time. The intensity also depends on the density of initial atoms. Furthermore, we show that as the intensity of X-ray source becomes high, the multi-inner-shell ionization predominates, leading to the formation of hollow atoms. As the density of hollow atoms is increased by the pumping X-ray power, the emission of X-rays is not only of significance for high brightness X-ray measurement but also is good for X-ray lasing. New classes of experiments of pump X-ray probe and X-ray laser are suggested. (author)

  7. Simultaneous emissions of X-rays and microwaves from long laboratory sparks and downward lightning leaders

    Science.gov (United States)

    Montanya, J.; Oscar, V. D. V.; Tapia, F. F.

    2017-12-01

    Since the discovery of the Terrestrial Gamma-ray Flashes more than 20 years ago, investigations on high energy emissions from natural lightning and high voltage laboratory sparks gained significant interest. X-ray emissions from lightning as well from high voltage laboratory sparks have in common the role played by negative leaders/streamers. On the other hand, negative leaders are well known to produce much more VHF and microwave radiation than positive leaders. Moreover, in previous works, microwave emissions from lightning leaders have been attributed to Bremsstrahlung process. The object of this work is to investigate if X-rays and RF microwave emissions share the same origin. We present simultaneous measurements of X-rays and microwaves in high voltage sparks and natural lightning. The instrumentation consists on a NaI(Tl) and LaBr3 scintillation detectors and two different receivers. One is fix tuned at 2.4 GHz with a bandwidth of 5.5 MHz. The second can be tuned at any frequency up to 18 GHz with different selectable bandwidths of 10 MHz, 40 MHz and 100 MHz. In the laboratory, results have shown that all the sparks presented microwave radiation before the breakdown of the gap, either X-rays were detected or not. In the cases where X-rays were identified, microwave emissions peaked at the same time (in the microsecond scale). We found that the power amplitudes of the microwave emissions are related to the applied voltage to the gap. In the same configuration, those cases where X-rays were detected microwave emissions presented higher power levels. The results suggest that in some part of the discharge electrons are very fast accelerated allowing, in some cases, to reach enought energy to produce X-rays. In the field, we have found similar results. On 13th of June of 2015 a bipolar cloud-to-ground flash struck 200 m close to the Eagle Nest instrumented tower (Spanish Pyrenees, 2536 m ASL). The flash presented four strokes and, in all of them, microwave

  8. Chandra X-ray Data Analysis in Educational Environments

    Science.gov (United States)

    Matilsky, T.; Etkina, E.; Lestition, K.; Mandel, E.; Joye, W.

    2004-12-01

    Recent progress in both software and remote connectivity capabilities have made it possible for authentic data analysis tasks to be presented in a wide range of educational venues. No longer are precollege teachers and students, and interested members of the public limited by their lack of access to the scientific workstations and UNIX-based imaging and analytical software used by the research community. Through a suite of programs that couples a simplified graphical user interface using the "DS9" imaging software with a "virtual observatory" capability that processes the analytical algorithms used by X-ray astronomers, we can access archived Chandra observations and generate images, as well as light curves, energy spectra, power spectra and other common examples of science tasks. The system connects to a remote UNIX server, but the user may be sited on a PC or Mac platform. Furthermore, the use of VNC (a remote desktop display environment) allows a teacher to view, comment on and debug any analysis task in real time, from anywhere in the world, and across any computer platform. This makes these programs especially useful in distance learning settings. We have developed, tested and used these capabilities in a wide variety of educational arenas, from 4 week intensive courses in X-ray astronomy research techniques for precollege students and teachers, to one day teacher enrichment workshops, to modules of classroom activities suitable for precollege grade levels, using a variety of cosmic X-ray sources. Examples using archived Chandra observations will be presented demonstrating the flexibility and usefulness of these resources.

  9. X-ray diffraction analysis of InAs nanowires

    International Nuclear Information System (INIS)

    Davydok, Anton

    2013-01-01

    Semiconductor nanowires have attracted great interest as building blocks for future electronic and optoelectronic devices. The variability of the growth process opens the opportunity to control and combine the various properties tailoring for specific application. It was shown that the electrical and optical characteristics of the nanowires are strongly connected with their structure. Despite intensive research in this field, the growth process is still not fully understood. In particular, extensive real structure investigations are required. Most of the reports dedicated on the structural researches are based on the results of scanning electron microscopy (SEM) or transmission electron microscopy (TEM). SEM provides an image of the surface with nanostructures and is mainly used to describe the morphology of the sample, but it does not bring information about the internal structure, phase composition and defect structure. At the same time, the internal structure can be examined by TEM down to atomic scale. TEM image of good quality are very expensive due to the efforts in sample preparation and in localisation of a single object. All these aspects make the statistical structural analysis difficult. In the present work, X-ray diffraction analysis has been applied for structural investigation of InAs nanowires grown by different techniques. Using various X-ray diffraction geometries, the nanowire systems were investigated in terms of the lattice parameters, phase composition, strains and displacement fields and stacking defects. In particular, realizing grazing incidence diffraction and controlling the penetration depth of X-ray beam, we characterized sample series grown by Au-assisted metal organic phase epitaxy on GaAs [111]B substrate with different growth time. According to the results of SEM and X-ray investigations, a model of the growth process has been proposed. A more detailed analysis was performed on InAs nanowires grown by molecular beam epitaxy (MBE) on

  10. X-ray absorption spectra and emission spectra of plasmas

    International Nuclear Information System (INIS)

    Peng Yonglun; Yang Li; Wang Minsheng; Li Jiaming

    2002-01-01

    The author reports a theoretical method to calculate the resolved absorption spectra and emission spectra (optically thin) of hot dense plasmas. Due to its fully relativistic treatment incorporated with the quantum defect theory, it calculates the absorption spectra and emission spectra for single element or multi-element plasmas with little computational efforts. The calculated absorption spectra of LTE gold plasmas agree well with the experimental ones. It also calculates the optical thin emission spectra of LTE gold plasmas, which is helpful to diagnose the plasmas of relevant ICF plasmas. It can also provide the relevant parameters such as population density of various ionic stages, precise radiative properties for ICF studies

  11. MODELING THE THERMAL DIFFUSE SOFT AND HARD X-RAY EMISSION IN M17

    International Nuclear Information System (INIS)

    Velázquez, P. F.; Rodríguez-González, A.; Esquivel, A.; Rosado, M.; Reyes-Iturbide, J.

    2013-01-01

    We present numerical models of very young wind driven superbubbles. The parameters chosen for the simulations correspond to the particular case of the M17 nebula, but are appropriate for any young superbubble in which the wind sources have not completely dispersed their parental cloud. From the simulations, we computed the diffuse emission in the soft ([0.5-1.5] keV) and hard ([1.5-5] keV) X-ray bands. The total luminosity in our simulations agrees with the observations of Hyodo et al., about two orders of magnitude below the prediction of the standard model of Weaver et al.. The difference with respect to the standard (adiabatic) model is the inclusion of radiative cooling, which is still important in such young bubbles. We show that for this type of object the diffuse hard X-ray luminosity is significant compared to that of soft X-rays, contributing as much as 10% of the total luminosity, in contrast with more evolved bubbles where the hard X-ray emission is indeed negligible, being at least four orders of magnitude lower than the soft X-ray emission.

  12. X-ray emission spectroscopic determination of iron in a polyurethane encapsulant curing agent

    International Nuclear Information System (INIS)

    Carter, J.M.; Kling, E.N.

    1979-01-01

    Presented is a procedure for determining the iron content in a polyurethane encapsulant curing agent by x-ray emission spectroscopy. Standards were prepared by adding ferric acetyl acetonate to a curing agent of identical composition to that being analyzed, but containing no iron. Results show that x-ray emission spectroscopy is feasible for determination of iron in the 30 to 50 ppM range. This range could probably be extended by the preparation of additional standards. Precision of the method is approximately 1.2 ppM at the 99 percent confidence level

  13. Calculation of X-ray emission produced by a quasi-monoenergetic electron distribution

    International Nuclear Information System (INIS)

    Fanaei, M.; Sadighi-Bonabi, R.

    2010-01-01

    Complete text of publication follows. By using an intense ultrafast laser interaction with plasma, generation of accelerated relativistic electrons with quasi monoenergetic spectrum has been possible. Analytic expressions for spectra and emission efficiencies of x-rays bremsstrahlung and characteristic line emission produced by a quasi-monoenergetic electron distribution from several targets are investigated. In this work, a Gaussian profile is assumed for the quasi-monoenergetic electron spectrum. The produced x-ray radiations are compared with the previous achieved results for a Maxwellian electron profile. These results and achievements are discussed in detail. Also, the outcomes can be evaluated with the experimental and simulated results.

  14. Study of x-ray emission enhancement via high contrast femtosecond laser interacting with solid foil

    International Nuclear Information System (INIS)

    Chen, Liming; Kando, Masaki; Bulanov, S.V.; Koga, James K.; Tajima, Toshiki; Xu M.H.; Yuan X.H.; Li Y.T.; Dong Q.L.; Zhang J.

    2007-01-01

    We studied the hard x-ray emission and the Kα x-ray conversion efficiency (η K ) produced by 60 fs high contrast frequency doubled Ti: sapphire laser pulse focused on Cu foil target. Cu Kα photon emission obtained with second harmonic laser pulse is more intense than the case of fundamental laser pulse. The Cu η K shows strong dependence on laser nonlinearly skewed pulse shape and reaches the maximum value 4x10 -4 with 100 fs negatively skewed pulse. It shows the electron spectrum shaping contribute to the increase of η K . (author)

  15. X-ray astronomy

    International Nuclear Information System (INIS)

    Giacconi, R.; Gursky, H.

    1974-01-01

    This text contains ten chapters and three appendices. Following an introduction, chapters two through five deal with observational techniques, mechanisms for the production of x rays in a cosmic setting, the x-ray sky and solar x-ray emission. Chapters six through ten include compact x-ray sources, supernova remnants, the interstellar medium, extragalactic x-ray sources and the cosmic x-ray background. Interactions of x rays with matter, units and conversion factors and a catalog of x-ray sources comprise the three appendices. (U.S.)

  16. Multi-elemental analysis of marine sediments of Sorsogon Bay using x-ray fluorescence spectroscopy

    International Nuclear Information System (INIS)

    Gonzales, Ralph Roly A.; Quirit, Leni L.; Rosales, Colleen Marciel F.; Pabroa, Preciosa Corazon B.; Sta Maria, Efren J.

    2011-01-01

    Metal composition and nutrient loadings of our bodies of water, when uncontrolled, may cause harmful bacterial contamination and pose threats in aquatic and human life. Toxic and trace element inputs in Sorsogon Bay sediments were determined using nuclear analytical techniques, more specifically, x-ray fluorescence spectrometry, in this study. Pre-treated marine sediment samples from Sorsogon Bay were homogenized using SPEX # 8000 mixer/mill and agate mortar and pestle, pelletized into 31-mm flat discs using SPEX 3630 X-Press and analyzed using PAN Analytical Epsilon 5 EDX X-ray Fluorescence Spectrometer with the emission and transmission method using silver and germanium secondary targets. Spectrum fitting performed using AXIL (Analysis of X-ray Spectra by Iterative Least-Squares Fitting), a subprogram in Quantitative X-ray Analysis System developed by the International Atomic Energy Agency and Quantitative Analysis of Environmental Samples program, was used for quantification of results. Results indicate generally moderate to high metal enrichment, specifically manganese, lead, cadmium, zinc and copper. Mercury and iron level enrichment are found to be low, marking an improvement from previous studies indicating high enrichment of these metals. (author)

  17. 1.2. X-ray phase analysis of borosilicate raw material

    International Nuclear Information System (INIS)

    Mirsaidov, U.M.; Kurbonov, A.S.; Mamatov, E.D.

    2015-01-01

    Present article is devoted to X-ray phase analysis of borosilicate raw material. The thermo gram of initial borosilicate ore was considered. The X-ray pattern of initial danburite of Ak-Arhar Deposit was considered as well. The X-ray pattern of danburite of Ak-Arhar Deposit after pre-baking was studied. The X-ray pattern of initial danburite concentrate was studied as well.

  18. Relations Between FUV Excess and Coronal Soft X-Ray Emission Among Dwarf Stars

    Science.gov (United States)

    Smith, Graeme H.; Hargrave, Mason; Eckholm, Elliot

    2017-11-01

    The far-ultraviolet magnitudes of late-F, G and early-K dwarfs with (B - V) ⩾ 0.50 as measured by the GALEX satellite are shown to correlate with soft X-ray luminosity. This result indicates that line and continuum emission from stellar active regions make significant contributions to the flux in the GALEX FUV band for late-F, G and K dwarfs. By contrast, detection of a correlation between FUV brightness and soft X-ray luminosity among early-F dwarfs requires subtraction of the photospheric component from the FUV flux. The range in (B - V) among F and G dwarfs over which a correlation between uncorrected FUV magnitude and X-ray luminosity is detected coincides with the range in colour over which coronal and chromospheric emission correlates with stellar rotation.

  19. K and L X-ray emission intensities of some radionuclides

    Energy Technology Data Exchange (ETDEWEB)

    Verma, H R; Pal, D [Punjabi Univ., Patiala (India). Dept. of Physics

    1985-01-01

    The K and L x-ray emission intensities per 100 disintegrations have been calculated for some radionuclides using the latest adopted data for gamma-ray intensities, electron capture and internal conversion coefficients for the parent nuclides, fluorescence yield values, Coster-Kronig transition probabilities, average total number of primary L shell vacancies produced in the decay of K shell vacancies and emission rates for various shells and subshells for the daughter nuclei. The results are in good agreement with theoretical and experimental values for the K x-ray intensities. There are no experimental results available to compare with the present calculations for the L x-ray intensities; however, there is a marked discrepancy in the L..cap alpha.. and L..beta.. intensities available on the basis of theoretical estimates.

  20. Obtaining attosecond x-ray pulses using a self-amplified spontaneous emission free electron laser

    Directory of Open Access Journals (Sweden)

    A. A. Zholents

    2005-05-01

    Full Text Available We describe a technique for the generation of a solitary attosecond x-ray pulse in a free-electron laser (FEL, via a process of self-amplified spontaneous emission. In this method, electrons experience an energy modulation upon interacting with laser pulses having a duration of a few cycles within single-period wiggler magnets. Two consecutive modulation sections, followed by compression in a dispersive section, are used to obtain a single, subfemtosecond spike in the electron peak current. This region of the electron beam experiences an enhanced growth rate for FEL amplification. After propagation through a long undulator, this current spike emits a ∼250   attosecond x-ray pulse whose intensity dominates the x-ray emission from the rest of the electron bunch.

  1. Einstein X-ray survey of the Pleiades - The dependence of X-ray emission on stellar age

    Science.gov (United States)

    Micela, G.; Sciortino, S.; Serio, S.; Vaiana, G. S.; Bookbinder, J.; Golub, L.; Harnden, F. R., Jr.; Rosner, R.

    1985-01-01

    The data obtained with two pointed observations of 1 deg by 1 deg fields of the Pleiades region have been analyzed, and the results are presented. The maximum-likelihood X-ray luminosity functions for the Pleiades G and K stars in the cluster are derived, and it is shown that, for the G stars, the Pleiades X-ray luminosity function is significantly brighter than the corresponding function for Hyades G dwarf stars. This finding indicates a dependence of X-ray luminosity on stellar age, which is confirmed by comparison of the same data with median X-ray luminosities of pre-main sequence and local disk population dwarf G stars. It is suggested that the significantly larger number of bright X-ray sources associated with G stars than with K stars, the lack of detection of M stars, and the relatively rapid rotation of the Pleiades K stars can be explained in terms of the onset of internal differential rotation near the convective envelope-radidative core interface after the spin-up phase during evolution to the main sequence.

  2. An x ray scatter approach for non-destructive chemical analysis of low atomic numbered elements

    Science.gov (United States)

    Ross, H. Richard

    1993-01-01

    A non-destructive x-ray scatter (XRS) approach has been developed, along with a rapid atomic scatter algorithm for the detection and analysis of low atomic-numbered elements in solids, powders, and liquids. The present method of energy dispersive x-ray fluorescence spectroscopy (EDXRF) makes the analysis of light elements (i.e., less than sodium; less than 11) extremely difficult. Detection and measurement become progressively worse as atomic numbers become smaller, due to a competing process called 'Auger Emission', which reduces fluorescent intensity, coupled with the high mass absorption coefficients exhibited by low energy x-rays, the detection and determination of low atomic-numbered elements by x-ray spectrometry is limited. However, an indirect approach based on the intensity ratio of Compton and Rayleigh scattered has been used to define light element components in alloys, plastics and other materials. This XRS technique provides qualitative and quantitative information about the overall constituents of a variety of samples.

  3. The Sun's X-ray Emission During the Recent Solar Minimum

    Science.gov (United States)

    Sylwester, Janusz; Kowalinski, Mirek; Gburek, Szymon; Siarkowski, Marek; Kuzin, Sergey; Farnik, Frantisek; Reale, Fabio; Phillips, Kenneth J. H.

    2010-02-01

    The Sun recently underwent a period of a remarkable lack of major activity such as large flares and sunspots, without equal since the advent of the space age a half century ago. A widely used measure of solar activity is the amount of solar soft X-ray emission, but until recently this has been below the threshold of the X-ray-monitoring Geostationary Operational Environmental Satellites (GOES). There is thus an urgent need for more sensitive instrumentation to record solar X-ray emission in this range. Anticipating this need, a highly sensitive spectrophotometer called Solar Photometer in X-rays (SphinX) was included in the solar telescope/spectrometer TESIS instrument package on the third spacecraft in Russia's Complex Orbital Observations Near-Earth of Activity of the Sun (CORONAS-PHOTON) program, launched 30 January 2009 into a near-polar orbit. SphinX measures X-rays in a band similar to the GOES longer-wavelength channel.

  4. Soft x-ray emission from gamma-ray bursts observed with ginga

    International Nuclear Information System (INIS)

    Yoshida, Atsumasa; Murakami, Toshio; Itoh, Masayuki

    1989-01-01

    The soft X-ray emission of gamma-ray bursts below 10 keV provides information about size, location, and emission mechanism. The Gamma-ray Burst Detector (GBD) on board Ginga, which consists of a proportional counter and a scintillation detector, covers an energy range down to 1.5 keV with 63 cm 2 effective area. In several of the observed gamma-ray bursts, the intensity of the soft X-ray emission showed a longer decay time of 50 to 100s after the higher energy gamma-ray emission had ended. Although we cannot rule out other models, such as bremsstrahlung and thermal cyclotron types, due to poor statistics, the soft X-ray spectra are consistent with a blackbody of 1 to 2 keV in the late phase of the gamma-ray bursts. This enables us to estimate the size of the blackbody responsible for the X-ray emission. (author)

  5. X-ray emission from a high-atomic-number z-pinch plasma created from compact wire arrays

    International Nuclear Information System (INIS)

    Sanford, T.W.L.; Nash, T.J.; Marder, B.M.

    1996-03-01

    Thermal and nonthermal x-ray emission from the implosion of compact tungsten wire arrays, driven by 5 MA from the Saturn accelerator, are measured and compared with LLNL Radiation-Hydro-Code (RHC) and SNL Hydro-Code (HC) numerical models. Multiple implosions, due to sequential compressions and expansions of the plasma, are inferred from the measured multiple x-radiation bursts. Timing of the multiple implosions and the thermal x-ray spectra measured between 1 and 10 keV are consistent with the RHC simulations. The magnitude of the nonthermal x-ray emission measured from 10 to 100 keV ranges from 0.02 to 0.08% of the total energy radiated and is correlated with bright-spot emission along the z-axis, as observed in earlier Gamble-11 single exploding-wire experiments. The similarities of the measured nonthermal spectrum and bright-spot emission with those measured at 0.8 MA on Gamble-II suggest a common production mechanism for this process. A model of electron acceleration across magnetic fields in highly-collisional, high-atomic-number plasmas is developed, which shows the existence of a critical electric field, E c , below which strong nonthermal electron creation (and the associated nonthermal x rays) do not occur. HC simulations show that significant nonthermal electrons are not expected in this experiment (as observed) because the calculated electric fields are at least one to two orders-of-magnitude below E c . These negative nonthermal results are confirmed by RHC simulations using a nonthermal model based on a Fokker-Plank analysis. Lastly, the lower production efficiency and the larger, more irregular pinch spots formed in this experiment relative to those measured on Gamble II suggest that implosion geometries are not as efficient as single exploding-wire geometries for warm x-ray production

  6. Scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX) and aerosol time-of-flight mass spectrometry (ATOFMS) single particle analysis of metallurgy plant emissions.

    Science.gov (United States)

    Arndt, J; Deboudt, K; Anderson, A; Blondel, A; Eliet, S; Flament, P; Fourmentin, M; Healy, R M; Savary, V; Setyan, A; Wenger, J C

    2016-03-01

    The chemical composition of single particles deposited on industrial filters located in three different chimneys of an iron-manganese (Fe-Mn) alloy manufacturing plant have been compared using aerosol time-of-flight mass spectrometry (ATOFMS) and scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX). Very similar types of particles were observed using both analytical techniques. Calcium-containing particles dominated in the firing area of the sintering unit, Mn and/or Al-bearing particles were observed at the cooling area of the sintering unit, while Mn-containing particles were dominant at the smelting unit. SEM-EDX analysis of particles collected downstream of the industrial filters showed that the composition of the particles emitted from the chimneys is very similar to those collected on the filters. ATOFMS analysis of ore samples was also performed to identify particulate emissions that could be generated by wind erosion and manual activities. Specific particle types have been identified for each emission source (chimneys and ore piles) and can be used as tracers for source apportionment of ambient PM measured in the vicinity of the industrial site. Copyright © 2015 Elsevier Ltd. All rights reserved.

  7. X-ray CT analysis on archaeological iron based artifacts

    International Nuclear Information System (INIS)

    Honda, Takashi; Gunji, Eiichi

    2005-01-01

    Corrosion analysis was carried out on twenty iron-plates, which had been dug out at the 6th Yamato ancient tomb (Nara-shi). It was evaluated through the inner-structural analysis by X-ray CT and the XRD and chemical analysis of the rusts that the most iron-plates had been buried in a slightly oxidizing environment and the maximum corrosion depth was 1.6 mm for about 1500 years. The analysis result of the extreme-value data indicates that the maximum depth of an overpack is estimated to be 2.5-2.7 mm. A part of small iron-plates were supposed to have been buried in an oxidizing environment, and about 1 mm-thick rust layers with cavities existed and the corrosion amount was figured out to be about 0.3 mm. (author)

  8. Handbook of practical X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Beckhoff, B.; Wedell, R.; Wolff, H.

    2006-01-01

    X-ray fluorescence analysis (XRF) is a reliable multi-elemental and nondestructive analytical method widely used in research and industrial applications. This practical handbook provides self-contained modules featuring XRF instrumentation, quantification methods, and most of the current applications. The broad spectrum of topics is due to the efforts of a large number of authors from a variety of different types of institutions such as universities, research institutes, and companies. The book gives a survey of the theoretical fundamentals, analytical instrumentation, software for data processing, various excitation regimes including gracing incidents and microfocus measurements, quantitative analysis, applications in routine and micro analysis, mineralogy, biology, medicine, criminal investigations, archeology, metallurgy, abrasion, microelectronics, environmental air and water analysis. It gives the basic knowledge on this technique, information on analytical equipment and guides the reader to the various applications. This practical handbook is intended as a resource for graduate students, research scientists, and industrial users. (orig.)

  9. Handbook of practical X-ray fluorescence analysis

    Energy Technology Data Exchange (ETDEWEB)

    Beckhoff, B. [Physikalisch-Technische Bundesanstalt, Berlin (Germany). X-ray Spectrometry; Kanngiesser, B. [Technische Univ. Berlin (Germany). Inst. fuer Atomare Physik und Fachdidaktik; Langhoff, N. [IfG-Institute for Scientific Instruments GmbH, Berlin (Germany); Wedell, R.; Wolff, H. (eds.) [Institut fuer Angewandte Photonik e.V., Berlin (Germany)

    2006-07-01

    X-ray fluorescence analysis (XRF) is a reliable multi-elemental and nondestructive analytical method widely used in research and industrial applications. This practical handbook provides self-contained modules featuring XRF instrumentation, quantification methods, and most of the current applications. The broad spectrum of topics is due to the efforts of a large number of authors from a variety of different types of institutions such as universities, research institutes, and companies. The book gives a survey of the theoretical fundamentals, analytical instrumentation, software for data processing, various excitation regimes including gracing incidents and microfocus measurements, quantitative analysis, applications in routine and micro analysis, mineralogy, biology, medicine, criminal investigations, archeology, metallurgy, abrasion, microelectronics, environmental air and water analysis. It gives the basic knowledge on this technique, information on analytical equipment and guides the reader to the various applications. This practical handbook is intended as a resource for graduate students, research scientists, and industrial users. (orig.)

  10. Quantitative x-ray fractographic analysis of fatigue fractures

    International Nuclear Information System (INIS)

    Saprykin, Yu.V.

    1983-01-01

    The study deals with quantitative X-ray fractographic investigation of fatigue fractures of samples with sharp notches tested at various stresses and temperatures with the purpose of establishing a connection between material crack resistance parameters and local plastic instability zones restraining and controlling the crack growth. At fatigue fractures of notched Kh18N9T steel samples tested at +20 and -196 deg C a zone of sharp ring notch effect being analogous to the zone in which crack growth rate is controlled by the microshifting mechanisms is singled out. The size of the notched effect zone in the investigate steel is unambiguosly bound to to the stress amplitude. This provides the possibility to determine the stress value by the results of quantitative fractographic analysis of notched sample fractures. A possibility of determining one of the threshold values of cyclic material fracture toughness by the results of fatigue testing and fractography of notched sample fractures is shown. Correlation between the size of the hsub(s) crack effect zone in the notched sample, delta material yield limit and characteristic of cyclic Ksub(s) fracture toughness has been found. Such correlation widens the possibilities of quantitative diagnostics of fractures by the methods of X-ray fractography

  11. X-ray continuum and iron K emission line from the radio galaxy 3C 390.3

    Science.gov (United States)

    Inda, M.; Makishima, K.; Kohmura, Y.; Tashiro, M.; Ohashi, T.; Barr, P.; Hayashida, K.; Palumbo, G. G. C.; Trinchieri, G.; Elvis, M.

    1994-01-01

    X-ray properties of the radio galaxy 3C 390.3 were investigated using the European X-ray Observatory Satellite (EXOSAT) and Ginga satellites. Long-term, large-amplitude X-ray intensity changes were detected over a period extending from 1984 through 1991, and high-quality X-ray spectra were obtained especially with Ginga. The X-ray continuum spectra were described with power-law model with photon slope in the range 1.5-1.8, and the slope flattened as the 2-20 keV luminosity decreased by 40%. There was a first detection of the iron emission line from this source at the 90% confidence level. An upper limit was derived on the thermal X-ray component. X-ray emission mechanisms and possible origins of the long-term variation are discussed.

  12. X-ray emission in heavy-ion collisions. Progress report, April 1, 1979-March 31, 1980

    International Nuclear Information System (INIS)

    Watson, R.L.

    1980-04-01

    Recent research in the cyclotron institute and department of chemistry at Texas A and M University on the x-ray emission in heavy-ion collisions is described. Areas covered include: spectra of Ka x-rays from 64 MeV sulfur ions traveling in solids; foil-excited Ka x-ray transitions in few-electron sulfur ions; high-resolution study of the target thickness dependence of x-ray emission from 65 MeV sulfur ions; dynamic screening of highly stripped sulfur ions in solids; Mg Ka x-ray satellites excited by ion bombardment, multiplet structure and dependence on projectile and chemical environment; angular distributions of beam and target Ka x-rays; chemical effects on K x-ray satellites of fluorine compounds; and a non-linear least-squares peak-fitting program employing Voight functions

  13. Application of proton-induced X-ray emission technique to gunshot residue analyses

    International Nuclear Information System (INIS)

    Sen, P.; Panigrahi, N.; Rao, M.S.; Varier, K.M.; Sen, S.; Mehta, G.K.

    1982-01-01

    The proton-induced X-ray emission (PIXE) technique was applied to the identification and analysis of gunshot residues. Studies were made of the type of bullet and bullet hole identification, firearm discharge element profiles, the effect of various target backings, and hand swabbings. The discussion of the results reviews the sensitivity of the PIXE technique, its nondestructive nature, and its role in determining the distance from the gun to the victim and identifying the type of bullet used and whether a wound was made by a bullet or not. The high sensitivity of the PIXE technique, which is able to analyze samples as small as 0.1 to 1 ng, and its usefulness for detecting a variety of elements should make it particularly useful in firearms residue investigations

  14. X-ray stress analysis in textured polycrystalline materials

    International Nuclear Information System (INIS)

    Yokoyama, Ryouichi; Harada, Jimpei

    2010-01-01

    The relationship between stress and strain in polycrystalline materials with fibre texture is examined on the basis of the strain analysis in the constituent crystallites within the Reuss approximation. By introducing the symmetry of reciprocal lattices for the constituent crystallites, the physical meaning of taking an average of the strains observed by X-ray diffraction (XRD) is made clear. By using formulae obtained by the present treatment for the stress-strain relation in cubic specimens with fibre texture in the Laue classes m3-bar m hkl Bragg reflections with h≠k≠l split into doublets owing to the existence of crystallites with two different orientations under the stress field. This technique was confirmed by the profile analysis in XRD data observed for reflections of 222 and 420 in a cubic TiN thin film sputtered on a polyimide film. The technique of the stress analysis and its confirmation are introduced. (author)

  15. Hair analysis by proton-induced-X-ray emission and atomic absorption. Part of a coordinated programme on nuclear-based methods for analysis of pollutants in human hair

    International Nuclear Information System (INIS)

    Mangelson, N.F.

    1979-07-01

    Specimens of small wild rodents comprised of 5 species were collected in an area near Lake Powell, Utah, (U.S.A.). Liver, lung, kidney and hair were sampled and analysed for several elements using proton-induced X-ray emission (PIXE). Various statistical tests were performed on the data gathered. Although many elements highly correlate among all tissues and animal species studies, it was not possible to determine from the present study which animal species or tissue type is the best indicator for the polluting elements surveyed

  16. X-RAY AND RADIO EMISSION FROM TYPE IIn SUPERNOVA SN 2010jl

    Energy Technology Data Exchange (ETDEWEB)

    Chandra, Poonam [National Centre for Radio Astrophysics, Tata Institute of Fundamental Research, Pune University Campus, Pune 411 007 (India); Chevalier, Roger A. [Department of Astronomy, University of Virginia, P.O. Box 400325, Charlottesville, VA 22904-4325 (United States); Chugai, Nikolai [Institute of Astronomy of Russian Academy of Sciences, Pyatnitskaya St. 48, 109017 Moscow (Russian Federation); Fransson, Claes [Oskar Klein Centre, Department of Astronomy, Stockholm University, AlbaNova, SE-106 91 Stockholm (Sweden); Soderberg, Alicia M., E-mail: poonam@ncra.tifr.res.in [Smithsonian Astrophysical Observatory, 60 Garden St., MS-20, Cambridge, MA 02138 (United States)

    2015-09-01

    We present all X-ray and radio observations of the Type IIn supernova SN 2010jl. The X-ray observations cover a period up to day 1500 with Chandra, XMM-Newton, NuSTAR, and Swift-X-ray Telescope (XRT). The Chandra observations after 2012 June, the XMM-Newton observation in 2013 November, and most of the Swift-XRT observations until 2014 December are presented for the first time. All the spectra can be fitted by an absorbed hot thermal model except for Chandra spectra on 2011 October and 2012 June when an additional component is needed. Although the origin of this component is uncertain, it is spatially coincident with the supernova and occurs when there are changes to the supernova spectrum in the energy range close to that of the extra component, indicating that the emission is related to the supernova. The X-ray light curve shows an initial plateau followed by a steep drop starting at day ∼300. We attribute the drop to a decrease in the circumstellar density. The column density to the X-ray emission drops rapidly with time, showing that the absorption is in the vicinity of the supernova. We also present Very Large Array radio observations of SN 2010jl. Radio emission was detected from SN 2010jl from day 570 onwards. The radio light curves and spectra suggest that the radio luminosity was close to its maximum at the first detection. The velocity of the shocked ejecta derived assuming synchrotron self-absorption is much less than that estimated from the optical and X-ray observations, suggesting that free–free absorption dominates.

  17. Positron emission CT and X-ray CT findings in chronic obstructive pulmonary diseases

    Energy Technology Data Exchange (ETDEWEB)

    Sato, Yoshikazu; Murata, Kiyoshi; Ito, Harumi; Senda, Michio; Yonekura, Yoshiharu; Konishi, Junji; Nishimura, Koichi; Izumi, Takahide; Oshima, Shunsaku

    1987-08-01

    Positron emission CT and X-ray CT were performed in fifteen patients with emphysema confirmed SAB and twelve patients with clinical DPB. In patients with emphysema, 20 of 36 areas showed a central pattern and their perfusion scintigrams showed stripe-signs. On the other hand, the patients with DPB showed outer layer progression of the disease.

  18. Optimization of soft x-ray line emission from laser-produced carbon ...

    Indian Academy of Sciences (India)

    Intense XUV soft x-ray emission from laser-produced plasma sources is currently ... absorption edges of oxygen and carbon respectively) is particularly attractive as it permits ... ability of the target element producing intense discrete lines in the water .... ficient due to Pert [17] and dielectronic recombination coefficient due to ...

  19. Cometary X-ray Emission: the View After the First Chandra Observations

    Science.gov (United States)

    Lisse, C. M.

    2002-01-01

    The unexpected discovery of x-ray emission from Comet Hyakutake in March 1996 (Lisse et al. 1996) has produced a number of questions about the physical mechanism producing the radiation. The original detection and subsequent observations (Dennerl et al. 1997, Mumma et al. 1997, Krasnopolsky et al. 1998, Owens et al. 1998, Lisse et al. 1999) have shown that the very soft (best fit thermal bremsstrahlung model kT ~ 0.2 keV) emission is due to an interaction between the solar wind and the comet's atmosphere. Using the results from the 15 comets detected to date in x-rays, we report on the latest results on cometary x-ray emission, including new results from Chandra and XMM. As-observed morphologies, spectra, and light curves will be discussed. Our emphasis will be on understanding the physical mechanism producing the emission, and using this to determine the nature of the cometary coma, the structure of the solar wind in the heliosphere, and the source of the local soft x-ray background. This work has been graciously supported by grants from the NASA Planetary Astronomy and Astrophysical Data Programs.

  20. Correlation between X-ray and high energy gamma-ray emission form Cygnus X-3

    International Nuclear Information System (INIS)

    Weekes, T.C.; Danaher, S.; Fegan, D.J.; Porter, N.A.

    1981-01-01

    In May-June 1980, the 4.8 hour modulated X-ray flux from Cygnus X-3 underwent a significant change in the shape of the light curve; this change correlates with the peak in the high-energy (E > 2 x 10 12 eV) gamma ray emission at the same epoch. (orig.)

  1. X-ray emission from reverse-shocked ejecta in supernova remnants

    Science.gov (United States)

    Cioffi, Denis F.; Mckee, Christopher F.

    1990-01-01

    A simple physical model of the dynamics of a young supernova remnant is used to derive a straightforward kinematical description of the reverse shock. With suitable approximations, formulae can then be developed to give the X-ray emission of the reverse-shocked ejecta. The results are found to agree favorably with observations of SN1006.

  2. Interpretation of x-ray emission from lithium-like ions in collisions with helium

    International Nuclear Information System (INIS)

    Armen, G.B.; Aaberg, T.

    1994-01-01

    We consider the continuous x-ray distribution on the low-energy side of the K α line in projectile spectra coincident with single-electron loss in collision of lithium-like ions with helium. We demonstrate that the observed distributions are due to two-photon emission rather than to the radiative Auger effect. (author)

  3. X-ray Emission from the Radio Jet in 3C 120

    DEFF Research Database (Denmark)

    Harris, D. E.; Hjorth, J.; Sadun, A. C.

    1999-01-01

    We report the discovery of X-ray emission from a radio knot at a projected distance of 25" from the nucleus of the Seyfert galaxy, 3C 120. The data were obtained with the ROSAT High Resolution Imager (HRI). Optical upper limits for the knot preclude a simple power law extension of the radio...

  4. The Relationship Between Solar Radio and Hard X-Ray Emission

    Science.gov (United States)

    White, S. M.; Benz, A. O.; Christe, S.; Farnik, F.; Kundu, M. R.; Mann, G.; Ning, Z.; Raulin, J.-P.; Silva-Valio, A. V. R.; Saint-Hilaire, P.; hide

    2011-01-01

    This review discusses the complementary relationship between radio and hard Xray observations of the Sun using primarily results from the era of the Reuven Ramaty High Energy Solar Spectroscopic Imager satellite. A primary focus of joint radio and hard X-ray studies of solar flares uses observations of nonthermal gyrosynchrotron emission at radio wavelengths and bremsstrahlung hard X-rays to study the properties of electrons accelerated in the main flare site, since it is well established that these two emissions show very similar temporal behavior. A quantitative prescription is given for comparing the electron energy distributions derived separately from the two wavelength ranges: this is an important application with the potential for measuring the magnetic field strength in the flaring region, and reveals significant differences between the electrons in different energy ranges. Examples of the use of simultaneous data from the two wavelength ranges to derive physical conditions are then discussed, including the case of microflares, and the comparison of images at radio and hard X-ray wavelengths is presented. There have been puzzling results obtained from observations of solar flares at millimeter and submillimeter wavelengths, and the comparison of these results with corresponding hard X-ray data is presented. Finally, the review discusses the association of hard X-ray releases with radio emission at decimeter and meter wavelengths, which is dominated by plasma emission (at lower frequencies) and electron cyclotron maser emission (at higher frequencies), both coherent emission mechanisms that require small numbers of energetic electrons. These comparisons show broad general associations but detailed correspondence remains more elusive.

  5. Soft X-ray emission from the radio pulsar PSR 0656 + 14

    Science.gov (United States)

    Cordova, F. A.; Middleditch, J.; Hjellming, R. M.; Mason, K. O.

    1989-01-01

    A radio source with a flux density of a few mJy was found in the error region of the soft X-ray source E0656 + 14, and identified as the radio pulsar PSR 0656 + 14. The radio source has a steep, nonthermal spectrum and a high degree of linear (62 percent) and circular (19 percent) polarization. The X-ray spectrum of the pulsar is among the softest sources observed with the Einstein Observatory. The X-ray data taken with the Einstein imaging proportional counter (IPC) permit a range of blackbody temperatures of 3-6 x 10 to the 5th K, and an equivalent column density of hydrogen smaller than 4 x 10 to the 20th/sq cm. If the assumption is made that the X-ray flux is thermal radiation from surface of the neutron star, then the pulsar must be at a distance smaller than 550 pc, consistent with the low dispersion measure of PSR 0656 + 14. The X-ray timing data suggest that the X-ray emission is modulated at the pulsar's 0.385-s spin period with an amplitude of 18 percent + or - 6 percent, and that there is a 0.0002 probability that this is spurious. It was noted that PSR 0656 + 14 is close to the geometric center of a 20-deg diameter soft X-ray emitting ring called the Gemini-Monoceros enhancement. The close distance of the pulsar, together with its relatively young age of 1.1 x 10 to the 5th yr, makes it possible that the ring is a supernova remnant from the explosion of the pulsar's progenitor. A radio source extending over a region 1.2 to 3.3 arcmin south of the pulsar is a candidate for association with the pulsar.

  6. Soft X-ray emission from the radio pulsar PSR 0656 + 14

    International Nuclear Information System (INIS)

    Cordova, F.A.; Middleditch, J.; Hjellming, R.M.; Mason, K.O.

    1989-01-01

    A radio source with a flux density of a few mJy was found in the error region of the soft X-ray source E0656 + 14, and identified as the radio pulsar PSR 0656 + 14. The radio source has a steep, nonthermal spectrum and a high degree of linear (62%) and circular (19%) polarization. The X-ray spectrum of the pulsar is among the softest sources observed with the Einstein Observatory. The X-ray data taken with the Einstein imaging proportional counter (IPC) permit a range of blackbody temperatures of 3-6 x 10 to the 5th K, and an equivalent column density of hydrogen smaller than 4 x 10 to the 20th/sq cm. If the assumption is made that the X-ray flux is thermal radiation from surface of the neutron star, then the pulsar must be at a distance smaller than 550 pc, consistent with the low dispersion measure of PSR 0656 + 14. The X-ray timing data suggest that the X-ray emission is modulated at the pulsar's 0.385-s spin period with an amplitude of 18% + or - 6%, and that there is a 0.0002 probability that this is spurious. It was noted that PSR 0656 + 14 is close to the geometric center of a 20-deg diameter soft X-ray emitting ring called the Gemini-Monoceros enhancement. The close distance of the pulsar, together with its relatively young age of 1.1 x 10 to the 5th yr, makes it possible that the ring is a supernova remnant from the explosion of the pulsar's progenitor. A radio source extending over a region 1.2 to 3.3 arcmin south of the pulsar is a candidate for association with the pulsar. 46 refs

  7. Development of suitable plastic standards for X-ray fluorescence analysis

    Energy Technology Data Exchange (ETDEWEB)

    Mans, Christian [University of Applied Sciences Muenster, Department of Chemical Engineering, Advanced Analytical Chemistry, Stegerwaldstr. 39, 48565 Steinfurt (Germany)], E-mail: c.mans@fh-muenster.de; Hanning, Stephanie [University of Applied Sciences Muenster, Department of Chemical Engineering, Advanced Analytical Chemistry, Stegerwaldstr. 39, 48565 Steinfurt (Germany)], E-mail: hanning@fh-muenster.de; Simons, Christoph [University of Applied Sciences Muenster, Department of Chemical Engineering, Advanced Analytical Chemistry, Stegerwaldstr. 39, 48565 Steinfurt (Germany)], E-mail: simons@fh-muenster.de; Wegner, Anne [University of Applied Sciences Muenster, Department of Chemical Engineering, Advanced Analytical Chemistry, Stegerwaldstr. 39, 48565 Steinfurt (Germany)], E-mail: awegner@fh-muenster.de; Janssen, Anton [University of Applied Sciences Muenster, Department of Chemical Engineering, Advanced Analytical Chemistry, Stegerwaldstr. 39, 48565 Steinfurt (Germany)], E-mail: janssena@fh-muenster.de; Kreyenschmidt, Martin [University of Applied Sciences Muenster, Department of Chemical Engineering, Advanced Analytical Chemistry, Stegerwaldstr. 39, 48565 Steinfurt (Germany)], E-mail: martin.kreyenschmidt@fh-muenster.de

    2007-02-15

    For the adoption of the EU directive 'Restriction on use of certain Hazardous Substances' and 'Waste Electrical and Electronic Equipment' using X-ray fluorescence analysis suitable standard materials are required. Plastic standards based on acrylonitrile-butadiene-styrene terpolymer, containing the regulated elements Br, Cd, Cr, Hg and Pb were developed and produced as granulates and solid bodies. The calibration materials were not generated as a dilution from one master batch but rather the element concentrations were distributed over nine independent calibration samples. This was necessary to enable inter-elemental corrections and empirical constant mass absorption coefficients. The produced standard materials are characterized by a homogenous element distribution, which is more than sufficient for X-ray fluorescence analysis. Concentrations for all elements except for Br could be determined by Inductively Coupled Plasma Atomic Emission Spectroscopy after microwave assisted digestion. The concentration of Br was determined by use of Neutron Activation Analysis at Hahn-Meitner-Institute in Berlin, Germany. The correlation of the X-ray fluorescence analysis measurements with the values determined using Inductively Coupled Plasma Atomic Emission Spectroscopy and Neutron Activation Analysis showed a very good linearity.

  8. Intelligent support of X-ray qualitative analysis

    International Nuclear Information System (INIS)

    Arai, Hiroshi; Uota, Atsushi; Ishida, Hidenobu

    1995-01-01

    'X-ray Diffraction AI Qualitative Analysis System' which can support analytical operation was developed. The purpose of this development is that even a beginner analyst can obtain the accurate results as well as specialists. This system has three new functions. The first one is to determine the suitable measuring conditions automatically for samples or analytical aim. The second is to guide the method of peak search. And, the third is to determine searching conditions same as measuring conditions. These were realized by applying experts' knowledge with 'AI techniques' and were added to our qualitative analysis systems. A beginner analyses through dialogue with this system, and can get the same results as a specialist would get. (author)

  9. X-ray emission in slow highly charged ion-surface collisions

    International Nuclear Information System (INIS)

    Watanabe, H; Abe, T; Fujita, Y; Sun, J; Takahashi, S; Tona, M; Yoshiyasu, N; Nakamura, N; Sakurai, M; Yamada, C; Ohtani, S

    2007-01-01

    X-rays emitted in the collisions of highly charged ions with a surface have been measured to investigate dissipation schemes of their potential energies. While 8.1% of the potential energy was dissipated in the collisions of He-like I ions with a W surface, 29.1% has been dissipated in the case of He-like Bi ions. The x-ray emissions play significant roles in the dissipation of the potential energies in the interaction of highly charged heavy ions with the surface

  10. Observation of hard X-rays line emission from Her X-1

    Energy Technology Data Exchange (ETDEWEB)

    Polcaro, V.F.; Bazzano, A.; la Padula, C.; Ubertini, P.; Vialetto, G.; Manchanda, R.K.; Damle, S.V.

    1982-04-01

    We present the results of a hard X-ray measurement of the binary source Her X-1, carried out with a balloon borne X-ray telescope consisting of two Multiwire Proportional Counters, having 900 cm/sup 2/ sensitive area each and spectral resolution of 15% and 24% FWHM respectively at 60 keV. The source was observed during the 'Mid-on' state. Our data confirm the previously reported high energy emission line overimposed on the low energy thermal spectrum.

  11. Polarized X-Ray Emission from Magnetized Neutron Stars: Signature of Strong-Field Vacuum Polarization

    Science.gov (United States)

    Lai, Dong; Ho, Wynn C.

    2003-08-01

    In the atmospheric plasma of a strongly magnetized neutron star, vacuum polarization can induce a Mikheyev-Smirnov-Wolfenstein type resonance across which an x-ray photon may (depending on its energy) convert from one mode into the other, with significant changes in opacities and polarizations. We show that this vacuum resonance effect gives rise to a unique energy-dependent polarization signature in the surface emission from neutron stars. The detection of polarized x rays from neutron stars can provide a direct probe of strong-field quantum electrodynamics and constrain the neutron star magnetic field and geometry.

  12. Polarized x-ray emission from magnetized neutron stars: signature of strong-field vacuum polarization.

    Science.gov (United States)

    Lai, Dong; Ho, Wynn C G

    2003-08-15

    In the atmospheric plasma of a strongly magnetized neutron star, vacuum polarization can induce a Mikheyev-Smirnov-Wolfenstein type resonance across which an x-ray photon may (depending on its energy) convert from one mode into the other, with significant changes in opacities and polarizations. We show that this vacuum resonance effect gives rise to a unique energy-dependent polarization signature in the surface emission from neutron stars. The detection of polarized x rays from neutron stars can provide a direct probe of strong-field quantum electrodynamics and constrain the neutron star magnetic field and geometry.

  13. THE SPECTACULAR RADIO-NEAR-IR-X-RAY JET OF 3C 111: THE X-RAY EMISSION MECHANISM AND JET KINEMATICS

    Energy Technology Data Exchange (ETDEWEB)

    Clautice, Devon; Perlman, Eric S. [Department of Physics and Space Sciences, Florida Institute of Technology, 150 W. University Boulevard, Melbourne, FL 32901 (United States); Georganopoulos, Markos [Department of Physics, University of Maryland—Baltimore County, 1000 Hilltop Circle, Baltimore, MD 21250 (United States); Lister, Matthew L.; Hogan, Brandon [Department of Physics and Astronomy, Purdue University, 525 Northwestern Avenue, West Lafayette, IN 47907 (United States); Tombesi, Francesco [Department of Astronomy, University of Maryland, College Park, MD 20742-2421 (United States); Cara, Mihai [Space Telescope Science Institute, 3700 San Martin Drive, Baltimore, MD 21218 (United States); Marshall, Herman L. [Kavli Institute for Astrophysics and Space Research, Massachusetts Institute of Technology, Cambridge, MA 02139 (United States); Kazanas, Demos [NASA’s Goddard Space Flight Center, Astrophysics Science Division, Code 663, Greenbelt, MD 20771 (United States)

    2016-08-01

    Relativistic jets are the most energetic manifestation of the active galactic nucleus (AGN) phenomenon. AGN jets are observed from the radio through gamma-rays and carry copious amounts of matter and energy from the sub-parsec central regions out to the kiloparsec and often megaparsec scale galaxy and cluster environs. While most spatially resolved jets are seen in the radio, an increasing number have been discovered to emit in the optical/near-IR and/or X-ray bands. Here we discuss a spectacular example of this class, the 3C 111 jet, housed in one of the nearest, double-lobed FR II radio galaxies known. We discuss new, deep Chandra and Hubble Space Telescope ( HST ) observations that reveal both near-IR and X-ray emission from several components of the 3C 111 jet, as well as both the northern and southern hotspots. Important differences are seen between the morphologies in the radio, X-ray, and near-IR bands. The long (over 100 kpc on each side), straight nature of this jet makes it an excellent prototype for future, deep observations, as it is one of the longest such features seen in the radio, near-IR/optical, and X-ray bands. Several independent lines of evidence, including the X-ray and broadband spectral shape as well as the implied velocity of the approaching hotspot, lead us to strongly disfavor the EC/CMB model and instead favor a two-component synchrotron model to explain the observed X-ray emission for several jet components. Future observations with NuSTAR , HST , and Chandra will allow us to further constrain the emission mechanisms.

  14. Evaluating fracture healing using digital x-ray image analysis

    African Journals Online (AJOL)

    2011-03-02

    Mar 2, 2011 ... with intensive imaging and modelling.6 dual energy X-ray ... techniques due to their high-quality digital output in ... the bone in the loaded X-ray is at an angular offset due to .... The research described in this article was carried ...

  15. X-RAY EMISSION FROM SUPERNOVAE IN DENSE CIRCUMSTELLAR MATTER ENVIRONMENTS: A SEARCH FOR COLLISIONLESS SHOCKS

    International Nuclear Information System (INIS)

    Ofek, E. O.; Gal-Yam, A.; Yaron, O.; Arcavi, I.; Fox, D.; Cenko, S. B.; Filippenko, A. V.; Bloom, J. S.; Sullivan, M.; Gnat, O.; Frail, D. A.; Horesh, A.; Kulkarni, S. R.; Corsi, A.; Quimby, R. M.; Gehrels, N.; Nugent, P. E.; Kasliwal, M. M.; Bildsten, L.; Poznanski, D.

    2013-01-01

    The optical light curve of some supernovae (SNe) may be powered by the outward diffusion of the energy deposited by the explosion shock (the so-called shock breakout) in optically thick (τ ∼> 30) circumstellar matter (CSM). Recently, it was shown that the radiation-mediated and radiation-dominated shock in an optically thick wind must transform into a collisionless shock and can produce hard X-rays. The X-rays are expected to peak at late times, relative to maximum visible light. Here we report on a search, using Swift/XRT and Chandra, for X-ray emission from 28 SNe that belong to classes whose progenitors are suspected to be embedded in dense CSM. Our sample includes 19 Type IIn SNe, one Type Ibn SN, and eight hydrogen-poor superluminous SNe (SLSN-I such as SN 2005ap). Two SNe (SN 2006jc and SN 2010jl) have X-ray properties that are roughly consistent with the expectation for X-rays from a collisionless shock in optically thick CSM. However, the X-ray emission from SN 2006jc can also be explained as originating in an optically thin region. Thus, we propose that the optical light curve of SN 2010jl is powered by shock breakout in CSM. We suggest that two other events (SN 2010al and SN 2011ht) were too X-ray bright during the SN maximum optical light to be explained by the shock-breakout model. We conclude that the light curves of some, but not all, SNe IIn/Ibn are powered by shock breakout in CSM. For the rest of the SNe in our sample, including all of the SLSN-I events, our X-ray limits are not deep enough and were typically obtained too early (i.e., near the SN maximum light) for definitive conclusions about their nature. Late-time X-ray observations are required in order to further test whether these SNe are indeed embedded in dense CSM. We review the conditions required for a shock breakout in a wind profile. We argue that the timescale, relative to maximum light, for the SN to peak in X-rays is a probe of the column density and the density profile above the

  16. CORRELATION OF HARD X-RAY AND WHITE LIGHT EMISSION IN SOLAR FLARES

    Energy Technology Data Exchange (ETDEWEB)

    Kuhar, Matej; Krucker, Säm; Battaglia, Marina; Kleint, Lucia; Casadei, Diego [University of Applied Sciences and Arts Northwestern Switzerland, Bahnhofstrasse 6, 5210 Windisch (Switzerland); Oliveros, Juan Carlos Martinez; Hudson, Hugh S. [Space Sciences Laboratory, University of California, Berkeley, CA 94720-7450 (United States)

    2016-01-01

    A statistical study of the correlation between hard X-ray and white light emission in solar flares is performed in order to search for a link between flare-accelerated electrons and white light formation. We analyze 43 flares spanning GOES classes M and X using observations from the Reuven Ramaty High Energy Solar Spectroscopic Imager and Helioseismic and Magnetic Imager. We calculate X-ray fluxes at 30 keV and white light fluxes at 6173 Å summed over the hard X-ray flare ribbons with an integration time of 45 s around the peak hard-X ray time. We find a good correlation between hard X-ray fluxes and excess white light fluxes, with a highest correlation coefficient of 0.68 for photons with energy of 30 keV. Assuming the thick target model, a similar correlation is found between the deposited power by flare-accelerated electrons and the white light fluxes. The correlation coefficient is found to be largest for energy deposition by electrons above ∼50 keV. At higher electron energies the correlation decreases gradually while a rapid decrease is seen if the energy provided by low-energy electrons is added. This suggests that flare-accelerated electrons of energy ∼50 keV are the main source for white light production.

  17. Dissecting Diffuse X-ray Emission in 30 Doradus with T-ReX

    Science.gov (United States)

    Townsley, Leisa K.; Broos, Patrick

    2017-08-01

    30 Doradus (the Tarantula Nebula) offers us a microscope on starburst astrophysics, having endured 25 Myrs of the birth and death of the most massive stars known. Across 30 Dor's 250-pc extent, stellar winds and supernovae have carved its ISM into an amazing display of arcs, pillars, and bubbles. For over 40 years, we have also known that 30 Dor is a bright X-ray emitter, so its familiar stars and cold ISM structures suffer irradiation by multi-million-degree plasmas. The 2-Ms Chandra X-ray Visionary Project ``The Tarantula -- Revealed by X-rays'' (T-ReX) exploits Chandra's fine spatial resolution and the ACIS-I field of view to study ISM interfaces on 1--10 pc scales across the entire 30 Dor complex. Here we give preliminary results from ongoing analyses of these data, focusing on the diffuse X-ray emission. Massive star winds and cavity supernovae over the millenia have contributed to a broad mix of X-ray-emitting plasmas and absorbing columns, showing that 30 Dor's hot ISM is just as complex and confusing as that seen at colder temperatures.

  18. Current sheath curvature correlation with the neon soft x-ray emission from plasma focus device

    International Nuclear Information System (INIS)

    Zhang, T; Lin, X; Chandra, K A; Tan, T L; Springham, S V; Patran, A; Lee, P; Lee, S; Rawat, R S

    2005-01-01

    The insulator sleeve length is one of the major parameters that can severely affect the neon soft x-ray yield from a plasma focus. The effect of the insulation sleeve length on various characteristic timings of plasma focus discharges and hence the soft x-ray emission characteristics has been investigated using a resistive divider. The pinhole images and laser shadowgraphy are used to explain the observed variation in the average soft x-ray yield (measured using a diode x-ray spectrometer) with variation of the insulator sleeve length. We have found that for a neon filled plasma focus device the change in insulator sleeve length changes the current sheath curvature angle and thus the length of the focused plasma column. The optimized current sheath curvature angle is found to be between 39 0 and 41 0 , at the specific axial position of 6.2-9.3 cm from the cathode support plate, for our 3.3 kJ plasma focus device. A strong dependence of the neon soft x-ray yield on the current sheath curvature angle has thus been reported

  19. Characterization of metallic nanoparticles by high-resolution X-ray absorption and X-ray emission spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Kuehn, Timna-Josua

    2012-03-15

    In almost all areas of technology, metallic nanoparticles are of interest due to their special thermal, electronic, magnetic and optical properties. Their special properties are mainly due to their small size which implies the relevance of quantum effects as well as the significance of the surface: For 2 nm nanoparticles, the surface-to-volume ratio is already 1:1. However, the identification of surface-to-volume interactions - that are responsible for the new properties - is a difficult task due to the small size that inhibits a lot of 'standard' techniques to be applicable. Here X-ray absorption/emission spectroscopy (XAS/XES) is a favorable tool for the characterization of nanoparticles, independent on size, degree of crystallinity and shape/condition of the surface. Using XAS, a tempered nanosized Co{sub 3}Pt/C catalyst have been investigated. Its outstanding oxygen-reduction reaction (ORR) properties in a fuel cell could be related to a lowered Pt 5d-band center connected to a tightened Pt-Pt bonding distance, leading to a weakening of the oxygen adsorption strength so that the ORR may proceed faster. One drawback remains, however, as the properties found by (standard) XAS are summed up for different chemical environments of the chosen element. Thus, no distinction can be made between, e.g., the pure metal in a nanoparticles' interior and the ligated metal in the outer shells or surface. Here, high-resolution fluorescence-detected XAS (HRFD-XAS) provides additional opportunities as, due to its chemical sensitivity, it leads to site-selective XAS. For a system of 6 nm sized Co nanoparticles, build up of a metallic core surrounded by a protecting shell, that resulted from the 'smooth oxidation' process, this technique of site-selective XAS was proven to be applicable. For the first time, the interior and outer shell of a metallic nanoparticle could be characterized separately. In particular, the Co-hcp phase could be determined for the

  20. The proton induced X-ray emission (PIXE) for the quantitative analysis of elements in thin samples, in surface layers of thick samples, and in aerosol filters

    International Nuclear Information System (INIS)

    Waetjen, U.

    1983-01-01

    The PIXE analysis method for the determination of elements in thick samples was investigated. The text of the present thesis is arranged under the following headings: physical fundamentals and measuring equipment, quantitative analysis of thin samples, matrix effects at the PIXE analysis of thick samples, matrix correction methods, analysis of 'infinite thick' model substances, PIXE analysis of aerosol filters. (GSCH)

  1. Application of synchrotron radiation to x-ray fluorescence analysis of trace elements

    International Nuclear Information System (INIS)

    Gordon, B.M.; Jones, K.W.; Hanson, A.L.

    1986-08-01

    The development of synchrotron radiation x-ray sources has provided the means to greatly extend the capabilities of x-ray fluorescence analysis for determinations of trace element concentrations. A brief description of synchrotron radiation properties provides a background for a discussion of the improved detection limits compared to existing x-ray fluorescence techniques. Calculated detection limits for x-ray microprobes with micrometer spatial resolutions are described and compared with experimental results beginning to appear from a number of laboratories. The current activities and future plans for a dedicated x-ray microprobe beam line at the National Synchrotron Light Source (NSLS) of Brookhaven National Laboratory are presented

  2. Revising the Local Bubble Model due to Solar Wind Charge Exchange X-ray Emission

    Science.gov (United States)

    Shelton, Robin L.

    2009-03-01

    The hot Local Bubble surrounding the solar neighborhood has been primarily studied through observations of its soft X-ray emission. The measurements were obtained by attributing all of the observed local soft X-rays to the bubble. However, mounting evidence shows that the heliosphere also produces diffuse X-rays. The source is solar wind ions that have received an electron from another atom. The presence of this alternate explanation for locally produced diffuse X-rays calls into question the existence and character of the Local Bubble. This article addresses these questions. It reviews the literature on solar wind charge exchange (SWCX) X-ray production, finding that SWCX accounts for roughly half of the observed local 1/4 keV X-rays found at low latitudes. This article also makes predictions for the heliospheric O VI column density and intensity, finding them to be smaller than the observational error bars. Evidence for the continued belief that the Local Bubble contains hot gas includes the remaining local 1/4 keV intensity, the observed local O VI column density, and the need to fill the local region with some sort of plasma. If the true Local Bubble is half as bright as previously thought, then its electron density and thermal pressure are 1/sqrt{2} as great as previously thought, and its energy requirements and emission measure are 1/2 as great as previously thought. These adjustments can be accommodated easily, and, in fact, bring the Local Bubble’s pressure more in line with that of the adjacent material. Suggestions for future work are made.

  3. Uranium concentrate analysis by X-ray fluorescence spectroscopy

    International Nuclear Information System (INIS)

    Diaz-Guerra, J.P.; Bayon, A.; Roca, R.

    1978-01-01

    The determination of As, Ca, Fe, Mo, P, S, Si. Th, V and U in uranium concentrates by X-ray fluorescence spectroscopy has been studied. As and U are determined in nitric solutions and for the rest of elements analysis is performed by a bead fusion technique using Li 2 B 4 O 7 and Li 2 CO 3 as fluxes. Although the uranium matrix minimizes the absorption and enhancement effects, because of the content variations of this element it is advisable to operate at a constant level of U 3 O 8 . Despite the high matrix absorption and the large dilution of the samples, sensitivity and speed are found to be satisfactory as the result of the use of a high sensitivity automatic spectrometer. The spectral interferences of Mo on S and P, and of Pb on As have been particularly considered. (author) [es

  4. X-RAY EMISSION FROM THE WOLF-RAYET BUBBLE S 308

    Energy Technology Data Exchange (ETDEWEB)

    Toala, J. A.; Guerrero, M. A. [Instituto de Astrofisica de Andalucia, IAA-CSIC, Glorieta de la Astronomia s/n, 18008 Granada (Spain); Chu, Y.-H.; Gruendl, R. A. [Department of Astronomy, University of Illinois, 1002 West Green Street, Urbana, IL 61801 (United States); Arthur, S. J. [Centro de Radioastronomia y Astrofisica, Universidad Nacional Autonoma de Mexico, Campus Morelia, Apartado Postal 3-72, 58090, Morelia, Michoacan (Mexico); Smith, R. C. [NOAO/CTIO, 950 N. Cherry Avenue, Tucson, AZ 85719 (United States); Snowden, S. L., E-mail: toala@iaa.es [NASA Goddard Space Flight Center, Code 662, Greenbelt, MD 20771 (United States)

    2012-08-10

    The Wolf-Rayet (WR) bubble S 308 around the WR star HD 50896 is one of the only two WR bubbles known to possess X-ray emission. We present XMM-Newton observations of three fields of this WR bubble that, in conjunction with an existing observation of its northwest quadrant, map most of the nebula. The X-ray emission from S 308 displays a limb-brightened morphology, with a central cavity {approx}22' in size and a shell thickness of {approx}8'. This X-ray shell is confined by the optical shell of ionized material. The spectrum is dominated by the He-like triplets of N VI at 0.43 keV and O VII at 0.57 keV, and declines toward high energies, with a faint tail up to 1 keV. This spectrum can be described by a two-temperature optically thin plasma emission model (T{sub 1} {approx} 1.1 Multiplication-Sign 10{sup 6} K, T{sub 2} {approx} 13 Multiplication-Sign 10{sup 6} K), with a total X-ray luminosity {approx}2 Multiplication-Sign 10{sup 33} erg s{sup -1} at the assumed distance of 1.5 kpc.

  5. X-RAY EMISSION FROM THE WOLF-RAYET BUBBLE S 308

    International Nuclear Information System (INIS)

    Toalá, J. A.; Guerrero, M. A.; Chu, Y.-H.; Gruendl, R. A.; Arthur, S. J.; Smith, R. C.; Snowden, S. L.

    2012-01-01

    The Wolf-Rayet (WR) bubble S 308 around the WR star HD 50896 is one of the only two WR bubbles known to possess X-ray emission. We present XMM-Newton observations of three fields of this WR bubble that, in conjunction with an existing observation of its northwest quadrant, map most of the nebula. The X-ray emission from S 308 displays a limb-brightened morphology, with a central cavity ∼22' in size and a shell thickness of ∼8'. This X-ray shell is confined by the optical shell of ionized material. The spectrum is dominated by the He-like triplets of N VI at 0.43 keV and O VII at 0.57 keV, and declines toward high energies, with a faint tail up to 1 keV. This spectrum can be described by a two-temperature optically thin plasma emission model (T 1 ∼ 1.1 × 10 6 K, T 2 ∼ 13 × 10 6 K), with a total X-ray luminosity ∼2 × 10 33 erg s –1 at the assumed distance of 1.5 kpc.

  6. Development of a Reference Database for Particle Induced Gamma Ray Emission (PIGE) Spectroscopy

    International Nuclear Information System (INIS)

    2017-09-01

    Ion beam analysis techniques are non-destructive analytical techniques used to identify the composition and structure of surface layers of materials. The applications of these techniques span environmental control, cultural heritage and conservation, materials and fusion technologies. The particle-induced gamma-ray emission (PIGE) spectroscopy technique in particular, is a powerful tool for detecting light elements in certain depths of surface layers. This publication describes the coordinated effort to measure and compile cross section data relevant to PIGE analysis and make these data available to the community of practice through a comprehensive online database.

  7. Application of proton induced x-ray emission (PIXE) in estimation of trace metals entrapped in silica matrix

    International Nuclear Information System (INIS)

    Jal, P.K.; Patel, Sabita; Mishra, B.K.; Sudarshan, M.; Saha, A.

    2005-01-01

    Proton induced x-ray emission technique is used for multielemental analysis of metal ions adsorbed on nanosilica surface. At pH 3.5, silica traps uranium selectively from a mixture of solutions of 13 different metal ions viz., K(I), Ca(II), Fe(III), Mn(II), Co(II), Ni(II), Cu(II), Zn(II), Sr(II), Cd(II). Ba(II), Hg(II) and UO 2 (VI). (author)

  8. Exploring the Diffuse X-ray Emission of Supernova Remnant Kesteven 69 with XMM-Newton

    Directory of Open Access Journals (Sweden)

    Kyoung-Ae Seo

    2013-06-01

    Full Text Available We have investigated the X-ray emission from the shock-heated plasma of the Galactic supernova remnant Kesteven 69 with XMM-Newton. Assuming the plasma is at collisional ionization equilibrium, a plasma temperature and a column absorption are found to be kT ~ 0.62 keV and NH ~ 2.85 ×1022 cm-2 respectively by imaging spectroscopy. Together with the deduced emission measure, we place constraints on its Sedov parameters.

  9. Background approximation in automatic qualitative X-ray-fluorescent analysis

    International Nuclear Information System (INIS)

    Jordanov, J.; Tsanov, T.; Stefanov, R.; Jordanov, N.; Paunov, M.

    1982-01-01

    An empirical method of finding the dependence of the background intensity (Isub(bg) on the wavelength is proposed, based on the approximation of the experimentally found values for the background in the course of an automatic qualitative X-ray fluorescent analysis with pre-set curve. It is assumed that the dependence I(lambda) will be well approximated by a curve of the type Isub(bg)=(lambda-lambda sub(o)sup(fsub(1)(lambda))exp[fsub(2)(lambda)] where fsub(1) (lambda) and f 2 (lambda) are linear functions with respect to the sought parameters. This assumption was checked out on a ''pure'' starch background, in which it is not known beforehand which points belong to the background. It was assumed that the dependence I(lambda) can be found from all minima in the spectrum. Three types of minima has been distinguished: 1. the lowest point between two well-solved X-ray lines; 2. a minimum obtained as a result of statistical fluctuations of the measured signal; 3. the lowest point between two overlapped lines. The minima strongly deviating from the background are removed from the obtained set. The sum-total of the remaining minima serves as a base for the approximation of the dependence I(lambda). The unknown parameters are determined by means of the LSM. The approximated curve obtained by this method is closer to the real background than the background determined by the method described by Kigaki Denki, as the effect of all recorded minima is taken into account. As an example the PbTe spectrum recorded with crystal LiF 220 is shown graphically. The curve well describes the background of the spectrum even in the regions in which there are no minima belonging to the background. (authors)

  10. Data reduction and analysis for the graphite crystal X-ray spectrometer and polarimeter experiment flown aboard OSO-8 spacecraft

    Science.gov (United States)

    Novick, R.

    1980-01-01

    The documentation and software programs developed for the reception, initial processing (quickbook), and production analysis of data obtained by solar X-ray spectroscopy, stellar spectroscopy, and X-ray polarimetry experiments on OSO-8 are listed. The effectiveness and sensitivity of the Bragg crystal scattering instruments used are assessed. The polarization data polarimetric data obtained shows that some X-ray sources are polarized and that a larger polarimeter of this type is required to perform the measurements necessary to fully understand the physics of X-ray sources. The scanning Bragg crystal spectrometer was ideally suited for studying rapidly changing solar conditions. Observations of the Crab Nebula and pulsar, Cyg X-1, Cyg X-2, Cyg X-3, Sco X-1, Cen X-3, and Her X-1 are discussed as well as of 4U1656-53 and 4U1820-30. Evidence was obtained for iron line emission from Cyg X-3.

  11. A plastic miniature x-ray emission spectrometer based on the cylindrical von Hamos geometry

    International Nuclear Information System (INIS)

    Mattern, B. A.; Seidler, G. T.; Haave, M.; Pacold, J. I.; Gordon, R. A.; Planillo, J.; Quintana, J.; Rusthoven, B.

    2012-01-01

    We present a short working distance miniature x-ray emission spectrometer (miniXES) based on the cylindrical von Hamos geometry. We describe the general design principles for the spectrometer and detail a specific implementation that covers Kβ and valence level emission from Fe. Large spatial and angular access to the sample region provides compatibility with environmental chambers, microprobe, and pump/probe measurements. The primary spectrometer structure and optic is plastic, printed using a 3-dimensional rapid-prototype machine. The spectrometer is inexpensive to construct and is portable; it can be quickly set up at any focused beamline with a tunable narrow bandwidth monochromator. The sample clearance is over 27 mm, providing compatibility with a variety of environment chambers. An overview is also given of the calibration and data processing procedures, which are implemented by a multiplatform user-friendly software package. Finally, representative measurements are presented. Background levels are below the level of the Kβ 2,5 valence emission, the weakest diagram line in the system, and photometric analysis of count rates finds that the instrument is performing at the theoretical limit.

  12. Characterizing the X-ray Emission in Small Magellanic Cloud Supernova Remnants

    Science.gov (United States)

    Man, Nicole; Auchettl, Katie; Lopez, Laura

    2018-01-01

    The Small Magellanic Cloud is a close, metal-poor galaxy with active star formation, and it has a diverse population of 24 supernova remnants (SNRs) that have been identified at several wavelengths. Past work has characterized the X-ray emission in these sources separately and aimed to constrain their explosive origins from observations with Chandra and XMM-Newton. Three SNRs have possible evidence for Type Ia explosions based on strong Fe-L emission in their X-ray spectra, although the environments and intermediate-mass element abundances are more consistent with those of core-collapse SNe. In this poster, we analyze the archival Chandra and XMM-Newton observations of the SMC SNR sample, and we model the sources' X-ray spectra in a systematic way to derive the plasma properties and to constrain the nature of the explosions. In one SNR, we note the presence of an X-ray binary near the source's geometric center, suggesting the compact object was produced in the SN explosion. As one of only three SNRs known in the Local Group to host a binary system, this source is worthy of follow-up investigations to probe explosions of massive stars in binary systems.

  13. Efficient high-resolution X-ray emission spectrometry using synchrotron radiation

    International Nuclear Information System (INIS)

    Unterumsberger, Rainer

    2015-01-01

    The aim of the present work is to get access to high-resolution X-Ray Emission Spectrometry (XES) at nanoscaled materials, consisting of light elements and transition metals, by the increase of the sensitivity of a Wavelength-Dispersive Spectrometer (WDS) in the soft X-Ray range. The increase of the sensitivity was achieved by a refocusing of the incident radiation. With the increased sensitivity of the WDS, it was possible to determine the chemical species of different, nominal 100 nm thin titanium oxides. The combination of the refocusing optic and calibrated spectrometer enabled the detection and deconvolution of the L-fluorescence radiation of these nanoscaled titanium oxides. Due to the calibration of the spectrometer, a reliable determination of the transition probabilities of the titanium La- and Ll-fluorescence lines as a function of the chemical state is possible. To the best of my knowledge, the determination of the transition probabilities as a function of the chemical state in the soft X-Ray range has not been investigated yet. The quality of the refocusing was characterized using different diagnostic tools. Vertical full width at half maximum (FWHM) values of the focused beam between 10 μm to 20 μm and horizontal FWHM values between 12 μm and 25 μm could be achieved over an energy range of 180 eV to 1310 eV. Using calibrated photodiodes, it was possible to determine the absolute transmission of the used single bounce monocapillary as well as to monitor the absolute photon flux. By means of the refocusing, it was possible to increase the photon flux by a factor of 4.9 experimentally. The increase of the photon flux enables the analysis of nanoscaled materials with the used spectrometer. This could be shown based on the determination of the lower limit of detection of boron Ka and titanium La. In both cases, the lower limit of detection of 0.4 nm equivalent layer thickness was achieved (about 1.10 -7 g/cm 2 to 2.10 -7 g/cm 2 or 3.10 15 atoms/cm 2 to

  14. Soft X-ray synchrotron radiation investigations of actinide materials systems utilizing X-ray emission spectroscopy and resonant inelastic X-ray scattering

    International Nuclear Information System (INIS)

    Shuh, D.K.; Butorin, S.M.; Guo, J.-H.; Nordgren, J.

    2004-01-01

    Synchrotron radiation (SR) methods have been utilized with increasing frequency over the past several years to study topics in actinide science, ranging from those of a fundamental nature to those that address a specifically-targeted technical need. In particular, the emergence of microspectroscopic and fluorescence-based techniques have permitted investigations of actinide materials at sources of soft x-ray SR. Spectroscopic techniques with fluorescence-based detection are useful for actinide investigations since they are sensitive to small amounts of material and the information sampling depth may be varied. These characteristics also serve to simplify both sample preparation and safety considerations. Examples of investigations using these fluorescence techniques will be described along with their results, as well as the prospects for future investigations utilizing these methodologies

  15. Where is the X-ray emission coming from in RT Cru Symbiotic System?

    Science.gov (United States)

    Karovska, Margarita

    2014-11-01

    RT Cru is a member of a new sub-class of symbiotic interacting binaries with copious hard X-ray emission. It consists of a high-mass WD (>1.3 Ms) accreting from the wind of an M giant, and it is an important system to study in order to constrain precursor conditions for asymmetric PN and SN Ia. The Chandra HRC-I observation (Dec 2012), and an overlapping Swift observation, detected intermittent soft X-ray flaring, and we find evidence for a significant soft component in the spectrum. The flaring could be a consequence of clumped absorption columns moving in and out of the line of sight, or the variations could be due to changes at the accretion boundary layer. Further observations are needed to determine the origin of the soft emission and its relation to the hard emission.

  16. Resonant x-ray emission from gas-phase TiCl{sub 4}

    Energy Technology Data Exchange (ETDEWEB)

    Hague, C.F.; Tronc, M. [Universite Pierre et Marie Curie, Paris (France); De Groot, F. [Univ. of Groningen (Netherlands)] [and others

    1997-04-01

    Resonant x-ray emission spectroscopy (RXES) has proved to be a powerful tool for studying the electronic structure of condensed matter. Over the past few years it has been used mainly for studying the valence bands of solids and condensed molecules. Very recently the advent of high brightness photon beams provided by third generation synchrotron radiation source undulators, associated with efficient x-ray emission spectrometers has made it possible to perform experiments on free diatomic molecular systems. RXE spectra of free molecules are of prime importance to gain insight into their electronic structure and bonding as they reflect the symmetry of orbitals engaged in the two-electron, two-step process with the l = 0, {+-}2 parity-conserving selection rule, and are free from solid state effects which can introduce difficulties in the interpretation. They provide information (more so than XAS) on the core excited states, and, when performed at fixed incident photon energy as a function of the emitted photon energy, on the electronic excitation (charge transfer, multiplet states). Moreover the anisotropy of the angular distribution of resonant x-ray emission affects the relative intensity of the emission peaks and provides information concerning the symmetries of final states. This is a preliminary report on what are the first RXE spectra of a 3d transition metal complex in the gas phase. The experiment concerns the Ti 3d {yields}2p emission spectrum of TiCl{sub 4} over the 450 to 470 eV region.

  17. Resonant x-ray emission from gas-phase TiCl4

    International Nuclear Information System (INIS)

    Hague, C.F.; Tronc, M.; De Groot, F.

    1997-01-01

    Resonant x-ray emission spectroscopy (RXES) has proved to be a powerful tool for studying the electronic structure of condensed matter. Over the past few years it has been used mainly for studying the valence bands of solids and condensed molecules. Very recently the advent of high brightness photon beams provided by third generation synchrotron radiation source undulators, associated with efficient x-ray emission spectrometers has made it possible to perform experiments on free diatomic molecular systems. RXE spectra of free molecules are of prime importance to gain insight into their electronic structure and bonding as they reflect the symmetry of orbitals engaged in the two-electron, two-step process with the l = 0, ±2 parity-conserving selection rule, and are free from solid state effects which can introduce difficulties in the interpretation. They provide information (more so than XAS) on the core excited states, and, when performed at fixed incident photon energy as a function of the emitted photon energy, on the electronic excitation (charge transfer, multiplet states). Moreover the anisotropy of the angular distribution of resonant x-ray emission affects the relative intensity of the emission peaks and provides information concerning the symmetries of final states. This is a preliminary report on what are the first RXE spectra of a 3d transition metal complex in the gas phase. The experiment concerns the Ti 3d →2p emission spectrum of TiCl 4 over the 450 to 470 eV region

  18. Chandra Observations of Extended X-Ray Emission in ARP 220

    Science.gov (United States)

    McDowell, J. C.; Clements, D. L.; Lamb, S. A.; Shaked, S.; Hearn, N. C.; Colina, L.; Mundell, C.; Borne, K.; Baker, A. C.; Arribas, S.

    2003-01-01

    We resolve the extended X-ray emission from the prototypical ultraluminous infrared galaxy Arp 220. Extended, faint, edge-brightened, soft X-ray lobes outside the optical galaxy are observed to a distance of 1CL 15 kpc on each side of the nuclear region. Bright plumes inside the optical isophotes coincide with the optical line emission and extend 1 1 kpc from end to end across the nucleus. The data for the plumes cannot be fitted by a single-temperature plasma and display a range of temperatures from 0.2 to 1 keV. The plumes emerge from bright, diffuse circumnuclear emission in the inner 3 kpc centered on the Ha peak, which is displaced from the radio nuclei. There is a close morphological correspondence between the Ha and soft X-ray emission on all spatial scales. We interpret the plumes as a starburst-driven superwind and discuss two interpretations of the emission from the lobes in the context of simulations of the merger dynamics of Arp 220.

  19. X-ray fluorescence analysis of Fe - Ni - Mo systems

    International Nuclear Information System (INIS)

    Belyaev, E.E.; Ershov, A.V.; Mashin, A.I.; Mashin, N.I.; Rudnevskij, N.K.

    1998-01-01

    Procedures for the X-ray fluorescence determination of the composition and thickness of Fe - Ni - Mo thin films and the concentration of elements in thick films of the Fe - Ni - Mo alloy are developed [ru

  20. Rapid rock analysis and microprobe scanning of dermatological material using proton-induced x-ray and γ-ray emission

    International Nuclear Information System (INIS)

    Carlsson, L.E.

    1983-01-01

    The dissertation report comprises 6 articles that have or will appear in open literature. The use of PIXE and PIGE analysis techniques on geological materials, and also on drill cores, is discussed. The accuracy of the methods have been tested on standards. The effect of sample thickness has been studied. A proton microprobe has been compared with an electron microprobe on human skin sections. Both probes give highly reproducible results, but a small systematic deviation between the probes is found. (author)

  1. Proton Induced X-Ray Emission (PIXE) Analysis to Measure Trace Metals in Soil Along the East River in Queens, New York

    Science.gov (United States)

    Chalise, Sajju; Conlan, Skye; Porat, Zachary; Labrake, Scott; Vineyard, Michael

    2017-09-01

    The Union College Ion-Beam Analysis Lab's 1.1 MV tandem Pelletron accelerator is used to determine the presence of heavy trace metals in Queens, NY between Astoria Park and 3.5 miles south to Gantry State Park. A PIXE analysis was performed on 0.5 g pelletized soil samples with a 2.2 MeV proton beam. The results show the presence of elements ranging from Ti to Pb with the concentration of Pb in Astoria Park (2200 +/-200 ppm) approximately ten times that of the Gantry State Park. We hypothesize that the high lead concentration at Astoria Park is due to the nearby Hell Gate Bridge, painted in 1916 with lead based paint, then sandblasted and repainted in the '90s. If the lead is from the repair of the bridge, then we should see the concentration decrease as we go further from the bridge. To test this, soil samples were collected and analyzed from seven different locations north and south of the bridge. The concentrations of lead decreased drastically within a 500 m radius and were approximately constant at greater distances. More soil samples need to be collected within the 500 m radius from bridge to identify the potential source of Pb. We will describe the experimental procedure, the PIXE analysis of soil samples, and present preliminary results on the distribution of heavy trace metals.

  2. X-ray Lβ215 emission spectrum of Ru in Ru(NH3)6Cl3

    International Nuclear Information System (INIS)

    Perera, R.C.C.; Barth, J.; LaVilla, R.E.; Nordling, C.

    1984-07-01

    One of the broader applications of synchrotron radiation has been to EXAFS studies for material structure determination, i.e., for an analysis of x-ray absorption over an extended energy region beyond a core ionization limit. Studies of the near edge structure (XANES) give a different type of information, characteristic of the local symmetry and electronic configuration of the absorbing atom. This type of information is reflected also in the x-ray emission spectra, in particular for transitions involving the valence levels. Examination of the near edge absorption or the emission spectrum does not require an instrument capable of scanning a wide energy range with high counting statistics, as does EXAFS; the needs are rather for good resolution and a reliable calibration of the energy scale. Some of the problems of near edge spectra were particularly evident in our investigation of Ru-Lβ 2 15 emission from Ru(NH 3 ) 6 Cl 3 . The Ru-Lβ 2 15 emission was measured with a laboratory Rowland circle x-ray spectrometer with a curved quartz (1010) crystal (radius = 22 inches) in a fixed position appropriate to the energy range, and a position sensitive detector which can be positioned along the Rowland circle. The Ru spectrum was excited mainly by Sn-L/sub α/ primary radiation from a Sn anode in a demountable x-ray tube operating at 13 kV and 120 mA. The resolution of the instrument in this region is 1.5 eV. An accurate calibration of the energy scale was conveniently obtained by measuring a reference x-ray emission line in the same instrumental configuration. In the present case the Pd-L/sub α/ emission line at 2838 eV was used to establish the energy scale. The energy dispersion of the instrument was determined from the Cl-K/sub β/ emission spectrum of CH 3 Cl between 2810 eV and 2830 eV and Pd-Lα 1 2 and extrapolated to the energy region of the recorded emission spectrum. 6 references, 1 figure

  3. Discovery of X-Ray Emission from the Crab Pulsar at Pulse Minimum

    Science.gov (United States)

    Tennant, Allyn F.; Becker, Werner; Juda, Michael; Elsner, Ronald F.; Kolodziejczak, Jeffery J.; Murray, Stephen S.; ODell, Stephen L.; Paerels, Frits; Swartz, Douglas A.

    2001-01-01

    The Chandra X-Ray Observatory observed the Crab pulsar using the Low-Energy Transmission Grating with the High-Resolution Camera. Time-resolved zeroth-order images reveal that the pulsar emits X-rays at all pulse phases. Analysis of the flux at minimum - most likely non-thermal in origin - places an upper limit (T(sub infinity) < 2.1 MK) on the surface temperature of the underlying neutron star. In addition, analysis of the pulse profile establishes that the error in the Chandra-determined absolute time is quite small, -0.2 +/- 0.1 ms.

  4. Scanning electron microscopy-energy dispersive X-ray spectrometry (SEM-EDX) and aerosol time-of-flight mass spectrometry (ATOFMS) single particle analysis of metallurgy plant emissions

    International Nuclear Information System (INIS)

    Arndt, J.; Deboudt, K.; Anderson, A.; Blondel, A.; Eliet, S.; Flament, P.; Fourmentin, M.; Healy, R.M.; Savary, V.; Setyan, A.; Wenger, J.C.

    2016-01-01

    The chemical composition of single particles deposited on industrial filters located in three different chimneys of an iron-manganese (Fe–Mn) alloy manufacturing plant have been compared using aerosol time-of-flight mass spectrometry (ATOFMS) and scanning electron microscopy–energy dispersive X-ray spectrometry (SEM-EDX). Very similar types of particles were observed using both analytical techniques. Calcium-containing particles dominated in the firing area of the sintering unit, Mn and/or Al-bearing particles were observed at the cooling area of the sintering unit, while Mn-containing particles were dominant at the smelting unit. SEM-EDX analysis of particles collected downstream of the industrial filters showed that the composition of the particles emitted from the chimneys is very similar to those collected on the filters. ATOFMS analysis of ore samples was also performed to identify particulate emissions that could be generated by wind erosion and manual activities. Specific particle types have been identified for each emission source (chimneys and ore piles) and can be used as tracers for source apportionment of ambient PM measured in the vicinity of the industrial site. - Highlights: • Similar composition for emitted particles as those collected on the chimney filters. • Emitted particles dominated by Ca-, Mn and/or Al-containing particles. • Identification of specific particle types emitted by the different process units. - The particles emitted by metallurgy activities are fully described by ATOFMS and SEM-EDX, enabling the identification of specific particle types from the different units of the process.

  5. Background radiation in inelastic X-ray scattering and X-ray emission spectroscopy. A study for Johann-type spectrometers

    Science.gov (United States)

    Paredes Mellone, O. A.; Bianco, L. M.; Ceppi, S. A.; Goncalves Honnicke, M.; Stutz, G. E.

    2018-06-01

    A study of the background radiation in inelastic X-ray scattering (IXS) and X-ray emission spectroscopy (XES) based on an analytical model is presented. The calculation model considers spurious radiation originated from elastic and inelastic scattering processes along the beam paths of a Johann-type spectrometer. The dependence of the background radiation intensity on the medium of the beam paths (air and helium), analysed energy and radius of the Rowland circle was studied. The present study shows that both for IXS and XES experiments the background radiation is dominated by spurious radiation owing to scattering processes along the sample-analyser beam path. For IXS experiments the spectral distribution of the main component of the background radiation shows a weak linear dependence on the energy for the most cases. In the case of XES, a strong non-linear behaviour of the background radiation intensity was predicted for energy analysis very close to the backdiffraction condition, with a rapid increase in intensity as the analyser Bragg angle approaches π / 2. The contribution of the analyser-detector beam path is significantly weaker and resembles the spectral distribution of the measured spectra. Present results show that for usual experimental conditions no appreciable structures are introduced by the background radiation into the measured spectra, both in IXS and XES experiments. The usefulness of properly calculating the background profile is demonstrated in a background subtraction procedure for a real experimental situation. The calculation model was able to simulate with high accuracy the energy dependence of the background radiation intensity measured in a particular XES experiment with air beam paths.

  6. A high-density relativistic reflection origin for the soft and hard X-ray excess emission from Mrk 1044

    Science.gov (United States)

    Mallick, L.; Alston, W. N.; Parker, M. L.; Fabian, A. C.; Pinto, C.; Dewangan, G. C.; Markowitz, A.; Gandhi, P.; Kembhavi, A. K.; Misra, R.

    2018-06-01

    We present the first results from a detailed spectral-timing analysis of a long (˜130 ks) XMM-Newton observation and quasi-simultaneous NuSTAR and Swift observations of the highly-accreting narrow-line Seyfert 1 galaxy Mrk 1044. The broadband (0.3-50 keV) spectrum reveals the presence of a strong soft X-ray excess emission below ˜1.5 keV, iron Kα emission complex at ˜6 -7 keV and a `Compton hump' at ˜15 -30 keV. We find that the relativistic reflection from a high-density accretion disc with a broken power-law emissivity profile can simultaneously explain the soft X-ray excess, highly ionized broad iron line and the Compton hump. At low frequencies ([2 - 6] × 10-5 Hz), the power-law continuum dominated 1.5-5 keV band lags behind the reflection dominated 0.3-1 keV band, which is explained with a combination of propagation fluctuation and Comptonization processes, while at higher frequencies ([1 - 2] × 10-4 Hz), we detect a soft lag which is interpreted as a signature of X-ray reverberation from the accretion disc. The fractional root-mean-squared (rms) variability of the source decreases with energy and is well described by two variable components: a less variable relativistic disc reflection and a more variable direct coronal emission. Our combined spectral-timing analyses suggest that the observed broadband X-ray variability of Mrk 1044 is mainly driven by variations in the location or geometry of the optically thin, hot corona.

  7. Optimization of neon soft X-ray emission from 200 J plasma focus device for application in soft X-ray lithography

    International Nuclear Information System (INIS)

    Kalaiselvi, S.M. P.; Tan, T.L.; Talebitaher, A.; Lee, Paul; Rawat, R.S.

    2014-01-01

    The Fast Miniature Plasma Focus (FMPF) device is basically made up of coaxial electrodes with centrally placed anode and six cathode rods surrounding them concentrically. They are enclosed in a vacuum chamber, filled with low pressure operating gas. However, in our experiments, these cathode rods were removed to investigate the influence of them on neon soft X-ray (SXR) and hard X-ray (HXR) emission from the device. On removal of cathode rods, the cathode base plate serves as cathode and the plasma sheath is formed between the anode and the base plate of cathode. Neon was used as the operating gas for our experiments and the FMPF device used is of 235 J energy capacities. The experimental results showed that the FMPF device was able to focus better and the SXR emission efficiency was five times higher without cathode rods than with cathode rods. On the contrary, HXR emission did not vary with and without cathode rods. This observed phenomenon was further cross-checked through imaging of plasma dynamics, with and without cathode rods. FMPF device consists of 4 Pseudo Spark Gap (PSG) switches, which need to operate synchronously to deliver high voltage from capacitors to the anode. It was also seen that, the presence or absence of cathode rods also influence the synchronous operation of PSG switches. It also implies that this is one definite way to optimize the SXR emission from the FMPF device. This study reveals an important finding that, cathode rods play a vital role in the formation of plasma sheath with consequential influence on the radiation emission from plasma focus devices. Enhancement of the X-ray emission from this device is definitely a stepping stone in the realization of this device for industrial applications such as X-ray lithography for semiconductor industries. (author)

  8. Measurements of fast electron beams and soft X-ray emission from plasma-focus experiments

    Directory of Open Access Journals (Sweden)

    Surała Władysław

    2016-06-01

    Full Text Available The paper reports results of the recent experimental studies of pulsed electron beams and soft X-rays in plasma-focus (PF experiments carried out within a modified PF-360U facility at the NCBJ, Poland. Particular attention was focused on time-resolved measurements of the fast electron beams by means of two different magnetic analyzers, which could record electrons of energy ranging from about 41 keV to about 715 keV in several (6 or 8 measuring channels. For discharges performed with the pure deuterium filling, many strong electron signals were recorded in all the measuring channels. Those signals were well correlated with the first hard X-ray pulse detected by an external scintillation neutron-counter. In some of the analyzer channels, electron spikes (lasting about dozens of nanoseconds and appearing in different instants after the current peculiarity (so-called current dip were also recorded. For several discharges, fast ion beams, which were emitted along the z-axis and recorded with nuclear track detectors, were also investigated. Those measurements confirmed a multibeam character of the ion emission. The time-integrated soft X-ray images, which were taken side-on by means of a pinhole camera and sensitive X-ray films, showed the appearance of some filamentary structures and so-called hot spots. The application of small amounts of admixtures of different heavy noble gases, i.e. of argon (4.8% volumetric, krypton (1.6% volumetric, or xenon (0.8% volumetric, decreased intensity of the recorded electron beams, but increased intensity of the soft X-ray emission and showed more distinct and numerous hot spots. The recorded electron spikes have been explained as signals produced by quasi-mono-energetic microbeams emitted from tiny sources (probably plasma diodes, which can be formed near the observed hot spots.

  9. A SUZAKU SEARCH FOR NONTHERMAL EMISSION AT HARD X-RAY ENERGIES IN THE COMA CLUSTER

    International Nuclear Information System (INIS)

    Wik, Daniel R.; Sarazin, Craig L.; Finoguenov, Alexis; Matsushita, Kyoko; Nakazawa, Kazuhiro; Clarke, Tracy E.

    2009-01-01

    The brightest cluster radio halo known resides in the Coma cluster of galaxies. The relativistic electrons producing this diffuse synchrotron emission should also produce inverse Compton emission that becomes competitive with thermal emission from the intracluster medium (ICM) at hard X-ray energies. Thus far, claimed detections of this emission in Coma are controversial. We present a Suzaku HXD-PIN observation of the Coma cluster in order to nail down its nonthermal hard X-ray content. The contribution of thermal emission to the HXD-PIN spectrum is constrained by simultaneously fitting thermal and nonthermal models to it and a spatially equivalent spectrum derived from an XMM-Newton mosaic of the Coma field. We fail to find statistically significant evidence for nonthermal emission in the spectra which are better described by only a single- or multitemperature model for the ICM. Including systematic uncertainties, we derive a 90% upper limit on the flux of nonthermal emission of 6.0 x 10 -12 erg s -1 cm -2 (20-80 keV, for Γ = 2.0), which implies a lower limit on the cluster-averaged magnetic field of B>0.15 μG. Our flux upper limit is 2.5 times lower than the detected nonthermal flux from RXTE and BeppoSAX. However, if the nonthermal hard X-ray emission in Coma is more spatially extended than the observed radio halo, the Suzaku HXD-PIN may miss some fraction of the emission. A detailed investigation indicates that ∼50%-67% of the emission might go undetected, which could make our limit consistent with that of Rephaeli and Gruber and Fusco-Femiano et al. The thermal interpretation of the hard Coma spectrum is consistent with recent analyses of INTEGRAL and Swift data.

  10. A Multiwavelength Exploration of the Grand Design Spiral M83: Diffuse X-ray Emission

    Science.gov (United States)

    Kuntz, K. D.; Long, K. S.; Blair, W. P.; Plucinsky, P. P.; Soria, R.; Winkler, P. F.

    2013-01-01

    We have obtained a series of deep X-ray images of the nearby galaxy M83, with a total exposure 729 ksec with the Chandra ACIS-S array. Since the bulk of the X-ray emitting disk falls within the BI chip, these observations allow a detailed study of the soft diffuse emission in the disk. Most of the diffuse emission is related to star-formation regions and must be powered by supernovae and stellar winds, though the amount of emission due to identifiable SNR is only a few percent. The relation between the spectral shape and surface brightness that was seen in M101 suggests that the properties of the X-ray emission in spiral disks are shaped by the local hot gas production rate (traced by the local star-formation rate) or the disk mid-plane pressure, but it is unclear which physical mechanism dominates. To illuminate this problem, we will compare M83 with the previous Chandra studies of M101 and M33.

  11. Determination of minor and trace elements in kidney stones by x-ray fluorescence analysis

    Science.gov (United States)

    Srivastava, Anjali; Heisinger, Brianne J.; Sinha, Vaibhav; Lee, Hyong-Koo; Liu, Xin; Qu, Mingliang; Duan, Xinhui; Leng, Shuai; McCollough, Cynthia H.

    2014-03-01

    The determination of accurate material composition of a kidney stone is crucial for understanding the formation of the kidney stone as well as for preventive therapeutic strategies. Radiations probing instrumental activation analysis techniques are excellent tools for identification of involved materials present in the kidney stone. In particular, x-ray fluorescence (XRF) can be very useful for the determination of minor and trace materials in the kidney stone. The X-ray fluorescence measurements were performed at the Radiation Measurements and Spectroscopy Laboratory (RMSL) of department of nuclear engineering of Missouri University of Science and Technology and different kidney stones were acquired from the Mayo Clinic, Rochester, Minnesota. Presently, experimental studies in conjunction with analytical techniques were used to determine the exact composition of the kidney stone. A new type of experimental set-up was developed and utilized for XRF analysis of the kidney stone. The correlation of applied radiation source intensity, emission of X-ray spectrum from involving elements and absorption coefficient characteristics were analyzed. To verify the experimental results with analytical calculation, several sets of kidney stones were analyzed using XRF technique. The elements which were identified from this techniques are Silver (Ag), Arsenic (As), Bromine (Br), Chromium (Cr), Copper (Cu), Gallium (Ga), Germanium (Ge), Molybdenum (Mo), Niobium (Nb), Rubidium (Rb), Selenium (Se), Strontium (Sr), Yttrium (Y), Zirconium (Zr). This paper presents a new approach for exact detection of accurate material composition of kidney stone materials using XRF instrumental activation analysis technique.

  12. X-ray Emission Spectrum of Liquid Ethanol: Origin of Split Peaks.

    Science.gov (United States)

    Takahashi, Osamu; Ljungberg, Mathias P; Pettersson, Lars G M

    2017-12-14

    The X-ray emission spectrum of liquid ethanol was calculated using density functional theory and a semiclassical approximation to the Kramers-Heisenberg formula including core-hole-induced dynamics. Our spectrum agrees well with the experimental spectrum. We found that the intensity ratio between the two peaks at 526 and 527 eV assigned as 10a' and 3a″ depends not only on the hydrogen bonding network around the target molecule but also on the intramolecular conformation. This effect is absent in liquid methanol and demonstrates the high sensitivity of X-ray emission to molecular structure. The dependence of spectral features on hydrogen-bonding as well as on dynamical effects following core excitation are also discussed.

  13. Bulk band gaps in divalent hexaborides: A soft x-ray emission study

    International Nuclear Information System (INIS)

    Denlinger, Jonathan D.; Gweon, Gey-Hong; Allen, James W.; Bianchi, Andrea D.; Fisk, Zachary

    2001-01-01

    Boron K-edge soft x-ray emission and absorption are used to address the fundamental question of whether divalent hexaborides are intrinsic semimetals or defect-doped bandgap insulators. These bulk sensitive measurements, complementary and consistent with surface-sensitive angle-resolved photoemission experiments, confirm the existence of a bulk band gap and the location of the chemical potential at the bottom of the conduction band

  14. X-ray emission spectroscopy of well-characterised non-LTE plasmas

    International Nuclear Information System (INIS)

    Bourgaux, A C; Bastiani-Ceccotti, S; Audebert, P; Marquès, J R; Vassura, L; Vinci, T; Jacquemot, S; Dorchies, F; Leguay, P M; Chung, H K; Bowen, C; Dervieux, V; Renaudin, P; Silvert, V

    2016-01-01

    This paper will present an experimental platform developed on LULI2000 to measure x-ray emission of non-LTE plasmas in well-defined hydrodynamic conditions thanks to implementation of a whole set of diagnostics, including time-resolved electronic and ionic Thomson scattering and self-optical pyrometry. K-, L- and M-shell spectra will be presented and the methodology, that has been developed to analyze them, discussed. (paper)

  15. Control of the Low-energy X-rays by Using MCNP5 and Numerical Analysis for a New Concept Intra-oral X-ray Imaging System

    Science.gov (United States)

    Huh, Jangyong; Ji, Yunseo; Lee, Rena

    2018-05-01

    An X-ray control algorithm to modulate the X-ray intensity distribution over the FOV (field of view) has been developed by using numerical analysis and MCNP5, a particle transport simulation code on the basis of the Monte Carlo method. X-rays, which are widely used in medical diagnostic imaging, should be controlled in order to maximize the performance of the X-ray imaging system. However, transporting X-rays, like a liquid or a gas is conveyed through a physical form such as pipes, is not possible. In the present study, an X-ray control algorithm and technique to uniformize the Xray intensity projected on the image sensor were developed using a flattening filter and a collimator in order to alleviate the anisotropy of the distribution of X-rays due to intrinsic features of the X-ray generator. The proposed method, which is combined with MCNP5 modeling and numerical analysis, aimed to optimize a flattening filter and a collimator for a uniform distribution of X-rays. Their size and shape were estimated from the method. The simulation and the experimental results both showed that the method yielded an intensity distribution over an X-ray field of 6×4 cm2 at SID (source to image-receptor distance) of 5 cm with a uniformity of more than 90% when the flattening filter and the collimator were mounted on the system. The proposed algorithm and technique are not only confined to flattening filter development but can also be applied for other X-ray related research and development efforts.

  16. Detection of non-thermal X-ray emission in the lobes and jets of Cygnus A

    Science.gov (United States)

    de Vries, M. N.; Wise, M. W.; Huppenkothen, D.; Nulsen, P. E. J.; Snios, B.; Hardcastle, M. J.; Birkinshaw, M.; Worrall, D. M.; Duffy, R. T.; McNamara, B. R.

    2018-06-01

    We present a spectral analysis of the lobes and X-ray jets of Cygnus A, using more than 2 Ms of Chandra observations. The X-ray jets are misaligned with the radio jets and significantly wider. We detect non-thermal emission components in both lobes and jets. For the eastern lobe and jet, we find 1 keV flux densities of 71_{-10}^{+10} nJy and 24_{-4}^{+4} nJy, and photon indices of 1.72_{-0.03}^{+0.03} and 1.64_{-0.04}^{+0.04} respectively. For the western lobe and jet, we find flux densities of 50_{-13}^{+12} nJy and 13_{-5}^{+5} nJy, and photon indices of 1.97_{-0.10}^{+0.23} and 1.86_{-0.12}^{+0.18} respectively. Using these results, we modeled the electron energy distributions of the lobes as broken power laws with age breaks. We find that a significant population of non-radiating particles is required to account for the total pressure of the eastern lobe. In the western lobe, no such population is required and the low energy cutoff to the electron distribution there needs to be raised to obtain pressures consistent with observations. This discrepancy is a consequence of the differing X-ray photon indices, which may indicate that the turnover in the inverse-Compton spectrum of the western lobe is at lower energies than in the eastern lobe. We modeled the emission from both jets as inverse-Compton emission. There is a narrow region of parameter space for which the X-ray jet can be a relic of an earlier active phase, although lack of knowledge about the jet's electron distribution and particle content makes the modelling uncertain.

  17. X-ray CT analysis of pore structure in sand

    Science.gov (United States)

    Mukunoki, Toshifumi; Miyata, Yoshihisa; Mikami, Kazuaki; Shiota, Erika

    2016-06-01

    The development of microfocused X-ray computed tomography (CT) devices enables digital imaging analysis at the pore scale. The applications of these devices are diverse in soil mechanics, geotechnical and geoenvironmental engineering, petroleum engineering, and agricultural engineering. In particular, the imaging of the pore space in porous media has contributed to numerical simulations for single-phase and multiphase flows or contaminant transport through the pore structure as three-dimensional image data. These obtained results are affected by the pore diameter; therefore, it is necessary to verify the image preprocessing for the image analysis and to validate the pore diameters obtained from the CT image data. Moreover, it is meaningful to produce the physical parameters in a representative element volume (REV) and significant to define the dimension of the REV. This paper describes the underlying method of image processing and analysis and discusses the physical properties of Toyoura sand for the verification of the image analysis based on the definition of the REV. On the basis of the obtained verification results, a pore-diameter analysis can be conducted and validated by a comparison with the experimental work and image analysis. The pore diameter is deduced from Young-Laplace's law and a water retention test for the drainage process. The results from previous study and perforated-pore diameter originally proposed in this study, called the voxel-percolation method (VPM), are compared in this paper. In addition, the limitations of the REV, the definition of the pore diameter, and the effectiveness of the VPM for an assessment of the pore diameter are discussed.

  18. Renal function measured by X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Boijsen, M.; Jacobsson, L.; Tylen, U.; Sahlgrenska Sjukhuset, Goeteborg

    1987-01-01

    In twenty-six patients injected with metrizoate during urography, plasma was analyzed for iodine concentration using X-ray fluorescence analysis, and total plasma clearance of contrast medium was calculated. Total plasma clearance of 51 Cr-EDTA was also determined, but not simultaneously, in order to find out if the urographic procedure would influence the kidneys to such an extent that the contrast medium clearance value would differ much from the 51 Cr-EDTA clearance value. The errors in the method were assessed and the total error of the contrast medium clearance determination was calculated. When comparing 51 Cr-EDTA and metrizoate clearance a correlation of 0.94 and a mean ratio of 1.046 (SD 0.138) was found. The assessable errors cannot fully explain the standard deviation, which might indicate a transient change in kidney function related to elements of the urographic procedure such as laxation with possible dehydration and/or the contrast medium dose. (orig.)

  19. Radioisotope sources for X-ray fluorescence analysis

    International Nuclear Information System (INIS)

    Leonowich, J.; Pandian, S.; Preiss, I.L.

    1977-01-01

    Problems involved in developing radioisotope sources and the characteristics of potentially useful radioisotopes for X-ray fluorescence analysis are presented. These include the following. The isotope must be evaluated for the physical and chemical forms available, purity, half-life, specific activity, toxicity, and cost. The radiation hazards of the source must be considered. The type and amount of radiation output of the source must be evaluated. The source construction must be planned. The source should also present an advance over those currently available in order to justify its development. Some of the isotopes, which are not in use but look very promising, are indicated, and their data are tabulated. A more or less ''perfect'' source within a given range of interest would exhibit the following characteristics. (1) Decay by an isometric transition with little or no internal conversion, (2) Have an intense gamma transition near the absorption edge of the element(s) of interest with no high energy gammas, (3) Have a sufficiently long half-life (in the order of years) for both economic and calibration reasons, (4) Have a sufficiently large cross-section for production in a reasonable amount of time. If there are competing reactions the interfering isotopes should be reasonably short-lived, or if not, be apt to be separated from the isotope chemically with a minimum of difficulty. (T.G.)

  20. X-ray quality assessment by MTF analysis

    International Nuclear Information System (INIS)

    Gais, P.; Burger, G.; Drexler, G.; Rappl, M.; Bunde, E.; Lissner, J.; Schaetzl, M.

    1985-01-01

    In a previous study a lucite phantom with several physical elements embedded, such as lead gratings with varying line widths, etc., was exposed at 200 X-ray installations in Bavaria, Federal Republic of Germany, by a conventional diagnostic standard technique. One of the parameters investigated was the local resolution achieved, determined visually by examination of the grating images. The same radiographs have now been used in a retrospective comparative study, based upon a quantitative analysis of TV images of the films. The films were positioned on a commercial illuminator screen and looked at by a TV camera through a simple magnifying optical system. The video signals were digitised, resulting in a pixel distance of 50 μm. In a first approach the edges of the broad frames of the lead gratings were adjusted vertically and the normalised sum of all 256 TV scanning lines taken as the edge function f(x). This was differentiated and suitably Fourier-transformed, delivering the modulation transfer function (MTF). The MTF can be analysed in several ways to describe quantitatively the maximum local resolution achievable. Correlation of some frequency measurements with the visually determined line resolution is generally good. (author)

  1. Recent measurements of soft X-ray emission from the DPF-1000U facility

    Directory of Open Access Journals (Sweden)

    Surała Władysław

    2015-06-01

    Full Text Available Soft X-ray imaging is a very useful diagnostic technique in plasma-focus (PF experiments. This paper reports results of four experimental sessions which were carried out at the DPF-1000U plasma-focus facility in 2013 and 2014. Over 200 discharges were performed at various experimental conditions. Measurements were taken using two X-ray pinhole cameras with a line of sight perpendicular to the z-axis, at different azimuthal angles (about 20° and 200°, and looking towards the centre of the PF-pinch column. They were equipped with diaphragms 1000 μm or 200–300 μm in diameter and coated with filters of 500 μm Al foil and 10 μm Be foil, respectively. Data on the neutron emission were collected with silver activation counters. For time-resolved measurements the use was made of four PIN diodes equipped with various filters and oriented towards the centre of the PF-column, in the direction perpendicular to the electrode axis. The recorded X-ray images revealed that when the additional gas-puff system is activated during the discharge, the stability of the discharge is improved. The data collected in these experiments confirmed the appearance of a filamentary fine structure in the PF discharges. In the past years the formation of such filaments was observed in many Z-pinch type experiments. Some of the recorded X-ray images have also revealed the appearance of the so-called hot-spots, i.e. small plasma regions of a very intense X-ray emission. Such a phenomenon was observed before in many PF experiments, e.g. in the MAJA-PF device, but it has not been investigated so far in a large facility such as the DPF-1000U. The time-resolved measurements provided the evidence of a time lapse between the X-ray emission from plasma regions located at different distance from the anode surface. The formation of distinct ‘hot-spots’ in different instants of the DPF-1000U discharge was also observed.

  2. INVERSE COMPTON X-RAY EMISSION FROM SUPERNOVAE WITH COMPACT PROGENITORS: APPLICATION TO SN2011fe

    International Nuclear Information System (INIS)

    Margutti, R.; Soderberg, A. M.; Chomiuk, L.; Milisavljevic, D.; Foley, R. J.; Slane, P.; Moe, M.; Chevalier, R.; Hurley, K.; Hughes, J. P.; Fransson, C.; Barthelmy, S.; Cummings, J.; Boynton, W.; Enos, H.; Fellows, C.; Briggs, M.; Connaughton, V.; Costa, E.; Del Monte, E.

    2012-01-01

    We present a generalized analytic formalism for the inverse Compton X-ray emission from hydrogen-poor supernovae and apply this framework to SN 2011fe using Swift X-Ray Telescope (XRT), UVOT, and Chandra observations. We characterize the optical properties of SN 2011fe in the Swift bands and find them to be broadly consistent with a 'normal' SN Ia, however, no X-ray source is detected by either XRT or Chandra. We constrain the progenitor system mass-loss rate M-dot -9 M ☉ yr -1 (3σ c.l.) for wind velocity v w = 100 km s –1 . Our result rules out symbiotic binary progenitors for SN 2011fe and argues against Roche lobe overflowing subgiants and main-sequence secondary stars if ∼> 1% of the transferred mass is lost at the Lagrangian points. Regardless of the density profile, the X-ray non-detections are suggestive of a clean environment (n CSM –3 ) for 2 × 10 15 ∼ 16 cm around the progenitor site. This is either consistent with the bulk of material being confined within the binary system or with a significant delay between mass loss and supernova explosion. We furthermore combine X-ray and radio limits from Chomiuk et al. to constrain the post-shock energy density in magnetic fields. Finally, we searched for the shock breakout pulse using gamma-ray observations from the Interplanetary Network and find no compelling evidence for a supernova-associated burst. Based on the compact radius of the progenitor star we estimate that the shock breakout pulse was likely not detectable by current satellites.

  3. Theory and analysis of soft x-ray laser experiments

    International Nuclear Information System (INIS)

    Whitten, B.L.; Hazi, A.U.

    1985-10-01

    The atomic modeling of soft x-ray laser schemes presents a formidable challenge to the theorists - a challenge magnified by the recent successful experiments. A complex plasma environment with many ion species present must be simulated. Effects such as turbulence, time dependence, and radiation transport, which are very difficult to model accurately, may be important. We shall describe our efforts to model the recently demonstrated soft x-ray laser in collisionally pumped neon-like selenium, with emphasis on the ionization balance and excited state kinetics. The relative importance of various atomic processes, such as collisional excitation and dielectronic recombination, on the inversion kinetics will be demonstrated. We shall compare our models with experimental results and evaluate the success of this technique in predicting and analyzing the results of x-ray laser experiments. 22 refs., 5 figs., 3 tabs

  4. Ancient administrative handwritten documents: X-ray analysis and imaging

    International Nuclear Information System (INIS)

    Albertin, F.; Astolfo, A.; Stampanoni, M.; Peccenini, Eva; Hwu, Y.; Kaplan, F.; Margaritondo, G.

    2015-01-01

    The heavy-element content of ink in ancient administrative documents makes it possible to detect the characters with different synchrotron imaging techniques, based on attenuation or refraction. This is the first step in the direction of non-interactive virtual X-ray reading. Handwritten characters in administrative antique documents from three centuries have been detected using different synchrotron X-ray imaging techniques. Heavy elements in ancient inks, present even for everyday administrative manuscripts as shown by X-ray fluorescence spectra, produce attenuation contrast. In most cases the image quality is good enough for tomography reconstruction in view of future applications to virtual page-by-page ‘reading’. When attenuation is too low, differential phase contrast imaging can reveal the characters from refractive index effects. The results are potentially important for new information harvesting strategies, for example from the huge Archivio di Stato collection, objective of the Venice Time Machine project

  5. X-ray Phase Contrast analysis - Digital wavefront development

    International Nuclear Information System (INIS)

    Idir, Mourad; Potier, Jonathan; Fricker, Sebastien; Snigirev, Anatoly; Snigireva, Irina; Modi, M. H.

    2010-01-01

    Optical schemes that enable imaging of the phase shift produced by an object have become popular in the x-ray region, where phase can be the dominant contrast mechanism. The propagation-based technique consists of recording the interference pattern produced by choosing one or several sample-to-detector distances. Pioneering studies, carried out making use of synchrotron radiation, demonstrated that this technique results in a dramatic increase of image contrast and detail visibility, allowing the detection of structures invisible with conventional techniques. An experimental and theoretical study of in-line hard x-ray phase-contrast imaging had been performed. The theoretical description of the technique is based on Fresnel diffraction. As an illustration of the potential of this quantitative imaging technique, high-resolution x-ray phase contrast images of simple objects will be presented.

  6. Bone quality analysis using X-ray microtomography and microfluorescence

    Energy Technology Data Exchange (ETDEWEB)

    Sales, E.; Lima, I. [Nuclear Instrumentation Laboratory, PEN/COPPE/UFRJ, PO Box: 68509, 21.941-972, Rio de Janeiro (Brazil); Assis, J.T. de [Polytechnic Institute, DEMEC/UERJ (Brazil); Gomez, W. [Department of Electrical Engineering, Center of the National Polytechnic Institute (Mexico); Pereira, W.C.A. [Biomedical Engineering Program, COPPE/UFRJ, Rio de Janeiro (Brazil); Lopes, R.T., E-mail: ricardo@lin.ufrj.br [Nuclear Instrumentation Laboratory, PEN/COPPE/UFRJ, PO Box: 68509, 21.941-972, Rio de Janeiro (Brazil)

    2012-07-15

    Bone quality is an evaluation index often applied in order to interpret clinical observations made upon bone health, such as bone mineral density, micro and macro architecture, and mineral content. Conventional inspection techniques do not provide full information on trabecular bone quality. This study shows the high resolution potential and the non-destructive character of X-ray microtomography and microfluorescence upon the application of such techniques for evaluating bone quality. The mineral content assessment was performed by two-dimensional concentration mappings of calcium, zinc, and strontium. The results showed significant changes in bone morphology. - Highlights: Black-Right-Pointing-Pointer This study shows bone microarchitectural evaluation by X-ray microtomography and microfluorescence. Black-Right-Pointing-Pointer For this purpose, lumbar vertebrae of Wistar rats have been used as test subjects. Black-Right-Pointing-Pointer X-ray techniques proved to have an excellent perfomance in quantifying bone mineral content.

  7. Ancient administrative handwritten documents: X-ray analysis and imaging

    Energy Technology Data Exchange (ETDEWEB)

    Albertin, F., E-mail: fauzia.albertin@epfl.ch [Ecole Polytechnique Fédérale de Lausanne (EPFL), CH-1015 Lausanne (Switzerland); Astolfo, A. [Paul Scherrer Institut (PSI), Villigen (Switzerland); Stampanoni, M. [Paul Scherrer Institut (PSI), Villigen (Switzerland); ETHZ, Zürich (Switzerland); Peccenini, Eva [University of Ferrara (Italy); Technopole of Ferrara (Italy); Hwu, Y. [Academia Sinica, Taipei, Taiwan (China); Kaplan, F. [Ecole Polytechnique Fédérale de Lausanne (EPFL) (Switzerland); Margaritondo, G. [Ecole Polytechnique Fédérale de Lausanne (EPFL), CH-1015 Lausanne (Switzerland)

    2015-01-30

    The heavy-element content of ink in ancient administrative documents makes it possible to detect the characters with different synchrotron imaging techniques, based on attenuation or refraction. This is the first step in the direction of non-interactive virtual X-ray reading. Handwritten characters in administrative antique documents from three centuries have been detected using different synchrotron X-ray imaging techniques. Heavy elements in ancient inks, present even for everyday administrative manuscripts as shown by X-ray fluorescence spectra, produce attenuation contrast. In most cases the image quality is good enough for tomography reconstruction in view of future applications to virtual page-by-page ‘reading’. When attenuation is too low, differential phase contrast imaging can reveal the characters from refractive index effects. The results are potentially important for new information harvesting strategies, for example from the huge Archivio di Stato collection, objective of the Venice Time Machine project.

  8. Development of a micro-X-ray fluorescence system based on polycapillary X-ray optics for non-destructive analysis of archaeological objects

    Science.gov (United States)

    Cheng, Lin; Ding, Xunliang; Liu, Zhiguo; Pan, Qiuli; Chu, Xuelian

    2007-08-01

    A new micro-X-ray fluorescence (micro-XRF) system based on rotating anode X-ray generator and polycapillary X-ray optics has been set up in XOL Lab, BNU, China, in order to be used for analysis of archaeological objects. The polycapillary X-ray optics used here can focus the primary X-ray beam down to tens of micrometers in diameter that allows for non-destructive and local analysis of sub-mm samples with minor/trace level sensitivity. The analytical characteristics and potential of this micro-XRF system in archaeological research are discussed. Some described uses of this instrument include studying Chinese ancient porcelain.

  9. Development of a micro-X-ray fluorescence system based on polycapillary X-ray optics for non-destructive analysis of archaeological objects

    Energy Technology Data Exchange (ETDEWEB)

    Cheng Lin [Key Laboratory of Beam Technology and Material Modification of Ministry of Education, Institute of Low Energy Nuclear Physics, Beijing Normal University, Beijing Radiation Center, Beijing, 100875 (China)], E-mail: chenglin@bnu.edu.cn; Ding Xunliang; Liu Zhiguo; Pan Qiuli; Chu Xuelian [Key Laboratory of Beam Technology and Material Modification of Ministry of Education, Institute of Low Energy Nuclear Physics, Beijing Normal University, Beijing Radiation Center, Beijing, 100875 (China)

    2007-08-15

    A new micro-X-ray fluorescence (micro-XRF) system based on rotating anode X-ray generator and polycapillary X-ray optics has been set up in XOL Lab, BNU, China, in order to be used for analysis of archaeological objects. The polycapillary X-ray optics used here can focus the primary X-ray beam down to tens of micrometers in diameter that allows for non-destructive and local analysis of sub-mm samples with minor/trace level sensitivity. The analytical characteristics and potential of this micro-XRF system in archaeological research are discussed. Some described uses of this instrument include studying Chinese ancient porcelain.

  10. Human soft tissue analysis using x-ray or gamma-ray techniques

    International Nuclear Information System (INIS)

    Theodorakou, C; Farquharson, M J

    2008-01-01

    This topical review is intended to describe the x-ray techniques used for human soft tissue analysis. X-ray techniques have been applied to human soft tissue characterization and interesting results have been presented over the last few decades. The motivation behind such studies is to provide improved patient outcome by using the data obtained to better understand a disease process and improve diagnosis. An overview of theoretical background as well as a complete set of references is presented. For each study, a brief summary of the methodology and results is given. The x-ray techniques include x-ray diffraction, x-ray fluorescence, Compton scattering, Compton to coherent scattering ratio and attenuation measurements. The soft tissues that have been classified using x-rays or gamma rays include brain, breast, colon, fat, kidney, liver, lung, muscle, prostate, skin, thyroid and uterus. (topical review)

  11. A few approaches to remove ambiguous factors in x-ray spectrum analysis

    International Nuclear Information System (INIS)

    Sera, K.; Futatsugawa, S.

    1993-01-01

    A few attempts have been done to reduce ambiguous factors in the analysis of complex x-ray spectra. Uncertainty in peak identification and separation due to overlapping of x-ray peaks can be reduced by taking into account the response function of x-ray peaks and by using peak functions including all the x-ray sub-lines in a x-ray series. Ambiguous factors due to discontinuity of backgrounds which is sometimes followed by huge peaks can be reduced by considering contributions from the pile-up, escape and tail functions. The problem of uncertainty in the background fitting in a region of low x-ray energy, where many peaks overlap each other and determination of the background function contains much difficulties and ambiguities, can be solved by using peak functions involving tails in place of Gaussians. (author)

  12. Elemental analysis of bronze artifacts by muonic X-ray spectroscopy

    International Nuclear Information System (INIS)

    Ninomiya, Kazuhiko; Shinohara, Atsushi; Kubo, Michael K.; Strasser, Patrick; Nagatomo, Takashi; Kawamura, Naritoshi; Shimomura, Koichiro; Miyake, Yasuhiro; Kobayashi, Yoshio; Ishida, Katsuhiko; Higemoto, Wataru; Suzuki, Takao; Saito, Tsutomu

    2015-01-01

    A quantitative and multi-elemental analysis method for bulk samples based on muonic X-ray spectroscopy was applied to bronze artifacts (Tempo-Tsuho coins and a Seiun-kyo mirror). This method is based on the measurement of the characteristic high-energy muonic X-rays emitted in a sample after muon irradiation. The elemental compositions of these bronze artifacts were determined from muonic X-ray intensities in a non-destructive manner, using the relation between the muonic X-ray intensity and the elemental composition of the Cu–Sn–Pb alloy system. The analyzed values agreed well with those determined by X-ray fluorescence spectroscopy. We also estimated the detection limit of this method in the present experimental setup as 0.81 wt% of the background signal of the muonic X-ray spectra. (author)

  13. Analysis of biological samples by x-ray attenuation measurements

    International Nuclear Information System (INIS)

    Cesareo, R.

    1988-01-01

    Over the last few years there has been an increasing interest in X-ray attenuation measurements, mainly due to the enormous development of computer assisted tomography (CAT). With CAT, analytical information concerning the density and the mean atomic number distributions in a sample is deduced from a large number of attenuation measurements. Particular transmission methods developed, based on the differential attenuation method are discussed. The theoretical background for attenuation of radiation and for differential attenuation of radiation is given. Details about the generation of monoenergetic X-rays are discussed. Applications of attenuation measurements in the field of Medicine are presented

  14. X-ray phase analysis of nickel superalloys

    International Nuclear Information System (INIS)

    Khayutin, S.G.

    2004-01-01

    An X-ray diffraction technique for determining phase composition is proposed for an intermetallic system of NiAl-Ni 3 Al and is based on the comparison of X-ray interference line intensity for two phases. Its application to heat resistant intermetallic coatings of nickel base alloys has restrictions associated with coatings nonhomogeneity in thickness. These restrictions are noted to be not essential if the reflecting layer thickness does not exceed the thickness of a chemically homogeneous layer in the coating [ru

  15. A comparative study of the ionic keV X-ray line emission from ...

    Indian Academy of Sciences (India)

    resolved X-ray diffraction [15] etc. High conversion efficiency of the laser ... picosecond ionic X-ray pulses are produced when both the plasma density and the tem- ..... X-ray spectrum of magnesium plasma produced using femtosecond laser.

  16. Temporal feature of X-ray laser plasma observed from 3ω0/2, 2ω0 harmonic emission

    International Nuclear Information System (INIS)

    Li Wenhong; Mei Qiyong; Zhao Xuewei; Chen Yuting; Chunyu Shutai

    1995-01-01

    Temporal feature of X-ray laser plasma density was observed from 3ω 0 /2, 2ω 0 harmonic emission in the experiments. The temporal feature of 3ω 0 /2 harmonic emission of the germanium film is much different from that of the slab germanium target. The production of x-ray laser is closely related to 3ω 0 /2 harmonic emission in the slab germanium targets

  17. Role of screening and angular distributions in resonant soft-x-ray emission of CO

    Energy Technology Data Exchange (ETDEWEB)

    Skytt, P.; Glans, P.; Gunnelin, K. [Uppsala Univ. (Sweden)] [and others

    1997-04-01

    In the present work the authors focus on two particular properties of resonant X-ray emission, namely core hole screening of the excited electron, and anisotropy caused by the polarization of the exciting synchrotron radiation. The screening of the core hole by the excited electron causes energy shifts and intensity variations in resonant spectra compared to the non-resonant case. The linear polarization of the synchrotron radiation and the dipole nature of the absorption process create a preferential alignment selection of the randomly oriented molecules in the case of resonant excitation, producing an anisotropy in the angular distribution of the emitted X-rays. The authors have chosen CO for this study because this molecule has previously served as a showcase for non-resonant X-ray emission, mapping the valence electronic structure differently according to the local selection rules. With the present work they take interest in how this characteristic feature of the spectroscopy is represented in the resonant case.

  18. Electron-electron correlation, resonant photoemission and X-ray emission spectra

    International Nuclear Information System (INIS)

    Parlebas, J.C.; Kotani, Akio; Tanaka, Satoshi.

    1991-01-01

    In this short review paper we essentially focus on the high energy spectroscopies which involve second order quantum processes, i.e., resonance photoemission, Auger and X-ray emission spectroscopies, denoted respectively by RXPS, AES and XES. First, we summarize the main 3p-RXPS and AES results obtained in Cu and Ni metals; especially we recall that the satellite near the 3p-threshold in the spectra, which arises from a d-hole pair bound state, needs a careful treatment of the electron-electron correlation. Then we analyze the RXPS spectra in a few Ce compounds (CeO 2 , Ce 2 O 3 and CeF 3 ) involving 3d or 4d core levels and we interpret the spectra consistently with the other spectroscopies, such as core XPS and XAS which are first order quantum processes. Finally within the same one-impurity model and basically with the same sets of parameters, we review a theory for the Ce 5p→3d XES, as well as for the corresponding RXES, where (1) the incident X-ray is tuned to resonate with the 3d→4f transition and (2) the X-ray emission due to the 5p→3d transition is actually observed. The paper ends with a general discussion. (author) 77 refs

  19. Soft X-ray and cathodoluminescence measurement, optimisation and analysis at liquid nitrogen temperatures

    Science.gov (United States)

    MacRae, C. M.; Wilson, N. C.; Torpy, A.; Delle Piane, C.

    2018-01-01

    Advances in field emission gun electron microprobes have led to significant gains in the beam power density and when analysis at high resolution is required then low voltages are often selected. The resulting beam power can lead to damage and this can be minimised by cooling the sample down to cryogenic temperatures allowing sub-micrometre imaging using a variety of spectrometers. Recent advances in soft X-ray emission spectrometers (SXES) offer a spectral tool to measure both chemistry and bonding and when combined with spectral cathodoluminescence the complementary techniques enable new knowledge to be gained from both mineral and materials. Magnesium and aluminium metals have been examined at both room and liquid nitrogen temperatures by SXES and the L-emission Fermi-edge has been observed to sharpen at the lower temperatures directly confirming thermal broadening of the X-ray spectra. Gains in emission intensity and resolution have been observed in cathodoluminescence for liquid nitrogen cooled quartz grains compared to ambient temperature quartz. This has enabled subtle growth features at quartz to quartz-cement boundaries to be imaged for the first time.

  20. Reconnection, Particle Acceleration, and Hard X-ray Emission in Eruptive Solar Flares

    Science.gov (United States)

    Martens, Petrus C.

    1998-11-01

    The frequent occurrence of Hard X-ray emission from the top of flaring loops was one of the discoveries by the Hard X-ray telescope on board the Japanese Yohkoh satellite. I will show how the combined effect of magnetic field convergence and pitch- angle scattering of non-thermal electrons injected at the top of the loop results in the generation of looptop sources with properties akin to those observed by Yohkoh. In addition it is shown that the injection of proton beams in the loop legs, expected from theory, reproduces the observed high temperature ``ridges" in the loop legs by mirroring and energy loss through collisions. I will interpret these numerical results as supporting the now widely accepted model of an erupting magnetic flux tube generating a reconnecting current sheet in its wake, where most of the energy release takes place. The strong similarity with the reconnection observed in the MRX experiment in Princeton will be analyzed in detail.