WorldWideScience

Sample records for on-line analysis systems

  1. On-line multidimensional separation systems for peptide analysis

    NARCIS (Netherlands)

    Stroink, T.

    2005-01-01

    Today, there is an increasing interest in selective and sensitive analysis of proteins and peptides with a relatively high speed. The first chapter of this thesis describes several strategies for the on-line multidimensional analysis of peptides and proteins in biological samples. This overview of t

  2. An on-line remote supervisory system for microparticles based on image analysis

    Science.gov (United States)

    Liu, Wei-Hua; Jiang, Ming-Shun; Sui, Qing-Mei

    2011-11-01

    A new on-line remote particle analysis system based on image processing has been developed to measure microparticles. The system is composed of particle collector sensor (PCS), particle image sensor (PIS), image remote transmit module and image processing system. Then some details of image processing are discussed. The main advantage of this system is more convenient in particle sample collection and particle image acquisition. The particle size can be obtained using the system with a deviation abot less than 1 μm, and the particle number can be obtained without deviation. The developed system is also convenient and versatile for other analyses of microparticle for academic and industrial application.

  3. An on-line remote supervisory system for microparticles based on image analysis

    Institute of Scientific and Technical Information of China (English)

    LIU Wei-hua; JIANG Ming-shun; SUI Qing-mei

    2011-01-01

    A new on-line remote particle analysis system based on image processing has been developed to measure microparticles.The system is composed of particle collector sensor (PCS),particle image sensor (PIS),image remote wansmit module and image processing system.Then some details of image processing are discussed.The main advantage of this system is more convenient in particle sample collection and particle image acquisition.The particle size can be obtained using the system with a deviation abot less than 1 μm,and the particle number can be obtained without deviation,The developed system is also convenient and versatile for other analyses of microparticle for academic and industrial application.

  4. PHENIX on-line systems

    Energy Technology Data Exchange (ETDEWEB)

    Adler, S.S.; Allen, M.; Alley, G.; Amirikas, R.; Arai, Y.; Awes, T.C.; Barish, K.N.; Barta, F.; Batsouli, S.; Belikov, S.; Bennett, M.J.; Bobrek, M.; Boissevain, J.G.; Boose, S.; Britton, C.; Britton, L.; Bryan, W.L.; Cafferty, M.M.; Carey, T.A.; Chang, W.C.; Chi, C.Y.; Chiu, M.; Cianciolo, V.; Cole, B.A.; Constantin, P.; Cook, K.C.; Cunitz, H.; Desmond, E.J.; Ebisu, K.; Efremenko, Y.V.; El Chenawi, K.; Emery, M.S.; Engo, D.; Ericson, N.; Fields, D.E.; Frank, S.; Frantz, J.E.; Franz, A.; Frawley, A.D.; Fried, J.; Gannon, J.; Gee, T.F.; Gentry, R.; Giannotti, P.; Gustafsson, H.-A.; Haggerty, J.S.; Hahn, S.; Halliwell, J.; Hamagaki, H.; Hansen, A.G.; Hara, H.; Harder, J.; He, X.; Heistermann, F.; Hemmick, T.K.; Hibino, M.; Hill, J.C. E-mail: jhill@iastate.edu; Homma, K.; Jacak, B.V.; Jagadish, U.; Jia, J.; Kajihara, F.; Kametani, S.; Kamyshkov, Y.; Kandasamy, A.; Kang, J.H.; Kapustinsky, J.; Katou, K.; Kelley, M.A.; Kelly, S.; Kikuchi, J.; Kim, S.Y.; Kim, Y.G.; Kistenev, E.; Kotchetkov, D.; Kurita, K.; Lajoie, J.G.; Lenz, M.; Lenz, W.; Li, X.H.; Lin, S.; Liu, M.X.; Markacs, S.; Matathias, F.; Matsumoto, T.; Mead, J.; Mischke, R.E.; Mishra, G.C.; Moore, A.; Muniruzzamann, M.; Musrock, M.; Nagle, J.L.; Nandi, B.K.; Newby, J.; Nystrand, J.; O' Brien, E.; O' Connor, P.; Ohnishi, H.; Oskarsson, A.; Osterman, L.; Oyama, K.; Paffrath, L.; Pancake, C.E.; Pantuev, V.S.; Petridis, A.N.; Pisani, R.P.; Plagge, T.; Plasil, F.; Purschke, M.L.; Rankowitz, S.; Rao, R.; Rau, M.; Read, K.F.; Ryu, S.S.; Sakaguchi, T.; Sato, H.D.; Seto, R.; Shiina, T.; Silvermyr, D.; Simon-Gillo, J.; Simpson, M.; Sippach, W.; Skank, H.D.; Skutnik, S.; Sleege, G.A.; Smith, G.D.; Smith, M.; Stankus, P.W.; Steinberg, P.; Sugitate, T.; Sullivan, J.P.; Taketani, A.; Tamai, M.; Tanaka, Y.; Thomas, W.D.; Todd, R.; Toldo, F.; Turner, G.; Ushiroda, T.; Velkovska, J.; Hecke, H.W. van; Lith, M. van; Villatte, L.; Achen, W. von; Walker, J.W.; Wang, H.Q.; White, S.N.; Wintenberg, A.L.; Witzig, C.; Wood, L.[and others

    2003-03-01

    The PHENIX On-Line system takes signals from the Front End Modules (FEM) on each detector subsystem for the purpose of generating events for physics analysis. Processing of event data begins when the Data Collection Modules (DCM) receive data via fiber-optic links from the FEMs. The DCMs format and zero suppress the data and generate data packets. These packets go to the Event Builders (EvB) that assemble the events in final form. The Level-1 trigger (LVL1) generates a decision for each beam crossing and eliminates uninteresting events. The FEMs carry out all detector processing of the data so that it is delivered to the DCMs using a standard format. The FEMs also provide buffering for LVL1 trigger processing and DCM data collection. This is carried out using an architecture that is pipelined and deadtimeless. All of this is controlled by the Master Timing System (MTS) that distributes the RHIC clocks. A Level-2 trigger (LVL2) gives additional discrimination. A description of the components and operation of the PHENIX On-Line system is given and the solution to a number of electronic infrastructure problems are discussed.

  5. On-line moisture analysis

    CERN Document Server

    Cutmore, N G

    2002-01-01

    Measurement of the moisture content of iron ore has become a key issue for controlling moisture additions for dust suppression. In most cases moisture content is still determined by manual or automatic sampling of the ore stream, followed by conventional laboratory analysis by oven drying. Although this procedure enables the moisture content to be routinely monitored, it is too slow for control purposes. This has generated renewed interest in on-line techniques for the accurate and rapid measurement of moisture in iron ore on conveyors. Microwave transmission techniques have emerged over the past 40 years as the dominant technology for on-line measurement of moisture in bulk materials, including iron ores. Alternative technologies have their limitations. Infra-red analysers are used in a variety of process industries, but rely on the measurement of absorption by moisture in a very thin surface layer. Consequently such probes may be compromised by particle size effects and biased presentation of the bulk mater...

  6. On-line digestion system for protein characterization and proteome analysis.

    Science.gov (United States)

    López-Ferrer, Daniel; Petritis, Konstantinos; Lourette, Natacha M; Clowers, Brian; Hixson, Kim K; Heibeck, Tyler; Prior, David C; Pasa-Tolić, Ljiljana; Camp, David G; Belov, Mikhail E; Smith, Richard D

    2008-12-01

    An efficient on-line digestion system that reduces the number of sample manipulation steps has been demonstrated for high-throughput proteomics. By incorporating a pressurized sample loop into a liquid chromatography-based separation system, both sample and enzyme (e.g., trypsin) can be simultaneously introduced to produce a complete, yet rapid digestion. Both standard proteins and a complex Shewanella oneidensis global protein extract were digested and analyzed using the automated online pressurized digestion system coupled to an ion mobility time-of-flight mass spectrometer, an ion trap mass spectrometer, or both. The system denatured, digested, and separated product peptides in a manner of minutes, making it amenable to on-line high-throughput applications. In addition to simplifying and expediting sample processing, the system was easy to implement and no cross-contamination was observed among samples. As a result, the online digestion system offers a powerful approach for high-throughput screening of proteins that could prove valuable in biochemical research (rapid screening of protein-based drugs).

  7. On-line acquisition, analysis and presentation of neurophysiological data based on a personal microcomputer system.

    Science.gov (United States)

    Stromquist, B R; Pavlides, C; Zelano, J A

    1990-12-01

    A microcomputer based system is described for the acquisition, averaging, displaying, analysis and storage of electrophysiological (EPSP and post-stimulus histogram) data. The system consists of commercially available hardware (IBM-PC AT compatible, 80286 or 80386 based microcomputer, Burr-Brown analog-to-digital (A/D) converter), a custom built interface module, and a combination of commercially available and custom built software packages. The software operates within a Microsoft Windows environment and is comprised of custom built data acquisition and review modules which are linked to Microsoft's Excel program. The system is capable of four channel A/D conversion of EPSP's at a sampling frequency of up to 10 KHz (50 KHz single channel), the averaging of data including the addition and subtraction of various channels, the graphical display of data, the extraction of various data parameters, and the transfer of data to an Excel spreadsheet. The spreadsheet allows for the development of mathematical formulas for statistical analysis of data and presentation of the results in graphical form. Finally, data can easily be output to a laser printer or plotter. A sample experiment, illustrating system operation, is presented.

  8. A novel inlet system for on-line chemical analysis of semi-volatile submicron particulate matter

    Directory of Open Access Journals (Sweden)

    P. Eichler

    2014-09-01

    Full Text Available We herein present the concept of a novel modular inlet system that allows using gas-phase analyzers for on-line chemical characterization of semi-volatile submicron particles. The "chemical analysis of aerosol on-line" (CHARON inlet consists of a gas-phase denuder for stripping off gas-phase analytes, an aerodynamic lens for particle enrichment in the sampling flow and a thermo-desorption unit for particle volatilization prior to chemical analysis. We coupled the CHARON inlet to a proton-transfer-reaction time-of-flight mass spectrometer (PTR-ToF-MS which quantitatively detects most organic analytes and ammonia. The combined set-up measures submicron organic and ammonium nitrate/sulfate particles online. Two proof-of-principle studies were carried out for demonstrating the analytical power of the new set-up in analyzing primarily emitted and secondarily generated particles. Oxygenated organics and their partitioning between the gas and the particulate phase were observed from the reaction of limonene with ozone. Abundant quasi-molecular ions of organic particulate constituents were observed when submicron particles were sampled from diluted mainstream cigarette smoke.

  9. Sequential injection system for on-line analysis of total nitrogen with UV-mineralization.

    Science.gov (United States)

    Oms, M T; Cerdà, A; Cerdà, V

    2003-02-01

    An automatic method for the determination of total nitrogen in wastewater by sequential injection analysis and mineralization with UV radiation has been developed. The method is based on the mineralization of the samples with sodium persulphate in basic medium under UV radiation. Small volumes of sample and reagents are firstly aspirated into a single channel and then propelled by flow reversal to the UV reactor and then to the detector. The organic and inorganic nitrogen compounds are oxidized to nitrate that is then measured at 226 nm. The sequential injection procedure has been optimized and the factors affecting the efficiency of the oxidation have been studied with a number of test substances with different chemical structures and properties. Solutions in the concentration range 1-56 gl(-1) of nitrogen can be analyzed with the described procedure. The sample rate is of 30-40 samples h(-1). The LOD is 0.6 mgl(-1) N and the reproducibility is 1.8% (28 mgl(-1) N). Organic carbon in the form of glucose was added to a number of test solutions to study the potential interference of organic matter. The method was compared with the Kjeldahl digestion method by analyzing 15 wastewater samples with both methods. The nitrate and nitrite content of the non-oxidized samples were subtracted from the corresponding nitrogen content determined after photo-oxidation and the value compared with the Kjeldahl nitrogen content.

  10. On-line HPLC Analysis System for Metabolism and Inhibition Studies in Precision-Cut Liver Slices

    NARCIS (Netherlands)

    van Midwoud, Paul M.; Janssen, Joost; Merema, M.T.; de Graaf, Inge A. M.; Groothuis, Geny M. M.; Verpoorte, Elisabeth

    2011-01-01

    A novel approach for on-line monitoring of drug metabolism in continuously perifused, precision-cut liver slices (PCLS) in a microfluidic system has been developed using high-performance liquid chromatography with UV detection (HPLC-UV). In this approach, PCLS are incubated in a microfluidic device

  11. Broadband network on-line data acquisition system with web based interface for control and basic analysis

    Science.gov (United States)

    Polkowski, Marcin; Grad, Marek

    2016-04-01

    Passive seismic experiment "13BB Star" is operated since mid 2013 in northern Poland and consists of 13 broadband seismic stations. One of the elements of this experiment is dedicated on-line data acquisition system comprised of both client (station) side and server side modules with web based interface that allows monitoring of network status and provides tools for preliminary data analysis. Station side is controlled by ARM Linux board that is programmed to maintain 3G/EDGE internet connection, receive data from digitizer, send data do central server among with additional auxiliary parameters like temperatures, voltages and electric current measurements. Station side is controlled by set of easy to install PHP scripts. Data is transmitted securely over SSH protocol to central server. Central server is a dedicated Linux based machine. Its duty is receiving and processing all data from all stations including auxiliary parameters. Server side software is written in PHP and Python. Additionally, it allows remote station configuration and provides web based interface for user friendly interaction. All collected data can be displayed for each day and station. It also allows manual creation of event oriented plots with different filtering abilities and provides numerous status and statistic information. Our solution is very flexible and easy to modify. In this presentation we would like to share our solution and experience. National Science Centre Poland provided financial support for this work via NCN grant DEC-2011/02/A/ST10/00284.

  12. Total on-line purchasing system (TOPS)

    Energy Technology Data Exchange (ETDEWEB)

    Collins, N.

    1995-11-01

    The Information Management Division (IMD) at LLNL is developing a new purchasing system for the Procurement Department. The first major development of this new system is called, {open_quotes}Total On-Line Purchasing System{close_quotes} (TOPS). TOPS will help speed up the requisitioning process by having requisitions electronically entered by requesters and electronically sent to buyers to be put on Purchase Orders. The new purchasing system will use Electronic Commerce (EC)/Electronic Data Interchange (EDI), to help increase transaction flows for shipping notices, RFQs, Quotes, Purchase Orders, and Invoices. ANSI X.12 is the EDI standard that this new EC will use.

  13. Tolerance analysis of a micro-optical detection system for on-line monitoring of lubricant oils

    Science.gov (United States)

    Van Overmeire, S.; Ottevaere, H.; Mignani, A. G.; Ciaccheri, L.; Desmet, G.; Thienpont, H.

    2010-10-01

    We present a functional prototype of a micro-optical detection unit for both absorbance and laser-induced fluorescence analysis in fused silica capillaries. Absorbance detection allows concentration measurements ranging from 0.6 µM to 12 mM, whereas fluorescence detection enables concentration measurements from 6 pM up to 0.6 mM. We make use of non-sequential optical ray tracing simulations combined with statistical design methodology to perform a complete tolerance analysis for manufacturability and we demonstrate experimentally that the efficiency of the system is insensitive to reasonable misalignment and fabrication errors of its building blocks. The possibility of using standard fabrication techniques to prototype and replicate this miniaturized plastic detection system, as well as its wide measurement range make it a good candidate for applications where low-cost and portable systems are needed to measure small volumes of liquid samples with low-level concentrations. As an example we demonstrate the use of the system for the optical characterization and differentiation of nanoliter volumes of lubricant oils.

  14. Automated on-line liquid–liquid extraction system for temporal mass spectrometric analysis of dynamic samples

    Energy Technology Data Exchange (ETDEWEB)

    Hsieh, Kai-Ta; Liu, Pei-Han [Department of Applied Chemistry, National Chiao Tung University, 1001 University Rd, Hsinchu, 300, Taiwan (China); Urban, Pawel L. [Department of Applied Chemistry, National Chiao Tung University, 1001 University Rd, Hsinchu, 300, Taiwan (China); Institute of Molecular Science, National Chiao Tung University, 1001 University Rd, Hsinchu, 300, Taiwan (China)

    2015-09-24

    Most real samples cannot directly be infused to mass spectrometers because they could contaminate delicate parts of ion source and guides, or cause ion suppression. Conventional sample preparation procedures limit temporal resolution of analysis. We have developed an automated liquid–liquid extraction system that enables unsupervised repetitive treatment of dynamic samples and instantaneous analysis by mass spectrometry (MS). It incorporates inexpensive open-source microcontroller boards (Arduino and Netduino) to guide the extraction and analysis process. Duration of every extraction cycle is 17 min. The system enables monitoring of dynamic processes over many hours. The extracts are automatically transferred to the ion source incorporating a Venturi pump. Operation of the device has been characterized (repeatability, RSD = 15%, n = 20; concentration range for ibuprofen, 0.053–2.000 mM; LOD for ibuprofen, ∼0.005 mM; including extraction and detection). To exemplify its usefulness in real-world applications, we implemented this device in chemical profiling of pharmaceutical formulation dissolution process. Temporal dissolution profiles of commercial ibuprofen and acetaminophen tablets were recorded during 10 h. The extraction-MS datasets were fitted with exponential functions to characterize the rates of release of the main and auxiliary ingredients (e.g. ibuprofen, k = 0.43 ± 0.01 h{sup −1}). The electronic control unit of this system interacts with the operator via touch screen, internet, voice, and short text messages sent to the mobile phone, which is helpful when launching long-term (e.g. overnight) measurements. Due to these interactive features, the platform brings the concept of the Internet-of-Things (IoT) to the chemistry laboratory environment. - Highlights: • Mass spectrometric analysis normally requires sample preparation. • Liquid–liquid extraction can isolate analytes from complex matrices. • The proposed system automates

  15. Multi-Sensor Distributive On-Line Processing, Visualization, and Analysis Infrastructure for an Agricultural Information System at the NASA Goddard Earth Sciences DAAC

    Science.gov (United States)

    Teng, William; Berrick, Steve; Leptuokh, Gregory; Liu, Zhong; Rui, Hualan; Pham, Long; Shen, Suhung; Zhu, Tong

    2004-01-01

    The Goddard Space Flight Center Earth Sciences Data and Information Services Center (GES DISC) Distributed Active Center (DAAC) is developing an Agricultural Information System (AIS), evolved from an existing TRMM On-line Visualization and Analysis System precipitation and other satellite data products and services. AIS outputs will be ,integrated into existing operational decision support system for global crop monitoring, such as that of the U.N. World Food Program. The ability to use the raw data stored in the GES DAAC archives is highly dependent on having a detailed understanding of the data's internal structure and physical implementation. To gain this understanding is a time-consuming process and not a productive investment of the user's time. This is an especially difficult challenge when users need to deal with multi-sensor data that usually are of different structures and resolutions. The AIS has taken a major step towards meeting this challenge by incorporating an underlying infrastructure, called the GES-DISC Interactive Online Visualization and Analysis Infrastructure or "Giovanni," that integrates various components to support web interfaces that ,allow users to perform interactive analysis on-line without downloading any data. Several instances of the Giovanni-based interface have been or are being created to serve users of TRMM precipitation, MODIS aerosol, and SeaWiFS ocean color data, as well as agricultural applications users. Giovanni-based interfaces are simple to use but powerful. The user selects geophysical ,parameters, area of interest, and time period; and the system generates an output ,on screen in a matter of seconds.

  16. On-line identification of vehicle fuel consumption for energy and emission management: an LTP System Analysis

    NARCIS (Netherlands)

    Kessels, J.T.B.A.; Sijs, J.; Hermans, R.M.; Damen, A.A.H.; Bosch, P.P.J. van den; Papp, Z.; Lazar, M.

    2008-01-01

    Abstract—An Energy Management (EM) system traditionally relies on (quasi) static maps offering efficiency parameters of the vehicle powertrain. During a vehicle’s life span, these maps lose validity, so optimal performance for EM is not assured. This paper presents a proof-of-concept for a novel mea

  17. A pipeline VLSI design of fast singular value decomposition processor for real-time EEG system based on on-line recursive independent component analysis.

    Science.gov (United States)

    Huang, Kuan-Ju; Shih, Wei-Yeh; Chang, Jui Chung; Feng, Chih Wei; Fang, Wai-Chi

    2013-01-01

    This paper presents a pipeline VLSI design of fast singular value decomposition (SVD) processor for real-time electroencephalography (EEG) system based on on-line recursive independent component analysis (ORICA). Since SVD is used frequently in computations of the real-time EEG system, a low-latency and high-accuracy SVD processor is essential. During the EEG system process, the proposed SVD processor aims to solve the diagonal, inverse and inverse square root matrices of the target matrices in real time. Generally, SVD requires a huge amount of computation in hardware implementation. Therefore, this work proposes a novel design concept for data flow updating to assist the pipeline VLSI implementation. The SVD processor can greatly improve the feasibility of real-time EEG system applications such as brain computer interfaces (BCIs). The proposed architecture is implemented using TSMC 90 nm CMOS technology. The sample rate of EEG raw data adopts 128 Hz. The core size of the SVD processor is 580×580 um(2), and the speed of operation frequency is 20MHz. It consumes 0.774mW of power during the 8-channel EEG system per execution time.

  18. 浅析BPM系统上线准备工作%Analysis of On-line Preparation Work of the BPM System

    Institute of Scientific and Technical Information of China (English)

    黄新华

    2013-01-01

      在了解清楚BPM想解决的问题基础上选择性的进行分析,研究,最终做好项目上线前的准备工作,确保BPM项目顺利上线。%Based on a clear understanding of problems BPM want to solve, this paper conducted selective analysis and research, to do well the on-line preparatory work of project and ensure the success on-line of BPM project.

  19. On-Line Coolant Chemistry Analysis

    Energy Technology Data Exchange (ETDEWEB)

    LM Bachman

    2006-07-19

    Impurities in the gas coolant of the space nuclear power plant (SNPP) can provide valuable indications of problems in the reactor and an overall view of system health. By monitoring the types and amounts of these impurities, much can be implied regarding the status of the reactor plant. However, a preliminary understanding of the expected impurities is important before evaluating prospective detection and monitoring systems. Currently, a spectroscopy system is judged to hold the greatest promise for monitoring the impurities of interest in the coolant because it minimizes the number of entry and exit points to the plant and provides the ability to detect impurities down to the 1 ppm level.

  20. Properties of on-line social systems

    Science.gov (United States)

    Grabowski, A.; Kruszewska, N.; Kosiński, R. A.

    2008-11-01

    We study properties of five different social systems: (i) internet society of friends consisting of over 106 people, (ii) social network consisting of 3 × 104 individuals, who interact in a large virtual world of Massive Multiplayer Online Role Playing Games (MMORPGs), (iii) over 106 users of music community website, (iv) over 5 × 106 users of gamers community server and (v) over 0.25 × 106 users of books admirer website. Individuals included in large social network form an Internet community and organize themselves in groups of different sizes. The destiny of those systems, as well as the method of creating of new connections, are different, however we found that the properties of these networks are very similar. We have found that the network components size distribution follow the power-law scaling form. In all five systems we have found interesting scaling laws concerning human dynamics. Our research has shown how long people are interested in a single task, how much time they devote to it and how fast they are making friends. It is surprising that the time evolution of an individual connectivity is very similar in each system.

  1. Multi-Sensor Distributive On-line Processing, Visualization, and Analysis Infrastructure for an Agricultural Information System at the NASA Goddard Earth Sciences DAAC

    Science.gov (United States)

    Teng, W.; Berrick, S.; Leptoukh, G.; Liu, Z.; Rui, H.; Pham, L.; Shen, S.; Zhu, T.

    2004-12-01

    The Goddard Space Flight Center Earth Sciences Data and Information Services Center (GES DISC) Distributed Active Archive Center (DAAC) is developing an Agricultural Information System (AIS), evolved from an existing TRMM Online Visualization and Analysis System (TOVAS), which will operationally provide precipitation and other satellite data products and services. AIS outputs will be integrated into existing operational decision support systems for global crop monitoring, such as that of the U.N. World Food Program. The ability to use the raw data stored in the GES DAAC archives is highly dependent on having a detailed understanding of the data's internal structure and physical implementation. To gain this understanding is a time-consuming process and not a productive investment of the user's time. This is an especially difficult challenge when users need to deal with multi-sensor data that usually are of different structures and resolutions. The AIS has taken a major step towards meeting this challenge by incorporating an underlying infrastructure, called the GES-DISC Interactive Online Visualization and Analysis Infrastructure or "Giovanni," that integrates various components to support web interfaces that allow users to perform interactive analysis on-line without downloading any data. Several instances of the Giovanni-based interface have been or are being created to serve users of TRMM precipitation, MODIS aerosol, and SeaWiFS ocean color data, as well as agricultural applications users. Giovanni-based interfaces are simple to use but powerful. The user selects geophysical parameters, area of interest, and time period; and the system generates an output on screen in a matter of seconds. The currently available output options are (1) area plot - averaged or accumulated over any available data period for any rectangular area; (2) time plot - time series averaged over any rectangular area; (3) Hovmoller plots - longitude-time and latitude-time plots; (4) ASCII

  2. The ISO SWS on-line system

    Science.gov (United States)

    Roelfsema, P. R.; Kester, D. J. M.; Wesselius, P. R.; Wieprech, E.; Sym, N.

    1992-01-01

    The software which is currently being developed for the Short Wavelength Spectrometer (SWS) of the Infrared Space Observatory (ISO) is described. The spectrometer has a wide range of capabilities in the 2-45 micron infrared band. SWS contains two independent gratings, one for the long and one for the short wavelength section of the band. With the gratings a spectral resolution of approximately 1000 to approximately 2500 can be obtained. The instrument also contains two Fabry-Perault's yielding a resolution between approximately 1000 and approximately 20000. Software is currently being developed for the acquisition, calibration, and analysis of SWS data. The software is firstly required to run in a pipeline mode without human interaction, to process data as they are received from the telescope. However, both for testing and calibration of the instrument as well as for evaluation of the planned operating procedures the software should also be suitable for interactive use. Thirdly the same software will be used for long term characterization of the instrument. The software must work properly within the environment designed by the European Space Agency (ESA) for the spacecraft operations. As a result strict constraints are put on I/O devices, throughput etc.

  3. Economic Analysis (EA) Support for Automated Information System Control Board (AISCB) Working Group. Part 1. Cataloging-Tools-on-Line (CTOL) Automated Information System (AIS) Economic Analysis.

    Science.gov (United States)

    1986-08-01

    functional sers thromaja actual observations draring NW, 1IM, of the itsm Identification processes in DOW cataloging operation*. Through analysis of the...time to cmplete processes and tho tim sawed -- der Alternative 5, the following benefits are derived: a. Tim required for the itsm identification...cataloging transaction will be reduced from 5.6 bore to 4.5 hour or as 20S reduction in tine. ICe Overall, time, required to prepare itsm ideutation data

  4. On-line Payment System Survey – eCash

    Directory of Open Access Journals (Sweden)

    Marius Popa

    2009-12-01

    Full Text Available The paper presents the main aspects regarding an on-line payment system. Some characteristics of such system are presented and an existing system is analyzed. On its fundamental sense, the electronic commerce is a concept that represents the purchase and sale process or exchange of products, services, information, using o computer network, inclusively the Internet. In the most part of the cases, the electronic commerce imply on-line payments that lead to creation of some kinds of electronic money and some specific payment systems. There are described the some electronic payment mechanisms and the architecture and the functions of the on-line payment system E-Cash are depicted.

  5. The dynamics of on-line principal component analysis

    NARCIS (Netherlands)

    Biehl, M.; Schlösser, E.

    1998-01-01

    The learning dynamics of an on-line algorithm for principal component analysis is described exactly in the thermodynamic limit by means of coupled ordinary differential equations for a set of order parameters. It is demonstrated that learning is delayed significantly because existing symmetries amon

  6. On-Line Synthesis and Analysis by Mass Spectrometry

    Science.gov (United States)

    Bain, Ryan M.; Pulliam, Christopher J.; Raab, Shannon A.; Cooks, R. Graham

    2015-01-01

    In this laboratory experiment, students learn how to use ESI to accelerate chemical synthesis and to couple it with on-line mass spectrometry for structural analysis. The Hantzsch synthesis of symmetric 1,4-dihydropyridines is a classic example of a one-pot reaction in which multiple intermediates can serve to indicate the progress of the reaction…

  7. On-Line Synthesis and Analysis by Mass Spectrometry

    Science.gov (United States)

    Bain, Ryan M.; Pulliam, Christopher J.; Raab, Shannon A.; Cooks, R. Graham

    2015-01-01

    In this laboratory experiment, students learn how to use ESI to accelerate chemical synthesis and to couple it with on-line mass spectrometry for structural analysis. The Hantzsch synthesis of symmetric 1,4-dihydropyridines is a classic example of a one-pot reaction in which multiple intermediates can serve to indicate the progress of the reaction…

  8. Isolation and Bioactivity Analysis of Ethyl Acetate Extract from Acer tegmentosum Using In Vitro Assay and On-Line Screening HPLC-ABTS+ System

    Directory of Open Access Journals (Sweden)

    Kwang Jin Lee

    2014-01-01

    Full Text Available The Acer tegmentosum (3 kg was extracted using hot water, and the freeze-dried extract powder was partitioned successively using dichloromethane (DCM, ethyl acetate (EA, butyl alcohol (n-BuOH, and water. From the EA extract fraction (1.24 g, five phenolic compounds were isolated by the silica gel, octadecyl silica gel, and Sephadex LH-20 column chromatography. Based on spectroscopic methods such as 1H-NMR, 13C-NMR, and LC/MS the chemical structures of the compounds were confirmed as feniculin (1, avicularin (2, (+-catechin (3, (−-epicatechin (4, and 6′-O-galloyl salidroside (5. Moreover, a rapid on-line screening HPLC-ABTS+ system for individual bioactivity of the EA-soluble fraction (five phenolic compounds was developed. The results indicated that compounds 1 and 2 were first isolated from the A. tegmentosum. The anti-inflammatory activities and on-line screening HPLC-ABTS+ assay method of these compounds in LPS-stimulated murine macrophages were rapid and efficient for the investigation of bioactivity of A. tegmentosum.

  9. Two Types of Designs for On-Line Circulation Systems

    Directory of Open Access Journals (Sweden)

    Rob McGee

    1972-09-01

    Full Text Available On-line circulation systems divide into two types. One type contains records only for charged or otherwise absent items. The other contains a file of records for all titles or volumes in the library collection, regardless of their circulation status. This paper traces differences between the two types, examining different kinds of files and terminals, transaction evidence, the quality of bibliographic data, querying, and the possibility of functions outside circulation. Aspects of both operational and potential systems are considered.

  10. On-line Dynamic Security Assessment in Power Systems

    DEFF Research Database (Denmark)

    Weckesser, Johannes Tilman Gabriel

    tools may no longer be feasible, since they are generally based on extensive off-line studies. A core component of an efficient on-line dynamic security assessment is a fast and reliable contingency screening. As part of this thesis a contingency screening method is developed and its performance......The thesis concerns the development of tools and methods for on-line dynamic security assessment (DSA). In a future power system with low-dependence or even independence of fossil fuels, generation will be based to a large extent on noncontrollable renewable energy sources (RES), such as wind...... and solar radiation. Moreover, ongoing research suggests that demand response will be introduced to maintain power balance between generation and consumption at all times. Due to these changes the operating point of the power system will be less predictable and today’s stability and security assessment...

  11. On-line corrosion monitoring in district heating systems

    DEFF Research Database (Denmark)

    Richter, Sonja; Thorarinsdottir, R.I.; Hilbert, Lisbeth Rischel

    2004-01-01

    complicates the chemistry of the environment. Hydrogen sulphide is present in geothermal systems and can be formed as a by-product of sulphate-reducing-bacteria (SRB). The application of electrochemical methods makes on-line monitoring possible. These methods include: Linear Polarization Resistance (LPR......), Electrochemical Noise (EN) and Zero Resistance Ammetry (ZRA). Electrochemical Resistance (ER) has also been used to measure corrosion. The method traditionally only measures corrosion off-line but with newly developed high-sensitive ER technique developed by MetriCorr in Denmark, on-line monitoring is possible......Traditionally corrosion monitoring in district heating systems has been performed offline via weight loss coupons. These measurements give information about the past and not the present situation and require long exposure time (weeks or months). The good quality of district heating medium makes...

  12. On-line Corrosion Monitoring in District Heating Systems

    DEFF Research Database (Denmark)

    Richter, Sonja; Thorarinsdottir, R.I.; Hilbert, Lisbeth Rischel

    2005-01-01

    The corrosion control in district heating systems is today performed primarily with control of the water quality. The corrosion rate is kept low by assuring low dissolved oxygen concentration, high pH and low conductivity. Corrosion failures can occur, e.g. as a result of unknown oxygen ingress......, precipitation of deposits or crevices. The authors describe methods used for on-line monitoring of corrosion, cover the complications and the main results of a Nordic project....

  13. Design and development of a miniaturised total chemical analysis system for on-line lactate and glucose monitoring in biological samples

    NARCIS (Netherlands)

    Dempsey, Eithne; Diamond, Dermot; Smyth, Malcolm R.; Urban, Gerald; Jobst, Gerhard; Moser, Isabella; Verpoorte, Elisabeth M.J.; Manz, Andreas; Widmer, H. Michael; Rabenstein, Kai; Freaney, Rosemarie

    1997-01-01

    A miniaturised Total chemical Analysis System (μTAS) for glucose and lactate measurement in biological samples constructed based on an integrated microdialysis sampling and detection system. The complete system incorporates a microdialysis probe for intravascular monitoring in an ex vivo mini-shunt

  14. On-line Test for Train Communication Based System

    Institute of Scientific and Technical Information of China (English)

    Zeng Xiaoqing; Masayuki Matsumoto; Kinji Mori; XU Fucang

    2002-01-01

    This paper gives out a new train automatic control system, which is based on train communication, and proposes a high assurance method to construct the system from current system. In current automatic train control (ATC) system, the central logic device detects position of each train and calculates permissible speed of each blocking section. Therefore, the central logic device controls speed of all trains. On the contrary, in the new system proposed in this paper, there is no central logical device and, train can communicate each other. The train detects the position and calculates the permissible speed itself according to the received position information of the preceding train. In the traditional method of changing an old system to a new one, test must be done off-line.While the integration technique proposed in this paper achieves on-line properties, and high assurance can be satisfied.

  15. Research of on-line detection system for power capacitor

    Science.gov (United States)

    Yao, Junda; Qian, Zheng; Yu, Hao; Xia, Jiuyun

    2016-01-01

    The hidden danger exists in the power capacitor of power system due to long-time operation under the environment of high voltage. Thus, it is possible to induce serious fault, and the on-line detection system is urgently required. In this paper, two methods of the on-line detection system are compared in order to realize the better real-time condition detection. The first method is based on the STM microprocessor with an internal 12 bit A/D converter, which converts analog signals which is arrived from the sample circuit into digital signals, and then the FFT algorithm is used to accomplish the measurement of the voltage and current values of the capacitor. The second method is based on the special electric energy metering IC, which can obtain RMS (Root Mean Square) of voltage and current by processing the sampled data of the voltage and current, and store RMS of voltage and current in its certain registers. The operating condition of the capacitor can be obtained after getting the values of voltage and current. By comparing the measuring results of two methods, the second method could achieve a higher measurement accuracy and more simple construction.

  16. A Distributed System for Learning Programming On-Line

    Science.gov (United States)

    Verdu, Elena; Regueras, Luisa M.; Verdu, Maria J.; Leal, Jose P.; de Castro, Juan P.; Queiros, Ricardo

    2012-01-01

    Several Web-based on-line judges or on-line programming trainers have been developed in order to allow students to train their programming skills. However, their pedagogical functionalities in the learning of programming have not been clearly defined. EduJudge is a project which aims to integrate the "UVA On-line Judge", an existing…

  17. Sequential flow injection analysis system on-line coupled to high intensity focused ultrasound: green methodology for trace analysis applications as demonstrated for the determination of inorganic and total mercury in waters and urine by cold vapor atomic absorption spectrometry.

    Science.gov (United States)

    Fernandez, C; Conceição, Antonio C L; Rial-Otero, R; Vaz, C; Capelo, J L

    2006-04-15

    A new concept is presented for green analytical applications based on coupling on-line high-intensity focused ultrasound (HIFU) with a sequential injection/flow injection analysis (SIA/FIA) system. The potential of the SIA/HIFU/FIA scheme is demonstrated by taking mercury as a model analyte. Using inorganic mercury, methylmercury, phenylmercury, and diphenylmercury, the usefulness of the proposed methodology for the determination of inorganic and total mercury in waters and urine was demonstrated. The procedure requires low sample volumes and reagents and can be further applied to all chemical reactions involving HIFU. The inherent advantages of SIA, FIA, and HIFU applications in terms of high throughput, automation, low reagent consumption, and green chemistry are accomplished together for the first time in the present work.

  18. On-line monitoring of gas-phase bioreactors for biogas treatment: hydrogen sulfide and sulfide analysis by automated flow systems

    Energy Technology Data Exchange (ETDEWEB)

    Redondo, Rosa; Cunha Machado, Vinicius; Lafuente, Javier; Gabriel, David [Universitat Autonoma de Barcelona, Departament d' Enginyeria Quimica, Escola Tecnica Superior d' Enginyeria (ETSE), Bellaterra (Spain); Baeza, Mireia [Edifici C-Nord, Universitat Autonoma de Barcelona, Grup de Sensors i Biosensors, Departament de Quimica, Facultat de Ciencies, Bellaterra (Spain)

    2008-06-15

    Biogas is produced by biological processes under anaerobic conditions and may contain up to 20,000 ppm{sub v} hydrogen sulfide (H{sub 2}S), a corrosive substance that attacks power engines and can affect the health of the industrial staff. H{sub 2}S must be removed from the biogas, especially in co-generation facilities where the biogas is burnt for energy production. Nowadays, biofiltration is being studied and considered as an interesting alternative for removing H{sub 2}S from the biogas besides classical chemical processes. The novelty of this work is the design and construction of an automated H{sub 2}S on-line analyser to assess the composition of the liquid and gas phases of gas-phase bioreactors. The analyser is made of two parallel flow configurations which share the same detection device. The first configuration is a single-channel flow injection analyser (FIA) to detect S{sup 2-} in the liquid phase. The second configuration is a continuous flow analyser (CFA) with a gaseous diffusion step (GD-CFA) for detecting H{sub 2}S in the gas phase. The diffusion step enables separation of the H{sub 2}S{sub (g)} from the sample and its conversion into a detectable chemical species (S{sup 2-}). S{sup 2-} detection was performed with an Ag{sub 2}S ion-selective electrode (ISE) selective to S{sup 2-}{sub (aq)}. The main response parameters of the FIA system are a linear range between 3 x 10{sup -5} and 1 x 10{sup -1} mol L{sup -1} S{sup 2-} (0.61-3,200 mg L{sup -1}), with a sensitivity of 27.9 mV decade{sup -1} and a detection limit of 1.93 x 10{sup -5} mol L{sup -1} S{sup 2-}. The GD-CFA configuration presents a linear range between 400 and 10,000 ppm{sub v} H{sub 2}S{sub (g)} with a sensitivity of 26.1 mV decade{sup -1} and a detection limit of 245 ppm{sub v} H{sub 2}S. The proposed analyser was used by analysing real gas and liquid samples with optimal results at a full-scale biotrickling filter for biogas treatment at a municipal wastewater treatment plant. (orig.)

  19. Polar On-Line Acquisition Relay and Transmission System (POLARATS)

    Energy Technology Data Exchange (ETDEWEB)

    Yuracko, K.

    2004-07-15

    POLARATS (Polar On-Line Acquisition Relay And Transmission System) is being developed by YAHSGS LLC (YAHSGS) and Oak Ridge National Laboratory (ORNL) to provide remote, unattended monitoring of environmental parameters under harsh environmental conditions. In particular, instrumental design and engineering is oriented towards protection of human health in the Arctic, and with the additional goal of advancing Arctic education and research. POLARATS will obtain and transmit environmental data from hardened monitoring devices deployed in locations important to understanding atmospheric and aquatic pollutant migration as it is biomagnified in Arctic food chains. An Internet- and personal computer (PC)-based educational module will provide real time sensor data, on-line educational content, and will be integrated with workbooks and textbooks for use in middle and high school science programs. The educational elements of POLARATS include an Internet-based educational module that will instruct students in the use of the data and how those data fit into changing Arctic environments and food chains. POLARATS will: (1) Enable students, members of the community, and scientific researchers to monitor local environmental conditions in real time over the Internet; and (2) Provide additional educational benefits through integration with middle- and high-school science curricula. Information will be relayed from POLARATS devices to classrooms and libraries along with custom-designed POLARATS teaching materials that will be integrated into existing curricula to enhance the educational benefits realized from the information obtained.

  20. The Monitor System for the LHCb on-line farm

    CERN Document Server

    Bonifazi, F; Carbone, A; Galli, D; Gregori, D; Marconi, U; Peco, G; Vagnoni, V

    2005-01-01

    The aim of the LHCb on-line farm Monitor System is to keep under control all the working indicators which are relevant for the farm operation, and to set the appropriate alarms whenever an error or a critical condition comes up. Since the most stressing tasks of the farm are the data transfer and processing, relevant indicators includes the CPU and the memory load of the system, the network interface and the TCP/IP stack parameters, the rates of the interrupts raised by the network interface card and the detailed status of the running processes. The monitoring of computers’ physical conditions (temperatures, fan speeds and motherboard voltages) are the subject of a separate technical note, since they are accessed in a different way, by using the IPMI protocol.

  1. On-line corrosion monitoring in district heating systems

    DEFF Research Database (Denmark)

    Richter, Sonja; Thorarinsdottir, R.I.; Hilbert, Lisbeth Rischel

    2004-01-01

    Traditionally corrosion monitoring in district heating systems has been performed offline via weight loss coupons. These measurements give information about the past and not the present situation and require long exposure time (weeks or months). The good quality of district heating medium makes...... corrosion monitoring a challenge. Under normal conditions the pH is high (app. 9), conductivity is low (app. 10-200 µS/cm) and the concentration of dissolved oxygen is negligible. The low corrosion rates (in the order of µm/y) are difficult to measure and furthermore, factors such as hydrogen sulphide......), Electrochemical Noise (EN) and Zero Resistance Ammetry (ZRA). Electrochemical Resistance (ER) has also been used to measure corrosion. The method traditionally only measures corrosion off-line but with newly developed high-sensitive ER technique developed by MetriCorr in Denmark, on-line monitoring is possible...

  2. Development and Application of On-line Wind Power Risk Assessment System

    Institute of Scientific and Technical Information of China (English)

    2012-01-01

    Because of the large-scale integration of wind power, the dynamic characteristics of power system have many uncertain effects. Based on deterministic analysis methods, traditional on-line security assessment system cannot quantitatively estimate the actual operating conditions of the power system for only considering the most serious and credible accidents. Therefore, the risk theory is introduced into an on-line security assessment system and then an on-line risk assessment dynamic security assessment system system for wind power is designed Based on multiple data integration, and implemented by combining with the the wind power disturbance probability is available and the security assessment of the power grid can obtain security indices in different aspects. The operating risk index is an expectation of severity, computed by summing up all the products of the result probability and its severity. Analysis results are reported to the dispatchers in on-line environment, while the comprehensive weak links are automatically provided to the power dispatching center. The risk assessment system in operation can verify the reasonableness of the system.

  3. SeaBuoySoft – an On-line Automated Windows based Ocean Wave height Data Acquisition and Analysis System for Coastal Field’s Data Collection

    Directory of Open Access Journals (Sweden)

    P.H.Tarudkar

    2014-12-01

    Full Text Available Measurement of various hydraulic parameters such as wave heights for the research and the practical purpose in the coastal fields is one of the critical and challenging but equally important criteria in the field of ocean engineering for the design and the development of hydraulic structures such as construction of sea walls, break waters, oil jetties, fisheries harbors, all other structures, and the ships maneuvering, embankments, berthing on jetties. This paper elucidates the development of “SeaBuoySoft online software system for coastal field‟s wave height data collection” for the coastal application work. The system could be installed along with the associated hardware such as a Digital Waverider Receiver unit and a Waverider Buoy at the shore. The ocean wave height data, transmitted by wave rider buoy installed in the shallow/offshore waters of sea is received by the digital waverider receiver unit and it is interfaced to the SeaBuoySoft software. The design and development of the software system has been worked out in-house at Central Water and Power Research Station, Pune, India. The software has been developed as a Windows based standalone version and is unique of its kind for the reception of real time ocean wave height data, it takes care of its local storage of wave height data for its further analysis work as and when required. The system acquires real time ocean wave height data round the clock requiring no operator intervention during data acquisition process on site.

  4. Development of on-line laser power monitoring system

    Science.gov (United States)

    Ding, Chien-Fang; Lee, Meng-Shiou; Li, Kuan-Ming

    2016-03-01

    Since the laser was invented, laser has been applied in many fields such as material processing, communication, measurement, biomedical engineering, defense industries and etc. Laser power is an important parameter in laser material processing, i.e. laser cutting, and laser drilling. However, the laser power is easily affected by the environment temperature, we tend to monitor the laser power status, ensuring there is an effective material processing. Besides, the response time of current laser power meters is too long, they cannot measure laser power accurately in a short time. To be more precisely, we can know the status of laser power and help us to achieve an effective material processing at the same time. To monitor the laser power, this study utilize a CMOS (Complementary metal-oxide-semiconductor) camera to develop an on-line laser power monitoring system. The CMOS camera captures images of incident laser beam after it is split and attenuated by beam splitter and neutral density filter. By comparing the average brightness of the beam spots and measurement results from laser power meter, laser power can be estimated. Under continuous measuring mode, the average measuring error is about 3%, and the response time is at least 3.6 second shorter than thermopile power meters; under trigger measuring mode which enables the CMOS camera to synchronize with intermittent laser output, the average measuring error is less than 3%, and the shortest response time is 20 millisecond.

  5. FDD-1 System On-line Monitoring Fuel Rod Failure of Nuclear Power Plant

    Institute of Scientific and Technical Information of China (English)

    CHENPeng; ZHANGYing-chao; JISong-tao; GAOYong-guang; YINZhen-guo; HANChuan-bin

    2003-01-01

    The FDD-1 system developed by CIAE for on-line monitoring fuel rod failure of nuclear power plant consists of γ-ray detector, γ-ray spectrum analyzer, computer, and an analysis code for evaluating the status of fuel rod failure. It would be determined that the fuel rod failure occurs when a large amount of γ activity increases in the primary system measured by γ-ray detector near the CVCS.

  6. On-line analysis capabilities developed to support the AFW wind-tunnel tests

    Science.gov (United States)

    Wieseman, Carol D.; Hoadley, Sherwood T.; Mcgraw, Sandra M.

    1992-01-01

    A variety of on-line analysis tools were developed to support two Active Flexible Wing wind-tunnel tests. These tools were developed to verify control law execution, to satisfy analysis requirements of the control law designers, to provide measures of system stability in a real-time environment, and to provide project managers with a quantitative measure of controller performance. Description and purposes of capabilities which were developed are presented in this paper along with examples. Procedures for saving and transferring data for near real-time analysis, and descriptions of the corresponding data interface programs are also presented. The on-line analysis tools worked well before, during, and after the wind-tunnel tests and proved to be a vital and important part of the entire test effort.

  7. A narrow-band injection-seeded pulsed titanium : sapphire oscillator-amplifier system with on-line chirp analysis for high-resolution spectroscopy

    NARCIS (Netherlands)

    Hannemann, S.; Duijn, van E.J.; Ubachs, W.M.G.

    2007-01-01

    A narrow-band tunable injection-seeded pulsed titanium:sapphire laser system has been developed for application in high-resolution spectroscopic studies at the fundamental wavelengths in the near infrared as well as in the ultraviolet, deep ultraviolet, and extreme ultraviolet after upconversion.

  8. A narrow-band injection-seeded pulsed titanium : sapphire oscillator-amplifier system with on-line chirp analysis for high-resolution spectroscopy

    NARCIS (Netherlands)

    Hannemann, S.; Duijn, van E.J.; Ubachs, W.M.G.

    2007-01-01

    A narrow-band tunable injection-seeded pulsed titanium:sapphire laser system has been developed for application in high-resolution spectroscopic studies at the fundamental wavelengths in the near infrared as well as in the ultraviolet, deep ultraviolet, and extreme ultraviolet after upconversion. Sp

  9. Simple and Excellent Selective Chemiluminescence-Based CS2 On-Line Detection System for Rapid Analysis of Sulfur-Containing Compounds in Complex Samples.

    Science.gov (United States)

    Zhang, Runkun; Li, Gongke; Hu, Yufei

    2015-06-02

    To study the interesting chemical reaction phenomenon can greatly contribute to the development of an innovative analytical method. In this paper, a simple CL reaction cell was constructed to study the chemiluminescence (CL) emission from the thermal oxidation of carbon disulfide (CS2). We found that the CL detection of CS2 exhibits unique characteristics of excellent selectivity and rapid response capacity. Experimental investigations together with theoretical calculation were performed to study the mechanism behind the CL reaction. The results revealed that the main luminous intermediates generated during the thermal degradation of CS2 are SO2* and CO2*. Significantly, this CL emission phenomenon has a wide application due to many sulfur-containing compounds that can convert to CS2 under special conditions. On the basis of this scheme, a CS2-generating and detection system was developed for rapid measurement of CS2 or other compounds that can convert to CS2. The usefulness of the system was demonstrated by measuring dithiocarbamate (DTC) pesticides (selected mancozeb as a representative analyte) based on the evolution of CS2 in spiked agricultural products. Results showed that the system allows online and large volume detection of CS2 under nonequilibrium condition, which greatly reduces the analytical time. The concentrations of mancozeb in the spiked samples were well-quantified with satisfied recoveries of 76.9-97.3%. The system not only addresses the urgent need for rapid in-field screening of DTC residues in foodstuffs but also opens a new opportunity for the fast, convenient, and cost-effective detection of CS2 and some other sulfur-containing compounds in complex samples.

  10. On-Line Broken-Bar Fault Diagnosis System of Induction Motor

    Institute of Scientific and Technical Information of China (English)

    ZHANG Rong; WANG Xiuhe

    2008-01-01

    Induction motor faults including mechanical and electrical faults are reviewed. The fault diagnosis methods are summarized. To analyze the influence of stator current, torque, speed and rotor current on faulted bars, a time-stepping transient finite element (FE) model of induction motor with bars faulted is created in this paper. With wavelet package analysis method and FFT method, the simulation result of finite element is analyzed. Based on the simulation analysis, the on-line fault diagnosis system of induction motor with bars faulted is developed. With the speed of broken bars motor changed from 1 478 r/min to 1 445 r/min, the FFT power spectra and the wavelet package decoupling factors are given. The comparison result shows that the on-line diagnosis system can detect broken-bar fault efficiently.

  11. Semi-on-line analysis for fast and precise monitoring of bioreaction processes

    DEFF Research Database (Denmark)

    Christensen, L.H.; Marcher, J.; Schulze, Ulrik

    1996-01-01

    Monitoring of substrates and products during fermentation processes can be achieved either by on-line, in situ sensors or by semi-on-line analysis consisting of an automatic sampling step followed by an ex situ analysis of the retrieved sample. The potential risk of introducing time delays...... and signal bias during sampling makes it necessary to distinguish between real-time, on-line, in situ methods and semi-on-line analysis. In addition, semi-on-line analyzers are often mechanically complex-a circumstance which has to be given special attention during their industrial use on a routine basis....... This review on semi-on-line analysis will focus both on the dynamics and precision of aseptic sampling devices and on the performance of flow injection analysis (FIA) and sequential injection analysis (SIA), especially with regard to their robustness when used in industry. (C) 1996 John Wiley & Sons, Inc....

  12. Integrated On-line Instrumentation System of Magnetic Properties Measurement

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    A portable microcomputer-controlled inspection system has been developed for detection of mag netic properties of soft magnetic materials. It incorporates custom designed software for control of the magnetic field during operation such as demagnetization, field sweeping, and for data logging and analysis. Results are recorded using a 12-bit analog to digital converter and are then stored on disk. The magnetic hysteresis loop and Barkhausen noise data can be converted into important magnetic parameters:, coecivity, remanence, and hysteresis loss, Barkhausen ampli tude, and Barkhausen noise energy. This system incorporated with the magnetostriction, and magnetoacoustic emission, is then related with the nondestructive detection of material degra dation.

  13. Entirely automatic on-line analysis system applied to catalytic cracking of gasoline%汽油催化裂化的全自动在线分析系统

    Institute of Scientific and Technical Information of China (English)

    薛青松; 王一萌

    2011-01-01

    With one set of idle catalyst-testing equipment and three gas chromatograph, a novel system for entirely automatic on-line analyzing gasoline catalytic cracking products was developed by re-equipping the only automatic pneumatic controller adapted for directing three way of six-channel valves simultaneously. The modified equipment results of synchronism, multitasking and high robotization of reaction-analysis system, more time and resources were saved, either. Furthermore, the six-channel valves on standby status were revised adapted for clearer analysis system.%利用实验室闲置的高压微反应装置和气相色谱仪,通过改装高压微反应装置上唯一一路自动气动控制系统,使其同时控制三路六通阀,实现高压微反应-三台色谱-三套色谱软件联动,全自动在线分析汽油催化裂解产物,不仅实现了反应-分析的同步性、多任务化和高度自动化,实验成本也大幅下降.并对六通阀原待采样模式进行了改进,大幅降低了对管道的污染.

  14. Off-line and on-line noise analysis for core surveillance in French LMFBR 'Anabel'

    Energy Technology Data Exchange (ETDEWEB)

    Gourdon, J.; Casejuane, R.

    1982-01-01

    Some results concerning noise analysis studies performed in French LMFBR are presented in support to the design of an on-line noise analysis system to be included in the core surveillance and protection system of SUPER-PHENIX. This computerized system is presented: signal processing, block diagram, operating modes.

  15. On-line Batch Process Monitoring with Improved Multi-way Independent Component Analysis

    Institute of Scientific and Technical Information of China (English)

    GUO Hui; LI Hongguang

    2013-01-01

    In the past decades,on-line monitoring of batch processes using multi-way independent component analysis (MICA) has received considerable attention in both academia and industry.This paper focuses on two troublesome issues concerning selecting dominant independent components without a standard criterion and determining the control limits of monitoring statistics in the presence of non-Gaussian distribution.To optimize the number of key independent components,we introduce a novel concept of system deviation,which is able to evaluate the reconstructed observations with different independent components.The monitored statistics are transformed to Gaussian distribution data by means of Box-Cox transformation,which helps readily determine the control limits.The proposed method is applied to on-line monitoring of a fed-batch penicillin fermentation simulator,and the experimental results indicate the advantages of the improved MICA monitoring compared to the conventional methods.

  16. On-Line Multichannel Raman Spectroscopic Detection System For Capillary Zone Electrophoresis

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    An on-line multichannel Raman spectroscopic detection system for capillary electrophoresis was established by using an Ar+ laser and a cryogenically cooled ICCD. Resonant excitation Raman spectra of methyl red and methyl orange were employed to test the system. The result shows that it could yield on-line electrophoretogram and time series of Raman spectra.

  17. Development of an on-line control system for the cultivation of animal cells in a hollow-fiber reactor using flowing injection analysis and a visual programming language.

    Science.gov (United States)

    Stoll, T S; Ruffieux, P A; von Stockar, U; Marison, I W

    1996-10-18

    A system for the independent control of ammonia and glutamine in a hollow-fiber reactor has been developed. On-line analysis of the two chemical species was performed using FIA. A custom-made program has been written to fully automate the FIA, to perform measurements, calibrations and data acquisition, and to activate two peristaltic feed pumps. Diagnostic tests were also automatically performed in order to identify, and in some cases eliminate, erroneous measurements and calibrations due to instrument failures. For this purpose, a visual programming language (LabVIEW) has been chosen. Ammonia concentration was controlled by varying the medium supply rate to the hollow-fiber reactor which was shown to behave like an ideal-stirred tank reactor. The glutamine concentration was controlled through the intermittent activation of a pump delivering a concentrated solution of this species to the reactor. This control system was tested with a culture of hybridoma cells at three different ammonia and one glutamine set-points. The hollow-fiber reactor was successfully operated automatically for more than 1200 h with ammonia and glutamine concentrations accurately controlled at non-limiting levels. The visual programming environment was found to be reliable and highly suitable for the development of custom programs for bioprocess control.

  18. Development of an on-line monitoring expert system for heating system fouling

    Science.gov (United States)

    Wang, Yuan-yuan; Wang, Jian-guo

    2008-12-01

    This paper intends to develop an on-line monitoring expert system for heating system fouling. It chooses pressure, flowing and temperature as basic diagnostic variables. The basic evaluative guide lines are the coefficient of flowing resistance, the efficiency and cost of heating system. This system can be used to monitor the fouling degrees and estimate the fouling positions. The expert system is programmed by Delphi to realize all functions.

  19. On-Line Booking Policies and Competitive Analysis of Medical Examination in Hospital

    Directory of Open Access Journals (Sweden)

    Li Luo

    2014-01-01

    Full Text Available From the on-line point, we consider the hospital’s medical examination appointment problem with hierarchical machines. This approach eliminates the need for both demand forecasts and a risk-neutrality assumption. Due to different unit revenue, uncertain demand, and arrival of patients, we design on-line booking policies for two kinds of different situations from the perspective of on-line policy and competitive analysis. After that, we prove the optimal competitive ratios. Through numerical examples, we compare advantages and disadvantages between on-line policies and traditional policies, finding that there is different superiority for these two policies under different arrival sequences.

  20. An On-line Assessment System for English-Chinese Translation

    Institute of Scientific and Technical Information of China (English)

    TIAN Yan; LU Ru-zhan; DUAN Jian-yong

    2007-01-01

    On-line assessment of English-Chinese translation is a challenging task as it involves natural language processing. YanFa, an on-line assessment system for English-Chinese translation, is a pilot research project into scoring student's translation on-line. Based on the theory of translation equivalence, an algorithm called "conceptual similarity matching" was developed. YanFa can assess students' translation on-line timely, generate test papers automatically, offer standard versions of translation, and the scores of each sentence to students. The evaluation proves that YanFa is practical compared with the scores given by experts.

  1. Computers in Information Sciences: On-Line Systems.

    Science.gov (United States)

    COMPUTERS, *BIBLIOGRAPHIES, *ONLINE SYSTEMS, * INFORMATION SCIENCES , DATA PROCESSING, DATA MANAGEMENT, COMPUTER PROGRAMMING, INFORMATION RETRIEVAL, COMPUTER GRAPHICS, DIGITAL COMPUTERS, ANALOG COMPUTERS.

  2. State-of-the-art steam generator on-line chemistry monitoring system

    Energy Technology Data Exchange (ETDEWEB)

    Mac Koul, L.J.; Mc Clendon, M.E.; Richards, J.E.; Wozniak, S.M.

    1986-04-01

    Recent understanding of corrosion mechanisms has changed the industry's approach to one of establishing and maintaining proper water chemistry conditions to increase steam generator life and availability. A rigorous sampling and analysis program, along with management's commitment to proper water chemistry, are integral to the success of this approach. This paper describes Virginia Power's recent commitment to better maintenance of secondary side water chemistry conditions at its nuclear power stations through an on-line, comprehensive, state-of-the-art chemistry monitoring system.

  3. Utilization of on-line corrosion monitoring in the flue gas cleaning system

    DEFF Research Database (Denmark)

    Montgomery, Melanie; Nielsen, Lars V.; Petersen, Michael B.

    2015-01-01

    such as HCl, KCl or chlorine containing corrosion products. Without knowing when corrosion occurs, it is difficult to take reasonable measures to reduce corrosion. In order to gain an improved understanding of the corrosion problem, an on-line corrosion measurement system was established before the booster....... A root cause analysis concluded that corrosion occurred due to corrosion products/deposit formed during operation; however it was unclear whether the majority of corrosion occurred during operation or downtime. In both cases the chlorine content in the flue gas results in the presence of chlorine species...

  4. Theory analysis and experimental research on on-line contamination detecting technology in hydraulic oil

    Institute of Scientific and Technical Information of China (English)

    YAO Cheng-yu; ZHAO Jing-yi; ZHANG Qi-sheng

    2006-01-01

    A system of on-line contamination detecting in hydraulic oil based on silting principle is accomplished, where, metal filter membrane as detector, solenoid as active force to propel piston to blotter and gain differential pressure, step motor drives the membrane to filtrate and counter-flush, LabVIEW as detecting software platform, oil's contamination detecting indirectly by gauging differential pressure. Based on theory analysis, accomplished is relation between contamination level and differential pressure, realizing polynomial curve fitting, and calibration experiment. Field experiment is simulated in the condition of experimental laboratory, has credible precision and real-time performance, which can popularize to the field of production.

  5. Overvoltage On-line Monitoring System for 110 kV Substation and Its Waveforms Analysis%110kV变电站过电压在线监测系统及其波形分析

    Institute of Scientific and Technical Information of China (English)

    杜林; 李欣; 司马文霞; 席世友; 杨庆; 袁涛

    2012-01-01

    Overvoltage is one of the main reasons to cause insulation damage and is also the decisive factor to choose insulation coordination for electrical accessory in power system,and overvoltage on-line monitoring system is of great importance for the analysis of origins of overvoltage failures and improvement of the electrical apparatus insulation coordination in the power system.We introduced an overvoltage on-line system monitoring system for 110 kV Xianfeng substation in Chongqing,which was developed successfully based on the divider and high,variable sampling speed data acquisition card.Moreover,we presented key modules of this system,including two low damping capacitance-resistance dividers,a transformer bushing divider,a variable sampling speed system,and a software system,and so on,and then analyzed overvoltage type and its forming causes by running records.The monitoring results can be utilized for transmission lines lightning protection,substation voltage protection,electrical grid layout,and design.%过电压是造成电网绝缘损害的主要原因之一,也是选择电气设备绝缘强度的决定性因素,电力系统过电压在线监测对分析过电压事故原因和改善系统绝缘配合具有重要的现实意义。在研制成功110kV过电压传感器以及高速变频采集系统的基础上,重庆110kV先锋过电压在线监测系统可自动捕获10、35、110kV电网中出现的外部和内部过电压。另外还介绍了该系统的结构、用于过电压信号采集的低阻尼阻容分压器和套管式分压器、变频采集系统及系统软件等关键模块。根据现场采集到的典型过电压波形样本,结合值班室记录,分析了雷电、操作及暂时等过电压的波形特点和产生原因,监测结果可为输电线路防雷、变电站过电压防护、电力系统规划和设计提供科学依据。

  6. Research of 3D On-line Analysis System of Mine Ventilation and Its Application%矿井三维通风在线分析系统的研究与应用

    Institute of Scientific and Technical Information of China (English)

    杨占国

    2011-01-01

    介绍了一种矿井三维通风在线分析系统的实现方案.该系统采用3DGIS数字矿山基础信息平台的企业管理器模块对井下数据进行整理、加工及存储,根据该模块中存储的巷道网路、通风设备以及通风设施等数据自动建立通风网络拓扑关系;结合煤矿安全监测监控系统监测的实时风速数据,利用通风网络解算算法实时监控矿井通风系统运行状况,分析通风异常原因,并采用3DGIS数字矿山基础信息平台的企业应用平台模块将分析结果以三维可视化形式予以展示.该系统在四台矿的应用取得了良好的效果.%The paper introduced an implement scheme of 3D on-line analysis system of mine ventilation. The system uses module of enterprise manager of basic information platform of digital mine based on 3DGIS to arrange, process and store underground data, and creates ventilation network topology automatically according to data of roadway network, ventilation facilities and ventilation equipments of the module. The system can monitor running status of ventilation system on the basis of real-time wind speed data monitored by mine safety monitoring and control system and calculation algorithm of ventilation network, analyze causes of abnormal ventilation, and display analysis results in the form of 3D form by use of module of enterprise application platform of basic information platform of digital mine based on 3DGIS. The application of the system in Sitai Mine achieved a good effect.

  7. On-Line Serials System at Laval University Library

    Directory of Open Access Journals (Sweden)

    Rosario de Varennes

    1970-06-01

    Full Text Available Description of a system, operational since June 1968, that provides control of all serials holdings in nine campus libraries, permits updating of the complete file every two or three days, and produces various outputs for library users and library staff from data in variable fields on disks (listings, statistics, etc.. The program, presently operating on an IBM 360/50 and utilizing an IBM 2314 disk-storage facility and three IBM 226 CRT terminals, is written in IBM System/360 Operating System Assembler Language and in PL/I; it could encompass a file of no more than 10 million records of variable length limited to 127/255 characters and subdivided in 25 or fewer fields.

  8. An automated on-line multidimensional HPLC system for protein and peptide mapping with integrated sample preparation

    NARCIS (Netherlands)

    Wagner, K.; Miliotis, T.; Marko-Varga, G; Bischoff, Rainer; Unger, K.K.

    2002-01-01

    A comprehensive on-line two-dimensional 2D-HPLC system with integrated sample preparation was developed for the analysis of proteins and peptides with a molecular weight below 20 kDa. The system setup provided fast separations and high resolving power and is considered to be a complementary techniqu

  9. On-line corrosion monitoring in geothermal district heating systems

    DEFF Research Database (Denmark)

    Richter, S.; Hilbert, Lisbeth Rischel; Thorarinsdottir, R.I.

    2006-01-01

    General corrosion rates in the geothermal district heating systems in Iceland are generally low, of the magnitude 1 lm/y. The reason is high pH (9.5), low-conductivity (200 lm/y) and negligible dissolved oxygen. The geothermal hot water is either used directly from source or to heat up cold ground...

  10. An on-line gasoline blending system put into production

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    @@ Anew system for online gasoline blending, which was developed by researchers from the CAS Institute of Automation (CASIA), has been put into production at China Petrochemical Corporation (SINOPEC) and PetroChina Corporation. It is expected to thoroughly renovate the technology in this regard and achieve maximal economic benefits in oil production stage.

  11. On-line Corrosion Monitoring in District Heating Systems

    DEFF Research Database (Denmark)

    Richter, Sonja; Thorarinsdottir, R.I.; Hilbert, Lisbeth Rischel

    2005-01-01

    The corrosion control in district heating systems is today performed primarily with control of the water quality. The corrosion rate is kept low by assuring low dissolved oxygen concentration, high pH and low conductivity. Corrosion failures can occur, e.g. as a result of unknown oxygen ingress...

  12. Planning an Integrated On-Line Library system (IOLS)

    Science.gov (United States)

    1989-03-01

    Information Technolo2gy and the Academi11c Librarv," Library Journal 109 (June 1. 1984):1204-1209. 15. Karen L. l-orniv, "Fifteen Years of Automation...Richard. "Integrated Online Library Systems: Perspectives, Percep- tions, & Practicalities." Library Journal 110 (February 1, 1985):37-40. De Gennaro...Richard. "Library Automation & Networking Perspectives on Three Decades." Library Journal 108 (1 April 1983):629-35. De Gennaro, Richard. "Shifting

  13. Multiple-function multi-input/multi-output digital control and on-line analysis

    Science.gov (United States)

    Hoadley, Sherwood T.; Wieseman, Carol D.; Mcgraw, Sandra M.

    1992-01-01

    The design and capabilities of two digital controller systems for aeroelastic wind-tunnel models are described. The first allowed control of flutter while performing roll maneuvers with wing load control as well as coordinating the acquisition, storage, and transfer of data for on-line analysis. This system, which employs several digital signal multi-processor (DSP) boards programmed in high-level software languages, is housed in a SUN Workstation environment. A second DCS provides a measure of wind-tunnel safety by functioning as a trip system during testing in the case of high model dynamic response or in case the first DCS fails. The second DCS uses National Instruments LabVIEW Software and Hardware within a Macintosh environment.

  14. Grid Environment for On-line Application Monitoring and Performance Analysis

    Directory of Open Access Journals (Sweden)

    Bartosz Baliś

    2004-01-01

    Full Text Available This paper presents an application monitoring infrastructure developed within the CrossGrid project. The software is aimed at enabling performance measurements for the application developer and in this way facilitating the development of applications in the Grid environment. The application monitoring infrastructure is composed of a distributed monitoring system, the OCM-G, and a performance analysis tool called G-PM. The OCM-G is an on-line, grid-enabled, monitoring system, while G-PM is an advanced graphical tool which allows to evaluate and present the results of performance monitoring, to support optimization of the application execution. G-PM supports build-in standard metrics and user-defined metrics expressed in the Performance Measurement Specification Language (PMSL. Communication between the G-PM and the OCM-G is performed according to a well-defined protocol, OMIS (On-line Monitoring Interface Specification. In this paper, the architecture and features of the OCM-G and G-PM are described as well as an example of use of the monitoring infrastructure to visualize the status and communication in the application, to evaluate the performance, including discovering the reason of the performance flaw.

  15. Research of PD on-line Monitoring System for DC Cable

    Directory of Open Access Journals (Sweden)

    Duan Da-Peng

    2014-01-01

    Full Text Available In order to monitor the insulation of XLPE cable of rail system, an On-line Partial Discharge (PD Monitoring System applied for 1500V DC cables of Shanghai Traction Substation is described, including its hardware and software structure. After installed, this system successfully detected one PD signal. The results demonstrated that this system worked stably and reliably.

  16. Metabolism analysis and on-line physiological state diagnosis of acetone-butanol fermentation

    Energy Technology Data Exchange (ETDEWEB)

    Chauvatcharin, S.; Seki, Tatsuji; Takagi, Mutsumi; Yoshida, Toshiomi [Osaka Univ., Suita, Osaka (Japan). International Center of Cooperative Research in Biotechnology; Siripatana, C. [Prince of Songkla Univ., Bangkok (Thailand). Dept. of Industrial Biotechnology

    1998-06-20

    Fermentation equations for acetone-butanol (AB) were applied in a metabolic analysis of the reaction network under various conditions; that is, at different pHs and a high NADH{sub 2} turnover rate using methyl viologen, in a Clostridium acetobutylicum culture. The results disclosed variations in the pattern of rate changes that reflected changes in the physiological state. A liner relationship was found to exist between NADH{sub 2} generation and butanol production rate. By coupling an automated measurement system with the fermentation model, on-line estimation of the culture state was accomplished. Based on the AB fermentation model, new parameters were defined for on-line diagnosis of the physiological state and determination of the best timing for amplifying NADH{sub 2} generation by the addition of methyl viologen to obtain a high level of butanol productivity. A potential means of achieving optimal control for a high level of solvent production, involving the correlation of certain rates, is proposed.

  17. Development of the Defense Documentation Center Remote On-Line Retrieval System - Past, Present and Future.

    Science.gov (United States)

    Bennertz, Richard K.

    The document highlights in nontechnical language the development of the Defense Documentation Center (DDC) Remote On-Line Retrieval System from its inception in 1967 to what is planned. It describes in detail the current operating system, equipment configuration and associated costs, user training and system evaluation and may be of value to other…

  18. The design and implementation of on-line monitoring system for UHV compact shunt capacitors

    Science.gov (United States)

    Tao, Weiliang; Ni, Xuefeng; Lin, Hao; Jiang, Shengbao

    2017-08-01

    Because of the large capacity and compact structure of the UHV compact shunt capacitor, it is difficult to take effective measures to detect and prevent the faults. If the fault capacitor fails to take timely maintenance, it will pose a threat to the safe operation of the system and the life safety of the maintenance personnel. The development of UHV compact shunt capacitor on-line monitoring system can detect and record the on-line operation information of UHV compact shunt capacitors, analyze and evaluate the early fault warning signs, find out the fault capacitor or the capacitor with fault symptom, to ensure safe and reliable operation of the system.

  19. On-line identification of hybrid systems using an adaptive growing and pruning RBF neural network

    DEFF Research Database (Denmark)

    Alizadeh, Tohid

    2008-01-01

    This paper introduces an adaptive growing and pruning radial basis function (GAP-RBF) neural network for on-line identification of hybrid systems. The main idea is to identify a global nonlinear model that can predict the continuous outputs of hybrid systems. In the proposed approach, GAP......-RBF neural network uses a modified unscented kalman filter (UKF) with forgetting factor scheme as the required on-line learning algorithm. The effectiveness of the resulting identification approach is tested and evaluated on a simulated benchmark hybrid system....

  20. On-Line Retrieval System Design; Part V of Scientific Report No. ISR-18, Information Storage and Retrieval...

    Science.gov (United States)

    Cornell Univ., Ithaca, NY. Dept. of Computer Science.

    On-line retrieval system design is discussed in the two papers which make up Part Five of this report on Salton's Magical Automatic Retriever of Texts (SMART) project report. The first paper: "A Prototype On-Line Document Retrieval System" by D. Williamson and R. Williamson outlines a design for a SMART on-line document retrieval system…

  1. Study of on-line analysis using energy dispersive X-ray fluorescence spectrometry for controlling lanthanum and neodymium extraction

    Energy Technology Data Exchange (ETDEWEB)

    Wenli, Li; Ascenzo, G.D`; Curini, R. [Department of Chemistry, University of Rome `La Sapienza`, Rome (Italy); Gasparini, G.M.; Casarci, M.; Mattia, B.; Traverso, D.M.; Bellisario, F. [ENEA, CRE Casaccia INN-NUMA (Italy)

    1998-05-04

    Many rare-earth extraction processes require frequent control over separation process quality. Ideally, an analysis method for this type should be simple, rapid and reliable. Energy dispersive X-ray fluorescence (EDXRF) spectrometry, due to its relative simplicity of instrumentation, speed of analysis, and non-destructive nature, is well suited to this on-line analysis application. In particular, since the radioisotope energy dispersive XRF method eliminates the need to transport samples to a laboratory which houses the X-ray spectrometry, it is most commonly used for on-line analysis of extraction systems. The present paper describes an attempt to type the radioisotope source {sup 241}Am XRF on-line analysis arrangement coupled with a personal computer for controlling a lanthanum and neodymium separation process. From the HpGe detector (high-purity germanium) response, a continuous spectral signal is observed during loading of the feed samples. The separation process using countercurrent extraction consists of a 16-stage laboratory mixer-settler, a switching valve, and a pumping system. The performance of this control system is illustrated by extracting La, Nd acidic solutions with 100% tributyl phosphate

  2. Chemiluminescence determination of cefotaxime sodium with flow-injection analysis of cerium (IV)-rhodamine 6G system and its application to the binding study of cefotaxime sodium to protein with on-line microdialysis sampling

    Science.gov (United States)

    Chen, Dinglong; Wang, Huiying; Zhang, Zhujun; Ci, Lijie; Zhang, Xuehong

    2011-01-01

    A simple, sensitive and rapid flow-injection chemiluminescence (CL) method has been developed for the determination of cefotaxime sodium based on the chemiluminescence reaction of cefotaxime sodium with ceric sulfate and rhodamine 6G in nitric acid solution. The concentration of cefotaxime sodium was proportional with the CL intensity in the range of 4 × 10 -8 - 8 × 10 -6 mol L -1. The detection limit (signal-to-noise ratio = 3) was 1 × 10 -8 mol L -1. Coupled to the technique of on-line microdialysis sampling, this method was successfully applied to study cefotaxime sodium-protein interaction. The drug and protein were mixed in different molar ratios in Ringer's solution, pH 7.4, and incubated at 37 °C in a water bath. The microdialysis probe was utilized to sample the mixed solution at a perfusion rate of 5 μL min -1 and the recovery of cefotaxime sodium under experimental condition was 16.2%. The data obtained by the present Microdialysis-Flow Injection Analysis-CL method was analyzed with the Scatchard analysis and Klotz plot. The estimated association constant ( K) and the number of the binding sites ( n) on one of BSA molecule were 5.94 × 10 4 M -1 and 1.29 (Klotz equation), respectively.

  3. A Phenomenological Study of Gifted Adolescents and Their Engagement with One On-Line Learning System

    Science.gov (United States)

    Swicord, Barbara

    2010-01-01

    Little research exists on the nature of the interactions between gifted students and the use of technology. Furthermore, no research has investigated the phenomenon of gifted adolescents using one internet-based program, the Renzulli Learning System (RLS). Renzulli Learning is an on-line educational profile with a matching database that provides…

  4. Assessment of corrosion in the flue gas cleaning system using on-line monitoring

    DEFF Research Database (Denmark)

    Montgomery, Melanie; Vendelbo Nielsen, Lars; Berggreen Petersen, Michael

    2015-01-01

    products/deposits were detected. An on-line corrosion measurement system was established to determine corrosion mechanisms. It was revealed that many shutdowns/start-ups of the plant influence corrosion and result in decreased lifetime of components and increased maintenance. The change of fuel from...

  5. Modern on-line control system for refuse-fueled power plants. Moderne Leittechnik fuer Muellverbrennungsanlage

    Energy Technology Data Exchange (ETDEWEB)

    Grasmueck, L. (Asea Brown Boveri AG, Mannheim (Germany, F.R.)); Klitzke, H.J. (Goepfert und Reimer und Partner, Beratende Ingenieure, Hamburg (Germany, F.R.)); Schumacher, E. (Technische Werke Ludwigshafen am Rhein AG (Germany, F.R.))

    1989-10-01

    30 years after commissioning a refuse-fueled power plant in Ludwigshafen was retrofitted and extended. A process control system provides an optimal waste combustion and flue gas cleanup. An on-line central strategy, special requirements on waste combustion and solutions are presented in this report. (orig.).

  6. Antioxidants in Raspberry: On-line analysis links antioxidant activity to a diversity of individual metabolites

    NARCIS (Netherlands)

    Beekwilder, M.J.; Jonker, H.H.; Hall, R.D.; Meer, van der I.M.; Vos, de C.H.

    2005-01-01

    The presence of antioxidant compounds can be considered as a quality parameter for edible fruit. In this paper, we studied the antioxidant compounds in raspberry (Rubus idaeus) fruits by high-performance liquid chromatography (HPLC) coupled to an on-line postcolumn antioxidant detection system. Both

  7. Development of an on-line froth vision system for control of coal flotation

    Energy Technology Data Exchange (ETDEWEB)

    Nguyen, K.K.; Holtham, P.N.; Brake, I.R. [University of Queensland, Brisbane, Qld. (Australia). Julius Kruttschnitt Mineral Research Centre

    1998-12-31

    Flotation is one of the important processes used to recover minus 0.5 mm coal, but the automatic control of flotation has always been difficult due to a lack of suitable process instrumentation. While cell levels can be readily measured, and feed and tailings pulps can be assayed for ash level and solids concentration using on-stream analysers, these measurements alone are not generally sufficient for effective process control. Visual inspection of froth conditions by the flotation operator can provide additional data, and experienced operators are able to make process adjustments based on examination of froth characteristics such as average bubble size and froth mobility. At present, instrumentation to evaluate the appearance of the froth is not available, and hence this aspect of flotation plant operation is still manually controlled. This paper presents the results from the development of an industrial video-based pattern recognition system for image analysis of flotation froth. The system has been applied to one of the sixteen 3 m diameter Microcel flotation columns at Peak Downs coal preparation plant in central Queensland. Results from the system to date show that it can successfully identify froth type and estimate average bubble size and froth speed. The machine vision system currently developed provides sufficient processing power to support minute by minute updates of these froth characteristics as well as a live video output to the screen. On-line predictions of percent ash and solids in the froth are well correlated with those obtained by laboratory analysis. The system is currently being linked to the Peak Downs plant PLC to allow a trial of closed loop control of flotation. 5 refs., 7 figs.

  8. On Line Service Composition in the Integrated Clinical Environment for eHealth and Medical Systems.

    Science.gov (United States)

    García-Valls, Marisol; Touahria, Imad Eddine

    2017-06-08

    Medical and eHealth systems are progressively realized in the context of standardized architectures that support safety and ease the integration of the heterogeneous (and often proprietary) medical devices and sensors. The Integrated Clinical Environment (ICE) architecture appeared recently with the goal of becoming a common framework for defining the structure of the medical applications as concerns the safe integration of medical devices and sensors. ICE is simply a high level architecture that defines the functional blocks that should be part of a medical system to support interoperability. As a result, the underlying communication backbone is broadly undefined as concerns the enabling software technology (including the middleware) and associated algorithms that meet the ICE requirements of the flexible integration of medical devices and services. Supporting the on line composition of services in a medical system is also not part of ICE; however, supporting this behavior would enable flexible orchestration of functions (e.g., addition and/or removal of services and medical equipment) on the fly. iLandis one of the few software technologies that supports on line service composition and reconfiguration, ensuring time-bounded transitions across different service orchestrations; it supports the design, deployment and on line reconfiguration of applications, which this paper applies to service-based eHealth domains. This paper designs the integration between ICE architecture and iLand middleware to enhance the capabilities of ICE with on line service composition and the time-bounded reconfiguration of medical systems based on distributed services. A prototype implementation of a service-based eHealth system for the remote monitoring of patients is described; it validates the enhanced capacity of ICE to support dynamic reconfiguration of the application services. Results show that the temporal cost of the on line reconfiguration of the eHealth application is bounded

  9. A new on-line leakage current monitoring system of ZnO surge arresters

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Bok-Hee [Research Center for Next-Generation High Voltage and Power Technology, Inha University, 253 Yonghyun-dong, Nam-ku, Incheon 402-751 (Korea, Republic of)]. E-mail: bhlee@inha.ac.kr; Kang, Sung-Man [Research Center for Next-Generation High Voltage and Power Technology, Inha University, 253 Yonghyun-dong, Nam-ku, Incheon 402-751 (Korea, Republic of)

    2005-05-15

    This paper presents a new on-line leakage current monitoring system of zinc oxide (ZnO) surge arresters. To effectively diagnose the deterioration of ZnO surge arresters, a new algorithm and on-line leakage current detection device, which uses the time-delay addition method, for discriminating the resistive and capacitive currents was developed to use in the aging test and durability evaluation for ZnO arrester blocks. A computer-based measurement system of the resistive leakage current, the on-line monitoring device can detect accurately the leakage currents flowing through ZnO surge arresters for power frequency ac applied voltages. The proposed on-line leakage current monitoring device of ZnO surge arresters is more highly sensitive and gives more linear response than the existing devices using the detection method of the third harmonic leakage currents. Therefore, the proposed leakage current monitoring device can be useful for predicting the defects and performance deterioration of ZnO surge arresters in power system applications.

  10. On-Line Partial Discharge Monitoring and Diagnostic System for Power Transformer

    Institute of Scientific and Technical Information of China (English)

    LIN Du; JIANG Lei; LI Fuqi; ZHU Deheng; TAN Kexiong; WU Chengqi; JIN Xianhe; WANG Changchang; CHENG T. C.

    2005-01-01

    This paper introduces a computerized on-line partial discharge (PD) monitoring and diagnostic system for transformers. The system, which is already in use in a power station, uses wide-band active transducers and a data acquisition unit with modularized and exchangeable components. The system software is a power equipment monitoring and diagnostic system, which is based on the component object model, and was developed for monitoring multiple parameters in multiple power supply systems. The statistical characteristics of PDs in power transformers were studied using 7 experimental models for simulating PDs in transformers and 3 models for simulating interfering discharges in air. The discharge features were analyzed using a 3-D pattern chart with a three-layer back-propagation artificial neural network used to recognize the patterns. The results show that PDs in air and oil can be distinguished. The model can be used for interference rejection on-line monitoring of partial discharge in transformers.

  11. On-line comprehensive two-dimensional HepG2 cell membrane chromatographic analysis system for charactering anti-hepatoma components from rat serum after oral administration of Radix scutellariae: A strategy for rapid screening active compounds in vivo.

    Science.gov (United States)

    Jia, Dan; Chen, Xiaofei; Cao, Yan; Wu, Xunxun; Ding, Xuan; Zhang, Hai; Zhang, Chuan; Chai, Yifeng; Zhu, Zhenyu

    2016-01-25

    Cell membrane chromatography (CMC) is a bioaffinity chromatography technique for characterizing interactions between drugs and membrane receptors and has been widely used to screen active components from complex samples such as herbal medicines (HMs). However, it has never been applied in vivo due to its relatively high limit of detection (LOD) and the matrix interferences. In this study, a novel on-line comprehensive two-dimensional HepG2/CMC/enrich columns/high performance liquid chromatography/time-of-flight mass spectrometry system was developed to rapidly screen potential anti-hepatoma components from drug-containing serum of rats after oral administration of Radix scutellariae. A matrix interference deduction method with a home-written program in MATLAB was developed, which could successfully eliminate the interference of endogenous substances in serum. Baicalein, wogonin, chrysin, oroxylin A, neobaicalein and rivularin from Radix scutellariae extraction were significantly retained in the HepG2/CMC column. Three potential active components, wogonin, oroxylin A and neobaicalein were firstly screened from the drug-containing serum as well. The cell counting kit-8 assay demonstrated that wogonin, oroxylin A and chrysin showed high inhibitory activities in a dose-dependent manner on HepG2 cells at the concentration of 12.5-200 μM (pactive components from complex biological samples and could be applied to other biochromatography models.

  12. First Field Experience of On-line Partial Discharge Monitoring of MV Cable Systems with location

    Energy Technology Data Exchange (ETDEWEB)

    Van der Wielen, P.; Steennis, F.

    2009-06-15

    A new measuring system is presented for the on-line monitoring and location of partial discharges (PDs) in medium-voltage power cables. The system uses two inductive sensors, each at one cable end. The measuring system is called PD-OL, which stands for PD detection Online with Location. A pulse injection system is used for the time synchronization of the data intake at both cable ends and for the on-line calibration. PD data is send via internet to the KEMA Control Center for interpretation and final presentation, made visible on a secured website for the network owners. This paper discusses the basics of PD-OL and a number of measurement results.

  13. On-line analysis of eye movements using a digital computer.

    Science.gov (United States)

    Baloh, R W; Langhofer, L; Honrubia, V; Yee, R D

    1980-06-01

    We describe a microcomputer system for on-line analysis of eye movement recordings. Quantitative data from the patient and statistical comparison with normative data is available within seconds of test completion. Three types of eye movements are analyzed--voluntary saccades, smooth pursuit, and nystagmus. The first two are induced by a computer-controlled laser dot projected onto a screen and the third by a computer-controlled optokinetic drum, caloric infusion, and rotatory chair. The computer algorithm differentiates the eye position signal to yield an instantaneous eye velocity record. Saccades are identified based on their characteristic velocity profile. For pursuit and nystagmus. The first two are induced by a computer-controlled laser dot projected onto a screen and the third by a computer-controlled optokinetic drum, caloric infusion, and rotatory chair. The computer algorithm differentiates the eye position signal to yield an instaneous eye velocity record. Saccades are identified based on their characteristic velocity profile. For pursuit and nystagmus, the velocity record is modified by linearly interpolating across segments in which saccades occurred. The gain (output eye velocity/input eye velocity) is calculated after Fourier analysis of the data.

  14. An Advisory System for On-line Control of Fed-batch Cultivation of Saccharomyces cerevisiae

    Directory of Open Access Journals (Sweden)

    Ljakova K.

    2008-12-01

    Full Text Available Free software for entering and documenting data EpiData is here used for design of an advisory system for on-line control of a fermentation process. Based on the preliminary developed system for functional state recognition, presented here system will advise the user which new functional state can be reached and what kind of control actions have to be taken. New-designed system appears as an expert system and comprises knowledge of well-trained operators of cultivation processes. Developed advisory system is further applied for a fed-batch cultivation of Saccharomyces cerevisiae.

  15. On-Line Analysis and Kinetic Behavior of Arsenic Release during Coal Combustion and Pyrolysis.

    Science.gov (United States)

    Shen, Fenghua; Liu, Jing; Zhang, Zhen; Dai, Jinxin

    2015-11-17

    The kinetic behavior of arsenic (As) release during coal combustion and pyrolysis in a fluidized bed was investigated by applying an on-line analysis system of trace elements in flue gas. This system, based on inductively coupled plasma optical emission spectroscopy (ICP-OES), was developed to measure trace elements concentrations in flue gas quantitatively and continuously. Obvious variations of arsenic concentration in flue gas were observed during coal combustion and pyrolysis, indicating strong influences of atmosphere and temperature on arsenic release behavior. Kinetic laws governing the arsenic release during coal combustion and pyrolysis were determined based on the results of instantaneous arsenic concentration in flue gas. A second-order kinetic law was determined for arsenic release during coal combustion, and the arsenic release during coal pyrolysis followed a fourth-order kinetic law. The results showed that the arsenic release rate during coal pyrolysis was faster than that during coal combustion. Thermodynamic calculations were carried out to identify the forms of arsenic in vapor and solid phases during coal combustion and pyrolysis, respectively. Ca3(AsO4)2 and Ca(AsO2)2 are the possible species resulting from As-Ca interaction during coal combustion. Ca(AsO2)2 is the most probable species during coal pyrolysis.

  16. The Design of Partial Discharge On-Line Monitoring System for XLPE Power Cable

    OpenAIRE

    Chen Rui-Long; Qian Yong; Ye Hai-Feng; Sheng Ge-Hao; Jiang Xiu-Chen

    2013-01-01

    Partial discharge detection is an important means to assess the situation of XLPE power cable’s insulation. This study has developed an on-line monitoring system which applies to the medium voltage XLPE cable on partial discharge, described its working principle, components of hardware, software designing and program implementation in details. Through monitoring the partial discharge signal in grounding lines of the XLPE cable’s shield, the system integrated assess the situation of XLPE cable...

  17. Advanced mathematical on-line analysis in nuclear experiments. Usage of parallel computing CUDA routines in standard root analysis

    Directory of Open Access Journals (Sweden)

    Grzeszczuk A.

    2015-01-01

    Full Text Available Compute Unified Device Architecture (CUDA is a parallel computing platform developed by Nvidia for increase speed of graphics by usage of parallel mode for processes calculation. The success of this solution has opened technology General-Purpose Graphic Processor Units (GPGPUs for applications not coupled with graphics. The GPGPUs system can be applying as effective tool for reducing huge number of data for pulse shape analysis measures, by on-line recalculation or by very quick system of compression. The simplified structure of CUDA system and model of programming based on example Nvidia GForce GTX580 card are presented by our poster contribution in stand-alone version and as ROOT application.

  18. Configuration Reusing in On-Line Task Scheduling for Reconfigurable Computing Systems

    Institute of Scientific and Technical Information of China (English)

    Maisam Mansub Bassiri; Hadi Shahriar Shahhoseini

    2011-01-01

    Reconfigurable computing systems can be reconfigured at runtime and support partial reconfigurability which makes us able to execute tasks in a true multitasking manner. To manage such systems at runtime, a reconfigurable operating system is needed. The main part of this operating system is resource management unit which performs on-line scheduling and placement of hardware tasks at runtime. Reconfiguration overhead is an important obstacle that limits the performance of on-line scheduling algorithms in reconfigurable computing systems and increases the overall execution time. Configuration reusing (task reusing) can decrease reconfiguration overhead considerably, particularly in periodic applications or the applications in which the probability of tasks recurrence is high. In this paper, we present a technique called reusing-based scheduling (RBS), for on-line scheduling and placement in which configuration reusing is considered as a main characteristic in order to reduce reconfiguration overhead and decrease total execution time of the tasks. Several experiments have been conducted on the proposed algorithm. Obtained results show considerable improvement in overall execution time of the tasks.

  19. A multisyringe flow-through sequential extraction system for on-line monitoring of orthophosphate in soils and sediments

    DEFF Research Database (Denmark)

    Buanuam, Janya; Miró, Manuel; Hansen, Elo Harald

    2007-01-01

    A fully automated flow-through microcolumn fractionation system with on-line post-extraction derivatization is proposed for monitoring of orthophosphate in solid samples of environmental relevance. The system integrates dynamic sequential extraction using 1.0 mol l-1 NH4Cl, 0.1 mol l-1 NaOH and 0.......5 mol l-1 HCl as extractants according to the Hietjles-Lijklema (HL) scheme for fractionation of phosphorus associated with different geological phases, and on-line processing of the extracts via the Molybdenum Blue (MB) reaction by exploiting multisyringe flow injection as the interface between...... the solid containing microcolumn and the flow-through detector. The proposed flow assembly, capitalizing on the features of the multicommutation concept, implies several advantages as compared to fractionation analysis in the batch mode in terms of saving of extractants and MB reagents, shortening...

  20. Small unmanned helicopter's attitude controller by an on-line adaptive fuzzy control system

    Institute of Scientific and Technical Information of China (English)

    GAO Tong-yue; RAO Jin-jun; GONG Zhen-bang; LUO Jun

    2009-01-01

    Since small unmanned helicopter flight attitude control process has strong time-varying characteristics and there are random disturbances, the conventional control methods with unchanged parameters are often unworkable. An on-line adaptive fuzzy control system (AFCS) was designed, in a way that does not depend on a process model of the plant or its approximation in the form of a Jacobian matrix. Neither is it necessary to know the desired response at each instant of time. AFCS implement a simultaneous on-line tuning of fuzzy rules and output scale of fuzzy control system. The two cascade controller design with an inner (attitude controller) and outer controller (navigation controller) of the small unmanned helicopter was proposed. At last, an attitude controller based on AFCS was implemented. The flight experiment showed that the proposed fuzzy logic controller provides quicker response, smaller overshoot, higher precision, robustness and adaptive ability. It satisfies the needs of autonomous flight.

  1. Development of On-Line Monitoring Systems for High Temperature Components in Power Plants

    Directory of Open Access Journals (Sweden)

    Hongcai Zhang

    2013-11-01

    Full Text Available To accurately detect deformation and extend the component life beyond the original design limits, structural safety monitoring techniques have attracted considerable attention in the power and process industries for decades. In this paper an on-line monitoring system for high temperature pipes in a power plant is developed. The extension-based sensing devices are amounted on straight pipes, T-Joints and elbows of a main steam pipeline. During on-site monitoring for more than two years, most of the sensors worked reliably and steadily. However, the direct strain gauge could not work for long periods because of the high temperature environment. Moreover, it is found that the installation and connection of the extensometers can have a significant influence on the measurement results. The on-line monitoring system has a good alarming function which is demonstrated by detecting a steam leakage of the header.

  2. Development of on-line monitoring systems for high temperature components in power plants.

    Science.gov (United States)

    Zhang, Hongcai; Jia, Jiuhong; Wang, Ning; Hu, Xiaoyin; Tu, Shan-Tung; Zhou, Shaoping; Wang, Zhengdong

    2013-11-13

    To accurately detect deformation and extend the component life beyond the original design limits, structural safety monitoring techniques have attracted considerable attention in the power and process industries for decades. In this paper an on-line monitoring system for high temperature pipes in a power plant is developed. The extension-based sensing devices are amounted on straight pipes, T-Joints and elbows of a main steam pipeline. During on-site monitoring for more than two years, most of the sensors worked reliably and steadily. However, the direct strain gauge could not work for long periods because of the high temperature environment. Moreover, it is found that the installation and connection of the extensometers can have a significant influence on the measurement results. The on-line monitoring system has a good alarming function which is demonstrated by detecting a steam leakage of the header.

  3. Robust On-Line Fault Diagnosis for Nonlinear Difference-Algebraic Systems Using Least Squares Estimate

    Institute of Scientific and Technical Information of China (English)

    2002-01-01

    A new robust on-line fault diagnosis method based on least squares estimate for nonlinear difference-algebraic systems (DAS) with uncertainties is proposed. Based on the known nominal model of the DAS, this method firstly constructs an auxiliary system consisting of a difference equation and an algebraic equation, then, based on the relationship between the state deviation and the faults in the difference equation and the relationship between the algebraic variable deviation and the faults in algebraic equation, it identifies the faults on-line through least squares estimate. This method can not only detect, isolate and identify faults for DAS, but also give the upper bound of the error of fault identification. The simulation results indicate that it can give satisfactory diagnostic results for both abrupt and incipient faults.

  4. Development of On-Line Monitoring Systems for High Temperature Components in Power Plants

    Science.gov (United States)

    Zhang, Hongcai; Jia, Jiuhong; Wang, Ning; Hu, Xiaoyin; Tu, Shan-Tung; Zhou, Shaoping; Wang, Zhengdong

    2013-01-01

    To accurately detect deformation and extend the component life beyond the original design limits, structural safety monitoring techniques have attracted considerable attention in the power and process industries for decades. In this paper an on-line monitoring system for high temperature pipes in a power plant is developed. The extension-based sensing devices are amounted on straight pipes, T-Joints and elbows of a main steam pipeline. During on-site monitoring for more than two years, most of the sensors worked reliably and steadily. However, the direct strain gauge could not work for long periods because of the high temperature environment. Moreover, it is found that the installation and connection of the extensometers can have a significant influence on the measurement results. The on-line monitoring system has a good alarming function which is demonstrated by detecting a steam leakage of the header. PMID:24233026

  5. Developing an EEG based On-line Closed-loop Lapse Detection and Mitigation System

    Directory of Open Access Journals (Sweden)

    Yu-Te eWang

    2014-10-01

    Full Text Available In America, sixty percent of adults reported that they have driven a motor vehicle while feeling drowsy, and at least 15-20% of fatal car accidents are fatigue-related. This study translates previous laboratory-oriented neurophysiological research to design, develop, and test an On-line Closed-loop Lapse Detection and Mitigation (OCLDM System featuring a mobile wireless dry-sensor EEG headgear and a cell-phone based real-time EEG processing platform. Eleven subjects participated in an event-related lane-keeping task, in which they were instructed to manipulate a randomly deviated, fixed-speed cruising car on a 4-lane highway. This was simulated in a 1st person view with an 8-screen and 8-projector immersive virtual-realty environment. When the subjects experienced lapses or failed to respond to events during the experiment, auditory feedback was delivered to rectify the performance decrements. However, the arousing auditory signals were not always effective. The EEG spectra exhibited statistically significant differences between effective and ineffective arousing signals, suggesting that EEG spectra could be used as a countermeasure of the efficacy of arousing signals. In this on-line pilot study, the proposed OCLDM System was able to continuously detect EEG signatures of fatigue, deliver arousing feedback to subjects suffering momentary cognitive lapses, and assess the efficacy of the feedback in near real-time to rectify cognitive lapses. The on-line testing results of the OCLDM System validated the efficacy of the arousing signals in improving subjects' response times to the subsequent lane-departure events. This study may lead to a practical on-line lapse detection and mitigation system in real-world environments.

  6. A Discrete Event System approach to On-line Testing of digital circuits with measurement limitation

    Directory of Open Access Journals (Sweden)

    P.K. Biswal

    2016-09-01

    Full Text Available In the present era of complex systems like avionics, industrial processes, electronic circuits, etc., on-the-fly or on-line fault detection is becoming necessary to provide uninterrupted services. Measurement limitation based fault detection schemes are applied to a wide range of systems because sensors cannot be deployed in all the locations from which measurements are required. This paper focuses towards On-Line Testing (OLT of faults in digital electronic circuits under measurement limitation using the theory of discrete event systems. Most of the techniques presented in the literature on OLT of digital circuits have emphasized on keeping the scheme non-intrusive, low area overhead, high fault coverage, low detection latency etc. However, minimizing tap points (i.e., measurement limitation of the circuit under test (CUT by the on-line tester was not considered. Minimizing tap points reduces load on the CUT and this reduces the area overhead of the tester. However, reduction in tap points compromises fault coverage and detection latency. This work studies the effect of minimizing tap points on fault coverage, detection latency and area overhead. Results on ISCAS89 benchmark circuits illustrate that measurement limitation have minimal impact on fault coverage and detection latency but reduces the area overhead of the tester. Further, it was also found that for a given detection latency and fault coverage, area overhead of the proposed scheme is lower compared to other similar schemes reported in the literature.

  7. The Design of Partial Discharge On-Line Monitoring System for XLPE Power Cable

    Directory of Open Access Journals (Sweden)

    Chen Rui-Long

    2013-09-01

    Full Text Available Partial discharge detection is an important means to assess the situation of XLPE power cable’s insulation. This study has developed an on-line monitoring system which applies to the medium voltage XLPE cable on partial discharge, described its working principle, components of hardware, software designing and program implementation in details. Through monitoring the partial discharge signal in grounding lines of the XLPE cable’s shield, the system integrated assess the situation of XLPE cable’s insulation. The results of running show that the system is stable and reliable.

  8. Development of an on-line measuring and monitoring system for fouling based on Delphi

    Science.gov (United States)

    Wang, Yuanyuan; Wang, Jianguo

    2010-12-01

    The presence of fouling reduced the heat transfer capability of heat transfer equipments and increased the flow resistance of the medium. Thus the resulting series of economic losses received worldwide attention of the relevant heat transfer industry and countries. For the heating system fouling, direct measurement is nearly impossible. And it is extremely difficulty of structuring mathematic model. Although there are existing monitoring methods, results are not satisfactory. This paper intends to develop a new on-line measuring and monitoring system for heating system fouling. The operating theory of this on-line measuring and monitoring system is based on the soft-sensor technology and Expert System. We select some easily measurements as primary variables, such as pressures, flow rates and temperatures. Through some algorithms, we obtained dozens of secondary variables, for example, the coefficient of flow resistance, the efficiency and cost of heating system and so on. Based on these variables, we construct the knowledge base of this System. This system mainly uses Delphi and Excel as development tools. Now, the system is running well in some heating station, and has reached the expecting result.

  9. Object-Oriented Control System Design Using On-Line Training of Artificial Neural Networks

    Science.gov (United States)

    Rubaai, Ahmed

    1997-01-01

    This report deals with the object-oriented model development of a neuro-controller design for permanent magnet (PM) dc motor drives. The system under study is described as a collection of interacting objects. Each object module describes the object behaviors, called methods. The characteristics of the object are included in its variables. The knowledge of the object exists within its variables, and the performance is determined by its methods. This structure maps well to the real world objects that comprise the system being modeled. A dynamic learning architecture that possesses the capabilities of simultaneous on-line identification and control is incorporated to enforce constraints on connections and control the dynamics of the motor. The control action is implemented "on-line", in "real time" in such a way that the predicted trajectory follows a specified reference model. A design example of controlling a PM dc motor drive on-line shows the effectiveness of the design tool. This will therefore be very useful in aerospace applications. It is expected to provide an innovative and noval software model for the rocket engine numerical simulator executive.

  10. On-line parameter and delay estimation of continuous-time dynamic systems

    Directory of Open Access Journals (Sweden)

    Kozłowski Janusz

    2015-06-01

    Full Text Available The problem of on-line identification of non-stationary delay systems is considered. The dynamics of supervised industrial processes are usually modeled by ordinary differential equations. Discrete-time mechanizations of continuous-time process models are implemented with the use of dedicated finite-horizon integrating filters. Least-squares and instrumental variable procedures mechanized in recursive forms are applied for simultaneous identification of input delay and spectral parameters of the system models. The performance of the proposed estimation algorithms is verified in an illustrative numerical simulation study.

  11. On-line Batch Process Monitoring and Diagnosing Based on Fisher Discriminant Analysis

    Institute of Scientific and Technical Information of China (English)

    ZHAO Xu; SHAO Hui-he

    2006-01-01

    A new on-line batch process monitoring and diagnosing approach based on Fisher discriminant analysis (FDA) was proposed. This method does not need to predict the future observations of variables, so it is more sensitive to fault detection and stronger implement for monitoring. In order to improve the monitoring performance,the variables trajectories of batch process are separated into several blocks. The key to the proposed approach for on-line monitoring is to calculate the distance of block data that project to low-dimension Fisher space between new batch and reference batch. Comparing the distance with the predefine threshold, it can be considered whether the batch process is normal or abnormal. Fault diagnosis is performed based on the weights in fault direction calculated by FDA. The proposed method was applied to the simulation model of fed-batch penicillin fermentation and the results were compared with those obtained using MPCA. The simulation results clearly show that the on-line monitoring method based on FDA is more efficient than the MPCA.

  12. An integrated on-line irradiation and in situ live cell imaging system

    Science.gov (United States)

    Liang, Ying; Fu, Qibin; Wang, Weikang; Liu, Yu; Liu, Feng; Yang, Gen; Wang, Yugang

    2015-09-01

    Ionizing radiation poses a threat to genome integrity by introducing DNA damages, particularly DNA double-strand breaks (DSB) in cells. Understanding how cells react to DSB and maintain genome integrity is of major importance, since increasing evidences indicate the links of DSB with genome instability and cancer predispositions. However, tracking the dynamics of DNA damages and repair response to ionizing radiation in individual cell is difficult. Here we describe the development of an on-line irradiation and in situ live cell imaging system based on isotopic sources at Institute of Heavy Ion Physics, Peking University. The system was designed to irradiate cells and in situ observe the cellular responses to ionizing radiation in real time. On-line irradiation was achieved by mounting a metal framework that hold an isotopic γ source above the cell culture dish for γ irradiation; or by integrating an isotopic α source to an objective lens under the specialized cell culture dish for α irradiation. Live cell imaging was performed on a confocal microscope with an environmental chamber installed on the microscope stage. Culture conditions in the environment chamber such as CO2, O2 concentration as well as temperature are adjustable, which further extends the capacity of the system and allows more flexible experimental design. We demonstrate the use of this system by tracking the DSB foci formation and disappearance in individual cells after exposure to irradiation. On-line irradiation together with in situ live cell imaging in adjustable culture conditions, the system overall provides a powerful tool for investigation of cellular and subcellular response to ionizing radiation under different physiological conditions such as hyperthermia or hypoxia.

  13. An integrated on-line irradiation and in situ live cell imaging system

    Energy Technology Data Exchange (ETDEWEB)

    Liang, Ying; Fu, Qibin; Wang, Weikang; Liu, Yu; Liu, Feng; Yang, Gen, E-mail: gen.yang@pku.edu.cn; Wang, Yugang

    2015-09-01

    Ionizing radiation poses a threat to genome integrity by introducing DNA damages, particularly DNA double-strand breaks (DSB) in cells. Understanding how cells react to DSB and maintain genome integrity is of major importance, since increasing evidences indicate the links of DSB with genome instability and cancer predispositions. However, tracking the dynamics of DNA damages and repair response to ionizing radiation in individual cell is difficult. Here we describe the development of an on-line irradiation and in situ live cell imaging system based on isotopic sources at Institute of Heavy Ion Physics, Peking University. The system was designed to irradiate cells and in situ observe the cellular responses to ionizing radiation in real time. On-line irradiation was achieved by mounting a metal framework that hold an isotopic γ source above the cell culture dish for γ irradiation; or by integrating an isotopic α source to an objective lens under the specialized cell culture dish for α irradiation. Live cell imaging was performed on a confocal microscope with an environmental chamber installed on the microscope stage. Culture conditions in the environment chamber such as CO{sub 2}, O{sub 2} concentration as well as temperature are adjustable, which further extends the capacity of the system and allows more flexible experimental design. We demonstrate the use of this system by tracking the DSB foci formation and disappearance in individual cells after exposure to irradiation. On-line irradiation together with in situ live cell imaging in adjustable culture conditions, the system overall provides a powerful tool for investigation of cellular and subcellular response to ionizing radiation under different physiological conditions such as hyperthermia or hypoxia.

  14. Simulated 'On-Line' Wear Metal Analysis of Lubricating Oils by X-Ray Fluorescence Spectroscopy

    Science.gov (United States)

    Kelliher, Warren C.; Partos, Richard D.; Nelson, Irina

    1996-01-01

    The objective of this project was to assess the sensitivity of X-ray Fluorescence Spectroscopy (XFS) for quantitative evaluation of metal particle content in engine oil suspensions and the feasibility of real-time, dynamic wear metal analysis. The study was focused on iron as the majority wear metal component. Variable parameters were: particle size, particle concentration and oil velocity. A commercial XFS spectrometer equipped with interchangeable static/dynamic (flow cell) sample chambers was used. XFS spectra were recorded for solutions of Fe-organometallic standard and for a series of DTE oil suspensions of high purity spherical iron particles of 2g, 4g, and 8g diameter, at concentrations from 5 ppm to 5,000 ppm. Real contaminated oil samples from Langley Air Force Base aircraft engines and NASA Langley Research Center wind tunnels were also analyzed. The experimental data conform the reliability of XFS as the analytical method of choice for this project. Intrinsic inadequacies of the instrument for precise analytic work at low metal concentrations were identified as being related to the particular x-ray beam definition, system geometry, and flow-cell materials selection. This work supports a proposal for the design, construction and testing of a conceptually new, miniature XFS spectrometer with superior performance, dedicated to on-line, real-time monitoring of lubricating oils in operating engines. Innovative design solutions include focalization of the incident x-ray beam, non-metal sample chamber, and miniaturization of the overall assembly. The instrument would contribute to prevention of catastrophic engine failures. A proposal for two-year funding has been presented to NASA Langley Research Center Internal Operation Group (IOG) Management, to continue the effort begun by this summer's project.

  15. On-line and off-line data analysis for the EUSO-TA experiment

    Energy Technology Data Exchange (ETDEWEB)

    Piotrowski, Lech Wiktor, E-mail: lech.piotrowski@riken.jp [RIKEN, Wako (Japan); Casolino, Marco [RIKEN, Wako (Japan); INFN and Univ. Rome Tor Vergata, Rome (Italy); Conti, Livio [International Telematic University UNINETTUNO, Rome (Italy); Ebisuzaki, Toshikazu [RIKEN, Wako (Japan); Fornaro, Claudio [International Telematic University UNINETTUNO, Rome (Italy); Kawasaki, Yoshiya; Hachisu, Yusuke; Ohmori, Hitoshi [RIKEN, Wako (Japan); De Santis, Cristian [INFN and Univ. Rome Tor Vergata, Rome (Italy); Shinozaki, Kenji [Institute for Astronomy and Astrophysics, Kepler Center, University of Tübingen, Sand 6, D-72076 Tübingen (Germany); RIKEN, Wako (Japan); Takizawa, Yoshiyuki; Uehara, Yoshihiro [RIKEN, Wako (Japan)

    2015-02-11

    We show the principles of the communication protocol, on-line calibration, off-line data format as well as basic visualisation and data analysis software implemented for the EUSO-TA on-ground experiment, being the first step towards implementation in a future space based mission. EUSO-TA is an on-ground detector for measuring UV (290–430 nm) light from extensive air showers induced by cosmic rays. It is a prototype experiment for the JEM-EUSO space-borne mission, built according to the same constraints of low mass, low power consumption and thus low computing power. Nevertheless, it needs to process a huge amount of data in short time, taking 2.5μs exposures for 2304 channels. The low processing power and high time resolution require an efficient communication protocol and simple yet powerful algorithms for on-line analysis. The off-line data format is designed for storing a huge amount of data, at the same time allowing easy access, analysis and sharing. Its structure is scalable and adjustable to different experimental designs. It is independent of the data origin, whether it is hardware or a Monte-Carlo simulator. Use of object-oriented techniques and the ROOT framework allows rapid development of dedicated analysis software, such as a Python based quick-view program described herein. Basic capabilities of the software, such as display of the focal surface, light curves and calibration data are shown in this paper.

  16. On-line and off-line data analysis for the EUSO-TA experiment

    Science.gov (United States)

    Piotrowski, Lech Wiktor; Casolino, Marco; Conti, Livio; Ebisuzaki, Toshikazu; Fornaro, Claudio; Kawasaki, Yoshiya; Hachisu, Yusuke; Ohmori, Hitoshi; De Santis, Cristian; Shinozaki, Kenji; Takizawa, Yoshiyuki; Uehara, Yoshihiro

    2015-02-01

    We show the principles of the communication protocol, on-line calibration, off-line data format as well as basic visualisation and data analysis software implemented for the EUSO-TA on-ground experiment, being the first step towards implementation in a future space based mission. EUSO-TA is an on-ground detector for measuring UV (290-430 nm) light from extensive air showers induced by cosmic rays. It is a prototype experiment for the JEM-EUSO space-borne mission, built according to the same constraints of low mass, low power consumption and thus low computing power. Nevertheless, it needs to process a huge amount of data in short time, taking 2.5 μs exposures for 2304 channels. The low processing power and high time resolution require an efficient communication protocol and simple yet powerful algorithms for on-line analysis. The off-line data format is designed for storing a huge amount of data, at the same time allowing easy access, analysis and sharing. Its structure is scalable and adjustable to different experimental designs. It is independent of the data origin, whether it is hardware or a Monte-Carlo simulator. Use of object-oriented techniques and the ROOT framework allows rapid development of dedicated analysis software, such as a Python based quick-view program described herein. Basic capabilities of the software, such as display of the focal surface, light curves and calibration data are shown in this paper.

  17. On-line welding quality inspection system for steel pipe based on machine vision

    Science.gov (United States)

    Yang, Yang

    2017-05-01

    In recent years, high frequency welding has been widely used in production because of its advantages of simplicity, reliability and high quality. In the production process, how to effectively control the weld penetration welding, ensure full penetration, weld uniform, so as to ensure the welding quality is to solve the problem of the present stage, it is an important research field in the field of welding technology. In this paper, based on the study of some methods of welding inspection, a set of on-line welding quality inspection system based on machine vision is designed.

  18. On-line corrosion monitoring in geothermal district heating systems. I. General corrosion rates

    DEFF Research Database (Denmark)

    Richter, S.; Hilbert, Lisbeth Rischel; Thorarinsdottir, R.I.

    2006-01-01

    General corrosion rates in the geothermal district heating systems in Iceland are generally low, of the magnitude 1 mu m/y. The reason is high pH (9.5), low-conductivity (200 mu m/y) and negligible dissolved oxygen. The geothermal hot water is either used directly from source or to heat up cold...... ground water. The fluid naturally contains sulphide, which helps keeping the fluid oxygen-free but complicates the electrochemical environment. In this research on-line techniques for corrosion monitoring were tested and evaluated in this medium. Electrochemical methods worked well as long as frequency...

  19. On-line monitoring system of lactic acid fermentation by using integrated enzyme sons ors; Shusekika koso sensa wo mochiita nyusan hakko keisokuyo onrain monitaringu shisutemu

    Energy Technology Data Exchange (ETDEWEB)

    Suzuki, Masayasu; Kumagi, Takeshi; Nakashima, Yuuichi [Kyushu University, Fukuoka (Japan). Dept. of Biochemical Engineering and Science

    1999-03-10

    An on-line monitoring system for lactic acid fermentation is developed by using integrated micro enzyme sensors, a flow injection analysis system, and a micro dialysis system. The calibration curves of micro glucose, lactose and lactate sensors show good linearity in the concentration range below 70 mM. By combination with the micro dialysis system, the enzyme sensors can measure the whole concentration range of lactic acid fermentation, and interference by the medium can not be observed. The on-line sensor system is then applied to lactic acid fermentation of Lactobacillus delbrueckii. The sensor system can monitor the glucose and lactate concentrations simultaneously during 24-h fermentation, and the measurements show good agreement with those of the conventional colorimetric method. The sensor system can also be applied to on-line monitoring of lactose and lactate during Lactobacillus lactis fermentation. (author)

  20. Control and monitoring of on-line trigger algorithms using a SCADA system

    CERN Document Server

    van Herwijnen, E; Barczyk, A; Damodaran, B; Frank, M; Gaidioz, B; Gaspar, C; Jacobsson, R; Jost, B; Neufeld, N; Bonifazi, F; Callot, O; Lopes, H

    2006-01-01

    LHCb [1] has an integrated Experiment Control System (ECS) [2], based on the commercial SCADA system PVSS [3]. The novelty of this approach is that, in addition to the usual control and monitoring of experimental equipment, it provides control and monitoring for software processes, namely the on-line trigger algorithms. Algorithms based on Gaudi [4] (the LHCb software framework) compute the trigger decisions on an event filter farm of around 2000 PCs. Gaucho [5], the GAUdi Component Helping Online, was developed to allow the control and monitoring of Gaudi algorithms. Using Gaucho, algorithms can be monitored from the run control system provided by the ECS. To achieve this, Gaucho implements a hierarchical control system using Finite State Machines. In this article we describe the Gaucho architecture, the experience of monitoring a large number of software processes and some requirements for future extensions.

  1. Quality control and patient dosimetry in digital radiology. On line system: new features and transportability.

    Science.gov (United States)

    Vano, E; Ten, J I; Fernandez, J M; Prieto, C; Ordiales, J M; Martinez, D

    2008-01-01

    New features have been added to a system (QCONLINE) for auditing patient dosimetric and technical parameters 'on line', working on a digital radiology department and using the information contained in the DICOM header of some modalities. The audit of other parameters than patient doses have been included, setting alarm conditions to alert on malfunction of the X-ray system or bad operation modes, in addition to the evaluation of patient doses. A new module to analyse, collect and process the relevant information transferred by the modality performed procedure step (MPPS) service has been launched. Several examples with the exploitation of the new features are presented. The transportability of the system has been tested in two remote hospitals during several months. The new MPPS module has demonstrated to be a good tool to complement the information existing in the DICOM header. The system allows to help in the optimisation of digital radiology departments managing patient dosimetry and procedure data in real time.

  2. On-line topical importance estimation: an effective focused crawling algorithm combining link and content analysis

    Institute of Scientific and Technical Information of China (English)

    Can WANG; Zi-yu GUAN; Chun CHEN; Jia-jun BU; Jun-feng WANG; Huai-zhong LIN

    2009-01-01

    Focused crawling is an important technique for topical resource discovery on the Web. The key issue in focusedcrawling is to prioritize uncrawled uniform resource locators (URLs) in the frontier to focus the crawling on relevant pages.Traditional focused crawlers mainly rely on content analysis. Link-based techniques are not effectively exploited despite their usefulness. In this paper, we propose a new frontier prioritizing algorithm, namely the on-line topical importance estimation (OTIE) algorithm. OTIE combines link-and content-based analysis to evaluate the priority of an uncrawled URL in the frontier. We performed real crawling experiments over 30 topics selected from the Open Directory Project (ODP) and compared harvest rate and target recall of the four crawling algorithms: breadth-first, link-context-prediction, on-line page importance computation (OPlC) and our OTIE. Experimental results showed that OTIE significantly outperforms the other three algorithms on the average target recall while maintaining an acceptable harvest rate. Moreover, OTIE is much faster than the traditional focused crawling algorithm.

  3. Comparison of quarter-hourly on-line dynamic headspace analysis to purge-and-trap analysis of varying volatile organic compounds in drinking water sources.

    Science.gov (United States)

    Schnable, J G; Dussert, B; Suffet, I H; Hertz, C D

    1990-07-27

    On-line dynamic headspace analysis was refined for the quarter-hourly monitoring of select volatile organic compounds (VOCs) in ground and surface waters, for extended periods of time. Hourly comparisons were made to on-line purge-and-trap analysis, and to purge-and-trap analysis after sample preservation and storage. Variations in VOC concentrations of 6047% biweekly, 222% daily, 97% hourly, and 35% quarter-hourly were observable, with the 15-min cycle of the dynamic headspace analysis. The headspace analyzer had superior retention time stability, required less maintenance, and had 1/4 the analysis time as a typical purge-and-trap-gas chromatograph system used for hourly comparisons.

  4. On-Line Model-Based System For Nuclear Plant Monitoring

    Science.gov (United States)

    Tsoukalas, Lefteri H.; Lee, G. W.; Ragheb, Magdi; McDonough, T.; Niziolek, F.; Parker, M.

    1989-03-01

    A prototypical on-line model-based system, LASALLE1, developed at the University of Illinois in collaboration with the Illinois Department of Nuclear Safety (IDNS) is described. Its main purpose is to interpret about 300 signals, updated every two minutes at IDNS from the LaSalle Nuclear Power Plant, and to diagnose possible abnormal conditions. It is written in VAX/VMS OPS5 and operates on both the on-line and testing modes. In its knowledge base, operator and plant actions pertaining to the Emergency Operating Procedure(EOP) A-01, are encoded. This is a procedure driven by a reactor's coolant level and pressure signals; with the purpose of shutting down the reactor, maintaining adequate core cooling and reducing the reactor pressure and temperature to cold shutdown conditions ( about 90 to 200 °F). The monitoring of the procedure is performed from the perspective of Emergency Preparedness. Two major issues are addressed in this system. First, the management of the short-term or working memory of the system. LASALLE1 must reach its inferences, display its conclusion and update a message file every two minutes before a new set of data arrives from the plant. This was achieved by superimposing additional layers of control over the inferencing strategies inherent in OPS5, and developing special rules for the management of the used or outdated information. The second issue is the representation of information and its uncertainty. The concepts of information granularity and performance-level, which are based on a coupling of Probability Theory and the theory of Fuzzy Sets, are used for this purpose. The estimation of the performance-level incorporates a mathematical methodology which accounts for two types of uncertainty encountered in monitoring physical systems: Random uncertainty, in the form of of probability density functions generated by observations, measurements and sensors data and fuzzy uncertainty represented by membership functions based on symbolic

  5. 利用 PGNAA 系统对铝土矿石进行在线检测的可行性研究%Feasibility study for on-line analysis of bauxite using a PGNAA system

    Institute of Scientific and Technical Information of China (English)

    宋青锋; 龚亚林; 张伟; 赵龙; 尚庆敏; 谢福生

    2015-01-01

    利用一款基于瞬发γ中子活化原理设计的主要针对皮带散状物料元素进行在线检测的工业仪器,研究这款仪器用于测量铝土矿组成分析的可行性,实验主要进行了两组样品中 Ca、Si、Al、Fe、Ti 五种元素的测试,其中一组样品由高纯氧化物组成,一组样品由铝土矿和高纯氧化物组成,测量结果表明, CaO、SiO2、Al2 O3、Fe2 O3、TiO2的测量精度分别为±0.23%、±0.18%、±0.35%、±0.14%、±0.08%,能够满足原料自动配比及入厂原料质量控制的要求。%An industrial prompt-gamma neutron activation analysis(PGNAA)system,designed for the real-time elemental analysis of bulk materiel on a conveyor belt,has been studied to examine the feasibility of using such a system for bauxite composition analysis.Experiments were conducted to measure Ca Si Fe Al in two simple,one simple is comprised of pure oxide,and the other simple is comprised of bauxite and pure oxide.The static accuracy are ± 0.23% (CaO),± 0.18% (SiO2 ),± 0.35% (Al2 O3 ),± 0.14% (Fe2 O3 ), ±0.08%(TiO2 ).The instrument can meet the requirements of automatic mixing system of row material and quality controlling after entering factory.

  6. On line automated system for the determination of Sb(V), Sb(III), thrimethyl antimony(v) and total antimony in soil employing multisyringe flow injection analysis coupled to HG-AFS.

    Science.gov (United States)

    Silva Junior, Mario M; Portugal, Lindomar A; Serra, Antonio M; Ferrer, Laura; Cerdà, Victor; Ferreira, Sergio L C

    2017-04-01

    This paper proposes the use of a multisyringe flow injection analysis (MSFIA) system for inorganic antimony speciation analysis, trimethyl antimony(V) and determination of total antimony in soil samples using hydride generation atomic fluorescence spectrometry (HG-AFS). Total antimony has been determined after reduction of antimony(V) to antimony(III) using potassium iodide and ascorbic acid. For determination of total inorganic antimony the sample is percolated in a mini-column containing the Dowex 50W-X8 resin for retention of the organic species of antimony. Antimony(III) is quantified in presence of 8-hydroxyquinoline as masking agent for antimony(V) after an extraction step of the organic antimony species using the also same mini-column. The trimethyl antimony(V) content is found by difference between total antimony and total inorganic antimony. By other hand, antimony(V) is quantified by difference between total inorganic antimony and antimony(III). The analytical determinations were performed using sodium tetrahydroborate as reducing agent. The optimization step was performed using two-level full factorial design and Doehlert matrix involving the factors: hydrochloric acid and sodium tetrahydroborate concentrations and sample flow rate. The optimized experimental conditions allow the antimony determination utilizing the external calibration technique with limits of detection and quantification of 0.9 and 3.1ngg(-1), respectively, and a precision expressed as relative standard deviation of 3.2% for an antimony solution of 5.0µgL(-1). The method accuracy was confirmed by analysis of the soil certified reference material furnished from Sigma-Aldrich RTC. Additionally, addition/recovery tests were performed employing synthetic solutions prepared using trimethyl antimony(V), antimony(III), antimony(V) and five soil samples. The antimony extraction step was performed in a closed system using hydrochloric acid, ultrasonic radiation and controlled temperature. The

  7. Vehicle dynamic prediction systems with on-line identification of vehicle parameters and road conditions.

    Science.gov (United States)

    Hsu, Ling-Yuan; Chen, Tsung-Lin

    2012-01-01

    This paper presents a vehicle dynamics prediction system, which consists of a sensor fusion system and a vehicle parameter identification system. This sensor fusion system can obtain the six degree-of-freedom vehicle dynamics and two road angles without using a vehicle model. The vehicle parameter identification system uses the vehicle dynamics from the sensor fusion system to identify ten vehicle parameters in real time, including vehicle mass, moment of inertial, and road friction coefficients. With above two systems, the future vehicle dynamics is predicted by using a vehicle dynamics model, obtained from the parameter identification system, to propagate with time the current vehicle state values, obtained from the sensor fusion system. Comparing with most existing literatures in this field, the proposed approach improves the prediction accuracy both by incorporating more vehicle dynamics to the prediction system and by on-line identification to minimize the vehicle modeling errors. Simulation results show that the proposed method successfully predicts the vehicle dynamics in a left-hand turn event and a rollover event. The prediction inaccuracy is 0.51% in a left-hand turn event and 27.3% in a rollover event.

  8. Development of an on-line coal quality management system in a lignite open pit mine in Serbia

    Energy Technology Data Exchange (ETDEWEB)

    Zimmer, B. [Montan Bildungs-und Entwicklungsgesellschaft mbH, Theiben, (Germany)

    2010-07-01

    This paper presented a study regarding the development of a coal quality management system (CQMS) for two open pit mines located in Serbia called Tamnava West and Veliki Crljeni. The study was based on on-line measurements, and was commissioned by the public energy corporation Elektroprivreda Srbjie. The purpose of the study was to develop a CQMS that met the quality requirements of the power plants by implementing a rigorous exploration, production planning, and production monitoring system in order to control the production according to certain quality parameters. The paper provided general information and described the initial situation. It also presented an analysis of the necessity to introduce a production monitoring and control system. The setup and layout of a production monitoring and control system based on on-line measurements were outlined, with particular reference to the determination of input parameters for every excavator for the tracking of masses; the simulation of mass tracking and summation of the masses at the transfer points towards the major conveyor; and the monitoring of the output and control of the mass flow according to determined limit values. Recommendations for implementation were also discussed. It was concluded that the newly developed CQMS at Tamnava West open pit mine could be classified as uncomplicated with regard to the quality parameters to be controlled, since currently only calorific value was being controlled. 5 refs., 8 figs.

  9. Study on an On-line Measurement System of Corrosion Rate by Linear Polarization Resistance

    Energy Technology Data Exchange (ETDEWEB)

    Moon, Jeon Soo; Lee, Jae Kun; Lee, Jae Bong; Park, Pyl Yang [Korea Electric Power Research Institute, Daejeon (Korea, Republic of)

    2012-04-15

    The linear polarization resistance method is one of the widely used techniques for the corrosion rate monitoring in the water circulating systems of plants. The measurement is simple and rapid, so that a continuous on-line monitoring is possible without any shutdown of plants. A 2-electrode polarization corrosion rate measurement system was installed in a laboratory using a data acquisition board and PC. The signal processing parameters were optimized for the accurate corrosion rate measurement, and the polarization resistance was compensated with the solution resistance measured by the high frequency sine wave signal of an output channel. The precision of corrosion rate data was greatly improved by removing the initial noise signals on measuring the polarization resistance.

  10. Robust on-line relay automatic tuning of PID control systems

    Science.gov (United States)

    Tan; Lee; Jiang

    2000-01-01

    In this paper, a robust on-line relay automatic tuning method for PID control systems is developed which expand on the application domain of Astrom's renowned relay autotuning method. In the proposed configuration, a relay is applied to an inner loop of a controller-stabilised process in the usual manner. Using the induced limit cycle oscillations from the closed-loop system, the controller settings may be re-tuned non-iteratively to achieve enhanced performance without disrupting closed-loop control. Two control tuning methodologies are developed -- a direct and an indirect method based on an explicit process model. Simulation examples and a real-time experiment are provided to illustrate the practical appeal and potential advantages of the proposed method over the basic one.

  11. The on-line electric vehicle wireless electric ground transportation systems

    CERN Document Server

    Cho, Dong

    2017-01-01

    This book details the design and technology of the on-line electric vehicle (OLEV) system and its enabling wireless power-transfer technology, the “shaped magnetic field in resonance” (SMFIR). The text shows how OLEV systems can achieve their three linked important goals: reduction of CO2 produced by ground transportation; improved energy efficiency of ground transportation; and contribution to the amelioration or prevention of climate change and global warming. SMFIR provides power to the OLEV by wireless transmission from underground cables using an alternating magnetic field and the reader learns how this is done. This cable network will in future be part of any local smart grid for energy supply and use thereby exploiting local and renewable energy generation to further its aims. In addition to the technical details involved with design and realization of a fleet of vehicles combined with extensive subsurface charging infrastructure, practical issues such as those involved with pedestrian safety are c...

  12. An On-Line Oxygen Forecasting System for Waterless Live Transportation of Flatfish Based on Feature Clustering

    Directory of Open Access Journals (Sweden)

    Yongjun Zhang

    2017-09-01

    Full Text Available Accurate prediction of forthcoming oxygen concentration during waterless live fish transportation plays a key role in reducing the abnormal occurrence, increasing the survival rate in delivery operations, and optimizing manufacturing costs. The most effective ambient monitoring techniques that are based on the analysis of historical process data when performing forecasting operations do not fully consider current ambient influence. This is likely lead to a greater deviation in on-line oxygen level forecasting in real situations. Therefore, it is not advisable for the system to perform early warning and on-line air adjustment in delivery. In this paper, we propose a hybrid method and its implementation system that combines a gray model (GM (1, 1 with least squares support vector machines (LSSVM that can be used effectively as a forecasting model to perform early warning effectively according to the dynamic changes of oxygen in a closed system. For accurately forecasting of the oxygen level, the fuzzy C-means clustering (FCM algorithm was utilized for classification according to the flatfish’s physical features—i.e., length and weight—for more pertinent training. The performance of the gray model-particle swarm optimization-least squares support vector machines (GM-PSO-LSSVM model was compared with the traditional modeling approaches of GM (1, 1 and LSSVM by applying it to predict on-line oxygen level, and the results showed that its predictions were more accurate than those of the LSSVM and grey model. Therefore, it is a suitable and effective method for abnormal condition forecasting and timely control in the waterless live transportation of flatfish.

  13. Radiation Effects on the On-line Monitoring System of a Hadrontherapy Center

    Directory of Open Access Journals (Sweden)

    Abdolkazem Ansarinejad

    2014-11-01

    Full Text Available Introduction Today, there is a growing interest in the use of hadrontherapy as an advanced radiotherapy technique. Hadrontherapy is considered a promising tool for cancer treatment, given its high radiobiological effectiveness and high accuracy of dose deposition due to the physical properties of hadrons. However, new radiation modalities of dose delivery and on-line beam monitoring play crucial roles in a successful treatment. In hadrontherapy, through interactions between the primary beam and patient’s tissue, secondary neutrons are produced. Materials and Methods This study, by using FLUKA Monte Carlo simulations, assessed the level of secondary neutron radiation, produced during patient treatment. In addition,  the evaluation included secondary neutron radiation, which was produced while hitting the on-line detectors of beam delivery system by the Italian National Center for Hadrontherapy (CNAO. This study assessed the effects of secondary neutron radiation on an electronics rack (including a data acquisition system, a power supply, and a gas system and a nozzle, where two monitoring boxes (each one consisting of two or three parallel plate ionization chambers were installed. Results The resulting neutron energy spectra and radiation doses were used to determine the life performance and the probability of damage to these devices. Findings showed that by using carbon ions of 400 MeV/u, the fluence rate of secondary neutrons will be approximately 3.4×1010 n/cm2 in a year. Conclusion This value is lower than the experimental threshold, which is responsible for less than 1% of changes in electrical characteristics, and would cause no single event upsets.

  14. On-line scheduling of Automatics and flexible Manufacturing System using SARSA technique

    Science.gov (United States)

    Aissani, N.; Beldjilali, B.

    2008-06-01

    In this paper context, we will show what will be the best organization of decision entities in flexible manufacturing system, but also show our approach steps to achieve a manufacturing control system which is more reliable insofar as it has responding to queries in online. With this intention, we use a multi-agent system of which the decisions taken by the system are the result of those agents group work, these agents ensure in the same time manufacturing scheduling solution and a continuously improvement of their quality thanks to the reinforcement learning technique and particularly SARSA algorithm which was introduced to them. This technique of learning makes it possible the agents to be adaptive and to learn the best behavior in their various roles (answer the requests, self-organization, plan…) without attenuating the system on-line. A computer implementation and experimentation of this model are provided in this paper to demonstrate the contribution of our approach compared to a famous metaheuristic: tabu search, widely used for scheduling in complex manufacturing systems.

  15. On-line tracking of pulverized coal and biomass fuels through flame spectrum analysis

    Institute of Scientific and Technical Information of China (English)

    迟天阳; 张宏建

    2007-01-01

    This paper presents a new approach to the on-line tracking of pulverized coal and biomass fuels through flame spectrum analysis. A flame detector containing four photodiodes is used to derive multiple signals covering a wide spectrum of the flame from visible, near-infrared and mid-infrared spectral bands as well as a part of far-infrared band. Different features are extracted in time and frequency domains to identify the dynamic "fingerprints" of the flame. Fuzzy logic inference techniques are employed to combine typical features together and infer the type of fuel being burnt. Four types of pulverized coal and five types of biomass are burnt on a laboratory-scale combustion test rig. Results obtained demonstrate that this approach is capable of tracking the type of fuel under steady combustion conditions.

  16. An On-Line Scheduler over Hard Real-Time Communication System

    Institute of Scientific and Technical Information of China (English)

    CHEN Hui; XIONG Guangze

    2003-01-01

    By thorough research on the prominent periodic and aperiodic scheduling algorithms, an on-line hard real-time scheduler is presented, which is applicable to the scheduling of packets over a link.This scheduler, based on both Rate Monotonic, pinwheel scheduling algorithm Sr and Polling Server scheduling algorithms, can rapidly judge the schedulability and then automatically generate a bus table for the scheduling algorithm to schedule the packets as the periodic packets. The implementation of the scheduler is simple and easy to use, and it is effective for the utilization of bus link. The orderly execution of the bus table can not only guarantee the performance of the hard real time but also avoid the blockage and interruption of the message transmission. So the scheduler perfectly meets the demand of hard realtime communication system on the field bus domain.

  17. Implementation of an on-line monitoring system for transmitters in a CANDU nuclear power plant

    Science.gov (United States)

    Labbe, A.; Abdul-Nour, G.; Vaillancourt, R.; Komljenovic, D.

    2012-05-01

    Many transmitters (pressure, level and flow) are used in a nuclear power plant. It is necessary to calibrate them periodically to ensure that their measurements are accurate. These calibration tasks are time consuming and often contribute to worker radiation exposure. Human errors can also sometimes degrade their performance since the calibration involves intrusive techniques. More importantly, experience has shown that the majority of current calibration efforts are not necessary. These facts motivated the nuclear industry to develop new technologies for identifying drifting instruments. These technologies, well known as on-line monitoring (OLM) techniques, are non-intrusive and allow focusing the maintenance efforts on the instruments that really need a calibration. Although few OLM systems have been implemented in some PWR and BWR plants, these technologies are not commonly used and have not been permanently implemented in a CANDU plant. This paper presents the results of a research project that has been performed in a CANDU plant in order to validate the implementation of an OLM system. An application project, based on the ICMP algorithm developed by EPRI, has been carried out in order to evaluate the performance of an OLM system. The results demonstrated that the OLM system was able to detect the drift of an instrument in the majority of the studied cases. A feasibility study has also been completed and has demonstrated that the implementation of an OLM system at a CANDU nuclear power plant could be advantageous under certain conditions.

  18. On-line Decentralized Charging of Plug-In Electric Vehicles in Power Systems

    CERN Document Server

    Li, Qiao; Negi, Rohit; Franchetti, Franz; Ilic, Marija D

    2011-01-01

    Plug-in electric vehicles (PEV) are gaining increasing popularity in recent years, due to the growing societal awareness of reducing greenhouse gas (GHG) emissions and the dependence on foreign oil or petroleum. Large-scale implementation of PEVs in the power system currently faces many challenges. One particular concern is that the PEV charging can potentially cause significant impact on the existing power distribution system, due to the increase in peak load. As such, this work tries to mitigate the PEV charging impact by proposing a decentralized smart PEV charging algorithm to minimize the distribution system load variance, so that a 'flat' total load profile can be obtained. The charging algorithm is on-line, in that it controls the PEV charging processes in each time slot based entirely on the current power system state. Thus, compared to other forecast based smart charging approaches in the literature, the charging algorithm is robust against various uncertainties in the power system, such as random PE...

  19. On-line Monitoring System based on Vibration Signal of High Voltage Circuit Breaker

    Directory of Open Access Journals (Sweden)

    Chao Fu

    2014-04-01

    Full Text Available High voltage circuit breaker is one of the most important switch apparatus in electrical power system. It play a role in the switch control, which can be used to switch the operating mode during normal operation (the equipment run or quit. In order to ensure the normal operation of the grid, it can be removed quickly when a malfunction on the device or circuit. Real-time online monitoring of high voltage circuit breaker can understand the running status, master the operation characteristics and its tend of development. As early as possible find the potential faults then take preventive measures timely, so as to ensure the reliable operation of power system. Online monitoring of high voltage circuit breakers can reduce the premature or unnecessary maintenance and maintenance cost, improve pertinence of the maintenance firstly. Secondly, it can improve the life of the switching device and improve the reliability of electric power system significantly. In this paper, on-line monitoring system based on vibration signal of high voltage circuit breaker is presented

  20. On-Line Smoothing for an Integrated Navigation System with Low-Cost MEMS Inertial Sensors

    Directory of Open Access Journals (Sweden)

    Shih-Ching Huang

    2012-12-01

    Full Text Available The integration of the Inertial Navigation System (INS and the Global Positioning System (GPS is widely applied to seamlessly determine the time-variable position and orientation parameters of a system for navigation and mobile mapping applications. For optimal data fusion, the Kalman filter (KF is often used for real-time applications. Backward smoothing is considered an optimal post-processing procedure. However, in current INS/GPS integration schemes, the KF and smoothing techniques still have some limitations. This article reviews the principles and analyzes the limitations of these estimators. In addition, an on-line smoothing method that overcomes the limitations of previous algorithms is proposed. For verification, an INS/GPS integrated architecture is implemented using a low-cost micro-electro-mechanical systems inertial measurement unit and a single-frequency GPS receiver. GPS signal outages are included in the testing trajectories to evaluate the effectiveness of the proposed method in comparison to conventional schemes.

  1. Investigations of on-line process analysis in batchwise and continuous ethanol production using Zymomonas mobilis. Untersuchungen zur on-line Prozessanalyse bei der satzweisen und kontinuierlichen Ethanolproduktion mit Zymomonas mobilis

    Energy Technology Data Exchange (ETDEWEB)

    Schmidt, W.

    1985-01-01

    A fermentation unit was connected to a process computer for on-line data acquisition, process observation and SPC control. The continuous measurement of relevant process parameters was to enable off-line modelling of growth and product formation of the bacterium Zymomonas mobilis. A continuous analysis of substrate and product concentrations beyond the conventional instrumentation of bioreactors was made possible by using membrane separation processes with subsequent detection of components. A glucose detection method adaptable to glucose was developed. Exhaust gas, dissolved gas and volatile components were measured using a mass spectrometer convected to the reactor. Data acquisition, data analysis and system control were carried out using the process computer system CASFA (= Computer Automation System for Fermentation Systems on the Laboratory Scale).

  2. A Novel Multi-Secret Sharing Approach for Secure Data Warehousing and On-Line Analysis Processing in the Cloud

    OpenAIRE

    Attasena, Varunya; Harbi, Nouria; Darmont, Jérôme

    2015-01-01

    International audience; Cloud computing helps reduce costs, increase business agility and deploy solutions with a high return on investment for many types of applications, including data warehouses and on-line analytical processing. However, storing and transferring sensitive data into the cloud raises legitimate security concerns. In this paper, we propose a new multi-secret sharing approach for deploying data warehouses in the cloud and allowing on-line analysis processing, while enforcing ...

  3. A Novel Multi-Secret Sharing Approach for Secure Data Warehousing and On-Line Analysis Processing in the Cloud

    OpenAIRE

    Attasena, Varunya; Harbi, Nouria; Darmont, Jérôme

    2017-01-01

    Cloud computing helps reduce costs, increase business agility and deploy solutions with a high return on investment for many types of applications, including data warehouses and on-line analytical processing. However, storing and transferring sensitive data into the cloud raises legitimate security concerns. In this paper, we propose a new multi-secret sharing approach for deploying data warehouses in the cloud and allowing on-line analysis processing, while enforcing data privacy, integrity ...

  4. On-line Speciation of Cr(III) and Cr(VI) by Flow Injection Analysis With Spectrophotometric Detection and Chemometrics

    DEFF Research Database (Denmark)

    Diacu, Elena; Andersen, Jens Enevold Thaulov

    2003-01-01

    A flow injection system has been developed, for on-line speciation. of Cr(III) and Cr(VI) by the Diphenylcarbazide (DPC) method with H2O2 oxidation followed by spectrophotometric detection at the 550 nm wavelength. The data thus obtained were subjected to a chemometric analysis (PLS), which showe...

  5. On-line metabolic pathway analysis based on metabolic signal flow diagram.

    Science.gov (United States)

    Shi, H; Shimizu, K

    In this work, an integrated modeling approach based on a metabolic signal flow diagram and cellular energetics was used to model the metabolic pathway analysis for the cultivation of yeast on glucose. This approach enables us to make a clear analysis of the flow direction of the carbon fluxes in the metabolic pathways as well as of the degree of activation of a particular pathway for the synthesis of biomaterials for cell growth. The analyses demonstrate that the main metabolic pathways of Saccharomyces cerevisiae change significantly during batch culture. Carbon flow direction is toward glycolysis to satisfy the increase of requirement for precursors and energy. The enzymatic activation of TCA cycle seems to always be at normal level, which may result in the overflow of ethanol due to its limited capacity. The advantage of this approach is that it adopts both virtues of the metabolic signal flow diagram and the simple network analysis method, focusing on the investigation of the flow directions of carbon fluxes and the degree of activation of a particular pathway or reaction loop. All of the variables used in the model equations were determined on-line; the information obtained from the calculated metabolic coefficients may result in a better understanding of cell physiology and help to evaluate the state of the cell culture process. Copyright 1998 John Wiley & Sons, Inc.

  6. The Corrosion Inhibition Characteristics of Sodium Nitrite Using an On-line Corrosion Rate Measurement System

    Energy Technology Data Exchange (ETDEWEB)

    Park, Mal-Yong; Kang, Dae-Jin [Korea Polytechnic University, Shiheung (Korea, Republic of); Moon, Jeon-Soo [Future Technology Research Laboratory, KEPCO Research Institute, Daejeon (Korea, Republic of)

    2015-04-15

    An on-line corrosion rate measurement system was developed using a personal computer, a data acquisition board and program, and a 2-electrode corrosion probe. Reliability of the developed system was confirmed with through comparison test. With this system, the effect of sodium nitrite (NaNO{sub 2}) as a corrosion inhibitor were studied on iron and aluminum brass that were immersed in sodium chloride (NaCl) solution. Corrosion rate was measured based on the linear polarization resistance method. The corrosion rates of aluminum brass and iron in 1% NaCl solutions were measured to be 0.290 mm per year (mmpy) and 0.2134 mmpy, respectively. With the addition of 200 ppm of NO{sub 2}{sup -}, the corrosion rates decreased to 0.0470 mmpy and 0.0254 mmpy. The addition of NO{sub 2}{sup -} caused a decrease in corrosion rates of both aluminum brass and iron, yet the NO{sub 2}{sup -} acted as a more effective corrosion inhibitor for iron. than aluminum brass.

  7. The 1-way on-line coupled atmospheric chemistry model system MECO(n – Part 2: On-line coupling with the Multi-Model-Driver (MMD

    Directory of Open Access Journals (Sweden)

    A. Kerkweg

    2012-01-01

    Full Text Available A new, highly flexible model system for the seamless dynamical down-scaling of meteorological and chemical processes from the global to the meso-γ scale is presented. A global model and a cascade of an arbitrary number of limited-area model instances run concurrently in the same parallel environment, in which the coarser grained instances provide the boundary data for the finer grained instances. Thus, disk-space intensive and time consuming intermediate and pre-processing steps are entirely avoided and the time interpolation errors of common off-line nesting approaches are minimised. More specifically, the regional model COSMO of the German Weather Service (DWD is nested on-line into the atmospheric general circulation model ECHAM5 within the Modular Earth Submodel System (MESSy framework. ECHAM5 and COSMO have previously been equipped with the MESSy infrastructure, implying that the same process formulations (MESSy submodels are available for both models. This guarantees the highest degree of achievable consistency, between both, the meteorological and chemical conditions at the domain boundaries of the nested limited-area model, and between the process formulations on all scales.

    The on-line nesting of the different models is established by a client-server approach with the newly developed Multi-Model-Driver (MMD, an additional component of the MESSy infrastructure. With MMD an arbitrary number of model instances can be run concurrently within the same message passing interface (MPI environment, the respective coarser model (either global or regional is the server for the nested finer (regional client model, i.e. it provides the data required to calculate the initial and boundary fields to the client model. On-line nesting means that the coupled (client-server models exchange their data via the computer memory, in contrast to the data exchange via files on disk in common off-line nesting approaches. MMD consists of a library

  8. The 1-way on-line coupled atmospheric chemistry model system MECO(n – Part 2: On-line coupling

    Directory of Open Access Journals (Sweden)

    A. Kerkweg

    2011-06-01

    Full Text Available A new, highly flexible model system for the seamless dynamical down-scaling of meteorological and chemical processes from the global to the meso-γ scale is presented. A global model and a cascade of an arbitrary number of limited-area model instances run concurrently in the same parallel environment, in which the coarser grained instances provide the boundary data for the finer grained instances. Thus, disk-space intensive and time consuming intermediate and pre-processing steps are entirely avoided and the time interpolation errors of common off-line nesting approaches are minimised. More specifically, the regional model COSMO of the German Weather Service (DWD is nested on-line into the atmospheric general circulation model ECHAM5 within the Modular Earth Submodel System (MESSy framework. ECHAM5 and COSMO have previously been equipped with the MESSy infrastructure, implying that the same process formulations (MESSy submodels are available for both models. This guarantees the highest degree of achievable consistency, between both, the meteorological and chemical conditions at the domain boundaries of the nested limited-area model, and between the process formulations on all scales.

    The on-line nesting of the different models is established by a client-server approach with the newly developed Multi-Model-Driver (MMD, an additional component of the MESSy infrastructure. With MMD an arbitrary number of model instances can be run concurrently within the same message passing interface (MPI environment, the respective coarser model (either global or regional is the server for the nested finer (regional client model, i.e., it provides the data required to calculate the initial and boundary fields to the client model. On-line nesting means that the coupled (client-server models exchange their data via the computer memory, in contrast to the data exchange via files on disk in common off-line nesting approaches. MMD consists of a library

  9. Thermoluminescence (TL) spectra from quartz grains using on-line TL-spectrometric system

    Energy Technology Data Exchange (ETDEWEB)

    Hashimoto, T.; Sugai, N.; Sakaue, H.; Shirai, N. [Niigata University, Niigata (Japan). Faculty of Science; Yasuda, K. [Daiwa Geological Laboratory Co. Ltd., Fukushima (Japan)

    1997-12-31

    An on-line spectrometric system installed with a small spectrometer and an image intensifier unit has been developed for weak and changeable TL-spectrum measurements with rising temperature for application to natural minerals. The detection sensitivity over visible wavelength regions was corrected using a known spectrum from a standard light source, and the detection sensitivity was also examined by a chemical luminol reaction. In an applied experiment, two quartz grain samples from two pyroclastic flows of the same origin, were subjected to testing with the present measuring system. The original data, consisting of 512 channels for every second at a constant heating rate of 1degC/s, were used to create a contour map or a 3-dimensional expression of TL-spectra after subtraction of background radiation. The artificially irradiated quartz grains clearly showed both red (RTL) and blue TL (BTL) in contrast to RTL alone from naturally accumulated TL. Both spectral expressions and glow curves from the same original data were found to be available to estimate quartz formation temperatures, together with thermoluminescence color images (TLCIs). 24 refs., 9 figs.

  10. Research on Quality Inspection and Sorting On-line System for Bearing Steel Ball

    Directory of Open Access Journals (Sweden)

    Yu Runxiang

    2015-01-01

    Full Text Available To detect the flaws of bearing steel ball and sort its quality on-line, a kind of online quality detecting and sorting system for bearing steel ball is developed, which based on the eddy current inspection theory. The design of scheme, circuit and mechanical structure of the system is described in detail. PSD(Phase Sensitive Detection is applied to pick up the signal of cracks and restrain interferential signal. The flaws will be quantificational analysed based on the X-R orthogonal decomposition technology which include the size and depth information of flaws. By analysing and processing the amplitude and phase of the defect signal, the flaws can be found with high accuracy and low error-detected ratio. ARM and MCU Processor ensures the real-time ability of discriminating algorithm. The CPLD is used for generating reference signal which can be easy to get synchronous with the source signal. It has good properties of real-time to detect the quality of bearing steel ball.

  11. Development of a Probabilistic Technique for On-line Parameter and State Estimation in Non-linear Dynamic Systems

    Energy Technology Data Exchange (ETDEWEB)

    Tunc Aldemir; Don W. Miller; Brian k. Hajek; Peng Wang

    2002-04-01

    The DSD (Dynamic System Doctor) is a system-independent, interactive software under development for on-line state/parameter estimation in dynamic systems (1), partially supported through a Nuclear Engineering Education (NEER) grant during 1998-2001. This paper summarizes the recent accomplishments in improving the user-friendliness and computational capability of DSD

  12. Flow analysis by using solenoid valves for As(III determination in natural waters by an on-line separation and pre-concentration system coupled to a tungsten coil atomizer

    Directory of Open Access Journals (Sweden)

    José Y. Neira

    2005-03-01

    Full Text Available A flow system coupled to a tungsten coil atomizer in an atomic absorption spectrometer (TCA-AAS was developed for As(III determination in waters, by extraction with sodium diethyldithiocarbamate (NaDDTC as complexing agent, and by sorption of the As(III-DDTC complex in a micro-column filled with 5 mg C18 reversed phase (10 µL dry sorbent, followed by elution with ethanol. A complete pre-concentration/elution cycle took 208 s, with 30 s sample load time (1.7 mL and 4 s elution time (71 µL. The interface and software for the synchronous control of two peristaltic pumps (RUN/ STOP, an autosampler arm, seven solenoid valves, one injection valve, the electrothermal atomizer and the spectrometer Read function were constructed. The system was characterized and validated by analytical recovery studies performed both in synthetic solutions and in natural waters. Using a 30 s pre-concentration period, the working curve was linear between 0.25 and 6.0 µg L-1 (r = 0.9976, the retention efficiency was 94±1% (6.0 µg L-1, and the pre-concentration coefficient was 28.9. The characteristic mass was 58 pg, the mean repeatability (expressed as the variation coefficient was 3.4% (n=5, the detection limit was 0.058 µg L-1 (4.1 pg in 71 µL of eluate injected into the coil, and the mean analytical recovery in natural waters was 92.6 ± 9.5 % (n=15. The procedure is simple, economic, less prone to sample loss and contamination and the useful lifetime of the micro-column was between 200-300 pre-concentration cycles.

  13. On-line Scanned Probe Microscopy Transparently Integrated with DualBeam SEM/FIB Systems

    Science.gov (United States)

    Ignatov, Andrey; Komissar, Anatoly; Lewis, Aaron

    2013-03-01

    A multifunctional scanning probe microscope (SPM) will be described that transparently integrates with a DualBeam SEM/FIB System. This is done without perturbing any of the capabilities of the Dual Beam in terms of detectors, gas injectors, analyzers etc while allowing for a completely exposed probe tip to be imaged online even with immersion objectives at working distances as short as 4 mm. In addition, the completely free motion of the rotation axis of the stage is maintained with the probe tip at the eucentric point, this makes it possible to orient the sample in any direction on any structure The X and Y scan range of the atomic force microscopic (AFM) imaging achieves 35 microns with rough motion over 10 millimeters. This permits the SPM to tilt into position perpendicular to the SEM or FIB or under an angle for rapid and accurate placement of the probe tip at or on structures such as biopolymeric materials that are nanometric in X, Y and Z extent. Thus, not only can a structure's nanometric height be accurately profiled but this can be accomplished with the on-line excellence of SEM for X, Y metrology. Furthermore, electron and ion beam sensitive samples can be imaged and characterized by AFM at high resolution.

  14. Design and experimental research of the on-line detection system for diamond arc grinding wheel

    Science.gov (United States)

    Zhang, Feihu; Li, Chen; Liu, Zhongde; Ren, Lele; Xie, Haisheng

    2016-10-01

    The principle of measuring displacement by eddy current sensor was derived. The calibration experiment was carried out for 5 kinds of different materials, which showed that the linearity of eddy current sensor was better, and the sensitivity of eddy current sensor varied with different materials. Based on the principle of measuring displacement by eddy current sensor, the on-line detection system for diamond circular wheel was designed, and the data acquisition was realized by using LABVIEW software. By moving the eddy current sensor in the vertical direction with the grinding wheel fixed, the coordinate of arc in the grinding wheel was obtained. The radius of the grinding wheel was fitted by using the genetic algorithm, which showed that the fitting results were accurate. The data acquisition of the grinding wheel was carried out in a cycle by fixing the electric eddy current sensor and the circulars of the grinding wheel in different processes, namely before dressing, after dressing and after shaping. The results showed that the circular of the grinding wheel after dressing and after shaping were significantly improved compared with that before dressing.

  15. On-line I-/Te- separation for the AMS analysis of 125I

    Science.gov (United States)

    Charles, C. R. J.; Cornett, R. J.; Zhao, X.-L.; Litherland, A. E.; Kieser, W. E.

    2015-10-01

    The isobar separator for anions (ISA) was used together with a 3 MV tandem accelerator mass spectrometer (AMS) to demonstrate the real time (on-line) separation of Te- from I-. Following the ion source mass spectrometry and major retardation to tens of eV, the ISA uses a radiofrequency quadrupole (RFQ) ion guide to confine and direct I- and associated Te- isobar anions through a gas-reaction cell, where chemical reactions occur at eV energies with the electronegative gas NO2. Anions are subsequently reaccelerated out of the ISA to near original ion source extraction energies for AMS analysis. At 5 mTorr NO2 in the ISA gas-reaction cell, 125Te- was observed to be attenuated by a factor of ∼107 as compared to 127I- that did not experience significant (107 relative to 37Cl- under the same ISA-AMS conditions. The preferential destruction of Te- (and S-) at eV energies in the ISA is likely due to a larger favorable destruction cross-section with NO2. This study is the first demonstration of I-Te anion separation for AMS, and makes possible the use of 125I, free of the contaminant 125Te isobar after suitable sample purification, for future 129I/125I carrier-free analyses of natural samples at ultra-low trace levels.

  16. Moving object detection based on on-line block-robust principal component analysis decomposition

    Science.gov (United States)

    Yang, Biao; Cao, Jinmeng; Zou, Ling

    2017-07-01

    Robust principal component analysis (RPCA) decomposition is widely applied in moving object detection due to its ability in suppressing environmental noises while separating sparse foreground from low rank background. However, it may suffer from constant punishing parameters (resulting in confusion between foreground and background) and holistic processing of all input frames (leading to bad real-time performance). Improvements to these issues are studied in this paper. A block-RPCA decomposition approach was proposed to handle the confusion while separating foreground from background. Input frame was initially separated into blocks using three-frame difference. Then, punishing parameter of each block was computed by its motion saliency acquired based on selective spatio-temporal interesting points. Aiming to improve the real-time performance of the proposed method, an on-line solution to block-RPCA decomposition was utilized. Both qualitative and quantitative tests were implemented and the results indicate the superiority of our method to some state-of-the-art approaches in detection accuracy or real-time performance, or both of them.

  17. Design and application of radiation apparatus for sup 6 sup 0 Co cargo train on-line inspection system

    CERN Document Server

    Wu Zhi Fang; Zhang Yuai

    2002-01-01

    Based on the special requirement for radiation apparatus of sup 6 sup 0 Co cargo train on-line inspection system, a radiation apparatus including two-level shutter, working container, storing container and electromagnetism are designed. The makeup, working mode and functional realization of the radiation apparatus are introduced. The system is used in Manzhouli customs cargo train on-line inspection system. The practice shows that the radiation apparatus is reliable to work steadily and the operating speed of the main shutter can reach 0.1 s open and 0.15 s close

  18. Development of FIA-enzyme systems for on-line monitoring of starch, cellulose and amygdalin concentrations

    Energy Technology Data Exchange (ETDEWEB)

    Umoh, E.

    1993-07-02

    Immobilized enzyme - FIA systems were developed for application in monitoring starch concentration during fermentation, cellulose concentration in hydrolysis process and amygdalin concentration in industrial effluents as an index of toxic potentiality of such effluents. The starch measuring system consisting of glucoamylase, glucose oxidase and mutarotase was employed to measure glucose and starch simultaneously. The system was used for on-line monitoring of starch concentration in a 24 hour Bacillus lichenifonnis fermentation and dextrin concentration in a 140 hour fermentation of Cephalosporium acremonium. The on-line measurements agree well with the concentrations determined off-line using both calorimetric and enzymatic methods. (orig.)

  19. The IBM System 7 On-Line Circulation System at Slippery Rock State College.

    Science.gov (United States)

    Wood, Richard J.

    This article describes and evalutes the IBM System 7 automated circulation system in use at Slippery Rock State College Library since 1973. Background information is furnished on the library and its locale as well as the general rationale and objectives for automated circulation systems. The presentation of the IBM S/7 includes (1) reasons for its…

  20. A system for accurate on-line measurement of total gas consumption or production rates in microbioreactors

    NARCIS (Netherlands)

    van Leeuwen, Michiel; Heijnen, Joseph J.; Gardeniers, Johannes G.E.; Oudshoorn, Arthur; Noorman, Henk; Visser, Jan; van der Wielen, Luuk A.M.; van Gulik, Walter M.

    2009-01-01

    A system has been developed, based on pressure controlled gas pumping, for accurate measurement of total gas consumption or production rates in the nmol/min range, applicable for on-line monitoring of bioconversions in microbioreactors. The system was validated by carrying out a bioconversion with

  1. A system for accurate on-line measurement of total gas consumption or production rates in microbioreactors

    NARCIS (Netherlands)

    Leeuwen, van Michiel; Heijnen, Joseph J.; Gardeniers, Han; Oudshoorn, Arthur; Noorman, Henk; Visser, Jan; Wielen, van der Luuk A.M.; Gulik, van Walter M.

    2009-01-01

    A system has been developed, based on pressure controlled gas pumping, for accurate measurement of total gas consumption or production rates in the nmol/min range, applicable for on-line monitoring of bioconversions in microbioreactors. The system was validated by carrying out a bioconversion with k

  2. Mixed-Initiative Tutorial System to Aid Users of the On-Line System (NLS).

    Science.gov (United States)

    Grignetti, Mario C.; And Others

    NLS-SCHOLAR is a prototype system that uses artificial intelligence techniques to teach computer-naive people how to use a powerful and complex text editor. It represents a new type of computer-assisted instruction (CAI) system that integrates systematic teaching with actual practice; i.e., one which can keep the user under tutorial supervision…

  3. On-line experimental validation of a model-based diagnostic algorithm dedicated to a solid oxide fuel cell system

    Science.gov (United States)

    Polverino, Pierpaolo; Esposito, Angelo; Pianese, Cesare; Ludwig, Bastian; Iwanschitz, Boris; Mai, Andreas

    2016-02-01

    In the current energetic scenario, Solid Oxide Fuel Cells (SOFCs) exhibit appealing features which make them suitable for environmental-friendly power production, especially for stationary applications. An example is represented by micro-combined heat and power (μ-CHP) generation units based on SOFC stacks, which are able to produce electric and thermal power with high efficiency and low pollutant and greenhouse gases emissions. However, the main limitations to their diffusion into the mass market consist in high maintenance and production costs and short lifetime. To improve these aspects, the current research activity focuses on the development of robust and generalizable diagnostic techniques, aimed at detecting and isolating faults within the entire system (i.e. SOFC stack and balance of plant). Coupled with appropriate recovery strategies, diagnosis can prevent undesired system shutdowns during faulty conditions, with consequent lifetime increase and maintenance costs reduction. This paper deals with the on-line experimental validation of a model-based diagnostic algorithm applied to a pre-commercial SOFC system. The proposed algorithm exploits a Fault Signature Matrix based on a Fault Tree Analysis and improved through fault simulations. The algorithm is characterized on the considered system and it is validated by means of experimental induction of faulty states in controlled conditions.

  4. On-line coupling of macroporous resin column chromatography with direct analysis in real time mass spectrometry utilizing a surface flowing mode sample holder.

    Science.gov (United States)

    Zeng, Shanshan; Wang, Lu; Chen, Teng; Qu, Haibin

    2014-02-06

    A surface flowing mode sample holder was designed as an alternative sampling strategy for direct analysis in real time mass spectrometry (DART-MS). With the sample holder, the on-line coupling of macroporous resin column chromatography with DART-MS was explored and the new system was employed to monitor the column chromatography elution process of Panax notoginseng. The effluent from macroporous resin column was first diluted and mixed with a derivatization reagent on-line, and the mixture was then directly transferred into the ionization region of DART-MS by the sample holder. Notoginsenosides were methylated and ionized in a metastable helium gas stream, and was introduced into MS for detection. The on-line system showed reasonable repeatability with a relative standard deviation of 12.3% for the peak area. Three notoginsenosides, i.e. notoginsenoside R1, ginsenoside Rb1 and ginsenoside Rg1, were simultaneously determined during the eluting process. The alteration of the chemical composition in the effluent was accurately identified in 9 min, agreeing well with the off-line analysis. The presented technique is more convenient compared to the traditional UPLC method. These results suggest that the surface flowing mode DART-MS has a good potential for the on-line process monitoring in the pharmaceutical industry.

  5. An on-line automated sleep-wake classification system for laboratory animals

    NARCIS (Netherlands)

    Witting, W; vanderWerf, D; Mirmiran, M

    1996-01-01

    A computerized sleep-wake classification program is presented that is capable of classifying sleep-wake states on-line in four animals simultaneously. Every 10 s the classification algorithm assigns sleep-wake states on the basis of the power spectrum of an EEG signal and the standard deviation of a

  6. On the use of on-line detection for maintenance of gradually deteriorating systems

    Energy Technology Data Exchange (ETDEWEB)

    Fouladirad, Mitra [Institut Charles Delaunay, Universite de Technologie de Troyes, FRE CNRS 2848, LM2S 12 rue Marie Curie, 10010 Troyes (France); Grall, Antoine [Institut Charles Delaunay, Universite de Technologie de Troyes, FRE CNRS 2848, LM2S 12 rue Marie Curie, 10010 Troyes (France)], E-mail: antoine.grall@utt.fr; Dieulle, Laurence [Institut Charles Delaunay, Universite de Technologie de Troyes, FRE CNRS 2848, LM2S 12 rue Marie Curie, 10010 Troyes (France)

    2008-12-15

    This paper deals with condition-based maintenance and non-stationary degradation process due to sudden changes. This is an attempt to propose an adaptive maintenance policy based on the on-line change detection procedure which can help to detect switches from a nominal mode to an accelerated mode in a non-informative context about the change mode time.

  7. ON LINE COMPUTATION OF EMPIRICAL FORMULA BY MEANS OF ELEMENTAL ANALYSIS AND ITS PROGRAM DESIGN

    Institute of Scientific and Technical Information of China (English)

    钱朴; 胡培荣; 金正成

    1995-01-01

    On line determination of empirical formula for organic compounds with an automatic elemental analyzer and its program design method were investigated. The computational results shews that the reliability of computational results depends on the accuracy of the analytical data and the organic compound itself.

  8. MODULAR RESEARCH EQUIPMENT FOR ON-LINE INSPECTION IN ADVANCED MANUFACTURING SYSTEMS

    Directory of Open Access Journals (Sweden)

    Davrajh, S.

    2012-11-01

    Full Text Available The significance of inspection processes increases when producing parts with high levels of customer input. These processes must adapt to variations in significant product characteristics. Mass customisation and reconfigurable manufacturing are currently being researched as ways to respond to high levels of customer input. This paper presents the research and development of modular inspection equipment that was designed to meet the on-line quality requirements of mass customisation and reconfigurable manufacturing environments. Simulated results were analysed for application in an industrial environment. The implementation of the equipment in South Africa is briefly discussed. The research indicates that manufacturers need only invest in the required equipment configurations when they are needed for on-line inspection.

  9. Probabilistic Forecasting for On-line Operation of Urban Drainage Systems

    DEFF Research Database (Denmark)

    Löwe, Roland

    -box model approach. Building on previous work concerning the development of conceptual stochastic rainfall-runoff model structures, we - investigate approaches for the calibration of model parameters that tune the models for multistep predictions, - develop an approach for generating probabilistic multistep......This thesis deals with the generation of probabilistic forecasts in urban hydrology. In particular, we focus on the case of runoff forecasting for real-time control (RTC) on horizons of up to two hours. For the generation of probabilistic on-line runoff forecasts, we apply the stochastic grey...... predictions of runoff volume in an on-line setting, - develop a new approach for dynamically modelling runoff forecast uncertainty. We investigate how rainfall inputs can be optimally combined for runoff forecasting with stochastic grey-box models and what effect different types of radar rainfall measurements...

  10. Real Time On-line Space Research Laboratory Environment Monitoring with Off-line Trend and Prediction Analysis

    Science.gov (United States)

    Jules, Kenol; Lin, Paul P.

    2006-01-01

    their g-level contribution to the environment. The system can detect both known and unknown vibratory disturbance activities. It can also perform trend analysis and prediction by analyzing past data over many Increments of the space station for selected disturbance activities. This feature can be used to monitor the health of onboard mechanical systems to detect and prevent potential system failure as well as for use by research scientists during their science results analysis. Examples of both real time on-line vibratory disturbance detection and off-line trend analysis are presented in this paper. Several soft computing techniques such as Kohonen s Self-Organizing Feature Map, Learning Vector Quantization, Back-Propagation Neural Networks, and Fuzzy Logic were used to design the system.

  11. On Designing Multicore-Aware Simulators for Systems Biology Endowed with OnLine Statistics

    Directory of Open Access Journals (Sweden)

    Marco Aldinucci

    2014-01-01

    Full Text Available The paper arguments are on enabling methodologies for the design of a fully parallel, online, interactive tool aiming to support the bioinformatics scientists .In particular, the features of these methodologies, supported by the FastFlow parallel programming framework, are shown on a simulation tool to perform the modeling, the tuning, and the sensitivity analysis of stochastic biological models. A stochastic simulation needs thousands of independent simulation trajectories turning into big data that should be analysed by statistic and data mining tools. In the considered approach the two stages are pipelined in such a way that the simulation stage streams out the partial results of all simulation trajectories to the analysis stage that immediately produces a partial result. The simulation-analysis workflow is validated for performance and effectiveness of the online analysis in capturing biological systems behavior on a multicore platform and representative proof-of-concept biological systems. The exploited methodologies include pattern-based parallel programming and data streaming that provide key features to the software designers such as performance portability and efficient in-memory (big data management and movement. Two paradigmatic classes of biological systems exhibiting multistable and oscillatory behavior are used as a testbed.

  12. On designing multicore-aware simulators for systems biology endowed with OnLine statistics.

    Science.gov (United States)

    Aldinucci, Marco; Calcagno, Cristina; Coppo, Mario; Damiani, Ferruccio; Drocco, Maurizio; Sciacca, Eva; Spinella, Salvatore; Torquati, Massimo; Troina, Angelo

    2014-01-01

    The paper arguments are on enabling methodologies for the design of a fully parallel, online, interactive tool aiming to support the bioinformatics scientists .In particular, the features of these methodologies, supported by the FastFlow parallel programming framework, are shown on a simulation tool to perform the modeling, the tuning, and the sensitivity analysis of stochastic biological models. A stochastic simulation needs thousands of independent simulation trajectories turning into big data that should be analysed by statistic and data mining tools. In the considered approach the two stages are pipelined in such a way that the simulation stage streams out the partial results of all simulation trajectories to the analysis stage that immediately produces a partial result. The simulation-analysis workflow is validated for performance and effectiveness of the online analysis in capturing biological systems behavior on a multicore platform and representative proof-of-concept biological systems. The exploited methodologies include pattern-based parallel programming and data streaming that provide key features to the software designers such as performance portability and efficient in-memory (big) data management and movement. Two paradigmatic classes of biological systems exhibiting multistable and oscillatory behavior are used as a testbed.

  13. An efficient ASIC implementation of 16-channel on-line recursive ICA processor for real-time EEG system.

    Science.gov (United States)

    Fang, Wai-Chi; Huang, Kuan-Ju; Chou, Chia-Ching; Chang, Jui-Chung; Cauwenberghs, Gert; Jung, Tzyy-Ping

    2014-01-01

    This is a proposal for an efficient very-large-scale integration (VLSI) design, 16-channel on-line recursive independent component analysis (ORICA) processor ASIC for real-time EEG system, implemented with TSMC 40 nm CMOS technology. ORICA is appropriate to be used in real-time EEG system to separate artifacts because of its highly efficient and real-time process features. The proposed ORICA processor is composed of an ORICA processing unit and a singular value decomposition (SVD) processing unit. Compared with previous work [1], this proposed ORICA processor has enhanced effectiveness and reduced hardware complexity by utilizing a deeper pipeline architecture, shared arithmetic processing unit, and shared registers. The 16-channel random signals which contain 8-channel super-Gaussian and 8-channel sub-Gaussian components are used to analyze the dependence of the source components, and the average correlation coefficient is 0.95452 between the original source signals and extracted ORICA signals. Finally, the proposed ORICA processor ASIC is implemented with TSMC 40 nm CMOS technology, and it consumes 15.72 mW at 100 MHz operating frequency.

  14. On-line MSPD-SPE-HPLC/FLD analysis of polycyclic aromatic hydrocarbons in bovine tissues.

    Science.gov (United States)

    Gutiérrez-Valencia, Tania M; García de Llasera, Martha P

    2017-05-15

    A fast method was optimized and validated for simultaneous trace determination of four polycyclic aromatic hydrocarbons: benzo[a]anthracene, benzo[b]fluoranthene, benzo[k]fluoranthene and benzo[a]pyrene in bovine tissues. The determination was performed by matrix solid-phase dispersion (MSPD) coupled on-line to solid phase extraction (SPE) and high performance liquid chromatography (HPLC) with fluorescence detection (FLD). The sample was dispersed on C18 silica sorbent and then the on-line MSPD-SPE-HPLC/FLD method was applied. Several parameters were optimized: cleaning and elution sequences applied to the MSPD cartridge, the flow rate and dilution of extract used for SPE loading. The on-line method was validated over a concentration range of 0.1-0.6ngg(-1) obtaining good linearity (r⩾0.998) and precision (RSD)⩽10%. Recovery ranged from 96 to 99% and the limits of detection were 0.012ngg(-1). This methodology was applied to liver samples from unhealthy animals. The results demonstrate that MSDP-SPE-HPLC/FLD method provides reliable, sensitive, accurate and fast data to the food control.

  15. FPGA implementation of a hybrid on-line process monitoring in PC based real-time systems

    Directory of Open Access Journals (Sweden)

    Jovanović Bojan

    2011-01-01

    Full Text Available This paper presents one way of FPGA implementation of hybrid (hardware-software based on-line process monitoring in Real-Time systems (RTS. The reasons for RTS monitoring are presented at the beginning. The summary of different RTS monitoring approaches along with its advantages and drawbacks are also exposed. Finally, monitoring module is described in details. Also, FPGA implementation results and some useful monitoring system applications are mentioned.

  16. On-line air quality management system for urban-areas in Norway

    Energy Technology Data Exchange (ETDEWEB)

    Sivertsen, B.; Trond, Bohler [Norwegian Institute for Air Research, Kjeller (Norway)

    2000-07-01

    The main feature of the modem environmental management system is the integrated approach that enables the user directly accesses to data for assessment and planning of actions. The demand of the integrated system to enable monitoring, forecasting and warning of pollution situations has been and will be increasing in the future. An important basis for the projects carried out in urban areas in Norway has been the modem Environmental Surveillance and Information System (ENSIS), developed in a close co-operation between institutions dealing with air and water pollution in Norway. The air pollution part of this system, AirQUIS, has been developed at the Norwegian Institute for Air Research and is being based on geographical information systems (GIS) platform. The NILU developed AirQUIS system is a map oriented user friendly air quality management system to be used in urban and industrial areas. It contains all modules necessary to perform air quality assessment, such as databases for measurement and emissions, dispersion models and exposure module for health and materials. The AirQUIS system operates through menus and maps on the modem Windows NT platform in network with several PC clients. The process of attaining acceptable urban air quality is definitely long term, and it is dynamic. The urban area develops, and population, sources and technology change. Throughout this process, it is very important to have an operating Information System of Air Quality (AQIS), in order to: Keep the authorities and the public well informed about the short-term and long-term air quality development. Control the results of abatement measures, and thereby. Provide feedback information to the abatement strategy process. The basic concept for an Air Quality Management Strategy contains the following main components: Air Quality Assessment; Environmental Damage Assessment; Abatement Options Assessment; Cost Benefit Analysis or Cost Effectiveness Analysis; Abatement Measures; Optimum

  17. Taxonomy and clustering in collaborative systems: the case of the on-line encyclopedia Wikipedia

    OpenAIRE

    Capocci, A.; Rao, F.; Caldarelli, G.

    2007-01-01

    In this paper we investigate the nature and structure of the relation between imposed classifications and real clustering in a particular case of a scale-free network given by the on-line encyclopedia Wikipedia. We find a statistical similarity in the distributions of community sizes both by using the top-down approach of the categories division present in the archive and in the bottom-up procedure of community detection given by an algorithm based on the spectral properties of the graph. Reg...

  18. On-line condition monitoring systems for high voltage circuit breakers : a collaborative research project 1997-2001

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2001-07-01

    A three year field project was initiated to review and evaluate the state of the art in on-line conditioning monitoring technology for a high voltage (240 kV SF6) circuit breaker located at Dorsey Converter Station. The ELF breaker is a three independent pole design which allows for three separate monitoring systems. This project involved the installation of a different type of monitoring system on each phase and incorporated many types of transducers. Each monitoring system measured the same basic parameters including contact travel, 'a' and 'b' auxiliary contacts, phase currents, coil currents, heater and pump current, plus SF6/CF4 pressure and temperature. Over the entire monitoring period the breaker was operated over 700 times at rated voltage and an additional 300 times during maintenance. Temperature conditions ranged from -35 to +30 degrees C. The use of on-line monitoring provided many valuable results and enhanced the knowledge base for the apparatus under the test. It was determined that on-line monitoring of HV circuit breakers has potential, but installation has to be considered carefully. Monitoring systems can offer improvement in the understanding of how circuit breakers work and provide input into RCM programs. However, monitoring systems themselves are subject to failure and require maintenance and attention. 2 refs., 2 tabs., 7 figs.

  19. 在线水质分析仪器应用技术的发展%Development of application techniques of on-line water quality analysis instruments

    Institute of Scientific and Technical Information of China (English)

    程立

    2011-01-01

    The monitoring type and the process control type on-line water quality analysis instruments have different technical features and application requirements, and their application techniques also have different development orientations and different technical characteristics. The on-line water quality analysis systems and application techniques with self-learning function nad expert-like feature are attracting more and more attention of users.%监测型和过程型在线水质分析仪器具有不同的技术特点和应用要求,对应的在线水质分析仪器应用技术也有着不同发展方向的技术特点;具有自学习功能和专家型的在线水质分析仪器系统及应用技术开始得到了市场的重视

  20. On-line transient stability assessment of large-scale power systems by using ball vector machines

    Energy Technology Data Exchange (ETDEWEB)

    Mohammadi, M., E-mail: m.mohammadi@aut.ac.i [School of Electrical and Computer Engineering, Shiraz University, Shiraz (Iran, Islamic Republic of); Gharehpetian, G.B., E-mail: grptian@aut.ac.i [Electrical Engineering Department, Amirkabir University of Technology, Tehran (Iran, Islamic Republic of)

    2010-04-15

    In this paper ball vector machine (BVM) has been used for on-line transient stability assessment of large-scale power systems. To classify the system transient security status, a BVM has been trained for all contingencies. The proposed BVM based security assessment algorithm has very small training time and space in comparison with artificial neural networks (ANN), support vector machines (SVM) and other machine learning based algorithms. In addition, the proposed algorithm has less support vectors (SV) and therefore is faster than existing algorithms for on-line applications. One of the main points, to apply a machine learning method is feature selection. In this paper, a new Decision Tree (DT) based feature selection technique has been presented. The proposed BVM based algorithm has been applied to New England 39-bus power system. The simulation results show the effectiveness and the stability of the proposed method for on-line transient stability assessment procedure of large-scale power system. The proposed feature selection algorithm has been compared with different feature selection algorithms. The simulation results demonstrate the effectiveness of the proposed feature algorithm.

  1. On-line elemental analysis of fossil fuel process streams by inductively coupled plasma spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Chisholm, W.P.

    1995-06-01

    METC is continuing development of a real-time, multi-element plasma based spectrometer system for application to high temperature and high pressure fossil fuel process streams. Two versions are under consideration for development. One is an Inductively Coupled Plasma system that has been described previously, and the other is a high power microwave system. The ICP torch operates on a mixture of argon and helium with a conventional annular swirl flow plasma gas, no auxiliary gas, and a conventional sample stream injection through the base of the plasma plume. A new, demountable torch design comprising three ceramic sections allows bolts passing the length of the torch to compress a double O-ring seal. This improves the reliability of the torch. The microwave system will use the same data acquisition and reduction components as the ICP system; only the plasma source itself is different. It will operate with a 750-Watt, 2.45 gigahertz microwave generator. The plasma discharge will be contained within a narrow quartz tube one quarter wavelength from a shorted waveguide termination. The plasma source will be observed via fiber optics and a battery of computer controlled monochromators. To extract more information from the raw spectral data, a neural net computer program is being developed. This program will calculate analyte concentrations from data that includes analyte and interferant spectral emission intensity. Matrix effects and spectral overlaps can be treated more effectively by this method than by conventional spectral analysis.

  2. Chemiluminescence Determination of Molybdenum by on-Line Reduction with a Flow Injection System

    Institute of Scientific and Technical Information of China (English)

    2000-01-01

    The chemiluminescence (CL) reaction between lucigenin (Lu) and molybdenum (Ⅲ) produced by a Jones reductor was investigated using a flow injection system. On the basis of this, a novel method for the determination of trace amount of molybdenum has been established. The emission intensity was linear with molybdenum concentration in the range of 0.1-1000 ng/mL; the detection limit was 0.02 ng/mL molybdenum; the relative standard deviation was less than 2% for the determination of 0.1 ng/mL molybdenum (n=11). The method has been applied successfully to the analysis of trace molybdenum in water and steel samples.

  3. On-line, proximate analysis of ground beef directly at a meat grinder outlet.

    Science.gov (United States)

    Isaksson, T; Nilsen, B N; Tøgersen, G; Hammond, R P; Hildrum, K I

    1996-07-01

    The fat, moisture and protein contents of ground beef were determined on-line by a diffuse reflectance near infrared (NIR) spectroscopy instrument at the outlet of a meat grinder. Beef samples in the range of 6.2-21.7% fat, 59.6-72.9% moisture and 18.1-20.7% protein were studied. Calibrations from samples ground with hole diameters of 4, 8, 13 or 19 mm in the grinder plate were validated. In addition, calibrations of combinations of these samples from the different hole diameters were validated. Prediction errors, expressed as root mean square error of cross validation of the beef samples, were 0.73-1.50% for fat, 0.75-1.33% for moisture and 0.23-0.32% for protein, depending on the hole diameter of the grinder plate. Calibrations from samples ground with the smallest hole diameters gave lowest prediction errors. The present prediction error results are only slightly higher compared to reported prediction error results using conventional at- and off-line NIR instruments. It is concluded that the on-line NIR prediction results were acceptable for samples ground with grinder plates of 4, 8 or 13 mm hole diameter.

  4. On-line Multiple-model Based Adaptive Control Reconfiguration for a Class of Non-linear Control Systems

    DEFF Research Database (Denmark)

    Yang, Z.; Izadi-Zamanabadi, Roozbeh; Blanke, M.

    2000-01-01

    Based on the model-matching strategy, an adaptive control reconfiguration method for a class of nonlinear control systems is proposed by using the multiple-model scheme. Instead of requiring the nominal and faulty nonlinear systems to match each other directly in some proper sense, three sets...... of LTI models are employed to approximate the faulty, reconfigured and nominal nonlinear systems respectively with respect to the on-line information of the operating system, and a set of compensating modules are proposed and designed so as to make the local LTI model approximating to the reconfigured...

  5. Building a Community Infrastructure for Scalable On-Line Performance Analysis Tools around Open|Speedshop

    Energy Technology Data Exchange (ETDEWEB)

    Miller, Barton

    2014-06-30

    Peta-scale computing environments pose significant challenges for both system and application developers and addressing them required more than simply scaling up existing tera-scale solutions. Performance analysis tools play an important role in gaining this understanding, but previous monolithic tools with fixed feature sets have not sufficed. Instead, this project worked on the design, implementation, and evaluation of a general, flexible tool infrastructure supporting the construction of performance tools as “pipelines” of high-quality tool building blocks. These tool building blocks provide common performance tool functionality, and are designed for scalability, lightweight data acquisition and analysis, and interoperability. For this project, we built on Open|SpeedShop, a modular and extensible open source performance analysis tool set. The design and implementation of such a general and reusable infrastructure targeted for petascale systems required us to address several challenging research issues. All components needed to be designed for scale, a task made more difficult by the need to provide general modules. The infrastructure needed to support online data aggregation to cope with the large amounts of performance and debugging data. We needed to be able to map any combination of tool components to each target architecture. And we needed to design interoperable tool APIs and workflows that were concrete enough to support the required functionality, yet provide the necessary flexibility to address a wide range of tools. A major result of this project is the ability to use this scalable infrastructure to quickly create tools that match with a machine architecture and a performance problem that needs to be understood. Another benefit is the ability for application engineers to use the highly scalable, interoperable version of Open|SpeedShop, which are reassembled from the tool building blocks into a flexible, multi-user interface set of tools. This set of

  6. Characterization of a new generation of computed radiography system based on line scanning and phosphor needles

    Science.gov (United States)

    Dragusin, Octavian; Rogge, Frank; Pauwels, Herman; Marchal, Guy; Bosmans, Hilde

    2006-03-01

    A new generation CR system that is based on phosphor needles and that uses a digitizer with line scan technology was compared to a clinically used CR system. Purely technical and more clinically related tests were run on both systems. This included the calculation of the DQE, signal-to-noise and contrast to noise ratios from Aluminum inserts, contrast detail analysis with the CDRAD phantom and the use of anthropomorphic phantoms (wrist, chest and skull) with scoring by a radiologist. X-ray exposures with various dose levels and 50kV, 70kV and 125kV were acquired. For detector doses above 0.8 μGy, all noise related measurements showed the superiority of the new technology. The MTF confirmed the improvement in sharpness: between 1 and 3 lp/mm increases ranged from 20 to 50%. Further work should be devoted to the determination of the required dose levels in the plate for the different radiological applications.

  7. Markov Decision Process Based Energy-Efficient On-Line Scheduling for Slice-Parallel Video Decoders on Multicore Systems

    CERN Document Server

    Mastronarde, Nicholas; Atienza, David; Frossard, Pascal; van der Schaar, Mihaela

    2011-01-01

    We consider the problem of energy-efficient on-line scheduling for slice-parallel video decoders on multicore systems. We assume that each of the processors are Dynamic Voltage Frequency Scaling (DVFS) enabled such that they can independently trade off performance for power, while taking the video decoding workload into account. In the past, scheduling and DVFS policies in multi-core systems have been formulated heuristically due to the inherent complexity of the on-line multicore scheduling problem. The key contribution of this report is that we rigorously formulate the problem as a Markov decision process (MDP), which simultaneously takes into account the on-line scheduling and per-core DVFS capabilities; the separate power consumption of the processor cores and caches; and the loss tolerant and dynamic nature of the video decoder's traffic. In particular, we model the video traffic using a Direct Acyclic Graph (DAG) to capture the precedence constraints among frames in a Group of Pictures (GOP) structure, ...

  8. Analysis of hexavalent chromium in Colla corii asini with on-line sample pretreatment valve-switching ion chromatography.

    Science.gov (United States)

    Yang, Yuling; He, Jie; Huang, Zhongping; Zhong, Naifei; Zhu, Zuoyi; Jiang, Renyu; You, Jinghua; Lu, Xiuyang; Zhu, Yan; He, Shiwei

    2013-08-30

    An ion chromatography (IC) system with on-line sample pretreatment using valve-switching technique was developed for the determination of hexavalent chromium (Cr(VI)) in Colla corii asini. Colla corii asini is a complicated sample with organics as main matrix. In this work, a polymer-based reversed-phase column was used as a pretreatment column. Via valve-switching technique, sample solution with target ions were eluted from a collection loop to analytical columns, with matrix eliminated on-line. Under the optimized separation conditions, the method showed good linearity (r=0.9998) in the range of 0.004-1.0mg/L and satisfactory repeatability (RSD<3%, n=6). The limit of detection (LOD) was 1.4μg/L (S/N=3). The average spiked recoveries of Cr(VI) were 93.4-102.0%. The result showed that the on-line sample pretreatment IC system was convenient and practical for the determination of trace Cr(VI) in Colla corii asini samples.

  9. On-line structural integrity monitoring and defect diagnosis of steam generators using analysis of guided acoustic waves

    Science.gov (United States)

    Lu, Baofu

    2005-11-01

    confirmed the behavior of the acoustic signals acquired from the experimental studies. The results of this research showed the feasibility of on-line detection of small structural flaws by the use of transient and nonlinear acoustic signal analysis, and its implementation by the proper design of a piezo-electric transducer suite. The techniques developed in this research would be applicable to civil structures and aerospace structures.

  10. Development of an automated high temperature valveless injection system for on-line gas chromatography

    Directory of Open Access Journals (Sweden)

    N. M. Kreisberg

    2014-07-01

    Full Text Available A reliable method of sample introduction is presented for on-line gas chromatography with a special application to in-situ field portable atmospheric sampling instruments. A traditional multi-port valve is replaced with a controlled pressure switching device that offers the advantage of long term reliability and stable sample transfer efficiency. An engineering design model is presented and tested that allows customizing the interface for other applications. Flow model accuracy is within measurement accuracy (1% when parameters are tuned for an ambient detector and 15% accurate when applied to a vacuum based detector. Laboratory comparisons made between the two methods of sample introduction using a thermal desorption aerosol gas chromatograph (TAG show approximately three times greater reproducibility maintained over the equivalent of a week of continuous sampling. Field performance results for two versions of the valveless interface used in the in-situ instrument demonstrate minimal trending and a zero failure rate during field deployments ranging up to four weeks of continuous sampling. Extension of the VLI to dual collection cells is presented with less than 3% cell-to-cell carry-over.

  11. A new on-line electrocardiographic records database and computer routines for data analysis.

    Science.gov (United States)

    Ledezma, Carlos A; Severeyn, Erika; Perpiñán, Gilberto; Altuve, Miguel; Wong, Sara

    2014-01-01

    Gathering experimental data to test computer methods developed during a research is a hard work. Nowadays, some databases have been stored online that can be freely downloaded, however there is not a wide range of databases yet and not all pathologies are covered. Researchers with low resources are in need of more data they can consult for free. To cope with this we present an on-line portal containing a compilation of ECG databases recorded over the last two decades for research purposes. The first version of this portal contains four databases of ECG records: ischemic cardiopathy (72 patients, 3-lead ECG each), ischemic preconditioning (20 patients, 3-lead ECG each), diabetes (51 patients, 8-lead ECG each) and metabolic syndrome (25 subjects, 12-lead ECG each). In addition, one computer program and three routines are provided in order to correctly read the signals, and two digital filters along with two ECG waves detectors are provided for further processing. This portal will be constantly growing, other ECG databases and signal processing software will be uploaded. With this project, we give the scientific community a resource to avoid hours of data collection and to develop free software.

  12. Processing of situational information in story problem texts. An analysis from on-line measures.

    Science.gov (United States)

    Orrantia, Josetxu; Muñez, David; Vicente, Santiago; Verschaffel, Lieven; Rosales, Javier

    2014-01-01

    In three experiments, we investigated the extent to which readers process information related to the construction of a situation model when they are confronted with solving word problems. Considering that generation of inferences to match actions with particular goals is part of constructing of the situation model, we constructed "rich story problems", that is, word problems included in the context of a story, in which the characters propose goals, and then these goals are followed by actions to achieve it. In Experiments 1 and 2 the story problems were designed so that the character's goal was related to the activation of a problem schema, either explicitly (Experiment 1) or implicitly (Experiment 2). In Experiment 3 the problem schema activation was clearly separated from the goal information. In all three experiments, goal information availability was assessed by on-line measures. The results showed that participants processed situational information by keeping track of characters' goals. These results fit nicely with those studies that emphasize the role of situation model construction in word problem solving.

  13. [Research on On-Line Calibration Based Photoacoustic Spectrometry System for Monitoring the Concentration of CO2 in Atmosphere].

    Science.gov (United States)

    Zhang, Jian-feng; Pan, Sun-qiang; Lin, Xiao-lu; Hu, Peng-bing; Chen, Zhe-min

    2016-01-01

    Resonate frequency and cell constant of photoacoustic spectrum system are usually calibrated by using standard gas in laboratory, whereas the resonate frequency and cell constant will be changed in-situ, leading to measurement accuracy errors, caused by uncertainties of standard gas, differences between standard and measured gas components and changes in environmental condition, such as temperature and humidity. As to overcome the above problems, we have proposed an on-line atmospheric oxygen-based calibration technology for photoacoustic spectrum system and used in measurement of concentration of carbon dioxide in atmosphere. As the concentration of atmospheric oxygen is kept as constant as 20.96%, the on-line calibration for the photoacoustic spectrum system can be realized by detecting the swept-frequency and peak signal at 763.73 nm. The cell of the PAS has a cavity with length of 100 mm and an inner diameter of 6 mm, and worked in a first longitudinal resonant mode. The influence of environmental temperature and humidity, gas components on the photoacoustic cell's performance has been theoretically analyzed, and meanwhile the resonant frequencies and cell constants were calibrated and acquired respectively using standard gas, indoor air and outdoor air. Compared with calibrated gas analyzer, concentration of carbon dioxide is more accurate by using the resonant frequency and cell constant calculated by oxygen in tested air, of which the relative error is less than 1%, much smaller than that calculated by the standard gas in laboratory. The innovation of this paper is that using atmospheric oxygen as photoacoustic spectrum system's calibration gas effectively reduces the error caused by using standard gas and environmental condition changes, and thus improves the on-line measuring accuracy and reliability of the photoacoustic spectrum system.

  14. Vehicle Dynamic Prediction Systems with On-Line Identification of Vehicle Parameters and Road Conditions

    OpenAIRE

    Ling-Yuan Hsu; Tsung-Lin Chen

    2012-01-01

    This paper presents a vehicle dynamics prediction system, which consists of a sensor fusion system and a vehicle parameter identification system. This sensor fusion system can obtain the six degree-of-freedom vehicle dynamics and two road angles without using a vehicle model. The vehicle parameter identification system uses the vehicle dynamics from the sensor fusion system to identify ten vehicle parameters in real time, including vehicle mass, moment of inertial, and road friction coefficie...

  15. ON-LINE PLATFORM FOR COMPETENCES DEVELOPMENT IN CORPORATE EDUCATIONAL SYSTEMS

    Directory of Open Access Journals (Sweden)

    L. G. Andreeva

    2016-01-01

    Full Text Available The aim of the study is to present the model of interaction of university and business corporations in uniform information and educational space, which consists of the uniform requirements to the contents and quality of education and requirements of science; education and business are equally satisfied.Methods. The methods involve summing up the results of the national and international researchers’ findings on the problem of vocational pedagogical education; methods of expert survey and system analysis.Results. The information research results disclosing the drawbacks of the existing online-education technologies are presented. There is also a presentation of online-platform concept «The University of the 3rd Millennium» where modern university is considered as a service provider responsible for corporate education. Outsourcing will allow the companies to cut their expenses on employee education programs, while universities will accumulate additional resources by means of developing and selling innovative educational products. The additional funds will enable the university to carry out scientific research, to effectively implement post graduates’ employment programs, to introduce innovations.Scientific novelty. The authors define «as is» competences, which the university must have to launch this online-platform project, and «as to be» competences, which every university is to master to successfully implement the project. Internal high-risk systemic tensions and external challenges facing the platform are defined; strategic matrix of their intersection is developed. The latter allowed the authors to specify essential tasks which demand solution within the project. There is also a description of interconnection of the defined tasks with the «as to be» competences, and a Canvas model of the suggested online platform.Practical significance: The authors of the article propose the model of business and education interaction, within which

  16. Automated analysis of heterogeneous carbon nanostructures by high-resolution electron microscopy and on-line image processing

    Energy Technology Data Exchange (ETDEWEB)

    Toth, P., E-mail: toth.pal@uni-miskolc.hu [Department of Chemical Engineering, University of Utah, 50 S. Central Campus Drive, Salt Lake City, UT 84112-9203 (United States); Farrer, J.K. [Department of Physics and Astronomy, Brigham Young University, N283 ESC, Provo, UT 84602 (United States); Palotas, A.B. [Department of Combustion Technology and Thermal Energy, University of Miskolc, H3515, Miskolc-Egyetemvaros (Hungary); Lighty, J.S.; Eddings, E.G. [Department of Chemical Engineering, University of Utah, 50 S. Central Campus Drive, Salt Lake City, UT 84112-9203 (United States)

    2013-06-15

    High-resolution electron microscopy is an efficient tool for characterizing heterogeneous nanostructures; however, currently the analysis is a laborious and time-consuming manual process. In order to be able to accurately and robustly quantify heterostructures, one must obtain a statistically high number of micrographs showing images of the appropriate sub-structures. The second step of analysis is usually the application of digital image processing techniques in order to extract meaningful structural descriptors from the acquired images. In this paper it will be shown that by applying on-line image processing and basic machine vision algorithms, it is possible to fully automate the image acquisition step; therefore, the number of acquired images in a given time can be increased drastically without the need for additional human labor. The proposed automation technique works by computing fields of structural descriptors in situ and thus outputs sets of the desired structural descriptors in real-time. The merits of the method are demonstrated by using combustion-generated black carbon samples. - Highlights: ► The HRTEM analysis of heterogeneous nanostructures is a tedious manual process. ► Automatic HRTEM image acquisition and analysis can improve data quantity and quality. ► We propose a method based on on-line image analysis for the automation of HRTEM image acquisition. ► The proposed method is demonstrated using HRTEM images of soot particles.

  17. On line monitoring systems of MIICON Cu-10Ni alloy in brackish water

    Energy Technology Data Exchange (ETDEWEB)

    Romero, M. F. de; Duque, Z.; Rincon, O.T. de; Araujo, I.; Perez, O. [Centro de Estudios de Corrosion. Facultad de Ingenieria. Universidad de Zulia, Venezuela (Venezuela)

    1998-12-31

    The alloy ASTM B-III UNS C70600 (Cu-1ONi) has been extensively used for surface condenser tubes in power stations. However, there have been cases of Microbiologically Induced Corrosion (MIC) in this alloy caused by Sulfate-Reducing Bacteria (SRB). This paper presents the evaluation of Alloy C70600 in a dynamic monitoring system with one-way circulation using brackish water (Lake Maracaibo water) with and without chlorine treatment, for 3,6,8 and 12 months exposure period. The physical-chemical results indicated favorable conditions for microbial development with planktonic SRB present in the order of 107 cell/ml SEM, EDXA, WDX and XRD analysis evidenced organic and inorganic fouling, Cu{sub 2}S (Chalcocite) and Cu{sub 2}O (Cuprite) as the corrosion product and the characteristic MIC onset morphology. The electrochemical tests indicated that the corrosion current increased with the chlorine content (4.0 A/cm{sup 2}/0.0 ppm Cl{sub 2}, 6.0 u A/cm{sup 2}/0.1 ppm Cl{sub 2} and 16.0 A/cm{sup 2}/2.0 ppm Cl{sub 2}). Furthermore, the polarization curves did not show passivation of this alloy. All these results suggest that Alloy C70600 is not resistant to MIC in brackish water even with chlorine treatment. (Author)

  18. Study on On-line Trace Analysis Technique for SG Tube Leakage Monitoring

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Seban; Park, Jongsuk; Kim, Seungil; Jo, Youngsoo; Kang, Dukwon [HaJI Co. Ltd., Radiation Eng. Center, Shihung (Korea, Republic of)

    2014-05-15

    NPPs steam generator leakage monitoring method is mainly adopted in the world. Since this method is using nuclear fission product of certain radionuclides ({sup 16}N, {sup 3}H, Xe, etc.), it is only available when the reactor power is more than 20%. Therefore, it requires alternative techniques of real-time leakage monitoring under a variety of operation conditions such as start-up, abnormal environment of NPPs, etc. Boron which exists mostly nonionic particle state has been weakly ionized, revealing the lowest anionic tendency in aqueous phase (SO{sub 4}{sup 2-}>Cl{sup -}>F{sup -}>SiO{sub 2}{sup -}>HBO{sub 3}{sup -}). In general, B has been titrated with a NaOH solution into a new compound forming a strong alkaline anion after being dissociated with addition of a polyhydric alcohol. And that has been also measured amplified conductivity that reacting directly polyhydric alcohol by conductivity detector. GE (General Electric Company) has applied monitoring equipment of ultrapure water production by using mannitol reagent as polyhydric alcohol, which is detected less than 20 ppb of boron in the semiconductor company. However, the separation of boron among the secondary water system has been regarded as a critical issue because it contains a lot of impurities and particulate materials which are N{sub 2}H{sub 4}, NH{sub 3}, ETA and component of the iron in the system. This study is a follow-up study concerning the separation of boron peak presented at the 2013 Korean Nuclear Society. This study indicates the possibility of analysis of trace-level boron. The study investigated the separation of boron peak with anion through 3-steps mode. In previous studies, the problem of peaks overlap has been solved through the rinse process completely removing the interfering ions presented on the line. The combination of mannitol and MSA was dissociated from the strong compound between boron and a chelating type resin in the CB column. In particular, the CB column will be able to

  19. On-line detection of Escherichia coli intrusion in a pilot-scale drinking water distribution system.

    Science.gov (United States)

    Ikonen, Jenni; Pitkänen, Tarja; Kosse, Pascal; Ciszek, Robert; Kolehmainen, Mikko; Miettinen, Ilkka T

    2017-08-01

    Improvements in microbial drinking water quality monitoring are needed for the better control of drinking water distribution systems and for public health protection. Conventional water quality monitoring programmes are not always able to detect a microbial contamination of drinking water. In the drinking water production chain, in addition to the vulnerability of source waters, the distribution networks are prone to contamination. In this study, a pilot-scale drinking-water distribution network with an on-line monitoring system was utilized for detecting bacterial intrusion. During the experimental Escherichia coli intrusions, the contaminant was measured by applying a set of on-line sensors for electric conductivity (EC), pH, temperature (T), turbidity, UV-absorbance at 254 nm (UVAS SC) and with a device for particle counting. Monitored parameters were compared with the measured E. coli counts using the integral calculations of the detected peaks. EC measurement gave the strongest signal compared with the measured baseline during the E. coli intrusion. Integral calculations showed that the peaks in the EC, pH, T, turbidity and UVAS SC data were detected corresponding to the time predicted. However, the pH and temperature peaks detected were barely above the measured baseline and could easily be mixed with the background noise. The results indicate that on-line monitoring can be utilized for the rapid detection of microbial contaminants in the drinking water distribution system although the peak interpretation has to be performed carefully to avoid being mixed up with normal variations in the measurement data. Copyright © 2017 Elsevier Ltd. All rights reserved.

  20. Computer vision system for on-line sorting of pot plants using artificial Neural Network Classifier

    NARCIS (Netherlands)

    Timmermans, A.J.M.

    1996-01-01

    A flexible grading system for pot plants is described. The system consists of a colour camera, an image processing system and specially developed software. It can be applied to several types of pot plants because of its implementation of learning techniques. Experiments are described for classificat

  1. On the Performance of Three In-Memory Data Systems for On Line Analytical Processing

    Directory of Open Access Journals (Sweden)

    Ionut HRUBARU

    2017-01-01

    Full Text Available In-memory database systems are among the most recent and most promising Big Data technologies, being developed and released either as brand new distributed systems or as extensions of old monolith (centralized database systems. As name suggests, in-memory systems cache all the data into special memory structures. Many are part of the NewSQL strand and target to bridge the gap between OLTP and OLAP into so-called Hybrid Transactional Analytical Systems (HTAP. This paper aims to test the performance of using such type of systems for TPCH analytical workloads. Performance is analyzed in terms of data loading, memory footprint and execution time of the TPCH query set for three in-memory data systems: Oracle, SQL Server and MemSQL. Tests are subsequently deployed on classical on-disk architectures and results compared to in-memory solutions. As in-memory is an enterprise edition feature, associated costs are also considered.

  2. Text-Based On-Line Conferencing: A Conceptual and Empirical Analysis Using a Minimal Prototype.

    Science.gov (United States)

    McCarthy, John C.; And Others

    1993-01-01

    Analyzes requirements for text-based online conferencing through the use of a minimal prototype. Topics discussed include prototyping with a minimal system; text-based communication; the system as a message passer versus the system as a shared data structure; and three exercises that showed how users worked with the prototype. (Contains 61…

  3. On-line ion chemistry for the AMS analysis of {sup 90}Sr and {sup 135,137}Cs

    Energy Technology Data Exchange (ETDEWEB)

    Eliades, J. [IsoTrace Laboratory, University of Toronto, 60 St. George St., Toronto, ON, M5S 1A7 (Canada); Zhao, X.-L. [Department of Physics, University of Ottawa, 150 Louis Pasteur, Ottawa, ON, K1N 6N5 (Canada); Litherland, A.E. [IsoTrace Laboratory, University of Toronto, 60 St. George St., Toronto, ON, M5S 1A7 (Canada); Kieser, W.E., E-mail: liam.kieser@utoronto.ca [Department of Physics, University of Ottawa, 150 Louis Pasteur, Ottawa, ON, K1N 6N5 (Canada)

    2013-01-15

    The analysis of {sup 90}Sr by AMS has so far required the use of very large tandem accelerators in order to separate the isobar {sup 90}Zr by the rate-of-energy-loss method. The analysis of {sup 135,137}Cs by AMS has never been attempted as the separation of the isobars {sup 135,137}Ba by the traditional method requires even higher energies, so that this approach would become prohibitively expensive for routine analysis. Following the successful demonstration of Cl{sup -}-S{sup -} separation by the Isobar Separator, the same apparatus was used to test the separation of other pairs of isobars. Surprisingly effective results were obtained with NO{sub 2} gas in the cases of SrF{sub 3}{sup -}-ZrF{sub 3}{sup -} and CsF{sub 2}{sup -}-BaF{sub 2}{sup -} separations. Reduction factors of {approx}4 Multiplication-Sign 10{sup -6} for ZrF{sub 3}{sup -}/SrF{sub 3}{sup -} and {approx}2 Multiplication-Sign 10{sup -5} for BaF{sub 2}{sup -}/CsF{sub 2}{sup -} were measured. SrF{sub 3}{sup -} and CsF{sub 2}{sup -} are both super-halogen anions and are preferentially produced in the ion source rather than ZrF{sub 3}{sup -} and BaF{sub 2}{sup -} when using the PbF{sub 2} matrix-assisted method. Reduction factors for ion source production with such targets of {approx}3 Multiplication-Sign 10{sup -5} for ZrF{sub 3}{sup -}-SrF{sub 3}{sup -} and {approx}5 Multiplication-Sign 10{sup -4} for BaF{sub 2}{sup -}-CsF{sub 2}{sup -} were found. The combined methods would suggest a theoretical detection sensitivity for {sup 90}Sr/Sr {approx}6 Multiplication-Sign 10{sup -16}, {sup 135}Cs/Cs {approx}7 Multiplication-Sign 10{sup -15} and {sup 137}Cs/Cs {approx}1 Multiplication-Sign 10{sup -14}, assuming 10 ppm Zr and Ba contamination in the AMS targets. In addition to the earlier Cl{sup -}-S{sup -} separation work, these measurements further illustrate the potential of on-line ion chemical methods for broadening the analytical scope of small AMS systems.

  4. An intelligent condition monitoring system for on-line classification of machine tool wear

    Energy Technology Data Exchange (ETDEWEB)

    Fu Pan; Hope, A.D.; Javed, M. [Systems Engineering Faculty, Southampton Institute (United Kingdom)

    1997-12-31

    The development of intelligent tool condition monitoring systems is a necessary requirement for successful automation of manufacturing processes. This presentation introduces a tool wear monitoring system for milling operations. The system utilizes power, force, acoustic emission and vibration sensors to monitor tool condition comprehensively. Features relevant to tool wear are drawn from time and frequency domain signals and a fuzzy pattern recognition technique is applied to combine the multisensor information and provide reliable classification results of tool wear states. (orig.) 10 refs.

  5. On-line experimental results of an argon gas cell-based laser ion source (KEK Isotope Separation System)

    Science.gov (United States)

    Hirayama, Y.; Watanabe, Y. X.; Imai, N.; Ishiyama, H.; Jeong, S. C.; Jung, H. S.; Miyatake, H.; Oyaizu, M.; Kimura, S.; Mukai, M.; Kim, Y. H.; Sonoda, T.; Wada, M.; Huyse, M.; Kudryavtsev, Yu.; Van Duppen, P.

    2016-06-01

    KEK Isotope Separation System (KISS) has been developed at RIKEN to produce neutron rich isotopes with N = 126 to study the β -decay properties for application to astrophysics. The KISS is an element-selective mass-separation system which consists of an argon gas cell-based on laser ion source for atomic number selection and an ISOL mass-separation system. The argon gas cell of KISS is a key component to stop and collect the unstable nuclei produced in a multi-nucleon transfer reaction, where the isotopes of interest will be selectively ionized using laser resonance ionization. We have performed off- and on-line experiments to study the basic properties of the gas cell as well as of the KISS. We successfully extracted the laser-ionized stable 56Fe (direct implantation of a 56Fe beam into the gas cell) atoms and 198Pt (emitted from the 198Pt target by elastic scattering with a 136Xe beam) atoms from the KISS during the commissioning on-line experiments. We furthermore extracted laser-ionized unstable 199Pt atoms and confirmed that the measured half-life was in good agreement with the reported value.

  6. On-line integration of computer controlled diagnostic devices and medical information systems in undergraduate medical physics education for physicians.

    Science.gov (United States)

    Hanus, Josef; Nosek, Tomas; Zahora, Jiri; Bezrouk, Ales; Masin, Vladimir

    2013-01-01

    We designed and evaluated an innovative computer-aided-learning environment based on the on-line integration of computer controlled medical diagnostic devices and a medical information system for use in the preclinical medical physics education of medical students. Our learning system simulates the actual clinical environment in a hospital or primary care unit. It uses a commercial medical information system for on-line storage and processing of clinical type data acquired during physics laboratory classes. Every student adopts two roles, the role of 'patient' and the role of 'physician'. As a 'physician' the student operates the medical devices to clinically assess 'patient' colleagues and records all results in an electronic 'patient' record. We also introduced an innovative approach to the use of supportive education materials, based on the methods of adaptive e-learning. A survey of student feedback is included and statistically evaluated. The results from the student feedback confirm the positive response of the latter to this novel implementation of medical physics and informatics in preclinical education. This approach not only significantly improves learning of medical physics and informatics skills but has the added advantage that it facilitates students' transition from preclinical to clinical subjects.

  7. On-line surveillance of a dynamic process by a moving system based on pulsed digital holographic interferometry.

    Science.gov (United States)

    Pedrini, Giancarlo; Alexeenko, Igor; Osten, Wolfgang; Schnars, Ulf

    2006-02-10

    A method based on pulsed digital holographic interferometry for the measurement of dynamic deformations of a surface by using a moving system is presented. The measuring system may move with a speed of several meters per minute and can measure deformation of the surface with an accuracy of better than 50 nm. The deformation is obtained by comparison of the wavefronts recorded at different times with different laser pulses produced by a Nd:YAG laser. The effect due to the movement of the measuring system is compensated for by digital processing of the different holograms. The system is well suited for on-line surveillance of a dynamic process such as laser welding and friction stir welding. Experimental results are presented, and the advantages of the method are discussed.

  8. On-Line Investment Analysis and Portfolio Management: Using Learning Outcome Statements To Design Projects.

    Science.gov (United States)

    Pettijohn, James B.; Ragan, Gay A.; Ragan, Kent P.

    2003-01-01

    Describes an Internet-based project to familiarize students with online investment analysis and stock portfolio management. Outlines a process for writing learning outcomes that address three levels of cognition: knowledge/comprehension, application/analysis, and synthesis/evaluation. (SK)

  9. On-Line Investment Analysis and Portfolio Management: Using Learning Outcome Statements To Design Projects.

    Science.gov (United States)

    Pettijohn, James B.; Ragan, Gay A.; Ragan, Kent P.

    2003-01-01

    Describes an Internet-based project to familiarize students with online investment analysis and stock portfolio management. Outlines a process for writing learning outcomes that address three levels of cognition: knowledge/comprehension, application/analysis, and synthesis/evaluation. (SK)

  10. On-Line Approximation Control of Uncertain Nonlinear Systems: Issues With Control Input Saturation

    Science.gov (United States)

    2005-01-01

    stability properties of the proposed feedback control law are obtained via Lyapunov analysis. Particular emphasis is given to aircraft longitudinal control, which extends the results to the backstepping feedback control procedure.

  11. SIDOL – Sistema de Identificação Dendrológica On-line / SIDOL - On-line Dendrologic Identification System

    Directory of Open Access Journals (Sweden)

    Daniel Saueressig

    2009-04-01

    Full Text Available ResumoApresenta-se um sistema informatizado, com uso via Internet, objetivando facilitar e agilizar o processo de identificação das espécies arbóreas e principais arbustos encontrados no Campus Universitário de Irati (UNICENTRO, que tem como base a combinação de características macromorfológicas informadas pelo usuário. O sistema de consulta, apresentado em modo formulário, é dinâmico. Os passos do usuário são guiados e as ações informadas, facilitando o entendimento e a interação com o sistema. Após a entrada das informações, o sistema consulta as tabelas do banco de dados em busca de resultados. Os resultados da busca, caso haja registro, são exibidas ao usuário, que não precisa ter conhecimento técnico para operar o sistema. Associado à criação do sistema foi realizado o estudo florístico do Campus, que mostrou a presença de 127 espécies pertencentes a 92 gêneros e 46 famílias. As famílias Myrtaceae (19 espécies, Fabaceae (15, Lauraceae (9, Asteraceae (7, Salicaceae (6 e Aquifoliaceae, Euphorbiaceae, Rosaceae e Solanaceae (5, apresentaram uma maior riqueza florística e juntas representam 59,84% das espécies catalogadas. Os gêneros mais ricos foram Ilex (5 espécies, Eugenia e Casearia (4 e Cinnamomum, Zanthoxylum, Ocotea e Myrcia (3.AbstractA virtual system supported by Internet is presented in order to facilitate and accelerate identification of trees and shrubs growing at the University Campus in Irati, Paraná State, Brazil (UNICENTRO - Universidade Estadual do Centro-Oeste. The system key is the combination of macromorphological characteristics informed by the user. The search system is dynamic and is presented in a chart format. User steps are guided and actions are informed in order to facilitate understanding and interaction with the system. After the information input, the system searches results in the data bank. When the input matches an existing record, the system displays the stored

  12. An adaptive linear combiner for on-line tracking of power system harmonics

    Energy Technology Data Exchange (ETDEWEB)

    Dash, P.K.; Swain, D.P. [Regional Engineering Coll., Rourkela (India). Dept. of Electrical Engineering; Liew, A.C. [National Univ. of Singapore (Singapore). Dept. of Electrical Engineering; Rahman, S. [Virginia Polytechnic Inst. and State Univ., VA (United States). Dept. of Electrical Engineering

    1996-11-01

    The paper presents a new approach for the estimation of harmonic components of a power system using a linear adaptive neuron called Adaline. The learning parameters in the proposed neural estimation algorithm are adjusted to force the error between the actual and desired outputs to satisfy a stable difference error equation. The estimator tracks the Fourier coefficients of the signal data corrupted with noise and decaying dc components very accurately. Adaptive tracking of harmonic components of a power system can easily be done using this algorithm. Several numerical tests have been conducted for the adaptive estimation of harmonic components of power system signals mixed with noise and decaying dc components.

  13. The on-line analysis of aerosol-delivered pharmaceuticals via single particle aerosol mass spectrometry.

    Science.gov (United States)

    Morrical, Bradley D; Balaxi, Maria; Fergenson, David

    2015-07-15

    The use of single particle aerosol mass spectrometry (SPAMS) was evaluated for the analysis of inhaled pharmaceuticals to determine the mass distribution of the individual active pharmaceutical ingredients (API) in both single ingredient and combination drug products. SPAMS is an analytical technique where the individual aerodynamic diameters and chemical compositions of many aerosol particles are determined in real-time. The analysis was performed using a Livermore Instruments SPAMS 3.0, which allowed the efficient analysis of aerosol particles with broad size distributions and can acquire data even under a very large particle load. Data similar to what would normally require roughly three days of experimentation and analysis was collected in a five minute period and analyzed automatically. The results were computed to be comparable to those returned by a typical Next Generation Impactor (NGI) particle size distribution experiment.

  14. Analysis of acrylamide in food products by microchip electrophoresis with on-line multiple-preconcentration techniques.

    Science.gov (United States)

    Wu, Minglei; Chen, Wujuan; Wang, Guan; He, Pingang; Wang, Qingjiang

    2016-10-15

    In this paper, a microchip electrophoresis method based on on-line multiple-preconcentration techniques combining field-amplified sample stacking and reversed-field stacking was developed for highly efficient analysis of acrylamide in food products. The related mechanism as well as important parameters governing separation and preconcentration have been investigated in order to obtain maximum resolution and sensitivity. The best separation was achieved using a 100mM borate solution at pH 9.3 as running buffer, and a sensitivity enhancement factor of 432 was obtained using this concentration method under optimal conditions. The detection limit of acrylamide was 1ng/mL, which was comparable to those previously obtained using CE methods with on-line preconcentration techniques and was 41-700 times lower than those previously reported CE methods without concentration process. The proposed method also gave satisfactory and reliable results in the analysis of acrylamide in potato chips and French fries. Copyright © 2016 Elsevier Ltd. All rights reserved.

  15. On-line controlling system for nitrogen and phosphorus removal of municipal wastewater in a sequencing batch reactor (SBR)

    Institute of Scientific and Technical Information of China (English)

    Jun LI; Yongjiong NI; Yongzhen PENG; Guowei GU; Jingen LU; Su WEI; Guobiao CHENG; Changjin OU

    2008-01-01

    The objectives of this study were to establish an on-line controlling system for nitrogen and phosphorus removal synchronously of municipal wastewater in a sequencing batch reactor (SBR). The SBR for municipal wastewater treatment was operated in sequences: filling, anaerobic, oxic, anoxic, oxic, settling and discharge. The reactor was equipped with on-line monitoring sensors for dissolved oxygen (DO), oxidation-reduction potential (ORP) and pH. The variation of DO, ORP and pH is relevant to each phase of biological process for nitrogen and phosphorus removal in this SBR. The characteristic points of DO, ORP and pH can be used to judge and control the stages of process that include: phosphate release by the turning points of ORP and pH; nitrification by the ammonia valley of pH and ammonia elbows of DO and ORP; denitrification by the nitrate knee of ORP and nitrate apex ofpH; phosphate uptake by the turning point ofpH; and residual organic carbon oxida-tion by the carbon elbows of DO and ORP. The controlling system can operate automatically for nitrogen and phosphorus efficiently removal.

  16. The NASA Astrophysics Data System Free Access to the Astronomical Literature On-Line and through Email

    CERN Document Server

    Eichhorn, G; Grant, C S; Kurtz, M J; Murray, S S

    2001-01-01

    The Astrophysics Data System (ADS) provides access to the astronomical literature through the World Wide Web. It is a NASA funded project and access to all the ADS services is free to everybody world-wide.The ADS Abstract Service allows the searching of four databases with abstracts in Astronomy, Instrumentation, Physics/Geophysics, and the LANL Preprints with a total of over 2.2 million references. The system also provides access to reference and citation information, links to on-line data, electronic journal articles, and other on-line information. The ADS Article Service contains the articles for most of the astronomical literature back to volume 1. It contains the scanned pages of all the major journals (Astrophysical Journal, Astronomical Journal, Astronomy & Astrophysics, Monthly Notices of the Royal Astronomical Society, and Solar Physics), as well as most smaller journals back to volume 1. The ADS can be accessed through any web browser without signup or login. Alternatively an email interface is ...

  17. Design of an on-line measuring system for 0.14 THz high-power terahertz pulse

    Energy Technology Data Exchange (ETDEWEB)

    Wang Guangqiang [Department of Engineering Physics, Tsinghua University, Beijing 100084 (China); Wang Jianguo; Li Xiaoze; Tong Changjiang; Wang Xuefeng, E-mail: wgq02@mails.tsinghua.edu.cn [Northwest Institute of Nuclear Technology, Xi' an 710024 (China)

    2011-02-01

    An on-line measuring system, including an aperture-coupling structure and a novel high-power pulse detector, is proposed in this paper to measure the output pulses from high-power 0.14THz surface wave oscillator (SWO). At first a T-type coupling structure between the TM{sub 01} mode of circular waveguide with radius of 6mm and TE{sub 10} mode of rectangular waveguide WR6 is designed. Based on loose coupling theory,the coupling degree of this structure is derived and calculated, reaching about -47dB with the aperture radius of 0.4mm and length of 0.5mm. The reasonable coincidence is found between the theoretical computation and numerical simulation employing the three-dimensional finite difference time domain method. Then a novel high-power terahertz pulse detector based on hot electron effect in semiconductors is developed for the detection of output pulses from T-type coupling structure. With hot electron theory, the working principle of the detector is elucidated, also its sensitivity is simply analyzed, showing that this detector is capable of handling the pulse power as high as 2kW. The present 0.14THz on-line measuring system would be convenient to monitor the terahertz pulse shape and pulse power during the application researches of SWO besides increasing the accuracy of its pulse power measurement.

  18. On-Line GIS Analysis and Image Processing for Geoportal Kielce/poland Development

    Science.gov (United States)

    Hejmanowska, B.; Głowienka, E.; Florek-Paszkowski, R.

    2016-06-01

    GIS databases are widely available on the Internet, but mainly for visualization with limited functionality; very simple queries are possible i.e. attribute query, coordinate readout, line and area measurements or pathfinder. A little more complex analysis (i.e. buffering or intersection) are rare offered. Paper aims at the concept of Geoportal functionality development in the field of GIS analysis. Multi-Criteria Evaluation (MCE) is planned to be implemented in web application. OGC Service is used for data acquisition from the server and results visualization. Advanced GIS analysis is planned in PostGIS and Python programming. In the paper an example of MCE analysis basing on Geoportal Kielce is presented. Other field where Geoportal can be developed is implementation of processing new available satellite images free of charge (Sentinel-2, Landsat 8, ASTER, WV-2). Now we are witnessing a revolution in access to the satellite imagery without charge. This should result in an increase of interest in the use of these data in various fields by a larger number of users, not necessarily specialists in remote sensing. Therefore, it seems reasonable to expand the functionality of Internet's tools for data processing by non-specialists, by automating data collection and prepared predefined analysis.

  19. Functional design standard of on-line digital core protection and monitoring systems for SMART

    Energy Technology Data Exchange (ETDEWEB)

    In, Wang Kee; Kim, Keung Koo; Zee, Sung Qunn [Korea Atomic Energy Research Institute, Taejon (Korea)

    1999-12-01

    The general requirements for the system I/O and the functional design were developed based on the conceptual design of SCOPS and SCOMS for SMART. The reactor trip functions were preliminarily determined to define the design basis events of SCOPS. The sensor requirements for SCOPS and SCOMS were also established. The sensor requirements for SCOPS and SCOMS were also established. The detailed functional design of the SMART digital core protection and monitoring systems will be performed based on the functional design standard in this report. The results of this study will also be useful to determine the reactor trip functions as well as the system and sensor requirements. 3 refs., 2 figs., 5 tabs. (Author)

  20. One to One Recommendation System in Apparel On-Line Shopping

    Science.gov (United States)

    Sekozawa, Teruji; Mitsuhashi, Hiroyuki; Ozawa, Yukio

    We propose an apparel online shopping site that the fashion adviser exists on the internet. The fashion adviser, who has detailed knowledge about the fashion in real shop, selects and coordinates the clothes of the customer's preference. However, the customer, who didn't have detailed knowledge about the fashion, was not able to choose the clothes suitable for the customer's preference from among the candidate of a large amount of clothes on a conventional apparel shopping site. Then, we compose the system that analyzes the customer's preference by the AHP technique, makes to the cluster by the correlation of clothes, and analyzes the market basket. As a result, this system can coordinate the clothes appropriate for the favor of an individual customer. Moreover, this system can propose the recommendation of other clothes based on past sales data.

  1. Transonic Compressor: Program System TXCO for Data Acquisition and On-Line Reduction.

    Science.gov (United States)

    1980-10-01

    8217A’ - ’B’ REDAB probe system. REDAB uses the data gathered by ABSRV. 10. Reduce flow data from the combination probe. REDCO REDCO uses the data... REDCO - T5rrss COMB VARIABLES: All variables, their type (REAL or INTEGER) and length (only if the variable is used as an array), together with a...probe system0054 * "tiX"rWEDAB/ 0055 "-T-- Reduce data from the combination probe ൝V" 005 I REDCO 𔃺- 0Ub7 i 1 Reduce steady state data ൫X" REDST

  2. Research on On-line detection system for natural gas pipeline

    Institute of Scientific and Technical Information of China (English)

    Zuo Jianyong; Yan Guozheng; Ding Guoqing; Fu Xiguang; Zhang Yunwei

    2005-01-01

    Four methods for testing the thickness and defect of pipeline are compared and analyzed in this paper. The testing principle of magnetic leakage flux based on electromagnetism is discussed in detail. From the experiments of sensor character, the effects caused by some factors are found, which give some important information for sensor design, and this method is proved reasonable and effective. The mechanical and electrical structures of inspection equipment, as well as its working principle and technical features are introduced. In this paper, control flow and software design are discussed, too. This detection system has been successfully developed. Experiments show that this detection system has high resolution and can be put into practice.

  3. On-Line Real-Time Management Information Systems and Their Impact Upon User Personnel and Organizational Structure in Aviation Maintenance Activities.

    Science.gov (United States)

    1979-12-01

    AD-AO85 III NAVAL POSTGRADUATE SCHOOL MONTEREY CA F/6 15/7 ON-LINE REAL- TIME MANAGEMENT INFORMATION SYSTEMS AND THEIR IMPA--ETC(U) UNCLASSIIED N...34&’ 1111CIPENT’S CAT ALOG NUMS9m 14. TITLE (11141 ANIN~e. ON-LINE REAL- TIME MANAGEMENT INFORMATION Master’s Thesis SYSTEMS AND THEIR IMPACT UPON USER PER- p...9.GOO*g e,ft Or too#$ pasemabin. &-we. Approved for Public Release; Ditribution Unlimited ON-LINE REAL- TIME MANAGEMENT INFORMATION SYSTEMS AND THEIR

  4. 76 FR 7102 - Simplified Network Application Processing System, On-line Registration and Account Maintenance

    Science.gov (United States)

    2011-02-09

    ... Regulatory Flexibility, Small Business, and Job Creation (January 18, 2011). DATES: Effective date: March 11... 12866 and Presidential Memorandum on Regulatory Flexibility, Small Business, and Job Creation (January... CIV. (b) Registration and use of BIS's Simplified Network Applications System--Redesign...

  5. An on-line image data base system: Managing image collections

    Science.gov (United States)

    Malchus B. Baker; Daniel P. Huebner; Peter F. Ffolliott

    2000-01-01

    Many researchers and land management personnel want photographic records of the phases of their studies or projects. Depending on the personnel and the type of project, a study can result in a few or hundreds of photographic images. A data base system allows users to query using various parameters, such as key words, dates, and project locations, and to view images...

  6. On-line monitoring of Glucose and penicillin by sequential injection analysis

    DEFF Research Database (Denmark)

    Min, R.W.; Nielsen, Jens Bredal; Villadsen, John

    1996-01-01

    and a detector. The glucose analyzer is based on an enzymatic reaction using glucose oxidase, which converts glucose to glucono-lactone with formation of hydrogen peroxide and subsequent detection of H2O2 by a chemiluminescence reaction involving luminol. The penicillin analysis is based on formation...

  7. An on-line calibration algorithm for external parameters of visual system based on binocular stereo cameras

    Science.gov (United States)

    Wang, Liqiang; Liu, Zhen; Zhang, Zhonghua

    2014-11-01

    Stereo vision is the key in the visual measurement, robot vision, and autonomous navigation. Before performing the system of stereo vision, it needs to calibrate the intrinsic parameters for each camera and the external parameters of the system. In engineering, the intrinsic parameters remain unchanged after calibrating cameras, and the positional relationship between the cameras could be changed because of vibration, knocks and pressures in the vicinity of the railway or motor workshops. Especially for large baselines, even minute changes in translation or rotation can affect the epipolar geometry and scene triangulation to such a degree that visual system becomes disabled. A technology including both real-time examination and on-line recalibration for the external parameters of stereo system becomes particularly important. This paper presents an on-line method for checking and recalibrating the positional relationship between stereo cameras. In epipolar geometry, the external parameters of cameras can be obtained by factorization of the fundamental matrix. Thus, it offers a method to calculate the external camera parameters without any special targets. If the intrinsic camera parameters are known, the external parameters of system can be calculated via a number of random matched points. The process is: (i) estimating the fundamental matrix via the feature point correspondences; (ii) computing the essential matrix from the fundamental matrix; (iii) obtaining the external parameters by decomposition of the essential matrix. In the step of computing the fundamental matrix, the traditional methods are sensitive to noise and cannot ensure the estimation accuracy. We consider the feature distribution situation in the actual scene images and introduce a regional weighted normalization algorithm to improve accuracy of the fundamental matrix estimation. In contrast to traditional algorithms, experiments on simulated data prove that the method improves estimation

  8. On-line Configuration of Network Emulator for Intelligent Energy System Testbed Applications

    DEFF Research Database (Denmark)

    Kemal, Mohammed Seifu; Iov, Florin; Olsen, Rasmus Løvenstein

    2015-01-01

    Intelligent energy networks (or Smart Grids) provide efficient solutions for a grid integrated with near-real-time communication technologies between various grid assets in power generation, transmission and distribution systems. The design of a communication network associated with intelligent......-operable and resilient Smart Grid networks and how the current state of the art communication technologies are employed for smart control of energy distribution grids....

  9. Monitoring on-line system for the lactic fermentation measurement using the integration enzyme sensor; Shusekika koso sensa wo mochiita nyusan hakko keisokuyo onrain monitringu shisutemu

    Energy Technology Data Exchange (ETDEWEB)

    Suzuki, Masayasu; Kumagaya, Tsuyoshi; Nakajima, Yoichi [Kyushu Institute of Technology, Fukuoka (Japan)

    1999-04-05

    The monitoring on-line system for the lactic fermentation measurement in which the simultaneous measurement of the substrate. Generation was possible was constructed without consuming the culture medium by using soliciting small enzyme sensor and flow injection analysis system integrate. There was the linearity that anyway was also range of concentration of 70mM or less and that it is good on the calibration curve of minute glucose, lactose, and lactic acid sensor. It became clear that it proved that all range of concentration of the substrate of these three which combining with the micro diary system, breaks in the lactic fermentation measurement with the necessity can be measured and not observe the interference by medium components, etc. either. Constructed monitoring on-line system is Lactobacillus delbrueckii and, it was applied to the lactic fermentation process of Lactobacillus lactis. Through the fermentation process for 24 hours, simultaneous measurement of glucose (or lactose) and lactic acid is possible. The measured value agreed well with the result of colorimetric method using the enzyme. (translated by NEDO)

  10. On-line core monitoring system based on buckling corrected modified one group model

    Energy Technology Data Exchange (ETDEWEB)

    Freire, Fernando S., E-mail: freire@eletronuclear.gov.br [ELETROBRAS Eletronuclear Gerencia de Combustivel Nuclear, Rio de Janeiro, RJ (Brazil)

    2011-07-01

    Nuclear power reactors require core monitoring during plant operation. To provide safe, clean and reliable core continuously evaluate core conditions. Currently, the reactor core monitoring process is carried out by nuclear code systems that together with data from plant instrumentation, such as, thermocouples, ex-core detectors and fixed or moveable In-core detectors, can easily predict and monitor a variety of plant conditions. Typically, the standard nodal methods can be found on the heart of such nuclear monitoring code systems. However, standard nodal methods require large computer running times when compared with standards course-mesh finite difference schemes. Unfortunately, classic finite-difference models require a fine mesh reactor core representation. To override this unlikely model characteristic we can usually use the classic modified one group model to take some account for the main core neutronic behavior. In this model a course-mesh core representation can be easily evaluated with a crude treatment of thermal neutrons leakage. In this work, an improvement made on classic modified one group model based on a buckling thermal correction was used to obtain a fast, accurate and reliable core monitoring system methodology for future applications, providing a powerful tool for core monitoring process. (author)

  11. Monosaccharide composition analysis of immunomodulatory polysaccharides by on-line hollow fiber microextraction with high-performance liquid chromatography.

    Science.gov (United States)

    Wang, Nani; Wang, Xuping; Huang, Xiaowen; Mao, Zhujun; Zhang, Yang; Yu, Yong; Shou, Dan

    2016-03-01

    The monosaccharide compositions of functional polysaccharides are essential for structure elucidation and biological activity determination. A sensitive method based on on-line hollow-fiber liquid-phase microextraction with high-performance liquid chromatography has been established for the analysis of ten monosaccharide compositions (two uronic acids, two amino sugars and six neutral sugars) of the immunomodulatory polysaccharides. After derivatization, the sample was injected into the lumen of a hollow fiber immersed in butyl ether and separated by liquid chromatography. Under optimized conditions, the calibration curves were linear (r ≥ 0.9996) in the range of 10-2000 μmol L(-1) . The limits of detection were in the range of 0.04-1.58 μmol L(-1) , and the recoveries were in the range of 92.1-99.6%, which shows that the method is applicable to the analysis of the monosaccharide composition of various polysaccharides.

  12. 活化法测量中子活化在线分析系统样品处的中子能谱%Neutron Spectrum Measurement with Activation Method in Sample Place of On-line Neutron Activation Analysis System

    Institute of Scientific and Technical Information of China (English)

    王松林; 孔祥忠; 邓勇军; 拓飞; 王琦; 位金锋; 李永明

    2009-01-01

    用多箔活化法测定了由Am-Be中子源慢化屏蔽系统构成的中子活化在线分析系统样品处的中子能谱.根据待测场点的中子注量率水平,选用了5种非裂变核材料箔,其中4种是中能区和热区的,1种是快区的,给出了各箔片的特性参数.通过在待测场点对箔片进行辐照,并测量其生成放射性核的γ放射性,计算出了各箔片的活化率.运用SAND-II和MSIT迭代方法,解出了待测场点的中子能谱.详细分析了数据处理过程中群截面的加工处理以及由于自屏蔽效应引起的群截面修正问题;研究了影响解谱精度的主要因素;对解谱结果作了一定的分析讨论;并用蒙特卡罗(MC)方法对最后的中子能谱做了不确定度分析.%The neutron spectrum in sample place of on-line neutron activation analysis system was measured with multiple foil activation technique. According to the neutron fluence level of measuring request, 5 kinds of non-fission nuclear material foils were selected, of which 4 were sensitive to thermal energy region and intermediate energy region, and 1 was sensitive to fast energy region. By measuring the foil activity, the neutron spectrum that was needed to measured was unfolded with the iterative methods SAND-II and MSIT. Meanwhile, the process of producing and modifying group cross section were analysed amply. The main factors which have influence on the accuracy of the solution were studied. The discussion for solution was done simply, and the uncertainty of solution was analysed by using the Monte Carlo method.

  13. The control system of the CERN-ISOLDE on-line mass-separator facility

    Energy Technology Data Exchange (ETDEWEB)

    Jonsson, O.C.; Bret, A.; Catherall, R.; Deloose, I.; Focker, G.J.; Forkel, D.; Kugler, E.; Olesen, G.; Pace, A.; Ravn, H.L.; Shering, G.; Tengblad, O. (CERN, Geneva (Switzerland)); Borch, O. (Aalborg Univ. (Denmark). Inst. of Electronic Systems); Richard-Serre, C. (IN2P3, 75 - Paris (France)); Torgersen, H.J. (Oslo Univ. (Norway). Dept. of Chemistry); ISOLDE Collaboration

    1992-08-01

    With the move of the ISOLDE facility to the PS-Booster from the now closed Synchro-Cyclotron at CERN, a new control system will be implented for the two separators. Personal computers, based on the Intel 80386 microprocessor running under MS-DOS and Microsoft Windows, are used. Network-wide distributed front end computers, which access the hardware for controls and measurements, are controlled by PC-consoles via a local area network with a PC file server used as a database. (orig.).

  14. The control system of the CERN-ISOLDE on-line mass-separator facility

    Science.gov (United States)

    Jonsson, O. C.; Borch, O.; Bret, A.; Catherall, R.; Deloose, I.; Focker, G. J.; Forkel, D.; Kugler, E.; Olesen, G.; Pace, A.; Ravn, H. L.; Richard-Serre, C.; Shering, G.; Tengblad, O.; Torgersen, H. J.; Isolde Collaboration

    1992-08-01

    With the move of the ISOLDE facility to the PS-Booster from the now closed Synchro-Cyclotron at CERN, a new control system will be implemented for the two separators. Personal computers, based on the Intel 80386 microprocessor running under MS-DOS and Microsoft Windows, are used. Network-wide distributed front end computers, which access the hardware for controls and measurements, are controlled by PC-consoles via a local area network with a PC file server used as a database.

  15. Utilization of on-line corrosion monitoring in the flue gas cleaning system

    DEFF Research Database (Denmark)

    Montgomery, Melanie; Nielsen, Lars V.; Petersen, Michael B.

    2015-01-01

    The power plant unit 1 at Amager, Denmark is a 350 MWth multifuel suspension-fired plant commissioned in 2009 which uses biomass. Increasing corrosion problems in the flue gas cleaning system have been observed since 2011 in both the gas-gas preheater and the booster fan and booster fan duct...... fan. The corrosion rates measured with respect to time were correlated to plant data such as load, temperature, gas composition, water content as well as change in the fuel used. From these results it is clear that many shutdowns/start-ups influence corrosion and therefore cause decreased lifetime...

  16. A novel system for continuous protein refolding and on-line capture by expanded bed adsorption

    DEFF Research Database (Denmark)

    Ferré, Henrik; Ruffet, E; Nielsen, L.L.B;

    2005-01-01

    -h beta(2)m) both at analytical, small, and preparative scale. In a single scalable operation, extracted and denatured inclusion body proteins from Escherichia coli were continuously diluted into refolding buffer, using a short pipe reactor, allowing for a defined retention and refolding time...... to be controlled and maintained throughout the process, irrespective of the batch size; i.e., it is readily scalable. Furthermore, the procedure is fast and tolerant toward aggregate formation, a common complication of in vitro protein refolding. In conclusion, this system represents a novel approach to small...

  17. On-line Alert Systems for Production Plants: A Conflict Based Approach

    DEFF Research Database (Denmark)

    Nielsen, Thomas Dyhre; Jensen, Finn V.

    2007-01-01

    system operation. Faults are detected by measuring the conflict between the model and the sensor readings, and knowledge about the possible faults is therefore not required. We illustrate the proposed method using real-world data from a coal driven power plant as well as simulated data from an oil......We present a new methodology for detecting faults and abnormal behavior in production plants. The methodology stems from a joint project with a Danish energy consortium. During the course of the project we encountered several problems that we believe are common for projects of this type. Most...

  18. Aging in biometrics: an experimental analysis on on-line signature.

    Directory of Open Access Journals (Sweden)

    Javier Galbally

    Full Text Available The first consistent and reproducible evaluation of the effect of aging on dynamic signature is reported. Experiments are carried out on a database generated from two previous datasets which were acquired, under very similar conditions, in 6 sessions distributed in a 15-month time span. Three different systems, representing the current most popular approaches in signature recognition, are used in the experiments, proving the degradation suffered by this trait with the passing of time. Several template update strategies are also studied as possible measures to reduce the impact of aging on the system's performance. Different results regarding the way in which signatures tend to change with time, and their most and least stable features, are also given.

  19. Aging in biometrics: an experimental analysis on on-line signature.

    Science.gov (United States)

    Galbally, Javier; Martinez-Diaz, Marcos; Fierrez, Julian

    2013-01-01

    The first consistent and reproducible evaluation of the effect of aging on dynamic signature is reported. Experiments are carried out on a database generated from two previous datasets which were acquired, under very similar conditions, in 6 sessions distributed in a 15-month time span. Three different systems, representing the current most popular approaches in signature recognition, are used in the experiments, proving the degradation suffered by this trait with the passing of time. Several template update strategies are also studied as possible measures to reduce the impact of aging on the system's performance. Different results regarding the way in which signatures tend to change with time, and their most and least stable features, are also given.

  20. System for on-line 3D measurement of rough natural surfaces

    Science.gov (United States)

    Paar, Gerhard; Poelzleitner, Wolfgang; Bauer, A.

    1995-09-01

    3D reconstruction of highly textured surfaces like those found in roads, as well as unvegetated (rock-like) terrain is of major interest for applications like autonomous navigation, or the 3D modeling of terrain for mapping purposes. We describe a system for automatic modeling of such scenes. It is based on two frame CCD cameras, which are tightly attached to eachother to ensure constant relative orientation. One camera is used for the acquisition of photogrammetrically measure reference points, the other records the surface images. The system is moved from the first position to the next by an operator carrying it. Automatic calibration using the images acquired by the calibration camera permits the computation of exterior orientation parameters of the surface camera. A fast matching method providing dense disparities together with a robust reconstruction algorithm renders an accurate grid of 3D points. We also describe procedures to merge stereo reconstruction results from all images taken, and report on accuracy, computational complexity, and practical experience in a road engineering application.

  1. New on-line method for water isotope analysis of speleothem fluid inclusions using laser absorption spectroscopy (WS-CRDS)

    Science.gov (United States)

    Affolter, S.; Fleitmann, D.; Leuenberger, M.

    2014-01-01

    A new online method to analyse water isotopes of speleothem fluid inclusions using a wavelength scanned cavity ring down spectroscopy (WS-CRDS) instrument is presented. This novel technique allows us to simultaneously measure hydrogen and oxygen isotopes for a released aliquot of water. To do so, we designed a new simple line that allows the on-line water extraction and isotope analysis of speleothem samples. The specificity of the method lies in the fact that fluid inclusions release is made on a standard water background, which mainly improves the δD reliability. To saturate the line, a peristaltic pump continuously injects standard water into the line that is permanently heated to 140 °C and flushed with dry nitrogen gas. This permits instantaneous and complete vaporisation of the standard water resulting in an artificial water background with well-known δD and δ18O values. The speleothem sample is placed into a copper tube, attached to the line and after system stabilisation is crushed using a simple hydraulic device to liberate speleothem fluid inclusions water. The released water is carried by the nitrogen/standard water gas stream directly to a Picarro L1102-i for isotope determination. To test the accuracy and reproducibility of the line and to measure standard water during speleothem measurements a syringe injection unit was added to the line. Peak evaluation is done similarly as in gas chromatography to obtain δD and δ18O isotopic composition of measured water aliquots. Precision is better than 1.5‰ for δD and 0.4‰ for δ18O for water measurement for an extended range (-210 to 0‰ for δD and -27 to 0‰ for δ18O) primarily dependent on the amount of water released from speleothem fluid inclusions and secondarily on the isotopic composition of the sample. The results show that WS-CRDS technology is suitable for speleothem fluid inclusion measurements and gives results that are comparable to Isotope Ratio Mass Spectrometry (IRMS) technique.

  2. On-line Chip based 2D RP/RP LC-MS/MS Method for Proteomic Analysis

    Science.gov (United States)

    Hunter, Christie; Albanese, Jenny; van Soest, Remco; Zhu, Xiang

    2013-01-01

    Two-dimensional (2D) liquid chromatography is widely used for proteome identification and quantification using the advantage of increasing peak capacity. Herein, we developed an simplified chip based 2D-LC workflow using a high pH/RP first dimensional separation and low pH/RP secondary dimension coupled to mass spectrometer for proteomic analysis. The 2D LC separation was performed using ekspert™ nanoLC 425(Eksigent, part of AB SCIEX) system. Digested E. coli cell lysates were first loaded onto a 200μm × 15cm C18 column at pH 9.8 with a flowrate of 1 μL/min. Step gradient was used to sequentially elute peptide fractions, which were diluted to pH 2.5 before being captured by a 200μm × 6mm C18 chip trap column. Each fraction was then separated with a 75 μm × 15cm C18 chip column at 300 nL/min and analyzed with TripleTOF® 5600 (AB SCIEX). Data was processed with ProteinPilot™ Software (AB SCIEX). The preliminary result suggested the on-line 2D RP-RP method as an easy and competitive approach for proteome discovery. The comparison experiments of 1D, 2D-6 fraction and 2D-10 fraction were performed. Using ∼1ug of E. coli digested cell lysates, there are 1.8× and 2.1× increase in the identification numbers for 2D-6 and 2D-10 fractions versus the 1D configuration at the peptide level (5% local FDR). The other advantage of 2D workflow is the larger sample loading capacities on the column. When the loading amount was increased by 10×, the number of detected peptides increased by 3.3× and 4× for the 2D 6 and 10 fraction workflows, respectively, over 1D workflow. The measured retention time of peptides detected in both the 1D 1ug and 2D 10ug experiments showed very good correlation (r2 0.99, slope 1.0). Further optimization of both the first and second dimension is ongoing to further improve the peptide detection rates.

  3. From on-line documentation to the network information system; Von der Leitungsdokumentation zum Netzinformationssystem

    Energy Technology Data Exchange (ETDEWEB)

    Knobloch, J. [Stadtwerke Heidenheim (Germany)

    1995-10-16

    The Heidenheim AG town works, a community supply undertaking for electricity, gas, water and heat, carried out the first steps towards introducing a digital line planning system in 1989. A digital line register was started for the surrounding communities for which one started to lay a new natural gas network. This is 50% complete, the other 50% will follow during the next 3 to 4 years. The author reports on execution of the project and gives the prospects for the future. (orig.) [Deutsch] Die Stadtwerke Heidenheim AG, ein kommunales Versorgungsunternehmen fuer Strom, Gas, Wasser und Waerme, haben 1989 die ersten Schritte zur Einfuehrung eines digitalen Leitungsplanwerks unternommen. Fuer die umliegenden Gemeinden, in denen man mit der Neuverlegung eines Erdgasnetzes begann, wurde ein digitales Leitungskataster angelegt. Dies ist zu 50% fertiggestellt, die weiteren 50% folgen innerhalb der naechsten drei bis vier Jahre. Der Verfasser berichtet ueber die Projektdurchfuehrung und gibt einen Ausblick auf die Zukunft. (orig.)

  4. Generators and automated generator systems for production and on-line injections of pet radiopharmaceuticals

    Science.gov (United States)

    Shimchuk, G.; Shimchuk, Gr; Pakhomov, G.; Avalishvili, G.; Zavrazhnov, G.; Polonsky-Byslaev, I.; Fedotov, A.; Polozov, P.

    2017-01-01

    One of the prospective directions of PET development is using generator positron radiating nuclides [1,2]. Introduction of this technology is financially promising, since it does not require expensive special accelerator and radiochemical laboratory in the medical institution, which considerably reduces costs of PET diagnostics and makes it available to more patients. POZITOM-PRO RPC LLC developed and produced an 82Sr-82Rb generator, an automated injection system, designed for automatic and fully-controlled injections of 82RbCl produced by this generator, automated radiopharmaceutical synthesis units based on generated 68Ga produced using a domestically-manufactured 68Ge-68Ga generator for preparing two pharmaceuticals: Ga-68-DOTA-TATE and Vascular Ga-68.

  5. Automated Protein Biomarker Analysis: on-line extraction of clinical samples by Molecularly Imprinted Polymers

    Science.gov (United States)

    Rossetti, Cecilia; Świtnicka-Plak, Magdalena A.; Grønhaug Halvorsen, Trine; Cormack, Peter A. G.; Sellergren, Börje; Reubsaet, Léon

    2017-03-01

    Robust biomarker quantification is essential for the accurate diagnosis of diseases and is of great value in cancer management. In this paper, an innovative diagnostic platform is presented which provides automated molecularly imprinted solid-phase extraction (MISPE) followed by liquid chromatography-mass spectrometry (LC-MS) for biomarker determination using ProGastrin Releasing Peptide (ProGRP), a highly sensitive biomarker for Small Cell Lung Cancer, as a model. Molecularly imprinted polymer microspheres were synthesized by precipitation polymerization and analytical optimization of the most promising material led to the development of an automated quantification method for ProGRP. The method enabled analysis of patient serum samples with elevated ProGRP levels. Particularly low sample volumes were permitted using the automated extraction within a method which was time-efficient, thereby demonstrating the potential of such a strategy in a clinical setting.

  6. Automated Protein Biomarker Analysis: on-line extraction of clinical samples by Molecularly Imprinted Polymers

    Science.gov (United States)

    Rossetti, Cecilia; Świtnicka-Plak, Magdalena A.; Grønhaug Halvorsen, Trine; Cormack, Peter A.G.; Sellergren, Börje; Reubsaet, Léon

    2017-01-01

    Robust biomarker quantification is essential for the accurate diagnosis of diseases and is of great value in cancer management. In this paper, an innovative diagnostic platform is presented which provides automated molecularly imprinted solid-phase extraction (MISPE) followed by liquid chromatography-mass spectrometry (LC-MS) for biomarker determination using ProGastrin Releasing Peptide (ProGRP), a highly sensitive biomarker for Small Cell Lung Cancer, as a model. Molecularly imprinted polymer microspheres were synthesized by precipitation polymerization and analytical optimization of the most promising material led to the development of an automated quantification method for ProGRP. The method enabled analysis of patient serum samples with elevated ProGRP levels. Particularly low sample volumes were permitted using the automated extraction within a method which was time-efficient, thereby demonstrating the potential of such a strategy in a clinical setting. PMID:28303910

  7. Development of a video-based slurry sensor for on-line ash analysis. Final technical report, October 1, 1994--September 30, 1996

    Energy Technology Data Exchange (ETDEWEB)

    Adel, G.T.; Luttrell, G.H.

    1996-12-02

    Automatic control of fine coal cleaning circuits has traditionally been limited by the lack of sensors for on-line ash analysis. Although several nuclear-based slurry analyzers are available, none have seen widespread acceptance. This is largely due to the fact that nuclear sensors are expensive and tend to be influenced by changes in seam type and pyrite content. In this investigation, an image analysis technique is used for on-line determination of ash content in fine coal slurries. The ash content of a flotation tailings stream is correlated to the mean gray level of the slurry. Based on a 90% prediction interval, an analysis of sensor performance indicates an accuracy of 73 {+-} 4% ash over a range from 65 - 90% ash. While this result is comparable to existing nuclear-based analyzers, the video-based system is only a fraction of the cost. The sensor is currently being used to monitor the column flotation tailings stream at the Middle Fork preparation plant owned and operated by Pittston Coal Company.

  8. The role of predictive on-line monitoring systems in the power generation industry

    Energy Technology Data Exchange (ETDEWEB)

    Gittings, S.D.; Baldwin, J. [AEA Technology Energy plc (United Kingdom)

    1998-12-31

    It has been apparent in the power generation sector for some time that utilities are moving away from large scale, labour intensive, inspection and overhaul programmes. These are being replaced by targeted inspection and replacement programmes supported by engineering assessment. Such engineering assessments address the predominant long-term damage mechanisms and are aimed at predicting failure timescales based upon historic operating data. From these predictions extended inspection intervals can be justified and replacement schedules planned in advance, ensuring maximum plant availability and deferred capital expenditure. However, as these assessments are based upon an examination of past operating history they must be periodically re-visited and up-dated. The cost of such reassessments is usually close to that performed initially, although cost savings can arise from reductions in work-scope which have been previously justified. As computers have become more advanced (and significantly cheaper) some of the expertise used in these assessments has been transferred into software based products. However, these products are generally aimed at replacing specific parts of the desk-based analysis, necessitating a suite of products to be used in order to address all of the components and damage mechanisms, which must be assessed. As these products require specialized knowledge to be used effectively they are often employed by consultants and rarely by plant operators, except in the largest of organisations which can support an in-house team of `experts`. This has in essence led to an increase in the number of companies capable of offering assessment services, but has maintained, in the majority of cases, the plant operators reliance upon external consultants. These software based assessment methods rely upon historic operating data (in the same manner as their desk- based counterparts) and hence also need to be periodically up-dated. However, as previous assessments can

  9. Characterization of the Mucor circinelloides life cycle by on-line image analysis

    DEFF Research Database (Denmark)

    Lübbehüsen, Tina Louise; Nielsen, Jens; Mcintyre, Mhairi

    2003-01-01

    Aims: The life cycle of the dimorphic fungus Mucor circinelloides was studied in a temperature-controlled flow-through cell, which constitutes an ideal tool when following the development of individual cells, with a view to understanding the growth and differentiation processes occurring in and b......Aims: The life cycle of the dimorphic fungus Mucor circinelloides was studied in a temperature-controlled flow-through cell, which constitutes an ideal tool when following the development of individual cells, with a view to understanding the growth and differentiation processes occurring...... in and between the different morphological forms of the organism.Methods and Results: Mycelial growth and the transformation of hyphae into chains of arthrospores were characterized by image analysis techniques and described quantitatively. The influence of the nature (glucose and xylose) and concentration...... of the carbon source on specific growth rate and hyphal growth unit length were studied. The organism branched more profusely on xylose than on glucose while the specific growth rates determined were rather similar. Methods were developed to study the yeast-like growth phase of M. circinelloides in the flow...

  10. Combination Method of Principal Component Analysis and Support Vector Machine for On-line Process Monitoring and Fault Diagnosis

    Institute of Scientific and Technical Information of China (English)

    2006-01-01

    On-line monitoring and fault diagnosis of chemical process is extremely important for operation safety and product quality. Principal component analysis (PCA) has been widely used in multivariate statistical process monitoring for its ability to reduce processes dimensions. PCA and other statistical techniques, however, have difficulties in differentiating faults correctly in complex chemical process.Support vector machine (SVM) is a novel approach based on statistical learning theory, which has emerged for feature identification and classification. In this paper, an integrated method is applied for process monitoring and fault diagnosis, which combines PCA for fault feature extraction and multiple SVMs for identification of different fault sources. This approach is verified and illustrated on the Tennessee Eastman benchmark process as a case study.Results show that the proposed PCA-SVMs method has good diagnosis capability and overall diagnosis correctness rate.

  11. Improvement of multi-machine power system stability with variable series capacitor using on-line learning neural network

    Energy Technology Data Exchange (ETDEWEB)

    Senjyu, Tomonobu; Yamane, Shotaro; Morishima, Yoshiteru; Uezato, Katsumi [Univ. of the Ryukyus, Dept. of Electrical and Electronics Engineering, Nakagami, Okinawa (Japan); Fujita, Hideki [Chubu Electric Power Co., Inc., Midori-ku, Nagoya (Japan)

    2003-06-01

    This paper presents an adaptive control technique for the variable series capacitor using a recurrent neural network (RNN). Since, the parameters of the controller are determined by Genetic Algorithm (GA), which is one of the optimization algorithms, they are optimum only for that operating point and it is not possible to obtain good control performance against variations in the operating and fault point. The adaptive controller proposed in this paper consists of an optimum controller using GA and an RNN. As the RNN was on-line training, robust control performance can be achieved for various operating conditions. The effectiveness of this control method is demonstrated by considering simulation of a multi-machine power system. (Author)

  12. On line separation of overlapped signals from multi-time photons for the GEM-based detection system

    Science.gov (United States)

    Czarski, T.; Pozniak, K. T.; Chernyshova, M.; Malinowski, K.; Kasprowicz, G.; Kolasinski, P.; Krawczyk, R.; Wojenski, A.; Zabolotny, W.

    2015-09-01

    The Triple Gas Electron Multiplier (T-GEM) is presented as soft X-ray (SXR) energy and position sensitive detector for high-resolution X-ray diagnostics of magnetic confinement fusion plasmas. Multi-channel measurement system and serial data acquisition for X-ray energy and position recognition is described. Fundamental characteristics are presented for two dimensional detector structure. Typical signals of ADC - Analog to Digital Converter are considered for charge value and position estimation. Coinciding signals for high flux radiation cause the problem for cluster charge identification. The amplifier with shaper determines time characteristics and limits the pulses frequency. Separation of coincided signals was introduced and verified for simulation experiments. On line separation of overlapped signals was implemented applying the FPGA technology with relatively simple firmware procedure. Representative results for reconstruction of coinciding signals are demonstrated.

  13. On-line sequential injection dispersive liquid-liquid microextraction system for flame atomic absorption spectrometric determination of copper and lead in water samples.

    Science.gov (United States)

    Anthemidis, Aristidis N; Ioannou, Kallirroy-Ioanna G

    2009-06-30

    A simple, sensitive and powerful on-line sequential injection (SI) dispersive liquid-liquid microextraction (DLLME) system was developed as an alternative approach for on-line metal preconcentration and separation, using extraction solvent at microlitre volume. The potentials of this novel schema, coupled to flame atomic absorption spectrometry (FAAS), were demonstrated for trace copper and lead determination in water samples. The stream of methanol (disperser solvent) containing 2.0% (v/v) xylene (extraction solvent) and 0.3% (m/v) ammonium diethyldithiophosphate (chelating agent) was merged on-line with the stream of sample (aqueous phase), resulting a cloudy mixture, which was consisted of fine droplets of the extraction solvent dispersed entirely into the aqueous phase. By this continuous process, metal chelating complexes were formed and extracted into the fine droplets of the extraction solvent. The hydrophobic droplets of organic phase were retained into a microcolumn packed with PTFE-turnings. A portion of 300 microL isobutylmethylketone was used for quantitative elution of the analytes, which transported directly to the nebulizer of FAAS. All the critical parameters of the system such as type of extraction solvent, flow-rate of disperser and sample, extraction time as well as the chemical parameters were studied. Under the optimum conditions the enhancement factor for copper and lead was 560 and 265, respectively. For copper, the detection limit and the precision (R.S.D.) were 0.04 microg L(-1) and 2.1% at 2.0 microg L(-1) Cu(II), respectively, while for lead were 0.54 microg L(-1) and 1.9% at 30.0 microg L(-1) Pb(II), respectively. The developed method was evaluated by analyzing certified reference material and applied successfully to the analysis of environmental water samples.

  14. Analysis of a Kalman filter based method for on-line estimation of atmospheric dispersion parameters using radiation monitoring data

    DEFF Research Database (Denmark)

    Drews, Martin; Lauritzen, Bent; Madsen, Henrik

    2005-01-01

    A Kalman filter method is discussed for on-line estimation of radioactive release and atmospheric dispersion from a time series of off-site radiation monitoring data. The method is based on a state space approach, where a stochastic system equation describes the dynamics of the plume model...... parameters, and the observables are linked to the state variables through a static measurement equation. The method is analysed for three simple state space models using experimental data obtained at a nuclear research reactor. Compared to direct measurements of the atmospheric dispersion, the Kalman filter...... estimates are found to agree well with the measured parameters, provided that the radiation measurements are spread out in the cross-wind direction. For less optimal detector placement it proves difficult to distinguish variations in the source term and plume height; yet the Kalman filter yields consistent...

  15. Total On-line Access Data System (TOADS): Phase II Final Report for the Period August 2002 - August 2004

    Energy Technology Data Exchange (ETDEWEB)

    Yuracko, K. L. [YAHSGS LLC, Richland, WA (United States); Parang, M. [YAHSGS LLC, Richland, WA (United States); Landguth, D. C. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Coleman, R. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2004-09-13

    TOADS (Total On-line Access Data System) is a new generation of real-time monitoring and information management system developed to support unattended environmental monitoring and long-term stewardship of U.S. Department of Energy facilities and sites. TOADS enables project managers, regulators, and stakeholders to view environmental monitoring information in realtime over the Internet. Deployment of TOADS at government facilities and sites will reduce the cost of monitoring while increasing confidence and trust in cleanup and long term stewardship activities. TOADS: Reliably interfaces with and acquires data from a wide variety of external databases, remote systems, and sensors such as contaminant monitors, area monitors, atmospheric condition monitors, visual surveillance systems, intrusion devices, motion detectors, fire/heat detection devices, and gas/vapor detectors; Provides notification and triggers alarms as appropriate; Performs QA/QC on data inputs and logs the status of instruments/devices; Provides a fully functional data management system capable of storing, analyzing, and reporting on data; Provides an easy-to-use Internet-based user interface that provides visualization of the site, data, and events; and Enables the community to monitor local environmental conditions in real time. During this Phase II STTR project, TOADS has been developed and successfully deployed for unattended facility, environmental, and radiological monitoring at a Department of Energy facility.

  16. The Health Experts onLine at Portsmouth (HELP system: One-year review of adult and Pediatric Asynchronous Telehealth Consultations

    Directory of Open Access Journals (Sweden)

    Andrew H Lin

    2016-01-01

    Full Text Available Introduction: The Health Experts onLine at Portsmouth teleconsultation system is designed to connect health providers in the Navy Medicine East Region to specialists at Naval Medical Center Portsmouth. Methods: A review of the first year of the Health Experts onLine at Portsmouth system was performed. Data on each teleconsultation were extracted from the Health Experts onLine at Portsmouth system database and analyzed. Results: From June 2014 to May 2015 there have been 585 teleconsultations. Providers stationed on 36 ships/submarines and at 28 remote military treatment facilities have utilized the Health Experts onLine at Portsmouth system. Over 280 specialists in 34 different specialties were consulted. The median time to first response from a specialist was 6 h and 8 min, with 75% of all consults being addressed within 24 h. Eighteen medevacs were recommended. Thirty-nine potential medevacs were prevented, and 100 potential civilian network deferrals were prevented, resulting in an estimated savings of over US$580,000. Discussion: Based on the 1-year metrics, Health Experts onLine at Portsmouth has provided improved access and quality of care to service members and their families throughout the Navy Medicine East Region. It has helped avoid over US$580,000 in unnecessary cost burden. Further review at the 2-year time interval will demonstrate the continued growth and effectiveness of the Health Experts onLine at Portsmouth system.

  17. Implementation of a neural network for digital pulse shape analysis on a FPGA for on-line identification of heavy ions

    Science.gov (United States)

    Jiménez, R.; Sánchez-Raya, M.; Gómez-Galán, J. A.; Flores, J. L.; Dueñas, J. A.; Martel, I.

    2012-05-01

    Pulse shape analysis techniques for the identification of heavy ions produced in nuclear reactions have been recently proposed as an alternative to energy loss and time of flight methods. However this technique requires a large amount of memory for storing the shapes of charge and current signals. We have implemented a hardware solution for fast on-line processing of the signals producing the relevant information needed for particle identification. Since the pulse shape analysis can be formulated in terms of a pattern recognition problem, a neural network has been implemented in a FPGA device. The design concept has been tested using 12,13C ions produced in heavy ion reactions. The actual latency of the system is about 20 μs when using a clock frequency of 50 MHz.

  18. Implementation of a neural network for digital pulse shape analysis on a FPGA for on-line identification of heavy ions

    Energy Technology Data Exchange (ETDEWEB)

    Jimenez, R., E-mail: naharro@uhu.es [Departamento de Ingenieria Eletronica, Sistemas Informaticos y Automatica, Universidad de Huelva, 21071 Huelva (Spain); Sanchez-Raya, M.; Gomez-Galan, J.A. [Departamento de Ingenieria Eletronica, Sistemas Informaticos y Automatica, Universidad de Huelva, 21071 Huelva (Spain); Flores, J.L. [Departamento Ingenieria Electrica y Termica, Universidad de Huelva, 21071 Huelva (Spain); Duenas, J.A.; Martel, I. [Departamento de Fisica Aplicada, Universidad de Huelva, 21071 Huelva (Spain)

    2012-05-11

    Pulse shape analysis techniques for the identification of heavy ions produced in nuclear reactions have been recently proposed as an alternative to energy loss and time of flight methods. However this technique requires a large amount of memory for storing the shapes of charge and current signals. We have implemented a hardware solution for fast on-line processing of the signals producing the relevant information needed for particle identification. Since the pulse shape analysis can be formulated in terms of a pattern recognition problem, a neural network has been implemented in a FPGA device. The design concept has been tested using {sup 12,13}C ions produced in heavy ion reactions. The actual latency of the system is about 20 {mu}s when using a clock frequency of 50 MHz.

  19. Experiences in the instrumentation of power generators with the on-line analysis of generators AnGel system, for the internal insulation condition diagnosis; Experiencias en la instrumentacion de generadores de potencia con el sistema de analisis de generadores en linea AnGeL, para el diagnostico del estado del aislamiento interno

    Energy Technology Data Exchange (ETDEWEB)

    Carrillo C, Jaime; Ramirez N, Jose T. [Instituto de Investigaciones Electricas, Cuernavaca, Morelos (Mexico)

    2009-07-01

    The instrumentation of power generators with monitoring systems on-line, allows the personnel responsible for its operation to determine the stator and rotor windings insulation condition, as well as to emit an opportune diagnosis of possible anomalies, to implant programs of predictive maintenance, to reduce costs and to increase its reliability. The experiences of the last five years in the commissioning of the AnGel System; the problematic to which these equipment is subjected to, is described within the intrinsic atmosphere of the area where they are installed in the turbo-generators and hydro-generators, and finally, the experiences in the commissioning of the monitoring systems are revised and analyzed. [Spanish] La instrumentacion de los generadores de potencia con sistemas de monitoreo en linea, permite al personal responsable de su operacion determinar el estado del aislamiento de los devanados del estator y rotor, asi como emitir un diagnostico oportuno de posibles anomalias, implantar programas de mantenimiento predictivo, reducir costos e incrementar su confiabilidad. Se presentan las experiencias de los ultimos cinco anos en la puesta en operacion del Sistema AnGeL; se describe la problematica a la que son sometidos estos equipos dentro del ambiente intrinseco del area donde se instalan en los turbogeneradores e hidrogeneradores, y por ultimo, se analizan y discuten las experiencias en la puesta en servicio de los sistemas de monitoreo.

  20. Research on One High Precision Megnetic Heading System Based on on-line Estimation and Correction of Remnant Devia- tion with Neural Network

    Institute of Scientific and Technical Information of China (English)

    Xu,Guanlei; Ge,Dehong; Ji,Chunsheng

    2003-01-01

    This paper presented one high precision megneticheading system,and use neural network to correct the remnantdeviation of compass.This system can study on-line and be tak-en into practice directly,which not only realize the automation ofcorrection of deviation of compass and improve the effficiency,butalso raise the precision of this megnetic heading system.

  1. Integrated Health Monitoring and Fast on-Line Actuator Reconfiguration Enhancement (IHM-FLARE) System for Air Vehicles Project

    Data.gov (United States)

    National Aeronautics and Space Administration — SSCI proposes to develop innovative algorithms for the integration of Health Monitoring (HM) subsystem with the existing FLARE (Fast on-Line Actuator Reconfiguration...

  2. 在线混药喷雾系统混药性能试验%Experiment on mixing performance of on-line mixing spray system

    Institute of Scientific and Technical Information of China (English)

    邱白晶; 马靖; 邓斌; 欧鸣雄; 董晓娅

    2014-01-01

    inhalation is a state that liquid water provided by hydraulic pump is imported into the jet nozzle through the water inlet A of the jet-mixing apparatus, and forms a pressure small enough to make the pesticide sucked into the sucking chamber through the pesticide inlet B. And when the water is imported into the jet-mixing apparatus and then flows out from the pesticide inlet and diffuses, the pesticide can’t be sucked;and this state is called as the backflow. Based on the theoretical analysis and experiments, two methods to solve the problem of liquid backflow were given: change the structural parameters of jet nozzle by increasing inlet diameter or decreasing outlet diameter of jet nozzle, and reduce the drag coefficient of the spraying system. In the spray system operated with the nozzle of F110-015 type, CV ( the space coefficients of variation ) of mixture concentration under 4 types of spray pressures (0.26, 0.30, 0.34 and 0.36 MPa) were 2.983%, 3.599%, 4.287%and 4.647%, respectively, all less than 5%. In conclusion, the jet-mixing apparatus can be well applied to the on-line mixing spray system.%为寻求在线混药喷雾系统中射流混药装置对系统工作状态的影响,该文以胭脂红溶液模拟农药,考察了24种不同结构参数的射流混药装置应用于3种不同流量特性的在线混药喷雾系统时的工作特性,采用分光光度法对F110-015喷雾系统中射流嘴出口直径d=2.00 mm,面积比m=4.00的射流混药装置进行混药均匀性检测。试验结果表明,射流混药装置的结构参数对喷雾系统的工作状态具有显著影响,在同一种喷雾系统中,改变射流混药装置的结构参数,喷雾系统的工作状态也发生改变。在不同试验方案中,喷雾系统呈现回流和吸药2种工作状态;在射流混药理论分析及试验的基础上,给出了解决药液回流问题的2种方案,即增大射流嘴进口直径或减小射流嘴出口直径和降低喷雾系统

  3. Laser mass spectrometry as on-line sensor for industrial process analysis: process control of coffee roasting.

    Science.gov (United States)

    Dorfner, Ralph; Ferge, Thomas; Yeretzian, Chahan; Kettrup, Antonius; Zimmermann, Ralf

    2004-03-01

    The objective of the project is to develop on-line, real-time, and noninvasive process control tools of coffee roasting that help deliver a consistent and high-quality coffee aroma. The coffee roasting process was analyzed by direct injection of the roaster gas into a time-of-flight mass spectrometer and ionized either by resonance enhanced multiphoton ionization (REMPI) at 266 and 248 nm or vacuum ultraviolet single-photon ionization (VUV-SPI) at 118 nm. The VUV ionization scheme allows detecting mainly the most volatile and abundant compounds of molecular mass below 100 m/z, while REMPI ionizes mainly aromatic compounds of molecular mass larger than 100 m/z. Combining the compounds ionized by resonant and single-photon ionization, approximately 30 volatile organic compounds are monitored in real time. Time-intensity profiles of 10 important volatile coffee compounds were discussed in connection with their formation chemistry during roasting. Applying multivariate statistics (principle component analysis) on time-intensity traces of nine volatile coffee compounds, the roasting degree could be traced as a consistent path in the score plot of the two most significant principle components (including 68% of the total variance), for a range of roasting temperatures (200-250 degrees C).

  4. Fluorescence method using on-line sodium cholate coacervate surfactant mediated extraction for the flow injections analysis of Rhodamine B.

    Science.gov (United States)

    Acosta, Gimena; Talio, María C; Luconi, Marta O; Hinze, Willie L; Fernández, Liliana P

    2014-11-01

    An on-line surfactant mediated extraction method in a flow injection analysis format with fluorescence detection was developed for the determination of Rhodamine B (RhB) in food condiments. The sample was extracted using the phase separation behavior exhibited by the bile salt surfactant, sodium cholate (NaC), upon addition of sodium dodecylsulfate (SDS) in the presence of acid at room temperature. The RhB in the sample was incorporated into the NaC/SDS coacervate phase which was then collected on a glass-wool packed mini column from which it was subsequently eluted using a 1.00 mol L(-1) HCl solution. The inherent fluorescence (λex=555 nm; λem=575 nm) of RhB was employed for detection. Good linearity (r(2)=0.9933) was obtained over the concentration range 0.4-4794-479.0 µg L(-1) RhB. The detection (LOD) and quantification (LOQ) limits were 0.12 and 0.40 µg L(-1), respectively. The method was successfully applied for analysis of RhB in food condiments and spiked samples. The average recoveries ranged from 95.3% to 118.9% at spiked concentration levels of 1.19 and 2.39 µg L(-1). Under optimized conditions, a throughput of 50 samples per hour was achieved. The proposed method may be a valuable tool not only for quality control of food condiments and similar food confectioneries but for the analysis of a variety of other RhB-containing samples as well.

  5. Quantitative analysis for isoforms of creatine kinase MM in plasma by chromatofocusing, with on-line monitoring of enzyme activity.

    Science.gov (United States)

    Nohara, R; Sobel, B E; Jaffe, A S; Abendschein, D R

    1988-02-01

    Changes in the proportions of individual isoforms of the MM isoenzyme of creatine kinase (CK; EC 2.7.3.2) in plasma promptly reflect both myocardial infarction and coronary recanalization. However, quantitative methods developed thus far are too slow or cumbersome for routine use in making clinical decisions. We report a convenient, quantitative chromatofocusing assay with on-line fluorometric detection of isoform activity in the column eluent that provides results within 40 min from the time of sample application. Sample eluted from a microbore chromatofocusing column (1.8-mL bed volume) is split between a reaction stream, into which CK reagents are added, and a reference stream. After incubation at 37 degrees C, NADPH formed by reaction of isoforms with CK reagent is detected at 340 nm. The system can detect activity of individual isoforms in plasma samples having total CK activity greater than or equal to 21 U/L (30 degrees C). Results correlated closely with those obtained by previously validated, but slow, chromatofocusing (r = 0.98, n = 30) and protein immunoblotting (r = 0.90, n = 20) procedures.

  6. Preliminary Characterization Tests of Detectors of on-Line Monitor Systems of the Italian National Center of Oncological Hadron-Therapy (CNAO

    Directory of Open Access Journals (Sweden)

    Abdolkazem Ansarinejad

    2013-03-01

    Full Text Available Introduction Hadron-therapy is an effective technique used to treat tumors that are located between or nearby vital organs. The Italian National Center of Oncological Hadron-therapy (CNAO has been realized as the first facility in Italy to treat very difficult tumors with protons and Carbon ions. The on-line monitor system for CNAO has been developed by the Department of Physics of the University of Torino and Italian National Institute of Nuclear Physics (INFN. The monitoring system performs the on-line checking of the beam intensity, dimension, and beam position. Materials and Methods The monitor system is based on parallel plate ionization chambers and is composed of five ionization chambers with the anodes fully integrated or segmented in pixels or strips that are placed in two boxes. A series of measurements were performed that involve the background current and the detectors have been characterized by means of a series of preliminary testes in order to verify reproducibility and uniformity of the chambers using an X-ray source. Results The measured background currents for StripX, StripY and Pixel chambers are five orders of magnitude smaller than the nominal treatment current. The reproducibility error of chambers is less than 1%. The analysis of the uniformity showed that the monitor devices have a spread in gain that varies, but only about 2%. Conclusion The reproducibility and the uniformity values are considered as a good result, taking into account that the X-ray energy range is several orders of magnitude smaller than the particle energies used at CNAO.

  7. Development of on-line type TSC for Seibu region power source system .; Online gata TSC no seibu homen dengen keito eno donyu

    Energy Technology Data Exchange (ETDEWEB)

    Inoue, I. [Chubu Electric Power Co. Inc., Nagoya (Japan)

    1996-07-01

    This paper summarizes an on-line computing type transient stability controller (TSC) introduced in a power source system. The controller deals with instability in a power source system caused by expansion in thermal power plants. The controller is intended to carry out optimal power source restriction during a fault caused by lightning and other events, and avoid load interruption. This system comprises a central computing device, a child station device, an actuator and a transfer interruption device, each being duplicate composition. The central computing device determines assumed faults according to the computation flow and selects an optimal power controller periodically in unstable cases. The TSC also calculates a correlation expression between power control amount and transmission line current. This primary relation expression allows the child station device to perform system stabilizing control even if both lines of the central computing device have failed. Characteristics of this power source TSC include the following: the analysis engine has higher speed than a trunk-based TSC; the measures to stabilize the system are as various as shutdown of generators and control of steam valves; it has excellent system expandability; and it has highly diverse child station back-up functions. 5 figs., 1 tab.

  8. The use of a polymer inclusion membrane in flow injection analysis for the on-line separation and determination of zinc.

    Science.gov (United States)

    Zhang, Lujia L; Cattrall, Robert W; Kolev, Spas D

    2011-06-15

    This paper reports the first use of a polymer inclusion membrane (PIM) for on-line separation in flow injection analysis (FIA) involving simultaneous extraction and back-extraction. The FIA system containing the PIM separation module was used for the determination of Zn(II) in aqueous samples in the presence of Mg(II), Ca(II), Cd(II), Co(II), Ni(II), Cu(II), and Fe(III). The Fe(III) and Cu(II) interferences were eliminated by off-line precipitation with phosphate and on-line complexation with chloride, respectively. The concentration of Zn(II) was determined spectrophotometrically using 4-(2-pyridylazo) resorcinol (PAR). The optimal composition of the PIM consisted of 40% (m/m) di(2-ethlyhexyl) phosphoric acid (D2EHPA) as carrier, 10% (m/m) dioctyl phthalate (DOP) as plasticizer and 50% (m/m) poly(vinyl chloride) (PVC) as the base polymer. The optimized FIA system was characterized by a linear calibration curve in the range from 1.0 to 30.0 mg L(-1) Zn(II), a detection limit of 0.05 mg L(-1) and a relative standard deviation of 3.4% with a sampling rate of 4h(-1). Reproducible results were obtained for 20 replicate injections over a 5h period which demonstrated a good membrane stability. The FIA system was applied to the determination of Zn(II) in pharmaceuticals and samples from the galvanizing industry and very good agreement with atomic absorption spectrometry was obtained.

  9. A visualization environment for an on-line monitoring and control system for an experiment to search for T-violation in $K^{+}$ decay

    CERN Document Server

    Grigoriev, M P; Ivashkin, A P; Kudenko, Yu G; Mineev, O V; Khabibullin, M M; Aoki, M; Imazato, J; Kuno, Y; Watanabe, A; Igarashi, Y; Yokoi, T; Shimizu, S

    1999-01-01

    The main goal of experiment E246 at the KEK 12-GeV proton synchrotron is the search for the T-odd muon polarization in the decay K/sup +/ to pi /sup 0/ mu /sup +/ nu (K/sub mu 3/). To satisfy the experimental requirements, a graphic user-oriented on-line system for data monitoring and graphic representation of the most significant experimental parameters in the form of histograms, indicators, and 2D-displays has been developed. This paper describes the E246 data acquisition system, on-line system environment, obtained monitoring capabilities, set of graphic user displays, and the GUI development methodology for the high-energy physics on-line visualization. (16 refs).

  10. On-line micro-volume introduction system developed for lower density than water extraction solvent and dispersive liquid-liquid microextraction coupled with flame atomic absorption spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Anthemidis, Aristidis N., E-mail: anthemid@chem.auth.gr [Laboratory of Analytical Chemistry, Department of Chemistry, Aristotle University, Thessaloniki 54124 (Greece); Mitani, Constantina; Balkatzopoulou, Paschalia; Tzanavaras, Paraskevas D. [Laboratory of Analytical Chemistry, Department of Chemistry, Aristotle University, Thessaloniki 54124 (Greece)

    2012-07-06

    Highlights: Black-Right-Pointing-Pointer A dispersive liquid-liquid micro extraction method for lead and copper determination. Black-Right-Pointing-Pointer A micro-volume transportation system for extractant solvent lighter than water. Black-Right-Pointing-Pointer Analysis of natural water samples. - Abstract: A simple and fast preconcentration/separation dispersive liquid-liquid micro extraction (DLLME) method for metal determination based on the use of extraction solvent with lower density than water has been developed. For this purpose a novel micro-volume introduction system was developed enabling the on-line injection of the organic solvent into flame atomic absorption spectrometry (FAAS). The effectiveness and efficiency of the proposed system were demonstrated for lead and copper preconcentration in environmental water samples using di-isobutyl ketone (DBIK) as extraction solvent. Under the optimum conditions the enhancement factor for lead and copper was 187 and 310 respectively. For a sample volume of 10 mL, the detection limit (3 s) and the relative standard deviation were 1.2 {mu}g L{sup -1} and 3.3% for lead and 0.12 {mu}g L{sup -1} and 2.9% for copper respectively. The developed method was evaluated by analyzing certified reference material and it was applied successfully to the analysis of environmental water samples.

  11. MySQL Data Warehouse Technology in Osteoporos Community Health Information Management System and On-line Analysis Processing%MySQL数据仓库在骨质疏松社区-综合医院互动管理模型中应用及在线分析的实现

    Institute of Scientific and Technical Information of China (English)

    高莉莉; 沈影超

    2011-01-01

    虽然针对糖尿病、高血压病等疾病已经有多项健康教育模式的建立和研究,但是,针对农村原发性骨质疏松症(Osteoporos,OP)的预防这个重大社会问题,社区-综合医院互动管理模型的建立还在尝试阶段.OP是一个具有明确的病理生理、社会心理和经济后果的健康问题.我们将数据仓库的基本原理和方法与骨质疏松社区干预相结合,面向社区内骨质疏松高危人群构建了专门的数据仓库.以数据仓库运行为核心探索社区-综合医院互动管理模型的实现,同时对数据进行在线分析OLAP(on-Line analysis processing),实现单一维度分析和多个维度的组合分析功能,通过在实践中的数据积累可以为下一步开展有针对性的社区健康干预做准备.

  12. Integrated microfluidic system enabling (bio)chemical reactions with on-line MALDI-TOF mass spectrometry

    NARCIS (Netherlands)

    Brivio, Monica; Fokkens, Roel H.; Verboom, Willem; Reinhoudt, David N.; Tas, Niels R.; Goedbloed, Martijn; Berg, van den Albert

    2002-01-01

    A continuous flow micro total analysis system (μ-TAS) consisting of an on-chip microfluidic device connected to a matrix assisted laser desorption ionization [MALDI] time-of-flight [TOF] mass spectrometer (MS) as an analytical screening system is presented. Reaction microchannels and inlet/outlet re

  13. New approaches to biocide effectiveness monitoring using on-site biocide active analysis, ATP analysis, and on-line dosage/monitoring control

    Energy Technology Data Exchange (ETDEWEB)

    Borchardt, S.A.; Wetegrove, R.L.; Martens, J.D. [Nalco Chemical Co., Naperville, IL (United States)

    1997-09-01

    Accurate monitoring and control of antimicrobial agents (biocides) are necessary to maintain optimum performance of industrial water systems. Evaluation of many biocides on-site is often difficult due to a lack of accurate field methods. For many non-oxidizing biocides, no field methods are available. The use of a bioluminescence bioassay allows on-site measurement of actual effective toxicant. This technology is based on a bioluminescence bioassay that measures the decrease in light output of a specific bacterium over a given time period in the presence of a toxicant. This response can be accurately correlated to the concentration of toxicant present. This system can also be used to monitor the response of microbiological populations to treatment programs by monitoring shifts in ATP levels. On-line dosage/monitoring control of a biocide product can be achieved by the addition of an inert fluorescent tracer molecule to a biocide formulation. The benefits of these traced biocides include precise documentation and on-line control of product feed and discharge, measurement of system consumption, and measurement of biocide concentration gradients throughout a system. The attributes of these new approaches to biocide effectiveness monitoring allow for more efficient and economical microbiological treatment of industrial water systems.

  14. An approach to an inhibition electronic tongue to detect on-line organophosphorus insecticides using a computer controlled multi-commuted flow system.

    Science.gov (United States)

    Alonso, Gustavo A; Dominguez, Rocio B; Marty, Jean-Louis; Muñoz, Roberto

    2011-01-01

    An approach to an inhibition bioelectronic tongue is presented. The work is focused on development of an automated flow system to carry out experimental assays, a custom potentiostat to measure the response from an enzymatic biosensor, and an inhibition protocol which allows on-line detections. A Multi-commuted Flow Analysis system (MCFA) was selected and developed to carry out assays with an improved inhibition method to detect the insecticides chlorpyrifos oxon (CPO), chlorfenvinfos (CFV) and azinphos methyl-oxon (AZMO). The system manifold comprised a peristaltic pump, a set of seven electronic valves controlled by a personal computer electronic interface and software based on LabView® to control the sample dilutions into the cell. The inhibition method consists in the injection of the insecticide when the enzyme activity has reached the plateau of the current; with this method the incubation time is avoided. A potentiostat was developed to measure the response from the enzymatic biosensor. Low limits of detection of 10 nM for CPO, CFV, and AZMO were achieved.

  15. An exploratory investigation of the translation of Pacific Northwest Laboratory`s print manuals system to an on-line manuals system

    Energy Technology Data Exchange (ETDEWEB)

    Heubach, J.G.; Hunt, S.T.; Pond, L.R.

    1992-06-01

    Information management technology has proliferated in the past decade in response to the information explosion. As documentation accumulates, the need to access information residing in manuals, handbooks and regulations conveniently, accurately, and quickly has increased. However, studies show that only fractions of the available information is read (Martin, 1978). Consequently, one of the biggest challenges in linking information and electronic management of information is to use the power of communication technology to meet the information needs of the audience. Pacific Northwest Laboratories` (PNL) investigation of translating its print manual system to an on-line system fits this challenge precisely. PNL`s manuals contain a tremendous amount of information for which manual holders are responsible. To perform their tasks in compliance with policy and procedure guidelines, users need to access information accurately, conveniently, and quickly. In order to select and use information management tools wisely, answers must be sought to a few basic questions. Communication experts cite four key questions: What do users want? What do users need? What characteristics of an on-line information system affect its usefulness? Who are the users whose wants and needs are to be met? Once these questions are answered, attention can be focused on finding the best match between user requirements and technology characteristics and weighing the costs and benefits of proposed options.

  16. An exploratory investigation of the translation of Pacific Northwest Laboratory's print manuals system to an on-line manuals system

    Energy Technology Data Exchange (ETDEWEB)

    Heubach, J.G.; Hunt, S.T.; Pond, L.R.

    1992-06-01

    Information management technology has proliferated in the past decade in response to the information explosion. As documentation accumulates, the need to access information residing in manuals, handbooks and regulations conveniently, accurately, and quickly has increased. However, studies show that only fractions of the available information is read (Martin, 1978). Consequently, one of the biggest challenges in linking information and electronic management of information is to use the power of communication technology to meet the information needs of the audience. Pacific Northwest Laboratories' (PNL) investigation of translating its print manual system to an on-line system fits this challenge precisely. PNL's manuals contain a tremendous amount of information for which manual holders are responsible. To perform their tasks in compliance with policy and procedure guidelines, users need to access information accurately, conveniently, and quickly. In order to select and use information management tools wisely, answers must be sought to a few basic questions. Communication experts cite four key questions: What do users want What do users need What characteristics of an on-line information system affect its usefulness Who are the users whose wants and needs are to be met Once these questions are answered, attention can be focused on finding the best match between user requirements and technology characteristics and weighing the costs and benefits of proposed options.

  17. Peculiarities of Communicative Style in The Advertisement Genre in English and Russian University On-line Communication Discourse Analysis

    Directory of Open Access Journals (Sweden)

    Милана Евгеньевна Куприянова

    2014-12-01

    Full Text Available Intercultural communicative competence is one of the integral parts of translators’ skills. The article analyses national and cultural peculiarities of English and Russian communicative styles in the advertisement speech genre in university on-line communication to address the problem of translatability of lexical units. Furthermore, the study explains the use of particular linguistic means and communication strategies as related to the specific features of Anglo-Saxon and Russian linguistic cultures.

  18. On-line monitoring of the photocatalytic degradation of 2,4-D and dicamba using a solid-phase extraction-multisyringe flow injection system.

    Science.gov (United States)

    Chávez-Moreno, Carmín; Ferrer, Laura; Hinojosa-Reyes, Laura; Hernández-Ramírez, Aracely; Cerdà, Víctor; Guzmán-Mar, Jorge

    2013-11-15

    A fully automated on-line system for monitoring the photocatalytic degradation of herbicides was developed using multisyringe flow injection analysis (MSFIA) coupled to a solid phase extraction (SPE) unit with UV detection. The calibration curves were linear in the concentration range of 100-1000 μg L(-1) for 3,6-dichloro-2-methoxybenzoic acid (dicamba) and 500-3000 μg L(-1) for 2,4-dichlorophenoxyacetic acid (2,4-D), while the detection limits were 30 and 135 μg L(-1) for dicamba and 2,4-D, respectively. The monitoring of the photocatalytic degradation (TiO2 anatase/UV 254 nm) of these two herbicides was performed by MSFIA-SPE system using a small sample volume (2 mL) in a fully automated approach. The degradation was assessed in ultrapure and drinking water with initial concentrations of 1000 and 2000 μg L(-1) for dicamba and 2,4-D, respectively. Degradation percentages of approximately 85% were obtained for both herbicides in ultrapure water after 45 min of photocatalytic treatment. A similar degradation efficiency in drinking water was observed for 2,4-D, whereas dicamba exhibited a lower degradation percentage (75%), which could be attributed to the presence of inorganic species in this kind of water. Copyright © 2013 Elsevier Ltd. All rights reserved.

  19. On-line coupled high performance liquid chromatography-gas chromatography for the analysis of contamination by mineral oil. Part 1: method of analysis.

    Science.gov (United States)

    Biedermann, Maurus; Grob, Koni

    2012-09-14

    For the analysis of mineral oil saturated hydrocarbons (MOSH) and mineral oil aromatic hydrocarbons (MOAH), on-line coupled high performance liquid chromatography-gas chromatography-flame ionization detection (HPLC-GC-FID) offers important advantages: it separates MOSH and MOAH in robust manner, enables direct injection of large aliquots of raw extracts (resulting in a low detection limit), avoids contamination of the sample during preparation and is fully automated. This review starts with an overview of the technology, particularly the fundamentals of introducing large volumes of solvent into GC, and their implementation into various transfer techniques. The main part deals with the concepts of MOSH and MOAH analysis, with a thorough discussion of the choices made. It is followed by a description of the method. Finally auxiliary tools are summarized to remove interfering components, enrich the sample in case of a high fat content and obtain additional information about the MOSH and MOAH composition.

  20. FINITE ELEMENT METHOD ANALYSIS OF PIPE MATERIAL TEMPERATURE CHANGES INFLUENCE ON LINE EXPANSION LOOPS IN HYDRAULIC INSTALLATIONS ON MODERN TANKERS

    OpenAIRE

    2011-01-01

    Finite element method analysis of main lines of hydraulic central loading system installation expansion loops mounted on product and chemical tankers has been presented in the paper. The axial forces problem in installations mounted along the ship's open decks executed from hull deformations on waves and thermal stresses is given. Use of "U" type expansion loops is described. Results of forces in anchor points and stresses of Mises due to expansion loop deformations are shown. Calculations we...

  1. Discussion on Operational Reliability of On-line Monitoring System of Transmission Line%输电线路在线监测系统的运行可靠性分析

    Institute of Scientific and Technical Information of China (English)

    岳灵平; 张志亮; 俞强; 严峥; 王志勇; 刘平平

    2014-01-01

    Low available ratio of on-line monitoring devices of transmission lines has threatened the reliable operation of grid monitoring system. Therefore, by collecting operation information of various types of on-line monitoring devices of transmission lines, this paper makes an in-depth analysis on failure causes and proposes technology to improve the reliability of on-line monitoring device of transmission line from aspects of power supply source and operation and maintenance quality; furthermore, it makes reliability evaluation on the life-time requirements and service condition of on-line monitoring devices of transmission lines.%输电线路在线监测装置可用率低的现状已对电网监测系统可靠运行造成了一定的威胁,因此,通过收集各类输电线路在线监测装置的运行情况资料,深入分析故障原因,从供电电源和运维质量两方面提出了提高输电线路在线监测装置可靠性的措施,并对输电线路在线监测装置的寿命要求及使用条件进行了可靠性评价。

  2. The Genomes OnLine Database (GOLD) v.5: a metadata management system based on a four level (meta)genome project classification.

    Science.gov (United States)

    Reddy, T B K; Thomas, Alex D; Stamatis, Dimitri; Bertsch, Jon; Isbandi, Michelle; Jansson, Jakob; Mallajosyula, Jyothi; Pagani, Ioanna; Lobos, Elizabeth A; Kyrpides, Nikos C

    2015-01-01

    The Genomes OnLine Database (GOLD; http://www.genomesonline.org) is a comprehensive online resource to catalog and monitor genetic studies worldwide. GOLD provides up-to-date status on complete and ongoing sequencing projects along with a broad array of curated metadata. Here we report version 5 (v.5) of the database. The newly designed database schema and web user interface supports several new features including the implementation of a four level (meta)genome project classification system and a simplified intuitive web interface to access reports and launch search tools. The database currently hosts information for about 19,200 studies, 56,000 Biosamples, 56,000 sequencing projects and 39,400 analysis projects. More than just a catalog of worldwide genome projects, GOLD is a manually curated, quality-controlled metadata warehouse. The problems encountered in integrating disparate and varying quality data into GOLD are briefly highlighted. GOLD fully supports and follows the Genomic Standards Consortium (GSC) Minimum Information standards.

  3. The Genomes OnLine Database (GOLD) v.5: a metadata management system based on a four level (meta)genome project classification

    Science.gov (United States)

    Reddy, T.B.K.; Thomas, Alex D.; Stamatis, Dimitri; Bertsch, Jon; Isbandi, Michelle; Jansson, Jakob; Mallajosyula, Jyothi; Pagani, Ioanna; Lobos, Elizabeth A.; Kyrpides, Nikos C.

    2015-01-01

    The Genomes OnLine Database (GOLD; http://www.genomesonline.org) is a comprehensive online resource to catalog and monitor genetic studies worldwide. GOLD provides up-to-date status on complete and ongoing sequencing projects along with a broad array of curated metadata. Here we report version 5 (v.5) of the database. The newly designed database schema and web user interface supports several new features including the implementation of a four level (meta)genome project classification system and a simplified intuitive web interface to access reports and launch search tools. The database currently hosts information for about 19 200 studies, 56 000 Biosamples, 56 000 sequencing projects and 39 400 analysis projects. More than just a catalog of worldwide genome projects, GOLD is a manually curated, quality-controlled metadata warehouse. The problems encountered in integrating disparate and varying quality data into GOLD are briefly highlighted. GOLD fully supports and follows the Genomic Standards Consortium (GSC) Minimum Information standards. PMID:25348402

  4. The Genomes OnLine Database (GOLD) v.5: a metadata management system based on a four level (meta)genome project classification

    Energy Technology Data Exchange (ETDEWEB)

    Reddy, Tatiparthi B. K. [USDOE Joint Genome Institute (JGI), Walnut Creek, CA (United States); Thomas, Alex D. [USDOE Joint Genome Institute (JGI), Walnut Creek, CA (United States); Stamatis, Dimitri [USDOE Joint Genome Institute (JGI), Walnut Creek, CA (United States); Bertsch, Jon [USDOE Joint Genome Institute (JGI), Walnut Creek, CA (United States); Isbandi, Michelle [USDOE Joint Genome Institute (JGI), Walnut Creek, CA (United States); Jansson, Jakob [USDOE Joint Genome Institute (JGI), Walnut Creek, CA (United States); Mallajosyula, Jyothi [USDOE Joint Genome Institute (JGI), Walnut Creek, CA (United States); Pagani, Ioanna [USDOE Joint Genome Institute (JGI), Walnut Creek, CA (United States); Lobos, Elizabeth A. [USDOE Joint Genome Institute (JGI), Walnut Creek, CA (United States); Kyrpides, Nikos C. [USDOE Joint Genome Institute (JGI), Walnut Creek, CA (United States); King Abdulaziz Univ., Jeddah (Saudi Arabia)

    2014-10-27

    The Genomes OnLine Database (GOLD; http://www.genomesonline.org) is a comprehensive online resource to catalog and monitor genetic studies worldwide. GOLD provides up-to-date status on complete and ongoing sequencing projects along with a broad array of curated metadata. Within this paper, we report version 5 (v.5) of the database. The newly designed database schema and web user interface supports several new features including the implementation of a four level (meta)genome project classification system and a simplified intuitive web interface to access reports and launch search tools. The database currently hosts information for about 19 200 studies, 56 000 Biosamples, 56 000 sequencing projects and 39 400 analysis projects. More than just a catalog of worldwide genome projects, GOLD is a manually curated, quality-controlled metadata warehouse. The problems encountered in integrating disparate and varying quality data into GOLD are briefly highlighted. Lastly, GOLD fully supports and follows the Genomic Standards Consortium (GSC) Minimum Information standards.

  5. Determination of Bingham Rheological Parameters of SCC using On-line Video Image Analysis of Automatic Slump Flow Testing

    DEFF Research Database (Denmark)

    Thrane, Lars Nyholm; Pade, Claus

    2005-01-01

    A “touch one bottom” prototype system for estimation of Bingham rheological parameters of SCC has been developed. Video image analysis is used to obtain a series of corresponding values of concrete spread versus time during an automatic slump flow test. The spread versus time curve is subsequentl...... used to estimate the Bingham rheological parameters by a least square search into a database. It takes less than 120 seconds from the start of the slump flow test to the SCC’s Bingham rheological parameters appear on the system’s PC....

  6. FINITE ELEMENT METHOD ANALYSIS OF PIPE MATERIAL TEMPERATURE CHANGES INFLUENCE ON LINE EXPANSION LOOPS IN HYDRAULIC INSTALLATIONS ON MODERN TANKERS

    Directory of Open Access Journals (Sweden)

    Bartlomiej Zylinski

    2011-01-01

    Full Text Available Finite element method analysis of main lines of hydraulic central loading system installation expansion loops mounted on product and chemical tankers has been presented in the paper. The axial forces problem in installations mounted along the ship's open decks executed from hull deformations on waves and thermal stresses is given. Use of "U" type expansion loops is described. Results of forces in anchor points and stresses of Mises due to expansion loop deformations are shown. Calculations were made by ABAQUS Ver.6.7 FEM computer program.

  7. 对加强反腐倡廉网络化建设的思考%Reflection on Enhancing Construction of On-line Anti-corruption System

    Institute of Scientific and Technical Information of China (English)

    王清

    2012-01-01

    网络技术以其特有的开放性、平等性、共享性融人了反腐倡廉的行列,网络反腐倡廉存在的问题有:法律存在空白、信息真伪难辨、易泄露机密和易受舆论误导。推进反腐倡廉网络化建设要制度建设先行化、网络建设系统化、行政监督电子化、监管反馈动态化、警示教育网络化。%Internet technology has been utilized in combating corruption and building an incorrupt govern- ment, because of its openness, equality, and sharing. But there are also problems existing in the on-line anti -corruption system, such as: no related law or regulation tion; leaking of confidential information; and being prone ; difficulty of distinguishing true and fake informa- to misleading public opinion. To promote construc- tion of on-line anti-corruption system, it requires institutional construction, systemization of network, e-su- pervision over administration, dynamic feedback mechanism of supervision, and on-line corruption prevention education programs.

  8. Procurement module for a MIS: user's manual. [PROQ, on-line interactive program for management information system

    Energy Technology Data Exchange (ETDEWEB)

    Lovin, J.K.; Clark, B.A.

    1976-12-01

    The temporary Procurement Module (PROQ) is an on-line interactive computer program. It can be used to answer many questions pertinent to the status of outside procurements and their obligating costs. The module prompts the user on what requests it is expecting. If the user has doubts as to the response, or if the meaning of the response is not clear, the module will give a detailed list of the options available at that level. The user has control of what data are to be considered, how they are to be grouped, and what format the output will take. As the user selects the options available at a given level, the module proceeds to the next lower level until sufficient input has been supplied to provide him with the requested information.

  9. Development of a video-based slurry sensor for on-line ash analysis. Eighth quarterly technical progress report, July 1, 1996--September 30, 1996

    Energy Technology Data Exchange (ETDEWEB)

    Adel, G.T.; Luttrell, G.H.

    1996-10-22

    Automatic control of fine coal cleaning circuits has traditionally been limited by the lack of sensors for on-line ash analysis. Although several nuclear-based analyzers are available, none have seen widespread acceptance. This is largely due to the fact that nuclear sensors are expensive and tend to be influenced by changes in seam type and pyrite content. Recently, researchers at VPI&SU have developed an optical sensor for phosphate analysis. The sensor uses image processing technology to analyze video images of phosphate ore. It is currently being used by PCS Phosphate for off-fine analysis of dry flotation concentrate. The primary advantages of optical sensors over nuclear sensors are that they are significantly cheaper, are not subject to measurement variations due to changes in high atomic number minerals, are inherently safer and require no special radiation permitting. The purpose of this work is to apply the knowledge gained in the development of an optical phosphate analyzer to the development of an on-fine ash analyzer for fine coal slurries. During the past quarter, installation of the video-based ash analyzer at the Middle Fork plant site was completed. A method of measuring and automatically adjusting for small variations in the sensor illumination scheme was developed and implemented. Initial on-line testing of the ash analyzer has yielded adequate calibration information, and the sensor is currently operating on-line. The on-line performance of the sensor is under review and the information from this review will be included in the final report.

  10. Improved Fuzzy Logic System to Evaluate Milk Electrical Conductivity Signals from On-Line Sensors to Monitor Dairy Goat Mastitis.

    Science.gov (United States)

    Zaninelli, Mauro; Tangorra, Francesco Maria; Costa, Annamaria; Rossi, Luciana; Dell'Orto, Vittorio; Savoini, Giovanni

    2016-07-13

    The aim of this study was to develop and test a new fuzzy logic model for monitoring the udder health status (HS) of goats. The model evaluated, as input variables, the milk electrical conductivity (EC) signal, acquired on-line for each gland by a dedicated sensor, the bandwidth length and the frequency and amplitude of the first main peak of the Fourier frequency spectrum of the recorded milk EC signal. Two foremilk gland samples were collected from eight Saanen goats for six months at morning milking (lactation stages (LS): 0-60 Days In Milking (DIM); 61-120 DIM; 121-180 DIM), for a total of 5592 samples. Bacteriological analyses and somatic cell counts (SCC) were used to define the HS of the glands. With negative bacteriological analyses and SCC 1,000,000 cells/mL, glands were classified as not healthy (NH). For each EC signal, an estimated EC value was calculated and a relative deviation was obtained. Furthermore, the Fourier frequency spectrum was evaluated and bandwidth length, frequency and amplitude of the first main peak were identified. Before using these indexes as input variables of the fuzzy logic model a linear mixed-effects model was developed to evaluate the acquired data considering the HS, LS and LS × HS as explanatory variables. Results showed that performance of a fuzzy logic model, in the monitoring of mammary gland HS, could be improved by the use of EC indexes derived from the Fourier frequency spectra of gland milk EC signals recorded by on-line EC sensors.

  11. Improved Fuzzy Logic System to Evaluate Milk Electrical Conductivity Signals from On-Line Sensors to Monitor Dairy Goat Mastitis

    Directory of Open Access Journals (Sweden)

    Mauro Zaninelli

    2016-07-01

    Full Text Available The aim of this study was to develop and test a new fuzzy logic model for monitoring the udder health status (HS of goats. The model evaluated, as input variables, the milk electrical conductivity (EC signal, acquired on-line for each gland by a dedicated sensor, the bandwidth length and the frequency and amplitude of the first main peak of the Fourier frequency spectrum of the recorded milk EC signal. Two foremilk gland samples were collected from eight Saanen goats for six months at morning milking (lactation stages (LS: 0–60 Days In Milking (DIM; 61–120 DIM; 121–180 DIM, for a total of 5592 samples. Bacteriological analyses and somatic cell counts (SCC were used to define the HS of the glands. With negative bacteriological analyses and SCC < 1,000,000 cells/mL, glands were classified as healthy. When bacteriological analyses were positive or showed a SCC > 1,000,000 cells/mL, glands were classified as not healthy (NH. For each EC signal, an estimated EC value was calculated and a relative deviation was obtained. Furthermore, the Fourier frequency spectrum was evaluated and bandwidth length, frequency and amplitude of the first main peak were identified. Before using these indexes as input variables of the fuzzy logic model a linear mixed-effects model was developed to evaluate the acquired data considering the HS, LS and LS × HS as explanatory variables. Results showed that performance of a fuzzy logic model, in the monitoring of mammary gland HS, could be improved by the use of EC indexes derived from the Fourier frequency spectra of gland milk EC signals recorded by on-line EC sensors.

  12. On-line immunoaffinity solid-phase extraction capillary electrophoresis mass spectrometry for the analysis of large biomolecules: a preliminary report.

    Science.gov (United States)

    Medina-Casanellas, Silvia; Benavente, Fernando; Giménez, Estela; Barbosa, José; Sanz-Nebot, Victoria

    2014-08-01

    The analysis of large biomolecules by on-line immunoaffinity solid-phase extraction capillary electrophoresis mass spectrometry (IA-SPE-CE-MS) remains unexplored because of the complex issues that need to be addressed. In this preliminary study, we used the human glycoprotein transferrin (Tf) as a model of a large biomolecule. First, we established by CE-UV a novel method compatible with IA-SPE-CE-MS, based on the use of a fused silica capillary coated with an anionic derivative of polyacrylamide (UltraTrol(TM) Dynamic Pre-Coat High Normal, HN) to prevent protein adsorption. The methodology allowed the detection of the most abundant Tf sialoforms. Repeatability studies demonstrated high stability of the coated capillaries, which was required for on-line immunoextraction and MS detection. IA-SPE-CE-UV and IA-SPE-CE-MS methods were optimized for the analysis of Tf standards and human serum samples using a laboratory-made IA sorbent. Three peaks corresponding to Tf were detected with UV detection when on-line immunoextraction was applied to the standards. The use of MS detection, however, reduced the resolution of the electrophoretic separation. Finally, we demonstrated that it was possible to detect Tf in human serum samples, after off-line serum sample de-salting by centrifugal filtration.

  13. An in-source stretched membrane inlet for on-line analysis of VOCs in water with single photon ionization TOFMS.

    Science.gov (United States)

    Hou, Keyong; Li, Fanglong; Chen, Wendong; Chen, Ping; Xie, Yuanyuan; Zhao, Wuduo; Hua, Lei; Pei, Kemei; Li, Haiyang

    2013-10-07

    An in-source, stretched, hollow fiber membrane (HFM) inlet has been developed to improve the sensitivity of on-line time-of-flight mass spectrometry (TOFMS) with a vacuum ultraviolet (VUV) lamp based single photon ionization (SPI) source for the direct analysis of liquid samples. A 2-cm HFM was stretched to 8 cm in length, and placed in the ion source and directly under the VUV lamp window with a distance of 15 mm. Compared with the conventional flow-through configuration under the same experimental conditions, the signal intensities of selected volatile organic compounds (VOCs) of methyl tert-butyl ether (MTBE), ethyl tert-butyl ether (ETBE), benzene, toluene and p-xylene were increased over 5-fold in magnitude, and the response time was shortened to one-third. The limits of detection (LOD) of MTBE, ETBE, benzene, toluene and p-xylene ranged from 0.25 to 1.3 μg L(-1) with a measurement time of 60 s, and three orders of linear range were obtained with correlation coefficients of 0.9972-0.9992. The present results suggest that the in-source stretched HFM is a simple and effective way to increase the sensitivity and shorten response time of the membrane inlet, and we believe that it will also be beneficial to other types of on-line mass spectrometer for the on-line analysis of VOCs in water with a VUV lamp based SPI ion source.

  14. Study for on-line system to identify inadvertent control rod drops in PWR reactors using ex-core detector and thermocouple measures

    Energy Technology Data Exchange (ETDEWEB)

    Souza, Thiago J.; Medeiros, Jose A.C.C.; Goncalves, Alessandro C., E-mail: tsouza@nuclear.ufrj.br, E-mail: canedo@lmp.ufrj.br, E-mail: alessandro@nuclear.ufrj.br [Coordenacao dos Programas de Pos-Graduacao em Engenharia (COPPE/UFRJ), Rio de Janeiro, RJ (Brazil). Programa de Engenharia Nuclear

    2015-07-01

    Accidental control rod drops event in PWR reactors leads to an unsafe operating condition. It is important to quickly identify the rod to minimize undesirable effects in such a scenario. In this event, there is a distortion in the power distribution and temperature in the reactor core. The goal of this study is to develop an on-line model to identify the inadvertent control rod dropped in PWR reactor. The proposed model is based on physical correlations and pattern recognition of ex-core detector responses and thermocouples measures. The results of the study demonstrated the feasibility of an on-line system, contributing to safer operation conditions and preventing undesirable effects, as its shutdown. (author)

  15. Considerations on fatigue stress range calculations in nuclear power plants using on-line monitoring systems and the ASME Code

    Energy Technology Data Exchange (ETDEWEB)

    Cicero, R., E-mail: ciceror@unican.e [INESCO INGENIEROS S.L., Santander (Spain); Departamento de Ciencia e Ingenieria del Terreno y los Materiales, Universidad de Cantabria, Santander (Spain); Cicero, S. [Departamento de Ciencia e Ingenieria del Terreno y los Materiales, Universidad de Cantabria, Santander (Spain); Gorrochategui, I. [Centro Tecnologico de Componentes, Santander (Spain); Lacalle, R. [INESCO INGENIEROS S.L., Santander (Spain); Departamento de Ciencia e Ingenieria del Terreno y los Materiales, Universidad de Cantabria, Santander (Spain)

    2010-01-15

    Nuclear power plants are generally designed and inspected according to the ASME Code. This code indicates stress intensity (S{sub INT}) as the parameter to be used in the stress analysis of components. One of the particularities of S{sub INT} is that it always takes positive values, independently of the nature of the stress (tensile or compressive). This circumstance is relevant in the Fatigue Monitoring Systems used in nuclear power plants, due to the manner in which the different variable stresses are combined in order to obtain the final total stress range. This paper describes some situations derived from the application of the ASME Code, shows different ways of dealing with them and illustrates their influence on the evaluation of the fatigue usage factor through a case study.

  16. Experimental study on the push-broom infrared imaging system based on line-plane-switching fiber bundle

    Science.gov (United States)

    Yan, Xingtao; Li, Fu; Ma, Xiaolong; Lv, Juan; He, Yinghong; Zhao, Yiyi; Bu, Fan

    2016-10-01

    The use of line-plane-switching infrared fiber bundle to achieve wide field of view push-broom infrared imaging has been studied with experiment. In this technology, the linear array end of the imaging fiber bundle is used as a long-linear array infrared detector, and the plane array end of the bundle is coupled by a mature small scale Infrared Focal Plane Array (IRFPA). It can evade the difficulty of getting the long-linear array infrared detector directly, and has a signally significance to the development of internal infrared imaging technology. Based on the introduction of the composition, working principle of this novel infrared optical system, the system principle-demonstrating experiment has been accomplished. The line-plane-switching fiber bundle used in this experiment is 64×9 format plane array and 192×3 format linear array. It is made from chalcogenide glass fibers, possessing core (As40S59.5Se0.5) of 45 μm, cladding (As40S60) of 5 μm, and error of 1% in diameter. Perfect imaging results prove that this novel technology is feasibility and superiority. The analysis of the experiment makes a foundation for the subsequent further verification experiments.

  17. Procurement module for a MIS: user's manual. [PROQ, on-line interactive program for management information system

    Energy Technology Data Exchange (ETDEWEB)

    Lovin, J. K.; Clark, B. A.

    1977-03-01

    The FED-MIS Procurement Module (PROQ) is an on-line interactive computer program. It can be used to answer many questions pertinent to the status of outside procurements and their obligating costs. Even an inexperienced computer user should have little difficulty in learning to use PROO, as the module prompts the user on what requests it is expecting. If the user has doubts as to the response, or if the meaning of the response is not clear, the module will give a detailed list of the options available at that level. The user has control of what data are to be considered, how they are to be grouped, and what format the output will take. This user control is the result of the module's hierarchical arrangement. As the user selects the options available at a given level, the module proceeds to the next lower level until sufficient input has been supplied to provide him with the requested information. At the entry level the user can request one of two actions. At the next level specific options are available. Some of these options can lead to lower levels having additional options. 7 figures, 3 tables.

  18. Generic on-line solid phase extraction sample preparation strategies for the analysis of drugs in biological matrices by LC-MS/MS.

    Science.gov (United States)

    Bourgogne, Emmanuel; Grivet, Chantal; Varesio, Emmanuel; Hopfgartner, Gérard

    2015-01-01

    In the present work we investigate the integration of a single hardware platform (Prospekt-2) allowing on-line SPE with pre-/post-trapping dilution and direct injection of plasma extracts, and also compare the benefits and challenges of the different approaches for pharmaceutical drugs with heterogeneous physicochemical properties. In the first part, the generic use of on-line SPE with direct plasma injection or after protein precipitation was investigated for the quantitative analysis of talinolol. In the second part, pre-trapping and post-trapping dilution for on-line SPE is discussed for generic method development on an oxadiazole and its major metabolite. Finally, the difference of performance between direct plasma injection vs. off-line liquid-liquid extraction is also described for the quantification of buprenorphine and naltrexone down to 50 and 100 pg/ml using a 0.25 ml plasma aliquot. All assays were in human plasma and detection was performed by mass spectrometry detection either on simple or triple stage quadrupoles. Regardless of the tested strategy, assays were found linear, with precision and accuracy with <15% for all quality controls samples and <20% for lower limit of quantitation.

  19. Automatic on-line monitoring of atmospheric volatile organic compounds: gas chromatography-mass spectrometry and gas chromatography-flame ionization detection as complementary systems.

    Science.gov (United States)

    de Blas, Maite; Navazo, Marino; Alonso, Lucio; Durana, Nieves; Iza, Jon

    2011-11-15

    Traditionally air quality networks have been carrying out the continuous, on-line measurement of volatile organic compounds (VOC) in ambient air with GC-FID. In this paper some identification and coelution problems observed while using this technique in long-term measurement campaigns are described. In order to solve these problems a GC-MS was set up and operated simultaneously with a GC-FID for C2-C11 VOCs measurement. There are few on-line, unattended, long term measurements of atmospheric VOCs performed with GC-MS. In this work such a system has been optimized for that purpose, achieving good repeatability, linearity, and detection limits of the order of the GC-FID ones, even smaller in some cases. VOC quantification has been made by using response factors, which is not frequent in on-line GC-MS. That way, the identification and coelution problems detected in the GC-FID, which may led to reporting erroneous data, could be corrected. The combination of GC-FID and GC-MS as complementary techniques for the measurement of speciated VOCs in ambient air at sub-ppbv levels is proposed. Some results of the measurements are presented, including concentration values for some compounds not found until now on public ambient air VOC databases, which were identified and quantified combining both techniques. Results may also help to correct previously published VOC data with wrongly identified compounds by reprocessing raw chromatographic data.

  20. Automatic on-line monitoring of atmospheric volatile organic compounds: Gas chromatography-mass spectrometry and gas chromatography-flame ionization detection as complementary systems

    Energy Technology Data Exchange (ETDEWEB)

    Blas, Maite de, E-mail: maite.deblas@ehu.es [Chemical and Environmental Engineering Department, University College of Technical Mining and Civil Engineering, University of the Basque Country, Colina de Beurco s/n, 48902 Barakaldo (Spain); Navazo, Marino; Alonso, Lucio; Durana, Nieves [Chemical and Environmental Engineering Department, School of Engineering, University of the Basque Country, Alameda de Urquijo s/n, 48013 Bilbao (Spain); Iza, Jon [Chemical and Environmental Engineering Department, Faculty of Pharmacy, University of the Basque Country, Paseo de la Universidad, 7, 01006, Vitoria-Gasteiz (Spain)

    2011-11-15

    Traditionally air quality networks have been carrying out the continuous, on-line measurement of volatile organic compounds (VOC) in ambient air with GC-FID. In this paper some identification and coelution problems observed while using this technique in long-term measurement campaigns are described. In order to solve these problems a GC-MS was set up and operated simultaneously with a GC-FID for C{sub 2}-C{sub 11} VOCs measurement. There are few on-line, unattended, long term measurements of atmospheric VOCs performed with GC-MS. In this work such a system has been optimized for that purpose, achieving good repeatability, linearity, and detection limits of the order of the GC-FID ones, even smaller in some cases. VOC quantification has been made by using response factors, which is not frequent in on-line GC-MS. That way, the identification and coelution problems detected in the GC-FID, which may led to reporting erroneous data, could be corrected. The combination of GC-FID and GC-MS as complementary techniques for the measurement of speciated VOCs in ambient air at sub-ppbv levels is proposed. Some results of the measurements are presented, including concentration values for some compounds not found until now on public ambient air VOC databases, which were identified and quantified combining both techniques. Results may also help to correct previously published VOC data with wrongly identified compounds by reprocessing raw chromatographic data.

  1. [Analysis of phthalate esters in plastic-packaging bags on-line sample stacking-microemulsion electrokinetic chromatography].

    Science.gov (United States)

    Xiao, Jia; Huang, Ying; Wang, Minyi; Chen, Guonan

    2012-09-01

    Two convenient, effective, and reproducible methods using microemulsion electrokinetic chromatography (MEEKC)-normal stacking mode (NSM) and reversed electrode polarity stacking mode (REPSM) were developed for the on-line sample stacking of phthalate esters (PAEs). REPSM coupled with MEEKC increased the sensitivity of 937.5 to 7,143 times for four PAEs compared to the conventional MEEKC. The separating conditions in the MEEKC method were studied, and many factors influencing the two sample stacking processes were investigated in detail. The optimum sample matrices for the two stacking methods were as follows: 30 mmol/L sodium cholate (SC) and 30.0 mmol/L borate (pH 8.5). Additionally, sample injections as large as 3.45 kPa x 40 s and 3.45 kPa x 90 s were applied for NSM-MEEKC and REPSM-MEEKC, respectively. The linear relationship and reproducibility were also examined. Under the optimum conditions, the detection limits (S/N = 3) of the PAEs were in the ranges of 0.021 - 0.33 mg/L and 0.7 - 4 microg/L for NSM-MEEKC and REPSM-MEEKC, respectively. The proposed REPSM-MEEKC has been successfully applied to determine PAEs in plastic-packaging bags, and the spiked recoveries were in the range of 89.1% - 105.6% with satisfactory results.

  2. Continuous Flow Liquid Microjunction Surface Sampling Probe Connected On-line with HPLC/MS for Spatially Resolved Analysis of Small Molecules and Proteins

    Energy Technology Data Exchange (ETDEWEB)

    Van Berkel, Gary J [ORNL; Kertesz, Vilmos [ORNL

    2013-01-01

    RATIONALE: A continuous flow liquid microjunction surface sampling probe extracts soluble material from surfaces for direct ionization and detection by MS. Demonstrated here is the on-line coupling of such a probe with HPLC/MS enabling extraction, separation and detection of small molecules and proteins from surfaces in a spatially resolved (~0.5 mm diameter spots) manner. Methods: A continuous flow liquid microjunction surface sampling probe was connected to a 6-port, 2-position valve for extract collection and injection to an HPLC column. A QTRAP 5500 hybrid triple quadrupole linear ion trap equipped with a Turbo V ion source operated in positive ESI mode was used for all experiments. System operation was tested with extraction, separation and detection of propranolol and associated metabolites from drug dosed tissues and proteins from dried sheep blood spots on paper. Results: Confirmed in the tissue were the parent drug and two different hydroxypropranolol glucuronides. The mass spectrometric response for these compounds from different locations in the liver showed an increase with increasing extraction time (5, 20 and 40 s extractions). For on-line separation and detection/identification of extracted proteins from dried sheep blood spots, two major protein peaks dominated the chromatogram and could be correlated with the expected masses for the hemoglobin and chains. Conclusions: Spatially resolved sampling, separation, and detection of small molecules and proteins from surfaces can be accomplished using a continuous flow liquid microjunction surface sampling probe coupled on-line with HPLC/MS detection.

  3. Initial Results of On-Line Earth System Science Course Offerings at the University of Nebraska-Omaha Through the Earth System Science Education Alliance

    Science.gov (United States)

    Shuster, R. D.; Grandgenett, N. F.; Schnase, W. L.; Hamersky, S.; Moshman, R.

    2008-12-01

    The University of Nebraska at Omaha has been offering on-line Earth System Science coursework to teachers in Nebraska since 2002. UNO was one of the initial members in the Earth Systems Science Education Alliance (ESSEA) and has offered three different ESSEA courses, with nearly 200 students having taken ESSEA courses at UNO for graduate credit. Our experiences in delivering this coursework have involved both teachers who have received a stipend to take the course and those who have paid their own tuition and fees and received graduate credit for the course. We will report on the online behavior of teachers from both populations and also discuss pros and cons of each approach. UNO has also experimented with different approaches in the support and management of the course, including using undergraduate majors as content experts. This improves access of teachers to content-related feedback and is a positive experience for the undergraduate major. Feedback surveys from earlier ESSEA offerings indicate a strongly positive perception of the courses by the teachers enrolled in the coursework. Project impact has been documented in teacher projects, quotes, and lessons associated with the coursework activities. We will also describe online course modules being developed within the UNO online course efforts, including one focusing on the global amphibian crisis.

  4. On-line system for preconcentration and determination of metals in vegetables by Inductively Coupled Plasma Optical Emission Spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Bezerra, Marcos A. [Universidade Federal da Bahia, Instituto de Quimica, Grupo de Pesquisa em Quimica Analitica, Campus Universitario de Ondina, Salvador, Bahia 40170-290 (Brazil); Universidade Estadual do Sudoeste da Bahia, Laboratorio de Quimica Analitica, Campus de Jequie, Jequie, Bahia 45206-190 (Brazil); Santos, Walter N.L. dos [Departamento de Ciencias Exatas e da Terra, Universidade do Estado da Bahia, R. Silveira Martins, 2555, Salvador, Bahia 41195-001 (Brazil); Lemos, Valfredo A. [Universidade Estadual do Sudoeste da Bahia, Laboratorio de Quimica Analitica, Campus de Jequie, Jequie, Bahia 45206-190 (Brazil)], E-mail: vlemos@uesb.br; Korn, Maria das Gracas A.; Ferreira, Sergio L.C. [Universidade Federal da Bahia, Instituto de Quimica, Grupo de Pesquisa em Quimica Analitica, Campus Universitario de Ondina, Salvador, Bahia 40170-290 (Brazil)

    2007-09-05

    A procedure has been developed for the simultaneous determination of trace amounts of cadmium, copper, chromium, nickel and lead in digested vegetable samples. The method involves solid-phase extraction of the metals using a minicolumn of Amberlite XAD-4 modified with dihydroxybenzoic acid (DHB) and detection by Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES). The elution of the metals from minicolumn was performed with 1.0 mol L{sup -1} hydrochloric acid. Variables associated with flow preconcentration system performance, such as pH, buffer concentration, eluent concentration and sampling flow rate, were optimized. The developed procedure provides enrichment factors of 100, 72, 16, 91 and 53, for cadmium, copper, chromium, nickel and lead, respectively. Detection limits (3{sigma}{sub B}) were 0.02 (Cd), 0.23 (Cu), 0.58 (Cr), 0.060 (Ni) and 0.54 (Pb) {mu}g L{sup -1}. The procedure was applied for determination of metals in samples of guarana and cabbage. The accuracy of the method was checked by the analysis of a certified reference material (NIST 1571, Orchard leaves). Results found were in agreement with certified values.

  5. Project Final Report: Building a Community Infrastructure for Scalable On-Line Performance Analysis Tools around Open|SpeedShop

    Energy Technology Data Exchange (ETDEWEB)

    Galarowicz, James

    2014-01-06

    In this project we created a community tool infrastructure for program development tools targeting Petascale class machines and beyond. This includes tools for performance analysis, debugging, and correctness tools, as well as tuning and optimization frameworks. The developed infrastructure provides a comprehensive and extensible set of individual tool building components. We started with the basic elements necessary across all tools in such an infrastructure followed by a set of generic core modules that allow a comprehensive performance analysis at scale. Further, we developed a methodology and workflow that allows others to add or replace modules, to integrate parts into their own tools, or to customize existing solutions. In order to form the core modules, we built on the existing Open|SpeedShop infrastructure and decomposed it into individual modules that match the necessary tool components. At the same time, we addressed the challenges found in performance tools for petascale systems in each module. When assembled, this instantiation of community tool infrastructure provides an enhanced version of Open|SpeedShop, which, while completely different in its architecture, provides scalable performance analysis for petascale applications through a familiar interface. This project also built upon and enhances capabilities and reusability of project partner components as specified in the original project proposal. The overall project team’s work over the project funding cycle was focused on several areas of research, which are described in the following sections. The reminder of this report also highlights related work as well as preliminary work that supported the project. In addition to the project partners funded by the Office of Science under this grant, the project team included several collaborators who contribute to the overall design of the envisioned tool infrastructure. In particular, the project team worked closely with the other two DOE NNSA

  6. Automatic on-line pre-concentration system using a knotted reactor for the FAAS determination of lead in drinking water

    Energy Technology Data Exchange (ETDEWEB)

    Souza, Anderson S. [Universidade Federal da Bahia, Instituto de Quimica, Nucleo de Excelencia em Quimica Analitica da Bahia, Campus Universitario de Ondina, Salvador, Bahia 40170-290 (Brazil); Universidade Estadual de Santa Cruz, Ilheus, Bahia (Brazil); Brandao, Geovani C. [Universidade Federal da Bahia, Instituto de Quimica, Nucleo de Excelencia em Quimica Analitica da Bahia, Campus Universitario de Ondina, Salvador, Bahia 40170-290 (Brazil); Santos, Walter N.L. dos [Universidade Estadual de Santa Cruz, Ilheus, Bahia (Brazil); Lemos, Valfredo A. [Universidade Estadual do Sudoeste da Bahia, Campus de Jequie, Jequie, Bahia 45206-190 (Brazil); Ganzarolli, Edgard M. [Universidade Estadual do Centro-Oeste, Departamento de Quimica, Rua Presidente Zacarias, 875, CP 33010, 85010-990 Guarapuava, PR (Brazil); Bruns, Roy E. [Universidade Estadual de Campinas, Instituto de Quimica, CP 6154, 13083-970 Campinas, SP (Brazil); Ferreira, Sergio L.C. [Universidade Federal da Bahia, Instituto de Quimica, Nucleo de Excelencia em Quimica Analitica da Bahia, Campus Universitario de Ondina, Salvador, Bahia 40170-290 (Brazil)]. E-mail: slcf@ufba.br

    2007-03-22

    An automatic on-line pre-concentration system is proposed for lead determination in drinking water using flame atomic absorption spectrometry (FAAS). Lead(II) ions are retained as the 1-(2-pyridylazo)-2-naphthol (PAN) complex in the walls of a knotted reactor, followed by an elution step using 0.50 mol L{sup -1} hydrochloric acid solution. Optimisation involving the sampling flow rate, pH and buffer concentration factors was performed using a Box-Behnken design. Other factors were established considering results of previous experiments. The procedure allows the determination of lead with a 0.43 {mu}g L{sup -1} detection limit (3{sigma}/S) and precisions (expressed as relative standard deviation) of 4.84% (N = 7) and 2.9% (N = 7) for lead concentrations of 5 and 25 {mu}g L{sup -1}, respectively. The accuracy was confirmed by the determination of lead in the NIST SRM 1643d trace elements in natural water standard reference material. The pre-concentration factor obtained is 26.5 and the sampling frequency is 48 h{sup -1}. The recovery achieved for lead determination in the presence of several ions demonstrated that this procedure could be applied to the analysis of drinking water samples. The method was applied for lead determination in drinking water samples collected in Jequie City, Brazil. The lead concentration found in 25 samples were always lower than the permissible maximum levels stipulated by World Health Organization.

  7. Flow injection analysis with on-line nylon powder extraction for room-temperature phosphorescence determination of thiabendazole.

    Science.gov (United States)

    Piccirilli, G N; Escandar, G M

    2009-07-30

    A fast and very selective flow-through phosphorescence optosensor was designed and characterized for the determination of the fungicide thiabendazole in water samples. For the first time, thiabendazole was determined using a flow-through optosensor based on the phosphorescence signals obtained when it is retained in a solid support. While thiabendazole does not phosphoresce in packing materials commonly used to fill the flow-cell, significant emission signals are observed when it is retained on nylon powder in the presence of iodide and sulfite. The experimental set-up was based on a flow-injection manifold coupled to an on-line phosphorescence detector containing nylon powder packed in a conventional flow-cell. Potassium iodide and sodium sulfite were added to sample aliquots to improve the thiabendazole phosphorescence and injected in the flow manifold using water as carrier. After the phosphorescence emission was registered, the analyte was eluted from the packed nylon with a 65% (v/v) methanol-water mixture. Optimal instrumentation, experimental and flow conditions were evaluated. Using a sample volume of 2000 microL, the analytical signal showed a very good linearity in the range 12.9-110 ng mL(-1), with a detection limit of 4.5 ng mL(-1), and a sample throughput of about 14 samples per hour. The effects of the presence of concomitant species in the thiabendazole phosphorescence signal were studied, and a comparison with the fluorescence nylon-powder optosensor was carried out and discussed. Finally, the applicability of the proposed optosensor was tested in water samples, and satisfactory recoveries ranging between 97% and 105% were obtained.

  8. Automatic on-line detection system design research on internal defects of metal materials based on optical fiber F-P sensing technology

    Science.gov (United States)

    Xia, Liu; Shan, Ning; Chao, Ban; Caoshan, Wang

    2016-10-01

    Metal materials have been used in aerospace and other industrial fields widely because of its excellent characteristics, so its internal defects detection is very important. Ultrasound technology is used widely in the fields of nondestructive detection because of its excellent characteristic. But the conventional detection instrument for ultrasound, which has shortcomings such as low intelligent level and long development cycles, limits its development. In this paper, the theory of ultrasound detection is analyzed. A computational method of the defects distributional position is given. The non-contact type optical fiber F-P interference cavity structure is designed and the length of origin cavity is given. The real-time on-line ultrasound detecting experiment devices for internal defects of metal materials is established based on the optical fiber F-P sensing system. The virtual instrument of automation ultrasound detection internal defects is developed based on LabVIEW software and the experimental study is carried out. The results show that this system can be used in internal defect real-time on-line locating of engineering structures effectively. This system has higher measurement precision. Relative error is 6.7%. It can be met the requirement of engineering practice. The system is characterized by simple operation, easy realization. The software has a friendly interface, good expansibility, and high intelligent level.

  9. Development of a video-based slurry sensor for on-line ash analysis. Quarterly report, April 1, 1996--June 30, 1996

    Energy Technology Data Exchange (ETDEWEB)

    Adel, G.T.; Luttrell, G.H.

    1996-07-22

    Automatic control of fine coal cleaning circuits has traditionally been limited by the lack of sensors for on-line ash analysis. Although several nuclear-based analyzers are available, none have seen widespread acceptance. This is largely due to the fact that nuclear sensors are expensive and tend to be influenced by changes in seam type and pyrite content. Recently, researchers at VPI&SU have developed an optical sensor for phosphate analysis. The sensor uses image processing technology to analyze video images of phosphate ore. It is currently being used by PCS Phosphate for off-line analysis of dry flotation concentrate. The primary advantages of optical sensors over nuclear sensors are that they are significantly cheaper, are not subject to measurement variations due to changes in high atomic number minerals, are inherently safer and require no special radiation permitting. The purpose of this work is to apply the knowledge gained in the development of an optical phosphate analyzer to the development of an on-line ash analyzer for fine coal slurries. During the past quarter, an industrially-hardened version of the video-based ash analyzer was designed and constructed. All components are now in place at the Middle Fork plant site awaiting the installation of a sample line from the flotation columns to the analyzer. The sensor now appears ready for long-term, in-plant testing during the final quarter of this project. 1 fig., 1 tab.

  10. On-line Multiple-model Based Adaptive Control Reconfiguration for a Class of Non-linear Control Systems

    DEFF Research Database (Denmark)

    Yang, Z.; Izadi-Zamanabadi, Roozbeh; Blanke, M.

    2000-01-01

    Based on the model-matching strategy, an adaptive control reconfiguration method for a class of nonlinear control systems is proposed by using the multiple-model scheme. Instead of requiring the nominal and faulty nonlinear systems to match each other directly in some proper sense, three sets of ...... corresponding to the updating of local LTI models, which validations are determined by the model approximation errors and the optimal index of local design. The test on a nonlinear ship propulsion system shows the promising potential of this method for system reconfiguration...

  11. 复合式制动气室性能在线检测系统设计%Disquisition of Performance On-line Detection System for Brake Chamber

    Institute of Scientific and Technical Information of China (English)

    刘宁霞; 罗哉

    2012-01-01

    设计并实现复合式制动气室性能在线检测系统,弥补国内对复合式制动气室性能在线检测研究存在的不足.引入伺服加载机构,突破以往检测中推杆行程限位装置加载速度不可控的局限,实现限位装置的加载速度精确可调;应用高速数据采集卡和计算机控制技术,提高系统的采集速度和测量精度.可对多类型的复合式制动气室驻车制动腔静特性、行车制动腔静特性、开始释放压力等性能进行在线测试和分析.通过试验分析表明检测系统能真实准确的对复合式制动气室的性能进行在线检测,检测周期小于2min/个,其测量精度达到实际应用的要求,并采用R&R法客观的分析检测系统,已达到新设备的验收条件.%The on-line detection system for brake chamber was designed and realized, which made up for the domestic deficiency of on-line detection research for brake chamber. Servo-loading mechanism was introduced in the design of test system to break through the limitation of which previous test can not control the load speed of brake chamber and to achieve load speed precisely and adjustably. Using high-Speed data collection card and computer control technology to improve the sampling speed and the measuring accuracy of the system. It can test as well as analysis the static characteristic of parking brake chamber, static characteristic of service brake chamber and hold-off pressure on-line. Through the test and analysis shows that, the detection system can true accurate the performance of complex braking gas chamber by on-line detection, which the period less than 2 min, the measuring precision has met the practical requirement. Using the R&R method to objectively analysis the detection system, has reached the conditions of the new equipment successfully.

  12. End-to-end encryption in on-line payment systems : The industry reluctance and the role of laws

    NARCIS (Netherlands)

    Kasiyanto, Safari

    2016-01-01

    Various security breaches at third-party payment processors show that online payment systems are the primary target for cyber-criminals. In general, the security of online payment systems relies on a number of factors, namely technical factors, processing factors, and legal factors. The industry giv

  13. End-to-end encryption in on-line payment systems : The industry reluctance and the role of laws

    NARCIS (Netherlands)

    Kasiyanto, Safari

    2016-01-01

    Various security breaches at third-party payment processors show that online payment systems are the primary target for cyber-criminals. In general, the security of online payment systems relies on a number of factors, namely technical factors, processing factors, and legal factors. The industry

  14. End-to-end encryption in on-line payment systems : The industry reluctance and the role of laws

    NARCIS (Netherlands)

    Kasiyanto, Safari

    2016-01-01

    Various security breaches at third-party payment processors show that online payment systems are the primary target for cyber-criminals. In general, the security of online payment systems relies on a number of factors, namely technical factors, processing factors, and legal factors. The industry giv

  15. Dynamic liquid-liquid-solid microextraction based on molecularly imprinted polymer filaments on-line coupling to high performance liquid chromatography for direct analysis of estrogens in complex samples.

    Science.gov (United States)

    Zhong, Qisheng; Hu, Yufei; Hu, Yuling; Li, Gongke

    2012-06-08

    A novel sample preparation technique termed dynamic liquid-liquid-solid microextraction (DLLSME) was developed and on-line coupled to high performance liquid chromatography (HPLC) for direct extraction, desorption, and analysis of trace estrogens in complex samples. The DLLSME consists of the aqueous donor phase, the organic medium phase and the molecularly imprinted polymer filaments (MIPFs) as solid acceptor phase. The organic solvent with lesser density was directly added on top of the aqueous sample, and the dynamic extraction was performed by circulating the organic solvent through the MIPFs inserted into a PEEK tube which served as an extraction and desorption chamber. Afterwards, the extracted analytes on the MIPFs were on-line desorbed and then introduced into the HPLC for analysis. To evaluate the feasibility of the on-line system, a new DLLSME-HPLC method was developed for the analysis of five estrogens in aqueous samples by using 17β-estradiol MIPFs as the solid phase. Under the optimized conditions, the enrichment factors of 51-70, limits of detection of 0.08-0.25 μg/L and precision within 4.5-6.9% were achieved. Furthermore, the proposed method was applied to the analysis of real samples including urine, milk and skin toner, satisfactory recovery (81.9-99.8%) and reproducibility (4.1-7.9%) were obtained. Especially, 0.59 μg/L of 17β-estradiol was determined in female urine sample. The DLLSME offers an attractive alternative for direct analysis of trace analytes in aqueous samples and could potentially be extended to other adsorptive materials.

  16. Development of On-Line Direct Current Glow Discharge Source for Analysis of Isotope Ratio of Hydrogen

    Institute of Scientific and Technical Information of China (English)

    2008-01-01

    <正>The present research is focused on the analysis of isotope ratio of the hydrogen by measuring an intensity ratio of hydrogen/deuterium/tritium fluxes. The direct current glow discharge tube may provide a

  17. On-Line Near-Infrared Transmittance Type Inspecting System for Protein Content of Grain%近红外透射式谷物蛋白质含量在线监测系统

    Institute of Scientific and Technical Information of China (English)

    张广军; Suranjan; Panigrahi

    2001-01-01

    用近红外透射光谱分析技术,建立了用于谷物加工过程中的蛋白质含量 在线 监测系统。宽光束照射、透射光谱的二阶微分处理和基于人工神经元网络的标定方法是保证监测系统有效工作的关键。同时建立了用于小麦蛋白质含 量现场在线监测的最佳BP(Back Propagation)网络结构,其SEC=0.12%,SEP=0.15%。该监测系统的研究不仅可以直接应用于谷物成份含量的在线监测,而且所涉及的方法也同样适合于其它光谱分析应用。%An on-line inspecting system for protein content of a grain during the grain processing process is set up by means of near-infrared transmittance spec tral analysis technique. A wide beam illuminating, second-order differential pro cessing for transmittance spectrum and a calibration method based on artificial neuron network are the key factors for ensuring the effective operating of the inspecting system. At the same time, an optimal Back Propagation (BP) network architecture for the field on-line inspecting the protein content of wheat is set up. Its SEC is 0.12% and SEP is 0.15%, respectively. The development of the system not only can directly on-line inspect the protein content of grains, but the related method also can be suitable for the other spectral analysis applications.

  18. Functional design and implementation with on-line programmable technology in optical fiber communication pulse code modulation test system

    Science.gov (United States)

    Xu, Yuan; Ding, Huan; Gao, Youtang

    2010-10-01

    In order to complete the functional design in the fiber optical communication pulse code modulation test system, taking advantage of CPLD / FPGA and SOPC technology, software solutions used to design system hardware features and control functions, thereby the whole system could attain optimisation in the logic control as well as encoding and decoding functional designs on the motherboard, enabling this system fulfill the capacities varying from simple digital simulation transmission modulate to the high speed fiber optical communication network information encoding and decoding functions. Simultaneously the application of logarithmic pressure companding technique, PCM encoding and decoding system to improve the small signal quantizing SNR(Signal-to-Noise Ratio), TP3067 adopting A rate thirteen broken lines to carry on signal pressure companding. When the signal at a certain stage, the quantizing SNR is invariable(as signal receives uniform quantization in this phase, therefore the quantizing SNR drops along with signal amplititude decreasing). Test results are as follows: ideal various signal encoding and decoding system waveforms, high performance parameters , achieve the desired designing aim, a entirely new approach to realize different kinds of information encoding and decoding model building and implementation, saving development costs, improving design efficiency, satisfactory actual results, stable operation.

  19. Application 0f GIS Partial Discharge UHF On-line Monitoring System%GIS局放特高频在线监测系统的应用

    Institute of Scientific and Technical Information of China (English)

    李杰祎

    2013-01-01

    气体绝缘组合电器GIS在城市电网中得到广泛应用,建立GIS局部放电在线监测系统,对准确掌握设备内部绝缘运行状态和指导检修具有重要意义。本文主要讨论了GIS局部放电产生的原因、GIS局部放电监测的方法、基于特高频检测原理的局放在线监测系统的结构和软件功能以及在工程设计中应该注意的问题。%Developing of GIS Partial Discharge UHF On-line Monitoring System is important for pinpoint holding of insulated run-state in GIS and coach-overhaul,As broad application of gas insulated switchgear in city electric wird.This paper introduces cause of prtial dscharge and measurement of prtial dscharge in GIS ,and instruct of GIS Partial Discharge UHF On-line Monitoring System,and attendant problems in egineering design.

  20. Pesticide residue analysis by off-line SPE and on-line reversed-phase LC-GC using the through-oven-transfer adsorption/desorption interface.

    Science.gov (United States)

    Perez, M; Alario, J; Vazquez, A; Villén, J

    2000-02-15

    A new method to determine pesticide residue in water is presented. The described method includes using off-line solid-phase extraction (SPE) and on-line reversed-phase liquid chromatography-gas chromatography (RPLC-GC). An interface, based on a modified programmed temperature vaporizer (PTV) injector, packed with a suitable trapping material, is used for on-line RPLC-GC. The changes made in the PTV injector affect the pneumatic system, sample introduction, and solvent elimination. The new interface is easily capable of automation. Methanol/wate (70/30) is used as the eluent in the LC preseparation step. The LC column flow during elution is different from the flow during the transfer step. The transferred volumes range from 500 to 1400 microL (volume of the fractions of interest). Solvent elimination is almost 100% before the sample reaches the GC column. The described system does not show any variation of the peak retention times. The detection limit for real samples ranges from 0.04 to 1.5 ng/L, using NP detection.

  1. On-line Auto-Tuning of PI Control of the Superheat for a Supermarket Refrigeration System

    DEFF Research Database (Denmark)

    Yang, Zhenyu; Andersen, Casper; Izadi-Zamanabadi, Roozbeh

    2011-01-01

    An online PI auto-tuning method is proposed for superheat control for a type of supermarket refrigeration systems. The proposed procedure consists of three serial steps: Step-One uses one of the two proposed empirical methods, namely multi-step method and relay method, for modeling initialization...... controller is auto-tuned based on the obtained FOPDT model and the SIMC method in Step-Three. The proposed method is implemented on a real-sized physical system and the experimental results showed a promising potential to apply the proposed method into commercial development....

  2. On-line Auto-Tuning of PI Control of the Superheat for a Supermarket Refrigeration System

    DEFF Research Database (Denmark)

    Yang, Zhenyu; Andersen, Casper; Izadi-Zamanabadi, Roozbeh

    2011-01-01

    An online PI auto-tuning method is proposed for superheat control for a type of supermarket refrigeration systems. The proposed procedure consists of three serial steps: Step-One uses one of the two proposed empirical methods, namely multi-step method and relay method, for modeling initialization...... controller is auto-tuned based on the obtained FOPDT model and the SIMC method in Step-Three. The proposed method is implemented on a real-sized physical system and the experimental results showed a promising potential to apply the proposed method into commercial development....

  3. An On-line Monitoring System for Hydrogen Distribution in the Metallic Wall Caused by Hydrogen Permeation

    Institute of Scientific and Technical Information of China (English)

    2001-01-01

    Based on the electrochemical permeation technique and the patent by Du, an intelligent electrochemical measurement system for determination of the hydrogen distribution in the wall of hydrogenation reactor has been developed and tested. lt consists of a PC computer, a single chip unit, an I/V converter and an electrochemical hydrogen probe. The construction of the electrochemical hydrogen probe is described and the features of the measured system are given.The diffusion coefficient of 2.25Cr1Mo steel determined with present system was in good agreement with the value in the literature. Experimental results of hydrogen concentration in a wall of hydrogen charged testing autoclave made of AlSl 321 stainless steel are presented. The present system can intelligently display hydrogen amount-of-substance concentration and mass fraction concentration, hydrogen concentration distribution curves in steels, permeation current density curve. An intelligent detection technique can be provided for predicting the susceptibility to hydrogen-induced cracks owing to hydrogen permeation in the wall of hydrogenation reactor in the field.

  4. Finding You on the Internet: an approach for finding on-line presences of people for fraud risk analysis

    NARCIS (Netherlands)

    Been, Henry; Keulen, van Maurice

    2014-01-01

    Fraud risk analysis on data from formal information sources, being a ‘paper reality', suffers from blindness to false information. Moreover, the very act of providing false information is a strong indicator for fraud. The technology presented in this paper provides one step towards the vision of har

  5. On-Line Fault Detection in Wind Turbine Transmission System using Adaptive Filter and Robust Statistical Features

    Directory of Open Access Journals (Sweden)

    Mark Frogley

    2013-01-01

    Full Text Available To reduce the maintenance cost, avoid catastrophic failure, and improve the wind transmission system reliability, online condition monitoring system is critical important. In the real applications, many rotating mechanical faults, such as bearing surface defect, gear tooth crack, chipped gear tooth and so on generate impulsive signals. When there are these types of faults developing inside rotating machinery, each time the rotating components pass over the damage point, an impact force could be generated. The impact force will cause a ringing of the support structure at the structural natural frequency. By effectively detecting those periodic impulse signals, one group of rotating machine faults could be detected and diagnosed. However, in real wind turbine operations, impulsive fault signals are usually relatively weak to the background noise and vibration signals generated from other healthy components, such as shaft, blades, gears and so on. Moreover, wind turbine transmission systems work under dynamic operating conditions. This will further increase the difficulties in fault detection and diagnostics. Therefore, developing advanced signal processing methods to enhance the impulsive signals is in great needs.In this paper, an adaptive filtering technique will be applied for enhancing the fault impulse signals-to-noise ratio in wind turbine gear transmission systems. Multiple statistical features designed to quantify the impulsive signals of the processed signal are extracted for bearing fault detection. The multiple dimensional features are then transformed into one dimensional feature. A minimum error rate classifier will be designed based on the compressed feature to identify the gear transmission system with defect. Real wind turbine vibration signals will be used to demonstrate the effectiveness of the presented methodology.

  6. Using a commercial mathematics software package for on-line analysis at the BNL Accelerator Test Facility

    Energy Technology Data Exchange (ETDEWEB)

    Malone, R.; Wang, X.J.

    1999-06-14

    BY WRITING BOTH A CUSTOM WINDOWS(NTTM) DYNAMIC LINK LIBRARY AND GENERIC COMPANION SERVER SOFTWARE, THE INTRINSIC FUNCTIONS OF MATHSOFT MATHCAD(TM) HAVE BEEN EXTENDED WITH NEW CAPABILITIES WHICH PERMIT DIRECT ACCESS TO THE CONTROL SYSTEM DATABASES OF BROOKHAVEN NATIONAL LABORATORY ACCELERATOR TEST FACILITY. UNDER THIS SCHEME, A MATHCAD WORKSHEET EXECUTING ON A PERSONAL COMPUTER BECOMES A CLIENT WHICH CAN BOTH IMPORT AND EXPORT DATA TO A CONTROL SYSTEM SERVER VIA A NETWORK STREAM SOCKET CONNECTION. THE RESULT IS AN ALTERNATIVE, MATHEMATICALLY ORIENTED VIEW OF CONTROLLING THE ACCELERATOR INTERACTIVELY.

  7. Development of real-time motion capture system for 3D on-line games linked with virtual character

    Science.gov (United States)

    Kim, Jong Hyeong; Ryu, Young Kee; Cho, Hyung Suck

    2004-10-01

    Motion tracking method is being issued as essential part of the entertainment, medical, sports, education and industry with the development of 3-D virtual reality. Virtual human character in the digital animation and game application has been controlled by interfacing devices; mouse, joysticks, midi-slider, and so on. Those devices could not enable virtual human character to move smoothly and naturally. Furthermore, high-end human motion capture systems in commercial market are expensive and complicated. In this paper, we proposed a practical and fast motion capturing system consisting of optic sensors, and linked the data with 3-D game character with real time. The prototype experiment setup is successfully applied to a boxing game which requires very fast movement of human character.

  8. Analysis of Patterns of Interaction and Knowledge Construction in On-Line Learning Environments: A Methodological Strategy

    Directory of Open Access Journals (Sweden)

    Benilde García Cabrero

    2008-05-01

    Full Text Available A model of analysis of interaction and construction of knowledge in educational environments based on computer-mediated communication (CMC is proposed. This proposal considers: 1 the contextual factors that constitute the input and the scenario of interaction, 2 the interaction processes: types of interaction and its contents (Garrison, Anderson and Archer, 2000 as well as the discursive strategies (Lemke, 1997, and 3 learning results that involve the quality of the knowledge constructed by the participants (Gunawardena, Lowe and Anderson, 1997. This model was applied to the analysis of the interaction among a group of participants in two web forums (with or without the presence of a teacher, during the teaching of a PhD in Psychology program. The results show evidence of the model’s viability to describe the patterns of interaction and the levels of construction of knowledge in web forums.

  9. Transient analysis and control of bias magnetic state in the transformer of on-line pulse-width-modulation switching full bridge direct current-direct current converter

    Science.gov (United States)

    Chen, Jiaxin; Guo, Youguang; Zhu, Jianguo; Wei Lin, Zhi

    2012-04-01

    This paper presents a finite element analysis (FEA) based method for analyzing and controlling the bias magnetic state of the transformer of a pulse-width-modulation (PWM) switching full bridge dc-dc converter. A field-circuit indirect coupling method for predicting the transient bias magnetic state is introduced first. To increase flexibility of the proposed method, a novel transformer model which can address not only its basic input-output characteristic, but also the nonlinear magnetizing inductance, is proposed. Both the asymmetric characteristic and the variable laws of the current flowing through the two secondary windings during the period of PWM switching-off state are highlighted. Finally, the peak magnetizing current controlled method based on the on-line magnetizing current computation is introduced. Analysis results show that this method can address the magnetic saturation at winding ends, and hence many previous difficulties, such as the start-up process and asymmetry of power electronics, can be easily controlled.

  10. Automatic On-line Solid-phase Extraction-Electrothermal Atomic Absorption Spectrometry Exploiting Sequential Injection Analysis for Trace Vanadium, Cadmium and Lead Determination in Human Urine Samples.

    Science.gov (United States)

    Giakisikli, Georgia; Ayala Quezada, Alejandro; Tanaka, Junpei; Anthemidis, Aristidis N; Murakami, Hiroya; Teshima, Norio; Sakai, Tadao

    2015-01-01

    A fully automated sequential injection column preconcentration method for the on-line determination of trace vanadium, cadmium and lead in urine samples was successfully developed, utilizing electrothermal atomic absorption spectrometry (ETAAS). Polyamino-polycarboxylic acid chelating resin (Nobias chelate PA-1) packed into a handmade minicolumn was used as a sorbent material. Effective on-line retention of chelate complexes of analytes was achieved at pH 6.0, while the highest elution effectiveness was observed with 1.0 mol L(-1) HNO3 in the reverse phase. Several analytical parameters, like the sample acidity, concentration and volume of the eluent as well as the loading/elution flow rates, have been studied, regarding the efficiency of the method, providing appropriate conditions for the analysis of real samples. For a 4.5 mL sample volume, the sampling frequency was 27 h(-1). The detection limits were found to be 3.0, 0.06 and 2.0 ng L(-1) for V(V), Cd(II) and Pb(II), respectively, with the relative standard deviations ranging between 1.9 - 3.7%. The accuracy of the proposed method was evaluated by analyzing a certified reference material (Seronorm(TM) trace elements urine) and spiked urine samples.

  11. Design and Development of a Relative Humidity and Room Temperature Measurement System with On Line Data Logging Feature for Monitoring the Fermentation Room of Tea Factory

    Directory of Open Access Journals (Sweden)

    Utpal SARMA

    2011-12-01

    Full Text Available The design and development of a Relative Humidity (RH and Room Temperature (RT monitoring system with on line data logging feature for monitoring fermentation room of a tea factory is presented in this paper. A capacitive RH sensor with on chip signal conditioner is taken as RH sensor and a temperature to digital converter (TDC is used for ambient temperature monitoring. An 8051 core microcontroller is the heart of the whole system which reads the digital equivalent of RH data with the help of a 12-bit Analog to Digital (A/D converter and synchronize TDC to get the ambient temperature. The online data logging is achieved with the help of RS-232C communication. Field performance is also studied by installing it in the fermentation room of a tea factory.

  12. On-line Monitoring System for Vapor Recovery in Oil Filling Station%加油站油气回收在线监测系统

    Institute of Scientific and Technical Information of China (English)

    孟振振; 吴锋棒; 张卫华

    2012-01-01

    In order to meet GB20952-2007 requirements and ensure vapor recovery in oil filling station, an on-line monitoring system for vapor recovery was developed. The test results from an oil filling station prove the system advantages of space saving, low cost and easy installation.%开发了加油站油气回收在线监测系统,实现了对加油站油气回收系统的在线监测,满足GB20952-2007的要求.该系统经过在模拟加油站的实验测试,已安装在中国石化北京某加油站试运行,运行效果良好,并具有占用空间小、成本低和施工安装方便的优点.

  13. Devolopment of an intrinsically safe on-line methane detection system%本质安全型甲烷在线检测系统的研制

    Institute of Scientific and Technical Information of China (English)

    李军; 孙世岭

    2009-01-01

    An intrinsically safe on-line methane detection system was designed for closed-cycle monitoring of the gas transfer tube of coal mine. The composition and the realization procedure of the sample handing system, and the characteristics of the infrared methane sensor are described.%针对煤矿输气管道甲烷检测的要求及环境条件的特殊性,设计了一种本质安全型甲烷在线检测系统,成功实现了煤矿输气管道甲烷长期稳定的闭环检测.介绍了样气处理系统的组成和实施方案,以及红外甲烷传感器的特点.

  14. Determination of cadmium in alcohol fuel using Moringa oleifera seeds as a biosorbent in an on-line system coupled to FAAS.

    Science.gov (United States)

    Alves, Vanessa Nunes; Mosquetta, Rafael; Coelho, Nívia Maria Melo; Bianchin, Joyce Nunes; Di Pietro Roux, Kalya Cravo; Martendal, Edmar; Carasek, Eduardo

    2010-01-15

    In this study a new method for determination of cadmium in alcohol fuel using Moringa oleifera seeds as a biosorbent in an on-line preconcentration system coupled to flame atomic absorption spectrometry (FAAS) was developed. Flow and chemical variables of the proposed system were optimized through multivariate designs. The limit of detection for cadmium was 5.50microg L(-1) and the precision was below 2.3% (35.0microg L(-1), n=9). The analytical curve was linear from 5 to 150microg L(-1), with a correlation coefficient of 0.9993. The developed method was successfully applied to spiked alcohol fuel, and accuracy was assessed through recovery tests, with recovery ranging from 97.50 to 100%.

  15. Application of Neural Network in the Measuring System On-line for Water Content of Crude Oil

    Directory of Open Access Journals (Sweden)

    Zengrong Zhao

    2013-03-01

    Full Text Available The aim of this study is to introduce a new way to measure the water content of Crude Oil. In this measurement system, capacitive sensor is used as sensitive element and BP neural network model is adopted to deal with data. Water content and temperature are used as input parameters to set up BP neural network model. By MATLAB simulation, a moisture content of crude oil is forecasted, so that the influence comes from temperature variation is compensated and the accuracy of the measurement result is improved.

  16. Single photon ionization time-of-flight mass spectrometry with a pulsed electron beam pumped excimer VUV lamp for on-line gas analysis: setup and first results on cigarette smoke and human breath.

    Science.gov (United States)

    Mühlberger, F; Streibel, T; Wieser, J; Ulrich, A; Zimmermann, R

    2005-11-15

    Single-photon ionization (SPI) using vacuum ultraviolet (VUV) light produced by an electron beam pumped rare gas excimer source has been coupled to a compact and mobile time-of-flight mass spectrometer (TOFMS). The novel device enables real-time on-line monitoring of organic trace substances in complex gaseous matrixes down to the ppb range. The pulsed VUV radiation of the light source is employed for SPI in the ion source of the TOFMS. Ion extraction is also carried out in a pulsed mode with a short time delay with respect to ionization. The experimental setup of the interface VUV light source/time-of-flight mass spectrometer is described, and the novel SPI-TOFMS system is characterized by means of standard calibration gases. Limits of detection down to 50 ppb for aliphatic and aromatic hydrocarbons were achieved. First on-line applications comprised real-time measurements of aromatic and aliphatic trace compounds in mainstream cigarette smoke, which represents a highly dynamic fluctuating gaseous matrix. Time resolution was sufficient to monitor the smoking process on a puff-by-puff resolved basis. Furthermore, human breath analysis has been carried out to detect differences in the breath of a smoker and a nonsmoker, respectively. Several well-known biomarkers for smoke could be identified in the smoker's breath. The possibility for even shorter measurement times while maintaining the achieved sensitivity makes this new device a promising tool for on-line analysis of organic trace compounds in process gases or biological systems.

  17. Towards automation in protein digestion: Development of a monolithic trypsin immobilized reactor for highly efficient on-line digestion and analysis.

    Science.gov (United States)

    Naldi, Marina; Černigoj, Urh; Štrancar, Ales; Bartolini, Manuela

    2017-05-15

    Reducing experimental variability, limiting contamination and increasing automation are essential goals in the development of reliable analytical platforms for mass spectrometry (MS)-based proteomics. In this work novel trypsin-based monolithic immobilized enzyme reactors (tryp-IMERs), obtained by covalent immobilization on convective interaction media (CIMac™) analytical columns (5mm×5.2mm I.D.), were developed. Notwithstanding the small dimensions, column format allowed the insertion in common high performance liquid chromatography (HPLC) systems, thus avoiding the use of expensive micro- or nano-platforms. Monolith pore diameter and surface chemistry were optimized to achieve high digestion efficiency even with high molecular weight proteins and to avoid protein/peptide adsorption, peak broadening and sample loss. A full characterization of the tryp-IMERs was undertaken to select the best protocol for preparation and type of trypsin. Optimization of the operational and storage conditions was carried out by an off-line approach. On-line studies were performed by setting a multidimensional analytical platform, which included the tryp-IMER, a trapping column, an analytical C4 column and a high resolution hybrid mass spectrometer (ESI-Q-TOF). In the optimized conditions rapid protein digestion (90±9s), high protein coverage (≥60%) and high score values were achieved for five selected sample proteins (cytochrome c, myoglobin and albumins from different sources) differing in molecular size, isoelectric point and accessibility to cleavage sites as well as for a protein mixture of 200ng. The best performing tryp-IMERs showed high sensitivity down to the pmole level. The platform also resulted suitable for the analysis of high-molecular weight proteins such as a pool of human immunoglobulins G (hIgG) and for the high molecular weight fraction of human plasma proteins, which were digested in less than two minutes to an extent similar to that achieved by overnight

  18. Comparison of direct infusion and on-line liquid chromatography/electrospray ionization mass spectrometry for the analysis of nucleic acids.

    Science.gov (United States)

    Huber, C G; Krajete, A

    2000-07-01

    The applicability of ion-pair reversed-phase high-performance liquid chromatography/electrospray ionization mass spectrometry (IP-RP-HPLC/ESI-MS) and direct infusion/ESI-MS to the characterization of nucleic acid mixtures was evaluated by the analysis of the reaction products obtained from solid-phase synthesis of a 39-mer oligonucleotide. IP-RP-HPLC/ESI-MS was performed using 200 microm i.d. capillary columns packed with octadecylated, micropellicular poly(styrene-divinylbenzene) particles and applying gradients of acetonitrile in 50 mM triethylammonium bicarbonate (TEAB). Three different solvent systems were utilized for direct infusion/ESI-MS with removal of metal cations by on-line cation exchange: (1) 10 mM triethylamine (TEA) in 50% aqueous acetonitrile, (2) 2.2 mM TEA, 400 mM hexafluoro-2-propanol (HFIP) in 20% aqueous methanol and (3) 50 mM TEAB in 10% aqueous acetonitrile. Owing to its separation capability, the highest selectivity and specificity were achieved with IP-RP-HPLC/ESI-MS, which, apart form the 39-mer target sequence, allowed the identification of two isobutyryl-protected target sequences and a 10-mer and 20-mer failure sequence. Direct infusion/ESI-MS with TEA-acetonitrile or TEA-HFIP-methanol as solvent revealed signals for the 39-mer in the m/z range 700-1600. The presence of derivatives containing one, two, three and four isobutyryl groups indicated that the hydrolysis of the protecting groups after solid-phase synthesis was not complete. Failure sequences could not be identified by direct infusion/ESI-MS under conditions favoring multiple charging of the analytes owing to the high chemical background and coincidental overlapping of m/z signals. However, efficient charge state reduction upon addition of carbonic acid to the electrosprayed solvent shifted the signals of the 39-mer and derivatives to m/z values >2400 and allowed the detection of seven different failure sequences, ranging from the 8-mer to the 23-mer, in the mixture.

  19. The first target ion source system for the SPIRAL project: results of the on-line tests

    Energy Technology Data Exchange (ETDEWEB)

    Leroy, R.; Bajeat, O.; Bertrand, P.; Foury, P.; Gaubert, G.; Huguet, Y.; Jardin, P.; Lecesne, N.; Lewitowicz, M.; Marry, C.; Maunoury, L.; Pacquet, J.Y.; Saint-Laurent, M.G.; Sortais, P.; Villari, A.C.C. [Grand Accelerateur National d' Ions Lourds (GANIL), 14 - Caen (France); Angelique, J.C.; Orr, N.A. [Laboratoire de Physique Corpusculaire (CNRS/IN2P3), ISMRA, 14 - Caen (France); Blank, B. [CENBG, Centre d' Etudes Nucleaires de Bordeaux Gradignan, 33 (France); Ducourtieux, M.; Kandri-Rody, S.; Obert, J.; Proust, J. [Institut de Physique Nucleaire, (IN2P3/CNRS) 91 - Orsay (France); Lepine, A. [IFUSP, C.P., Sao Paulo (Brazil)

    1999-07-01

    The first radioactive ion beams of the SPIRAL facility will be produced by the nuclear reactions of the primary beam on an external target. In a first step, a target ion source system (TISS) has been developed with the goal to produce noble gas radioactive ion beams. This TISS is based on the coupling of a carbon external target with a permanent magnet ECR ion source called NANOGAN 2 and has been tested on the SIRa separator. The target is heated by the primary beam and by an extra ohmic heating up to 2000 K to allow a good diffusion of the radioactive atoms. The atoms are then ionised in the ECR ion source, extracted from the source, selected and driven to a collection point where they are identified. The results of these tests will be presented. A description of the TISS in the production cave will also be done. (authors)

  20. Telematics System dedicated for Provisioning of On-Line Information about Predicted Occupancy of Highway Parking Areas

    Directory of Open Access Journals (Sweden)

    Tomas Zelinka

    2014-08-01

    Full Text Available More and more often occurs problem with the lack of parking places for trucks over 3.5t, which is related to the increase in the intensity of freight transport. Consequently this can lead to very dangerous situations with parking of trucks because drivers do not have information about the occupancy of the nearest parking. The paper presents an intelligent transportation system, which provides information about the predicted occupancy of parking lots to truck drivers. Providing this information leads to optimizing the use of existing parking areas on the highway network and also makes it easier for drivers to deciding on a suitable location for parking, which ultimately contributes to the fluency and safety of traffic.

  1. On-line parallel reversed phase two-dimensional liquid chromatography for high-throughput analysis of complex proteomic samples

    Institute of Scientific and Technical Information of China (English)

    WANG Zhicong; ZHANG Qinghe; LI Tong; ZHAO Zhongyi; ZHANG Weibing

    2006-01-01

    A comprehensive two-dimensional liquid chromatographic system (2D SCX/RP) is constructed with a 10-port-2-way valve using strong cation exchange chromatography (Hypersil SCX, 100 mm×4.6 mm I.D.) followed by reversed phase chromatography (Hypersil BDS C18, 15 mm×4.6 mm I.D.) to separate the complex peptides from globin peptic hydrolysate. After the sample was loaded on the SCX column, the phosphate buffer (pH 4.0) was used to elute the peptides. Then, elutes flowed through the interface and the peptides focused on the head of the trapping columns (Hypersil BDS C18, 15 mm×4.6 mm I.D.) but salt passed into the waste. After the valve was switched, the samples were flushed with a backward flow into the RP analytical column. The peptides on the SCX were eluted with 12 discontinuous steps linearly increasing salt concentrations. The peptides enriched on the trapping column were desalted and separated by the RP columns. The resolution and the resolved peaks of the 2D SCX/RP system were greatly increased and the total peak capacity reached as high as 2280.

  2. Development of a video-based slurry sensor for on-line ash analysis. Sixth quarterly technical progress report, January 1, 1996--March 31, 1996

    Energy Technology Data Exchange (ETDEWEB)

    Adel, G.T.; Luttrell, G.H.

    1996-04-28

    Automatic control of fine coal cleaning circuits has traditionally been limited by the lack of sensors for on-line ash analysis. Although several nuclear-based analyzers are available, none have seen widespread acceptance. This is largely due to the fact that nuclear sensors are expensive and tend to be influenced by changes in seam type and pyrite content. Recently, researchers at VPI&SU have developed an optical sensor for phosphate analysis. The sensor uses image processing technology to analyze video images of phosphate ore. It is currently being used by PCS Phosphate for off-line analysis of dry flotation concentrate. The primary advantages of optical sensors over nuclear sensors are that they are significantly cheaper, are not subject to measurement variations due to changes in high atomic number minerals, are inherently safer and require no special radiation permitting. The purpose of this work is to apply the knowledge gained in the development of an optical phosphate analyzer to the development of an on-line ash analyzer for fine coal slurries. During the past quarter, calibration tests were conducted on-site at the Middle Fork coal preparation plant owned and operated by Pittston Coal Company. After several plant visits, a consistent sensor calibration was obtained with approximately 95% of all samples analyzed falling within {plus_minus}2% ash of the best fit calibration line. The resolution of the optical analyzer was found to be approximately 0.5% ash per gray level increment. A linear neural network learning algorithm was found to be the most appropriate method for calibrating the sensor. The sensor now appears to be ready for installation and long-term testing at the Middle Fork test site.

  3. A new aerosol collector for on-line analysis of particulate organic matter: the Aerosol Collection Module (ACM)

    Science.gov (United States)

    Hohaus, T.; Trimborn, D.; Kiendler-Scharr, A.; Gensch, I.; Laumer, W.; Kammer, B.; Andres, S.; Boudries, H.; Smith, K. A.; Worsnop, D. R.; Jayne, J. T.

    2010-03-01

    In many environments organic matter significantly contributes to the composition of atmospheric aerosol particles influencing its properties. Detailed chemical characterization of ambient aerosols is critical in order to understand the formation process, composition, and properties of aerosols in the atmosphere. However, current analytical methods are far from full speciation of organic aerosols and often require long sampling times. Offline methods are also subjected to artifacts during aerosol collection and storage. In the present work a new technique for quasi-online compound specific measurements of organic aerosol particles was developed. The Aerosol Collection Module (ACM) is designed to sample, collect and transfer gasified atmospheric aerosol particles. The system focuses particles into a beam which is directed to a cooled sampling surface. The sampling takes places in a high vacuum environment where the gas phase from the sample volume is removed. After collection the particle sample is evaporated from the collection surface through heating and transferred to a detector. For laboratory characterization the ACM was interfaced with a Gas Chromatograph Mass Spectrometer system (GC-MS). The particle collection efficiency, gas phase transfer efficiency, and linearity of the ACM-GC-MS were determined using laboratory generated octadecane aerosols. The ACM-GC-MS is linear over the investigated mass range of 10 to 100 ng and a recovery rate of 100% was found for octadecane particles. The ACM-GC-MS was applied to investigate secondary organic aerosol (SOA) formed from β-pinene oxidation. Nopinone, myrtanal, myrtenol, 1-hydroxynopinone, 3-oxonopinone, 3,7-dihydroxynopinone, and bicyclo[3,1,1]hept-3-ene-2-one were found as products in the SOA. The ACM results are compared to quartz filter samples taken in parallel to the ACM measurements. First measurements of ambient atmospheric aerosols are presented.

  4. A new aerosol collector for on-line analysis of particulate organic matter: the Aerosol Collection Module (ACM

    Directory of Open Access Journals (Sweden)

    T. Hohaus

    2010-03-01

    Full Text Available In many environments organic matter significantly contributes to the composition of atmospheric aerosol particles influencing its properties. Detailed chemical characterization of ambient aerosols is critical in order to understand the formation process, composition, and properties of aerosols in the atmosphere. However, current analytical methods are far from full speciation of organic aerosols and often require long sampling times. Offline methods are also subjected to artifacts during aerosol collection and storage.

    In the present work a new technique for quasi-online compound specific measurements of organic aerosol particles was developed. The Aerosol Collection Module (ACM is designed to sample, collect and transfer gasified atmospheric aerosol particles. The system focuses particles into a beam which is directed to a cooled sampling surface. The sampling takes places in a high vacuum environment where the gas phase from the sample volume is removed. After collection the particle sample is evaporated from the collection surface through heating and transferred to a detector.

    For laboratory characterization the ACM was interfaced with a Gas Chromatograph Mass Spectrometer system (GC-MS. The particle collection efficiency, gas phase transfer efficiency, and linearity of the ACM-GC-MS were determined using laboratory generated octadecane aerosols. The ACM-GC-MS is linear over the investigated mass range of 10 to 100 ng and a recovery rate of 100% was found for octadecane particles.

    The ACM-GC-MS was applied to investigate secondary organic aerosol (SOA formed from β-pinene oxidation. Nopinone, myrtanal, myrtenol, 1-hydroxynopinone, 3-oxonopinone, 3,7-dihydroxynopinone, and bicyclo[3,1,1]hept-3-ene-2-one were found as products in the SOA. The ACM results are compared to quartz filter samples taken in parallel to the ACM measurements. First measurements of ambient atmospheric aerosols are presented.

  5. Looking into individual coffee beans during the roasting process: direct micro-probe sampling on-line photo-ionisation mass spectrometric analysis of coffee roasting gases.

    Science.gov (United States)

    Hertz-Schünemann, Romy; Streibel, Thorsten; Ehlert, Sven; Zimmermann, Ralf

    2013-09-01

    A micro-probe (μ-probe) gas sampling device for on-line analysis of gases evolving in confined, small objects by single-photon ionisation time-of-flight mass spectrometry (SPI-TOFMS) was developed. The technique is applied for the first time in a feasibility study to record the formation of volatile and flavour compounds during the roasting process within (inside) or in the direct vicinity (outside) of individual coffee beans. A real-time on-line analysis of evolving volatile and semi-volatile organic compounds (VOC and SVOC) as they are formed under the mild pyrolytic conditions of the roasting process was performed. The soft-ionisation mass spectra depict a molecular ion signature, which is well corresponding with the existing knowledge of coffee roasting and evolving compounds. Additionally, thereby it is possible to discriminate between Coffea arabica (Arabica) and Coffea canephora (Robusta). The recognized differences in the roasting gas profiles reflect the differences in the precursor composition of the coffee cultivars very well. Furthermore, a well-known set of marker compounds for Arabica and Robusta, namely the lipids kahweol and cafestol (detected in their dehydrated form at m/z 296 and m/z 298, respectively) were observed. If the variation in time of different compounds is observed, distinctly different evolution behaviours were detected. Here, phenol (m/z 94) and caffeine (m/z 194) are exemplary chosen, whereas phenol shows very sharp emission peaks, caffeine do not have this highly transient behaviour. Finally, the changes of the chemical signature as a function of the roasting time, the influence of sampling position (inside, outside) and cultivar (Arabica, Robusta) is investigated by multivariate statistics (PCA). In summary, this pilot study demonstrates the high potential of the measurement technique to enhance the fundamental knowledge of the formation processes of volatile and semi-volatile flavour compounds inside the individual coffee bean.

  6. Trace analysis of anions in organic matrices by ion chromatography coupled with a novel reversed-phase column for on-line sample pretreatment

    Institute of Scientific and Technical Information of China (English)

    Ying Ying Zhong; Wen Fang Zhou; Xue Ling Zeng; Ming Li Ye; Yan Zhu

    2011-01-01

    An ion chromatography (IC) system coupled with on-line column-switching technique was used to determine anions of μg/g levels in organic chemicals of analytical reagent grade. A novel polystyrene-divinylbenzene-carbon nanotube (PS-DVB-CNT) stationary phase was utilized for matrix elimination. A calibration study was conducted by preparing and analyzing eight concentrations (between 10 and 5000 μg/L) of eight standards in deionized water. The linearity was between 0.9978 and 1. And the detection limits ranged from 1.54 μg/L to 10.02 μg/L. A spiking study was performed on two representative organic chemicals. The recoveries were between 84.3% and 119.6%.

  7. An integrated sample pretreatment platform for quantitative N-glycoproteome analysis with combination of on-line glycopeptide enrichment, deglycosylation and dimethyl labeling

    Energy Technology Data Exchange (ETDEWEB)

    Weng, Yejing; Qu, Yanyan; Jiang, Hao; Wu, Qi [National Chromatographic Research and Analysis Center, Key Laboratory of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023 (China); University of the Chinese Academy of Sciences, Beijing 100039 (China); Zhang, Lihua, E-mail: lihuazhang@dicp.ac.cn [National Chromatographic Research and Analysis Center, Key Laboratory of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023 (China); Yuan, Huiming [National Chromatographic Research and Analysis Center, Key Laboratory of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023 (China); Zhou, Yuan [National Chromatographic Research and Analysis Center, Key Laboratory of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023 (China); University of the Chinese Academy of Sciences, Beijing 100039 (China); Zhang, Xiaodan; Zhang, Yukui [National Chromatographic Research and Analysis Center, Key Laboratory of Separation Science for Analytical Chemistry, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023 (China)

    2014-06-23

    Highlights: • An integrated platform for quantitative N-glycoproteome analysis was established. • On-line enrichment, deglycosylation and labeling could be achieved within 160 min. • A N{sub 2}-assisted interface was applied to improve the compatibility of the platform. • The platform exhibited improved quantification accuracy, precision and throughput. - Abstract: Relative quantification of N-glycoproteomes shows great promise for the discovery of candidate biomarkers and therapeutic targets. The traditional protocol for quantitative analysis of glycoproteomes is usually off-line performed, and suffers from long sample preparation time, and the risk of sample loss or contamination due to manual manipulation. In this study, a novel integrated sample preparation platform for quantitative N-glycoproteome analysis was established, with combination of online N-glycopeptide capture by a HILIC column, sample buffer exchange by a N{sub 2}-assisted HILIC–RPLC interface, deglycosylation by a hydrophilic PNGase F immobilized enzymatic reactor (hIMER) and solid dimethyl labeling on a C18 precolumn. To evaluate the performance of such a platform, two equal aliquots of immunoglobulin G (IgG) digests were sequentially pretreated, followed by MALDI-TOF MS analysis. The signal intensity ratio of heavy/light (H/L) labeled deglycosylated peptides with the equal aliquots was 1.00 (RSD = 6.2%, n = 3), much better than those obtained by the offline protocol, with H/L ratio as 0.76 (RSD = 11.6%, n = 3). Additionally, the total on-line sample preparation time was greatly shortened to 160 min, much faster than that of offline approach (24 h). Furthermore, such an integrated pretreatment platform was successfully applied to analyze the two kinds of hepatocarcinoma ascites syngeneic cell lines with high (Hca-F) and low (Hca-P) lymph node metastasis rates. For H/L labeled Hca-P lysates with the equal aliquots, 99.6% of log 2 ratios (H/L) of quantified glycopeptides ranged from −1

  8. On-Line Pattern Analysis and Recognition System. OLPARS VI. Software Reference Manual,

    Science.gov (United States)

    1982-06-18

    TIPVDV TIPMN +ADUPCII PANR NOICOA AD"PC ADINCY INSINT IN"PS INSRET TISCOP TICV TIGHDR TI6JiN + APEND CRANDIS D’JEC NAKEREE HEASXFRAi IIOVEC NRSTNBR...TRMIS" ALL VEC FILPJT INSINT IN"Pi IKSRET PACKI TRWPUT V6VEC +PRTDS ALNCPR INSCNR INSINT INSPG ItISRET TISCOP TiPVAP TIPCOP TIPNAM + APEND DANDE ANYTHING

  9. On-line Monitoring System of Circulating Current of XLPE Cables%XLPE电缆金属护套环流在线监测系统

    Institute of Scientific and Technical Information of China (English)

    喻世根; 张亮; 李锰; 吴畏

    2011-01-01

    XLPE cable has been widely applied in the grid because of its good electrical properties. Its insulation state directly relates to the safe and reliable operation of power system, how to effectively monitor the insulation state of XLPE cables is very important for power system. In order to meet the needs of power system, XLPE cables metal sheath circulation current on-line monitoring system is designed based on LabVIEW and described the hardware and software designed methods in this paper.%XLPE电缆由于其良好的电气性能在电网中得到了广泛地应用,XLPE电缆的绝缘状况直接影响到电力系统的安全和稳定,如何有效地监测XLPE电缆的绝缘状态对电力系统的安全稳定运行意义重大.为了满足电力系统的需要,有效地监测电缆绝缘状况,以LabVIEW图形可视化编程软件作为开发工具,设计了XLPE电缆金属护套环流在线监测系统,以此监测电缆的绝缘状况,文中阐述了监测系统的硬件组成和软件设计方法.

  10. Product of Likelihood Ratio Scores Fusion of Dynamic Face, Text Independent Speech and On-line Signature Based Biometrics Verification Application Systems

    Directory of Open Access Journals (Sweden)

    Mohamed SOLTANE

    2015-09-01

    Full Text Available In this paper, the use of finite Gaussian mixture modal (GMM tuned using Expectation Maximization (EM estimating algorithms for score level data fusion is proposed. Automated biometric systems for human identification measure a “signature” of the human body, compare the resulting characteristic to a database, and render an application dependent decision. These biometric systems for personal authentication and identification are based upon physiological or behavioral features which are typically distinctive, Multi-biometric systems, which consolidate information from multiple biometric sources, are gaining popularity because they are able to overcome limitations such as non-universality, noisy sensor data, large intra-user variations and susceptibility to spoof attacks that are commonly encountered in mono modal biometric systems. Simulation result show that finite mixture modal (GMM is quite effective in modelling the genuine and impostor score densities, fusion based the product of Likelihood Ratio achieves a significant performance on eNTERFACE 2005 multi-biometric database based on dynamic face, on-line signature and text independent speech modalities.

  11. Analysis of drug-protein binding using on-line immunoextraction and high-performance affinity microcolumns: Studies with normal and glycated human serum albumin.

    Science.gov (United States)

    Matsuda, Ryan; Jobe, Donald; Beyersdorf, Jared; Hage, David S

    2015-10-16

    A method combining on-line immunoextraction microcolumns with high-performance affinity chromatography (HPAC) was developed and tested for use in examining drug-protein interactions with normal or modified proteins. Normal human serum albumin (HSA) and glycated HSA were used as model proteins for this work. High-performance immunoextraction microcolumns with sizes of 1.0-2.0 cm × 2.1mm i.d. and containing anti-HSA polyclonal antibodies were developed and tested for their ability to bind normal HSA or glycated HSA. These microcolumns were able to extract up to 82-93% for either type of protein at 0.05-0.10 mL/min and had a binding capacity of 0.34-0.42 nmol HSA for a 1.0 cm × 2.1mm i.d. microcolumn. The immunoextraction microcolumns and their adsorbed proteins were tested for use in various approaches for drug binding studies. Frontal analysis was used with the adsorbed HSA/glycated HSA to measure the overall affinities of these proteins for the drugs warfarin and gliclazide, giving comparable values to those obtained previously using similar protein preparations that had been covalently immobilized within HPAC columns. Zonal elution competition studies with gliclazide were next performed to examine the specific interactions of this drug at Sudlow sites I and II of the adsorbed proteins. These results were also comparable to those noted in prior work with covalently immobilized samples of normal HSA or glycated HSA. These experiments indicated that drug-protein binding studies can be carried out by using on-line immunoextraction microcolumns with HPAC. The same method could be used in the future with clinical samples and other drugs or proteins of interest in pharmaceutical studies or biomedical research.

  12. Design and construction of a prototype advanced on-line fuel burn-up monitoring system for the modular pebble bed reactor

    Energy Technology Data Exchange (ETDEWEB)

    Su, Bingjing; Hawari, Ayman, I.

    2004-03-30

    Modular Pebble Bed Reactor (MPBR) is a high temperature gas-cooled nuclear power reactor currently under study as a next generation reactor system. In addition to its inherently safe design, a unique feature of this reactor is its multi-pass fuel circulation in which the fuel pebbles are randomly loaded and continuously cycled through the core until they reach their prescribed End-of-Life burn-up limit. Unlike the situation with a conventional light water reactor, depending solely on computational methods to perform in-core fuel management for MPBR will be highly inaccurate. An on-line measurement system is needed to accurately assess whether a given pebble has reached its End-of-Life burn-up limit and thereby provide an on-line, automated go/no-go decision on fuel disposition on a pebble-by-pebble basis. This project investigated approaches to analyzing fuel pebbles in real time using gamma spectroscopy and possibly using passive neutron counting of spontaneous fission neutrons to provide the speed, accuracy, and burn-up range required for burnup determination of MPBR. It involved all phases necessary to develop and construct a burn-up monitor, including a review of the design requirements of the system, identification of detection methodologies, modeling and development of potential designs, and finally, the construction and testing of an operational detector system. Based upon the research work performed in this project, the following conclusions are made. In terms of using gamma spectrometry, two possible approaches were identified for burnup assay. The first approach is based on the measurement of the absolute activity of Cs-137. However, due to spectral interference and the need for absolute calibration of the spectrometer, the uncertainty in burnup determination using this approach was found to range from {approx} {+-}40% at beginning of life to {approx} {+-}10% at the discharge burnup. An alternative approach is to use a relative burnup indicator. In this

  13. Laboratory Earth Under the Lens: Diachronic Evaluation of an Integrated Graduate-Level On-Line Earth System Science Course Series for K-12 Educators

    Science.gov (United States)

    Low, R.; Gosselin, D. C.; Haney, C.; Larson-Miller, C.; Bonnstetter, R.; Mandryk, C.

    2012-12-01

    Wilcoxan Signed Ranks Test is included in the battery of assessments to ensure that the courses achieve a statistically significant increase in participants' beliefs about their personal science teaching efficacy. The research design also includes the analysis of concept maps and content mastery assignments to assist in documentation of a teacher's transition from mastery of novice to expert knowledge. Content-based, course-specific pre and post knowledge surveys are included in the battery of assessments. In the analysis of on-line discussions, the project employs a textual analysis technique outlined in "The Rhetoric of Social Intervention," (RSI) (Opt and Gring 2009). RSI provides a promising analytical framework, especially when examining the development of understanding of scientific topics with societal implications, such as sustainability and climate change. The session provides a description of the integrated research design and data collection and analysis in the first year of this project.

  14. Systematic optimisation and evaluation of on-line, off-line and stop-flow comprehensive hydrophilic interaction chromatography×reversed phase liquid chromatographic analysis of procyanidins, part I: theoretical considerations.

    Science.gov (United States)

    Kalili, Kathithileni M; de Villiers, André

    2013-05-10

    Comprehensive two-dimensional liquid chromatography (LC×LC) provides significantly improved separation for complex real-life samples. LC×LC can be performed in one of three different ways, using on-line, off-line, or stop-flow configurations. We have previously shown how off-line comprehensive hydrophilic interaction chromatography (HILIC)×reversed-phase liquid chromatography (RP-LC) provides a powerful separation system for procyanidins (PCs), one of the most complex fractions of natural phenolics. In the current contribution, a systematic approach for the optimisation and evaluation of each of the LC×LC methodologies is presented using HILIC×RP-LC analysis of PCs as application. Optimisation was performed using the peak capacities of individual one-dimensional separations measured for different gradient times and flow rates and their combination in each of the three LC×LC modes by taking into account the effects of first dimension under-sampling, the degree of orthogonality between the two dimensions and additional band broadening associated with stop-flow analysis. The performance of all three methods is compared in terms of practical peak capacities, analysis times and peak production rates. One-dimensional LC provided the best performance for separations requiring relatively low peak capacities, whereas the on-line LC×LC system was advantageous for required practical peak capacities up to ~600. For higher resolution, the off-line or stop-flow systems should be used. Especially noteworthy is the fact that, due to slow diffusion of PCs, the contribution of stop-flow to first dimension band broadening was negligible for stop-flow times of up to 15min. In a separate contribution, the experimental verification of the findings of this study will be reported.

  15. Determination of carbofuran in surface water and biological tissue by sol-gel immunoaffinity extraction and on-line preconcentration/HPLC/UV analysis.

    Science.gov (United States)

    Vera-Avila, Luz E; Márquez-Lira, Bani P; Villanueva, Marcos; Covarrubias, Rosario; Zelada, Gustavo; Thibert, Valérie

    2012-01-15

    A selective and simple analytical method for the trace level determination of carbofuran in complex environmental and biological samples was developed based on immunoaffinity extraction (IAE) followed by on-line preconcentration and HPLC/UV analysis of the purified extract. The immunosorbent for IAE was prepared by sol-gel encapsulation of monoclonal anti-carbofuran antibodies, and was fully characterized for capacity, repeatability, binding strength, binding kinetics and cross-reactivity. Method performance was evaluated with two different types of difficult samples: dam water and methanolic extracts of epithelial cervical-uterine tissue. Linear behavior and quantitative recoveries were obtained from the analysis of samples spiked with carbofuran at 0.2-4 ng/mL (dam water, 50 mL samples) and 10-40 ng/mL (biological tissue extract, 2 mL samples). RSD (n=7) and detection limits were, respectively, 10.1% (spike 0.40 ng/mL) and 0.13 ng/mL for dam water; 8.5% (spike 20 ng/mL) and 5 ng/mL for the biological tissue extract. The excellent sample purification achieved with the IAE column allows precise and accurate determination of carbofuran in complex matrices, even when using non-selective UV detection in the chromatographic analysis.

  16. Demonstration of a Novel Synchrophasor-based Situational Awareness System: Wide Area Power System Visualization, On-line Event Replay and Early Warning of Grid Problems

    Energy Technology Data Exchange (ETDEWEB)

    Rosso, A.

    2012-12-31

    Since the large North Eastern power system blackout on August 14, 2003, U.S. electric utilities have spent lot of effort on preventing power system cascading outages. Two of the main causes of the August 14, 2003 blackout were inadequate situational awareness and inadequate operator training In addition to the enhancements of the infrastructure of the interconnected power systems, more research and development of advanced power system applications are required for improving the wide-area security monitoring, operation and planning in order to prevent large- scale cascading outages of interconnected power systems. It is critically important for improving the wide-area situation awareness of the operators or operational engineers and regional reliability coordinators of large interconnected systems. With the installation of large number of phasor measurement units (PMU) and the related communication infrastructure, it will be possible to improve the operators’ situation awareness and to quickly identify the sequence of events during a large system disturbance for the post-event analysis using the real-time or historical synchrophasor data. The purpose of this project was to develop and demonstrate a novel synchrophasor-based comprehensive situational awareness system for control centers of power transmission systems. The developed system named WASA (Wide Area Situation Awareness) is intended to improve situational awareness at control centers of the power system operators and regional reliability coordinators. It consists of following main software modules: • Wide-area visualizations of real-time frequency, voltage, and phase angle measurements and their contour displays for security monitoring. • Online detection and location of a major event (location, time, size, and type, such as generator or line outage). • Near-real-time event replay (in seconds) after a major event occurs. • Early warning of potential wide-area stability problems. The system has been

  17. Description and characterization of an on-line system for long-term measurements of isoprene, methyl vinyl ketone, and methacrolein in ambient air.

    Science.gov (United States)

    Komenda, M; Schaub, A; Koppmann, R

    2003-05-02

    In this work we present a detailed technical description of the system that was set up for long-term on-line measurements of isoprene and two of its major degradation products, methyl vinyl ketone and methacrolein in order to provide a better understanding of the role of forest stands as a complex source of reactive trace gases into the troposphere and to elucidate the role of forests as chemical reactors. Volatile organic compounds (VOCs) are preconcentrated on cartridges containing a package of two solid adsorbents (Tenax TA and Carbopack X). Ozone removal is performed prior to sampling by titration with nitrogen monoxide. For the calibration and characterization of the system, a diffusion source was built to produce standard gas mixtures of up to 16 different compounds with mixing ratios at tens ppt (parts per trillion) level mixing ratios and high accuracy. The developed system allows a reliable quantification of these VOCs (detection limit approximately 10 ppt, reproducibility approximately 5%) with a high temporal resolution (approximately 30 min) and has proven to be stable and run automatically without major maintainence.

  18. Automated Analysis of Oxytocin by On-Line in-Tube Solid-Phase Microextraction Coupled with Liquid Chromatography-Tandem Mass Spectrometry

    Directory of Open Access Journals (Sweden)

    Eri Moriyama

    2015-06-01

    Full Text Available A simple and sensitive method for the analysis of oxytocin was developed using automated on-line in-tube solid-phase microextraction (SPME coupled with liquid chromatography-tandem mass spectrometry (LC–MS/MS. Oxytocin was separated within 3 min on a Zorbax Eclipse XDB-C8 column, with water/methanol (10/90, v/v as the mobile phase at a flow rate of 0.2 mL min−1. Electrospray ionization conditions in the positive ion mode were optimized for MS/MS detection by multiple reaction monitoring. The optimum in-tube SPME conditions were 20 draw/eject cycles of 40 µL sample at a flow rate of 250 µL min−1 using a Supel-Q PLOT capillary column as an extraction device. The extracted oxytocin was easily desorbed from the capillary by passage of the mobile phase, and no carryover was observed. The calibration curves for oxytocin were linear (r = 0.9981 in the range of 0−5.0 ng mL−1, and the relative standard deviations at each point were below 14.7% (n = 3. The limit of detection of this method was 4.0 pg mL−1, and its sensitivity was 58-fold higher than that of the direct injection method. This method was applied successfully to the analysis of oxytocin in saliva samples without any other interference peaks.

  19. On-line analysis of secondary ozonides from cyclohexene and D-limonene ozonolysis using atmospheric sampling townsend discharge ionization mass spectrometry

    Science.gov (United States)

    Nøjgaard, J. K.; Nørgaard, A. W.; Wolkoff, P.

    An on-line technique has been developed for analysis of gas-phase oxidation products formed in a reaction flow tube using different reaction times, concentrations and humidities. Products of ozonolysis, including thermally labile secondary ozonides (SOZ), were directly introduced into an atmospheric sampling townsend discharge ionization (ASTDI) source coupled to a triple quadrupole mass spectrometer (MS). Instant changes in the product composition were monitored in the total-ion chromatogram, or by fragment ions in the collision activated dissociation mass spectra by use of MS/MS scan techniques. Assignment of the individual ions was accomplished by inspection of the products' mass spectra obtained by pre-concentration of the gas phase on a dedicated short column followed by chromatographic analysis. The observed reaction products correspond to those identified with other techniques. Of relevance for future mechanistic modelling, is the point that conditions of excess D-limonene favoured the formation of the D-limonene SOZ (major product), which was observed to be quite stable in dry and humid air, without oxidants. The D-limonene/ozone ratio was observed to be crucial for the stability of the SOZ, because it is prone to ozonolysis, and no SOZ could be detected in completely reacted 1:1 mixtures.

  20. A new method for change-point detection developed for on-line analysis of the heart beat variability during sleep

    Science.gov (United States)

    Staudacher, M.; Telser, S.; Amann, A.; Hinterhuber, H.; Ritsch-Marte, M.

    2005-04-01

    We present a novel scaling-dependent measure for times series analysis, the progressive detrended fluctuation analysis (PDFA). Since this method progressively includes and analyzes all data points of the time series, it is suitable for on-line change-point detection: Sudden changes in the statistics of the data points, in the type of correlation or in the statistical variance, or both, are reliably indicated and localized in time. This is first shown for numerous artificially generated data sets of Gaussian random numbers. Also time series with various non-stationarities, such as non-polynomial trends and “spiking”, are included as examples. Although generally applicable, our method was specifically developed as a tool for numerical sleep evaluation based on heart rate variability in the ECG-channel of polysomnographic whole night recordings. It is demonstrated that PDFA can detect specific sleep stage transitions, typically ascending transitions involving sympathetic activation as for example short episodes of wakefulness, and that the method is capable to discern between NREM sleep and REM sleep.

  1. On-line preconcentration system using a microcolumn packed with Alizarin Red S-modified alumina for zinc determination by flame atomic absorption spectrometry

    Directory of Open Access Journals (Sweden)

    A.M. Haji Shabani

    2009-01-01

    Full Text Available A simple and sensitive on-line flow injection system for determination of zinc with FAAS has been described. The method is based on the separation and preconcentration of zinc on a microcolumn of immobilized Alizarin Red S on alumina. The adsorbed analyte is then eluted with 250 µL of nitric acid (1 mol L-1 and is transported to flame atomic absorption spectrometer for quantification. The effect of pH, sample and eluent flow rates and presence of various cations and anions on the retention of zinc was investigated. The sorption of zinc was quantitative in the pH range of 5.5-8.5. For a sample volume of 25 mL an enrichment factor of 144 and a detection limit (3S of 0.2 µg L-1 was obtained. The precision (RSD, n=7 was 3.0% at the 20 µg L-1 level. The developed system was successfully applied to the determination of zinc in water samples, hair, urine and saliva.

  2. 金属氧化锌避雷器在线监测系统的设计%Design of On-line Monitoring System for MOA

    Institute of Scientific and Technical Information of China (English)

    文桦; 张亚军

    2014-01-01

    以微处理器MSP430为核心,由泄漏电流采集、雷击计数脉冲、无线收/发控制、LCD显示等电路组成,设计了一种金属氧化锌避雷器(MOA)阻性漏电流在线检测系统。系统通过对MOA阻性漏电流的实时检测,并将检测结果发射到终端监控中心,实现对MOA运行状态的在线监测。%A kind of monitoring system for MOA ( Metal-oxide surge Arrester ) resistance leakage current was de-signed.In the design, the chip MSP430 is used as the controller .The system was consisted of the acquisition of leak-age current ,the count pulse of lightning arrester ,wireless receiving /transmitting control ,LCD display and so on .The on-line monitoring of MOA can be effectively realized by real-time detecting the resistive leakage current of MOA , and sending it to the RF receive device by wireless .

  3. Design of an expert system based on neuro-fuzzy inference analyzer for on-line microstructural characterization using magnetic NDT method

    Energy Technology Data Exchange (ETDEWEB)

    Ghanei, S., E-mail: Sadegh.Ghanei@yahoo.com [Department of Materials Engineering, Faculty of Engineering, Ferdowsi University of Mashhad, Azadi Square, Mashhad (Iran, Islamic Republic of); Vafaeenezhad, H. [Centre of Excellence for High Strength Alloys Technology (CEHSAT), School of Metallurgical and Materials Engineering, Iran University of Science and Technology (IUST), Narmak, Tehran (Iran, Islamic Republic of); Kashefi, M. [Department of Materials Engineering, Faculty of Engineering, Ferdowsi University of Mashhad, Azadi Square, Mashhad (Iran, Islamic Republic of); Eivani, A.R. [Centre of Excellence for High Strength Alloys Technology (CEHSAT), School of Metallurgical and Materials Engineering, Iran University of Science and Technology (IUST), Narmak, Tehran (Iran, Islamic Republic of); Mazinani, M. [Department of Materials Engineering, Faculty of Engineering, Ferdowsi University of Mashhad, Azadi Square, Mashhad (Iran, Islamic Republic of)

    2015-04-01

    Tracing microstructural evolution has a significant importance and priority in manufacturing lines of dual-phase steels. In this paper, an artificial intelligence method is presented for on-line microstructural characterization of dual-phase steels. A new method for microstructure characterization based on the theory of magnetic Barkhausen noise nondestructive testing method is introduced using adaptive neuro-fuzzy inference system (ANFIS). In order to predict the accurate martensite volume fraction of dual-phase steels while eliminating the effect and interference of frequency on the magnetic Barkhausen noise outputs, the magnetic responses were fed into the ANFIS structure in terms of position, height and width of the Barkhausen profiles. The results showed that ANFIS approach has the potential to detect and characterize microstructural evolution while the considerable effect of the frequency on magnetic outputs is overlooked. In fact implementing multiple outputs simultaneously enables ANFIS to approach to the accurate results using only height, position and width of the magnetic Barkhausen noise peaks without knowing the value of the used frequency. - Highlights: • New NDT system for microstructural evaluation based on MBN using ANFIS modeling. • Sensitivity of magnetic Barkhausen noise to microstructure changes of the DP steels. • Accurate prediction of martensite by feeding multiple MBN outputs simultaneously. • Obtaining the modeled output without knowing the amount of the used frequency.

  4. Novel analytical approach to monitoring advanced glycosylation end products in human serum with on-line spectrophotometric and spectrofluorometric detection in a flow system.

    Science.gov (United States)

    Wróbel, K; Wróbel, K; Garay-Sevilla, M E; Nava, L E; Malacara, J M

    1997-09-01

    We proposed a simple analytical procedure for measurement of serum advanced glycosylation end products (AGEs) based on simultaneous detection of low-molecular-mass peptides and AGEs with a flow system and two detectors connected on-line: spectrophotometric for peptides (lambda = 280 nm) and spectrofluorometric for AGEs (lambda ex = 247 nm, lambda em = 440 nm). Sample pretreatment was carried out in microcentrifuge tubes: Serum (20 microL) was deproteinized with trichloroacetic acid (480 microL, 0.15 mol/L) and lipids were extracted with chloroform (100 microL). Twenty microliters of the filtered aqueous layer was injected to the flow system and the relation between fluorescence and absorption signals was measured. A peptide-derived AGE calibrator was used for calibration. Within-day and between-day CVs were 6.7% and 9.1%, respectively, at an AGE concentration corresponding approximately to that in healthy individuals. Mean results (+/-SD) in 10 healthy individuals were 10.1% +/- 1.0%, in 21 patients with diabetes without complications 18.0% +/- 6.2%, in 25 patients with complications 24.1% +/- 15.4%, and in 12 diabetic patients in end-stage renal disease 92% +/- 30%. Comparison with an ELISA procedure (x, in arbitrary units/L) yields a regression equation y = 0.713x + 1.24 (Sy [symbol: see text] x = 6777, r = 0.8477, n = 41).

  5. 悬浮粒子在线监测系统设计实例%The Design Example of On-Line Monitoring System to Airborne Rapticles

    Institute of Scientific and Technical Information of China (English)

    魏嵬; 叶涛; 张颖聪; 岳兰瑜; 赵璞

    2012-01-01

    按照中国《药品生产质量管理规范》(2010修订的新版GMP)附录1的要求,对于洁净区A级区,在关键工艺(包括设备的组装)的全过程中,应当对悬浮粒子进行连续的监测,同时在B级区采用相似的系统。为此,我公司在新建车间的分装线A级区,安装了悬浮粒子的在线监测系统,对A级洁净区的悬浮粒子进行了有效的监控。%The continuos monitoring to the whole procedures of key process, including equipment installation, in clean area of Grade A, with similar system for Grade B, are required in Annex 1, the new version of Chinese GMP-2010. The airborne particle on-line monitoring system was intalled in an assembly line in area of Grade A of new cleanroom, having effective monitoring results.

  6. High efficiency cell-recycle continuous sodium gluconate production by Aspergillus niger using on-line physiological parameters association analysis to regulate feed rate rationally.

    Science.gov (United States)

    Lu, Fei; Li, Chao; Wang, Zejian; Zhao, Wei; Chu, Ju; Zhuang, Yingping; Zhang, Siliang

    2016-11-01

    In this paper, a system of cell-recycle continuous fermentation for sodium gluconate (SG) production by Aspergillus niger (A. niger) was established. Based on initial continuous fermentation result (100.0h) with constant feed rate, an automatic feedback strategy to regulate feed rate using on-line physiological parameters (OUR and DO) was proposed and applied successfully for the first time in the improved continuous fermentation (240.5h). Due to less auxiliary time, highest SG production rate (31.05±0.29gL(-1)h(-1)) and highest yield (0.984±0.067molmol(-1)), overall SG production capacity (975.8±5.8gh(-1)) in 50-L fermentor of improved continuous fermentation increased more than 300.0% compared to that of batch fermentation. Improvement of mass transfer and dispersed mycelia morphology were the two major reasons responsible for the high SG production rate. This system had been successfully applied to industrial fermentation and SG production was greatly improved.

  7. Decision support system on line to minimize the NO{sub x} emission. Results from Oerebro Energi; Beslutsstoed on line foer minimering av NO{sub x}. Resultat fraan Oerebro Energi

    Energy Technology Data Exchange (ETDEWEB)

    Bergdahl, B.G.; Liao, B.; Sieurin, J. [EuroSim AB, Nykoeping (Sweden)

    1996-05-01

    A Decision Support System to reduce NO{sub x} emission from combustion processes with SNCR system have been developed and tested in full scale at Oerebro Energy. The boiler is a 165 MWh{sub th} CFB and have been fired with a mixture of biomass, peat and coal. The results proves that the EuroSim method works to calculate the derivative included in the Decision Support System. The Decision Support System is a tool for the operator of the plant, he will be informed of the advantage of making an increase or decrease of the ammonia flow or excess air. The trend curves that are presented to the operator includes information about the economic value to make an adjustment of the ammonia flow. The derivative dNO{sub x}/dO{sub 2} shows the advantage of making a reduction in the excess air level, concerning the fee for NO{sub x}. In this case it is important to take into consideration the risk for understoichiometric combustion and corrosion. The results from the full scale test in the Oerebro Plant shows that during some time periods it is economical to shut off the ammonia flow. The derivative dNO{sub x}/dAF is under the profitability limit. This indicate that the cost for the ammonia is higher than the fee for the NO{sub x} emission. If the ammonia flow is added in excess, the emission of ammonia and N{sub 2}O will increase. During other time periods the Decision Support System shows that it is profitable to increase the ammonia flow, the derivative is lower than -0,2. The derivative dNO{sub x}/dO{sub 2} is normally between 10 and 20 (ppm/%). This indicate that it is a great potential to reduce the NO{sub x} fee by decreasing the excess air level in the boiler. 3 refs, 23 figs

  8. A Bypass Diode of Photovoltaic On-line Monitoring System%光伏旁路二极管在线监测系统

    Institute of Scientific and Technical Information of China (English)

    陈斯; 戴新宇; 杨增汪; 黄智

    2012-01-01

    基于飞思卡尔MC9S08DZ60微控制器,设计了一种光伏旁路二极管在线监测系统.系统以MC9S08DZ60为核心,包括节点检测、集中器和ZigBee无线传输及上位机四部分.节点检测装置采集二极管接线盒的温度、电流、电压参数,经CAN总线传输至集中器,并经ZigBee网络无线输送至上位机监测中心.本系统可以实现光伏旁路二极管状态的实时采集、测量、无线传输功能.测试表明,该系统具有测量精确度高、可靠性好、抗干扰能力强等特点.%A bypass diode of photovoltaic on-line monitoring system is designed based on freescale MC9S08DZ60 microcontroller. The system uses MC9S08DZ60 as its core, including node detection, concentrator, ZigBee wireless transmission and the host computer. Node detection device acquaints the temperature, current, voltage parameters of the bypass diode. The acquainted data will be transmitted to concentrator through the CAN bus and uploaded to the master computer monitoring center by ZigBee wireless transmission network. The system can achieve the function of photovoltaic bypass diode real-time acquisition, measurement and wireless transmission. Tests show that the system has the feature of measurement accuracy, reliability and strong anti-interference etc.

  9. Analysis of recombinant Schistosoma mansoni antigen rSmp28 by on-line liquid chromatography-mass spectrometry combined with sodium dodecyl sulfate polyacrylamide gel electrophoresis

    NARCIS (Netherlands)

    Klarskov, K.; Roecklin, D.; Bouchon, B.; Sabatie, J.; Van Dorsselaer, A.; Bischoff, Rainer

    1994-01-01

    A recombinant Schistosoma mansoni antigen produced in Saccharomyces cerevisiae and purified by glutathione-Sepharose affinity chromatography was analyzed by tryptic peptide mapping using on-line reversed-phase high-performance liquid chromatography pneumatically assisted electrospray mass

  10. Molecularly imprinted polymer cartridges coupled on-line with high performance liquid chromatography for simple and rapid analysis of human insulin in plasma and pharmaceutical formulations.

    Science.gov (United States)

    Moein, Mohammad Mahdi; Javanbakht, Mehran; Akbari-adergani, Behrouz

    2014-04-01

    In this paper, a novel method is described for automated determination of human insulin in biological fluids using principle of sequential injection on a molecularly imprinted solid-phase extraction (MISPE) cartridge as a sample clean-up technique combined with high performance liquid chromatography (HPLC). The water-compatible molecularly imprinted polymers (MIPs) were prepared using methacrylic acid as a functional monomer, ethylene glycol dimethacrylate as a cross-linker, chloroform as a porogen and insulin as a template molecule. The imprinted polymers were then employed as the solid-phase extraction sorbent for on-line extraction of insulin from human plasma samples. To achieve the best condition, influential parameters on the extraction efficiency were thoroughly investigated. Rapid and simple analysis of the hormone was successfully accomplished through the good selectivity of the prepared sorbent coupled with HPLC. Limits of detection (LOD) and quantification (LOQ) of 0.2 ng mL(-1), 0.7 ng mL(-1), and 0.03 ng mL(-1), 0.1 ng mL(-1) were obtained in plasma and urine respectively. The obtained data exhibited the great recoveries for extraction of insulin from human plasma and pharmaceutical samples, higher than 87%.

  11. Design of an expert system based on neuro-fuzzy inference analyzer for on-line microstructural characterization using magnetic NDT method

    Science.gov (United States)

    Ghanei, S.; Vafaeenezhad, H.; Kashefi, M.; Eivani, A. R.; Mazinani, M.

    2015-04-01

    Tracing microstructural evolution has a significant importance and priority in manufacturing lines of dual-phase steels. In this paper, an artificial intelligence method is presented for on-line microstructural characterization of dual-phase steels. A new method for microstructure characterization based on the theory of magnetic Barkhausen noise nondestructive testing method is introduced using adaptive neuro-fuzzy inference system (ANFIS). In order to predict the accurate martensite volume fraction of dual-phase steels while eliminating the effect and interference of frequency on the magnetic Barkhausen noise outputs, the magnetic responses were fed into the ANFIS structure in terms of position, height and width of the Barkhausen profiles. The results showed that ANFIS approach has the potential to detect and characterize microstructural evolution while the considerable effect of the frequency on magnetic outputs is overlooked. In fact implementing multiple outputs simultaneously enables ANFIS to approach to the accurate results using only height, position and width of the magnetic Barkhausen noise peaks without knowing the value of the used frequency.

  12. 在线考试系统在实验机房中的应用%Application of On-line Examination System in Experimental Computer Room

    Institute of Scientific and Technical Information of China (English)

    于萧榕

    2011-01-01

    利用PHP技术完成在线考试系统的制作,能够减轻机房工作人员的工作负担,优化学生考试的流程,利用FTP实现自动下载与上传的方法比其他在线考试模式节省人力、财力和时间.该系统具有系统管理、在线考试两大功能模块,实现了用户管理、考试管理、成绩生成及查询等功能,无客户端情况下的自动下裁与上传和全面的防作弊功能是本系统的特点,从而极大的提高了工作效率.%The on-line examination system realized by PHP technology can reduce the workload of the staff in computer room and optimize the process of student examination. The automatical download and upload methods implemented by FTP can save more manpower, financial resources and time than any other online exam modes. The system is composed of two function modules (ystem management and online examination) , which implements user's information management, examination management, score generation and query. The functions of automatical download / upload in the case of no client terminals and comprehensive anti-cheat feature are the advantages of the system. Real applications show that the proposed method can greatly improve the working efficiency.

  13. Simultaneous determination of nanomole amounts of sulphur dioxide and hydrogen sulphide by flow injection analysis with on-line preconcentration by means of capillary denuder tubes.

    Science.gov (United States)

    Achilli, Marco; Gács, Istvan

    2002-01-01

    A simple and rapid method for trace determination of SO2 and H2S in gaseous samples by using a flow injection system with on line preconcentration on capillary denuder is described. The gaseous samples are led through a 0.4 M sulphamic acid solution, retaining nitrogen dioxide, ammonia and hydrogen chloride. The sulphur dioxide is collected from the carrier gas stream (250 cm3 min-1) as sulphuric acid in a capillary denuder tube coated with a thin layer of 0.01-0.03 M hydrogen peroxide solution of 0.05 mM sulphuric acid; hydrogen sulphide passes into a second tube coated with 0.075 mM sodium sulphide solution of 0.1 M aqueous sodium hydroxide. The films containing the sulphuric acid and the sodium sulphide, respectively, are eluted with the corresponding circulating absorbent streams and pass through the detectors. Sulphuric acid is detected by conductimetry and sulphide is determined spectrophotometrically at 230 nm. If nanoequivalent amounts of H2S are present in the sample containing a large concentration of SO2 (SO2/H2S concentration ratio > 20), the sulphur dioxide is filtered out of the sample gas stream by solid sodium hydrogen carbonate. A limit of detection of 3.5 micrograms m-3 is obtained.

  14. Application of Box-Behnken design in the optimisation of an on-line pre-concentration system using knotted reactor for cadmium determination by flame atomic absorption spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Souza, Anderson S. [Universidade Federal da Bahia, Instituto de Quimica, Nucleo de Excelencia em Quimica Analitica da Bahia, Campus Universitario de Ondina, Salvador, Bahia 40170-290 (Brazil); Universidade Estadual do Sudoeste da Bahia, Departamento de Quimica e Exatas, Campus de Jequie, Jequie, Bahia 45206-190 (Brazil); Santos, Walter N.L. dos [Universidade Federal da Bahia, Instituto de Quimica, Nucleo de Excelencia em Quimica Analitica da Bahia, Campus Universitario de Ondina, Salvador, Bahia 40170-290 (Brazil); Ferreira, Sergio L.C. [Universidade Federal da Bahia, Instituto de Quimica, Nucleo de Excelencia em Quimica Analitica da Bahia, Campus Universitario de Ondina, Salvador, Bahia 40170-290 (Brazil)]. E-mail: slcf@ufba.br

    2005-06-30

    The present paper proposes an on-line pre-concentration system for cadmium determination in drinking water using flame atomic absorption spectrometry (FAAS). Cadmium(II) ions are retained as 1-(2-pyridylazo)-2-naphthol (PAN) complex at the walls of a knotted reactor, followed of elution using hydrochloric acid solution. The optimization was performed in two steps using factorial design for preliminary evaluation and a Box-Behnken design for determination of the critical experimental conditions. The variables involved were: sampling flow-rate, reagent concentration, pH and buffer concentration, and as response the analytical signal (absorbance). The validation process was performed considering the parameters: linearity and other characteristics of the calibration curve, analytical features of on-line pre-concentration system, precision, effect of other ions in the pre-concentration system and accuracy. Using the optimized experimental conditions, the procedure allows cadmium determination with a detection limit (3 {sigma} / S) of 0.10 {mu}g L{sup -1}, a quantification limit (10 {sigma} / S) of 0.33 {mu}g L{sup -1}, and a precision, calculated as relative standard deviation (RSD) of 2.7% (n = 7) and 2.4% (n = 7) for cadmium concentrations of 5 and 25 {mu}g L{sup -1}, respectively. A pre-concentration factor of 18 and a sampling frequency of 48 h{sup -1} were obtained. The recovery for cadmium in the presence of several ions demonstrated that this procedure could be applied for the analysis of water samples. The method was applied for cadmium determination in drinking water samples collected in Salvador City, Brazil. The cadmium concentrations found in five samples were lower than the maximum permissible levels established by the World Health Organization.

  15. Texts On-Line.

    Science.gov (United States)

    Thomas, Jean-Jacques

    1993-01-01

    Maintains that the study of signs is divided between those scholars who use the Saussurian binary sign (semiology) and those who prefer the Peirce tripartite sign (semiotics). Concludes that neither the Saussurian nor Peircian analysis methods can produce a semiotic interpretation based on a hierarchy of the text's various components. (CFR)

  16. Texts On-Line.

    Science.gov (United States)

    Thomas, Jean-Jacques

    1993-01-01

    Maintains that the study of signs is divided between those scholars who use the Saussurian binary sign (semiology) and those who prefer the Peirce tripartite sign (semiotics). Concludes that neither the Saussurian nor Peircian analysis methods can produce a semiotic interpretation based on a hierarchy of the text's various components. (CFR)

  17. On line routing per mobile phone

    DEFF Research Database (Denmark)

    Bieding, Thomas; Görtz, Simon; Klose, Andreas

    2009-01-01

    . Additionally it is of utmost importance that the employed communication system is suitable integrated with the firm’s enterprise application system and business processes. On basis of a case study, we describe in this paper a system that is cheap and easy to implement due to the use of simple mobile phones......On-line routing is concerned with building vehicle routes in an ongoing fashion in such a way that customer requests arriving dynamically in time are efficiently and effectively served. An indispensable prerequisite for applying on-line routing methods is mobile communication technology...

  18. MIS On-Line.

    Science.gov (United States)

    Thomson, Nancy S.; Echeverria, Donna Rose; Mills, Bob

    This paper describes the resources, processes and outcomes involved in the development of an introductory Management Information Systems (MIS) course designed to utilize as many of the technologies as possible to redefine the teaching/learning paradigm. The MIS-Online project at Northwest Missouri State University encompasses the available campus…

  19. Research of On-line Monitoring System for Transmission Line Insulator Flashover%输电线路绝缘子闪络在线监测系统

    Institute of Scientific and Technical Information of China (English)

    黄会贤; 陈新岗; 汪能文; 袁兴旺; 古亮; 马志鹏; 陈果

    2013-01-01

    针对电力系统输电线路绝缘子闪络现象频繁发生且监测困难等问题,建立了以STM32F系列、内核为32位ARM的微控制器为控制电路核心的输电线路绝缘子闪络在线监测系统.介绍了系统控制电路硬件设计方案及软件流程,给出了模块硬件连接网络图与软件流程图.该系统以太阳能为供电来源,将闪络的产生转换为电信号,进而进行采集与处理.通过控制器控制显示模块与GPRS模块实现显示闪络发生次数与短信报警功能.该系统可准确定位闪络绝缘子和及时报警,为寻线检修提供有利条件,为输电线路安全运行提供可靠保障.%With the influence of pollutant or thunder, it is very often that transmission line insulators flashover occurs. It is because that flashover is one of the main reason for transmission line accident, so insulator flashover should be long-term monitored. According to the damage of flashover of insulators along the transmission line, this paper introduces a kind of on-line monitoring system about the transmission line insulator flashover. This system uses 32-bit microcontroller STM32 as the core. The principle of hardware circuit and software flow chart about the system are given in this paper. The system takes solar energy as power supply. It realized signal conversion that changes the flashover to e-lectrical signals. The system can also realize the functions of monitoring flashover of insulator such as signal collection, processing, display, alarm etc. This system can provide favorable conditions for the transmission line maintenance and a reliable guarantee of transmission lines.

  20. On-Line Tests

    Directory of Open Access Journals (Sweden)

    Florentina Anica Pintea

    2007-01-01

    Full Text Available This paper presents an interactive implementation which makes the link between a human operator and a system of an administration of relational databases MySQL. This application conceived as a multimedia presentations is illustrative for the way in which the transfer and the remaking of the information between the human operator, the module of data processing and the database which stores the information can be solved (with help of the PHP language and the web use.

  1. Formación on line On line learning

    Directory of Open Access Journals (Sweden)

    O. Grau-Perejoan

    2008-09-01

    Full Text Available La formación on line es una modalidad de enseñanza a distancia basada en las nuevas tecnologías. En este artículo se pretende hacer una introducción a base de describir a grandes rasgos sus características principales: asincronía, no presencialidad, comunicación escrita, función del profesor on line, así como los retos, los riesgos, las ventajas y los inconvenientes que plantea. Se exponen las diferencias entre la formación on line y la formación presencial, de manera que los docentes puedan adaptar de la mejor manera posible sus propuestas formativas a la modalidad on line. Se introduce el importantísimo papel de la planificación y de la fase de diseño y, finalmente, se repasan conceptos útiles para comprender mejor el mundo de la formación on line como son los conceptos entorno virtual de aprendizaje (EVA o Blended Learning (B-Learning.On line learning is a type of distance education based on new technologies. This article's aim is to introduce its main characteristics -asynchrony, non-presentiality, written communication, e-teacher role- as well as its challenges, risks, advantages and limitations. Differences between on line learning and face-to-face learning are presented in order to enable educational professionals to adapt their courses to the on line methodology. Planning and designing are introduced as key phases and, finally, useful concepts such as Virtual Learning Environment (VLE or Blended Learning (B-Learning are reviewed in order to achieve a better understanding of the on line learning field.

  2. The on-line detection system design of power capacitor dielectric loss factor%电力电容器介质损耗因数在线检测系统的设计

    Institute of Scientific and Technical Information of China (English)

    延红艳; 黄知超; 杨升振

    2012-01-01

    针对目前对电力电容器介质损耗角因数在线检测的精度要求越来越高的现状,设计了基于AD7656和TMS320F2812的电力电容器介质损耗因数在线检测系统.利用电压互感器和电流传感器采集电力电容器母线电压信号以及泄漏电流信号,将采集到的信号经过信号调理转换成可以被AD7656接收的信号;利用AD7656进行模数转换,锁相倍频保证同步采样,TMS320F2812用以控制AD转换并利用谐波分析法进行数据处理,计算出介质损耗因数.在电网频率波动以及白噪声影响条件下计算介质损耗因数的相对误差.结果表明,本系统具有较高的可靠性和准确性,能达到介质损耗因数在线检测的精度要求.%Aiming at the current situation of the increasing precision requirement for the power capacitor dielectric loss angle factor on-line detection, the on-line detection system of dielectric loss factor in power capacitor based on AD7656 and TMS320F2812 was designed. The voltage transformer and current sensor were used to collect bus voltage signals and leak current signals of the power capacitor, the collected signals were converted into the signals which can be received by AD7656 through signal conditioning circuit) AD7656 was used to be analog-to-digital converter, PLL can ensure synchronous sampling, TMS320F2812 was used to control the AD transform, harmonic a-nalysis method was used for data processing and tan 8 calculation. The measuring relative errors of tan S on the conditions of the power grid frequency waving and white noise influencing were calculated. The experimental results show that the system has the good feature of veracity and reliability, the method can achieve the required accuracy of the power capacitor tan S on-line detecting.

  3. DEVELOPMENT OF AN ON-LINE COAL WASHABILITY ANALYZER

    Energy Technology Data Exchange (ETDEWEB)

    J.D. Miller; C.L. Lin; G.H. Luttrell; G.T. Adel; Barbara Marin

    2001-06-26

    Washability analysis is the basis for nearly all coal preparation plant separations. Unfortunately, there are no on- line techniques for determining this most fundamental of all coal cleaning information. In light of recent successes at the University of Utah, it now appears possible to determine coal washability on-line through the use of x-ray computed tomography (CT) analysis. The successful development of such a device is critical to the establishment of process control and automated coal blending systems. In this regard, Virginia Tech, Terra Tek Inc., and U.S. coal producers have joined with the University of Utah and to undertake the development of an X-ray CT-based on- line coal washability analyzer with financial assistance from DOE. Each project participant brought special expertise to the project in order to create a new dimension in coal cleaning technology. The project involves development of appropriate software and extensive testing/evaluation of well-characterized coal samples from operating coal preparation plants. Data collected to date suggest that this new technology is capable of serving as a universal analyzer that can not only provide washability analysis, but also particle size distribution analysis, ash analysis, and perhaps pyritic sulfur analysis.

  4. DEVELOPMENT OF AN ON-LINE COAL WASHABILITY ANALYZER

    Energy Technology Data Exchange (ETDEWEB)

    J.D. Miller

    1999-09-30

    Washability analysis is the basis for nearly all coal preparation plant separations. Unfortunately, there are no on-line techniques for determining this most fundamental of all coal cleaning information. In light of recent successes at the University of Utah, it now appears possible to determine coal washability on-line through the use of x-ray computed tomography (CT) analysis. The successful development of such a device is critical to the establishment of process control and automated coal blending systems. In this regard, Virginia Tech, Terra Tek Inc., and several eastern coal companies have joined with the University of Utah and agreed to undertake the development of a x-ray CT-based on-line coal washability analyzer with financial assistance from DOE. The three-year project will cost $594,571, of which 33% ($194,575) will be cost-shared by the participants. The project involves development of appropriate software and extensive testing/evaluation of well-characterized coal samples from operating coal preparation plants. Each project participant brings special expertise to the project which is expected to create a new dimension in coal cleaning technology. Finally, it should be noted that the analyzer may prove to be a universal analyzer capable of providing not only washability analysis, but also particle size distribution analysis, ash analysis and perhaps pyritic sulfur analysis.

  5. On-line gas analysis in animal cell cultivation: II. Methods for oxygen uptake rate estimation and its application to controlled feeding of glutamine.

    Science.gov (United States)

    Eyer, K; Oeggerli, A; Heinzle, E

    1995-01-05

    Different methods for oxygen uptake rate (OUR) determinations in animal cell cultivation were investigated using a high quality mass spectrometer. Dynamic measurements have considerable disadvantages because of disturbances of the growing cells by the necessary variations of dissolved oxygen concentration. Only infrequent discrete measurements are possible using this method. Stationary liquid phase balance yielded better results with much higher frequency. Gas phase balancing has the advantage of not requiring dissolved oxygen measurement and knowledge of K(L)a, both of them are easily biased. It was found that simple gas phase balancing is either very inaccurate (error larger than expected signal) or very slow, with gas phase residence times of several hours. Therefore, a new method of aeration was designed. Oxygen and CO(2) transfer are mainly achieved via sparging. The gas released to the headspace is diluted with a roughly 100-fold stream of an inert gas (helium). Through this dilution, gas ratios are not changed for O(2), CO(2), Ar, and N(2). The measurement of lower concentrations (parts per million and below) is easy using mass spectrometry with a secondary electron multiplier. With this new method an excellent accuracy and sufficient speed of analysis were obtained. All these on-line methods for OUR measurement were tested during the cultivation of animal cells. The new method allowed better study of the kinetics of animal cell cultures as was shown with a hybridoma cell line (HFN 7.1, ATCC CRL 1606) producing monoclonal antibodies against human fibronectin. With the aid of these methods it was possible to find a correlation between a rapid decrease in oxygen uptake rate (OUR) and glutamine concentration. The sudden decrease in OUR can be attributed to glutamine depletion. This provided a basis for the controlled addition of glutamine to reduce the formation of ammonia produced by hydrolysis. This control method based on OUR measurement resulted in

  6. GEM-AQ/EC, an on-line global multi-scale chemical weather modelling system: model development and evaluation of global aerosol climatology

    Directory of Open Access Journals (Sweden)

    S. L. Gong

    2012-09-01

    Full Text Available A global air quality modeling system GEM-AQ/EC was developed by implementing tropospheric chemistry and aerosol processes on-line into the Global Environmental Multiscale weather prediction model – GEM. Due to the multi-scale features of the GEM, the integrated model, GEM-AQ/EC, is able to investigate chemical weather at scales from global to urban domains. The current chemical mechanism is comprised of 50 gas-phase species, 116 chemical and 19 photolysis reactions, and is complemented by a sectional aerosol module CAM (The Canadian Aerosol Module with 5 aerosols types: sulphate, black carbon, organic carbon, sea-salt and soil dust. Monthly emission inventories of black carbon and organic carbon from boreal and temperate vegetation fires were assembled using the most reliable areas burned datasets by countries, from statistical databases and derived from remote sensing products of 1995–2004. The model was run for ten years from from 1995–2004 with re-analyzed meteorology on a global uniform 1° × 1° horizontal resolution domain and 28 hybrid levels extending up to 10 hPa. The simulating results were compared with various observations including surface network around the globe and satellite data. Regional features of global aerosols are reasonably captured including emission, surface concentrations and aerosol optical depth. For various types of aerosols, satisfactory correlations were achieved between modeled and observed with some degree of systematic bias possibly due to large uncertainties in the emissions used in this study. A global distribution of natural aerosol contributions to the total aerosols is obtained and compared with observations.

  7. GEM-AQ/EC, an on-line global multiscale chemical weather modelling system: model development and evaluations of global aerosol climatology

    Directory of Open Access Journals (Sweden)

    S. L. Gong

    2012-04-01

    Full Text Available A global air quality modeling system GEM-AQ/EC was developed by implementing tropospheric chemistry and aerosol processes on-line into the Global Environmental Multiscale weather prediction model – GEM. Due to the multi-scale features of the GEM, the integrated model, GEM-AQ/EC, is able to investigate chemical weather at scales from global to urban domains. The current chemical mechanism is comprised of 50 gas-phase species, 116 chemical and 19 photolysis reactions, and is complemented by a sectional aerosol module CAM (The Canadian Aerosol Module with 5 aerosols types: sulphate, black carbon, organic carbon, sea-salt and soil dust. Monthly emission inventories of black carbon and organic carbon from boreal and temperate vegetation fires were assembled using the most reliable areas burned datasets by countries, from statistical databases and derived from remote sensing products of 1995–2004. The model was run for ten years from from 1995–2004 with re-analyzed meteorology on a global uniform 1 × 1° horizontal resolution domain and 28 hybrid levels extending up to 10 hPa. The simulating results were compared with various observations including surface network around the globe and satellite data. Regional features of global aerosols are reasonably captured including emission, surface concentrations and aerosol optical depth. For various types of aerosols, satisfactory correlations were achieved between modeled and observed with some degree of systematic bias possibly due to large uncertainties in the emissions used in this study. A global distribution of natural aerosol contributions to the total aerosols is obtained and compared with observations.

  8. A new aerosol collector for quasi on-line analysis of particulate organic matter: the Aerosol Collection Module (ACM) and first applications with a GC/MS-FID

    Science.gov (United States)

    Hohaus, T.; Trimborn, D.; Kiendler-Scharr, A.; Gensch, I.; Laumer, W.; Kammer, B.; Andres, S.; Boudries, H.; Smith, K. A.; Worsnop, D. R.; Jayne, J. T.

    2010-10-01

    In many environments organic matter significantly contributes to the composition of atmospheric aerosol particles influencing its properties. Detailed chemical characterization of ambient aerosols is critical in order to understand the formation process, composition, and properties of aerosols and facilitates source identification and relative contributions from different types of sources to ambient aerosols in the atmosphere. However, current analytical methods are far from full speciation of organic aerosols and often require sampling times of up to one week. Offline methods are also subjected to artifacts during aerosol collection and storage. In the present work a new technique for quasi on-line compound specific measurements of organic aerosol particles was developed. The Aerosol Collection Module (ACM) focuses particles into a beam which is directed to a cooled sampling surface. The sampling takes place in a high vacuum environment where the gas phase from the sample volume is removed. After collection is completed volatile and semi-volatile compounds are evaporated from the collection surface through heating and transferred to a detector. For laboratory characterization the ACM was interfaced with a Gas Chromatograph Mass Spectrometer, Flame Ionization Detector system (GC/MS-FID), abbreviated as ACM GC-MS. The particle collection efficiency, gas phase transfer efficiency, and linearity of the ACM GC-MS were determined using laboratory generated octadecane aerosols. The ACM GC-MS is linear over the investigated mass range of 10 to 100 ng and a recovery rate of 100% was found for octadecane particles. The ACM GC-MS was applied to investigate secondary organic aerosol (SOA) formed from β-pinene oxidation. Nopinone, myrtanal, myrtenol, 1-hydroxynopinone, 3-oxonopinone, 3,7-dihydroxynopinone, and bicyclo[3,1,1]hept-3-ene-2-one were found as products in the SOA. The ACM GC-MS results are compared to quartz filter samples taken in parallel to the ACM GC

  9. 网络社区中的意见领袖特征分析%A Feature Analysis of the Opinion Leader in On-Line Communities

    Institute of Scientific and Technical Information of China (English)

    肖宇; 许炜; 夏霖

    2011-01-01

    We use a method of social network analysis to indentify opinion leaders in social networks.First of all we analyze the characteristics of the social networks of on-line communities, consider the difference between BBS, blogosphere and Q&-A network, and propose that undirected weighted network models will enhance the identification accuracy of opinion leaders.Then, we analyze the features of social networks.We validate that BBS is small-world and scale-free, and we make a quantitative analysis of the social background of opinion leaders.We also propose a PageRank algorithm based on undirected weighted networks, and test several algorithms proposed before our experiment.We use four years' data from a BBS, and test these algorithms.Finally, we make a profound analysis and find the relationship between opinion leaders and boards, and the result shows that we can find a majority of opinion leaders from covering few boards.%本文通过社会网络分析方法识别网络社区中的意见领袖.首先对意见领袖存在的人际关系网络结构特征进行分析,对比论坛、博客和问答网络之间的区别,提出基于无向、有权重网络模型更能真实准确地识别意见领袖.并基于该网络模型研究和分析了网络论坛结构特征,通过测量其小世界和无标度的复杂网络特征,定量分析意见领袖存在的社会性根源.其次提出了基于无向、有权重网络下的PageRank算法,并对比前人提出多种意见领袖识别算法,以某论坛四年历史数据实证了算法的有效性.最后对识别结果进行深入分析,并研究了意见领袖同活跃版块之间的关系,发现通过覆盖少量版块即可覆盖绝大部分意见领袖.

  10. IOOS Data Portals and Uniform On-line Browse Capabilities

    Science.gov (United States)

    Howard, M.; Currier, R. D.; Kobara, S.; Gayanilo, F.

    2015-12-01

    The Gulf of Mexico Coastal Ocean Observing System Regional Association (GCOOS-RA) is one of eleven Regional Associations organized under the NOAA-led U.S. Integrated Ocean Observing System (IOOS) Program Office. Each of the RAs operate standards-based regional data portals designed to aggregate near real-time and historical observed data and modeled outputs from distributed providers and to offer these and derived products in standardized ways to a diverse set of users. The RA's portals are based on the IOOS Data and Communications Plan which describes the functional elements needed for an interoperable system. One of these elements is called "Uniform On-line Browse" which is an informational service designed primarily to visualize the inventory of a portal. An on-line browse service supports the end user's need to discover what parameters are available, to learn the spatial and temporal extend of the holdings, and to examine the character of the data (e.g, variability, gappiness, etc). These pieces of information help the end user decide if the data are fit for his/her purpose and to construct valid data requests. Note that on-line browse is a distinctly different activity than data analysis because it seeks to yield knowledge about the inventory and not about what the data mean. "Uniform" on-line browse is a service that takes advantage of the standardization of the data portal's data access points. Most portals represent station locations on a map. This is a view of the data inventory but these plots are rarely generated by pulling data through the standards-based services offered to the end users but through methods only available to the portal programmers. This work will present results of Uniform On-line browse tools developed within GCOOS-RA and their applicability to other RA portals.

  11. A radio-high-performance liquid chromatography dual-flow cell gamma-detection system for on-line radiochemical purity and labeling efficiency determination

    DEFF Research Database (Denmark)

    Lindegren, S; Jensen, H; Jacobsson, L

    2014-01-01

    into the well of a NaI(Tl) detector. The radio-HPLC flow was directed from the injector to the reference cell allowing on-line detection of the total injected sample activity prior to entering the HPLC column. The radioactivity eluted from the column was then detected in the analytical cell. In this way...

  12. Development of a microfluidic confocal fluorescence detection system for the hyphenation of nano-LC to on-line biochemical assays

    NARCIS (Netherlands)

    Heus, F.; Giera, M.A.; Kloe, de G.E.; Iperen, van D.; Buijs, J.B.; Nahar, T.T.; Smit, A.B.; Lingeman, H.; Esch, de I.J.P.; Niessen, W.M.A.; Irth, H.; Kool, J.

    2010-01-01

    One way to profile complex mixtures for receptor affinity is to couple liquid chromatography (LC) on-line to biochemical detection (BCD). A drawback of this hyphenated screening approach is the relatively high consumption of sample, receptor protein and (fluorescently labeled) tracer ligand. Here, w

  13. Development of an on-line high performance liquid chromatography detection system for human cytochrome P450 1A2 inhibitors in extracts of natural products

    NARCIS (Netherlands)

    Jeurissen, S.M.F.; Claassen, F.W.; Havlik, J.; Bouwmans, E.E.; Cnubben, N.H.P.; Sudhölter, E.J.R.; Rietjens, I.M.C.M.; Beek, T.A. van

    2007-01-01

    An on-line HPLC screening method for detection of inhibitors of human cytochrome P450 1A2 in extracts was developed. HPLC separation of extracts is connected to a continuous methoxyresorufin-O-demethylation (MROD) assay in which recombinant human P450 1A2 converts methoxyresorufin to its fluorescent

  14. An automated method for the analysis of phenolic acids in plasma based on ion-pairing micro-extraction coupled on-line to gas chromatography/mass spectrometry with in-liner derivatisation

    NARCIS (Netherlands)

    Peters, S.; Kaal, E.; Horsting, I.; Janssen, H.-G.

    2012-01-01

    A new method is presented for the analysis of phenolic acids in plasma based on ion-pairing ‘Micro-extraction in packed sorbent’ (MEPS) coupled on-line to in-liner derivatisation-gas chromatography-mass spectrometry (GC-MS). The ion-pairing reagent served a dual purpose. It was used both to improve

  15. The Trace Analysis of DEET in Water using an On-line Preconcentration Column and Liquid Chromatography with UV Photodiode Array Detection

    Science.gov (United States)

    A method for the detection of trace levels of N,N-diethyl-m-toluamide (DEET) in water is discussed. The method utilizes an on-line preconcentration column in series with high performance liquid chromatography (HPLC) and UV photodiode array detection. DEET, a common insect repel...

  16. 变压器在线色谱监测装置的应用分析%Application Analysis of Transformer On-line Chromatograph Monitor

    Institute of Scientific and Technical Information of China (English)

    劳永闯; 何燕

    2014-01-01

    简述了在线色谱监测装置的类型及其相关检测原理,将中分3000型在线色谱监测装置与实验室色谱仪进行比较,并通过应用实例分析,指出在线色谱监测技术在变压器状态检修和运行监测中的重要性,最后对在线色谱监测装置的选用提出了一些建议。%This paper briefly describes types and relevant testing principles of the on-line chromatograph monitors. By comparing Zhongfen-3000 on-line chromatograph monitoring device with chromatograph in labo-ratory and analyzing application examples , this paper illustrates the importance of on-line chromatograph mon-itoring technology in condition-based maintenance and operation monitoring of transformer. Finally the paper puts forward suggestions for selecting and use of on-line chromatograph monitoring device.

  17. Determination of trace metal ions via on-line separation and preconcentration by means of chelating Sepharose beads in a sequential injection lab-on-valve (SI-LOV) system coupled to electrothermal atomic absorption spectrometric detection

    DEFF Research Database (Denmark)

    Long, Xiangbao; Hansen, Elo Harald; Miró, Manuel

    2005-01-01

    . The samples are adjusted to pH 5.0 on-line in the system for optimum operation. The target ions are adsorbed by chelation on the surface of the beads, contained in a 20 mul microcolumn within the LOV, and following elution by 50 mul 2M nitric acid, the eluate is, as sandwiched by air segments, introduced...

  18. Determination of trace metal ions via on-line separation and preconcentration by means of chelating Sepharose beads in a sequential injection lab-on-valve (SI-LOV) system coupled to electrothermal atomic absorption spectrometric detection

    DEFF Research Database (Denmark)

    Long, Xiangbao; Hansen, Elo Harald; Miró, Manuel

    2005-01-01

    The analytical performance of an on-line sequential injection lab-on-valve (SI-LOV) system using chelating Sepharose beads as sorbent material for the determination of ultra trace levels of Cd(II), Pb(II) and Ni(II) by electrothermal atomic absorption spectrometry (ETAAS) is described and discussed...

  19. Total on-line monitoring system of Tokyo gas transmission pipelines; Systeme global de controle et de surveillance des canalisations de transport du gaz developpe par Tokyo gas

    Energy Technology Data Exchange (ETDEWEB)

    Shibata, M. [Tokyo Gas Co., Ltd (Japan)

    2000-07-01

    As Tokyo Gas transmission pipeline is located in residential areas of Metropolitan Tokyo, more precise and advanced maintenance and inspection methods become necessary. A more efficient maintenance and inspection management system is being sought in line with the extension of gas transmission pipelines. Research and development is underway for various types of maintenance /monitoring systems that predict or detect pipeline damage or failure. Some systems have already been put to practical use. Tokyo Gas has developed a total online monitoring system featuring upgraded performance and centralized data processing. This system carries out 24-hour monitoring for damage and failure, and sends warnings to operators at the Pipeline Regional Network Office. This paper introduces the functions of the system, as well as the functions which are currently in the R and D stage. (author)

  20. RECURSOS TECNOLÓGICOS AUDIOVISUALES DE FORMACIÓN EN RED: SISTEMAS STREAMING MEDIA Y TELEINMERSIVOS TECHNOLOGICAL RESOURCES FOR ON-LINE INSTRUCTION: STREAMING MEDIA AND TELEIMMERSION SYSTEMS

    Directory of Open Access Journals (Sweden)

    Juan Antonio Juanes Méndez

    2010-06-01

    Full Text Available Presentamos dos modalidades tecnológicas de enseñanza en red: la consolidada y ampliamente utilizada tecnología video-streaming, y el futuro de la comunicación a distancia, la teleinmersión. La primera permite la transmisión de audio/vídeo por la red para que puede ser vista por el usuario en su ordenador personal, desde cualquier lugar que disponga de una conexión a red. La información será recibida y decodificada por el usuario final utilizando cualquier reproductor de los que existen en el mercado. La teleinmersión, por su parte, permite crear espacios virtuales de colaboración entre profesionales, ofreciendo entornos muy cercanos a la realidad. Esta tecnología revolucionará, sin duda, nuestros sistemas de enseñanza en los próximos años, facilitando la interacción profesor-alumno. Es evidente que la formación e-learning aporta a los alumnos y a los docentes grandes ventajas como: menores tiempos de aprendizaje, flexibilidad de horarios y de ubicación geográfica, entre otras. We describe two technological modes of on-line teaching: the consolidated and widely used video-streaming mode and teleimmersion, the future of distance communications. The former mode allows the transmission of audio/video through the network so that it can be seen by the user on a PC from anywhere harbouring a network connection. The information is received and decoded by the final user using any reproducer available on the market. Teleimmersion allows the creation of virtual spaces for collaboration among professionals, offering venues that are very similar to reality. This technology will undoubtedly revolutionize our teaching systems in the near future, facilitating instructor-student interaction. It is clear that e-learning- instruction offers both students and instructors huge advantages, such as shorter learning times and schedule and geographic flexibility, among others.

  1. Analysis of electrophoretic soil humic acids fractions by reversed-phase high performance liquid chromatography with on-line absorbance and fluorescence detection.

    Science.gov (United States)

    Trubetskoj, Oleg A; Richard, Claire; Guyot, Ghislain; Voyard, Guillaume; Trubetskaya, Olga E

    2012-06-22

    A combination of reversed-phase high performance liquid chromatography (RP HPLC) with on-line absorbance and fluorescence detection was used for analysis of chernozem soil humic acids (HAs) and their fractions A, B and C+D with different electrophoretic mobility (EM) and molecular size (MS). Samples were injected onto the column at the identical volume and absorbance. All chromatograms exhibit the resolution of seven peaks. The estimation of relative recovery of HAs and fractions from the reverse-phase column has been done. High MS fraction A, which possesses the low EM, is essentially more hydrophobic (73% of the fraction amount remained adsorbed on the column) and aliphatic than medium MS and EM fraction B (33% of the fraction amount remained adsorbed on the column). The most hydrophilic and aromatic properties belong to low MS fraction C+D, which possess the highest EM and practically was not adsorbed on the column. The hydrophobicity of the bulk HAs lies within the range of fractions hydrophobicity. The absorption spectra of bulk HAs, electrophoretic fractions A, B, C+D and corresponding RP HPLC peaks were featureless but had differences in the values of absorbance ratio at 300 and 400 nm (A3/A4). For fractions A and B this ratio gradually decreased from peak 1 to 7 (from 3.05 to 2.80 and 3.00 to 2.40, respectively). This trend was less pronounced in HAs and practically absent in fraction C+D, where ratio A3/A4 varied within a small range. The strong relationship between fluorescence properties, EM, MS, polarity and aliphaticity/aromaticity of HAs fractions was found. Humic and protein-like fluorescence had different polarity nature. The protein-like fluorescence is located in humic material which irreversibly adsorbed on the reverse-phase column and not subjected to RP HPLC characterization. The humic-like fluorescence at Ex/Em 270/450 nm is mostly located in the hydrophilic peak of low MS fraction C+D. Taking into account that high MS fraction A consisted

  2. Update of on-line coupled liquid chromatography - gas chromatography for the analysis of mineral oil hydrocarbons in foods and cosmetics.

    Science.gov (United States)

    Biedermann, Maurus; Munoz, Celine; Grob, Koni

    2017-09-13

    On-line coupled high performance liquid chromatography-gas chromatography-flame ionization detection (HPLC-GC-FID) is the most widely used method for the analysis of mineral oil hydrocarbons in food, food contact materials, tissues and cosmetics. With comprehensive two-dimensional gas chromatography (GCxGC), a tool became available for better establishing the elution sequence of the various types of hydrocarbons from the HPLC column used for isolating the mineral oil saturated hydrocarbons (MOSH) and mineral oil aromatic hydrocarbons (MOAH). The performance of a heavily used HPLC column with reduced retention for MOAH was investigated to improve the robustness of the method. Updates are recommended that render the MOSH/MOAH separation less dependent of the state of the HPLC column and more correct in cases of highly refined mineral oil products of high molecular mass. Cyclohexyl cyclohexane (Cycy), used as internal standard, turned out to be eluted slightly after cholestane (Cho); apparently the size exclusion effect predominates the extra retention by ring number on the 60Å pore size silica gel. Hence, Cycy can be used to determine the end of the MOSH fraction. Long chain alkyl benzenes were eluted earlier than tri-tert. butyl benzene (Tbb). It is proposed to start the MOAH transfer immediately after the MOSH fraction and use a gradient causing breakthrough of dichloromethane (visible in the UV chromatogram) at a time suitable to elute perylene (Per) at the end of the fraction. In this way, a decrease in retention power of the HPLC column can be tolerated without adjustment of the MOAH fraction until some MOAH start being eluted into the MOSH fraction. This critical point can be checked either with di(2-ethylhexyl) benzene (DEHB) as a marker or the HPLC-UV chromatogram. Finally, based on new findings in rats and human tissues, it is recommended to integrate the MOSH and MOAH up to the retention time of the n-alkane C40. Copyright © 2017 Elsevier B.V. All rights

  3. Research and Design of On-line Monitoring System of XLPE Cable Based on Water Tree Phenomenon%基于水树枝现象XLPE电缆在线监测系统的研究与设计

    Institute of Scientific and Technical Information of China (English)

    周笑阳; 杨建华; 卢伟

    2015-01-01

    基于交联聚乙烯(XLPE)电缆水树状老化的原理,直流分量法和交流叠加法是两种有效的XLPE电缆在线监测方法。设计了综合上述两种方法的在线监测系统,其中包括设计方案、系统构成、关键技术等。结果表明:设计的XLPE电缆在线监测系统能够反映运行中电缆绝缘的老化程度,实现了XLPE电缆的在线监测。%Based on the theory of water tree ageing of XLPE cable, the DC component method and AC superposition method are effective methods for on-line monitoring of XLPE cable. An on-line monitoring system of XLPE cable based on the above two methods was designed, which included design plan, system construction, and key technology. The experiment results show that the on-line monitoring system can reflect the ageing degree of the running cable, and realize the on-line monitoring of the cable.

  4. 決策樹形式知識之線上預測系統架構 | An On-Line Decision Tree-Based Predictive System Architecture

    Directory of Open Access Journals (Sweden)

    馬芳資、林我聰 Fang-Tz Ma、Woo-Tsong Lin

    2003-10-01

    ="font-size: small;">This paper presents an on-line decision tree-based predictive system architecture. The architecture contains nine components, including a database of the examples, a learning system of the decision trees, a knowledge base, a historical knowledge base, a maintaining interface of the decision trees, an interface to upload training and testing examples, a PMML (Predictive Model Markup Language translator, an on-line predictive system, and a merging optional decision trees system. There are three channels to import knowledge in the architecture; the developers can upload the examples to the learning system to induce the decision tree, directly input the information of decision trees through the user interface, or import the decision trees in PMML format. In order to integrate the knowledge of the decision trees, we added the merging optional decision trees system into this architecture. The merging optional decision trees system can combine multiple decision trees into a single decision tree to integrate the knowledge of the trees. In the future research, we will implement this architecture as a real system in the web-based platform to do some empirical analyses. And in order to improve the performance of the merging decision trees, we will also develop some pruning strategies in the merging optional decision trees system.

  5. Application of off/on line sequential injection system with high resolution ICP-MS to measurement radionuclides in environmental samples

    Energy Technology Data Exchange (ETDEWEB)

    Chang-Kyu Kim (IAEA, Physics, Chemistry and Instrumentation Lab., Agency' s Laboratories, Seibersdorf (Austria))

    2010-03-15

    A sequential injection system was developed, which can be widely used for the separation and preconcentration of analytes from diverse environmental samples. The system enables the separation time to be shortened by maintaining a constant flow rate of solution and by avoiding clogging or bubbling in a chromatographic column. The SI system was successfully applied to the separation of 237Np and Pu isotopes in IAEA reference materials and environmental samples, and to the sequential separation of 210Po and 210Pb in a phosphogypsum candidate reference material. The replicate analysis results of 237Np, 239+240Pu 210Po and 210Pb in some IAEA reference materials using the SI system associated with HR-ICP-MS, alpha-spectrometry and LSC are in good agreement with the recommended value within 5% of standard deviation. The SI system enabled a halving of the separation time required for radionuclides. (author)

  6. A new aerosol collector for quasi on-line analysis of particulate organic matter: the Aerosol Collection Module (ACM and first applications with a GC/MS-FID

    Directory of Open Access Journals (Sweden)

    T. Hohaus

    2010-10-01

    Full Text Available In many environments organic matter significantly contributes to the composition of atmospheric aerosol particles influencing its properties. Detailed chemical characterization of ambient aerosols is critical in order to understand the formation process, composition, and properties of aerosols and facilitates source identification and relative contributions from different types of sources to ambient aerosols in the atmosphere. However, current analytical methods are far from full speciation of organic aerosols and often require sampling times of up to one week. Offline methods are also subjected to artifacts during aerosol collection and storage.

    In the present work a new technique for quasi on-line compound specific measurements of organic aerosol particles was developed. The Aerosol Collection Module (ACM focuses particles into a beam which is directed to a cooled sampling surface. The sampling takes place in a high vacuum environment where the gas phase from the sample volume is removed. After collection is completed volatile and semi-volatile compounds are evaporated from the collection surface through heating and transferred to a detector.

    For laboratory characterization the ACM was interfaced with a Gas Chromatograph Mass Spectrometer, Flame Ionization Detector system (GC/MS-FID, abbreviated as ACM GC-MS. The particle collection efficiency, gas phase transfer efficiency, and linearity of the ACM GC-MS were determined using laboratory generated octadecane aerosols. The ACM GC-MS is linear over the investigated mass range of 10 to 100 ng and a recovery rate of 100% was found for octadecane particles.

    The ACM GC-MS was applied to investigate secondary organic aerosol (SOA formed from β-pinene oxidation. Nopinone, myrtanal, myrtenol, 1-hydroxynopinone, 3-oxonopinone, 3,7-dihydroxynopinone, and bicyclo[3,1,1]hept-3-ene-2-one were found as products in the SOA. The ACM GC-MS results are compared to quartz filter

  7. Validation of a high performance liquid chromatography analysis for the determination of noradrenaline and adrenaline in human urine with an on-line sample purification

    DEFF Research Database (Denmark)

    Hansen, Åse Marie; Kristiansen, J; Nielsen, J L

    1999-01-01

    A high performance liquid chromatography (HPLC) method with fluorescence detection including an on-line purification was established for determination of catecholamines in human urine. The method was evaluated using samples of pooled urine spiked with catecholamines and validated for measurements...... deviation of the method was sufficiently low to distinguish between persons working with two different processes of garbage collection, i.e. collection using four wheeled containers versus collection using bins....

  8. Business Analytics as a Tool to Transforming Information into an Informing System: The Case of the On-Line Course Registration System

    Directory of Open Access Journals (Sweden)

    Dimitar Grozdanov Christozov

    2017-06-01

    Impact on Society\tTransforming Information towards Informing Systems has a significant impact by allowing users to make rational data driven decisions in an efficient way. Future Research:\tThe future of this project is implementation of developed ideas and assessment of the results. Impact on Society\t: Transforming Information towards Informing Systems has a significant impact by allowing users to make rational data driven decisions in an efficient way. Future Research: The future of this project is implementation of developed ideas and assessment of the results.

  9. GEM-AQ, an on-line global multiscale chemical weather system: model description and evaluation of gas phase chemistry processes

    Directory of Open Access Journals (Sweden)

    J. W. Kaminski

    2007-10-01

    Full Text Available Tropospheric chemistry and air quality processes were implemented on-line in the Global Environmental Multiscale model. The integrated model, GEM-AQ, has been developed as a platform to investigate chemical weather at scales from global to urban. The model was exercised for five years (2001–2005 to evaluate its ability to simulate seasonal variations and regional distributions of trace gases such as ozone, nitrogen dioxide and carbon monoxide on the global scale. The model results presented are compared with observations from satellites, aircraft measurement campaigns and balloon sondes.

  10. An Interface for Sensitive Analysis of Monoamine Neurotransmitters by Ion-Pair Chromatography–ESI-MS with Continuous On-Line Elimination of Ion-Pair Reagents

    OpenAIRE

    Shi,Shuyun; Zhao, Binqing; Yagnik, Gargey; Zhou, Feimeng

    2013-01-01

    A challenge in coupling ion-pair chromatography (IPC) on-line with electrospray ionization-mass spectrometry (ESI-MS) is that the nonvolatile ion-pair reagent (e.g., alkyl sulfate for amines or tetrabutylammonium for carboxylic acids) in the mobile phase suppresses the ESI-MS signals in the gas phase and their accumulation can clog the MS sampling interface. Consequently, IPC–ESI-MS is conducted either with a volatile ion-pair reagent, which could compromise the analyte separation efficiency,...

  11. CERN Video News on line

    CERN Multimedia

    2003-01-01

    The latest CERN video news is on line. In this issue : an interview with the Director General and reports on the new home for the DELPHI barrel and the CERN firemen's spectacular training programme. There's also a vintage video news clip from 1954. See: www.cern.ch/video or Bulletin web page

  12. 镀镍槽液中镍含量的在线监测系统研究%Concentration of Nickel in Nickel Plating Bath by on-line Monitoring System

    Institute of Scientific and Technical Information of China (English)

    乔永莲; 沙春鹏; 董宇; 刘冰

    2015-01-01

    Objective To develop a new method for on-line monitoring of the concentration of nickel ions in nickel plating, and to expand its application to chromeplate, cadmium plating, copper plating and so on. Methods The system was composed by VC++Language programming, Modbus communication technology and PLC Siemens technology. The amount of nickel plating bath was controlled and revised by meter pump and flowmeter for nickel ion monitoring. The bath solution was automatically monitored by electrochemical testing method and then the results were collected by VC++Language programming. Thus, the composition of nick-el plating bath can be automatically monitored by this excellent and reliable method. Results The relationship between the nickel ions and the polarization current value at-1. 0 V(vs. SCE)was fitted as I=0. 002 01+6. 90×10-5ρby the system of on-line monito- ring of nickel ion concentration. For 120 g/L nickel plating solution, the concentration of the nickel ions was detected as 115. 5 g/L and 113. 7 g/L and the measuring error was 3. 78% and 5. 25% by this on-line monitoring and the EDTA titrimetric analysis, re-spectively. Conclusion With its high reliability, the system can not only be used to monitor the status of nickel plating bath, but also for the cadmium plating bath and the chromium plating bath. Most importantly, it can be used in harsh environment.%目的 研发一种能够在线监测镀镍槽液中镍离子含量的测试系统,并将此方法推广至镀铬、镉、铜等槽液. 方法 利用计算机VC++语言编程技术、Modbus通讯技术、西门子PLC技术组成监控系统,通过耐酸碱计量泵和耐酸碱流量计对镀镍槽液取液量进行控制和校正,采用电化学测试方法对待测槽液在线监测,采用VC++语言编程技术采集电化学测试数据,最终实现对镀镍槽液中镍离子含量的自动监测.结果 采用此自动控制系统测量镀镍槽液中镍离子的质量浓度,其与极化曲线中-1. 0 V

  13. Design of the On-line Detecting System for the Total Alkalinity in Boiler Water%锅炉水总碱度在线检测系统设计

    Institute of Scientific and Technical Information of China (English)

    邓宏康; 郁燕东; 吉训生; 贾云龙

    2013-01-01

    以流动注射分析系统为核心、LabVIEW为软件开发平台,设计了锅炉水总碱度在线检测系统.通过LabVIEW平台,实时采集流动注射分析系统中由pH电极测得的电压值并对采集到的信号进行分析和处理.根据流动注射分析峰的面积与锅炉水总碱度对数之间的线性关系,通过计算得到锅炉水的总碱度.运行测试结果表明,该系统测量精度高、可扩展性强、操作简单、人机界面友好,可在线、实时、有效、快速地测定锅炉水总碱度.%The on-line detecting system for total alkalinity in boiler water is designed with flow injection analysis (FIA) system as the core and LabVIEW as software developing platform.The voltage values that measured by the pH electrode in FIA system are acquired in real time through the LabVIEW platform,and the acquired signals are analyzed and processed.In accordance with the linear relationship between the peak area of FIA and the logarithm of the total alkalinity in boiler water,the total alkalinity in boiler water can be determined.The test result shows that the system features high precision,good extensibility,simply operation and user-friendly interface; it implements online,effective and rapid measurement in real time for the total alkalinity in boiler water.

  14. Connecting to On-line Data

    Science.gov (United States)

    Eichhorn, G.; Astrophysics Datacenter Executive Committee (ADEC)

    2004-05-01

    The Astrophysics Datacenter Executive Committee (ADEC) is coordinating the development of a system to facilitate the linking to on-line data. This system has three components: 1. Unique dataset identifiers. 2. A verification system for identifiers. 3. Permanent links to on-line data sets. 1. The ADEC has agreed on a naming scheme for data sets that allows for the unique identification of any data set. The ADEC data centers will clearly mark their data with these identifiers to allow the generation of links to these data. 2. Each data center has a utility that can check whether a data set identifier is a valid identifier at that center. A central verifier allows third parties access to these individual verifiers through a single portal. 3. The central verifier also provides permanent links to data sets through a central link forwarding system. This makes it possible to move data sets between data centers while maintaining the permanent links. The ADEC plans to first use this system to implement the linking from the literature to on-line data in a collaboration with the AAS and the University of Chicago Press for the AAS journals.

  15. 粘土湿型砂处理系统的在线检测及质量控制%On-Line Test and Quality Control of Green Clay Moulding Sand Treating System

    Institute of Scientific and Technical Information of China (English)

    吴毅

    2011-01-01

    简述了型砂在线检测装置与质量控制系统的发展过程,介绍了以日本新东公司的MIA、MIC、MIE型砂控制系统为典型代表的全程在线检测装置与质量控制系统、以德国爱立许公司的质量师系统为典型代表的全程在线检测装置与质量控制系统和以常州好迪公司为代表的国产SC在线检测及质量控制装置的特点、控制精度及适用范围,总结了在线检测装置与质量控制系统的选用原则及注意事项.%The development process of the on-line test device and the quality control system was briefly described. An introduction was given to the characteristics and their application scope of some typical on-line full process test devices and the quality control systems including the SINTO-MIA, MIC, MIE moulding sand control system (Japan), EIRICH quality master system (Germany), and as well as, the on-line test and control device developed by the Haodi company(Changzhou, China) through assimilating the advanced technique from abroad. The usage principle and matters to be pay attentions of the on-line test device and quality system was also proposed.

  16. Application of On-line Cleaning and Prefilming Technology in Refinery Circulating Cooling Water System%不停车清洗预膜技术在炼油循环冷却水系统的应用

    Institute of Scientific and Technical Information of China (English)

    2015-01-01

    Plants in refinery are various, due to the needs of production and operation, circulating cooling water system cannot be shut down for cleaning and prefilming, resulting in corrosion and fouling problems of the water cooler. The on-line cleaning and prefilming technology can realize the cleaning and prefilming of the circulating cooling water system without stopping, so that the scaling and corrosion of the circulating cooling water system can be controlled. The feasibility of the on-line cleaning and prefilming technology was investigated through using the on-line cleaning and prefilming technology in the circulating cooling water system of a refinery, and some suggestions were put forward.%炼化企业装置较多,由于生产经营的需要,循环冷却水系统可能不能停工进行清洗预膜,导致水冷器的腐蚀、结垢问题。不停车清洗预膜可以实现在不停车的情况下在线进行清洗预膜,这样就可以控制系统的结垢和腐蚀问题。某炼油厂通过不停车清洗预膜的实施效果,考察了其可行性,并提出了一些建议。

  17. Development of on-line sorting system for detection of infected seed potatoes using visible near-infrared transmittance spectral technique

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Dae Yong; Cho, Byoung Kwan [Dept. of Biosystems Engineering, Chungnam National University, Daejeon (Korea, Republic of); Mo, Chang Yeun [Rural Development Administration, National Institute of Agricultural Engineering, Jeonju (Korea, Republic of); Kang, Jun Soon [Dept. of Horticultural Bioscience, Pusan National University, Pusan (Korea, Republic of)

    2015-02-15

    In this study, an online seed potato sorting system using a visible and near infrared (40 1100 nm) transmittance spectral technique and statistical model was evaluated for the nondestructive determination of infected and sound seed potatoes. Seed potatoes that had been artificially infected with Pectobacterium atrosepticum, which is known to cause a soil borne disease infection, were prepared for the experiments. After acquiring transmittance spectra from sound and infected seed potatoes, a determination algorithm for detecting infected seed potatoes was developed using the partial least square discriminant analysis method. The coefficient of determination(R{sup 2}{sub p}) of the prediction model was 0.943, and the classification accuracy was above 99% (n = 80) for discriminating diseased seed potatoes from sound ones. This online sorting system has good potential for developing a technique to detect agricultural products that are infected and contaminated by pathogens.

  18. Development of an on-line image analysis for assessment of pyrite liberation. Technical report, December 1, 1992--February 28, 1993

    Energy Technology Data Exchange (ETDEWEB)

    Yen, M.S.C.; Chu, P.T.C. [Southern Illinois Univ., Carbondale, IL (United States); Ho, K. [Illinois Clean Coal Inst., Carterville, IL (United States)

    1993-05-01

    An automation procedure based on the principles of image processing is proposed to perform the analysis of pyrite/minerals liberation of coal. To make the automated image analysis system possible, a data base of the light reflectance characteristics of different coal constituents must be established. Characterization of coal images through the analysis of their histogram was conducted. In general, it was found that the distinction of coal particles or particle groups may be accomplished by determining the gray levels of zero pixel or by taking average gray level of each particle. In particular, when the gray level averaging is applied, the spread of gray levels of a given maceral becomes smaller. In other words, the spread in gray level among different maceral group becomes larger. This has led to a distinct boundary between different material group of coal. Two computer programs based on these findings are being developed. The implementation of these criteria will cover most of the coal samples that are previously analyzed. Consideration of special cases will require additional data analysis of histogram.

  19. Design and application of on-line monitoring system for capacitor voltage transformer%电容式电压互感器绝缘在线监测系统设计与应用

    Institute of Scientific and Technical Information of China (English)

    黄嘉鹏; 陈贤顺; 张福州; 李涛

    2016-01-01

    In order to ensure capacitor voltage transformer(CVT) in safe operation, an on-line monitoring system has been designed. In this paper, on on-line monitoring program is given and equivalent circuit of CVT is established. Calc-ulation formula of dielectric loss factor and capacity for CVT are deduced. Design of on-line monitoring system for ins-ulating property is in detail introduced, including current signal acquisition circuit, voltage signal acquisition circuit and A/D sampling circuit. The on-line monitoring system has been applicated to 500kV substation in Sichuan. The accuracy and effectiveness of the online monitoring system monitoring are verified by monitoring results.%为保障电容式电压互感器(Capacitor Voltage Transformer, CVT)的安全可靠运行,设计了绝缘在线监测系统。给出了CVT在线监测方案,建立了CVT等值电路,推导了介质损耗角正切值和电容量的计算公式,详细阐述了绝缘在线监测系统的设计,包括:电流信号采集电路、电压信号采集电路和A/D采样电路等。该监测系统已经在四川某500kV变电站进行了挂网运行,在线监测结果验证了在线监测系统监测的准确性和有效性。

  20. Problems in On-line Correction and Production of Instrument Control System%仪表控制系统联校与投运中必须注意的几个问题

    Institute of Scientific and Technical Information of China (English)

    陈永刚

    2001-01-01

    本文阐述了在仪表控制系统联校与投运过程中必须注意的准备工作、安全及精度等问题。%Some problems that must be paid attention to during on-line correction and production of instrument control system, such as preparation, safety and precision, are described in this paper.

  1. Clean Air OnLine

    Energy Technology Data Exchange (ETDEWEB)

    Finney, D. [Environment Canada, Gatineau, PQ (Canada). Air Pollution Prevention Directorate

    2004-04-07

    This presentation describes Clean Air OnLine, a multi-tiered website dedicated to providing Canadians with information on air quality. The website is under development to support action to reduce air emissions, demonstrate the links between air emissions and environmental impacts, and enhance the understanding of sustainable community development issues such as health, energy, and urban sprawl. Partners in the Clean Air OnLine (CAOL) initiative include Environment Canada and the Clean Air Partnership which includes the Greater Toronto Area pilot project. The audience for CAOL includes municipal decision makers, local decision makers, community leaders, and the general public. The project provides Canadians with air pollution contextual information on pollution sources, pollutants, and related issues. It also provides information on health, environmental and economic impacts and the interrelationships with climate change issues and energy use. tabs., figs.

  2. Analysis on Diagnosis of MOA On-line Detection%金属氧化物避雷器带电检测诊断分析

    Institute of Scientific and Technical Information of China (English)

    陈颖

    2013-01-01

    This paper introduces the principle of metal oxide surge arrester charged detection,analyzes the metal oxide surge arrester live detection and diagnosis methods,takes the on-line detection test combined with the examples,considers that detection diagnosis method can j udge metal oxide surge arrester defects,and puts forward the suggestions.%介绍金属氧化物避雷器带电检测的原理,分析金属氧化物避雷器带电检测和诊断的方法,结合实例进行带电诊断试验,认为带电检测诊断方法可有效判断金属氧化物避雷器运行中的缺陷,并提出相关建议。

  3. An analysis of Taguchi's on-line quality monitoring procedure for variables based on the results of a sequence of inspections

    Directory of Open Access Journals (Sweden)

    Linda Lee Ho

    2012-04-01

    Full Text Available In this paper, a procedure for the on-line process control of variables is proposed. This procedure consists of inspecting the m-th item from every m produced items and deciding, at each inspection, whether the process is out-of-control. Two sets of limits, warning (µ0 ± W and control (µ0 ± C, are used. If the value of the monitored statistic falls beyond the control limits or if a sequence of h observations falls between the warning limits and the control limits, the production is stopped for adjustment; otherwise, production goes on. The properties of an ergodic Markov chain are used to obtain an expression for the average cost per item. The parameters (the sampling interval m, the widths of the warning, the control limits W and C(W < C, and the sequence length (h are optimized by minimizing the cost function. A numerical example illustrates the proposed procedure.

  4. Epoxidized soy bean oil migrating from the gaskets of lids into food packed in glass jars. Analysis by on-line liquid chromatography-gas chromatography.

    Science.gov (United States)

    Fankhauser-Noti, Anja; Fiselier, Katell; Biedermann-Brem, Sandra; Grob, Koni

    2005-08-01

    The migration of epoxidized soy bean oil (ESBO) from the gasket in the lids of glass jars into foods, particularly those rich in edible oil, often far exceeds the legal limit (60 mg/kg). ESBO was determined through a methyl ester isomer of diepoxy linoleic acid. Transesterification occurred directly in the homogenized food. From the extracted methyl esters, the diepoxy components were isolated by normal-phase LC and transferred on-line to gas chromatography with flame ionization detection using the on-column interface in the concurrent solvent evaporation mode. The method involves verification elements to ensure the reliability of the results for every sample analyzed. The detection limit is 2-5 mg/kg, depending on the food. Uncertainty of the procedure is below 10%.

  5. DESIGN AND IMPLEMENTATION OF HALF ON -LINE EXAMINATION SYSTEMS FOR CONTINUING MEDICAL EDUCATION%半网络化的医学继续教育考试系统设计与实施

    Institute of Scientific and Technical Information of China (English)

    吴东; 唐丽娜; 何建璋

    2015-01-01

    由于大型的网络化在线学习与考试系统对资金、技术、人员均有一定要求,因此,虽已有较为成熟的产品,但是,至今为止都没有得到普遍的推广和应用。本文实现的半网络化的医学继续教育考试系统,仅在发卷与收卷过程中采用在线操作方式,命题、考试(练习)、阅卷等过程均可离线进行,这样既避免了对网络的实时依赖,又解决了远程考试的用户需求,是对目前的在线考试系统的一种良好补充。对于技术力量较弱的边远地区和基层医院,半网格化的考试系统也许更有应用优势。%A large coverage on-line learning and examination systems on the internet so far has not gained wide usage and application even though some systems are available commercially because those internet based systems have certain demands of capitals , technology and skilled personals .Our system is half on -line and half off line for examinations .The on-line part is for giving out examination questions and collecting answers , whereas student writ-ing exams and instructors marking the exams are carried out by going off -line.Such a exam-writing application re-duces its dependence on the internet , which is easier for exam-writers in a remote area to use .This half on-line system can be used as a back -up application for the whole on -line examination system , but definitely has more ad-vantages for hospitals in remote areas where the internet is not reliable and popular , and well-trained technicians are lacking.

  6. Research of on-line monitoring method for insulation condition of power transformer bushing

    Science.gov (United States)

    Xia, Jiuyun; Qian, Zheng; Yu, Hao; Yao, Junda

    2016-01-01

    The power transformer is the key equipment of the power system; its insulation condition will directly influence the security and reliability of the power system. Thus, the on-line monitoring of power transformer is urgently required in order to guarantee the normal operation of the power system. Moreover, the dielectric loss factor is a significant parameter reflecting the condition of transformer bushing, so the on-line measurement of dielectric loss factor is really important. In this paper, the phase-to-phase comparison method is selected as the on-line monitoring method based on the overall analysis and discussion of the existing on-line monitoring methods. At first, the harmonic analysis method is utilized to calculate the dielectric loss of each phase of the three-phase transformer bushing, and then the differences of dielectric loss between every two phases are calculated and analyzed. So the insulation condition of each bushing could be achieved based on the careful analysis of different phase-to-phase dielectric loss. The simulation results of phase-to-phase comparison method are carried out in this paper, and the validity is verified. At last, this method is utilized in an actual equipment of on-line monitoring.

  7. Quantitative Determination of ABT-925 in Human Plasma by On-Line SPE and LC-MS/MS: Validation and Sample Analysis in Phase II Studies

    Directory of Open Access Journals (Sweden)

    Katty Wan

    2010-05-01

    Full Text Available A fully automated 96-well On-Line Solid Phase Extraction (SPE followed by High Performance Liquid Chromatography (HPLC-Tandem Mass Spectrometric (MS/MS method for the determination of ABT-925 (2-{3-[4-(2-tert-Butyl-6-trifluoromethyl-pyrimidin-4-yl-piperazin-1-yl-propyl-sulfanyl}-3H-pyrimidin-4-one fumarate in human plasma was developed, validated and utilized in Phase II clinical studies. 50 µL of plasma sample was fortified with internal standard (IS, d8-ABT-925 and extracted on-line with Cohesive Turbo Flow Cyclone P HTLC column. The chromatographic separation was performed on Aquasil C18 (3 μm 50 × 3 mm HPLC column with a mobile phase consisting of 50/50/0.1 (v/v/v ACN/H2O/formic acid. The mass spectrometric measurement was conducted under positive ion mode using multiple reaction monitoring (MRM of m/z 457.4 → 329.4 for analyte and m/z 465.5 → 337.5 for IS.The peak area ratio (analyte/IS was used to quantitate ABT-925. A dynamic range of 0.0102 μg/mL to 5.24 μg/mL was established after the validation. The validated method was then used for two Phase II studies. To demonstrate the method reproducibility, approximately 10% of the incurred samples from one study were repeated in singlet. The repeated values were compared to the initial values. All repeated values agreed within ±15% of the mean values.

  8. Quantitative Determination of ABT-925 in Human Plasma by On-Line SPE and LC-MS/MS: Validation and Sample Analysis in Phase II Studies.

    Science.gov (United States)

    Wan, Katty; Rieser, Matthew; El-Shourbagy, Tawakol

    2010-05-04

    A fully automated 96-well On-Line Solid Phase Extraction (SPE) followed by High Performance Liquid Chromatography (HPLC)-Tandem Mass Spectrometric (MS/MS) method for the determination of ABT-925 (2-{3-[4-(2-tert-Butyl-6-trifluoromethyl-pyrimidin-4-yl)-piperazin-1-yl)-propyl-sulfanyl}-3H-pyrimidin-4-one fumarate) in human plasma was developed, validated and utilized in Phase II clinical studies. 50 µL of plasma sample was fortified with internal standard (IS, d8-ABT-925) and extracted on-line with Cohesive Turbo Flow Cyclone P HTLC column. The chromatographic separation was performed on Aquasil C18 (3 μm 50 × 3 mm) HPLC column with a mobile phase consisting of 50/50/0.1 (v/v/v) ACN/H₂O/formic acid. The mass spectrometric measurement was conducted under positive ion mode using multiple reaction monitoring (MRM) of m/z 457.4 → 329.4 for analyte and m/z 465.5 → 337.5 for IS.The peak area ratio (analyte/IS) was used to quantitate ABT-925. A dynamic range of 0.0102 μg/mL to 5.24 μg/mL was established after the validation. The validated method was then used for two Phase II studies. To demonstrate the method reproducibility, approximately 10% of the incurred samples from one study were repeated in singlet. The repeated values were compared to the initial values. All repeated values agreed within ±15% of the mean values.

  9. Are we effectively informing patients? A quantitative analysis of on-line patient education resources from the American Society of Neuroradiology.

    Science.gov (United States)

    Hansberry, D R; Agarwal, N; Gonzales, S F; Baker, S R

    2014-07-01

    The ubiquitous use of the Internet by the public in an attempt to better understand their health care requires the on-line resources written at an appropriate level to maximize comprehension for the average user. The National Institutes of Health and the American Medical Association recommend on-line patient education resources written at a third-to-seventh grade level. We evaluated the readability of the patient education resources provided on the Web site of the American Society of Neuroradiology (http://www.asnr.org/patientinfo/). All patient education material from the ASNR Web site and the Society of Neurointerventional Surgery Web site were downloaded and evaluated with the computer software, Readability Studio Professional Edition, by using 10 quantitative readability scales: the Flesch Reading Ease, Flesch-Kincaid Grade Level, Simple Measure of Gobbledygook, Coleman-Liau Index, Gunning Fog Index, New Dale-Chall, FORCAST Formula, Fry Graph, Raygor Reading Estimate, and New Fog Count. An unpaired t test was used to compare the readability level of resources available on the American Society of Neuroradiology and the Society of Neurointerventional Surgery Web sites. The 20 individual patient education articles were written at a 13.9 ± 1.4 grade level with only 5% written at Society of Neuroradiology and Society of Neurointerventional Surgery Web sites. The patient education resources on these Web sites fail to meet the guidelines of the National Institutes of Health and American Medical Association. Members of the public may fail to fully understand these resources and would benefit from revisions that result in more comprehensible information cast in simpler language. © 2014 by American Journal of Neuroradiology.

  10. On-line cut-off technique and organic modifier addition aided signal enhancement for trace analysis of carbohydrates in cellulase hydrolysate by ion exclusion chromatography-electrospray ionization mass spectrometry.

    Science.gov (United States)

    Cheng, Cheanyeh; Tsai, Hsiang-Rong; Chang, Kuo-Chung

    2006-06-30

    Paper cellulose has been hydrolyzed with calcium alginate immobilized cellulase to produce carbohydrate products and the three trace sugars, galactose, arabinose, and mannose in the cellulase hydrolysate have been analyzed by HPIEC/ESI-MS. Applying the on-line cut-off technique to the HPIEC/ESI-MS can cut the high concentration glucose off to eliminate its interference on the peaks of minor sugars and enhance their signals from 1.1- to 1.6-fold. However, the on-line post column addition of 15% ethanol to the eluate can increase the signal of the three trace sugars, galactose, arabinose, and mannose up to 17-, 23-, and 11-fold, respectively, and make the corresponding detection limits as 0.04, 0.04, and 0.03 ppm. The accuracies of the quantitative analysis for the three trace sugars with the signal enhanced HPIEC/ESI-MS by the two enhancement methods were larger than 95%. The precisions of the analytical results were also greatly improved by the assistance of the two techniques and were less than 6.5%. The quantitative analysis of the three trace sugars was performed with the internal standard method and the internal standard (IS) was sorbitol. Overall, the signal enhancement of HPIEC/ESI-MS and quantification of the three trace sugars by the on-line cut-off technique and organic modifier addition was successful.

  11. 基于广域测量系统的电压稳定指标%A On-Line Voltage Stability Index Based on Wide Area Measurement System

    Institute of Scientific and Technical Information of China (English)

    巩伟峥; 房鑫炎

    2011-01-01

    综述和比较了多种基于广域测量的在线电压静态稳定指标,通过理论分析指出了这几种指标的理论缺陷和使用限制.利用同步测量的母线电压相量、线路潮流等电气量,根据线路潮流电压方程计算比较线路两侧电压水平,提出了一种新的电压稳定性指标Ivs,指示被监测线路或母线的电压稳定情况.通过系统等效的方法解耦多机系统的线路电压耦合性,可将该指标推广到多机系统.在单机单负荷系统和IEEE 14节点系统的仿真表明,Ivs可以准确快速地判断系统线路电压稳定情况,预测线路电压失稳点,且适用于所有种类的线路.与之前的电压静态稳定指标相比,Ivs具有无需判断线路电阻,物理概念清晰,适用范围广,线性度好等优点,有利于实现在线电压稳定监测和评估.%On-line steady state voltage stability indices based on wide area measurement system (WAMS) are summarized and compared. Based on theoretical analysis, the theoretical defects and usage limitations of these indices are pointed out. Utilizing synchronously measured electric quantities such as bus voltage phasors and line power flows and according to the comparison results of voltage levels, which are calculated by power flow and voltage equations of transmission line, at both terminals oftransmission lines, a new voltage stability index Ivs is proposed to indicate the voltage stability condition of monitored bus or transmission line. By means of system equivalence, the coupling of line voltage in multi-machine power system is decoupled, thus the proposed voltage stability index can be applied to multi-machine power system. Simulation results fiom single-machine single-load system and IEEE 14-bus system show that voltage stability condition of transmission line can be rapidly judged and the voltage instability point can be predicted by the proposed index IVS, and the proposed index is suitable to all kinds of transmission

  12. Countermeasures of Stimulated-Raman-Scattering-Induced Video Distortion in 1.65 μm Optical Time-domain Reflectometer On-line Monitoring 1.55 μm Cable Television System

    Science.gov (United States)

    Tsai, Szu-Chi; Tu, Yuan-Kuang; Chen, Yung-Kuang

    2003-07-01

    The countermeasures of stimulated-Raman-scattering (SRS)-induced baseband video distortion in the 1.65 μm optical time-domain reflectometer (OTDR) on-line monitoring 1.55 μm amplitude modulation with vestigial sideband (AM-VSB) cable television (CATV) transmission system are investigated theoretically and experimentally. The countermeasures entail the reduction in the optical modulation index (OMI) of the AM transmitter, OTDR peak power and/or pulse width. The results of numerical simulations and experimental measurements are in good agreement. Moreover, the countermeasure for eliminating the SRS-induced baseband video distortion by the 1.31 μm OTDR on-line monitoring technique is investigated and demonstrated.

  13. Sistema portátil para medida on-line da distribuição de tempo de residência na extrusão Portable system for on-line measurement of the residence time distribution in twin-screw extrusion

    Directory of Open Access Journals (Sweden)

    Denilson M. Santos

    1999-06-01

    Full Text Available A Curva de Distribuição de Tempos de Residência - CDTR tem sido largamente usada para caracterização do tipo de fluxo em extrusoras, sendo que medidas "on-line" permitem diagnosticar de modo muito rápido problemas como desgaste entre a rosca e o barril da extrusora, estagnação do material e outros. A CDTR pode ser determinada fazendo-se uso da técnica de estímulo de pulso único, onde um traçador é introduzido no sistema em um dado instante e sua concentração é estimada na saída. Este artigo propõe um sistema portátil de medida "on-line" feito através da variação da luz transmitida medida com um detector constituído por uma fonte de radiação visível e uma célula fotoelétrica e um software de coleta e tratamento de dados. Usando-se este sistema em uma extrusora de dupla rosca co-rotacional interpenetrante, pode-se verificar que a CDTR é muito mais sensível à variações na taxa de alimentação do que da velocidade de rotação da rosca e que as frações mais lentas do traçador podem demorar quatro vezes mais que as mais rápidas para saírem. Aumento na velocidade de rotação da rosca e/ou redução na taxa de alimentação aumenta o fluxo axial alargando a CDTR.The residence time distribution curve (RTDC is largely used to characterize extruder and continuous mixers flow types and on-line measurements allow quick diagnosis of their related problems. The RTDC can be obtained by the single impulse technique, where the tracer is fed into the system at one time and its concentration is estimated at the exit. This paper presents a portable on-line system consisting of a detector which has a light source, an photoelectric cell and a software to collect and analyze the data. Using this system in an intermeshing co-rotating double screw extruder one can verify that the RTDC is much more sensitive to changes of the feeding rate than the screw speed and that the slower tracer fractions may take four times longer than the

  14. On-line Monitoring and Active Control for Transformer Noise

    Science.gov (United States)

    Liang, Jiabi; Zhao, Tong; Tian, Chun; Wang, Xia; He, Zhenhua; Duan, Lunfeng

    This paper introduces the system for on-line monitoring and active noise control towards the transformer noise based on LabVIEW and the hardware equipment including the hardware and software. For the hardware part, it is mainly focused on the composition and the role of hardware devices, as well as the mounting location in the active noise control experiment. And the software part introduces the software flow chats, the measurement and analysis module for the sound pressure level including A, B, C weighting methods, the 1/n octave spectrum and the power spectrum, active noise control module and noise data access module.

  15. On-Line Wavelength Calibration of Pulsed Laser for CO2 Differential Absorption LIDAR

    Science.gov (United States)

    Xiang, Chengzhi; Ma, Xin; Han, Ge; Liang, Ailin; Gong, Wei

    2016-06-01

    Differential absorption lidar (DIAL) remote sensing is a promising technology for atmospheric CO2 detection. However, stringent wavelength accuracy and stability are required in DIAL system. Accurate on-line wavelength calibration is a crucial procedure for retrieving atmospheric CO2 concentration using the DIAL, particularly when pulsed lasers are adopted in the system. Large fluctuations in the intensities of a pulsed laser pose a great challenge for accurate on-line wavelength calibration. In this paper, a wavelength calibration strategy based on multi-wavelength scanning (MWS) was proposed for accurate on-line wavelength calibration of a pulsed laser for CO2 detection. The MWS conducted segmented sampling across the CO2 absorption line with appropriate number of points and range of widths by using a tunable laser. Complete absorption line of CO2 can be obtained through a curve fitting. Then, the on-line wavelength can be easily found at the peak of the absorption line. Furthermore, another algorithm called the energy matching was introduced in the MWS to eliminate the backlash error of tunable lasers during the process of on-line wavelength calibration. Finally, a series of tests was conducted to elevate the calibration precision of MWS. Analysis of tests demonstrated that the MWS proposed in this paper could calibrate the on-line wavelength of pulsed laser accurately and steadily.

  16. From Off-line to On-line Handwriting Recognition

    NARCIS (Netherlands)

    Lallican, P.; Viard-Gaudin, C.; Knerr, S.

    2004-01-01

    On-line handwriting includes more information on time order of the writing signal and on the dynamics of the writing process than off-line handwriting. Therefore, on-line recognition systems achieve higher recognition rates. This can be concluded from results reported in the literature, and has been

  17. On-line restricted access molecularly imprinted solid phase extraction of ivermectin in meat samples followed by HPLC-UV analysis.

    Science.gov (United States)

    de Lima, Marcela Marília; Vieira, André Coutinho; Martins, Isarita; Boralli, Vanessa Bergamin; Borges, Keyller Bastos; Figueiredo, Eduardo Costa

    2016-04-15

    A new restricted access molecularly imprinted polymer coated with bovine serum albumin (RAMIP-BSA) was synthesized, characterized and used for direct analysis of ivermectin from bovine meat samples, in a two-dimensional liquid chromatography system with UV detection. Ivermectin, 4-vynilpiridine and ethylene glycol dimethacrylate were employed as template, functional monomer and cross-linker, respectively. A BSA layer was cross-linked around the polymer, resulting in a biocompatible chemical barrier able to eliminate about 100% of protein from the samples. Ivermectin was extracted from the minced meat samples through a solvent extraction using methanol:water (70:30, v:v), and the extracts were directly injected into the two-dimensional liquid chromatography system, without any other treatment. Samples, fortified with ivermectin from 50 to 500 μg kg(-1), were used to build the analytical calibration curve (r=0.996). The limit of quantification was 50 μg kg(-1). Precision and accuracy presented variation coefficients, as well as relative errors lower than 17.0% and within -18.5% and 22.0%, respectively.

  18. On-line extractive separation in flow injection analysis based on polymer inclusion membranes: a study on membrane stability and approaches for improving membrane permeability.

    Science.gov (United States)

    Zhang, Lujia L; Cattrall, Robert W; Ashokkumar, Muthupandian; Kolev, Spas D

    2012-08-15

    The effect of temperature on the sensitivity and sampling rate is studied for a flow injection analysis (FIA) system that uses a membrane separation cell fitted with a polymer inclusion membrane (PIM) for the determination of Zn(II). A temperature of 50 °C for the flowing donor and acceptor solutions and the membrane separation cell improves the sensitivity and the sampling rate relative to 20 °C up to 10-fold and 2-fold, respectively. Studies on the stability of the PIM are reported that show a limited loss of the membrane liquid phase into the aqueous phases used in the FIA system but this has exhibited a negligible effect on the amount of Zn(II) transported across the membrane. Most importantly, the extent of leaching of the PIM components is shown to depend on the nature of the aqueous phase with the membrane eventually reaching a stable composition. It is also shown that the application of ultrasound to the membrane separation cell leads to a slight increase in sensitivity without affecting the long term membrane stability.

  19. Analysis of heterocyclic amines in hair by on-line in-tube solid-phase microextraction coupled with liquid chromatography−tandem mass spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Kataoka, Hiroyuki, E-mail: hkataoka@shujitsu.ac.jp; Inoue, Tsutomu; Saito, Keita; Kato, Hisato; Masuda, Kazufumi

    2013-07-05

    Graphical abstract: Mutagenic and carcinogenic heterocyclic amines are accumulated in the hair of smoker. -- Highlights: •On-line in-tube solid-phase microextraction of heterocyclic amines was optimized. •Fourteen heterocyclic amines were simultaneously determined by LC–MS/MS. •Pico gram levels of heterocyclic amines could be easily analyzed within 15 min. •Heterocyclic amines could be quantitatively analyzed from several milligrams of hair. •The method is useful for the assessment of long-term exposure to heterocyclic amines. -- Abstract: Mutagenic and carcinogenic heterocyclic amines (HCAs) are formed during heating of various proteinaceous foods, but human exposure to HCAs has not yet been elucidated in detail. To assess long-term exposure to HCAs, we developed a simple and sensitive method for measuring HCAs in hair by automated on-line in-tube solid-phase microextraction (SPME) coupled with liquid chromatography–tandem mass spectrometry (LC–MS/MS). Using a Zorbax Eclipse XDB-C8 column, 16 HCAs were analyzed within 15 min. The optimum in-tube SPME conditions were 20 draw/eject cycles of 40 μL sample at a flow rate of 200 μL min{sup −1} using a Supel-Q PLOT capillary column as an extraction device. The extracted HCAs were easily desorbed from the column by passage of the mobile phase, with no carryover observed. This in-tube SPME LC–MS/MS method showed good linearity for HCAs in the range of 10–2000 pg mL{sup −1}, with correlation coefficients above 0.9989 (n = 18), using stable isotope-labeled HCA internal standards. The detection limits (S/N = 3) of 14 HCAs except for MeAαC and Glu-P-1 were 0.10–0.79 pg mL{sup −1}. This method was successfully utilized to analyze 14 HCAs in hair samples without any interference peaks, with quantitative limits (S/N = 10) of about 0.17–1.32 pg mg{sup −1} hair. Using this method, we evaluated the exposure to HCAs in cigarette smoke and the suitability of using hair HCAs as exposure biomarkers.

  20. The influence of specific mechanical energy on cornmeal viscosity measured by an on-line system during twin-screw extrusion

    Directory of Open Access Journals (Sweden)

    CHANG Y. K.

    1999-01-01

    Full Text Available The influence of specific mechanical energy (SME on cornmeal viscosity during the twin-screw extrusion at feed moisture contents of 25 and 30% and screw speeds in the range from 100 to 500 rpm was measured. Cornmeal was extruded in a co-rotating, intermeshing twin-screw coupled to a slit die rheometer. One approach to the on-line rheological measurement is to use a slit die with the extruder. In the present work it was show that shear viscosity decreased as a function of SME. The viscosity of cornmeal at the exit die was influenced by screw speed, rate of total mass flow, mass temperature inside the extruder and SME. An increase in screw speed resulted in an increase in SME and a decrease in viscosity. A reduction in slit die height and an increase in screw speed and mass temperature led to a remarkable macromolecular degradation of the starch, as evidenced by the decrease in viscosity.

  1. ISTAR: Intelligent System for Telemetry Analysis in Real-time

    Science.gov (United States)

    Simmons, Charles

    1994-01-01

    The intelligent system for telemetry analysis in real-time (ISTAR) is an advanced vehicle monitoring environment incorporating expert systems, analysis tools, and on-line hypermedia documentation. The system was developed for the Air Force Space and Missile Systems Center (SMC) in Los Angeles, California, in support of the inertial upper stage (IUS) booster vehicle. Over a five year period the system progressed from rapid prototype to operational system. ISTAR has been used to support five IUS missions and countless mission simulations. There were a significant number of lessons learned with respect to integrating an expert system capability into an existing ground system.

  2. On-line capillary isotachophoresis-capillary zone electrophoresis analysis of bromate in drinking waters in an automated analyzer with coupled columns and photometric detection.

    Science.gov (United States)

    Marák, Jozef; Staňová, Andrea; Vaváková, Veronika; Hrenáková, Martina; Kaniansky, Dušan

    2012-12-07

    A new, sensitive, and robust analytical method based on capillary zone electrophoresis with on-line capillary isotachophoresis sample pretreatment (ITP-CZE) using a column-coupling (CC) arrangement of automated capillary electrophoretic analyzer was developed for determination of bromate in different type of drinking water samples. Both columns were provided with contact-less conductivity detectors and in CZE step UV detection at 200 nm wavelength was used. Electroosmotic flow of the buffer solutions was suppressed with the addition of 0.1% or 0.05% (m/v) methylhydroxyethylcellulose into the leading and terminating electrolyte, respectively. Hydrodynamic and electroosmotic flows of the buffer solutions were successfully suppressed and therefore, only the electrophoretic transport of ions was significant. Limit of detection for bromate approaching 0.6 μg/L was achieved. Good repeatabilities of migration time (RSD less than 0.3%) and peak area (RSD less than 4.0%) at concentration level 1 μg/L were obtained. Robustness of proposed ITP-CZE method and validation parameters were evaluated. Developed automated ITP-CZE method was applied to the determination of bromate in drinking water samples with different content of inorganic macroconstituents without the need of further sample preparation.

  3. Accelerated solvent extraction followed by on-line solid-phase extraction coupled to ion trap LC/MS/MS for analysis of benzalkonium chlorides in sediment samples

    Science.gov (United States)

    Ferrer, I.; Furlong, E.T.

    2002-01-01

    Benzalkonium chlorides (BACs) were successfully extracted from sediment samples using a new methodology based on accelerated solvent extraction (ASE) followed by an on-line cleanup step. The BACs were detected by liquid chromatography/ion trap mass spectrometry (LC/MS) or tandem mass spectrometry (MS/MS) using an electrospray interface operated in the positive ion mode. This methodology combines the high efficiency of extraction provided by a pressurized fluid and the high sensitivity offered by the ion trap MS/MS. The effects of solvent type and ASE operational variables, such as temperature and pressure, were evaluated. After optimization, a mixture of acetonitrile/water (6:4 or 7:3) was found to be most efficient for extracting BACs from the sediment samples. Extraction recoveries ranged from 95 to 105% for C12 and C14 homologues, respectively. Total method recoveries from fortified sediment samples, using a cleanup step followed by ASE, were 85% for C12BAC and 79% for C14-BAC. The methodology developed in this work provides detection limits in the subnanogram per gram range. Concentrations of BAC homologues ranged from 22 to 206 ??g/kg in sediment samples from different river sites downstream from wastewater treatment plants. The high affinity of BACs for soil suggests that BACs preferentially concentrate in sediment rather than in water.

  4. Arsenic speciation analysis in mono-varietal wines by on-line ionic liquid-based dispersive liquid-liquid microextraction.

    Science.gov (United States)

    Escudero, Leticia B; Martinis, Estefanía M; Olsina, Roberto A; Wuilloud, Rodolfo G

    2013-05-01

    A highly efficient separation and pre-concentration method for arsenic species determination, based on ionic liquid (IL) dispersive microextraction technique implemented in a flow analysis system, is proposed. Highly selective separation of arsenite species [As(III)] was achieved by chelation with sodium diethyldithiocarbamate (DDTC) followed by dispersion with 40 mg of 1-octyl-3-methylimidazolium hexafluorophosphate ([C(8)mim][PF(6)]) IL. Analyte extraction, retention and separation of IL phase were achieved with a packed microcolumn and As(III) was determined in eluent solution by electrothermal atomic absorption spectrometry (ETAAS). Concentration of As(V) was deduced by the difference between total inorganic arsenic and As(III). Thus, determination of total arsenic was performed by previous degradation of organo-arsenic species, followed by a reduction. Under optimal conditions, As(III) extraction efficiency was 100% and a sensitivity enhancement factor of 46 was obtained with only 4.0 ml of sample The method was successfully applied for arsenic speciation studies in mono-varietal wines.

  5. An on-line spectrophotometric determination of trace amounts of thiourea in tap water, orange juice, and orange peel samples using multi-channel flow injection analysis.

    Science.gov (United States)

    Arab Chamjangali, M; Goudarzi, N; Ghochani Moghadam, A; Amin, A H

    2015-01-01

    In this work, a flow injection analysis (FIA) method was introduced for the determination of trace amounts of thiourea in tap water. This method is based upon the inhibition effect of thiourea on the reaction between meta-cresol purple (MCP) and potassium bromate catalyzed by bromide ions in a sulfuric acid medium. In the presence of thiourea, an induction period appears in the reaction system, and as a result, the absorbance of MCP increases at 525 nm in the FIA manifold. The chemical and FIA variables are studied and optimized using the univariate and Simplex optimization methods. Under the optimum conditions, thiourea can be determined in the range of 0.100-13.0 μg mL(-1). The limit of detection (3σ) for thiourea was found to be 0.0310 μg mL(-1). The relative standard deviations (RSDs) for six replicate determinations of 0.500, 5.00, and 12.0 μg mL(-1) of thiourea were 4.0%, 1.8%, and 1.2%, respectively. The proposed method was also applied for the determination of thiourea in orange juice and orange peel samples with recoveries in the range of 98.0-101%. The analytical speed of the method was calculated to be about 120 sample per hour.

  6. Electrochemical oxidation and cleavage of peptides analyzed with on-line mass spectrometric detection

    NARCIS (Netherlands)

    Permentier, H.P.; Jurva, U; Barroso, B.; Bruins, A.P.

    2003-01-01

    An on-line electrochernistry/electrospray mass spectrometry system (EC/MS) is described that allows fast analysis of the oxidation products of peptides. A range of peptides was oxidized in an electrochemical cell by application of a potential ramp from 0 to 1.5 V during passage of the sample. Electr

  7. Simultaneous analysis of aspartame and its hydrolysis products of Coca-Cola Zero by on-line postcolumn derivation fluorescence detection and ultraviolet detection coupled two-dimensional high-performance liquid chromatography.

    Science.gov (United States)

    Cheng, Cheanyeh; Wu, Shing-Chen

    2011-05-20

    An innovative two-dimensional high-performance liquid chromatography system was developed for the simultaneous analysis of aspartame and its hydrolysis products of Coca-Cola Zero. A C8 reversed-phase chromatographic column with ultraviolet detection was used as the first dimension for the determination of aspartame, and a ligand-exchange chromatographic column with on-line postcolumn derivation fluorescence detection was employed as the second dimension for the analysis of amino acid enantiomers. The fluorimetric derivative reagent of amino acid enantiomers was o-phthaldialdehyde. The hydrolysis of aspartame in Coca-Cola Zero was induced by electric-heating or microwave heating. Aspartame was quantified by the matrix matched external standard calibration curve with a linear concentration range of 0-50 μg mL(-1) (r(2)=0.9984). The limit of detection (LOD) and the limit of quantification (LOQ) were 1.3 μg mL(-1) and 4.3 μg mL(-1), respectively. The amino acid enantiomers was analyzed by the matrix matched internal standard calibration method (D-leucine as the internal standard) with a linear concentration range of 0-10 μg mL(-1) (r(2)=0.9988-0.9997). The LODs and LOQs for L- and D-aspartic acid and L- and D-phenylalanine were 0.16-0.17 μg mL(-1) and 0.52-0.55 μg mL(-1), respectively, that was 12-13 times more sensitive than ultraviolet detection. The overall analysis accuracy for aspartame and amino acid enantiomers was 90.2-99.2% and 90.4-96.2%, respectively. The overall analysis precision for aspartame and amino acid enantiomers was 0.1-1.7% and 0.5-6.7%, respectively. Generally, the extent of aspartame hydrolysis increases with the increase of electro-thermal temperature, microwave power, and the duration of hydrolysis time. D-aspartic acid and D-phenylalanine can be observed with the electro-thermal racemization at the hydrolysis temperature 120°C for 1 day and only D-aspartic acid can be observed at the hydrolysis temperature 90°C for 2 and 3 days. For

  8. On-Line Monitoring System for Insulator Salt Density Based on Optical Fiber Sensing Technology and Its Application%绝缘子盐密在线监测系统及其应用

    Institute of Scientific and Technical Information of China (English)

    骆东松; 黄靖梅

    2013-01-01

    The optical field distribution theory of optical waveguide was introduced based on the feasibility study of the optical fiber sensor to measure the external insulation pollution degree of the transmission and transformation power equipment.The light energy parameters of quartz glass used as the optical sensor was analyzed by spectral data analysis algorithm and the corresponding relationship between luminous flux attenuation and salt density was set up.Subsequently the optical sensor Pollution Monitoring System was developed to realize the on-line monitoring of insulator salt density.The system has already been applied in Tianshui 330 kV transmission line and the results are satisfied.The test results indicate that the system can timely and accurately monitor the salt density of the transmission and distribution equipment,and guide the production department to clean the transmission and distribution equipment in order to avoid excessive or insufficient maintenance.%基于光纤传感器测量输变电设备外绝缘污秽度的可行性研究,引入了光波导中的光场分布理论.通过光谱数据分析算法,分析了石英玻璃作为光传感器的各种光能特性,建立了光通量的衰减与盐密间的数学模型,进而研制了基于光传感器的污秽在线监测系统,实现对绝缘子盐密的在线监测.该系统已在天水330 kV输电线路陇西1-2线瓷绝缘子和复合绝缘子测点挂网运行,并取得了良好的监测效果.试验结果表明,该系统能实时、准确地监测输变电设备的盐密值,掌握输变电设备的积污规律,进而指导生产部门对输变电设备的状态清扫.以避免过度检修和检修不足的状况.

  9. Cable Fault Traveling Wave on Line Monitoring System Based on LabVIEW%基于LabVIEW的电缆故障行波在线监测系统

    Institute of Scientific and Technical Information of China (English)

    段金英

    2011-01-01

    The buried cables effected by complex, uneven electric field and thermal field, the surrounding environment and many other factors,has high rate of accidents. This paper presented a better real-time monitoring system,with the use of the development platform of National Instruments Corporation Lab VIEW virtual instrument and data acquisition cards, collects the continuous voltage,current of cable line and other parameters,to monitor the operation of transmission lines,The monitoring system realizes the fault current on-line monitoring through the device at the scene access to the Hall sensor cable voltage and current signals from the data acquisition card on the fault wave pop electric high-speed sampling and storage control, with the use of graphical programming language designed to monitor PC interface. Experimental results show that the system can accurately record fault current waveforms, amplitude, provide important data analysis of fault type and location.%针对埋地电缆敷设复杂,发生事故率高的情况,提出了使用LabVIEW和数据采集卡,不间断采集电缆线路上的电压、电流等参数,监视输电线路运行状况,并通过TCP节点,构建了一个实时性较好的监测系统.该监控系统通过装在现场的霍尔传感器获取电缆的电压电流信号,由数据采集卡对故障电流行波进行高速采样和存储控制,利用具有图形化的编程语言设计上位机监控界面,实现了故障电流的在线监测.试验结果表明:该系统能够准确地记录故障电流波形、幅值,为故障类型分析和定位提供了重要数据.

  10. 智能变电站二次系统在线监测评估的研究%Research on secondary system on-line monitoring and evaluation in smart substation

    Institute of Scientific and Technical Information of China (English)

    李妍; 车勇; 单强; 孙建龙; 胡国伟; 李鹏; 李建波; 刘战朋

    2016-01-01

    In view of the changes in communication structure, operating environment and quantity of information of the secondary system of smart substation, an online monitoring and assessing system structure of the secondary system is proposed. Such a system structure will make trend judgement and loss assessment of safety risks in smart substation through monitoring and evaluating its core parameters and operating conditions. Around 6 parts with protection and bay control unit, smart terminal, merging unit, HMI, time synchronization system and switch in the secondary system, the complete on-line monitoring and assessment model is described from three aspects — the evaluation parameter model, the evaluation sub-item model and the evaluation model, and finally the evaluation process of the on-line monitoring system is given. It can carry out the on-line monitoring and status assessment to the secondary system of the smart substation, bring great convenience for the maintenance and repair of the system and lay a foundation for performing the condition based maintenance and it also plays an important role in improving the safety and stable operation of the system.%针对智能变电站二次系统的通信结构、运行环境、信息量等的变化,提出了二次系统在线监测评估的体系架构。通过对其核心参数及运行状态的监测评估,对智能变电站安全隐患进行趋势性判断和损失性评估。围绕二次系统保护测控、智能终端、合并单元、监控系统、对时系统、交换机六大部分,从评估参量模型、评估子项模型和评估对象模型三个方面描述了完整的在线监测评估模型,最后给出了在线监测的评估流程。对智能变电站的二次系统进行在线监测与状态评估,为系统的维护检修带来很大的便利,为开展状态检修打下基础,对提高系统的安全稳定运行有重要作用。

  11. Enterprise Systems Analysis

    Science.gov (United States)

    2017-04-30

    is unavailable until a remediation process fixes the contamination problem. The final infrastructure system is the internet. The internet operates...Enterprise Systems Analysis Technical Report SERC-2017-TR-106 April 30 2017 Principal Investigator: Dr. Michael Pennock, Stevens Institute...Date April 30, 2017 Copyright © 2017 Stevens Institute of Technology The Systems Engineering Research Center (SERC

  12. Analysis for impedance electrochemistry 'on-line' of membrane/electrode assemble (MEA) of protons exchange membrane fuel cells (PEMFC); Analise por impedancia eletroquimica 'on-line' de conjuntos eletrodos/membrana (MEA) de celulas a combustivel a membrana polimetrica (PEMFC)

    Energy Technology Data Exchange (ETDEWEB)

    Santos, Antonio Rodolfo dos

    2007-07-01

    This work reports results of studies and characterization on membrane electrode assemblies (MEAs) for proton exchange membrane fuel cell (PEMFC). Some cell operation conditions and different processes of MEA production were investigated. The electrochemical impedance spectroscopy technique (EIS) (in situ - 0 to 16 A) was used 'on-line' as a tool for diagnosis, concerning the cell performance. The EIS measurements were carried out with a FC350 Fuel Cell EIS System (GAMRY), coupled to a PC4 potentiostat/galvanostat and connected to the electronic load (TDI) for 'on-line' EIS experiments (100 mHz - 10 kHz, dU = 5 mV). MEAs with 25 cm{sup 2} surface area, using PtM/C 20% (M Ru, Sn or Ni) electrocatalysts were manufactured using the alcohol reduction process (ARP). The catalytic ink was applied directly into the carbon cloth (GDL) and pressed in the Nafion membrane (105). MEAs using Pt/C and Pt Ru/C 20% from E-TEK electrocatalysts were manufactured by comparison. All the cathodes were sprayed with Pt/C 20% from E-TEK. The noble metal concentrations used were set to 0.4 mg Pt.cm{sup -2} at the anode and 0.6 mg Pt.cm{sup -2} at the cathode (E-TEK). Nyquist diagrams of the MEAs with Pt/C and PtRu/C from E-TEK or PtM/C (M = Ru, Sn or Ni) ARP showed essentially the same ohmic resistances for the MEAs. This fact can be explained by suppression of agglomerates during the MEA preparation process or by the homogeneity of the anchored electrocatalysts at the carbon surface. It could also be observed, at low current densities, that there was a significant performance difference between the electrocatalysts from E-TEK and those prepared with the alcohol reduction process. The polarization curves results confirmed that the Pt M/C (M = Ru, Sn or Ni) ARP showed an activity increase for the methanol and ethanol fed cells. The technique of EIE was shown efficient for the evaluation of the method preparation of MEAs and the acting of the cell, the results of EIE

  13. The BIOSIS data base: Evaluation of its indexes and the STRATBLDR, CHEMFILE, STAIRS and DIALOG systems for on-line searching

    Science.gov (United States)

    Nees, M.; Green, H. O.

    1977-01-01

    An IBM-developed program, STAIRS, was selected for performing a search on the BIOSIS file. The evaluation of the hardware and search systems and the strategies used are discussed. The searches are analyzed by type of end user.

  14. Evolving factor analysis-based method for correcting monitoring delay in different batch runs for use with PLS: On-line monitoring of a transesterification reaction by ATR-FTIR.

    Science.gov (United States)

    Trevisan, Marcello G; Garcia, Camila M; Schuchardt, Ulf; Poppi, Ronei J

    2008-01-15

    In this work, the base-catalyzed transesterification of soybean oil with ethanol was monitored on-line using mid-infrared spectroscopy (MIRS) and the yield of fatty acid ethyl esters (biodiesel) was obtained by (1)H NMR spectroscopy. The MIRS monitoring carried out for 12min, was performed using a cylindrical internal reflectance cell of PbSe in the range of 3707-814cm(-1) with eight co-added scans. Two different data treatment strategies were used: in the first, the models were built using the raw data and in the other, evolving factor analysis (EFA) was used to overcome the sensor time delay due to the on-line analysis, producing significantly better results. In addition, models based on partial least squares (PLS) using three batches for calibration and another for validation were compared with models with just one batch for calibration and three for validation. The models were compared between each other using root mean square error of prediction (RMSEP) and root mean square prediction difference (RMSPD), obtaining relative errors under 3%.

  15. Analysis of Giga-size Earth Observation Data in Open Source GRASS GIS 7 - from Desktop to On-line Solutions.

    Science.gov (United States)

    Stepinski, T. F.; Mitasova, H.; Jasiewicz, J.; Neteler, M.; Gebbert, S.

    2014-12-01

    GRASS GIS is a leading open source GIS for geospatial analysis and modeling. In addition to being utilized as a desktop GIS it also serves as a processing engine for high performance geospatial computing for applications in diverse disciplines. The newly released GRASS GIS 7 supports big data analysis including temporal framework, image segmentation, watershed analysis, synchronized 2D/3D animations and many others. This presentation will focus on new GRASS GIS 7-powered tools for geoprocessing giga-size earth observation (EO) data using spatial pattern analysis. Pattern-based analysis connects to human visual perception of space as well as makes geoprocessing of giga-size EO data possible in an efficient and robust manner. GeoPAT is a collection of GRASS GIS 7 modules that fully integrates procedures for pattern representation of EO data and patterns similarity calculations with standard GIS tasks of mapping, maps overlay, segmentation, classification(Fig 1a), change detections etc. GeoPAT works very well on a desktop but it also underpins several GeoWeb applications (http://sil.uc.edu/ ) which allow users to do analysis on selected EO datasets without the need to download them. The GRASS GIS 7 temporal framework and high resolution visualizations will be illustrated using time series of giga-size, lidar-based digital elevation models representing the dynamics of North Carolina barrier islands over the past 15 years. The temporal framework supports efficient raster and vector data series analysis and simplifies data input for visual analysis of dynamic landscapes (Fig. 1b) allowing users to rapidly identify vulnerable locations, changes in built environment and eroding coastlines. Numerous improvements in GRASS GIS 7 were implemented to support terabyte size data processing for reconstruction of MODIS land surface temperature (LST) at 250m resolution using multiple regressions and PCA (Fig. 1c) . The new MODIS LST series (http://gis.cri.fmach.it/eurolst/) includes

  16. On-Line Core Thermal-Hydraulic Model Improvement

    Energy Technology Data Exchange (ETDEWEB)

    In, Wang Kee; Chun, Tae Hyun; Oh, Dong Seok; Shin, Chang Hwan; Hwang, Dae Hyun; Seo, Kyung Won

    2007-02-15

    The objective of this project is to implement a fast-running 4-channel based code CETOP-D in an advanced reactor core protection calculator system(RCOPS). The part required for the on-line calculation of DNBR were extracted from the source of the CETOP-D code based on analysis of the CETOP-D code. The CETOP-D code was revised to maintain the input and output variables which are the same as in CPC DNBR module. Since the DNBR module performs a complex calculation, it is divided into sub-modules per major calculation step. The functional design requirements for the DNBR module is documented and the values of the database(DB) constants were decided. This project also developed a Fortran module(BEST) of the RCOPS Fortran Simulator and a computer code RCOPS-SDNBR to independently calculate DNBR. A test was also conducted to verify the functional design and DB of thermal-hydraulic model which is necessary to calculate the DNBR on-line in RCOPS. The DNBR margin is expected to increase by 2%-3% once the CETOP-D code is used to calculate the RCOPS DNBR. It should be noted that the final DNBR margin improvement could be determined in the future based on overall uncertainty analysis of the RCOPS.

  17. Application of learning from examples methods for on-line dynamic security assessment of electric power systems - state of the art

    Energy Technology Data Exchange (ETDEWEB)

    Pecas Lopes, J.A. [Universidade do Porto, Porto (Portugal). Faculdade de Engenharia] Hatziargyriou, Nikos D. [National Technical University of Athens, Athens (Greece)

    1994-12-31

    This paper provides an overview of the application of `learning from examples` techniques like pattern recognition, artificial neural networks and decision trees, when used for fast dynamic security assessment. Problems concerning the system security evaluation relatively to transient stability and voltage stability are addressed with more details and references to research works in this field are briefly described. (author) 44 refs., 3 tabs.

  18. Multidisciplinary System Reliability Analysis

    Science.gov (United States)

    Mahadevan, Sankaran; Han, Song; Chamis, Christos C. (Technical Monitor)

    2001-01-01

    The objective of this study is to develop a new methodology for estimating the reliability of engineering systems that encompass multiple disciplines. The methodology is formulated in the context of the NESSUS probabilistic structural analysis code, developed under the leadership of NASA Glenn Research Center. The NESSUS code has been successfully applied to the reliability estimation of a variety of structural engineering systems. This study examines whether the features of NESSUS could be used to investigate the reliability of systems in other disciplines such as heat transfer, fluid mechanics, electrical circuits etc., without considerable programming effort specific to each discipline. In this study, the mechanical equivalence between system behavior models in different disciplines are investigated to achieve this objective. A new methodology is presented for the analysis of heat transfer, fluid flow, and electrical circuit problems using the structural analysis routines within NESSUS, by utilizing the equivalence between the computational quantities in different disciplines. This technique is integrated with the fast probability integration and system reliability techniques within the NESSUS code, to successfully compute the system reliability of multidisciplinary systems. Traditional as well as progressive failure analysis methods for system reliability estimation are demonstrated, through a numerical example of a heat exchanger system involving failure modes in structural, heat transfer and fluid flow disciplines.

  19. Collaboratory for Research on Electronic Work. Analysis of JSTOR: The Impact on Scholarly Practice of Access to On-Line Journal Archives.

    Science.gov (United States)

    Finholt, Thomas A.; Brooks, JoAnn M.

    This study reports on faculty response to the Journal STORage project (JSTOR), an online system for accessing digital back archives of core journals in history and economics. Data were collected about general journal use, Internet use, and JSTOR use via a survey administered to 160 historians and economists at the University of Michigan and at…

  20. On-line coupling of solid-phase extraction with mass spectrometry for the analysis of biological samples III. Determination of prednisolone in serum

    NARCIS (Netherlands)

    van Hout, M.W.J.; Hofland, C.M; Niederlander, H.A G; Bruins, A.P.; de Zeeuw, R.A.; de Jong, G.J.

    2003-01-01

    Solid-phase extraction (SPE) was directly coupled to mass spectrometry (MS) to assess the feasibility of the system for the rapid determination of prednisolone in serum. A C-18 stationary phase allowed washing of the cartridge with 25% methanol. Elution was performed by switching the methanol

  1. Electrochemically assisted Fenton reaction : reaction of hydroxyl radicals with xenobiotics followed by on-line analysis with high-performance liquid chromatography/tandem mass spectrometry

    NARCIS (Netherlands)

    Jurva, U; Wikstrom, HV; Bruins, AP

    2002-01-01

    Oxygen radicals are generated in vivo by various processes, often as toxic intermediates in different metabolic transformations, and have been shown to play an important role for a large number of diseases. In this article we introduce an electrochemical flow-through system that allows generation of

  2. On-line coupling of solid-phase extraction with mass spectrometry for the analysis of biological samples III. Determination of prednisolone in serum

    NARCIS (Netherlands)

    van Hout, MWJ; Hofland, CM; Niederlander, HAG; Bruins, AP; de Zeeuw, RA; de Jong, GJ

    2003-01-01

    Solid-phase extraction (SPE) was directly coupled to mass spectrometry (MS) to assess the feasibility of the system for the rapid determination of prednisolone in serum. A C-18 stationary phase allowed washing of the cartridge with 25% methanol. Elution was performed by switching the methanol percen

  3. Tunable diode laser absorption spectroscopy-based tomography system for on-line monitoring of two-dimensional distributions of temperature and H{sub 2}O mole fraction

    Energy Technology Data Exchange (ETDEWEB)

    Xu, Lijun, E-mail: lijunxu@buaa.edu.cn; Liu, Chang; Jing, Wenyang; Cao, Zhang [School of Instrument Science and Opto-Electronic Engineering, Beihang University, Beijing 100191 (China); Ministry of Education’s Key Laboratory of Precision Opto-Mechatronics Technology, Beijing 100191 (China); Xue, Xin; Lin, Yuzhen [School of Energy and Power Engineering, Beihang University, Beijing 100191 (China)

    2016-01-15

    To monitor two-dimensional (2D) distributions of temperature and H{sub 2}O mole fraction, an on-line tomography system based on tunable diode laser absorption spectroscopy (TDLAS) was developed. To the best of the authors’ knowledge, this is the first report on a multi-view TDLAS-based system for simultaneous tomographic visualization of temperature and H{sub 2}O mole fraction in real time. The system consists of two distributed feedback (DFB) laser diodes, a tomographic sensor, electronic circuits, and a computer. The central frequencies of the two DFB laser diodes are at 7444.36 cm{sup −1} (1343.3 nm) and 7185.6 cm{sup −1} (1391.67 nm), respectively. The tomographic sensor is used to generate fan-beam illumination from five views and to produce 60 ray measurements. The electronic circuits not only provide stable temperature and precise current controlling signals for the laser diodes but also can accurately sample the transmitted laser intensities and extract integrated absorbances in real time. Finally, the integrated absorbances are transferred to the computer, in which the 2D distributions of temperature and H{sub 2}O mole fraction are reconstructed by using a modified Landweber algorithm. In the experiments, the TDLAS-based tomography system was validated by using asymmetric premixed flames with fixed and time-varying equivalent ratios, respectively. The results demonstrate that the system is able to reconstruct the profiles of the 2D distributions of temperature and H{sub 2}O mole fraction of the flame and effectively capture the dynamics of the combustion process, which exhibits good potential for flame monitoring and on-line combustion diagnosis.

  4. The National Shipbuilding Research Program. Proceedings of the REAPS Technical Symposium. Paper No. 9: Drawing Office to Part Cutting With a Mini-Based On-Line System

    Science.gov (United States)

    1980-10-01

    shipyard has recently installed AUTOKON-79, AUTOPART , AUTONEST and developed several pipe fabrication and installation programs on an in-house PRIME 550...The most significant additions were TRALOS TRADET, and DRAW programs for the design office, and AUTOPART , AUTONEST, and AUTODRAW for the mould loft...incompatibility between the various systems. ALKON,TRALOS,TRADET and DRAW employ the AUTOBASE type database. AUTOPART and AUTONEST each employ their awn

  5. The 1-way on-line coupled atmospheric chemistry model system MECO(n – Part 1: The limited-area atmospheric chemistry model COSMO/MESSy

    Directory of Open Access Journals (Sweden)

    A. Kerkweg

    2011-06-01

    Full Text Available The numerical weather prediction model of the Consortium for Small Scale Modelling (COSMO, maintained by the German weather service (DWD, is connected with the Modular Earth Submodel System (MESSy. This effort is undertaken in preparation of a~new, limited-area atmospheric chemistry model. This model is as consistent as possible, with respect to atmospheric chemistry and related processes, with a previously developed global atmospheric chemistry general circulation model: the ECHAM/MESSy Atmospheric Chemistry (EMAC model. The combined system constitutes a new research tool, bridging the global to the meso-γ scale for atmospheric chemistry research. MESSy provides the infrastructure and includes, among others, the process and diagnostic submodels for atmospheric chemistry simulations. Furthermore, MESSy is highly flexible allowing model setups with tailor made complexity, depending on the scientific question. Here, the connection of the MESSy infrastructure to the COSMO model is documented. Previously published prototype submodels for simplified tracer studies are generalised to be plugged-in and used in the global and the limited-area model. They are used to evaluate the tracer transport characteristics of the new COSMO/MESSy model system, an important prerequisite for future atmospheric chemistry applications. A supplementary document with further details on the technical implementation of the MESSy interface into COSMO with a complete list of modifications to the COSMO code is provided.

  6. Analysis of Dietary Pattern Impact on Weight Status for Personalised Nutrition through On-Line Advice: The Food4Me Spanish Cohort.

    Science.gov (United States)

    San-Cristobal, Rodrigo; Navas-Carretero, Santiago; Celis-Morales, Carlos; Brennan, Lorraine; Walsh, Marianne; Lovegrove, Julie A; Daniel, Hannelore; Saris, Wim H M; Traczyk, Iwonna; Manios, Yannis; Gibney, Eileen R; Gibney, Michael J; Mathers, John C; Martinez, J Alfredo

    2015-11-17

    Obesity prevalence is increasing. The management of this condition requires a detailed analysis of the global risk factors in order to develop personalised advice. This study is aimed to identify current dietary patterns and habits in Spanish population interested in personalised nutrition and investigate associations with weight status. Self-reported dietary and anthropometrical data from the Spanish participants in the Food4Me study, were used in a multidimensional exploratory analysis to define specific dietary profiles. Two opposing factors were obtained according to food groups' intake: Factor 1 characterised by a more frequent consumption of traditionally considered unhealthy foods; and Factor 2, where the consumption of "Mediterranean diet" foods was prevalent. Factor 1 showed a direct relationship with BMI (β = 0.226; r² = 0.259; p dietary patterns, which were characterized by high-density foods consumption, showed positive associations with overweight prevalence. Further analysis showed that prevention of overweight must focus on limiting the intake of known deleterious foods rather than exclusively enhance healthy products.

  7. From User Comments to On-line Conversations

    OpenAIRE

    Wang, Chunyan; Ye, Mao; Huberman, Bernardo A.

    2012-01-01

    We present an analysis of user conversations in on-line social media and their evolution over time. We propose a dynamic model that accurately predicts the growth dynamics and structural properties of conversation threads. The model successfully reconciles the differing observations that have been reported in existing studies. By separating artificial factors from user behaviors, we show that there are actually underlying rules in common for on-line conversations in different social media web...

  8. Design and implementation of an automated liquid-phase microextraction-chip system coupled on-line with high performance liquid chromatography.

    Science.gov (United States)

    Li, Bin; Petersen, Nickolaj Jacob; Payán, María D Ramos; Hansen, Steen Honoré; Pedersen-Bjergaard, Stig

    2014-03-01

    An automated liquid-phase microextraction (LPME) device in a chip format has been developed and coupled directly to high performance liquid chromatography (HPLC). A 10-port 2-position switching valve was used to hyphenate the LPME-chip with the HPLC autosampler, and to collect the extracted analytes, which then were delivered to the HPLC column. The LPME-chip-HPLC system was completely automated and controlled by the software of the HPLC instrument. The performance of this system was demonstrated with five alkaloids i.e. morphine, codeine, thebaine, papaverine, and noscapine as model analytes. The composition of the supported liquid membrane (SLM) and carrier was optimized in order to achieve reasonable extraction performance of all the five alkaloids. With 1-octanol as SLM solvent and with 25 mM sodium octanoate as anionic carrier, extraction recoveries for the different opium alkaloids ranged between 17% and 45%. The extraction provided high selectivity, and no interfering peaks in the chromatograms were observed when applied to human urine samples spiked with alkaloids. The detection limits using UV-detection were in the range of 1-21 ng/mL for the five opium alkaloids presented in water samples. The repeatability was within 5.0-10.8% (RSD). The membrane liquid in the LPME-chip was regenerated automatically between every third injection. With this procedure the liquid membrane in the LPME-chip was stable in 3-7 days depending on the complexity of sample solutions with continuous operation. With this LPME-chip-HPLC system, series of samples were automatically injected, extracted, separated, and detected without any operator interaction.

  9. Enantioselective analysis of pheniramine in urine by charged CD-mediated CZE provided with a fiber-based DAD and an on-line sample pretreatment by capillary ITP.

    Science.gov (United States)

    Marák, Jozef; Mikus, Peter; Maráková, Katarína; Kaniansky, Dusan; Valásková, Iva; Havránek, Emil

    2007-08-01

    Application potentialities of CZE on-line coupled with capillary ITP and DAD to the identification and determination of trace concentration levels (microg/L) of pheniramine (PHM) enantiomers and their metabolites present in complex ionic matrices of biological origin (urine) are shown. An enhanced (enantio)selectivity of the CZE separation system obtained by the addition of carboxyethyl-beta-CD (CE-beta-CD) to the carrier electrolyte provided CZE conditions for a reliable identification of similar/identical DAD spectra of structurally related compounds (PHM enantiomers and their metabolites) in clinical urine samples differing in qualitative and quantitative composition of sample matrix constituents. A high sample loadability (a 30 microL sample injection volume), partial sample clean-up (removing macroconstituents from the sample), and preconcentration of the analytes in ITP stage resulted in the decrease of concentration LOD for PHM enantiomers in urine to 5.2 and 6.8 microg/L (2.2 x 10(-8) and 2.8 x 10(-8) mol/L), without using any sample pretreatment technique. The background correction and smoothing procedure applied to the raw DAD spectra provided analytically relevant DAD spectra of PHM enantiomers and their metabolites also when they were present in urine sample (30 microL injection volumes of ten-times diluted urine sample) at a 9 x 10(-) (8) mol/L concentration. DAD spectra of PHM enantiomers present in urine samples matched their reference spectra with reasonable certainties. DAD spectra of PHM metabolites were compared with the reference spectra of PHM enantiomers and a good match was found which indicates the similarities in the structures of enantiomers and their metabolites detected in the urine samples. This fact allows performing the quantitative analyses of PHM metabolites in the urine samples by applying the calibration parameters of PHM enantiomers also for PHM metabolites and the results show the possibilities of using the ITP

  10. Stable isotopic internal standard correction for quantitative analysis of hydroxyeicosatetraenoic acids (HETEs) in serum by on-line SPE-LC-MS/MS in selected reaction monitoring mode.

    Science.gov (United States)

    Fernández-Peralbo, M A; Ferreiro Vera, C; Priego-Capote, F; Luque de Castro, M D

    2014-08-01

    The influence of the inclusion of a stable isotopic labeled internal standard (SIL-IS) on the quantitative analysis of hydroxyeicosatetranoic acids (HETEs) in human serum is evaluated in this research. A solid-phase extraction-liquid chromatography-tandem mass spectrometry (SPE-LC-MS/MS) platform, one of the preferred approaches for targeted analysis of biofluids through the selected reaction monitoring (SRM) operational mode, was used to determine HETEs. These compounds were chosen as targeted metabolites because of their involvement in cardiovascular disease, cancer and osteoporosis. 15HETE-d8 was chosen as internal standard to evaluate matrix effects. Thus, the physico-chemical properties of the SIL-IS were the basis to evaluate the analytical features of the method for each metabolite through four calibration models. Two of the models were built with standard solutions at different concentration levels, but one of the calibration sets was spiked with an internal standard (IS). The other two models were built with the serum pool from osteoporotic patients, which was spiked at different concentrations with the target analytes. In this case, one of the serum calibration sets was also spiked with the IS. The study shows that the IS allowed noticeable correction of matrix effects for some HETE isomers at certain concentration levels, while accuracy was decreased at low concentration (15ng/mL) of them. Therefore, characterization of the method has been properly completed at different concentration levels. Copyright © 2014 Elsevier B.V. All rights reserved.

  11. On-Line Organic Solvent Field Enhanced Sample Injection in Capillary Zone Electrophoresis for Analysis of Quetiapine in Beagle Dog Plasma.

    Science.gov (United States)

    Cao, Yuqing; Wen, Jun; Zhou, Tingting; Fan, Guorong

    2016-01-21

    A rapid and sensitive capillary zone electrophoresis (CZE) method with field enhanced sample injection (FESI) was developed and validated for the determination of quetiapine fumarate in beagle dog plasma, with a sample pretreatment by LLE in 96-well deep format plate. The optimum separation was carried out in an uncoated 31.2 cm × 75 μm fused-silica capillary with an applied voltage of 13 kV. The electrophoretic analysis was performed by 50 mM phosphate at pH 2.5. The detection wavelength was 210 nm. Under these optimized conditions, FESI with acetonitrile enhanced the sensitivity of quetiapine about 40-50 folds in total. The method was suitably validated with respect to stability, specificity, linearity, lower limit of quantitation, accuracy, precision and extraction recovery. Using mirtazapine as an internal standard (100 ng/mL), the response of quetiapine was linear over the range of 1-1000 ng/mL. The lower limit of quantification was 1 ng/mL. The intra- and inter-day precisions for the assay were within 4.8% and 12.7%, respectively. The method represents the first application of FESI-CZE to the analysis of quetiapine fumarate in beagle dog plasma after oral administration.

  12. On-Line Organic Solvent Field Enhanced Sample Injection in Capillary Zone Electrophoresis for Analysis of Quetiapine in Beagle Dog Plasma

    Directory of Open Access Journals (Sweden)

    Yuqing Cao

    2016-01-01

    Full Text Available A rapid and sensitive capillary zone electrophoresis (CZE method with field enhanced sample injection (FESI was developed and validated for the determination of quetiapine fumarate in beagle dog plasma, with a sample pretreatment by LLE in 96-well deep format plate. The optimum separation was carried out in an uncoated 31.2 cm × 75 μm fused-silica capillary with an applied voltage of 13 kV. The electrophoretic analysis was performed by 50 mM phosphate at pH 2.5. The detection wavelength was 210 nm. Under these optimized conditions, FESI with acetonitrile enhanced the sensitivity of quetiapine about 40–50 folds in total. The method was suitably validated with respect to stability, specificity, linearity, lower limit of quantitation, accuracy, precision and extraction recovery. Using mirtazapine as an internal standard (100 ng/mL, the response of quetiapine was linear over the range of 1–1000 ng/mL. The lower limit of quantification was 1 ng/mL. The intra- and inter-day precisions for the assay were within 4.8% and 12.7%, respectively. The method represents the first application of FESI-CZE to the analysis of quetiapine fumarate in beagle dog plasma after oral administration.

  13. Linking NASA Environmental Data with a National Public Health Cohort Study and a CDC On-Line System to Enhance Public Health Decision Making

    Science.gov (United States)

    Al-Hamdan, Mohammad; Crosson, William; Economou, Sigrid; Estes, Maurice, Jr.; Estes, Sue; Hemmings, Sarah; Kent, Shia; Puckett, Mark; Quattrochi, Dale; Wade, Gina; McClure, Leslie

    2012-01-01

    The overall goal of this study is to address issues of environmental health and enhance public health decision making by utilizing NASA remotely-sensed data and products. This study is a collaboration between NASA Marshall Space Flight Center, Universities Space Research Association (USRA), the University of Alabama at Birmingham (UAB) School of Public Health and the Centers for Disease Control and Prevention (CDC) National Center for Public Health Informatics. The objectives of this study are to develop high-quality spatial data sets of environmental variables, link these with public health data from a national cohort study, and deliver the linked data sets and associated analyses to local, state and federal end-user groups. Three daily environmental data sets were developed for the conterminous U.S. on different spatial resolutions for the period 2003-2008: (1) spatial surfaces of estimated fine particulate matter (PM2.5) exposures on a 10-km grid utilizing the US Environmental Protection Agency (EPA) ground observations and NASA s MODerate-resolution Imaging Spectroradiometer (MODIS) data; (2) a 1-km grid of Land Surface Temperature (LST) using MODIS data; and (3) a 12-km grid of daily Solar Insolation (SI) and maximum and minimum air temperature using the North American Land Data Assimilation System (NLDAS) forcing data. These environmental datasets were linked with public health data from the UAB REasons for Geographic and Racial Differences in Stroke (REGARDS) national cohort study to determine whether exposures to these environmental risk factors are related to cognitive decline and other health outcomes. These environmental national datasets will also be made available to public health professionals, researchers and the general public via the CDC Wide-ranging Online Data for Epidemiologic Research (WONDER) system, where they can be aggregated to the county, state or regional level as per users need and downloaded in tabular, graphical, and map formats. The

  14. The Construction of the on-line Customization System based on Silverlight%基于Silverlight的在线定制系统的构建

    Institute of Scientific and Technical Information of China (English)

    蔡志恒

    2012-01-01

    名字首饰在线定制需要耗费大量的人工成本,主要表现在定制服务提供商与顾客、首饰生产商之间的频繁沟通。这个沟通过程繁琐且耗时,人工成本在名字首饰定制中占很大的比重。基于Silverlight RIA的名字首饰在线定制生产系统,通过改良Web交互性能,改造企业的业务流程,解决电子商务企业运营中遇到的实际问题,该系统降低了人工成本,提高了生产效率。Silverlight RIA在电子商务的这个解决方案,可以作为其他类似场合的借鉴。%The name jewelry online customization needs to consume a large number of labour cost,which primarily shows in frequent communication between customized service providers and customers,and between jewelry manufacturers.This process of communication is cumbersome and time-consuming,labour cost accounts for a large proportion in the name jewelry customization. Based on Silverlight RIA,the production system of name jewelry online customization reduces the labor cost and improves productivity by upgrading Web interactive performance and transforming business process,and the production system also solves the practical problems in the process of E-business enterprise operation.The solution of Silverlight RIA in the E-business can be used for reference in other similar occasion.

  15. On-line chemical composition analyzer development

    Energy Technology Data Exchange (ETDEWEB)

    Roberts, M.J.; Garrison, A.A.; Muly, E.C.; Moore, C.F.

    1992-02-01

    The energy consumed in distillation processes in the United States represents nearly three percent of the total national energy consumption. If effective control of distillation columns can be accomplished, it has been estimated that it would result in a reduction in the national energy consumption of 0.3%. Real-time control based on mixture composition could achieve these savings. However, the major distillation processes represent diverse applications and at present there does not exist a proven on-line chemical composition sensor technology which can be used to control these diverse processes in real-time. This report presents a summary of the findings of the second phase of a three phase effort undertaken to develop an on-line real-time measurement and control system utilizing Raman spectroscopy. A prototype instrument system has been constructed utilizing a Perkin Elmer 1700 Spectrometer, a diode pumped YAG laser, two three axis positioning systems, a process sample cell land a personal computer. This system has been successfully tested using industrially supplied process samples to establish its performance. Also, continued application development was undertaken during this Phase of the program using both the spontaneous Raman and Surface-enhanced Raman modes of operation. The study was performed for the US Department of Energy, Office of Industrial Technologies, whose mission is to conduct cost-shared R D for new high-risk, high-payoff industrial energy conservation technologies. Although this document contains references to individual manufacturers and their products, the opinions expressed on the products reported do not necessarily reflect the position of the Department of Energy.

  16. The 1-way on-line coupled model system MECO(n) - Part 4: Chemical evaluation (based on MESSy v2.52)

    Science.gov (United States)

    Mertens, Mariano; Kerkweg, Astrid; Jöckel, Patrick; Tost, Holger; Hofmann, Christiane

    2016-10-01

    For the first time, a simulation incorporating tropospheric and stratospheric chemistry using the newly developed MECO(n) model system is performed. MECO(n) is short for MESSy-fied ECHAM and COSMO models nested n times. It features an online coupling of the COSMO-CLM model, equipped with the Modular Earth Submodel System (MESSy) interface (called COSMO/MESSy), with the global atmospheric chemistry model ECHAM5/MESSy for Atmospheric Chemistry (EMAC). This online coupling allows a consistent model chain with respect to chemical and meteorological boundary conditions from the global scale down to the regional kilometre scale. A MECO(2) simulation incorporating one regional instance over Europe with 50 km resolution and one instance over Germany with 12 km resolution is conducted for the evaluation of MECO(n) with respect to tropospheric gas-phase chemistry. The main goal of this evaluation is to ensure that the chemistry-related MESSy submodels and the online coupling with respect to the chemistry are correctly implemented. This evaluation is a prerequisite for the further usage of MECO(n) in atmospheric chemistry-related studies. Results of EMAC and the two COSMO/MESSy instances are compared with satellite, ground-based and aircraft in situ observations, focusing on ozone, carbon monoxide and nitrogen dioxide. Further, the methane lifetimes in EMAC and the two COSMO/MESSy instances are analysed in view of the tropospheric oxidation capacity. From this evaluation, we conclude that the chemistry-related submodels and the online coupling with respect to the chemistry are correctly implemented. In comparison with observations, both EMAC and COSMO/MESSy show strengths and weaknesses. Especially in comparison to aircraft in situ observations, COSMO/MESSy shows very promising results. However, the amplitude of the diurnal cycle of ground-level ozone measurements is underestimated. Most of the differences between COSMO/MESSy and EMAC can be attributed to differences in the

  17. On-Line Long-Exposure Phase Diversity: a Powerful Tool for Sensing Quasi-Static Aberrations of Extreme Adaptive Optics Imaging Systems

    CERN Document Server

    Mugnier, L M; Fusco, T; Cornia, A; Dandy, S

    2008-01-01

    The phase diversity technique is a useful tool to measure and pre-compensate for quasi-static aberrations, in particular non-common path aberrations, in an adaptive optics corrected imaging system. In this paper, we propose and validate by simulations an extension of the phase diversity technique that uses long exposure adaptive optics corrected images for sensing quasi-static aberrations during the scientific observation, in particular for high-contrast imaging. The principle of the method is that, for a sufficiently long exposure time, the residual turbulence is averaged into a convolutive component of the image and that phase diversity estimates the sole static aberrations of interest. The advantages of such a procedure, compared to the processing of short-exposure image pairs, are that the separation between static aberrations and turbulence-induced ones is performed by the long-exposure itself and not numerically, that only one image pair must be processed, that the estimation benefits from the high SNR ...

  18. WINDOWS98下 XRF联机软件分析系统 (X荧光光谱仪改造升级技术)%The XRF On-line Software Analytical System Under Windows 98

    Institute of Scientific and Technical Information of China (English)

    向浩; 李国会; 王永青; 张天佑

    2001-01-01

    XRF On-line software analytical system under windows 98 is been studied and developed to remake and to enhance computer system of XRF spectrometer 3080 E1, E2, E3, 3070, 3530, VF-320. The 586 and the better than computer can be equipped with. The DF-151A(B), DF-350(B), 3070, 3530 and DP-32 software are replaced by the new software system, which has been carried out on the platform of Chinese window. The operating information of the on-line and off-line window interface are all Chinese. Many new modules are developed and expanded too. So the computer hardware and software of the 3080 E1, E2, E3, 3070, 3530 and VF-320, and so on are achieved advanced level.%WINDOWS98下 XRF联机软件分析系统是为日本理学、岛津等公司的3080E1,E2,E3,3070,3530,VF-320等XRF光谱仪计算机系统升级换代研究开发的,它可以配置586以上计算机,以新的软件取代DF-151A(B),DF-350(B),3070软件,DP-32软件,在中文WINDOWS平台上运行。联机及脱机窗口界面操作信息全部汉化,扩充和开发了许多新的软件模块,从而使3080,3070,3530,和VF-320等XRF光谱仪的计算机硬件及软件基本上达到了先进水平。

  19. On-line brain-computer interface system design based on alpha wave and motor imagery%基于脑电alpha波及运动想象的在线脑机接口系统设计

    Institute of Scientific and Technical Information of China (English)

    王磊; 王江; 刘丽芳; 杨硕; 徐桂芝; 颜威利

    2011-01-01

    背景:目前在线脑机接口系统绝大多数采用同步式设计,无法区分"工作"状态与"空闲"状态.目的:设计一种能够自由在"工作"与"空闲"状态间切换,方便灵活的脑机接口系统.方法:设计了综合睁眼产生的alpha波阻断现象,以及进行运动想象时产生事件相关同步及去同步现象这些生理特征的在线脑机接口系统.通过检测使用者枕部脑电信号alpha波状况,来切换"空闲"与"工作"状态;在"工作"状态下,通过想象不同的肢体运动,分析运动皮质脑电信号的频率特征,来实现对外界的信息传输.结果与结论:实验证明,经过训练的使用者在该在线脑机接口平台上可以自如的在不同状态间进行切换,并且能以很高的分类正确率发出控制命令.采用此方法进行设计,脑机接口系统的实用性得到了增强.%BACKGROUND: At present, most of on-line brain-computer interface (BCI) systems adopt synchronous design, which cannot tell the switch between "active" state and "idle" state.OBJECTIVE: To design an effective BCI system design, which is free to switch between "active" state and "idle" state.METHODS: In this paper, an on-line BCI system was designed based on a series of physiological phenomenon, such as alpha wave-block, event related synchronization (ERS) and event related desynchronization (ERD). Through detecting the EEG recorded from occipital area, the two states being "active" and "idle" could be switched. Under the statement of "active", EEG captured from motor cortex was processed, and the frequency feature was extracted during different motor imagery tasks, in the end, the mind that user wanted to express was estimated.RESULTS AND CONCLUSION: The results show that the subject can switch freely between the two states by using this on-line BCI system after training. Using this method, the practicability of on-line BCI system is getting improved greatly.

  20. 纯电动客车在线诊断系统设计及应用%Design and Application of On-line Diagnosis System for Pure Electric Bus

    Institute of Scientific and Technical Information of China (English)

    陈顺东; 尹剑

    2012-01-01

    At present, most pure electric bus production still relies on the artificial debugging of technicians. This can not adapt the mass production. The authors detail the on-line rapid diagnosis system for pure electric bus, which vails the mass production of the pure electric bus.%目前大部分纯电动客车生产时的整车性能调试依赖技术开发人员.非常不利于纯电动客车的批量生产。本文详述一种能够对纯电动客车进行快速调试和在线诊断的系统,有利于纯电动客车的批量生产。

  1. CONVEYOR SYSTEM SAFETY ANALYSIS

    Energy Technology Data Exchange (ETDEWEB)

    M. Salem

    1995-06-23

    The purpose and objective of this analysis is to systematically identify and evaluate hazards related to the Yucca Mountain Project Exploratory Studies Facility (ESF) surface and subsurface conveyor system (for a list of conveyor subsystems see section 3). This process is an integral part of the systems engineering process; whereby safety is considered during planning, design, testing, and construction. A largely qualitative approach was used since a radiological System Safety Analysis is not required. The risk assessment in this analysis characterizes the accident scenarios associated with the conveyor structures/systems/components in terms of relative risk and includes recommendations for mitigating all identified risks. The priority for recommending and implementing mitigation control features is: (1) Incorporate measures to reduce risks and hazards into the structure/system/component (S/S/C) design, (2) add safety devices and capabilities to the designs that reduce risk, (3) provide devices that detect and warn personnel of hazardous conditions, and (4) develop procedures and conduct training to increase worker awareness of potential hazards, on methods to reduce exposure to hazards, and on the actions required to avoid accidents or correct hazardous conditions. The scope of this analysis is limited to the hazards related to the design of conveyor structures/systems/components (S/S/Cs) that occur during normal operation. Hazards occurring during assembly, test and maintenance or ''off normal'' operations have not been included in this analysis. Construction related work activities are specifically excluded per DOE Order 5481.1B section 4. c.

  2. A versatile apparatus for on-line emission channeling experiments

    CERN Document Server

    da Silva, Manuel Ribeiro; Correia, João Guilherme; Amorim, Lígia Marina; Pereira, Lino Miguel da Costa

    2013-01-01

    The concept and functionality of an apparatus dedicated to emission channeling experiments using short-lived isotopes on-line at ISOLDE/CERN is described. The setup is assembled in two functional blocks - (a) base stand including beam collimation, implantation and measurement chamber, cryogenic extension, and vacuum control system and - (b) Panmure goniometer extension including maneuvering cradle and sample heating furnace. This setup allows for in situ implantation and sample analysis in the as-implanted state and upon cooling down to 50 K and during annealing up to 1200 K. The functionality of the setup will be illustrated with the example of establishing the lattice location of $^{56}$Mn probes implanted into GaAs.

  3. Are on-line currencies virtual banknotes?

    OpenAIRE

    Stephen F. Quinn; William Roberds

    2003-01-01

    The history of money is marked by innovations that have expanded the role of "inside money"-money created by the private sector. For instance, the past few years have seen the development of several types of on-line payment arrangements, some of which have been dubbed "on-line currencies." ; This article examines the likely success or failure of on-line currencies by means of a historical analogy. The discussion compares the introduction of on-line currencies to the debut of the bearer bankno...

  4. INTERACTIVE SYSTEM FOR ON-LINE CONSULTING

    Directory of Open Access Journals (Sweden)

    Negoescu Gheorghe

    2009-05-01

    Full Text Available Liberal professions, developed after 1990, require an historical casuistry that enable them to reach a pertinent conclusion to another similar case. Where there is not a similar case tried, it is required the need for a procedure for resolving differences

  5. INTERACTIVE SYSTEM FOR ON-LINE CONSULTING

    OpenAIRE

    Negoescu Gheorghe

    2009-01-01

    Liberal professions, developed after 1990, require an historical casuistry that enable them to reach a pertinent conclusion to another similar case. Where there is not a similar case tried, it is required the need for a procedure for resolving differences

  6. Digital Systems Analysis

    Science.gov (United States)

    Martin, Vance S.

    2009-01-01

    There have been many attempts to understand how the Internet affects our modern world. There have also been numerous attempts to understand specific areas of the Internet. This article applies Immanuel Wallerstein's World Systems Analysis to our informationalist society. Understanding this world as divided among individual core, semi-periphery,…

  7. URBAN EDUCATION SYSTEMS ANALYSIS.

    Science.gov (United States)

    CLARK, STEPHEN C.; AND OTHERS

    ANALYSIS OF URBAN EDUCATIONAL SYSTEMS MAY BE ACHIEVED BY USE OF AN ANALYTICAL MODEL. THE MODEL MAY BE USED IN DECISION-MAKING REGARDING SCHOOL LOCATION, ENROLLMENT, FACILITIES, ORGANIZATION, PROGRAMS AND COSTS. KNOWN DATA SUCH AS MONIES AVAILABLE, STAFF ALLOCATION, AND CURRENT SCHOOL PLANT ARE INTRODUCED INTO THE MODEL. IN THE STRUCTURE OF THE…

  8. Digital Systems Analysis

    Science.gov (United States)

    Martin, Vance S.

    2009-01-01

    There have been many attempts to understand how the Internet affects our modern world. There have also been numerous attempts to understand specific areas of the Internet. This article applies Immanuel Wallerstein's World Systems Analysis to our informationalist society. Understanding this world as divided among individual core, semi-periphery,…

  9. Asphalt pavement surface 3D data acquisition system based on line-structure light%基于线结构光的沥青路面三维数据采集系统

    Institute of Scientific and Technical Information of China (English)

    孙朝云; 呼延菊; 李伟; 魏子尧; 刘祝

    2016-01-01

    To solve the problem of poor real-time,low accuracy of current asphalt pavement surface 3D data acquisition system,which can not provide 3D pavement data comprehensively,this paper studied an asphalt pavement 3D data acquisition system based on line-structure light.The system was a three-dimensional equipment with optical and electrical integration and automation,which was designed for domestic road three-dimensional information detection.It could realize data collection,analysis,processing,3D display for asphalt pavement surface topography.The system used infrared laser light source,planar array CCD camera and digital image detection technology.This system computed the 3D depth information based on laser triangulation algorithm,finished 3D reconstruction of road surface morphology by use of MATLAB software to obtain 3D display after reconstruction,and did quantitative analysis of detection results.Based on modular design,this system mainly consisted of power supply module,salve computer control module,counting trigger module,laser triangulation detection module,GPS module and data processing module.The 3D data of asphalt pavement were obtained through testing software's driving hardware modules.The results show that modular design improves anti-interference,making the system structure simple and clear,and relieve from the complex wires.It is convenient for debugging,maintenance,shorten development cycle,and the cost for development and maintenance is also reduced.The results also show that the system can not only meet the requirements of asphalt pavement 3D data acquisition and the requirements of real-time detection,but also provide vivid and visualized 3D visual topography.17 figs,21 refs.%针对目前沥青路面表面形貌三维数据采集实时性差、精确度低,难以准确全面地提供路面三维构造形态的问题,研究了基于线结构光的沥青路面表面形貌三维数据采集系统.该系统是针对中国道路三维信息检测要求

  10. On-Line Voltage Stability Assessment based on PMU Measurements

    DEFF Research Database (Denmark)

    Garcia-Valle, Rodrigo; P. Da Silva, Luiz C.; Nielsen, Arne Hejde

    2009-01-01

    through statistic analysis. During the off-line analysis, a memory of high-risk situations following a pre-defined voltage stability criterion is obtained. Thereafter, basic statistics analyses are applied resulting in the definition of voltage regions. During on-line operation, voltage magnitudes......This paper presents a method for on-line monitoring of risk voltage collapse based on synchronised phasor measurement. As there is no room for intensive computation and analysis in real-time, the method is based on the combination of off-line computation and on-line monitoring, which are correlated...... of critical buses obtained by phasor measurements are monitored in relation to the risk regions. Comprehensive studies demonstrate that the proposed method could assist operators to avoid voltage collapse events, by taking preventive or emergency actions....

  11. Analysis of biogenic carbonates by inductively coupled plasma-mass spectrometry (ICP-MS). Flow injection on-line solid-phase preconcentration for trace element determination in fish otoliths.

    Science.gov (United States)

    Arslan, Z; Paulson, A J

    2002-04-01

    The aragonite deposits within the ear bones (otoliths) of teleost fish retain a chemical signal reflecting the life history of fish (similar to rings of trees) and the nature of fish habitats. Otoliths dissolved in acid solutions contain high concentrations of calcium and a variety of proteins. Elimination of matrix salts and organic interferences during preconcentration is essential for accurate determination of trace elements in otolith solutions by inductively coupled plasma-quadrupole mass spectrometry. An iminodiacetate-based chelating resin (Toyopearl AF-Chelate 650 M) has been used for on-line preconcentration and matrix separation for the determination of 31 transition and rare elements. Successful preconcentration of the elements was achieved at pH 5 by on-line buffering, except Mn which required pH 8.8. Sample solutions were loaded on to the column for 1 min at 3.2 mL min(-1), and then eluted directly into the mass spectrometer with 4% v/v nitric acid. This procedure enabled up to 25-fold preconcentration with successful removal of the calcium matrix. The effect of heat-assisted oxidation with concentrated nitric acid was investigated to eliminate the organic matrix. It was found that heating to dryness after dissolution and further mineralization with the acid significantly improved the retention of the transition elements. The method was validated by analysis of a certified reference material produced from saggittal otoliths of emperor snapper ( Lutjanus sebae), and then applied to the determination of trace metal concentrations in juvenile bluefin tuna ( Thunnus thynnus) from the Western Pacific Ocean.

  12. Analysis of biogenic carbonates by inductively coupled plasma-mass spectrometry (ICP-MS). Flow injection on-line solid-phase preconcentration for trace element determination in fish otoliths

    Energy Technology Data Exchange (ETDEWEB)

    Arslan, Z.; Paulson, A.J. [National Oceanic and Atmospheric Administration (NOAA), Northeast Fisheries Science Center (NFSC), James J. Howard Marine Sciences Laboratory, Highlands, NJ (United States)

    2002-04-01

    The aragonite deposits within the ear bones (otoliths) of teleost fish retain a chemical signal reflecting the life history of fish (similar to rings of trees) and the nature of fish habitats. Otoliths dissolved in acid solutions contain high concentrations of calcium and a variety of proteins. Elimination of matrix salts and organic interferences during preconcentration is essential for accurate determination of trace elements in otolith solutions by inductively coupled plasma-quadrupole mass spectrometry. An iminodiacetate-based chelating resin (Toyopearl AF-Chelate 650 M) has been used for on-line preconcentration and matrix separation for the determination of 31 transition and rare elements. Successful preconcentration of the elements was achieved at pH 5 by on-line buffering, except Mn which required pH 8.8. Sample solutions were loaded on to the column for 1 min at 3.2 mL min{sup -1}, and then eluted directly into the mass spectrometer with 4% v/v nitric acid. This procedure enabled up to 25-fold preconcentration with successful removal of the calcium matrix. The effect of heat-assisted oxidation with concentrated nitric acid was investigated to eliminate the organic matrix. It was found that heating to dryness after dissolution and further mineralization with the acid significantly improved the retention of the transition elements. The method was validated by analysis of a certified reference material produced from saggittal otoliths of emperor snapper (Lutjanus sebae), and then applied to the determination of trace metal concentrations in juvenile bluefin tuna (Thunnus thynnus) from the Western Pacific Ocean. (orig.)

  13. Sistema de Optimización en Línea y Diagnosis de Fallos para Procesos Químicos An On-line Optimization and Fault Diagnosis System for Chemical Processes

    Directory of Open Access Journals (Sweden)

    Ignacio Yélamos

    2007-01-01

    Full Text Available En este artículo, la técnica Evolución en Tiempo Real (ETR es aplicada a la optimización en línea de una columna de destilación multicomponente. Un Sistema de Diagnóstico de Fallos (SDF dentro de un módulo de supervisión es responsable de la gestión de cualquier incidencia (fallos o perturbaciones que ocurra en la planta, consiguiéndose un funcionamiento en línea más robusto. La implementación de este módulo supervisado (ETRS se ha llevado a cabo usando Matlab® y el simulador comercial Hysys®, aprovechando las posibilidades de comunicación existentes entre ambos. Se tratan diferentes incidencias, involucrando diferentes fuentes y tipos de perturbaciones. Los resultados de la ETRS son comparados con los que se obtuvieron mediante la Optimización en Tiempo Real clásica.In this paper, the Real Time Evolution technique (RTE is applied to the on-line optimization of a multi-component distillation column. A Fault Diagnosis System (FDS implemented within a supervisory module is responsible for handling incidences (faults or disturbances occurring in the plant, achieving more robust on-line performance. The implementation of the supervised scheme (SRTE has been performed using Matlab® and the commercial simulation software Hysys®, taking advantage of their communication capabilities. Different possible plant incidences are considered involving different sources and types of disturbances. Results of SRTE are compared with those obtained using the standard Real Time Optimization approach.

  14. On-Line and Back at S.F.U.

    Directory of Open Access Journals (Sweden)

    M. Sanderson

    1973-06-01

    Full Text Available Simon Fraser University library began operation with an automated circulation system. After deliberation, it mounted the first phase of a two-phase online circulation system. A radically revised loan pol·icy caused the system design and assumptions to be called into question. A cheaper, simpler, and more effective off-line system eventually replaced the on-line system. The systems, fiscal, and administrative implications of this decision are reviewed.

  15. An On-Line Monitoring System for Nitrate in Seawater Based on UV Spectrum%一种基于紫外光谱法的海水硝酸盐在线监测系统

    Institute of Scientific and Technical Information of China (English)

    李丹; 冯巍巍; 陈令新; 张骏

    2016-01-01

    Nitrate is one of the evaluation indicators of water quality ,which is particularly important for water quality monito-ring .A real-time on-line monitoring system of nitrate in water is introduced in this paper .And the ultraviolet absorption technol-ogy (190~370 nm) with partial least squares method is used to detect nitrate concentration .The automated online system based on ultraviolet absorption spectrum is capable of analyzing samples without any sample preservation and without contamination problems .This system is fast ,reliable ,and sensitive enough for continuous use on monitoring stations and nitrate concentration can also be determined directly via its ultraviolet absorption spectrum .This system uses flow sample cell with 1cm optical path length ,and a reference light is used to eliminate system error .The correlation coefficient for a linear function of the nitrate con-centrations is 0 .999 98 .So the results of the system model test are in good correlation with the laboratory ones .Data collected has been analyzed statistically to determine how system model behave throughout the test ,with special attention being paid to er-ror analysis .As the average relative error is 0.65% ,this system has greater stability and higher accuracy .The results of nitrate measurements by the field seawater tests in Yantai coast are obtained ,which nitrate concentrations are about 0.2 mg · L -1 in seawater ,and the recoveries of samples for standard recovery tests are in 95% ~110% ,it shows that this system is accurate ,re-liability and practicability and could be developed for detected nitrate concentration in natural water .%硝酸盐含量是水体质量指标之一 ,对于水质质量监测尤其重要.本文搭建了一种水体中硝酸盐在线原位监测系统 ,采用紫外吸收光谱法(190~240 nm )计算水样吸光度 ,并通过建立的偏最小二乘模型测定硝酸盐浓度 ,可用于海洋 ,河流 ,湖泊等多种水体.该自动在线监测系统

  16. Improving the efficiencies of simultaneous organic substance and nitrogen removal in a multi-stage loop membrane bioreactor-based PWWTP using an on-line Knowledge-Based Expert System.

    Science.gov (United States)

    Chen, Zhao-Bo; Nie, Shu-Kai; Ren, Nan-Qi; Chen, Zhi-Qiang; Wang, Hong-Cheng; Cui, Min-Hua

    2011-10-15

    The results of the use of an expert system (ES) to control a novel multi-stage loop membrane bioreactor (MLMBR) for the simultaneous removal of organic substances and nutrients are reported. The study was conducted at a bench-scale plant for the purpose of meeting new discharge standards (GB21904-2008) for the treatment of chemical synthesis-based pharmaceutical wastewater (1200-9600 mg/L COD, 500-2500 mg/L BOD5, 50-200 mg/L NH4+-N and 105-400 mg/L TN in the influent water) by developing a distributed control system. The system allows various expert operational approaches to be deployed with the goal of minimizing organic substances and nitrogen levels in the outlet while using the minimum amount of energy. The proposed distributed control system, which is supervised by a Knowledge-Based Expert System (KBES) constructed with G2 (a tool for expert system development) and a back propagation BP artificial neural network, permits the on-line implementation of every operating strategy of the experimental system. A support vector machine (SVM) is applied to achieve pattern recognition. A set of experiments involving variable sludge retention time (SRT), hydraulic retention time (HRT) and dissolved oxygen (DO) was carried out. Using the proposed system, the amounts of COD, TN and NH4+-N in the effluent decreased by 55%, 62% and 38%, respectively, compared to the usual operating conditions. These improvements were achieved with little energy cost because the performance of the treatment plant was optimized using operating rules implemented in real time. Copyright © 2011 Elsevier Ltd. All rights reserved.

  17. Development of an analytical method for the determination of the misuse in sports of boldenone through the analysis of urine by on-line coupling liquid chromatography-gas chromatography-combustion-isotope ratio mass spectrometry.

    Science.gov (United States)

    Toledano, R M; Díaz-Plaza, E M; Cortes, J M; Aragón, A; Vázquez, A M; Villén, J; Muñoz-Guerra, J

    2014-11-28

    Boldenone (Bo), androsta-1,4-dien-17β-ol-3-one, is an anabolic androgenic steroid not clinically approved for human application. Despite this, many cases are reported every year of athletes testing positive for Bo or its main metabolite 5β-androst-1-en-17β-ol-3-one (BoM). Recently the capability of different human intestinal bacteria to produce enzymes able to modify endogenous steroids in Bo has been demonstrated. When a urinary concentration of Bo and/or BoM between 5 and 30 ng/mL is measured a complementary analysis by gas chromatography combustion isotope ratio mass spectrometry (GC-C-IRMS) must be carried out to discriminate the endogenous or exogenous origin. In the present work, a novel analytical method that couples LC-GC by means of the TOTAD interface with C-IRMS is described. The method is based on a first RPLC separation of unacetyled steroids, followed by acetylation and automated on-line LC-GC-C-IRMS, which includes a second RPLC clean-up of acetyl Bo and BoM, isolation of the two fractions in a fraction collector and their consecutive analysis by GC-C-IRMS. The method has been applied to the analysis of urine samples fortified at 5 and 10 ng/mL, where it has shown a good performance.

  18. Automated document analysis system

    Science.gov (United States)

    Black, Jeffrey D.; Dietzel, Robert; Hartnett, David

    2002-08-01

    A software application has been developed to aid law enforcement and government intelligence gathering organizations in the translation and analysis of foreign language documents with potential intelligence content. The Automated Document Analysis System (ADAS) provides the capability to search (data or text mine) documents in English and the most commonly encountered foreign languages, including Arabic. Hardcopy documents are scanned by a high-speed scanner and are optical character recognized (OCR). Documents obtained in an electronic format bypass the OCR and are copied directly to a working directory. For translation and analysis, the script and the language of the documents are first determined. If the document is not in English, the document is machine translated to English. The documents are searched for keywords and key features in either the native language or translated English. The user can quickly review the document to determine if it has any intelligence content and whether detailed, verbatim human translation is required. The documents and document content are cataloged for potential future analysis. The system allows non-linguists to evaluate foreign language documents and allows for the quick analysis of a large quantity of documents. All document processing can be performed manually or automatically on a single document or a batch of documents.

  19. Determination of anions with an on-line capillary electrophoresis method; Anionien on-line maeaeritys kapillaarielektroforeesilla - MPKT 10

    Energy Technology Data Exchange (ETDEWEB)

    Siren, H.; Saerme, T.; Kotiaho, T.; Hiissa, T.; Savolahti, P.; Komppa, V. [VTT Chemical Technology, Espoo (Finland)

    1998-12-31

    The aim of the study was to set-up an on-line capillary electrophoresis method for determination of anions in process waters of pulp and paper industry with exporting the results to the process control system of the mill. The quantification is important, since it will give information about the possible causes of precipitation. In recent years, the capillary electrophoresis (CE) due to its high separation efficiency has been shown as a method to take into consideration when analyzing chemical species ranging from small inorganic anions to different macromolecules. Many compounds are not easily detected in their native state, why analysis methods must be developed to improve their detection. Especially, small inorganic and organic anions which do not have chromophores are not sensitive enough for direct-UV detection. In such analyses the anions are mostly detected with indirect-UV technique. Capillary electrophoresis instruments are used to analyze samples in off-line, which seldom represent the situation in process. Therefore, on-line instrument technology with autoanalyzing settings will be needed in quality control. The development of a fully automatic capillary electrophoresis system is underway in co-operation with KCL (The Finnish Pulp and Paper Research Institute). In our research, we have first concentrated on the determination of sulphate in waters of paper industry. The method used for detection of sulphate is based on indirect-UV detection with CE, where the background electrolyte (BGE) is an absorbing mixture of secondary amines. The whole procedure for quantification of sulphate is performed within 15 minutes, after which a new sample is analyzed automatically. The only sample pretreatment is filtration, which is necessary before analysis. The concentrations of sulphate in process waters tested were between 300 and 800 ppm. Our tests show that a simultaneous determination of chloride, sulphate, nitrate, nitrite, sulphite, carbonate and oxalate is also

  20. On line routing per mobile phone

    DEFF Research Database (Denmark)

    Bieding, Thomas; Görtz, Simon; Klose, Andreas

    2009-01-01

    On-line routing is concerned with building vehicle routes in an ongoing fashion in such a way that customer requests arriving dynamically in time are efficiently and effectively served. An indispensable prerequisite for applying on-line routing methods is mobile communication technology. Addition...