Non-destructive inservice inspections

International Nuclear Information System (INIS)

Kauppinen, P.; Sarkimo, M.; Lahdenperae, K.

1998-01-01

In order to assess the possible damages occurring in the components and structures of operating nuclear power plants during service the main components and structures are periodically inspected by non-destructive testing techniques. The reliability of non-destructive testing techniques applied in these inservice inspections is of major importance because the decisions concerning the needs for repair of components are mainly based on the results of inspections. One of the targets of this research program has been to improve the reliability of non-destructive testing. This has been addressed in the sub-projects which are briefly summarised here. (author)

Material characterization and non destructive testing by ultrasounds; modelling, simulation and experimental validation; Caracterisation des materiaux et controle non destructif par ultrasons; modelisation, simulation et validation experimentale

Energy Technology Data Exchange (ETDEWEB)

Noroy-Nadal, M H

2002-06-15

This memory presents the research concerning the characterization of materials and the Non Destructive Testing (N.D.T) by ultrasonics. The different topics include three steps: modeling, computations and experimental validation. The studied materials concern mainly metals. The memory is divided in four parts. The first one concerns the characterization of materials versus temperature. The determination of the shear modulus G(T) is especially studied for a large temperature range, and around the melting point. The second part is devoted to studies by photothermal devices essentially focused on the modeling of the mechanical displacement and the stress field in coated materials. In this particular field of interest, applications concern either the mechanical characterization of the coating, the defect detection in the structure and finally the evaluation of the coating adhesion. The third section is dedicated to microstructural characterization using acoustic microscopy. The evaluation of crystallographic texture is especially approached, for metallic objects obtained by forming. Before concluding and pointing out some perspectives to this work, the last section concerns the introduction of optimization techniques, applied to the material characterization by acoustic microscopy. (author)

A Versatile System for the In-Field Non-Destructive Characterization of Radioactive Waste Packages and of Objects in the Defense against Nuclear Threats

International Nuclear Information System (INIS)

Buecherl, T.; Gostomski, Ch.-Lierse-von

2013-06-01

In-filed non-destructive characterization of radioactive waste packages and of objects in the defense of nuclear threats requires purpose-built but similar equipment. Based on commercially available measuring devices like dose-rate and gamma detectors, X-ray and gamma-transmission sources etc. a versatile and mobile mechanical positioning system for these devices is designed, assembled and operated facilitating basic to even complex measuring procedures. Several in-field measuring campaigns resulted in its further optimization. Today an highly mobile and flexible mechanical manipulator system is available supporting nearly all types of required measuring devices thus rising to nearly all occasions. (authors)

Fatigue crack growth monitoring: fracture mechanics and non-destructive testing requirements

International Nuclear Information System (INIS)

Williams, S.; Mudge, P.J.

1982-01-01

If a fatigue crack is found in a component in service, two options exist if plant integrity is to be maintained: first, the plant can be removed from service and repairs effected or replacements fitted; second, the growth of the crack can be monitored non-destructively until it is either considered to be too large to tolerate, in which case it must be repaired, or until a convenient down time when repair can be effected. The second option has obvious benefits for plant operators, but in such a situation it is essential that errors of the non-destructive estimate of defect size, which will undoubtedly exist, and uncertainties in the fatigue crack growth laws in operation must both be allowed for if a safe extension of service life is to be obtained; i.e. without failure by leakage or fast fracture arising from the fatigue crack. This paper analyses the accuracy required of non-destructive crack measurement techniques to permit the safe monitoring of crack growth by periodic inspection. It then demonstrates that it is possible to achieve adequate crack monitoring using conventional ultrasonic techniques. (author)

Non-destructive analysis in a study of the religious art objects

International Nuclear Information System (INIS)

Vornicu, Nicoleta; Bibire, Cristina; Geba, Maria

2009-01-01

The icon Descending of the Saint Spirit from Bucium Church, dating in the year 1814 and was done in tempera on wood technology. The characterization of cultural heritage materials is essential for the comprehension of their degradation mechanisms. The present study aims at identifying the pigments in the various layers, establishing the possible existence of an organic binder and scientifically evaluating the state of preservation. To this end, were used non-destructive methods, as: microscopic (SEM), XRF and spectroscopic (FTIR).

Characterization of legacy low level waste at the Svafo facility using gamma non-destructive assay and X-ray non-destructive examination techniques - 59289

International Nuclear Information System (INIS)

Halliwell, Stephen; Mottershead, Gary; Ekenborg, Fredrik

2012-01-01

Document available in abstract form only. Full text of publication follows: Over 7000 drums containing legacy, low level radioactive waste are stored at four SVAFO facilities on the Studsvik site which is located near Nykoeping, Sweden. The vast majority of the waste drums (>6000) were produced between 1969 and 1979. The remainder were produced from 1980 onwards. Characterization of the waste was achieved using a combination of non-destructive techniques via mobile equipment located in the AU building at the Studsvik site. Each drum was weighed and a dose rate measurement was recorded. Gamma spectroscopy was used to measure and estimate radionuclide content. Real time xray examination was performed to identify such prohibited items as free liquids. (authors)

Non destructive characterization of cracks in concrete by ultrasonic auscultation of civil engineering structures

International Nuclear Information System (INIS)

Quiviger, A.; Payan, C.; Chaix, J.F.; Zardan, J.P.; Garnier, V.; Salin, J.

2011-01-01

Concrete Non Destructive Characterisation is one of the important issues to evaluate the life duration in the present and future civil engineering structures. The damaging modes of the structures often imply the phases of the appearance and after growth of the cracks. We have to detect, identify and characterize them. The characterization result must lead to a diagnosis of the criticality of a crack regarding to the integrity of the structure and its ability to fulfill its function. The Non Destructive Evaluation techniques are numerous but the ultrasonic ones are able to give an answer to both the characterization and the follow-up of the defect on site. Yet if this method is potentially relevant to detect and identify the cracks in the concrete, we have today a certain amount of locks to remove in order to offer robust and reproducible industrial solutions. These locks range from research points like the description of the real propagation of linear or non linear ultrasonic waves in a heterogeneous material, to more industrial concepts such as the development of devices designed to be applied in the concrete control. For this purpose, we present our latest works on this topic. We develop an overview of the problem: first, to extract the most important theoretical solutions to analyse an unstopping and closed crack in concrete with an only one face access. Then we suggest a methodology to apply one of these solutions on site. A first step of this work after having chosen a solution is to check the ability of the technique to detect a crack, and its sensitivity to the length, depth and opening of the crack. We have developed an experimental plan based on theoretical concept to compare the linear and non linear survey on a set of specimens composed of concrete beams cracked to different depths. We describe the devices and give the latest results. The non linear technique is able to extract information on the size of the cracks. It is an important step to progress in

Non destructive characterization of cracks in concrete by ultrasonic auscultation of civil engineering structures

Energy Technology Data Exchange (ETDEWEB)

Quiviger, A.; Payan, C.; Chaix, J.F.; Zardan, J.P.; Garnier, V. [EDF, LCND (France); Salin, J. [EDF Paris (France)

2011-07-01

Concrete Non Destructive Characterisation is one of the important issues to evaluate the life duration in the present and future civil engineering structures. The damaging modes of the structures often imply the phases of the appearance and after growth of the cracks. We have to detect, identify and characterize them. The characterization result must lead to a diagnosis of the criticality of a crack regarding to the integrity of the structure and its ability to fulfill its function. The Non Destructive Evaluation techniques are numerous but the ultrasonic ones are able to give an answer to both the characterization and the follow-up of the defect on site. Yet if this method is potentially relevant to detect and identify the cracks in the concrete, we have today a certain amount of locks to remove in order to offer robust and reproducible industrial solutions. These locks range from research points like the description of the real propagation of linear or non linear ultrasonic waves in a heterogeneous material, to more industrial concepts such as the development of devices designed to be applied in the concrete control. For this purpose, we present our latest works on this topic. We develop an overview of the problem: first, to extract the most important theoretical solutions to analyse an unstopping and closed crack in concrete with an only one face access. Then we suggest a methodology to apply one of these solutions on site. A first step of this work after having chosen a solution is to check the ability of the technique to detect a crack, and its sensitivity to the length, depth and opening of the crack. We have developed an experimental plan based on theoretical concept to compare the linear and non linear survey on a set of specimens composed of concrete beams cracked to different depths. We describe the devices and give the latest results. The non linear technique is able to extract information on the size of the cracks. It is an important step to progress in

Innovation in Non Destructive Testing

NARCIS (Netherlands)

Wassink, C.H.P.

2012-01-01

In many established companies the pace of innovation is low. The Non-Destructive Testing sector is an example of a sector where the pace of innovation is very slow. Non-Destructive Testing (NDT) refers to the set of non-invasive activities used to determine the condition of objects or installations

Static characterization of a soft elastomeric capacitor for non destructive evaluation applications

International Nuclear Information System (INIS)

Saleem, Hussam; Laflamme, Simon; Zhang, Huanhuan; Geiger, Randall; Kessler, Michael; Rajan, Krishna

2014-01-01

A large and flexible strain transducer consisting of a soft elastomeric capacitor (SEC) has been proposed by the authors. Arranged in a network setup, the sensing strategy offers tremendous potential at conducting non-destructive evaluation of large-scale surfaces. In prior work, the authors have demonstrated the performance of the sensor at tracking strain history, localizing cracks, and detecting vibration signatures. In this paper, we characterize the static performance of the proposed SEC. The characterization includes sensitivity of the signal, and temperature and humidity dependences. Tests are conducted on a simply supported aluminum beam subjected to bending as well as on a free standing sensor. The performance of the SEC is compared against off-the-shelf resistance-based strain gauges with resolution of 1 με. A sensitivity of 1190 pF/ε is obtained experimentally, in agreement with theory. Results also show the sensor linearity over the given level of strain, showing the promise of the SEC at monitoring of surface strain

Static characterization of a soft elastomeric capacitor for non destructive evaluation applications

Science.gov (United States)

Saleem, Hussam; Laflamme, Simon; Zhang, Huanhuan; Geiger, Randall; Kessler, Michael; Rajan, Krishna

2014-02-01

A large and flexible strain transducer consisting of a soft elastomeric capacitor (SEC) has been proposed by the authors. Arranged in a network setup, the sensing strategy offers tremendous potential at conducting non-destructive evaluation of large-scale surfaces. In prior work, the authors have demonstrated the performance of the sensor at tracking strain history, localizing cracks, and detecting vibration signatures. In this paper, we characterize the static performance of the proposed SEC. The characterization includes sensitivity of the signal, and temperature and humidity dependences. Tests are conducted on a simply supported aluminum beam subjected to bending as well as on a free standing sensor. The performance of the SEC is compared against off-the-shelf resistance-based strain gauges with resolution of 1 μɛ. A sensitivity of 1190 pF/ɛ is obtained experimentally, in agreement with theory. Results also show the sensor linearity over the given level of strain, showing the promise of the SEC at monitoring of surface strain.

Mapping of mechanical properties of cast iron melts using non-destructive structuroscopy

Directory of Open Access Journals (Sweden)

J. Dočekal

2008-07-01

Full Text Available The contribution is focused on mapping of mechanical properties using methods of non-destructive structuroscopy of cast irons, which are a result of research at TU of Liberec and Institute of Physics of ASCR. Investigated samples become from melts of FOCAM s.r.o Olomouc Foundry shop. It compares data of mechanical properties obtained using ultrasound method with data from magnetic spot method and MAT. These are interpreted by mathematic models applicable in practice. In the following it concerns to derivation of loading tensile curve method, which can be used to obtain yield and fatigue strength limits even for cast irons with flake graphite. In spite of promising results reported by literature the experiments are bothered with error. This method can be applied to structure checking both before casting and at vendor inspection of castings.

Laser active thermography for non-destructive testing

International Nuclear Information System (INIS)

Semerok, A.; Grisolia, C.; Fomichev, S.V.; Thro, P.Y.

2013-01-01

Thermography methods have found their applications in different fields of human activity. The non-destructive feature of these methods along with the additional advantage by automated remote control and tests of nuclear installations without personnel attendance in the contaminated zone are of particular interest. Laser active pyrometry and laser lock-in thermography for in situ non-destructive characterization of micrometric layers on graphite substrates from European tokamaks were under extensive experimental and theoretical studies in CEA (France). The studies were aimed to obtain layer characterization with cross-checking the layer thermal contact coefficients determined by active laser pyrometry and lock-in thermography. The experimental installation comprised a Nd-YAG pulsed repetition rate laser (1 Hz - 10 kHz repetition rate frequency, homogeneous spot) and a home-made pyrometer system based on two pyrometers for the temperature measurements in 500 - 2600 K range. For both methods, the layer characterization was provided by the best fit of the experimental results and simulations. The layer thermal contact coefficients determined by both methods were quite comparable. Though there was no gain in the measurements accuracy, lock-in measurements have proved their advantage as being much more rapid. The obtained experimental and theoretical results are presented. Some practical applications and possible improvements of the methods are discussed. (authors)

Laser active thermography for non-destructive testing

Science.gov (United States)

Semerok, A.; Grisolia, C.; Fomichev, S. V.; Thro, P.-Y.

2013-11-01

Thermography methods have found their applications in different fields of human activity. The non-destructive feature of these methods along with the additional advantage by automated remote control and tests of nuclear installations without personnel attendance in the contaminated zone are of particular interest. Laser active pyrometry and laser lock-in thermography for in situ non-destructive characterization of micrometric layers on graphite substrates from European tokamaks were under extensive experimental and theoretical studies in CEA (France). The studies were aimed to obtain layer characterization with cross-checking the layer thermal contact coefficients determined by active laser pyrometry and lock-in thermography. The experimental installation comprised a Nd-YAG pulsed repetition rate laser (1 Hz - 10 kHz repetition rate frequency, homogeneous spot) and a home-made pyrometer system based on two pyrometers for the temperature measurements in 500 - 2600 K range. For both methods, the layer characterization was provided by the best fit of the experimental results and simulations. The layer thermal contact coefficients determined by both methods were quite comparable. Though there was no gain in the measurements accuracy, lock-in measurements have proved their advantage as being much more rapid. The obtained experimental and theoretical results are presented. Some practical applications and possible improvements of the methods are discussed.

Non-destructive characterization using pulsed fast-thermal neutrons

International Nuclear Information System (INIS)

Womble, P.C.

1995-01-01

Explosives, illicit drugs, and other contraband materials contain various chemical elements in quantities and ratios that differentiate them from each other and from innocuous substances. Furthermore, the major chemical elements in coal can provide information about various parameters of importance to the coal industry. In both examples, the non-destructive identification of chemical elements can be performed using pulsed fast-thermal neutrons that, through nuclear reactions, excite the nuclei of the various elements. This technique is being currently developed for the dismantling of nuclear weapons classified as trainers, and for the on-line coal bulk analysis. (orig.)

Thermal shock resistance of ceramic fibre composites characterized by non-destructive methods

Directory of Open Access Journals (Sweden)

M. Dimitrijević

2008-12-01

Full Text Available Alumina based ceramic fibres and alumina based ceramic were used to produce composite material. Behaviour of composite ceramics after thermal shock treatments was investigated. Thermal shock of the samples was evaluated using water quench test. Surface deterioration level of samples was monitored by image analysis before and after a number of quenching cycles. Ultrasonic measurements were done on samples after quench tests. Dynamic Young modulus of elasticity and strength degradation were calculated using measured values of ultrasonic velocities. Strengths deterioration was calculated using the non-destructive measurements and correlated to degradation of surface area and number of quenches. The addition of small amount of ceramic fibres improves the strengths and diminishes the loss of mechanical properties of samples during thermal shock experiments.

About a sequential method for non destructive testing of structures by mechanical vibrations

International Nuclear Information System (INIS)

Suarez Antola, R.

2001-01-01

The presence and growth of cracks voids or fields of pores under applied forces or environmental actions can produce a meaningful lowering in the proper frequencies of normal modes of mechanical vibration in structures.A quite general expression for the square of modes proper frequency as a functional of displacement field,density field and elastic moduli fields is used as a starting point.The effect of defects on frequency are modeled as equivalent changes in density and elastic moduli fields,introducing the concept of region of influence of each defect.An approximate expression is obtained which relates the relative lowering in the square of modes proper frequency with position,size,shape and orientation of defects in mode displacement field.Some simple examples of structural elements with cracks or fields of pores are considered.the connection with linear elastic fracture mechanics is briefly exemplified.A sequential method is proposed for non-destructive testing of structures using mechanical vibrations combined with properly chosen local nondestructive testing methods

Non-destructive controls

International Nuclear Information System (INIS)

Nouvet, A.

1978-01-01

The non-destructive controls permit, while respecting their integrity, the direct and individual examination of parts or complete objects as they are manufactured, as well as to follow the evolution of their eventual defects while in operation. The choice of control methods depends on the manufacturing process and shapes of parts, on the physical properties of their components as well as the nature, position and size of the defects which are likely to be detected. Whether it is a question of controls by means of ionizing radiation, flux of neutrons, ultrasons, acoustic source, sweating, magnetoscopy. Foucault currents, thermography, detection of leaks or non-destructive metallography, each has a limited field of application such that they are less competitive than complementary [fr

Nonconventional concrete hollow blocks evaluation by destructive and non-destructive testing

Directory of Open Access Journals (Sweden)

M.S. Rodrigues

Full Text Available The aim of this study was to evaluate cementitious matrices properties by partial replacement of Portland cement by silica fume (SF or by rice husk ash (RHA, and their application in nonbearing hollow blocks, tested by destructive and non-destructive methods. The following mixtures were produced: reference (100% of Portland cement and Portland cement replacement (10% by mass with SF or RHA. The non-destructive testing showed that the highest values of UPV were obtained for SF-based blocks and RHA-based blocks. The destructive test showed better results for SF-based blocks, but there was no statistical difference between the RHA-based and control ones.

Effectiveness Analysis of a Non-Destructive Single Event Burnout Test Methodology

CERN Document Server

Oser, P; Spiezia, G; Fadakis, E; Foucard, G; Peronnard, P; Masi, A; Gaillard, R

2014-01-01

It is essential to characterize power MosFETs regarding their tolerance to destructive Single Event Burnouts (SEB). Therefore, several non-destructive test methods have been developed to evaluate the SEB cross-section of power devices. A power MosFET has been evaluated using a test circuit, designed according to standard non-destructive test methods discussed in the literature. Guidelines suggest a prior adaptation of auxiliary components to the device sensitivity before the radiation test. With the first value chosen for the de-coupling capacitor, the external component initiated destructive events and affected the evaluation of the cross-section. As a result, the influence of auxiliary components on the device cross-section was studied. This paper presents the obtained experimental results, supported by SPICE simulations, to evaluate and discuss how the circuit effectiveness depends on the external components.

Qualifying program on Non-Destructive Testing, Visual Inspection of the welding (level 2)

International Nuclear Information System (INIS)

Shafee, M. A.

2011-01-01

Nondestructive testing is a wide group of analysis technique used in science and industry to evaluate the properties of a material, component or system without causing damage. Common Non-Destructive Testing methods include ultrasonic, magnetic-particle, liquid penetrate, radiographic, visual inspection and eddy-current testing. AAEA put the new book of the Non-Destructive Testing publication series that focused on Q ualifying program on Non-Destructive Testing, visual inspection of welding-level 2 . This book was done in accordance with the Arab standard certification of Non-Destructive Testing (ARAB-NDT-CERT-002) which is agreeing with the ISO-9712 (2005) and IAEA- TEC-DOC-487. It includes twenty one chapters dealing with engineering materials used in industry, the mechanical behavior of metals, metal forming equipments, welding, metallurgy, testing of welds, introduction to Non-Destructive Testing, defects in metals, welding defects and discontinuities, introduction to visual inspection theory, properties and tools of visual testing, visual testing, quality control regulations, standards, codes and specifications, procedures of welding inspections, responsibility of welding test inspector, qualification of Non-Destructive Testing inspector and health safety during working.

Mechanisms of CFR composites destruction studying with pulse acoustic microscopy

Science.gov (United States)

Petronyuk, Y. S.; Morokov, E. S.; Levin, V. M.; Ryzhova, T. B.; Chernov, A. V.

2016-05-01

Non-destructive inspection of carbon-fiber-reinforced (CFR) composites applied in aerospace industry attracts a wide attention. In the paper, high frequency focused ultrasound (50-100 MHz) has been applied to study the bulk microstructure of the CFR material and mechanisms of its destruction under the mechanical loading. It has been shown impulse acoustic microscopy provides detecting the areas of adhesion loss at millimeter and micron level. Behavior of the CFR laminate structure fabricated by prepreg or infusion technology has been investigated under the tensile and impact loading.

Characterization of Old Nuclear Waste Packages Coupling Photon Activation Analysis and Complementary Non-Destructive Techniques

International Nuclear Information System (INIS)

Carrel, Frederick; Coulon, Romain; Laine, Frederic; Normand, Stephane; Sari, Adrien; Charbonnier, Bruno; Salmon, Corine

2013-06-01

Radiological characterization of nuclear waste packages is an industrial issue in order to select the best mode of storage. The characterization becomes crucial particularly for waste packages produced at the beginning of the French nuclear industry. For the latter, available information is often incomplete and some key parameters are sometimes missing (content of the package, alpha-activity, fissile mass...) In this case, the use of non-destructive methods, both passive and active, is an appropriate solution to characterize nuclear waste packages and to obtain all the information of interest. In this article, we present the results of a complete characterization carried out on the TE 1060 block, which is a nuclear waste package produced during the 1960's in Saclay. This characterization is part of the DEMSAC (Dismantling of Saclay's facilities) project (ICPE part). It has been carried out in the SAPHIR facility, located in Saclay and housing a linear electron accelerator. This work enables to show the great interest of active methods (photon activation analysis and high-energy imaging) as soon as passive techniques encounter severe limitations. (authors)

Can non-destructive inspection be reliable

International Nuclear Information System (INIS)

Silk, M.G.; Stoneham, A.M.; Temple, J.A.G.

1988-01-01

The paper on inspection is based on the book ''The reliability of non-destructive inspection: assessing the assessment of structures under stress'' by the present authors (published by Adam Hilger 1987). Emphasis is placed on the reliability of inspection and whether cracks in welds or flaws in components can be detected. The need for non-destructive testing and the historical attitudes to non-destructive testing are outlined, along with the case of failure. Factors influencing reliable inspection are discussed, and defect detection trials involving round robin tests are described. The development of reliable inspection techniques and the costs of reliability and unreliability are also examined. (U.K.)

R and D applied to the non-destructive characterization of waste packages for long term storage or deep disposal

Energy Technology Data Exchange (ETDEWEB)

Malvache, P.; Perot, B.; Ma, J.L.; Pettier, J.L. [CEA Cadarache, Dept. d' Etudes des Dechets, DED, 13 - Saint Paul lez Durance (France); Capdevila, J.M.; Huot, N. [CEA Saclay, Dir. du Developpement et de l' Innovation Nucleares DDIN, 91 - Gif Sur Yvette (France); Moulin, V. [CEA Grenoble, Lab. d' Electronique, de Technologie de l' Information LETI, DSYS, 38 (France)

2001-07-01

To ensure the quality and traceability of waste package management in the long term, knowledge on these packages is necessary so as to confirm their compliance to storage or disposal specifications. Research is focused on the management of the knowledge on these packages (fabrication means, materials contained,...) and on the acquisition, through measurement, of their characteristics. Within this context, many studies are underway at the CEA in the field of measurements so as to obtain non- destructive tools to access the parameters which allow the waste packages to be characterized. The two main R and D investigations concern: the nuclear measurement methods for the detection and quantification of radionuclides and of chemical elements considered as important for storage or disposal safety ; the measurement methods for the physical characteristics of the packages by high energy photon imaging, thus allowing pictures of the contents of large, high density and sometimes irradiating packages to be known. During the last five years, the research at the CEA focused on these two areas and resulted in a significant evolution in the non-destructive characterization means for long lived waste packages. (author)

R and D applied to the non-destructive characterization of waste packages for long term storage or deep disposal

International Nuclear Information System (INIS)

Malvache, P.; Perot, B.; Ma, J.L.; Pettier, J.L.; Capdevila, J.M.; Huot, N.; Moulin, V.

2001-01-01

To ensure the quality and traceability of waste package management in the long term, knowledge on these packages is necessary so as to confirm their compliance to storage or disposal specifications. Research is focused on the management of the knowledge on these packages (fabrication means, materials contained,...) and on the acquisition, through measurement, of their characteristics. Within this context, many studies are underway at the CEA in the field of measurements so as to obtain non- destructive tools to access the parameters which allow the waste packages to be characterized. The two main R and D investigations concern: the nuclear measurement methods for the detection and quantification of radionuclides and of chemical elements considered as important for storage or disposal safety ; the measurement methods for the physical characteristics of the packages by high energy photon imaging, thus allowing pictures of the contents of large, high density and sometimes irradiating packages to be known. During the last five years, the research at the CEA focused on these two areas and resulted in a significant evolution in the non-destructive characterization means for long lived waste packages. (author)

Non-Destructive Metallic Materials Testing—Recent Research and Future Perspectives

Directory of Open Access Journals (Sweden)

João Manuel R. S. Tavares

2017-10-01

Full Text Available Non-destructive testing (NDT has become extremely important formicrostructural characterization, mainly by allowing the assessment of metallic material properties in an effective and reasonable manner, in addition to maintaining the integrity of the evaluated metallic samples and applicability in service in many cases [...

Mechanical and Non-Destructive Study of CFRP Adhesive Bonds Subjected to Pre-Bond Thermal Treatment and De-Icing Fluid Contamination

Directory of Open Access Journals (Sweden)

Paweł H. Malinowski

2018-04-01

Full Text Available Composite materials are commonly used in many branches of industry. One of the effective methods to join the carbon fibre reinforced polymer (CFRP parts includes the use of adhesives. There is a search on effective methods for quality assurance of bonded parts. In the research here reported the influence of surface pre-bond modification on the adhesive bonds of CFRP plates has been analyzed. Adherends surface modifications, to include defects affecting the bonding quality, were obtained through surface thermal treatment, surface contamination with de-icing fluid and a combination of both the previously described treatments. Characterization of bonded joints was performed by means of mechanical testing, ultrasounds and electromechanical impedance (EMI measurements. The study here proposed has also the aim to evaluate the ability of different destructive and non-destructive techniques to assess the quality of the bonds. While mechanical tests were strongly affected by the surface modifications, results obtained ultrasound and EMI test have demonstrate only a limited ability of these techniques to differentiate between the different samples. In fact, ultrasounds did not show any changes in the bondline, due to pre-bond modifications. However, this technique was able to detect delamination in CFRP for one of the samples thermally treated at 280 °C. Electromechanical impedance (EMI measurements showed similar behavior as mechanical tests for samples thermally treated at 260 °C and 280 °C, and for the sample whose surface modification was made with a combination of thermally and de-icing fluid treatments.

Non-destructive testing at Chalk River

International Nuclear Information System (INIS)

Hilborn, J.W.

1976-01-01

In 1969 CRNL recognized the need for a strong group skilled in non-destructive test procedures. Within two years a new branch called Quality Control Branch was staffed and working. This branch engages in all aspects of non-destructive testing including development of new techniques, new applications of known technology, and special problems in support of operating reactors. (author)

Non-Destructive Analysis of Degradation Mechanisms in Cycle-Aged Graphite/LiCoO2 Batteries

Directory of Open Access Journals (Sweden)

Liqiang Zhang

2014-09-01

Full Text Available Non-destructive analysis of degradation mechanisms can be very beneficial for the prognostics and health management (PHM study of lithium-ion batteries. In this paper, a type of graphite/LiCoO2 battery was cycle aged at high ambient temperature, then 25 parameters of the multi-physics model were identified. Nine key parameters degraded with the cycle life, and they were treated as indicators of battery degradation. Accordingly, the degradation mechanism was discussed by using the multi-physics model and key parameters, and the reasons for capacity fade and the internal resistance increase were analyzed in detail. All evidence indicates that the formation reaction of the solid electrolyte interface (SEI film is the main cause of battery degradation at high ambient temperature.

Recent Trends in Electromagnetic Non-Destructive Sensing

Directory of Open Access Journals (Sweden)

Klara Capova

2008-01-01

Full Text Available The paper deals with material electromagnetic non-destructive testing (eNDT with emphasize on eddy current testing (ECT. Various modifications of ECT sensing are compared and discussed from the desired detected signal characteristics point of view. Except of the optimization of usual probe coils arrangements for the concrete applications, the new magnetic sensors as giant magneto-resistance (GMR and spin dependent tunneling (SDT are presented. The advanced ECT sensors are characterized by their sensitivity, frequency range and sensor dimensions

Non-destructive and destructive examination of the retired North Anna 2 Reactor Pressure Vessel Head

International Nuclear Information System (INIS)

Ahluwalia, Kawaljit; Barnes, Robert; Rao, Gutti; Cattant, Francois; Peat, Noel

2006-09-01

Stress corrosion cracking of Alloy 600 and nickel-based weld materials has been the single biggest challenge facing the PWR industry. A fundamental and thorough knowledge was needed to properly explain this phenomenon and develop appropriate mitigation strategies. Non Destructive Examination (NDE) of the North Anna Unit 2 Reactor Vessel Head (RVH) during the 2002 fall outage identified widespread crack indications in the Alloy 600 CRDM penetrations and associated Alloy 182 and 82 J-groove attachment welds. When the Utility decided to replace the RVH, a rare opportunity was provided to the industry to undertake in-depth studies of representative defective CRDM penetrations from a retired RVH. Accordingly, the Materials Reliability Program, undertook a two-phase program on the retired North Anna 2 Alloy 600 RVH. The first phase involved selection and removal of six penetrations from the RVH and penetration decontamination, replication and laboratory NDE. The second phase consisted of a detailed destructive examination of penetration number 54. This paper provides a summary of work undertaken during this program. Criteria for selection of penetrations for removal and procedures used in removal of the penetrations are described. Extreme care was undertaken in decontamination of the penetrations to facilitate laboratory NDE. Penetration number 54 was then subjected to destructive examination to establish a correlation between NDE findings (from both field and laboratory inspections) and actual flaws. Additional objectives of the destructive examination included mechanistic assessment of defect formation and investigation of the annulus environment and wastage characterization. Data obtained from these studies is invaluable in validating safety assessment statements by developing the correlation between field NDE and actual defects. In addition, information gathered from non-destructive and destructive examinations is used to assess accuracy of the NDE techniques

Attributes identification of nuclear material by non-destructive radiation measurement methods

International Nuclear Information System (INIS)

Gan Lin

2002-01-01

Full text: The nuclear materials should be controlled under the regulation of National Safeguard System. The non-destructive analysis method, which is simple and quick, provide a effective process in determining the nuclear materials, nuclear scraps and wastes. The method play a very important role in the fields of nuclear material control and physical protection against the illegal removal and smuggling of nuclear material. The application of non-destructive analysis in attributes identification of nuclear material is briefly described in this paper. The attributes determined by radioactive detection technique are useful tolls to identify the characterization of special nuclear material (isotopic composition, enrichment etc.). (author)

Contribution of expert systems to data processing in non-destructive control

International Nuclear Information System (INIS)

Augendre, H.; Perron, M.C.

1990-01-01

The increase of non-destructive control in industrial applications requires the development of new data processing methods. The expert system approach is able to provide signal modelling means which are closer to the human behaviour. Such methods used in more traditional programs lead to substantial improvements. These investigations come within our design to apply sophisticated methods to industrial non-destructive control. For defect characterization purposes in ultrasonic control, various supervised learning methods have been investigated in an experimental study. The traditional approach is concerned with statistics based methods, whereas the second one lies in learning logical decision rules valid within a numerical description space [fr

Non-destructive testing. V. 2

International Nuclear Information System (INIS)

Farley, J.M.; Nichols, R.W.

1988-01-01

The book entitled 'Non-destructive Testing' Volume 2, contains the proceedings of the fourth European Conference, organized by the British Institute of Non-Destructive Testing and held in London, September 1987. The volume contains seven chapters which examine the reliability of NDT, the economics of NDT and the use of NDT in:- civil engineering; oil, gas, coal and petrochemical industries; iron and steel industries; aerospace industry; and the nuclear and electricity supply industries. The seven chapters contain 78 papers, of which 19 are selected for INIS and indexed separately. (U.K.)

PANDA-A novel instrument for non-destructive sample analysis

International Nuclear Information System (INIS)

Turunen, Jani; Peraejaervi, Kari; Poellaenen, Roy; Toivonen, Harri

2010-01-01

An instrument known as PANDA (Particles And Non-Destructive Analysis) for non-destructive sample analysis has been designed and built at the Finnish Radiation and Nuclear Safety Authority (STUK). In PANDA the measurement techniques and instruments designed for the basic research are applied to the analysis of environmental samples. PANDA has two vacuum chambers, one for loading samples and the other for measurements. In the measurement chamber there are two individual measurement positions. Currently the first one hosts an HPGe gamma detector and a position-sensitive alpha detector. The second measurement position is intended for precise characterization of found particles. PANDA's data are recorded in event mode and events are timestamped. In the present article the technical design of PANDA is presented in detail. In addition, its performance using depleted uranium particles and an air filter is demonstrated.

The complementary roles of fracture mechanics and non-destructive examination in the safety assessment of components

International Nuclear Information System (INIS)

1988-01-01

This document presents the various speeches of the workshop of the Committee on Safety of Nuclear Installations (CSNI) that took place in Wuerenligen, Switzerland, in October 1988. The speeches deal with the roles of Non-Destructive Examination (NDE) and Fracture Mechanics (FM) in the safety assessment of reactor components, such as pressure vessels. Some calibration standards and reference values of defects are presented, and several NDE and FM methods for the assessment of components are described. Separate abstracts were prepared for all the papers in this volume. (TEC)

The complementary roles of fracture mechanics and non-destructive examination in the safety assessment of components

Energy Technology Data Exchange (ETDEWEB)

NONE

1988-12-31

This document presents the various speeches of the workshop of the Committee on Safety of Nuclear Installations (CSNI) that took place in Wuerenligen, Switzerland, in October 1988. The speeches deal with the roles of Non-Destructive Examination (NDE) and Fracture Mechanics (FM) in the safety assessment of reactor components, such as pressure vessels. Some calibration standards and reference values of defects are presented, and several NDE and FM methods for the assessment of components are described. Separate abstracts were prepared for all the papers in this volume. (TEC).

Current developments in mechanized non-destructive testing in nuclear power plants; Aktuelle Entwicklungen bei mechanisierten, zerstoerungsfreien Pruefungen in Kernkraftwerken

Energy Technology Data Exchange (ETDEWEB)

Zeilinger, R. [intelligeNDT System und Services GmbH und Co. KG, Erlangen (Germany)

2008-01-15

Nuclear power plants require frequent in-service activities to be carried out conscientiously in areas potentially hazardous to human operators (because of the associated radiation exposure), such as non-destructive testing of pressurized components of the steam system. Locations to be inspected in this way include the reactor pressure vessel, core internals, steam generators, pressurizers, and pipes. The codes to be used as a basis of these inspections demand high absolute positioning and repeating accuracy. These requirements can be met by mechanized test procedures. Accordingly, many new applications of, mostly mobile, robots have been developed over the past few years. The innovative control and sensor systems for stationary and mobile robots now on the market offer a potential for economic application in a large number of new areas in inspection, maintenance and service in nuclear power plants. More progress in this area is expected for the near future. Areva NP founded the new NDT Center, NETEC (Non-destructive Examination Technical Center), as a global technical center for non-destructive materials testing. NETEC is to advance research and development of all basic NDT technologies, robotics included. For many years, intelligeNDT has offered solutions and products for a variety of inspection and testing purposes and locations in nuclear power plants and is involved in continuous further development of the experience collected in nuclear power plants on the spot. (orig.)

Non-destructive spatial characterization of buried interfaces in multilayer stacks via two color picosecond acoustics

Science.gov (United States)

Faria, Jorge C. D.; Garnier, Philippe; Devos, Arnaud

2017-12-01

We demonstrate the ability to construct wide-area spatial mappings of buried interfaces in thin film stacks in a non-destructive manner using two color picosecond acoustics. Along with the extraction of layer thicknesses and sound velocities from acoustic signals, the morphological information presented is a powerful demonstration of phonon imaging as a metrological tool. For a series of heterogeneous (polymer, metal, and semiconductor) thin film stacks that have been treated with a chemical procedure known to alter layer properties, the spatial mappings reveal changes to interior thicknesses and chemically modified surface features without the need to remove uppermost layers. These results compare well to atomic force microscopy scans showing that the technique provides a significant advantage to current characterization methods for industrially important device stacks.

Non-destructive characterization of oriental porcelain glazes and blue underglaze pigments using μ-EDXRF, μ-Raman and VP-SEM

Energy Technology Data Exchange (ETDEWEB)

Coutinho, M.L. [Universidade Nova de Lisboa, REQUIMTE-CQFB, Faculdade de Ciencias e Tecnologia, Caparica (Portugal); Universidade Nova de Lisboa, Departamento de Conservacao e Restauro, Faculdade de Ciencias e Tecnologia, Caparica (Portugal); Muralha, V.S.F. [Universidade Nova de Lisboa, Research Unit VICARTE, Vidro e Ceramica para as Artes, Faculdade de Ciencias e Tecnologia, Caparica (Portugal); Mirao, J. [Universidade de Evora, Laboratorio HERCULES, Evora (Portugal); Veiga, J.P. [Universidade Nova de Lisboa, CENIMAT/I3N, Departamento de Ciencia dos Materiais, Faculdade de Ciencias e Tecnologia, Caparica (Portugal)

2014-03-15

The study of ancient materials with recognized cultural and economic value is a challenge to scientists and conservators, since it is usually necessary an approach through non-destructive techniques. Difficulties in establishing a correct analytical strategy are often significantly increased by the lack of knowledge on manufacture technologies and raw materials employed combined with the diversity of decay processes that may have acted during the lifetime of the cultural artefacts. A non-destructive characterization was performed on the glaze and underglaze pigments from a group of Chinese porcelain shards dated from the late Ming Dynasty (1368-1644) excavated at the Monastery of Santa Clara-a-Velha in Coimbra (Portugal). Chemical analysis was performed using micro-energy dispersive X-ray fluorescence spectrometry (μ-EDXRF). Mineralogical characterization was achieved by Raman microscopy (μ-Raman) and observation of small-surface crystallization dark spots with a metallic lustre in areas with high pigment concentration was done by variable pressure scanning electron microscopy (VP-SEM). Cobalt aluminate was identified as the blue underglaze pigment and a comparison of blue and dark blue pigments was performed by the ratio of Co, Mn, and Fe oxides, indicating a compositional difference between the two blue tonalities. Manganese oxide compounds were also identified as colouring agents in dark blue areas and surface migration of manganese compounds was verified. (orig.)

Non-destructive characterization of oriental porcelain glazes and blue underglaze pigments using μ-EDXRF, μ-Raman and VP-SEM

International Nuclear Information System (INIS)

Coutinho, M.L.; Muralha, V.S.F.; Mirao, J.; Veiga, J.P.

2014-01-01

The study of ancient materials with recognized cultural and economic value is a challenge to scientists and conservators, since it is usually necessary an approach through non-destructive techniques. Difficulties in establishing a correct analytical strategy are often significantly increased by the lack of knowledge on manufacture technologies and raw materials employed combined with the diversity of decay processes that may have acted during the lifetime of the cultural artefacts. A non-destructive characterization was performed on the glaze and underglaze pigments from a group of Chinese porcelain shards dated from the late Ming Dynasty (1368-1644) excavated at the Monastery of Santa Clara-a-Velha in Coimbra (Portugal). Chemical analysis was performed using micro-energy dispersive X-ray fluorescence spectrometry (μ-EDXRF). Mineralogical characterization was achieved by Raman microscopy (μ-Raman) and observation of small-surface crystallization dark spots with a metallic lustre in areas with high pigment concentration was done by variable pressure scanning electron microscopy (VP-SEM). Cobalt aluminate was identified as the blue underglaze pigment and a comparison of blue and dark blue pigments was performed by the ratio of Co, Mn, and Fe oxides, indicating a compositional difference between the two blue tonalities. Manganese oxide compounds were also identified as colouring agents in dark blue areas and surface migration of manganese compounds was verified. (orig.)

Non-destructive characterization of oriental porcelain glazes and blue underglaze pigments using μ-EDXRF, μ-Raman and VP-SEM

Science.gov (United States)

Coutinho, M. L.; Muralha, V. S. F.; Mirão, J.; Veiga, J. P.

2014-03-01

The study of ancient materials with recognized cultural and economic value is a challenge to scientists and conservators, since it is usually necessary an approach through non-destructive techniques. Difficulties in establishing a correct analytical strategy are often significantly increased by the lack of knowledge on manufacture technologies and raw materials employed combined with the diversity of decay processes that may have acted during the lifetime of the cultural artefacts. A non-destructive characterization was performed on the glaze and underglaze pigments from a group of Chinese porcelain shards dated from the late Ming Dynasty (1368-1644) excavated at the Monastery of Santa Clara- a- Velha in Coimbra (Portugal). Chemical analysis was performed using micro-energy dispersive X-ray fluorescence spectrometry (μ-EDXRF). Mineralogical characterization was achieved by Raman microscopy (μ-Raman) and observation of small-surface crystallization dark spots with a metallic lustre in areas with high pigment concentration was done by variable pressure scanning electron microscopy (VP-SEM). Cobalt aluminate was identified as the blue underglaze pigment and a comparison of blue and dark blue pigments was performed by the ratio of Co, Mn, and Fe oxides, indicating a compositional difference between the two blue tonalities. Manganese oxide compounds were also identified as colouring agents in dark blue areas and surface migration of manganese compounds was verified.

Characterization of the Teotihuacan mural painting: application of the external particle beam as non destructive technique

International Nuclear Information System (INIS)

Martinez, C.; Manzanilla, L.; Ruvalcaba, J.L.; Ontalba, M.A.

2005-01-01

The characterization of technical indicators contained in the painting mural should follow a minim methodology from their discovery in the archaeological excavations until their analysis in the laboratory, with the purpose of rescuing diagnostic elements that mark the stages of socio cultural development in the towns. With this spirit it was carried out the present study analyzing some fragments of the Teotihuacan mural painting. The analysis consisted on applying some of the analytical techniques with particle beams used for archaeometry like the Proton induced X-ray emission (PIXE) and the particle elastic backscattering (RBS), due to it is treated of complementary techniques, very sensitive, of multielemental character, but mainly because its are non destructive analytical techniques. (Author)

Non-destructive control of castings

International Nuclear Information System (INIS)

Boutault, J.; Mascre, C.

1978-01-01

The object of non-destructive control in foundries is to verify the metal structure, the absence of unacceptable discontinuity, total tightness, etc. This leads to a range of very varied controls according to the importance of the series, the quality level required by the specifications, the nature of the alloy. The originality of the solutions which are imperative for castings is shown through examples: casting of high quality complex forms in short series; very thick unit parts; very large series of parts requiring on efficient automation of non-destructive control. Lastly the publishing of testing methods and interpretating rules, which are the base of a friendly understanding between constructors and founders are recalled [fr

Non-destructive test of lock actuator component using neutron radiography technique

International Nuclear Information System (INIS)

Juliyanti; Setiawan; Sutiarso

2012-01-01

Non-destructive test of lock actuator using neutron radiography technique has been done. The lock actuator is a mechanical system which is controlled by central lock module consisting of electronic circuit which drives the lock actuator works accordingly to open and lock the vehicle door. The non-destructive test using neutron radiography is carried out to identify the type of defect is presence by comparing between the broken and the brand new one. The method used to test the lock actuator component is film method (direct method). The result show that the radiography procedure has complied with the ASTM standard for neutron radiography with background density of 2.2, 7 lines and 3 holes was seen in the sensitivity indicator (SI) and the quite good image quality was obtained. In the brand new actuator is seen that isolator part which separated the coils has melted. By this non-destructive test using neutron radiography technique is able to detect in early stage the type of component's defect inside the lock actuator without to dismantle it. (author)

Non-destructive testing of electronic parts

International Nuclear Information System (INIS)

Widenhorn, G.

1980-01-01

The requirements on quality, safety, faultlessness and reliability of electric components increase because of the high complexity of the appliances in which they are used. By means of examples a survey is given on the common non-destructive testing methods, testing operation and evaluation of test results on electric components which must meet in their application high requirements on quality and reliability. Defective components, especially those with hidden failures are sorted out by non-destructive testing and the failure frequency of the appliances and plants in testing and operation is greatly reduced. (orig.) [de

European Non Destructive Examination Forum (ENDEF)

International Nuclear Information System (INIS)

Deffrennes, M.; Engl, G.; Estorff, U. von

1998-01-01

Non destructive examination (NDE) during fabrication, Pre-service inspection (PSI) and In service inspection (ISI) are considered key issues for the safe use of nuclear energy. They are important elements of plant lifetime management which is a critical item in decision making on nuclear policies. The European non destructive examination forum (ENDEF) founded by European Commission provides a platform for open discussion between representatives of the European industries with the purpose to establish cooperation between EU, Central and Eastern European Countries and New Independent States in the field of NDE and ISI

Non-Destructive Testing for Control of Radioactive Waste Package

Science.gov (United States)

Plumeri, S.; Carrel, F.

2015-10-01

Characterization and control of radioactive waste packages are important issues in the management of a radioactive waste repository. Therefore, Andra performs quality control inspection on radwaste package before disposal to ensure the compliance of the radwast characteristics with Andra waste disposal specifications and to check the consistency between Andra measurements results and producer declared properties. Objectives of this quality control are: assessment and improvement of producer radwaste packages quality mastery, guarantee of the radwaste disposal safety, maintain of the public confidence. To control radiological characteristics of radwaste package, non-destructive passive methods (gamma spectrometry and neutrons counting) are commonly used. These passive methods may not be sufficient, for instance to control the mass of fissile material contained inside radwaste package. This is particularly true for large concrete hull of heterogeneous radwaste containing several actinides mixed with fission products like 137Cs. Non-destructive active methods, like measurement of photofission delayed neutrons, allow to quantify the global mass of actinides and is a promising method to quantify mass of fissile material. Andra has performed different non-destructive measurements on concrete intermediate-level short lived nuclear waste (ILW-SL) package to control its nuclear material content. These tests have allowed Andra to have a first evaluation of the performance of photofission delayed neutron measurement and to identify development needed to have a reliable method, especially for fissile material mass control in intermediate-level long lived waste package.

Non-destructive control at the Kozloduy NPP; Nerazrushayushchij kontrol` v AEhS `Kozloduy`

Energy Technology Data Exchange (ETDEWEB)

Mikhovsky, M [Institute of Mechanics, Bulgarian Academy of Sciences, Sofia (Bulgaria); Skordev, A [SIME-CONTROL, Sofia (Bulgaria); Nichev, V; Tsokov, P; Popova, N [Kombinat Atomna Energetika, Kozloduj (Bulgaria)

1996-12-31

A program for technical diagnostics using non-destructive methods is being carried out at the Kozloduy NPP. The main target is to test mechanical equipment integrity (metal control, mechanical stress control, etc.) as well as electrical equipment. Computer methods and simulation are widely used in program implementation. Non-destructive testing is based on methods involving optical, radiation, ultrasonic and magnetic processes. Control procedures are standardised in special technological documents and one of them is described as an example. It refers to ultrasonic control of the austenitic steel welds of the WWER-440 piping system (DU-500). Graphic representing the microstructure of the welds, the distribution of surface ultrasonic wave and the longitudinal and vertically polarised perpendicular waves are presented. 6 refs. 8 figs.

Experimental investigations of nonlinearities and destruction mechanisms of an experimental phospholipid-based ultrasound contrast agent.

Science.gov (United States)

Casciaro, Sergio; Palmizio Errico, Rosa; Errico, Rosa Palmizio; Conversano, Francesco; Demitri, Christian; Distante, Alessandro

2007-02-01

We sought to characterize the acoustical behavior of the experimental ultrasound contrast agent BR14 by determining the acoustic pressure threshold above which nonlinear oscillation becomes significant and investigating microbubble destruction mechanisms. We used a custom-designed in vitro setup to conduct broadband attenuation measurements at 3.5 MHz varying acoustic pressure (range, 50-190 kPa). We also performed granulometric analyses on contrast agent solutions to accurately measure microbubble size distribution and to evaluate insonification effects. Attenuation did not depend on acoustic pressure less than 100 kPa, indicating this pressure as the threshold for the appearance of microbubble nonlinear behavior. At the lowest excitation amplitude, attenuation increased during insonification, while, at higher excitation levels, the attenuation decreased over time, indicating microbubble destruction. The destruction rate changed with pressure amplitude suggesting different destruction mechanisms, as it was confirmed by granulometric analysis. Microbubbles showed a linear behavior until 100 kPa, whereas beyond this value significant nonlinearities occurred. Observed destruction phenomena seem to be mainly due to gas diffusion and bubble fragmentation mechanisms.

Analysis of Radiation Accident of Non-destructive Inspection and Rational Preparing Bills

International Nuclear Information System (INIS)

Bae, Junwoo; Yoo, Donghan; Kim, Hee Reyoung

2013-01-01

After 2006, according to enactment of Non-destructive Inspection Promotion Act, the number of non-destructive inspection companies and corresponding accident is increased sharply. In this research, it includes characteristic analysis of field of the non-destructive inspection. And from the result of analysis, the purpose of this research is discovering reason for 'Why there is higher accident ratio in non-destructive inspection field, relatively' and preparing effective bill for reducing radiation accidents. The number of worker for non-destructive inspect is increased steadily and non-destructive inspect worker take highest dose. Corresponding to these, it must be needed to prepare bills to protect non-destructive inspect workers. By analysis of accident case, there are many case of carelessness that tools are too heavy to carry it everywhere workers go. And there are some cases caused by deficiency of education that less understanding of radiation and poor operation by less understanding of structure of tools. Also, there is no data specialized to non-destructive inspect field. So, it has to take information from statistical data. Because of this, it is hard to analyze nondestructive inspect field accurately. So, it is required to; preparing rational bills to protect non-destructive inspect workers nondestructive inspect instrument lightening and easy manual which can understandable for low education background people accurate survey data from real worker. To accomplish these, we needs to do; analyze and comprehend the present law about non-destructive inspect worker understand non-destructive inspect instruments accurately and conduct research for developing material developing rational survey to measuring real condition for non-destructive inspect workers

Development of hotcell non-destructive examination techniques

Energy Technology Data Exchange (ETDEWEB)

Kim, Young Uhn; Yu, S. C.; Kang, B. S.; Byun, K. S. [Chungbuk National University, Chungju (Korea)

2002-01-01

The purpose of this project is to establish non-destructive examination techniques which needs to determine the status of spent nuclear fuel and/or bundles. Through the project, we will establish an image reconstruction tomography which is a kind of non-destructive techniques in Hotcell. The tomography technique can be used to identify the 2-dimensional density distribution of fission products in the spent fuel rods and/or bundles. And form results of the measurement and analysis of magnetic properties of neutron irradiated material in the press vessel and reactor, we will develop some techniques to test its hardness and defects. In 2001, the first year, we have established mathematical background and necessary data and informations to develop the techniques. We will try to find some experimental results that are necessary in developing the Hotcell non-destructive examination techniques in the coming year. 14 refs., 65 figs., 5 tabs. (Author)

Destructive electronics from electrochemical-mechanically triggered chemical dissolution

International Nuclear Information System (INIS)

Sim, Kyoseung; Wang, Xu; Yu, Cunjiang; Li, Yuhang; Linghu, Changhong; Song, Jizhou; Gao, Yang

2017-01-01

The considerable need to enhance data and hardware security suggest one possible future for electronics where it is possible to destroy them and even make them disappear physically. This paper reports a type of destructive electronics which features fast transience from chemical dissolution on-demand triggered in an electrochemical-mechanical manner. The detailed materials, mechanics, and device construction of the destructive electronics are presented. Experiment and analysis of the triggered releasing and transience study of electronic materials, resistors and metal-oxide-semiconductor field effect transistors illustrate the key aspects of the destructive electronics. The reported destructive electronics is useful in a wide range of areas from security and defense, to medical applications (paper)

Advanced non-destructive methods for an efficient service performance

International Nuclear Information System (INIS)

Rauschenbach, H.; Clossen-von Lanken Schulz, M.; Oberlin, R.

2015-01-01

Due to the power generation industry's desire to decrease outage time and extend inspection intervals for highly stressed turbine parts, advanced and reliable Non-destructive methods were developed by Siemens Non-destructive laboratory. Effective outage performance requires the optimized planning of all outage activities as well as modern Non-destructive examination methods, in order to examine the highly stressed components (turbine rotor, casings, valves, generator rotor) reliably and in short periods of access. This paper describes the experience of Siemens Energy with an ultrasonic Phased Array inspection technique for the inspection of radial entry pinned turbine blade roots. The developed inspection technique allows the ultrasonic inspection of steam turbine blades without blade removal. Furthermore advanced Non-destructive examination methods for joint bolts will be described, which offer a significant reduction of outage duration in comparison to conventional inspection techniques. (authors)

Quantitative impact characterization of aeronautical CFRP materials with non-destructive testing methods

Energy Technology Data Exchange (ETDEWEB)

Kiefel, Denis, E-mail: Denis.Kiefel@airbus.com, E-mail: Rainer.Stoessel@airbus.com; Stoessel, Rainer, E-mail: Denis.Kiefel@airbus.com, E-mail: Rainer.Stoessel@airbus.com [Airbus Group Innovations, Munich (Germany); Grosse, Christian, E-mail: Grosse@tum.de [Technical University Munich (Germany)

2015-03-31

In recent years, an increasing number of safety-relevant structures are designed and manufactured from carbon fiber reinforced polymers (CFRP) in order to reduce weight of airplanes by taking the advantage of their specific strength into account. Non-destructive testing (NDT) methods for quantitative defect analysis of damages are liquid- or air-coupled ultrasonic testing (UT), phased array ultrasonic techniques, and active thermography (IR). The advantage of these testing methods is the applicability on large areas. However, their quantitative information is often limited on impact localization and size. In addition to these techniques, Airbus Group Innovations operates a micro x-ray computed tomography (μ-XCT) system, which was developed for CFRP characterization. It is an open system which allows different kinds of acquisition, reconstruction, and data evaluation. One main advantage of this μ-XCT system is its high resolution with 3-dimensional analysis and visualization opportunities, which enables to gain important quantitative information for composite part design and stress analysis. Within this study, different NDT methods will be compared at CFRP samples with specified artificial impact damages. The results can be used to select the most suitable NDT-method for specific application cases. Furthermore, novel evaluation and visualization methods for impact analyzes are developed and will be presented.

Quantitative impact characterization of aeronautical CFRP materials with non-destructive testing methods

International Nuclear Information System (INIS)

Kiefel, Denis; Stoessel, Rainer; Grosse, Christian

2015-01-01

In recent years, an increasing number of safety-relevant structures are designed and manufactured from carbon fiber reinforced polymers (CFRP) in order to reduce weight of airplanes by taking the advantage of their specific strength into account. Non-destructive testing (NDT) methods for quantitative defect analysis of damages are liquid- or air-coupled ultrasonic testing (UT), phased array ultrasonic techniques, and active thermography (IR). The advantage of these testing methods is the applicability on large areas. However, their quantitative information is often limited on impact localization and size. In addition to these techniques, Airbus Group Innovations operates a micro x-ray computed tomography (μ-XCT) system, which was developed for CFRP characterization. It is an open system which allows different kinds of acquisition, reconstruction, and data evaluation. One main advantage of this μ-XCT system is its high resolution with 3-dimensional analysis and visualization opportunities, which enables to gain important quantitative information for composite part design and stress analysis. Within this study, different NDT methods will be compared at CFRP samples with specified artificial impact damages. The results can be used to select the most suitable NDT-method for specific application cases. Furthermore, novel evaluation and visualization methods for impact analyzes are developed and will be presented

Application of digital radiography for the non-destructive characterization of radioactive waste packages

International Nuclear Information System (INIS)

Lierse, C.; Goebel, H.; Kaciniel, E.; Buecherl, T.; Krebs, K.

1995-01-01

Digital radiography (DR) using gamma-rays is a powerful tool for the non-destructive determination of various parameters which are relevant within the quality control procedure of radioactive waste packages prior to an interim storage or a final disposal. DR provides information about the waste form and the extent of filling in a typical container. It can identify internal structures and defects, gives their geometric dimensions and helps to detect non-declared inner containers, shielding materials etc. From a digital radiographic image the waste matrix homogeneity may be determined and mean attenuation coefficients as well as density values for selected regions of interest can be calculated. This data provides the basis for an appropriate attenuation correction of gamma emission measurements (gamma scanning) and makes a reliable quantification of gamma emitters in waste containers possible. Information from DR measurements are also used for the selection of interesting height positions of the object which are subsequently inspected in more detail by other non-destructive methods, e. g. by transmission computerized tomography (TCT). The present paper gives important technical specifications of an integrated tomography system (ITS) which is used to perform digital radiography as well as transmission/emission computerized tomography (TCT/ECT) on radioactive waste packages. It describes the DR mode and some of its main applications and shows typical examples of radiographs of real radioactive waste drums

Comparative study of destructive and non-destructive methods in the activation analysis of rocks

International Nuclear Information System (INIS)

Vasconcellos, M.B.A.

1978-01-01

A comparative study between non-destructive thermal neutron activation analysis and activation analysis with radiochemical group separation is made Both methods are applied to the determination of trace elements minor and major elements in rocks. The treatment of the rocks, with special reference to the problems related to grinding and contamination by foreign elements is described. The choice of standards for multielement trace activation analysis is discussed. Two types of computer programs for the evalution of data obtained through Ge-li detector counting are used. All the phases of the destructive and non destructive analysis are described. In the destructive analysis, an adaptation of the group separation scheme developed by Morrison et al for the activation analysis of geological samples is made. The changes introduced make the radiochemical separation simpler and more rapid. Both destructive and non destructive methods are tested by means of the analysis of the United States Geological Survey standard rock AGV-1, which has been analysed by many authors. The same procedure is then applied to some alcaline rocks taken from the apatite mine of Jacupiranga, in the State of Sao Paulo, Brazil. The knowledge of the trace element concentration in these rocks is important for geochemical studies. A detailed study of the possible interferences encountered in the neutron activation analysis of these rocks is made, considering the interferences due to major activities, and to the proximity of the several gamma ray energies of the radioisotopes produced. Finally, the comparative study between the two methods is presented, using statistical tests for the quantitative evalution of results. (Author) [pt

Modelling, simulation and visualisation for electromagnetic non-destructive testing

International Nuclear Information System (INIS)

Ilham Mukriz Zainal Abidin; Abdul Razak Hamzah

2010-01-01

This paper reviews the state-of-the art and the recent development of modelling, simulation and visualization for eddy current Non-Destructive Testing (NDT) technique. Simulation and visualization has aid in the design and development of electromagnetic sensors and imaging techniques and systems for Electromagnetic Non-Destructive Testing (ENDT); feature extraction and inverse problems for Quantitative Non-Destructive Testing (QNDT). After reviewing the state-of-the art of electromagnetic modelling and simulation, case studies of Research and Development in eddy current NDT technique via magnetic field mapping and thermography for eddy current distribution are discussed. (author)

Non-destructive Faraday imaging of dynamically controlled ultracold atoms

Science.gov (United States)

Gajdacz, Miroslav; Pedersen, Poul; Mørch, Troels; Hilliard, Andrew; Arlt, Jan; Sherson, Jacob

2013-05-01

We investigate non-destructive measurements of ultra-cold atomic clouds based on dark field imaging of spatially resolved Faraday rotation. In particular, we pursue applications to dynamically controlled ultracold atoms. The dependence of the Faraday signal on laser detuning, atomic density and temperature is characterized in a detailed comparison with theory. In particular the destructivity per measurement is extremely low and we illustrate this by imaging the same cloud up to 2000 times. The technique is applied to avoid the effect of shot-to-shot fluctuations in atom number calibration. Adding dynamic changes to system parameters, we demonstrate single-run vector magnetic field imaging and single-run spatial imaging of the system's dynamic behavior. The method can be implemented particularly easily in standard imaging systems by the insertion of an extra polarizing beam splitter. These results are steps towards quantum state engineering using feedback control of ultracold atoms.

Addition of magnetic markers for non-destructive evaluation of polymer composites

Directory of Open Access Journals (Sweden)

Ana Paula Pereira Fulco

2011-12-01

Full Text Available Polymer composite pipes are an appealing option as a substitute for conventional steel pipes, particularly due to their inherent corrosion resistance. However, the composite pipes currently used do not allow non-destructive evaluation (NDE using instrumented devices which operate with magnetic sensors. The present work aims at the development of polymer composites with the addition magnetic markers to allow the application non-destructive evaluation techniques which use magnetic sensors. Glass-polyester composite flat, circular plates were fabricated with the addition of ferrite particles (barium ferrite and strontium ferrite and four types of notches were introduced on the plates' surfaces. The influence of these notches on the measured magnetic properties of each material was measured. X-ray diffraction (XRD, X-ray fluorescence (XRF and Brunauer, Emmett, and Teller (BET nitrogen adsorption were used for the characterization of the ferrite particles. Particle dispersion in the polymer matrix was analyzed by scanning electron microscopy (SEM. According to the results, a particular variation in magnetic field was detected over the region surrounding each type of notch. The results suggest that the proposed technique has great potential for damage detection in polymer composites using magnetic sensors and thus constitute a valuable contribution which may ultimately lead to the development of non-destructive evaluation techniques for assessing the structural integrity polymer composite pipes.

Infrared image processing devoted to thermal non-contact characterization-Applications to Non-Destructive Evaluation, Microfluidics and 2D source term distribution for multispectral tomography

International Nuclear Information System (INIS)

Batsale, Jean-Christophe; Pradere, Christophe

2015-01-01

The cost of IR cameras is more and more decreasing. Beyond the preliminary calibration step and the global instrumentation, the infrared image processing is then one of the key step for achieving in very broad domains.Generally the IR images are coming from the transient temperature field related to the emission of a black surface in response to an external or internal heating (active IR thermography). The first applications were devoted to the so called thermal Non-Destructive Evaluation methods by considering a thin sample and 1D transient heat diffusion through the sample (transverse diffusion). With simplified assumptions related to the transverse diffusion, the in-plane diffusion and transport phenomena can be also considered.A general equation can be applied in order to balance the heat transfer at the pixel scale or between groups of pixels in order to estimate several fields of thermophysical properties (heterogeneous field of in-plane diffusivity, flow distributions, source terms).There is a lot of possible strategies to process the space and time distributed big amount of data (previous integral transformation of the images, compression, elimination of the non useful areas...), generally based on the necessity to analyse the derivative versus space and time of the temperature field. Several illustrative examples related to the Non-Destructive Evaluation of heterogeneous solids, the thermal characterization of chemical reactions in microfluidic channels and the design of systems for multispectral tomography, will be presented. (paper)

Economic importance of non-destructive testing

International Nuclear Information System (INIS)

Loebert, P.

1979-01-01

On May 21 to 23, 1979, the annual meeting of the Deutsche Gesellschaft fuer Zerstoerungsfreie Pruefung took place in Lindau near the Bodensee lake. About 600 experts from Germany and abroad participated in the meeting, whose general subject was 'The Economic Importance of Non-Destructive Testing'. Theoretical problems and practical investigations were discussed in a number of papers on special subjects. Apart from the 33 papers, there was also a poster show with 53 stands with texts, drawings, diagrams, and figures where the authors informed those interested on the latest state of knowledge in testing. The short papers were read in six sessions under the headings of rentability of non-destructive testing, X-ray methods, electromagnetic methods, and ultrasonic methods 1 and 2. (orig.) [de

Role of research in non-destructive evaluation for nuclear technology

International Nuclear Information System (INIS)

Jayakumar, T.; Rao, B.P.C.; Raj, Baldev

2010-01-01

This paper presents the role of research in non-destructive evaluation (NDE) of microstructures and mechanical properties in materials, assessment of manufacturing quality and early detection of in-service damage in nuclear components and structures. A few applications and case studies are discussed based on the results of systematic research and developmental activities pursued in different NDE techniques at the authors' laboratory for three different types of Indian nuclear reactors. (author)

Application of positron annihilation techniques in non-destructive testing

International Nuclear Information System (INIS)

Zeng Hui; Chen Zhiqiang; Jiang Jing; Xue Xudong; Wu Yichu; Liang Jianping; Liu Xiangbing; Wang Rongshan

2014-01-01

Background: The investigation of the material damage state is very important for industrial application. Most mechanical damage starts with a change in the microstructure of the material. Positron annihilation techniques are very sensitive probes for detecting defects and damage on an atomic scale in materials, which are of great concern in the engineering applications. Additionally they are apparatus of non-destruction, high-sensitivity and easy-use. Purpose: Our goal is to develop a system to exploit new non-destructive testing (NDT) methods using positron annihilation spectroscopy, a powerful tool to detect vacancy-type defects and their chemical environment. Methods: A positron NDT system was designed and constructed by modifying the 'sandwich structure' of sample-source-sample in conventional Doppler broadening and positron lifetime spectrometers. Doppler broadening and positron lifetime spectra of a single sample can be measured and analyzed by subtracting the contribution of a reference sample. Results: The feasibility and reliability of positron NDT system have been tested by analyzing nondestructively deformation and damage caused by mechanical treatment or by irradiation of metal alloys. This system can be used for detecting defects and damage in thick or large-size samples, as well as for measuring the two-dimension distribution of defects in portable, sensitive, fast way. Conclusion: Positron NDT measurement shows changes in real atomic-scale defects prior to changes in the mechanical properties, which are detectable by other methods of NDT, such as ultrasonic testing and eddy current testing. This system can be developed for use in both the laboratory and field in the future. (authors)

Non-destructive and micro-invasive testing techniques for characterizing materials, structures and restoration problems in mural paintings

Science.gov (United States)

Tortora, Mariagrazia; Sfarra, Stefano; Chiarini, Marco; Daniele, Valeria; Taglieri, Giuliana; Cerichelli, Giorgio

2016-11-01

In this paper, chemical and structural studies of medieval wall paintings in Ocre (L'Aquila, Italy) are presented. During the latest restoration campaign, non-destructive (Near-Infrared Reflectography and Infrared Thermography) and micro-invasive (Nuclear Magnetic Resonance, Fourier Transform Infrared Spectroscopy, μ-Raman, Scanning Electron Microscopy with X-ray Microanalysis, X-Ray Diffraction, X-Ray Fluorescence, Optical Microscopy, Mass Spectrometry, Thermogravimetry) analyses were performed in order to determine the detachments of wall surfaces and the characterization of original and restoration materials. Data integration allowed to reconstruct the conservative history, the execution techniques and the conservation problems of the artefact, as well as to assess the effectiveness of restoration activities adopted. The combined use of physical and micro-chemical techniques proved to be effective for an in-depth study of materials stratification of paintings.

A comparison between destructive and non-destructive techniques in determining coating thickness

Science.gov (United States)

Haider, F. I.; Suryanto; Ani, M. H.; Mahmood, M. H.

2018-01-01

Measuring coating thickness is an important part in research works related to coating applications. In general, techniques for measuring coating thickness may be divided into destructive and non-destructive methods which are commonly used depending on the applications. The objective of this study is to compare two methods measuring the coating thickness of electroplating copper coating on the austenitic stainless-steel substrate. The electroplating was carried out in a solution containing 200 g/L CuSO4, 100 g/L H2SO4 at room temperature and current of 40mA/cm2 during 20, 40, 60, 80 and 100 mins as coating periods. And the coating thickness was measured by two methods, cross sectional analysis as a destructive technique and weight gain as a non-destructive technique. The results show that at 20 mins coating time interval, the thickness measured by cross sectional method was 16.67 μm and by weight gain method was 17.37 μm, with difference of 0.7 μm and percentage error of 4.11%. This error increased to 5.27% at 100mins time interval, where the values of the thickness measured by cross sectional and weight gain were 86.33 μm and 81.9 μm respectively, and the difference was 4.43 μm. Moreover, though the weight gain method is fast and gives the indication for the termination of a coating process, information regarding the uniformity, porosity and the presence of cracks cannot be obtained. On the other hand, determining the coating thickness using destructive method will damage the sample.

Investigation of shear distance in Michelson interferometer-based shearography for mechanical characterization

International Nuclear Information System (INIS)

Lee, Jung-Ryul; Yoon, Dong-Jin; Kim, Jung-Seok; Vautrin, Alain

2008-01-01

Shearography is a growing industrial field in both quantitative mechanical characterization and relatively qualitative non-destructive testing. In shearography, shear distance is the most important parameter to control measurement performances. In this paper, the role of the shear distance is systematically investigated, focusing on the application of full-field mechanical characterization. A modified Michelson interferometer is considered as the shearing device, which is most commonly adopted for mechanical characterization applications because it enables easy and precise shearing and phase shifting. This paper also includes theoretical and experimental investigations of the relationship between shear distance and performance issues such as the immeasurable zone in the target with discontinuity, signal-to-noise ratio, sensitivity and shear distortion. In addition, this study is verified with actual shearographic results and a phase-shifting grid method capable of full-field displacement evaluation in the submicrometer regime

Development of non-destructive Young's modulus measurement techniques in non-oriented CeF$_{3}$ crystals

CERN Document Server

Pietroni, P; Lebeau, M; Majni, G; Rinaldi, D

2005-01-01

For a reliable mechanical assembly of scintillating crystals for the application to radiographic systems such as Positron Emission Tomographer (PET) and high-energy physics calorimeters (e.g. in CMS at CERN LHC), the evaluation of the monocrystal elastic constant (Young's modulus) is needed. Its knowledge is also essential in the photoelastic analysis for the determination of residual stresses. In this work non-destructive techniques based on elastic wave propagation are tested. They differ in the mechanical excitation device: instrumented hammer, traditional ultrasonic probes and laser- generated ultrasound. We have analysed three non-oriented cerium fluoride crystal samples produced for scintillation applications. Finally, we have validated the experimental results comparing them with the elastic constant calculated by using the stiffness matrix.

Development of non-destructive Young's modulus measurement techniques in non-oriented CeF3 crystals

International Nuclear Information System (INIS)

Pietroni, P.; Paone, N.; Lebeau, M.; Majni, G.; Rinaldi, D.

2005-01-01

For a reliable mechanical assembly of scintillating crystals for the application to radiographic systems such as Positron Emission Tomographer (PET) and high-energy physics calorimeters (e.g. in CMS at CERN LHC), the evaluation of the monocrystal elastic constant (Young's modulus) is needed. Its knowledge is also essential in the photoelastic analysis for the determination of residual stresses. In this work non-destructive techniques based on elastic wave propagation are tested. They differ in the mechanical excitation device: instrumented hammer, traditional ultrasonic probes and laser-generated ultrasound. We have analysed three non-oriented cerium fluoride crystal samples produced for scintillation applications. Finally, we have validated the experimental results comparing them with the elastic constant calculated by using the stiffness matrix

High-Energy X-ray imaging applied to non destructive characterization of large nuclear waste drums

International Nuclear Information System (INIS)

Estre, Nicolas; Eck, Daniel; Pettier, Jean-Luc; Payan, Emmanuel; Roure, Christophe; Simon, Eric

2013-06-01

As part of its R and D programs on non-destructive testing of nuclear waste drums, CEA is commissioning an irradiation cell named CINPHONIE, at Cadarache. This cell allows high-energy imaging (radiography and tomography) on large volumes (up to 5 m 3 ) and heavy weights (up to 5 tons). A demonstrator has been finalized, based on existing components. The X-ray source is a 9 MeV LINAC which produces Bremsstrahlung X-rays (up to 23 Gy/min at 1 meter in the beam axis). The mechanical bench is digitally controlled on three axes (translation, rotation, elevation) and can handle objects up to 2 t. This bench performs trajectories necessary for acquisition of projections (sinograms) according to different geometries: Translation-Rotation, Fan-Beam and Cone-Beam. Two detection systems both developed by CEA-Leti are available. The first one is a large GADOX scintillating screen (800*600 mm 2 ) coupled to a low-noise pixelated camera. The second one is a multi- CdTe semiconductor detector, offering measurements up to 5 decades of attenuation (equivalent to 25 cm of lead or 180 cm of standard concrete). At the end of the acquisition, a Filtered Back Projection-based algorithm is performed. Then, a density slice (fan-beam tomography) or a density volume (cone-beam tomography or helical tomography) is produced and used to examine the waste. Characterization of LINAC, associated detectors as well as the full acquisition chain, are presented. Experimental performances on phantoms and real drum are discussed and expected limits on defect detectability are evaluated by simulation. The final system, designed to handle objects up to 5 tons is then presented. (authors)

Non-destructive evaluation of thermal aging embrittlement of duplex stainless steels

International Nuclear Information System (INIS)

Yi, Y.S.; Tomobe, T.; Watanabe, Y.; Shoji, T.

1993-01-01

The non-destructive evaluation procedure for detecting thermal aging embrittlement of cast duplex stainless steels has been investigated. As a novel measurement technique for the thermal aging embrittlement, an electrochemical method was used and anodic polarization behaviors were measured on new, service exposed, and laboratory aged materials and then were compared with the results of the mechanical tests and microstructural changes. During the polarization experiments performed in potassium hydroxide solution (KOH), M 23 C 6 carbides on phase boundary were preferentially dissolved, which was comfirmed by the SEM after polarization measurements. The preferential dissolution of M 23 C 6 carbides were obtained. Also, the non-destructive measurement and evaluation method of spinodal decomposition, which has been known as the primary mechanism of embrittlement inferrite phase, was reviewed. When the materials, where spinodal decomposition occurred, were polarized in an acetic acid solution (CH 3 COOH), larger critical anodic current densities were observed than those observed on new materials, and these results were consistent with the result of the microhardness measurement. Concerning these polarization results, a critical electric charge, which was required for stable passive films in passive metals, was defined and the relationship between the microstructural changes and this charge amount was reviewed under various polarization conditions in order to verify the polarization mechanism of the spinodally decomposed ferrite phase

Issues of weapons of mass destruction non-proliferation in Tajikistan

International Nuclear Information System (INIS)

Mirsaidov, U.M.

2010-01-01

This article is devoted to issues of weapons of mass destruction non-proliferation in Tajikistan. Over a period of 20 century, starting from First World War, the weapons of mass destruction arouse serious concern of world community. Geneva protocol of 1925 prohibits the use of chemical and biological weapons. Once nuclear weapon was created, the weapons of mass destruction distributions become the subject of high concern. Besides, during the end of 'cold war', regional conflicts, collapse of Soviet Union, as well as access to sensitive technologies considerably increase the danger of weapons of mass destruction distribution. More than 10 countries have active programs, relating to weapons of mass destruction and, possibly, more than ten countries have potential to start implementing such kinds of programs. Nowadays, trans national organized criminal groups and international terrorist networks are appeared in the world scene, which show interest in obtaining an access to sensitive materials, technologies, weapons and their distribution. After 11 September events, the risk of such weapons of mass destruction components use by such forces for Governments blackmail become real scene, which, despite of low possibility of this threat implementation, could have very serious and disastrous consequences. International community responded to these problems and challenges, basically through the following actions, which is detailed regime development of multilateral international treaties, directed to weapons of mass destruction distribution prevention. Non-proliferation treaty of nuclear weapons, Convention on prohibition of chemical weapons and Convention on prohibition of biological and toxin weapons are some of them. As it is known, Tajikistan signed all these treaties. For different reasons these treaties were subject of serious tests. Nuclear weapons tests in India and Pakistan in 1998 year, actual Israel status as state having nuclear weapon and North Korean program on

Non-destructive testing and evaluation for structural integrity

International Nuclear Information System (INIS)

Baldev Raj; Jayakumar, T.; Rao, B.P.C.

1995-01-01

In this paper, a brief description of the physical concepts of non-destructive evaluation (NDE) methods and the physical/derived parameters that are used for assessing defects, stresses and microstructures are given. A few case studies highlighting the importance of non-destructive testing and evaluation for structural integrity assessment are also discussed based on the investigations carried out. Emerging concepts like intelligent processing of materials, expert systems, neural networks, use of multisensors with fusion of data and exploitation of signal analysis and imaging approaches are also addressed in this paper. (author). 92 refs., 1 tab

Use of non-standardised micro-destructive techniques in the characterization of traditional construction materials

Science.gov (United States)

Ioannou, Ioannis; Theodoridou, Magdalini; Modestou, Sevasti; Fournari, Revecca; Dagrain, Fabrice

2013-04-01

The characterization of material properties and the diagnosis of their state of weathering and conservation are three of the most important steps in the field of cultural heritage preservation. Several standardised experimental methods exist, especially for determining the material properties and their durability. However, they are limited in their application by the required size of test specimens and the controlled laboratory conditions needed to undertake the tests; this is especially true when the materials under study constitute immovable parts of heritage structures. The current use of other advanced methods of analysis, such as imaging techniques, in the aforementioned field of research offers invaluable results. However, these techniques may not always be accessible to the wider research community due to their complex nature and relatively high cost of application. This study presents innovative applications of two recently developed cutting techniques; the portable Drilling Resistance Measuring System (DRMS) and the scratch tool. Both methods are defined as micro-destructive, since they only destroy a very small portion of sample material. The general concept of both methods lies within the forces needed to cut a material by linear (scratch tool) or rotational (DRMS) cutting action; these forces are related to the mechanical properties of the material and the technological parameters applied on the tool. Therefore, for a given testing configuration, the only parameter influencing the forces applied is the strength of the material. These two techniques have been used alongside a series of standardised laboratory tests aiming at the correlation of various stone properties (density, porosity, dynamic elastic modulus and uniaxial compressive strength). The results prove the potential of both techniques in assessing the uniaxial compressive strength of stones. The scratch tool has also been used effectively to estimate the compressive strength of mud bricks. It

Non-destructive testing of CFC/Cu joints

International Nuclear Information System (INIS)

Casalegno, V.; Ferraris, M.; Salvo, M.; Vesprini, R.; Merola, M.

2006-01-01

Reliable non-destructive tests (NDT) are fundamental for the manufacturing of ITER components, especially for high heat flux plasma facing components. NDT include various techniques, which allow inspection of a component without impairing serviceability; it's important to detect and characterize defects (type, size and position) as well as the set-up of acceptance standards in order to predict their influence on the component performance in service conditions. The present study shows a description of NDT used to assess the manufacturing quality of CFC (carbon fibre reinforced carbon matrix composites)/Cu/CuCrZr joints. In the ITER divertor, armor tiles made of CFC are joined to the cooling structure made of precipitation hardened copper alloy CuCrZr; a soft pure Cu interlayer is required between the heat sink and the armour in order to mitigate the stresses at the joint interface. NDT on CFC/Cu joint are difficult because of the different behavior of CFC and copper with regard to physical excitations (e.g. ultrasonic wave) used to test the component; furthermore the response to this input must be accurately studied to identify the detachment of CFC tiles from Cu alloy. The inspected CFC/Cu/CuCrZr joints were obtained through direct casting of pure Cu on modified CFC surface and subsequently through brazing of CFC/Cu joints to CuCrZr by a Cu-based alloy. Different non-destructive methods were used for inspecting these joints: lock-in thermography, ultrasonic inspections, microtomography and microradiography. The NDT tests were followed by metallographic investigation on the samples, since the reliability of a certain non destructive test can be only validated by morphological evidence of the detected defects. This study will undertake a direct comparison of NDT used on CFC/Cu joints in terms of real flaws presence. The purpose of this work is to detect defects at the joining interface as well as in the cast copper ( for instance voids). The experimental work was

The Destructive/Non-Destructive Identification of Enameled Pottery, Glass Artifacts and Associated Pigments—A Brief Overview

Directory of Open Access Journals (Sweden)

Philippe Colomban

2013-07-01

Full Text Available The birth of Chemistry can be found in two main practices: (i the Arts du feu (ceramic and glass, metallurgy, i.e., inorganic and solid state chemistry and (ii the preparation of remedies, alcohols and perfumes, dyes, i.e., organic and liquid state chemistry. After a brief survey of the history of (glazed pottery and (enameled glass artifacts, the development of destructive and non-destructive analytical techniques during the last few centuries is reviewed. Emphasis is put on mobile non-destructive Raman microspectroscopy of pigments and their glass/glaze host matrices for chronological/technological expertise. The techniques of white opacification, blue, yellow, green, red, and black coloring, are used as examples to point out the interest of pigments as chronological/technological markers.

Local destruction of superconductivity by non-magnetic impurities in mesoscopic iron-based superconductors.

Science.gov (United States)

Li, Jun; Ji, Min; Schwarz, Tobias; Ke, Xiaoxing; Van Tendeloo, Gustaaf; Yuan, Jie; Pereira, Paulo J; Huang, Ya; Zhang, Gufei; Feng, Hai-Luke; Yuan, Ya-Hua; Hatano, Takeshi; Kleiner, Reinhold; Koelle, Dieter; Chibotaru, Liviu F; Yamaura, Kazunari; Wang, Hua-Bing; Wu, Pei-Heng; Takayama-Muromachi, Eiji; Vanacken, Johan; Moshchalkov, Victor V

2015-07-03

The determination of the pairing symmetry is one of the most crucial issues for the iron-based superconductors, for which various scenarios are discussed controversially. Non-magnetic impurity substitution is one of the most promising approaches to address the issue, because the pair-breaking mechanism from the non-magnetic impurities should be different for various models. Previous substitution experiments demonstrated that the non-magnetic zinc can suppress the superconductivity of various iron-based superconductors. Here we demonstrate the local destruction of superconductivity by non-magnetic zinc impurities in Ba0.5K0.5Fe2As2 by exploring phase-slip phenomena in a mesoscopic structure with 119 × 102 nm(2) cross-section. The impurities suppress superconductivity in a three-dimensional 'Swiss cheese'-like pattern with in-plane and out-of-plane characteristic lengths slightly below ∼1.34 nm. This causes the superconducting order parameter to vary along abundant narrow channels with effective cross-section of a few square nanometres. The local destruction of superconductivity can be related to Cooper pair breaking by non-magnetic impurities.

Training Guidelines in Non-destructive Testing Techniques. 2013 Edition

International Nuclear Information System (INIS)

2014-12-01

The IAEA promotes industrial applications of radiation technology, including non-destructive testing (NDT), through activities such as Technical Cooperation Projects (national and regional) and Coordinated Research Projects. Through this cooperation, Member States have initiated national programmes for the training and certification of NDT personnel. National certifying bodies have also been established based on International Organization for Standardization (ISO) standards. As part of these efforts, the IAEA has been actively involved in developing training materials. Consequently, IAEA-TECDOC-407, Training Guidelines in Non-destructive Testing Techniques, was published in 1987, then revised and expanded as IAEA-TECDOC-628 in 1991. Revisions of IAEA-TECDOC-628 were considered essential to meet the demands of end-user industries in Member States, and revised and expanded versions were issued in 2002 and 2008. These latter versions included work conducted by the International Committee for Non-Destructive Testing (ICNDT) and many national NDT societies. It is one of the publications referred to in ISO 9712:2005, Non-destructive Testing: Qualification and Certification of Personnel, which in turn is an internationally accepted standard, revised as ISO 9712:2012, Non-destructive Testing: Qualification and Certification of NDT Personnel. This publication is an updated version of IAEA-TECDOC-628. The content of which has been revised following the changes of ISO 9712 converging with EN 473 and becoming EN ISO 9712:2012, based on the experience of experts and comments from end-user industries. The details of the topics on each subject have been expanded to include the latest developments in the respective methods. The incorporated changes will assist the end-user industries to update their NDT qualification and certification schemes and course materials. This publication, like the previous versions, will continue to play an important role in international harmonization

In situ non-destructive measurement of biofilm thickness and topology in an interferometric optical microscope

Energy Technology Data Exchange (ETDEWEB)

Larimer, Curtis [Pacific Northwest National Laboratory, Battelle for the USDOE, PO Box 999, MSIN P7-50 Richland WA 99354 USA; Suter, Jonathan D. [Pacific Northwest National Laboratory, Battelle for the USDOE, PO Box 999, MSIN P7-50 Richland WA 99354 USA; Bonheyo, George [Pacific Northwest National Laboratory, Battelle for the USDOE, PO Box 999, MSIN P7-50 Richland WA 99354 USA; Addleman, Raymond Shane [Pacific Northwest National Laboratory, Battelle for the USDOE, PO Box 999, MSIN P7-50 Richland WA 99354 USA

2016-03-15

Biofilms are ubiquitous and deleteriously impact a wide range of industrial processes, medical and dental health issues, and environmental problems such as transport of invasive species and the fuel efficiency of ocean going vessels. Biofilms are difficult to characterize when fully hydrated, especially in a non-destructive manner, because of their soft structure and water-like bulk properties. Herein we describe a non-destructive high resolution method of measuring and monitoring the thickness and topology of live biofilms of using white light interferometric optical microscopy. Using this technique, surface morphology, surface roughness, and biofilm thickness can be measured non-destructively and with high resolution as a function of time without disruption of the biofilm activity and processes. The thickness and surface topology of a P. putida biofilm were monitored growing from initial colonization to a mature biofilm. Typical bacterial growth curves were observed. Increase in surface roughness was a leading indicator of biofilm growth.

Cell wall proteome of sugarcane stems: comparison of a destructive and a non-destructive extraction method showed differences in glycoside hydrolases and peroxidases.

Science.gov (United States)

Calderan-Rodrigues, Maria Juliana; Jamet, Elisabeth; Douché, Thibaut; Bonassi, Maria Beatriz Rodrigues; Cataldi, Thaís Regiani; Fonseca, Juliana Guimarães; San Clemente, Hélène; Pont-Lezica, Rafael; Labate, Carlos Alberto

2016-01-11

Sugarcane has been used as the main crop for ethanol production for more than 40 years in Brazil. Recently, the production of bioethanol from bagasse and straw, also called second generation (2G) ethanol, became a reality with the first commercial plants started in the USA and Brazil. However, the industrial processes still need to be improved to generate a low cost fuel. One possibility is the remodeling of cell walls, by means of genetic improvement or transgenesis, in order to make the bagasse more accessible to hydrolytic enzymes. We aimed at characterizing the cell wall proteome of young sugarcane culms, to identify proteins involved in cell wall biogenesis. Proteins were extracted from the cell walls of 2-month-old culms using two protocols, non-destructive by vacuum infiltration vs destructive. The proteins were identified by mass spectrometry and bioinformatics. A predicted signal peptide was found in 84 different proteins, called cell wall proteins (CWPs). As expected, the non-destructive method showed a lower percentage of proteins predicted to be intracellular than the destructive one (33% vs 44%). About 19% of CWPs were identified with both methods, whilst the infiltration protocol could lead to the identification of 75% more CWPs. In both cases, the most populated protein functional classes were those of proteins related to lipid metabolism and oxido-reductases. Curiously, a single glycoside hydrolase (GH) was identified using the non-destructive method whereas 10 GHs were found with the destructive one. Quantitative data analysis allowed the identification of the most abundant proteins. The results highlighted the importance of using different protocols to extract proteins from cell walls to expand the coverage of the cell wall proteome. Ten GHs were indicated as possible targets for further studies in order to obtain cell walls less recalcitrant to deconstruction. Therefore, this work contributed to two goals: enlarge the coverage of the sugarcane

Non-destructive characterization of materials by single-sided NMR

International Nuclear Information System (INIS)

Goga, Nicolae-Octavian

2007-01-01

The experiments conducted in this work demonstrate the efficiency and sensitivity of single-sided NMR for investigating macromolecular materials on large time and length scales. Elastomers can readily be characterized by unilateral NMR of protons in terms of a variety of parameters, which correlate with the overall molecular mobility. In this way information about the cross-link density, state of cure and strain, the effects of aging and product heterogeneity can obtained. For these purposes, the NMR-MOUSE was used to optimize product development and to monitor product and production quality on-line. The sensor is also suitable for nondestructive probing of the mechanical deformation in cross-linked elastomers. A special magnet design that fits a stress-strain device has been used for complementary investigation of a series of different rubber stripes during mechanical testing. The profile NMR-MOUSE was found to be a unique tool for the characterization of changes induced by the UV irradiation in natural rubber. The aging profiles were interpreted for the first time based on a novel model in which the radiation absorption coefficient depends on the depth in the sample. (orig.)

Non-destructive characterization of materials by single-sided NMR

Energy Technology Data Exchange (ETDEWEB)

Goga, Nicolae-Octavian

2007-08-20

The experiments conducted in this work demonstrate the efficiency and sensitivity of single-sided NMR for investigating macromolecular materials on large time and length scales. Elastomers can readily be characterized by unilateral NMR of protons in terms of a variety of parameters, which correlate with the overall molecular mobility. In this way information about the cross-link density, state of cure and strain, the effects of aging and product heterogeneity can obtained. For these purposes, the NMR-MOUSE was used to optimize product development and to monitor product and production quality on-line. The sensor is also suitable for nondestructive probing of the mechanical deformation in cross-linked elastomers. A special magnet design that fits a stress-strain device has been used for complementary investigation of a series of different rubber stripes during mechanical testing. The profile NMR-MOUSE was found to be a unique tool for the characterization of changes induced by the UV irradiation in natural rubber. The aging profiles were interpreted for the first time based on a novel model in which the radiation absorption coefficient depends on the depth in the sample. (orig.)

Non-destructive nuclear forensics of radioactive samples

Energy Technology Data Exchange (ETDEWEB)

Rogge, R.B. [Canadian Neutron Beam Centre, Chalk River, ON (Canada); Alexander, Q.; Bentoumi, G.; Dimayuga, F. [Atomic Energy of Canada Limited, Chalk River, ON (Canada); Flacau, R. [Canadian Neutron Beam Centre, Chalk River, ON (Canada); Li, G.; Li, L.; Sur, B. [Atomic Energy of Canada Limited, Chalk River, ON (Canada)

2014-07-01

It is a matter of public safety and security to be able to examine suspicious packages of unknown origin. If the package is radioactive and sealed (i.e., the radioactive materials contained in the package, including their chemical and physical forms, are unknown), there is a significant risk on how to handle the package and eventually safely dispose of its contents. Within the context of nuclear security, nuclear forensics helps address the key issue of identifying the nature and origin of radioactive and nuclear material in order to improve physical protection measures and prevent future theft or diversion of these materials. Nuclear forensics utilizes analytical techniques, destructive and non-destructive, developed for applications related to nuclear fuel cycles. This paper demonstrates the non-destructive examination techniques that can be used to inspect encapsulated radioactive samples. Results of γ spectroscopy, X-ray spectroscopy, neutron imaging, neutron diffraction, and delayed neutron analysis as applied to an examination of sealed capsules containing unknown radioactive materials are presented. The paper also highlights the value of these techniques to the overall nuclear forensic investigation to determine the origin of these unknown radioactive materials. (author)

Non-destructive elecrochemical monitoring of reinforcement corrosion

DEFF Research Database (Denmark)

Nygaard, Peter Vagn

been widely accepted as a non-destructive ”state of the art” technique for detection of corrosion in concrete structures. And, over the last decade, the trend in corrosion monitoring has moved towards quantitative non-destructive monitoring of the corrosion rate of the steel reinforcement. A few...... corrosion rate measurement instruments have been developed and are commercially available. The main features of these instruments are the combined use of an electrochemical technique for determining the corrosion rate and a so-called ”confinement technique”, which in principle controls the polarised surface...... area of the reinforcement, i.e. the measurement area. Both on-site investigations and laboratory studies have shown that varying corrosion rates are obtained when the various commercially available instruments are used. And in the published studies, conflicting explanations are given illustrating...

Non-destructive examination system of vitreous body

Science.gov (United States)

Shibata, Takuma; Gong, Jin; Watanabe, Yosuke; Kabir, M. Hasnat; Masato, Makino; Furukawa, Hidemitsu; Nishitsuka, Koichi

2014-04-01

Eyeball plays a quite important role in acquiring the vision. Vitreous body occupies the largest part of the eyeball and consists of biological, elastic, transparent, gel materials. In the present medical examination, the non-destructive examination method of the vitreous body has not been well established. Here, we focus on an application of dynamic light scattering to this topic. We tried to apply our lab-made apparatus, scanning microscopic light scattering (SMILS), which was specially designed for observing the nanometer-scale network structure in gel materials. In order to examine the vitreous body using SMILS method, a commercial apparatus, nano Partica (Horiba Co. Ltd.) was also customized. We analyzed vitreous body using both the SMILS and the customized nano Partica. We successfully examined the vitreous bodies of healthy pigs in non-destructive way.

New tasks for non-destructive testing

International Nuclear Information System (INIS)

1990-01-01

The proceedings contain 29 lectures and 43 posters which were presented in Trier at the annual meeting of the DGZfP in May 1990. The contributions report on further development of non-destructive testing methods towards more reliability, both of inspections and with regard to interpretation of the results. (MM) [de

National seminar on non-destructive evaluation techniques: proceedings cum souvenir

International Nuclear Information System (INIS)

Dutta, N.G.; Kulkarni, P.G.; Purushotham, D.S.C.

1994-01-01

This volume contains selected papers presented at the National Seminar on Non-Destructive Evaluation Techniques held at Bhabha Atomic Research Centre, Mumbai during December 8-9, 1994. The papers covered a wide spectrum of non-destructive evaluation activities including that for quality assurance of various nuclear components and structures with the focal theme being computerization and robotics. The papers relevant to INIS are indexed separately

Non destructive testing in amusement park

International Nuclear Information System (INIS)

Dominguez Marrero, Humberto; Hernandez Torres, Debora; Sendoya Puente, Felix; Herrera Palma, Victoria; Suarez Guerra, Yarelis; Moreno Hernandez, Eduardo; Lopez Hernandez, Pedro

2009-01-01

In 2006 began the installation of Chinese amusement parks at several places in Havana City. Structural security is one of the principal tasks that should be done, since the beginning of the services of these installations. The use on Non Destructive Testing Techniques (NDT), has to be development and implemented in order to avoid the possibility of failure during services with a consequence threat to safety for the public presented. In this work it is shown the results of application of NDT techniques and recommendations for the quality control of the different welds and mechanical components presented. Techniques as Visual Examination, Liquid Penetrant and Ultrasonic have been used for these purposes in order to obtain a structural diagnostic in the amusement parks. There are also exposed the use and implementation of international recommendations and Standards, which are very rigorous in its applications for the case of recreation industry. This is a consequence to its social service fundamentally to children and teenage people. (Author)

Design of eddy current probes and signal inversion for non-destructive testing

International Nuclear Information System (INIS)

Ravat, C.

2008-01-01

Non destructive testing is widely used in aerospace industry and nuclear industry. The growing complexity of industrial processes and manufactured parts, the increasing need of safety in service and the will of life span optimization, require more and more complex quality evaluations to be set up. Among the different anomalies to consider, sub-millimetric breaking surface notches have to be subject to special care. Indeed, it often constitutes a start to larger notches, which can cause the destruction of parts. Penetrant testing is nowadays widely used for that kind of defect, owing to its good performances. Nevertheless, it should be eventually dropped because of environmental norms. Among the possible substitution solutions, the use of eddy currents (EC) for conductive parts is a reliable, fast and inexpensive alternative. The study is about the conception and the use of multi-elements EC probe structures featuring microsensors for non destructive testing of surface breaking defects. A methodology has been established in order to develop such structures and to compare their performances within the framework of sub-millimetric surface breaking notch research. These structures has been employed for calibrated notches evaluation with a specific acquisition bench. Original detection and defect characterization algorithms have been designed and implemented on acquired signals. The most efficient structure has been determined, the notch detection quality has been quantified, and the geometric characteristics of notches has been estimated. (author)

Non-destructive evaluation of containment walls in nuclear power plants

Science.gov (United States)

Garnier, V.; Payan, C.; Lott, M.; Ranaivomanana, N.; Balayssac, J. P.; Verdier, J.; Larose, E.; Zhang, Y.; Saliba, J.; Boniface, A.; Sbartai, Z. M.; Piwakowski, B.; Ciccarone, C.; Hafid, H.; Henault, J. M.; Buffet, F. Ouvrier

2017-02-01

Two functions are regularly tested on containment walls in order to anticipate a possible accident. The first is mechanical to resist a possible internal over-pressure and the second is to prevent leakage. The AAPR reference accident is the rupture of a pipe in the primary circuit of a nuclear plant. In this case, the pressure and temperature can reach 5 bar and 180°C in 20 seconds. The national project `Non-destructive testing of the containment structures of nuclear plants' aims at studying the non-destructive techniques capable to evaluate the concrete properties and its damaging and cracks. This 4-year-project is segmented into two parts. The first consists in developing and selecting the most relevant NDEs in the laboratory to reach these goals. These evaluations are developed in conditions representing the real conditions of the stresses generated during ten-yearly visits of the plants or those related to an accident. The second part consists in applying the selected techniques to two containment structures under pressure. The first structure is proposed by ONERA and the second is a mockup of a containment wall on a 1/3 scale made by EDF within the VeRCoRs project. Communication is focused on the part of the project that concerns the damage and crack process characterization by means of NDT. The tests are done in 3 or 4 points bending in order to study the cracks' generation, their propagation, as well as their opening and closing. The main ultrasonic techniques developed concern linear or non-linear acoustic: acoustic emission [1], Locadiff [2], energy diffusion, surface wave's velocity and attenuation, DAET [3]. The recorded data contribute to providing the mapping of the investigated parameters, either in volume, in surface or globally. Digital image correlation is an important additional asset to validate the coherence of the data. The spatial normalization of the data in the specimen space allows proposing algorithms on the combination of the

Microwave Metamaterial Absorber for Non-Destructive Sensing Applications of Grain

Directory of Open Access Journals (Sweden)

Yin Zhang

2018-06-01

Full Text Available In this work, we propose a metamaterial absorber at microwave frequencies with significant sensitivity and non-destructive sensing capability for grain samples. This absorber is composed of cross-resonators periodically arranged on an ultrathin substrate, a sensing layer filled with grain samples, and a metal ground. The cross-resonator array is fabricated using the printed circuit board process on an FR-4 board. The performance of the proposed metamaterial is demonstrated with both full-wave simulation and measurement results, and the working mechanism is revealed through multi-reflection interference theory. It can serve as a non-contact sensor for food quality control such as adulteration, variety, etc. by detecting shifts in the resonant frequencies. As a direct application, it is shown that the resonant frequency displays a significant blue shift from 7.11 GHz to 7.52 GHz when the mass fraction of stale rice in the mixture of fresh and stale rice is changed from 0% to 100%. In addition, the absorber shows a distinct difference in the resonant absorption frequency for different varieties of grain, which also makes it a candidate for a grain classification sensor. The presented scheme could open up opportunities for microwave metamaterial absorbers to be applied as efficient sensors in the non-destructive evaluation of agricultural and food product quality.

Non-destructive sampling of ancient insect DNA

DEFF Research Database (Denmark)

Thomsen, Philip Francis; Elias, Scott; Gilbert, Tom

2009-01-01

BACKGROUND: A major challenge for ancient DNA (aDNA) studies on insect remains is that sampling procedures involve at least partial destruction of the specimens. A recent extraction protocol reveals the possibility of obtaining DNA from past insect remains without causing visual morphological...... of 77-204 base pairs (-bp) in size using species-specific and general insect primers. CONCLUSION/SIGNIFICANCE: The applied non-destructive DNA extraction method shows promising potential on insect museum specimens of historical age as far back as AD 1820, but less so on the ancient permafrost......-preserved insect fossil remains tested, where DNA was obtained from samples up to ca. 26,000 years old. The non-frozen sediment DNA approach appears to have great potential for recording the former presence of insect taxa not normally preserved as macrofossils and opens new frontiers in research on ancient...

In-situ Non-destructive Studies on Biofouling Processes in Reverse Osmosis Membrane Systems

KAUST Repository

Farhat, Nadia

2016-12-01

Reverse osmosis (RO) and nanofiltration (NF) membrane systems are high-pressure membrane filtration processes that can produce high quality drinking water. Biofouling, biofilm formation that exceeds a certain threshold, is a major problem in spiral wound RO and NF membrane systems resulting in a decline in membrane performance, produced water quality, and quantity. In practice, detection of biofouling is typically done indirectly through measurements of performance decline. Existing direct biofouling detection methods are mainly destructive, such as membrane autopsies, where biofilm samples can be contaminated, damaged and resulting in biofilm structural changes. The objective of this study was to test whether transparent luminescent planar oxygen sensing optodes, in combination with a simple imaging system, can be used for in-situ, non-destructive biofouling characterization. Aspects of the study were early detection of biofouling, biofilm spatial patterning in spacer filled channels, and the effect of feed cross-flow velocity, and feed flow temperature. Oxygen sensing optode imaging was found suitable for studying biofilm processes and gave detailed spatial and quantitative biofilm development information enabling better understanding of the biofouling development process. The outcome of this study attests the importance of in-situ, non-destructive imaging in acquiring detailed knowledge on biofilm development in membrane systems contributing to the development of effective biofouling control strategies.

Non-destructive and micro-invasive testing techniques for characterizing materials, structures and restoration problems in mural paintings

Energy Technology Data Exchange (ETDEWEB)

Tortora, Mariagrazia, E-mail: Mariagrazia.Tortora@univaq.it [University of L’Aquila, Department of Physical and Chemical Sciences, Via Vetoio (Coppito 1), I-67100, Loc. Coppito, L’Aquila, AQ (Italy); Sfarra, Stefano, E-mail: Stefano.Sfarra@univaq.it [Las.E.R. Laboratory, University of L’Aquila, Department of Industrial and Information Engineering and Economics, Piazzale E. Pontieri 1, I-67100, Loc. Monteluco di Roio, Roio Poggio, L’Aquila, AQ, Italy, (Italy); Chiarini, Marco, E-mail: mchiarini@unite.it [University of Teramo, Department of Bioscience and Technology for Food Agriculture and Environment, Via Carlo Lerici 1, I-64023, Mosciano Sant’Angelo, Teramo, TE, Italy, (Italy); Daniele, Valeria, E-mail: Valeria.Daniele@univaq.it [University of L’Aquila, Department of Industrial and Information Engineering and Economics, Piazzale E. Pontieri 1, I-67100, Loc. Monteluco di Roio, Roio Poggio, L’Aquila, AQ (Italy); Taglieri, Giuliana, E-mail: Giuliana.Taglieri@univaq.it [University of L’Aquila, Department of Industrial and Information Engineering and Economics, Piazzale E. Pontieri 1, I-67100, Loc. Monteluco di Roio, Roio Poggio, L’Aquila, AQ (Italy); Cerichelli, Giorgio, E-mail: Giorgio.Cerichelli@univaq.it [University of L’Aquila, Department of Physical and Chemical Sciences, Via Vetoio (Coppito 1), I-67100, Loc. Coppito, L’Aquila, AQ (Italy)

2016-11-30

Highlights: • Infrared thermography allowed to identify structural damage and rising damp effect. • The present approach provided insights on the used pigments and painting techniques. • FT-IR, XRF and XRD analyses of the mortar sample showed the peculiar composition. • 1D, 2D NMR analyses were useful for the identification of the restoration polymer. • NMR technique also allowed to characterize the plasticizing agents. - Abstract: In this paper, chemical and structural studies of medieval wall paintings in Ocre (L’Aquila, Italy) are presented. During the latest restoration campaign, non-destructive (Near-Infrared Reflectography and Infrared Thermography) and micro-invasive (Nuclear Magnetic Resonance, Fourier Transform Infrared Spectroscopy, μ-Raman, Scanning Electron Microscopy with X-ray Microanalysis, X-Ray Diffraction, X-Ray Fluorescence, Optical Microscopy, Mass Spectrometry, Thermogravimetry) analyses were performed in order to determine the detachments of wall surfaces and the characterization of original and restoration materials. Data integration allowed to reconstruct the conservative history, the execution techniques and the conservation problems of the artefact, as well as to assess the effectiveness of restoration activities adopted. The combined use of physical and micro-chemical techniques proved to be effective for an in-depth study of materials stratification of paintings.

Non-destructive and micro-invasive testing techniques for characterizing materials, structures and restoration problems in mural paintings

International Nuclear Information System (INIS)

Tortora, Mariagrazia; Sfarra, Stefano; Chiarini, Marco; Daniele, Valeria; Taglieri, Giuliana; Cerichelli, Giorgio

2016-01-01

Highlights: • Infrared thermography allowed to identify structural damage and rising damp effect. • The present approach provided insights on the used pigments and painting techniques. • FT-IR, XRF and XRD analyses of the mortar sample showed the peculiar composition. • 1D, 2D NMR analyses were useful for the identification of the restoration polymer. • NMR technique also allowed to characterize the plasticizing agents. - Abstract: In this paper, chemical and structural studies of medieval wall paintings in Ocre (L’Aquila, Italy) are presented. During the latest restoration campaign, non-destructive (Near-Infrared Reflectography and Infrared Thermography) and micro-invasive (Nuclear Magnetic Resonance, Fourier Transform Infrared Spectroscopy, μ-Raman, Scanning Electron Microscopy with X-ray Microanalysis, X-Ray Diffraction, X-Ray Fluorescence, Optical Microscopy, Mass Spectrometry, Thermogravimetry) analyses were performed in order to determine the detachments of wall surfaces and the characterization of original and restoration materials. Data integration allowed to reconstruct the conservative history, the execution techniques and the conservation problems of the artefact, as well as to assess the effectiveness of restoration activities adopted. The combined use of physical and micro-chemical techniques proved to be effective for an in-depth study of materials stratification of paintings.

Non-destructive study of ancient documents and books by means of ion beams

International Nuclear Information System (INIS)

Ruvalcaba S, J.L.; Monroy, M.

2004-01-01

In this work, a non destructive methodology for the analysis of ancient manuscripts and books using an external beam system and the techniques Particle Induced X-ray Emission Spectroscopy (PIXE) and Rutherford Backscattering Spectrometry (RBS) is presented. This application shows the analytical features of the particle accelerator based techniques for the characterization of this kind of historical materials. This methodology was used for the analysis of inks of an European book from XVII century. This is the first study in Mexico of an ancient book using simultaneously PIXE and RBS non-vacuum techniques. (Author) 21 refs., 9 figs

Eddy currents non-destructive testing. use of a numeric/symbolic method to separate and characterize the transitions of a signal

International Nuclear Information System (INIS)

Benas, J.C.; Lefevre, F.; Gaillard, P.; Georgel, B.

1995-01-01

This paper presents an original numeric/symbolic method for solving an inverse problem in the field of non-destructive testing. The purpose of this method is to characterize the transitions of a signal even when they are superimposed. Its principle is to solve as many direct problems as necessary to obtain the solution, and to use some hypothesis to manage the reasoning of the process. The direct problem calculation yields to a 'model signal', and the solution is reached when the model signal is close to the measured one. This method calculates the directions of minimization thanks to a symbolic reasoning based on the peaks of the residual signal. The results of the method are good and seem very promising. (authors). 13 refs., 13 figs., 5 tabs

Non-destructive Preirradiation Assessment of UN / U-Si “LANL1” ATF formulation

Energy Technology Data Exchange (ETDEWEB)

Vogel, Sven C. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Losko, Adrian Simon [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Pokharel, Reeju [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Ickes, Timothy Lee [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Hunter, James F. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Brown, Donald William [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Voit, Stewart Lancaster [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Tremsin, Anton S. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Bourke, Mark Andrew [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); McClellan, Kenneth James [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

2016-09-15

The goal of the Advanced Non-destructive Fuel Examination (ANDE) work package is the development and application of non-destructive neutron imaging and scattering techniques to ceramic and metallic nuclear fuels, ultimately also to irradiated fuels. The results of these characterizations provide complete pre- and post-irradiation on length scales ranging from mm to nm, guide destructive examination, and inform modelling efforts. Besides technique development and application to samples to be irradiated, the ANDE work package also examines possible technologies to provide these characterization techniques pool-side, e.g. at the Advanced Test Reactor (ATR) at Idaho National Laboratory (INL) using laser-driven intense pulsed neutron and gamma sources. Neutron tomography and neutron diffraction characterizations were performed on nine pellets; four UN/ U-Si composite formulations (two enrichment levels), three pure U₃Si₅ reference formulations (two enrichment levels), and two reject pellets with visible flaws (to qualify the technique). The ²³⁵U enrichments ranged from 0.2 to 8.8 wt. %. The nitride/silicide composites are candidate compositions for use as Accident Tolerant Fuel (ATF). The monophase U₃Si₅ material was included as a reference. Pellets from the same fabrication batches will be inserted in the Advanced Test Reactor at Idaho during 2016. We have also proposed a data format to build a database for characterization results of individual pellets. Neutron data reported in this report were collected in the LANSCE run cycle that started in September 2015 and ended in March 2016. This report provides the results for the characterized samples and discussion in the context of ANDE and APIE. We quantified the gamma spectra of several samples in their received state as well as after neutron irradiation to ensure that the neutron irradiation does not add significant activation that would complicate shipment and

Magnetic Non-destructive Testing of Plastically Deformed Mild Steel

Directory of Open Access Journals (Sweden)

Jozef Pala

2004-01-01

Full Text Available The Barkhausen noise analysis and coercive field measurement have been used as magnetic non-destructive testing methods for plastically deformed high quality carbon steel specimens. The strain dependence of root mean square value and power spectrum of the Barkhausen noise and the coercive field are explained in terms of the dislocation density. The specimens have been subjected to different magnetizing frequencies to show the overlapping nature of the Barkhausen noise. The results are discussed in the context of usage of magnetic non-destructive testing to evaluate the plastic deformation of high quality carbon steel products.

A Monte Carlo approach applied to ultrasonic non-destructive testing

Science.gov (United States)

Mosca, I.; Bilgili, F.; Meier, T.; Sigloch, K.

2012-04-01

Non-destructive testing based on ultrasound allows us to detect, characterize and size discrete flaws in geotechnical and architectural structures and materials. This information is needed to determine whether such flaws can be tolerated in future service. In typical ultrasonic experiments, only the first-arriving P-wave is interpreted, and the remainder of the recorded waveform is neglected. Our work aims at understanding surface waves, which are strong signals in the later wave train, with the ultimate goal of full waveform tomography. At present, even the structural estimation of layered media is still challenging because material properties of the samples can vary widely, and good initial models for inversion do not often exist. The aim of the present study is to combine non-destructive testing with a theoretical data analysis and hence to contribute to conservation strategies of archaeological and architectural structures. We analyze ultrasonic waveforms measured at the surface of a variety of samples, and define the behaviour of surface waves in structures of increasing complexity. The tremendous potential of ultrasonic surface waves becomes an advantage only if numerical forward modelling tools are available to describe the waveforms accurately. We compute synthetic full seismograms as well as group and phase velocities for the data. We invert them for the elastic properties of the sample via a global search of the parameter space, using the Neighbourhood Algorithm. Such a Monte Carlo approach allows us to perform a complete uncertainty and resolution analysis, but the computational cost is high and increases quickly with the number of model parameters. Therefore it is practical only for defining the seismic properties of media with a limited number of degrees of freedom, such as layered structures. We have applied this approach to both synthetic layered structures and real samples. The former contributed to benchmark the propagation of ultrasonic surface

Non-Destructive Techniques Based on Eddy Current Testing

Science.gov (United States)

García-Martín, Javier; Gómez-Gil, Jaime; Vázquez-Sánchez, Ernesto

2011-01-01

Non-destructive techniques are used widely in the metal industry in order to control the quality of materials. Eddy current testing is one of the most extensively used non-destructive techniques for inspecting electrically conductive materials at very high speeds that does not require any contact between the test piece and the sensor. This paper includes an overview of the fundamentals and main variables of eddy current testing. It also describes the state-of-the-art sensors and modern techniques such as multi-frequency and pulsed systems. Recent advances in complex models towards solving crack-sensor interaction, developments in instrumentation due to advances in electronic devices, and the evolution of data processing suggest that eddy current testing systems will be increasingly used in the future. PMID:22163754

Art, historical and cultural heritage objects studied with different non-destructive analysis

International Nuclear Information System (INIS)

Rizzutto, Marcia A.; Tabacniks, Manfredo H.; Added, Nemitala; Campos, Pedro H.O.V.; Curado, Jessica F.; Kajiya, Elizabeth A.M.

2012-01-01

Full text: Since 2003, the analysis of art, historical and cultural heritage objects has being performed at the Laboratorio de Analise de Materiais of the Instituto de Fisica of the Universidade de Sao Paulo (LAMFI-USP). Initially the studies were restricted to non-destructive methods using ion beams to characterize the chemical elements present in the objects. Recently, new analytical techniques and procedures have been incorporated to the better characterization of the objects and the examinations were expanded to other non-destructive analytical techniques such as portable X-Ray fluorescence (XRF), digitalized radiography, high resolution photography with visible, UV (ultraviolet) light and reflectography in the infrared region. These non-destructive analytical techniques systematically applied to the objects are helping the better understanding of these objects and allow studying them by examining their main components; their conservation status and also the creative process of the artist, particularly in easel paintings allow making new discoveries. The setup of the external beam in the LAMFI laboratory is configured to allow different simultaneous analysis by PIXE / PIGE (Particle Induced X-ray emission / Particle Induced gamma rays emission), RBS (Rutherford Backscattering) and IBL (Ion Beam Luminescence) and to expand the archaeometric results using ion beams. PIXE and XRF analysis are important to characterize the elements presents in the objects, pigments and others materials. The digitized radiography has provided important information about the internal structure of the objects, the manufacturing process, the internal particles existing and in case of easel paintings it can reveal features of the artist's creative process showing hidden images and the first paintings done by the artist in the background. Some Brazilian paintings studied by IR imaging revealed underlying drawings, which allowed us to discover the process of creation and also some

Art, historical and cultural heritage objects studied with different non-destructive analysis

Energy Technology Data Exchange (ETDEWEB)

Rizzutto, Marcia A.; Tabacniks, Manfredo H.; Added, Nemitala; Campos, Pedro H.O.V.; Curado, Jessica F.; Kajiya, Elizabeth A.M. [Universidade de Sao Paulo (IF/USP), SP (Brazil). Inst. de Fisica

2012-07-01

Full text: Since 2003, the analysis of art, historical and cultural heritage objects has being performed at the Laboratorio de Analise de Materiais of the Instituto de Fisica of the Universidade de Sao Paulo (LAMFI-USP). Initially the studies were restricted to non-destructive methods using ion beams to characterize the chemical elements present in the objects. Recently, new analytical techniques and procedures have been incorporated to the better characterization of the objects and the examinations were expanded to other non-destructive analytical techniques such as portable X-Ray fluorescence (XRF), digitalized radiography, high resolution photography with visible, UV (ultraviolet) light and reflectography in the infrared region. These non-destructive analytical techniques systematically applied to the objects are helping the better understanding of these objects and allow studying them by examining their main components; their conservation status and also the creative process of the artist, particularly in easel paintings allow making new discoveries. The setup of the external beam in the LAMFI laboratory is configured to allow different simultaneous analysis by PIXE / PIGE (Particle Induced X-ray emission / Particle Induced gamma rays emission), RBS (Rutherford Backscattering) and IBL (Ion Beam Luminescence) and to expand the archaeometric results using ion beams. PIXE and XRF analysis are important to characterize the elements presents in the objects, pigments and others materials. The digitized radiography has provided important information about the internal structure of the objects, the manufacturing process, the internal particles existing and in case of easel paintings it can reveal features of the artist's creative process showing hidden images and the first paintings done by the artist in the background. Some Brazilian paintings studied by IR imaging revealed underlying drawings, which allowed us to discover the process of creation and also some

Non-destructive qualification tests for ITER cryogenic axial insulating breaks

International Nuclear Information System (INIS)

Kosek, Jacek; Lopez, Roberto; Tommasini, Davide; Rodriguez-Mateos, Felix

2014-01-01

In the ITER superconducting magnets the dielectric separation between the CICC (Cable-In-Conduit Conductors) and the helium supply pipes is made through the so-called insulating breaks (IB). These devices shall provide the required dielectric insulation at a 30 kV level under different types of stresses and constraints: thermal, mechanical, dielectric and ionizing radiations. As part of the R and D program, the ITER Organization launched contracts with industrial companies aimed at the qualification of the manufacturing techniques. After reviewing the main functional aspects, this paper describes and discusses the protocol established for non-destructive qualification tests of the prototypes

Non-destructive qualification tests for ITER cryogenic axial insulating breaks

Energy Technology Data Exchange (ETDEWEB)

Kosek, Jacek [Wroclaw University of Technology, Wybrzeze Wyspianskiego 27, 50-370 Wroclaw, Poland and CERN, Geneva 23,CH-1211 (Switzerland); Lopez, Roberto; Tommasini, Davide [CERN, Geneva 23,CH-1211 (Switzerland); Rodriguez-Mateos, Felix [CERN, Geneva 23,CH-1211, Switzerland and ITER Organization, Route de Vinon sur Verdon, 13115 Saint Paul lez Durance (France)

2014-01-29

In the ITER superconducting magnets the dielectric separation between the CICC (Cable-In-Conduit Conductors) and the helium supply pipes is made through the so-called insulating breaks (IB). These devices shall provide the required dielectric insulation at a 30 kV level under different types of stresses and constraints: thermal, mechanical, dielectric and ionizing radiations. As part of the R and D program, the ITER Organization launched contracts with industrial companies aimed at the qualification of the manufacturing techniques. After reviewing the main functional aspects, this paper describes and discusses the protocol established for non-destructive qualification tests of the prototypes.

Status report on the destructive and non-destructive examinations of U-bends removed from Trojan steam generator D

International Nuclear Information System (INIS)

Aspden, R.G.

1981-01-01

The last status report on the non-destructive examination of U-bends removed from Trojan steam generator D was dated July 7, 1980. As part of this activity, the measurement of wall thicknesses on selected U-bends was planned using an ultrasonic gage. These readings were not made because reproducible results could not be obtained using water as the coupling fluid which was necessary to avoid contamination. Three tubes from the same heat were selected for destructive examination at Westinghouse: one leaking U-bend (R1-C6) and two tubes with no indications (R1-C10 and R1-C22). Results of the examination procedure are presented. The non-destructive examination results from the July 7, 1980 report for 29 U-bends are included

Short time evaluation of metallic materials' fatigue potential combining destructive and non-destructive testing methods

International Nuclear Information System (INIS)

Starke, Peter; Wu, Haoran; Boller, Christian

2015-01-01

Fatigue of engineering structures is an issue from an engineering design point. The lifetime of materials being subject to repeated mechanical loads is limited. Different examples of failures and fateful air accidents have caused significant cost and claims to the operators as well as manufacturers in excess of fatalities. Criticality of failure increases with increasing age and the uncertainty of operational loads applied. In such a case a reassessment of a structural materials' condition is in big need should damage tolerance criteria still be met, being the essential ground rule for aeronautical structural design. It is therefore the challenging aim to use a metallic material's microstructure characterizing non-destructive testing (NDT) parameter or a combination of those as a parameter to be scanned over a defined surface of the component considered to more realistically characterize the damage condition and to use this information twofold: (a) to more precisely assess the structural component's residual life and (b) to feed the information recorded back into a specific database belonging to an approach named PHYBAL. The physically based fatigue life evaluation method (PHYBAL) is a short-time procedure for the evaluation of fatigue data based on a small number of fatigue tests performed on un-notched specimens only. This method significantly reduces the effort for experimentation in terms of time and cost by around 90 % and inhibits remarkable scientific as well as economic advantages. The paper highlights the high capability of PHYBAL as well as the suitability for assessing the residual life of aeronautical components also with respect to the application of this approach in the light of structural health monitoring issues.

Non-destructive testing of electronic component packages

International Nuclear Information System (INIS)

Anderle, C.

1975-01-01

A non-destructive method of investigating packaged parts of semiconductor components by X radiation is described and the relevant theoretical relations limiting this technique are derived. The application of the technique is demonstrated in testing several components. The described method is iNsimple and quick. (author)

Application of the Positron Lifetime Spectroscopy as Method of Non-Destructive Testing

OpenAIRE

Somieski , B.; Krause-Rehberg , R.; Salz , H.; Meyendorf , N.

1995-01-01

In order to show the suitability of the Positron Lifetime Spectroscopy (POLIS) as a method of Non-Destructive Testing (NDT) several iron alloys / steels were mechanically damaged (tensile stress, fatigue, creeping). The positron annihilation parameters show clear changes during all applied kinds of damage. After tensile stress as well as after creeping a homogeneous distribution of damage in the sample was detected. During the very first elastic cycle of a fatigue experiment, a change in the ...

Non destructive examination of UN / U-Si fuel pellets using neutrons (preliminary assessment)

Energy Technology Data Exchange (ETDEWEB)

Bourke, Mark Andrew [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Vogel, Sven C. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Voit, Stewart Lancaster [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Mcclellan, Kenneth James [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Losko, Adrian S. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Tremsin, Anton [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

2016-03-31

Tomographic imaging and diffraction measurements were performed on nine pellets; four UN/ U Si composite formulations (two enrichment levels), three pure U₃Si₅ reference formulations (two enrichment levels) and two reject pellets with visible flaws (to qualify the technique). The U-235 enrichments ranged from 0.2 to 8.8 wt.%. The nitride/silicide composites are candidate compositions for use as Accident Tolerant Fuel (ATF). The monophase U₃Si₅ material was included as a reference. Pellets from the same fabrication batches will be inserted in the Advanced Test Reactor at Idaho during 2016. The goal of the Advanced Non-destructive Fuel Examination work package is the development and application of non-destructive neutron imaging and scattering techniques to ceramic and metallic nuclear fuels. Data reported in this report were collected in the LANSCE run cycle that started in September 2015 and ended in March 2016. Data analysis is ongoing; thus, this report provides a preliminary review of the measurements and provides an overview of the characterized samples.

Characterization of airborne particulate matter in Santiago, Chile. Part 5: non-destructive determination by x-ray fluorescence

International Nuclear Information System (INIS)

Poblete, V.H.; Hurtado, O.; Toro, P.

1995-01-01

A procedure for non-destructive analysis of airborne particular matter using X ray fluorescence is presented. The elements Fe, Pb and Zn were determined and their concentration compared with the results reported by other techniques. The homogeneity of the distribution of Fe in the samples was investigated. (author). 4 refs, 5 figs

Non-destructive Preirradiation Assessment of UN / U-Si ''LANL1'' ATF formulation

International Nuclear Information System (INIS)

Vogel, Sven C.; Losko, Adrian Simon; Pokharel, Reeju; Ickes, Timothy Lee; Hunter, James F.; Brown, Donald William; Voit, Stewart Lancaster; Tremsin, Anton S.; Bourke, Mark Andrew; McClellan, Kenneth James

2016-01-01

The goal of the Advanced Non-destructive Fuel Examination (ANDE) work package is the development and application of non-destructive neutron imaging and scattering techniques to ceramic and metallic nuclear fuels, ultimately also to irradiated fuels. The results of these characterizations provide complete pre- and post-irradiation on length scales ranging from mm to nm, guide destructive examination, and inform modelling efforts. Besides technique development and application to samples to be irradiated, the ANDE work package also examines possible technologies to provide these characterization techniques pool-side, e.g. at the Advanced Test Reactor (ATR) at Idaho National Laboratory (INL) using laser-driven intense pulsed neutron and gamma sources. Neutron tomography and neutron diffraction characterizations were performed on nine pellets; four UN/ U-Si composite formulations (two enrichment levels), three pure U 3 Si 5 reference formulations (two enrichment levels), and two reject pellets with visible flaws (to qualify the technique). The 235 U enrichments ranged from 0.2 to 8.8 wt. %. The nitride/silicide composites are candidate compositions for use as Accident Tolerant Fuel (ATF). The monophase U 3 Si 5 material was included as a reference. Pellets from the same fabrication batches will be inserted in the Advanced Test Reactor at Idaho during 2016. We have also proposed a data format to build a database for characterization results of individual pellets. Neutron data reported in this report were collected in the LANSCE run cycle that started in September 2015 and ended in March 2016. This report provides the results for the characterized samples and discussion in the context of ANDE and APIE. We quantified the gamma spectra of several samples in their received state as well as after neutron irradiation to ensure that the neutron irradiation does not add significant activation that would complicate shipment and handling. We demonstrated synchrotron-based 3D X

Thermographic Non-Destructive Evaluation for Natural Fiber-Reinforced Composite Laminates

Directory of Open Access Journals (Sweden)

Hai Zhang

2018-02-01

Full Text Available Natural fibers, including mineral and plant fibers, are increasingly used for polymer composite materials due to their low environmental impact. In this paper, thermographic non-destructive inspection techniques were used to evaluate and characterize basalt, jute/hemp and bagasse fibers composite panels. Different defects were analyzed in terms of impact damage, delaminations and resin abnormalities. Of particular interest, homogeneous particleboards of sugarcane bagasse, a new plant fiber material, were studied. Pulsed phase thermography and principal component thermography were used as the post-processing methods. In addition, ultrasonic C-scan and continuous wave terahertz imaging were also carried out on the mineral fiber laminates for comparative purposes. Finally, an analytical comparison of different methods was given.

Application of ICT in the non-destructive inspection of explosive device

International Nuclear Information System (INIS)

Wang Zhe; Li Tiantuo; Liu Zhiqiang; Pei Zhihua; Wang Zhiping

2003-01-01

The inspection of explosive device is an important task in the store of the weapons. The technique of non-destructive examination with radial, especially the ICT, is an effective method. The paper mainly introduces the design and the theories on the inspection system and software system of the application of industrial ICT in the non-destructive examination of explosive device, and gives a reference to the work in such fields

Optical generation,detection and non-destructive testing applications of terahertz waves

Institute of Scientific and Technical Information of China (English)

ZHANG; Weili; LIANG; Dachuan; TIAN; Zhen; HAN; Jiaguang; GU; Jianqiang; HE; Mingxia; OUYANG; Chunmei

2016-01-01

Optoelectronic terahertz generation and detection play a key role in the applications of non-destructive testing,which involves different areas such as physics,biological,material science,imaging,explosions detection,astronomy applications,semiconductor technology and superconductiong electronics. In this article,we present a reviewof the principle and performance of typical terahertz sources,detectors and non-destructive testing applications. On this basis,the newdevelopment and trends of terahertz radiation detectors are also discussed.

NonDestructive Evaluation for Industrial & Development Applications

Energy Technology Data Exchange (ETDEWEB)

Hunter, James F. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

2016-10-12

Provide overview of weld inspection for Non-Destructive Testing at LANL. This includes radiography (RT/DR/CR/CT for x-ray & neutron sources), ultrasonic testing (UT/PAUT), dye penetrant inspection (PT), eddy current inspection (ET) and magnetic particle testing (MT). Facilities and capabilities for weld inspection will be summarized with examples.

Edward's sword? - A non-destructive study of a medieval king's sword

Science.gov (United States)

Segebade, Chr.

2013-04-01

Non-destructive and instrumental methods including photon activation analysis were applied in an examination of an ancient sword. It was tried to find indication of forgery or, if authentic, any later processing and alteration. Metal components of the hilt and the blade were analysed by instrumental photon activation. Non-destructive metallurgical studies (hardness measurements, microscopic microstructure analysis) are briefly described, too. The results of these investigations did not yield indication of non-authenticity. This stood in agreement with the results of stylistic and scientific studies by weapon experts.

Inspection with non destructive assay techniques of the aluminium coating of the TRIGA Mark III reactor vat

International Nuclear Information System (INIS)

Reyes A, A.I.; Gonzalez M, A.; Castaneda J, G.; Rivera M, H.; Sandoval G, I.

2001-01-01

In June 2000, the Reactor Department assigned to the Scientific Research Direction of the National Institute of Nuclear Research requested to the Non-destructive Assays Laboratory (LEND), assigned to the Materials Science Management, the inspection and measurement of thickness of the aluminium coating (liner) of the TRIGA Mark III reactor vat with non-destructive assay techniques, due to that the aluminium coating is exposed mainly to undergo slimming on its back side due to corrosion phenomena. Activity that was able to be carried out from april until august 2001. It is worth pointing out that this type of inspection with these techniques was realized by first time. The non-destructive assays (NDA) are techniques which use indirect physical methods for inspecting the sanitation of components in process or in service, for detect lack of continuity or defects which affect their quality or usefulness. The application of those do not alter the physical, chemical, mechanical or dimensional properties of the part subject of inspection. The results of the application of the ultrasound inspection techniques, industrial radiography and penetrating liquids are presented. (Author)

Advanced uses of radiation in non-destructive evaluation

International Nuclear Information System (INIS)

Baldev Raj; Viswanathan, B.; Venkataraman, B.

1998-01-01

The increasing demand for newer materials and stringency of specifications, have expanded the scope of advanced uses of radiation in non-destructive evaluation of materials and industrial components. This paper highlights the application of some of the advanced techniques of radiography and residual stress measurements, using x-ray diffraction, for materials characterisation and testing, based on the results obtained at the author's laboratory. The application of positron annihilation techniques based on the use of radioisotopes and high resolution gamma ray spectroscopy, is introduced as non-destructive tools for materials characterisation. Selective examples of significant results obtained using this technique, on the radiation damage and early stages of fatigue damage in technologically important steels are reviewed from recent works at the author's laboratory and elsewhere. The scope of application of charge particle based thin layer activation method is briefly outlined. (author)

Non-destructive testing; Examenes no destructivos

Energy Technology Data Exchange (ETDEWEB)

Calva, Mauricio; Loske, Achim [Instituto de Investigaciones Electricas, Cuernavaca (Mexico)

1988-12-31

The application of non-destructive testing (NDT) in several technical and industrial fields is pointed out, standing out its utilization in the detection of future failures without affecting the examined element. Likewise, the different types of NDTs and their processes, such as x-rays, ultrasoud, magnetic particles, induced currents, penetrating fluids, and optical means, are described. The Non-Destructive Tests Laboratory of the Instituto de Investigaciones Electricas (IIE), plans to create new and more reliable systems independent from the operator`s capacity, to contribute to fulfill the inspection and quality control needs of the generating Mexican power plants. [Espanol] Se senala la aplicacion de los examenes no destructivos (END) a diversos campos tecnicos e industriales, destacando su utilizacion en la deteccion de futuras fallas sin afectar el elemento examinado. Asimismo, se describen los diferentes tipos de END y sus procesos, tales como radiografia, ultrasonido, particulas magneticas, corrientes inducidas, liquidos penetrantes y metodos opticos. El Laboratorio de Pruebas no Destructivas, del Instituto de Investigaciones Electricas (IIE), planea crear sistemas novedosos mas confiables, que no dependan de la capacidad del operador, para contribuir a satisfacer las necesidades de inspeccion y control de calidad que se presentan en las plantas generadoras de energia mexicanas.

Non-destructive testing; Examenes no destructivos

Energy Technology Data Exchange (ETDEWEB)

Calva, Mauricio; Loske, Achim [Instituto de Investigaciones Electricas, Cuernavaca (Mexico)

1987-12-31

The application of non-destructive testing (NDT) in several technical and industrial fields is pointed out, standing out its utilization in the detection of future failures without affecting the examined element. Likewise, the different types of NDTs and their processes, such as x-rays, ultrasoud, magnetic particles, induced currents, penetrating fluids, and optical means, are described. The Non-Destructive Tests Laboratory of the Instituto de Investigaciones Electricas (IIE), plans to create new and more reliable systems independent from the operator`s capacity, to contribute to fulfill the inspection and quality control needs of the generating Mexican power plants. [Espanol] Se senala la aplicacion de los examenes no destructivos (END) a diversos campos tecnicos e industriales, destacando su utilizacion en la deteccion de futuras fallas sin afectar el elemento examinado. Asimismo, se describen los diferentes tipos de END y sus procesos, tales como radiografia, ultrasonido, particulas magneticas, corrientes inducidas, liquidos penetrantes y metodos opticos. El Laboratorio de Pruebas no Destructivas, del Instituto de Investigaciones Electricas (IIE), planea crear sistemas novedosos mas confiables, que no dependan de la capacidad del operador, para contribuir a satisfacer las necesidades de inspeccion y control de calidad que se presentan en las plantas generadoras de energia mexicanas.

Characterization of the mechanical properties of resected porcine organ tissue using optical fiber photoelastic polarimetry.

Science.gov (United States)

Hudnut, Alexa W; Babaei, Behzad; Liu, Sonya; Larson, Brent K; Mumenthaler, Shannon M; Armani, Andrea M

2017-10-01

Characterizing the mechanical behavior of living tissue presents an interesting challenge because the elasticity varies by eight orders of magnitude, from 50Pa to 5GPa. In the present work, a non-destructive optical fiber photoelastic polarimetry system is used to analyze the mechanical properties of resected samples from porcine liver, kidney, and pancreas. Using a quasi-linear viscoelastic fit, the elastic modulus values of the different organ systems are determined. They are in agreement with previous work. In addition, a histological assessment of compressed and uncompressed tissues confirms that the tissue is not damaged during testing.

Non-destructive control in nuclear construction

International Nuclear Information System (INIS)

Banus; Barbier; Launay

1978-01-01

Having recalled the characteristics of the fundamental components of the main primary circuit of nuclear boilers (900 MW) and the means appropriated for their control, it is recalled that the 'French Electricity Board's specifications and control rules' often prescribe more severe criteria than those existing in the U.S.A. Then practical examples of non-destructive controls concerning the steam generator end plates, vessel stainless steel linings, pump attachements, steam generator pipes are given [fr

Destructive and non-destructive tests for radioactive waste packages Task 3 Characterization of radioactive waste forms. A series of final reports (1985-89) No 43

International Nuclear Information System (INIS)

Odoj, R.

1991-01-01

On the basis of preliminary waste acceptance requirements quality control of radioactive waste has to be performed prior to interim storage or final disposal. The quality control can either be achieved by random tests on conditioned radioactive waste packages or by process qualification of the conditioning processes. One of the most important criteria is the activity of the radioactive waste product or packages. To get some first information on the waste package γ-spectrometric measurement is performed as non-destructive test. Besides the γ-emitting nuclides the α and β-emitting nuclides can be estimated by calculation if the waste was generated in nuclear power plants and the nuclide relations are known. If the non-destructive determination of nuclides is not sufficient or the non-radioactive content of the waste packages has to be identified sampling from the waste packages has to be performed. This can best be done by core drilling. To avoid the need of water for cooling the drill head, air cooled core drilling is investigated. As mixed wastes is not allowed for final disposal the determination of possible organic toxic materials like PCB, dioxin and furane-compounds in cemented wastes is conducted by GC-MS-investigations. For getting more knowledge in the field of process qualification concerning super compaction, instrumentation of the super compaction process is investigated and tested

Non-destructive Testing by Infrared Thermography Under Random Excitation and ARMA Analysis

Science.gov (United States)

Bodnar, J. L.; Nicolas, J. L.; Candoré, J. C.; Detalle, V.

2012-11-01

Photothermal thermography is a non-destructive testing (NDT) method, which has many applications in the field of control and characterization of thin materials. This technique is usually implemented under CW or flash excitation. Such excitations are not adapted for control of fragile materials or for multi-frequency analysis. To allow these analyses, in this article, the use of a new control mode is proposed: infrared thermography under random excitation and auto regressive moving average analysis. First, the principle of this NDT method is presented. Then, the method is shown to permit detection, with low energy constraints, of detachments situated in mural paintings.

Non-Destructive Techniques in the Tacis and Phare Nuclear Safety Programmes

International Nuclear Information System (INIS)

Bieth, Michel

2002-01-01

Decisions regarding the verification of design plant lifetime and potential license renewal periods involve a determination of the component and circuit condition. In Service Inspection of key reactor components becomes a crucial consideration for continued safe plant operation. The determination of the equipment properties by Non Destructive Techniques during periodic intervals is an important aspect of the assessment of fitness-for-service and safe operation of nuclear power plants The Tacis and Phare were established since 1991 by the European Union as support mechanisms through which projects could be identified and addressed satisfactorily. In Nuclear Safety, the countries mainly concerned are Russia, Ukraine, Armenia, and Kazakhstan for the Tacis programme, and Bulgaria, Czech Republic, Hungary, Slovak Republic, Lithuania, Romania and Slovenia for the Phare programme. The Tacis and Phare programs concerning the Nuclear Power Plants consist of: - On Site Assistance and Operational Safety, - Design Safety, - Regulatory Authorities, - Waste management, and are focused on reactor safety issues, contributing to the improvement in the safety of East European reactors and providing technology and safety culture transfer. The main parts of these programmes are related to the On-Site Assistance and to the Design Safety of VVER and RBMK Nuclear power plants where Non Destructive Techniques for In Service Inspection of the primary circuit components are addressed. (authors)

Synchrotron radiation microtomography of musical instruments: a non-destructive monitoring technique for insect infestations

Directory of Open Access Journals (Sweden)

Beatrice Bentivoglio-Ravasio

2011-08-01

Full Text Available X-ray computed tomography is becoming a common technique for the structural analysis of samples of cultural relevance, providing luthiers, art historians, conservators and restorators with a unique tool for the characterization of musical instruments. Synchrotron-radiation phase-contrast microtomography is an ideal technique for the non-destructive 3D analysis of samples where small lowabsorbing details such as larvae and eggs can be detected. We report results from the first feasibility studies performed at the Elettra synchrotron laboratory, where the 1494 organ by Lorenzo Gusnasco da Pavia has been studied. Together with important information about the structural conditions, the presence of xylophages could be detected and characterized.

Mathematical modelling of ultrasonic non-destructive evaluation

Directory of Open Access Journals (Sweden)

Larissa Ju Fradkin

2001-01-01

Full Text Available High-frequency asymptotics have been used at our Centre to develop codes for modelling pulse propagation and scattering in the near-field of the ultrasonic transducers used in NDE (Non-Destructive Evaluation, particularly of walls of nuclear reactors. The codes are hundreds of times faster than the direct numerical codes but no less accurate.

Simulated Performances of a Very High Energy Tomograph for Non-Destructive Characterization of large objects

Science.gov (United States)

Kistler, Marc; Estre, Nicolas; Merle, Elsa

2018-01-01

As part of its R&D activities on high-energy X-ray imaging for non-destructive characterization, the Nuclear Measurement Laboratory has started an upgrade of its imaging system currently implemented at the CEA-Cadarache center. The goals are to achieve a sub-millimeter spatial resolution and the ability to perform tomographies on very large objects (more than 100-cm standard concrete or 40-cm steel). This paper presentsresults on the detection part of the imaging system. The upgrade of the detection part needs a thorough study of the performance of two detectors: a series of CdTe semiconductor sensors and two arrays of segmented CdWO4 scintillators with different pixel sizes. This study consists in a Quantum Accounting Diagram (QAD) analysis coupled with Monte-Carlo simulations. The scintillator arrays are able to detect millimeter details through 140 cm of concrete, but are limited to 120 cm for smaller ones. CdTe sensors have lower but more stable performance, with a 0.5 mm resolution for 90 cm of concrete. The choice of the detector then depends on the preferred characteristic: the spatial resolution or the use on large volumes. The combination of the features of the source and the studies on the detectors gives the expected performance of the whole equipment, in terms of signal-over-noise ratio (SNR), spatial resolution and acquisition time.

Non-invasive and non-destructive measurements of confluence in cultured adherent cell lines.

Science.gov (United States)

Busschots, Steven; O'Toole, Sharon; O'Leary, John J; Stordal, Britta

2015-01-01

Many protocols used for measuring the growth of adherent monolayer cells in vitro are invasive, destructive and do not allow for the continued, undisturbed growth of cells within flasks. Protocols often use indirect methods for measuring proliferation. Microscopy techniques can analyse cell proliferation in a non-invasive or non-destructive manner but often use expensive equipment and software algorithms. In this method images of cells within flasks are captured by photographing under a standard inverted phase contract light microscope using a digital camera with a camera lens adaptor. Images are analysed for confluence using ImageJ freeware resulting in a measure of confluence known as an Area Fraction (AF) output. An example of the AF method in use on OVCAR8 and UPN251 cell lines is included. •Measurements of confluence from growing adherent cell lines in cell culture flasks is obtained in a non-invasive, non-destructive, label-free manner.•The technique is quick, affordable and eliminates sample manipulation.•The technique provides an objective, consistent measure of when cells reach confluence and is highly correlated to manual counting with a haemocytometer. The average correlation co-efficient from a Spearman correlation (n = 3) was 0.99 ± 0.008 for OVCAR8 (p = 0.01) and 0.99 ± 0.01 for UPN251 (p = 0.01) cell lines.

234Th distributions in coastal and open ocean waters by non-destructive β-counting

International Nuclear Information System (INIS)

Miller, L.A.; Svaeren, I.

2003-01-01

Non-destructive β-counting analyses of particulate and dissolved 234 Th activities in seawater are simpler but no less precise than traditional radioanalytical methods. The inherent accuracy limitations of the non-destructive β-counting method, particularly in samples likely to be contaminated with anthropogenic nuclides, are alleviated by recounting the samples over several half-lives and fitting the counting data to the 234 Th decay curve. Precision (including accuracy, estimated at an average of 3%) is better than 10% for particulate or 5% for dissolved samples. Thorium-234 distributions in the Skagerrak indicated a vigorous, presumably biological, particle export from the surface waters, and while bottom sediment resuspension was not an effective export mechanism, it did strip thorium from the dissolved phase. In the Greenland and Norwegian Seas, we saw clear evidence of particulate export from the surface waters, but at 75 m, total 234 Th activities were generally in equilibrium with 238 U. (author)

Non-destructive testing and radiation in industry

International Nuclear Information System (INIS)

Woodford, C; Ashby, P.

2001-01-01

Non-destructive testing (NDT) is a little known discipline which uses non-invasive and passive techniques to investigate the condition of materials and structures. Some of these techniques employ the use of radioisotopes. The penetrating radiations produced by these materials are applied in various ways to obtain the required information. This presentation is an overview of the application of radioisotopes within the scope of NDT. Notwithstanding the well established use of traditional materials, new forms of radioisotopes are being developed which will extend their capabilities

Non-destructive investigation of a time capsule using neutron radiography and X-ray fluorescence

Energy Technology Data Exchange (ETDEWEB)

MacDonald, B.L., E-mail: macdonbl@mcmaster.ca [McMaster University, Department of Medical Physics and Applied Radiation Sciences, Hamilton (Canada); Vanderstelt, J., E-mail: joshv@nray.ca [Nray Services Inc., 56A Head Street, Dundas, ON (Canada); O’Meara, J. [University of Guelph, Department of Physics, Guelph (Canada); McNeill, F.E. [McMaster University, Department of Medical Physics and Applied Radiation Sciences, Hamilton (Canada)

2016-01-15

Non-destructive analytical techniques are becoming increasingly important for the study of objects of cultural heritage interest. This study applied two techniques: X-ray fluorescence and neutron radiography, for the investigation of a capped, tubular metal object recovered from an urban construction site in Gore Park, Hamilton, Canada. The site is an urban park containing a World War I commemorative monument that underwent renovation and relocation. Historical documentation suggested that the object buried underneath the monument was a time capsule containing a paper document listing the names of 1800 Canadians who died during WWI. The purpose of this study was to assess the condition of the object, and to verify if it was what the historical records purported. XRF analysis was used to characterize the elemental composition of the metal artifact, while neutron radiography revealed that its contents were congruent with historical records and remained intact after being interred for 91 years. Results of this study demonstrate the value of non-destructive techniques for the analysis and preservation of cultural heritage.

Non-destructive investigation of a time capsule using neutron radiography and X-ray fluorescence

Science.gov (United States)

MacDonald, B. L.; Vanderstelt, J.; O'Meara, J.; McNeill, F. E.

2016-01-01

Non-destructive analytical techniques are becoming increasingly important for the study of objects of cultural heritage interest. This study applied two techniques: X-ray fluorescence and neutron radiography, for the investigation of a capped, tubular metal object recovered from an urban construction site in Gore Park, Hamilton, Canada. The site is an urban park containing a World War I commemorative monument that underwent renovation and relocation. Historical documentation suggested that the object buried underneath the monument was a time capsule containing a paper document listing the names of 1800 Canadians who died during WWI. The purpose of this study was to assess the condition of the object, and to verify if it was what the historical records purported. XRF analysis was used to characterize the elemental composition of the metal artifact, while neutron radiography revealed that its contents were congruent with historical records and remained intact after being interred for 91 years. Results of this study demonstrate the value of non-destructive techniques for the analysis and preservation of cultural heritage.

Non-destructive testing: significant facts

International Nuclear Information System (INIS)

Espejo, Hector; Ruch, Marta C.

2006-01-01

In the last fifty years different organisations, both public and private, have been assigned to the mission of introducing into the country the most relevant aspects of the modern technological discipline 'Non Destructive Testing' (NDT) through a manifold of activities, such as training and education, research, development, technical assistance and services, personnel qualification/certification and standardisation. A review is given of the significant facts in this process, in which the Argentine Atomic Energy Commission, CNEA, played a leading part, a balance of the accomplishments is made and a forecast of the future of the activity is sketched. (author) [es

Development of non-destructive testing. Turkey

International Nuclear Information System (INIS)

1991-01-01

A National Scheme for the qualification and certification of Non-Destructive Testing (NDT) personnel in various methods has been established as the first stage of implementation. Systematic training in such methods as radiography (RT), ultrasonics (UT), magnetic particles (MT), liquid penetrant (PT) and eddy currents (ET) at levels I, II and some at III has been initiated and should be continued. Direct link with the industry and continuous effort to extend practical applications is strongly recommended

Combined Mechanical Destruction and Alkaline Pretreatment of Wheat Straw for Enhanced Enzymatic Saccharification

Directory of Open Access Journals (Sweden)

Qianqian Wang

2014-09-01

Full Text Available Wheat straw was pretreated by combined mechanical destruction and alkaline pretreatments to enhance enzymatic saccharification. Four strategies were employed to evaluate the potential of wheat straw as a feedstock for fermentable sugar production. The effects of the pretreatments on the substrate morphology, size distribution, chemical composition, and cellulose crystallinity, along with the subsequent enzymatic digestibility, were investigated. Optical microscope images showed that mechanical pretreatment alone resulted in poor fiber defibrillation, wherein samples mostly consisted of rigid fiber bundles, while integrated mechanical destruction and alkaline pretreatment led to relatively good fiber defibrillation. Low temperature NaOH/urea pretreatment can fibrillate the rigid fiber bundles into a relatively loose network and alter the structure of the treated substrate to make cellulose more accessible. The glucan conversion rates were 77% and 95% for integrated mechanical destruction and alkaline pretreatments and mechanical destruction followed by low temperature NaOH/urea and ammonium/urea pretreatments, respectively, after 72 h of enzymatic hydrolysis with enzyme loadings of 10 FPU cellulase per g of oven-dry substrate.

Application of the positron lifetime spectroscopy as method of non-destructive testing

International Nuclear Information System (INIS)

Somieski, B.; Krause-Rehberg, R.; Salz, H.; Meyendorf, N.

1995-01-01

In order to show the suitability of the Positron Lifetime Spectroscopy (POLIS) as a method of Non-Destructive Testing (NDT) several iron alloys/steels were mechanically damaged (tensile stress, fatigue, creeping). The positron annihilation parameters show clear changes during all applied kinds of damage. After tensile stress as well as after creeping a homogeneous distribution of damage in the sample was detected. During the very first elastic cycle of a fatigue experiment, a change in the defect structure occurs in well annealed materials. A modified spectrometer for in the field mapping is presented. (orig.)

Non destructive analysis apparatus by eddy currents for non magnetic metallic products

International Nuclear Information System (INIS)

Coutanceau-Monteil, N.; Billy, F.; Bernard, A.

1993-01-01

The device for non destructive testing of nonmagnetic metallic surfaces uses eddy currents with two independent receptors at different positions around the emitting coil which is fed with current impulses and whose axis is parallel to the surface under study. 4 figs

Utilization of radiation in non destructive tests

International Nuclear Information System (INIS)

Lopes, R.T.; Jesus, E.F.O. de; Junqueira, M.M.; Matos, J.A. de; Castello Branco, L.M.; Barros Junior, J.D.; Borges, J.C.

1987-01-01

The Nuclear Instrumentation Laboratory from COPPE/UFRJ has been developed techniques for using nuclear radiations to obtain images for non-destructive materials testing and medicine. With this objective, some prototypes of transmission computerized tomography systems using parallel beans and fan beans, with computer automation, including the mathematical process of image reprocessing and presentation in videos or printers are constructed [pt

Influence of Kaolin in Fly Ash Based Geopolymer Concrete: Destructive and Non-Destructive Testing

Science.gov (United States)

Yahya, Z.; Abdullah, M. M. A. B.; Ramli, N. Mohd; Burduhos-Nergis, D. D.; Razak, R. Abd

2018-06-01

Development of geopolymer concrete is mainly to reduce the production of ordinary Portland cement (OPC) that adverse the natural effect. Fly ash is a by-product collected from electrical generating power plant which resulted from burning pulverized coal. Since fly ash is waste materials, it can be recycled for future advantages particularly as pozzolanic materials in construction industry. This study focused on the feasibility of fly ash based geopolymer concrete to which kaolin has been added. The main constituents of geopolymer production for this study were class F fly ash, sodium silicate and sodium hydroxide (NaOH) solution. The concentration of NaOH solution was fixed at 12 Molar, ratio of fly ash/alkaline activator and sodium silicate/NaOH fixed at 1.5 and 2.5, respectively. Kaolin was added in range 5% to 15% from the mass of fly ash and all the samples were cured at room temperature. Destructive and non-destructive test were performed on geopolymer concrete to evaluate the best mix proportions that yield the highest strength as well as the quality of the concrete. Compressive strength, flexural strength, rebound hammer and ultrasonic pulse velocity (UPV) result have been obtained. It shown that 5% replacement of kaolin contributed to maximum compressive strength and flexural strength of 40.4 MPa and 12.35 MPa at 28 days. These result was supported by non-destructive test for the same mix proportion.

Developments in non-destructive beam diagnostics

International Nuclear Information System (INIS)

Fraser, J.S.

1981-01-01

With the large average beam currents being achieved in accelerators and storage rings, there is an increasing need for non-destructive beam diagnostic devices. For continuous beams, position monitors of the capacitive pick-up type are replaced by resonant devices that respond to the transverse displacement of the beam centroid. Bunch length monitors of the SLAC type using resonant cavities operating in the TM 010 mode can be used for continuous beams. The more detailed information derivable from beam profile scanners requires development of improved non-destructive devices. Profile monitors which scan the visible light produced by high current beams may be more reliable than ones using the residual ionization if the light intensity from gas molecules following nonionizing collisions with beam particles gives a measure of the beam current density independent of the local electron density. The intense Balmer series lines from neutral hydrogen beams have been used successfully to measure beam profiles. At CRNL and at LASL, beam light profile monitors are being developed for high average current accelerators. Three or more projections will be recorded to allow tomographic reconstruction of the two-dimensional beam current density. Light detection is either by intensified Reticons or ISIT vidicons. The use of three or more beam light monitors on a beam transport line will also permit estimates of the transverse emittance to be made through the reconstruction technique

On the systems of automatic non-destructive control of NPP metallic structures

International Nuclear Information System (INIS)

Grebennik, V.S.; Lantukh, V.M.

1980-01-01

The main stages of developing automatic systems of non- destructive control (NC) of NPP metallic structures are pointed out. The main requirements for automatic NC systems are formulated. Recommendations on the use of the developed experimental automatic facilities for control of certain NPP components are given. It is noted that the present facilities may be used in the future in development of modular sets of non-destructive control systems [ru

Mechanism of radiation destruction of dyes in polymers

International Nuclear Information System (INIS)

Belichenko, A.S.; Dyumaev, K.M.; Maslyukov, A.P.; Matyushin, G.A.; Nechitailo, V.S.

1991-01-01

Considering the experimental results, it might be expected that the mechanism of radiation destruction of dyed polymers by UV-and γ-irradiation should also be associated with a chemical reaction between dye molecules and oxyradicals which appear either on destruction of polymer macromolecules or on oxidation of macroradicals by the oxygen dissolved in the matrix. Thus, the radiation stability of dyes should depend on the rate of formation of primary radicals in the polymer under the action of UV- and γ-irradiation. As has been demostrated, this rate can be influenced by 'resonant' low-molecular additives which perform oscillative cross-relaxation. (author) 8 refs.; 2 figs

Non destructive testing of green parts in powder metallurgy

International Nuclear Information System (INIS)

Accary, A.

1979-01-01

The non destructive testing of green parts is potentially advantageous by making possible a lowering of the material and energy consumption as well as the production of parts with a 100% reliability. After a survey of the possible methods and of the defects to be detected it is shown that the goal can be achieved using a 'blind detection' method and that the difficulty of the problem depends on the size and shape of the part to be controled. The gravimetric, dimensional, γ absorption and thermal diffusivity methods are then examined. It is concluded that a unit control is paying only if it allows to enter the high reliability part market. Used statisticaly the non destructive testing of green parts can possibly lead to savings on materials and energy [fr

Safeguards and Non-destructive Assay

International Nuclear Information System (INIS)

Carchon, R.; Bruggeman, M.

2001-01-01

SCK-CEN's programme on safeguards and non-destructive assay includes: (1) various activities to assure nuclear materials accountancy; (2) contributes to the implementation of Integrated Safeguards measures in Belgium and to assist the IAEA through the Belgian Support Programme; (3) renders services to internal and external customers in the field of safeguards; (4) improves passive neutron coincidence counting techniques for waste assay and safeguards verification measurements by R and D on correlation algorithms implemented via software or dedicated hardware; (5) improves gamma assay techniques for waste assay by implementing advanced scanning techniques and different correlation algorithms; and (6) develops numerical calibration techniques. Major achievements in these areas in 2000 are reported

Non-destructive controls in the steel tube industry

International Nuclear Information System (INIS)

Mondot, J.

1978-01-01

The main non-destructive control methods in the tube industry are reviewed: eddy currents, particularly well adapted to small tubes; magnetoscopic testing for weldless tubes; ultrasonic waves widely used for thick weldless tubes and weldings; radiography, to examine tube ends and the known questionable zones; measure of diameters by laser [fr

Laser plasma X-ray for non-destructive inspection

International Nuclear Information System (INIS)

Yagi, T.; Kusama, H.

1995-01-01

External electric field is applied to the laser produced plasma, and its found that plasma shape in soft X-ray region is changed due to the penetrating electric field. The plasma emits strong hard X-ray, which can be used as a compact light source for non-destructive inspection. (author)

Mechanical properties of MEMS materials: reliability investigations by mechanical- and HRXRD-characterization related to environmental testing

Science.gov (United States)

Bandi, T.; Shea, H.; Neels, A.

2014-06-01

The performance and aging of MEMS often rely on the stability of the mechanical properties over time and under harsh conditions. An overview is given on methods to investigate small variations of the mechanical properties of structural MEMS materials by functional characterization, high-resolution x-ray diffraction methods (HR-XRD) and environmental testing. The measurement of the dynamical properties of micro-resonators is a powerful method for the investigation of elasticity variations in structures relevant to microtechnology. X-ray diffraction techniques are used to analyze residual strains and deformations with high accuracy and in a non-destructive manner at surfaces and in buried micro-structures. The influence of elevated temperatures and radiation damage on the performance of resonant microstructures with a focus on quartz and single crystal silicon is discussed and illustrated with examples including work done in our laboratories at CSEM and EPFL.

The non-destructive control, a major constituent of quality

International Nuclear Information System (INIS)

Anon.

1998-01-01

The number of continuous research and development works about non-destructive control in all sectors of activity is justified by the increasing need for high quality materials without anomalies. This paper gives a overview of the state of the art and of the recent trends in non-destructive testing researches in different sectors: aeronautics, nuclear industry, automotive industry. New studies and techniques are presented: ultrasonic testing of welds on large diameter pipes, automated applications of ultrasonic testing, ultrasound/computer-aided design coupling, pressure vessels inspection using acoustic emission testing (leaks detection, application to composite materials), numerical radiography (image visualisation and processing), magnetic testing (steel damage detection using Barkhausen noise testing), 'shearography' (detection of the loss of thickness in pipes due to corrosion), X-ray tomography (density measurement of sintered steels, fluid flow calculations in automobile parts). (J.S.)

Non-destructive evaluation of UV pulse laser-induced damage performance of fused silica optics.

Science.gov (United States)

Huang, Jin; Wang, Fengrui; Liu, Hongjie; Geng, Feng; Jiang, Xiaodong; Sun, Laixi; Ye, Xin; Li, Qingzhi; Wu, Weidong; Zheng, Wanguo; Sun, Dunlu

2017-11-24

The surface laser damage performance of fused silica optics is related to the distribution of surface defects. In this study, we used chemical etching assisted by ultrasound and magnetorheological finishing to modify defect distribution in a fused silica surface, resulting in fused silica samples with different laser damage performance. Non-destructive test methods such as UV laser-induced fluorescence imaging and photo-thermal deflection were used to characterize the surface defects that contribute to the absorption of UV laser radiation. Our results indicate that the two methods can quantitatively distinguish differences in the distribution of absorptive defects in fused silica samples subjected to different post-processing steps. The percentage of fluorescence defects and the weak absorption coefficient were strongly related to the damage threshold and damage density of fused silica optics, as confirmed by the correlation curves built from statistical analysis of experimental data. The results show that non-destructive evaluation methods such as laser-induced fluorescence and photo-thermal absorption can be effectively applied to estimate the damage performance of fused silica optics at 351 nm pulse laser radiation. This indirect evaluation method is effective for laser damage performance assessment of fused silica optics prior to utilization.

Online Preventative Non-Destructive Evaluation in Automated Fibre Placement

NARCIS (Netherlands)

Tonnaer, R.; Shroff, S.; Groves, R.M.

2016-01-01

The strict quality requirements for aerospace composite struc- tures give rise to costly quality control procedures. In automated bre placement (AFP) these procedures rely heavily on manual work and inspection. This research aims at performing preventative non-destructive evaluation of composite

Ionizing radiations for non-destructive evaluation

International Nuclear Information System (INIS)

Raj, Baldev; Venkataraman, B.

1989-01-01

A state of the art of major non-destructive testing (NDT) techniques based on ionising radiations is presented. These techniques are broadly classified into three categories, namely, radiography, radiation gaging and analytical applications. The basic principles behind each method are explained and salient features of each technique which make it suitable for a particular task are described. Several illustrative applications drawn from the nuclear industry are given. The monograph is intended to serve as an introductory guide to scientist and engineers engaged in NDT activities. (M.G.B.). 32 refs., 13 figs., 5 tabs

Characterization and source term assessments of radioactive particles from Marshall Islands using non-destructive analytical techniques

Science.gov (United States)

Jernström, J.; Eriksson, M.; Simon, R.; Tamborini, G.; Bildstein, O.; Marquez, R. Carlos; Kehl, S. R.; Hamilton, T. F.; Ranebo, Y.; Betti, M.

2006-08-01

Six plutonium-containing particles stemming from Runit Island soil (Marshall Islands) were characterized by non-destructive analytical and microanalytical methods. Composition and elemental distribution in the particles were studied with synchrotron radiation based micro X-ray fluorescence spectrometry. Scanning electron microscope equipped with energy dispersive X-ray detector and with wavelength dispersive system as well as a secondary ion mass spectrometer were used to examine particle surfaces. Based on the elemental composition the particles were divided into two groups: particles with pure Pu matrix, and particles where the plutonium is included in Si/O-rich matrix being more heterogenously distributed. All of the particles were identified as nuclear fuel fragments of exploded weapon components. As containing plutonium with low 240Pu/ 239Pu atomic ratio, less than 0.065, which corresponds to weapons-grade plutonium or a detonation with low fission yield, the particles were identified to originate from the safety test and low-yield tests conducted in the history of Runit Island. The Si/O-rich particles contained traces of 137Cs ( 239 + 240 Pu/ 137Cs activity ratio higher than 2500), which indicated that a minor fission process occurred during the explosion. The average 241Am/ 239Pu atomic ratio in the six particles was 3.7 × 10 - 3 ± 0.2 × 10 - 3 (February 2006), which indicated that plutonium in the different particles had similar age.

Challenges of Non-Destructive Assay Waste Measurement

International Nuclear Information System (INIS)

Shull, A.H.

2003-01-01

Historically, the Savannah River Site (SRS) routinely produced special nuclear material (SNM), which provided stable measurement conditions for the non-destructive assay (NDA) methods. However, the main mission of SRS has changed from the production of SNM to the processing of waste and material stabilization. Currently, the purpose of processing is to recover the SNM from the waste and stabilization materials, much of which is from other DOE facilities. These missions are usually of a short duration, but require non-destructive assay (NDA) accountability measurements on materials of varying composition and geometric configuration. These missions usually have cost and time constraints, which sometimes require re-application of existing NDA methods to waste measurements. Usually, each new material or re-application of the NDA method to a different SNM campaign requires new standards and timely re-calibration of the method. These constraints provide numerous challenges for the NDA methods, particularly in the area of measurement uncertainty. This paper will discuss the challenges of these situations, mainly from a measurement and statistical point of view and provide some possible solutions to the problems encountered. Specific examples will be discussed for the segmented gamma scanner (SGS), neutron multiplicity counter (NMC) and passive neutron coincidence counter (PNCC), which are some of the most common NDA instruments at SRS

Non-destructive study of iron gall inks in manuscripts

Science.gov (United States)

Duh, Jelena; Krstić, Dragica; Desnica, Vladan; Fazinić, Stjepko

2018-02-01

The aim of this research is to establish an effective procedure of iron gall ink characterization using complementary non-destructive methods. By this, it is possible to better understand correlation of chemical composition of the inks and the state of preservation of iron gall ink manuscripts, as well as the effects of conservation treatment performed upon them. This study was undertaken on a bound 16th century manuscript comprised of different types of paper and ink from the National and University Library in Zagreb. Analytical methods used included Particle Induced X-ray Emission (PIXE) and X-ray Fluorescence (XRF). Paper fibers were identified by optical microscopy and the degradation state, as well as ink differentiation, transit metal migrations and detection of stains, with ultraviolet (UV) and infrared (IR) photography. The techniques applied on original writing materials gave important information about paper and ink composition, its preservation state and efficiency of conservation treatment performed upon them.

Non-destructive Faraday imaging of dynamically controlled ultracold atoms

DEFF Research Database (Denmark)

Gajdacz, Miroslav; Pedersen, Poul Lindholm; Mørch, Troels

2013-01-01

We describe an easily implementable method for non-destructive measurements of ultracold atomic clouds based on dark field imaging of spatially resolved Faraday rotation. The signal-to-noise ratio is analyzed theoretically and, in the absence of experimental imperfections, the sensitivity limit...

Visualization of Tooth for Non-Destructive Evaluation from CT Images

Energy Technology Data Exchange (ETDEWEB)

Gao, Hui; Chae, Ok Sam [Kyung Hee University, Seoul (Korea, Republic of)

2009-06-15

This paper reports an effort to develop 3D tooth visualization system from CT sequence images as a part of the non-destructive evaluation suitable for the simulation of endodontics, orthodontics and other dental treatments. We focus on the segmentation and visualization for the individual tooth. In dental CT images teeth are touching the adjacent teeth or surrounded by the alveolar bones with similar intensity. We propose an improved level set method with shape prior to separate a tooth from other teeth as well as the alveolar bones. Reconstructed 3D model of individual tooth based on the segmentation results indicates that our technique is a very conducive tool for tooth visualization, evaluation and diagnosis. Some comparative visualization results validate the non-destructive function of our method.

Rapid and non-destructive discrimination of tea varieties by near ...

African Journals Online (AJOL)

Rapid and non-destructive discrimination of tea varieties by near infrared diffuse reflection spectroscopy coupled with classification and regression trees. SM Tan, RM Luo, YP Zhou, H Gong, Z Tan ...

Laser ultrasonics for civil engineering : some applications in development for concrete non destructive testing

International Nuclear Information System (INIS)

Abraham, O; Cottineau, L-M; Durand, O; Popovics, J S

2011-01-01

Non destructive testing of civil engineering infrastructures is becoming of primary importance for their diagnosis, residual time life estimation and/or structural health monitoring. A particularity of civil engineering application is the large size of the survey zones and the expected low cost of inspection. In this context non contact ultrasonics may offer the possibility to built robots that can automatically scan large areas (or eventually be integrated in moving vehicles) to recover mechanical properties of material or to perform imagery for geometrical information recovery. In this paper we present two possible applications of in situ laser ultrasonics : one is the detection of voids in tendon duct with the impact echo method, the other is the use of surface waves to recover mechanical properties of the first centimetres of concrete structures (here after called cover concrete).

Mechanics of ultrasound elastography

Science.gov (United States)

Li, Guo-Yang

2017-01-01

Ultrasound elastography enables in vivo measurement of the mechanical properties of living soft tissues in a non-destructive and non-invasive manner and has attracted considerable interest for clinical use in recent years. Continuum mechanics plays an essential role in understanding and improving ultrasound-based elastography methods and is the main focus of this review. In particular, the mechanics theories involved in both static and dynamic elastography methods are surveyed. They may help understand the challenges in and opportunities for the practical applications of various ultrasound elastography methods to characterize the linear elastic, viscoelastic, anisotropic elastic and hyperelastic properties of both bulk and thin-walled soft materials, especially the in vivo characterization of biological soft tissues. PMID:28413350

Resonant ultrasound spectroscopy and non-destructive testing

Science.gov (United States)

Migliori, A.; Darling, T. W.

The use of mechanical resonances to test properties of materials is perhaps older than the industrial revolution. Early documented cases of British railroad engineers tapping the wheels of a train and using the sound to detect cracks perhaps mark the first real use of resonances to test the integrity of high-performance alloys. Attempts were made in the following years to understand the resonances of solids mathematically, based on the shape and composition. But Nobel Laureate Lord Rayleigh best summarized the state of affairs in 1894, stating 'the problem has, for the most part, resisted attack'. More recently, modern computers and electronics have enabled Anderson and co-workers with their work on minerals, and our work at Los Alamos on new materials and manufactured components to advance the use of resonances to a precision non-destructive testing tool that makes anisotropic modulus measurements, defect detection and geometry error detection routine. The result is that resonances can achieve the highest absolute accuracy for any dynamic modulus measurement technique, can be used on the smallest samples, and can also enable detection of errors in certain classes of precision manufactured components faster and more accurately than any other technique.

Signal processing for non-destructive testing of railway tracks

Science.gov (United States)

Heckel, Thomas; Casperson, Ralf; Rühe, Sven; Mook, Gerhard

2018-04-01

Increased speed, heavier loads, altered material and modern drive systems result in an increasing number of rail flaws. The appearance of these flaws also changes continually due to the rapid change in damage mechanisms of modern rolling stock. Hence, interpretation has become difficult when evaluating non-destructive rail testing results. Due to the changed interplay between detection methods and flaws, the recorded signals may result in unclassified types of rail flaws. Methods for automatic rail inspection (according to defect detection and classification) undergo continual development. Signal processing is a key technology to master the challenge of classification and maintain resolution and detection quality, independent of operation speed. The basic ideas of signal processing, based on the Glassy-Rail-Diagram for classification purposes, are presented herein. Examples for the detection of damages caused by rolling contact fatigue also are given, and synergetic effects of combined evaluation of diverse inspection methods are shown.

Non-destructive testing of rocket fuse by thermal neutron radiography

International Nuclear Information System (INIS)

An Fulin; Li Furong

1999-01-01

A neutron radiography system in reactor horizontal hole of Tsinghua University was introduced, and its capability of neutron radiography was evaluated by theory and experiment, the non-destructive testing for rocket fuse is successful

Ultrasonic non-destructive testing on CFC monoblock divertor mock-up

International Nuclear Information System (INIS)

Ezato, K.; Taniguchi, M.; Sato, K.; Araki, M.; Akiba, M.

2001-01-01

Non-destructive ultrasonic testing has been applied for the characterization of joints by means of a polymer transducer. One of the advantages of the polymer transducer is flexibility in its shape and the possibility to install multiple transducers in one probe, which can reduce the time for inspection. As a first step, the size effect of the transducer on the resolution and sensitivity was examined to detect the joint flaw. Transducers with circumferential angles of 5 , 10 and 30 were tested. For this test a small divertor element with a driller hole was prepared, which simulates a joint defect. The transducers with angles of 30 could not characterize the size of the artificial joint flaw. On the contrary, the size of the artificial defect was successfully detected with an accuracy of 90% by means of the transducers with angles of 5 and 10 . From the viewpoint of the sensitivity of the detection of the joint flaw, the transducer with the angle of 10 is appropriate because it could detect the largest intensity of the reflected signal caused by the same artificial defect of the joint interface. (orig.)

Non-Destructive Investigation on Short Circuit Capability of Wind-Turbine-Scale IGBT Power Modules

DEFF Research Database (Denmark)

Wu, Rui; Iannuzzo, Francesco; Wang, Huai

2014-01-01

This paper presents a comprehensive investigation on the short circuit capability of wind-turbine-scale IGBT power modules by means of a 6 kA/1.1 kV non-destructive testing system. A Field Programmable Gate Array (FPGA) supervising unit is adpoted to achieve an accurate time control for short...... circuit test, which enables to define the driving signals with an accuracy of 10 ns. Thanks to the capability and the effectiveness of the constructed setup, oscillations appearing during short circuits of the new-generation 1.7 kV/1 kA IGBT power modules have been evidenced and characterized under...

Training guidelines in non-destructive testing techniques

International Nuclear Information System (INIS)

1987-02-01

With the conclusion in 1979 of a successful Agency executed UNDP project in Argentina, whose aim was the establishment of a national non-destructive testing centre, the Agency was asked by other countries in the Latin American and Caribbean Region to evaluate the possibility of transferring this success to the whole region. In 1982, with the financial cooperation of UNFSSTD and UNIDO, a regional project was started with the principal objective of assisting the countries in the region to reinforce autonomous NDT capability through regional cooperation. One essential component of this project has been the harmonization of training through the development and use of course syllabi by the 17 countries now participating in the project. To this end, a Regional Working Group was formed and one of its tasks is the development of these syllabi for the more common NDT methods. This publication is a collection of the training programmes elaborated to date which have so far been followed by some 10,000 persons in the region who have received training in NDT as a direct result of the project. These syllabi take into account the development work done by the International Committee for Non-destructive Testing and many national training programmes, and are meant to be an objective guide to assist in the formation of NDT personnel

Development and characterization of enhanced green fluorescent protein and luciferase expressing cell line for non-destructive evaluation of tissue engineering constructs.

NARCIS (Netherlands)

Blum, J.S.; Temenoff, J.S.; Park, H.; Jansen, J.A.; Mikos, A.G.; Barry, M.A.

2004-01-01

This study investigates the utility of genetically modified cells developed for the qualitative and quantitative non-destructive evaluation of cells on biomaterials. The Fisher rat fibroblastic cell line has been genetically modified to stably express the reporter genes enhanced green fluorescence

Application of microCT to the non-destructive testing of an additive manufactured titanium component

Directory of Open Access Journals (Sweden)

Anton du Plessis

2015-11-01

Full Text Available In this paper the application of X-ray microCT to the non-destructive testing of an additive manufactured titanium alloy component of complex geometry is demonstrated. Additive manufacturing of metal components is fast growing and shows great promise, yet these parts may contain defects which affect mechanical properties of the components. In this work a layered form of defect is found by microCT, which would have been very difficult or impossible to detect by other non-destructive testing methods due to the object complexity, defect size and shape and because the pores are entirely contained inside the object and not connected to the surface. Additionally, this test part was subjected to hot isostatic pressing (HIPPING and subsequently scanned. Comparing before and after scans by alignment of the volumes allows visualization and quantification of the pore size changes. The application of X-ray microCT to additive manufacturing is thus demonstrated in this example to be an ideal combination, especially for process improvements and for high value components.

Theoretical and practical program in the non-destructive testing by eddy currents - the first level

International Nuclear Information System (INIS)

Shaaban, H.I.; Addarwish, J.M.A.

2014-11-01

The testing using eddy currents is one of the non-destructive tests that use electromagnetic property as a basis for testing procedures, and there are many other ways to use this principle, including Remote Field Testing and the Magnetic Flux Leakage test. Eddy currents are electrical currents moving in a circular path, and took the name eddy of eddies that form when a liquid or gas is moving in a circular path because of objection obstacles to its track. They are generated in the material using a variable magnetic field. Non-destructive testing by eddy currents is a technique used for the detection of defects and interruptions in a material and it is a process that relies on the generation of small eddy currents in the material of the part to be examined, provided that this part is of an electrically conducting material. This technique and its scientific basis are explained in this book. Also the devices used in this technique and how to use these devices in details are explained. The book contains Twelve chapters: Introduction to non destructive testing - Engineering materials and its mechanical characteristics - Electrical and magnetic characteristics of engineering materials - Introduction to testing by eddy currents - Factors affecting eddy currents - Basis of electrical circuits used in eddy currents testing devices - Probes of eddy currents testing - Eddy currents testing devices (Theoretical) - Analysis of the examination results of testing by eddy currents: techniques and applications - Applications of testing by eddy currents - Eddy currents testing devices (Application) - Practical lessons for the first level in testing by eddy currents.

Evaluation of corrosion of prestressing steel in concrete using non-destructive techniques

International Nuclear Information System (INIS)

Ali, M.G.; Maddocks, A.R.

2003-01-01

Use of high strength steel in pre-stressed concrete structures has been in use in Australia for many decades. Highway bridges, among other structures, have extensively used pre-stress-ing and post-tensioning techniques. Although prestressing offers many competitive edges to it's traditional rival reinforced concrete, the consequence of damage to prestressing tendons could be catastrophic. Periodic visual inspections of prestressed concrete bridges throughout the world have demonstrated the growing problem of deterioration of prestressing steel as a result of corrosion. Early detection of damage to prestressing steel therefore is of paramount importance. Unfortunately no reliable and practical non-destructive evaluation technique has been available for assessing the condition of prestressing steel within concrete although a number of techniques appear promising. The following inspection methods have been highlighted in recent literature for their use as non-destructive inspection methods for prestressed concrete structures. In addition to the techniques discussed, a number of destructive, or invasive techniques also exist for determination of the corrosion status of prestressing tendons in prestressed structures. The following non-destructive techniques are discussed in some detail: Radiography; Computed Tomography; Surface Penetrating Radar; Impact Echo; Acoustic Emission Monitoring; Magnetic Field Disturbance Technique; Remnant Magnetism Method; Linear Polarisation Method; Electrical Resistance and Surface Potential Survey. The portability, limitations and use in Australia of these techniques are summarised in a table

Non-Destructive Thermography Analysis of Impact Damage on Large-Scale CFRP Automotive Parts

Science.gov (United States)

Maier, Alexander; Schmidt, Roland; Oswald-Tranta, Beate; Schledjewski, Ralf

2014-01-01

Laminated composites are increasingly used in aeronautics and the wind energy industry, as well as in the automotive industry. In these applications, the construction and processing need to fulfill the highest requirements regarding weight and mechanical properties. Environmental issues, like fuel consumption and CO2-footprint, set new challenges in producing lightweight parts that meet the highly monitored standards for these branches. In the automotive industry, one main aspect of construction is the impact behavior of structural parts. To verify the quality of parts made from composite materials with little effort, cost and time, non-destructive test methods are increasingly used. A highly recommended non-destructive testing method is thermography analysis. In this work, a prototype for a car’s base plate was produced by using vacuum infusion. For research work, testing specimens were produced with the same multi-layer build up as the prototypes. These specimens were charged with defined loads in impact tests to simulate the effect of stone chips. Afterwards, the impacted specimens were investigated with thermography analysis. The research results in that work will help to understand the possible fields of application and the usage of thermography analysis as the first quick and economic failure detection method for automotive parts. PMID:28788464

Non-Destructive Thermography Analysis of Impact Damage on Large-Scale CFRP Automotive Parts

Directory of Open Access Journals (Sweden)

Alexander Maier

2014-01-01

Full Text Available Laminated composites are increasingly used in aeronautics and the wind energy industry, as well as in the automotive industry. In these applications, the construction and processing need to fulfill the highest requirements regarding weight and mechanical properties. Environmental issues, like fuel consumption and CO2-footprint, set new challenges in producing lightweight parts that meet the highly monitored standards for these branches. In the automotive industry, one main aspect of construction is the impact behavior of structural parts. To verify the quality of parts made from composite materials with little effort, cost and time, non-destructive test methods are increasingly used. A highly recommended non-destructive testing method is thermography analysis. In this work, a prototype for a car’s base plate was produced by using vacuum infusion. For research work, testing specimens were produced with the same multi-layer build up as the prototypes. These specimens were charged with defined loads in impact tests to simulate the effect of stone chips. Afterwards, the impacted specimens were investigated with thermography analysis. The research results in that work will help to understand the possible fields of application and the usage of thermography analysis as the first quick and economic failure detection method for automotive parts.

Non-Destructive Thermography Analysis of Impact Damage on Large-Scale CFRP Automotive Parts.

Science.gov (United States)

Maier, Alexander; Schmidt, Roland; Oswald-Tranta, Beate; Schledjewski, Ralf

2014-01-14

Laminated composites are increasingly used in aeronautics and the wind energy industry, as well as in the automotive industry. In these applications, the construction and processing need to fulfill the highest requirements regarding weight and mechanical properties. Environmental issues, like fuel consumption and CO₂-footprint, set new challenges in producing lightweight parts that meet the highly monitored standards for these branches. In the automotive industry, one main aspect of construction is the impact behavior of structural parts. To verify the quality of parts made from composite materials with little effort, cost and time, non-destructive test methods are increasingly used. A highly recommended non-destructive testing method is thermography analysis. In this work, a prototype for a car's base plate was produced by using vacuum infusion. For research work, testing specimens were produced with the same multi-layer build up as the prototypes. These specimens were charged with defined loads in impact tests to simulate the effect of stone chips. Afterwards, the impacted specimens were investigated with thermography analysis. The research results in that work will help to understand the possible fields of application and the usage of thermography analysis as the first quick and economic failure detection method for automotive parts.

Characterization and source term assessments of radioactive particles from Marshall Islands using non-destructive analytical techniques

Energy Technology Data Exchange (ETDEWEB)

Jernstroem, J. [Laboratory of Radiochemistry, Department of Chemistry, P.O. Box 55, FI-00014 University of Helsinki (Finland)]. E-mail: jussi.jernstrom@helsinki.fi; Eriksson, M. [IAEA-MEL, International Atomic Energy Agency - Marine Environment Laboratory, 4 Quai Antoine 1er, MC 98000 Monaco (Monaco); Simon, R. [Institute for Synchrotron Radiation, Forschungszentrum Karlsruhe GmbH, D-76021 Karlsruhe (Germany); Tamborini, G. [European Commission, Joint Research Centre, Institute for Transuranium Elements, P.O. Box 2340, D-76125 Karlsruhe (Germany); Bildstein, O. [European Commission, Joint Research Centre, Institute for Transuranium Elements, P.O. Box 2340, D-76125 Karlsruhe (Germany); Marquez, R. Carlos [European Commission, Joint Research Centre, Institute for Transuranium Elements, P.O. Box 2340, D-76125 Karlsruhe (Germany); Kehl, S.R. [Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, CA 94551-0808 (United States); Hamilton, T.F. [Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, CA 94551-0808 (United States); Ranebo, Y. [European Commission, Joint Research Centre, Institute for Transuranium Elements, P.O. Box 2340, D-76125 Karlsruhe (Germany); Betti, M. [European Commission, Joint Research Centre, Institute for Transuranium Elements, P.O. Box 2340, D-76125 Karlsruhe (Germany)]. E-mail: maria.betti@ec.europa.eu

2006-08-15

Six plutonium-containing particles stemming from Runit Island soil (Marshall Islands) were characterized by non-destructive analytical and microanalytical methods. Composition and elemental distribution in the particles were studied with synchrotron radiation based micro X-ray fluorescence spectrometry. Scanning electron microscope equipped with energy dispersive X-ray detector and with wavelength dispersive system as well as a secondary ion mass spectrometer were used to examine particle surfaces. Based on the elemental composition the particles were divided into two groups: particles with pure Pu matrix, and particles where the plutonium is included in Si/O-rich matrix being more heterogenously distributed. All of the particles were identified as nuclear fuel fragments of exploded weapon components. As containing plutonium with low {sup 240}Pu/{sup 239}Pu atomic ratio, less than 0.065, which corresponds to weapons-grade plutonium or a detonation with low fission yield, the particles were identified to originate from the safety test and low-yield tests conducted in the history of Runit Island. The Si/O-rich particles contained traces of {sup 137}Cs ({sup 239+240}Pu/{sup 137}Cs activity ratio higher than 2500), which indicated that a minor fission process occurred during the explosion. The average {sup 241}Am/{sup 239}Pu atomic ratio in the six particles was 3.7 x 10{sup -3} {+-} 0.2 x 10{sup -3} (February 2006), which indicated that plutonium in the different particles had similar age.

Non-destructive beam profile monitor at HIMAC

International Nuclear Information System (INIS)

Sato, S.; Araki, N.; Hosaka, M.

1995-01-01

Non-destructive profile monitors (NDPM), based on micro-channel plate (MCP), have been developed and installed in both the synchrotron ring and high-energy beam transport (HEBT) line at HIMAC. Beam test using these monitors have been carried out since April of 1995 to investigate a change of vertical beam size in synchrotron and a possibility of observing beam with high energy by one pass. In this paper the measurement system is mainly reported, and the preliminary results are also briefly presented. (author)

Checking collagen preservation in archaeological bone by non-destructive studies (Micro-CT and IBA)

Science.gov (United States)

Beck, L.; Cuif, J.-P.; Pichon, L.; Vaubaillon, S.; Dambricourt Malassé, A.; Abel, R. L.

2012-02-01

The material to be studied is a piece of human skull discovered (1999) in Pleistocene sediments from the Orsang river (Gujarat state, India). From anatomical view point, this skull is highly composite: modern Homo sapiens characters are associated to undoubtedly more ancient features. Absolute dating by 14C is critical to understand this discovery. Prior to dating measurements, non-destructive studies have been carried out. Micro-CT reconstruction (X-ray microtomography) and Ion Beam Analysis (IBA) have been undertaken to check the structural preservation of the fossil and the collagen preservation. PIXE elemental map was used to select well-preserved bone area. RBS/EBS and NRA were used for light element quantification, in particular C, N and O contents. We also demonstrate that the PIXE-RBS/EBS combination is a effective tool for the whole characterization of archaeological and recent bones by analysing in one experiment both mineral and organic fractions. We have shown that the archaeological bone, a fragment of the potentially oldest modern Indian, is enough preserved for radiocarbon dating. We propose that Elastic Backscattering Spectrometry (EBS) using 3 MeV protons could be a good non destructive alternative to conventional CHN method using Carbon-Hydrogen-Nitrogen analyzer for measuring C and N before 14C dating.

Checking collagen preservation in archaeological bone by non-destructive studies (Micro-CT and IBA)

International Nuclear Information System (INIS)

Beck, L.; Cuif, J.-P.; Pichon, L.; Vaubaillon, S.; Dambricourt Malassé, A.; Abel, R.L.

2012-01-01

The material to be studied is a piece of human skull discovered (1999) in Pleistocene sediments from the Orsang river (Gujarat state, India). From anatomical view point, this skull is highly composite: modern Homo sapiens characters are associated to undoubtedly more ancient features. Absolute dating by 14 C is critical to understand this discovery. Prior to dating measurements, non-destructive studies have been carried out. Micro-CT reconstruction (X-ray microtomography) and Ion Beam Analysis (IBA) have been undertaken to check the structural preservation of the fossil and the collagen preservation. PIXE elemental map was used to select well-preserved bone area. RBS/EBS and NRA were used for light element quantification, in particular C, N and O contents. We also demonstrate that the PIXE-RBS/EBS combination is a effective tool for the whole characterization of archaeological and recent bones by analysing in one experiment both mineral and organic fractions. We have shown that the archaeological bone, a fragment of the potentially oldest modern Indian, is enough preserved for radiocarbon dating. We propose that Elastic Backscattering Spectrometry (EBS) using 3 MeV protons could be a good non destructive alternative to conventional CHN method using Carbon–Hydrogen–Nitrogen analyzer for measuring C and N before 14 C dating.

Checking collagen preservation in archaeological bone by non-destructive studies (Micro-CT and IBA)

Energy Technology Data Exchange (ETDEWEB)

Beck, L., E-mail: lucile.beck@cea.fr [C2RMF - UMR171 CNRS, Centre de Recherche et de Restauration des Musees de France, Palais du Louvre, Porte des Lions, 14 quai Francois Mitterrand, 75001 Paris (France); CEA, DEN, Service de Recherches de Metallurgie Physique, Laboratoire JANNUS, 91191 Gif-sur-Yvette (France); Cuif, J.-P. [UMR IDES 8148, Universite Paris XI-Orsay, 91405 Orsay cedex (France); Pichon, L. [C2RMF - UMR171 CNRS, Centre de Recherche et de Restauration des Musees de France, Palais du Louvre, Porte des Lions, 14 quai Francois Mitterrand, 75001 Paris (France); Vaubaillon, S. [CEA, INSTN, Laboratoire JANNUS, 91191 Gif-sur-Yvette (France); Dambricourt Malasse, A. [Departement de Prehistoire, Museum national d' Histoire naturelle, UMR 7194 - CNRS, Institut de Paleontologie Humaine, 1, rue Rene Panhard, 75013 Paris (France); Abel, R.L. [The Natural History Museum, London (United Kingdom)

2012-02-15

The material to be studied is a piece of human skull discovered (1999) in Pleistocene sediments from the Orsang river (Gujarat state, India). From anatomical view point, this skull is highly composite: modern Homo sapiens characters are associated to undoubtedly more ancient features. Absolute dating by {sup 14}C is critical to understand this discovery. Prior to dating measurements, non-destructive studies have been carried out. Micro-CT reconstruction (X-ray microtomography) and Ion Beam Analysis (IBA) have been undertaken to check the structural preservation of the fossil and the collagen preservation. PIXE elemental map was used to select well-preserved bone area. RBS/EBS and NRA were used for light element quantification, in particular C, N and O contents. We also demonstrate that the PIXE-RBS/EBS combination is a effective tool for the whole characterization of archaeological and recent bones by analysing in one experiment both mineral and organic fractions. We have shown that the archaeological bone, a fragment of the potentially oldest modern Indian, is enough preserved for radiocarbon dating. We propose that Elastic Backscattering Spectrometry (EBS) using 3 MeV protons could be a good non destructive alternative to conventional CHN method using Carbon-Hydrogen-Nitrogen analyzer for measuring C and N before {sup 14}C dating.

Non-destructive testing of tubes by electromagnetic processes

International Nuclear Information System (INIS)

Kowarski, A.

1979-01-01

This article reviews and assesses the non destructive testing techniques used for locating defects in tubes by electromagnetic processes. These form the basis of many testing devices, the diversity of which results from various factors: range of materials, methods of fabrication, specific defects of the product. There are two distinct main families of devices utilising two different principles: dispersion flow and Foucault currents [fr

Guidebook on non-destructive testing of concrete structures

International Nuclear Information System (INIS)

2002-01-01

The International Atomic Energy Agency has been active in the promotion of non-destructive testing (NDT) technology for many years. NDT is an important component of a number of IAEA regional projects. This guidebook deals with NDT of concrete. This book covers a wide range of NDT methods including industrial radiography, ultrasonic testing, electromagnetic testing, infrared thermography, etc. Codes, standards, specifications and procedures are also covered

A non-destructive method for estimating onion leaf area

Directory of Open Access Journals (Sweden)

Córcoles J.I.

2015-06-01

Full Text Available Leaf area is one of the most important parameters for characterizing crop growth and development, and its measurement is useful for examining the effects of agronomic management on crop production. It is related to interception of radiation, photosynthesis, biomass accumulation, transpiration and gas exchange in crop canopies. Several direct and indirect methods have been developed for determining leaf area. The aim of this study is to develop an indirect method, based on the use of a mathematical model, to compute leaf area in an onion crop using non-destructive measurements with the condition that the model must be practical and useful as a Decision Support System tool to improve crop management. A field experiment was conducted in a 4.75 ha commercial onion plot irrigated with a centre pivot system in Aguas Nuevas (Albacete, Spain, during the 2010 irrigation season. To determine onion crop leaf area in the laboratory, the crop was sampled on four occasions between 15 June and 15 September. At each sampling event, eight experimental plots of 1 m2 were used and the leaf area for individual leaves was computed using two indirect methods, one based on the use of an automated infrared imaging system, LI-COR-3100C, and the other using a digital scanner EPSON GT-8000, obtaining several images that were processed using Image J v 1.43 software. A total of 1146 leaves were used. Before measuring the leaf area, 25 parameters related to leaf length and width were determined for each leaf. The combined application of principal components analysis and cluster analysis for grouping leaf parameters was used to reduce the number of variables from 25 to 12. The parameter derived from the product of the total leaf length (L and the leaf diameter at a distance of 25% of the total leaf length (A25 gave the best results for estimating leaf area using a simple linear regression model. The model obtained was useful for computing leaf area using a non-destructive

Introduction to non-destructive testing of materials: part II

International Nuclear Information System (INIS)

Ahmed, M.; Ahmed, B.

2001-01-01

Ultrasonic waves are mechanical vibrations that require a medium, which functions as carrier. Ultrasonics are widely used in non-destructive testing of materials in which high frequency sound waves are introduced into the material being inspected. If the frequency of sound waves in within the range 10 to 20,000 Hz, the sound is audible, i.e. the range of hearing, above 20,000 Hz, the sound waves are referred to as Ultrasound or Ultrasonics. Sound waves do not cause any permanent change in material although its transient presence is very noticeable. An energy transport through a sound wave is possible only when constituent particles are connected to each other by elastic forces. Liquids and Gases are also suitable media for the transmission of sound. In vacuum no matter exists and thus no sound transmission is possible. At the end of this article advantages and limitations of ultrasonic testing are also given. (A.B.)

Non-Destructive Testing for Concrete Structure

International Nuclear Information System (INIS)

Tengku Sarah Tengku Amran; Noor Azreen Masenwat; Mohamad Pauzi Ismail

2015-01-01

Nondestructive testing (NDT) is a technique to determine the integrity of a material, component or structure. It is essential in the inspection of alteration, repair and new construction in the building industry. There are a number of non-destructive testing techniques that can be applied to determine the integrity of concrete in a completed structure. Each has its own advantages and limitations. For concrete, these problems relate to strength, cracking, dimensions, delamination, and inhomogeneities. NDT is reasonably good and reliable tool to measure the property of concrete which also gives the fair indication of the compressive strength development. This paper discussed the concrete inspection using combined methods of NDT. (author)

2014 annual meeting of the German Society for Non-Destructive Testing (DGZfP). NDE in research development and application

International Nuclear Information System (INIS)

2014-01-01

The proceedings of the 2014 annual meeting of the German Society for Non-Destructive Testing (DGZfP) includes contributions to the following issues: process control, methods for surface analysis, dimensional measuring methods, computerized tomography, materials characterization, construction engineering, energy engineering, adhesive joints, equipment condition monitoring, thermography, guided waves, simulation - reconstruction - imaging techniques, phased array methods, combination of test procedures, microwave-terahertz-methods, fiber-reinforced composites.

Time Domain Terahertz Axial Computed Tomography Non Destructive Evaluation, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — We propose to demonstrate key elements of feasibility for a high speed automated time domain terahertz computed axial tomography (TD-THz CT) non destructive...

Microwave Detection of Laser Ultrasonic for Non-Destructive Testing, Phase II

Data.gov (United States)

National Aeronautics and Space Administration — In this proposal, we describe a program to develop a high-performance, cost-effective and robust microwave receiver prototype for multi-purpose Non-Destructive...

Non-destructive local determination of doping additions and main components in single crystals

International Nuclear Information System (INIS)

Ehksperiandova, L.P.; Blank, A.B.; Kukhtina, N.N.; Afanasiadi, L.I.

1994-01-01

Procedures for local non-destructive determination of elements in optical and scintillation single crystals are developed. They are applied for determination of the main components (in cadmium tungstate) and doping additions (tellurium in zinc selenide, europium in gadolinium silicate). The metrological characteristics of the developed micro-analysis methods are estimated. Segregation of the main components and doping additions in the objects under consideration are investigated. Tellurium is found to be distributed uniformly on the cross-sections of bulk zinc selenide single crystals. The segregation of europium along gadolinium silicate ingots is almost absent. On the cross-section surface of cadmium tungstate single crystals the microregions are found characterized by the prevailing contents of cadmium or tungsten

Homogeneity test of the ceramic reference materials for non-destructive quantitative

International Nuclear Information System (INIS)

Li Li; Fong Songlin; Zhu Jihao; Feng Xiangqian; Xie Guoxi; Yan Lingtong

2010-01-01

In order to study elemental composition of ancient porcelain samples, we developed a set of ceramic reference materials for non-destructive quantitative analysis. In this paper,homogeneity of Al, Si, K, Ca, Ti, Mn and Fe contents in the ceramic reference materials is investigated by EDXRF. The F test and the relative standard deviation are used to treat the normalized net counts by SPSS. The results show that apart from the DY2 and JDZ4 reference materials, to which further investigation would be needed, homogeneity of the DH, DY3, JDZ3, JDZ6, GY1, RY1, LQ4, YJ1, YY2 and JY2 meets the requirements of ceramic reference materials for non-destructive quantitative analysis. (authors)

Edward’s sword? – A non-destructive study of a medieval king’s sword

International Nuclear Information System (INIS)

Segebade, Chr.

2013-01-01

Non-destructive and instrumental methods including photon activation analysis were applied in an examination of an ancient sword. It was tried to find indication of forgery or, if authentic, any later processing and alteration. Metal components of the hilt and the blade were analysed by instrumental photon activation. Non-destructive metallurgical studies (hardness measurements, microscopic microstructure analysis) are briefly described, too. The results of these investigations did not yield indication of non-authenticity. This stood in agreement with the results of stylistic and scientific studies by weapon experts.

Non-destructive NIR-FT-Raman analyses in practice. Part I. Analyses of plants and historic textiles.

Science.gov (United States)

Andreev, G N; Schrader, B; Schulz, H; Fuchs, R; Popov, S; Handjieva, N

2001-12-01

Non-destructive analysis of natural substances in plants as well as of old dyed textiles by Raman spectroscopy has not been possible using conventional techniques. Exciting lines from the visible part of the spectrum produced photochemical and thermal decomposition of the objects as well as strong fluorescence. Using Nd:YAG laser excitation at 1,064 nm together with a special sample arrangement and interferometric recording, various polyacetylenes in Aethusa cynapium and in chamomile (Chamomilla recutita) and the main valuable substances in gentian species (Gentiana lutea and G. punctata), curcuma roots (Curcuma longa), cinnamon (Cinnamomum zeylanicum), fennel (Foeniculum vulgare), clove (Caryophyllus aromaticus), and ginger (Zingiber officinale) were analyzed non-destructively and discussed in comparison with the corresponding pure standard compounds. We further analyzed non-destructively the FT Raman spectra of collections of historical textiles and lakes used for dyeing. It is possible to distinguish the main dye component non-destructively by using Raman bands.

Time Domain Terahertz Axial Computed Tomography Non Destructive Evaluation, Phase II

Data.gov (United States)

National Aeronautics and Space Administration — In this Phase 2 project, we propose to develop, construct, and deliver to NASA a computed axial tomography time-domain terahertz (CT TD-THz) non destructive...

Non-destructive X-ray examination of weft knitted wire structures

Science.gov (United States)

Obermann, M.; Ellouz, M.; Aumann, S.; Martens, Y.; Bartelt, P.; Klöcker, M.; Kordisch, T.; Ehrmann, A.; Weber, M. O.

2016-07-01

Conductive yarns or wires are often integrated in smart textiles to enable data or energy transmission. In woven fabrics, these conductive parts are fixed at defined positions and thus protected from external loads. Knitted fabrics, however, have relatively loose structures, resulting in higher impacts of possible mechanical forces on the individual yarns. Hence, metallic wires with smaller diameters in particular are prone to break when integrated in knitted fabrics. In a recent project, wires of various materials including copper, silver and nickel with diameters varying between 0.05 mm and 0.23 mm were knitted in combination with textile yarns. Hand flat knitting machines of appropriate gauges were used to produce different structures. On these samples, non-destructive examinations, using an industrial X-ray system Seifert x|cube (225 kV) equipped with a minifocus X-ray tube, were carried out, directly after knitting as well as after different mechanical treatments (tensile, burst, and washing tests). In this way, structural changes of the stitch geometry could be visualized before failure. In this paper, the loop geometries in the knitted fabrics are depicted depending on knitted structures, wire properties and the applied mechanical load. Consequently, it is shown which metallic wires and yarns are most suitable to be integrated into knitted smart textiles.

Structural characterization of selective area growth GaN nanowires by non-destructive optical and electrical techniques

International Nuclear Information System (INIS)

Secco, Eleonora; Minj, Albert; Garro, Núria; Cantarero, Andrés; Colchero, Jaime; Urban, Arne; Oppo, Carla Ivana; Malindretos, Joerg; Rizzi, Angela

2015-01-01

The growth selectivity and structural quality of GaN nanowires obtained by plasma-assisted molecular beam epitaxy on pre-patterned GaN(0001) templates are investigated by means of non-destructive techniques. Optimum control over the nanowire arrangement and size requires a pitch between the mask apertures below twice the diffusion length of Ga atoms. Lower pitches, however, seem to slightly diminish the structural quality of the material, as revealed by the increase of the Raman peak linewidths. The photoluminescence spectra of the nanowires show a considerable presence of basal plane stacking faults, whose density increases for decreasing nanowire diameter. The capabilities of Kelvin probe force microscopy for imaging these kind of defects are also demonstrated. (paper)

Structural characterization of selective area growth GaN nanowires by non-destructive optical and electrical techniques

Science.gov (United States)

Secco, Eleonora; Minj, Albert; Garro, Núria; Cantarero, Andrés; Colchero, Jaime; Urban, Arne; Ivana Oppo, Carla; Malindretos, Joerg; Rizzi, Angela

2015-08-01

The growth selectivity and structural quality of GaN nanowires obtained by plasma-assisted molecular beam epitaxy on pre-patterned GaN(0001) templates are investigated by means of non-destructive techniques. Optimum control over the nanowire arrangement and size requires a pitch between the mask apertures below twice the diffusion length of Ga atoms. Lower pitches, however, seem to slightly diminish the structural quality of the material, as revealed by the increase of the Raman peak linewidths. The photoluminescence spectra of the nanowires show a considerable presence of basal plane stacking faults, whose density increases for decreasing nanowire diameter. The capabilities of Kelvin probe force microscopy for imaging these kind of defects are also demonstrated.

Dam safety review using non-destructive methods for reinforced concrete structure

Energy Technology Data Exchange (ETDEWEB)

Philibert, Alain; Saint-Pierre, Francois; Turcotte, Bernard [Le Groupe S.M. International Inc., Sherbrooke, (Canada)

2010-07-01

Dams built at the beginning of the twentieth century include concrete structures that were put in under rehabilitation works. In some cases, the details of the structures are not well documented. In other cases, concrete damage can be hidden under new layers of undamaged material. This requires that the dam safety review in a real investigation gather the information necessary for carrying out the hydraulic and stability studies required by the Dam Safety Act. This paper presented the process of dam safety review using non-destructive methods for reinforced concrete structures. Two reinforced concrete dams built in the 1900's, the Eustic dam on the Coaticook River and the Frontenac dam on the Magog River near Sherbrooke, were evaluated by S.M. International using non-destructive methods such as sonic and ground penetrating radar methods. The studies allowed mapping of concrete damage and provided geometric information on some non visible structure elements that were part of previous reinforcement operations.

Aging material evaluation and studies by non-destructive techniques (AMES-NDT) - a European network project

International Nuclear Information System (INIS)

Dobmann, Gerd; Debarberis, Luigi; Coste, Jean-Francois

2001-01-01

This paper presents results obtained in a round-robin action organized in a concerted action of ten partners in the EURATOM program of the European Community. The objective of the research was to document the state of the art of available non-destructive testing (NDT) techniques in order to characterize material aging phenomena based on a reduction of Charpy-V energy and a shift in the fracture appearance transition temperature. Therefore, samples from the Japanese nuclear reactor pressure vessel JRQ-steel (ASMT Standard A533-B Class 1) have been thermally treated at 700 deg. C for 18 h with a subsequent water quenching. Besides micromagnetic and electromagnetic NDT, the positron annihilation technique, ultrasonic reverberation by using Laser ultrasonics and the thermo-electrical power have been applied to characterize the aged material states

Operational experience in the non-destructive assay of fissile material in General Electric's nuclear fuel fabrication facility

International Nuclear Information System (INIS)

Stewart, J.P.

1976-01-01

Operational experience in the non-destructive assay of fissile material in a variety of forms and containers and incorporation of the assay devices into the accountability measurement system for General Electric's Wilmington Fuel Fabrication Facility measurement control programme is detailed. Description of the purpose and related operational requirements of each non-destructive assay system is also included. In addition, the accountability data acquisition and processing system is described in relation to its interaction with the various non-destructive assay devices and scales used for accountability purposes within the facility. (author)

Modelling and simulation of eddy current non-destructive testing

International Nuclear Information System (INIS)

Mansir, H.; Burais, N.; Nicolas, A.

1986-01-01

This paper presents the practical configuration for detecting cracks in conducting materials by eddy current non destructive testing. An electromagnetic field formulation is proposed using Maxwell's relations. Geometrical and physical properties of the crack are taken into account by several models, particularly with a new finite element called ''crack element''. Modelisation is applied to sensor impedance calculation with classical numerical methods [fr

Characterization of Nuclear Materials Using Complex of Non-Destructive and Mass-Spectroscopy Methods of Measurements

International Nuclear Information System (INIS)

Gorbunova, A.; Kramchaninov, A.

2015-01-01

Information and Analytical Centre for nuclear materials investigations was established in Russian Federation in the February 2 of 2009 by ROSATOM State Atomic Energy Corporation (the order #80). Its purpose is in preventing unauthorized access to nuclear materials and excluding their illicit traffic. Information and Analytical Centre includes analytical laboratory to provide composition and properties of nuclear materials of unknown origin for their identification. According to Regulation the Centre deals with: · identification of nuclear materials of unknown origin to provide information about their composition and properties; · arbitration analyzes of nuclear materials; · comprehensive research of nuclear and radioactive materials for developing techniques characterization of materials; · interlaboratory measurements; · measurements for control and accounting; · confirmatory measurements. Complex of non-destructive and mass-spectroscopy techniques was developed for the measurements. The complex consists of: · gamma-ray techniques on the base of MGAU, MGA and FRAM codes for uranium and plutonium isotopic composition; · gravimetrical technique with gamma-spectroscopy in addition for uranium content; · calorimetric technique for plutonium mass; · neutron multiplicity technique for plutonium mass; · measurement technique on the base of mass-spectroscopy for uranium isotopic composition; · measurement technique on the base of mass-spectroscopy for metallic impurities. Complex satisfies the state regulation requirements of ensuring the uniformity of measurements including the Russian Federation Federal Law on Ensuring the Uniformity of Measurements #102-FZ, Interstate Standard GOST R ISO/IEC 17025-2006, National Standards of Russian Federation GOST R 8.563-2009, GOST R 8.703-2010, Federal Regulations NRB-99/2009, OSPORB 99/2010. Created complex is provided in reference materials, equipment end certificated techniques. The complex is included in accredited

Polychrome glass from Etruscan sites: first non-destructive characterization with synchrotron μ-XRF, μ-XANES and XRPD

International Nuclear Information System (INIS)

Arletti, R.; Vezzalini, G.; Quartieri, S.; Ferrari, D.; Merlini, M.; Cotte, M.

2008-01-01

This work is devoted to the characterization of a suite of very rare, highly decorated and coloured glass vessels and beads from the VII to the IV century BC. The most serious difficulty in developing this study was that any sampling - even micro-sampling - was absolutely forbidden. As a consequence, the mineralogical and chemical nature of chromophores and opacifiers present in these Iron Age finds were identified by means of the following synchrotron-based, strictly non-destructive, techniques: micro X-ray fluorescence (μ-XRF), Fe K-edge micro X-ray absorption near edge spectroscopy (μ-XANES) and X-ray powder diffraction (XRPD). The μ-XRF mapping evidenced high levels of Pb and Sb in the yellow decorations and the presence of only Sb in the white and light-blue ones. Purple and black glass show high amounts of Mn and Fe, respectively. The XRPD analyses confirmed the presence of lead and calcium antimonates in yellow, turquoise and white decorations. Fe K-edge μ-XANES spectra were collected in different coloured parts of the finds, thus enabling the mapping of the oxidation state of these elements across the samples. In most of the samples iron is present in the reduced form Fe 2+ in the bulk glass of the vessels, and in the oxidized form Fe 3+ in the decorations, indicating that these glass artefacts were produced in at least two distinct processing steps under different furnace conditions. (orig.)

Measurement of mango firmness by non-destructive limited compression technique

NARCIS (Netherlands)

Penchaiya, P.; Uthairatanakij, A.; Srilaong, V.; Kanlayanarat, S.; Tijskens, L.M.M.; Tansakul, A.

2015-01-01

Thai mango 'Nam Dok Mai Si-Thong' has an attractive golden yellow skin colour even in immature fruit, not ready for consumption. Firmness becomes an important quality attribute to assess the ripening stage of the fruit during storage. In this study, the possibility of a non-destructive method

Non-destructive analysis for the inspection and control of metalic monuments and historical manuscripts

International Nuclear Information System (INIS)

Faubel, W.; Heissler, S.; Klewe-Nebenius, H.; Willin, E.

2003-01-01

As a contribution to the increasing efforts to preserve cultural heritage of historical bronze monuments exposed to atmospheric corrosion as well as historical books and manuscripts non-destructive analytical methods are highly desirable enabling an in-situ examination of the surface status of an object. The development and application of novel non-destructive analytical methods based on the photoacoustic and photothermal deflection spectroscopy allowed to investigate the state of bronze patina as well as the effectiveness of conservation procedures for historical manuscripts. (orig.)

Non-invasive and micro-destructive investigation of the Domus Aurea wall painting decorations.

Science.gov (United States)

Clementi, Catia; Ciocan, Valeria; Vagnini, Manuela; Doherty, Brenda; Tabasso, Marisa Laurenzi; Conti, Cinzia; Brunetti, Brunetto Giovanni; Miliani, Costanza

2011-10-01

The paper reports on the exploitation of an educated multi-technique analytical approach based on a wide non invasive step followed by a focused micro-destructive step, aimed at the minimally invasive identification of the pigments decorating the ceiling of the Gilded Vault of the Domus Aurea in Rome. The combination of elemental analysis with molecular characterization provided by X-ray fluorescence and UV-vis spectroscopies, respectively, allowed for the in situ non-invasive identification of a remarkable number of pigments, namely Egyptian blue, green earth, cinnabar, red ochre and an anthraquinonic lake. The study was completed with the Raman analysis of two bulk samples, in particular, SERS measurements allowed for the speciation of the anthraquinonic pigment. Elemental mapping by scanning electron microscopy-energy dispersive spectrometer combined with micro-fluorimetry on cross-section gave an insight into both the distribution of different blend of pigments and on the nature of the inorganic support of the red dye.

NON DESTRUCTIVE APPLICATION OF RADIOACTIVE TRACER TECHNIQUE FOR CHARACTERIZATION OF INDUSTRIAL GRADE ANION EXCHANGE RESINS INDION GS-300 AND INDION-860

Directory of Open Access Journals (Sweden)

P.U. SINGARE

2014-02-01

Full Text Available The paper deals with the application of radio isotopic non-destructive technique in the characterization of two industrial grade anion exchange resins Indion GS-300 and Indion-860. For the characterization of the two resins, 131I and 82Br were used as tracer isotopes to trace the kinetics of iodide and bromide ion-isotopic exchange reactions. It was observed that the values of specific reaction rate (min−1, amount of iodide ion exchanged (mmol, initial rate of iodide ion exchange (mmol/min and log Kd were calculated as 0.328, 0.577, 0.189 and 19.7 respectively for Indion GS-300 resin, which was higher than the respective values of 0.180, 0.386, 0.070 and 17.0 calculated for Indion-860 resins when measured under identical experimental conditions. Also at a constant temperature of 40.0 °C, as the concentration of labeled iodide ion solution increases 0.001 M to 0.004 M, the percentage of iodide ions exchanged increases from 75.16 % to 78.36 % for Indion GS-300 resins, which was higher than the increases from 49.65 % to 52.36 % compared to that obtained for Indion-860 resins. The overall results indicate that under identical experimental conditions, Indion GS-300 resins show superior performance over Indion-860 resins.

Non Destructive Application of Radioactive Tracer Technique for Characterization of Industrial Grade Anion Exchange Resins Indio GS-300 and Indion-860

International Nuclear Information System (INIS)

Singare, P. U.

2014-01-01

The paper deals with the application of radio isotopic non-destructive technique in the characterization of two industrial grade anion exchange resins Indion GS-300 and Indion-860. For the characterization of the two resins, 131 I and 82 Br were used as tracer isotopes to trace the kinetics of iodide and bromide ion-isotopic exchange reactions. It was observed that the values of specific reaction rate (min -1 ), amount of iodide ion exchanged (mmol), initial rate of iodide ion exchange (mmol/min) and log K d were calculated as 0.328, 0.577, 0.189 and 19.7 respectively for Indion GS-300 resin, which was higher than the respective values of 0.180, 0.386, 0.070 and 17.0 calculated for Indion-860 resins when measured under identical experimental conditions. Also at a constant temperature of 40.0 .deg. C, as the concentration of labeled iodide ion solution increases 0.001 M to 0.004 M, the percentage of iodide ions exchanged increases from 75.16 % to 78.36 % for Indion GS-300 resins, which was higher than the increases from 49.65 % to 52.36 % compared to that obtained for Indion-860 resins. The overall results indicate that under identical experimental conditions, Indion GS-300 resins show superior performance over Indion-860 resins

3D RoboMET Characterization

Energy Technology Data Exchange (ETDEWEB)

Madison, Jonathan D. [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Susan, Donald F. [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States); Kilgo, Alice C. [Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)

2015-10-01

The goal of this project is to generate 3D microstructural data by destructive and non-destructive means and provide accompanying characterization and quantitative analysis of such data. This work is a continuing part of a larger effort to relate material performance variability to microstructural variability. That larger effort is called “Predicting Performance Margins” or PPM. In conjunction with that overarching initiative, the RoboMET.3D™ is a specific asset of Center 1800 and is an automated serialsectioning system for destructive analysis of microstructure, which is called upon to provide direct customer support to 1800 and non-1800 customers. To that end, data collection, 3d reconstruction and analysis of typical and atypical microstructures have been pursued for the purposes of qualitative and quantitative characterization with a goal toward linking microstructural defects and/or microstructural features with mechanical response. Material systems examined in FY15 include precipitation hardened 17-4 steel, laser-welds of 304L stainless steel, thermal spray coatings of 304L and geological samples of sandstone.

Potential development of non-destructive assay for nuclear safeguards

International Nuclear Information System (INIS)

Benoit, R.; Cuypers, M.; Guardini, S.

1983-01-01

After a brief summary on the role of non-destructive assay in safeguarding the nuclear fuel cycle, its evolution from NDA methods development to other areas is illustrated. These areas are essentially: a) the evaluation of the performances of NDA techniques in field conditions; b) introduction of full automation of measurement instrument operation, using interactive microprocessors and of measurement data handling evaluation and retrieval features; c) introduction of the adequate link and compatibility to assure NDA measurement data transfer in an integrated safeguards data evaluation scheme. In this field, the Joint Research Centre (JRC) of the Commission of the European Communities (CEC) is developing and implementing a number of techniques and methodologies allowing an integrated and rational treatment of the large amount of safeguards data produced. In particular for the non-destructive assay measurements and techniques, the JRC has studied and tested methodologies for the automatic generation and validation of data of inventory verification. In order to apply these techniques successfully in field, the JRC has studied the design requirements of NDA data management and evaluation systems. This paper also discusses the functional requirements of an integrated system for NDA safeguards data evaluation

Multi-energy radiography for non-destructive testing of materials and structures for civil engineering

International Nuclear Information System (INIS)

Naydenov, S.V.; Ryzhikov, V.

2003-01-01

Development of the technological base of modern non-destructive testing require new methods allowing determination of specified properties of materials and structures under study. A traditional direction of works is determination of internal spatial structure of the materials and other constructions. Restoration of this geometrical information is of qualitative character, though provides for determination of technical parameters affecting physical properties of the system. Reconstruction of the chemical composition, density and atomic structure (effective atomic number) is an inverse problem of direct quantitative determination of properties starting from data obtained by means of non-destructive testing. In the present work, we propose the use of multi-energy radiography for reconstruction of the substantial structure of materials. In framework of simple theoretical model it is shown that, using multi-channel absorption of X-rays, important substantial characteristics of materials and multi-compound structures can be readily reconstructed. The results obtained show high efficiency of 2-energy radiography for non-destructive testing in civil engineering

Space Qualified Non-Destructive Evaluation and Structural Health Monitoring Technology, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — NextGen Aeronautics is proposing an innovative space qualified non-destructive evaluation and health monitoring technology. The technology is built on concepts...

The characterization of natural gemstones using non-invasive FT-IR spectroscopy: New data on tourmalines.

Science.gov (United States)

Mercurio, Mariano; Rossi, Manuela; Izzo, Francesco; Cappelletti, Piergiulio; Germinario, Chiara; Grifa, Celestino; Petrelli, Maurizio; Vergara, Alessandro; Langella, Alessio

2018-02-01

Fourteen samples of tourmaline from the Real Museo Mineralogico of Federico II University (Naples) have been characterized through multi-methodological investigations (EMPA-WDS, SEM-EDS, LA-ICP-MS, and FT-IR spectroscopy). The samples show different size, morphology and color, and are often associated with other minerals. Data on major and minor elements allowed to identify and classify tourmalines as follows: elbaites, tsilaisite, schorl, dravites, uvites and rossmanite. Non-invasive, non-destructive FT-IR and in-situ analyses were carried out on the same samples to validate this chemically-based identification and classification. The results of this research show that a complete characterization of this mineral species, usually time-consuming and expensive, can be successfully achieved through non-destructive FT-IR technique, thus representing a reliable tool for a fast classification extremely useful to plan further analytical strategies, as well as to support gemological appraisals. Copyright © 2017 Elsevier B.V. All rights reserved.

Prompt-gamma neutron activation analysis for the non-destructive characterization of radioactive wastes; Prompt-Gamma-Neutronen-Aktivierungs-Analyse zur zerstoerungsfreien Charakterisierung radioaktiver Abfaelle

Energy Technology Data Exchange (ETDEWEB)

Kettler, John Paul Hermann

2010-07-01

understand this correlation. Several homogeneous and inhomogeneous sample drums were produced for the qualification of the prototype system. The sample drums were characterized with different systems and methods to verify the results of the PGNAA-Prototype-System. At the end of the present work, the detection limits of selected elements for different irradiation and measurement conditions were determined. The element compilation refers to relevant elements for the final disposal Konrad. The results of the measurements, which were realized with the PGNAA-Prototype-System, show, that a non-destructive characterization of large samples is possible. Furthermore a routine test procedure, based on the results of the present work, is in development to characterize 200 l drums. (orig.)

Space Qualified Non-Destructive Evaluation and Structural Health Monitoring Technology, Phase II

Data.gov (United States)

National Aeronautics and Space Administration — Encouraged by Phase I accomplishments, the proposed Phase II program will significantly mature and align the development of a Space Qualified Non-Destructive...

Non destructive testing and neutron radiography in 1994

International Nuclear Information System (INIS)

Bayon, G.

1994-01-01

Neutron radiography has been considered for a long time as a promising technique; however it plays a minor part in the world of non destructive testing today, due to the lack of suitable neutron sources and lack of new industrial applications. This paper reviews the present status of neutron sources, neutron radiography activities, especially in France (such as the neutron-capture-issued secondary radiation spectrometry), in nuclear, aerospace, aeronautical and metallurgical sectors, and the last applications of neutron dynamic imaging. 9 refs

Edward's sword? - A non-destructive study of a medieval king's sword

Energy Technology Data Exchange (ETDEWEB)

Segebade, Chr. [Idaho Accelerator Centre, Idaho State University, 1500 Alvin Ricken Drive, Pocatello, ID 83201 (United States)

2013-04-19

Non-destructive and instrumental methods including photon activation analysis were applied in an examination of an ancient sword. It was tried to find indication of forgery or, if authentic, any later processing and alteration. Metal components of the hilt and the blade were analysed by instrumental photon activation. Non-destructive metallurgical studies (hardness measurements, microscopic microstructure analysis) are briefly described, too. The results of these investigations did not yield indication of non-authenticity. This stood in agreement with the results of stylistic and scientific studies by weapon experts.

Guidebook on destructive examination of water reactor fuel

International Nuclear Information System (INIS)

1997-01-01

As a result of common efforts of fuel vendors, utilities and research institutes the average burnup pf design batch fuels was increased for both PWRs and BWRs and the fuel failure rate has been reduced. The previously published Guidebook on Non-Destructive Examination of Water Reactor Fuel recommended that more detailed destructive techniques are required for complete understanding of fuel performance. On the basis of contributions of the 14 participants in the ED-WARF-II CRP and proceedings of IAEA Technical Committee on Recent Developments in Post-irradiation Examination Techniques for Water Reactor Fuel this guidebook was compiled. It gives a complete survey of destructive techniques available to date worldwide. The following examination techniques are described in detailed including major principles of equipment design: microstructural studies; elemental analysis; isotopic analysis; measurement of physical properties; measurement of mechanical properties. Besides the examination techniques, methods for refabrication of experimental rods from high burnup power reactor rods as well as methods for verification of non-destructive techniques by using destructive techniques is included

Micro-cantilevers for non-destructive characterization of nanograss uniformity

DEFF Research Database (Denmark)

Petersen, Dirch Hjorth; Wang, Fei; Olesen, Mikkel Buster

2011-01-01

We demonstrate an application of three-way flexible micro four-point probes for indirect uniformity characterization of surface morphology. The mean sheet conductance of a quasi-planar 3D nanostructured surface is highly dependent on the surface morphology, and thus accurate sheet conductance...... measurements may be useful for process uniformity characterization. The method is applied for characterization of TiW coated nanograss uniformity. Three-way flexible L-shaped cantilever electrodes are used to avoid damage to the fragile surface, and a relative standard deviation on measurement repeatability...... of 0.12 % is obtained with a measurement yield of 97%. Finally, variations in measured sheet conductance are correlated to the surface morphology as characterized by electron microscopy....

The non-destructive identification of early Chinese porcelain by PIXE

International Nuclear Information System (INIS)

Cheng, H.S.; Zhang, Z.Q.; Zhang, B.; Yang, F.J.

2004-01-01

PIXE is used for the non-destructive differentiation of early precious Chinese blue and white porcelain made in Yuan (AD 1206-1368), Ming (AD 1368-1644) Dynasty in Jingdezhen from imitations. Also, ancient celadon made in Song Dynasty (AD 960-1279) is identified by measuring the trace elements contained in the glazes

An improved technique for non-destructive measurement of the stem ...

African Journals Online (AJOL)

It was concluded that the standard volume model based on the non-destructive measurement technique meets the requirements for precision in forest surveys. The precision of the standard volume model for L. gmelinii (a coniferous tree) was superior to that of the model for P. tomentosa (a broad-leaved tree). The electronic ...

The non-destructive identification of early Chinese porcelain by PIXE

Science.gov (United States)

Cheng, H. S.; Zhang, Z. Q.; Zhang, B.; Yang, F. J.

2004-06-01

PIXE is used for the non-destructive differentiation of early precious Chinese blue and white porcelain made in Yuan (AD 1206-1368), Ming (AD 1368-1644) Dynasty in Jingdezhen from imitations. Also, ancient celadon made in Song Dynasty (AD 960-1279) is identified by measuring the trace elements contained in the glazes.

Confirm calculation of 12 MeV non-destructive testing electron linear accelerator target

International Nuclear Information System (INIS)

Ma Shudong; Zhang Rutong; Guo Yanbin; Zhou Yuan; Li Xuexian; Chen Yan

2012-01-01

The confirm calculation of 12 MeV non-destructive testing (NDT) electron linear accelerator (LINAC) target was studied. Firstly, the most optimal target thickness and related photon dose yield, distributions of dose rate, and related photon conversion efficiencies were got by calculation with specific analysis of the physical mechanism of the interactions between the beam and target; Secondly, the photon dose rate distribution, converter efficiencies, and thickness of various kinds of targets, such as W, Au, Ta, etc. were verified by MCNP simulation and the most optimal target was got using the MCNP code; Lastly, the calculation results of theory and MCNP were compared to confirm the validity of target calculation. (authors)

The need to qualify Non Destructive Tests (NDT) has been recognized for many years in the European countries engaged in nuclear power generation

International Nuclear Information System (INIS)

Walczak, M.; Wojas, M.

2008-01-01

The European Network for Inspection Qualification, ENIQ, which groups the major part of the nuclear power plant operators in the European Union and in the Applicant Countries, has developed the European methodology for Qualification of Non Destructive Tests. As qualification of NDT is nowadays a standard method in the nuclear industry and in other industries. CEN (European Committee for Standardization) Technical Committee 138 '' Non Destructive Testing '' has established a Working Group, which is responsible for developing a Standard document detailing the CEN Methodology for the qualification of Non Destructive Tests applicable to all industries carrying out Non-Destructive Tests. This Standard document sets out basic principles and provides recommendations and general guidelines for carrying out qualification of NDT. It describes a methodology for qualification of Non-Destructive Tests, applicable to all NDT methods and considers qualification of equipment, procedure and personnel training. This paper presents a short background of the European Methodology for Qualification of Non-Destructive Tests and the Standard document CEN/TR 14748 '' Non-destructive testing - Methodology for qualification of non-destructive tests ''. (author)

Assessment of hydrogen levels in Zircaloy-2 by non-destructive testing

International Nuclear Information System (INIS)

De, P.K.; John, J.T.; Banerjee, S.; Jayakumar, T.; Thavasimuthu, M.; Raj, B.

1998-01-01

A non-destructive assessment of Zircaloy-2 samples charged with hydrogen in the range of 50 to 1150 mg/kg has been made using ultrasonic and eddy current testing. It has been found that the ratio of the longitudinal to the shear wave velocity is a parameter which can be directly correlated with the hydrogen content up to a level of 100 to 200 mg/kg. This parameter together with the values of longitudinal and shear wave velocities can be utilized in a multi-parametric correlation approach for estimation of higher levels of the hydrogen content (up to 1150 mg/kg). The sensitivity at different ranges has been found to be acceptable. Ultrasonic attenuation measurements at higher frequencies and eddy current test parameter are also effective for estimation of hydrogen levels above 250 mg/kg in zirconium alloys. Microstructural characterization including TEM studies have been carried out for studying the influence of the type and the morphology of hydride precipitates on ultrasonic parameters. (orig.)

Comparative analysis of non-destructive methods to control fissile materials in large-size containers

Directory of Open Access Journals (Sweden)

Batyaev V.F.

2017-01-01

Full Text Available The analysis of various non-destructive methods to control fissile materials (FM in large-size containers filled with radioactive waste (RAW has been carried out. The difficulty of applying passive gamma-neutron monitoring FM in large containers filled with concreted RAW is shown. Selection of an active non-destructive assay technique depends on the container contents; and in case of a concrete or iron matrix with very low activity and low activity RAW the neutron radiation method appears to be more preferable as compared with the photonuclear one.

Non-destructive methods and means for quality control of structural products

International Nuclear Information System (INIS)

Dmitriev, V.V.

1989-01-01

Progressive non-destructive methods (acoustic, magnetic, radiation with liquid penetrants) and means of control of structural product quality, allowing to determine the state of products and structures not only immediately after their production but directly at the erected or reconstructed objects are described

Rapid, non-destructive and non-contact inspection of solid foods by means of photothermal radiometry; thermal effusivity and initial heating coefficient

Science.gov (United States)

Gijsbertsen, A.; Bicanic, D.; Gielen, J. L. W.; Chirtoc, M.

2004-03-01

CO 2-laser photothermal radiometry (PTR) was demonstrated to be suitable for the non-destructive and non-contact characterization (both optical and thermal) of solid phase agricultural commodities (fresh vegetables, fruits) and confectionery products (candy). Proper interpretation of PTR signals enable one to calculate two parameters, i.e. the well known thermal effusivity e ( e= λρc p, where λ and ρcp are the thermal conductivity and the volume specific heat, respectively) and a newly introduced physical quantity termed 'initial heating coefficient' chi ( χ= β/( ρcp), β is the absorption coefficient). Obtained values for e are in a good agreement with data reported in the literature. PTR enables one to rapidly determine e via a single measurement. As opposed to this, the knowledge of two out of three thermophysical parameters (thermal diffusivity, thermal conductivity and volume specific heat) is a condition sine qua non for determining effusivity in the conventional manner.

A non-destructive DNA sampling technique for herbarium specimens.

Science.gov (United States)

Shepherd, Lara D

2017-01-01

Herbarium specimens are an important source of DNA for plant research but current sampling methods require the removal of material for DNA extraction. This is undesirable for irreplaceable specimens such as rare species or type material. Here I present the first non-destructive sampling method for extracting DNA from herbarium specimens. DNA was successfully retrieved from robust leaves and/or stems of herbarium specimens up to 73 years old.

Feasibility Study of Non-Destructive Techniques to Measure Corrosion in SAVY Containers

Energy Technology Data Exchange (ETDEWEB)

Davenport, Matthew Nicholas [Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

2016-07-15

Stainless Steel SAVY containers are used to transport and store nuclear material. They are prone to interior corrosion in the presence of certain chemicals and a low-oxygen environment. SAVY containers also have relatively thin walls to reduce their weight, making their structural integrity more vulnerable to the effects of corrosion. A nondestructive evaluation system that finds and monitors corrosion within containers in use would improve safety conditions and preclude hazards. Non-destructive testing can determine whether oxidation or corrosion is occurring inside the SAVY containers, and there are a variety of non-destructive testing methods that may be viable. The feasibility study described will objectively decide which method best fits the requirements of the facility and the problem. To improve efficiency, the containers cannot be opened during the non-destructive examination. The chosen technique should also be user-friendly and relatively quick to apply. It must also meet facility requirements regarding wireless technology and maintenance. A feasibility study is an objective search for a new technology or product to solve a particular problem. First, the design, technical, and facility feasibility requirements are chosen and ranked in order of importance. Then each technology considered is given a score based upon a standard ranking system. The technology with the highest total score is deemed the best fit for a certain application.

Non-destructive system to evaluate critical properties of asphalt compaction : [research brief].

Science.gov (United States)

2013-12-01

The Wisconsin Highway Research Program sponsored a two-stage investigation to develop a non-destructive system to evaluate critical compaction properties and characteristics of asphalt pavements during the densification process. Stage One activities ...

Treatment of statin compounds by advanced oxidation processes: Kinetic considerations and destruction mechanisms

Science.gov (United States)

Razavi, Behnaz; Song, Weihua; Santoke, Hanoz; Cooper, William J.

2011-03-01

This study examined the use of advanced oxidation/reduction processes (AO/RPs) for the destruction of cholesterol lowering statin pharmaceuticals. AO/RPs which utilize the oxidizing hydroxyl radical ( rad OH) and reducing aqueous electron (e -aq), to degrade chemical contaminants are alternatives to traditional water treatment methods, and are alternatives as water reuse becomes more generally implemented. Four major statin pharmaceuticals, fluvastatin, lovastatin, pravastatin and simvastatin, were studied, and the absolute bimolecular reaction rate constants with rad OH determined, (6.96±0.16)×10 9, (2.92±0.06)×10 9, (4.16±0.13)×10 9, and (3.13±0.15)×10 9 M -1 s -1, and for e -aq (2.31±0.06)×10 9, (0.45±0.01)×10 9, (1.26±0.01)×10 9, and (0.69±0.02)×10 9 M -1 s -1, respectively. To provide additional information on the radicals formed upon oxidation, transient spectra were measured and the overall reaction efficiency determined. Radical-based destruction mechanisms for destruction of the statins are proposed based on the LC-MS determination of the stable reaction by-products formed using 137Cs γ-irradiation of statin solutions. Knowing the reaction rates, reaction efficiencies and destruction mechanisms of these compounds is essential for the consideration of the use of advanced oxidation/reduction processes for the destruction of statins in aqueous systems.

Treatment of statin compounds by advanced oxidation processes: Kinetic considerations and destruction mechanisms

International Nuclear Information System (INIS)

Razavi, Behnaz; Song Weihua; Santoke, Hanoz; Cooper, William J.

2011-01-01

This study examined the use of advanced oxidation/reduction processes (AO/RPs) for the destruction of cholesterol lowering statin pharmaceuticals. AO/RPs which utilize the oxidizing hydroxyl radical ( · OH) and reducing aqueous electron (e - aq ), to degrade chemical contaminants are alternatives to traditional water treatment methods, and are alternatives as water reuse becomes more generally implemented. Four major statin pharmaceuticals, fluvastatin, lovastatin, pravastatin and simvastatin, were studied, and the absolute bimolecular reaction rate constants with · OH determined, (6.96±0.16)x10 9 , (2.92±0.06)x10 9 , (4.16±0.13)x10 9 , and (3.13±0.15)x10 9 M -1 s -1 , and for e - aq (2.31±0.06)x10 9 , (0.45±0.01)x10 9 , (1.26±0.01)x10 9 , and (0.69±0.02)x10 9 M -1 s -1 , respectively. To provide additional information on the radicals formed upon oxidation, transient spectra were measured and the overall reaction efficiency determined. Radical-based destruction mechanisms for destruction of the statins are proposed based on the LC-MS determination of the stable reaction by-products formed using 137 Cs γ-irradiation of statin solutions. Knowing the reaction rates, reaction efficiencies and destruction mechanisms of these compounds is essential for the consideration of the use of advanced oxidation/reduction processes for the destruction of statins in aqueous systems.

Local defect resonance for sensitive non-destructive testing

Science.gov (United States)

Adebahr, W.; Solodov, I.; Rahammer, M.; Gulnizkij, N.; Kreutzbruck, M.

2016-02-01

Ultrasonic wave-defect interaction is a background of ultrasound activated techniques for imaging and non-destructive testing (NDT) of materials and industrial components. The interaction, primarily, results in acoustic response of a defect which provides attenuation and scattering of ultrasound used as an indicator of defects in conventional ultrasonic NDT. The derivative ultrasonic-induced effects include e.g. nonlinear, thermal, acousto-optic, etc. responses also applied for NDT and defect imaging. These secondary effects are normally relatively inefficient so that the corresponding NDT techniques require an elevated acoustic power and stand out from conventional ultrasonic NDT counterparts for their specific instrumentation particularly adapted to high-power ultrasonic. In this paper, a consistent way to enhance ultrasonic, optical and thermal defect responses and thus to reduce an ultrasonic power required is suggested by using selective ultrasonic activation of defects based on the concept of local defect resonance (LDR). A strong increase in vibration amplitude at LDR enables to reliably detect and visualize the defect as soon as the driving ultrasonic frequency is matched to the LDR frequency. This also provides a high frequency selectivity of the LDR-based imaging, i.e. an opportunity of detecting a certain defect among a multitude of other defects in material. Some examples are shown how to use LDR in non-destructive testing techniques, like vibrometry, ultrasonic thermography and shearography in order to enhance the sensitivity of defect visualization.

Human and organisational factors in the reliability of non-destructive testing (NOT)

International Nuclear Information System (INIS)

Norros, L.

1998-01-01

Non-destructive testing used in in-service inspections can be seen as a complicated activity system including three mutually related sub-activities: (1) definition of inspection programs and necessary resources, (2) carrying out diagnostic inspections, and (3) interpretation of the results from the view of plant safety and corrective measures. Various studies to investigate and measure the NDT performance have produced disappointing result. No clear correlations between single human factors and performance have been identified even though general agreement exists concerning the significance of human factors to the reliability of testing. Another incentive for our studies has been to test and evaluate the applicability of the international results in the Finnish circumstances. Three successive studies have thus been carried out on the human and organisational factors in non-destructive testing. (author)

Using photons for non-destructive testing of thick materials: a simulation study

International Nuclear Information System (INIS)

Oishi, Ryutaro; Nagai, Hideki

2004-01-01

Positron annihilation spectroscopy using positron annihilation lifetimes has been successfully studied for non-destructive material testing. A positron inspection probe is annihilated with an electron at the front of the material. The application of the positron lifetime method is restricted to thin materials. A photon with energy exceeding 1.02MeV reaches the materials' depth and can produce a positron through γ-conversion. Such a photon-produced positron is a probe for thick materials. The probability of γ-conversion, however, is low. The method of photon-produced positron annihilation lifetimes is restricted by statistics. We estimated the expected number of events and the statistical uncertainties of the lifetime measurements for a non-destructive test, such as an SUS316 fatigue monitoring, to construct a fatigue-monitoring system

Image-based phenotyping for non-destructive screening of different salinity tolerance traits in rice

KAUST Repository

Hairmansis, Aris

2014-08-14

Background Soil salinity is an abiotic stress wide spread in rice producing areas, limiting both plant growth and yield. The development of salt-tolerant rice requires efficient and high-throughput screening techniques to identify promising lines for salt affected areas. Advances made in image-based phenotyping techniques provide an opportunity to use non-destructive imaging to screen for salinity tolerance traits in a wide range of germplasm in a reliable, quantitative and efficient way. However, the application of image-based phenotyping in the development of salt-tolerant rice remains limited. Results A non-destructive image-based phenotyping protocol to assess salinity tolerance traits of two rice cultivars (IR64 and Fatmawati) has been established in this study. The response of rice to different levels of salt stress was quantified over time based on total shoot area and senescent shoot area, calculated from visible red-green-blue (RGB) and fluorescence images. The response of rice to salt stress (50, 75 and 100 mM NaCl) could be clearly distinguished from the control as indicated by the reduced increase of shoot area. The salt concentrations used had only a small effect on the growth of rice during the initial phase of stress, the shoot Na+ accumulation independent phase termed the ‘osmotic stress’ phase. However, after 20 d of treatment, the shoot area of salt stressed plants was reduced compared with non-stressed plants. This was accompanied by a significant increase in the concentration of Na+ in the shoot. Variation in the senescent area of the cultivars IR64 and Fatmawati in response to a high concentration of Na+ in the shoot indicates variation in tissue tolerance mechanisms between the cultivars. Conclusions Image analysis has the potential to be used for high-throughput screening procedures in the development of salt-tolerant rice. The ability of image analysis to discriminate between the different aspects of salt stress (shoot ion

APPARATUS FOR NON-DESTRUCTIVE INSPECTION OF CANTILEVERED MEMBERS

Science.gov (United States)

Taylor, E.R.; Mahoney, C.H.; Lay, C.R.

1961-10-24

An apparatus for non-destructive inspection of cantilevered members, such as compressor blades, is described. The member under inspection is vibrated with a regulated source of air under pressure. The amplitude of vibration of the member is maintained at its natural frequency. The frequency of vibration of the member is measured. An indication of an excessive decay or erratic shifting in the measured frequency above an allowable hysteretic decay is provided as an indication of a fault in the member. The member is vibrated for a selected test period. (AEC)

Non-destructive tests of capsules for JMTR irradiation examination

International Nuclear Information System (INIS)

Tanaka, Hidetaka; Nagao, Yoshiharu; Sato, Masashi; Osawa, Kenji

2007-03-01

Irradiation examination are increasing in advanced irradiation research for accurate prediction control and evaluation of irradiation parameter such as neutron fluence, etc. by using JMTR. Irradiation capsule internals are therefore structurally complicated recently. This report described the procedure of non destructive tests such as radiographic test, penetrant test, ultrasonic test, etc. for inspection of irradiation capsules in JMTR, and the result of Test-case of confirmation procedure for internal parts of irradiation capsules. (author)

Usage of FTIR-ATR as Non-Destructive Analysis of Selected Toxic Dyes

Science.gov (United States)

Bartošová, Alica; Blinová, Lenka; Sirotiak, Maroš; Michalíková, Anna

2017-06-01

The degradation of the environment which is due to the discharge of polluting wastewater from industrial sources poses a real problem in several countries. Textile industries use large volumes of water in their operations, discharging thus large volume of wastewater into the environment, most of which is untreated. The wastewater contains a variety of chemicals from various stages of process operations, including desizing, scouring, bleaching and dyeing. The main purpose of this paper is to introduce Infrared Spectrometry with Fourier transformation as a non-destructive method for study, identifation and rapid determination of selected representatives of cationic (Methylene Blue), azo (Congo Red, Eriochrome Black T) and nitroso (Naphthol Green B) dyes. In conjunction with the ATR technique, FTIR offers a reliable detection method of dyes without extraction by other dangerous substances. Spectral interpretation of dye spectra revealed valuable information about the identification and characterization of each group of dyes.

Proceedings of the national workshop on non destructive evaluation of structures

International Nuclear Information System (INIS)

2013-01-01

In spite of the care and best efforts to improve the quality of structures, problems do occur, raising alarm. This makes doubtful about the understanding. Distresses in the structures start immediately after construction and these are often concealed under the external finishes. A defect takes time to manifest itself. To add further, structures remain unattended for several years. As it is uneconomical to replace the assets before the intended service life by another capital investment, it is essential to periodically monitor the health of structures throughout its life. Success of both, the construction and restoration work depends on right diagnosis of the problem thorough proper testing techniques. Non destructive evaluation is one of the reliable methods for the scientific assessment of health and prediction of residual service life of structure. The workshop shall provide a platform to students, engineers and professionals for acquaintance with the current state of art technology of non-destructive evaluation techniques. Papers relevant to INIS are indexed separately

Comparative analysis of non-destructive methods to control fissile materials in large-size containers

Science.gov (United States)

Batyaev, V. F.; Sklyarov, S. V.

2017-09-01

The analysis of various non-destructive methods to control fissile materials (FM) in large-size containers filled with radioactive waste (RAW) has been carried out. The difficulty of applying passive gamma-neutron monitoring FM in large containers filled with concreted RAW is shown. Selection of an active non-destructive assay technique depends on the container contents; and in case of a concrete or iron matrix with very low activity and low activity RAW the neutron radiation method appears to be more preferable as compared with the photonuclear one. Note to the reader: the pdf file has been changed on September 22, 2017.

Non-destructive forensic latent fingerprint acquisition with chromatic white light sensors

Science.gov (United States)

Leich, Marcus; Kiltz, Stefan; Dittmann, Jana; Vielhauer, Claus

2011-02-01

Non-destructive latent fingerprint acquisition is an emerging field of research, which, unlike traditional methods, makes latent fingerprints available for additional verification or further analysis like tests for substance abuse or age estimation. In this paper a series of tests is performed to investigate the overall suitability of a high resolution off-the-shelf chromatic white light sensor for the contact-less and non-destructive latent fingerprint acquisition. Our paper focuses on scanning previously determined regions with exemplary acquisition parameter settings. 3D height field and reflection data of five different latent fingerprints on six different types of surfaces (HDD platter, brushed metal, painted car body (metallic and non-metallic finish), blued metal, veneered plywood) are experimentally studied. Pre-processing is performed by removing low-frequency gradients. The quality of the results is assessed subjectively; no automated feature extraction is performed. Additionally, the degradation of the fingerprint during the acquisition period is observed. While the quality of the acquired data is highly dependent on surface structure, the sensor is capable of detecting the fingerprint on all sample surfaces. On blued metal the residual material is detected; however, the ridge line structure dissolves within minutes after fingerprint placement.

A non-destructive approach for assessing decay in preservative treated wood

NARCIS (Netherlands)

Machek, L.; Edlund, M.L.; Sierra-Alvarez, R.; Militz, H.

2004-01-01

This study investigated the suitability of the non-destructive vibration-impulse excitation technique to assess the attack of preservative-treated wood in contact with the ground. Small stakes (10×5×100 mm3) of treated and untreated Scots pine sapwood were exposed to decay in laboratory-scale

Non destructive testing of industrial pieces by radiography: quantitative characterization and 3 D reconstruction by the way of a limited number of images

International Nuclear Information System (INIS)

Retraint, F.

1998-01-01

The non destructive testing of industrial pieces is evaluated on the basis of numerical radiographies.The context of the study is the online control of the fuel rods production. A direct model of a numerical radiography formation is proposed and detailed for an acquisition system consisting of a CCD video connected to a converter screen by an optical system. As this approach does not allow the determination of the measured matter thickness from the X-ray photograph, an approximate model based on realistic approximations of the industrial non destructive testing, has been developed. For the specific cases it is possible to inverse the model and to reach the quantitative information present in the x-ray photograph, in other words, the map of the X-rays measured matter thickness. It becomes then possible to access to the quantitative parameters of the possible defects present in the measured specimen, such as the surface and the bulk. To reach the 3 D information on the defects a 3 D reconstruction method, from 3 X-rays photographs, is proposed.The inverse problem is solved by the non convex energy minimization. (A.L.B.)

Treatment of statin compounds by advanced oxidation processes: Kinetic considerations and destruction mechanisms

Energy Technology Data Exchange (ETDEWEB)

Razavi, Behnaz, E-mail: brazavi@uci.ed [Urban Water Research Center, Department of Civil and Environmental Engineering, University of California, Irvine, Irvine, CA 92697-2175 (United States); Song Weihua, E-mail: wsong@uci.ed [Urban Water Research Center, Department of Civil and Environmental Engineering, University of California, Irvine, Irvine, CA 92697-2175 (United States); Santoke, Hanoz, E-mail: hsantoke@uci.ed [Urban Water Research Center, Department of Civil and Environmental Engineering, University of California, Irvine, Irvine, CA 92697-2175 (United States); Cooper, William J., E-mail: wcooper@uci.ed [Urban Water Research Center, Department of Civil and Environmental Engineering, University of California, Irvine, Irvine, CA 92697-2175 (United States)

2011-03-15

This study examined the use of advanced oxidation/reduction processes (AO/RPs) for the destruction of cholesterol lowering statin pharmaceuticals. AO/RPs which utilize the oxidizing hydroxyl radical ({sup {center_dot}O}H) and reducing aqueous electron (e{sup -}{sub aq}), to degrade chemical contaminants are alternatives to traditional water treatment methods, and are alternatives as water reuse becomes more generally implemented. Four major statin pharmaceuticals, fluvastatin, lovastatin, pravastatin and simvastatin, were studied, and the absolute bimolecular reaction rate constants with {sup {center_dot}O}H determined, (6.96{+-}0.16)x10{sup 9}, (2.92{+-}0.06)x10{sup 9}, (4.16{+-}0.13)x10{sup 9}, and (3.13{+-}0.15)x10{sup 9} M{sup -1} s{sup -1}, and for e{sup -}{sub aq} (2.31{+-}0.06)x10{sup 9}, (0.45{+-}0.01)x10{sup 9}, (1.26{+-}0.01)x10{sup 9}, and (0.69{+-}0.02)x10{sup 9} M{sup -1} s{sup -1}, respectively. To provide additional information on the radicals formed upon oxidation, transient spectra were measured and the overall reaction efficiency determined. Radical-based destruction mechanisms for destruction of the statins are proposed based on the LC-MS determination of the stable reaction by-products formed using {sup 137}Cs {gamma}-irradiation of statin solutions. Knowing the reaction rates, reaction efficiencies and destruction mechanisms of these compounds is essential for the consideration of the use of advanced oxidation/reduction processes for the destruction of statins in aqueous systems.

Development and assembly of equipment for non destructive assay system control using nuclear radiation

International Nuclear Information System (INIS)

Melo, Jose Altino Tupinamba

2006-01-01

Nondestructive Assay (NDA) is applied to machines and components quality tests. These elements would not have a good performance if they were conceived without concern about the mechanical project quality, used materials, manufacture processes and inspection and maintenance methodology. There are constant developments in high level of technology with the objective of guaranteeing the components quality and the good functioning of these machines, in the mechanics, naval, aeronautical, petrochemical and steel industry, energy and nuclear generation as well. The globalization in the industry lines is a fact, leading to an increase in the multinational projects and products. The following questions arise: how to assure the high quality of components and processes? How to optimize the test methods to assure that the materials do not have defects affecting the performance of the components? The answers to the questions above are found in the application of NDA. The complex materials analysis (inhomogeneous) using NDA requires a detailed study of the sensors response signal. In this work, a measure and control system of non destructive processes was developed, using a radioactive source with a defined energy in function of the material to be analyzed. This system involves: (a) Interface of input/output (I/O) (the Hardware) and (b) graphical Interface (Software). In the non destructive analysis, it is made the comparison of the signal proceeding from the sensor with a signal preset (Set Point) or analogical signal of reference (Base Line), which is adjusted in the I/O Interface. Analyzed the signal, the system will make the decision: (a) to reject or (b) to accept the analyzed material. The I/O Interface is implemented by electronic equipment with a MCS51. The purpose of this interface is to supply conditions to exchange information, using serial RS232, between the sensor and the microcomputer. The graphical Interface (software) is written in visual C++ language (author)

Destructive and non-destructive methods of measuring the quantity and isotopic composition of fissile materials for purposes of national safeguards in the German Democratic Republic

International Nuclear Information System (INIS)

Villun, K.; Gruner, V.; Siebert, Kh.U.; Hoffmann, D.

1979-01-01

The authors give a brief description of the destructive and non-destructive methods of measuring the quantity and isotopic composition of fissile materials used in the nuclear materials accounting and control system of the German Democratic Republic. They cite examples of the use of gamma-spectrometry, X-ray fluorescence analysis, neutron activation, radiochemical techniques, mass-spectrometry and alpha-spectrometry. (author)

Non-destructive measurements of nuclear wastes. Validation and industrial operating experience

International Nuclear Information System (INIS)

Saas, A.; Tchemitciieff, E.

1993-01-01

After a short survey of the means employed for the non-destructive measurement of specific activities (γ and X-ray) in waste packages and raw waste, the performances of the device and the ANDRA requirements are presented. The validation of the γ and X-ray measurements on packages is obtained through determining, by destructive means, the same activity on coring samples. The same procedure is used for validating the homogeneity measurements on packages (either homogeneous or heterogeneous). Different operating experiences are then exposed for several kinds of packages and waste. Up to now, about twenty different types of packages have been examined and more than 200 packages have allowed the calibration, validation, and control

Non-destructive examination of a time capsule recovered from the Gore Park excavations, Hamilton, Ontario

International Nuclear Information System (INIS)

MacDonald, B.L.; Vanderstelt, J.

2015-01-01

Non-destructive analytical techniques are becoming increasingly important for the study of objects of cultural heritage interest. We present a study that applied two techniques: x-ray fluorescence (XRF) and neutron radiography, for the investigation of a time capsule recovered from an urban construction site in Gore Park, Hamilton. XRF analysis revealed the composition of the artifact, while n-radiography showed that its contents remained intact after being interred for 91 years. Results of this study demonstrate the value of non-destructive techniques for the analysis and preservation of cultural heritage. (author)

RESEARCH ON NON-DESTRUCTIVE TESTING TECHNOLOGY IN CONSERVATION REPAIR PROJECT OF ANCESTRAL TEMPLE IN MUKDEN PALACE

Directory of Open Access Journals (Sweden)

J. Yang

2017-08-01

Full Text Available Due to the use of wood and other non-permanent materials, traditional Chinese architecture is one of the most fragile constructions in various heritage objects today. With the increasing emphasis on the protection of cultural relics, the repair project of wooden structure has become more and more important. There are various kinds of destructions, which pose a hidden danger to the overall safety of the ancient buildings, caused not only by time and nature, but also by improper repairs in history or nowadays. Today, the use of digital technology is a basic requirement in the conservation of cultural heritage. Detection technology, especially non-destructive testing technology, could provide more accurate records in capturing detailed physical characteristics of structures such as geometric deformation and invisible damage, as well as prevent a man-made destruction in the process of repair project. This paper aims to interpret with a typical example, Ancestral Temple in Mukden Palace, along with a discussion of how to use the non-destructive testing technology with ground penetrating radar, stress wave, resistograph and so on, in addition to find an appropriate protection method in repair project of traditional Chinese wooden architecture.

Research on Non-Destructive Testing Technology in Conservation Repair Project of Ancestral Temple in Mukden Palace

Science.gov (United States)

Yang, J.; Fu, M.

2017-08-01

Due to the use of wood and other non-permanent materials, traditional Chinese architecture is one of the most fragile constructions in various heritage objects today. With the increasing emphasis on the protection of cultural relics, the repair project of wooden structure has become more and more important. There are various kinds of destructions, which pose a hidden danger to the overall safety of the ancient buildings, caused not only by time and nature, but also by improper repairs in history or nowadays. Today, the use of digital technology is a basic requirement in the conservation of cultural heritage. Detection technology, especially non-destructive testing technology, could provide more accurate records in capturing detailed physical characteristics of structures such as geometric deformation and invisible damage, as well as prevent a man-made destruction in the process of repair project. This paper aims to interpret with a typical example, Ancestral Temple in Mukden Palace, along with a discussion of how to use the non-destructive testing technology with ground penetrating radar, stress wave, resistograph and so on, in addition to find an appropriate protection method in repair project of traditional Chinese wooden architecture.

Acceptance criteria for non-destructive examination of double-shell tanks

International Nuclear Information System (INIS)

Jensen, C.E.

1995-09-01

This supporting document provides requirements for acceptance of relevant indications found during non-destructive examination of double-shell tanks (DSTs) at Hanford 200 areas. Requirements for evaluation of relevant indications are provided to determine acceptability of continued safe operation of the DSTs. Areas of the DSTs considered include the tank wall vapor space, liquid-vapor interface, wetted tank wall, sludge-liquid interface, and the knuckle region

New technologies in electromagnetic non-destructive testing

CERN Document Server

Huang, Songling

2016-01-01

This book introduces novel developments in the field of electromagnetic non-destructive testing and evaluation (NDT/E). The topics include electromagnetic ultrasonic guided wave testing, pulsed eddy current testing, remote field eddy current testing, low frequency eddy current testing, metal magnetic memory testing, and magnetic flux leakage testing. Considering the increasing concern about the safety maintenance of critical structures in various industries and everyday life, these topics presented here will be of particular interest to the readers in the NDT/E field. This book covers both theoretical researches and the engineering applications of the electromagnetic NDT technology. It could serve as a valuable reference for college students and relevant NDT technicians. It is also a useful material for qualification training and higher learning for nondestructive testing professionals.

Low frequency electrical and magnetic methods for non-destructive analysis of fiber dispersion in fiber reinforced cementitious composites: an overview.

Science.gov (United States)

Faifer, Marco; Ferrara, Liberato; Ottoboni, Roberto; Toscani, Sergio

2013-01-21

Non-destructive analysis of fiber dispersion in structural elements made of Fiber Reinforced Concrete (FRC) and Fiber Reinforced Cementitious Composites (FRCCs) plays a significant role in the framework of quality control and performance prediction. In this paper, the research activity of the authors in the aforementioned field all over the last lustrum will be reviewed. A method based on the measurement of the inductance of a probe to be placed on the specimen will be presented and its progressive development will be described. Obtained correlation with actual fiber dispersion, as checked by means of destructive methods, as well as with the mechanical performance of the composite will also be presented, in an attempt to address the significance of the method from an engineering application perspective.

Quality assurance and non-destructive testing for nuclear power plants

International Nuclear Information System (INIS)

Manlucu, F.A.

1991-01-01

This article discussed the quality assurance requirements which have been extensively applied in plant design, fabrication, construction and operation and has played a major role in the excellent safety record of nuclear power plants. The application of non-destructive testing techniques, plays a very important role during the in-service inspection (ISI) in order to prevent dangerous accident and to assure continuous safe operation of nuclear power plants. (IMA). 12 refs

Analysis of body fluids for forensic purposes: from laboratory testing to non-destructive rapid confirmatory identification at a crime scene.

Science.gov (United States)

Virkler, Kelly; Lednev, Igor K

2009-07-01

Body fluid traces recovered at crime scenes are among the most important types of evidence to forensic investigators. They contain valuable DNA evidence which can identify a suspect or victim as well as exonerate an innocent individual. The first step of identifying a particular body fluid is highly important since the nature of the fluid is itself very informative to the investigation, and the destructive nature of a screening test must be considered when only a small amount of material is available. The ability to characterize an unknown stain at the scene of the crime without having to wait for results from a laboratory is another very critical step in the development of forensic body fluid analysis. Driven by the importance for forensic applications, body fluid identification methods have been extensively developed in recent years. The systematic analysis of these new developments is vital for forensic investigators to be continuously educated on possible superior techniques. Significant advances in laser technology and the development of novel light detectors have dramatically improved spectroscopic methods for molecular characterization over the last decade. The application of this novel biospectroscopy for forensic purposes opens new and exciting opportunities for the development of on-field, non-destructive, confirmatory methods for body fluid identification at a crime scene. In addition, the biospectroscopy methods are universally applicable to all body fluids unlike the majority of current techniques which are valid for individual fluids only. This article analyzes the current methods being used to identify body fluid stains including blood, semen, saliva, vaginal fluid, urine, and sweat, and also focuses on new techniques that have been developed in the last 5-6 years. In addition, the potential of new biospectroscopic techniques based on Raman and fluorescence spectroscopy is evaluated for rapid, confirmatory, non-destructive identification of a body

Non-destructive digital imaging in poplar allows detailed analysis of adventitious rooting dynamics

Science.gov (United States)

R.J. Kodrzycki; R.B. Michaels; A.L. Friend; R.S. Zalesny; Ch.P. Mawata; D.W. McDonald

2008-01-01

The dynamics of root formation are difficult to observe directly over time without disturbing the rooting environment. A novel system for a non-destructive, non-invasive root analysis (RootViz FS, Phenotype Screening Corp.) was evaluated for its ability to analyze root formation from cuttings over a 32 day period in three poplar genotypes (DN70, P. Deltoides x...

PlantSize Offers an Affordable, Non-destructive Method to Measure Plant Size and Color in Vitro

Directory of Open Access Journals (Sweden)

Dóra Faragó

2018-02-01

Full Text Available Plant size, shape and color are important parameters of plants, which have traditionally been measured by destructive and time-consuming methods. Non-destructive image analysis is an increasingly popular technology to characterize plant development in time. High throughput automatic phenotyping platforms can simultaneously analyze multiple morphological and physiological parameters of hundreds or thousands of plants. Such platforms are, however, expensive and are not affordable for many laboratories. Moreover, determination of basic parameters is sufficient for most studies. Here we describe a non-invasive method, which simultaneously measures basic morphological and physiological parameters of in vitro cultured plants. Changes of plant size, shape and color is monitored by repeated photography with a commercial digital camera using neutral white background. Images are analyzed with the MatLab-based computer application PlantSize, which simultaneously calculates several parameters including rosette size, convex area, convex ratio, chlorophyll and anthocyanin contents of all plants identified on the image. Numerical data are exported in MS Excel-compatible format. Subsequent data processing provides information on growth rates, chlorophyll and anthocyanin contents. Proof-of-concept validation of the imaging technology was demonstrated by revealing small but significant differences between wild type and transgenic Arabidopsis plants overexpressing the HSFA4A transcription factor or the hsfa4a knockout mutant, subjected to different stress conditions. While HSFA4A overexpression was associated with better growth, higher chlorophyll and lower anthocyanin content in saline conditions, the knockout hsfa4a mutant showed hypersensitivity to various stresses. Morphological differences were revealed by comparing rosette size, shape and color of wild type plants with phytochrome B (phyB-9 mutant. While the technology was developed with Arabidopsis plants

First-time observation of Mastro Giorgio masterpieces by means of non-destructive techniques

Science.gov (United States)

Padeletti, G.; Ingo, G. M.; Bouquillon, A.; Pages-Camagna, S.; Aucouturier, M.; Roehrs, S.; Fermo, P.

2006-06-01

For the first time some excellent pieces belonging to the majolica production of the great master Giorgio Andreoli from Gubbio (Central Italy) have been characterized from a chemical and structural point of view with the aim to identify the composition of both pigments and lustres. A series of particle-induced X-ray emission (PIXE), Rutherford backscattering spectrometry (RBS) and Raman analyses have been performed on some plates coming from Museo del Palazzo dei Consoli (Gubbio) and several French museums (Louvre, Musée National de la Céramique, Musée National de la Renaissance) lustred by Giorgio Andreoli and decorated by famous majolica painters such as Francesco Xanto Avelli. The three techniques are complementary and useful in the investigation of art objects since they are non-destructive. Furthermore, the low detection limits allow the identification of all elements and compounds present, and RBS allows concentration profiling, too. It is worth noticing that the examined objects are characterized by the presence of both gold and ruby-red lustres, a peculiarity of Mastro Giorgio’s technique. The measurements by PIXE and RBS have been carried out on the AGLAE accelerator at C2RMF, Louvre Palace.

Study on personnel qualification for non-destructive tests in the field of reactor safety

International Nuclear Information System (INIS)

Trusch, K.; Wuestenberg, H.

1977-01-01

The training system for non-destructive testing is described, and the available and necessary personnel is analyzed; the personnel required for reactor safety problems is treated separately. On this basis, the subjects discussed in the study - available personnel, personnel requirements, training, training requirements, and suggestions for realisation - are treated in a general manner to begin with and afterwards with a view to specific problems of reactor safety. The methods employed are adapted to this situation. To obtain the necessary empirical data, questionnaires were set up and distributed, and experts in selected business companies and institutions were interviewed who work in the field of reactor safety or do same training in non-destructive testing. (orig.) [de

Quality parameters of mango and potential of non-destructive techniques for their measurement- a review

International Nuclear Information System (INIS)

Jha, S.N.; Narsaiah, K.; Sharma, A.D.; Singh, M.; Bansal, S.; Kumar, R.

2010-01-01

The king of fruits 'Mango' (Mangifera indica L.) is very nutritious and rich in carotenes. India produces about 50% of the total world's mango. Many researchers have reported the maturity indices and quality parameters for determination of harvesting time and eating quality. The methods currently used for determination of quality of mango are mostly based on the biochemical analysis, which leads to destruction of the fruits. Numerous works are being carried out to explore some non-destructive methods such as Near Infrared (NIR), Nuclear Magnetic Resonance (NMR), X-ray and Computed Tomography (CT), electronic nose, machine vision and ultrasound for quality determination of fruits. This paper deals with some recent work reported on quality parameters, harvesting and post-harvest treatments in relation to quality of mango fruits and reviews on some of the potential non-destructive techniques that can be explored for quality determination of mango cultivars. (author)

Qualification of non-destructive examination for belgian nuclear reactor pressure vessel inspection

International Nuclear Information System (INIS)

Couplet, D.; Francoise, T.

2001-01-01

In Service Inspection (ISI) participates to the assessment of Nuclear Reactor Pressure Vessel Integrity. The performance of Non Destructive Examination (NDE) techniques must be demonstrated according to predefined objectives. The qualification process is essential to trust the reliability of the information provided by NDE. In Belgian Nuclear Power Plants, the qualification was conducted through a collaboration between the vendor and a technical group from the Electricity Utility. The important facts of this qualification will be presented: - the detailed definition of the inspection and qualifications objectives, based on a combination of the ASME code and the European Methodology for Qualification; - the systematic verification of the NDE performance and limitations, for each ISI objective, through an adequate combination of tests on blocks and technical justification; - the continuous improvement of the NDE procedure; - the feedback and the lessons learnt from site experience; - the necessary multi-disciplinary approach (NDE, degradation mechanisms, structural integrity)

Giant Magnetoresistance Sensors: A Review on Structures and Non-Destructive Eddy Current Testing Applications

Directory of Open Access Journals (Sweden)

Damhuji Rifai

2016-02-01

Full Text Available Non-destructive eddy current testing (ECT is widely used to examine structural defects in ferromagnetic pipe in the oil and gas industry. Implementation of giant magnetoresistance (GMR sensors as magnetic field sensors to detect the changes of magnetic field continuity have increased the sensitivity of eddy current techniques in detecting the material defect profile. However, not many researchers have described in detail the structure and issues of GMR sensors and their application in eddy current techniques for nondestructive testing. This paper will describe the implementation of GMR sensors in non-destructive testing eddy current testing. The first part of this paper will describe the structure and principles of GMR sensors. The second part outlines the principles and types of eddy current testing probe that have been studied and developed by previous researchers. The influence of various parameters on the GMR measurement and a factor affecting in eddy current testing will be described in detail in the third part of this paper. Finally, this paper will discuss the limitations of coil probe and compensation techniques that researchers have applied in eddy current testing probes. A comprehensive review of previous studies on the application of GMR sensors in non-destructive eddy current testing also be given at the end of this paper.

Giant Magnetoresistance Sensors: A Review on Structures and Non-Destructive Eddy Current Testing Applications

Science.gov (United States)

Rifai, Damhuji; Abdalla, Ahmed N.; Ali, Kharudin; Razali, Ramdan

2016-01-01

Non-destructive eddy current testing (ECT) is widely used to examine structural defects in ferromagnetic pipe in the oil and gas industry. Implementation of giant magnetoresistance (GMR) sensors as magnetic field sensors to detect the changes of magnetic field continuity have increased the sensitivity of eddy current techniques in detecting the material defect profile. However, not many researchers have described in detail the structure and issues of GMR sensors and their application in eddy current techniques for nondestructive testing. This paper will describe the implementation of GMR sensors in non-destructive testing eddy current testing. The first part of this paper will describe the structure and principles of GMR sensors. The second part outlines the principles and types of eddy current testing probe that have been studied and developed by previous researchers. The influence of various parameters on the GMR measurement and a factor affecting in eddy current testing will be described in detail in the third part of this paper. Finally, this paper will discuss the limitations of coil probe and compensation techniques that researchers have applied in eddy current testing probes. A comprehensive review of previous studies on the application of GMR sensors in non-destructive eddy current testing also be given at the end of this paper. PMID:26927123

Fast and Accurate Non-destructive Testing System for Inspection of Canning Tubes

DEFF Research Database (Denmark)

Gundtoft, Hans Erik; Nielsen, E.

1973-01-01

The authors describe the development of an inspection bench for the non-destructive examination of canning tubes. The bench is original in that the internal diameter is calculated from exact measurement of the outer diameter and the wall thickness. The transducers for inspection and control are r...

Interactive ultrasonic field simulations for complex non-destructive testing configurations

International Nuclear Information System (INIS)

Chouh, Hamza

2016-01-01

In order to fulfill increasing reliability and safety requirements, non-destructive testing techniques are constantly evolving and so does their complexity. Consequently, simulation is an essential part of their design. We developed a tool for the simulation of the ultrasonic field radiated by any planar probes into non-destructive testing configurations involving meshed geometries without prominent edges, isotropic and anisotropic, homogeneous and heterogeneous materials, and wave trajectories that can include reflections and transmissions. We approximate the ultrasonic wave fronts by using polynomial interpolators that are local to ultrasonic ray pencils. They are obtained using a surface research algorithm based on pencil tracing and successive subdivisions. Their interpolators enable the computation of the necessary quantities for the impulse responses on each point of a sampling of the transducer surface that fulfills the Shannon criterion. By doing so, we can compute a global impulse response which, when convolved with the excitation signal of the transducer, results in the ultrasonic field. The usage of task parallelism and of SIMD instructions on the most computationally expensive steps yields an important performance boost. Finally, we developed a tool for progressive visualization of field images. It benefits from an image reconstruction technique and schedules field computations in order to accelerate convergence towards the final image. (author) [fr

Non-destructive screening method for radiation hardened performance of large scale integration

International Nuclear Information System (INIS)

Zhou Dong; Xi Shanbin; Guo Qi; Ren Diyuan; Li Yudong; Sun Jing; Wen Lin

2013-01-01

The space radiation environment could induce radiation damage on the electronic devices. As the performance of commercial devices is generally superior to that of radiation hardened devices, it is necessary to screen out the devices with good radiation hardened performance from the commercial devices and applying these devices to space systems could improve the reliability of the systems. Combining the mathematical regression analysis with the different physical stressing experiments, we investigated the non-destructive screening method for radiation hardened performance of the integrated circuit. The relationship between the change of typical parameters and the radiation performance of the circuit was discussed. The irradiation-sensitive parameters were confirmed. The pluralistic linear regression equation toward the prediction of the radiation performance was established. Finally, the regression equations under stress conditions were verified by practical irradiation. The results show that the reliability and accuracy of the non-destructive screening method can be elevated by combining the mathematical regression analysis with the practical stressing experiment. (authors)

Non destructive Testing (NDT) of concrete containing hematite

International Nuclear Information System (INIS)

Mohamad Pauzi Ismail; Noor Azreen Masenwat; Suhairy Sani; Nasharuddin Isa; Mohamad Haniza Mahmud

2014-01-01

This paper described the results of Non-destructive ultrasonic and rebound hammer measurements on concrete containing hematite. Local hematite stones were used as aggregates to produce high density concrete for application in X-and gamma shielding. Concrete cube samples (150 mm x 150 mm x 150 mm) containing hematite as coarse aggregates were prepared by changing mix ratio, water to cement ratio (w/c) and types of fine aggregate. All samples were cured in water for 7 days and then tested after 28 days. Density, rebound number(N) and ultrasonic pulse velocity (UPV) of the samples were taken before compressed to failure. The measurement results are explained and discussed. (author)

Elemental chemical characterization of coins of currently national circulating by X-ray fluorescence non-destructive techniques

International Nuclear Information System (INIS)

Olivera, Paula; Calcina, Esly

2013-01-01

Given the frequent counterfeit bills and coins is proposed in this paper to identify the elemental chemical composition; for now, the current official currencies circulating in our country, by Energy Dispersive X-ray Fluorescence technique and non-destructive methods, the goal is to compare with the false and establish the differences that could help identify them immediately taking advantage of the fast response of this technique. Have been identified the elements Al in the coins of 5 cents, Cu and Zn for 10 and 20 cents, Ni, Cu and Zn for 50 cents and a Un Nuevo Sol and Cr, Cu and Zn 2 coins 5 Nuevos Soles. 57 Peruvian coins of different production years and a counterfeit coin of 5 Nuevos Soles have been analyzed, finding Cu and Zn in central part and Fe in circulating edge ring, looking for this one the absence of Ni and Cr, which in the official currency was found. (authors).

A simple, sensitive and non-destructive technique for characterizing bovine dental enamel erosion: attenuated total reflection Fourier transform infrared spectroscopy.

Science.gov (United States)

Kim, In-Hye; Son, Jun Sik; Min, Bong Ki; Kim, Young Kyoung; Kim, Kyo-Han; Kwon, Tae-Yub

2016-03-30

Although many techniques are available to assess enamel erosion in vitro, a simple, non-destructive method with sufficient sensitivity for quantifying dental erosion is required. This study characterized the bovine dental enamel erosion induced by various acidic beverages in vitro using attenuated total reflection Fourier transform infrared (ATR-FTIR) spectroscopy. Deionized water (control) and 10 acidic beverages were selected to study erosion, and the pH and neutralizable acidity were measured. Bovine anterior teeth (110) were polished with up to 1 200-grit silicon carbide paper to produce flat enamel surfaces, which were then immersed in 20 mL of the beverages for 30 min at 37 °C. The degree of erosion was evaluated using ATR-FTIR spectroscopy and Vickers' microhardness measurements. The spectra obtained were interpreted in two ways that focused on the ν1, ν3 phosphate contour: the ratio of the height amplitude of ν3 PO4 to that of ν1 PO4 (Method 1) and the shift of the ν3 PO4 peak to a higher wavenumber (Method 2). The percentage changes in microhardness after the erosion treatments were primarily affected by the pH of the immersion media. Regression analyses revealed highly significant correlations between the surface hardness change and the degree of erosion, as detected by ATR-FTIR spectroscopy (Perosion.

Role of non destructive techniques for monitoring structural integrity of primary circuit of pressurized water reactor nuclear power plant

International Nuclear Information System (INIS)

Sharma, P.K.; Sreenivas, P.

2015-01-01

The safety of nuclear installations is ensured by assessing status of primary equipment for performing the intended function reliably and maintaining the integrity of pressure boundaries. The pressure boundary materials undergo material degradation during the plant operation. Pressure boundary materials are subjected to operating stresses and material degradation that results in material properties changes, discontinuities initiation and increase in size of existing discontinuities. Pre-Service Inspection (PSI) is performed to generate reference base line data of initial condition of the pressure boundary. In-Service Inspections (ISI) are performed periodically to confirm integrity of pressure boundaries through comparison with respect to base line data. The non destructive techniques are deployed considering nature of the discontinuities expected to be generated through operating conditions and degradation mechanisms. The paper is prepared considering Pressurized Water Reactor (PWR) Nuclear Power Plant. The paper describes the degradation mechanisms observed in the PWR nuclear power plants and salient aspect of PSI and ISI and considerations in selecting non destructive testing. The paper also emphasises on application of acoustic emission (AE) based condition monitoring systems that can supplement in-service inspections for detecting and locating discontinuities in pressure boundaries. Criticality of flaws can be quantitatively evaluated by determining their size through in-service inspection. Challenges anticipated in deployment of AE based monitoring system and solutions to cater those challenges are also discussed. (author)

Augmented reality application for industrial non-destructive inspection training

Science.gov (United States)

Amza, Catalin Gheorghe; Zapciu, Aurelian; Teodorescu, Octav

2018-02-01

Such a technology - Augmented Reality (AR) has great potential of use, especially for training purposes of new operators on using expensive equipment. In this context, the paper presents an augmented reality training system developed for phased-array ultrasonic non-destructive testing (NDT) equipment. The application has been developed using Unity 5.6.0 game-engine platform integrated with Vuforia sdk toolkit for devices with Android operating system. The test results performed by several NDT operators showed good results, thus proving the potential of using the application in the industrial field.

Non-destructive test for VHTR fuel using 160kV X-ray system in Hotcell

Energy Technology Data Exchange (ETDEWEB)

Kim, Young Jun; Yoo, Boung Ok; Choo, Yong sun; Baik Sang youl; Kim, Hee Moon; Ahn, Sang Bok [KAERI, Daejeon (Korea, Republic of)

2016-05-15

The research for VHTR which is one of the next generation reactor has been actively carried out. As a part of the research for VHTR, an irradiation examination for the VHTR fuel was performed to confirm an in-pile behavior in HANARO. The non-destructive test for the irradiated fuel is very important to understand the in-pile behavior of the fuel. Especially, the X-ray system is useful to observe the fuel shape without destruction. A dimensional change and defect of the fuel can be confirmed thorough the Xray system. Also, using the 3-D software and CT technology, the fuel shape can be intuitionally observed. The 450kV and 160kV X-ray system were installed and operated in IMEF hotcell. The 160kV X-ray system relatively using a low voltage is suitable to a small scale sample. And high resolution images can be obtained. In this study, the non-destructive test for the unirradiated and irradiated VHTR fuel were performed using the 160kV X-ray system. Through these test, the possibility for the X-ray inspection of irradiated fuel was confirmed. The non-destructive test for the unirradiated and irradiated VHTR fuel were performed using the 160kV X-ray system. The clear images of the irradiated coated particle were produced without the radiation damage during the Xray inspection. The X-ray images of the VHTR fuel will be utilized as the in-pile performance validation data.

Non-destructive test for VHTR fuel using 160kV X-ray system in Hotcell

International Nuclear Information System (INIS)

Kim, Young Jun; Yoo, Boung Ok; Choo, Yong sun; Baik Sang youl; Kim, Hee Moon; Ahn, Sang Bok

2016-01-01

The research for VHTR which is one of the next generation reactor has been actively carried out. As a part of the research for VHTR, an irradiation examination for the VHTR fuel was performed to confirm an in-pile behavior in HANARO. The non-destructive test for the irradiated fuel is very important to understand the in-pile behavior of the fuel. Especially, the X-ray system is useful to observe the fuel shape without destruction. A dimensional change and defect of the fuel can be confirmed thorough the Xray system. Also, using the 3-D software and CT technology, the fuel shape can be intuitionally observed. The 450kV and 160kV X-ray system were installed and operated in IMEF hotcell. The 160kV X-ray system relatively using a low voltage is suitable to a small scale sample. And high resolution images can be obtained. In this study, the non-destructive test for the unirradiated and irradiated VHTR fuel were performed using the 160kV X-ray system. Through these test, the possibility for the X-ray inspection of irradiated fuel was confirmed. The non-destructive test for the unirradiated and irradiated VHTR fuel were performed using the 160kV X-ray system. The clear images of the irradiated coated particle were produced without the radiation damage during the Xray inspection. The X-ray images of the VHTR fuel will be utilized as the in-pile performance validation data.

Kinetics and mechanism of azo dye destruction in advanced oxidation processes

International Nuclear Information System (INIS)

Wojnarovits, L.; Palfi, T.; Takacs, E.

2007-01-01

The kinetics and mechanism of dye destruction in advanced oxidation processes is discussed on the example of Apollofix Red (Ar-28) radiolysis in aqueous solution. When the reactive intermediate reacts with the color bearing part of the molecule causing with nearly 100% efficiency destruction of the conjugation, the dose dependence, or time dependence of color disappearance is linear. In this case, spectrophotometry can be used to follow-up dye decomposition. Linear dependence was observed when hydrated electrons or hydrogen atoms reacted with the dye. In hydroxyl radical reactions some colored products form with spectra similar to those of the starting dye molecules. For that reason, spectrophotometry gives false result about the intact dye molecule concentration. Analysis by the HPLC reveals logarithmic time dependence in agreement with a theoretical model developed

Quality assurance in ceramic materials and components. High-resolution non-destructive testing especially of ceramic surfaces

International Nuclear Information System (INIS)

Reiter, H.; Hoffmann, B.; Morsch, A.; Arnold, W.; Schneider, E.

1988-01-01

This report discusses the influence of defects on the failure behavior of ceramic materials under four-point bending stress. In this connection various Si 3 N 4 and SiC materials with and without artificially introduced defect particles (Fe, WC, Si, pores) were examined by the following non-destructive test methods: photoacoustic microscopy, scanning laser acoustic microscopy, microfocus roentgenoscopy and ultrasound transit-time measurements. Finally, a four-point bending test and a fracture-mechanical evaluation of the fracture-incuding defects were carried out at the Institute for reliability and failure studies in mechanical engineering of the University of Karlsruhe. According to the type of stress the samples predominantly failed in the case of defects in the surface zone of the side in tension. Among the ndt methods applied the photoacoustic microscopy as a typical surface testing method could predict most of the fracture-inducing defects (30-50 %) without causing destruction. In this connection a different detection sensitivity which corresponds to the thermal reflection factors became apparent according to the type of defect. Furthermore the reports describes the results of some preliminary tests on ndt of green ceramics. In these investigations both the microfocus roentgenoscopy test and the roentgen computed tomography showed a high potential of detecting inhomogeneities and defects in green Si 3 N 4 and SiC components. (orig.) [de

Non-Destructive Method by Gamma Sampling Measurements for Radiological Characterization of a Steam Generator: Physical and Numerical Modeling for ANIMMA (23-27 June 2013)

International Nuclear Information System (INIS)

Auge, G.; Rottner, B.; Dubois, C.

2013-06-01

The radiological characterization of a steam generator consists of evaluating the global radiological activity in the tube bundle. In this paper, we present a non-destructive method and the results analysis of the gamma sampling measurements from a sample of U-tubes in the bundle. On site, the implementation of the methodology is fairly easy. But the analysis of the results is more complicated due to the long path of the gamma ray (from 60 Co quite penetrating), and also the heterogeneous activity of U-tubes bundle, which have not the same life cycle. We explain why the periodic spatial arrangement complicates also the analysis. Furthermore, we have taken into account the environment of all tubes measured because of all the external influence activity of others U-tubes (the nearest, the most distant and potential hot spot). A great amount of independent influence coefficient had to be considered (roughly 18 million). Based on a physical and numerical modeling, and using a Cholesky algorithm solving the problem and saving time machine. (authors)

Non destructive evaluation of containment nuclear plants structures

Energy Technology Data Exchange (ETDEWEB)

Garnier, V. [Aix Marseille Univ., Aix en Provence (France). LMA, CNRS UPR 7051, IUT; Verdier, J. [Toulouse Univ. (France). UPS, INSA, LMDC; Sbartai, Z.M. [Bordeaux Univ., Talence (France). I2M; and others

2015-07-01

French Projects of Investment for the Future, called ''Research for Nuclear Safety and Radiation Protection'' have been initiated to further research on the causes, the management, the impact of the observed nuclear accidents and to propose and validate solutions to limit the risk and the consequences. In this context the ''Non Destructive Evaluation of nuclear plants containment'' project (ENDE) with eight partners (six research institutes and two industrials) supported by the ''National Agency of Research'', proposes a methodology for the Non Destructive Evaluation of the containment capacity to fulfil its two major functions: strength and leak tightness. The NDE measurements will be performed under conditions representing the specific solicitations of a decennial inspection, and after or during a reference accident. The project aims to develop NDEs, to combine them by data fusion and to select the most efficient combinations with quantitative criteria. The work is based on: - Structuring the knowledge and developing an experimental plan. - Evaluating the material in representative conditions of accidental solicitations (water saturation, porosity, strength, elastic modulus, stress) and the diffuse thermal damage (micro cracks) - Monitoring the transition from diffuse to continuous damage (cracks) and monitoring a crack under stress (opening and width). - Implementing ND Techniques on-site. The ND techniques retained after selection will be implemented on a containment mock-up on the 1/3 scale. This mock-up developed by EDF (Electricite de France) will be available in 2016. It will be comparable to those of real size containment regarding pressure and temperature conditions. The measures deduced from the NDEs will be introduced in another project (Macena) that aims to simulate the water and heat transfers as well as creep occurring in a reference accident. We will present the methodology and the results

Endoplasmic reticulum stress as a novel mechanism in amiodarone-induced destructive thyroiditis.

Science.gov (United States)

Lombardi, Angela; Inabnet, William Barlow; Owen, Randall; Farenholtz, Kaitlyn Ellen; Tomer, Yaron

2015-01-01

Amiodarone (AMIO) is one of the most effective antiarrhythmic drugs available; however, its use is limited by a serious side effect profile, including thyroiditis. The mechanisms underlying AMIO thyroid toxicity have been elusive; thus, identification of novel approaches in order to prevent thyroiditis is essential in patients treated with AMIO. Our aim was to evaluate whether AMIO treatment could induce endoplasmic reticulum (ER) stress in human thyroid cells and the possible implications of this effect in AMIO-induced destructive thyroiditis. Here we report that AMIO, but not iodine, significantly induced the expression of ER stress markers including Ig heavy chain-binding protein (BiP), phosphoeukaryotic translation initiation factor 2α (eIF2α), CCAAT/enhancer-binding protein homologous protein (CHOP) and spliced X-box binding protein-1 (XBP-1) in human thyroid ML-1 cells and human primary thyrocytes. In both experimental systems AMIO down-regulated thyroglobulin (Tg) protein but had little effect on Tg mRNA levels, suggesting a mechanism involving Tg protein degradation. Indeed, pretreatment with the specific proteasome inhibitor MG132 reversed AMIO-induced down-regulation of Tg protein levels, confirming a proteasome-dependent degradation of Tg protein. Corroborating our findings, pretreatment of ML-1 cells and human primary thyrocytes with the chemical chaperone 4-phenylbutyric acid completely prevented the effect of AMIO on both ER stress induction and Tg down-regulation. We identified ER stress as a novel mechanism contributing to AMIO-induced destructive thyroiditis. Our data establish that AMIO-induced ER stress impairs Tg expression via proteasome activation, providing a valuable therapeutic avenue for the treatment of AMIO-induced destructive thyroiditis.

Improving the Repair Planning System for Mining Equipment on the Basis of Non-destructive Evaluation Data

Science.gov (United States)

Drygin, Michael; Kuryshkin, Nicholas

2017-11-01

The article tells about forming a new concept of scheduled preventive repair system of the equipment at coal mining enterprises, based on the use of modem non-destructive evaluation methods. The approach to the solution for this task is based on the system-oriented analysis of the regulatory documentation, non-destructive evaluation methods and means, experimental studies with compilation of statistics and subsequent grapho-analytical analysis. The main result of the work is a feasible explanation of using non-destructive evaluation methods within the current scheduled preventive repair system, their high efficiency and the potential of gradual transition to condition-based maintenance. In practice wide use of nondestructive evaluation means w;ill allow to reduce significantly the number of equipment failures and to repair only the nodes in pre-accident condition. Considering the import phase-out policy, the solution for this task will allow to adapt the SPR system to Russian market economy conditions and give the opportunity of commercial move by reducing the expenses for maintenance of Russian-made and imported equipment.

An accurate method for determining residual stresses with magnetic non-destructive techniques in welded ferromagnetic steels

International Nuclear Information System (INIS)

Vourna, P

2016-01-01

The scope of the present research work was to investigate the proper selection criteria for developing a suitable methodology for the accurate determination of residual stresses existing in welded parts. Magnetic non-destructive testing took place by the use of two magnetic non-destructive techniques: by the measurement of the magnetic Barkhausen noise and by the evaluation of the magnetic hysteresis loop parameters. The spatial distribution of residual stresses in welded metal parts by both non-destructive magnetic methods and two diffraction methods was determined. The conduction of magnetic measurements required an initial calibration of ferromagnetic steels. Based on the examined volume of the sample, all methods used were divided into two large categories: the first one was related to the determination of surface residual stress, whereas the second one was related to bulk residual stress determination. The first category included the magnetic Barkhausen noise and the X-ray diffraction measurements, while the second one included the magnetic permeability and the neutron diffraction data. The residual stresses determined by the magnetic techniques were in a good agreement with the diffraction ones. (paper)

Non-Destructive Evaluation Method Based On Dynamic Invariant Stress Resultants

Directory of Open Access Journals (Sweden)

Zhang Junchi

2015-01-01

Full Text Available Most of the vibration based damage detection methods are based on changes in frequencies, mode shapes, mode shape curvature, and flexibilities. These methods are limited and typically can only detect the presence and location of damage. Current methods seldom can identify the exact severity of damage to structures. This paper will present research in the development of a new non-destructive evaluation method to identify the existence, location, and severity of damage for structural systems. The method utilizes the concept of invariant stress resultants (ISR. The basic concept of ISR is that at any given cross section the resultant internal force distribution in a structural member is not affected by the inflicted damage. The method utilizes dynamic analysis of the structure to simulate direct measurements of acceleration, velocity and displacement simultaneously. The proposed dynamic ISR method is developed and utilized to detect the damage of corresponding changes in mass, damping and stiffness. The objectives of this research are to develop the basic theory of the dynamic ISR method, apply it to the specific types of structures, and verify the accuracy of the developed theory. Numerical results that demonstrate the application of the method will reflect the advanced sensitivity and accuracy in characterizing multiple damage locations.

Using magnetic levitation for non-destructive quality control of plastic parts.

Science.gov (United States)

Hennek, Jonathan W; Nemiroski, Alex; Subramaniam, Anand Bala; Bwambok, David K; Yang, Dian; Harburg, Daniel V; Tricard, Simon; Ellerbee, Audrey K; Whitesides, George M

2015-03-04

Magnetic levitation (MagLev) enables rapid and non-destructive quality control of plastic parts. The feasibility of MagLev as a method to: i) rapidly assess injection-molded plastic parts for defects during process optimization, ii) monitor the degradation of plastics after exposure to harsh environmental conditions, and iii) detect counterfeit polymers by density is demonstrated. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Method and equipment for the non-destructive analysis of nuclear fuels

International Nuclear Information System (INIS)

Michaelis, W.

1975-01-01

This is a method for the non-destructive analysis of the content of fissile isotopes in nuclear fuels. In this analysis a neutron beam is directed to the nuclear fuel which is to be analysed. The beam penetrates the nuclear fuel, thus causing a secondany radiation by nuclear reactions which reaches a space directly surrounding the nuclear fuel and is measuned there. (orig./UA) [de

Control of abusive water addition to Octopus vulgaris with non-destructive methods.

Science.gov (United States)

Mendes, Rogério; Schimmer, Ove; Vieira, Helena; Pereira, João; Teixeira, Bárbara

2018-01-01

Abusive water addition to octopus has evidenced the need for quick non-destructive methods for product qualification in the industry and control of fresh commercial products in markets. Electric conductivity (EC)/pH and dielectric property measurements were selected to detect water uptake in octopus. A significant EC decrease was determined after soaking octopus in freshwater for 4 h. EC reflected the water uptake of octopus and the correspondent concentration decrease of available ions in the interstitial fluid. Significant correlations were determined between octopus water uptake, EC (R = -0.940) and moisture/protein (M/P) ratio (R = 0.923) changes. Seasonal and spatial variation in proximate composition did not introduce any uncertainty in EC discrimination of freshwater tampering. Immersion in 5 g L -1 sodium tripolyphosphate (STPP) increased EC to a value similar to control octopus. EC false negatives resulting from the use of additives (STPP and citric acid) were eliminated with the additional determination of pH. Octopus soaked in freshwater, STPP and citric acid can also be clearly discriminated from untreated samples (control) and also from frozen (thawed) ones using the dielectric properties. No significant differences in the dielectric property scores were found between octopus sizes or geographical locations. Simultaneous EC/pH or dielectric property measurements can be used in a handheld device for non-destructive water addition detection in octopus. M/P ratio can be used as a reference destructive method. © 2017 Society of Chemical Industry. © 2017 Society of Chemical Industry.

Multiparameter thermo-mechanical OCT-based characterization of laser-induced cornea reshaping

Science.gov (United States)

Zaitsev, Vladimir Yu.; Matveyev, Alexandr L.; Matveev, Lev A.; Gelikonov, Grigory V.; Vitkin, Alex; Omelchenko, Alexander I.; Baum, Olga I.; Shabanov, Dmitry V.; Sovetsky, Alexander A.; Sobol, Emil N.

2017-02-01

Phase-sensitive optical coherence tomography (OCT) is used for visualizing dynamic and cumulative strains and corneashape changes during laser-produced tissue heating. Such non-destructive (non-ablative) cornea reshaping can be used as a basis of emerging technologies of laser vision correction. In experiments with cartilaginous samples, polyacrilamide phantoms and excised rabbit eyes we demonstrate ability of the developed OCT system to simultaneously characterize transient and cumulated strain distributions, surface displacements, scattering tissue properties and possibility of temperature estimation via thermal-expansion measurements. The proposed approach can be implemented in perspective real-time OCT systems for ensuring safety of new methods of laser reshaping of cornea.

Ultrasonic non-destructive testing of pieces of complex geometry with a flexible phased array transducer

Science.gov (United States)

Chatillon; Cattiaux; Serre; Roy

2000-03-01

Ultrasonic non-destructive testing of components of complex geometry in the nuclear industry faces several difficulties: sensitivity variations due to unmatched contact, inaccurate localization of defects due to variations of transducer orientation, and uncovered area of the component. To improve the performances of such testing and defect characterization, we propose a new concept of ultrasonic contact phased array transducer. The phased array transducer has a flexible radiating surface able to fit the actual surface of the piece to optimize the contact and thus the sensitivity of the test. To control the transmitted field, and therefore to improve the defect characterization, a delay law optimizing algorithm is developed. To assess the capability of such a transducer, the Champ-Sons model, developed at the French Atomic Energy Commission for predicting field radiated by arbitrary transducers into pieces, has to be extended to sources directly in contact with pieces of complex geometry. The good behavior of this new type of probe predicted by computations is experimentally validated with a jointed transducer positioned on pieces of various profiles.

Training guidelines in non-destructive testing techniques

International Nuclear Information System (INIS)

1991-10-01

Non-destructive testing methods (NDT), by their very nature, allow components to be fully examined for properties or flaws without interfering with their usefulness. This grouping of inspection methods has grown from a handful of primitive techniques practised by artists to a widely known discipline which is an essential part of quality control, largely as a result of the standards demanded by the nuclear and aerospace industries. Recognizing the need for an international publication of NDT training syllabi, the IAEA Consultants Meeting on ''Qualification and Certification of NDT Personnel'' (Milan, 20-21 May 1986), recommended that the Agency publish the guidelines developed by Regional Working Group of the Latin America and Caribbean project. It was first issued in English in 1987 and has now been re-edited in English and Spanish and enlarged by the addition of programmes for other techniques

Metabolic self-destruction in critically ill patients: origins, mechanisms and therapeutic principles.

Science.gov (United States)

Hartl, Wolfgang H; Jauch, Karl-Walter

2014-03-01

The aim of this study was to describe the evolution and nature of self-destructive metabolic responses observed in critically ill patients, and to analyze therapeutic principles on how best to avoid or diminish these responses. We electronically identified articles through a search of PubMed and Google Scholar. Metabolic reactions associated with surgical injury or infections comprise hyperglycemia, insulin resistance, increased hepatic glucose production, and muscle protein breakdown. From an evolutionary perspective, these responses have been necessary and successful to overcome spontaneously survivable insults (minor surgical trauma). If prolonged and exaggerated, however, these reactions may become self-destructive, causing secondary metabolic damage. There is overwhelming evidence that extreme metabolic responses have not been selected by evolution, but are brought about by modern medicine enabling survival of severe, otherwise lethal insults and giving patients the chance to develop such exaggerated self-destructive metabolic reactions. Poorly adapted metabolic responses to severe insults, however, may have persisted because of unavoidable evolutionary constraints. Self-destructive metabolic responses cannot be prevented by adjuvant therapies such as artificial nutrition, which may only help to ameliorate secondary metabolic damage. Minor surgical trauma is associated with a beneficial adaptive metabolic response. After a severe insult, however, emergence of self-destructive responses will be unavoidable if the patient survives the acute phase. Effective treatment is only possible by an aggressive therapy of underlying pathologies (such as shock, trauma or infection) thereby interrupting secondary metabolic trigger mechanisms at an early stage. Copyright © 2014 Elsevier Inc. All rights reserved.

Isotope techniques in non-destructive testing of dynamic systems

International Nuclear Information System (INIS)

Singh, Gursharan; Pant, H.J.

1996-01-01

A few applications of gamma scanning and radiotracer techniques for Non-destructive Testing (NDT) of dynamic systems in chemical and petrochemical industries are briefly discussed in this paper. Examples of gamma scanning inspections carried out for troubleshooting of various types of columns such as vacuum, extraction, separator and rectifier, with trays and packed beds and having diameters from 1 meter to 8.4 meters are given. Radiotracer applications for Residence Time Distribution (RTD) studies on different systems like an aniline production reactor in a chemical industry and a laboratory scale solid-liquid fluidized bed column are mentioned. (author)

Integrated non-destructive assessment of relevant structural elements of an Italian heritage site: the Carthusian monastery of Trisulti

International Nuclear Information System (INIS)

Rainieri, C; Marra, A; Gargaro, D; Fabbrocino, G; Rainieri, G M; Pepe, M

2015-01-01

The analysis of historical structures in need of preservation and restoration interventions is a very complex task due to the large uncertainties in the characterization of structural properties and detailing in view of the structural response. Moreover, the predictive performance of numerical analyses and simulations depend on the availability of information about the constructional properties of the architectural complex, crack patterns and active degradation phenomena. In particular, local changes in material properties or damage due to past events (such as earthquakes) can affect individual structural elements. They can be hardly detected as a result of the maintenance interventions carried out over the centuries and the possibility to carry out limited or even no destructive investigations due to the historical relevance of the structure. Thus, non-destructive investigations play a fundamental role in the assessment of historical structures minimizing, at the same time, the invasiveness of interventions. The present paper deals with an explanatory case study concerning the structural investigations carried out in view of the seismic assessment of an Italian historical monument, the Carthusian monastery of Trisulti in Collepardo, erected in 1204 under Pope Innocenzo HI. The relevance of the case study is due to the application, in combination, of different NDT methods, such as sonic tests, and active and passive infrared thermography, in order to characterize relevant masonry elements. Moreover, an advanced system for the in-situ nondestructive vibration-based estimation of the tensile loads in ancient tie-rods is described and the main results obtained from its application for the characterization of the tie-rods of the cloister are presented. (paper)

The Combine Use of Semi-destructive and Non-destructive Methods for Tiled Floor Diagnostics

Science.gov (United States)

Štainbruch, Jakub; Bayer, Karol; Jiroušek, Tomáš; Červinka, Josef

2017-04-01

The combination of semi-destructive and non-destructive methods was used to asset the conditions of a tiled floor in the historical monument Minaret, situated in the park complex of the Chateau Lednice (South Moravia Region, Czech Republic), before its renovation. Another set of measurements is going to be performed after the conservation works are finished. (The comparison of the results collected during pre- and post-remediation measurements will be known and presented during the General Assembly meeting in Wien.) The diagnostic complex of methods consisted of photogrammetry, resistivity drilling and georadar. The survey was aimed to contour extends of air gaps beneath the tiles and the efficiency of filling gaps by means of injection, consolidation and gluing individual layers. The state chateau Lednice creates a part of the Lednice-Valtice precinct, a UNESCO landmark, and belongs among the greatest historic monuments in Southern Moravia. In the chateau park there is a romantic observation tower in the shape of a minaret built according to the plans of Josef Hardtmuth between 1798-1804. The Minaret has been extensively renovated for many decades including the restoration of mosaic floors from Venetian terazzo. During the static works of the Minaret building between 1999-2000, the mosaic floors in the rooms on the second floor were transferred and put back onto concrete slabs. Specifically, the floor was cut up to tiles and these were glued to square slabs which were then attached to the base plate. The transfer was not successful and the floor restoration was finalized between 2016-2017. The damage consisted in separating the original floor from the concrete plate which led to creating gaps. Furthermore, the layers of the floor were not compact. It was necessary to fill the gaps and consolidate and glue the layers. The existence of air gap between individual layers of the tiles and their degradation was detected using two different diagnostic methods: semi-destructive

Synthesis & Studies of New Non-Destructive Read-Out Materials for Optical Storage and Optical Switches

National Research Council Canada - National Science Library

Rentzepis, Peter M

2005-01-01

.... The optical, chemical and spectroscopic properties of this non-destructive write/read/erase computer memory material have been studied This organic storage system consists of two different molecular...

Project GRETE: evaluation of non destructive testing techniques for monitoring of material degradation

International Nuclear Information System (INIS)

Coste, J.F.

2001-01-01

The material aging of major critical components of nuclear installations due to in-service conditions may lead to a degradation of their mechanical characteristics. The early detection of material changes and their monitoring using innovative non destructive testing techniques would allow to plan actions in order to prevent the apparition of macroscopic damage (e.g. cracks). One major difficulty in using these particular techniques is to correlate the changes in the measured NDT signals to the microstructural changes in the material due to aging. This problem may be solved through careful microstructural examinations of the material damage. The objective of the project GRETE is to illustrate the potential use of NDT techniques for the monitoring of material degradation through two examples: neutron irradiation of reactor pressure vessel steel and thermal fatigue of piping. The purpose of this paper is to present the project and its programme of work. (author)

Non-Destructive Detection and Separation of Radiation Damaged Cells in Miniaturized, Inexpensive Device, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — There is a clear and well-identified need for rapid, efficient, non-destructive detection and isolation of radiation damaged cells. Available commercial technologies...

Applying thermal neutron radiography to non-destructive assays of dynamic systems

International Nuclear Information System (INIS)

Silvani, Maria I.; Almeida, Gevaldo L. de; Goncalves, Marcelo J.; Lopes, Ricardo T.

2008-01-01

Dynamic processes or systems frequently can not have their behavior directly analyzed due to safety reasons or because they require destructive assays, which can not be always afforded when high-cost equipment, devices and components are involved. Under these circumstances, some kind of non-destructive technique should be applied to preserve the safety of the personnel performing the assay, as well as the integrity of the piece being inspected. Thermal neutrons are specially suited as a tool for this purpose, thanks to their capability to pass through metallic materials, which could be utterly opaque to X-rays. This paper describes the accomplishments achieved at the Instituto de Engenharia Nuclear / CNEN, Brazil, aiming at the development of an Image Acquisition System capable to perform non-destructive assays using thermal neutrons. It is comprised of a thermal neutron source provided by the Argonauta research reactor, a converter-scintillating screen, and a CCD-based video camera optically coupled to the screen through a dark chamber equipped with a mirror. The developed system has been used to acquire 2D neutron radiographic images of static devices to reveal their inner structure, as well as movies of running systems and working devices to verify its functioning and soundness. Radiographic images of objects taken at different angles would be later on used as projections to retrieve - through a proper unfolding software - their 3D images expressed as attenuation coefficients for thermal neutrons. A quantitative performance of the system has been assessed through its Modulation Transfer Function - MTF. In order to determine this curve, unique collimators designed to simulate different spatial frequencies have been manufactured. Besides that, images of some objects have been acquired with the system being developed as well as using the conventional radiographic film, allowing thus a qualitative comparison between them. (author)

In situ non-destructive measurement of biofilm thickness and topology in an interferometric optical microscope.

Science.gov (United States)

Larimer, Curtis; Suter, Jonathan D; Bonheyo, George; Addleman, Raymond Shane

2016-06-01

Biofilms are ubiquitous and impact the environment, human health, dental hygiene, and a wide range of industrial processes. Biofilms are difficult to characterize when fully hydrated, especially in a non-destructive manner, because of their soft structure and water-like bulk properties. Herein a method of measuring and monitoring the thickness and topology of live biofilms of using white light interferometry is described. Using this technique, surface morphology, surface roughness, and biofilm thickness were measured over time without while the biofilm continued to grow. The thickness and surface topology of a P. putida biofilm were monitored growing from initial colonization to a mature biofilm. Measured thickness followed expected trends for bacterial growth. Surface roughness also increased over time and was a leading indicator of biofilm growth. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Non-destructive sampling of rock-dwelling microbial communities using sterile adhesive tape.

Science.gov (United States)

Cutler, Nick A; Oliver, Anna E; Viles, Heather A; Whiteley, Andrew S

2012-12-01

Building stone provides a habitat for an array of microorganisms, many of which have been demonstrated to have a deleterious effect on the appearance and/or structural integrity of stone masonry. It is essential to understand the composition and structure of stone-dwelling (lithobiontic) microbial communities if successful stone conservation strategies are to be applied, particularly in the face of global environmental change. Ideally, the techniques used to sample such assemblages should be non-destructive due to the sensitive conservation status of many stone buildings. This paper quantitatively assesses the performance of sterile adhesive tape as a non-destructive sampling technique and compares the results of tape sampling with an alternative, destructive, sampling method. We used DNA fingerprinting (TRFLP) to characterise the algal, fungal and bacterial communities living on a stone slab. Our results demonstrate that tape sampling may be used to collect viable quantities of microbial DNA from environmental samples. This technique is ideally suited to the sampling of microbial biofilms, particularly when these communities are dominated by green algae. It provides a good approximation of total community diversity (i.e. the aggregate diversity of epilithic and endolithic communities). Tape sampling is straightforward, rapid and cost effective. When combined with molecular analytical techniques, this sampling method has the potential to make a major contribution to efforts to understand the structure of lithobiontic microbial communities and our ability to predict the response of such communities to future environmental change. Copyright © 2012 Elsevier B.V. All rights reserved.

Non-destructive evaluation of the hidden voids in integrated circuit packages using terahertz time-domain spectroscopy

International Nuclear Information System (INIS)

Park, Sung-Hyeon; Kim, Hak-Sung; Jang, Jin-Wook

2015-01-01

In this work, a terahertz time-domain spectroscopy (THz-TDS) imaging technique was used as a non-destructive inspection method for detecting voids in integrated circuit (IC) packages. Transmission and reflection modes, with an angle of incidence of 30°, were used to detect voids in IC packages. The locations of the detected voids in the IC packages could be calculated by analyzing THz waveforms. Finally, voids that are positioned at the different interfaces in the IC package samples could be successfully detected and imaged. Therefore, this THz-TDS imaging technique is expected to be a promising technique for non-destructive evaluation of IC packages. (paper)

39 CFR 762.41 - Advice of non-receipt or loss, destruction, or mutilation.

Science.gov (United States)

2010-07-01

... Center, P.O. Box 14963, St. Louis, MO 63182, describing the Disbursement Postal Money Order, stating the...; DISBURSEMENT POSTAL MONEY ORDERS DISBURSEMENT POSTAL MONEY ORDERS Issuance of Substitutes for Lost, Destroyed, Mutilated, and Defaced Disbursement Postal Money Orders § 762.41 Advice of non-receipt or loss, destruction...

Evaluation of the MIT-Scan-T2 for non-destructive PCC pavement thickness determination.

Science.gov (United States)

2008-07-01

The MIT-Scan-T2 device is marketed as a non-destructive way to determine pavement thickness on both : HMA and PCC pavements. PCC pavement thickness determination is an important incentivedisincentive : measurement for the Iowa DOT and contractors. Th...

A spatially offset Raman spectroscopy method for non-destructive detection of gelatin-encapsulated powders

Science.gov (United States)

Non-destructive subsurface detection of encapsulated, coated, or seal-packaged foods and pharmaceuticals can help prevent distribution and consumption of counterfeit or hazardous products. This study used a Spatially Offset Raman Spectroscopy (SORS) method to detect and identify urea, ibuprofen, and...

Multispectral UV imaging for fast and non-destructive quality control of chemical and physical tablet attributes

DEFF Research Database (Denmark)

Klukkert, Marten; Wu, Jian X; Rantanen, Jukka

2016-01-01

Monitoring of tablet quality attributes in direct vicinity of the production process requires analytical techniques that allow fast, non-destructive, and accurate tablet characterization. The overall objective of this study was to investigate the applicability of multispectral UV imaging...... as a reliable, rapid technique for estimation of the tablet API content and tablet hardness, as well as determination of tablet intactness and the tablet surface density profile. One of the aims was to establish an image analysis approach based on multivariate image analysis and pattern recognition to evaluate...... the potential of UV imaging for automatized quality control of tablets with respect to their intactness and surface density profile. Various tablets of different composition and different quality regarding their API content, radial tensile strength, intactness, and surface density profile were prepared using...

Optical metrics of the extracellular matrix predict compositional and mechanical changes after myocardial infarction

Science.gov (United States)

Quinn, Kyle P.; Sullivan, Kelly E.; Liu, Zhiyi; Ballard, Zachary; Siokatas, Christos; Georgakoudi, Irene; Black, Lauren D.

2016-11-01

Understanding the organization and mechanical function of the extracellular matrix (ECM) is critical for the development of therapeutic strategies that regulate wound healing following disease or injury. However, these relationships are challenging to elucidate during remodeling following myocardial infarction (MI) due to rapid changes in cellularity and an inability to characterize both ECM microstructure and function non-destructively. In this study, we overcome those challenges through whole organ decellularization and non-linear optical microscopy to directly relate the microstructure and mechanical properties of myocardial ECM. We non-destructively quantify collagen organization, content, and cross-linking within decellularized healthy and infarcted myocardium using second harmonic generation (SHG) and two photon excited autofluorescence. Tensile mechanical testing and compositional analysis reveal that the cumulative SHG intensity within each image volume and the average collagen autofluorescence are significantly correlated with collagen content and elastic modulus of the ECM, respectively. Compared to healthy ECM, infarcted tissues demonstrate a significant increase in collagen content and fiber alignment, and a decrease in cross-linking and elastic modulus. These findings indicate that cross-linking plays a key role in stiffness at the collagen fiber level following infarction, and highlight how this non-destructive approach to assessing remodeling can be used to understand ECM structure-function relationships.

Combined Non-destructive Testing (NDT) methods for evaluating concrete quality

International Nuclear Information System (INIS)

Mohamad Pauzi Ismail; Noor Azreen Masenwat; Suhairy Sani; Nasharuddin Isa; Mohamad Haniza Mahmud

2014-01-01

This paper described the results of combining Non-destructive measurements on concrete. Local crushed granite and hematite were used as coarse aggregates; mining sand and river sand were used as fine aggregates to produce various density and strength of concrete. Concrete samples (150 mm cubes and interlocked blocks) were prepared by changing mix ratio, water to cement ratio (w/c) and types of aggregates. Density, rebound number(N) and ultrasonic pulse velocity (UPV) of the samples were taken before compressed to failure. The measurement results are explained and discussed. (author)

Non-destructive provenance differentiation of prehistoric pigments by external PIXE

International Nuclear Information System (INIS)

Beck, L.; Salomon, H.; Lahlil, S.; Lebon, M.; Odin, G.P.; Coquinot, Y.; Pichon, L.

2012-01-01

The elemental analysis of minerals/rocks has been often used for the determination of their geological origin. When these natural rocks were exploited by prehistoric civilizations as objects, weapons, or pigments, the composition of the minerals can provide information on the mobility, the exchanges and the interaction between groups of population. In this paper, we will present results obtained from archaeological samples of prehistoric pigments, mainly iron and manganese oxides. PIXE analysis has been applied to samples of the prehistoric cave “La grotte du Renne” in Arcy-sur-Cure, France (Chatelperronian, 38,000–34,000 BP). Because most of the archaeological objects are decorated or display some use marks, it is not possible to take samples. Consequently, we have used a non-destructive technique thanks to the external beam of AGLAE (C2RMF, Paris). In order to improve the limits of detection (LOD less than 10 ppm from Cu to Sb), a metal absorber has been placed on the X-ray detector to preferentially filter the Fe–K or Mn–K lines. Based on the quantitative analysis of major and trace elements, we have obtained groups of compositions corresponding to different geological sources. We demonstrate in this study that it is possible to extend PIXE analysis to the characterization of prehistoric pigments such as iron and manganese oxides for differentiating potential sources of pigments in archaeological contexts.

Analysis of non-destructive current simulators of flux compression generators.

Science.gov (United States)

O'Connor, K A; Curry, R D

2014-06-01

Development and evaluation of power conditioning systems and high power microwave components often used with flux compression generators (FCGs) requires repeated testing and characterization. In an effort to minimize the cost and time required for testing with explosive generators, non-destructive simulators of an FCG's output current have been developed. Flux compression generators and simulators of FCGs are unique pulsed power sources in that the current waveform exhibits a quasi-exponential increasing rate at which the current rises. Accurately reproducing the quasi-exponential current waveform of a FCG can be important in designing electroexplosive opening switches and other power conditioning components that are dependent on the integral of current action and the rate of energy dissipation. Three versions of FCG simulators have been developed that include an inductive network with decreasing impedance in time. A primary difference between these simulators is the voltage source driving them. It is shown that a capacitor-inductor-capacitor network driving a constant or decreasing inductive load can produce the desired high-order derivatives of the load current to replicate a quasi-exponential waveform. The operation of the FCG simulators is reviewed and described mathematically for the first time to aid in the design of new simulators. Experimental and calculated results of two recent simulators are reported with recommendations for future designs.

Models on reliability of non-destructive testing

International Nuclear Information System (INIS)

Simola, K.; Pulkkinen, U.

1998-01-01

The reliability of ultrasonic inspections has been studied in e.g. international PISC (Programme for the Inspection of Steel Components) exercises. These exercises have produced a large amount of information on the effect of various factors on the reliability of inspections. The information obtained from reliability experiments are used to model the dependency of flaw detection probability on various factors and to evaluate the performance of inspection equipment, including the sizing accuracy. The information from experiments is utilised in a most effective way when mathematical models are applied. Here, some statistical models for reliability of non-destructive tests are introduced. In order to demonstrate the use of inspection reliability models, they have been applied to the inspection results of intergranular stress corrosion cracking (IGSCC) type flaws in PISC III exercise (PISC 1995). The models are applied to both flaw detection frequency data of all inspection teams and to flaw sizing data of one participating team. (author)

Digital transfer of non-destructive testing images

International Nuclear Information System (INIS)

Nelson, S.

1996-01-01

This paper intends to address a possible avenue to assist the Non-Destructive Testing Industry in managing and transferring results to their clients in a more efficient way. Data is sent around the globe in various forms to a multitude of destinations. The problem has been twofold in any industry: how to get the data into a communication network and, how to manage and utilize this data. There are many types of scanners which can digitize the graph which can then be displayed on a computer screen via a software programme. The one presented in this paper has been jointly developed by a Melbourne company, Compu Medics and AGFA Australia. This system can also capture a video signal from Ultrasound Units and display on the screen. The author also explore what can be done with this data. Possibilities are endless and include: sending it via satellite or land line to a remote reader, saving or archiving for future reference and utilising the data base for education

Analysis of a Single Hot Particle by a Combination of Non-Destructive Analytical Methods

Energy Technology Data Exchange (ETDEWEB)

Hrnecek, E.; Aldave de las Heras, L.; Bielewski, M.; Carlos, R. [EC JRC Institute for Transuranium Elements, Karlsruhe (Germany); Betti, M. [IAEA Environment Laboratories (Monaco)

2013-07-15

Radioactive substances are often released to the environment in the form of particles. The determination of their chemical composition is a key factor in the overall understanding of their environmental behaviour. The aim of this investigation was to identify the source of one single radioactive particle collected from the Irish Sea and to understand its fate in the environment and in human body fluids. As the particle was supposed to be analysed for its dissolution behaviour in humans after ingestion, it was necessary to gain as much information as possible beforehand on the chemical and isotopic composition by means of non-destructive analysis such as SEM, SIMS, {mu}-XRF and {mu}-XANES. In this paper, an overview of the different non-destructive methods applied for the analysis of this particle and the results obtained is given. Additionally, the dissolution behaviour in human digestive solutions is discussed. (author)

Direct non-destructive observation of bulk nucleation in 30% deformed aluminum

DEFF Research Database (Denmark)

West, Stine; Schmidt, Søren; Sørensen, Henning Osholm

2009-01-01

A 30% deformed aluminum sample was mapped non-destructively using three-dimensional X-ray diffraction (3DXRD) before and after annealing to nucleation of recrystallization. Nuclei appeared in the bulk of the sample. Their positions and volumes were determined, and the crystallographic orientations...... were compared with the orientations of the deformed grains. It was found that nuclei with new orientations can form and their orientations have been related to the dislocation structure in the deformed grains....

The results of cutting disks testing for rock destruction

Directory of Open Access Journals (Sweden)

Khoreshok Aleksey

2017-01-01

Full Text Available To determine the rational order of disk tools placement on the working body is necessary to know the maximum amount of rock, destroyed by the disk tool in benching cutting mode depending on the tool geometry parameters, physical and mechanical parameters of rocks. The article contains the definition of rational parameters of cutting disk tools as well as power and energy parameters of the destruction process by cutting disks and by executive body of the coal cutter. The rational geometric parameters of cutting discs are specified. It was found that each step of cutting with a minimum depth of penetration has its own maximum height of bench outcrop. The dependence of the volumes of large items destroyed by the disk tool on the cutting step height was determined. The existence of the cyclic alternation of destruction phases, regardless the fracture parameters, the height of the ledge outcrop, and tools like free cutting geometry were found. In contrast to the free cutting in benching mode of destruction two large fragments of rocks in one cycle were observed. Consequently, the cyclical nature of the destruction process in the benching mode will be characterized by two chips and crushing, and this cycling repeats throughout the destruction process with the same parameters of destruction.

Evaluation of non destructive testing to characterize the resistance of the prefabricated system of columns and floor tiles for single family homes of a level: permeability meter, determination of wave velocity by ultrasound, Schmidt sclerometer and metal detector

International Nuclear Information System (INIS)

Quesada Chacon, Dannell

2014-01-01

Non destructive testing are determined to be correlated with resistance to compression and flexion of elements belonging to prefabricated system of columns and floor tiles for single family homes of a level. The characteristics of the non destructive testing are described, such as: measurer of permeability, Schmidt sclerometer, determination of wave velocity by ultrasound and metal detector. The columns and floor tiles are elaborated with 2 mixtures of different resistances at 28 days. The first more than 30 MPa and the second less than 25 MPa are sampled together with the control cylinders necessary to obtain the actual resistance according to ASTM C39. Last resistance testings to compression and Schmidt sclerometer are realized to control cylinders to 1, 2, and 4 weeks after being cast. Non destructive testings (permeability meter Torrent, Schmidt sclerometer and determination of wave velocity by ultrasound) are performed in columns and floor tiles to 1, 2, and 4 weeks after being cast. Last resistance testings to flexion is obtained by means of destructive tests of the columns and floor tiles sampled. The correlation of the data obtained is determined to derive values of compression resistance from non destructive testing [es

Non-destructive control of cladding thickness of fuel elements for research reactors

Energy Technology Data Exchange (ETDEWEB)

Karlov, Y.; Zhukov, Y.; Chashchin, S

1997-07-01

The control method of fuel elements for research reactors by means of measuring beta particles back scattering made it possible to perform complete automatic non-destructive control of internal and external claddings at our plant. This control gives high guarantees of the fuel element correspondence to the requirements. The method can be used to control the three-layer items of different geometry, including plates. (author)

Direct chemical oxidation: a non-thermal technology for the destruction of organic wastes

Energy Technology Data Exchange (ETDEWEB)

Balazs, G.B.; Cooper, J. F.; Lewis, P. R.; Adamson, M. G.

1998-02-01

Direct Chemical Oxidation (DCO) is a non-thermal, ambient pressure, aqueous-based technology for the oxidative destruction of the organic components of hazardous or mixed waste streams. The process has been developed for applications in waste treatment and chemical demilitarization and decontamination at LLNL since 1992, and is applicable to the destruction of virtually all solid or liquid organics, including: chlorosolvents, oils and greases, detergents, organic-contaminated soils or sludges, explosives, chemical and biological warfare agents, and PCB's. [1-15] The process normally operates at 80-100 C, a heating requirement which increases the difficulty of surface decontamination of large objects or, for example, treatment of a wide area contaminated soil site. The driver for DCO work in FY98 was thus to investigate the use of catalysts to demonstrate the effectiveness of the technology for organics destruction at temperatures closer to ambient. In addition, DCO is at a sufficiently mature stage of development that technology transfer to a commercial entity was a logical next step, and was thus included in FY98 tasks.

Conservation and restoration of natural building stones monitored through non-destructive X-ray computed tomography

Science.gov (United States)

Jacobs, P. Js; Cnudde, V.

2003-04-01

X-ray computed micro-tomography (μCT) is a promising non-destructive imaging technique to study building materials. μCT analysis provides information on the internal structure and petrophysical properties of small samples (size up to 2 cm diameter and 6 cm height), with to date a maximum resolution of 10 μm for commercial systems (Skyscan 1072). μCT allows visualising and measuring complete three-dimensional object structures without sample preparation. Possible applications of the μCT-technique for the monitoring of natural building stones are multiple: (i) to determine non-destructively porosity based on 3D images, (ii) to visualise weathering phenomena at the μ-scale, (iii) to understand the rationale of weathering processes, (iv) to visualise the presence of waterrepellents and consolidation products, (v) to monitor the protective effects of these products during weathering in order to understand the underlying weathering mechanisms and (vi) to provide advise on the suitability of products for the treatment of a particular rock-type. μCT-technique in combination with micro-Raman spectroscopy could prove to be a powerful tool for the future, as the combination of 3D visualisation and 2D chemical determination of inorganic as well as organic components could provide new insights to optimise conservation and restoration techniques of building materials. Determining the penetration depth of restoration products, used to consolidate or to protect natural building stones from weathering, is crucial if the application of conservation products is planned. Every type of natural building stone has its own petrophysical characteristics and each rock type reacts differently on the various restoration products available on the market. To assess the penetration depth and the effectiveness of a certain restoration product, μCT technology in combination with micro-Raman spectroscopy could be applied. Due to its non-destructive character and its resolution down to

Destructive analysis capabilities for plutonium and uranium characterization at Los Alamos National Laboratory

International Nuclear Information System (INIS)

Tandon, Lav; Kuhn, Kevin J.; Drake, Lawrence R.; Decker, Diana L.; Walker, Laurie F.; Colletti, Lisa M.; Spencer, Khalil J.; Peterson, Dominic S.; Herrera, Jaclyn A.; Wong, Amy S.

2010-01-01

Los Alamos National Laboratory's (LANL) Actinide Analytical Chemistry (AAC) group has been in existence since the Manhattan Project. It maintains a complete set of analytical capabilities for performing complete characterization (elemental assay, isotopic, metallic and non metallic trace impurities) of uranium and plutonium samples in different forms. For a majority of the customers there are strong quality assurance (QA) and quality control (QC) objectives including highest accuracy and precision with well defined uncertainties associated with the analytical results. Los Alamos participates in various international and national programs such as the Plutonium Metal Exchange Program, New Brunswick Laboratory's (NBL' s) Safeguards Measurement Evaluation Program (SME) and several other inter-laboratory round robin exercises to monitor and evaluate the data quality generated by AAC. These programs also provide independent verification of analytical measurement capabilities, and allow any technical problems with analytical measurements to be identified and corrected. This presentation will focus on key analytical capabilities for destructive analysis in AAC and also comparative data between LANL and peer groups for Pu assay and isotopic analysis.

Non destructive testing of works of art by terahertz analysis

Science.gov (United States)

Bodnar, Jean-Luc; Metayer, Jean-Jacques; Mouhoubi, Kamel; Detalle, Vincent

2013-11-01

Improvements in technologies and the growing security needs in airport terminals lead to the development of non destructive testing devices using terahertz waves. Indeed, these waves have the advantage of being, on one hand, relatively penetrating. They also have the asset of not being ionizing. It is thus potentially an interesting contribution in the non destructive testing field. With the help of the VISIOM Company, the possibilities of this new industrial analysis method in assisting the restoration of works of art were then approached. The results obtained within this framework are presented here and compared with those obtained by infrared thermography. The results obtained show first that the THZ method, like the stimulated infrared thermography allows the detection of delamination located in murals paintings or in marquetries. They show then that the THZ method seems to allow detecting defects located relatively deeply (10 mm) and defects potentially concealed by other defects. It is an advantage compared to the stimulated infra-red thermography which does not make it possible to obtain these results. Furthermore, they show that the method does not seem sensitive to the various pigments constituting the pictorial layer, to the presence of a layer of "Japan paper" and to the presence of a layer of whitewash. It is not the case of the stimulated infrared thermography. It is another advantage of the THZ method. Finally, they show that the THZ method is limited in the detection of low-size defects. It is a disadvantage compared to the stimulated infrared thermography.

High-resolution non-destructive three-dimensional imaging of integrated circuits.

Science.gov (United States)

Holler, Mirko; Guizar-Sicairos, Manuel; Tsai, Esther H R; Dinapoli, Roberto; Müller, Elisabeth; Bunk, Oliver; Raabe, Jörg; Aeppli, Gabriel

2017-03-15

Modern nanoelectronics has advanced to a point at which it is impossible to image entire devices and their interconnections non-destructively because of their small feature sizes and the complex three-dimensional structures resulting from their integration on a chip. This metrology gap implies a lack of direct feedback between design and manufacturing processes, and hampers quality control during production, shipment and use. Here we demonstrate that X-ray ptychography-a high-resolution coherent diffractive imaging technique-can create three-dimensional images of integrated circuits of known and unknown designs with a lateral resolution in all directions down to 14.6 nanometres. We obtained detailed device geometries and corresponding elemental maps, and show how the devices are integrated with each other to form the chip. Our experiments represent a major advance in chip inspection and reverse engineering over the traditional destructive electron microscopy and ion milling techniques. Foreseeable developments in X-ray sources, optics and detectors, as well as adoption of an instrument geometry optimized for planar rather than cylindrical samples, could lead to a thousand-fold increase in efficiency, with concomitant reductions in scan times and voxel sizes.

High-resolution non-destructive three-dimensional imaging of integrated circuits

Science.gov (United States)

Holler, Mirko; Guizar-Sicairos, Manuel; Tsai, Esther H. R.; Dinapoli, Roberto; Müller, Elisabeth; Bunk, Oliver; Raabe, Jörg; Aeppli, Gabriel

2017-03-01

Modern nanoelectronics has advanced to a point at which it is impossible to image entire devices and their interconnections non-destructively because of their small feature sizes and the complex three-dimensional structures resulting from their integration on a chip. This metrology gap implies a lack of direct feedback between design and manufacturing processes, and hampers quality control during production, shipment and use. Here we demonstrate that X-ray ptychography—a high-resolution coherent diffractive imaging technique—can create three-dimensional images of integrated circuits of known and unknown designs with a lateral resolution in all directions down to 14.6 nanometres. We obtained detailed device geometries and corresponding elemental maps, and show how the devices are integrated with each other to form the chip. Our experiments represent a major advance in chip inspection and reverse engineering over the traditional destructive electron microscopy and ion milling techniques. Foreseeable developments in X-ray sources, optics and detectors, as well as adoption of an instrument geometry optimized for planar rather than cylindrical samples, could lead to a thousand-fold increase in efficiency, with concomitant reductions in scan times and voxel sizes.

Non-destructive evaluation of water ingress in photovoltaic modules

Energy Technology Data Exchange (ETDEWEB)

Bora, Mihail; Kotovsky, Jack

2017-03-07

Systems and techniques for non-destructive evaluation of water ingress in photovoltaic modules include and/or are configured to illuminate a photovoltaic module comprising a photovoltaic cell and an encapsulant with at least one beam of light having a wavelength in a range from about 1400 nm to about 2700 nm; capture one or more images of the illuminated photovoltaic module, each image relating to a water content of the photovoltaic module; and determine a water content of the photovoltaic module based on the one or more images. Systems preferably include one or more of a light source, a moving mirror, a focusing lens, a beam splitter, a stationary mirror, an objective lens and an imaging module.

High-speed image processing systems in non-destructive testing

Science.gov (United States)

Shashev, D. V.; Shidlovskiy, S. V.

2017-08-01

Digital imaging systems are using in most of both industrial and scientific industries. Such systems effectively solve a wide range of tasks in the field of non-destructive testing. There are problems in digital image processing for decades associated with the speed of the operation of such systems, sufficient to efficiently process and analyze video streams in real time, ideally in mobile small-sized devices. In this paper, we consider the use of parallel-pipeline computing architectures in image processing problems using the example of an algorithm for calculating the area of an object on a binary image. The approach used allows us to achieve high-speed performance in the tasks of digital image processing.

Development of non-destructive testing (NDT) technology in Pakistan

International Nuclear Information System (INIS)

Khan, A.A.

2005-01-01

Non-Destructive Testing (NDT) techniques are being extensively used to improve and maintain the quality of manufactured goods as well as for proper maintenance of industrial plants and equipment. Typical industries that benefit most include Aerospace, Chemical, Heavy Mechanical Fabrication, Conventional and Nuclear Power Generation, Automobiles, Oil and Gas, Shipbuilding, Foundries, and Armaments, etc. As the name implies, with these techniques an industrial product is inspected mostly for defects in its structure without destroying it. Among the most widely used NDT techniques for the detection of internal defects are Radiographic and Ultrasonic Testing. For surface and just below the surface defects Magnetic Particle Testing, Penetrant Testing and Eddy Current Testing are commonly used. In addition to these, there are some NDT methods which have specific applications. These include Acoustic Emission, Thermal and Infrared Testing, Microwave Testing, Computer Tomography, Strain Gauging, Leak Testing and Holography, etc. This paper describes various phases through which the development of NDT technology passed and its present state of the art. It started with the undertaking of a nuclear technology programme and has matured along with it. As it stands we are fully competent to undertake various essential activities related to this technology, namely, (I) raining and certification of NDT personnel at various levels. (II) revision of NDT services to various industrial sectors including nuclear power during manufacture, fabrication, pre-service inspection (PSI) and in-service inspection (ISI). (author)

Non-destructive study of ancient documents and books by means of ion beams; Estudio no destructivo de documentos y libros antiguos mediante haces de iones

Energy Technology Data Exchange (ETDEWEB)

Ruvalcaba S, J.L.; Monroy, M. [IFUNAM, A.P. 20-364, 01000 Mexico D.F. (Mexico)

2004-07-01

In this work, a non destructive methodology for the analysis of ancient manuscripts and books using an external beam system and the techniques Particle Induced X-ray Emission Spectroscopy (PIXE) and Rutherford Backscattering Spectrometry (RBS) is presented. This application shows the analytical features of the particle accelerator based techniques for the characterization of this kind of historical materials. This methodology was used for the analysis of inks of an European book from XVII century. This is the first study in Mexico of an ancient book using simultaneously PIXE and RBS non-vacuum techniques. (Author) 21 refs., 9 figs.

Catalogue of test specimens for non-destructive examination

International Nuclear Information System (INIS)

1985-05-01

One of the key elements in assuring the integrity of reactor primary circuits is the availability of trustworthy non-destructive methods for detecting dangerous defects that may be present. Various approaches to making such examinations are being developed, including the use of ultrasonic and radiographic techniques. To demonstrate their capability and reliability, they must be tested on steel specimens reproducing the various types of faults which may arise in real primary circuit vessels and piping. Such specimens are costly to fabricate. It is therefore clearly desirable that existing specimens should be made accessible to as many organisations as possible for testing. This catalogue contains detailed Information on forty-odd deliberately flawed plates, blocks, vessels, etc. which have been produced in OECD countries, along with the name of a contact person to whom inquiries should be directed in each case

Explosive mechanism of metal destruction by intense electromagnetic radiation flux

International Nuclear Information System (INIS)

Martynyuk, M.M.

1977-01-01

The metal destruction by a powerful flux of electromagnetic radiation is considered on the basis of thermodynamics and kinetics of the transition of molten metal to vapour during its rapid heating. The possibility is discussed of obtaining a metastable liquid-metal phase and of its explosion transition to a stable two-phase state (phase explosion of metastable liquid). It has been shown that at densities of radiation beam ensuring the heating of the metal to the spinodal point Tsub(s) during a time tsub(s)=10 -5 -10 -7 s the vaporization of the matter from the surface of the liquid is negligible, and the main mechanism of the metal destruction is the phase explosion of the metastable liquid-metal phase which originates in the Tsub(s) vicinity. The experimental data on the electric explosion of conductors for tsub(s)=10 -6 -10 -5 s has served as a basis for calculating the excess enthalpy and the proportion of the vapour phase formed in the phase explosion of Cu, Ag, Au, Zn, Cd, Al, Pb, Zr, Nb, Mo, W, Pt and Re. The particularities of the phase explosion at flux densities corresponding to tsub(s)( -8 s are considered

Assessment of recovery and recrystallisation behaviours of cold rolled IF steel through non-destructive electromagnetic characterisation

Science.gov (United States)

Roy, Rajat K.; Dutta, Siuli; Panda, Ashis K.; Rajinikanth, V.; Das, Swapan K.; Mitra, Amitava; Strangwood, M.; Davis, Claire L.

2018-07-01

The recovery and recrystallisation behaviours of cold rolled IF steel have been investigated by destructive (optical microscopy and hardness) and non-destructive electromagnetic sensor, (which allows direct measurement of strip samples with no surface preparation) techniques. The onset and completion of recrystallisation are clearly monitored through destructive techniques of optical microscopy and hardness measurements. The nucleation of new recrystallised grains is observed in the sample annealed at 600 °C/15 min, while completion of recrystallisation takes place at 700 °C/15 min. The destructive techniques are not very accurate in monitoring recovery, for example, changes in hardness of accounting for ≈60% change in the coercivity value. Therefore, the measurement of magnetic softening through an electromagnetic sensor acts a crucial role for understanding recovery and recrystallisation behaviours of steels during industrial processing. The present investigation is aimed not only for controlling product quality but also saving characterisation time through off line monitoring during steel processing at industry.

Human and organisational factors influencing the reliability of non-destructive testing. An international literary survey

International Nuclear Information System (INIS)

Kettunen, J.; Norros, L.

1996-04-01

The aim of the study is to chart human and organisational factors influencing the reliability of non-destructive testing (NDT). The emphasis will be in ultrasonic testing (UT) and in the planning and execution of in-service inspections during nuclear power plant maintenance outages. Being a literary survey this study is mainly based on the foreign and domestic research available on the topic. In consequence, the results presented in this report reflect the ideas of international research community. In addition to this, Finnish nuclear power plant operators (Imatran Voima Oy and Teollisuuden Voima Oy), independent inspection organisations and the Finnish Centre for Radiation and Nuclear Safety have provided us with valuable information on NDT theory and practice. Especially, a kind of 'big picture' of non-destructive testing has been pursued in the study. (6 figs., 2 tabs.)

Dynamic laser speckle for non-destructive quality evaluation of bread

Science.gov (United States)

Stoykova, E.; Ivanov, B.; Shopova, M.; Lyubenova, T.; Panchev, I.; Sainov, V.

2010-10-01

Coherent illumination of a diffuse object yields a randomly varying interference pattern, which changes over time at any modification of the object. This phenomenon can be used for detection and visualization of physical or biological activity in various objects (e.g. fruits, seeds, coatings) through statistical description of laser speckle dynamics. The present report aims at non-destructive full-field evaluation of bread by spatial-temporal characterization of laser speckle. The main purpose of the conducted experiments was to prove the ability of the dynamic speckle method to indicate activity within the studied bread samples. In the set-up for acquisition and storage of dynamic speckle patterns an expanded beam from a DPSS laser (532 nm and 100mW) illuminated the sample through a ground glass diffuser. A CCD camera, adjusted to focus the sample, recorded regularly a sequence of images (8 bits and 780 x 582 squared pixels, sized 8.1 × 8.1 μm) at sampling frequency 0.25 Hz. A temporal structure function was calculated to evaluate activity of the bread samples in time using the full images in the sequence. In total, 7 samples of two types of bread were monitored during a chemical and physical process of bread's staling. Segmentation of images into matrixes of isometric fragments was also utilized. The results proved the potential of dynamic speckle as effective means for monitoring the process of bread staling and ability of this approach to differentiate between different types of bread.

The Effect of Localized Damage on the Electrical Conductivity of Bare Carbon Fiber Tow and its Use as a Non-Destructive Evaluation Tool for Composite Overwrapped Pressure Vessels

Science.gov (United States)

Wentzel, Daniel

2015-01-01

Composite materials are beneficial because of their high specific strength and low weight. Safety, Destructive testing and destructive testing, Non-Destructive Testing (NDT) and Non-Destructive Evaluation (NDE). Problem: Neither NDT nor NDE can provide sufficient data to determine life expectancy or quantify the damage state of a composite material.

The use of computers for the performance and analysis of non-destructive testing

International Nuclear Information System (INIS)

Edelmann, X.; Pfister, O.

1988-01-01

Examples of the use of computers in non-destructive testing are related. Ultrasonic testing is especially addressed. The employment of computers means improvements for the user, the possibility of registering the reflector position, storage of test data and help with documentation. The test can be automated. The introduction of expert systems is expected for the future. 8 figs., 12 refs

Coded excitation for infrared non-destructive testing of carbon fiber reinforced plastics.

Science.gov (United States)

Mulaveesala, Ravibabu; Venkata Ghali, Subbarao

2011-05-01

This paper proposes a Barker coded excitation for defect detection using infrared non-destructive testing. Capability of the proposed excitation scheme is highlighted with recently introduced correlation based post processing approach and compared with the existing phase based analysis by taking the signal to noise ratio into consideration. Applicability of the proposed scheme has been experimentally validated on a carbon fiber reinforced plastic specimen containing flat bottom holes located at different depths.

Nondestructive characterization of austenitic stainless steels

International Nuclear Information System (INIS)

Jayakumar, T.; Kumar, Anish

2010-01-01

The paper presents an overview of the non-destructive methodologies developed at the authors' laboratory for characterization of various microstructural features, residual stresses and corrosion in austenitic stainless steels. Various non-destructive evaluation (NDE) parameters such as ultrasonic velocity, ultrasonic attenuation, spectral analysis of the ultrasonic signals, magnetic hysteresis parameters and eddy current amplitude have been used for characterization of grain size, precipitation behaviour, texture, recrystallization, thermomechanical processing, degree of sensitization, formation of martensite from metastable austenite, assessment of residual stresses, degree of sensitization and propensity for intergranular corrosion in different austenitic steels. (author)

Non-destructive testing of the MEGAPIE target

Science.gov (United States)

Dai, Y.; Wohlmuther, M.; Boutellier, V.; Hahl, S.; Lagotzki, A.; Leu, H.; Linder, H. P.; Schwarz, R.; Spahr, A.; Zanini, L.; Kuster, D.; Gavillet, D.; Wagner, W.

2016-01-01

Non-destructive testing (NDT) is one important part of the post-irradiation examination (PIE) of the MEGAPIE target. It includes visual inspection and ultrasonic measurement of the beam window of the T91 LBE container and gamma mapping of the beam window of the AlMg3 safety-container. The visual inspection showed no visible failure in the proton beam window area of the T91 LBE container. The ultrasonic measurement demonstrated no detectable change in the wall thickness of the T91 beam window, which implies no severe corrosion effect induced by flowing LBE during the four-month irradiation period. The gamma mapping provided the distribution of 22Na, a spallation product, in the proton beam window area of the AlMg3 safety-container. The result was used to evaluate the accumulated proton fluence distribution profile, the input data for determining irradiation parameters. A maximum proton fluence of 1.9 × 1025 p/m2 was deduced. The corresponding displacement damage degree in the T91 beam window was 7.1 dpa.

Energy convergence of shock waves and its destruction mechanism in cone-roof combustion chambers

International Nuclear Information System (INIS)

Xu, Han; Yao, Anren; Yao, Chunde; Gao, Jian

2016-01-01

Highlights: • Experiments with simulations are designed to probe into engine severe knock. • Energy convergence at central and edge region is observed in closed-limited space. • Modes with different intensities and mechanism of energy convergence are revealed. • Chamber shape and equivalence ratio can affect the energy convergence. • The destruction effects of energy convergence on pistons are recognized. - Abstract: Energy convergence is considered as an important phenomenon in internal combustion engines under severe knock, in which shock waves caused by violent combustion may aggregate the energy released by fuel burning to damage engine parts like pistons and spark plugs easily. In order to reveal such convergence mechanism and its destruction effects, a novel detonation bomb experiment combined with numerical simulations are conducted. In bomb experiments, a detonation wave is forcibly introduced into a clearance-variable cone-roof combustion chamber by a high energy spark ignition. Four pressure transducers were installed in different positions to monitor the energy convergence. Combined with the experiments, numerical simulations were conducted to reveal the convergence modes and mechanisms. Finally, destruction samples were presented to validate this research. It’s found that the energy convergence of shock waves always occurs in middle and edge region, which are vulnerable to be damaged. Three modes of energy convergence are concluded for middle region while several ways of energy convergence are concluded for edge region, which are all related with the chamber shape and may result in different levels of convergence. It’s also found that though detonation strength (knock intensity) can be changed by both equivalence ratios and initial pressures, only the equivalence ratios can change the convergence modes while the initial pressures cannot.

Impact of the 'non-destructive' multiple-readout on the Lorentzian noise

International Nuclear Information System (INIS)

Guazzoni, C.; Gatti, E.; Geraci, A.

2006-01-01

In this paper, we discuss the effect of 'non-destructive' multiple-readout on the Lorentzian noise. To our knowledge, it is the first time that such interaction is investigated. We have studied the peculiarities of the shape of the optimum weighting function for the multiple-readout technique in the presence of Lorentzian noise and other noise sources. The impact of the Lorentzian noise on the resolution achievable with the multiple-readout technique is analyzed in detail with respect to the interaction between the oscillation time and the characteristic time constant of the Lorentzian noise

Non-destructive measurement methods for large scale gaseous diffusion process equipment

International Nuclear Information System (INIS)

Mayer, R.L.; Hagenauer, R.C.; McGinnis, B.R.

1994-01-01

Two measurement methods have been developed to measure non-destructively uranium hold-up in gaseous diffusion plants. These methods include passive neutron and passive γ ray measurements. An additional method, high resolution γ ray spectroscopy, provides supplementary information about additional γ ray emitting isotopes, γ ray correction factors, 235 U/ 234 U ratios and 235 U enrichment. Many of these methods can be used as a general purpose measurement technique for large containers of uranium. Measurement applications for these methods include uranium hold-up, waste measurements, criticality safety and nuclear accountability

Non-destructive and non-invasive analyses shed light on the realization technique of ancient polychrome prints

Science.gov (United States)

Striová, Jana; Coccolini, Gabriele; Micheli, Sara; Lofrumento, Cristiana; Galeotti, Monica; Cagnini, Andrea; Castellucci, Emilio Mario

2009-08-01

Five polychrome prints representing famous painters, such as Albrecht Dürer, were analyzed using a non-destructive and non-invasive methodology as required by the artwork typology. The diagnostic strategy includes X-ray fluorescence (XRF), reflectance micro-infrared (μFTIR) and micro-Raman (μRaman) spectroscopy. These prints were realized with a la poupée method that involves application of the polychrome inks on a single copper plate, before the printing process. A broad range of compounds (i.e., cinnabar, red lead, white lead, umber earth, hydrated calcium sulfate, calcium carbonate, amorphous carbon, and Prussian blue) was employed as chalcographic inks, using linseed oil as a binding medium. Gamboge was identified in the delicate finishing brush touches realized in watercolor.

Non-destructive isotopic uranium assay by multiple delayed neutron measurements

International Nuclear Information System (INIS)

Papadopoulos, N.N.; Tsagas, N.F.

1991-01-01

The high accuracy and precision required in nuclear safeguards measurements can be achieved by an improved neutron activation technique based on multiple delayed fission neutron counting under various experimental conditions. For the necessary ultrahigh counting statistics required, cyclic activation of multiple subsamples has been applied. The home-made automated flexible analytical system with neutron flux and spectrum differentiation by irradiation position adjustment and cadmium screening, permits the non-destructive determination of the U235 abundance and the total U element concentration needed in nuclear safeguards sample analysis, with a high throughout and a low operational cost. Careful experimental optimization led to considerable improvement of the results

Failure mechanism dependence and reliability evaluation of non-repairable system

International Nuclear Information System (INIS)

Chen, Ying; Yang, Liu; Ye, Cui; Kang, Rui

2015-01-01

Reliability study of electronic system with the physics-of-failure method has been promoted due to the increase knowledge of electronic failure mechanisms. System failure initiates from independent failure mechanisms, have effect on or affect by other failure mechanisms and finally result in system failure. Failure mechanisms in a non-repairable system have many kinds of correlation. One failure mechanism developing to a certain degree will trigger, accelerate or inhibit another or many other failure mechanisms, some kind of failure mechanisms may have the same effect on the failure site, component or system. The destructive effect will be accumulated and result in early failure. This paper presents a reliability evaluation method considering correlativity among failure mechanisms, which includes trigger, acceleration, inhibition, accumulation, and competition. Based on fundamental rule of physics of failure, decoupling methods of these correlations are discussed. With a case, reliability of electronic system is evaluated considering failure mechanism dependence. - Highlights: • Five types of failure mechanism correlations are described. • Decoupling methods of these correlations are discussed. • A reliability evaluation method considering mechanism dependence is proposed. • Results are quite different to results under failure independence assumption

Non-Destructive Radiological Characterisation Of Contaminated And Activated Concrete

International Nuclear Information System (INIS)

Cantrel, E.

2005-01-01

The decommissioning of nuclear facilities leads to large quantities of concrete and building material wastes. Radioactivity in building structures arise from very different physical processes such as neutron activation (bioshield), diffusion of the contaminants in the material (primary coolant leakage, maintenance and fuel loading) or aerosol deposition. The variety of the building material also extends the range of faced radiological characteristics. Therefore the minimization of concrete waste generation requires extensive characterisations and the availability of different measurement tools and methods. Up to now, these measurements came from the coring and the radiological analysis of the concrete, which is a destructive, long and costly technique. Looking for alternative solutions, SCK-CEN has started to investigate in collaboration with EDF -research and development and CEA (France) several non destructive methods based on gamma spectroscopy and different spectral examinations using mathematical calibration and modelling tools available on the market. Information on in-depth activity distribution can be derived from in situ gamma spectra by modelling absorption laws (peak to peak ratios) and photons interactions (Compton front) in the bulk of the concrete. As they combine modelling and measurement, the different methodologies being evaluated involve a lot of uncertainty sources linked to the measurement environment, to the knowledge available on site (historical background, material composition), to the operator responsible for the data acquisition and to the performance of the equipment. Therefore a detailed sensitivity analysis is required to define the range of applicability and the performances of the different methods

Fabrication and characterization of non-resonant magneto-mechanical low-frequency vibration energy harvester

Science.gov (United States)

Nammari, Abdullah; Caskey, Logan; Negrete, Johnny; Bardaweel, Hamzeh

2018-03-01

This article presents a non-resonant magneto-mechanical vibration energy harvester. When externally excited, the energy harvester converts vibrations into electric charge using a guided levitated magnet oscillating inside a multi-turn coil that is fixed around the exterior of the energy harvester. The levitated magnet is guided using four oblique mechanical springs. A prototype of the energy harvester is fabricated using additive manufacturing. Both experiment and model are used to characterize the static and dynamic behavior of the energy harvester. Measured restoring forces show that the fabricated energy harvester retains a mono-stable potential energy well with desired stiffness nonlinearities. Results show that magnetic spring results in hardening effect which increases the resonant frequency of the energy harvester. Additionally, oblique mechanical springs introduce geometric, negative, nonlinear stiffness which improves the harvester's response towards lower frequency spectrum. The unique design can produce a tunable energy harvester with multi-well potential energy characteristics. A finite element model is developed to estimate the average radial flux density experienced by the multi-turn coil. Also, a lumped parameter model of the energy harvester is developed and validated against measured data. Both upward and downward frequency sweeps are performed to determine the frequency response of the harvester. Results show that at higher excitation levels hardening effects become more apparent, and the system dynamic response turns into non-resonant. Frequency response curves exhibit frequency jump phenomena as a result of coexistence of multiple energy states at the frequency branch. The fabricated energy harvester is hand-held and measures approximately 100.5 [cm3] total volume. For a base excitation of 1.0 g [m/s2], the prototype generates a peak voltage and normalized power density of approximately 3.5 [V] and 0.133 [mW/cm3 g2], respectively, at 15.5 [Hz].

Identification of the Thickness of Nugget on Worksheet Spot Welding Using Non Destructive Test (NDT) - Effect of Pressure

Science.gov (United States)

Sifa, A.; Baskoro, A. S.; Sugeng, S.; Badruzzaman, B.; Endramawan, T.

2018-02-01

Resistance Spot Welding (RSW) is a process of connecting between two worksheet with thermomechanical loading process, RSW is widely used in automotive industry, the quality of splicing spot welding is influenced by several factors. One of the factors at the time of the welding process is pressure. The quality of welding on the nuggets can be determined by undertaking non-destructive testing by using Non Destructive Test (NDT) - Ultrasonic Test. In the NDT test is done by detecting the thickness of the nugget area, the purpose of research conducted to determine the effect of pressure to welding quality with Nugget thickness gauge measurement with Non Destructive Test method and manual measurement with micrometer, Experimental welding process by entering the welding parameters that have been specified and pressure variables 1 -5 bars on the worksheet thickness of 1 mm. The results of testing with NDT show there is addition of thickness in nugget superiority after compare with measurement result of thickness of nugget with micrometer which slightly experience thickness in nugget area, this indicates that the welding results have a connection between worksheet 1 and worksheet 2.

Recent advances in seismic non-destructive testing of concrete plate like structures

International Nuclear Information System (INIS)

Ryden, N.; Kristensen, A.; Jovall, O.

2009-01-01

This paper describes recent advances in seismic/acoustic non-destructive testing of concrete containment walls. The presented technique is focused on the characterization of the mean stiffness (seismic velocities) and thickness of the containment wall. The Impact Echo (IE) method is a well-established technique to measure the thickness of concrete plates or to locate defects in concrete plate like structures. The method relies on a good estimate of the mean velocity through the thickness of the plate and a precisely measured thickness resonant frequency. Recently the underlying theory of the IE method has been redefined and improved based on Lamb waves in a free plate. Based on this theory we have developed a new data processing technique where both propagating and standing Lamb waves are analysed in a combined manner using multichannel data. With this approach the mean velocity through the plate thickness is evaluated by using the fundamental mode Lamb wave dispersion curves. The accuracy and detection ability of the measured resonant frequency is improved by utilizing both amplitude and phase information from the multichannel record. The method has been tested on several nuclear power plants in Sweden and Finland and proved to be more robust compared to conventional IE and surface wave measurements

Nanorobotic Manipulation Setup for Pick-and-Place Handling and non-destructive Characterization of Carbon Nanotubes

DEFF Research Database (Denmark)

Eicchorn, V.; Carlson, Kenneth; Andersen, Karin Nordström

2007-01-01

. The pick-and-place task is carried out by using an electrothermal actuated microgripper, designed for controlled manipulation of nanotubes. The nanotube is picked up from an array of multiwalled carbon nanotubes (MWCNTs) and transferred to the tip of an atomic force microscope (AFM) probe in order...... to assemble a high-aspect ratio AFM supertip. Another application of the nanorobotic setup considered in this paper is the nondestructive mechanical characterization of CNTs. A piezoresistive AFM probe is used to bend MWCNTs, while the bending force is measured, in order to estimate the Young's modulus...

Mechanical Characterization of Bone: State of the Art in Experimental Approaches-What Types of Experiments Do People Do and How Does One Interpret the Results?

Science.gov (United States)

Bailey, Stacyann; Vashishth, Deepak

2018-06-18

The mechanical integrity of bone is determined by the direct measurement of bone mechanical properties. This article presents an overview of the current, most common, and new and upcoming experimental approaches for the mechanical characterization of bone. The key outcome variables of mechanical testing, as well as interpretations of the results in the context of bone structure and biology are also discussed. Quasi-static tests are the most commonly used for determining the resistance to structural failure by a single load at the organ (whole bone) level. The resistance to crack initiation or growth by fracture toughness testing and fatigue loading offers additional and more direct characterization of tissue material properties. Non-traditional indentation techniques and in situ testing are being increasingly used to probe the material properties of bone ultrastructure. Destructive ex vivo testing or clinical surrogate measures are considered to be the gold standard for estimating fracture risk. The type of mechanical test used for a particular investigation depends on the length scale of interest, where the outcome variables are influenced by the interrelationship between bone structure and composition. Advancement in the sensitivity of mechanical characterization techniques to detect changes in bone at the levels subjected to modifications by aging, disease, and/or pharmaceutical treatment is required. As such, a number of techniques are now available to aid our understanding of the factors that contribute to fracture risk.

Combining data in non-destructive testing

International Nuclear Information System (INIS)

Lavayssiere, B.

1994-03-01

Non-destructive testing of some components requires quite often the use of several methods such as X-ray, ultrasonics, Eddy Currents. But the efficiency of a NDT method is highly dependent on the fact that the detectability of flaws in a specimen relies on the choice of the best method. Moreover a lot of inspection issues could benefit from the use of more than one test method, as each NDT method has its own physical properties and technological limits. Some questions still remain: how to combine data, at what level and for what functionality. Simple monomethod processes are well-known now. They include techniques like reconstruction which belongs to the so-called ill-posed problems in the field of mathematics. For NDT data processing, it has the ability to estimate real data from distorted ones coming from a probe. But, up to now there has been very few approaches for computer aided combination of results from different advanced techniques. This report presents the various mathematical fields involved towards that goal (statistical decision theory which allows the use of multiple hypothesis, non-linear decision theory for its capability to classify and to discriminate, graph theory to find the optimal path in an hypothesis graph and also fuzzy logic, multiple resolution analysis, artificial intelligence,...) and which combinations of methods are useful. Some images will illustrate this topic in which EDF is involved, and will explain what are the major goals of this work. Combining is not only an improvement of 3D visualisation which would allow to display simultaneously CAD or NDT data for example, but it consists in exploiting multisensor data collected via a variety of sophisticated techniques and presenting this information to the operator without overloading the operator/system capacities in order to reduce the uncertainty and to resolve the ambiguity inherent to mono method inspection. (author). 7 figs., 35 refs

Radioisotopes in non-destructive testing

International Nuclear Information System (INIS)

Domanus, J.C.

1976-12-01

After defining nondestructive testing (NDT) and comparing this concept with destructive testing, a short description is given of NDT methods other than radiologic. The basic concepts of radiologic methods are discussed and the principles of radiography are explained. Radiation sources and gamma radiography machines are next reviewed and radiographic inspection of weldings and castings is described. A brief description is given of the radiographic darkroom and accessories. Other radioisotope methods, such as neutron radiography, are shortly reviewed. Cost estimations for radioisotopic equipment conclude the report. (author)

Advances in Non-Destructive Early Assessment of Fruit Ripeness towards Defining Optimal Time of Harvest and Yield Prediction—A Review

Directory of Open Access Journals (Sweden)

Bo Li

2018-01-01

Full Text Available Global food security for the increasing world population not only requires increased sustainable production of food but a significant reduction in pre- and post-harvest waste. The timing of when a fruit is harvested is critical for reducing waste along the supply chain and increasing fruit quality for consumers. The early in-field assessment of fruit ripeness and prediction of the harvest date and yield by non-destructive technologies have the potential to revolutionize farming practices and enable the consumer to eat the tastiest and freshest fruit possible. A variety of non-destructive techniques have been applied to estimate the ripeness or maturity but not all of them are applicable for in situ (field or glasshouse assessment. This review focuses on the non-destructive methods which are promising for, or have already been applied to, the pre-harvest in-field measurements including colorimetry, visible imaging, spectroscopy and spectroscopic imaging. Machine learning and regression models used in assessing ripeness are also discussed.

Mini-review: novel non-destructivein situbiofilm characterization techniques in membrane systems

KAUST Repository

Valladares Linares, Rodrigo; Fortunato, Luca; Farhat, Nadia; Bucs, Szilard; Staal, M.; Fridjonsson, E.O.; Johns, M.L.; Vrouwenvelder, Johannes S.; Leiknes, TorOve

2016-01-01

Membrane systems are commonly used in the water industry to produce potable water and for advanced wastewater treatment. One of the major drawbacks of membrane systems is biofilm formation (biofouling), which results in an unacceptable decline in membrane performance. Three novel in situ biofouling characterization techniques were assessed: (i) optical coherence tomography (OCT), (ii) planar optodes, and (iii) nuclear magnetic resonance (NMR). The first two techniques were assessed using a biofilm grown on the surface of nanofiltration (NF) membranes using a transparent membrane fouling simulator that accurately simulates spiral wound modules, modified for in situ biofilm imaging. For the NMR study, a spiral wound reverse osmosis membrane module was used. Results show that these techniques can provide information to reconstruct the biofilm accurately, either with 2-D (OCT, planar optodes and NMR), or 3-D (OCT and NMR) scans. These non-destructive tools can elucidate the interaction of hydrodynamics and mass transport on biofilm accumulation in membrane systems. Oxygen distribution in the biofilm can be mapped and linked to water flow and substrate characteristics; insights on the effect of crossflow velocity, flow stagnation, and feed spacer presence can be obtained, and in situ information on biofilm structure, thickness, and spatial distribution can be quantitatively assessed. The combination of these novel non-destructive in situ biofilm characterization techniques can provide real-time observation of biofilm formation at the mesoscale. The information obtained with these tools could potentially be used for further improvement in the design of membrane systems and operational parameters to reduce impact of biofouling on membrane performance. © 2016 Balaban Desalination Publications. All rights reserved.

Mini-review: novel non-destructivein situbiofilm characterization techniques in membrane systems

KAUST Repository

Valladares Linares, R.

2016-05-12

Membrane systems are commonly used in the water industry to produce potable water and for advanced wastewater treatment. One of the major drawbacks of membrane systems is biofilm formation (biofouling), which results in an unacceptable decline in membrane performance. Three novel in situ biofouling characterization techniques were assessed: (i) optical coherence tomography (OCT), (ii) planar optodes, and (iii) nuclear magnetic resonance (NMR). The first two techniques were assessed using a biofilm grown on the surface of nanofiltration (NF) membranes using a transparent membrane fouling simulator that accurately simulates spiral wound modules, modified for in situ biofilm imaging. For the NMR study, a spiral wound reverse osmosis membrane module was used. Results show that these techniques can provide information to reconstruct the biofilm accurately, either with 2-D (OCT, planar optodes and NMR), or 3-D (OCT and NMR) scans. These non-destructive tools can elucidate the interaction of hydrodynamics and mass transport on biofilm accumulation in membrane systems. Oxygen distribution in the biofilm can be mapped and linked to water flow and substrate characteristics; insights on the effect of crossflow velocity, flow stagnation, and feed spacer presence can be obtained, and in situ information on biofilm structure, thickness, and spatial distribution can be quantitatively assessed. The combination of these novel non-destructive in situ biofilm characterization techniques can provide real-time observation of biofilm formation at the mesoscale. The information obtained with these tools could potentially be used for further improvement in the design of membrane systems and operational parameters to reduce impact of biofouling on membrane performance. © 2016 Balaban Desalination Publications. All rights reserved.

Efficiency evaluation test of waste non-destructive analysis device

International Nuclear Information System (INIS)

Maeda, Kouichi; Ogasawara, Kensuke; Nisizawa, Ichio

2000-03-01

A device for non-destructive analysis of plutonium in alpha solid waste has been installed in NUCEF; Nuclear Fuel Cycle Safety Engineering Research Facility. The device has been designed to determine the amount of radioisotopes in carton-boxes, 45 l steel cans and 200 l steel cans containing relatively low density waste. Considering the waste density and the heterogeneity of radio-sources, the proper distance between the detector and the waste, and the open degree of the collimator have been settled, because real waste may contain several kinds of material and the heterogeneity of radioactivity. It has been confirmed from the evaluation of the detect limit that plutonium of about 8 MBq can be determined with the accuracy of 10% and the device may be proper for the practical application. (author)

Non destructive testing and neutron radiography in 1994; Les controles non destructifs et la neutronographie en 1994

Energy Technology Data Exchange (ETDEWEB)

Bayon, G.

1994-12-31

Neutron radiography has been considered for a long time as a promising technique; however it plays a minor part in the world of non destructive testing today, due to the lack of suitable neutron sources and lack of new industrial applications. This paper reviews the present status of neutron sources, neutron radiography activities, especially in France (such as the neutron-capture-issued secondary radiation spectrometry), in nuclear, aerospace, aeronautical and metallurgical sectors, and the last applications of neutron dynamic imaging. 9 refs.

Diagnosis of structures. Practical applications and future tasks of non-destructive testing. Papers; Bauwerksdiagnose. Praktische Anwendungen Zerstoerungsfreier Pruefungen und Zukunftsaufgaben. Vortraege

Energy Technology Data Exchange (ETDEWEB)

NONE

2008-07-01

The CD contains 17 papers and 20 posters on the subject of non-destructive diagnosis of structures. The titles of the 17 papers are: 1. Non-destructive testing in transition - from quality testing to life management; 2. Non-destructive testing of bridges on German motorways; 3. Structural diagnosis of concrete components - results obtained by a group of scientists of Deutsche Forschungsgemeinschaft; 4. Building diagnosis - its relevance and options for the building authorities; 5. Optimisation of permanent monitoring of structures by non-destructive test methods; 6. Assessment of Structures using Fibre-optic Sensors; 7. Methods and results in wood structure diagnosis; 8. The collapse of the roof of the Bad Reichenhall ice-skating rink - how could it have been prevented? 9. Integration of non-destructive structural tests in structure management of PPP models (Powerpoint); 10: Elements of sustainable life cycle management of engineering structures; 11. Structure monitoring as a component of life management systems; 12. Chloride and Sulfate analysis using LIBS - from the laboratory to the construction site; 13. Applications of georadar und ultrasonics - examples from the working practice of an engineering consultants' office; 14. Bridge analysis by automatic methods - new developments; 15. Fast large-area condition monitoring of reinforced-concrete bridges, floors and ceilings; 16. Influence of roof gap pressing on non-destructive thickness testing of the inner shells of motorway tunnels; 17. Non-destructive test methods for structure diagnosis - status and perspectives. [German] Die CD enthaelt 17 Vortraege und 20 Posterbeitraege zum Thema: ''Zerstoerungsfreie Pruefverahren fuer die Bauwerksdiagnose''. Die Themen der 17 Vortraege sind: 1. Die Zerstoerungsfreie Pruefung im Wandel - Von der Qualitaetspruefung zum Lebensdauermanagement; 2. ZfPBau-Verfahren fuer die Zustandserfassung von Bruecken der Bundesfernstrassen; 3. Strukturbestimmung von

Non-destructive examination of the bonding interface in DEMO divertor fingers

International Nuclear Information System (INIS)

Richou, Marianne; Missirlian, Marc; Vignal, Nicolas; Cantone, Vincent; Hernandez, Caroline; Norajitra, Prachai; Spatafora, Luigi

2013-01-01

Highlights: • SATIR tests on DEMO divertor fingers (integrating or not He cooling system). • Millimeter size artificial defects were manufactured. • Detectability of millimeter size artificial defects was evaluated. • SATIR can detect defect in DEMO divertor fingers. • Simulations are well correlated to SATIR tests. -- Abstract: Plasma facing components (PFCs) with tungsten (W) armor materials for DEMO divertor require a high heat flux removal capability (at least 10 MW/m 2 in steady-state conditions). The reference divertor PFC concept is a finger with a tungsten tile as a protection and sacrificial layer brazed to a thimble made of tungsten alloy W – 1% La 2 O 3 (WL10). Defects may be located at the W thimble to W tile interface. As the number of fingers is considerable (>250,000), it is then a major issue to develop a reliable control procedure in order to control with a non-destructive examination the fabrication processes. The feasibility for detecting defect with infrared thermography SATIR test bed is presented. SATIR is based on the heat transient method and is used as an inspection tool in order to assess component heat transfer capability. SATIR tests were performed on fingers integrating or not the complex He cooling system (steel cartridge with jet holes). Millimeter size artificial defects were manufactured and their detectability was evaluated. Results of this study demonstrate that the SATIR method can be considered as a relevant non-destructive technique examination for the defect detection of DEMO divertor fingers

European Non Destructive Examination Forum (ENDEF)

International Nuclear Information System (INIS)

Deffrennes, M.; Engl, G.; Estorff, U. von

1998-01-01

ENDEF, an initiative of the European Commission, DG XVII (Energy) was well supported by the European industrial institutions working in assistance with nuclear industrial organisations in the CEEC's (Central and Eastern European Countries) and NIS's (New Independent States). This Forum provides effectively a platform for open discussion between representatives of industrial actors active in the NDE (Non Destructive Examination)/ISI (In Service Inspection) field with the purpose to establish a co-operation pattern between qualified representatives of the EU (European Union) industry to offer a better co-ordinated and well defined assistance to the CEEC's and NIS in the field of NDE/ISI, and to lay the ground for further industrial co-operation. ENDEF developed a strategy to follow for the establishment of co-operation projects. This strategy is now used to understand the extent of past or present assistance projects and to identify the areas where more co-operation is needed. ENDEF encourages the creation in the NIS's and CEEC's of similar forums in order to increase the co-operation and co-ordination. ENDEF is also working in perfect agreement with the European Network ENIQ, piloted by the European plant operators. This identity of views lead to the leadership by the ENDEF co-ordinator of the ENIQ Task 3 involving Applications of the European Methodology for ISI qualification in the CEEC's and NIS's and presently fully integrated in ENDEF. (orig.)

NON-DESTRUCTIVE IN SITU SOIL CARBON ANALYSIS: PRINCIPLE AND RESULTS

International Nuclear Information System (INIS)

WIELOPOLSKI, L.; MITRA, S.; HENDREY, G.; ROGERS, H.; TORBERT, A.; PRIOR, S.

2003-01-01

Global warming is promoted by anthropogenic CO 2 emissions into the atmosphere, while at the same time it is partially mitigated by carbon sequestration by terrestrial ecosystems. However, improvement in the understanding and monitoring of below ground carbon processes is essential for evaluating strategies for carbon sequestration including quantification of carbon stores for credits. A system for non-destructive in situ carbon monitoring in soil, based on inelastic neutron scattering (INS), is described. The system can be operated in stationary or scanning mode and measures soil to depth of approximately 30 cm. There is a good agreement between results obtained from INS and standard chemical analysis of soil cores collected from the same study site

Template synthesis of test tube nanoparticles using non-destructive replication.

Science.gov (United States)

Wagner, Jonathan; Yao, Jingyuan; Rodgers, David; Hinds, Bruce

2013-03-01

Nano test tubes are a promising delivery vehicle for a range of therapeutics, including small molecule drugs and biologics. However, current template synthesis methods of producing nano test tubes are prohibitively expensive and time consuming. Here, non-destructive template replication was used to increase nano test tube yield from porous alumina by more than a hundredfold. We demonstrate how to produce nano test tubes of several sizes and compositions, including hybrid tubes with different inner and outer surfaces for targeted surface chemistry. Nano test tubes were readily suspended and stored in aqueous solutions without the need for chemical treatment. These nano test tubes should find application as delivery vehicles for therapeutics, particularly for processive 'bionanoreactors' loaded with enzymes.

Use of non-destructive controls for the supervision of operating apparatus

International Nuclear Information System (INIS)

Ducrot, Bernard.

1978-01-01

The scope of application of this paper, that is standard apparatus whether pressure or not, is presented. Then the particular problem of the use of non-destructive controls for the supervision of operating apparatus is outlined. The subject of how to exercise that supervision is developed by replying to four questions: why, when, how, who. A summary of the main advantages and disadvantages of the different control techniquess used is given in a tabular form. A last part deals with a series of practical applications, which show at the same time the interest and difficulties of that type of control [fr

Guidebook for the fabrication of non-destructive testing (NDT) test specimens

International Nuclear Information System (INIS)

2001-01-01

Non-destructive testing (NDT) test specimens constitute a very important part of training and certification of NDT personnel and are important for carrying out actual inspection and testing, and for achieving international harmonization of NDT practices. The IAEA organized an advisory group of experts to develop a Guidebook for Fabrication of NDT Test Specimens. The experts consulted the ISO/FDIS 9712-1999 requirements for training and certification of personnel and the suitability of various types of NDT test specimens that are needed to meet such requirements This guidebook presents a set of NDT test specimens, and the methodology and procedures for their fabrication

Non Destructive Analysis of Uranium by Radiometry

International Nuclear Information System (INIS)

Yusuf Nampira

2007-01-01

Uranium used in nuclear fuel development activity. the Substance use incurred by regulation safeguard. On that account in uranium acceptance conducted by verification of according to document by the specification of goods. Verification done by analysing performed uranium. The activity require by analyse method which simple and rapid analyses and has accurate result of analyses, is hence done by validation of non destructive uranium analysis that is with count gamma radiation from 235 U and product decay from 238 U. Quantitative analysis of uranium in substance determined by through count radiation-g at energy 185.72 keV and the use assess ratio of gamma radiation count from 235 U to 234 Pa to determine isotope content 235 U in substance. The result of analyses were given result of analysis with above correctness storey level 95% and have limit detect equivalent by 0.0174 mg U in U 3 O 8 . This method use at isotope uranium-235 analysis through count gamma radiation comparing method 235 U/ 234 Pa giving accuracy level 95% at sample equivalent uranium its content in 1 g uranium with isotope 235 U smaller than 75 weight percent. (author)

Early non-destructive biofouling detection and spatial distribution: Application of oxygen sensing optodes

KAUST Repository

Farhat, Nadia

2015-06-11

Biofouling is a serious problem in reverse osmosis/nanofiltration (RO/NF) applications, reducing membrane performance. Early detection of biofouling plays an essential role in an adequate anti-biofouling strategy. Presently, fouling of membrane filtration systems is mainly determined by measuring changes in pressure drop, which is not exclusively linked to biofouling. Non-destructive imaging of oxygen concentrations (i) is specific for biological activity of biofilms and (ii) may enable earlier detection of biofilm accumulation than pressure drop. The objective of this study was to test whether transparent luminescent planar O2 optodes, in combination with a simple imaging system, can be used for early non-destructive biofouling detection. This biofouling detection is done by mapping the two-dimensional distribution of O2 concentrations and O2 decrease rates inside a membrane fouling simulator (MFS). Results show that at an early stage, biofouling development was detected by the oxygen sensing optodes while no significant increase in pressure drop was yet observed. Additionally, optodes could detect spatial heterogeneities in biofouling distribution at a micro scale. Biofilm development started mainly at the feed spacer crossings. The spatial and quantitative information on biological activity will lead to better understanding of the biofouling processes, contributing to the development of more effective biofouling control strategies.

Non-destructive evaluation of timber structures in a historical building of Tiradentes , MG

Directory of Open Access Journals (Sweden)

Luciana Barbosa de Abreu

2013-09-01

Full Text Available Problems related to the durability of wood are commonly found in historical buildings structures. Preservation and conservation resolutions must be adopted, in order to avoid losses and substitutions, which mischaracterize buildings. Non-destructive methods for detecting deterioration should be used in order to substantiate decisions and increase the longevity of historical heritage. This work was carried out in order to perform non-destructive essays to infer about the integrity of a beam and a pillar of the original construction of the Sobrado Ramalho, a historical building of the city of Tiradentes, MG. The equipments utilized were the Stress Wave Timer and resistograph. Samples of the elements were taken for analysis of density. The results showed that, in both structures, to calculate the dynamic modulus of elasticity, there was no significant difference for the application of stress wave timer on the alignments studied. There was no significant difference between the directions of application of the resistograph on the pillar, due to its apparent entirety and regular sessions, practically square, and to not being loaded eccentrically. In the case of the beam, there was significant difference, presumably because it has cracks in its traction line. The equipments, unknown by professionals of heritage conservation allow promising methodologies for inspection of timber structures in service.

Radiation shielding material characterization by non-destructive neutron radiography technique

International Nuclear Information System (INIS)

Hafizal Yazid; Azali Muhammad; Abdul Aziz Mohamed; Rafhayudi Jamro; Hishamuddin Husain

2007-01-01

Shielding property of boronated rubber was characterized easily by the use of neutron radiography technique. For 10 phr of boron carbide in the natural rubber composite, the ability to completely shield against neutron was found to have 8mm thickness and above for the neutron flux of 1.04 x 10 5 n/cm 2 s (author)

Design and fabrication of liner-arroy ultrasonic transducer using KLM and FEM simulation for non-destructive testing

International Nuclear Information System (INIS)

Park, Chan Yuk; Sung, Jin Ho; Jeong, Jong Seob

2015-01-01

In this paper, a linear-array transducer capable of overcoming the faults of a single element and phased array transducers with convex shape for non-destructive ultrasonic testing was designed and fabricated. A 5.5 MHz linear-array transducer was designed using the PiezoCAD program based on the KLM analysis and the PZFlex program based on the FEM analysis. A 2-2 composite structure was employed to achieve broad-band characteristics. A 128 element linear-array transducer was fabricated and its performance was compared with the simulation results. The center frequency of the fabricated transducer was 5.5 Mhzand the -6 dB frequency bandwidth was 70 %. Thus, we expect that the designed transducer can provide an effective inner image of the test material during non-destructive ultrasonic testing.

Design and fabrication of liner-arroy ultrasonic transducer using KLM and FEM simulation for non-destructive testing

Energy Technology Data Exchange (ETDEWEB)

Park, Chan Yuk; Sung, Jin Ho; Jeong, Jong Seob [Dept. of Medical Biotechnology, Dongguk University Biomedi Campus, Goyang (Korea, Republic of)

2015-04-15

In this paper, a linear-array transducer capable of overcoming the faults of a single element and phased array transducers with convex shape for non-destructive ultrasonic testing was designed and fabricated. A 5.5 MHz linear-array transducer was designed using the PiezoCAD program based on the KLM analysis and the PZFlex program based on the FEM analysis. A 2-2 composite structure was employed to achieve broad-band characteristics. A 128 element linear-array transducer was fabricated and its performance was compared with the simulation results. The center frequency of the fabricated transducer was 5.5 Mhzand the -6 dB frequency bandwidth was 70 %. Thus, we expect that the designed transducer can provide an effective inner image of the test material during non-destructive ultrasonic testing.

Training guidelines in non-destructive testing techniques. 1991 edition

International Nuclear Information System (INIS)

1991-10-01

Non-destructive testing methods (NDT), by their very nature, allow components to be fully examined for properties or flaws without interfering with their usefulness. This grouping of inspection methods has grown from a handful of primitive techniques practised by artists to a widely known discipline which is an essential part of quality control, largely as a result of the standards demanded by the nuclear and aerospace industries. Recognizing the need for an international publication of NDT training syllabi, the IAEA Consultants Meeting on ''Qualification and Certification of NDT Personnel'' (Milan, 20-21 May 1986), recommended that the Agency publish the guidelines developed by Regional Working Group of the Latin America and Caribbean project. It was first issued in English in 1987 and has now been re-edited in English and Spanish and enlarged by the addition of programmes for other techniques

Data fusion: a new concept in non-destructive testing

International Nuclear Information System (INIS)

Georgel, B.; Lavayssiere, B.

1995-01-01

Non-destructive testing of some components (made of austenitic steel, or of a complex shape for example) requires quite often the use of several methods such as X-ray, ultrasonics, Eddy Currents. Then, a skilled operator is able to perform the expertise of the specimen. The main goal of this paper is to show that 3D diagnosis may be improved in term of reliability and precision by fusion of several NDT techniques. A data fusion algorithm is more that trying to improve the visualisation or the rendering of NDT data sets. It consists for each volume element, in computing a new value representing the combined information and in formulating a diagnosis on this basis. To achieve such a goal, know-how in modeling of physical phenomena and in applied mathematics is crucial. (authors). 4 refs., 2 figs

A new look at trends in non-destructive testing

International Nuclear Information System (INIS)

Forsten, J.

1984-01-01

Non-destructive testing (NDT) has been performed extensively for several decades. However, the NDT area is not in a static condition, as sophisticated equipment, improved procedures and new innovations keep development going on. Neither is the NDT field isolated from other fields, and this influences strongly the current situation, i.e.: The cost of electronics is decreasing and complex problems can now be solved; Safety requirements on products and components become more stringent; Quality requirements of the whole life span of a product or a component become more accentuated; Improved testing reliability is required; Quality assurance requirements must be imposed on NDT itself; New materials, e.g., fiber reinforced materials, and materials combinations, e.g., sandwich structures, will be used for special purposes; New production techniques, like glueing of metals, put new requirements on the NDT techniques

A novel combined approach of diffuse reflectance UV-Vis-NIR spectroscopy and multivariate analysis for non-destructive examination of blue ballpoint pen inks in forensic application.

Science.gov (United States)

Kumar, Raj; Sharma, Vishal

2017-03-15

The present research is focused on the analysis of writing inks using destructive UV-Vis spectroscopy (dissolution of ink by the solvent) and non-destructive diffuse reflectance UV-Vis-NIR spectroscopy along with Chemometrics. Fifty seven samples of blue ballpoint pen inks were analyzed under optimum conditions to determine the differences in spectral features of inks among same and different manufacturers. Normalization was performed on the spectroscopic data before chemometric analysis. Principal Component Analysis (PCA) and K-mean cluster analysis were used on the data to ascertain whether the blue ballpoint pen inks could be differentiated by their UV-Vis/UV-Vis NIR spectra. The discriminating power is calculated by qualitative analysis by the visual comparison of the spectra (absorbance peaks), produced by the destructive and non-destructive methods. In the latter two methods, the pairwise comparison is made by incorporating the clustering method. It is found that chemometric method provides better discriminating power (98.72% and 99.46%, in destructive and non-destructive, respectively) in comparison to the qualitative analysis (69.67%). Copyright © 2016 Elsevier B.V. All rights reserved.

Practical Uses of Neutron Radiography for Non-Destructive Testing

International Nuclear Information System (INIS)

Middleton, M.F.; de Beer, F.; Pazsit, Imre; Li, Kewen; Hilson, Jodie

2006-01-01

Over the past nine years, a research collaboration has been developed around the use of neutron radiography in non-destructive testing of porous rocks and other materials. This paper is a review of that work, with a critical reflection on the future potential of the technique. Neutrons are ideal for detecting water concentration, due to the high attenuation of neutrons by hydrogen, in porous or semi-porous media. Problems, which involve the determination of water concentration in porous media, are particularly amenable for neutron radiography analysis. In this context, water concentration in porous media is important in groundwater studies, petroleum reservoir studies, studies of geothermal systems, the understanding of water absorption in building materials, and more recently in mineral exploration and processing applications. Beyond these applications, neutron analysis of flawed and corroded aircraft parts has emerged as a valuable tool to support conventional non-destructive testing (NDT) techniques. Such investigations, using neutron radiography of aircraft parts, have been active in the United States, Canada and South Africa for over two decades. In 2001, an Australian Research Council (ARC) grant enabled the informal collaboration to establish a semi-portable neutron imaging system in Australia. Preliminary results of that ongoing research will also be presented herein. In overview, neutron radiography presents a powerful non-destructive testing method, which in many new areas of application remains to be evaluated. It has proven to be most valuable where water detection, in quantities greater than approximately 0.1 percent of the total volume, is required. This concentration is not a limitation on the technique, but only current applications. It has been demonstrated to be powerful tool to detect natural substances containing bound-water and neutron-attenuating minerals, such as clay, Glauconite and the various water-rich iron-bearing minerals (e.g. Goethite

Classification by a neural network approach applied to non destructive testing

International Nuclear Information System (INIS)

Lefevre, M.; Preteux, F.; Lavayssiere, B.

1995-01-01

Radiography is used by EDF for pipe inspection in nuclear power plants in order to detect defects. The radiographs obtained are then digitized in a well-defined protocol. The aim of EDF consists of developing a non destructive testing system for recognizing defects. In this paper, we describe the recognition procedure of areas with defects. We first present the digitization protocol, specifies the poor quality of images under study and propose a procedure to enhance defects. We then examine the problem raised by the choice of good features for classification. After having proved that statistical or standard textural features such as homogeneity, entropy or contrast are not relevant, we develop a geometrical-statistical approach based on the cooperation between signal correlations study and regional extrema analysis. The principle consists of analysing and comparing for areas with defects and without any defect, the evolution of conditional probabilities matrices for increasing neighborhood sizes, the shape of variograms and the location of regional minima. We demonstrate that anisotropy and surface of series of 'comet tails' associated with probability matrices, variograms slope and statistical indices, regional extrema location, are features able to discriminate areas with defects from areas without any. The classification is then realized by a neural network, which structure, properties and learning mechanisms are detailed. Finally we discuss the results. (authors). 21 refs., 5 figs

Non destructive methods for evaluating the mechanical properties of cemented toxic wastes

Energy Technology Data Exchange (ETDEWEB)

De Angelis, G. [ENEA, Centro Ricerche Casaccia, Rome (Italy). Dipt. Ambiente

1999-07-01

Measurements of resonant frequency and ultrasonic pulse velocity proved quite useful in order to follow the development of mechanical properties of cemented wastes in laboratory scale. Values of the elastic modulus (Young's modulus), shear and Poisson' s ratio have been obtained from these techniques and compared with dimensional movements and mechanical strength determined on the same formulations. The influence of crack formation on resonant frequency and quenching coefficient has also been evaluated in one case, in order to demonstrate the validity of such techniques for verifying any modification in the internal structure of the material. Sclerometric hardness was also determined on small samples and related to the compressive strength. However sclerometric measurements on full scale samples did not prove reliable. [Italian] Misure di frequenza di risonanza e di diffusione degli impulsi ultrasonici si sono rilevate un utile metodo di indagine a livello di laboratorio per meglio comprendere lo sviluppo delle proprieta' meccaniche dei rifiuti tossici condizionati in matrice cementizia. I valori del modulo di elasticita' (o modulo di Young), del modulo a torsione e del rapporto di Poisson, ottenuti mediante queste tecniche, sono stati messi in relazione con le variazioni dimensionali e con le proprieta' meccaniche di campioni ottenuti dallo stesso impasto. In un singolo caso e' stato valutato anche l'effetto che la formazione di crepe nel materiale esercita sul valore del picco di risonanza e sul coefficiente di smorzamento, allo scopo di dimostrare la validita' di queste tecniche nella verifica di modifiche insorte nella struttura interna di tali prodotti. Sono state fatte anche determinazioni di durezza per mezzo dello sclerometro, correlando i valori ottenuti con la resistenza alla compressione, mettendo altresi' in evidenza la non applicabilita' di tale metodo a manufatti preparati industrialmente.

Non-destructive estimation of leaf area for different plant ages and accessions of Capsicum annuum L.

NARCIS (Netherlands)

Swart, de E.A.M.; Groenwold, R.; Kanne, H.J.; Stam, P.; Marcelis, L.F.M.; Voorrips, R.E.

2004-01-01

Accurate measurements of leaf area are important for agronomic and physiological studies. To be able to perform repeated measurements of leaf area on single (genetically unique) plants, a method was developed to estimate leaf area from non-destructive measurements in Capsicum annuum L. independent

Non-inflammatory destructive periodontal disease: a clinical, microbiological, immunological and genetic investigation

Directory of Open Access Journals (Sweden)

Carlos Eduardo Repeke

2012-02-01

Full Text Available Periodontitis comprises a group of multifactorial diseases in which periodontopathogens accumulate in dental plaque and trigger host chronic inflammatory and immune responses against periodontal structures, which are determinant to the disease outcome. Although unusual cases of non-inflammatory destructive periodontal disease (NIDPD are described, their pathogenesis remains unknown. A unique NIDPD case was investigated by clinical, microbiological, immunological and genetic tools. The patient, a non-smoking dental surgeon with excessive oral hygiene practice, presented a generalized bone resorption and tooth mobility, but not gingival inflammation or occlusion problems. No hematological, immunological or endocrine alterations were found. No periodontopathogens (A. actinomycetemcomitans, P. gingivalis, F. nucleatum and T. denticola or viruses (HCMV, EBV-1 and HSV-1 were detected, along with levels of IL-1β and TNF-a in GCF compatible with healthy tissues. Conversely ALP, ACP and RANKL GCF levels were similar to diseased periodontal sites. Genetic investigation demonstrated that the patient carried some SNPs, as well HLA-DR4 (*0404 and HLA-B27 alleles, considered risk factors for bone loss. Then, a less vigorous and diminished frequency of toothbrushing was recommended to the patient, resulting in the arrest of alveolar bone loss, associated with the return of ALP, ACP and RANKL in GCF to normality levels. In conclusion, the unusual case presented here is compatible with the previous description of NIDPD, and the results that a possible combination of excessive force and frequency of mechanical stimulation with a potentially bone loss prone genotype could result in the alveolar bone loss seen in NIDPD.

Assessment of the excitelet algorithm for in-situ mechanical characterization of orthotropic structures

Science.gov (United States)

Ostiguy, Pierre-Claude; Quaegebeur, Nicolas; Masson, Patrice

2012-04-01

Damage detection and localization on composites can be impaired by inaccurate knowledge of the mechanical properties of the structure. This paper demonstrates the feasibility of using a chirplet-based correlation technique, called Excitelet, to evaluate the mechanical properties of orthotropic carbon fibre-based composite laminates. The method relies on the identification of an optimal correlation coefficient between measured and simulated dispersed signals measured on a structure using piezoceramic (PZT) transducers. Finite Element Model (FEM) is first conducted to demonstrate the capability of the approach to evaluate the mechanical properties of a composite structure. Experimental validation is then conducted on a unidirectionnal 2.30 mm thick laminate composed of unidirectional plies and a 2.35 mm thick laminate composed of unidirectional plies oriented at [0, 90]4s. Surface bonded PZT transducers were used both for actuation and sensing of guided waves bursts measured at 0° and 90° with respect to upper ply fibre orientation. The characterization is performed at various frequencies below 100 kHz using A0 or S0 modes and comparison with the material properties measured following ASTM standard testing is presented. The results indicate that large correlation coefficients are obtained between the measurements and simulated signals for both A0 and S0 modes when accurate properties are used as inputs for the model. Strategies based on multiple modes correlation are also assessed in order to improve the accuracy of the characterization approach. The results obtained using the proposed approach for the unidirectional plate and most of the results obtained using the proposed approach for the [0, 90]4s laminate are in agreement with the uncertainty associated with ASTM tests results while the proposed method is non destructive and can be performed prior to each imaging processing.

Accuracy of Non-Destructive Testing of PBRs to Estimate Fragilities

Science.gov (United States)

Brune, J. N.; Brune, R.; Biasi, G. P.; Anooshehpoor, R.; Purvance, M.

2011-12-01

Prior studies of Precariously Balanced Rocks (PBRs) have involved various methods of documenting rock shapes and fragilities. These have included non-destructive testing (NDT) methods such as photomodeling, and potentially destructive testing (PDT) such as forced tilt tests. PDT methods usually have the potential of damaging or disturbing the rock or its pedestal so that the PBR usefulness for future generations is compromised. To date we have force-tilt tested approximately 28 PBRs, and of these we believe 7 have been compromised. We suggest here that given other inherent uncertainties in the current methodologies, NDT methods are now sufficiently advanced as to be adequate for the current state of the art use for comparison with Ground Motion Prediction Equations (GMPEs) and seismic hazard maps (SHMs). Here we compare tilt-test static toppling estimates to three non-destructive methods: (1) 3-D photographic modeling (2) profile analysis assuming the rock is 2-D, and (3) expert judgments from photographs. 3-D modeling uses the commercial Photomodeler program and photographs in the field taken from numerous directions around the rock. The output polyhedral shape is analyzed in Matlab determine the center of mass and in Autocad to estimate the static overturning angle alpha. For the 2-D method we chose the photograph in profile looking perpendicular to the estimated direction of toppling. The rock is outlined as a 2-D object in Matlab. Rock dimensions, rocking points, and a vertical reference are supplied by the photo analyst to estimate the center of gravity and static force overturning angles. For the expert opinion method we used additional photographs taken from different directions to improve the estimates of the center of mass and the rocking points. We used 7 rocks for comparisons. The error in estimating tan alpha from 3-D modeling is about 0.05. For 2-D estimates an average error is about 0.1 (?). For expert opinion estimates the error is about 0.06. For

Non-destructive ripeness sensing by using proton NMR [Nuclear Magnetic Resonance

International Nuclear Information System (INIS)

Cho, Seong In; Krutz, G.W.; Stroshine, R.L.

1990-01-01

More than 80 kinds of fruits and vegetables are available in the United States. But only about 6 of them have their quality standards (Dull, 1986). In the 1990 Fresh Trends survey (Zind, 1990), consumers were asked to rate 16 characteristics important to their decision to purchase fresh produce. The four top ranking factors were ripeness/freshness, taste/flavor, appearance/condition and nutritional value. Of these surveyed, 96% rated ripeness/freshness as extremely important or very important. Therefore, the development of reliable grading or sorting techniques for fresh commodities is essential. Determination of fruit quality often involves cutting and tasting. Non-destructive quality control in fruit and vegetables is a goal of growers and distributors, as well as the food processing industry. Many nondestructive techniques have been evaluated including soft x-ray, optical transmission, near infrared radiation, and machine vision. However, there are few reports of successful non-destructive measurement of sugar content directly in fruit. Higher quality fruit could be harvested and available to consumers if a nondestructive sensor that detects ripeness level directly by measuring sugar content were available. Using proton Nuclear Magnetic Resonance (NMR) principle is the possibility. A nondestructive ripeness (or sweetness) sensor for fruit quality control can be developed with the proton NMR principle (Cho, 1989). Several feasibility studies were necessary for the ripeness sensor development. Main objectives in this paper was to investigate the feasibilities (1) to detect ripeness (or sweetness level) of raw fruit tissue with an high resolution proton NMR spectroscopy (200 MHz) and (2) to measure sugar content of intact fruit with a low resolution proton NMR spectroscopy (10 MHz). 7 refs., 4 figs

Non-destructive Ripeness Sensing by Using Proton NMR [Nuclear Magnetic Resonance

Science.gov (United States)

Cho, Seong In; Krutz, G. W.; Stroshine, R. L.; Bellon, V.

1990-01-01

More than 80 kinds of fruits and vegetables are available in the United States. But only about 6 of them have their quality standards (Dull, 1986). In the 1990 Fresh Trends survey (Zind, 1990), consumers were asked to rate 16 characteristics important to their decision to purchase fresh produce. The four top ranking factors were ripeness/freshness, taste/flavor, appearance/condition and nutritional value. Of these surveyed, 96% rated ripeness/freshness as extremely important or very important. Therefore, the development of reliable grading or sorting techniques for fresh commodities is essential. Determination of fruit quality often involves cutting and tasting. Non-destructive quality control in fruit and vegetables is a goal of growers and distributors, as well as the food processing industry. Many nondestructive techniques have been evaluated including soft x-ray, optical transmission, near infrared radiation, and machine vision. However, there are few reports of successful non-destructive measurement of sugar content directly in fruit. Higher quality fruit could be harvested and available to consumers if a nondestructive sensor that detects ripeness level directly by measuring sugar content were available. Using proton Nuclear Magnetic Resonance (NMR) principle is the possibility. A nondestructive ripeness (or sweetness) sensor for fruit quality control can be developed with the proton NMR principle (Cho, 1989). Several feasibility studies were necessary for the ripeness sensor development. Main objectives in this paper was to investigate the feasibilities (1) to detect ripeness (or sweetness level) of raw fruit tissue with an high resolution proton NMR spectroscopy (200 MHz) and (2) to measure sugar content of intact fruit with a low resolution proton NMR spectroscopy (10 MHz).

Terahertz non-destructive imaging of cracks and cracking in structures of cement-based materials

Directory of Open Access Journals (Sweden)

Shujie Fan

2017-11-01

Full Text Available Cracks and crack propagation in cement-based materials are key factors leading to failure of structures, affecting safety in construction engineering. This work investigated the application of terahertz (THz non-destructive imaging to inspections on structures of cement-based materials, so as to explore the potential of THz imaging in crack detection. Two kinds of disk specimens made of plain cement mortar and UHMWPE fiber concrete were prepared respectively. A mechanical expansion load device was deployed to generate cracks and control the whole process of cracking. Experimental tests were carried out on cracked specimens by using a commercial THz time domain spectroscopy (THz-TDS during loading. The results show that crack opening and propagation could be examined by THz clearly and the material factors influence the ability of crack resistance significantly. It was found that the THz imaging of crack initiation and propagation agrees with the practical phenomenon and supplies more information about damage of samples. It is demonstrated that the damage behavior of structures of cement-based materials can be successfully detected by THz imaging.

Terahertz non-destructive imaging of cracks and cracking in structures of cement-based materials

Science.gov (United States)

Fan, Shujie; Li, Tongchun; Zhou, Jun; Liu, Xiaoqing; Liu, Xiaoming; Qi, Huijun; Mu, Zhiyong

2017-11-01

Cracks and crack propagation in cement-based materials are key factors leading to failure of structures, affecting safety in construction engineering. This work investigated the application of terahertz (THz) non-destructive imaging to inspections on structures of cement-based materials, so as to explore the potential of THz imaging in crack detection. Two kinds of disk specimens made of plain cement mortar and UHMWPE fiber concrete were prepared respectively. A mechanical expansion load device was deployed to generate cracks and control the whole process of cracking. Experimental tests were carried out on cracked specimens by using a commercial THz time domain spectroscopy (THz-TDS) during loading. The results show that crack opening and propagation could be examined by THz clearly and the material factors influence the ability of crack resistance significantly. It was found that the THz imaging of crack initiation and propagation agrees with the practical phenomenon and supplies more information about damage of samples. It is demonstrated that the damage behavior of structures of cement-based materials can be successfully detected by THz imaging.

A new facility for non-destructive assay using a 252Cf source.

Science.gov (United States)

Stevanato, L; Caldogno, M; Dima, R; Fabris, D; Hao, Xin; Lunardon, M; Moretto, S; Nebbia, G; Pesente, S; Pino, F; Sajo-Bohus, L; Viesti, G

2013-03-01

A new laboratory facility for non-destructive analysis (NDA) using a time-tagged (252)Cf source is presented. The system is designed to analyze samples having maximum size of about 20 × 25 cm(2), the material recognition being obtained by measuring simultaneously total and energy dependent transmission of neutrons and gamma rays. The equipment technical characteristics and performances of the NDA system are presented, exploring also limits due to the sample thickness. Some recent applications in the field of cultural heritage are presented. Copyright © 2012 Elsevier Ltd. All rights reserved.

Template synthesis of test tube nanoparticles using non-destructive replication

International Nuclear Information System (INIS)

Wagner, Jonathan; Rodgers, David; Yao Jingyuan; Hinds, Bruce

2013-01-01

Nano test tubes are a promising delivery vehicle for a range of therapeutics, including small molecule drugs and biologics. However, current template synthesis methods of producing nano test tubes are prohibitively expensive and time consuming. Here, non-destructive template replication was used to increase nano test tube yield from porous alumina by more than a hundredfold. We demonstrate how to produce nano test tubes of several sizes and compositions, including hybrid tubes with different inner and outer surfaces for targeted surface chemistry. Nano test tubes were readily suspended and stored in aqueous solutions without the need for chemical treatment. These nano test tubes should find application as delivery vehicles for therapeutics, particularly for processive ‘bionanoreactors’ loaded with enzymes. (paper)

European Non Destructive Examination Forum (ENDEF)

Energy Technology Data Exchange (ETDEWEB)

Deffrennes, M [EC, DG XVII, Nuclear Energy, Brussels (Belgium); Engl, G [Siemens AG Energieerzeugung KWU, Erlangen (Germany); Estorff, U von [EC, JRC/IAM, Petten (Netherlands)

1998-11-01

ENDEF, an initiative of the European Commission, DG XVII (Energy) was well supported by the European industrial institutions working in assistance with nuclear industrial organisations in the CEEC`s (Central and Eastern European Countries) and NIS`s (New Independent States). This Forum provides effectively a platform for open discussion between representatives of industrial actors active in the NDE (Non Destructive Examination)/ISI (In Service Inspection) field with the purpose to establish a co-operation pattern between qualified representatives of the EU (European Union) industry to offer a better co-ordinated and well defined assistance to the CEEC`s and NIS in the field of NDE/ISI, and to lay the ground for further industrial co-operation. ENDEF developed a strategy to follow for the establishment of co-operation projects. This strategy is now used to understand the extent of past or present assistance projects and to identify the areas where more co-operation is needed. ENDEF encourages the creation in the NIS`s and CEEC`s of similar forums in order to increase the co-operation and co-ordination. ENDEF is also working in perfect agreement with the European Network ENIQ, piloted by the European plant operators. This identity of views lead to the leadership by the ENDEF co-ordinator of the ENIQ Task 3 involving Applications of the European Methodology for ISI qualification in the CEEC`s and NIS`s and presently fully integrated in ENDEF. (orig.)

Example value-impact analysis of non-destructive examination methods used for inservice inspection of BWR piping

International Nuclear Information System (INIS)

Tabatabai, A.S.; Simonen, F.A.

1985-12-01

This paper describes work recently completed at Pacific Northwest Laboratory (PNL) to use value-impact (V/I) analysis methods to help guide research to improve the effectiveness of inservice inspection (ISI) procedures at nuclear power plants. The example developed at PNL uses the results of probabilistic fracture mechanics and probabilistic risk analysis (PRA) studies to compare three generic categories of non-destructive examination (NDE) methods. These NDE methods are used to detect possible pipe cracks such as those induced by intergranular stress corrosion (IGSCC). The results of the analysis of this example include (1) quantification of the effectiveness of ISI in increasing plant safety in terms of reduction in core-melt frequency, (2) estimates of the industry cost of performing ISI, (3) estimates of radiation exposures to plant personnel as a result of performing ISI, and (4) potential areas of improvement in the NDE and ISI process

Fouling development in direct contact membrane distillation: Non-invasive monitoring and destructive analysis

KAUST Repository

Fortunato, Luca

2017-12-26

Fouling development in direct contact membrane distillation (DCMD) for seawater desalination was evaluated combining in-situ monitoring performed using optical coherence tomography (OCT) together with destructive techniques. The non-invasive monitoring with OCT provided a better understanding of the fouling mechanism by giving an appropriate sampling timing for the membrane autopsy. The on-line monitoring system allowed linking the flux trend with the structure of fouling deposited on the membrane surface. The water vapor flux trend was divided in three phases based on the deposition and formation of different foulants over time. The initial flux decline was due to the deposition of a 50–70 nm porous fouling layer consisting of a mixture of organic compounds and salts. Liquid chromatography with organic carbon detection (LC-OCD) analysis revealed the abundance of biopolymer in the fouling layer formed at the initial phase. In the second phase, formation of carbonate crystals on the membrane surface was observed but did not affect the flux significantly. In the last phase, the water vapor flux dropped to almost zero due to the deposition of a dense thick layer of sulfate crystals on the membrane surface.

Non-destructive evaluation of welding part of stainless steels by phased array system

International Nuclear Information System (INIS)

Tatematsu, Nobuhiro; Matsumoto, Eiji

2009-01-01

Recently, more accurate and convenient Non-Destructive Evaluation techniques are required for flaw inspection of structural materials. Phased array ultrasonic transducers are expected as such as NDE technique but there are many subjects to be solved. Furthermore, commercial phased array systems with conventional scanning and imaging techniques have not fulfilled their maximum potential. The purpose of this paper is to improve the phased array system to be applicable to the inhomogeneity evaluation of welding part of stainless steels. (author)

Additive Manufacturing (AM) Activities and Non-Destructive Evaluation (NDE) at GSFC

Science.gov (United States)

Jones, Justin S.

2017-01-01

NASA personnel will be meeting with a delegation from the Japan Aerospace Exploration Agency (JAXA) Office of Safety and Mission Assurance (OSMA) at Langley Research Center on 2217 through 3217. The purpose of the meeting is a technical interchange between NASA and JAXA to discuss Non-Destructive Evaluation (NDE) of Additive Manufacturing (AM) parts and the HALT process (relates to accelerated life testing). The visitors will be a small group of Japanese citizens. Goddard Space Flight Center (GSFC) has been asked to participate in the meeting, either in person or via teleconference. This presentation covers NDE efforts at GSFC and provides a cursory overview of AM and lab capabilities.

Non-destructive synchrotron X-ray diffraction mapping of a Roman painting

International Nuclear Information System (INIS)

Dooryhee, E.; Anne, M.; Hodeau, J.-L.; Martinetto, P.; Rondot, S.; Bardies, I.; Salomon, J.; Walter, P.; Vaughan, G.B.M.

2005-01-01

The history and the properties of materials are deduced not only from their elemental and molecular signatures, but also from their exact phase compositions, and from the structures and the defects of their constituents. Here we implement a non-destructive synchrotron X-ray based method, which combines both the quantitative structural content of diffraction and the imaging mode. As a demonstration case, the pigments of a Roman wall painting are examined. The joined elemental and mineral maps mimic the major features of the painting. Different structural phases made of common atomic elements are differentiated. Textures and graininess are measured and related to the artist's know-how. (orig.)

An integrated approach of non-destructive tests for inspection and characterization of cultural heritage: case study of Monastery of Batalha, Portugal

Science.gov (United States)

Gonçalves, Luisa; Valença, Jonatas; Barraca, Nuno; Gaspar, Florindo

2017-04-01

The built heritage under the ambient conditions, even with a proper maintenance, can have pathologies and defects due to deterioration of materials, repeated loads and exceptional events. It is widely recognized that new technologies can play an important role in documentation, interpretation, diagnosis, monitoring and preservation of our cultural heritage legacy. The complexity of these innovative systems continues to increase and 3D digital construction and documentation of built heritage remains a complex issue. The methodologies typically involves a hybrid approach to the visualization of heterogeneous datasets such as multispectral images, geophysics data, thermographic images and 3D imaging data (laser scanning, photogrammetry). Thus an integrated approach to understand and support heritage documentation and preservation of ancient historical environments is demanded. In this paper the authors present a method that merge a set of non-destructive tests performed using terrestrial laser scanning, infrared thermography, ground penetrating radar (GPR) and multispectral images. The method was applied in the inspection and characterization of the Monastery of Santa Maria da Vitória, also known as the Monastery of Batalha. The historical Monastery of Batalha is one of the most beautiful and important examples of Portuguese and European architecture, composed by several styles, namely Gothic, Manuelino and some renaissance details, being part of the UNESCO World Heritage List since December 1983. A framework based on integrate innovative techniques was applied in order to obtain high-fidelity 3D models from existing heritage, allowing to record and analyze relevant spatial 3D data. Ground-penetrating radar (GPR) is also proposed as a solution to characterize and document structural damages and other pathologies as well as to provide information regarding the internal structure and building technics of the monument. Methodologies for data acquisition are also

LL/ILW: Post-Qualification of Old Waste through Non-Destructive Extraction of Barrels from Cement Shields - 13535

International Nuclear Information System (INIS)

Oehmigen, Steffen; Ambos, Frank

2013-01-01

Currently there is a large number of radioactive waste drums entombed in cement shields at German nuclear power plants. These concrete containers used in the past for the waste are not approved for the final repository. Compliance with current acceptance criteria of the final repository has to be proven by qualification measures on the waste. To meet these criteria, a new declaration and new packing is necessary. A simple non-destructive extraction of about 2000 drums from their concrete shields is not possible. So different methods were tested to find a way of non-destructive extraction of old waste drums from cement shields and therefore reduce the final repository volume and final repository costs by using a container accepted and approved for Konrad. The main objective was to build a mobile system to offer this service to nuclear plant stations. (authors)

Non-destructive flavour evaluation of red onion (Allium cepa L.) ecotypes: an electronic-nose-based approach.

Science.gov (United States)

Russo, Mariateresa; di Sanzo, Rosa; Cefaly, Vittoria; Carabetta, Sonia; Serra, Demetrio; Fuda, Salvatore

2013-11-15

This work reports preliminary results on the potential of a metal oxide sensor (MOS)-based electronic nose, as a non-destructive method to discriminate three "Tropea Red Onion" PGI ecotypes (TrT, TrMC and TrA) from each other and the common red onion (RO), which is usually used to counterfeit. The signals from the sensor array were processed using a canonical discriminant function analysis (DFA) pattern recognition technique. The DFA on onion samples showed a clear separation among the four onion groups with an overall correct classification rate (CR) of 97.5%. Onion flavour is closely linked to pungency and thus to the pyruvic acid content. The e-nose analysis results are in good agreement with pyruvic acid analysis. This work demonstrated that artificial olfactory systems have potential for use as an innovative, rapid and specific non-destructive technique, and may provide a method to protect food products against counterfeiting. Copyright © 2013 Elsevier Ltd. All rights reserved.

Sampling methods and non-destructive examination techniques for large radioactive waste packages

International Nuclear Information System (INIS)

Green, T.H.; Smith, D.L.; Burgoyne, K.E.; Maxwell, D.J.; Norris, G.H.; Billington, D.M.; Pipe, R.G.; Smith, J.E.; Inman, C.M.

1992-01-01

Progress is reported on work undertaken to evaluate quality checking methods for radioactive wastes. A sampling rig was designed, fabricated and used to develop techniques for the destructive sampling of cemented simulant waste using remotely operated equipment. An engineered system for the containment of cooling water was designed and manufactured and successfully demonstrated with the drum and coring equipment mounted in both vertical and horizontal orientations. The preferred in-cell orientation was found to be with the drum and coring machinery mounted in a horizontal position. Small powdered samples can be taken from cemented homogeneous waste cores using a hollow drill/vacuum section technique with the preferred subsampling technique being to discard the outer 10 mm layer to obtain a representative sample of the cement core. Cement blends can be dissolved using fusion techniques and the resulting solutions are stable to gelling for periods in excess of one year. Although hydrochloric acid and nitric acid are promising solvents for dissolution of cement blends, the resultant solutions tend to form silicic acid gels. An estimate of the beta-emitter content of cemented waste packages can be obtained by a combination of non-destructive and destructive techniques. The errors will probably be in excess of +/-60 % at the 95 % confidence level. Real-time X-ray video-imaging techniques have been used to analyse drums of uncompressed, hand-compressed, in-drum compacted and high-force compacted (i.e. supercompacted) simulant waste. The results have confirmed the applicability of this technique for NDT of low-level waste. 8 refs., 12 figs., 3 tabs

Non-destructive technique to verify clearance of pipes

Directory of Open Access Journals (Sweden)

Savidou Anastasia

2010-01-01

Full Text Available A semi-empirical, non-destructive technique to evaluate the activity of gamma ray emitters in contaminated pipes is discussed. The technique is based on in-situ measurements by a portable NaI gamma ray spectrometer. The efficiency of the detector for the pipe and detector configuration was evaluated by Monte Carlo calculations performed using the MCNP code. Gamma ray detector full-energy peak efficiency was predicted assuming a homogeneous activity distribution over the internal surface of the pipe for 344 keV, 614 keV, 662 keV, and 1332 keV photons, representing Eu-152, Ag-118m, Cs-137, and Co-60 contamination, respectively. The effect of inhomogeneity on the accuracy of the technique was also examined. The model was validated against experimental measurements performed using a Cs-137 volume calibration source representing a contaminated pipe and good agreement was found between the calculated and experimental results. The technique represents a sensitive and cost-effective technology for calibrating portable gamma ray spectrometry systems and can be applied in a range of radiation protection and waste management applications.

Characterisation of nuclear dispersion fuels. The non-destructive examination of silicon carbide by selenium immersion

Energy Technology Data Exchange (ETDEWEB)

Ambler, J.F.R.; Ferguson, I.F.

1974-07-15

The non-destructive microscopic examination of silicon-carbide-coated spheres containing uranium carbide, which involves immersing the coated spheres in selenium, is particularly suited for the examination of flaws in the coats but it is not possible to measure coating thicknesses by this method. Some coats are found to be opaque and this is related to their porosity. (auth)

A non-destructive ammonium detection method as indicator for freshness for packed fish: Application on cod

NARCIS (Netherlands)

Heising, J.K.; Dekker, M.; Bartels, P.V.; Boekel, van M.A.J.S.

2012-01-01

This paper introduces a non-destructive method for monitoring headspace ammonium as an indicator for changes in the freshness status of packed fish. Electrodes in an aqueous phase in the package monitor changes in the concentration of ammonia produced in/on the packed fish and released in the

A non-destructive selection method for faster growth at suboptimal temperature in common bean (Phaseolus vulgaris)

NARCIS (Netherlands)

Drijfhout, E.; Oeveren, J.C. van; Jansen, R.C.

1991-01-01

A non-destructive method has been developed to select common bean (Phaseolus vulgaris L.) plants whose growth is less effected at a suboptimal temperature. Shoot weight was determined at a suboptimal (14°C) and optimal temperature (20°C), 38 days after sowing and accessions identified with a

Characterization of Irradiated and Non-Irradiated Rubber from Automotive Scrap Tires

Science.gov (United States)

Souza, Clécia Moura; Silva, Leonardo G.

The aim of this work was to characterize the samples of irradiated and non-irradiated rubber from automotive scrap tires. Rubber samples from scrap tires were irradiated at irradiation doses of 200, 400 and 600kGy in an electron beam accelerator. Subsequently, both the irradiated and non-irradiated samples were characterized by thermogravimetry (TG), differential scanning calorimetry (DSC), tensile strength mechanical test, and Fourier transform infrared (FTIR) spectrophotometry.

Non destructive testing: a unique R and D platform in Europe in Saclay

International Nuclear Information System (INIS)

On, Dinhill

2012-01-01

This article presents the 'Gerim 2' R and D platform which is dedicated to non destructive testing (NDT) in the field of information and communication technology (ICT). It is the first of its kind in Europe and is located in Saclay. It possesses a wide spectrum of NDT technologies: contactless ultrasonic testing, ultrasonic adaptive imagery, automated and multi-resolution X-ray tomography, etc. Founded by public research institutions and industrial partners, this centre is dedicated only to research and development

Survey of EEC solid waste arisings and performance of non-destructive assay systems

International Nuclear Information System (INIS)

Bremner, W.B.; Adaway, D.W.; Yates, A.

1992-01-01

This report covers the work carried out during an one-year contract which surveyed the radioactive solid waste arisings in EEC Member States and also tabulated information on the performance of the non-destructive assay (NDA) system used. The work was jointly carried out with CEA partners at Cadarache and Paris. The tabulated data give information on types, packaging, associated activity, and NDA capability of the utilities or research organisations. Some short comings in NDA capabilities are identified and possible solutions are given

Interpretation of Actinide-Distribution Data Obtained from Non-Destructive and Destructive Post-Test Analyses of an Intact-Core Column of Culebra Dolomite

International Nuclear Information System (INIS)

LUCERO, DANIEL A.; PERKINS, W. GEORGE

1999-01-01

The US DOE, with technical assistance from Sandia National Laboratories, has successfully received EPA certification and opened the Waste Isolation Pilot Plant (WIPP), a nuclear waste disposal facility located approximately 42 km east of Carlsbad, New Mexico. Performance assessment analyses indicate that human intrusions by inadvertent, intermittent drilling for resources provide the only credible mechanisms for releases of radionuclides from the disposal system. In modeling long-term brine releases, subsequent to a drilling event, potential migration pathways through the permeable layers of rock above the Salado formation were analyzed. Major emphasis is placed on the Culebra Member of the Rustler Formation because this is the most transmissive geologic layer overlying the WIPP site. In order to help quantify parameters for the calculated releases, radionuclide transport experiments have been earned out using intact-core columns obtained from the Culebra dolomite member of the Rustler Formation within the WIPP site. This paper deals primarily with results of analyses for 241 Pu and 241 Am distributions developed during transport experiments in one of these cores. Transport experiments were done using a synthetic brine that simulates Culebra brine at the core recovery location (the WIPP air-intake shaft--AIS). Hydraulic characteristics (i.e., apparent porosity and apparent dispersion coefficient) for intact-core columns were obtained via experiments using the conservative tracer 22 Na. Elution experiments carried out over periods of a few days with tracers 232 U and 239 Np indicated that these tracers were weakly retarded as indicated by delayed elution of the species. Elution experiments with tracers 241 Pu and 241 Am were attempted, but no elution of either species has been observed to date, including experiments of many months' duration. In order to quantify retardation of the non-eluted species 241 Pu and 241 Am after a period of brine flow, non-destructive and

Thermal Transmission through Existing Building Enclosures: Destructive Monitoring in Intermediate Layers versus Non-Destructive Monitoring with Sensors on Surfaces.

Science.gov (United States)

Echarri, Víctor; Espinosa, Almudena; Rizo, Carlos

2017-12-08

Opaque enclosures of buildings play an essential role in the level of comfort experienced indoors and annual energy demand. The impact of solar radiation and thermal inertia of the materials that make up the multi-layer enclosures substantially modify thermal transmittance behaviour of the enclosures. This dynamic form of heat transfer, additionally affected by indoor HVAC systems, has a substantial effect on the parameters that define comfort. It also has an impact on energy demand within a daily cycle as well as throughout a one-year use cycle. This study describes the destructive monitoring of an existing block of flats located in Alicante. Once the enclosure was opened, sensors of temperature (PT100), air velocity, and relative humidity were located in the different layers of the enclosure, as well as in the interior and exterior surfaces. A pyranometer was also installed to measure solar radiation levels. A temperature data correction algorithm was drawn up to address irregularities produced in the enclosure. The algorithm was applied using a Raspberry Pi processor in the data collection system. The comparative results of temperature gradients versus non-destructive monitoring systems are presented, providing measures of the transmittance value, surface temperatures and indoor and outdoor air temperatures. This remote sensing system can be used in future studies to quantify and compare the energy savings of different enclosure construction solutions.

Thermal Transmission through Existing Building Enclosures: Destructive Monitoring in Intermediate Layers versus Non-Destructive Monitoring with Sensors on Surfaces

Directory of Open Access Journals (Sweden)

Víctor Echarri

2017-12-01

Full Text Available Opaque enclosures of buildings play an essential role in the level of comfort experienced indoors and annual energy demand. The impact of solar radiation and thermal inertia of the materials that make up the multi-layer enclosures substantially modify thermal transmittance behaviour of the enclosures. This dynamic form of heat transfer, additionally affected by indoor HVAC systems, has a substantial effect on the parameters that define comfort. It also has an impact on energy demand within a daily cycle as well as throughout a one-year use cycle. This study describes the destructive monitoring of an existing block of flats located in Alicante. Once the enclosure was opened, sensors of temperature (PT100, air velocity, and relative humidity were located in the different layers of the enclosure, as well as in the interior and exterior surfaces. A pyranometer was also installed to measure solar radiation levels. A temperature data correction algorithm was drawn up to address irregularities produced in the enclosure. The algorithm was applied using a Raspberry Pi processor in the data collection system. The comparative results of temperature gradients versus non-destructive monitoring systems are presented, providing measures of the transmittance value, surface temperatures and indoor and outdoor air temperatures. This remote sensing system can be used in future studies to quantify and compare the energy savings of different enclosure construction solutions.

Thermal Transmission through Existing Building Enclosures: Destructive Monitoring in Intermediate Layers versus Non-Destructive Monitoring with Sensors on Surfaces

Science.gov (United States)

Echarri, Víctor; Espinosa, Almudena; Rizo, Carlos

2017-01-01

Opaque enclosures of buildings play an essential role in the level of comfort experienced indoors and annual energy demand. The impact of solar radiation and thermal inertia of the materials that make up the multi-layer enclosures substantially modify thermal transmittance behaviour of the enclosures. This dynamic form of heat transfer, additionally affected by indoor HVAC systems, has a substantial effect on the parameters that define comfort. It also has an impact on energy demand within a daily cycle as well as throughout a one-year use cycle. This study describes the destructive monitoring of an existing block of flats located in Alicante. Once the enclosure was opened, sensors of temperature (PT100), air velocity, and relative humidity were located in the different layers of the enclosure, as well as in the interior and exterior surfaces. A pyranometer was also installed to measure solar radiation levels. A temperature data correction algorithm was drawn up to address irregularities produced in the enclosure. The algorithm was applied using a Raspberry Pi processor in the data collection system. The comparative results of temperature gradients versus non-destructive monitoring systems are presented, providing measures of the transmittance value, surface temperatures and indoor and outdoor air temperatures. This remote sensing system can be used in future studies to quantify and compare the energy savings of different enclosure construction solutions. PMID:29292781

Non-destructive pollution exposure assessment in the European hedgehog (Erinaceus europaeus): IV hair versus soil analysis in exposure and risk assessment of organochlorine compounds

NARCIS (Netherlands)

Havé, D' H.; Scheirs, J.; Covaci, A.; Brink, van den N.W.; Verhagen, R.; Coen, De W.

2007-01-01

Few ecotoxicological studies on mammals use non-destructive methodologies, despite the growing ethical concern over the use of destructive sampling methods. In the present study we assessed exposure of hedgehogs (Erinaceus europaeus) to polychlorinated biphenyls (PCBs),

Non-destructive in situ study of “Mad Meg” by Pieter Bruegel the Elder using mobile X-ray fluorescence, X-ray diffraction and Raman spectrometers

Energy Technology Data Exchange (ETDEWEB)

Van de Voorde, Lien, E-mail: lien.vandevoorde@ugent.be [Ghent University, Department of Analytical Chemistry, X-ray Microspectroscopy and Imaging Research Group, Krijgslaan 281 S12, B-9000 Gent (Belgium); Van Pevenage, Jolien [Ghent University, Department of Analytical Chemistry, Raman Spectroscopy Research Group, Krijgslaan 281 S12, B-9000 Gent (Belgium); De Langhe, Kaat [Ghent University, Department of Archaeology, Archaeometry Research Group, Sint-Pietersnieuwstraat 35, B-9000 Gent (Belgium); De Wolf, Robin; Vekemans, Bart; Vincze, Laszlo [Ghent University, Department of Analytical Chemistry, X-ray Microspectroscopy and Imaging Research Group, Krijgslaan 281 S12, B-9000 Gent (Belgium); Vandenabeele, Peter [Ghent University, Department of Archaeology, Archaeometry Research Group, Sint-Pietersnieuwstraat 35, B-9000 Gent (Belgium); Martens, Maximiliaan P.J. [Ghent University, Department of Art, Music and Theatre Sciences, Blandijnberg 2, B-9000 Gent (Belgium)

2014-07-01

“Mad Meg”, a figure of Flemish folklore, is the subject of a famous oil-on-panel painting by the Flemish renaissance artist Pieter Bruegel the Elder, exhibited in the Museum Mayer van den Bergh (Antwerp, Belgium). This article reports on the in situ chemical characterization of this masterpiece by using currently available state-of-the-art portable analytical instruments. The applied non-destructive analytical approach involved the use of a) handheld X-ray fluorescence instrumentation for retrieving elemental information and b) portable X-ray fluorescence/X-ray diffraction instrumentation and laser-based Raman spectrometers for obtaining structural/molecular information. Next to material characterization of the used pigments and of the different preparation layers of the painting, also the verification of two important historical iconographic hypotheses is performed concerning the economic way of painting by Brueghel, and whether or not he used blue smalt pigment for painting the boat that appears towards the top of the painting. The pigments identified are smalt pigment (65% SiO{sub 2} + 15% K{sub 2}O + 10% CoO + 5% Al{sub 2}O{sub 3}) for the blue color present in all blue areas of the painting, probably copper resinate for the green colors, vermillion (HgS) as red pigment and lead white is used to form different colors. The comparison of blue pigments used on different areas of the painting gives no differences in the elemental fingerprint which confirms the existing hypothesis concerning the economic painting method by Bruegel. - Highlights: • In situ, non-destructive investigation of a famous painting by Pieter Bruegel. • Use of a new, commercial available, portable XRF/XRD instrumentation. • Multi-methodological approach: make also use of a mobile Raman spectrometer. • Used pigments and different preparation layers of the painting are characterized. • The verification of two important historical iconographic hypotheses are performed.

Non-destructive in situ study of “Mad Meg” by Pieter Bruegel the Elder using mobile X-ray fluorescence, X-ray diffraction and Raman spectrometers

International Nuclear Information System (INIS)

Van de Voorde, Lien; Van Pevenage, Jolien; De Langhe, Kaat; De Wolf, Robin; Vekemans, Bart; Vincze, Laszlo; Vandenabeele, Peter; Martens, Maximiliaan P.J.

2014-01-01

“Mad Meg”, a figure of Flemish folklore, is the subject of a famous oil-on-panel painting by the Flemish renaissance artist Pieter Bruegel the Elder, exhibited in the Museum Mayer van den Bergh (Antwerp, Belgium). This article reports on the in situ chemical characterization of this masterpiece by using currently available state-of-the-art portable analytical instruments. The applied non-destructive analytical approach involved the use of a) handheld X-ray fluorescence instrumentation for retrieving elemental information and b) portable X-ray fluorescence/X-ray diffraction instrumentation and laser-based Raman spectrometers for obtaining structural/molecular information. Next to material characterization of the used pigments and of the different preparation layers of the painting, also the verification of two important historical iconographic hypotheses is performed concerning the economic way of painting by Brueghel, and whether or not he used blue smalt pigment for painting the boat that appears towards the top of the painting. The pigments identified are smalt pigment (65% SiO 2 + 15% K 2 O + 10% CoO + 5% Al 2 O 3 ) for the blue color present in all blue areas of the painting, probably copper resinate for the green colors, vermillion (HgS) as red pigment and lead white is used to form different colors. The comparison of blue pigments used on different areas of the painting gives no differences in the elemental fingerprint which confirms the existing hypothesis concerning the economic painting method by Bruegel. - Highlights: • In situ, non-destructive investigation of a famous painting by Pieter Bruegel. • Use of a new, commercial available, portable XRF/XRD instrumentation. • Multi-methodological approach: make also use of a mobile Raman spectrometer. • Used pigments and different preparation layers of the painting are characterized. • The verification of two important historical iconographic hypotheses are performed

Non-destructive analysis of rape plant pod by neutron radiography

International Nuclear Information System (INIS)

Makino-Nakanishi, Tomoko; Inanaga, Shinobu; Kobayashi, Hisao.

1991-01-01

Since the ripening process of the rape plant pod has not been studied well, non-destructive analysis of the pod has been carried out by neutron radiography. From the water distribution in the pod, the formation of pod parenchyma as well as vascular system were clearly observed. During the ripening process of the pod water content and weight of the seed were measured. It was found that at the early stage of the ripening process the water content of the seed became maximum and began to decrease, whereas the weight of each seed was gradually increased throughout the ripening process. Neutron radiography, which shows the water content of the pod, will give the clue to the decrease of the water content of the seed from the middle of the ripening process. (author)

Application of magnetic resonance imaging to non-destructive void detection in watermelon

Science.gov (United States)

Saito, K.; Miki, T.; Hayashi, S.; Kajikawa, H.; Shimada, M.; Kawate, Y.; Nishizawa, T.; Ikegaya, D.; Kimura, N.; Takabatake, K.; Sugiura, N.; Suzuki, M.

A novel application of magnetic resonance imaging (MRI) is described. The possibility of utilizing MRI for non-destructive quality evaluation of watermelons was studied. In this study, we applied MRI to the detection of internal voids in watermelons. In order to increase the measurement rate, we employed a one-dimensional projection profile method instead of observing a two-dimensional cross-sectional image. The void detection was carried out with this technique over 30 samples and 28 samples were correctly evaluated. The measurement rate was 900 ms per sample, which is an acceptable speed for a sorting machine in the agricultural field.

The Heterogeneity of Job Creation and Destruction in Transition and Non-transition Developing Countries: The Effects of Firm Size, Age and Ownership

Directory of Open Access Journals (Sweden)

Haggai Kennedy Ochieng

2017-12-01

Full Text Available This paper investigates how firm age, size and ownership are related with job creation and destruction, and how these patterns differ across transition and non-transition economies. The analysis finds that age is inversely related with gross job creation and net job creation in the two samples. This finding is consistent with the theory of the learning effect. The relationship between age and job destruction is indifferent in non-transition economies. On the contrary, old firms in transition economies destroy more jobs than young ones. The paper further establishes an inverse relationship between size and gross job creation in the two groups. However, there is divergence between the two samples; small firms in non-transition economies also exhibit a higher gross job destruction rate. Consequently large firms have a higher net job creation rate. In transition economies, small and large firms exhibit similar rates of job destruction. But small firms retain a higher net job creation rate. A more intriguing finding is that state owned firms do not underperform domestic private ones. This means these countries may be using soft budget constraint which allows state owned firms to overstaff. Finally, crowding out of SMEs by foreign owned firms is not evident in transition economies.

Mechanical and physical properties of hydrothermally altered rocks, Taupo Volcanic Zone, New Zealand

Science.gov (United States)

Wyering, L. D.; Villeneuve, M. C.; Wallis, I. C.; Siratovich, P. A.; Kennedy, B. M.; Gravley, D. M.; Cant, J. L.

2014-11-01

Mechanical characterization of hydrothermally altered rocks from geothermal reservoirs will lead to an improved understanding of rock mechanics in a geothermal environment. To characterize rock properties of the selected formations, we prepared samples from intact core for non-destructive (porosity, density and ultrasonic wave velocities) and destructive laboratory testing (uniaxial compressive strength). We characterised the hydrothermal alteration assemblage using optical mineralogy and existing petrography reports and showed that lithologies had a spread of secondary mineralisation that occurred across the smectite, argillic and propylitic alteration zones. The results from the three geothermal fields show a wide variety of physical rock properties. The testing results for the non-destructive testing shows that samples that originated from the shallow and low temperature section of the geothermal field had higher porosity (15 - 56%), lower density (1222 - 2114 kg/m3) and slower ultrasonic waves (1925 - 3512 m/s (vp) and 818 - 1980 m/s (vs)), than the samples from a deeper and higher temperature section of the field (1.5 - 20%, 2072 - 2837 kg/m3, 2639 - 4593 m/s (vp) and 1476 - 2752 m/s (vs), respectively). The shallow lithologies had uniaxial compressive strengths of 2 - 75 MPa, and the deep lithologies had strengths of 16 - 211 MPa. Typically samples of the same lithologies that originate from multiple wells across a field have variable rock properties because of the different alteration zones from which each sample originates. However, in addition to the alteration zones, the primary rock properties and burial depth of the samples also have an impact on the physical and mechanical properties of the rock. Where this data spread exists, we have been able to derive trends for this specific dataset and subsequently have gained an improved understanding of how hydrothermal alteration affects physical and mechanical properties.

Inspection with non destructive assay techniques of the aluminium coating of the TRIGA Mark III reactor vat; Inspeccion con tecnicas de ensayos no destructivos del recubrimiento de aluminio de la tina del reactor TRIGA Mark III

Energy Technology Data Exchange (ETDEWEB)

Reyes A, A.I.; Gonzalez M, A.; Castaneda J, G.; Rivera M, H.; Sandoval G, I. [Instituto Nacional de Investigaciones Nucleares, A.P. 18-1027, 11801 Mexico D.F. (Mexico)

2001-07-01

In June 2000, the Reactor Department assigned to the Scientific Research Direction of the National Institute of Nuclear Research requested to the Non-destructive Assays Laboratory (LEND), assigned to the Materials Science Management, the inspection and measurement of thickness of the aluminium coating (liner) of the TRIGA Mark III reactor vat with non-destructive assay techniques, due to that the aluminium coating is exposed mainly to undergo slimming on its back side due to corrosion phenomena. Activity that was able to be carried out from april until august 2001. It is worth pointing out that this type of inspection with these techniques was realized by first time. The non-destructive assays (NDA) are techniques which use indirect physical methods for inspecting the sanitation of components in process or in service, for detect lack of continuity or defects which affect their quality or usefulness. The application of those do not alter the physical, chemical, mechanical or dimensional properties of the part subject of inspection. The results of the application of the ultrasound inspection techniques, industrial radiography and penetrating liquids are presented. (Author)

Non-destructive grading of peaches by near-infrared spectrometry

Science.gov (United States)

Carlomagno, G.; Capozzo, L.; Attolico, G.; Distante, A.

2004-12-01

This paper describes an experimental study on non-destructive methods for sorting peaches according to their degree of ripeness. The method is based on near-infrared (NIR) transmittance spectrometry in the region between 730 and 900 nm. It estimates the ripeness in terms of internal sugar content and firmness. A station for acquiring the NIR signal has been designed and realized, carefully choosing between several options for each component. Four different stations have been realized and compared during the experimental phase. The signals acquired by the station have been pre-processed using a noise-reducing method based on a packets-wavelet transform. In addition, an outlier detection technique has been applied for identifying irregular behaviors inside each of the considered classes. Finally, a minimum distance classifier estimates the grade of each experimental data. The results obtained in classification show that this early version of the station enables the correct discrimination of peaches with a percentage of 82.5%.

Comparative testing of radiographic testing, ultrasonic testing and phased array advanced ultrasonic testing non destructive testing techniques in accordance with the AWS D1.5 bridge welding code.

Science.gov (United States)

2014-02-01

A comprehensive body of non-destructive testing data was collected from steel bridge welds under real-world conditions in a fabricators shop. Three different non-destructive testing (NDT) techniques were used on each weld inspection, these being R...

Incoherent scattering of gamma photons for non-destructive tomographic inspection of pipeline

International Nuclear Information System (INIS)

Sharma, Amandeep; Sandhu, B.S.; Singh, Bhajan

2010-01-01

A scanner system, operating in a non-destructive and non-invasive way, is presented for pipeline to determine its location in land soil, wall thickness, type of liquid flowing and crack/blockage position. The present experiment simulates a real case where pipe corrosion (wall thinning) under insulation can be known from the study of incoherent scattering of 662 keV gamma photons. The incoherent scattered intensity, obtained by unfolding (deconvolution) the experimental pulse-height distribution of NaI(Tl) scintillation detector with the help of inverse response matrix, provides the desired information. The method is quite sensitive for small change (∼1 mm) in the thickness of pipe wall, locating a defect of 1 mm width under insulation and a small change (∼0.1 gm cm -3 ) in the density of liquid flowing through pipe.

Questions of qualification exam for non-destructive testing and materials science - the first level

International Nuclear Information System (INIS)

Shaaban, H.I.; Addarwish, J.M.A.

2013-01-01

The book contains seven chapters: Questions of qualification for magnetic particles testing method - Questions of qualification for liquids penetrant testing method - Questions of qualification for the visual inspection testing method - Questions of qualification for the ultrasonic testing method - Questions of qualification for the eddy current testing method - Questions of rehabilitation for industrial radiographic testing method - Qualification questions about materials science and manufacturing defects of castings and welding and comparison between non-destructive testing methods.

Non-Destructive Evaluation of Kissing Bonds using Local Defect Resonance (LDR) Spectroscopy: A Simulation Study

Science.gov (United States)

Delrue, S.; Tabatabaeipour, M.; Hettler, J.; Van Den Abeele, K.

With the growing demand from industry to optimize and further develop existing Non-Destructive Testing & Evaluation (NDT&E) techniques or new methods to detect and characterize incipient damage with high sensitivity and increased quality, ample efforts have been devoted to better understand the typical behavior of kissing bonds, such as delaminations and cracks. Recently, it has been shown experimentally that the nonlinear ultrasonic response of kissing bonds could be enhanced by using Local Defect Resonance (LDR) spectroscopy. LDR spectroscopy is an efficient NDT technique that takes advantage of the characteristic fre- quencies of the defect (defect resonances) in order to provide maximum acoustic wave-defect interaction. In fact, for nonlinear methodologies, the ultrasonic excitation of the sample should occur at either multiples or integer ratios of the characteristic defect resonance frequencies, in order to obtain the highest signal-to-noise response in the nonlinear LDR spectroscopy. In this paper, the potential of using LDR spectroscopy for the detection, localization and characterization of kissing bonds is illustrated using a 3D simulation code for elastic wave propagation in materials containing closed but dynamically active cracks or delaminations. Using the model, we are able to define an appropriate method, based on the Scaling Subtraction Method (SSM), to determine the local defect resonance frequencies of a delamination in a composite plate and to illustrate an increase in defect nonlinearity due to LDR. The simulation results will help us to obtain a better understanding of the concept of LDR and to assist in the further design and testing of LDR spectroscopy for the detection, localization and characterization of kissing bonds.

A versatile passive and active non-destructive device for spent fuel assemblies monitoring

International Nuclear Information System (INIS)

Berne, R.; Bignan, G.; Andrieu, G.; Dethan, B.

1993-01-01

The monitoring of spent fuel assemblies in reactor pools or in reprocessing plants with NDA methods is interesting (non-destructivity, non-intrusivity) for process control, safety-criticality and/or nuclear material management. In this context, the authors present the results of the development and design of a prototype device (physical methods used, qualification...) called PYTHON. The aim of PYTHON is to check the declared characteristic values of an irradiated assembly before taking it into a transport cask for safety criticality control. The PYTHON device consists of a detector head in two sections and a 252 Cf source if active neutron counting is to be used. Each section of the detection head consists of two detectors: one fission chamber and one ionization chamber

Destruction mechanism of the internal structure in Lithium-ion batteries used in aviation industry

International Nuclear Information System (INIS)

Swornowski, Paweł J.

2017-01-01

In the article, the reasons for destruction of the internal structure in Lithium-ion batteries used in aviation industry have been explained. They manifest themselves in the battery's overheating, and in extreme cases they result in explosion. The report presents the results of experiments, which consisted in subjecting the tested Lithium-ion battery to vibration over a specified period of time and observing the changes of temperature inside it with the use of a thermal infrared camera. Another focal point of the study was the influence of vibrations on voltage change in relation to variable current load, and the influence of ambient temperature change on the Lithium-ion battery's voltage change. It has also been demonstrated that vibrations can damage the control electronics of the Lithium-ion battery. Moreover, the mechanism by which potentially dangerous thermal hot spots are formed in a Lithium-ion battery has been presented, as well as an uncertainty analysis of all measurement results. - Highlights: • The causes of internal destruction of Lithium-ion batteries are external vibrations. • The influence of vibrations on the change of a Lithium-ion battery's most parameters. • The mechanism leading to the explosion of a Lithium-ion battery was demonstrated. • The conclusions ensuring safe exploitation of a Lithium-ion battery were presented.

S.S. Annunziata Church (L'Aquila, Italy) unveiled by non- and micro-destructive testing techniques

Science.gov (United States)

Sfarra, Stefano; Cheilakou, Eleni; Theodorakeas, Panagiotis; Paoletti, Domenica; Koui, Maria

2017-03-01

The present research work explores the potential of an integrated inspection methodology, combining Non-destructive testing and micro-destructive analytical techniques, for both the structural assessment of the S.S. Annunziata Church located in Roio Colle (L'Aquila, Italy) and the characterization of its wall paintings' pigments. The study started by applying passive thermal imaging for the structural monitoring of the church before and after the application of a consolidation treatment, while active thermal imaging was further used for assessing this consolidation procedure. After the earthquake of 2009, which seriously damaged the city of L'Aquila and its surroundings, part of the internal plaster fell off revealing the presence of an ancient mural painting that was subsequently investigated by means of a combined analytical approach involving portable VIS-NIR fiber optics diffuse reflectance spectroscopy (FORS) and laboratory methods, such as environmental scanning electron microscopy (ESEM) coupled with energy dispersive X-ray analysis (EDX), and attenuated total reflectance-fourier transform infrared spectroscopy (ATR-FTIR). The results obtained from the thermographic analysis provided information concerning the two different constrictive phases of the Church, enabled the assessment of the consolidation treatment, and contributed to the detection of localized problems mainly related to the rising damp phenomenon and to biological attack. In addition, the results obtained from the combined analytical approach allowed the identification of the wall painting pigments (red and yellow ochre, green earth, and smalt) and provided information on the binding media and the painting technique possibly applied by the artist. From the results of the present study, it is possible to conclude that the joint use of the above stated methods into an integrated methodology can produce the complete set of useful information required for the planning of the Church's restoration

Destruction of Refractory Carbon in Protoplanetary Disks

Energy Technology Data Exchange (ETDEWEB)

Anderson, Dana E.; Blake, Geoffrey A. [Division of Geological and Planetary Sciences, California Institute of Technology, 1200 E. California Blvd., Pasadena, CA 91125 (United States); Bergin, Edwin A. [Department of Astronomy, University of Michigan, 1085 S. University, Ann Arbor, MI 48109-1107 (United States); Ciesla, Fred J. [Department of Geophysical Sciences, The University of Chicago, 5734 South Ellis Ave., Chicago, IL 60637 (United States); Visser, Ruud [European Southern Observatory, Karl-Schwarzschild-Str. 2, D-85748, Garching (Germany); Lee, Jeong-Eun [School of Space Research, Kyung Hee University, 1732, Deogyeong-daero, Giheung-gu, Yongin-si, Gyeonggi-do 17104 (Korea, Republic of)

2017-08-10

The Earth and other rocky bodies in the inner solar system contain significantly less carbon than the primordial materials that seeded their formation. These carbon-poor objects include the parent bodies of primitive meteorites, suggesting that at least one process responsible for solid-phase carbon depletion was active prior to the early stages of planet formation. Potential mechanisms include the erosion of carbonaceous materials by photons or atomic oxygen in the surface layers of the protoplanetary disk. Under photochemically generated favorable conditions, these reactions can deplete the near-surface abundance of carbon grains and polycyclic aromatic hydrocarbons by several orders of magnitude on short timescales relative to the lifetime of the disk out to radii of ∼20–100+ au from the central star depending on the form of refractory carbon present. Due to the reliance of destruction mechanisms on a high influx of photons, the extent of refractory carbon depletion is quite sensitive to the disk’s internal radiation field. Dust transport within the disk is required to affect the composition of the midplane. In our current model of a passive, constant- α disk, where α = 0.01, carbon grains can be turbulently lofted into the destructive surface layers and depleted out to radii of ∼3–10 au for 0.1–1 μ m grains. Smaller grains can be cleared out of the planet-forming region completely. Destruction may be more effective in an actively accreting disk or when considering individual grain trajectories in non-idealized disks.

Operator performance in non-destructive testing: A study of operator performance in a performance test

Energy Technology Data Exchange (ETDEWEB)

Enkvist, J.; Edland, A.; Svenson, Ola [Stockholm Univ. (Sweden). Dept. of Psychology

2000-05-15

In the process industries there is a need of inspecting the integrity of critical components without disrupting the process. Such in-service inspections are typically performed with non-destructive testing (NDT). In NDT the task of the operator is to (based on diagnostic information) decide if the component can remain in service or not. The present study looks at the performance in NDT. The aim is to improve performance, in the long run, by exploring the operators' decision strategies and other underlying factors and to this way find out what makes some operators more successful than others. Sixteen operators performed manual ultrasonic inspections of four test pieces with the aim to detect (implanted) cracks. In addition to these performance demonstration tests (PDT), the operators performed independent ability tests and filled out questionnaires. The results show that operators who trust their gut feeling more than the procedure (when the two come to different results) and that at the same time have a positive attitude towards the procedure have a higher PDT performance. These results indicate the need for operators to be motivated and confident when performing NDT. It was also found that the operators who performed better rated more decision criteria higher in the detection phase than the operators who performed worse. For characterizing it was the other way around. Also, the operators who performed better used more time, both detecting and characterizing, than the operators who performed worse.

Operator performance in non-destructive testing: A study of operator performance in a performance test

International Nuclear Information System (INIS)

Enkvist, J.; Edland, A.; Svenson, Ola

2000-05-01

In the process industries there is a need of inspecting the integrity of critical components without disrupting the process. Such in-service inspections are typically performed with non-destructive testing (NDT). In NDT the task of the operator is to (based on diagnostic information) decide if the component can remain in service or not. The present study looks at the performance in NDT. The aim is to improve performance, in the long run, by exploring the operators' decision strategies and other underlying factors and to this way find out what makes some operators more successful than others. Sixteen operators performed manual ultrasonic inspections of four test pieces with the aim to detect (implanted) cracks. In addition to these performance demonstration tests (PDT), the operators performed independent ability tests and filled out questionnaires. The results show that operators who trust their gut feeling more than the procedure (when the two come to different results) and that at the same time have a positive attitude towards the procedure have a higher PDT performance. These results indicate the need for operators to be motivated and confident when performing NDT. It was also found that the operators who performed better rated more decision criteria higher in the detection phase than the operators who performed worse. For characterizing it was the other way around. Also, the operators who performed better used more time, both detecting and characterizing, than the operators who performed worse

Review of intermediate and final product characterization on coated particles preparation

International Nuclear Information System (INIS)

Sukarsono; Kristanti Nurwidyaningrum

2015-01-01

Review of the intermediate and final product characterization on preparation of coated particles was done. Product characterization included a tool to measure the character of raw materials, intermediate product and the final product of the process, which affects the success of getting the high temperature reactor fuel are eligible. Equipment's for the characterization of such materials were pH meter, viscometer, microbalance, turbidity meter, tab density measurement, true density measurement and auto pycnometer. Being for the measurement of particles there are two types destructive testing and non destructive. Destructive testing was done by polished the particles then cross sectional imaging of particle observed using an optical microscope. In this way contains errors due to polishing treatment that could not be right on the equator section so it needs correction. Destructive testing also create waste that must be processed from the remnants of the polishing process. By using non-destructive testing, waste was not formed but the imaging results are often unclear due to lack of contrast. Development of non-destructive test equipment has been made using radiographic method and automated microscopy. The overall activity is still much needed additional tools for measurement and for processing, so that the results obtained will not rejected as the specification of nuclear fuel. Similarly, in the case of a sampling test method and limits to a product accepted or rejected, it should be determined based on statistical methods. (author)

Challenges of characterization of radioactive waste with High composition variability and their consequences measurement methodology

International Nuclear Information System (INIS)

Lexa, D.

2014-01-01

Radioactive waste characterization is a key step in every nuclear decommissioning project. It normally relies on a combination of facility operational history with results of destructive and non-destructive analysis. A particularly challenging situation arises when historical waste from a nuclear research facility is to be characterized, meaning little or no radiological information is available and the composition of the waste is highly variable. The nuclide vector concept is of limited utility, resulting in increased requirements placed on both the extent and performance of destructive and non-destructive analysis. Specific challenges are illustrated on an example of the decommissioning project underway at the Joint Research Center of the European Commission in Ispra. (author)

Physical basis of destruction of concrete and other building materials

Science.gov (United States)

Suleymanova, L. A.; Pogorelova, I. A.; Kirilenko, S. V.; Suleymanov, K. A.

2018-03-01

In the article the scientifically-grounded views of authors on the physical essence of destruction process of concrete and other materials are stated; it is shown that the mechanism of destruction of materials is similar in its essence during the mechanical, thermal, physical-chemical and combined influences, and that in its basis Newton's third law lays. In all cases destruction consists in decompaction of structures, loosening of the internal bonds in materials, in the further integrity damage and their division into separate loosely-bound (full destruction) and unbound with each other (incomplete destruction) elements, which depends on the kind of external influence and perfection of materials structure.

The Non-Destructive Test of Steel Corrosion in Reinforced Concrete Bridges Using a Micro-Magnetic Sensor

Directory of Open Access Journals (Sweden)

Hong Zhang

2016-09-01

Full Text Available This paper presents a non-destructive test method for steel corrosion in reinforced concrete bridges by using a 3-dimensional digital micro-magnetic sensor to detect and analyze the self-magnetic field leakage from corroded reinforced concrete. The setup of the magnetic scanning device and the measurement mode of the micro-magnetic sensor are introduced. The numerical analysis model is also built based on the linear magnetic charge theory. Compared to the self-magnetic field leakage data obtained from magnetic sensor-based measurement and numerical calculation, it is shown that the curves of tangential magnetic field at different lift-off height all intersect near the edge of the steel corrosion zone. The result indicates that the intersection of magnetic field curves can be used to detect and evaluate the range of the inner steel corrosion in engineering structures. The findings of this work propose a new and effective non-destructive test method for steel corrosion, and therefore enlarge the application of the micro-magnetic sensor.

Design of an electron-accelerator-driven compact neutron source for non-destructive assay

Science.gov (United States)

Murata, A.; Ikeda, S.; Hayashizaki, N.

2017-09-01

The threat of nuclear and radiological terrorism remains one of the greatest challenges to international security, and the threat is constantly evolving. In order to prevent nuclear terrorism, it is important to avoid unlawful import of nuclear materials, such as uranium and plutonium. Development of technologies for non-destructive measurement, detection and recognition of nuclear materials is essential for control at national borders. At Tokyo Institute of Technology, a compact neutron source system driven by an electron-accelerator has been designed for non-destructive assay (NDA). This system is composed of a combination of an S-band (2.856 GHz) RF-gun, a tungsten target to produce photons by bremsstrahlung, a beryllium target, which is suitable for use in generating neutrons because of the low threshold energy of photonuclear reactions, and a moderator to thermalize the fast neutrons. The advantage of this system can accelerate a short pulse beam with a pulse width less than 1 μs which is difficult to produce by neutron generators. The amounts of photons and neutron produced by electron beams were simulated using the Monte Carlo simulation code PHITS 2.82. When the RF-gun is operated with an average electron beam current of 0.1 mA, it is expected that the neutron intensities are 1.19 × 109 n/s and 9.94 × 109 n/s for incident electron beam energies of 5 MeV and 10 MeV, respectively.

Laser photothermal non-destructive metrology of cracks in un-sintered powder metallurgy manufactured automotive transmission sprockets

International Nuclear Information System (INIS)

Tolev, J; Mandelis, A

2010-01-01

A non-contact and non-intrusive method of revealing crack presence in un-sintered (green) automotive transmission parts (sprockets), manufactured by means of a powder metallurgy technology based on analysis of photo-thermal radiometric (PTR) signals and their statistical analysis was developed. The inspection methodology relies on the interaction of a modulated laser generated thermal wave with the potential crack and the resulting change in amplitude and phase of the detected signal [1-5]. The crack existence at points in high stress regions of a group of green (unsintered) sprockets was evaluated through frequency scans. The results were validated by independent destructive cross-sectioning of the sprockets following sintering and polishing. Examination of the sectioned sprockets under a microscope at the locations where signal changes was used for correlation with the PTR signals. Statistical analysis confirmed the capabilities of the method to detect the presence of hairline cracks (∼5 - 10 μm size) with excellent sensitivity (91%) and good accuracy (78%) and specificity (61%). This measurement technique and the associated statistical analysis can be used as a simple and reliable on-line inspection methodology of industrial powder metallurgy manufactured steel products for non-destructive quality and feedback control of the parts forming process.

Early identification and characterization of waste

International Nuclear Information System (INIS)

Vandevelde, L.; Carchon, R.

1998-01-01

At the Belgian Nuclear Research Centre SCK-CEN, destructive and non-destructive analytical techniques are developed in the framework of activities related to the characterization of radioactive waste. This program aims to measure the inventory of critical key-nuclides in different waste streams and to identify and develop correlations between those isotopes. Main activities and results in 1997 are described

Manufacturing of reliable actively cooled fusion components - a challenge for non-destructive inspections

International Nuclear Information System (INIS)

Reheis, N.; Zabernig, A.; Ploechl, L.

1994-01-01

Actively cooled in-vessel components like divertors or limiters require high quality and reliability to ensure safe operation during long term use. Such components are subjected to very severe thermal and mechanical cyclic loads and high power densities. Key requirements for materials in question are e.g. high melting point and thermal conductivity and low atomic mass number. Since no single material can simultaneously meet all of these requirements the selection of materials to be combined in composite components as well as of manufacturing and non-destructive inspection (NDI) methods is a particularly challenging task. Armour materials like graphite intended to face the plasma and help to maintain its desired properties, are bonded to metallic substrates like copper, molybdenum or stainless steel providing cooling and mechanical support. Several techniques such as brazing and active metal casting have been developed and successfully applied for joining materials with different thermophysical properties, pursuing the objective of sufficient heat dissipation from the hot, plasma facing surface to the coolant. NDI methods are an integral part of the manufacturing schedule of these components, starting in the design phase and ending in the final inspection. They apply all kinds of divertor types (monobloc and flat-tile concept). Particular focus is put on the feasibility of detecting small flaws and defects in complex interfaces and on the limits of these techniques. Special test pieces with defined defects acting as standards were inspected. Accompanying metallographic investigations were carried out to compare actual defects with results recorded during NDI

Study of Lamb Waves for Non-Destructive Testing Behind Screens

Science.gov (United States)

Kauffmann, P.; Ploix, M.-A.; Chaix, J.-F.; Gueudré, C.; Corneloup, G.; Baqué, F. AF(; )

2018-01-01

The inspection and control of sodium-cooled fast reactors (SFR) is a major issue for the nuclear industry. Ultrasonic solutions are under study because of the opacity of liquid sodium. In this paper, the use of leaky Lamb waves is considered for non-destructive testing (NDT) on parallel and immersed structures assimilated as plates. The first phase of our approach involved studying the propagation properties of leaky Lamb waves. Equations that model the propagation of Lamb waves in an immersed plate were solved numerically. The phase velocity can be experimentally measured using a two dimensional Fourier transform. The group velocity can be experimentally measured using a short-time Fourier transform technique. Attenuation of leaky Lamb waves is mostly due to the re-emission of energy into the surrounding fluid, and it can be measured by these two techniques.

Determination of nuclear fuel burnup by non-destructive gamma spectroscopy

International Nuclear Information System (INIS)

Soares, A.J.

1979-01-01

The determination of nuclear fuel burnup by the non-destructive gamma spectroscopy method is studied. A MTR (Materials Testing Reactor) -type fuel element is used in the measurement. The fuel element was removed from the reactor core in 1958 and, because of the long decay time, show only one peak in is gamma spectrum at 661.6 Kev. Corresponding to 137 Cs. Measurements are made at 330 points of the element using a Nal detector and the final result revealed that the quantity of 235 U consumed was 3.3 +- 0,8 milligram in the entire element. The effect of the migration of 137 Cs in the element is neglected in view of the fact that it occurs only when the temperature is above 1000 0 C, which is not the case in IEAR-1. (Author)

The use of fracture mechanics methodologies for NDT results evaluation and comparison

International Nuclear Information System (INIS)

Reale, S.

1995-01-01

In the general frame of analysing the interactions amongst the information from non destructive evaluation (NDE) and the methodologies to assess the integrity of a defective structure (such as fracture mechanics), the aim of the paper is to analyse and compare, in terms of indices related to safety margins, NDE results from round robin testing trials to acheive assessments of capabilities and limitations.A structural integrity/fracture mechanics approach for evaluating and comparing results from non destructive techniques is presented. Safety factors can be associated to flaws detected and characterized by inspections (estimated flaws) and to flaws actually present (reference flaws). The mismatch between safety factors associated to estimated flaws and safety factors associated to reference flaws can be used to assess capabilities and limitations of procedures and techniques in use for inspections.As an example, to show how the above procedure is applied and its potential as a method of data evaluation and comparison, the NDE results produced by the PISC (project for the inspection of steel components) activity have been considered. (orig.)

Development of a non-destructive method to identify different grades of stainless steel

International Nuclear Information System (INIS)

Meor Yusoff Meor Sulaiman

2004-01-01

One of the non-destructive methods used for the identification and verification of metals is by the energy-dispersive x-ray fluorescence (EDXRF) technique. EDXRF analysis provides several important advantages such as simultaneous determination of the elements present, enable to analyze a very wide concentration range, fast analysis with no tedious sample preparation. The paper shows how this technique is developed and applied in the identification and verification of different grades of stainless steels. Comparison of the results obtained from this analysis with certified reference standards show very small differences between them. (Author)

Non-Destructive Current Sensing for Energy Efficiency Monitoring in Buildings with Environmental Certification.

Science.gov (United States)

Mota, Lia Toledo Moreira; Mota, Alexandre de Assis; Coiado, Lorenzo Campos

2015-07-10

Nowadays, buildings environmental certifications encourage the implementation of initiatives aiming to increase energy efficiency in buildings. In these certification systems, increased energy efficiency arising from such initiatives must be demonstrated. Thus, a challenge to be faced is how to check the increase in energy efficiency related to each of the employed initiatives without a considerable building retrofit. In this context, this work presents a non-destructive method for electric current sensing to assess implemented initiatives to increase energy efficiency in buildings with environmental certification. This method proposes the use of a sensor that can be installed directly in the low voltage electrical circuit conductors that are powering the initiative under evaluation, without the need for reforms that result in significant costs, repair, and maintenance. The proposed sensor consists of three elements: an air-core transformer current sensor, an amplifying/filtering stage, and a microprocessor. A prototype of the proposed sensor was developed and tests were performed to validate this sensor. Based on laboratory tests, it was possible to characterize the proposed current sensor with respect to the number of turns and cross-sectional area of the primary and secondary coils. Furthermore, using the Least Squares Method, it was possible to determine the efficiency of the air core transformer current sensor (the best efficiency found, considering different test conditions, was 2%), which leads to a linear output response.

Non-Destructive Current Sensing for Energy Efficiency Monitoring in Buildings with Environmental Certification

Science.gov (United States)

Mota, Lia Toledo Moreira; Mota, Alexandre de Assis; Coiado, Lorenzo Campos

2015-01-01

Nowadays, buildings environmental certifications encourage the implementation of initiatives aiming to increase energy efficiency in buildings. In these certification systems, increased energy efficiency arising from such initiatives must be demonstrated. Thus, a challenge to be faced is how to check the increase in energy efficiency related to each of the employed initiatives without a considerable building retrofit. In this context, this work presents a non-destructive method for electric current sensing to assess implemented initiatives to increase energy efficiency in buildings with environmental certification. This method proposes the use of a sensor that can be installed directly in the low voltage electrical circuit conductors that are powering the initiative under evaluation, without the need for reforms that result in significant costs, repair, and maintenance. The proposed sensor consists of three elements: an air-core transformer current sensor, an amplifying/filtering stage, and a microprocessor. A prototype of the proposed sensor was developed and tests were performed to validate this sensor. Based on laboratory tests, it was possible to characterize the proposed current sensor with respect to the number of turns and cross-sectional area of the primary and secondary coils. Furthermore, using the Least Squares Method, it was possible to determine the efficiency of the air core transformer current sensor (the best efficiency found, considering different test conditions, was 2%), which leads to a linear output response. PMID:26184208

Non-Destructive Current Sensing for Energy Efficiency Monitoring in Buildings with Environmental Certification

Directory of Open Access Journals (Sweden)

Lia Toledo Moreira Mota

2015-07-01

Full Text Available Nowadays, buildings environmental certifications encourage the implementation of initiatives aiming to increase energy efficiency in buildings. In these certification systems, increased energy efficiency arising from such initiatives must be demonstrated. Thus, a challenge to be faced is how to check the increase in energy efficiency related to each of the employed initiatives without a considerable building retrofit. In this context, this work presents a non-destructive method for electric current sensing to assess implemented initiatives to increase energy efficiency in buildings with environmental certification. This method proposes the use of a sensor that can be installed directly in the low voltage electrical circuit conductors that are powering the initiative under evaluation, without the need for reforms that result in significant costs, repair, and maintenance. The proposed sensor consists of three elements: an air-core transformer current sensor, an amplifying/filtering stage, and a microprocessor. A prototype of the proposed sensor was developed and tests were performed to validate this sensor. Based on laboratory tests, it was possible to characterize the proposed current sensor with respect to the number of turns and cross-sectional area of the primary and secondary coils. Furthermore, using the Least Squares Method, it was possible to determine the efficiency of the air core transformer current sensor (the best efficiency found, considering different test conditions, was 2%, which leads to a linear output response.

Application of lock-in thermography non destructive technique to CFC armoured plasma facing components

International Nuclear Information System (INIS)

Escourbiac, F.; Constans, S.; Courtois, X.; Durocher, A.

2007-01-01

A non destructive testing technique - so called modulated photothermal thermography or lock-in thermography - has been set-up for plasma facing components examination. Reliable measurements of phase contrast were obtained on 8 mm carbon fiber composite (CFC) armoured W7-X divertor component with calibrated flaws. A 3D finite element analysis allowed the correlation of the measured phase contrast and showed that a 4 mm strip flaw can be detected at the CFC/copper interface

A Non-destructive and Continuous Measurement of Gelatinization of Rice in Rice Cooking Process

OpenAIRE

Hagura, Yoshio; Suzuki, Kanichi

2002-01-01

A non-destructive and continuous method to measure gelatinization of rice samples in a rice-water system during rice cooking process was examined. An aluminum pot and a lid of a rice cooker were used as two electrode plates, and changes in dielectric properties (capacitance : C, and dielectric dissipation factor : tan δ) of the samples in the rice cooking process were measured by a capacitance meter. Differential scanning calorimetry (DSC) was used to measure gelatinization enthalpy and to de...

Application of golay complementary coded excitation schemes for non-destructive testing of sandwich structures

Science.gov (United States)

Arora, Vanita; Mulaveesala, Ravibabu

2017-06-01

In recent years, InfraRed Thermography (IRT) has become a widely accepted non-destructive testing technique to evaluate the structural integrity of composite sandwich structures due to its full-field, remote, fast and in-service inspection capabilities. This paper presents a novel infrared thermographic approach named as Golay complementary coded thermal wave imaging is presented to detect disbonds in a sandwich structure having face sheets from Glass/Carbon Fibre Reinforced (GFR/CFR) laminates and core of the wooden block.

Automatic non-destructive system for quality assurance of welded elements in the aircraft industry

Science.gov (United States)

Chady, Tomasz; Waszczuk, Paweł; Szydłowski, Michał; Szwagiel, Mariusz

2018-04-01

Flaws that might be a result of the welding process have to be detected, in order to assure high quality thus reliability of elements exploited in aircraft industry. Currently the inspection stage is conducted manually by a qualified workforce. There are no commercially available systems that could support or replace humans in the flaw detection process. In this paper authors present a novel non-destructive system developed for quality assurance purposes of welded elements utilized in the aircraft industry.

Elastase-coupled beads as a tool for characterizing localized alveolar tissue destruction associated with the onset of emphysema

Science.gov (United States)

Craig, J. M.; Scott, A. L.

2013-01-01

Intratracheal elastase challenge of laboratory animals has long been established as a model for observing the physiological and morphological changes that result from alveolar destruction, the hallmark of emphysema. However, instillation of elastase suspended in buffer results in widespread inflammation and variable emphysematous lesions, which has made the identification of specific cellular and molecular events associated with the onset of emphysema difficult to define. Here we establish a bead-based elastase delivery system that induces localized tissue destruction, a key event in the initiation of emphysema. Elastase was coupled to bisacrylamide beads, which were shown to retain enzymatic activity prior to intratracheal administration in mice. C57BL/6 mice were given a single dose of 40,000 beads, which became distributed throughout the small airways and parenchyma of the lung. Elastase-coupled beads resulted in a quantifiable loss of alveolar tissue immediately surrounding the beads, an effect that was not observed with beads that lacked protein altogether or with beads containing elastase inactivated by an irreversible inhibitor. Furthermore, beads bound with active elastase elicited local recruitment of mononuclear cells, including macrophages, and polymorphonuclear neutrophils to the site of bead deposition, a feature consistent with the cellular infiltration observed following conventional solubilized elastase challenges. This work identifies a novel bead-based enzyme delivery system that also extends the elastase model of emphysema to permit the characterization of mechanisms that drive alveolar surface area loss following elastin degradation in focal emphysematous lesions. PMID:23558388

Neutrophil-Derived MMP-8 Drives AMPK-Dependent Matrix Destruction in Human Pulmonary Tuberculosis

Science.gov (United States)

Ong, Catherine W. M.; Elkington, Paul T.; Brilha, Sara; Ugarte-Gil, Cesar; Tome-Esteban, Maite T.; Tezera, Liku B.; Pabisiak, Przemyslaw J.; Moores, Rachel C.; Sathyamoorthy, Tarangini; Patel, Vimal; Gilman, Robert H.; Porter, Joanna C.; Friedland, Jon S.

2015-01-01

Pulmonary cavities, the hallmark of tuberculosis (TB), are characterized by high mycobacterial load and perpetuate the spread of M. tuberculosis. The mechanism of matrix destruction resulting in cavitation is not well defined. Neutrophils are emerging as key mediators of TB immunopathology and their influx are associated with poor outcomes. We investigated neutrophil-dependent mechanisms involved in TB-associated matrix destruction using a cellular model, a cohort of 108 patients, and in separate patient lung biopsies. Neutrophil-derived NF-kB-dependent matrix metalloproteinase-8 (MMP-8) secretion was up-regulated in TB and caused matrix destruction both in vitro and in respiratory samples of TB patients. Collagen destruction induced by TB infection was abolished by doxycycline, a licensed MMP inhibitor. Neutrophil extracellular traps (NETs) contain MMP-8 and are increased in samples from TB patients. Neutrophils lined the circumference of human pulmonary TB cavities and sputum MMP-8 concentrations reflected TB radiological and clinical disease severity. AMPK, a central regulator of catabolism, drove neutrophil MMP-8 secretion and neutrophils from AMPK-deficient patients secrete lower MMP-8 concentrations. AMPK-expressing neutrophils are present in human TB lung biopsies with phospho-AMPK detected in nuclei. These data demonstrate that neutrophil-derived MMP-8 has a key role in the immunopathology of TB and is a potential target for host-directed therapy in this infectious disease. PMID:25996154

Neutrophil-Derived MMP-8 Drives AMPK-Dependent Matrix Destruction in Human Pulmonary Tuberculosis.

Science.gov (United States)

Ong, Catherine W M; Elkington, Paul T; Brilha, Sara; Ugarte-Gil, Cesar; Tome-Esteban, Maite T; Tezera, Liku B; Pabisiak, Przemyslaw J; Moores, Rachel C; Sathyamoorthy, Tarangini; Patel, Vimal; Gilman, Robert H; Porter, Joanna C; Friedland, Jon S

2015-05-01

Pulmonary cavities, the hallmark of tuberculosis (TB), are characterized by high mycobacterial load and perpetuate the spread of M. tuberculosis. The mechanism of matrix destruction resulting in cavitation is not well defined. Neutrophils are emerging as key mediators of TB immunopathology and their influx are associated with poor outcomes. We investigated neutrophil-dependent mechanisms involved in TB-associated matrix destruction using a cellular model, a cohort of 108 patients, and in separate patient lung biopsies. Neutrophil-derived NF-kB-dependent matrix metalloproteinase-8 (MMP-8) secretion was up-regulated in TB and caused matrix destruction both in vitro and in respiratory samples of TB patients. Collagen destruction induced by TB infection was abolished by doxycycline, a licensed MMP inhibitor. Neutrophil extracellular traps (NETs) contain MMP-8 and are increased in samples from TB patients. Neutrophils lined the circumference of human pulmonary TB cavities and sputum MMP-8 concentrations reflected TB radiological and clinical disease severity. AMPK, a central regulator of catabolism, drove neutrophil MMP-8 secretion and neutrophils from AMPK-deficient patients secrete lower MMP-8 concentrations. AMPK-expressing neutrophils are present in human TB lung biopsies with phospho-AMPK detected in nuclei. These data demonstrate that neutrophil-derived MMP-8 has a key role in the immunopathology of TB and is a potential target for host-directed therapy in this infectious disease.

Non-destructive Testing of Wood Defects Based on Discriminant Analysis Method

Directory of Open Access Journals (Sweden)

Wenshu LIN

2015-09-01

Full Text Available The defects of wood samples were tested by the technique of stress wave and ultrasonic technology, and the testing results were comparatively analyzed by using the Fisher discriminant analysis in the statistic software of SPSS. The differences of defect detection sensitivity and accuracy for stress wave and ultrasonic under different wood properties and defects were concluded. Therefore, in practical applications, according to different situations the corresponding wood non- destructive testing method should be used, or the two detection methods are applied at the same time in order to compensate for its shortcomings with each other to improve the ability to distinguish the timber defects. The results can provide a reference for further improvement of the reliability of timber defects detection.

Analysis of unbalanced sensor in eddy current method of non destructive testing

International Nuclear Information System (INIS)

Chegodaev, V.V.

2001-01-01

Different types of sensors are used in eddy current method of non-destructive testing. The choosing of sensor type depends on control object. Different types of sensors can have the same schemes of cut-in in device for formation of information signal. The most common scheme of sensor cut-in is presented. The calculation of output voltage when the sensor is on a segment of the control object, which has not defect is made. The conditions of balancing are adduced and it was shown that the balancing of sensor is very difficult. The methods of compensation or account of voltage of an imbalance are indicated. (author)

Yucca Mountain project container fabrication, closure and non-destructive evaluation development activities

International Nuclear Information System (INIS)

Russell, E.W.; Nelson, T.A.

1989-06-01

In this presentation, container fabrication, closure, and non-destructive evaluation (NDE) process development activities are described. All of these activities are interrelated, and will contribute to the metal barrier selection activity. The plan is to use a corrosion-resistant material in the form of a cylinder with a wall thickness of ∼1cm (2cm for pure copper.) The materials under consideration include the three austenitic alloys: stainless steel-304L, stainless steel-316L and alloy 825, as well as the three copper alloys: CDA 102, CDA 613, and CDA 715. This document reviews the recommended procedures and processes for fabricating, closing and evaluating each of the candidate materials

Photothermal Analysis Applied To Non-Destructive Evaluation Of Paint On Polymer Substrates

Science.gov (United States)

Vergne, D.; Busse, G.

1988-10-01

The decoration and protection quality of coatings on polymers is of considerable interest for industrial applications. However, at present there is no non-destructive (NDE) method to monitor the quality of these coatings during the manufacturing process or while they are in use. As an approach for such a method we use photothermal analysis where the propagation and reflection of optically generated thermal waves is investigated. We found that one can monitor the drying process, the effect of surface temperature treatment, and coating thickness (accuracy + 2 μm in 50 μm thickness). The information obtained with this remote NDE method is adequate for most industrial applications, eg car manufacturing.

Pipe robots for internal inspection, non-destructive testing and machining of pipelines

International Nuclear Information System (INIS)

Reiss, Alexander

2016-01-01

Inspector Systems is a specialist in manufacturing of tethered self-propelled pipe robots for internal inspection, non-destructive testing and machining of pipeline systems. Our industrial sectors, which originates from 30 year experience in the nuclear industry, are Gas and Oil (On-/Offshore, Refineries), Chemical, Petrochemical, Water etc. The pipe robots are able to get inserted through poor access points (e.g. valves) and to pass in bi-directional travelling vertical sections and numerous bends with small arc radius. The paper describes the system concept and performance of the pipe robot technology. A modular construction allows to equip the robots with different operational elements for the respective application.

Interpretation of non destructive combined nuclear measurements for the characterization of radioactive wastes and waste packages

International Nuclear Information System (INIS)

Raoux, Anne-Cecile

2000-01-01

Nuclear industry produces radioactive waste and is faced with the problem of their management, especially for those which have a long radioactive decay time. In view to be able to define the best storage solution, alpha bearing solid waste are identified by different specific parameters (alpha, beta activities,... ). Then, the storage and cost optimizations are essential stakes. The quantification of these parameters can be obtained by the implementation of non destructive nuclear measurement methods generally associated with information from the manufacturing process of the waste. The works presented in this report are dedicated to two complementary aspects of the nuclear waste management issue. On the one hand, an experimental study concerning the possibilities of the prompt and delayed neutron counting with only one measurement result from neutron interrogation is presented. On the other hand, an interpretation method allowing the determination of the waste package specific parameters and their uncertainties has been developed. It is based on random trials which allow to describe the parameters as statistical distributions (Monte Carlo method). It was resulting in the realization of a software called RECITAL (information combination and solving process by random trials). This software was applied to the isotopic quantification of "2"3"5U and "2"3"9Pu from prompt and delayed signals of neutron interrogation. It was also used to demonstrate the complementarity of photofission interrogation with neutron interrogation in view to correct "2"3"8U interference on the delayed fission signal, especially when "2"3"8U contribution is similar to "2"3"5U and "2"3"9Pu ones. (author) [fr

The correlation between microstructure and mechanical properties of high-pressure die-cast AM50 alloy

International Nuclear Information System (INIS)

Song Jie; Xiong Shoumei; Li Mei; Allison, John

2009-01-01

Scanning acoustic microscopy was used to characterize the micro-voids distribution for specimens in non-destructive mode. In addition, the in-situ scanning electron microscopy observation was performed during tensile deformation of high-pressure die-cast (HPDC) of AM50 alloy to obtain the mechanism of fracture induced by micro-voids. The effects of micro-voids on the mechanical properties were discussed. The results obtained from the examination suggest that fracture tends to occur at bigger micro-voids or in the cluster micro-voids area.

A Spatially Offset Raman Spectroscopy Method for Non-Destructive Detection of Gelatin-Encapsulated Powders

Directory of Open Access Journals (Sweden)

Kuanglin Chao

2017-03-01

Full Text Available Non-destructive subsurface detection of encapsulated, coated, or seal-packaged foods and pharmaceuticals can help prevent distribution and consumption of counterfeit or hazardous products. This study used a Spatially Offset Raman Spectroscopy (SORS method to detect and identify urea, ibuprofen, and acetaminophen powders contained within one or more (up to eight layers of gelatin capsules to demonstrate subsurface chemical detection and identification. A 785-nm point-scan Raman spectroscopy system was used to acquire spatially offset Raman spectra for an offset range of 0 to 10 mm from the surfaces of 24 encapsulated samples, using a step size of 0.1 mm to obtain 101 spectral measurements per sample. As the offset distance was increased, the spectral contribution from the subsurface powder gradually outweighed that of the surface capsule layers, allowing for detection of the encapsulated powders. Containing mixed contributions from the powder and capsule, the SORS spectra for each sample were resolved into pure component spectra using self-modeling mixture analysis (SMA and the corresponding components were identified using spectral information divergence values. As demonstrated here for detecting chemicals contained inside thick capsule layers, this SORS measurement technique coupled with SMA has the potential to be a reliable non-destructive method for subsurface inspection and authentication of foods, health supplements, and pharmaceutical products that are prepared or packaged with semi-transparent materials.

Non-destructive investigations of Swiss museums objects with neutron and x-ray imaging methods

International Nuclear Information System (INIS)

Lehmann, E.H.; Deschler, E.; Pernet, L.; Vontobel, P.

2004-01-01

Many objects of archaeological relevance found in Switzerland are from the Celtic and Roman era. Because of their uniqueness in most cases it is demanded to perform any investigation with such samples non-destructively. Depending on the structure and size of the objects a transmission experiment performed either with X-ray or neutron can alight inner structures, composition, defects or the principles of the manufacturing procedures. Furthermore, the treatment by conservators and restaurateurs becomes visible in many cases. This report describes some examples of such investigations. In the case of neutron investigations, beside the transmission imaging as a radiograph the three-dimensional structure was observed with a tomography technique. For X-ray radiography, the images were obtained in the same digital format because the similar experimental method (imaging plates) was applied. It becomes evident in the described examples that the combination and complementary use of both methods (neutrons and X-ray) brings insights in different aspects of the samples properties and treatment. This approach to study museums objects stored and exhibit in Switzerland can be extrapolated to other countries where these techniques are also simultaneously available in order to investigate other objects of relevance. The European network COST-G8 entitled 'Non-destructive analysis and testing of museum objects' can help to support initiatives in this direction. (author)

Miniaturized Time Domain Terahertz Non Destructive Evaluation for In-Orbit Inspection of Inflatable Habitats and Thermal Protection Systems, Phase II

Data.gov (United States)

National Aeronautics and Space Administration — Picometrix's time-domain terahertz (TD-THz) non-destructive evaluation (NDE) technology could be used to inspect space flight structures such as inflatable space...

Miniaturized Time Domain Terahertz Non Destructive Evaluation for In-Orbit Inspection of Inflatable Habitats and Thermal Protection Systems, Phase I

Data.gov (United States)

National Aeronautics and Space Administration — Picometrix's time-domain terahertz (TD-THz) non-destructive evaluation (NDE) technology could be used to inspect space flight structures such as inflatable space...

Development of a non-destructive micro-analytical method for stable carbon isotope analysis of transmission electron microscope (TEM) samples

Energy Technology Data Exchange (ETDEWEB)

Hode, Tomas [Department of Geology, Portland State University, Portland, P.O. Box 751, OR 97201 (United States)], E-mail: hode@pdx.edu; Kristiansson, Per; Elfman, Mikael [Division of Nuclear Physics, Department of Physics, Lund Institute of Technology, Lund University, P.O. Box 118, SE-221 00 Lund (Sweden); Hugo, Richard C.; Cady, Sherry L. [Department of Geology, Portland State University, Portland, P.O. Box 751, OR 97201 (United States)

2009-10-01

The biogenicity of ancient morphological microfossil-like objects can be established by linking morphological (e.g. cell remnants and extracellular polymeric matrix) and chemical (e.g. isotopes, biomarkers and biominerals) evidence indicative of microorganisms or microbial activity. We have developed a non-destructive micro-analytical ion beam system capable of measuring with high spatial resolution the stable carbon isotope ratios of thin samples used for transmission electron microscopy. The technique is based on elastic scattering of alpha particles with an energy of 2.751 MeV. At this energy the {sup 13}C cross section is enhanced relative to the pure Rutherford cross section for {sup 13}C, whereas the {sup 12}C cross section is reduced relative to its pure Rutherford cross section. Here we report the initial results of this experimental approach used to characterize ultramicrotomed sections of sulfur-embedded graphite and microbial cells.

Assay of Uranium Isotopic Ratios 234U/238U, 235U/238U in Bottom Sediment Samples Using Destructive and Non Destructive Techniques (Nasser Lake)

International Nuclear Information System (INIS)

Agha, A.R.; El-Mongy, S.A.; Kandel, A.E.

2011-01-01

Nasser Lake is the greatest man-made lake in the World. It is considered as the main source of water where the Nile water is impounded behind the Aswan high dam.. Uranium has three naturally occurring isotopes 234 U, 235 U and 238 U with isotopic abundance 0.00548, 0.7200 and 99.2745 atom percent. Dissolved uranium in the lake is primary due to weathering process. Monitoring of the isotopic ratios of uranium is used as a good indicator to trace and evaluate the origin and activities associated with any variation of uranium in the lake environment. The main objective of the present study is to clarify any potential variation of natural uranium 234 U/ 238 U, 235 U/ 238 U ratios in sediment samples of Nasser Lake by using destructive alpha and non destructive gamma- techniques. The results show that the uranium isotopic activity ratios are very close to the natural values. This study can also be used for radiological protection and safety evaluation purposes.

Contributions to ultrasounds applications in non-destructive tests on materials used in nuclear technologies

International Nuclear Information System (INIS)

Stanica, V.

1979-01-01

The problems expounded in the paper, besides servjng the practical purpose generated by the need to perform quality tests on fuel element compounds by means of the ultrasounds method, are also interesting to ultrasounds non-destructive tests applied in all industry branches as they assert the necessity of passing from manual to automation tests carried out by installations which should record the signals caused by failures, both to increase the productivjty and especially to transform it into an objective, effective test. (author)

Design and manufacturing of nuclear non destructive measurement systems and coupled metrology in order to quantify the radionuclides contaminating the wastes and the processes of the nuclear industry

International Nuclear Information System (INIS)

Saurel, N.

2013-01-01

The non-destructive nuclear measurement has to provide responses for the main challenges of the nuclear industry such as nuclear facility safety, health, environmental impact, performance, reliability and cost control. The goal of the non-destructive nuclear measurement is to characterize, without any deterioration, an object contaminated by one or more radionuclides. The passive or active nuclear measurement are utilized for quantifying the radionuclides in the effluents, the liquid and solid wastes and the nuclear material hold-up. It is also deployed for the process control. In this case, it is a standard production control but, the most of the time, it controls the validity of the safety domain of the production unit. The results of these measurements are used to establish the radiological inventory or the nuclear material balance. The radiological inventory is needed for the nuclear wastes outlets while the nuclear material balance is needed to follow through with the criticality units. The most important objective is to give the quantitative and/or qualitative value and its uncertainty are confident of the radionuclides contaminating the object. This contaminated object might be of different geometrical shapes, sizes or physico-chemical compositions. In order to be efficient, the non-destructive nuclear measurement has to include the apparatus, the measurement actions, the settings and the use of the coupled methodologies. I relate, in this memoir, my main research and development works that I drove or in which I took part for achieving these goals. These works are about the metrology of nuclear radiations and are used in three main types of measurement which are the gamma spectrometry, the alpha spectrometry and the passive or active neutron counting. (author) [fr

Complementary Methods for the Characterization of Corrosion Products on a Plant-Exposed Superheater Tube

DEFF Research Database (Denmark)

Okoro, Sunday Chukwudi; Nießen, Frank; Villa, Matteo

2017-01-01

In this work, complex corrosion products on a superheater tube exposed to biomass firing were characterized by the complementary use of energy-dispersive synchrotron diffraction, electron microscopy, and energy-dispersive X-ray spectroscopy. Non-destructive synchrotron diffraction in transmission......-rich austenite phase to selective removal of Fe and Cr from the alloy, via a KCl-induced corrosion mechanism. Compositional variations were related to diffraction results and revealed a qualitative influence of the spinel cation concentration on the observed diffraction lines.......In this work, complex corrosion products on a superheater tube exposed to biomass firing were characterized by the complementary use of energy-dispersive synchrotron diffraction, electron microscopy, and energy-dispersive X-ray spectroscopy. Non-destructive synchrotron diffraction in transmission...... geometry measuring with a small gauge volume from the sample surface through the corrosion product allowed depth-resolved phase identification and revealed the presence of (Fe,Cr)2O3 and FeCr2O4. This was supplemented by microstructural and elemental analysis correlating the additional presence of a Ni...

Non-destructive state detection for quantum logic spectroscopy of molecular ions.

Science.gov (United States)

Wolf, Fabian; Wan, Yong; Heip, Jan C; Gebert, Florian; Shi, Chunyan; Schmidt, Piet O

2016-02-25

Precision laser spectroscopy of cold and trapped molecular ions is a powerful tool in fundamental physics--used, for example, in determining fundamental constants, testing for their possible variation in the laboratory, and searching for a possible electric dipole moment of the electron. However, the absence of cycling transitions in molecules poses a challenge for direct laser cooling of the ions, and for controlling and detecting their quantum states. Previously used state-detection techniques based on photodissociation or chemical reactions are destructive and therefore inefficient, restricting the achievable resolution in laser spectroscopy. Here, we experimentally demonstrate non-destructive detection of the quantum state of a single trapped molecular ion through its strong Coulomb coupling to a well controlled, co-trapped atomic ion. An algorithm based on a state-dependent optical dipole force changes the internal state of the atom according to the internal state of the molecule. We show that individual quantum states in the molecular ion can be distinguished by the strength of their coupling to the optical dipole force. We also observe quantum jumps (induced by black-body radiation) between rotational states of a single molecular ion. Using the detuning dependence of the state-detection signal, we implement a variant of quantum logic spectroscopy of a molecular resonance. Our state-detection technique is relevant to a wide range of molecular ions, and could be applied to state-controlled quantum chemistry and to spectroscopic investigations of molecules that serve as probes for interstellar clouds.

THz QCL-based active imaging dedicated to non-destructive testing of composite materials used in aeronautics

Science.gov (United States)

Destic, F.; Petitjean, Y.; Massenot, S.; Mollier, J.-C.; Barbieri, S.

2010-08-01

This paper presents a CW raster-scanning THz imaging setup, used to perform Non-Destructive Testing of KevlarTMand carbon fibre samples. The setup uses a 2.5 THz Quantum Cascade Laser as a source. Delamination defect in a Kevlar sample was detected showing a sensitivity to laser polarization orientation. Detection of a break in a carbon/epoxy sample was also performed.

THz QCL-based active imaging dedicated to non-destructive testing of composite materials used in aeronautics

OpenAIRE

Destic, Fabien; Petitjean, Yoann; Massenot, Sébastien; Mollier, Jean-Claude; Barbieri, Stefano

2010-01-01

This paper presents a CW raster-scanning THz imaging setup, used to perform Non-Destructive Testing of KevlarTMand carbon fibre samples. The setup uses a 2.5 THz Quantum Cascade Laser as a source. Delamination defect in a Kevlar sample was detected showing a sensitivity to laser polarization orientation. Detection of a break in a carbon/epoxy sample was also performed.

Non-destructive, high-content analysis of wheat grain traits using X-ray micro computed tomography

Directory of Open Access Journals (Sweden)

Nathan Hughes

2017-11-01

Full Text Available Abstract Background Wheat is one of the most widely grown crop in temperate climates for food and animal feed. In order to meet the demands of the predicted population increase in an ever-changing climate, wheat production needs to dramatically increase. Spike and grain traits are critical determinants of final yield and grain uniformity a commercially desired trait, but their analysis is laborious and often requires destructive harvest. One of the current challenges is to develop an accurate, non-destructive method for spike and grain trait analysis capable of handling large populations. Results In this study we describe the development of a robust method for the accurate extraction and measurement of spike and grain morphometric parameters from images acquired by X-ray micro-computed tomography (μCT. The image analysis pipeline developed automatically identifies plant material of interest in μCT images, performs image analysis, and extracts morphometric data. As a proof of principle, this integrated methodology was used to analyse the spikes from a population of wheat plants subjected to high temperatures under two different water regimes. Temperature has a negative effect on spike height and grain number with the middle of the spike being the most affected region. The data also confirmed that increased grain volume was correlated with the decrease in grain number under mild stress. Conclusions Being able to quickly measure plant phenotypes in a non-destructive manner is crucial to advance our understanding of gene function and the effects of the environment. We report on the development of an image analysis pipeline capable of accurately and reliably extracting spike and grain traits from crops without the loss of positional information. This methodology was applied to the analysis of wheat spikes can be readily applied to other economically important crop species.

Non-Destructive Methods for Determining Burn-Up in Nuclear Fuel; Methodes Non Destructives d'Evaluation du Taux de Combustion dans le Combustible Nucleaire; Metody opredeleniya vygoraniya v yadernom toplive bez razrusheniya obraztsa; Metodos No Destructivos para Determinai el Grado de Combustion de los Elementos Combustibles Nucleares

Energy Technology Data Exchange (ETDEWEB)

McGonnagle, W. J. [Illinois Institute of Technology, Chicago, IL (United States)

1966-02-15

Non-destructive methods for quantitative measurement of burn-up in nuclear reactor fuel elements are useful and desirable. The ideal method for fuel assay would be one that requires no special information about the neutron spectra, radiation history, or cooling time. The irradiated fuel element contains a record of the fuel burn-up. This record is in the form of radioactive and stable isotopes resulting from the fission process. Unfortunately, in the non-destructive as well as the destructive fuel assay methods, the neutron spectrum, irradiation history, and cooling period influence this record. Likewise, the lack of precise nuclear data, such as values of nuclear cross-sections, affects any calculations that can be made. Another difficulty in the non-destructive assay is the presence of high radiation fields which contribute to the ''noise'' background of the measurements. The development of useful and realistic standards is difficult. The non-destructive burn-up methods do serve a useful purpose especially when an approximate value of burn-up is required quickly and economically even though in the present state of the art they lack the desired precision and accuracy. Several non-destructive methods for determining burn-up have been used, are being evaluated, or have been proposed. Various types of spectrometers including the bent crystal, magnetic Compton, Compton coincidence, and scintillation have been used to analyse the gamma radiation from the radioactive material formed during the fission process. Other non-destructive methods include foil activation, neutron transmission, activation analysis, measurement of capture gamma rays, and the measurement of prompt and delayed neutrons. The basic principles of each of the above instruments and methods, their sensitivities and their limitations will be reviewed. Non-destructive methods using stable isotopes produced during the fission process are proposed. In the use of stable isotopes, detailed irradiation history

Complex Archaeological Prospection Using Combination of Non-destructive Techniques

Science.gov (United States)

Faltýnová, M.; Pavelka, K.; Nový, P.; Šedina, J.

2015-08-01

This article describes the use of a combination of non-destructive techniques for the complex documentation of a fabulous historical site called Devil's Furrow, an unusual linear formation lying in the landscape of central Bohemia. In spite of many efforts towards interpretation of the formation, its original form and purpose have not yet been explained in a satisfactory manner. The study focuses on the northern part of the furrow which appears to be a dissimilar element within the scope of the whole Devil's Furrow. This article presents detailed description of relics of the formation based on historical map searches and modern investigation methods including airborne laser scanning, aerial photogrammetry (based on airplane and RPAS) and ground-penetrating radar. Airborne laser scanning data and aerial orthoimages acquired by the Czech Office for Surveying, Mapping and Cadastre were used. Other measurements were conducted by our laboratory. Data acquired by various methods provide sufficient information to determine the probable original shape of the formation and proves explicitly the anthropological origin of the northern part of the formation (around village Lipany).

Complex Archaeological Prospection Using Combination of Non-destructive Techniques

Directory of Open Access Journals (Sweden)

M. Faltýnová

2015-08-01

Full Text Available This article describes the use of a combination of non-destructive techniques for the complex documentation of a fabulous historical site called Devil’s Furrow, an unusual linear formation lying in the landscape of central Bohemia. In spite of many efforts towards interpretation of the formation, its original form and purpose have not yet been explained in a satisfactory manner. The study focuses on the northern part of the furrow which appears to be a dissimilar element within the scope of the whole Devil’s Furrow. This article presents detailed description of relics of the formation based on historical map searches and modern investigation methods including airborne laser scanning, aerial photogrammetry (based on airplane and RPAS and ground-penetrating radar. Airborne laser scanning data and aerial orthoimages acquired by the Czech Office for Surveying, Mapping and Cadastre were used. Other measurements were conducted by our laboratory. Data acquired by various methods provide sufficient information to determine the probable original shape of the formation and proves explicitly the anthropological origin of the northern part of the formation (around village Lipany.

Thermal inactivation of Escherichia coli 0157:H7 (ECOH) and non-0157 Shiga toxin-producing E.coli (STEC)in mechanically tenderized veal

Science.gov (United States)

We quantified thermal destruction of Shiga toxin-producing Escherichia coli O157:H7 (ECOH) and Shiga toxin-producing non-O157 E. coli (STEC) cells within mechanically tenderized veal cutlets following cooking on an electric skillet. For each of five trials, flattened veal cutlets (ca. 71.6 g; ca. 1/...

Investigation and development of a non-destructive system to evaluate critical properties of asphalt pavements during the compaction process.

Science.gov (United States)

2013-10-01

The purpose of this report is to present findings from a two-stage investigation to develop a non-destructive system to : evaluate critical properties and characteristics of asphalt pavements during the compaction process. The first stage aligned : c...

Non destructive assay of nuclear LEU spent fuels for burnup credit application

International Nuclear Information System (INIS)

Lebrun, A.; Bignan, G.

2001-01-01

Criticality safety analysis devoted to spent fuel storage and transportation has to be conservative in order to be sure no accident will ever happen. In the spent fuel storage field, the assumption of freshness has been used to achieve the conservative aspect of criticality safety procedures. Nevertheless, after being irradiated in a reactor core, the fuel elements have obviously lost part of their original reactivity. The concept of taking into account this reactivity loss in criticality safety analysis is known as Burnup credit. To be used, Burnup credit involves obtaining evidence of the reactivity loss with a Burnup measurement. Many non destructive assays (NDA) based on neutron as well as on gamma ray emissions are devoted to spent fuel characterization. Heavy nuclei that compose the fuels are modified during irradiation and cooling. Some of them emit neutrons spontaneously and the link to Burnup is a power link. As a result, burn-up determination with passive neutron measurement is extremely accurate. Some gamma emitters also have interesting properties in order to characterize spent fuels but the convenience of the gamma spectrometric methods is very dependent on characteristics of spent fuel. In addition, contrary to the neutron emission, the gamma signal is mostly representative of the peripheral rods of the fuels. Two devices based on neutron methods but combining different NDA methods which have been studied in the past are described in detail: 1. The PYTHON device is a combination of a passive neutron measurement, a collimated total gamma measurement, and an online depletion code. This device, which has been used in several Nuclear Power Plants in western Europe, gives the average Burnup within a 5% uncertainty and also the extremity Burnup, 2. The NAJA device is an automatic device that involves three nuclear methods and an online depletion code. It is designed to cover the whole fuel assembly panel (Active Neutron Interrogation, Passive Neutron

Non-destructive observation of damage in mortar and concrete during mechanical loading for the evaluation of moisture transfer profiles

DEFF Research Database (Denmark)

Rouchier, Simon; Janssen, Hans; Rode, Carsten

2012-01-01

Coupled heat and mass transfer modelling in building materials now plays an important part in the design of energy-efficient buildings. However, concrete and other construction materials subjected to mechanical loading and atmospheric excitation inevitably develop fractures patterns during...... characterization with a hygric modelling can provide an appropriate prediction of the water infiltration in fractured porous building materials....

Opto-thermal transient emission radiometry for rapid, non-destructive and non-contact determination of hydration and hydration depth profile in the skin of a grape

NARCIS (Netherlands)

Guo, X.; Bicanic, D.D.; Keijser, K.; Imhof, R.

2003-01-01

.The concept of optothermal transient emission radiometry at a wavelength of 2.94 µm was applied to non-destructively determine the level of hydration and the profile of hydration in the skin of intact fresh grapes taken from top and bottom sections of the same bunch.

Development of a non-destructive method to identify different grades of stainless steel

International Nuclear Information System (INIS)

Meor Yusoff Meor Sulaiman

2003-01-01

One of the non-destructive methods used for the identification and verification of metals is by the energy-dispersive X-ray fluorescence (EDXRF) technique. EDXRF analysis provides several important advantages such as simultaneous determination of the elements present, enable to analyse a very wide concentration range, fast analysis with no sample preparation. The paper shows how this technique is developed and applied in the identification and verification of different grades of stainless steels. Comparison of the results for certified reference standards obtained from this analysis and that of its certified value shows very small differences between them. (Author)

Ultrasonic transverse velocity calibration of standard blocks for use in non-destructive testing

International Nuclear Information System (INIS)

Silva, C E R; Braz, D S; Maggi, L E; Felix, R P B Costa

2015-01-01

Standard blocks are employed in the verification of the equipment used in Ultrasound Non-Destructive Testing. To assure the metrology reliability of all the measurement process, it is necessary to calibrate or certify these Standard blocks. In this work, the transverse wave velocity and main dimensions were assessed according to the specifications ISO Standards. For transverse wave velocity measurement, a 5 MHz transverse wave transducer, a waveform generator, an oscilloscope and a computer with a program developed in LabVIEW TM were used. Concerning the transverse wave velocity calibration, only two Standard blocks of the 4 tested is in accordance with the standard

Effects of time pressure and noise on non-destructive testing

Energy Technology Data Exchange (ETDEWEB)

Enkvist, J.; Svenson, Ola [Stockholm Univ. (Sweden). Dept. of Psychology; Edland, A. [Swedish Nuclear Power Inspectorate, Stockholm (Sweden)

2001-12-01

Manual ultrasonic testing (UT) is the most frequently used non-destructive testing (NDT) method for in-service inspection of components important to safety and/or plant availability. Earlier, great variations have been found in operator performance, often attributed to operator fatigue. However, no conclusive findings have been reported. According to the Yerkes-Dodson law there is an optimal arousal level where performance is highest, for simple tasks this optimum is higher than for more complex tasks. In the present study twenty operators performed manual ultrasonic inspections of six test pieces with manufactured flaws. The operators performed the inspections under stress (high arousal - time pressure and noise) and non-stress conditions; one condition the first day and the other the second and last day. It was hypothesised that the stress condition led to a level of arousal so high that it would affect the results negatively. The results confirmed that the operators were affected by the stress condition. However, contrary to the hypotheses it was found that the manipulation increased operator performance. Operators with the stress condition the first day performed better than the other operators did (under both the stress and the non-stress condition). This was interpreted as the 'stress first' (group 1) operators had established efficient performance patterns the first day - affecting also the second day. Operators beginning with stress condition also tended to be more motivated. It was concluded that operator performance is affected by arousal. The operators with non-stress first (group 2) worked hard with the complex task but their arousal level was assumed to be above the optimal, resulting in a low hit rate.

Effects of time pressure and noise on non-destructive testing

Energy Technology Data Exchange (ETDEWEB)

Enkvist, J; Svenson, Ola [Stockholm Univ. (Sweden). Dept. of Psychology; Edland, A [Swedish Nuclear Power Inspectorate, Stockholm (Sweden)

2001-12-01

Manual ultrasonic testing (UT) is the most frequently used non-destructive testing (NDT) method for in-service inspection of components important to safety and/or plant availability. Earlier, great variations have been found in operator performance, often attributed to operator fatigue. However, no conclusive findings have been reported. According to the Yerkes-Dodson law there is an optimal arousal level where performance is highest, for simple tasks this optimum is higher than for more complex tasks. In the present study twenty operators performed manual ultrasonic inspections of six test pieces with manufactured flaws. The operators performed the inspections under stress (high arousal - time pressure and noise) and non-stress conditions; one condition the first day and the other the second and last day. It was hypothesised that the stress condition led to a level of arousal so high that it would affect the results negatively. The results confirmed that the operators were affected by the stress condition. However, contrary to the hypotheses it was found that the manipulation increased operator performance. Operators with the stress condition the first day performed better than the other operators did (under both the stress and the non-stress condition). This was interpreted as the 'stress first' (group 1) operators had established efficient performance patterns the first day - affecting also the second day. Operators beginning with stress condition also tended to be more motivated. It was concluded that operator performance is affected by arousal. The operators with non-stress first (group 2) worked hard with the complex task but their arousal level was assumed to be above the optimal, resulting in a low hit rate.

Effects of time pressure and noise on non-destructive testing

International Nuclear Information System (INIS)

Enkvist, J.; Svenson, Ola

2001-12-01

Manual ultrasonic testing (UT) is the most frequently used non-destructive testing (NDT) method for in-service inspection of components important to safety and/or plant availability. Earlier, great variations have been found in operator performance, often attributed to operator fatigue. However, no conclusive findings have been reported. According to the Yerkes-Dodson law there is an optimal arousal level where performance is highest, for simple tasks this optimum is higher than for more complex tasks. In the present study twenty operators performed manual ultrasonic inspections of six test pieces with manufactured flaws. The operators performed the inspections under stress (high arousal - time pressure and noise) and non-stress conditions; one condition the first day and the other the second and last day. It was hypothesised that the stress condition led to a level of arousal so high that it would affect the results negatively. The results confirmed that the operators were affected by the stress condition. However, contrary to the hypotheses it was found that the manipulation increased operator performance. Operators with the stress condition the first day performed better than the other operators did (under both the stress and the non-stress condition). This was interpreted as the 'stress first' (group 1) operators had established efficient performance patterns the first day - affecting also the second day. Operators beginning with stress condition also tended to be more motivated. It was concluded that operator performance is affected by arousal. The operators with non-stress first (group 2) worked hard with the complex task but their arousal level was assumed to be above the optimal, resulting in a low hit rate

Post-harvest Quality Evaluation of Grapes using Non-destructive Electronic Nose

Directory of Open Access Journals (Sweden)

RAJIN S. M. Ataul Karim

2015-10-01

Full Text Available Over the past decades, electronic nose has opened a variety of possibilities and is becoming one of the most important non-destructive odour inspection technologies in the food industry. The objective of this study is to determine the quality degradation of the fruit by monitoring the change in the volatile compound while kept in storage using a lab manufactured electronic nose. Here, grapes are chosen as the fruit sample for experiment. Principal component analysis (PCA is used to determine the ability of the electronic nose to distinguish the different quality of the fruit stored over an interval of time. The result shows that using PCA analysis, the electronic nose is able to identify a clear distinction between the aromas of grapes stored for different time intervals.