WorldWideScience

Sample records for multi-element analysis

  1. Multi-element analysis for environmental characterization and its future trends

    International Nuclear Information System (INIS)

    Sansoni, B.

    1987-04-01

    Before starting to characterize the environment by its elemental composition, it may be useful to ask about the objective of these efforts. This includes questions about the scope of environmental protection, the definition of the environment and the limitations of its characterization by elemental composition alone. In the second part of this lecture, examples are given of the elemental composition of well analysed samples from the atmosphere, hydrosphere, lithosphere and biosphere. The third part introduces the principle of multi-element analysis and the fourth part gives examples. Finally, future aspects of modern chemical analysis are outlined with respect to the multi-element principle. (orig.)

  2. Multi-element analysis of unidentified fallen objects from Tatale in ...

    African Journals Online (AJOL)

    A multi-element analysis has been carried out on two fallen objects, # 01 and # 02, using instrumental neutron activation analysis technique. A total of 17 elements were identified in object # 01 while 21 elements were found in object # 02. The two major elements in object # 01 were Fe and Mg, which together constitute ...

  3. Validation of multi-element isotope dilution ICPMS for the analysis of basalts

    Energy Technology Data Exchange (ETDEWEB)

    Willbold, M.; Jochum, K.P.; Raczek, I.; Amini, M.A.; Stoll, B.; Hofmann, A.W. [Max-Planck-Institut fuer Chemie, Mainz (Germany)

    2003-09-01

    In this study we have validated a newly developed multi-element isotope dilution (ID) ICPMS method for the simultaneous analysis of up to 12 trace elements in geological samples. By evaluating the analytical uncertainty of individual components using certified reference materials we have quantified the overall analytical uncertainty of the multi-element ID ICPMS method at 1-2%. Individual components include sampling/weighing, purity of reagents, purity of spike solutions, calibration of spikes, determination of isotopic ratios, instrumental sources of error, correction of mass discrimination effect, values of constants, and operator bias. We have used the ID-determined trace elements for internal standardization to improve indirectly the analysis of 14 other (mainly mono-isotopic trace elements) by external calibration. The overall analytical uncertainty for those data is about 2-3%. In addition, we have analyzed USGS and MPI-DING geological reference materials (BHVO-1, BHVO-2, KL2-G, ML3B-G) to quantify the overall bias of the measurement procedure. Trace element analysis of geological reference materials yielded results that agree mostly within about 2-3% relative to the reference values. Since these results match the conclusions obtained by the investigation of the overall analytical uncertainty, we take this as a measure for the validity of multi-element ID ICPMS. (orig.)

  4. Simultaneous multi-element analysis of some edible pulses using neutron activation analysis

    International Nuclear Information System (INIS)

    El-Sweify, F.H.; Metwally, E.; Abdel-Khalik, H.

    2007-01-01

    This paper comprises the application of instrumental neutron activation analysis (INAA) for multi-element determination in some edible pulse samples. These edible pulses are usually daily used in the Egyptian kitchen. These were: anise, cumin, coriander, caraway, black cumin, white kidney bean, lupine, lentil, chickpea, broad bean, peanut, almond, and fenugreek. The pulses have been analyzed as dehulled pulses, in the case of legume and oil pulses with simultaneous analysis of their respective skins. The determined elements were: Ce, Co, Cr, Cs, Eu, Fe, Hf, Rb, Sb, Sc, Sr, Th and Zn. The element content in the dehulled pulses and their respective skins has been compared. Some elements were major or minor elements where others were trace elements. Standard reference materials were used to assure quality control, accuracy and precision of the technique. (author)

  5. Multi-element trace analysis of solid samples using one-photon two-step RIMS

    International Nuclear Information System (INIS)

    Telle, H. H.; Abraham, C. J.; Jones, O. R.; Krustev, T.

    1998-01-01

    In this study we have investigated the feasibility of multi-element analysis using a simple 1+1 photo-excitation/photo-ionization scheme. Although such schemes are usually far from ideal for optimum resonance ionization, they are the approach of choice if one wishes to maintain a simple, easy-to-operate laser set-up which is potentially suitable for routine analysis. In addition, we only made use of the second-harmonic tuning range of a single dye. While this limits the range of elements which are accessible in the 1+1 RIS scheme it further adds to the simplicity and allows for automation of sequential multi-element analysis

  6. Infinite elements for soil-structure interaction analysis in multi-layered halfspaces

    International Nuclear Information System (INIS)

    Yun, Chung Bang; Kim, Jae Min; Yang, Shin Chu

    1994-01-01

    This paper presents the theoretical aspects of a computer code (KIESSI) for soil-structure interaction analysis in a multi-layered halfspace using infinite elements. The shape functions of the infinite elements are derived from approximate expressions of the analytical solutions. Three different infinite elements are developed. They are the horizontal, the vertical and the comer infinite elements (HIE, VIE and CIE). Numerical example analyses are presented for demonstrating the effectiveness of the proposed infinite elements

  7. Multi-element analysis of emeralds and associated rocks by k0 neutron activation analysis

    International Nuclear Information System (INIS)

    Acharya, R.N.; Mondal, R.K.; Burte, P.P.; Nair, A.G.C.; Reddy, N.B.Y.; Reddy, L.K.; Reddy, A.V.R.; Manohar, S.B.

    2000-01-01

    Multi-element analysis was carried out in natural emeralds, their associated rocks and one sample of beryl obtained from Rajasthan, India. The concentrations of 21 elements were assayed by Instrumental Neutron Activation Analysis using the k 0 method (k 0 INAA method) and high-resolution gamma ray spectrometry. The data reveal the segregation of some elements from associated (trapped and host) rocks to the mineral beryl forming the gemstones. A reference rock standard of the US Geological Survey (USGS BCR-1) was also analysed as a control of the method

  8. Multi-element neutron activation analysis and solution of classification problems using multidimensional statistics

    International Nuclear Information System (INIS)

    Vaganov, P.A.; Kol'tsov, A.A.; Kulikov, V.D.; Mejer, V.A.

    1983-01-01

    The multi-element instrumental neutron activation analysis of samples of mountain rocks (sandstones, aleurolites and shales of one of gold deposits) is performed. The spectra of irradiated samples are measured by Ge(Li) detector of the volume of 35 mm 3 . The content of 22 chemical elements is determined in each sample. The results of analysis serve as reliable basis for multi-dimensional statistic information processing, they constitute the basis for the generalized characteristics of rocks which brings about the solution of classification problem for rocks of different deposits

  9. Multi-element analysis of emeralds and associated rocks by k{sub 0} neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Acharya, R.N.; Mondal, R.K.; Burte, P.P.; Nair, A.G.C.; Reddy, N.B.Y.; Reddy, L.K.; Reddy, A.V.R.; Manohar, S.B

    2000-12-15

    Multi-element analysis was carried out in natural emeralds, their associated rocks and one sample of beryl obtained from Rajasthan, India. The concentrations of 21 elements were assayed by Instrumental Neutron Activation Analysis using the k{sub 0} method (k{sub 0} INAA method) and high-resolution gamma ray spectrometry. The data reveal the segregation of some elements from associated (trapped and host) rocks to the mineral beryl forming the gemstones. A reference rock standard of the US Geological Survey (USGS BCR-1) was also analysed as a control of the method.

  10. Optimal acid digestion for multi-element analysis of different waste matrices

    DEFF Research Database (Denmark)

    Götze, Ramona; Astrup, Thomas Fruergaard

    of the distinct waste materials and recyclables. The purpose of this study is to evaluate the performance of different standardized microwave assisted acid digestion methods on waste samples and subsequent multi-element analysis. Six acid digestion methods were applied on a Paper & Cardboard and Composite waste...

  11. Provenance Establishment of Stingless Bee Honey Using Multi-element Analysis in Combination with Chemometrics Techniques.

    Science.gov (United States)

    Shadan, Aidil Fahmi; Mahat, Naji A; Wan Ibrahim, Wan Aini; Ariffin, Zaiton; Ismail, Dzulkiflee

    2018-01-01

    As consumption of stingless bee honey has been gaining popularity in many countries including Malaysia, ability to identify accurately its geographical origin proves pertinent for investigating fraudulent activities for consumer protection. Because a chemical signature can be location-specific, multi-element distribution patterns may prove useful for provenancing such product. Using the inductively coupled-plasma optical emission spectrometer as well as principal component analysis (PCA) and linear discriminant analysis (LDA), the distributions of multi-elements in stingless bee honey collected at four different geographical locations (North, West, East, and South) in Johor, Malaysia, were investigated. While cross-validation using PCA demonstrated 87.0% correct classification rate, the same was improved (96.2%) with the use of LDA, indicating that discrimination was possible for the different geographical regions. Therefore, utilization of multi-element analysis coupled with chemometrics techniques for assigning the provenance of stingless bee honeys for forensic applications is supported. © 2017 American Academy of Forensic Sciences.

  12. Multi-element determination in environmental samples by mass spectrometric isotope dilution analysis using thermal ionization. Pt. 2

    International Nuclear Information System (INIS)

    Hilpert, K.; Waidmann, E.

    1988-01-01

    An analytical procedure for the multi-element analysis of the elements Fe, Ni, Cu, Zn, Ga, Rb, Sr, Cd, Ba, Tl, and Pb in pine needles by mass spectrometric isotope dilution analysis using thermal ionization has been reported in Part I of this paper. This procedure is now transferred to the non-vegetable material 'Oyster Tissue' (Standard Reference Material 1566, National Bureau of Standards, USA). By a modification of the analytical procedure, it was possible to determine Cr in this material in addition to the aforementioned elements. No concentrations are certified for the elements Ga, Ba and Tl analyzed in this work. The concentrations of the remaining elements obtained by the multi-element analysis agree well with those certified. (orig.)

  13. Non destructive multi elemental analysis using prompt gamma neutron activation analysis techniques: Preliminary results for concrete sample

    Energy Technology Data Exchange (ETDEWEB)

    Dahing, Lahasen Normanshah [School of Applied Physics, Universiti Kebangsaan Malaysia, 43600 Bangi, Selangor, Malaysia and Malaysian Nuclear Agency (Nuklear Malaysia), Bangi 43000, Kajang (Malaysia); Yahya, Redzuan [School of Applied Physics, Universiti Kebangsaan Malaysia, 43600 Bangi, Selangor (Malaysia); Yahya, Roslan; Hassan, Hearie [Malaysian Nuclear Agency (Nuklear Malaysia), Bangi 43000, Kajang (Malaysia)

    2014-09-03

    In this study, principle of prompt gamma neutron activation analysis has been used as a technique to determine the elements in the sample. The system consists of collimated isotopic neutron source, Cf-252 with HPGe detector and Multichannel Analysis (MCA). Concrete with size of 10×10×10 cm{sup 3} and 15×15×15 cm{sup 3} were analysed as sample. When neutrons enter and interact with elements in the concrete, the neutron capture reaction will occur and produce characteristic prompt gamma ray of the elements. The preliminary result of this study demonstrate the major element in the concrete was determined such as Si, Mg, Ca, Al, Fe and H as well as others element, such as Cl by analysis the gamma ray lines respectively. The results obtained were compared with NAA and XRF techniques as a part of reference and validation. The potential and the capability of neutron induced prompt gamma as tool for multi elemental analysis qualitatively to identify the elements present in the concrete sample discussed.

  14. Precision and Accuracy of k0-NAA Method for Analysis of Multi Elements in Reference Samples

    International Nuclear Information System (INIS)

    Sri-Wardani

    2004-01-01

    Accuracy and precision of k 0 -NAA method could determine in the analysis of multi elements contained in reference samples. The analyzed results of multi elements in SRM 1633b sample were obtained with optimum results in bias of 20% but it is in a good accuracy and precision. The analyzed results of As, Cd and Zn in CCQM-P29 rice flour sample were obtained with very good result in bias of 0.5 - 5.6%. (author)

  15. Micro-scaled high-throughput digestion of plant tissue samples for multi-elemental analysis

    Directory of Open Access Journals (Sweden)

    Husted Søren

    2009-09-01

    Full Text Available Abstract Background Quantitative multi-elemental analysis by inductively coupled plasma (ICP spectrometry depends on a complete digestion of solid samples. However, fast and thorough sample digestion is a challenging analytical task which constitutes a bottleneck in modern multi-elemental analysis. Additional obstacles may be that sample quantities are limited and elemental concentrations low. In such cases, digestion in small volumes with minimum dilution and contamination is required in order to obtain high accuracy data. Results We have developed a micro-scaled microwave digestion procedure and optimized it for accurate elemental profiling of plant materials (1-20 mg dry weight. A commercially available 64-position rotor with 5 ml disposable glass vials, originally designed for microwave-based parallel organic synthesis, was used as a platform for the digestion. The novel micro-scaled method was successfully validated by the use of various certified reference materials (CRM with matrices rich in starch, lipid or protein. When the micro-scaled digestion procedure was applied on single rice grains or small batches of Arabidopsis seeds (1 mg, corresponding to approximately 50 seeds, the obtained elemental profiles closely matched those obtained by conventional analysis using digestion in large volume vessels. Accumulated elemental contents derived from separate analyses of rice grain fractions (aleurone, embryo and endosperm closely matched the total content obtained by analysis of the whole rice grain. Conclusion A high-throughput micro-scaled method has been developed which enables digestion of small quantities of plant samples for subsequent elemental profiling by ICP-spectrometry. The method constitutes a valuable tool for screening of mutants and transformants. In addition, the method facilitates studies of the distribution of essential trace elements between and within plant organs which is relevant for, e.g., breeding programmes aiming at

  16. Evaluation of pressed powders and thin section standards for multi-elemental analysis by conventional and micro-PIXE analysis

    International Nuclear Information System (INIS)

    Homma-Takeda, Shino; Iso, Hiroyuki; Ito, Masaki

    2010-01-01

    For multi-elemental analysis, various standards are used to quantify the elements consists of environmental and biological samples. In this paper two different configuration standards, pressed powders and thin section standards, were assessed for their purpose as standards by conventional and micro-PIXE analysis. Homogeneity of manganese, iron, zinc (Zn), copper and yttrium added to pressed powder standard materials were validated and the relative standard deviation (RSD) of the X-ray intensity of the standards was 2 area and the metal concentration was acceptable. (author)

  17. Multi-Element Composition of Honey as a Suitable Tool for Its Authenticity Analysis

    Directory of Open Access Journals (Sweden)

    Oroian Mircea

    2015-06-01

    Full Text Available The aim of this study was to evaluate the composition of 36 honey samples of 4 different botanical origins (acacia, sun flower, tilia and honeydew from the North East region of Romania. An inductively coupled plasma-mass spectrometry (ICP-MS method was used to determine 27 elements in honey (Ag, Al, As, Ba, Be, Ca, Cd, Co, Cr, Cs, Cu, Fe, Ga, K, Li, Mg, Mn, Na, Ni, Pb, Rb, Se, Sr, Tl, U, V and Zn. We would like to achieve the following goal: to demonstrate that the qualitative and quantitative multi-element composition determination of honey can be used as a suitable tool to classify honey according to its botanical origin. The principal component analysis allowed the reduction of the 27 variables to 2 principal components which explained 74% of the total variance. The dominant elements which were strongly associated with the principal component were K, Mg and Ca. Discriminant models obtained for each kind of botanical honey confirmed that the differentiation of honeys according to their botanical origin was mainly based on multi-element composition. A correct classification of all samples was achieved with the exception of 11.1% of honeydew honeys.

  18. Multi-elemental profile of some Brazilian make-up products by instrumental neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Dalmazio, Ilza; Menezes, Maria Angela de B.C., E-mail: id@cdtn.b, E-mail: menezes@cdtn.b [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil). Servico de Reator e Tecnicas Analiticas. Lab. de Ativacao Neutronica

    2011-07-01

    Recent works have shown that analysis in cosmetics and beauty products from the European and Asian markets indicate the presence of U, Th and rare earths besides other trace elements. Considering these previous findings and health issues, it would be valuable to obtain information on elements in cosmetics available in the Brazilian market. The purpose of this study was to acquire a multi-elemental profile of some Brazilian make-up products of diverse brands. Samples of eye shadow, liquid base, facial concealer, lipstick, and compact face powder were analyzed applying neutron activation analysis, k{sub 0}-standardization method at CDTN/CNEN, using the TRIGA Mark I IPR-R1 research reactor. Concentrations of more than 30 elements in samples are presented and it was found elements included in Brazilian National Health Surveillance Agency prohibitive list, rare earths, Th and U in a minimum of two cosmetic samples. (author)

  19. Multi-elemental profile of some Brazilian make-up products by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Dalmazio, Ilza; Menezes, Maria Angela de B.C.

    2011-01-01

    Recent works have shown that analysis in cosmetics and beauty products from the European and Asian markets indicate the presence of U, Th and rare earths besides other trace elements. Considering these previous findings and health issues, it would be valuable to obtain information on elements in cosmetics available in the Brazilian market. The purpose of this study was to acquire a multi-elemental profile of some Brazilian make-up products of diverse brands. Samples of eye shadow, liquid base, facial concealer, lipstick, and compact face powder were analyzed applying neutron activation analysis, k 0 -standardization method at CDTN/CNEN, using the TRIGA Mark I IPR-R1 research reactor. Concentrations of more than 30 elements in samples are presented and it was found elements included in Brazilian National Health Surveillance Agency prohibitive list, rare earths, Th and U in a minimum of two cosmetic samples. (author)

  20. Multi Elemental Study Using Prompt Gamma Technique

    International Nuclear Information System (INIS)

    Normanshah Dahing; Muhamad Samudi Yasir; Normanshah Dahing; Hanafi Ithnin; Mohd Fitri Abdul Rahman; Hearie Hassan

    2016-01-01

    In this study, principle of prompt gamma neutron activation analysis has been used as a technique to determine the elements in the sample. The system consists of collimated isotopic neutron source, Cf-252 with HPGe detector and Multichannel Analysis (MCA). Concrete with size of 10x10x10 cm 3 and 15x15x15 cm 3 were analysed as sample. When neutrons enter and interact with elements in the concrete, the neutron capture reaction will occur and produce characteristic prompt gamma ray of the elements. The preliminary result of this study demonstrate the major element in the concrete was determined such as Si, Mg, Ca, Al, Fe and H as well as others element, such as Cl by analysis the gamma ray lines respectively. The results obtained were compared with computer simulation, NAA and XRF as a part of reference and validation. The potential and the capability of neutron induced prompt gamma as tool for multi elemental analysis qualitatively to identify the elements present in the concrete sample discussed. (author)

  1. [Rapid multi-elemental analysis on four precious Tibetan medicines based on LIBS technique].

    Science.gov (United States)

    Liu, Xiao-na; Shi, Xin-yuan; Jia, Shuai-yun; Zhao, Na; Wu, Zhi-sheng; Qiao, Yan-jiang

    2015-06-01

    The laser-induced breakdown spectroscopy (LIBS) was applied to perform a qualitative elementary analysis on four precious Tibetan medicines, i. e. Renqing Mangjue, Renqing Changjue, 25-herb coral pills and 25-herb pearl pills. The specific spectra of the four Tibetan medicines were established. In the experiment, Nd: YAG and 1 064 nm-baseband pulse laser were adopted to collect the spectra. A laser beam focused on the surface of the samples to generate plasma. Its spectral signal was detected by using spectrograph. Based on the National Institute of Standard and Technology (NIST) database, LIBS spectral lines were indentified. The four Tibetan medicines mainly included Ca, Na, K, Mg and other elements and C-N molecular band. Specifically, Fe was detected in Renqing Changjue and 25-herb pearl pills; heavy mental elements Hg and Cu were shown in Renqing Mangjue and Renqing Changjue; Ag was found in Renqing Changjue. The results demonstrated that LIBS is a reliable and rapid multi-element analysis on the four Tibetan medicines. With Real-time, rapid and nondestructive advantages, LIBS has a wide application prospect in the element analysis on ethnic medicines.

  2. Multi trace element analysis of dry biological materials by neutron activation analysis including a chemical group separation

    International Nuclear Information System (INIS)

    Weers, C.A.

    1980-07-01

    Multi-element analysis of dry biological material by neutron activation analysis has to include radiochemical separation. The evaporation process is described in terms of the half-volume. The pretreatment of the samples and the development of the destruction-evaporation apparatus are described. The successive adsorption steps with active charcoal, Al 2 O 3 and coprecipitation with Fe(OH) 3 are described. Results obtained for standard reference materials are summarized. (G.T.H.)

  3. Multi-element analysis of lubricant oil by WDXRF technique using thin-film sample preparation

    International Nuclear Information System (INIS)

    Scapin, M. A.; Salvador, V. L. R.; Lopes, C. D.; Sato, I. M.

    2006-01-01

    The quantitative analysis of the chemical elements in matrices like oils or gels represents a challenge for the analytical chemists. The classics methods or instrumental techniques such as atomic absorption spectrometry (AAS) and plasma optical emission spectrometry (ICP-OES) need chemical treatments, mainly sample dissolution and degradation processes. X-ray fluorescence technique allows a direct and multi-element analysis without previous sample treatments. In this work, a sensible method for the determination of elements Mg, Al, Si, P, Ca, Ti, V, Cr, Mn, Fe, Ni, Cu, Zn, Mo, Ag, Sn, Ba and Pb in lubricating oil is presented. The x-ray fluorescence (WDXRF) technique using linear regression method and thin film sample preparation was used. The validation of the methodology (repeatability and accuracy) was obtained by the analysis of the standard reference materials SRM Alpha AESAR lot 703527D, applying the Chauvenet, Cochrane, ANOVA and Z-score statistical tests. The method presents a relative standard deviation lower than 10% for all the elements, except for Pb determination (RSD Pb 15%). The Z-score values for all the elements were in the range -2 < Z < 2, indicating a very good accuracy.(Full text)

  4. XRF and TXRF techniques for multi-element determination of trace elements in whole blood and human hair samples

    International Nuclear Information System (INIS)

    Khuder, A.; Karjou, J.; Sawan, M.Kh.; Bakir, M.A.

    2007-01-01

    XRF and TXRF were established as useful techniques for multi-element analysis of whole blood and human head hair samples. Direct-XRF with different collimation units and different X-ray excitation modes was successfully used for the determination of S, P, K, Ca, Fe, and Br elements in blood samples and K, Ca, Mn, Fe elements in human hair samples. Direct analysis by TXRF was used for the determination of Rb and Sr in digested blood and human hair samples, respectively, while, the co-precipitation method using APDC for TXRF analysis was used for the determination of Ni, Cu, Zn, and Pb elements in both matrices. As a result, the improved XRF and TXRF methods were applied for multi-element determination of elements in whole blood and human hair samples in non-occupational exposed population living in Damascus city. The mean concentrations of analyzed elements in both matrices were on the reported range values for non-occupational population in other countries. (author)

  5. XRF and TXRF techniques for multi-element determination of trace elements in whole blood and human hair samples

    International Nuclear Information System (INIS)

    Khuder, A.; Karjou, J.; Sawan, M.Kh.; Bakir, M.A.

    2008-01-01

    XRF and TXRF were established as useful techniques for multi-element analysis of whole blood and human head hair samples. Direct-XRF with different collimation units and different X-ray excitation modes was successfully used for the determination of S, P, K, Ca, Fe, and Br elements in blood samples and K, Ca, Mn, Fe elements in human hair samples. Direct analysis by TXRF was used for the determination of Rb and Sr in digested blood and human hair samples, respectively, while, the co-precipitation method using APDC for TXRF analysis was used for the determination of Ni, Cu, Zn, and Pb elements in both matrices. As a result, the improved XRF and TXRF methods were applied for multi-element determination of elements in whole blood and human hair samples in non-occupational exposed population living in Damascus city. The mean concentrations of analyzed elements in both matrices were on the reported range values for non-occupational population in other countries. (author)

  6. Multi-element analysis of crude-oil samples by 14.6 MeV neutron activation

    International Nuclear Information System (INIS)

    Cam, N.F.; Cigeroglu, F.; Erduran, M.N.

    1997-01-01

    The instrumental neutron activation technique, using the SAMEST T-400 neutron generator with 14.6 MeV neutrons produced from 3 H(d,n) 4 He reaction, is demonstrated for multi-element analysis of Saudi-Arabian crude-oil samples. The system parameters for the absolute method (e.g., the counting solid-angle, intrinsic efficiency of the γ-ray detector, effective neutron flux, activation cross sections, etc.)were determined and the results of elemental concentrations were presented with the corrections for all possible interferences having been carefully considered. (author)

  7. Computational complexity and memory usage for multi-frontal direct solvers used in p finite element analysis

    KAUST Repository

    Calo, Victor M.; Collier, Nathan; Pardo, David; Paszyński, Maciej R.

    2011-01-01

    The multi-frontal direct solver is the state of the art for the direct solution of linear systems. This paper provides computational complexity and memory usage estimates for the application of the multi-frontal direct solver algorithm on linear systems resulting from p finite elements. Specifically we provide the estimates for systems resulting from C0 polynomial spaces spanned by B-splines. The structured grid and uniform polynomial order used in isogeometric meshes simplifies the analysis.

  8. Computational complexity and memory usage for multi-frontal direct solvers used in p finite element analysis

    KAUST Repository

    Calo, Victor M.

    2011-05-14

    The multi-frontal direct solver is the state of the art for the direct solution of linear systems. This paper provides computational complexity and memory usage estimates for the application of the multi-frontal direct solver algorithm on linear systems resulting from p finite elements. Specifically we provide the estimates for systems resulting from C0 polynomial spaces spanned by B-splines. The structured grid and uniform polynomial order used in isogeometric meshes simplifies the analysis.

  9. Simultaneous multi-element determination in different seed samples of Dodonaea viscosa hopseed using instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    El-Sweify, Fatma H.; El-Amir, Mahmoud A.; Mostafa, Mohamed; Ramadan, Hala E.; Rashad, Ghada M.

    2016-01-01

    Instrumental neutron activation analysis technique (INAA) was applied for nondestructive multi-element analysis of seed samples of the plant Dodonaea viscosa hopseed. This plant is distributed all over Egypt, because of its suitable properties. The samples were collected from some bushes grown at different sites in some governorates, in July of each year during the period from 2004 to 2011. The determined elements are: Co, Cs, Eu, Fe, Hg, Ni, Rb, Sc, Se, Sr and Zn, under the chosen irradiation and cooling times. The content of some elements has been compared with data obtained from previous work on analysis of various kinds of seeds. The influence of some parameters on the determined elemental content is discussed. Standard reference materials IAEA-155 and IAEA-V-10 were used to assure quality control, accuracy and precision of the technique.

  10. Simultaneous multi-element determination in different seed samples of Dodonaea viscosa hopseed using instrumental neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    El-Sweify, Fatma H.; El-Amir, Mahmoud A.; Mostafa, Mohamed; Ramadan, Hala E.; Rashad, Ghada M. [Atomic Energy Authority, Cairo (Egypt). Hot Lab. Center

    2016-07-01

    Instrumental neutron activation analysis technique (INAA) was applied for nondestructive multi-element analysis of seed samples of the plant Dodonaea viscosa hopseed. This plant is distributed all over Egypt, because of its suitable properties. The samples were collected from some bushes grown at different sites in some governorates, in July of each year during the period from 2004 to 2011. The determined elements are: Co, Cs, Eu, Fe, Hg, Ni, Rb, Sc, Se, Sr and Zn, under the chosen irradiation and cooling times. The content of some elements has been compared with data obtained from previous work on analysis of various kinds of seeds. The influence of some parameters on the determined elemental content is discussed. Standard reference materials IAEA-155 and IAEA-V-10 were used to assure quality control, accuracy and precision of the technique.

  11. Multi-element analysis of small biological samples

    International Nuclear Information System (INIS)

    Rokita, E.; Cafmeyer, J.; Maenhaut, W.

    1983-01-01

    A method combining PIXE and INAA was developed to determine the elemental composition of small biological samples. The method needs virtually no sample preparation and less than 1 mg is sufficient for the analysis. The method was used for determining up to 18 elements in leaves taken from Cracow Herbaceous. The factors which influence the elemental composition of leaves and the possible use of leaves as an environmental pollution indicator are discussed

  12. Application of the multi-element analysis by X-fluorescence and neutron activation to the characterization of an archaeological site

    International Nuclear Information System (INIS)

    Rossini, I.

    1991-06-01

    The first part of this thesis is about possible analysis methods (XRF, PIXE, INAA, laser fluorimetry, and ICP), applied to Uranium, Thorium and Rubidium assays in archaeological clays and potteries. The best results have been obtained with Neutron Activation technics. The second part is about the multi-element analysis of quarries and about the research by statistical treatment of correlations between the element concentrations and the sampling sites (excavations, quarries)

  13. Multi-element probabilistic collocation method in high dimensions

    International Nuclear Information System (INIS)

    Foo, Jasmine; Karniadakis, George Em

    2010-01-01

    We combine multi-element polynomial chaos with analysis of variance (ANOVA) functional decomposition to enhance the convergence rate of polynomial chaos in high dimensions and in problems with low stochastic regularity. Specifically, we employ the multi-element probabilistic collocation method MEPCM and so we refer to the new method as MEPCM-A. We investigate the dependence of the convergence of MEPCM-A on two decomposition parameters, the polynomial order μ and the effective dimension ν, with ν<< N, and N the nominal dimension. Numerical tests for multi-dimensional integration and for stochastic elliptic problems suggest that ν≥μ for monotonic convergence of the method. We also employ MEPCM-A to obtain error bars for the piezometric head at the Hanford nuclear waste site under stochastic hydraulic conductivity conditions. Finally, we compare the cost of MEPCM-A against Monte Carlo in several hundred dimensions, and we find MEPCM-A to be more efficient for up to 600 dimensions for a specific multi-dimensional integration problem involving a discontinuous function.

  14. Multi-element neutron activation analysis of biological tissues: contribution to the study of trace element accumulation as a function of aging

    International Nuclear Information System (INIS)

    Gaudry, Andre.

    1975-01-01

    The accumulation of trace elements in various organs as a function of age was studied in rats, in connection with tissue aging phenomena. Part one reviews the various methods available to develop a programme of simultaneous multi-element analysis in biological matrices. Part two studies the precision and accuracy offered by neutron activation analysis. Special attention is paid to the problem of sample contamination by the silica glass irradiation supports. The possible causes of this effect are mentioned and a procedure limiting its harmful influence is proposed. Part three defines the restrictions introduced by the use of a method to separate the activable matrix. The fourth and last chapter describes the development of a multielement chemical separation system, designed to work semi-automatically for the simultaneous treatment of three samples and a standard in a shielded cell of small dimensions. The principles of a multi-comparator calibration where a knowledge of certain conventional but imprecise nuclear data is unnecessary owing to an experimental expedient are outlined briefly. Finally the separation method is tried out on various biological samples, including a reference (bovine liver SRM1577-NBS), and some results are given [fr

  15. Wear And Tear Determination By Trace Multi-Element Analysis Of An Unused And Used Lubricant Oil Using Instrumental Neutron Activation Analysis

    International Nuclear Information System (INIS)

    Adeyemo, D.J.

    2004-01-01

    Instrumental neutron activation analysis technique using the Imperial College Centre consort M. K. II nuclear reactor was utilized for the determination of: As, Ba Ca CI, Co, Cr, Cu, Fe, K, Mn, Mo, Na Ni, Rb, Sb, Se, Ti, V, and Zn, in an imported and used car lubricant oil. The wear of the oil lubricated parts of the car engine was monitored by establishing a correlation between the results obtained in the analysis. The result obtained from the analysis of the unused and then used samples on a low performing oil leaking four stroke car engine showed an increase on all the elements determined except for Se and Rb. The precision for the multi-element analysis is less than 12% for most of the elements. The accuracy of the measurement is also validated by the result obtained from the analysis of NBS-SRM1635 (sub-bituminous) coal standard for the elements. The results obtained indicate that analysis of unused and used lubricant oil samples can aid in locating defects in engine parts and hence facilitated maintenance procedures

  16. Detailed Modeling and Irreversible Transfer Process Analysis of a Multi-Element Thermoelectric Generator System

    Science.gov (United States)

    Xiao, Heng; Gou, Xiaolong; Yang, Suwen

    2011-05-01

    Thermoelectric (TE) power generation technology, due to its several advantages, is becoming a noteworthy research direction. Many researchers conduct their performance analysis and optimization of TE devices and related applications based on the generalized thermoelectric energy balance equations. These generalized TE equations involve the internal irreversibility of Joule heating inside the thermoelectric device and heat leakage through the thermoelectric couple leg. However, it is assumed that the thermoelectric generator (TEG) is thermally isolated from the surroundings except for the heat flows at the cold and hot junctions. Since the thermoelectric generator is a multi-element device in practice, being composed of many fundamental TE couple legs, the effect of heat transfer between the TE couple leg and the ambient environment is not negligible. In this paper, based on basic theories of thermoelectric power generation and thermal science, detailed modeling of a thermoelectric generator taking account of the phenomenon of energy loss from the TE couple leg is reported. The revised generalized thermoelectric energy balance equations considering the effect of heat transfer between the TE couple leg and the ambient environment have been derived. Furthermore, characteristics of a multi-element thermoelectric generator with irreversibility have been investigated on the basis of the new derived TE equations. In the present investigation, second-law-based thermodynamic analysis (exergy analysis) has been applied to the irreversible heat transfer process in particular. It is found that the existence of the irreversible heat convection process causes a large loss of heat exergy in the TEG system, and using thermoelectric generators for low-grade waste heat recovery has promising potential. The results of irreversibility analysis, especially irreversible effects on generator system performance, based on the system model established in detail have guiding significance for

  17. Effects of Heat Input and Bead Generation Methods on Finite Element Analysis of Multi-Pass Welding Process

    Energy Technology Data Exchange (ETDEWEB)

    Park, Won Dong; Kim, Ji Hoon; Bahn, Chi Bum [Pusan National University, Busan (Korea, Republic of)

    2016-10-15

    Welding residual stresses are determined by various factors such as heat input, initial temperature of molten bead, heating time, cooling time, cooling conditions, and boundary conditions. In this study, a sensitivity analysis was performed to find the major factors and reasonable assumptions for simulation. Two-dimensional axisymmetric simulation was conducted by using commercial finite element analysis program ABAQUS, for multi-pass Alloy 82 welds in a 304 Stainless Steel and SA-105 Carbon Steel. The major object is to evaluate effects of the heat input methods and weld bead generation methods on the welding residual stress distribution. Totally four kinds of methods were compared. From the previous results, we could make the following conclusions. 1. Although there are non-negligible differences in HAZ depending on heat input method, welding residual stress distributions have roughly similar trends. However, it is needed to perform the more exact analysis to apply heat energy more carefully into the individual bead. 2. Residual stress distribution were similar for the two weld bead generation technique. However, overlapping was happened when element birth technique was applied. Effects of overlapping could not ignore as deformation increases. However, overlapping problem was avoided when quiet element technique was used. 3. Since existence of inactive bead elements, inaccurate weld residual stresses could be occurred in boundaries of previous and next weld elements in case of quiet element technique.

  18. Rapid methods for multi-elemental X-ray fluorescence analysis using excitation isotope sources and Si(Li)-semiconductor detector

    International Nuclear Information System (INIS)

    Zhuravleva, E.L.

    1980-01-01

    Some rapid methods using an unique calibration curve have been developed for multi-elemental X-ray fluorescence analysis of thin and thick layers of various samples having low contents of heavy elements. The matrix absorption effect in thick samples is taken into account according to the scattered radiation.The similar method using a unique calibration curve for determination of low contents of trace elements in thin layers without account of matrix effect is proposed. The results on the intercomposition run soil-5 are in good agreement with the data obtained in different laboratories. The errors of the method are 10 %; in a case of peak superposition - 15 %

  19. Wideband multi-element Er-doped fiber amplifier

    International Nuclear Information System (INIS)

    Thipparapu, N K; Jain, S; May-Smith, T C; Sahu, J K

    2014-01-01

    A multi-element Er-doped fiber amplifier (MEEDFA) is demonstrated in which the gain profile is extended into the S and L bands. Each fiber element of the MEEDFA is found to provide a maximum gain of 37 dB and a noise figure of < 4 dB in the C-band. The gain profile of the amplifier is shifted towards longer wavelength by cascading fiber elements. The novel geometry of the multi-element fiber (MEF) could allow for the development of a broadband amplifier in a split-band configuration. The proposed amplifier can operate in the wavelength band of 1520 to 1595 nm (75 nm), with a minimum gain of 20 dB. (letter)

  20. Laser ablation-inductively coupled plasma-dynamic reaction cell-mass spectrometry for the multi-element analysis of polymers

    International Nuclear Information System (INIS)

    Resano, M.; Garcia-Ruiz, E.; Vanhaecke, F.

    2005-01-01

    In this work, the potential of laser ablation-inductively coupled plasma-mass spectrometry for the fast analysis of polymers has been explored. Different real-life samples (polyethylene shopping bags, an acrylonitrile butadiene styrene material and various plastic bricks) as well as several reference materials (VDA 001 to 004, Cd in polyethylene) have been selected for the study. Two polyethylene reference materials (ERM-EC 680 and 681), for which a reference or indicative value for the most relevant metals is available, have proved their suitability as standards for calibration. Special attention has been paid to the difficulties expected for the determination of Cr at the μg g -1 level in this kind of materials, due to the interference of ArC + ions on the most abundant isotopes of Cr. The use of ammonia as a reaction gas in a dynamic reaction cell is shown to alleviate this problem, resulting in a limit of detection of 0.15 μg g -1 for this element, while limiting only modestly the possibilities of the technique for simultaneous multi-element analysis. In this regard, As is the analyte most seriously affected by the use of ammonia, and its determination has to be carried out in vented mode, at the expense of measuring time. In all cases studied, accurate results could be obtained for elements ranging in content from the sub-μg g -1 level to tens of thousands of μg g -1 . However, the use of an element of known concentration as internal standard may be needed for materials with a matrix significantly different from that of the standard (polyethylene in this work). Precision ranged between 5% and 10% RSD for elements found at the 10 μg g -1 level or higher, while this value could deteriorate to 20% for analytes found at the sub-μg g -1 level. Overall, the technique evaluated presents many advantages for the fast and accurate multi-element analysis of these materials, avoiding laborious digestion procedures and minimizing the risk of analyte losses due to the

  1. Laser ablation inductively coupled plasma dynamic reaction cell mass spectrometry for the multi-element analysis of polymers

    Science.gov (United States)

    Resano, M.; García-Ruiz, E.; Vanhaecke, F.

    2005-11-01

    In this work, the potential of laser ablation-inductively coupled plasma-mass spectrometry for the fast analysis of polymers has been explored. Different real-life samples (polyethylene shopping bags, an acrylonitrile butadiene styrene material and various plastic bricks) as well as several reference materials (VDA 001 to 004, Cd in polyethylene) have been selected for the study. Two polyethylene reference materials (ERM-EC 680 and 681), for which a reference or indicative value for the most relevant metals is available, have proved their suitability as standards for calibration. Special attention has been paid to the difficulties expected for the determination of Cr at the μg g - 1 level in this kind of materials, due to the interference of ArC + ions on the most abundant isotopes of Cr. The use of ammonia as a reaction gas in a dynamic reaction cell is shown to alleviate this problem, resulting in a limit of detection of 0.15 μg g - 1 for this element, while limiting only modestly the possibilities of the technique for simultaneous multi-element analysis. In this regard, As is the analyte most seriously affected by the use of ammonia, and its determination has to be carried out in vented mode, at the expense of measuring time. In all cases studied, accurate results could be obtained for elements ranging in content from the sub-μg g - 1 level to tens of thousands of μg g - 1 . However, the use of an element of known concentration as internal standard may be needed for materials with a matrix significantly different from that of the standard (polyethylene in this work). Precision ranged between 5% and 10% RSD for elements found at the 10 μg g - 1 level or higher, while this value could deteriorate to 20% for analytes found at the sub-μg g - 1 level. Overall, the technique evaluated presents many advantages for the fast and accurate multi-element analysis of these materials, avoiding laborious digestion procedures and minimizing the risk of analyte losses due

  2. Multi-elemental analysis of aqueous geological samples by inductively coupled plasma-optical emission spectrometry

    Science.gov (United States)

    Todorov, Todor I.; Wolf, Ruth E.; Adams, Monique

    2014-01-01

    Typically, 27 major, minor, and trace elements are determined in natural waters, acid mine drainage, extraction fluids, and leachates of geological and environmental samples by inductively coupled plasma-optical emission spectrometry (ICP-OES). At the discretion of the analyst, additional elements may be determined after suitable method modifications and performance data are established. Samples are preserved in 1–2 percent nitric acid (HNO3) at sample collection or as soon as possible after collection. The aqueous samples are aspirated into the ICP-OES discharge, where the elemental emission signals are measured simultaneously for 27 elements. Calibration is performed with a series of matrix-matched, multi-element solution standards.

  3. MicroCT parameters for multi material elements assessment

    Energy Technology Data Exchange (ETDEWEB)

    Araújo, Olga M.O. de; Machado, Alessandra S.; Santos, Thaís M.P. dos; Ferreira, Cintia G.; Lopes, Ricardo T., E-mail: olgaufrjlin@gmail.com [Universidade Federal do Rio de Janeiro (UFRJ), Rio de Janeiro, RJ (Brazil). Programa de Engenharia Nuclear; Bastos, Jaqueline Silva [Universidade Estadual Paulista Julio de Mesquita Filho (UNESP), São Paulo, SP (Brazil)

    2017-07-01

    Microtomography is a non-destructive testing technique for quantitative and qualitative analysis. The investigation of multi material elements with great difference of density can result in artifacts that degrade image quality depending on combination of additional filter. The aim of this study is the selection of parameters most appropriate for analysis of bone tissue with metallic implant. The results show the simulation with MCNPX code for the distribution of energy without additional filter, with use of aluminum, copper and brass filters and their respective reconstructed images showing the importance of the choice of these parameters in image acquisition process on computed microtomography. (author)

  4. Multi element analysis by X-ray fluorescence. A powerful tool of ivory identification from various origins

    International Nuclear Information System (INIS)

    Kautenburger, R.; Mueller, P.; Wannemacher, J.

    2004-01-01

    The 11th CITES Conference in 2000 decided to maintain a total worldwide ban on trade of elephant ivory. The 12th Conference in 2002 decided to allow a conditional trade in stockpiled ivory in 2004. Reopening of the ivory trade would require methods to identify the origin of the ivory so that legal ivory can be distinguished from the black-market ones. X-ray fluorescence multi-element analysis of ivory samples from various regions of Africa and Southeast-Asia to characterize ivory of the various elephant populations is described. (author)

  5. Reliability modelling and analysis of a multi-state element based on a dynamic Bayesian network

    Science.gov (United States)

    Li, Zhiqiang; Xu, Tingxue; Gu, Junyuan; Dong, Qi; Fu, Linyu

    2018-04-01

    This paper presents a quantitative reliability modelling and analysis method for multi-state elements based on a combination of the Markov process and a dynamic Bayesian network (DBN), taking perfect repair, imperfect repair and condition-based maintenance (CBM) into consideration. The Markov models of elements without repair and under CBM are established, and an absorbing set is introduced to determine the reliability of the repairable element. According to the state-transition relations between the states determined by the Markov process, a DBN model is built. In addition, its parameters for series and parallel systems, namely, conditional probability tables, can be calculated by referring to the conditional degradation probabilities. Finally, the power of a control unit in a failure model is used as an example. A dynamic fault tree (DFT) is translated into a Bayesian network model, and subsequently extended to a DBN. The results show the state probabilities of an element and the system without repair, with perfect and imperfect repair, and under CBM, with an absorbing set plotted by differential equations and verified. Through referring forward, the reliability value of the control unit is determined in different kinds of modes. Finally, weak nodes are noted in the control unit.

  6. Finite element analysis of multi-material models using a balancing domain decomposition method combined with the diagonal scaling preconditioner

    International Nuclear Information System (INIS)

    Ogino, Masao

    2016-01-01

    Actual problems in science and industrial applications are modeled by multi-materials and large-scale unstructured mesh, and the finite element analysis has been widely used to solve such problems on the parallel computer. However, for large-scale problems, the iterative methods for linear finite element equations suffer from slow or no convergence. Therefore, numerical methods having both robust convergence and scalable parallel efficiency are in great demand. The domain decomposition method is well known as an iterative substructuring method, and is an efficient approach for parallel finite element methods. Moreover, the balancing preconditioner achieves robust convergence. However, in case of problems consisting of very different materials, the convergence becomes bad. There are some research to solve this issue, however not suitable for cases of complex shape and composite materials. In this study, to improve convergence of the balancing preconditioner for multi-materials, a balancing preconditioner combined with the diagonal scaling preconditioner, called Scaled-BDD method, is proposed. Some numerical results are included which indicate that the proposed method has robust convergence for the number of subdomains and shows high performances compared with the original balancing preconditioner. (author)

  7. Effects of Heat Input and Bead Generation Methods on Finite Element Analysis of Cylindrical Multi-Pass Welding Process of Metals

    International Nuclear Information System (INIS)

    Park, Won Dong; Bahn, Chi Bum; Kim, Ji Hoon

    2017-01-01

    In this study, a finite element analysis of a cylindrical multi-pass weldment for dissimilar metals was performed. The effects of the heat input method and weld bead generation method were considered. We compared two heat input methods: the heat flux method and the temperature method. We also compared two weld bead generation methods: the element birth method and the quiet element method. Although the results of the thermal analysis show deviations between the two heat input methods, the welding residual stresses were similar. Because the areas exposed to high temperature were similar and the strength of the material was very low in high temperature (above the 1000 ℃), the effects of the weld bead temperature were insignificant. The distributions of the welding residual stress were similar to each other. However, gaps and overlaps occurred on the welding boundary surfaces when the element birth method was applied. The quiet element method is more suitable for a large deformation model in order to simulate a more accurate weld shape.

  8. Effects of Heat Input and Bead Generation Methods on Finite Element Analysis of Cylindrical Multi-Pass Welding Process of Metals

    Energy Technology Data Exchange (ETDEWEB)

    Park, Won Dong; Bahn, Chi Bum; Kim, Ji Hoon [Pusan Nat’l Univ., Busan (Korea, Republic of)

    2017-06-15

    In this study, a finite element analysis of a cylindrical multi-pass weldment for dissimilar metals was performed. The effects of the heat input method and weld bead generation method were considered. We compared two heat input methods: the heat flux method and the temperature method. We also compared two weld bead generation methods: the element birth method and the quiet element method. Although the results of the thermal analysis show deviations between the two heat input methods, the welding residual stresses were similar. Because the areas exposed to high temperature were similar and the strength of the material was very low in high temperature (above the 1000 ℃), the effects of the weld bead temperature were insignificant. The distributions of the welding residual stress were similar to each other. However, gaps and overlaps occurred on the welding boundary surfaces when the element birth method was applied. The quiet element method is more suitable for a large deformation model in order to simulate a more accurate weld shape.

  9. Application of a microwave-based desolvation system for multi-elemental analysis of wine by inductively coupled plasma based techniques

    Energy Technology Data Exchange (ETDEWEB)

    Grindlay, Guillermo [Department of Analytical Chemistry, Nutrition and Food Sciences, University of Alicante, P.O. Box 99, 03080 Alicante (Spain)], E-mail: guillermo.grindlay@ua.es; Mora, Juan; Maestre, Salvador; Gras, Luis [Department of Analytical Chemistry, Nutrition and Food Sciences, University of Alicante, P.O. Box 99, 03080 Alicante (Spain)

    2008-11-23

    Elemental wine analysis is often required from a nutritional, toxicological, origin and authenticity point of view. Inductively coupled plasma based techniques are usually employed for this analysis because of their multi-elemental capabilities and good limits of detection. However, the accurate analysis of wine samples strongly depends on their matrix composition (i.e. salts, ethanol, organic acids) since they lead to both spectral and non-spectral interferences. To mitigate ethanol (up to 10% w/w) related matrix effects in inductively coupled plasma atomic emission spectrometry (ICP-AES), a microwave-based desolvation system (MWDS) can be successfully employed. This finding suggests that the MWDS could be employed for elemental wine analysis. The goal of this work is to evaluate the applicability of the MWDS for elemental wine analysis in ICP-AES and inductively coupled plasma mass spectrometry (ICP-MS). For the sake of comparison a conventional sample introduction system (i.e. pneumatic nebulizer attached to a spray chamber) was employed. Matrix effects, precision, accuracy and analysis throughput have been selected as comparison criteria. For ICP-AES measurements, wine samples can be directly analyzed without any sample treatment (i.e. sample dilution or digestion) using pure aqueous standards although internal standardization (IS) (i.e. Sc) is required. The behaviour of the MWDS operating with organic solutions in ICP-MS has been characterized for the first time. In this technique the MWDS has shown its efficiency to mitigate ethanol related matrix effects up to concentrations of 1% (w/w). Therefore, wine samples must be diluted to reduce the ethanol concentration up to this value. The results obtained have shown that the MWDS is a powerful device for the elemental analysis of wine samples in both ICP-AES and ICP-MS. In general, the MWDS has some attractive advantages for elemental wine analysis when compared to a conventional sample introduction system such

  10. Application of a microwave-based desolvation system for multi-elemental analysis of wine by inductively coupled plasma based techniques

    International Nuclear Information System (INIS)

    Grindlay, Guillermo; Mora, Juan; Maestre, Salvador; Gras, Luis

    2008-01-01

    Elemental wine analysis is often required from a nutritional, toxicological, origin and authenticity point of view. Inductively coupled plasma based techniques are usually employed for this analysis because of their multi-elemental capabilities and good limits of detection. However, the accurate analysis of wine samples strongly depends on their matrix composition (i.e. salts, ethanol, organic acids) since they lead to both spectral and non-spectral interferences. To mitigate ethanol (up to 10% w/w) related matrix effects in inductively coupled plasma atomic emission spectrometry (ICP-AES), a microwave-based desolvation system (MWDS) can be successfully employed. This finding suggests that the MWDS could be employed for elemental wine analysis. The goal of this work is to evaluate the applicability of the MWDS for elemental wine analysis in ICP-AES and inductively coupled plasma mass spectrometry (ICP-MS). For the sake of comparison a conventional sample introduction system (i.e. pneumatic nebulizer attached to a spray chamber) was employed. Matrix effects, precision, accuracy and analysis throughput have been selected as comparison criteria. For ICP-AES measurements, wine samples can be directly analyzed without any sample treatment (i.e. sample dilution or digestion) using pure aqueous standards although internal standardization (IS) (i.e. Sc) is required. The behaviour of the MWDS operating with organic solutions in ICP-MS has been characterized for the first time. In this technique the MWDS has shown its efficiency to mitigate ethanol related matrix effects up to concentrations of 1% (w/w). Therefore, wine samples must be diluted to reduce the ethanol concentration up to this value. The results obtained have shown that the MWDS is a powerful device for the elemental analysis of wine samples in both ICP-AES and ICP-MS. In general, the MWDS has some attractive advantages for elemental wine analysis when compared to a conventional sample introduction system such

  11. Integrated Process Design and Control of Multi-element Reactive Distillation Processes

    DEFF Research Database (Denmark)

    Mansouri, Seyed Soheil; Sales-Cruz, Mauricio; Huusom, Jakob Kjøbsted

    2016-01-01

    In this work, integrated process design and control of reactive distillation processes involving multi-elements is presented. The reactive distillation column is designed using methods and tools which are similar in concept to non-reactive distillation design methods, such as driving force approach....... The methods employed in this work are based on equivalent element concept. This concept facilitates the representation of a multi-element reactive system as equivalent binary light and heavy key elements. First, the reactive distillation column is designed at the maximum driving force where through steady...

  12. Head of detector for multi-element analysis

    International Nuclear Information System (INIS)

    Frynta, Z.

    1983-01-01

    The detector head mounted on the scintillation counter consists of a hollow hexagonal rotary support axially arranged with the photomultiplier of the scintillation counter. In the walls of the hexagonal rotary support there are openings in which are inserted absorption filters. The mounting of the absorption filters on the rotary support allows the analysis of a greater number of elements without the dismantling of the head and the replacement of filters. The suitable geometry of the head is retained so that it is possible to insert the head into the hollows similarly as the scintillation counter. (J.P.)

  13. Multi-element analysis, bioavailability and fractionation of herbal tea products

    Energy Technology Data Exchange (ETDEWEB)

    Szymczycha-Madeja, Anna; Welna, Maja; Zyrnicki, Wieslaw, E-mail: anna.szymczycha@pwr.wroc.pl [Wroclaw University of Technology, Chemistry Department, Analytical Chemistry Division, Wroclaw (Poland)

    2013-05-15

    Herbal teas (Mentha piperitae foliumand mixture Marticaria chamomilla flos with Lavandula officinalis flos) were compared considering the total contents of micro (Al, Ba, Cd, Cr, Cu, Fe, Mn, Ni, Pb, Sr, Ti, V) and macro (C, H, N, S, Ca, Mg, P) elements, bioavailability and fractionation. Different methods (inductively coupled plasma optical emission spectrometry (ICP OES), Fourier transform infrared spectroscopy (FTIR) and CHNS elemental analysis) were applied. The microwave-assisted digestion procedure was found to be more effective than the hot-plate heating for the wet acid digestion of tea. The application of the modified BCR (Community Bureau of Reference) sequential extraction procedure exhibited differences in the concentrations of metal bound to reducible and oxidizable fractions. The accuracy of method was verified by analysis of certified reference material INCT-TL{sup -1} Tea Leaves. The daily intake of all elements from the analyzed herbal tea infusion did not exceed the maximum permissible levels and does not constitute health risk. (author)

  14. Multi-element analysis, bioavailability and fractionation of herbal tea products

    International Nuclear Information System (INIS)

    Szymczycha-Madeja, Anna; Welna, Maja; Zyrnicki, Wieslaw

    2013-01-01

    Herbal teas (Mentha piperitae foliumand mixture Marticaria chamomilla flos with Lavandula officinalis flos) were compared considering the total contents of micro (Al, Ba, Cd, Cr, Cu, Fe, Mn, Ni, Pb, Sr, Ti, V) and macro (C, H, N, S, Ca, Mg, P) elements, bioavailability and fractionation. Different methods (inductively coupled plasma optical emission spectrometry (ICP OES), Fourier transform infrared spectroscopy (FTIR) and CHNS elemental analysis) were applied. The microwave-assisted digestion procedure was found to be more effective than the hot-plate heating for the wet acid digestion of tea. The application of the modified BCR (Community Bureau of Reference) sequential extraction procedure exhibited differences in the concentrations of metal bound to reducible and oxidizable fractions. The accuracy of method was verified by analysis of certified reference material INCT-TL -1 Tea Leaves. The daily intake of all elements from the analyzed herbal tea infusion did not exceed the maximum permissible levels and does not constitute health risk. (author)

  15. Characterisation of synthetic multi-element standards (SMELS) used for the validation of k(o)-NAA

    Czech Academy of Sciences Publication Activity Database

    Vermaercke, P.; Robouch, P.; Eguskiza, M.; De Corte, F.; Kennedy, G.; Smodiš, B.; Jaćimović, R.; Yonezawa, C.; Matsue, H.; Lin, X.; Blaauw, M.; Kučera, Jan

    2006-01-01

    Roč. 564, č. 2 (2006), s. 675-682 ISSN 0168-9002 Institutional research plan: CEZ:AV0Z10480505 Keywords : neutron activation analysis * ko-standardization * multi-element standard Subject RIV: CB - Analytical Chemistry, Separation

  16. Theoretical background and implementation of the finite element method for multi-dimensional Fokker-Planck equation analysis

    Czech Academy of Sciences Publication Activity Database

    Král, Radomil; Náprstek, Jiří

    2017-01-01

    Roč. 113, November (2017), s. 54-75 ISSN 0965-9978 R&D Projects: GA ČR(CZ) GP14-34467P; GA ČR(CZ) GA15-01035S Institutional support: RVO:68378297 Keywords : Fokker-Planck equation * finite element method * simplex element * multi-dimensional problem * non-symmetric operator Subject RIV: JM - Building Engineering OBOR OECD: Mechanical engineering Impact factor: 3.000, year: 2016 https://www.sciencedirect.com/science/ article /pii/S0965997817301904

  17. Multi-Element Analysis and Geochemical Spatial Trends of Groundwater in Rural Northern New York

    Directory of Open Access Journals (Sweden)

    Michael O’Connor

    2010-05-01

    Full Text Available Samples from private wells (n = 169 throughout St. Lawrence County, NY were analyzed by ICP-MS multi-element techniques. St. Lawrence County spans three diverse bedrock terranes including Precambrian crystalline rocks of the Adirondack Lowlands (mostly paragneisses and Highlands (mostly orthogneisses, as well as Paleozoic sedimentary rocks of the St. Lawrence Valley. An ArcGIS database was constructed and used to generate contour plots for elements across the county. Strontium isotopes and unique geochemical signatures were used to distinguish water from various geologic units. The results were consistent with a large (7,309 km2, sparsely populated (~110,000, rural region with diverse bedrock and glacial cover.

  18. Neutron activation analysis of trace elements in foodstuffs

    International Nuclear Information System (INIS)

    Schelenz, R.; Fischer, E.

    1976-05-01

    A neutron activation method for multielement determination in biological material was developed. The individual steps of the method include radiochemical processing as well as nondestructive techniques. In order to develop a high resolution gamma spectrometric method the indispensable assumptions were the application of Ge(Li)-semiconductor detectors, multi-channel pulse height analyzers and the use of electronic data evaluation with mini-computers for the automatic evaluation of complex gamma spectra. After radiochemical separation (RNAA) 33 elements can be determined in biological materials and by application of nondestructive, purely instrumental techniques (INAA) 25 elements. The time required for the analysis of 33 elements can be determined in biological materials and by application of nondestructive, purely instrumental techniques (INAA) 25 elements. The time required for the analysis of 33 elements is 4 days. The neutron activation method is used routinely for the determination of trace elements in foodstuffs and in the field of nutrition research. (orig.) [de

  19. Multi elemental analysis of indigenous food spices in Southern Ethiopia using INAA technique

    International Nuclear Information System (INIS)

    Melkegna, T.H.; Chaubey, A.K.; Beyene, G.A.; Bitewlign, T.A.

    2017-01-01

    The objective of this study is a quantitative and qualitative analysis of essential and trace elements of four indigenous Ethiopian spices and herbs using instrumental neutron activation analysis technique. Results obtained for 16 elements: Major elements; Mg, Cl, and K; Minor elements; Na, Fe, and Mn, Zn, Br. While Al, V, Sm, Sc, La, Ba, Eu, Rb were found in traces. The spices, Affromumom korarima and Lippa Adonesis var. Koseret sebsebe were found to be very good sources of essential trace elements like Fe, Zn and Mn. The highest concentration of Mg was found in Ajowan whereas K and Fe were measured in Coriander seeds. The average daily dietary intake of some essential elements from the use of these spices were found to be below the recommended upper limit by WHO. (author)

  20. Multidisciplinary approach and multi-scale elemental analysis and separation chemistry

    International Nuclear Information System (INIS)

    Mariet, Clarisse

    2014-01-01

    The development of methods for the analysis of trace elements is an important component of my research activities either for a radiometric measure or mass spectrometric detection. Many studies raise the question of the chemical signature of a sample or a process: eruptive behavior of a volcano, indicator of pollution, ion exchange in vectors vesicles of active principles,... Each time, highly sensitive analytical procedures, accurate and multi-elementary as well as the development of specific protocols were needed. Neutron activation analysis has often been used as reference procedure and allowed to validate the chemical lixiviation and the measurement by ICP-MS. Analysis of radioactive samples requires skills in analysis of trace but also separation chemistry. Two separation methods occupy an important place in the separation chemistry of radionuclides: chromatography and liquid-liquid extraction. The study of extraction of Lanthanide (III) by the oxide octyl (phenyl)-n, N-diisobutyl-carbamoylmethyl phosphine (CMPO) and a calixarene-CMPO led to better understand and quantify the influence of operating conditions on their performance of extraction and selectivity. The high concentration of salts in aqueous solutions required to reason in terms of thermodynamic activities in relying on a comprehensive approach to quantification of deviations from ideality. In order to reduce the amount of waste generated and costs, alternatives to the hydrometallurgical extraction processes were considered using ionic liquids at low temperatures as alternative solvents in biphasic processes. Remaining in this logic of effluent reduction, miniaturization of the liquid-liquid extraction is also study so as to exploit the characteristics of microscopic scale (very large specific surface, short diffusion distances). The miniaturization of chromatographic separations carries the same ambitions of gain of volumes of wastes and reagents. The miniaturization of the separation Uranium

  1. Coulomb matrix elements in multi-orbital Hubbard models.

    Science.gov (United States)

    Bünemann, Jörg; Gebhard, Florian

    2017-04-26

    Coulomb matrix elements are needed in all studies in solid-state theory that are based on Hubbard-type multi-orbital models. Due to symmetries, the matrix elements are not independent. We determine a set of independent Coulomb parameters for a d-shell and an f-shell and all point groups with up to 16 elements (O h , O, T d , T h , D 6h , and D 4h ). Furthermore, we express all other matrix elements as a function of the independent Coulomb parameters. Apart from the solution of the general point-group problem we investigate in detail the spherical approximation and first-order corrections to the spherical approximation.

  2. Structural analysis of ITER multi-purpose deployer

    International Nuclear Information System (INIS)

    Manuelraj, Manoah Stephen; Dutta, Pramit; Gotewal, Krishan Kumar; Rastogi, Naveen; Tesini, Alessandro; Choi, Chang-Hwan

    2016-01-01

    Highlights: • System modelling for structural analysis of the Multi-Purpose Deployer (MPD). • Finite element modeling of the Multi-Purpose Deployer (MPD). • Static, modal and seismic response analysis of the Multi-Purpose Deployer (MPD). • Iterative structural analysis and design update to satisfy the structural criteria. • Modal analysis for various kinematic configurations. • Reaction force calculations on the interfacing systems. - Abstract: The Multi-Purpose Deployer (MPD) is a general purpose ITER in-vessel remote handling (RH) system. The main handling equipment, known as the MPD Transporter, consists of a series of linked bodies, which provide anchoring to the vacuum vessel port and an articulated multi-degree of freedom motion to perform various in-vessel maintenance tasks. During the in-vessel operations, the structural integrity of the system should be guaranteed against various operational and seismic loads. This paper presents the structural analysis results of the concept design of the MPD Transporter considering the seismic events. Static structural, modal and frequency response spectrum analyses have been performed to verify the structural integrity of the system, and to provide reaction forces to the interfacing systems such as vacuum vessel and cask. Iterative analyses and design updates are carried out based on the reference design of the system to improve the structural behavior of the system. The frequency responses of the system in various kinematics and payloads are assessed.

  3. Homogenization on Multi-Materials’ Elements: Application to Printed Circuit Boards and Warpage Analysis

    Directory of Open Access Journals (Sweden)

    Araújo Manuel

    2016-01-01

    Full Text Available Multi-material domains are often found in industrial applications. Modelling them can be computationally very expensive due to meshing requirements. The finite element properties comprising different materials are hardly accurate. In this work, a new homogenization method that simplifies the computation of the homogenized Young modulus, Poisson ratio and thermal expansion coefficient is proposed, and applied to composite-like material on a printed circuit board. The results show a good properties correspondence between the homogenized domain and the real geometry simulation.

  4. Multi-element neutron activation analysis of Brazilian coal samples

    International Nuclear Information System (INIS)

    Atalla, L.T.; Requejo, C.S.

    1982-09-01

    The elements U, Th, La, Ce, Nd, Sm, Eu, Dy, Tb, Yb, Lu, Sc, Ta, Hf, Co, Ni, Cr, Mo, Ti, V, W, In, Ga, Mn, Ba, Sr, Mg, Rb, Cs, K, Cl, Br, As, Sb, Au, Ca, Al and Fe were determined in coal samples by instrumental neutron activation analysis, by using both thermal and epithermal neutron irradiations. The irradiation times were 10 minutes and 8 or 16 hours in a position where the thermal neutron flux was about 10 12 n.cm - 2 .s - 1 and 72 non-consecutive hours for epithermal irradiation at a flux of about 10 11 n.Cm - 2 .s - 1 . After the instrumental analysis of the above mentioned elements, Zn and Se were determined with chemical separation. The relative standard deviation of, at least, 4 determinations was about + - 10% for the majority of the results. The coal samples analysed were supplied by: Cia. Estadual da Tecnologia e Saneamento Basico (CETESB-SP), Cia. de Pesquisas e Lavras Minerais (COPELMI-RS), Cia. Carbonifera Urussunga (SC), Cia. Carbonifera Prospera (SC), Cia. Carbonifera Treviso (SC), Cia. Nacional de Mineracao de Carvao do Barro Branco (SC) and Comissao Nacional de Energia Nuclear (CNEN-RJ). (Author) [pt

  5. Multi-element analysis of wheat flour and white bread by neutron activation

    International Nuclear Information System (INIS)

    Godinez A, M.A.

    1994-01-01

    One of the best source of feeding even for the human being as for animals are the Cereals. Although they are mainly energetic aliment, due to its composition in starch, they are a very important source of proteins and amino acids. They contribute mineral elements to the diet. Even those elements constitute a very small part of the total diet, they take a very important place in many human metabolic processes. To make a multielemental analysis of an aliment is very important that we are based on a very sensible analytic technique so we are able to find them, just as the Neutronic Activation. This Nuclear technique allows you to make a qualitative and quantitative analysis of the elements that are in a sample, but it does n't show the way in which the elements are presented. It is based in turning those elements into radioactive ones through its exposition to an uniform and constant fluid of neutrons, so then its radioactivity can be determined. The present work has as a main purpose to make a multielemental analysis of the wheat flour and white bread through the Neutronic Activation Technique, using the comparator method and establishing previously the most appropriate work conditions as much irradiation as digestion and measuring of the radioactivity of the sample. In this way, it was able to know that the wheat flour has potassium, chlorine, magnesium, sodium, iron, zinc, manganese, rubidium and selenium elements in a concentration of 2000, 700, 500, 25, 18, 13, 5.5, 0.9 and 0.01 - 0.3 mg/g respectively. In an other hand it was found that the white bread has the same elements than the wheat flour but its concentration was: 1700, 9000, 400, 7000, 52, 13, 6, 1 and 0.05 - 0.3 mg/g respectively. (Author)

  6. Multi Scale Finite Element Analyses By Using SEM-EBSD Crystallographic Modeling and Parallel Computing

    International Nuclear Information System (INIS)

    Nakamachi, Eiji

    2005-01-01

    A crystallographic homogenization procedure is introduced to the conventional static-explicit and dynamic-explicit finite element formulation to develop a multi scale - double scale - analysis code to predict the plastic strain induced texture evolution, yield loci and formability of sheet metal. The double-scale structure consists of a crystal aggregation - micro-structure - and a macroscopic elastic plastic continuum. At first, we measure crystal morphologies by using SEM-EBSD apparatus, and define a unit cell of micro structure, which satisfy the periodicity condition in the real scale of polycrystal. Next, this crystallographic homogenization FE code is applied to 3N pure-iron and 'Benchmark' aluminum A6022 polycrystal sheets. It reveals that the initial crystal orientation distribution - the texture - affects very much to a plastic strain induced texture and anisotropic hardening evolutions and sheet deformation. Since, the multi-scale finite element analysis requires a large computation time, a parallel computing technique by using PC cluster is developed for a quick calculation. In this parallelization scheme, a dynamic workload balancing technique is introduced for quick and efficient calculations

  7. Multi-Element Lean Direct Injection Combustor Module, Phase I

    Data.gov (United States)

    National Aeronautics and Space Administration — We propose to develop a Multi-Element Lean Direct Injection, ME-LDI, Combustion concept with the following innovative features: 1. Independent, mini burning zones...

  8. Design and Fabrication of High Gain Multi-element Multi-segment Quarter-sector Cylindrical Dielectric Resonator Antenna

    Science.gov (United States)

    Ranjan, Pinku; Gangwar, Ravi Kumar

    2017-12-01

    A novel design and analysis of quarter cylindrical dielectric resonator antenna (q-CDRA) with multi-element and multi-segment (MEMS) approach has been presented. The MEMS q-CDRA has been designed by splitting four identical quarters from a solid cylinder and then multi-segmentation approach has been utilized to design q-CDRA. The proposed antenna has been designed for enhancement in bandwidth as well as for high gain. For bandwidth enhancement, multi-segmentation method has been explained for the selection of dielectric constant of materials. The performance of the proposed MEMS q-CDRA has been demonstrated with design guideline of MEMS approach. To validate the antenna performance, three segments q-CDRA has been fabricated and analyzed practically. The simulated results have been in good agreement with measured one. The MEMS q-CDRA has wide impedance bandwidth (|S11|≤-10 dB) of 133.8 % with monopole-like radiation pattern. The proposed MEMS q-CDRA has been operating at TM01δ mode with the measured gain of 6.65 dBi and minimum gain of 4.5 dBi in entire operating frequency band (5.1-13.7 GHz). The proposed MEMS q-CDRA may find appropriate applications in WiMAX and WLAN band.

  9. Radiochemical neutron activation analysis based multi-elemental analysis of high purity gallium

    International Nuclear Information System (INIS)

    Tashimova, F.A.; Sadikov, I.I; Salimov, M.I.; Zinov'ev, V.G.

    2006-01-01

    Full text: Gallium is one of the widely used materials in semiconductor and optoelectronics industry. Gallium is used to produce infrared detectors, piezoelectric sensors, high- and low-temperature transistors for space and defense technology. One of the most important requirements for semiconductor materials of gallium compounds is an excessive high purity for layers and films. Information on impurities (type of an impurity, concentration, character of distribution) is important as for better understanding of the physical and chemical processes taking place in formed semiconductor structures and for the 'know-how' of devices on their basis. The object of this work is to develop radiochemical neutron activation technique for analysis of high purity gallium. Irradiation of 0.1 g of gallium sample in neutron flux of 5·10 13 cm -2 s -1 for 5 hours will result in induced activity of more than 10 8 Bq, due to 72 Ga radionuclide, half-life of which is 14.1 hours. Therefore to perform instrumental NAA of gallium long period (10 day) cooling is required, and high sensitive determination of elements producing short- and long-lived radionuclides (T 1/2 72 Ga. We have studied the behavior of gallium in extraction-chromatographic system 'TBP-HCl'. The experiments have shown that higher factor of distribution (D) and capacity on gallium can be achieved when 'TBP-4M HCl' system is used. However more than 10 trace elements have high D and thus they cannot be separated from 72 Ga. To resolve the problem and increase the number of separated trace elements we have used preliminary satisfaction of chromatographic column with tellurium, which has D higher than the most of elements in 'TBP-4M HCl' system and thus suppresses extraction of elements. Distribution profile of gallium along the column and elution curve of 25 trace elements have been measured. Chemical yields of separated elements measured by using radiotracers are more than 93%. On the basis of the carried out researches

  10. Operational trials of single- and multi-element CR-39 dosemeters for the DIDO and PLUTO reactors at the Harwell Laboratory

    International Nuclear Information System (INIS)

    Gallacher, G.G.; Perks, C.A.

    1993-01-01

    Single- and multi-element CR-39 dosemeters, developed at the Harwell Laboratory, and a commercially available multi-element CR-39 dosemeter (obtained from Track Analysis Systems Ltd), were evaluated for their potential as neutron dosemeters for personnel working at Harwell Laboratory's research reactors. Owing to the angular dependence of the CR-39 (processed using electrochemical etching), the single-element dosemeter was found to be impractical. Consequently, a multi-element dosemeter was developed, which consisted of a cube of side 36 mm with CR-39 elements (also processed using electrochemical etching) attached to each of the sides. Although this dosemeter was technically suitable for this type of dosimetry, it was considered to be unacceptably bulky in personnel trials. The commercially available CR-39 dosemeter tested was much smaller (the CR-39 was only chemically etched) and this was considered to be acceptable as a personnel dosemeter. In addition, trials with personnel working at active handling glove boxes indicated that single-element dosemeters might be adequate, but further work would be needed to verify this. (author)

  11. Finite Element Analysis and Optimization for the Multi-stage Deep Drawing of Molybdenum Sheet

    International Nuclear Information System (INIS)

    Kim, Heung-Kyu; Hong, Seok Kwan; Kang, Jeong Jin; Heo, Young-moo; Lee, Jong-Kil; Jeon, Byung-Hee

    2005-01-01

    Molybdenum, a bcc refractory metal with a melting point of about 2600 deg. C, has a high heat and electrical conductivity. In addition, it remains strong mechanically at high temperatures as well as at low temperatures. Therefore it is a technologically very important material for the applications operating at high temperatures. However, a multi-stage process is required due to the low drawability for making a deep drawn part from the molybdenum sheet. In this study, a multi-stage deep drawing process for a molybdenum circular cup was designed by combining the drawing with the ironing, which was effective for the low drawability materials. A parametric study by FE analysis for the multi-stage deep drawing was conducted for evaluation of the design variables effect. Based on the FE analysis result, the multi-stage deep drawing process was parameterized by the design variables, and an optimum process design was obtained by the process optimization based on the FE simulation at each stage

  12. Quantitative and qualitative analysis of fluoride and multi elements of shark teeth by PIXE

    International Nuclear Information System (INIS)

    Sakurai, S.; Asakawa, R.; Hirota, F.; Sato, T.; Sera, K.; Itoh, J.

    2008-01-01

    Biomineralization has two types, biologically induced mineralization (BIM) and biologically controlled mineralization (BCM). Shark teeth is a typical representative of BCM. We have measured concentrations of fluorine and multi elements in shark teeth collected in the south of Japan. As a result, it was confirmed that the sample preparation method, which was established for the biological samples, is applicable to the shark teeth samples and the elemental concentration was obtained in good accuracy and reproducibility. Moreover, we clarified that the shark teeth is composed of Fluorapatite by the combination with X-ray Diffraction. Fluorine concentration is found to be 5500 μg/g in the shark teeth. We have 100 samples of Shark teeth and are planning on reporting the findings of a study with larger samples in the near future. (author)

  13. Clustering of samples and elements based on multi-variable chemical data

    International Nuclear Information System (INIS)

    Op de Beeck, J.

    1984-01-01

    Clustering and classification are defined in the context of multivariable chemical analysis data. Classical multi-variate techniques, commonly used to interpret such data, are shown to be based on probabilistic and geometrical principles which are not justified for analytical data, since in that case one assumes or expects a system of more or less systematically related objects (samples) as defined by measurements on more or less systematically interdependent variables (elements). For the specific analytical problem of data set concerning a large number of trace elements determined in a large number of samples, a deterministic cluster analysis can be used to develop the underlying classification structure. Three main steps can be distinguished: diagnostic evaluation and preprocessing of the raw input data; computation of a symmetric matrix with pairwise standardized dissimilarity values between all possible pairs of samples and/or elements; and ultrametric clustering strategy to produce the final classification as a dendrogram. The software packages designed to perform these tasks are discussed and final results are given. Conclusions are formulated concerning the dangers of using multivariate, clustering and classification software packages as a black-box

  14. Multi-element isotope dilution analyses using ICP-MS

    International Nuclear Information System (INIS)

    Volpe, A.M.

    1996-01-01

    Presently, 37 elements ranging from light (Li,B) through transition metals, noble, rare earth and heavy elements, to actinides and transuranics (Pu, Am, Cm) are measured by isotope dilution at Lawrence Livermore National Laboratory. Projects range from geological and hydrological to biological. The research goal is to measure accurately many elements present in diverse matrices at trace (ppb) levels using isotope dilution methods. Major advantages of isotope dilution methods are accuracy, elimination of ion intensity calibration, and quantitation for samples that require chemical separation. Accuracy depends on tracer isotope calibration, tracer-sample isotopic equilibration, and appropriate background, isobaric and mass bias corrections. Propagation of isotope ratio error due to improper tracer isotope addition is a major concern with multi-element analyses when abundances vary widely. 11 refs., 3 figs

  15. The multi-element probabilistic collocation method (ME-PCM): Error analysis and applications

    International Nuclear Information System (INIS)

    Foo, Jasmine; Wan Xiaoliang; Karniadakis, George Em

    2008-01-01

    Stochastic spectral methods are numerical techniques for approximating solutions to partial differential equations with random parameters. In this work, we present and examine the multi-element probabilistic collocation method (ME-PCM), which is a generalized form of the probabilistic collocation method. In the ME-PCM, the parametric space is discretized and a collocation/cubature grid is prescribed on each element. Both full and sparse tensor product grids based on Gauss and Clenshaw-Curtis quadrature rules are considered. We prove analytically and observe in numerical tests that as the parameter space mesh is refined, the convergence rate of the solution depends on the quadrature rule of each element only through its degree of exactness. In addition, the L 2 error of the tensor product interpolant is examined and an adaptivity algorithm is provided. Numerical examples demonstrating adaptive ME-PCM are shown, including low-regularity problems and long-time integration. We test the ME-PCM on two-dimensional Navier-Stokes examples and a stochastic diffusion problem with various random input distributions and up to 50 dimensions. While the convergence rate of ME-PCM deteriorates in 50 dimensions, the error in the mean and variance is two orders of magnitude lower than the error obtained with the Monte Carlo method using only a small number of samples (e.g., 100). The computational cost of ME-PCM is found to be favorable when compared to the cost of other methods including stochastic Galerkin, Monte Carlo and quasi-random sequence methods

  16. Multi-elemental imaging of paraffin-embedded human samples by laser-induced breakdown spectroscopy

    Science.gov (United States)

    Moncayo, S.; Trichard, F.; Busser, B.; Sabatier-Vincent, M.; Pelascini, F.; Pinel, N.; Templier, I.; Charles, J.; Sancey, L.; Motto-Ros, V.

    2017-07-01

    Chemical elements play central roles for physiological homeostasis in human cells, and their dysregulation might lead to a certain number of pathologies. Novel imaging techniques that improve the work of pathologists for tissue analysis and diagnostics are continuously sought. We report the use of Laser-Induced Breakdown Spectroscopy (LIBS) to perform multi-elemental images of human paraffin-embedded skin samples on the entire biopsy scale in a complementary and compatible way with microscope histopathological examination. A specific instrumental configuration is proposed in order to detect most of the elements of medical interest (i.e. P, Al, Mg, Na, Zn, Si, Fe, and Cu). As an example of medical application, we selected and analysed skin biopsies, including healthy skin tissue, cutaneous metastasis of melanoma, Merkel-cell carcinoma and squamous cell carcinoma. Clear distinctions in the distribution of chemical elements are observed from the different samples investigated. This study demonstrates the high complementarity of LIBS elemental imaging with conventional histopathology, opening new opportunities for any medical application involving metals.

  17. A computer programme for use in the development of multi-element x-ray-fluorescence methods of analysis

    International Nuclear Information System (INIS)

    Wall, G.J.

    1985-01-01

    A computer programme (written in BASIC) is described for the evaluation of spectral-line intensities in X-ray-fluorescence spectrometry. The programme is designed to assist the analyst while he is developing new analytical methods, because it facilitates the selection of the following evaluation parameters: calculation models, spectral-line correction factors, calibration curves, calibration ranges, and point deletions. In addition, the programme enables the analyst to undertake routine calculations of data from multi-element analyses in which variable data-reduction parameters are used for each element

  18. Pump radiation distribution in multi-element first cladding laser fibres

    International Nuclear Information System (INIS)

    Mel'kumov, Mikhail A; Bufetov, Igor' A; Bubnov, M M; Shubin, Aleksei V; Semenov, S L; Dianov, Evgenii M

    2005-01-01

    Pump radiation transfer is studied experimentally in multi-element first cladding laser fibres. A model of this process is proposed, which is in good agreement with experimental results. An all-fibre single-mode cw ytterbium laser based on a three-element first cladding fibre with an output power of 100W is fabricated. (lasers)

  19. Hydrothermal analysis in engineering using control volume finite element method

    CERN Document Server

    Sheikholeslami, Mohsen

    2015-01-01

    Control volume finite element methods (CVFEM) bridge the gap between finite difference and finite element methods, using the advantages of both methods for simulation of multi-physics problems in complex geometries. In Hydrothermal Analysis in Engineering Using Control Volume Finite Element Method, CVFEM is covered in detail and applied to key areas of thermal engineering. Examples, exercises, and extensive references are used to show the use of the technique to model key engineering problems such as heat transfer in nanofluids (to enhance performance and compactness of energy systems),

  20. The use of synchrotron radiation for trace element analysis and element mapping by scanning X-ray fluorescence

    International Nuclear Information System (INIS)

    Davies, S.T.

    1983-01-01

    Synchrotron Radiation excited X-Ray Fluorescence is a potentially powerful tool for the routine quantitative chemical analysis of materials, with minimum detection limits typically of the order of a tenth of a ppm, and with the added advantages of simultaneous multi-element detection capability, spatial resolution on a micron scale, large signal to noise ratios and short analysis times. This paper presents a brief review of the use of Synchrotron Radiation in Trace Element Analysis and discusses the requirements for a microprobe for chemical analysis utilising SR. Data obtained at the Synchrotron Radiation Source, Daresbury Laboratory include XRF spectra of standard reference materials and an application of the technique to the study of ion implanted layers in semiconductors is outlined. (author)

  1. Chemical elements in the environment: multi-element geochemical datasets from continental to national scale surveys on four continents

    Science.gov (United States)

    Caritat, Patrice de; Reimann, Clemens; Smith, David; Wang, Xueqiu

    2017-01-01

    During the last 10-20 years, Geological Surveys around the world have undertaken a major effort towards delivering fully harmonized and tightly quality-controlled low-density multi-element soil geochemical maps and datasets of vast regions including up to whole continents. Concentrations of between 45 and 60 elements commonly have been determined in a variety of different regolith types (e.g., sediment, soil). The multi-element datasets are published as complete geochemical atlases and made available to the general public. Several other geochemical datasets covering smaller areas but generally at a higher spatial density are also available. These datasets may, however, not be found by superficial internet-based searches because the elements are not mentioned individually either in the title or in the keyword lists of the original references. This publication attempts to increase the visibility and discoverability of these fundamental background datasets covering large areas up to whole continents.

  2. Particle induced X-ray emission for quantitative trace-element analysis using the Eindhoven cyclotron

    International Nuclear Information System (INIS)

    Kivits, H.

    1980-01-01

    Development of a multi-elemental trace analysis technique using PIXE (Particle Induced X-ray Emission), was started almost five years ago at the Eindhoven University of Technology, in the Cyclotron Applications Group of the Physics Department. The aim of the work presented is to improve the quantitative aspects of trace-element analysis with PIXE, as well as versatility, speed and simplicity. (Auth.)

  3. Numerical solution of multi group-Two dimensional- Adjoint equation with finite element method

    International Nuclear Information System (INIS)

    Poursalehi, N.; Khalafi, H.; Shahriari, M.; Minoochehr

    2008-01-01

    Adjoint equation is used for perturbation theory in nuclear reactor design. For numerical solution of adjoint equation, usually two methods are applied. These are Finite Element and Finite Difference procedures. Usually Finite Element Procedure is chosen for solving of adjoint equation, because it is more use able in variety of geometries. In this article, Galerkin Finite Element method is discussed. This method is applied for numerical solving multi group, multi region and two dimensional (X, Y) adjoint equation. Typical reactor geometry is partitioned with triangular meshes and boundary condition for adjoint flux is considered zero. Finally, for a case of defined parameters, Finite Element Code was applied and results were compared with Citation Code

  4. [Principal component analysis and cluster analysis of inorganic elements in sea cucumber Apostichopus japonicus].

    Science.gov (United States)

    Liu, Xiao-Fang; Xue, Chang-Hu; Wang, Yu-Ming; Li, Zhao-Jie; Xue, Yong; Xu, Jie

    2011-11-01

    The present study is to investigate the feasibility of multi-elements analysis in determination of the geographical origin of sea cucumber Apostichopus japonicus, and to make choice of the effective tracers in sea cucumber Apostichopus japonicus geographical origin assessment. The content of the elements such as Al, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, As, Se, Mo, Cd, Hg and Pb in sea cucumber Apostichopus japonicus samples from seven places of geographical origin were determined by means of ICP-MS. The results were used for the development of elements database. Cluster analysis(CA) and principal component analysis (PCA) were applied to differentiate the sea cucumber Apostichopus japonicus geographical origin. Three principal components which accounted for over 89% of the total variance were extracted from the standardized data. The results of Q-type cluster analysis showed that the 26 samples could be clustered reasonably into five groups, the classification results were significantly associated with the marine distribution of the sea cucumber Apostichopus japonicus samples. The CA and PCA were the effective methods for elements analysis of sea cucumber Apostichopus japonicus samples. The content of the mineral elements in sea cucumber Apostichopus japonicus samples was good chemical descriptors for differentiating their geographical origins.

  5. Determination of multi-element in marine sediment samples collected in Angola by the k0-NAA technique

    International Nuclear Information System (INIS)

    Teixeira, M.C.P.; Ho Manh Dung; Cao Dong Vu; Nguyen Thi Sy; Nguyen Thanh Binh; Vuong Huu Tan

    2006-01-01

    The marine sediment samples were designed to collect in Angola for marine environmental pollution study. The k 0 -standardization method of neutron activation analysis (k 0 -NAA) on Dalat research reactor has been developed to determine of multi-element in the Angola marine sediment samples. The samples were irradiated in cell 7-1 for short- and middle-lived nuclides and rotary specimen rack for long-lived nuclides. The irradiation facilities were characterized for neutron spectrum parameters and post-activated samples were measured on the calibrated gamma-ray spectrometers using HPGe detectors. The analytical results for 9 marine sediment samples with 27 elements: Al, As, Br, Ca, Ce,Cl, Co, Cs, Dy, Fe, Hf, I, K, Mg, Mn, Na, Rb, Sb, Sc, Se, Sm, Th, Ti, U, V and Zn in term of mean concentration, standard deviation and their content range are shown in the report. The analytical quality assurance was done by analysis of a Japan's certified reference material namely marine sediment NMIJ-CRM-7302a. These preliminary results revealed that the k 0 -NAA technique on the Dalat research reactor is a good analytical technique for determination of multi-element in the marine sediment samples. Some heavy metals and trace elements determined in this work possibly connected to the human activities at the sampling region. (author)

  6. Multi-element analysis of urine using dynamic reaction cell inductively coupled plasma mass spectrometry (ICP-DRC-MS — A practical application

    Directory of Open Access Journals (Sweden)

    Renata Brodzka

    2013-04-01

    Full Text Available Objectives: The method for the determination of As, Al, Cd, Ni, Pb (toxic elements and Cr, Co, Cu, Fe, Mn, Zn (essential elements in human urine by the use of Inductively Coupled Plasma Mass Spectrometry (quadrupole ICP-MS DRCe Elan, Perkin Elmer with the dynamic reaction cell (DRC was developed. Materials and Methods: The method has been applied for multi-element analysis of the urine of 16 non-exposed healthy volunteers and 27 workers employed in a copper smelter. The analysis was conducted after initial 10-fold dilution of the urine samples with 0,1% nitric acid. Rhodium was used as an internal standard. The method validation parameters such as detection limit, sensitivity, precision were described for all elements. Accuracy of the method was checked by the regular use of certified reference materials ClinCheck®-Control Urine (Recipe as well as by participation of the laboratory in the German External Quality Assessment Scheme (G-EQUAS. Results: The detection limits (DL 3s of the applied method were 0.025, 0.007, 0.002, 0.004, 0.004, 0.086, 0.037, 0.009, 0.016, 0.008, 0.064 (μg/l for Al, As, Cd, Cr, Co, Cu, Fe, Mn, Ni, Pb, Zn in urine, respectively. For each element linearity with correlation coefficient of at least 0.999 was determined. Spectral interferences from some of the ions were removed using DRC-e with addition of alternative gas: methane for cobalt, copper, cadmium, chromium, iron, manganese, nickel and rhodium, and oxygen for arsenic. Conclusions: The developed method allows to determine simultaneously eleven elements in the urine with low detection limits, high sensitivity and good accuracy. Moreover, the method is appropriate for the assessment of both environmental and occupational exposure.

  7. SAFE-AXISYM, Stress Analysis of Axisymmetric Composite Structure by Finite Elements Method

    International Nuclear Information System (INIS)

    Cornell, D.C.

    1967-01-01

    1 - Nature of physical problem solved: SAFE-AXISYM is a program for the analysis of multi-material axisymmetric composite structures. It is designed for the analysis of heterogeneous structures such as reinforced and/or prestressed concrete vessels. The structure is assumed to be linearly elastic, and only bodies of revolution subjected to axisymmetric loading can be treated. 2 - Method of solution: SAFE-AXISYM uses a finite element method with a modified Gauss-Seidel iteration scheme. A reference grid subdivides the structure into ring-like small, finite elements, the vertices of which are called nodes. The grid may be generated by hand, by the computer or by a combination of the two methods. Each node has two degrees of freedom, translation in the and in the axial direction. Both zero and non-zero fixed displacement constraints may be assumed, and the loading condition may be mechanical and/or thermal. 3 - Restrictions on the complexity of the problem: Multi-material structures with varying rigidities converge very slowly. Not valid for incompressible materials. Maximum number of nodes = 475. Maximum number of elements = 1100

  8. Multi-element analysis of the rat hippocampus by proton induced x-ray emission spectroscopy (phosphorus, sulfur, chlorine, potassium, calcium, iron, zinc, copper, lead, bromine, and rubidium)

    Energy Technology Data Exchange (ETDEWEB)

    Kemp, K.; Danscher, G.

    1979-01-22

    A technique for multi-element analysis of brain tissue by proton induced x-ray emission spectroscopy (PIXE) is described and data from analysis of fixed and unfixed samples from rat hippocampus, neocortex, amygdala, and spinal cord are presented and commented on. The atoms present in the tissue are bombarded with protons which cause the ejection of electrons from the inner shells. When the holes are refilled with electrons from outer shells, x-ray quanta characteristic for each element are emitted. Using a high resolution energy dispersive detector, a complete x-ray spectrum of the specimen can be recorded in a single measurement. Detection limits less than or approximately 5 ppM of dry matter are obtained for most elements with atomic number greater than 14 (silicon). Around 13 elements were found in concentrations above the detection limits. The grand means for non-fixed hippocampi were e.g., for Zn-120 ppM; Rb-20 ppM; Fe-150 ppM; Pb-3 ppM; Ni-5 ppM.

  9. Statistical Methods in Assembly Quality Management of Multi-Element Products on Automatic Rotor Lines

    Science.gov (United States)

    Pries, V. V.; Proskuriakov, N. E.

    2018-04-01

    To control the assembly quality of multi-element mass-produced products on automatic rotor lines, control methods with operational feedback are required. However, due to possible failures in the operation of the devices and systems of automatic rotor line, there is always a real probability of getting defective (incomplete) products into the output process stream. Therefore, a continuous sampling control of the products completeness, based on the use of statistical methods, remains an important element in managing the quality of assembly of multi-element mass products on automatic rotor lines. The feature of continuous sampling control of the multi-element products completeness in the assembly process is its breaking sort, which excludes the possibility of returning component parts after sampling control to the process stream and leads to a decrease in the actual productivity of the assembly equipment. Therefore, the use of statistical procedures for continuous sampling control of the multi-element products completeness when assembled on automatic rotor lines requires the use of such sampling plans that ensure a minimum size of control samples. Comparison of the values of the limit of the average output defect level for the continuous sampling plan (CSP) and for the automated continuous sampling plan (ACSP) shows the possibility of providing lower limit values for the average output defects level using the ACSP-1. Also, the average sample size when using the ACSP-1 plan is less than when using the CSP-1 plan. Thus, the application of statistical methods in the assembly quality management of multi-element products on automatic rotor lines, involving the use of proposed plans and methods for continuous selective control, will allow to automating sampling control procedures and the required level of quality of assembled products while minimizing sample size.

  10. Measurements of environmental gamma-ray spectra using a multi-element TL dosemeter

    International Nuclear Information System (INIS)

    Furuta, Sadaaki; Boetter-Jensen, L.; Nielsen, S.P.

    1986-12-01

    A method to estimate the energy distribution and dose of environmental gamma radiation was developed using a multielement TL dosemeter. Experimentally obtained energy responses from a multi-element TL dosemeter with different kinds of filters were used to calculate the energy distribution and related dose by the SAND-II computer code. The code was originally developed to estimate the neutron flux using a multiple foil activation method. Measurements were made at several locations with the multi-element TL dosemeter and comparisons were made with results from a NaI(Tl) scintillation detector and a high-pressure ionization chamber. (author)

  11. Solving the Einstein constraint equations on multi-block triangulations using finite element methods

    Energy Technology Data Exchange (ETDEWEB)

    Korobkin, Oleg; Pazos, Enrique [Department of Physics and Astronomy, Louisiana State University, Baton Rouge, LA 70803 (United States); Aksoylu, Burak [Center for Computation and Technology, Louisiana State University, Baton Rouge, LA 70803 (United States); Holst, Michael [Department of Mathematics, University of California at San Diego 9500 Gilman Drive La Jolla, CA 92093-0112 (United States); Tiglio, Manuel [Department of Physics, University of Maryland, College Park, MD 20742 (United States)

    2009-07-21

    In order to generate initial data for nonlinear relativistic simulations, one needs to solve the Einstein constraints, which can be cast into a coupled set of nonlinear elliptic equations. Here we present an approach for solving these equations on three-dimensional multi-block domains using finite element methods. We illustrate our approach on a simple example of Brill wave initial data, with the constraints reducing to a single linear elliptic equation for the conformal factor psi. We use quadratic Lagrange elements on semi-structured simplicial meshes, obtained by triangulation of multi-block grids. In the case of uniform refinement the scheme is superconvergent at most mesh vertices, due to local symmetry of the finite element basis with respect to local spatial inversions. We show that in the superconvergent case subsequent unstructured mesh refinements do not improve the quality of our initial data. As proof of concept that this approach is feasible for generating multi-block initial data in three dimensions, after constructing the initial data we evolve them in time using a high-order finite-differencing multi-block approach and extract the gravitational waves from the numerical solution.

  12. Solving the Einstein constraint equations on multi-block triangulations using finite element methods

    International Nuclear Information System (INIS)

    Korobkin, Oleg; Pazos, Enrique; Aksoylu, Burak; Holst, Michael; Tiglio, Manuel

    2009-01-01

    In order to generate initial data for nonlinear relativistic simulations, one needs to solve the Einstein constraints, which can be cast into a coupled set of nonlinear elliptic equations. Here we present an approach for solving these equations on three-dimensional multi-block domains using finite element methods. We illustrate our approach on a simple example of Brill wave initial data, with the constraints reducing to a single linear elliptic equation for the conformal factor ψ. We use quadratic Lagrange elements on semi-structured simplicial meshes, obtained by triangulation of multi-block grids. In the case of uniform refinement the scheme is superconvergent at most mesh vertices, due to local symmetry of the finite element basis with respect to local spatial inversions. We show that in the superconvergent case subsequent unstructured mesh refinements do not improve the quality of our initial data. As proof of concept that this approach is feasible for generating multi-block initial data in three dimensions, after constructing the initial data we evolve them in time using a high-order finite-differencing multi-block approach and extract the gravitational waves from the numerical solution.

  13. MULTI ELEMENT SI SENSOR WITH READOUT ASIC FOR EXAFS SPECTROSCOPY.

    Energy Technology Data Exchange (ETDEWEB)

    DE GERONIMO,G.; O CONNOR,P.; BEUTTENMULLER,R.H.; LI,Z.; KUCZEWSKI,A.J.; SIDDONS,D.P.

    2002-09-09

    Extended X-ray Absorption Fine Structure (EXAFS) experiments impose stringent requirements on a detection system, due to the need for processing ionizing events at a high rate, typically above of 10Mcps/cm{sup 2}, and with a high resolution, typically better than 300eV. The detection system here presented is being developed targeting these stringent requirements. It is the result of a cooperation between the Instrumentation Division and the National Synchrotron Light Source (NSLS) of the Brookhaven National Laboratory (BNL). The system is composed of a multi-element Si sensor with dedicated per pixel electronics. The combination of high rate, high resolution and moderate complexity makes this system attractive when compared to other multi-element solutions. In sections 2, 3 and 4 the sensor, the interconnect and the electronics are briefly described. Section 5 reports on the first experimental results.

  14. Studies of the source complex behaviour and of the ultrasound radiation of contact flexible multi-element transducers; Etudes du comportement complexe de source et du rayonnement ultrasonore des traducteurs multi-elements flexibles au contact

    Energy Technology Data Exchange (ETDEWEB)

    Amory, V

    2007-12-15

    This work deals with the ultrasonic nondestructive testing of parts with complex geometries using soft multi-element sensors. The different types of contact control configurations are presented first. Then, the difficulties encountered with conventional contact transducers are explained and the multi-element piezoelectric transducers technology, developed to meet these difficulties, is presented. The second chapter presents the results of finite-element calculations showing the complexity of a transducer in a condition of testing utilization. In a same configuration, the radiated far field calculated by finite-elements is compared to the measurement in order to validate the way the source behaviour is calculated. However, despite the efficiency of the finite-elements simulation, this tool is numerically too costly and cannot be used to optimize a full multi-element transducer. Therefore, a realistic source model is built and implemented in a radiation code based on high-frequency asymptotic approximations where only L and T volume waves are calculated. The incapacity of this model to reproduce the behaviour of T waves in some directions of propagation has led to give a particular attention to the fore-waves, neglected in the radiation calculation. Chapter 3 treats of the building of an exact radiation model taking into consideration the fore-waves contribution emitted by a contact transducer exerting a random space-time distribution constraint at the surface of the considered medium. A radiation model, based on the calculation of exact Green functions of the Lamb problem is proposed. The exact model is particularly interesting in the case of sensor geometries with a long length with respect to other dimensions (2D case). Field calculation results are shown for an element of the matrix network (3D case) and for a linear element (2D case). A study of different existing approached models is carried out as well. The last chapter presents some results of the field

  15. Spectral response of multi-element silicon detectors

    Energy Technology Data Exchange (ETDEWEB)

    Ludewigt, B.A.; Rossington, C.S.; Chapman, K. [Univ. of California, Berkeley, CA (United States)

    1997-04-01

    Multi-element silicon strip detectors, in conjunction with integrated circuit pulse-processing electronics, offer an attractive alternative to conventional lithium-drifted silicon Si(Li) and high purity germanium detectors (HPGe) for high count rate, low noise synchrotron x-ray fluorescence applications. One of the major differences between the segmented Si detectors and the commercially available single-element Si(Li) or HPGe detectors is that hundreds of elements can be fabricated on a single Si substrate using standard silicon processing technologies. The segmentation of the detector substrate into many small elements results in very low noise performance at or near, room temperature, and the count rate of the detector is increased many-fold due to the multiplication in the total number of detectors. Traditionally, a single channel of detector with electronics can handle {approximately}100 kHz count rates while maintaining good energy resolution; the segmented detectors can operate at greater than MHz count rates merely due to the multiplication in the number of channels. One of the most critical aspects in the development of the segmented detectors is characterizing the charge sharing and charge loss that occur between the individual detector strips, and determining how these affect the spectral response of the detectors.

  16. MultiSIMNRA: A computational tool for self-consistent ion beam analysis using SIMNRA

    International Nuclear Information System (INIS)

    Silva, T.F.; Rodrigues, C.L.; Mayer, M.; Moro, M.V.; Trindade, G.F.; Aguirre, F.R.; Added, N.; Rizzutto, M.A.; Tabacniks, M.H.

    2016-01-01

    Highlights: • MultiSIMNRA enables the self-consistent analysis of multiple ion beam techniques. • Self-consistent analysis enables unequivocal and reliable modeling of the sample. • Four different computational algorithms available for model optimizations. • Definition of constraints enables to include prior knowledge into the analysis. - Abstract: SIMNRA is widely adopted by the scientific community of ion beam analysis for the simulation and interpretation of nuclear scattering techniques for material characterization. Taking advantage of its recognized reliability and quality of the simulations, we developed a computer program that uses multiple parallel sessions of SIMNRA to perform self-consistent analysis of data obtained by different ion beam techniques or in different experimental conditions of a given sample. In this paper, we present a result using MultiSIMNRA for a self-consistent multi-elemental analysis of a thin film produced by magnetron sputtering. The results demonstrate the potentialities of the self-consistent analysis and its feasibility using MultiSIMNRA.

  17. A framework for developing finite element codes for multi-disciplinary applications.

    OpenAIRE

    Dadvand, Pooyan

    2007-01-01

    The world of computing simulation has experienced great progresses in recent years and requires more exigent multidisciplinary challenges to satisfy the new upcoming demands. Increasing the importance of solving multi-disciplinary problems makes developers put more attention to these problems and deal with difficulties involved in developing software in this area. Conventional finite element codes have several difficulties in dealing with multi-disciplinary problems. Many of these codes are d...

  18. Process recognition in multi-element soil and stream-sediment geochemical data

    Science.gov (United States)

    Grunsky, E.C.; Drew, L.J.; Sutphin, D.M.

    2009-01-01

    Stream-sediment and soil geochemical data from the Upper and Lower Coastal Plains of South Carolina (USA) were studied to determine relationships between soils and stream sediments. From multi-element associations, characteristic compositions were determined for both media. Primary associations of elements reflect mineralogy, including heavy minerals, carbonates and clays, and the effects of groundwater. The effects of groundwater on element concentrations are more evident in soils than stream sediments. A "winnowing index" was created using ratios of Th to Al that revealed differing erosional and depositional environments. Both soils and stream sediments from the Upper and Lower Coastal Plains show derivation from similar materials and subsequent similar multi-element relationships, but have some distinct differences. In the Lower Coastal Plain, soils have high values of elements concentrated in heavy minerals (Ce, Y, Th) that grade into high values of elements concentrated into finer-grain-size, lower-density materials, primarily comprised of carbonates and feldspar minerals (Mg, Ca, Na, K, Al). These gradational trends in mineralogy and geochemistry are inferred to reflect reworking of materials during marine transgressions and regressions. Upper Coastal Plain stream-sediment geochemistry shows a higher winnowing index relative to soil geochemistry. A comparison of the 4 media (Upper Coastal Plain soils and stream sediments and Lower Coastal Plain soils and stream sediments) shows that Upper Coastal Plain stream sediments have a higher winnowing index and a higher concentration of elements contained within heavy minerals, whereas Lower Coastal Plain stream sediments show a strong correlation between elements typically contained within clays. It is not possible to calculate a functional relationship between stream sediment-soil compositions for all elements due to the complex history of weathering, deposition, reworking and re-deposition. However, depending on

  19. Grammar-Based Multi-Frontal Solver for One Dimensional Isogeometric Analysis with Multiple Right-Hand-Sides

    KAUST Repository

    Kuźnik, Krzysztof

    2013-06-01

    This paper introduces a grammar-based model for developing a multi-thread multi-frontal parallel direct solver for one- dimensional isogeometric finite element method. The model includes the integration of B-splines for construction of the element local matrices and the multi-frontal solver algorithm. The integration and the solver algorithm are partitioned into basic indivisible tasks, namely the grammar productions, that can be executed squentially. The partial order of execution of the basic tasks is analyzed to provide the scheduling for the execution of the concurrent integration and multi-frontal solver algo- rithm. This graph grammar analysis allows for optimal concurrent execution of all tasks. The model has been implemented and tested on NVIDIA CUDA GPU, delivering logarithmic execution time for linear, quadratic, cubic and higher order B-splines. Thus, the CUDA implementation delivers the optimal performance predicted by our graph grammar analysis. We utilize the solver for multiple right hand sides related to the solution of non-stationary or inverse problems.

  20. An analysis of the electromagnetic field in multi-polar linear induction system

    International Nuclear Information System (INIS)

    Chervenkova, Todorka; Chervenkov, Atanas

    2002-01-01

    In this paper a new method for determination of the electromagnetic field vectors in a multi-polar linear induction system (LIS) is described. The analysis of the electromagnetic field has been done by four dimensional electromagnetic potentials in conjunction with theory of the magnetic loops . The electromagnetic field vectors are determined in the Minkovski's space as elements of the Maxwell's tensor. The results obtained are compared with those got from the analysis made by the finite elements method (FEM).With the method represented in this paper one can determine the electromagnetic field vectors in the multi-polar linear induction system using four-dimensional potential. A priority of this method is the obtaining of analytical results for the electromagnetic field vectors. These results are also valid for linear media. The dependencies are valid also at high speeds of movement. The results of the investigated linear induction system are comparable to those got by the finite elements method. The investigations may be continued in the determination of other characteristics such as drag force, levitation force, etc. The method proposed in this paper for an analysis of linear induction system can be used for optimization calculations. (Author)

  1. Studies on absorption coefficient near edge of multi elements

    International Nuclear Information System (INIS)

    Eisa, M.H.; Shen, H.; Yao, H.Y.; Mi, Y.; Zhou, Z.Y.; Hu, T.D.; Xie, Y.N.

    2005-01-01

    X-ray absorption near edge structure (XANES) was used to study the near edge mass-absorption coefficients of seven elements, such as, Ti, V, Fe, Co, Ni, Cu and Zn. It is well known that, on the near edge absorption of element, when incident X-ray a few eV change can make the absorption coefficient an order magnitude alteration. So that, there are only a few points mass-absorption coefficient at the near edge absorption and that always average value in published table. Our results showed a wide range of data, the total measured data of mass-absorption coefficient of the seven elements was about 505. The investigation confirmed that XANES is useful technique for multi-element absorption coefficient measurement. Details of experimental methods and results are given and discussed. The experimental work has been performed at Beijing Synchrotron Radiation Facility. The measured values were compared with the published data. Good agreement between experimental results and published data is obtained

  2. Studies on absorption coefficient near edge of multi elements

    Science.gov (United States)

    Eisa, M. H.; Shen, H.; Yao, H. Y.; Mi, Y.; Zhou, Z. Y.; Hu, T. D.; Xie, Y. N.

    2005-12-01

    X-ray absorption near edge structure (XANES) was used to study the near edge mass-absorption coefficients of seven elements, such as, Ti, V, Fe, Co, Ni, Cu and Zn. It is well known that, on the near edge absorption of element, when incident X-ray a few eV change can make the absorption coefficient an order magnitude alteration. So that, there are only a few points mass-absorption coefficient at the near edge absorption and that always average value in published table. Our results showed a wide range of data, the total measured data of mass-absorption coefficient of the seven elements was about 505. The investigation confirmed that XANES is useful technique for multi-element absorption coefficient measurement. Details of experimental methods and results are given and discussed. The experimental work has been performed at Beijing Synchrotron Radiation Facility. The measured values were compared with the published data. Good agreement between experimental results and published data is obtained.

  3. Analysis and synthesis of multi-qubit, multi-mode quantum devices

    Energy Technology Data Exchange (ETDEWEB)

    Solgun, Firat

    2015-03-27

    In this thesis we propose new methods in multi-qubit multi-mode circuit quantum electrodynamics (circuit-QED) architectures. First we describe a direct parity measurement method for three qubits, which can be realized in 2D circuit-QED with a possible extension to four qubits in a 3D circuit-QED setup for the implementation of the surface code. In Chapter 3 we show how to derive Hamiltonians and compute relaxation rates of the multi-mode superconducting microwave circuits consisting of single Josephson junctions using an exact impedance synthesis technique (the Brune synthesis) and applying previous formalisms for lumped element circuit quantization. In the rest of the thesis we extend our method to multi-junction (multi-qubit) multi-mode circuits through the use of state-space descriptions which allows us to quantize any multiport microwave superconducting circuit with a reciprocal lossy impedance response.

  4. Elemental analysis of Oum er Rbia Moroccan river-water using TXRF

    International Nuclear Information System (INIS)

    Zahry, F.; Bounakhla, M.; El Hamdaoui, A.; Labraimi, M.

    2000-01-01

    The x-ray fluorescence analysis of water and suspended particulate matter (SPM) from Oum er Rbia Moroccan river for the content of 17 elements has been performed utilizing the energy dispersive x-ray fluorescence spectrometer and total reflection excitation. SPM samples were dissolved in nitric acid. For all samples direct measurements are feasible by spiking a few ml of the sample with Ga as internal standard element, and drying an aliquot of 20 μl on a quartz glass carrier. The detection limits of 10 to 20 ppb are sufficient for most of the elements to be determined. Results were assessed for accuracy by the analysis of the 15474 ICP multi-elemental standard I. Some results were also compared with AAS and ICP-AES. The results for most of the elements obtained by TXRF were accurate to about 2-15 %. The objectives of the analysis were to determine the geo-chemical areas on this river, to explain the mechanism of sediment transport and to assess the pollution of the river by human activities. 36 samples had been collected along the river between its source in Middle Atlas and the Atlantic ocean at Azemour city. (author)

  5. Finite element method for radiation heat transfer in multi-dimensional graded index medium

    International Nuclear Information System (INIS)

    Liu, L.H.; Zhang, L.; Tan, H.P.

    2006-01-01

    In graded index medium, ray goes along a curved path determined by Fermat principle, and curved ray-tracing is very difficult and complex. To avoid the complicated and time-consuming computation of curved ray trajectories, a finite element method based on discrete ordinate equation is developed to solve the radiative transfer problem in a multi-dimensional semitransparent graded index medium. Two particular test problems of radiative transfer are taken as examples to verify this finite element method. The predicted dimensionless net radiative heat fluxes are determined by the proposed method and compared with the results obtained by finite volume method. The results show that the finite element method presented in this paper has a good accuracy in solving the multi-dimensional radiative transfer problem in semitransparent graded index medium

  6. ED-XRF spectrometric analysis of comparative elemental composition of in vivo and in vitro roots of Andrographis paniculata (Burm.f.) Wall. ex Nees-a multi-medicinal herb

    Energy Technology Data Exchange (ETDEWEB)

    Behera, P.R., E-mail: priyaranjan2004@gmail.co [Plant Cell and Tissue culture Facility, Post-Graduate Department of Botany, Utkal University, Vani Vihar, Bhubaneswar 751004, Orissa (India); Plant Biotechnology Lab, Institute of Minerals and Materials Technology (CSIR), Bhubaneswar 751013, Orissa (India); Nayak, P [Plant Cell and Tissue culture Facility, Post-Graduate Department of Botany, Utkal University, Vani Vihar, Bhubaneswar 751004, Orissa (India); Plant Biotechnology Lab, Institute of Minerals and Materials Technology (CSIR), Bhubaneswar 751013, Orissa (India); Barik, D.P., E-mail: barikdp@yahoo.co [Plant Cell and Tissue culture Facility, Post-Graduate Department of Botany, Utkal University, Vani Vihar, Bhubaneswar 751004, Orissa (India); Rautray, T.R., E-mail: trrautray@gmail.co [Ion Beam Laboratory, Institute of Physics, Bhubaneswar 751013, Orissa (India); Thirunavoukkarasu, M [Plant Biotechnology Lab, Institute of Minerals and Materials Technology (CSIR), Bhubaneswar 751013, Orissa (India); Chand, P.K., E-mail: pkchanduubot@yahoo.co.i [Plant Cell and Tissue culture Facility, Post-Graduate Department of Botany, Utkal University, Vani Vihar, Bhubaneswar 751004, Orissa (India)

    2010-12-15

    The multi-elemental composition of in vitro-proliferated root tissues of Andrographis paniculata (Burm.f.) Wall. ex Nees was compared with that of the naturally grown in vivo plants. Trace elements namely Cr, Mn, Fe, Co, Ni, Cu, Zn, Se, Rb, Sr and Pb in addition to two macro-elements K and Ca were identified and quantified in root tissues of both sources using the energy dispersive X-ray fluorescence (ED-XRF) technique. ED-XRF analysis was performed using Mo K X-rays generated from a secondary molybdenum target. The elemental content of in vitro roots was found to be at par with that of naturally grown plants of the same species. This opens up a possibility of exploiting in vitro root cultures as a viable, alternative and renewable source of phytochemicals of relevance, besides providing a means for conservation of the valuable natural resources.

  7. ED-XRF spectrometric analysis of comparative elemental composition of in vivo and in vitro roots of Andrographis paniculata (Burm.f.) Wall. ex Nees-a multi-medicinal herb

    International Nuclear Information System (INIS)

    Behera, P.R.; Nayak, P.; Barik, D.P.; Rautray, T.R.; Thirunavoukkarasu, M.; Chand, P.K.

    2010-01-01

    The multi-elemental composition of in vitro-proliferated root tissues of Andrographis paniculata (Burm.f.) Wall. ex Nees was compared with that of the naturally grown in vivo plants. Trace elements namely Cr, Mn, Fe, Co, Ni, Cu, Zn, Se, Rb, Sr and Pb in addition to two macro-elements K and Ca were identified and quantified in root tissues of both sources using the energy dispersive X-ray fluorescence (ED-XRF) technique. ED-XRF analysis was performed using Mo K X-rays generated from a secondary molybdenum target. The elemental content of in vitro roots was found to be at par with that of naturally grown plants of the same species. This opens up a possibility of exploiting in vitro root cultures as a viable, alternative and renewable source of phytochemicals of relevance, besides providing a means for conservation of the valuable natural resources.

  8. Development of Multi-Scale Finite Element Analysis Codes for High Formability Sheet Metal Generation

    International Nuclear Information System (INIS)

    Nnakamachi, Eiji; Kuramae, Hiroyuki; Ngoc Tam, Nguyen; Nakamura, Yasunori; Sakamoto, Hidetoshi; Morimoto, Hideo

    2007-01-01

    In this study, the dynamic- and static-explicit multi-scale finite element (F.E.) codes are developed by employing the homogenization method, the crystalplasticity constitutive equation and SEM-EBSD measurement based polycrystal model. These can predict the crystal morphological change and the hardening evolution at the micro level, and the macroscopic plastic anisotropy evolution. These codes are applied to analyze the asymmetrical rolling process, which is introduced to control the crystal texture of the sheet metal for generating a high formability sheet metal. These codes can predict the yield surface and the sheet formability by analyzing the strain path dependent yield, the simple sheet forming process, such as the limit dome height test and the cylindrical deep drawing problems. It shows that the shear dominant rolling process, such as the asymmetric rolling, generates ''high formability'' textures and eventually the high formability sheet. The texture evolution and the high formability of the newly generated sheet metal experimentally were confirmed by the SEM-EBSD measurement and LDH test. It is concluded that these explicit type crystallographic homogenized multi-scale F.E. code could be a comprehensive tool to predict the plastic induced texture evolution, anisotropy and formability by the rolling process and the limit dome height test analyses

  9. Synthetic multi-element standards: a good tool for calibration and quality control of irradiation facilities used for neutron activation analysis

    International Nuclear Information System (INIS)

    Vermaercke, P.

    2007-01-01

    determined by the nuclear cross sections. The cross sections depend on the neutron energy E and also these physical properties are parameterised in the k0-NAA method resulting in the so-called k0-factors for each element and for the different isotopes of an element. The quantification of an element then involves the use of a ratio of k0-factors in which one k0-factor is the one for 198Au. In practice, ratios of k0-factors accounting for the energy spectrum of the neutrons (f, a) are used in an analysis. These ratios are called the comparator factor FC. It is clear that the quality assurance of the k0-NAA method requires the control of the parameters f and a for each irradiation of samples. This is generally realised by using several flux monitors e.g. a set of Zr and Au monitors which are co-irradiated with the samples to analyse. However, this approach is quite labour intensive and recently we started investigating an approach based on co-irradiation of Synthetic Multi-Element Standards (SMELS) for this purpose. SMELS contain different elements in known concentrations, and three types of materials exist: Type I (elements forming short-lived radionuclides), Type II (elements forming medium lived radionuclides) and Type III (elements forming long lived radionuclides). Au was added to all three SMELS types and Zr in type III. The objectives are to optimise the ratio of quality of analysis to workload by appropriate quality control methods to determine and monitor the irradiation parameters (f, a) using SMELS and to set up a Quality Control (QC) system for the complete measurement and analysis process for k0-NAA

  10. Applications of X-ray emission to elemental analysis of foods

    International Nuclear Information System (INIS)

    Flocchini, R.G.; Lagunas-Solar, M.C.; Perley, B.P.

    1996-01-01

    Trace element analysis via X-Ray Fluorescence (XRF) and Proton-Induced X-Ray Emission (PIXE) techniques were applied to several samples of fresh and processed foods. Thin samples of fresh fruits and vegetables, processed dry foods, and spices were included in these analyses. The results indicate that XRF and/or PIXE analysis is applicable to these types of samples but require special and simple modifications in sample preparation techniques, and the inclusion of new matrix type corrections for data analysis. However, the non-destructive nature, reproducibility, efficiency and high sensitivity that characterize these multi-element analytical procedures can provide new potential methods for detecting trace elements in foods and in many agricultural commodities. Toxic metals such as Hg, Pb, and As were detected in some foods. In addition, other essential or neutral trace elements such as Na, K, Mg, Ca, Cu, Cr, V, Zn, Mo, Fe, Mn, Ni, Se, Cl, S, and P were also detected. These and other elements can be analyzed rapidly and with high sensitivity for applications in process control and for certification of food quality. Developing these techniques and procedures specifically for food and for various agricultural products may provide new analytical options and help mitigate the expected impact of forthcoming regulations intended to establish limits and tolerance levels for micro toxicants and other essential nutrients in foods and agricultural products. (author)

  11. A full-spectrum analysis of high-speed train interior noise under multi-physical-field coupling excitations

    Science.gov (United States)

    Zheng, Xu; Hao, Zhiyong; Wang, Xu; Mao, Jie

    2016-06-01

    High-speed-railway-train interior noise at low, medium, and high frequencies could be simulated by finite element analysis (FEA) or boundary element analysis (BEA), hybrid finite element analysis-statistical energy analysis (FEA-SEA) and statistical energy analysis (SEA), respectively. First, a new method named statistical acoustic energy flow (SAEF) is proposed, which can be applied to the full-spectrum HST interior noise simulation (including low, medium, and high frequencies) with only one model. In an SAEF model, the corresponding multi-physical-field coupling excitations are firstly fully considered and coupled to excite the interior noise. The interior noise attenuated by sound insulation panels of carriage is simulated through modeling the inflow acoustic energy from the exterior excitations into the interior acoustic cavities. Rigid multi-body dynamics, fast multi-pole BEA, and large-eddy simulation with indirect boundary element analysis are first employed to extract the multi-physical-field excitations, which include the wheel-rail interaction forces/secondary suspension forces, the wheel-rail rolling noise, and aerodynamic noise, respectively. All the peak values and their frequency bands of the simulated acoustic excitations are validated with those from the noise source identification test. Besides, the measured equipment noise inside equipment compartment is used as one of the excitation sources which contribute to the interior noise. Second, a full-trimmed FE carriage model is firstly constructed, and the simulated modal shapes and frequencies agree well with the measured ones, which has validated the global FE carriage model as well as the local FE models of the aluminum alloy-trim composite panel. Thus, the sound transmission loss model of any composite panel has indirectly been validated. Finally, the SAEF model of the carriage is constructed based on the accurate FE model and stimulated by the multi-physical-field excitations. The results show

  12. Finite element modeling of temperature load effects on the vibration of local modes in multi-cable structures

    Science.gov (United States)

    Treyssède, Fabien

    2018-01-01

    Understanding thermal effects on the vibration of local (cable-dominant) modes in multi-cable structures is a complicated task. The main difficulty lies in the modification by temperature change of cable tensions, which are then undetermined. This paper applies a finite element procedure to investigate the effects of thermal loads on the linear dynamics of prestressed self-weighted multi-cable structures. Provided that boundary conditions are carefully handled, the discretization of cables with nonlinear curved beam elements can properly represent the thermoelastic behavior of cables as well as their linearized dynamics. A three-step procedure that aims to replace applied pretension forces with displacement continuity conditions is used. Despite an increase in the computational cost related to beam rotational degrees of freedom, such an approach has several advantages. Nonlinear beam finite elements are usually available in commercial codes. The overall method follows a thermoelastic geometrically non-linear analysis and hereby includes the main sources of non-linearities in multi-cable structures. The effects of cable bending stiffness, which can be significant, are also naturally accounted for. The accuracy of the numerical approach is assessed thanks to an analytical model for the vibration of a single inclined cable under temperature change. Then, the effects of thermal loads are investigated for two cable bridges, highlighting how natural frequencies can be affected by temperature. Although counterintuitive, a reverse relative change of natural frequency may occur for certain local modes. This phenomenon can be explained by two distinct mechanisms, one related to the physics intrinsic to cables and the other related to the thermal deflection of the superstructure. Numerical results show that cables cannot be isolated from the rest of the structure and the importance of modeling the whole structure for a quantitative analysis of temperature effects on the

  13. A 3D analysis of reinforced concrete structures by the finite element method

    International Nuclear Information System (INIS)

    Claure, J.D.; Campos Filho, A.

    1995-01-01

    Fundamental features of a computational model, based on the finite element methods, for the analysis of concrete structure are presented. The study comprehends short and long-term loading situations, where creep and shrinkage in concrete are considered. The reinforcement is inserted in the finite element model using an embedded model. A smeared crack model is used for the concrete cracking, which considers the contribution of concrete between cracks and allows the closing the cracks closing. The computational code MPGS (Multi-Purpose Graphic System) is used, to make easy the analysis and interpretation of the numeric results. (author). 8 refs., 4 figs

  14. Elemental analysis of oum er rbia moroccan river-water Using icp-aes and chromatography

    International Nuclear Information System (INIS)

    Zahry, F.; Bounakhla, M.; Labraimi, M.; Moutte, J.; Bilal, E.

    2001-01-01

    The analysis of water and suspended particulate matter (SPM) from Oum er Rbia Moroccan river for the content of 22 elements has been performed utilizing ICP-AES and chromatography methods. MPS samples were dissolved in nitric acid. The element analyzed are : Na, Mg, Al, Si, P, S, Cl, K, Ca, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Br, Ba and Pb. The detection limits are sufficient for most of the elements to be determined. Results were assessed for the accuracy by the analysis of a multi-elemental standard. The results for most of the elements obtained were accurate to about 2-15%. The objective of the analysis were to determine the geochemical areas on this river, to explain the mechanisms of sediment transport and nevertheless, to assess the pollution of the river by human activities. 48 samples were collected along the river, between its source in meddle atlas and the Atlantic ocean at Azemour city

  15. Elemental analysis of bronze artifacts by muonic X-ray spectroscopy

    International Nuclear Information System (INIS)

    Ninomiya, Kazuhiko; Shinohara, Atsushi; Kubo, Michael K.; Strasser, Patrick; Nagatomo, Takashi; Kawamura, Naritoshi; Shimomura, Koichiro; Miyake, Yasuhiro; Kobayashi, Yoshio; Ishida, Katsuhiko; Higemoto, Wataru; Suzuki, Takao; Saito, Tsutomu

    2015-01-01

    A quantitative and multi-elemental analysis method for bulk samples based on muonic X-ray spectroscopy was applied to bronze artifacts (Tempo-Tsuho coins and a Seiun-kyo mirror). This method is based on the measurement of the characteristic high-energy muonic X-rays emitted in a sample after muon irradiation. The elemental compositions of these bronze artifacts were determined from muonic X-ray intensities in a non-destructive manner, using the relation between the muonic X-ray intensity and the elemental composition of the Cu–Sn–Pb alloy system. The analyzed values agreed well with those determined by X-ray fluorescence spectroscopy. We also estimated the detection limit of this method in the present experimental setup as 0.81 wt% of the background signal of the muonic X-ray spectra. (author)

  16. Analysis of oil shale and oil shale products for certain minor elements

    International Nuclear Information System (INIS)

    Dickman, P.T.; Purdy, M.; Doerges, J.E.; Ryan, V.A.; Poulson, R.E.

    1977-01-01

    The University of Wyoming was contracted by the Department of Energy's Laramie Energy Research Center (LERC) to develop rapid, inexpensive, and simple methods of quantitative and qualitative elemental analysis for products used and generated in the simulated in-situ retorting of oil shale. Alpha particle spectrometry was used to determine the radioisotope content of the aqueous retort products. Alpha particles are mono-energetic and the spectrometry method employed had very low background levels (1 count per 2000 seconds). These factors allow for both the quantitative and qualitative analysis of natural radioisotopes at the 1 ppm level. Sample preparation does not require any chemical treatment. Energy dispersive x-ray fluorescence (XRF) was used for the multi-element analysis of the retort products. The XRF, integrated with a mini-computer, allows rapid analysis of several elements in multiple samples. XRF samples require minimal amounts of preparation and analytical results are highly reproducible. This paper presents the methods developed and preliminary analytical results from oil shale by-products. Results from the analysis of oil shale rocks are not yet ready for presentation

  17. Limitation of multi-elemental fingerprinting of wheat grains: Effect of cultivar, sowing date, and nutrient management

    DEFF Research Database (Denmark)

    Suarez-Tapia, Alfonso; Kucheryavskiy, Sergey V.; Christensen, Bent Tolstrup

    2017-01-01

    Multi-element fingerprinting demonstrates some potential for tracing the origin of agricultural products but not for discriminating among crop cultivars and nutrient management (source, rate). With principal component analysis (PCA) and univariate statistics, we examined 19 elements in grains from...... two winter wheat cultivars (Hereford, Mariboss) grown with different rates of animal manure (AM) or mineral fertilisers (NPK) in a long-term field experiment and two sowing dates (early, timely). Nitrogen, Cd and Mn related to NPK, and Mo and Na to AM. Barium, Fe, and P reflected nutrient rate......; these elements increased with nutrient rate regardless of source. Unmanured grains were enriched in Cu. Mariboss was characterized by higher concentrations of Sr, Ba and Sc compared to Hereford with Sr in grain as the main separator. Univariate statistics showed higher concentrations of N, P, Mg, Ba, Cu, Mo...

  18. Multi-elemental characterization of Cuban natural zeolites

    International Nuclear Information System (INIS)

    Diaz Rizo, O.; Herrera Peraza, E.F.

    1996-01-01

    Concentrations of 38 elements in samples from four important Cuban zeolite bed have beam obtained by Instrumental Neutron Activation (INAA) and X-Ray Fluorescence Analysis (XRFA). In comparison with other analytical techniques good agreement was achieved. The concentration values of minor element Ba, Sr, Zn, and Mn, and 25 trace element (including 9 REE) are at the first time reported in Cuban zeolite. It is important for the zeolite evaluation in different industrial uses

  19. Multi-element proportional counter for radiation protection measurements

    International Nuclear Information System (INIS)

    Kliauga, P.; Rossi, H.H.; Johnson, G.

    1988-01-01

    This article discusses design modifications of a multi-element proportional counter. The original counter exhibited poor resolution, as measured by the width of the event-size spectrum for low-energy photons. It was also suspected that the field inside each volume was not sufficiently symmetric. Results of the modifications showed that a dramatic improvement in resolution could be obtained in the chamber with tissue-equivalent septa if their potentials were adjusted to obtain optimal resolution. The full width at half maximum then approached, although it did not equal, that of a standard spherical counter

  20. Fast sequential multi-element determination of major and minor elements in environmental samples and drinking waters by high-resolution continuum source flame atomic absorption spectrometry.

    Science.gov (United States)

    Gómez-Nieto, Beatriz; Gismera, Ma Jesús; Sevilla, Ma Teresa; Procopio, Jesús R

    2015-01-07

    The fast sequential multi-element determination of 11 elements present at different concentration levels in environmental samples and drinking waters has been investigated using high-resolution continuum source flame atomic absorption spectrometry. The main lines for Cu (324.754 nm), Zn (213.857 nm), Cd (228.802 nm), Ni (232.003 nm) and Pb (217.001 nm), main and secondary absorption lines for Mn (279.482 and 279.827 nm), Fe (248.327, 248.514 and 302.064 nm) and Ca (422.673 and 239.856 nm), secondary lines with different sensitivities for Na (589.592 and 330.237 nm) and K (769.897 and 404.414 nm) and a secondary line for Mg (202.582 nm) have been chosen to perform the analysis. A flow injection system has been used for sample introduction so sample consumption has been reduced up to less than 1 mL per element, measured in triplicate. Furthermore, the use of multiplets for Fe and the side pixel registration approach for Mg have been studied in order to reduce sensitivity and extend the linear working range. The figures of merit have been calculated and the proposed method was applied to determine these elements in a pine needles reference material (SRM 1575a), drinking and natural waters and soil extracts. Recoveries of analytes added at different concentration levels to water samples and extracts of soils were within 88-115% interval. In this way, the fast sequential multi-element determination of major and minor elements can be carried out, in triplicate, with successful results without requiring additional dilutions of samples or several different strategies for sample preparation using about 8-9 mL of sample. Copyright © 2014 Elsevier B.V. All rights reserved.

  1. Studies of the source complex behaviour and of the ultrasound radiation of contact flexible multi-element transducers

    International Nuclear Information System (INIS)

    Amory, V.

    2007-12-01

    This work deals with the ultrasonic nondestructive testing of parts with complex geometries using soft multi-element sensors. The different types of contact control configurations are presented first. Then, the difficulties encountered with conventional contact transducers are explained and the multi-element piezoelectric transducers technology, developed to meet these difficulties, is presented. The second chapter presents the results of finite-element calculations showing the complexity of a transducer in a condition of testing utilization. In a same configuration, the radiated far field calculated by finite-elements is compared to the measurement in order to validate the way the source behaviour is calculated. However, despite the efficiency of the finite-elements simulation, this tool is numerically too costly and cannot be used to optimize a full multi-element transducer. Therefore, a realistic source model is built and implemented in a radiation code based on high-frequency asymptotic approximations where only L and T volume waves are calculated. The incapacity of this model to reproduce the behaviour of T waves in some directions of propagation has led to give a particular attention to the fore-waves, neglected in the radiation calculation. Chapter 3 treats of the building of an exact radiation model taking into consideration the fore-waves contribution emitted by a contact transducer exerting a random space-time distribution constraint at the surface of the considered medium. A radiation model, based on the calculation of exact Green functions of the Lamb problem is proposed. The exact model is particularly interesting in the case of sensor geometries with a long length with respect to other dimensions (2D case). Field calculation results are shown for an element of the matrix network (3D case) and for a linear element (2D case). A study of different existing approached models is carried out as well. The last chapter presents some results of the field

  2. Finite element analysis of degraded concrete structures - Workshop proceedings

    International Nuclear Information System (INIS)

    1999-09-01

    This workshop is related to the finite element analysis of degraded concrete structures. It is composed of three sessions. The first session (which title is: the use of finite element analysis in safety assessments) comprises six papers which titles are: Historical Development of Concrete Finite Element Modeling for Safety Evaluation of Accident-Challenged and Aging Concrete Structures; Experience with Finite Element Methods for Safety Assessments in Switzerland; Stress State Analysis of the Ignalina NPP Confinement System; Prestressed Containment: Behaviour when Concrete Cracking is Modelled; Application of FEA for Design and Support of NPP Containment in Russia; Verification Problems of Nuclear Installations Safety Software of Strength Analysis (NISS SA). The second session (title: concrete containment structures under accident loads) comprises seven papers which titles are: Two Application Examples of Concrete Containment Structures under Accident Load Conditions Using Finite Element Analysis; What Kind of Prediction for Leak rates for Nuclear Power Plant Containments in Accidental Conditions; Influence of Different Hypotheses Used in Numerical Models for Concrete At Elevated Temperatures on the Predicted Behaviour of NPP Core Catchers Under Severe Accident Conditions; Observations on the Constitutive Modeling of Concrete Under Multi-Axial States at Elevated Temperatures; Analyses of a Reinforced Concrete Containment with Liner Corrosion Damage; Program of Containment Concrete Control During Operation for the Temelin Nuclear Power Plant; Static Limit Load of a Deteriorated Hyperbolic Cooling Tower. The third session (concrete structures under extreme environmental load) comprised five papers which titles are: Shear Transfer Mechanism of RC Plates After Cracking; Seismic Back Calculation of an Auxiliary Building of the Nuclear Power Plant Muehleberg, Switzerland; Seismic Behaviour of Slightly Reinforced Shear Wall Structures; FE Analysis of Degraded Concrete

  3. Modelling optimization involving different types of elements in finite element analysis

    International Nuclear Information System (INIS)

    Wai, C M; Rivai, Ahmad; Bapokutty, Omar

    2013-01-01

    Finite elements are used to express the mechanical behaviour of a structure in finite element analysis. Therefore, the selection of the elements determines the quality of the analysis. The aim of this paper is to compare and contrast 1D element, 2D element, and 3D element used in finite element analysis. A simple case study was carried out on a standard W460x74 I-beam. The I-beam was modelled and analyzed statically with 1D elements, 2D elements and 3D elements. The results for the three separate finite element models were compared in terms of stresses, deformation and displacement of the I-beam. All three finite element models yield satisfactory results with acceptable errors. The advantages and limitations of these elements are discussed. 1D elements offer simplicity although lacking in their ability to model complicated geometry. 2D elements and 3D elements provide more detail yet sophisticated results which require more time and computer memory in the modelling process. It is also found that the choice of element in finite element analysis is influence by a few factors such as the geometry of the structure, desired analysis results, and the capability of the computer

  4. A multi-element cosmological model with a complex space-time topology

    Science.gov (United States)

    Kardashev, N. S.; Lipatova, L. N.; Novikov, I. D.; Shatskiy, A. A.

    2015-02-01

    Wormhole models with a complex topology having one entrance and two exits into the same space-time of another universe are considered, as well as models with two entrances from the same space-time and one exit to another universe. These models are used to build a model of a multi-sheeted universe (a multi-element model of the "Multiverse") with a complex topology. Spherical symmetry is assumed in all the models. A Reissner-Norström black-hole model having no singularity beyond the horizon is constructed. The strength of the central singularity of the black hole is analyzed.

  5. Finite Macro-Element Mesh Deformation in a Structured Multi-Block Navier-Stokes Code

    Science.gov (United States)

    Bartels, Robert E.

    2005-01-01

    A mesh deformation scheme is developed for a structured multi-block Navier-Stokes code consisting of two steps. The first step is a finite element solution of either user defined or automatically generated macro-elements. Macro-elements are hexagonal finite elements created from a subset of points from the full mesh. When assembled, the finite element system spans the complete flow domain. Macro-element moduli vary according to the distance to the nearest surface, resulting in extremely stiff elements near a moving surface and very pliable elements away from boundaries. Solution of the finite element system for the imposed boundary deflections generally produces smoothly varying nodal deflections. The manner in which distance to the nearest surface has been found to critically influence the quality of the element deformation. The second step is a transfinite interpolation which distributes the macro-element nodal deflections to the remaining fluid mesh points. The scheme is demonstrated for several two-dimensional applications.

  6. Costs of Quality: Exploratory Analysis of Hidden Elements and Prioritization using Analytic Hierarchy Process

    Directory of Open Access Journals (Sweden)

    Sailaja A

    2015-02-01

    Full Text Available Cost of Quality analysis is emerged as an effective tool for the industrial managers for pinpointing the deficiencies in the system as well as for identifying the improvement areas by highlighting the cost reduction opportunities. However , this analysis will be fully effective only if it is further extended to identify the cost incurred in ensuring quality in all areas of the supply chain including the hidden costs and costs of missed out opportunities. Most of the hidden elements of quality costs are difficult to track and not accounted by the traditional accounting tools. An exploratory analysis is made in this research to identify the hidden elements of quality costs in manufacturing industry. Further, the identified cost elements are classified into various groups for better analysis and, finally, prioritized to identify the vital few among them. Analytic Hierarchy Process (AHP technique which is one of the most popular Multi Criteria Decision Method (MCDM and Pareto analysis were used in this study for prioritizing the hidden quality cost elements based on their degree of impact on overall cost of quality. By this analysis, the key cost elements which are to be addressed to reduce the overall cost of quality are identified.

  7. Application and Mechanics Analysis of Multi-Function Construction Platforms in Prefabricated-Concrete Construction

    Science.gov (United States)

    Wang, Meihua; Li, Rongshuai; Zhang, Wenze

    2017-11-01

    Multi-function construction platforms (MCPs) as an “old construction technology, new application” of the building facade construction equipment, its efforts to reduce labour intensity, improve labour productivity, ensure construction safety, shorten the duration of construction and other aspects of the effect are significant. In this study, the functional analysis of the multi-function construction platforms is carried out in the construction of the assembly building. Based on the general finite element software ANSYS, the static calculation and dynamic characteristics analysis of the MCPs structure are analysed, the simplified finite element model is constructed, and the selection of the unit, the processing and solution of boundary are under discussion and research. The maximum deformation value, the maximum stress value and the structural dynamic characteristic model are obtained. The dangerous parts of the platform structure are analysed, too. Multiple types of MCPs under engineering construction conditions are calculated, so as to put forward the rationalization suggestions for engineering application of the MCPs.

  8. Neutron activation analysis on sediments from Victoria Land, Antarctica. Multi-elemental characterization of potential atmospheric dust sources

    International Nuclear Information System (INIS)

    Baccolo, G.; Maggi, V.; Baroni, C.; Clemenza, M.; Motta, A.; Nastasi, M.; Previtali, E.; University of Milano-Bicocca, Milan; Delmonte, B.; Salvatore, M.C.

    2014-01-01

    The elemental composition of 40 samples of mineral sediments collected in Victoria Land, Antarctica, in correspondence of ice-free sites, is presented. Concentration of 36 elements was determined by instrumental neutron activation analysis, INAA. The selection of 6 standard reference materials and the development of a specific analytical procedure allowed to reduce measurements uncertainties and to verify the reproducibility of the results. The decision to analyze sediment samples from Victoria Land ice-free areas is related to recent investigations regarding mineral dust content in the TALos Dome ICE core (159deg11'E; 72deg49'S, East Antarctica, Victoria Land), in which a coarse local fraction of dust was recognized. The characterization of Antarctic potential source areas of atmospheric mineral dust is the first step to identify the active sources of dust for the Talos Dome area and to reconstruct the atmospheric pathways followed by air masses in this region during different climatic periods. Principal components analysis was used to identify elements and samples correlations; attention was paid specially to rare earth elements (REE) and incompatible/compatible elements (ICE) in respect to iron, which proved to be the most discriminating elemental groups. The analysis of REE and ICE concentration profiles supported evidences of chemical weathering in ice-free areas of Victoria Land, whereas cold and dry climate conditions of the Talos Dome area and in general of East Antarctica. (author)

  9. Low-resolution continuum source simultaneous multi-element electrothermal atomic absorption spectrometry: steps into practice

    International Nuclear Information System (INIS)

    Katskov, Dmitri

    2015-01-01

    The theory and practical problems of continuum source simultaneous multi-element electrothermal atomic absorption spectrometry (SMET AAS) are discussed by the example of direct analysis of underground water. The experimental methodology is based on pulse vaporization of the sample in a fast heated graphite tube and measurement of transient absorption of continuum spectrum radiation from D 2 and Xe lamps within 200–400 nm wavelengths range with a low resolution spectral instrument and linear charge-coupled device. The setup permits the acquisition of 200 spectra during 1 s atomization pulse. Respective data matrix absorbance vs wavelength/time is employed for the quantification of elements in the sample. The calculation algorithm developed includes broad band and continuum background correction, linearization of function absorbance vs. concentration of atomic vapor and integration of thus modified absorbance at the resonance lines of the elements to be determined. Practical application shows that the method can be employed for the direct simultaneous determination of about 20 elements above microgram per liter level within 3–5 orders of the magnitude concentration range. The investigated sources of measurement errors are mainly associated with the atomization and vapor transportation problems, which are aggravated for the simultaneous release of major and minor sample constituents. Respective corrections concerning the selection of analytical lines, optimal sampling volume, matrix modification and cleaning of the atomizer have been introduced in the SMET AAS analytical technology. Under the optimized experimental conditions the calibration curves in Log-Log coordinates for all the investigated analytes in the single or multi-element reference solutions are approximated by the first order equations. The use of these equations as permanent characteristics of the setup enables instant quantification of Al, Ca, Co, Cr, Cu, Fe, Mg, Mn and Ni in the underground water

  10. Low-resolution continuum source simultaneous multi-element electrothermal atomic absorption spectrometry: steps into practice

    Energy Technology Data Exchange (ETDEWEB)

    Katskov, Dmitri, E-mail: katskovda@tut.ac.za

    2015-03-01

    The theory and practical problems of continuum source simultaneous multi-element electrothermal atomic absorption spectrometry (SMET AAS) are discussed by the example of direct analysis of underground water. The experimental methodology is based on pulse vaporization of the sample in a fast heated graphite tube and measurement of transient absorption of continuum spectrum radiation from D{sub 2} and Xe lamps within 200–400 nm wavelengths range with a low resolution spectral instrument and linear charge-coupled device. The setup permits the acquisition of 200 spectra during 1 s atomization pulse. Respective data matrix absorbance vs wavelength/time is employed for the quantification of elements in the sample. The calculation algorithm developed includes broad band and continuum background correction, linearization of function absorbance vs. concentration of atomic vapor and integration of thus modified absorbance at the resonance lines of the elements to be determined. Practical application shows that the method can be employed for the direct simultaneous determination of about 20 elements above microgram per liter level within 3–5 orders of the magnitude concentration range. The investigated sources of measurement errors are mainly associated with the atomization and vapor transportation problems, which are aggravated for the simultaneous release of major and minor sample constituents. Respective corrections concerning the selection of analytical lines, optimal sampling volume, matrix modification and cleaning of the atomizer have been introduced in the SMET AAS analytical technology. Under the optimized experimental conditions the calibration curves in Log-Log coordinates for all the investigated analytes in the single or multi-element reference solutions are approximated by the first order equations. The use of these equations as permanent characteristics of the setup enables instant quantification of Al, Ca, Co, Cr, Cu, Fe, Mg, Mn and Ni in the underground

  11. Analysis and Simulation of Multi-target Echo Signals from a Phased Array Radar

    OpenAIRE

    Jia Zhen; Zhou Rui

    2017-01-01

    The construction of digital radar simulation systems has been a research hotspot of the radar field. This paper focuses on theoretical analysis and simulation of multi-target echo signals produced in a phased array radar system, and constructs an array antenna element and a signal generation environment. The antenna element is able to simulate planar arrays and optimizes these arrays by adding window functions. And the signal environment can model and simulate radar transmission signals, rada...

  12. Creating a Test Validated Structural Dynamic Finite Element Model of the Multi-Utility Technology Test Bed Aircraft

    Science.gov (United States)

    Pak, Chan-Gi; Truong, Samson S.

    2014-01-01

    Small modeling errors in the finite element model will eventually induce errors in the structural flexibility and mass, thus propagating into unpredictable errors in the unsteady aerodynamics and the control law design. One of the primary objectives of Multi Utility Technology Test Bed, X-56A, aircraft is the flight demonstration of active flutter suppression, and therefore in this study, the identification of the primary and secondary modes for the structural model tuning based on the flutter analysis of X-56A. The ground vibration test validated structural dynamic finite element model of the X-56A is created in this study. The structural dynamic finite element model of the X-56A is improved using a model tuning tool. In this study, two different weight configurations of the X-56A have been improved in a single optimization run.

  13. Ultraviolet-light-induced multi-physics behaviors of 0–3 polarized transparent PLZT plates: II. Finite element analysis and validation

    International Nuclear Information System (INIS)

    Luo, Quantian; Tong, Liyong

    2011-01-01

    This paper presents a novel finite element formulation for 0–3 polarized PbLaZrTi (PLZT) plates and a comparison of the predicted and measured bending displacements. The coupled multi-physics fields and Hamilton's principle for piezoelectric (PZT) materials are first extended to PLZT ceramics by including the anomalous photovoltaic and photo-thermal effects. The photo-induced non-uniform electrical field and mechanical strains across the thickness are modeled in the present finite element formulation for 0–3 polarized PLZT plates, and the associated actuator and sensor equations are derived. The transverse displacements of a 0–3 polarized PLZT plate are predicted using the present finite element formulation and compared with the measured data given in part I. A reasonably good correlation is noted for the transverse displacements at the ten measurement points

  14. MEGHNAD – A multi element detector array for heavy ion collision ...

    Indian Academy of Sciences (India)

    When heavy ion beam available from such machines fall on a target and undergo collision, very rich and often pristine fields of research open up. In order to carry on such activities, we have taken up a project to build a multi element gamma, heavy ion and neutron array of detectors (MEGHNAD) to detect and study the ...

  15. Hybrid Direct and Iterative Solver with Library of Multi-criteria Optimal Orderings for h Adaptive Finite Element Method Computations

    KAUST Repository

    AbouEisha, Hassan M.

    2016-06-02

    In this paper we present a multi-criteria optimization of element partition trees and resulting orderings for multi-frontal solver algorithms executed for two dimensional h adaptive finite element method. In particular, the problem of optimal ordering of elimination of rows in the sparse matrices resulting from adaptive finite element method computations is reduced to the problem of finding of optimal element partition trees. Given a two dimensional h refined mesh, we find all optimal element partition trees by using the dynamic programming approach. An element partition tree defines a prescribed order of elimination of degrees of freedom over the mesh. We utilize three different metrics to estimate the quality of the element partition tree. As the first criterion we consider the number of floating point operations(FLOPs) performed by the multi-frontal solver. As the second criterion we consider the number of memory transfers (MEMOPS) performed by the multi-frontal solver algorithm. As the third criterion we consider memory usage (NONZEROS) of the multi-frontal direct solver. We show the optimization results for FLOPs vs MEMOPS as well as for the execution time estimated as FLOPs+100MEMOPS vs NONZEROS. We obtain Pareto fronts with multiple optimal trees, for each mesh, and for each refinement level. We generate a library of optimal elimination trees for small grids with local singularities. We also propose an algorithm that for a given large mesh with identified local sub-grids, each one with local singularity. We compute Schur complements over the sub-grids using the optimal trees from the library, and we submit the sequence of Schur complements into the iterative solver ILUPCG.

  16. Large scale multi-zone creep finite element modelling of a main steam line branch intersection

    International Nuclear Information System (INIS)

    Payten, Warwick

    2006-01-01

    A number of papers detail the non-linear creep finite element analysis of branch pieces. Predominately these models have incorporated only a single material zone representing the parent material. Multi-zone models incorporating weld material and heat affected zones have primarily been two-dimensional analyses, in part due to the large number of elements required to adequately represent all of the zones. This paper describes a non-linear creep analysis of a main steam line branch intersection using creep properties to represent the parent metal, weld metal, and heat affected zone (HAZ), the stress redistribution over 100,000 h is examined. The results show that the redistribution leads to a complex stress state, particularly at the heat affected zone. Although, there is damage on the external surface of the branch piece as expected, the results indicate that the damage would be more widespread through extensive sections of the heat affected zone. This would appear to indicate that the time between damage indications on the surface using techniques such as replication and full thickness damage may be more limited then previously expected

  17. Morphing the feature-based multi-blocks of normative/healthy vertebral geometries to scoliosis vertebral geometries: development of personalized finite element models.

    Science.gov (United States)

    Hadagali, Prasannaah; Peters, James R; Balasubramanian, Sriram

    2018-03-12

    Personalized Finite Element (FE) models and hexahedral elements are preferred for biomechanical investigations. Feature-based multi-block methods are used to develop anatomically accurate personalized FE models with hexahedral mesh. It is tedious to manually construct multi-blocks for large number of geometries on an individual basis to develop personalized FE models. Mesh-morphing method mitigates the aforementioned tediousness in meshing personalized geometries every time, but leads to element warping and loss of geometrical data. Such issues increase in magnitude when normative spine FE model is morphed to scoliosis-affected spinal geometry. The only way to bypass the issue of hex-mesh distortion or loss of geometry as a result of morphing is to rely on manually constructing the multi-blocks for scoliosis-affected spine geometry of each individual, which is time intensive. A method to semi-automate the construction of multi-blocks on the geometry of scoliosis vertebrae from the existing multi-blocks of normative vertebrae is demonstrated in this paper. High-quality hexahedral elements were generated on the scoliosis vertebrae from the morphed multi-blocks of normative vertebrae. Time taken was 3 months to construct the multi-blocks for normative spine and less than a day for scoliosis. Efforts taken to construct multi-blocks on personalized scoliosis spinal geometries are significantly reduced by morphing existing multi-blocks.

  18. An approach to unfold the response of a multi-element system using an artificial neural network

    International Nuclear Information System (INIS)

    Cordes, E.; Fehrenbacher, G.; Schuetz, R.; Sprunck, M.; Hahn, K.; Hofmann, R.; Wahl, W.

    1998-01-01

    An unfolding procedure is proposed which aims at obtaining spectral information of a neutron radiation field by the analysis of the response of a multi-element system consisting of converter type semiconductors. For the unfolding procedure an artificial neural network (feed forward network), trained by the back-propagation method, was used. The response functions of the single elements to neutron radiation were calculated by application of a computational model for an energy range from 10 -2 eV to 10 MeV. The training of the artificial neural network was based on the computation of responses of a six-element system for a set of 300 neutron spectra and the application of the back-propagation method. The validation was performed by the unfolding of 100 computed responses. Two unfolding examples were pointed out for the determination of the neutron spectra. The spectra resulting from the unfolding procedure agree well with the original spectra used for the response computation

  19. Anomalous decrease in X-ray diffraction intensities of Cu-Ni-Al-Co-Cr-Fe-Si alloy systems with multi-principal elements

    International Nuclear Information System (INIS)

    Yeh, J.-W.; Chang, S.-Y.; Hong, Y.-D.; Chen, S.-K.; Lin, S.-J.

    2007-01-01

    With an aim to understand the great reduction in the X-ray diffraction (XRD) intensities of high-entropy alloys, a series of Cu-Ni-Al-Co-Cr-Fe-Si alloys with systematic addition of principal elements from pure element to seven elements was investigated for quantitative analysis of XRD intensities. The variation of XRD peak intensities of the alloy system is similar to that caused by thermal effect, but the intensities further drop beyond the thermal effect with increasing number of incorporated principal elements. An intrinsic lattice distortion effect caused by the addition of multi-principal elements with different atomic sizes is expected for the anomalous decrease in XRD intensities. The mathematical factor of this distortion effect for the modification of XRD structure factor is formulated analogue to that of thermal effect

  20. A 2D multi-term time and space fractional Bloch-Torrey model based on bilinear rectangular finite elements

    Science.gov (United States)

    Qin, Shanlin; Liu, Fawang; Turner, Ian W.

    2018-03-01

    The consideration of diffusion processes in magnetic resonance imaging (MRI) signal attenuation is classically described by the Bloch-Torrey equation. However, many recent works highlight the distinct deviation in MRI signal decay due to anomalous diffusion, which motivates the fractional order generalization of the Bloch-Torrey equation. In this work, we study the two-dimensional multi-term time and space fractional diffusion equation generalized from the time and space fractional Bloch-Torrey equation. By using the Galerkin finite element method with a structured mesh consisting of rectangular elements to discretize in space and the L1 approximation of the Caputo fractional derivative in time, a fully discrete numerical scheme is derived. A rigorous analysis of stability and error estimation is provided. Numerical experiments in the square and L-shaped domains are performed to give an insight into the efficiency and reliability of our method. Then the scheme is applied to solve the multi-term time and space fractional Bloch-Torrey equation, which shows that the extra time derivative terms impact the relaxation process.

  1. Comparison of Elemental Composition in Korean Irradiated Foods using Instrumental Neutron Activation Analysis

    International Nuclear Information System (INIS)

    Chung, Yong Sam; Kim, Sun Ha; Sun, Gwang Min; Lim, Jong Myung; Moon, Jong Hwa; Lee, Kye Hong; Kim, Young Jin; Choi, Jong Il; Lee, Joo Eun

    2010-01-01

    The information and role of trace mineral elements from an intake of created and processed foodstuff are important as a indicator of human health and nutritional parameter, as well as a quality control of food and diet. Particularly, special food created for consumption by astronauts in outer space may differ with common food on the earth in order to compensate a decrease of taste and nutrition by strong cosmic rays, a state of nongravitation, low pressure, and enclosed space environment. In April 2008, Korea's first astronaut became a crew member of the international space station and she was brought special space versions of Korea's national dishes such as Kimchi, boiled rice, hot red paste, green tea, ramyun, and so on. Accurate quantitative analysis of trace elements in various kinds of biological samples is also important for data quality. Neutron activation analysis is a sensitive, non-destructive, multi-elemental analytical method, and is proper for tracing elements in a biological sample in order to avoid loss and contamination by chemical pretreatment. This study analyses the distribution of concentrations for both essential and toxic elements in six kinds of Korean space foods developed by KAERI. The quantitative analytical results from instrumental neutron activation analysis are presented

  2. The trace element analysis of ancient Indian coins using proton induced x-ray emission (PIXE) technique

    International Nuclear Information System (INIS)

    PURI, N.K.; HAJIVALIEI, M.; BEDI, S.C.; SINGH, N.; GOVIL, I.M.; GARG, M.L.; HANDA, D.K.; GOVIL, K.L.; ROUT, B.; VIJAYAN, V.

    2004-01-01

    Elemental analysis of ancient Indian coins viz. thirty-three punched marked coins (6 th century B.C.), fifty-nine coins belonging to Kusanas (78-250 A.D) and twenty-five coins belonging to medieval period (11 th -14 th century A.D), from India have been analysed using Proton Induced X-ray Emission (PIXE) technique. The elements namely S, Ca, Fe, Ag, Cu, Ni and Pb were detected in most of the punch-marked coins while elements namely S, Cl, K, Ca, Ti, Cr, Mn, Fe, Ni, Cu, As and Zn were detected in most of the Kusanas coins and the S, Ca, Fe, Cu, Ag, Sn, Pb were detected in 11 th -14 th century A.D. coins. Based on the elemental analysis different hypotheses put forward in the earlier literature were examined. This is the first attempt where reasonable number of ancient coins belonging to different periods were analysed by modern non destructive multi-elemental technique such as PIXE and has put the importance of the elemental analysis of ancient Indian coins in the proper perspective

  3. Elemental mapping and quantitative analysis of Cu, Zn, and Fe in rat brain sections by laser ablation ICP-MS

    Energy Technology Data Exchange (ETDEWEB)

    Jackson, Brian [Dartmouth College, Departments of Earth Sciences and Chemistry, Hanover, NH (United States); Harper, Steve [University of Georgia, Savannah River Ecology Laboratory, Aiken, SC (United States); Smith, Laura; Flinn, Jane [George Mason University, Department of Psychology, Fairfax, VA (United States)

    2006-02-15

    This report details the application of laser ablation quadrupole ICP-MS for the (multi)elemental mapping of 100-{mu}m-thick sections of rat brain. The laser spot size used was 60 {mu}m, and the laser scan speed was 120 {mu}m s{sup -1}. The analysis was relatively rapid, allowing mapping of a whole brain thin section ({approx}1 cm{sup 2}) in about 2 h. Furthermore, the method was amenable to multi-element data collection including the physiologically important elements P and S and afforded sub {mu}g g{sup -1} detection limits for the important trace elements Cu and Zn. Calibrations were performed with pressed pellets of biological certified reference materials, and the elemental distributions and concentrations of Cu, Zn, and Fe were determined in whole rat brain sections. The distributions and concentration ranges for these elements were consistent with previous studies and demonstrate the utility of this technique for rapid mapping of brain thin sections. (orig.)

  4. Data structures supporting multi-region adaptive isogeometric analysis

    Science.gov (United States)

    Perduta, Anna; Putanowicz, Roman

    2018-01-01

    Since the first paper published in 2005 Isogeometric Analysis (IGA) has gained strong interest and found applications in many engineering problems. Despite the advancement of the method, there are still far fewer software implementations comparing to Finite Element Method. The paper presents an approach to the development of data structures that can support multi-region IGA with local mesh refinement (patch-based) and possible application in IGA-FEM models. The purpose of this paper is to share original design concepts, that authors have created while developing an IGA package, which other researchers may find beneficial for their own simulation codes.

  5. Macro elemental analysis of food samples by nuclear analytical technique

    Science.gov (United States)

    Syahfitri, W. Y. N.; Kurniawati, S.; Adventini, N.; Damastuti, E.; Lestiani, D. D.

    2017-06-01

    Energy-dispersive X-ray fluorescence (EDXRF) spectrometry is a non-destructive, rapid, multi elemental, accurate, and environment friendly analysis compared with other detection methods. Thus, EDXRF spectrometry is applicable for food inspection. The macro elements calcium and potassium constitute important nutrients required by the human body for optimal physiological functions. Therefore, the determination of Ca and K content in various foods needs to be done. The aim of this work is to demonstrate the applicability of EDXRF for food analysis. The analytical performance of non-destructive EDXRF was compared with other analytical techniques; neutron activation analysis and atomic absorption spectrometry. Comparison of methods performed as cross checking results of the analysis and to overcome the limitations of the three methods. Analysis results showed that Ca found in food using EDXRF and AAS were not significantly different with p-value 0.9687, whereas p-value of K between EDXRF and NAA is 0.6575. The correlation between those results was also examined. The Pearson correlations for Ca and K were 0.9871 and 0.9558, respectively. Method validation using SRM NIST 1548a Typical Diet was also applied. The results showed good agreement between methods; therefore EDXRF method can be used as an alternative method for the determination of Ca and K in food samples.

  6. Non-Linear Multi-Physics Analysis and Multi-Objective Optimization in Electroheating Applications

    Czech Academy of Sciences Publication Activity Database

    di Barba, P.; Doležel, Ivo; Mognaschi, M. E.; Savini, A.; Karban, P.

    2014-01-01

    Roč. 50, č. 2 (2014), s. 7016604-7016604 ISSN 0018-9464 Institutional support: RVO:61388998 Keywords : coupled multi-physics problems * finite element method * non-linear equations Subject RIV: JA - Electronics ; Optoelectronics, Electrical Engineering Impact factor: 1.386, year: 2014

  7. Parameter Optimization of Multi-Element Synthetic Aperture Imaging Systems

    Directory of Open Access Journals (Sweden)

    Vera Behar

    2007-03-01

    Full Text Available In conventional ultrasound imaging systems with phased arrays, the further improvement of lateral resolution requires enlarging of the number of array elements that in turn increases both, the complexity and the cost, of imaging systems. Multi-element synthetic aperture focusing (MSAF systems are a very good alternative to conventional systems with phased arrays. The benefit of the synthetic aperture is in reduction of the system complexity, cost and acquisition time. In a MSAF system considered in the paper, a group of elements transmit and receive signals simultaneously, and the transmit beam is defocused to emulate a single element response. The echo received at each element of a receive sub-aperture is recorded in the computer memory. The process of transmission/reception is repeated for all positions of a transmit sub-aperture. All the data recordings associated with each corresponding pair "transmit-receive sub-aperture" are then focused synthetically producing a low-resolution image. The final high-resolution image is formed by summing of the all low-resolution images associated with transmit/receive sub-apertures. A problem of parameter optimization of a MSAF system is considered in this paper. The quality of imaging (lateral resolution and contrast is expressed in terms of the beam characteristics - beam width and side lobe level. The comparison between the MSAF system described in the paper and an equivalent conventional phased array system shows that the MSAF system acquires images of equivalent quality much faster using only a small part of the power per image.

  8. Investigation of multi-stage cold forward extrusion process using coupled thermo-mechanical finite element analysis

    Science.gov (United States)

    Görtan, Mehmet Okan

    2018-05-01

    Cold extrusion processes are distinguished by their low material usage as well as great efficiency in the production of mid-range and large component series. Although majority of the cold extruded parts are produced using die systems containing multiple forming stages, this subject has rarely been investigated so far. Therefore, the characteristics of multi-stage cold forward rod extrusion is studied in the current work using thermo-mechanically coupled finite element (FE) analysis. A case hardening steel, 16MnCr5 (1.7131) was used as experimental material. Its strain, strain rate and temperature dependent mechanical characteristics were determined using compression testing and modeled in FE simulations via a Johnson-Cook material model. Friction coefficients for the same material while in contact with a tool steel (1.2379) were determined dependent on temperature and contact pressure using sliding compression test (SCT) and modeled by an adaptive friction model developed by the author. In the first set of simulations, rod material with a diameter of 14.9 mm was extruded down to a diameter of 9.6 mm in a single step using three different die opening angles (2α); 20°, 40° and 60°. In the second set of investigations, the same rod was reduced first to 12 mm and then to 9.6 mm in two steps within the same forming die. Press forces, contact normal stresses between extruded material and forming die, material temperature and axial stresses are compared in these two set of simulations and the differences are discussed.

  9. Detailed finite element method modeling of evaporating multi-component droplets

    Energy Technology Data Exchange (ETDEWEB)

    Diddens, Christian, E-mail: C.Diddens@tue.nl

    2017-07-01

    The evaporation of sessile multi-component droplets is modeled with an axisymmetic finite element method. The model comprises the coupled processes of mixture evaporation, multi-component flow with composition-dependent fluid properties and thermal effects. Based on representative examples of water–glycerol and water–ethanol droplets, regular and chaotic examples of solutal Marangoni flows are discussed. Furthermore, the relevance of the substrate thickness for the evaporative cooling of volatile binary mixture droplets is pointed out. It is shown how the evaporation of the more volatile component can drastically decrease the interface temperature, so that ambient vapor of the less volatile component condenses on the droplet. Finally, results of this model are compared with corresponding results of a lubrication theory model, showing that the application of lubrication theory can cause considerable errors even for moderate contact angles of 40°. - Graphical abstract:.

  10. Homogenization-based interval analysis for structural-acoustic problem involving periodical composites and multi-scale uncertain-but-bounded parameters.

    Science.gov (United States)

    Chen, Ning; Yu, Dejie; Xia, Baizhan; Liu, Jian; Ma, Zhengdong

    2017-04-01

    This paper presents a homogenization-based interval analysis method for the prediction of coupled structural-acoustic systems involving periodical composites and multi-scale uncertain-but-bounded parameters. In the structural-acoustic system, the macro plate structure is assumed to be composed of a periodically uniform microstructure. The equivalent macro material properties of the microstructure are computed using the homogenization method. By integrating the first-order Taylor expansion interval analysis method with the homogenization-based finite element method, a homogenization-based interval finite element method (HIFEM) is developed to solve a periodical composite structural-acoustic system with multi-scale uncertain-but-bounded parameters. The corresponding formulations of the HIFEM are deduced. A subinterval technique is also introduced into the HIFEM for higher accuracy. Numerical examples of a hexahedral box and an automobile passenger compartment are given to demonstrate the efficiency of the presented method for a periodical composite structural-acoustic system with multi-scale uncertain-but-bounded parameters.

  11. An Assessment of the Icing Blade and the SEA Multi-Element Sensor for Liquid Water Content Calibration of the NASA GRC Icing Research Tunnel

    Science.gov (United States)

    Steen, Laura E.; Ide, Robert F.; Van Zante, Judith Foss

    2017-01-01

    The Icing Research Tunnel at NASA Glenn has recently switched to from using the Icing Blade to using the SEA Multi-Element Sensor (also known as the multi-wire) for its calibration of cloud liquid water content. In order to perform this transition, tests were completed to compare the Multi-Element Sensor to the Icing Blade, particularly with respect to liquid water content, airspeed, and drop size. The two instruments were found to compare well for the majority of Appendix C conditions. However, it was discovered that the Icing Blade under-measures when the conditions approach the Ludlam Limit. This paper also describes data processing procedures for the Multi-Element Sensor in the IRT, including collection efficiency corrections, mounting underneath a splitter plate, and correcting for a jump in the compensation wire power. Further data is presented to describe the repeatability of the IRT with the Multi-Element sensor, health-monitoring checks for the instrument, and a sensing-element configuration comparison.

  12. AC power flow importance measures considering multi-element failures

    International Nuclear Information System (INIS)

    Li, Jian; Dueñas-Osorio, Leonardo; Chen, Changkun; Shi, Congling

    2017-01-01

    Quantifying the criticality of individual components of power systems is essential for overall reliability and management. This paper proposes an AC-based power flow element importance measure, while considering multi-element failures. The measure relies on a proposed AC-based cascading failure model, which captures branch overflow, bus load shedding, and branch failures, via AC power flow and optimal power flow analyses. Taking the IEEE 30, 57 and 118-bus power systems as case studies, we find that N-3 analyses are sufficient to measure the importance of a bus or branch. It is observed that for a substation bus, its importance is statistically proportional to its power demand, but this trend is not observed for power plant buses. While comparing with other reliability, functionality, and topology-based importance measures popular today, we find that a DC power flow model, although better correlated with the benchmark AC model as a whole, still fails to locate some critical elements. This is due to the focus of DC-based models on real power that ignores reactive power. The proposed importance measure is aimed to inform decision makers about key components in complex systems, while improving cascading failure prevention, system backup setting, and overall resilience. - Highlights: • We propose a novel importance measure based on joint failures and AC power flow. • A cascading failure model considers both AC power flow and optimal power flow. • We find that N-3 analyses are sufficient to measure the importance of an element. • Power demand impacts the importance of substations but less so that of generators. • DC models fail to identify some key elements, despite correlating with AC models.

  13. Experimental analysis of influence of different lubricants types on the multi-phase ironing process

    Directory of Open Access Journals (Sweden)

    Milan Djordjević

    2013-05-01

    Full Text Available This paper is aimed at presenting results of an experimental analysis of the different types of lubricants influence on the multi-phase ironing process. Based on sliding of the metal strip between the two contact elements a special tribological model was adopted. The subject of experimental investigations was variations of the drawing force, contact pressure and the friction coefficient for each type of the applied lubricants. The ironing process was conducted in three-phases at the constant sliding velocity. The objective of this analysis was to compare all the applied lubricants in order to estimate their quality from the point of view of their applicability in the multi-phase ironing process.

  14. EXPERIMENTAL ANALYSIS OF INFLUENCE OF DIFFERENT LUBRICANTS TYPES ON THE MULTI-PHASE IRONING PROCESS

    Directory of Open Access Journals (Sweden)

    Milan Djordjević

    2013-09-01

    Full Text Available This paper is aimed at presenting results of an experimental analysis of the different types of lubricants influence on the multi-phase ironing process. Based on sliding of the metal strip between the two contact elements a special tribological model was adopted. The subject of experimental investigations was variations of the drawing force, contact pressure and the friction coefficient for each type of the applied lubricants. The ironing process was conducted in three-phases at the constant sliding velocity. The objective of this analysis was to compare all the applied lubricants in order to estimate their quality from the point of view of their applicability in the multi-phase ironing process.

  15. Development of the multitracer technology for a simultaneous multi-elemental analysis and its evolution in RI-beam factory project

    International Nuclear Information System (INIS)

    Enomoto, Shuichi

    2003-01-01

    This review describes the method to produce the multitracer, its biobehavior, its application for environmental sciences, Nuclear Energy Fundamentals Crossover Research (for upgrading multitracer production technology, and development of the automatic chemical separation units and of the simultaneous imaging apparatus for multi gamma-ray nuclides), and Inst. of Physical and Chemical Research (RIKEN) RI-beam factory project. The multitracer technology is an efficient (i.e., many information's are available through one experimentation) tracer technique for studying the physical, chemical and biological behavior of elements with use of their multiple radioisotopes produced by accelerators like RIKEN ring cyclotron and of computer/semiconductor detector for their individual gamma-ray spectrometry. The multitracer elements are produced in their carrier-free forms by irradiation of the target element with the heavy particle (up to Ta, in RIKEN cyclotron) and by resultant nuclear fragmentation of the target. The multitracer through nuclear fragmentation and/or fission with an automated separation apparatus will be sophisticatedly supplied in future. GREI (gamma-ray emission imaging) is under investigation. The RI-beam factory project aims to irradiate/accelerate the radioisotope, which is expected to give novel knowledge's in biology like metabolic physiology. (N.I.)

  16. Multi-element analysis of the obese subject by in vivo neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Siwek, R A; Burkinshaw, L; Oxby, C B [Leeds General Infirmary (UK); Robinson, P A.J. [Saint James' s University Hospital, Leeds (UK)

    1984-06-01

    The Leeds facility for in vivo neutron activation analysis has been modified and calibrated for the simultaneous measurement of nitrogen, potassium, sodium, chlorine, phosphorus and calcium in obese patients weighing up to 210 kg. The effects of body size and shape were incorporated into the calibration by measuring 14 anthropomorphic phantoms of known composition representing individual patients being treated for obesity. The phantoms were constructed from tissue substitutes representing lean skeletal and adipose tissues, arranged to simulate the distributions of the corresponding tissues within the patients, as visualised by CT scanning. The precision of the method, determined by measuring a single phantom ten times over a period of ten weeks, is between two and three per cent for all elements except calcium, for which it is 11.3%. Accuracy is estimated to be similar to precision. The procedure has been used to study changes in body composition of patients undergoing therapeutic starvation.

  17. Multi-elemental analysis of marine sediments of Manila Bay using x-ray fluorescence spectrometry

    International Nuclear Information System (INIS)

    Rosales, Colleen Marciel Fontelera

    2011-04-01

    An analysis of the marine sediments of Manila Bay was done by employing X-ray fluorescence spectrometry. The general trends observed in sediments are increasing (Ca and Sr), decreasing (Zr), or constant (Cl, Na, S, K) with respect to depth, sometimes, no trend can be observed. These trends are further explained by correlations present among these elements, plus all the other elements. The two X RF data analysis methods Auto Quantify and AXIL were also compared on the basis of the correlation plot obtained. AutoQuantify gave clearer correlations; thus, results from this method were used for constructing correlation plots. Correlations using Microsoft Excel and Stat graphics Centurion X V show that there are naturally occurring [lithogenic (Si, Ti, Al, Mg, Rb, Zn and Fe), biogenic (Ca, Mg), and conservative (Na, Cl)] and non-naturally occurring [mostly anthropogenic, brought to the bodies of water by aeolian or fluvial input (heavy metals Pb-Cu-Zn and Ni-Cr)] correlation present in the sediments. Moreover, pairs of elements that may coexist in a source and not coexist in another (Cr and Mg, Cr and Ni) have also been observed. The heavy metal enrichment was attributed to the burning of fossil fuels, iron and steel manufacturing (present in Valenzuela-Bulacan area), ferry and fishing services and other industrialization activities present in Manila Bay. Marine organisms are affected by the presence of these heavy metals by means of bioaccumulations, and may later on affect humans because of trophic transfer and bio magnification. (author)

  18. US Participation in the Solar Orbiter Multi Element Telescope for Imaging and Spectroscopy (METIS) Project

    Data.gov (United States)

    National Aeronautics and Space Administration — The Multi Element Telescope for Imaging and Spectroscopy, METIS, investigation has been conceived to perform off-limb and near-Sun coronagraphy and is motivated by...

  19. Particle-induced X-ray emission: thick-target analysis of inorganic materials in the determination of light elements

    International Nuclear Information System (INIS)

    Perez-Arantegui, J.; Castillo, J.R.; Querre, G.

    1994-01-01

    Particle-induced X-ray emission (PIXE) has been applied to the analysis of inorganic materials to determine some elements with Z < 27: Na, Mg, Al, Si, K, Ca, Ti, Mn and Fe, in thick-target analysis. A PIXE method has been developed for the analysis of geological materials, ceramics and pottery. Work has been carried out with an ion beam analytical system, using a low particle beam energy. Relative sensitivity, detection limits, reproducibility and accuracy of the method were calculated based on the analysis of geological standard materials (river sediments, argillaceous limestone, basalt, diorite and granite). Analysis using PIXE offers a number of advantages, such as short analysis time, multi-elemental and nondestructive determinations, and the results are similar to those obtained with other instrumental techniques of analysis. (Author)

  20. The evaluation of multi-element personal dosemeters using the linear programming method

    International Nuclear Information System (INIS)

    Kragh, P.; Ambrosi, P.; Boehm, J.; Hilgers, G.

    1996-01-01

    Multi-element dosemeters are frequently used in individual monitoring. Each element can be regarded as an individual dosemeter with its own individual dose measurement value. In general, the individual dose values of one dosemeter vary according to the exposure conditions, i. e. the energy and angle of incidence of the radiation. The (final) dose measurement value of the personal dosemeter is calculated from the individual dose values by means of an evaluation algorithm. The best possible dose value, i.e. that of the smallest systematic (type B) uncertainty if the exposure conditions are changed in the dosemeter's rated range of use, is obtained by the method of linear programming. (author)

  1. Energy dispersive X-ray fluorescence spectrometry for the direct multi-element analysis of dried blood spots

    Science.gov (United States)

    Marguí, E.; Queralt, I.; García-Ruiz, E.; García-González, E.; Rello, L.; Resano, M.

    2018-01-01

    Home-based collection protocols for clinical specimens are actively pursued as a means of improving life quality of patients. In this sense, dried blood spots (DBS) are proposed as a non-invasive and even self-administered alternative to sampling whole venous blood. This contribution explores the potential of energy dispersive X-ray fluorescence spectrometry for the simultaneous and direct determination of some major (S, Cl, K, Na), minor (P, Fe) and trace (Ca, Cu, Zn) elements in blood, after its deposition onto clinical filter papers, thus giving rise to DBS. For quantification purposes the best strategy was to use matrix-matched blood samples of known analyte concentrations. The accuracy and precision of the method were evaluated by analysis of a blood reference material (Seronorm™ trace elements whole blood L3). Quantitative results were obtained for the determination of P, S, Cl, K and Fe, and limits of detection for these elements were adequate, taking into account their typical concentrations in real blood samples. Determination of Na, Ca, Cu and Zn was hampered by the occurrence of high sample support (Na, Ca) and instrumental blanks (Cu, Zn). Therefore, the quantitative determination of these elements at the levels expected in blood samples was not feasible. The methodology developed was applied to the analysis of several blood samples and the results obtained were compared with those reported by standard techniques. Overall, the performance of the method developed is promising and it could be used to determine the aforementioned elements in blood samples in a simple, fast and economic way. Furthermore, its non-destructive nature enables further analyses by means of complementary techniques to be carried out.

  2. Boundary element numerical method for the electric field generated by oblique multi-needle electrodes

    Institute of Scientific and Technical Information of China (English)

    LIU FuPing; WANG AnLing; WANG AnXuan; CAO YueZu; CHEN Qiang; YANG ChangChun

    2009-01-01

    According to the electric potential of oblique multi-needle electrodes (OMNE) in biological tissue, the discrete equations based on the indetermination linear current density were established by the boundary element integral equations (BEIE). The non-uniform distribution of the current flowing from multi-needle electrodes to conductive biological tissues was imaged by solving a set of linear equa-tions. Then, the electric field and potential generated by OMNE in biological tissues at any point may be determined through the boundary element method (BEM). The time of program running and stability of computing method are examined by an example. It demonstrates that the algorithm possesses a quick speed and the steady computed results. It means that this method has an important referenced significance for computing the field and the potential generated by OMNE in bio-tissue, which is a fast, effective and accurate computing method.

  3. Application of PCA-LDA method to determine the geographical origin of tea based on determination of stable isotopes and multi-elements

    International Nuclear Information System (INIS)

    Yuan Yuwei; Zhang Yongzhi; Yang Guiling; Zhang Zhiheng; Fu Haiyan; Han Wenyan; Li Shufang

    2013-01-01

    The ratio of stable isotope and concentration of multi-element in tea was determinated with isotope ratio mass spectrometry (IRMS) and inductively coupled plasma mass spectrometry (ICP-MS). Pattern recognition techniques with principal component analysis (PCA) and linear discriminant analysis (LDA) were used to classify the geographical origins of tea from Fujian, Shandong and Zhejiang province, and Yuyao, Jinhua and Xihu region of Zhejiang. The results showed the values of δ"1"5N, δ"1"3C, δD, δ"1"8O and the ratios of "2"0"6Pb/"2"0"7Pb, "2"0"8Pb/"2"0"6Pb and "8"7Sr/"8"6Sr in tea samples were different from different origins. There was also large variable for the concentrations of 27 mineral elements, such as Li, Be, Na and so on, with a specific character of origin. The method of PCA could be used to classify the geographical origin of tea from different origins but with a cross in the scatter plot. However, PCA combining with LDA could gave correct assignation percentages of 99% for the tea samples among Fujian, Shandong and Zhejiang provinces, and 87% for the tea samples among Yuyao, Jinhua and Xihu region of Zhejiang. These results revealed that it was possible and feasible to classify the geographical origin of tea by the method of PCA-LDA based on the determination of isotopes and multi-elements. (authors)

  4. Analysis of the jet pipe electro-hydraulic servo valve with finite element methods

    Directory of Open Access Journals (Sweden)

    Kaiyu Zhao

    2018-01-01

    Full Text Available The dynamic characteristics analysis about the jet pipe electro-hydraulic servo valve based on experience and mathematical derivation was difficult and not so precise. So we have analysed the armature feedback components, torque motor and jet pipe receiver in electrohydraulic servo valve by sophisticated finite element analysis tools respectively and have got physical meaning data on these parts. Then the data were fitted by Matlab and the mathematical relationships among them were calculated. We have done the dynamic multi-physical fields’ Simulink co-simulation using above mathematical relationship, and have got the input-output relationship of the overall valve, the frequency response and step response. This work can show the actual working condition accurately. At the same time, we have considered the materials and the impact of the critical design dimensions in the finite element analysis process. It provides some new ideas to the overall design of jet pipe electro-hydraulic servo valve.

  5. Multi-element RIMS Analysis of Genesis Solar Wind Collectors

    Science.gov (United States)

    Veryovkin, I. V.; Tripa, C. E.; Zinovev, A. V.; King, B. V.; Pellin, M. J.; Burnett, D. S.

    2009-12-01

    The samples of Solar Wind (SW) delivered by the NASA Genesis mission, present significant challenges for surface analytical techniques, in part due to severe terrestrial contamination of the samples on reentry, in part due to the ultra-shallow and diffused ion implants in the SW collector materials. We are performing measurements of metallic elements in the Genesis collectors using Resonance Ionization Mass Spectrometry (RIMS), an ultra-sensitive analytical method capable of detecting SW in samples with lateral dimensions of only a few mm and at concentrations from above one ppm to below one ppt. Since our last report at 2008 AGU Fall Meeting, we have (a) developed and tested new resonance ionization schemes permitting simultaneous measurements of up to three (Ca, Cr, and Mg) elements, and (b) improved reproducibility and accuracy of our RIMS analyses for SW-like samples (i.e. shallow ion implants) by developing and implementing an optimized set of new analytical protocols. This is important since the quality of scientific results from the Genesis mission critically depends on the accuracy of analytical techniques. In this work, we report on simultaneous RIMS measurements of Ca and Cr performed on two silicon SW collector samples, (#60179 and #60476). First, we have conducted test experiments with 3×1013 at/cm2 52Cr and 44Ca implants in silicon to evaluate the accuracy of our quantitative analyses. Implant fluencies were measured by RIMS to be 2.73×1013 and 2.71×1013 at/cm2 for 52Cr and 44Ca, respectively, which corresponds to an accuracy of ≈10%. Using the same implanted wafer as a reference, we conducted RIMS analyses of the Genesis samples: 3 spots on #60179 and 4 spots on #60476. The elemental SW fluencies expected for Cr and Ca are 2.95×1010 and 1.33×1011 at/cm2 , respectively. Our measurements of 52Cr yielded 3.0±0.6×1011 at/cm2 and 5.1±4.1×1010 at/cm2 for #60179 and #60476, respectively. For 40Ca, SW fluencies of 1.39±0.70×1011 at/cm2 in #60179

  6. Development of Viscoelastic Multi-Body Simulation and Impact Response Analysis of a Ballasted Railway Track under Cyclic Loading

    Directory of Open Access Journals (Sweden)

    Daisuke Nishiura

    2017-06-01

    Full Text Available Simulation of a large number of deformable bodies is often difficult because complex high-level modeling is required to address both multi-body contact and viscoelastic deformation. This necessitates the combined use of a discrete element method (DEM and a finite element method (FEM. In this study, a quadruple discrete element method (QDEM was developed for dynamic analysis of viscoelastic materials using a simpler algorithm compared to the standard FEM. QDEM easily incorporates the contact algorithm used in DEM. As the first step toward multi-body simulation, the fundamental performance of QDEM was investigated for viscoelastic analysis. The amplitude and frequency of cantilever elastic vibration were nearly equal to those obtained by the standard FEM. A comparison of creep recovery tests with an analytical solution showed good agreement between them. In addition, good correlation between the attenuation degree and the real physical viscosity was confirmed for viscoelastic vibration analysis. Therefore, the high accuracy of QDEM in the fundamental analysis of infinitesimal viscoelastic deformations was verified. Finally, the impact response of a ballast and sleeper under cyclic loading on a railway track was analyzed using QDEM as an application of deformable multi-body dynamics. The results showed that the vibration of the ballasted track was qualitatively in good agreement with the actual measurements. Moreover, the ballast layer with high friction reduced the ballasted track deterioration. This study suggests that QDEM, as an alternative to DEM and FEM, can provide deeper insights into the contact dynamics of a large number of deformable bodies.

  7. Design and Wind Tunnel Testing of a Thick, Multi-Element High-Lift Airfoil

    DEFF Research Database (Denmark)

    Zahle, Frederik; Gaunaa, Mac; Sørensen, Niels N.

    2012-01-01

    In this work a 2D CFD solver has been used to optimize the shape of a leading edge slat with a chord length of 30% of the main airfoil which was 40% thick. The airfoil configuration was subsequently tested in a wind tunnel and compared to numerical predictions. The multi-element airfoil was predi...

  8. Determination of trace elements in Turkish tea leaves by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Demiralp, R.

    1986-01-01

    The human body continuously assimilates a variety of inorganic elements from food and the environment. Some of these elements are closely related to human health and disorder. Tea is one of the most popular stimulating beverages which is consumed by low and high income family groups in many countries. Instrumental neutron activation analysis is one of the preferred methods because information on a large number of elements can be obtained simultaneously. Five packets each of the seven commonly used brands of tea were obtained from the market. In order to determine the transfer of trace elements into the drinkable portion about 2-3g. of the tea leaves were boiled in hot water for 2 min. After filtration the used tea leaves were dried at 65 deg. C in an oven and a portion, about 200mg was used for analysis. Samples and standards were irradiated 10 min. and 2 hrs. at pneumatic system and central thimble in the TRIGA MARK-II research reactor. After irradiation, the activities of samples and standards were measured with a aoaxial Ge detector coupled to a spectroscopic amplifier. A Canbera 90 model multi- channel analyzer with an 8K memory was used for pulse height analysis. The system has a resolution of 2.0 KeV. for the 1332.5 KeV gamma ray of 60 Co. The activity of the sample and standard was compared and the element contst of the sample was calculated. (author)

  9. Efficiency Evaluation of Food Waste Materials for the Removal of Metals and Metalloids from Complex Multi-Element Solutions.

    Science.gov (United States)

    Massimi, Lorenzo; Giuliano, Antonella; Astolfi, Maria Luisa; Congedo, Rossana; Masotti, Andrea; Canepari, Silvia

    2018-02-26

    Recent studies have shown the potential of food waste materials as low cost adsorbents for the removal of heavy metals and toxic elements from wastewater. However, the adsorption experiments have been performed in heterogeneous conditions, consequently it is difficult to compare the efficiency of the individual adsorbents. In this study, the adsorption capacities of 12 food waste materials were evaluated by comparing the adsorbents' efficiency for the removal of 23 elements from complex multi-element solutions, maintaining homogeneous experimental conditions. The examined materials resulted to be extremely efficient for the adsorption of many elements from synthetic multi-element solutions as well as from a heavy metal wastewater. The 12 adsorbent surfaces were analyzed by Fourier transform infrared spectroscopy and showed different types and amounts of functional groups, which demonstrated to act as adsorption active sites for various elements. By multivariate statistical computations of the obtained data, the 12 food waste materials were grouped in five clusters characterized by different elements' removal efficiency which resulted to be in correlation with the specific adsorbents' chemical structures. Banana peel, watermelon peel and grape waste resulted the least selective and the most efficient food waste materials for the removal of most of the elements.

  10. Analysis of some metallic elements and metalloids composition and relationships in parasol mushroom Macrolepiota procera.

    Science.gov (United States)

    Falandysz, Jerzy; Sapkota, Atindra; Dryżałowska, Anna; Mędyk, Małgorzata; Feng, Xinbin

    2017-06-01

    The aim of the study was to characterise the multi-elemental composition and associations between a group of 32 elements and 16 rare earth elements collected by mycelium from growing substrates and accumulated in fruiting bodies of Macrolepiota procera from 16 sites from the lowland areas of Poland. The elements were quantified by inductively coupled plasma quadrupole mass spectrometry using validated method. The correlation matrix obtained from a possible 48 × 16 data matrix has been used to examine if any association exits between 48 elements in mushrooms foraged from 16 sampling localizations by multivariate approach using principal component (PC) analysis. The model could explain up to 93% variability by eight factors for which an eigenvalue value was ≥1. Absolute values of the correlation coefficient were above 0.72 (significance at p < 0.05) for 43 elements. From a point of view by consumer, the absolute content of Cd, Hg, Pb in caps of M. procera collected from background (unpolluted) areas could be considered elevated while sporadic/occasional ingestion of this mushroom is considered safe. The multivariate functional analysis revealed on associated accumulation of many elements in this mushroom. M. procera seem to possess some features of a bio-indicative species for anthropogenic Pb but also for some geogenic metals.

  11. Traceability of Opuntia ficus-indica L. Miller by ICP-MS multi-element profile and chemometric approach.

    Science.gov (United States)

    Mottese, Antonio Francesco; Naccari, Clara; Vadalà, Rossella; Bua, Giuseppe Daniel; Bartolomeo, Giovanni; Rando, Rossana; Cicero, Nicola; Dugo, Giacomo

    2018-01-01

    Opuntia ficus-indica L. Miller fruits, particularly 'Ficodindia dell'Etna' of Biancavilla (POD), 'Fico d'india tradizionale di Roccapalumba' with protected brand and samples from an experimental field in Pezzolo (Sicily) were analyzed by inductively coupled plasma mass spectrometry in order to determine the multi-element profile. A multivariate chemometric approach, specifically principal component analysis (PCA), was applied to individuate how mineral elements may represent a marker of geographic origin, which would be useful for traceability. PCA has allowed us to verify that the geographical origin of prickly pear fruits is significantly influenced by trace element content, and the results found in Biancavilla PDO samples were linked to the geological composition of this volcanic areas. It was observed that two principal components accounted for 72.03% of the total variance in the data and, in more detail, PC1 explains 45.51% and PC2 26.52%, respectively. This study demonstrated that PCA is an integrated tool for the traceability of food products and, at the same time, a useful method of authentication of typical local fruits such as prickly pear. © 2017 Society of Chemical Industry. © 2017 Society of Chemical Industry.

  12. A novel network of chaotic elements and its application in multi-valued associative memory

    International Nuclear Information System (INIS)

    Xiu Chunbo; Liu Xiangdong; Tang Yunyu; Zhang Yuhe

    2004-01-01

    We give a novel chaotic element model whose activation function composed of Gauss and Sigmoid function. It is shown that the model may exhibit a complex dynamic behavior. The most significant bifurcation processes, leading to chaos, are investigated through the computation of the Lyapunov exponents. Based on this model, we propose a novel network of chaotic elements, which can be applied in associative memory, and then investigate its dynamic behavior. It is worth noting that multi-valued associative memory can also be realized by this network

  13. Numerical Analysis of Deflections of Multi-Layered Beams

    Science.gov (United States)

    Biliński, Tadeusz; Socha, Tomasz

    2015-03-01

    The paper concerns the rheological bending problem of wooden beams reinforced with embedded composite bars. A theoretical model of the behaviour of a multi-layered beam is presented. The component materials of this beam are described with equations for the linear viscoelastic five-parameter rheological model. Two numerical analysis methods for the long-term response of wood structures are presented. The first method has been developed with SCILAB software. The second one has been developed with the finite element calculation software ABAQUS and user subroutine UMAT. Laboratory investigations were conducted on sample beams of natural dimensions in order to validate the proposed theoretical model and verify numerical simulations. Good agreement between experimental measurements and numerical results is observed.

  14. Materials characterization of radioactive waste forms using a multi-element detection method based on the instrumental neutron activation analysis. MEDINA; Stoffliche Charakterisierung radioaktiver Abfallprodukte durch ein Multi-Element-Analyseverfahren basierend auf der instrumentellen Neutronen-Aktivierungs-Analyse. MEDINA

    Energy Technology Data Exchange (ETDEWEB)

    Havenith, Andreas Wilhelm

    2015-07-01

    Radioactive waste has to meet the specifications and acceptance criteria defined by national regulatory and management authorities for its intermediate and final storage. In Germany the Federal Office for Radiation Protection (Bundesamt fuer Strahlenschutz - BfS) has established waste acceptance requirements for the Konrad repository. Konrad is the disposal for radioactive waste with negligible heat generation and is located near the city of Salzgitter and is currently under construction. It will start operation not before the year 2021. The waste-acceptance-requirements are derived from a site-specific safety assessment. They include specific requirements on waste forms, packaging as well as limitations to activities of individual radionuclides and limitations to masses of non-radioactive harmful substances. The amount of chemically toxic elements in the waste is limited in order to avoid pollution of underground water reserves. To comply with these requirements every waste package has to be characterised in its radiological and chemical composition. This characterisation can be performed on the basis of existing documentation or, if the documentation is insufficient, on further analytical analysis. Segmented or integral gamma-scanning as well as active or passive neutron counting are used worldwide as the standard measurement methods for the radiological characterisation and quality checking of radioactive waste. These techniques determine the isotope specific activity of waste packages, but they do not allow the detection of non-radioactive hazardous substances inside the waste packages. Against this background the Institute of Nuclear Engineering and Technology Transfer (NET) at RWTH Aachen University and the Institute of Safety Research and Reactor Technology at Forschungszentrum Juelich jointly develop an innovative non-destructive analytical technique called MEDINA - ''Multi-Element Detection based on Instrumental Neutron Activation'' for

  15. Multi-group transport methods for high-resolution neutron activation analysis

    International Nuclear Information System (INIS)

    Burns, K. A.; Smith, L. E.; Gesh, C. J.; Shaver, M. W.

    2009-01-01

    The accurate and efficient simulation of coupled neutron-photon problems is necessary for several important radiation detection applications. Examples include the detection of nuclear threats concealed in cargo containers and prompt gamma neutron activation analysis for nondestructive determination of elemental composition of unknown samples. In these applications, high-resolution gamma-ray spectrometers are used to preserve as much information as possible about the emitted photon flux, which consists of both continuum and characteristic gamma rays with discrete energies. Monte Carlo transport is the most commonly used modeling tool for this type of problem, but computational times for many problems can be prohibitive. This work explores the use of multi-group deterministic methods for the simulation of neutron activation problems. Central to this work is the development of a method for generating multi-group neutron-photon cross-sections in a way that separates the discrete and continuum photon emissions so that the key signatures in neutron activation analysis (i.e., the characteristic line energies) are preserved. The mechanics of the cross-section preparation method are described and contrasted with standard neutron-gamma cross-section sets. These custom cross-sections are then applied to several benchmark problems. Multi-group results for neutron and photon flux are compared to MCNP results. Finally, calculated responses of high-resolution spectrometers are compared. Preliminary findings show promising results when compared to MCNP. A detailed discussion of the potential benefits and shortcomings of the multi-group-based approach, in terms of accuracy, and computational efficiency, is provided. (authors)

  16. Efficiency Evaluation of Food Waste Materials for the Removal of Metals and Metalloids from Complex Multi-Element Solutions

    Science.gov (United States)

    Giuliano, Antonella; Astolfi, Maria Luisa; Congedo, Rossana; Masotti, Andrea; Canepari, Silvia

    2018-01-01

    Recent studies have shown the potential of food waste materials as low cost adsorbents for the removal of heavy metals and toxic elements from wastewater. However, the adsorption experiments have been performed in heterogeneous conditions, consequently it is difficult to compare the efficiency of the individual adsorbents. In this study, the adsorption capacities of 12 food waste materials were evaluated by comparing the adsorbents’ efficiency for the removal of 23 elements from complex multi-element solutions, maintaining homogeneous experimental conditions. The examined materials resulted to be extremely efficient for the adsorption of many elements from synthetic multi-element solutions as well as from a heavy metal wastewater. The 12 adsorbent surfaces were analyzed by Fourier transform infrared spectroscopy and showed different types and amounts of functional groups, which demonstrated to act as adsorption active sites for various elements. By multivariate statistical computations of the obtained data, the 12 food waste materials were grouped in five clusters characterized by different elements’ removal efficiency which resulted to be in correlation with the specific adsorbents’ chemical structures. Banana peel, watermelon peel and grape waste resulted the least selective and the most efficient food waste materials for the removal of most of the elements. PMID:29495363

  17. Efficiency Evaluation of Food Waste Materials for the Removal of Metals and Metalloids from Complex Multi-Element Solutions

    Directory of Open Access Journals (Sweden)

    Lorenzo Massimi

    2018-02-01

    Full Text Available Recent studies have shown the potential of food waste materials as low cost adsorbents for the removal of heavy metals and toxic elements from wastewater. However, the adsorption experiments have been performed in heterogeneous conditions, consequently it is difficult to compare the efficiency of the individual adsorbents. In this study, the adsorption capacities of 12 food waste materials were evaluated by comparing the adsorbents’ efficiency for the removal of 23 elements from complex multi-element solutions, maintaining homogeneous experimental conditions. The examined materials resulted to be extremely efficient for the adsorption of many elements from synthetic multi-element solutions as well as from a heavy metal wastewater. The 12 adsorbent surfaces were analyzed by Fourier transform infrared spectroscopy and showed different types and amounts of functional groups, which demonstrated to act as adsorption active sites for various elements. By multivariate statistical computations of the obtained data, the 12 food waste materials were grouped in five clusters characterized by different elements’ removal efficiency which resulted to be in correlation with the specific adsorbents’ chemical structures. Banana peel, watermelon peel and grape waste resulted the least selective and the most efficient food waste materials for the removal of most of the elements.

  18. Multi-element measurements in mexican cigarette tobacco

    International Nuclear Information System (INIS)

    Vega-Carrillo, H.R.; Texas Univ., Austin, TX; Zacatecas Univ.; Iskander, F.Y.; Manzanares-Acuna, E.

    1995-01-01

    The concentration of 21 elements in cigarette tobacco in nine different brands manufactured and commercially available in Mexico has been determined using neutron activation analysis. The concentration range of the measured elements (in μg g -1 ) were: As, (four brands) <0.55-3.24; Ba, 64-251; Br, (four brands) 49-136; Ce, <0.3-1.7; Co, 0.29-0.55, Cr, <0.8-2.4; Cs, 0.091-0.40; Eu, <0.03; Fe, 420-680; Hf, <0.03-0.13; K, (four brands) 18300-40300; La, (four brands) < 0.2-0.66; Na, (four brands) 309-566; Rb, 19-50; Sb, <0.7; Sc, 0.13-0.22; Se, <0.7; Sm, (four brands) 0.07-0.14; Sr, 227-472; Th, < 0.1-0.17 and Zn, 14-56. The results are compared with the literature values for the concentration of the above elements in cigarette tobacco from other countries. (author) 18 refs.; 2 tabs

  19. Optical selection of trace elements for discriminant analysis

    International Nuclear Information System (INIS)

    Rasmussen, S.E.; Erasmus, C.S.; Watterson, J.I.W.; Sellschop, J.P.F.

    This report describes different methods of element selection; a combination of stepwise multivariate analysis of variance for primary element selection, and principle component analysis regression for the element interrelationship analysis. These offer a satisfactory solution to the problem of element selection

  20. An Assessment of the SEA Multi-Element Sensor for Liquid Water Content Calibration of the NASA GRC Icing Research Tunnel

    Science.gov (United States)

    Steen, Laura E.; Ide, Robert F.; Van Zante, Judith F.

    2015-01-01

    The NASA Glenn Icing Research tunnel has been using an Icing Blade technique to measure cloud liquid water content (LWC) since 1980. The IRT conducted tests with SEA Multi-Element sensors from 2009 to 2011 to assess their performance in measuring LWC. These tests revealed that the Multi-Element sensors showed some significant advantages over the Icing Blade, particularly at higher water contents, higher impingement rates, and large drop sizes. Results of these and other tests are presented here.

  1. Free and Forced Vibrations of an Axially-Loaded Timoshenko Multi-Span Beam Carrying a Number of Various Concentrated Elements

    Directory of Open Access Journals (Sweden)

    Yusuf Yesilce

    2012-01-01

    Full Text Available In the existing reports regarding free and forced vibrations of the beams, most of them studied a uniform beam carrying various concentrated elements using Bernoulli-Euler Beam Theory (BET but without axial force. The purpose of this paper is to utilize the numerical assembly technique to determine the exact frequency-response amplitudes of the axially-loaded Timoshenko multi-span beam carrying a number of various concentrated elements (including point masses, rotary inertias, linear springs and rotational springs and subjected to a harmonic concentrated force and the exact natural frequencies and mode shapes of the beam for the free vibration analysis. The model allows analyzing the influence of the shear and axial force and harmonic concentrated force effects and intermediate concentrated elements on the dynamic behavior of the beams by using Timoshenko Beam Theory (TBT. At first, the coefficient matrices for the intermediate concentrated elements, an intermediate pinned support, applied harmonic force, left-end support and right-end support of Timoshenko beam are derived. After the derivation of the coefficient matrices, the numerical assembly technique is used to establish the overall coefficient matrix for the whole vibrating system. Finally, solving the equations associated with the last overall coefficient matrix one determines the exact dynamic response amplitudes of the forced vibrating system corresponding to each specified exciting frequency of the harmonic force. Equating the determinant of the overall coefficient matrix to zero one determines the natural frequencies of the free vibrating system (the case of zero harmonic force and substituting the corresponding values of integration constants into the related eigenfunctions one determines the associated mode shapes. The calculated vibration amplitudes of the forced vibrating systems and the natural frequencies of the free vibrating systems are given in tables for different values of

  2. Progress in multi-element silicon detectors for synchrotron XRF applications

    International Nuclear Information System (INIS)

    Ludewigt, B.; Rossington, C.; Kipnis, I.; Krieger, B.

    1995-10-01

    Multi-element silicon strip detectors, in conjunction with integrated circuit pulse-processing electronics, offer an attractive alternative to conventional lithium-drifted silicon and high purity germanium detectors for high count rate, low noise synchrotron x-ray fluorescence applications. We have been developing these types of detectors specifically for low noise synchrotron applications, such as extended x-ray absorption fine structure spectroscopy, microprobe x-ray fluorescence and total reflection x-ray fluorescence. The current version of the 192-element detector and integrated circuit preamplifier, cooled to -25 degrees C with a single-stage thermoelectric cooler, achieves an energy resolution of <200 eV full width of half maximum (FWHM) per channel (at 5.9 keV, 2 μs peaking time), and each detector element is designed to handle ∼20 kHz count rate. The detector system will soon be completed to 64 channels using new application specific integrated circuit (ASIC) amplifier chips, new CAMAC (Computer Automated Measurement and Control standard) analog-to-digital converters recently developed at Lawrence Berkeley National Laboratory (LBNL), CAMAC histogramming modules, and Macintosh-based data acquisition software. We report on the characteristics of this detector system, and the work in progress towards the next generation system

  3. Materials characterization of radioactive waste forms using a multi-element detection method based on the instrumental neutron activation analysis. MEDINA

    International Nuclear Information System (INIS)

    Havenith, Andreas Wilhelm

    2015-01-01

    Radioactive waste has to meet the specifications and acceptance criteria defined by national regulatory and management authorities for its intermediate and final storage. In Germany the Federal Office for Radiation Protection (Bundesamt fuer Strahlenschutz - BfS) has established waste acceptance requirements for the Konrad repository. Konrad is the disposal for radioactive waste with negligible heat generation and is located near the city of Salzgitter and is currently under construction. It will start operation not before the year 2021. The waste-acceptance-requirements are derived from a site-specific safety assessment. They include specific requirements on waste forms, packaging as well as limitations to activities of individual radionuclides and limitations to masses of non-radioactive harmful substances. The amount of chemically toxic elements in the waste is limited in order to avoid pollution of underground water reserves. To comply with these requirements every waste package has to be characterised in its radiological and chemical composition. This characterisation can be performed on the basis of existing documentation or, if the documentation is insufficient, on further analytical analysis. Segmented or integral gamma-scanning as well as active or passive neutron counting are used worldwide as the standard measurement methods for the radiological characterisation and quality checking of radioactive waste. These techniques determine the isotope specific activity of waste packages, but they do not allow the detection of non-radioactive hazardous substances inside the waste packages. Against this background the Institute of Nuclear Engineering and Technology Transfer (NET) at RWTH Aachen University and the Institute of Safety Research and Reactor Technology at Forschungszentrum Juelich jointly develop an innovative non-destructive analytical technique called MEDINA - ''Multi-Element Detection based on Instrumental Neutron Activation'' for

  4. SU(3) techniques for angular momentum projected matrix elements in multi-cluster problems

    International Nuclear Information System (INIS)

    Hecht, K.T.; Zahn, W.

    1978-01-01

    In the theory of integral transforms for the evaluation of the resonating group kernels needed for cluster model calculations, the evaluation of matrix elements in an angular momentum coupled basis has proved to be difficult for cluster problems involving more than two fragments. For multi-cluster wave functions SU(3) coupling and recoupling techniques can furnish a tool for the practical evaluation matrix elements in an angular momentum coupled basis if the several relative motion harmonic oscillator functions in Bargmann space have simple SU(3) coupling properties. The method is illustrated by a three-cluster problem, such as 12 C = α + α + α, involving three 1 S clusters. 2 references

  5. Investigation of elements contamination and analysis of electrical effect of this contamination in silicon on the neutron transmutation doping in the RSG-GAS

    International Nuclear Information System (INIS)

    Sudjadi, U.

    1998-01-01

    The elements of the contamination on the Neutron Transmutation Doping Process (NTD) have investigated by Multi Channel Analyser (MCA). This Investigation is important to know the quality of silicon doping in NTD. We have found that Mn-45, Ga-72 and Au-198 are elements of contamination in silicon after NTD process. Analysis of electrical effect of this elements contamination on semiconductor silicon is described also in this paper

  6. Multi-objective optimization of linear multi-state multiple sliding window system

    International Nuclear Information System (INIS)

    Konak, Abdullah; Kulturel-Konak, Sadan; Levitin, Gregory

    2012-01-01

    This paper considers the optimal element sequencing in a linear multi-state multiple sliding window system that consists of n linearly ordered multi-state elements. Each multi-state element can have different states: from complete failure up to perfect functioning. A performance rate is associated with each state. The failure of type i in the system occurs if for any i (1≤i≤I) the cumulative performance of any r i consecutive elements is lower than w i . The element sequence strongly affects the probability of any type of system failure. The sequence that minimizes the probability of certain type of failure can provide high probability of other types of failures. Therefore the optimization problem for the multiple sliding window system is essentially multi-objective. The paper formulates and solves the multi-objective optimization problem for the multiple sliding window systems. A multi-objective Genetic Algorithm is used as the optimization engine. Illustrative examples are presented.

  7. A Dual Super-Element Domain Decomposition Approach for Parallel Nonlinear Finite Element Analysis

    Science.gov (United States)

    Jokhio, G. A.; Izzuddin, B. A.

    2015-05-01

    This article presents a new domain decomposition method for nonlinear finite element analysis introducing the concept of dual partition super-elements. The method extends ideas from the displacement frame method and is ideally suited for parallel nonlinear static/dynamic analysis of structural systems. In the new method, domain decomposition is realized by replacing one or more subdomains in a "parent system," each with a placeholder super-element, where the subdomains are processed separately as "child partitions," each wrapped by a dual super-element along the partition boundary. The analysis of the overall system, including the satisfaction of equilibrium and compatibility at all partition boundaries, is realized through direct communication between all pairs of placeholder and dual super-elements. The proposed method has particular advantages for matrix solution methods based on the frontal scheme, and can be readily implemented for existing finite element analysis programs to achieve parallelization on distributed memory systems with minimal intervention, thus overcoming memory bottlenecks typically faced in the analysis of large-scale problems. Several examples are presented in this article which demonstrate the computational benefits of the proposed parallel domain decomposition approach and its applicability to the nonlinear structural analysis of realistic structural systems.

  8. Neutron activation analysis of trace elements in rain water

    International Nuclear Information System (INIS)

    Luten, J.B.

    1977-01-01

    In this thesis the principles and practical aspects of activation analysis which are of direct importance in the analysis of rain water, are presented together with recent literature data on other techniques. Problems due to the storage of rain water samples are discussed. A multi-element method for the determination of trace elements in rain water by instrumental neutron activation analysis is described. Gamma ray spectrometry using Ge(Li) detectors offers the possibility to determine Na, Al, Cl, V, Mn, Co, Cu, Br and I in rain water samples of 2.5 ml after a 4-min irradiation in a thermal neutron flux of 5 x 10 13 n cm -2 s -1 . In residues of rain water samples of 100 ml, irradiated during 2 days in a thermal neutron flux of >5 x 10 13 n cm -2 s -1 Cr, Fe, Co, Zn and Sb can be determined after a cooling period of approximately 21 days. The detection limits are lower than those reported in previous investigations except for Cu. The precision is about 10% or better, except for Co, Cu and I. A routine method for the determination of bromine and iodine in rain water by n.a.a. is presented. The elements are isolated by isotope exchange between the irradiated sample and a solution of Br 2 or I 2 in CCl 4 . The method is not sensitive to the chemical species in which the halogen is present. Irradiation of solutions of iodine compounds in a high thermal neutron flux gives rise to the formation of iodate. Results of a further investigation of this phenomenon are given, as well as the determination of iodate in rain water by n.a.a. Iodate is separated by anion exchange. The combination of n.a.a. and solvent extraction is used for the determination of five trace elements (V, Co, Cu, Zn and In) in 10-ml rain water samples. For V, Co and Cu this method is more sensitive and reproducible than instrumental n.a.a. The results of the analysis of eleven sequential 30-ml samples from the beginning of the shower are presented as an illustration of possible applications of the

  9. Multi-element, multi-compound isotope profiling as a means to distinguish the geographical and varietal origin of fermented cocoa (Theobroma cacao L.) beans.

    Science.gov (United States)

    Diomande, Didier; Antheaume, Ingrid; Leroux, Maël; Lalande, Julie; Balayssac, Stéphane; Remaud, Gérald S; Tea, Illa

    2015-12-01

    Multi-element stable isotope ratios have been assessed as a means to distinguish between fermented cocoa beans from different geographical and varietal origins. Isotope ratios and percentage composition for C and N were measured in different tissues (cotyledons, shells) and extracts (pure theobromine, defatted cocoa solids, protein, lipids) obtained from fermented cocoa bean samples. Sixty-one samples from 24 different geographical origins covering all four continental areas producing cocoa were analyzed. Treatment of the data with unsupervised (Principal Component Analysis) and supervised (Partial Least Squares Discriminant Analysis) multiparametric statistical methods allowed the cocoa beans from different origins to be distinguished. The most discriminant variables identified as responsible for geographical and varietal differences were the δ(15)N and δ(13)C values of cocoa beans and some extracts and tissues. It can be shown that the isotope ratios are correlated with the altitude and precipitation conditions found in the different cocoa-growing regions. Copyright © 2015 Elsevier Ltd. All rights reserved.

  10. Numerical Analysis of Deflections of Multi-Layered Beams

    Directory of Open Access Journals (Sweden)

    Biliński Tadeusz

    2015-03-01

    Full Text Available The paper concerns the rheological bending problem of wooden beams reinforced with embedded composite bars. A theoretical model of the behaviour of a multi-layered beam is presented. The component materials of this beam are described with equations for the linear viscoelastic five-parameter rheological model. Two numerical analysis methods for the long-term response of wood structures are presented. The first method has been developed with SCILAB software. The second one has been developed with the finite element calculation software ABAQUS and user subroutine UMAT. Laboratory investigations were conducted on sample beams of natural dimensions in order to validate the proposed theoretical model and verify numerical simulations. Good agreement between experimental measurements and numerical results is observed.

  11. Effect of randomness on multi-frequency aeroelastic responses resolved by Unsteady Adaptive Stochastic Finite Elements

    International Nuclear Information System (INIS)

    Witteveen, Jeroen A.S.; Bijl, Hester

    2009-01-01

    The Unsteady Adaptive Stochastic Finite Elements (UASFE) method resolves the effect of randomness in numerical simulations of single-mode aeroelastic responses with a constant accuracy in time for a constant number of samples. In this paper, the UASFE framework is extended to multi-frequency responses and continuous structures by employing a wavelet decomposition pre-processing step to decompose the sampled multi-frequency signals into single-frequency components. The effect of the randomness on the multi-frequency response is then obtained by summing the results of the UASFE interpolation at constant phase for the different frequency components. Results for multi-frequency responses and continuous structures show a three orders of magnitude reduction of computational costs compared to crude Monte Carlo simulations in a harmonically forced oscillator, a flutter panel problem, and the three-dimensional transonic AGARD 445.6 wing aeroelastic benchmark subject to random fields and random parameters with various probability distributions.

  12. Neutron activation analysis of trace elements in foodstuffs

    International Nuclear Information System (INIS)

    Schelenz, R.; Bayat, I.; Fischer, E.

    1976-05-01

    For the determination of trace elements in foodstuffs with the aid of neutron activation analysis the separation of volatile radionuclides after digestion of the sample is of special interest for radiochemical processing. A distillation procedure was developed to give reproducable results, however optimal conditions were not found for all volatile radionuclides studied. The required selective separation of Br-82 from the distillate was best achieved by the application of an ion-exchange column-chromatography technique. The computer programs for the evaluation of complex gamma spectra have been developed further. The automatic peak search and peak area determination is based on a computer program using the correlation technique and carried out with a mini-computer coupled with a multi-channel gamma spectrometer. The results, which are presented in 3 earlier reports relating to this research program, reveal the advantages and disadvantages of the individual steps of the radiochemical separation scheme. Before neutron activation analysis can be introduced on a routine basis, some aspects of the radiochemical process remain to be tested; these studies will be published in a fourth and final report. (orig.) [de

  13. Design considerations regarding an atomizer for multi-element electrothermal atomic absorption spectrometry

    Energy Technology Data Exchange (ETDEWEB)

    Katskov, Dmitri A., E-mail: katskovda@tut.ac.za [Department of Chemistry, Tshwane University of Technology, Private Bag X680, Pretoria 0001 (South Africa); Sadagov, Yuri M. [All-Russian Scientific Research Institute of Optical and Physical Measurements (VNIIOFI), Ozernaya St. 46, Moscow 119361 (Russian Federation)

    2011-06-15

    The methodology of simultaneous multi-element electrothermal atomic absorption spectrometry (ETAAS-Electrothermal Atomic Absorption Spectrometry) stipulates rigid requirements to the design and operation of the atomizer. It must provide high degree of atomization for the group of analytes, invariant respective to the vaporization kinetics and heating ramp residence time of atoms in the absorption volume and absence of memory effects from major sample components. For the low resolution spectrometer with a continuum radiation source the reduced compared to traditional ETAAS (Electrothermal Atomic Absorption Spectrometry) sensitivity should be, at least partially, compensated by creating high density of atomic vapor in the absorption pulse. The sought-for characteristics were obtained for the 18 mm in length and 2.5 mm in internal diameter longitudinally heated graphite tube atomizer furnished with 2-4.5 mg of ring shaped carbon fiber yarn collector. The collector located next to the sampling port provides large substrate area that helps to keep the sample and its residue in the central part of the tube after drying. The collector also provides a 'platform' effect that delays the vaporization and stipulates vapor release into absorption volume having already stabilized gas temperature. Due to the shape of external surface of the tube, presence of collector and rapid (about 10 {sup o}C/ms) heating, an inverse temperature distribution along the tube is attained at the beginnings of the atomization and cleaning steps. The effect is employed for cleaning of the atomizer using the set of short maximum power heating pulses. Preparation, optimal maintenance of the atomizer and its compliance to the multi-element determination requirements are evaluated and discussed. The experimental setup provides direct simultaneous determination of large group of element within 3-4 order concentration range. Limits of detection are close to those for sequential single element

  14. Elemental investigation of (Al-Cu) alloys and some geological samples using neutron activation and XRF analysis techniques

    International Nuclear Information System (INIS)

    Hammad, E.A.M.

    2012-01-01

    Neutron activation analysis (NAA) using k 0 - standardization (k 0 -NAA) is well known method for multi-elemental analysis. The method is used to analyze different samples belonging to different fields. In addition, X- ray fluorescence (XRF) is also used for multi-elemental analysis. XRF complements NAA methods. Both methods were used for investigation of some iron ores and aluminum- cupper alloy (Al-Cu) samples. Elemental concentration of Iron ores and Al-Cu alloy samples were determined by k 0 - NAA and XRF methods. The iron ore samples were collected from Wadi Kareim and Umm Nar sites (the Eastern desert of Egypt). Six and two samples representing the ores of Wadi Kareim and Umm Nar, respectively altogether with the standard samples consisting of Fe, Au , Zr and W and the certified reference sample IAEA Soil-7 were irradiated in one of the irradiated boxes at the Second Egyptian Research Reactor (ETRR- 2). The induced activities were counted using an efficiency calibrated HPGe detector systems. The neutron spectrum parameters α and f characterizing the neutron irradiation position that are needed in applying k 0 -NAA method were determined using the activation product of Zr , Au, Fe and W and found α≅ - 0.048 ±0.002 and f ≅ 38± k 0 -NAA method was applied to determine the elemental concentrations in the two iron ore samples. The concentrations determined were found to vary erratically form one sample to another. The results were discussed and compared with similar results in literature. The accuracy of the k 0 - NAA method was checked by determining the elemental concentration in the IAEA-Soil 7 reference sample. The obtained results are compared with the recommended values. Good agreements were found within 10 %. Short time neutron activation analysis (STNAA) was carried out to determine concentration of major elements in Al-Cu alloy samples. Three (Al-Cu) alloys samples with different concentrations of Cu (2, 3.5 and 5 %) altogether. Au standard sample

  15. Why do probabilistic finite element analysis ?

    CERN Document Server

    Thacker, Ben H

    2008-01-01

    The intention of this book is to provide an introduction to performing probabilistic finite element analysis. As a short guideline, the objective is to inform the reader of the use, benefits and issues associated with performing probabilistic finite element analysis without excessive theory or mathematical detail.

  16. Trace elements determination in red and white wines using total-reflection X-ray fluorescence

    International Nuclear Information System (INIS)

    Anjos, M.J.; Lopes, R.T.; Jesus, E.F.O. de; Moreira, S.; Barroso, R.C.; Castro, C.R.F.

    2003-01-01

    Several wines produced in different regions from south of Brazil and available in markets in Rio de Janeiro were analyzed for their contents of elements such as: P, S, Cl, Ca, Ti, Cr, Mn, Fe, Ni, Cu, Zn, Rb and Sr. Multi-element analysis was possible with simple sample preparation and subsequent analysis by total-reflection X-ray fluorescence using synchrotron radiation. The measurement was carried at the X-ray fluorescence beamline in the Synchrotron Light Source Laboratory in Campinas, Brazil. The levels of the various elements obtained were lower in the Brazilian wines than the values generally found in the literature. The present study indicates the capability of multi-element analysis for determining the contents of various elements present in wines coming from Brazil vineyards by using a simple, sensitive and precise method

  17. Multi trace element analysis of dry biological materials by neutron activation analysis including a chemical group separation

    International Nuclear Information System (INIS)

    Weers, C.A.

    1980-01-01

    The principles of activation analysis and the practical aspects of neutron activation analysis are outlined. The limits which are set to accuracy and precision are defined. The description of the evaporation process is summarised in terms of the half-volume. This quantity is then used to define the resolving power. The formulation is checked by radiotracer experiments. Dried animal blood is used as the testing material. The pretreatment of the samples and (the development of) the destruction-evaporation apparatus is described. Four successive devices were built and tested. The development of the successive adsorption steps with active charcoal, Al 2 O 3 and coprecipitation with Fe(OH) 3 is presented. Seven groups of about 25 elements in total can be determined this way. The results obtained for standard reference materials are summarized and compared with literature data. (Auth.)

  18. Determination of the critical bending speeds of a multy-rotor shaft from the vibration signal analysis

    Science.gov (United States)

    Crâştiu, I.; Nyaguly, E.; Deac, S.; Gozman-Pop, C.; Bârgău, A.; Bereteu, L.

    2018-01-01

    The purpose of this paper is the development and validation of an impulse excitation technique to determine flexural critical speeds of a single rotor shaft and multy-rotor shaft. The experimental measurement of the vibroacoustic response is carried out by using a condenser microphone as a transducer. By the means of Modal Analysis using Finite Element Method (FEM), the natural frequencies and shape modes of one rotor and three rotor specimens are determined. The vibration responses of the specimens, in simple supported conditions, are carried out using algorithms based on Fast Fourier Transform (FFT). To validate the results of the modal parameters estimated using Finite Element Analysis (FEA) these are compared with experimental ones.

  19. Generalized modeling of multi-component vaporization/condensation phenomena for multi-phase-flow analysis

    International Nuclear Information System (INIS)

    Morita, K.; Fukuda, K.; Tobita, Y.; Kondo, Sa.; Suzuki, T.; Maschek, W.

    2003-01-01

    A new multi-component vaporization/condensation (V/C) model was developed to provide a generalized model for safety analysis codes of liquid metal cooled reactors (LMRs). These codes simulate thermal-hydraulic phenomena of multi-phase, multi-component flows, which is essential to investigate core disruptive accidents of LMRs such as fast breeder reactors and accelerator driven systems. The developed model characterizes the V/C processes associated with phase transition by employing heat transfer and mass-diffusion limited models for analyses of relatively short-time-scale multi-phase, multi-component hydraulic problems, among which vaporization and condensation, or simultaneous heat and mass transfer, play an important role. The heat transfer limited model describes the non-equilibrium phase transition processes occurring at interfaces, while the mass-diffusion limited model is employed to represent effects of non-condensable gases and multi-component mixture on V/C processes. Verification of the model and method employed in the multi-component V/C model of a multi-phase flow code was performed successfully by analyzing a series of multi-bubble condensation experiments. The applicability of the model to the accident analysis of LMRs is also discussed by comparison between steam and metallic vapor systems. (orig.)

  20. Stress analysis of disconnected structures in contact through finite element gaps

    International Nuclear Information System (INIS)

    Stadter, J.T.; Weiss, R.O.

    1976-07-01

    A numerical procedure is presented for analyzing thermal stress problems of disconnected structures in contact across separations or gaps. The new procedure is called SAASGAPS, an adaptation of the basic SAAS III computer program. The SAAS program uses the finite element method and allows analyses of plane and axisymmetric bodies with temperature dependent material properties, subject to thermal and mechanical loads. A secant modulus approach with a bilinear stress-strain curve is used for elastic-plastic problems. The SAASGAPS version contains all of the features of the original SAAS program. A special gap element is used together with a stress invariance principle to model the contact process. The iterative procedure implemented in SAASGAPS is described. Results are discussed for five problems involving frictionless contact. Two of these problems are associated with the thermal stress analysis of the heat shield for the Multi-Hundred Watt Radioisotope Thermoelectric Generator. Input instructions for the program are described in an appendix

  1. A new XRF probe for in-situ determining concentration of multi-elements in ocean sediments

    International Nuclear Information System (INIS)

    Ge Liangquan; Lai Wanchang; Zhou Sichun; Lin Ling; Lin Yanchang; Ren Jiafu

    2001-01-01

    The author introduces a new X-ray fluorescence probe for in-situ determining the concentration of multi-elements in ocean sediments. The probe consists of Si-Pin X-ray detector with an electro-thermal colder, two isotope sources, essential electrical signal processing units and a notebook computer. More than 10 elements can be simultaneously determined at a detection limit of (10-200) x 10 -6 and precision of 5%-30% without liquid Nitrogen supply. tests show that the probe can perform the analytical tasks under the water at the depth of less than 1000 meters

  2. Phytochemical screening, proximate and elemental analysis of ...

    African Journals Online (AJOL)

    Citrus sinensis was screened for its phytochemical composition and was evaluated for the proximate and elemental analysis. The phytochemical analysis indicated the presence of reducing sugar, saponins, cardiac glycosides, tannins and flavonoids. The elemental analysis indicated the presence of the following mineral ...

  3. Generation of a multi-photon Greenberger-Horne-Zeilinger state with linear optical elements and photon detectors

    International Nuclear Information System (INIS)

    Zou, X B; Pahlke, K; Mathis, W

    2005-01-01

    We present a scheme to generate a multi-photon Greenberger-Horne-Zeilinger (GHZ) state by using single-photon sources, linear optical elements and photon detectors. Such a maximum entanglement has wide applications in the demonstration of quantum nonlocality and quantum information processing

  4. Multi-elemental analysis of aqueous geochemical samples by quadrupole inductively coupled plasma-mass spectrometry (ICP-MS)

    Science.gov (United States)

    Wolf, Ruth E.; Adams, Monique

    2015-01-01

    Typically, quadrupole inductively coupled plasma-mass spectrometry (ICP-MS) is used to determine as many as 57 major, minor, and trace elements in aqueous geochemical samples, including natural surface water and groundwater, acid mine drainage water, and extracts or leachates from geological samples. The sample solution is aspirated into the inductively coupled plasma (ICP) which is an electrodeless discharge of ionized argon gas at a temperature of approximately 6,000 degrees Celsius. The elements in the sample solution are subsequently volatilized, atomized, and ionized by the ICP. The ions generated are then focused and introduced into a quadrupole mass filter which only allows one mass to reach the detector at a given moment in time. As the settings of the mass analyzer change, subsequent masses are allowed to impact the detector. Although the typical quadrupole ICP-MS system is a sequential scanning instrument (determining each mass separately), the scan speed of modern instruments is on the order of several thousand masses per second. Consequently, typical total sample analysis times of 2–3 minutes are readily achievable for up to 57 elements.

  5. Overview of multi-element monolithic germanium detectors for XAFS experiments at diamond light source

    International Nuclear Information System (INIS)

    Chatterji, S.; Dennis, G. J.; Dent, A.; Diaz-Moreno, S.; Cibin, G.; Tartoni, N.; Helsby, W. I.

    2016-01-01

    An overview of multi-element monolithic germanium detectors being used at the X-ray absorption spectroscopy (XAS) beam lines at Diamond Light Source (DLS) is being reported. The hardware details and a summary of the performance of these detectors have also been provided. Recent updates about various ongoing projects being worked on to improve the performance of these detectors are summarized.

  6. Overview of multi-element monolithic germanium detectors for XAFS experiments at diamond light source

    Energy Technology Data Exchange (ETDEWEB)

    Chatterji, S.; Dennis, G. J.; Dent, A.; Diaz-Moreno, S.; Cibin, G.; Tartoni, N. [Diamond Light Source Ltd, Oxfordshire (United Kingdom); Helsby, W. I. [STFC Daresbury Laboratory, Warrington (United Kingdom)

    2016-07-27

    An overview of multi-element monolithic germanium detectors being used at the X-ray absorption spectroscopy (XAS) beam lines at Diamond Light Source (DLS) is being reported. The hardware details and a summary of the performance of these detectors have also been provided. Recent updates about various ongoing projects being worked on to improve the performance of these detectors are summarized.

  7. A new large solid angle multi-element silicon drift detector system for low energy X-ray fluorescence spectroscopy

    Science.gov (United States)

    Bufon, J.; Schillani, S.; Altissimo, M.; Bellutti, P.; Bertuccio, G.; Billè, F.; Borghes, R.; Borghi, G.; Cautero, G.; Cirrincione, D.; Fabiani, S.; Ficorella, F.; Gandola, M.; Gianoncelli, A.; Giuressi, D.; Kourousias, G.; Mele, F.; Menk, R. H.; Picciotto, A.; Rachevski, A.; Rashevskaya, I.; Sammartini, M.; Stolfa, A.; Zampa, G.; Zampa, N.; Zorzi, N.; Vacchi, A.

    2018-03-01

    Low-energy X-ray fluorescence (LEXRF) is an essential tool for bio-related research of organic samples, whose composition is dominated by light elements. Working at energies below 2 keV and being able to detect fluorescence photons of lightweight elements such as carbon (277 eV) is still a challenge, since it requires in-vacuum operations to avoid in-air photon absorption. Moreover, the detectors must have a thin entrance window and collect photons at an angle of incidence near 90 degrees to minimize the absorption by the protective coating. Considering the low fluorescence yield of light elements, it is important to cover a substantial part of the solid angle detecting ideally all emitted X-ray fluorescence (XRF) photons. Furthermore, the energy resolution of the detection system should be close to the Fano limit in order to discriminate elements whose XRF emission lines are often very close within the energy spectra. To ensure all these features, a system consisting of four monolithic multi-element silicon drift detectors was developed. The use of four separate detector units allows optimizing the incidence angle on all the sensor elements. The multi-element approach in turn provides a lower leakage current on each anode, which, in combination with ultra-low noise preamplifiers, is necessary to achieve an energy resolution close to the Fano limit. The potential of the new detection system and its applicability for typical LEXRF applications has been proved on the Elettra TwinMic beamline.

  8. Elemental analysis with external-beam PIXE

    Science.gov (United States)

    Lin, E. K.; Wang, C. W.; Teng, P. K.; Huang, Y. M.; Chen, C. Y.

    1992-05-01

    A beamline system and experimental setup has been established for elemental analysis using PIXE with an external beam. Experiments for the study of the elemental composition of ancient Chinese potsherds (the Min and Ching ages) were performed. Continuum X-ray spectra from the samples bombarded by 3 MeV protons have been measured with a Si(Li) detector. From the analysis of PIXE data, the concentration of the main elements (Al, Si, K, and Ca) and of more than ten trace elements in the matrices and glazed surfaces were determined. Results for two different potsherds are presented, and those obtained from the glaze colorants are compared with the results of measurements on a Ching blue-and-white porcelain vase.

  9. Finite element analysis and genetic algorithm optimization design for the actuator placement on a large adaptive structure

    Science.gov (United States)

    Sheng, Lizeng

    The dissertation focuses on one of the major research needs in the area of adaptive/intelligent/smart structures, the development and application of finite element analysis and genetic algorithms for optimal design of large-scale adaptive structures. We first review some basic concepts in finite element method and genetic algorithms, along with the research on smart structures. Then we propose a solution methodology for solving a critical problem in the design of a next generation of large-scale adaptive structures---optimal placements of a large number of actuators to control thermal deformations. After briefly reviewing the three most frequently used general approaches to derive a finite element formulation, the dissertation presents techniques associated with general shell finite element analysis using flat triangular laminated composite elements. The element used here has three nodes and eighteen degrees of freedom and is obtained by combining a triangular membrane element and a triangular plate bending element. The element includes the coupling effect between membrane deformation and bending deformation. The membrane element is derived from the linear strain triangular element using Cook's transformation. The discrete Kirchhoff triangular (DKT) element is used as the plate bending element. For completeness, a complete derivation of the DKT is presented. Geometrically nonlinear finite element formulation is derived for the analysis of adaptive structures under the combined thermal and electrical loads. Next, we solve the optimization problems of placing a large number of piezoelectric actuators to control thermal distortions in a large mirror in the presence of four different thermal loads. We then extend this to a multi-objective optimization problem of determining only one set of piezoelectric actuator locations that can be used to control the deformation in the same mirror under the action of any one of the four thermal loads. A series of genetic algorithms

  10. Chemical analysis of rare earth elements

    International Nuclear Information System (INIS)

    Tsukahara, Ryoichi; Sakoh, Takefumi; Nagai, Iwao

    1994-01-01

    Recently attention has been paid to ICP-AES or ICP-MS, and the reports on the analysis of rare earth elements by utilizing these methods continue to increase. These reports have become to take about 30% of the reports on rare earth analysis, and this is because these methods are highly sensitive to rare earth elements, and also these methods have spread widely. In ICP-AES and ICP-MS, mostly solution samples are measured, therefore, solids must be made into solution. At the time of quantitatively determining the rare earth elements of low concentration, separation and concentration are necessary. Referring to the literatures reported partially in 1990 and from 1991 to 1993, the progress of ICP-AES and ICP-MS is reported. Rare earth oxides and the alloys containing rare earth elements are easily decomposed with acids, but the decomposition of rocks is difficult, and its method is discussed. The separation of the rare earth elements from others in geochemical samples, cation exchange process is frequently utilized. Also solvent extraction process has been studied. For the separation of rare earth elements mutually, chromatography is used. The spectral interference in spectral analysis was studied. The comparison of these methods with other methods is reported. (K.I)

  11. Finite element analysis of piezoelectric materials

    International Nuclear Information System (INIS)

    Lowrie, F.; Stewart, M.; Cain, M.; Gee, M.

    1999-01-01

    This guide is intended to help people wanting to do finite element analysis of piezoelectric materials by answering some of the questions that are peculiar to piezoelectric materials. The document is not intended as a complete beginners guide for finite element analysis in general as this is better dealt with by the individual software producers. The guide is based around the commercial package ANSYS as this is a popular package amongst piezoelectric material users, however much of the information will still be useful to users of other finite element codes. (author)

  12. Environmental application of elemental speciation analysis based on liquid or gas chromatography hyphenated to inductively coupled plasma mass spectrometry-A review

    International Nuclear Information System (INIS)

    Popp, Maximilian; Hann, Stephan; Koellensperger, Gunda

    2010-01-01

    In recent years the number of environmental applications of elemental speciation analysis using inductively coupled plasma mass spectrometry (ICP-MS) as detector has increased significantly. The analytical characteristics, such as extremely low detection limits (LOD) for almost all elements, the wide linear range, the possibility for multi-elemental analysis and the possibility to apply isotope dilution mass spectrometry (IDMS) make ICP-MS an attractive tool for elemental speciation analysis. Two methodological approaches, i.e. the combination of ICP-MS with high performance liquid chromatography (HPLC) and gas chromatography (GC), dominate the field. Besides the investigation of metals and metalloids and their species (e.g. Sn, Hg, As), representing 'classic' elements in environmental science, more recently other elements (e.g. P, S, Br, I) amenable to ICP-MS determination were addressed. In addition, the introduction of isotope dilution analysis and the development of isotopically labeled species-specific standards have contributed to the success of ICP-MS in the field. The aim of this review is to summarize these developments and to highlight recent trends in the environmental application of ICP-MS coupled to GC and HPLC.

  13. The Multi-Element Electronstatic Lens Systems for Controlling and Focusing Charged Particle

    International Nuclear Information System (INIS)

    Sise, O.

    2004-01-01

    Particle optics are very close anolog of photon optics and most of the principles of an barged particle beam can be understood by thinking of the particles as rays of light. There are similar behaviours between particle and photon optics in controlling beams of light and charged particles, such as lenses and mirrors. Extensive information about the properties of charged particle optics, from which appropriate systems can be designed for any specific problem. In this way electrostatic lens systems are used to control beams of c/iarged particle with various energy and directions in several fields, for example electron microscopy, cathode ray tubes, ion accelerators and electron impact studies. In an electrostatic lens system quantative information is required over a wide energy range and a zoom-type of optics is needed. If the magnification is to remain constant over a wide range of energies, quite complicated electrostatic lens systems are required, .containing three, four, five, or even more lens elements. We firstly calculated the optical properties of three and four element cylinder electrostatic lenses with the help of the SIMION and LENSYS programs and developed the method for the calculation of the focal properties of five and more element lenses with afocal mode. In this method we used the combination of three and four element lenses to derive focal properties of multi-element lenses and presented this data over a wide range of energy

  14. Sequential determination of multi-nutrient elements in natural water samples with a reverse flow injection system.

    Science.gov (United States)

    Lin, Kunning; Ma, Jian; Yuan, Dongxing; Feng, Sichao; Su, Haitao; Huang, Yongming; Shangguan, Qipei

    2017-05-15

    An integrated system was developed for automatic and sequential determination of NO 2 - , NO 3 - , PO 4 3- , Fe 2+ , Fe 3+ and Mn 2+ in natural waters based on reverse flow injection analysis combined with spectrophotometric detection. The system operation was controlled by a single chip microcomputer and laboratory-programmed software written in LabVIEW. The experimental parameters for each nutrient element analysis were optimized based on a univariate experimental design, and interferences from common ions were evaluated. The upper limits of the linear range (along with detection limit, µmolL -1 ) of the proposed method was 20 (0.03), 200 (0.7), 12 (0.3), 5 (0.03), 5 (0.03), 9 (0.2) µmolL -1 , for NO 2 - , NO 3 - , PO 4 3- , Fe 2+ , Fe 3+ and Mn 2+ , respectively. The relative standard deviations were below 5% (n=9-13) and the recoveries varied from 88.0±1.0% to 104.5±1.0% for spiked water samples. The sample throughput was about 20h -1 . This system has been successfully applied for the determination of multi-nutrient elements in different kinds of water samples and showed good agreement with reference methods (slope 1.0260±0.0043, R 2 =0.9991, n=50). Copyright © 2017 Elsevier B.V. All rights reserved.

  15. DETERMINATION OF MULTI ELEMENT LEVELS IN LEAVES AND ...

    African Journals Online (AJOL)

    Preferred Customer

    ICP-OES (Spectro Analytical Instruments, Kleve, Germany) was used for the determination of elements. ... Samples. In this study, 18 different herbal tea samples (leaves and flowers) that are traditionally used for medical ... analysis of CRM were all within the 95% reliability limit. The results ..... reasons for serious health risks.

  16. Finite element analysis theory and application with ANSYS

    CERN Document Server

    Moaveni, Saeed

    2015-01-01

    For courses in Finite Element Analysis, offered in departments of Mechanical or Civil and Environmental Engineering. While many good textbooks cover the theory of finite element modeling, Finite Element Analysis: Theory and Application with ANSYS is the only text available that incorporates ANSYS as an integral part of its content. Moaveni presents the theory of finite element analysis, explores its application as a design/modeling tool, and explains in detail how to use ANSYS intelligently and effectively. Teaching and Learning Experience This program will provide a better teaching and learning experience-for you and your students. It will help: *Present the Theory of Finite Element Analysis: The presentation of theoretical aspects of finite element analysis is carefully designed not to overwhelm students. *Explain How to Use ANSYS Effectively: ANSYS is incorporated as an integral part of the content throughout the book. *Explore How to Use FEA as a Design/Modeling Tool: Open-ended design problems help stude...

  17. Multi-objective Calibration of DHSVM Based on Hydrologic Key Elements in Jinhua River Basin, East China

    Science.gov (United States)

    Pan, S.; Liu, L.; Xu, Y. P.

    2017-12-01

    Abstract: In physically based distributed hydrological model, large number of parameters, representing spatial heterogeneity of watershed and various processes in hydrologic cycle, are involved. For lack of calibration module in Distributed Hydrology Soil Vegetation Model, this study developed a multi-objective calibration module using Epsilon-Dominance Non-Dominated Sorted Genetic Algorithm II (ɛ-NSGAII) and based on parallel computing of Linux cluster for DHSVM (ɛP-DHSVM). In this study, two hydrologic key elements (i.e., runoff and evapotranspiration) are used as objectives in multi-objective calibration of model. MODIS evapotranspiration obtained by SEBAL is adopted to fill the gap of lack of observation for evapotranspiration. The results show that good performance of runoff simulation in single objective calibration cannot ensure good simulation performance of other hydrologic key elements. Self-developed ɛP-DHSVM model can make multi-objective calibration more efficiently and effectively. The running speed can be increased by more than 20-30 times via applying ɛP-DHSVM. In addition, runoff and evapotranspiration can be simulated very well simultaneously by ɛP-DHSVM, with superior values for two efficiency coefficients (0.74 for NS of runoff and 0.79 for NS of evapotranspiration, -10.5% and -8.6% for PBIAS of runoff and evapotranspiration respectively).

  18. Instrumental trace element analysis of California market milk

    International Nuclear Information System (INIS)

    Ragaini, R.C.; Langhorst, A.L.; Ralston, H.R.; Heft, R.

    1975-01-01

    Trace element analysis for 15 elements (Zn, Na, Br, Rb, Sr, Mg, Al, Ca, Cl, I, K, Fe, Co, Se, Cs) was carried out on 32 samples of California market milk and 6 samples of Colorado milk in a pilot study of toxic and nutrient trace elements in the soil-forage-cow-milk food chain. The techniques of instrumental neutron activation analysis and x-ray fluorescence analysis are described. Sample collection, preparation, analysis, and data reduction procedures are discussed. The mean values and variations of trace element concentrations in milk are compared to data from other studies. (U.S.)

  19. A new XRF probe for in-situ determining concentration of multi-elements in ocean sediments

    CERN Document Server

    Ge Liang Quan; Zhou Si Chun; Lin Ling; Lin Yan Chang; Ren Jia Fu

    2001-01-01

    The author introduces a new X-ray fluorescence probe for in-situ determining the concentration of multi-elements in ocean sediments. The probe consists of Si-Pin X-ray detector with an electro-thermal colder, two isotope sources, essential electrical signal processing units and a notebook computer. More than 10 elements can be simultaneously determined at a detection limit of (10-200) x 10 sup - sup 6 and precision of 5%-30% without liquid Nitrogen supply. tests show that the probe can perform the analytical tasks under the water at the depth of less than 1000 meters

  20. Spatially resolved element analysis of historical violin varnishes by use of muPIXE.

    Science.gov (United States)

    von Bohlen, Alex; Röhrs, Stefan; Salomon, Joseph

    2007-02-01

    External muPIXE has been used for characterisation of small samples of varnish from historical violins, and pieces of varnished wood from historical and modern stringed instruments. To obtain spatially resolved information about the distribution of elements across the varnish layers single-spot analysis, line-scans, and area-mapping were performed. Local resolution of approximately 20 mum was obtained from the 3 MeV, 1 nA proton micro-probe. Results from simultaneous multi-element determination of Na, Mg, Al, Si, P, S, K, Ca, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, As, Br, Rb, Sr, Ag, Cd, Sn, Ba, and Pb in historical varnishes are presented. Semi-quantitative evaluation of line-scans recorded on diverse historical varnishes is reported. The applied method is discussed in detail and the results obtained are critically reviewed and compared with those in the literature.

  1. Finite elements for analysis and design

    CERN Document Server

    Akin, J E; Davenport, J H

    1994-01-01

    The finite element method (FEM) is an analysis tool for problem-solving used throughout applied mathematics, engineering, and scientific computing. Finite Elements for Analysis and Design provides a thoroughlyrevised and up-to-date account of this important tool and its numerous applications, with added emphasis on basic theory. Numerous worked examples are included to illustrate the material.Key Features* Akin clearly explains the FEM, a numerical analysis tool for problem-solving throughout applied mathematics, engineering and scientific computing* Basic theory has bee

  2. Aspects of cleaning environmental materials for multi-element analysis, e.g. plant samples

    International Nuclear Information System (INIS)

    Markert, B.

    1992-01-01

    Cleaning of samples is often the first step in the entire procedure of sample preparation in environmental trace element research. The question must generally be raised of whether cleaning is meaningful before chemical investigations with plant material (e.g. for the determination of transfer factors in the soil/plant system) or not (e.g. for food chain analysis in the plant/animal system). The most varied cleaning procedures for plant samples are currently available ranging from dry and wet wiping of the leaf or needle surface up to the complete removal of the cuticule with the aid of chlorofom. There is at present no standardized cleaning procedure for plant samples so that it is frequently not possible to compare analytical data from different working groups studying the same plant species. (orig.)

  3. Buckling Analysis of Single and Multi Delamination In Composite Beam Using Finite Element Method

    Science.gov (United States)

    Simanjorang, Hans Charles; Syamsudin, Hendri; Giri Suada, Muhammad

    2018-04-01

    Delamination is one type of imperfection in structure which found usually in the composite structure. Delamination may exist due to some factors namely in-service condition where the foreign objects hit the composite structure and creates inner defect and poor manufacturing that causes the initial imperfections. Composite structure is susceptible to the compressive loading. Compressive loading leads the instability phenomenon in the composite structure called buckling. The existence of delamination inside of the structure will cause reduction in buckling strength. This paper will explain the effect of delamination location to the buckling strength. The analysis will use the one-dimensional modelling approach using two- dimensional finite element method.

  4. Comparative measurement of inorganic elements in Korean space foods using instrumental neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Yong Sam; Kim, Sun Ha; Baek, Sung Ryel; Sun, Gwang Min; Moon, Jong Hwa; Choi, Jong Il; Lee, Joo Eun [KAERI, Daejeon (Korea, Republic of)

    2012-10-15

    In April 2008, Korea's first astronaut became a crew member of the international space station and she brought special space versions of traditional Korean dishes such as kimchi, boiled rice, hot red pepper paste, soybean paste soup, ginseng tea, green tea, and ramyun. To date, seventy kinds of Korean space foods (KSFs) have been developed by KAERI. The information and role of trace mineral elements from an intake of created and processed foodstuff are important as a indicator of human health and nutrition, as well as a quality control of food and diet. In particular, special food created for consumption by astronauts in outer space may differ with common food on the earth to compensate a decrease in taste and nutrition by hygienic sterilization processing as well as strong cosmic rays, a state of non gravitation, low pressure, and an enclosed space environment. An accurate quantitative analysis of trace elements in various kinds of biological samples is serious work for analytical data quality. An neutron activation analysis is a sensitive, non destructive, multi elemental analytical method without loss and contamination of a sample by chemical pre treatment. The aim of this study is to identify and to compare the distribution of concentrations for essential and functional inorganic elements in six kinds of Korean space foods developed by KAERI in 2011 using INAA.

  5. Comparative measurement of inorganic elements in Korean space foods using instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Chung, Yong Sam; Kim, Sun Ha; Baek, Sung Ryel; Sun, Gwang Min; Moon, Jong Hwa; Choi, Jong Il; Lee, Joo Eun

    2012-01-01

    In April 2008, Korea's first astronaut became a crew member of the international space station and she brought special space versions of traditional Korean dishes such as kimchi, boiled rice, hot red pepper paste, soybean paste soup, ginseng tea, green tea, and ramyun. To date, seventy kinds of Korean space foods (KSFs) have been developed by KAERI. The information and role of trace mineral elements from an intake of created and processed foodstuff are important as a indicator of human health and nutrition, as well as a quality control of food and diet. In particular, special food created for consumption by astronauts in outer space may differ with common food on the earth to compensate a decrease in taste and nutrition by hygienic sterilization processing as well as strong cosmic rays, a state of non gravitation, low pressure, and an enclosed space environment. An accurate quantitative analysis of trace elements in various kinds of biological samples is serious work for analytical data quality. An neutron activation analysis is a sensitive, non destructive, multi elemental analytical method without loss and contamination of a sample by chemical pre treatment. The aim of this study is to identify and to compare the distribution of concentrations for essential and functional inorganic elements in six kinds of Korean space foods developed by KAERI in 2011 using INAA

  6. Development of MARS for multi-dimensional and multi-purpose thermal-hydraulic system analysis

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Won Jae; Chung, Bub Dong; Kim, Kyung Doo; Hwang, Moon Kyu; Jeong, Jae Jun; Ha, Kwi Seok; Joo, Han Gyu [Korea Atomic Energy Research Institute, T/H Safety Research Team, Yusung, Daejeon (Korea)

    2000-10-01

    MARS (Multi-dimensional Analysis of Reactor Safety) code is being developed by KAERI for the realistic thermal-hydraulic simulation of light water reactor system transients. MARS 1.4 has been developed as a final version of basic code frame for the multi-dimensional analysis of system thermal-hydraulics. Since MARS 1.3, MARS 1.4 has been improved to have the enhanced code capability and user friendliness through the unification of input/output features, code models and code functions, and through the code modernization. Further improvements of thermal-hydraulic models, numerical method and user friendliness are being carried out for the enhanced code accuracy. As a multi-purpose safety analysis code system, a coupled analysis system, MARS/MASTER/CONTEMPT, has been developed using multiple DLL (Dynamic Link Library) techniques of Windows system. This code system enables the coupled, that is, more realistic analysis of multi-dimensional thermal-hydraulics (MARS 2.0), three-dimensional core kinetics (MASTER) and containment thermal-hydraulics (CONTEMPT). This paper discusses the MARS development program, and the developmental progress of the MARS 1.4 and the MARS/MASTER/CONTEMPT focusing on major features of the codes and their verification. It also discusses thermal hydraulic models and new code features under development. (author)

  7. Development of MARS for multi-dimensional and multi-purpose thermal-hydraulic system analysis

    International Nuclear Information System (INIS)

    Lee, Won Jae; Chung, Bub Dong; Kim, Kyung Doo; Hwang, Moon Kyu; Jeong, Jae Jun; Ha, Kwi Seok; Joo, Han Gyu

    2000-01-01

    MARS (Multi-dimensional Analysis of Reactor Safety) code is being developed by KAERI for the realistic thermal-hydraulic simulation of light water reactor system transients. MARS 1.4 has been developed as a final version of basic code frame for the multi-dimensional analysis of system thermal-hydraulics. Since MARS 1.3, MARS 1.4 has been improved to have the enhanced code capability and user friendliness through the unification of input/output features, code models and code functions, and through the code modernization. Further improvements of thermal-hydraulic models, numerical method and user friendliness are being carried out for the enhanced code accuracy. As a multi-purpose safety analysis code system, a coupled analysis system, MARS/MASTER/CONTEMPT, has been developed using multiple DLL (Dynamic Link Library) techniques of Windows system. This code system enables the coupled, that is, more realistic analysis of multi-dimensional thermal-hydraulics (MARS 2.0), three-dimensional core kinetics (MASTER) and containment thermal-hydraulics (CONTEMPT). This paper discusses the MARS development program, and the developmental progress of the MARS 1.4 and the MARS/MASTER/CONTEMPT focusing on major features of the codes and their verification. It also discusses thermal hydraulic models and new code features under development. (author)

  8. Finite element circuit theory of the numerical code EDDYMULT for solving eddy current problems in a multi-torus system

    International Nuclear Information System (INIS)

    Nakamura, Yukiharu; Ozeki, Takahisa

    1986-07-01

    The finite element circuit theory is extended to the general eddy current problem in a multi-torus system, which consists of various torus conductors and axisymmetric coil systems. The numerical procedures are devised to avoid practical restrictions of computer storage and computing time, that is, the reduction technique of eddy current eigen modes to save storage and the introduction of shape function into the double area integral of mode coupling to save time. The numerical code EDDYMULT based on the theory is developed to use in designing tokamak device from the viewpoints of the evaluation of electromagnetic loading on the device components and the control analysis of tokamak equilibrium. (author)

  9. Multi-elemental analysis of marine sediments of Sorsogon Bay using x-ray fluorescence spectroscopy

    International Nuclear Information System (INIS)

    Gonzales, Ralph Roly A.; Quirit, Leni L.; Rosales, Colleen Marciel F.; Pabroa, Preciosa Corazon B.; Sta Maria, Efren J.

    2011-01-01

    Metal composition and nutrient loadings of our bodies of water, when uncontrolled, may cause harmful bacterial contamination and pose threats in aquatic and human life. Toxic and trace element inputs in Sorsogon Bay sediments were determined using nuclear analytical techniques, more specifically, x-ray fluorescence spectrometry, in this study. Pre-treated marine sediment samples from Sorsogon Bay were homogenized using SPEX # 8000 mixer/mill and agate mortar and pestle, pelletized into 31-mm flat discs using SPEX 3630 X-Press and analyzed using PAN Analytical Epsilon 5 EDX X-ray Fluorescence Spectrometer with the emission and transmission method using silver and germanium secondary targets. Spectrum fitting performed using AXIL (Analysis of X-ray Spectra by Iterative Least-Squares Fitting), a subprogram in Quantitative X-ray Analysis System developed by the International Atomic Energy Agency and Quantitative Analysis of Environmental Samples program, was used for quantification of results. Results indicate generally moderate to high metal enrichment, specifically manganese, lead, cadmium, zinc and copper. Mercury and iron level enrichment are found to be low, marking an improvement from previous studies indicating high enrichment of these metals. (author)

  10. Evaluation and optimization of footwear comfort parameters using finite element analysis and a discrete optimization algorithm

    Science.gov (United States)

    Papagiannis, P.; Azariadis, P.; Papanikos, P.

    2017-10-01

    Footwear is subject to bending and torsion deformations that affect comfort perception. Following review of Finite Element Analysis studies of sole rigidity and comfort, a three-dimensional, linear multi-material finite element sole model for quasi-static bending and torsion simulation, overcoming boundary and optimisation limitations, is described. Common footwear materials properties and boundary conditions from gait biomechanics are used. The use of normalised strain energy for product benchmarking is demonstrated along with comfort level determination through strain energy density stratification. Sensitivity of strain energy against material thickness is greater for bending than for torsion, with results of both deformations showing positive correlation. Optimization for a targeted performance level and given layer thickness is demonstrated with bending simulations sufficing for overall comfort assessment. An algorithm for comfort optimization w.r.t. bending is presented, based on a discrete approach with thickness values set in line with practical manufacturing accuracy. This work illustrates the potential of the developed finite element analysis applications to offer viable and proven aids to modern footwear sole design assessment and optimization.

  11. Multi-Directional Environmental Sensors

    Science.gov (United States)

    Manohara, Harish (Inventor); Del Castillo, Linda Y. (Inventor); Mojarradi, Mohammed M. (Inventor)

    2016-01-01

    Systems and methods in accordance with embodiments of the invention implement multi-directional environmental sensors. In one embodiment, a multi-directional environmental sensor includes: an inner conductive element that is substantially symmetrical about three orthogonal planes; an outer conductive element that is substantially symmetrical about three orthogonal planes; and a device that measures the electrical characteristics of the multi-directional environmental sensor, the device having a first terminal and a second terminal; where the inner conductive element is substantially enclosed within the outer conductive element; where the inner conductive element is electrically coupled to the first terminal of the device; and where the outer conductive element is electrically coupled to the second terminal of the device.

  12. [Ultra-Fine Pressed Powder Pellet Sample Preparation XRF Determination of Multi-Elements and Carbon Dioxide in Carbonate].

    Science.gov (United States)

    Li, Xiao-li; An, Shu-qing; Xu, Tie-min; Liu, Yi-bo; Zhang, Li-juan; Zeng, Jiang-ping; Wang, Na

    2015-06-01

    The main analysis error of pressed powder pellet of carbonate comes from particle-size effect and mineral effect. So in the article in order to eliminate the particle-size effect, the ultrafine pressed powder pellet sample preparation is used to the determination of multi-elements and carbon-dioxide in carbonate. To prepare the ultrafine powder the FRITSCH planetary Micro Mill machine and tungsten carbide media is utilized. To conquer the conglomeration during the process of grinding, the wet grinding is preferred. The surface morphology of the pellet is more smooth and neat, the Compton scatter effect is reduced with the decrease in particle size. The intensity of the spectral line is varied with the change of the particle size, generally the intensity of the spectral line is increased with the decrease in the particle size. But when the particle size of more than one component of the material is decreased, the intensity of the spectral line may increase for S, Si, Mg, or decrease for Ca, Al, Ti, K, which depend on the respective mass absorption coefficient . The change of the composition of the phase with milling is also researched. The incident depth of respective element is given from theoretical calculation. When the sample is grounded to the particle size of less than the penetration depth of all the analyte, the effect of the particle size on the intensity of the spectral line is much reduced. In the experiment, when grounded the sample to less than 8 μm(d95), the particle-size effect is much eliminated, with the correction method of theoretical α coefficient and the empirical coefficient, 14 major, minor and trace element in the carbonate can be determined accurately. And the precision of the method is much improved with RSD element, the fluorescence yield is low and the interference is serious. With the manual multi-layer crystal PX4, coarse collimator, empirical correction, X-ray spectrometer can be used to determine the carbon dioxide in the carbonate

  13. A blended continuous–discontinuous finite element method for solving the multi-fluid plasma model

    Energy Technology Data Exchange (ETDEWEB)

    Sousa, E.M., E-mail: sousae@uw.edu; Shumlak, U., E-mail: shumlak@uw.edu

    2016-12-01

    The multi-fluid plasma model represents electrons, multiple ion species, and multiple neutral species as separate fluids that interact through short-range collisions and long-range electromagnetic fields. The model spans a large range of temporal and spatial scales, which renders the model stiff and presents numerical challenges. To address the large range of timescales, a blended continuous and discontinuous Galerkin method is proposed, where the massive ion and neutral species are modeled using an explicit discontinuous Galerkin method while the electrons and electromagnetic fields are modeled using an implicit continuous Galerkin method. This approach is able to capture large-gradient ion and neutral physics like shock formation, while resolving high-frequency electron dynamics in a computationally efficient manner. The details of the Blended Finite Element Method (BFEM) are presented. The numerical method is benchmarked for accuracy and tested using two-fluid one-dimensional soliton problem and electromagnetic shock problem. The results are compared to conventional finite volume and finite element methods, and demonstrate that the BFEM is particularly effective in resolving physics in stiff problems involving realistic physical parameters, including realistic electron mass and speed of light. The benefit is illustrated by computing a three-fluid plasma application that demonstrates species separation in multi-component plasmas.

  14. Finite Element Analysis of Pipe T-Joint

    OpenAIRE

    P.M.Gedkar; Dr. D.V. Bhope

    2012-01-01

    This paper reports stress analysis of two pressurized cylindrical intersection using finite element method. The different combinations of dimensions of run pipe and the branch pipe are used to investigate thestresses in pipe at the intersection. In this study the stress analysis is accomplished by finite element package ANSYS.

  15. Individual-specific multi-scale finite element simulation of cortical bone of human proximal femur

    International Nuclear Information System (INIS)

    Ascenzi, Maria-Grazia; Kawas, Neal P.; Lutz, Andre; Kardas, Dieter; Nackenhorst, Udo; Keyak, Joyce H.

    2013-01-01

    We present an innovative method to perform multi-scale finite element analyses of the cortical component of the femur using the individual’s (1) computed tomography scan; and (2) a bone specimen obtained in conjunction with orthopedic surgery. The method enables study of micro-structural characteristics regulating strains and stresses under physiological loading conditions. The analysis of the micro-structural scenarios that cause variation of strain and stress is the first step in understanding the elevated strains and stresses in bone tissue, which are indicative of higher likelihood of micro-crack formation in bone, implicated in consequent remodeling or macroscopic bone fracture. Evidence that micro-structure varies with clinical history and contributes in significant, but poorly understood, ways to bone function, motivates the method’s development, as does need for software tools to investigate relationships between macroscopic loading and micro-structure. Three applications – varying region of interest, bone mineral density, and orientation of collagen type I, illustrate the method. We show, in comparison between physiological loading and simple compression of a patient’s femur, that strains computed at the multi-scale model’s micro-level: (i) differ; and (ii) depend on local collagen-apatite orientation and degree of calcification. Our findings confirm the strain concentration role of osteocyte lacunae, important for mechano-transduction. We hypothesize occurrence of micro-crack formation, leading either to remodeling or macroscopic fracture, when the computed strains exceed the elastic range observed in micro-structural testing

  16. Individual-specific multi-scale finite element simulation of cortical bone of human proximal femur

    Energy Technology Data Exchange (ETDEWEB)

    Ascenzi, Maria-Grazia, E-mail: mgascenzi@mednet.ucla.edu [UCLA/Orthopaedic Hospital, Department of Orthopaedic Surgery, Rehabilitation Bldg, Room 22-69, 1000 Veteran Avenue, University of California, Los Angeles, CA 90095 (United States); Kawas, Neal P., E-mail: nealkawas@ucla.edu [UCLA/Orthopaedic Hospital, Department of Orthopaedic Surgery, Rehabilitation Bldg, Room 22-69, 1000 Veteran Avenue, University of California, Los Angeles, CA 90095 (United States); Lutz, Andre, E-mail: andre.lutz@hotmail.de [Institute of Biomechanics and Numerical Mechanics, Leibniz University Hannover, 30167 Hannover (Germany); Kardas, Dieter, E-mail: kardas@ibnm.uni-hannover.de [ContiTech Vibration Control, Jaedekamp 30 None, 30419 Hannover (Germany); Nackenhorst, Udo, E-mail: nackenhorst@ibnm.uni-hannover.de [Institute of Biomechanics and Numerical Mechanics, Leibniz University Hannover, 30167 Hannover (Germany); Keyak, Joyce H., E-mail: jhkeyak@uci.edu [Department of Radiological Sciences, Medical Sciences I, Bldg 811, Room B140, University of California, Irvine, CA 92697-5000 (United States)

    2013-07-01

    We present an innovative method to perform multi-scale finite element analyses of the cortical component of the femur using the individual’s (1) computed tomography scan; and (2) a bone specimen obtained in conjunction with orthopedic surgery. The method enables study of micro-structural characteristics regulating strains and stresses under physiological loading conditions. The analysis of the micro-structural scenarios that cause variation of strain and stress is the first step in understanding the elevated strains and stresses in bone tissue, which are indicative of higher likelihood of micro-crack formation in bone, implicated in consequent remodeling or macroscopic bone fracture. Evidence that micro-structure varies with clinical history and contributes in significant, but poorly understood, ways to bone function, motivates the method’s development, as does need for software tools to investigate relationships between macroscopic loading and micro-structure. Three applications – varying region of interest, bone mineral density, and orientation of collagen type I, illustrate the method. We show, in comparison between physiological loading and simple compression of a patient’s femur, that strains computed at the multi-scale model’s micro-level: (i) differ; and (ii) depend on local collagen-apatite orientation and degree of calcification. Our findings confirm the strain concentration role of osteocyte lacunae, important for mechano-transduction. We hypothesize occurrence of micro-crack formation, leading either to remodeling or macroscopic fracture, when the computed strains exceed the elastic range observed in micro-structural testing.

  17. Quantitative real-time monitoring of multi-elements in airborne particulates by direct introduction into an inductively coupled plasma mass spectrometer

    International Nuclear Information System (INIS)

    Suzuki, Yoshinari; Sato, Hikaru; Hiyoshi, Katsuhiro; Furuta, Naoki

    2012-01-01

    A new calibration system for real-time determination of trace elements in airborne particulates was developed. Airborne particulates were directly introduced into an inductively coupled plasma mass spectrometer, and the concentrations of 15 trace elements were determined by means of an external calibration method. External standard solutions were nebulized by an ultrasonic nebulizer (USN) coupled with a desolvation system, and the resulting aerosol was introduced into the plasma. The efficiency of sample introduction via the USN was calculated by two methods: (1) the introduction of a Cr standard solution via the USN was compared with introduction of a Cr(CO) 6 standard gas via a standard gas generator and (2) the aerosol generated by the USN was trapped on filters and then analyzed. The Cr introduction efficiencies obtained by the two methods were the same, and the introduction efficiencies of the other elements were equal to the introduction efficiency of Cr. Our results indicated that our calibration method for introduction efficiency worked well for the 15 elements (Ti, V, Cr, Mn, Co, Ni, Cu, Zn, As, Mo, Sn, Sb, Ba, Tl and Pb). The real-time data and the filter-collection data agreed well for elements with low-melting oxides (V, Co, As, Mo, Sb, Tl, and Pb). In contrast, the real-time data were smaller than the filter-collection data for elements with high-melting oxides (Ti, Cr, Mn, Ni, Cu, Zn, Sn, and Ba). This result implies that the oxides of these 8 elements were not completely fused, vaporized, atomized, and ionized in the initial radiation zone of the inductively coupled plasma. However, quantitative real-time monitoring can be realized after correction for the element recoveries which can be calculated from the ratio of real-time data/filter-collection data. - Highlights: ► APs were directly introduced into ICP-MS and real-time analysis was performed. ► The real-time data were calibrated by a multi-element standard solution from USN. ► During real

  18. Finite element analysis of inclined nozzle-plate junctions

    International Nuclear Information System (INIS)

    Dixit, K.B.; Seth, V.K.; Krishnan, A.; Ramamurthy, T.S.; Dattaguru, B.; Rao, A.K.

    1979-01-01

    Estimation of stress concentration at nozzle to plate or shell junctions is a significant problem in the stress analysis of nuclear reactors. The topic is a subject matter of extensive investigations and earlier considerable success has been reported on analysis for the cases when the nozzle is perpendicular to the plate or is radial to the shell. Analytical methods for the estimation of stress concentrations for the practical situations when the intersecting nozzle is inclined to the plate or is non-radial to the shell is rather scanty. Specific complications arise in dealing with the junction region when the nozzle with circular cross-section meets the non-circular cut-out on the plate or shell. In this paper a finite element analysis is developed for inclined nozzles and results are presented for nozzle-plate junctions. A method of analysis is developed with a view to achieving simultaneously accuracy of results and simplicity in the choice of elements and their connectivity. The circular nozzle is treated by axisymmetric conical shell elements. The nozzle portion in the region around the junction and the flat plate is dealt with by triangular flat shell elements. Special transition elements are developed for joining the flat shell elements with the axisymmetric elements under non-axisymmetric loading. A substructure method of analysis is adopted which achieves considerable economy in handling the structure and also conveniently combines the different types of elements in the structure. (orig.)

  19. The multi-element ultrasonic technology: examples of application on military naval structures

    International Nuclear Information System (INIS)

    Recolin, P.; Rivalin, S.

    2009-01-01

    DCNS is the European leader in the military ship construction and maintenance (conventional and nuclear propulsion). The potential of ultrasonic technologies with multi-element probes has been studied in its Materials laboratory since the end of the 80's, and a growing number of applications has appeared these last ten years. A series of examples is given: in-service nuclear reactor pipe welds monitoring, time-of-flight diffraction (TOFD) technique for the inspection of containment welds, coating fabrication control, detection of laminating corrosion on aluminum rings, detection of corrosion on submarine hulls in basin, inspection of hull welded joints

  20. Graph Grammar-Based Multi-Frontal Parallel Direct Solver for Two-Dimensional Isogeometric Analysis

    KAUST Repository

    Kuźnik, Krzysztof

    2012-06-02

    This paper introduces the graph grammar based model for developing multi-thread multi-frontal parallel direct solver for two dimensional isogeometric finite element method. Execution of the solver algorithm has been expressed as the sequence of graph grammar productions. At the beginning productions construct the elimination tree with leaves corresponding to finite elements. Following sequence of graph grammar productions generates element frontal matri-ces at leaf nodes, merges matrices at parent nodes and eliminates rows corresponding to fully assembled degrees of freedom. Finally, there are graph grammar productions responsible for root problem solution and recursive backward substitutions. Expressing the solver algorithm by graph grammar productions allows us to explore the concurrency of the algorithm. The graph grammar productions are grouped into sets of independent tasks that can be executed concurrently. The resulting concurrent multi-frontal solver algorithm is implemented and tested on NVIDIA GPU, providing O(NlogN) execution time complexity where N is the number of degrees of freedom. We have confirmed this complexity by solving up to 1 million of degrees of freedom with 448 cores GPU.

  1. Geographic authentication of Asian rice (Oryza sativa L.) using multi-elemental and stable isotopic data combined with multivariate analysis.

    Science.gov (United States)

    Chung, Ill-Min; Kim, Jae-Kwang; Lee, Kyoung-Jin; Park, Sung-Kyu; Lee, Ji-Hee; Son, Na-Young; Jin, Yong-Ik; Kim, Seung-Hyun

    2018-02-01

    Rice (Oryza sativa L.) is the world's third largest food crop after wheat and corn. Geographic authentication of rice has recently emerged asan important issue for enhancing human health via food safety and quality assurance. Here, we aimed to discriminate rice of six Asian countries through geographic authentication using combinations of elemental/isotopic composition analysis and chemometric techniques. Principal components analysis could distinguish samples cultivated from most countries, except for those cultivated in the Philippines and Japan. Furthermore, orthogonal projection to latent structure-discriminant analysis provided clear discrimination between rice cultivated in Korea and other countries. The major common variables responsible for differentiation in these models were δ 34 S, Mn, and Mg. Our findings contribute to understanding the variations of elemental and isotopic compositions in rice depending on geographic origins, and offer valuable insight into the control of fraudulent labeling regarding the geographic origins of rice traded among Asian countries. Copyright © 2017 Elsevier Ltd. All rights reserved.

  2. Investigation on trace elements in crude oil and organic matter extracted from rocks with instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Ding Zuguo; Chai Zhifang

    1990-01-01

    Solvent extraction, column chromatography and instrumental neutron activation analysis(INAA) have been used to investigate the trace elements in crude oil, organic matter extracted from rocks and their related fractions. With these methods, about 70 crude oil samples from eight different oil fields in China and 6 extracted asphaltene samples of the lower paleozoic from the upper Yangtze region have been analyzed, and about 40 elements of interest have been determined. Those elements include Al, As, Au, Ba, Br, Cl, Co, Cr, Cs, Cu, Fe, Hf, I, Ir, Mg, Mn, Mo, Na, Ni, Rb, Re, S, Sb, Sc, Se, Sr, Th, Zn, V and parts of REE. The experimental results show that the method possesses several advantages, i.e. non-destructive, multi-elements, sensitive, precise and accurate. Without ashing samples, the loss of volatile elements such as Cl, S, Se and Sb are avoided. The column chromatography makes it possible to study the distributions of trace elements in different fractions of crude oil and organic matter extracted. Meanwhile, the characters of trace elements in them have also been discussed

  3. Trace element analysis with PIXE using Trombay 5.5 MeV Van de Graaff accelerator

    International Nuclear Information System (INIS)

    Govil, Rekha; Kataria, S.K.; Kapoor, S.S.; Madan Lal; Nadkarni, D.M.; Rama Rao, P.N.; Viswanathan, K.V.

    1980-01-01

    The work on trace element analysis using proton induced X-ray emission technique (PIXE) with the proton beam from 5.5 MeV Van de Graaff accelerator at Trombay, is described. The experimental set up consisted of an indigeneously built 220 eV resolution Si(Li) x-ray spectrometer and target chamber having arrangements to mount upto twelve targets. In the present work, a variety of samples of biological nature, monazite mineral and some other samples were analyzed along with a standard multi-element sample. The sample preparation technique for different samples is also given in the report. For quantitative estimation of trace elements, a computer code developed earlier was used. The proton induced x-ray spectra of various samples and their computer fits are presented and quantitative results for some selected samples are also given. The minimum detection limits which were achieved with the present set up are also given. (auth.)

  4. Multi-Metric Sustainability Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Cowlin, Shannon [National Renewable Energy Lab. (NREL), Golden, CO (United States); Heimiller, Donna [National Renewable Energy Lab. (NREL), Golden, CO (United States); Macknick, Jordan [National Renewable Energy Lab. (NREL), Golden, CO (United States); Mann, Margaret [National Renewable Energy Lab. (NREL), Golden, CO (United States); Pless, Jacquelyn [National Renewable Energy Lab. (NREL), Golden, CO (United States); Munoz, David [Colorado School of Mines, Golden, CO (United States)

    2014-12-01

    A readily accessible framework that allows for evaluating impacts and comparing tradeoffs among factors in energy policy, expansion planning, and investment decision making is lacking. Recognizing this, the Joint Institute for Strategic Energy Analysis (JISEA) funded an exploration of multi-metric sustainability analysis (MMSA) to provide energy decision makers with a means to make more comprehensive comparisons of energy technologies. The resulting MMSA tool lets decision makers simultaneously compare technologies and potential deployment locations.

  5. Multi-Unit Considerations for Human Reliability Analysis

    Energy Technology Data Exchange (ETDEWEB)

    St. Germain, S.; Boring, R.; Banaseanu, G.; Akl, Y.; Chatri, H.

    2017-03-01

    This paper uses the insights from the Standardized Plant Analysis Risk-Human Reliability Analysis (SPAR-H) methodology to help identify human actions currently modeled in the single unit PSA that may need to be modified to account for additional challenges imposed by a multi-unit accident as well as identify possible new human actions that might be modeled to more accurately characterize multi-unit risk. In identifying these potential human action impacts, the use of the SPAR-H strategy to include both errors in diagnosis and errors in action is considered as well as identifying characteristics of a multi-unit accident scenario that may impact the selection of the performance shaping factors (PSFs) used in SPAR-H. The lessons learned from the Fukushima Daiichi reactor accident will be addressed to further help identify areas where improved modeling may be required. While these multi-unit impacts may require modifications to a Level 1 PSA model, it is expected to have much more importance for Level 2 modeling. There is little currently written specifically about multi-unit HRA issues. A review of related published research will be presented. While this paper cannot answer all issues related to multi-unit HRA, it will hopefully serve as a starting point to generate discussion and spark additional ideas towards the proper treatment of HRA in a multi-unit PSA.

  6. Ring-element analysis of layered orthotropic bodies

    DEFF Research Database (Denmark)

    Jørgensen, O.

    1993-01-01

    For the analysis of arbitrarily laminated circular bodies, a displacement-based ring-element is presented. The analysis is performed in a cylindrical coordinate system. The method of analysis requires the boundary conditions as well as the external forces to be pi-periodic. The element formulation...... accounts for a desired degree of approximation of the displacement field in the direction of the circumference. This is done by a truncated Fourier expansion of the angular dependence of the displacements in terms of trigonometric functions. Thus the Fourier expansion coefficients are the unknowns...... to that of solutions obtained by traditional 3D elements. A scheme for analytical integration of the angular dependence of the stiffness matrix is given....

  7. Electrical machine analysis using finite elements

    CERN Document Server

    Bianchi, Nicola

    2005-01-01

    OUTLINE OF ELECTROMAGNETIC FIELDSVector AnalysisElectromagnetic FieldsFundamental Equations SummaryReferencesBASIC PRINCIPLES OF FINITE ELEMENT METHODSIntroductionField Problems with Boundary ConditionsClassical Method for the Field Problem SolutionThe Classical Residual Method (Galerkin's Method)The Classical Variational Method (Rayleigh-Ritz's Method)The Finite Element MethodReferencesAPPLICATIONS OF THE FINITE ELEMENT METHOD TO TWO-DIMENSIONAL FIELDSIntroductionLinear Interpolation of the Function fApplication of the Variational MethodSimple Descriptions of Electromagnetic FieldsAppendix: I

  8. NanoSIMS multi-element imaging reveals internalisation and nucleolar targeting for a highly-charged polynuclear platinum compound.

    Science.gov (United States)

    Wedlock, Louise E; Kilburn, Matt R; Liu, Rong; Shaw, Jeremy A; Berners-Price, Susan J; Farrell, Nicholas P

    2013-08-11

    Simultaneous multi-element imaging using NanoSIMS (nano-scale secondary ion mass spectrometry), exploiting the novel combination of (195)Pt and (15)N in platinum-am(m)ine antitumour drugs, provides information on the internalisation and subcellular localisation of both metal and ligands, and allows identification of ligand exchange.

  9. Elemental hair analysis: A review of procedures and applications

    International Nuclear Information System (INIS)

    Pozebon, D.; Scheffler, G.L.; Dressler, V.L.

    2017-01-01

    Although exogenous contamination and unreliable reference values have limited the utility of scalp hair as a biomarker of chemical elements exposure, its use in toxicological, clinical, environmental and forensic investigations is growing and becoming more extensive. Therefore, hair elemental analysis is reviewed in the current manuscript which spans articles published in the last 10 years. It starts with a general discussion of history, morphology and possible techniques for elemental analysis, where inductively coupled plasma-mass spectrometry (ICP-MS) is clearly highlighted since this technique is leading quantitative ultra-trace elemental analysis. Emphasis over sampling, quality assurance, washing procedures and sample decomposition is given with detailed protocols compiled in tables as well as the utility of hair to identify human gender, age, diseases, healthy conditions, nutrition status and contamination sites. Isotope ratio information, chemical speciation analysis and analyte preconcentration are also considered for hair. Finally, the potential of laser ablation ICP-MS (LA-ICP-MS) to provide spatial resolution and time-track the monitoring of elements in hair strands instead of conventional bulk analysis is spotlighted as a real future trend in the field. - Highlights: • Elemental analysis of hair is critically reviewed, with focus on ICP-MS employment. • Standards protocols of hair washing and sample decomposition are compiled. • The usefulness of elemental and/or isotopic analysis of hair is demonstrated. • The potential of LA-ICP-MS for elemental time tracking in hair is highlighted.

  10. Finite element analysis of tibial fractures

    DEFF Research Database (Denmark)

    Wong, Christian Nai En; Mikkelsen, Mikkel Peter W; Hansen, Leif Berner

    2010-01-01

    Project. The data consisted of 21,219 3D elements with a cortical shell and a trabecular core. Three types of load of torsion, a direct lateral load and axial compression were applied. RESULTS: The finite element linear static analysis resulted in relevant fracture localizations and indicated relevant...

  11. Sequential assimilation of multi-mission dynamical topography into a global finite-element ocean model

    Directory of Open Access Journals (Sweden)

    S. Skachko

    2008-12-01

    Full Text Available This study focuses on an accurate estimation of ocean circulation via assimilation of satellite measurements of ocean dynamical topography into the global finite-element ocean model (FEOM. The dynamical topography data are derived from a complex analysis of multi-mission altimetry data combined with a referenced earth geoid. The assimilation is split into two parts. First, the mean dynamic topography is adjusted. To this end an adiabatic pressure correction method is used which reduces model divergence from the real evolution. Second, a sequential assimilation technique is applied to improve the representation of thermodynamical processes by assimilating the time varying dynamic topography. A method is used according to which the temperature and salinity are updated following the vertical structure of the first baroclinic mode. It is shown that the method leads to a partially successful assimilation approach reducing the rms difference between the model and data from 16 cm to 2 cm. This improvement of the mean state is accompanied by significant improvement of temporal variability in our analysis. However, it remains suboptimal, showing a tendency in the forecast phase of returning toward a free run without data assimilation. Both the mean difference and standard deviation of the difference between the forecast and observation data are reduced as the result of assimilation.

  12. Multi-Dimensional Path Queries

    DEFF Research Database (Denmark)

    Bækgaard, Lars

    1998-01-01

    to create nested path structures. We present an SQL-like query language that is based on path expressions and we show how to use it to express multi-dimensional path queries that are suited for advanced data analysis in decision support environments like data warehousing environments......We present the path-relationship model that supports multi-dimensional data modeling and querying. A path-relationship database is composed of sets of paths and sets of relationships. A path is a sequence of related elements (atoms, paths, and sets of paths). A relationship is a binary path...

  13. METHODOLOGICAL ELEMENTS OF SITUATIONAL ANALYSIS

    Directory of Open Access Journals (Sweden)

    Tetyana KOVALCHUK

    2016-07-01

    Full Text Available The article deals with the investigation of theoretical and methodological principles of situational analysis. The necessity of situational analysis is proved in modern conditions. The notion “situational analysis” is determined. We have concluded that situational analysis is a continuous system study which purpose is to identify dangerous situation signs, to evaluate comprehensively such signs influenced by a system of objective and subjective factors, to search for motivated targeted actions used to eliminate adverse effects of the exposure of the system to the situation now and in the future and to develop the managerial actions needed to bring the system back to norm. It is developed a methodological approach to the situational analysis, its goal is substantiated, proved the expediency of diagnostic, evaluative and searching functions in the process of situational analysis. The basic methodological elements of the situational analysis are grounded. The substantiation of the principal methodological elements of system analysis will enable the analyst to develop adaptive methods able to take into account the peculiar features of a unique object which is a situation that has emerged in a complex system, to diagnose such situation and subject it to system and in-depth analysis, to identify risks opportunities, to make timely management decisions as required by a particular period.

  14. Neutron-activation analysis of trace elements in thyroids

    International Nuclear Information System (INIS)

    Boulyga, S.F.; Petri, H.; Kanash, N.V.; Malenchenko, A.F.

    1999-01-01

    Neutron activation analysis was used for routine measurement of trace elements in thyroids of inhabitants of Belarus as well as in thyroids of people operated for thyroid cancer. The method chosen allowed the analysis of 28 elements, among them essential and toxic ones, with a good accuracy. The results obtained showed significant differences in the elemental composition of thyroid from the different regions. The changes of elemental composition of thyroids of inhabitants of the Gomel region, where goiter is endemic, seem to be identical to those in the tumor tissue. (author)

  15. A new method based on low background instrumental neutron activation analysis for major, trace and ultra-trace element determination in atmospheric mineral dust from polar ice cores

    Energy Technology Data Exchange (ETDEWEB)

    Baccolo, Giovanni, E-mail: giovanni.baccolo@mib.infn.it [Graduate School in Polar Sciences, University of Siena, Via Laterina 8, 53100, Siena (Italy); Department of Environmental Sciences, University of Milano-Bicocca, P.zza della Scienza 1, 20126, Milano (Italy); INFN, Section of Milano-Bicocca, P.zza della Scienza 3, 20126, Milano (Italy); Clemenza, Massimiliano [INFN, Section of Milano-Bicocca, P.zza della Scienza 3, 20126, Milano (Italy); Department of Physics, University of Milano-Bicocca, P.zza della Scienza 3, 20126, Milano (Italy); Delmonte, Barbara [Department of Environmental Sciences, University of Milano-Bicocca, P.zza della Scienza 1, 20126, Milano (Italy); Maffezzoli, Niccolò [Centre for Ice and Climate, Niels Bohr Institute, Juliane Maries Vej, 30, 2100, Copenhagen (Denmark); Nastasi, Massimiliano; Previtali, Ezio [INFN, Section of Milano-Bicocca, P.zza della Scienza 3, 20126, Milano (Italy); Department of Physics, University of Milano-Bicocca, P.zza della Scienza 3, 20126, Milano (Italy); Prata, Michele; Salvini, Andrea [LENA, University of Pavia, Pavia (Italy); Maggi, Valter [Department of Environmental Sciences, University of Milano-Bicocca, P.zza della Scienza 1, 20126, Milano (Italy); INFN, Section of Milano-Bicocca, P.zza della Scienza 3, 20126, Milano (Italy)

    2016-05-30

    Dust found in polar ice core samples present extremely low concentrations, in addition the availability of such samples is usually strictly limited. For these reasons the chemical and physical analysis of polar ice cores is an analytical challenge. In this work a new method based on low background instrumental neutron activation analysis (LB-INAA) for the multi-elemental characterization of the insoluble fraction of dust from polar ice cores is presented. Thanks to an accurate selection of the most proper materials and procedures it was possible to reach unprecedented analytical performances, suitable for ice core analyses. The method was applied to Antarctic ice core samples. Five samples of atmospheric dust (μg size) from ice sections of the Antarctic Talos Dome ice core were prepared and analyzed. A set of 37 elements was quantified, spanning from all the major elements (Na, Mg, Al, Si, K, Ca, Ti, Mn and Fe) to trace ones, including 10 (La, Ce, Nd, Sm, Eu, Tb, Ho, Tm, Yb and Lu) of the 14 natural occurring lanthanides. The detection limits are in the range of 10{sup −13}–10{sup −6} g, improving previous results of 1–3 orders of magnitude depending on the element; uncertainties lies between 4% and 60%. - Highlights: • A new method based on neutron activation for the multi-elemental characterization of atmospheric dust entrapped in polar ice cores is proposed. • 37 elements were quantified in μg size dust samples with detection limits ranging from 10{sup −13} to 10{sup −6} g. • A low background approach and a clean analytical protocol improved INAA performances to unprecedented levels for multi-elemental analyses.

  16. Elemental mapping of medieval teeth using XRF technique

    International Nuclear Information System (INIS)

    Muja, Cristina; Therese, Laurent; Guillot, Philippe

    2011-01-01

    Full text: Recent developments in X-Ray Fluorescence micro-analysis techniques made the traditional range of XRF applications expand, benefiting from the combination of single point analysis with high spatial element imaging. The sample is scanned through the X-Ray beam and corresponding spectra are continuously read from the detector and correlated to a particular position on the sample. In this work, elemental concentrations were obtained by X-ray fluorescence (XRF) technique (Jobin Yvon Horiba XGT-5000 instrument) offering detailed elemental analysis. The instrument is equipped with a tungsten X-ray tube and a beryllium window, operating at 50 kV with a beam collimator of 100μm in diameter to irradiate the sample and with a Si detector. Tooth mapping provided semi-quantitative information and highlighted the regions of interest. Then multi-points analysis was used to obtain quantitative results on calcium, phosphorus, strontium and iron. As the chemical composition of dental tissues is similar to the one of bone tissue, the certified reference materials NIST SRM 1400 Bone Ash and NIST SRM 1486 Bone Meal were used for calibration. In this study, only permanent first molars were selected for analysis. The material comes from the medieval cemetery (XII th . XIII th ) of Feldioara (Bra.ov County, Romania). In the same time, modern teeth were used as reference. The top of the tooth was removed using a diamond disk, with a cut lying perpendicular to the dental cusps, creating a flat transversal surface to be characterized. XRF elemental (Ca, P, Sr, Fe) and ratio (Ca/P, Sr/Ca, Sr/Fe) distribution images for dental tissues (enamel and dentin) were obtained from past and modern teeth with and without caries and the results are presented and discussed. The analysis of the spatial element distribution in the teeth tissues revealed severe alterations in elemental composition of both enamel and dentin from the regions affected by caries that were confirmed by the multi

  17. Elemental mapping of medieval teeth using XRF technique

    Energy Technology Data Exchange (ETDEWEB)

    Muja, Cristina [Laboratoire Diagnostics des Plasma, CUFR J.F.C, Albi (France); Faculty of Biology, University of Bucharest (Romania); Vasile Parvan Institute of Archaeology, Bucharest (Romania); Therese, Laurent; Guillot, Philippe, E-mail: philippe.guillot@univ-jfc.fr [Laboratoire Diagnostics des Plasma, CUFR J.F.C, Albi (France)

    2011-07-01

    Full text: Recent developments in X-Ray Fluorescence micro-analysis techniques made the traditional range of XRF applications expand, benefiting from the combination of single point analysis with high spatial element imaging. The sample is scanned through the X-Ray beam and corresponding spectra are continuously read from the detector and correlated to a particular position on the sample. In this work, elemental concentrations were obtained by X-ray fluorescence (XRF) technique (Jobin Yvon Horiba XGT-5000 instrument) offering detailed elemental analysis. The instrument is equipped with a tungsten X-ray tube and a beryllium window, operating at 50 kV with a beam collimator of 100{mu}m in diameter to irradiate the sample and with a Si detector. Tooth mapping provided semi-quantitative information and highlighted the regions of interest. Then multi-points analysis was used to obtain quantitative results on calcium, phosphorus, strontium and iron. As the chemical composition of dental tissues is similar to the one of bone tissue, the certified reference materials NIST SRM 1400 Bone Ash and NIST SRM 1486 Bone Meal were used for calibration. In this study, only permanent first molars were selected for analysis. The material comes from the medieval cemetery (XII{sup th} . XIII{sup th}) of Feldioara (Bra.ov County, Romania). In the same time, modern teeth were used as reference. The top of the tooth was removed using a diamond disk, with a cut lying perpendicular to the dental cusps, creating a flat transversal surface to be characterized. XRF elemental (Ca, P, Sr, Fe) and ratio (Ca/P, Sr/Ca, Sr/Fe) distribution images for dental tissues (enamel and dentin) were obtained from past and modern teeth with and without caries and the results are presented and discussed. The analysis of the spatial element distribution in the teeth tissues revealed severe alterations in elemental composition of both enamel and dentin from the regions affected by caries that were confirmed by the

  18. VIRTUAL EXPERIMENTAL ANALYSIS ON CLEANING ELEMENT OF SUGARCANE HARVESTER

    Institute of Scientific and Technical Information of China (English)

    Ma Fanglan; Li Shangping; He Yulin; Meng Yanmei; Chen Weixu

    2005-01-01

    The laws of influence of different factors have been analyzed in order to enhance the working efficiency and fatigue life of the cleaning element in brush shape of the sugarcane harvester.Based on the principle of orthogonal experiment design, the virtual-orthogonal-experimental analysis for the cleaning element is carried out on the finite element analysis (FEA) software-ANSYS after analyzing the nonlinear structural behavior in the working procedure. The results are analyzed with the overall balancing method, and then the optimal combination is got, which is made up of different levels of different factors. Also the optimal combination of design parameters of the cleaning element received from the virtual experimental analysis is conducted an experiment to confirm that the virtual analysis model and results are right, and the effect of factors on the function of the cleaning element is obtained by more analysis and further optimizing.

  19. The effectiveness of various treatments in changing the nutrient status and bioavailability of risk elements in multi-element contaminated soil.

    Science.gov (United States)

    García-Sánchez, Mercedes; García-Romera, Inmaculada; Száková, Jiřina; Kaplan, Lukáš; Tlustoš, Pavel

    2015-09-01

    Potential changes in the mobility and bioavailability of risk and essential macro- and micro-elements achieved by adding various ameliorative materials were evaluated in a model pot experiment. Spring wheat (Triticum aestivum L.) was cultivated under controlled condition for 60 days in two soils, uncontaminated Chernozem and multi-element contaminated Fluvisol containing 4900 ± 200 mg/kg Zn, 35.4 ± 3.6 mg/kg Cd, and 3035 ± 26 mg/kg Pb. The treatments were all contained the same amount of sulfur and were as follows: (i) digestate from the anaerobic fermentation of biowaste, (ii) fly ash from wood chip combustion, and (iii) ammonium sulfate. Macro- and micro-nutrients Ca, Mg, K, Fe, Mn, Cu, P, and S, and risk elements Cd, Cr, Pb, and Zn were assayed in soil extracts with 0.11 mol/l solution of CH3COOH and in roots, shoots, and grain of wheat after 30 and 60 days of cultivation. Both digestate and fly ash increased levels of macro- and micro-nutrients as well as risk elements (especially Cd and Zn; the mobility of Pb decreased after 30 days of cultivation). The changes in element mobility in ammonium sulfate-treated soils appear to be due to both changes in soil pH level and inter-element interactions. Ammonium sulfate tended to be the most effective measure for increasing nutrient uptake by plants in Chernozem but with opposite pattern in Fluvisol. Changes in plant yield and element uptake in treated plants may have been associated with the higher proline content of wheat shoots cultivated in both soils compared to control. None of the treatments decreased uptake of risk elements by wheat plants in the extremely contaminated Fluvisol, and their accumulation in wheat grains significantly exceeded maximum permissible levels; these treatments cannot be used to enable cereal and other crop production in such soils. However, the combination of increased plant growth alongside unchanged element content in plant biomass in pots treated with digestate

  20. Analysis of concrete beams using applied element method

    Science.gov (United States)

    Lincy Christy, D.; Madhavan Pillai, T. M.; Nagarajan, Praveen

    2018-03-01

    The Applied Element Method (AEM) is a displacement based method of structural analysis. Some of its features are similar to that of Finite Element Method (FEM). In AEM, the structure is analysed by dividing it into several elements similar to FEM. But, in AEM, elements are connected by springs instead of nodes as in the case of FEM. In this paper, background to AEM is discussed and necessary equations are derived. For illustrating the application of AEM, it has been used to analyse plain concrete beam of fixed support condition. The analysis is limited to the analysis of 2-dimensional structures. It was found that the number of springs has no much influence on the results. AEM could predict deflection and reactions with reasonable degree of accuracy.

  1. Elemental analysis of vegetables on the market. Comparison with wild plants

    International Nuclear Information System (INIS)

    Itoh, J.; Saitoh, Y.; Futatsugawa, S.; Sera, K.

    2006-01-01

    We have measured concentration of multi elements in vegetables on the market and a wild plant gathered around Nishina Memorial Cyclotron Center in Iwate prefecture by means of PIXE. Elemental concentration in vegetables cultivated by spraying mineral-rich waters was also analyzed. As a result, it is found that the mineral-supplying vegetables abundantly contain essential elements for body such as K, Ca, Fe, Cu and Zn in comparison with ordinary ones. With regard to a wild plant, concentration of essential elements such as Ca, Cu and Zn shows no clear difference in comparison with that in commercially available one of the same kind, while that of toxic elements such as Cr and Pb is relatively higher. Moreover, it is suggested that the wild plant has a certain property of concentrating a specific element depending on its growing period. The relation between elemental concentration in the plants and that in their growing environment, such as water and soil, was also examined. It is also suggested that elemental concentration in vegetables reflects elemental constituent not only of the soil but also of the sprayed water as well as of the fertilizer. (author)

  2. Dose determination algorithms for a nearly tissue equivalent multi-element thermoluminescent dosimeter

    International Nuclear Information System (INIS)

    Moscovitch, M.; Chamberlain, J.; Velbeck, K.J.

    1988-01-01

    In a continuing effort to develop dosimetric systems that will enable reliable interpretation of dosimeter readings in terms of the absorbed dose or dose-equivalent, a new multi-element TL dosimeter assembly for Beta and Gamma dose monitoring has been designed. The radiation-sensitive volumes are four LiF-TLD elements, each covered by its own unique filter. For media-matching, care has been taken to employ nearly tissue equivalent filters of thicknesses of 1000 mg/cm 2 and 300 mg/cm 2 for deep dose and dose to the lens-of-the-eye measurements respectively. Only one metal filter (Cu) is employed to provide low energy photon discrimination. A Thin TL element (0.09 mm thick) is located behind an open window designed to improve the energy under-response to low energy beta rays and to provide closer estimate of the shallow dose equivalent. The deep and shallow dose equivalents are derived from the correlation of the response of the various TL elements to the above quantities through computations based on previously defined relationships obtained from experimental results. The theoretical formalization for the dose calculation algorithms is described in detail, and provides a useful methodology which can be applied to different tissue-equivalent dosimeter assemblies. Experimental data has been obtained by performing irradiation according to the specifications established by DOELAP, using 27 types of pure and mixed radiation fields including Cs-137 gamma rays, low energy photons down to 20 keV, Sr/Y-90, Uranium, and Tl-204 beta particles

  3. PIXE-based quantification of health-proactive trace elements in genetically transformed roots of a multi-medicinal plant, Sida acuta Burm.f

    International Nuclear Information System (INIS)

    Somanatha Jena; Lopamudra Sahu; Chand, P.K.; Ray, D.K.; Mishra, S.K.

    2015-01-01

    Inorganic element composition of genetically transformed hairy root cultures (HRCs) of a medicinal plant, Sida acuta was determined using PIXE technique. HRCs had a higher accumulation of pro-health trace elements compared to natural roots. It was estimated that < 160 g d.wt. of a selected rhizoclone could suffice to provide nearly all tested essential elements catering to per diem requirement of the human body. The ideal multi-elemental profile ushers a new possibility of integrating hairy root extracts in modern therapeutics ('rhizotherapy') as complementary medicine or a dietary nutraceutical supplement. (author)

  4. Analysis of Bullying in Cooperative Multi-agent Systems’ Communications

    Directory of Open Access Journals (Sweden)

    Celia Gutiérrez

    2013-12-01

    Full Text Available Cooperative Multi-agent Systems frameworks do not include modules to test communications yet. The proposed framework incorporates robust analysis tools using IDKAnalysis2.0 to evaluate bullying effect in communications. The present work is based on ICARO-T. This platform follows the Adaptive Multi-agent Systems paradigm. Experimentation with ICARO-T includes two deployments: the equitative and the authoritative. Results confirm the usefulness of the analysis tools when exporting to Cooperative Multi-agent Systems that use different configurations. Besides, ICARO-T is provided with new functionality by a set of tools for communication analysis.

  5. Diversity and MIMO Performance Evaluation of Common Phase Center Multi Element Antenna Systems

    Directory of Open Access Journals (Sweden)

    V. Papamichael

    2008-06-01

    Full Text Available The diversity and Multiple Input Multiple Output (MIMO performance provided by common phase center multi element antenna (CPCMEA systems is evaluated using two practical methods which make use of the realized active element antenna patterns. These patterns include both the impact of the mutual coupling and the mismatch power loss at antenna ports. As a case study, two and four printed Inverted F Antenna (IFA systems are evaluated by means of Effective Diversity Gain (EDG and Capacity (C. EDG is measured in terms of the signal-to-noise ratio (SNR enhancement at a specific outage probability and in terms of the SNR reduction for achieving a desired average bit error rate (BER. The concept of receive antenna selection in MIMO systems is also investigated and the simulation results show a 43% improvement in the 1% outage C of a reconfigurable 2x2 MIMO system over a fixed 2x2 one.

  6. Unified Modeling Language description of the object-oriented multi-scale adaptive finite element method for Step-and-Flash Imprint Lithography Simulations

    International Nuclear Information System (INIS)

    Paszynski, Maciej; Gurgul, Piotr; Sieniek, Marcin; Pardo, David

    2010-01-01

    In the first part of the paper we present the multi-scale simulation of the Step-and-Flash Imprint Lithography (SFIL), a modern patterning process. The simulation utilizes the hp adaptive Finite Element Method (hp-FEM) coupled with Molecular Statics (MS) model. Thus, we consider the multi-scale problem, with molecular statics applied in the areas of the mesh where the highest accuracy is required, and the continuous linear elasticity with thermal expansion coefficient applied in the remaining part of the domain. The degrees of freedom from macro-scale element's nodes located on the macro-scale side of the interface have been identified with particles from nano-scale elements located on the nano-scale side of the interface. In the second part of the paper we present Unified Modeling Language (UML) description of the resulting multi-scale application (hp-FEM coupled with MS). We investigated classical, procedural codes from the point of view of the object-oriented (O-O) programming paradigm. The discovered hierarchical structure of classes and algorithms makes the UML project as independent on the spatial dimension of the problem as possible. The O-O UML project was defined at an abstract level, independent on the programming language used.

  7. Multi-Pulse Excitation for Underwater Analysis of Copper-Based Alloys Using a Novel Remote Laser-Induced Breakdown Spectroscopy (LIBS) System.

    Science.gov (United States)

    Guirado, Salvador; Fortes, Francisco J; Laserna, J Javier

    2016-04-01

    In this work, the use of multi-pulse excitation has been evaluated as an effective solution to mitigate the preferential ablation of the most volatile elements, namely Sn, Pb, and Zn, observed during laser-induced breakdown spectroscopy (LIBS) analysis of copper-based alloys. The novel remote LIBS prototype used in this experiments featured both single-pulse (SP-LIBS) and multi-pulse excitation (MP-LIBS). The remote instrument is capable of performing chemical analysis of submersed materials up to a depth of 50 m. Laser-induced breakdown spectroscopy analysis was performed at air pressure settings simulating the conditions during a real subsea analysis. A set of five certified bronze standards with variable concentration of Cu, As, Sn, Pb, and Zn were used. In SP-LIBS, signal emission is strongly sensitive to ambient pressure. In this case, fractionation effect was observed. Multi-pulse excitation circumvents the effect of pressure over the quantitative analysis, thus avoiding the fractionation phenomena observed in single pulse LIBS. The use of copper as internal standard minimizes matrix effects and discrepancies due to variation in ablated mass. © The Author(s) 2016.

  8. Single cell elemental analysis using nuclear microscopy

    International Nuclear Information System (INIS)

    Ren, M.Q.; Thong, P.S.P.; Kara, U.; Watt, F.

    1999-01-01

    The use of Particle Induced X-ray Emission (PIXE), Rutherford Backscattering Spectrometry (RBS) and Scanning Transmission Ion Microscopy (STIM) to provide quantitative elemental analysis of single cells is an area which has high potential, particularly when the trace elements such as Ca, Fe, Zn and Cu can be monitored. We describe the methodology of sample preparation for two cell types, the procedures of cell imaging using STIM, and the quantitative elemental analysis of single cells using RBS and PIXE. Recent work on single cells at the Nuclear Microscopy Research Centre,National University of Singapore has centred around two research areas: (a) Apoptosis (programmed cell death), which has been recently implicated in a wide range of pathological conditions such as cancer, Parkinson's disease etc, and (b) Malaria (infection of red blood cells by the malaria parasite). Firstly we present results on the elemental analysis of human Chang liver cells (ATTCC CCL 13) where vanadium ions were used to trigger apoptosis, and demonstrate that nuclear microscopy has the capability of monitoring vanadium loading within individual cells. Secondly we present the results of elemental changes taking place in individual mouse red blood cells which have been infected with the malaria parasite and treated with the anti-malaria drug Qinghaosu (QHS)

  9. Elemental characterization of herbal medicines used in Ghana by instrumental neutron activation analysis and atomic absorption spectrometry and multivariate statistical analysis

    International Nuclear Information System (INIS)

    Ayivor, J.E.; Nyarko, B.J.B.; Dampare, S.B.; Okine, L.K.

    2010-01-01

    k 0 instrumental neutron activation analysis and atomic absorption spectrometry were applied to determine multi elements in thirteen Ghanaian herbal medicines used for the management of various diseases. Concentrations of AI, Cu, Mg, Mn and Na were determined. As, Br, K, CI, and Na were determined by short and medium irradiations at a thermal neutron flux of 5x10ncm -2 s -1 . Fe, Cr, Pb, Co, Ni, Sn, Ca, Ba, Li and Sb were determined using atomic absorption spectrometry. Ba, Cu, Li and V were present at trace levels whereas AI, CI, Na, Ca were present at major levels. K, Br, Mg, Mn, Co, Ni, Fe and Sb were also present at minor levels. The precision and accuracy of the method using real samples and standard reference materials were within ±10% of the reported value. Multivariate analytical techniques, such as cluster analysis and principal component analysis (PCA)/factor analysis (FA), have been applied to evaluate the chemical variations in the herbal medicine dataset. All the 13 samples may be grouped into two statistically significant clusters, reflecting the different chemical compositions. The concentrations of elements were within the recommended daily allowances or maximum permissible levels posing no adverse effects on human health.

  10. Towards atomically resolved EELS elemental and fine structure mapping via multi-frame and energy-offset correction spectroscopy.

    Science.gov (United States)

    Wang, Yi; Huang, Michael R S; Salzberger, Ute; Hahn, Kersten; Sigle, Wilfried; van Aken, Peter A

    2018-01-01

    Electron energy-loss spectroscopy and energy-dispersive X-ray spectroscopy are two of the most common means for chemical analysis in the scanning transmission electron microscope. The marked progress of the instrumentation hardware has made chemical analysis at atomic resolution readily possible nowadays. However, the acquisition and interpretation of atomically resolved spectra can still be problematic due to image distortions and poor signal-to-noise ratio of the spectra, especially for investigation of energy-loss near-edge fine structures. By combining multi-frame spectrum imaging and automatic energy-offset correction, we developed a spectrum imaging technique implemented into customized DigitalMicrograph scripts for suppressing image distortions and improving the signal-to-noise ratio. With practical examples, i.e. SrTiO 3 bulk material and Sr-doped La 2 CuO 4 superlattices, we demonstrate the improvement of elemental mapping and the EELS spectrum quality, which opens up new possibilities for atomically resolved EELS fine structure mapping. Copyright © 2017 The Authors. Published by Elsevier B.V. All rights reserved.

  11. Characteristic Elemental Composition of Oil Pigments using Instrumental Neutron Activation Analysis

    International Nuclear Information System (INIS)

    Chung, Yong Sam; Kim, Sun Ha; Sun, Gwang Min; Lim, Jong Myung; Moon, Jong Hwa; Kim, Young Jin; Lim, Sung Jin; Song, Yu Na; Kim, Ken

    2009-01-01

    The principal aim of this study is to identify the applicability of instrumental neutron activation analysis as a non-destructive examination tool for the quantitative composition analysis associated with authentication, restoration, and conservation of art objects in the field of cultural heritage. Generally, the chemical composition of pigments are associated with the colors such as white, yellow, orange, red, green, blue and black, and it varies with raw materials of pigments. According to the colors of a different pigments, chemical compositions are as follows; for example, white pigments were used for a mixture of Pb(CO 3 ) 2 , PbSO 4 , PbO, Pb(OH) 2 , ZnO, ZnS, TiO 2 , BaSO 4 , CaCO 3 , Al 2 O 3 , As 2 S 3 , etc.; black pigments were series of carbon black, borne ash, MnO+Mn 2 O 3 , etc.; red pigments were Fe 2 O 3 , Pb 3 O 4 , HgS, PbMo 4 , CdS+CdSe, etc.; brown and yellow pigments were PbCrO 4 , ZnCrO 4 , CdS-ZnS, K 3 [Co(NO 2 ) 6 ], Pb(SbO 3 ) 2 , C 19 H 16 O 11 Mg, SrCrO 4 , etc.; green pigments were Cr 2 O 3 , Cr 2 O(OH) 4 , Cu(C 2 H 3 O 2 )-2Cu(OH) 2 ), Cr 2 O 3 -Al 2 O 3 -CoO, etc.; blue pigments were Fe 4 [Fe(CN) 6 ] 3 , CoO-Al 2 O 3 , Na 8 - 10 Al 6 Si 6 O 24 S 2-4 , etc. This first step is to obtain quantitative data on the concentrations of major, minor and trace elements in oil pigments and to explain pigment sources by statistical treatment as reported in many literatures. The determination of major, minor and micro elements in the subject materials are essential in many fields of basic science and technology as well as commercial and industrial fields. In particular, direct analysis of a sample offers a more effective investigation method in these fields. Instrumental neutron activation analysis (INAA) has an inherent advantage of being a non-destructive, simultaneously multi-elemental analysis with high accuracy and sensitivity. In order to characterize the elemental contents of art objects, the quantitative analysis of oil pigment series was

  12. Analysis of light elements by PIGE

    International Nuclear Information System (INIS)

    Kim, Y. S.; Choi, H. W.; Kim, D. K.; Woo, H. J.; Kim, N. B.; Park, K. S.

    2000-01-01

    The PIGE (Proton Induced Gamma ray Emission) method was applied for the measurement of light elements Li - K. A test measurement has been performed for geological, biological, environmental and material samples by using a standard sample for each element. The measurement was performed for the two proton energies of 2.4 and 3.4 MeV, and 3.4MeV was found to yield better result for multielemental analysis. The result shows a fair agreement within 15% for all elements with standard values. The detection limits of Li, B, F and Na are less than 100 ppm, while those of the other elements are from a few hundred ppm to a few percents. (author)

  13. Principle of neutron activation analysis and its use for determination of trace elements in sediment

    International Nuclear Information System (INIS)

    Verma, Rakesh

    2012-01-01

    Neutron Activation analysis (NAA) is a multi element analysis technique, often non-destructive in nature where approximately 75 elements can be measured with the detection limits ranging from 10 -6 to 10 -12 g of element in a sample. Typical sample sizes range from 1 mg to 1 g, however in principle much larger samples can be activated and the size is only limited by the capacity of the neutron irradiation facility. In NAA, a sample (solid or liquid or gas) is exposed to neutrons and radiations emitted by the radioactive products, formed during the nuclear reaction, are measured using a suitable detector. The energy of the emitted radiation is a characteristic of a radioisotope whereas the intensity of the emitted radiation is proportional to the mass of the analyte. NAA can be carried out by measurement of (i) prompt gamma rays emitted by compound nucleus, called prompt gamma ray NAA (PGNAA) and (ii) β rays emitted from radioactive product or delayed gamma rays emitted subsequent to β decay, called conventional NAA or simply NAA. PGNAA is an online measurement method. PGNAA is complementary to conventional NAA in terms of analyzing low Z elements. Conventional NAA is an offline method and is easy to perform. Depending upon the nature of matrix and analyte to be determined, three approaches are possible in NAA namely, (i) instrumental neutron activation analysis (INAA), (ii) radiochemical neutron activation analysis (RNAA), and (iii) chemical neutron activation analysis (CNAA). Quantification is accomplished by any of the three standardisation methodologies namely (i) absolute method (ii) relative method and (iii) single comparator method. The relative method is most precise and simple to perform. Natural processes responsible for the formation of bottom sediments can be altered by anthropogenic activities. Bottom sediments are a sink as well as a source of contaminants in the aquatic environment. Analysis of-sediments provides environmentally significant

  14. Automation system for measurement of gamma-ray spectra of induced activity for multi-element high-volume neutron activation analysis at the IBR-2 reactor of FLNP at JINR

    International Nuclear Information System (INIS)

    Pavlov, S.S.; Dmitriev, A.Yu.; Chepurchenko, I.A.; Frontas'eva, M.V.

    2014-01-01

    The automation system for measurement of induced activity of gamma-ray spectra for multi-element high-volume neutron activation analysis (NAA) was designed, developed and implemented at the IBR-2 reactor. The system consists of three devices of automatic sample changers for three Canberra HPGe detector-based gamma spectrometry systems. Each sample changer consists of two-axis linear positioning module M202A by DriveSet (DriveSet.de) company and disk with 45 slots for containers with samples. Control of automatic sample changer is performed by the Xemo S360U controller by Systec (systec.de) company. Positioning accuracy can reach 0.1 mm. Special software performs automatic changing of samples and measurement of gamma spectra at constant interaction with the NAA database. The system is unique and can be recommended for other laboratories as one of the possible ways of the NAA integrated automation

  15. Finite Element Analysis of Circular Plate using SolidWorks

    International Nuclear Information System (INIS)

    Kang, Yeo Jin; Jhung, Myung Jo

    2011-01-01

    Circular plates are used extensively in mechanical engineering for nuclear reactor internal components. The examples in the reactor vessel internals are upper guide structure support plate, fuel alignment plate, lower support plate etc. To verify the structural integrity of these plates, the finite element analyses are performed, which require the development of the finite element model. Sometimes it is very costly and time consuming to make the model especially for the beginners who start their engineering job for the structural analysis, necessitating a simple method to develop the finite element model for the pursuing structural analysis. Therefore in this study, the input decks are generated for the finite element analysis of a circular plate as shown in Fig. 1, which can be used for the structural analysis such as modal analysis, response spectrum analysis, stress analysis, etc using the commercial program Solid Works. The example problems are solved and the results are included for analysts to perform easily the finite element analysis of the mechanical plate components due to various loadings. The various results presented in this study would be helpful not only for the benchmark calculations and results comparisons but also as a part of the knowledge management for the future generation of young designers, scientists and computer analysts

  16. X-ray fluorescent elemental analysis. Ch. 16

    International Nuclear Information System (INIS)

    Baryshev, V.; Kulipanov, G.; Skrinsky, A.

    1991-01-01

    X-ray fluorescence analysis (XFA) is used worldwide to define a quantitative content of the elements as well as to visualize the distribution of elements in different regions (element mapping). Utilization of synchrotron radiation (SR) to excite X-ray fluorescence enables the XFA method to be qualitatively improved. This chapter reviews the experimental work in especially the last decade (author). 71 refs.; 24 figs.; 3 tabs

  17. Multi dimensional analysis of Design Basis Events using MARS-LMR

    International Nuclear Information System (INIS)

    Woo, Seung Min; Chang, Soon Heung

    2012-01-01

    Highlights: ► The one dimensional analyzed sodium hot pool is modified to a three dimensional node system, because the one dimensional analysis cannot represent the phenomena of the inside pool of a big size pool with many compositions. ► The results of the multi-dimensional analysis compared with the one dimensional analysis results in normal operation, TOP (Transient of Over Power), LOF (Loss of Flow), and LOHS (Loss of Heat Sink) conditions. ► The difference of the sodium flow pattern due to structure effect in the hot pool and mass flow rates in the core lead the different sodium temperature and temperature history under transient condition. - Abstract: KALIMER-600 (Korea Advanced Liquid Metal Reactor), which is a pool type SFR (Sodium-cooled Fast Reactor), was developed by KAERI (Korea Atomic Energy Research Institute). DBE (Design Basis Events) for KALIMER-600 has been analyzed in the one dimension. In this study, the one dimensional analyzed sodium hot pool is modified to a three dimensional node system, because the one dimensional analysis cannot represent the phenomena of the inside pool of a big size pool with many compositions, such as UIS (Upper Internal Structure), IHX (Intermediate Heat eXchanger), DHX (Decay Heat eXchanger), and pump. The results of the multi-dimensional analysis compared with the one dimensional analysis results in normal operation, TOP (Transient of Over Power), LOF (Loss of Flow), and LOHS (Loss of Heat Sink) conditions. First, the results in normal operation condition show the good agreement between the one and multi-dimensional analysis. However, according to the sodium temperatures of the core inlet, outlet, the fuel central line, cladding and PDRC (Passive Decay heat Removal Circuit), the temperatures of the one dimensional analysis are generally higher than the multi-dimensional analysis in conditions except the normal operation state, and the PDRC operation time in the one dimensional analysis is generally longer than

  18. Analysis of trace elements in opal using PIXE

    Energy Technology Data Exchange (ETDEWEB)

    Hinrichs, Ruth, E-mail: ruth.hinrichs@ufrgs.br [Instituto de Geociências, Universidade Federal do Rio Grande do Sul, Porto Alegre, RS (Brazil); Programa de Pós-graduação em Física, UFRGS, Porto Alegre, RS (Brazil); Bertol, A.P.L. [Programa de Pós-graduação em Física, UFRGS, Porto Alegre, RS (Brazil); Vasconcellos, M.A.Z. [Programa de Pós-graduação em Física, UFRGS, Porto Alegre, RS (Brazil); Instituto de Física, UFRGS, Porto Alegre, RS (Brazil)

    2015-11-15

    Particle induced X-ray emission (PIXE) analysis is particularly important for the analysis of trace elements of precious samples, being one of the few methods to determine elements with ppm concentration that does not affect sample integrity. A PIXE methodology for trace element analysis in opal was developed. To avoid detector count saturation due to the high number of Si-Kα X-rays generated in the sample, several filters were employed to optimize the reduction of the Si-Kα signal, while maintaining acceptable intensities of the other relevant X-ray lines. Two proton beam energies were tested, to establish the signal to noise ratio in different X-ray energies. Spectra were fitted with the software GUPIX, using a matrix composition determined with electron beam excited energy dispersive X-ray spectrometry. Above the energy of the silicon X-ray, several trace elements were quantified.

  19. Contribution to assessing the stiffness reduction of structural elements in the global stability analysis of precast concrete multi-storey buildings

    Directory of Open Access Journals (Sweden)

    M. C. Marin

    Full Text Available This study deals with the reduction of the stiffness in precast concrete structural elements of multi-storey buildings to analyze global stability. Having reviewed the technical literature, this paper present indications of stiffness reduction in different codes, standards, and recommendations and compare these to the values found in the present study. The structural model analyzed in this study was constructed with finite elements using ANSYS® software. Physical Non-Linearity (PNL was considered in relation to the diagrams M x N x 1/r, and Geometric Non-Linearity (GNL was calculated following the Newton-Raphson method. Using a typical precast concrete structure with multiple floors and a semi-rigid beam-to-column connection, expressions for a stiffness reduction coefficient are presented. The main conclusions of the study are as follows: the reduction coefficients obtained from the diagram M x N x 1/r differ from standards that use a simplified consideration of PNL; the stiffness reduction coefficient for columns in the arrangements analyzed were approximately 0.5 to 0.6; and the variation of values found for stiffness reduction coefficient in concrete beams, which were subjected to the effects of creep with linear coefficients from 0 to 3, ranged from 0.45 to 0.2 for positive bending moments and 0.3 to 0.2 for negative bending moments.

  20. An economic analysis of a multi-commodity fruit and vegetable irradiator

    International Nuclear Information System (INIS)

    Brown, M.D.; Eakin, D.E.; Young, J.K.; Tingey, G.L.

    1987-01-01

    Although irradiation of foods has been studied since the late 1940's and irradiation of grains and potatoes has been approved for years, only recently has the Food and Drug Administration approved irradiation of pork, fresh fruits and vegetables at doses up to 100 krad for commercial sale. A key element in commercializing irradiation technology by the food processing industry is economic viability. This paper presents an economic analysis for a multi-commodity fruit and vegetable irradiator processing apples, cherries, pears, asparagus, onions, and potatoes. Dose, throughput, and the schedule were examined. Design information and capital and operating costs for various sizes of irradiators are presented. The economics look promising, with typical costs in larger facilities in the range of a few cents per pound of product

  1. Trace and ultratrace level elemental and speciation analysis

    International Nuclear Information System (INIS)

    Arunachalam, J.

    2012-01-01

    Accurate determination of elements present at parts per million and billion levels in various matrices is a growing requirement in different fields. In environmental sciences various trace elements need to be analyzed so as establish the dispersal models of pollutants or the adequacy of effluent treatment prior to discharge into water bodies. The issues of bioaccumulation and magnification are important in aquatic systems. In nutrition and biochemistry one has to establish the bio-availability of essential and toxic elemental species as toxic elements prevent assimilation of essential elements. Fission and fusion technologies use a variety of structural materials requiring many trace elements to be present at levels strictly below the specified levels. Ultra-pure bulk semiconductor materials are required for fabrication devices. In metallurgy and materials sciences too, various trace elements are known to influence the properties. In the emerging fields like nanotechnology, it is necessary to understand the passage and accumulation of nano-particles inside the cells, through trace analysis. Many analytical techniques exist which can provide the concentration information in the bulk materials with good accuracy. They include ICP-AES, FAAS, and ICP-MS, which are solution based techniques. Direct solid state analytical techniques are Glow Discharge Mass Spectrometry (GDMS) and XRF. Accelerator based ion-beam analysis techniques can provide information on concentration and depth profiles of different elements in layered structures. Hyphenated techniques such as HPLC/lC-ICPMS, are helpful in identifying various chemical oxidation states in which a given element might be present in a matrix, which is termed as speciation analysis. This presentation will include the existing analytical competencies and the laboratory requirements for trace and ultra trace element elemental and speciation analyses and their applications. (author)

  2. Determination of multi-element composition of Vietnamese marine sediment and tuna fish by k0-standardized neutron activation analysis

    International Nuclear Information System (INIS)

    Manh-Dung Ho; Quang-Thien Tran; Van-Doanh Ho; Thi-Sy Nguyen

    2016-01-01

    The k 0 -standardized neutron activation analysis (k 0 -NAA) has been applied for determination of multiple elements (25 elements: Al, As, Ba, Br, Ca, Cl, Co, Cr, Cs, Cu, Eu, Fe, Hg, K, La, Mg, Na, Rb, Sc, Se, Sm, Th, Ti, V and Zn) in marine sediment and tuna fish. About 50 marine sediment and 9 tuna fish samples were collected in two coastal areas of Vietnam. The health risk index (HRI) values of As and Br were higher than 1.0 for the tuna fish. Also, HRI value of Hg was 8.92 × 10 -1 indicating a relatively high potential health risk, whiles Co and Mn with HRIs = 1.56 × 10 -4 and 8.56 × 10 -4 , respectively, have the lowest potential health risks. Average enrichment factors using Al as a reference element (EF Al ) were higher than 1.5 for Eu, La, Zn, Th, Cs and As in which the highest EF Al value for As was higher than 10. This study showed that the HRI value of As in the tuna fish correlated positively with the EF Al value for the element in the marine sediment. (author)

  3. SAFE-PLANE, Stress Analysis of Planar Structure by Finite Elements Method

    International Nuclear Information System (INIS)

    Cornell, D.C.; Reich, Morris

    1967-01-01

    1 - Description of problem or function: SAFE-PLANE is applied to two- dimensional structures of arbitrary geometry under in-plane loads. Either plane stress or plane strain conditions may be imposed. Mechanical and thermal loads are permitted. 2 - Method of solution: The finite-element method is used to construct a mathematical model by assembling discrete elements. The total potential energy of the structure is determined and subsequently minimized by iteration on components of the displacement field until static equilibrium of the structure is attained. Strains and stresses are computed from the resulting displacements. 3 - Restrictions on the complexity of the problem: Multi-material structures with varying rigidities converge very slowly. Not valid for incompressible materials. Maximum number of nodal points = 675. Maximum number of elements = 1350

  4. Trace element analysis of common salt using neutron activation analysis

    International Nuclear Information System (INIS)

    Usman, K.

    1993-01-01

    Instrumental Fast Neutron Activation Analysis (IFNAA) technique has been used in the qualitative and quantitative determination of the impurity elements in common salt. Samples of the different types of common salt processed in Nigeria and some of those imported into the country were used. The type A711 KAMAN neutron generator and a high-purity Germanium (HpGe) gamma spectrometer available at the Centre for Energy Research and Training, Ahmadu Bello University, Zaria has been used. The ORTEC ADCAM 100 Emulation Software (Maestro) was used in the qualitative measurement of the detected elements. The G.R.G Activation Analysis System by G. R. Gilmore, 1987, was used in the quantitative determination of the elements detected by relative method. Aluminium and arsenic were detected and measured

  5. Code Coupling for Multi-Dimensional Core Transient Analysis

    International Nuclear Information System (INIS)

    Park, Jin-Woo; Park, Guen-Tae; Park, Min-Ho; Ryu, Seok-Hee; Um, Kil-Sup; Lee Jae-Il

    2015-01-01

    After the CEA ejection, the nuclear power of the reactor dramatically increases in an exponential behavior until the Doppler effect becomes important and turns the reactivity balance and power down to lower levels. Although this happens in a very short period of time, only few seconds, the energy generated can be very significant and cause fuel failures. The current safety analysis methodology which is based on overly conservative assumptions with the point kinetics model results in quite adverse consequences. Thus, KEPCO Nuclear Fuel(KNF) is developing the multi-dimensional safety analysis methodology to mitigate the consequences of the single CEA ejection accident. For this purpose, three-dimensional core neutron kinetics code ASTRA, sub-channel analysis code THALES, and fuel performance analysis code FROST, which have transient calculation performance, were coupled using message passing interface (MPI). This paper presents the methodology used for code coupling and the preliminary simulation results with the coupled code system (CHASER). Multi-dimensional core transient analysis code system, CHASER, has been developed and it was applied to simulate a single CEA ejection accident. CHASER gave a good prediction of multi-dimensional core transient behaviors during transient. In the near future, the multi-dimension CEA ejection analysis methodology using CHASER is planning to be developed. CHASER is expected to be a useful tool to gain safety margin for reactivity initiated accidents (RIAs), such as a single CEA ejection accident

  6. Code Coupling for Multi-Dimensional Core Transient Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Park, Jin-Woo; Park, Guen-Tae; Park, Min-Ho; Ryu, Seok-Hee; Um, Kil-Sup; Lee Jae-Il [KEPCO NF, Daejeon (Korea, Republic of)

    2015-05-15

    After the CEA ejection, the nuclear power of the reactor dramatically increases in an exponential behavior until the Doppler effect becomes important and turns the reactivity balance and power down to lower levels. Although this happens in a very short period of time, only few seconds, the energy generated can be very significant and cause fuel failures. The current safety analysis methodology which is based on overly conservative assumptions with the point kinetics model results in quite adverse consequences. Thus, KEPCO Nuclear Fuel(KNF) is developing the multi-dimensional safety analysis methodology to mitigate the consequences of the single CEA ejection accident. For this purpose, three-dimensional core neutron kinetics code ASTRA, sub-channel analysis code THALES, and fuel performance analysis code FROST, which have transient calculation performance, were coupled using message passing interface (MPI). This paper presents the methodology used for code coupling and the preliminary simulation results with the coupled code system (CHASER). Multi-dimensional core transient analysis code system, CHASER, has been developed and it was applied to simulate a single CEA ejection accident. CHASER gave a good prediction of multi-dimensional core transient behaviors during transient. In the near future, the multi-dimension CEA ejection analysis methodology using CHASER is planning to be developed. CHASER is expected to be a useful tool to gain safety margin for reactivity initiated accidents (RIAs), such as a single CEA ejection accident.

  7. Storage and pre-neutron-activation-analysis treatment for trace-element analysis in urine

    International Nuclear Information System (INIS)

    Blotcky, A.J.; Rack, E.P.

    1985-01-01

    The problems regarding storage and pre-neutron-activation-analysis treatment for the elements aluminum, calcium, vanadium, selenium, copper, iodine, zinc, manganese, and magnesium in a urine matrix are reviewed. The type of collection and storage procedure and pre-neutron activation analysis treatment of urine depend on the specific trace element; that is, its inherent physical and chemical properties. Specifically polyethylene in teflon containers are the most suitable for general determinations. Whether any preservative is added would depend upon the stability of the trace element and its tendency for surface adsorption. Preferably, preservatives should contain no radioactivatable elements for maximum efficacy. Freeze drying or packing urine shipments under dry ice needs to be explored on an individual basis. Each pre- or post-neutron activation analysis treatment is specific and optimized for the trace element analyzed

  8. ANSYS mechanical APDL for finite element analysis

    CERN Document Server

    Thompson, Mary Kathryn

    2017-01-01

    ANSYS Mechanical APDL for Finite Element Analysis provides a hands-on introduction to engineering analysis using one of the most powerful commercial general purposes finite element programs on the market. Students will find a practical and integrated approach that combines finite element theory with best practices for developing, verifying, validating and interpreting the results of finite element models, while engineering professionals will appreciate the deep insight presented on the program's structure and behavior. Additional topics covered include an introduction to commands, input files, batch processing, and other advanced features in ANSYS. The book is written in a lecture/lab style, and each topic is supported by examples, exercises and suggestions for additional readings in the program documentation. Exercises gradually increase in difficulty and complexity, helping readers quickly gain confidence to independently use the program. This provides a solid foundation on which to build, preparing readers...

  9. Assessment of Material Solutions of Multi-level Garage Structure Within Integrated Life Cycle Design Process

    Science.gov (United States)

    Wałach, Daniel; Sagan, Joanna; Gicala, Magdalena

    2017-10-01

    The paper presents an environmental and economic analysis of the material solutions of multi-level garage. The construction project approach considered reinforced concrete structure under conditions of use of ordinary concrete and high-performance concrete (HPC). Using of HPC allowed to significant reduction of reinforcement steel, mainly in compression elements (columns) in the construction of the object. The analysis includes elements of the methodology of integrated lice cycle design (ILCD). By making multi-criteria analysis based on established weight of the economic and environmental parameters, three solutions have been evaluated and compared within phase of material production (information modules A1-A3).

  10. Multi criteria analysis in the renewable energy industry

    CERN Document Server

    San Cristóbal Mateo, José Ramón

    2012-01-01

    Decision makers in the Renewable Energy sector face an increasingly complex social, economic, technological, and environmental scenario in their decision process. Different groups of decision-makers become involved in the process, each group bringing along different criteria therefore, policy formulation for fossil fuel substitution by Renewable Energies must be addressed in a multi-criteria context. Multi Criteria Analysis in the Renewable Energy Industry is a direct response to the increasing interest in the Renewable Energy industry which can be seen as an important remedy to many environmental problems that the world faces today. The multiplicity of criteria and the increasingly complex social, economic, technological, and environmental scenario makes multi-criteria analysis a valuable tool in the decision-making process for fossil fuel substitution. The detailed chapters explore the use of the Multi-criteria decision-making methods and how they provide valuable assistance in reaching equitable and accept...

  11. Stability analysis of multi-infeed HVDC system applying VSC-HVDC

    DEFF Research Database (Denmark)

    Liu, Yan; Chen, Zhe

    2010-01-01

    This paper presents a general model of dual infeed HVDC system applying VSC-HVDC, which can be used as an element in large multi infeed HVDC system. The model may have different structure under different grid faults because of the action of breakers. Hence power flow of the system based on this m...

  12. Aerodynamic multi-objective integrated optimization based on principal component analysis

    Directory of Open Access Journals (Sweden)

    Jiangtao HUANG

    2017-08-01

    Full Text Available Based on improved multi-objective particle swarm optimization (MOPSO algorithm with principal component analysis (PCA methodology, an efficient high-dimension multi-objective optimization method is proposed, which, as the purpose of this paper, aims to improve the convergence of Pareto front in multi-objective optimization design. The mathematical efficiency, the physical reasonableness and the reliability in dealing with redundant objectives of PCA are verified by typical DTLZ5 test function and multi-objective correlation analysis of supercritical airfoil, and the proposed method is integrated into aircraft multi-disciplinary design (AMDEsign platform, which contains aerodynamics, stealth and structure weight analysis and optimization module. Then the proposed method is used for the multi-point integrated aerodynamic optimization of a wide-body passenger aircraft, in which the redundant objectives identified by PCA are transformed to optimization constraints, and several design methods are compared. The design results illustrate that the strategy used in this paper is sufficient and multi-point design requirements of the passenger aircraft are reached. The visualization level of non-dominant Pareto set is improved by effectively reducing the dimension without losing the primary feature of the problem.

  13. Finite element application to global reactor analysis

    International Nuclear Information System (INIS)

    Schmidt, F.A.R.

    1981-01-01

    The Finite Element Method is described as a Coarse Mesh Method with general basis and trial functions. Various consequences concerning programming and application of Finite Element Methods in reactor physics are drawn. One of the conclusions is that the Finite Element Method is a valuable tool in solving global reactor analysis problems. However, problems which can be described by rectangular boxes still can be solved with special coarse mesh programs more efficiently. (orig.) [de

  14. A CAREM type fuel element dynamic analysis

    International Nuclear Information System (INIS)

    Magoia, J.E.

    1990-01-01

    A first analysis on the dynamic behaviour of a fuel element designed for the CAREM nuclear reactor (Central Argentina de Elementos Modulares) was performed. The model used to represent this dynamic behaviour was satisfactorily evaluated. Using primary estimations for some of its numerical parameters, a first approximation to its natural vibrational modes was obtained. Results obtained from fuel elements frequently used in nuclear power plants of the PWR (Pressurized Water Reactors) type, are compared with values resulting from similar analysis. (Author) [es

  15. Exploration of multi-fold symmetry element-loaded superconducting radio frequency structure for reliable acceleration of low- & medium-beta ion species

    International Nuclear Information System (INIS)

    Huang, Shichun; Geng, Rongli

    2015-09-01

    Reliable acceleration of low- to medium-beta proton or heavy ion species is needed for future high-current superconducting radio frequency (SRF) accelerators. Due to the high-Q nature of an SRF resonator, it is sensitive to many factors such as electron loading (from either the accelerated beam or from parasitic field emitted electrons), mechanical vibration, and liquid helium bath pressure fluctuation etc. To increase the stability against those factors, a mechanically strong and stable RF structure is desirable. Guided by this consideration, multi-fold symmetry element-loaded SRF structures (MFSEL), cylindrical tanks with multiple (n>=3) rod-shaped radial elements, are being explored. The top goal of its optimization is to improve mechanical stability. A natural consequence of this structure is a lowered ratio of the peak surface electromagnetic field to the acceleration gradient as compared to the traditional spoke cavity. A disadvantage of this new structure is an increased size for a fixed resonant frequency and optimal beta. This paper describes the optimization of the electro-magnetic (EM) design and preliminary mechanical analysis for such structures.

  16. Trace element analysis of nail polishes

    International Nuclear Information System (INIS)

    Misra, G.; Mittal, V.K.; Sahota, H.S.

    1999-01-01

    Instrumental neutron activation analysis (INAA) technique was used to measure the concentrations of various trace elements in nail polishes of popular Indian and foreign brands. The aim of the present experiment was to see whether trace elements could distinguish nail polishes of different Indian and foreign brands from forensic point of view. It was found that cesium can act as a marker to differentiate foreign and Indian brands. (author)

  17. Association of glass fragments by their trace elemental content using ICP-MS and LA-ICP-MS in the analysis scheme

    Science.gov (United States)

    Almirall, Jose R.; Montero, Shirly; Furton, Kenneth G.

    2002-08-01

    The importance of glass as evidence of association between a crime event and a suspect has been recognized for some time. Glass is a fragile material that is often found at the scenes of crimes such as burglaries, hit-and-run accidents and violent crime offenses. The physical and chemical properties of glass can be used to differentiate between possible sources and as evidence of association between two fragments of glass thought to originate from the same source. Refractive index (RI) comparisons have been used for this purpose but due to the improved control over glass manufacturing processes, RI values often cannot differentiate glasses, even if the glass originates from different sources. Elemental analysis methods such as NAA, XRF, ICP-AES, and Inductively Coupled Plasma Mass Spectrometry (ICP-MS) have also been used for the comparison of trace elemental compositions and these techniques have been shown to provide an improvement in the discrimination of glass fragments over RI comparisons alone. The multi-element capability and the sensitivity of ICP-MS combined with the simplified sample introduction of laser ablation prior to ion detection provides for an excellent and relatively non-destructive technique for elemental analysis of glass fragments. The methodology for solution analysis (digestion procedure) and solid sample analysis (laser ablation) of glass is reported and the analytical results are compared. An isotope dilution method is also reported as a high precision technique for elemental analysis of glass fragments. The optimum sampling parameters for laser ablation, for semi-quantitative analysis and element ratio comparisons are also presented. Finally, the results of a case involving the breaking of 15 vehicle windows in an airport parking lot and the association of a suspect to the breakings by the glass fragments found on his person are also presented.

  18. Computer simulation of multi-elemental fusion reactor materials

    International Nuclear Information System (INIS)

    Voertler, K.

    2011-01-01

    Thermonuclear fusion is a sustainable energy solution, in which energy is produced using similar processes as in the sun. In this technology hydrogen isotopes are fused to gain energy and consequently to produce electricity. In a fusion reactor hydrogen isotopes are confined by magnetic fields as ionized gas, the plasma. Since the core plasma is millions of degrees hot, there are special needs for the plasma-facing materials. Moreover, in the plasma the fusion of hydrogen isotopes leads to the production of high energetic neutrons which sets demanding abilities for the structural materials of the reactor. This thesis investigates the irradiation response of materials to be used in future fusion reactors. Interactions of the plasma with the reactor wall leads to the removal of surface atoms, migration of them, and formation of co-deposited layers such as tungsten carbide. Sputtering of tungsten carbide and deuterium trapping in tungsten carbide was investigated in this thesis. As the second topic the primary interaction of the neutrons in the structural material steel was examined. As model materials for steel iron chromium and iron nickel were used. This study was performed theoretically by the means of computer simulations on the atomic level. In contrast to previous studies in the field, in which simulations were limited to pure elements, in this work more complex materials were used, i.e. they were multi-elemental including two or more atom species. The results of this thesis are in the microscale. One of the results is a catalogue of atom species, which were removed from tungsten carbide by the plasma. Another result is e.g. the atomic distributions of defects in iron chromium caused by the energetic neutrons. These microscopic results are used in data bases for multiscale modelling of fusion reactor materials, which has the aim to explain the macroscopic degradation in the materials. This thesis is therefore a relevant contribution to investigate the

  19. Using the ion microprobe mass analyser for trace element analysis

    International Nuclear Information System (INIS)

    Schilling, J.H.

    1978-01-01

    Most techniques for the analysis of trace elements are capable of determining the concentrations in a bulk sample or solution, but without reflecting their distribution. In a bulk analysis therefore elements which occur in high concentration in a few precipitates would still be considered trace elements even though their local concentration greatly exceed the normally accepted trace elements concentration limit. Anomalous distribution is also shown by an oxide layer, a few hundred Angstrom thick, on an aluminium sample. A low oxide concentration would be reported if it were included in the bulk analysis, which contradicts the high surface concentration. The importance of a knowledge of the trace element distribution is therefore demonstrated. Distributional trace element analysis can be carried out using the ion microprobe mass analyser (IMMA). Since the analytical technique used in this instrument, namely secondary ion mass spectrometry (SIMS), is not universally appreciated, the instrument and its features will be described briefly followed by a discussion of quantitative analysis and the related subjects of detection limit and sample consumption. Finally, a few examples of the use of the instrument are given

  20. Combined multi-criteria and cost-benefit analysis

    DEFF Research Database (Denmark)

    Moshøj, Claus Rehfeld

    1996-01-01

    The paper is an introduction to both theory and application of combined Cost-Benefit and Multi-Criteria Analysis. The first section is devoted to basic utility theory and its practical application in Cost-Benefit Analysis. Based on some of the problems encountered, arguments in favour...... of the application of utility-based Multi-Criteria Analyses methods as an extension and refinement of the traditional Cost-Benefit Analysis are provided. The theory presented in this paper is closely related the methods used in the WARP software (Leleur & Jensen, 1989). The presentation is however wider in scope.......The second section introduces the stated preference methodology used in WARP to create weight profiles for project pool sensitivity analysis. This section includes a simple example. The third section discusses how decision makers can get a priori aid to make their pair-wise comparisons based on project pool...

  1. Finite element analysis of an inflatable torus considering air mass structural element

    Science.gov (United States)

    Gajbhiye, S. C.; Upadhyay, S. H.; Harsha, S. P.

    2014-01-01

    Inflatable structures, also known as gossamer structures, are at high boom in the current space technology due to their low mass and compact size comparing to the traditional spacecraft designing. Internal pressure becomes the major source of strength and rigidity, essentially stiffen the structure. However, inflatable space based membrane structure are at high risk to the vibration disturbance due to their low structural stiffness and material damping. Hence, the vibration modes of the structure should be known to a high degree of accuracy in order to provide better control authority. In the past, most of the studies conducted on the vibration analysis of gossamer structures used inaccurate or approximate theories in modeling the internal pressure. The toroidal shaped structure is one of the important key element in space application, helps to support the reflector in space application. This paper discusses the finite-element analysis of an inflated torus. The eigen-frequencies are obtained via three-dimensional small-strain elasticity theory, based on extremum energy principle. The two finite-element model (model-1 and model-2) have cases have been generated using a commercial finite-element package. The structure model-1 with shell element and model-2 with the combination of the mass of enclosed fluid (air) added to the shell elements have been taken for the study. The model-1 is computed with present analytical approach to understand the convergence rate and the accuracy. The convergence study is made available for the symmetric modes and anti-symmetric modes about the centroidal-axis plane, meeting the eigen-frequencies of an inflatable torus with the circular cross section. The structural model-2 is introduced with air mass element and analyzed its eigen-frequency with different aspect ratio and mode shape response using in-plane and out-plane loading condition are studied.

  2. Multi codes and multi-scale analysis for void fraction prediction in hot channel for VVER-1000/V392

    International Nuclear Information System (INIS)

    Hoang Minh Giang; Hoang Tan Hung; Nguyen Huu Tiep

    2015-01-01

    Recently, an approach of multi codes and multi-scale analysis is widely applied to study core thermal hydraulic behavior such as void fraction prediction. Better results are achieved by using multi codes or coupling codes such as PARCS and RELAP5. The advantage of multi-scale analysis is zooming of the interested part in the simulated domain for detail investigation. Therefore, in this study, the multi codes between MCNP5, RELAP5, CTF and also the multi-scale analysis based RELAP5 and CTF are applied to investigate void fraction in hot channel of VVER-1000/V392 reactor. Since VVER-1000/V392 reactor is a typical advanced reactor that can be considered as the base to develop later VVER-1200 reactor, then understanding core behavior in transient conditions is necessary in order to investigate VVER technology. It is shown that the item of near wall boiling, Γ w in RELAP5 proposed by Lahey mechanistic method may not give enough accuracy of void fraction prediction as smaller scale code as CTF. (author)

  3. Elemental analysis techniques using proton microbeam

    International Nuclear Information System (INIS)

    Sakai, Takuro; Oikawa, Masakazu; Sato, Takahiro

    2005-01-01

    Proton microbeam is a powerful tool for two-dimensional elemental analysis. The analysis is based on Particle Induced X-ray Emission (PIXE) and Particle Induced Gamma-ray Emission (PIGE) techniques. The paper outlines the principles and instruments, and describes the dental application has been done in JAERI Takasaki. (author)

  4. The 1 MV multi-element AMS system for biomedical applications at the Netherlands Organization for Applied Scientific Research (TNO)

    Energy Technology Data Exchange (ETDEWEB)

    Klein, Matthias, E-mail: mklein@highvolteng.com [High Voltage Engineering Europa B.V., P.O. Box 99, 3800 AB Amersfoort (Netherlands); Vaes, W.H.J.; Fabriek, B.; Sandman, H. [TNO, P.O. Box 360, 3700 AJ Zeist (Netherlands); Mous, D.J.W.; Gottdang, A. [High Voltage Engineering Europa B.V., P.O. Box 99, 3800 AB Amersfoort (Netherlands)

    2013-01-15

    The Netherlands Organization for Applied Scientific Research (TNO) has installed a compact 1 MV multi-element AMS system manufactured by High Voltage Engineering Europa B.V., The Netherlands. TNO performs clinical research programs for pharmaceutical and innovative foods industry to obtain early pharmacokinetic data and to provide anti-osteoporotic efficacy data of new treatments. The AMS system will analyze carbon, iodine and calcium samples for this purpose. The first measurements on blank samples indicate background levels in the low 10{sup -12} for calcium and iodine, making the system well suited for these biomedical applications. Carbon blanks have been measured at low 10{sup -16}. For unattended, around-the-clock analysis, the system features the 200 sample version of the SO110 hybrid ion source and user friendly control software.

  5. Optimal task partition and state-dependent loading in heterogeneous two-element work sharing system

    International Nuclear Information System (INIS)

    Levitin, Gregory; Xing, Liudong; Ben-Haim, Hanoch; Dai, Yuanshun

    2016-01-01

    Many real-world systems such as multi-channel data communication, multi-path flow transmission and multi-processor computing systems have work sharing attributes where system elements perform different portions of the same task simultaneously. Motivated by these applications, this paper models a heterogeneous work-sharing system with two non-repairable elements. When one element fails, the other element takes over the uncompleted task of the failed element upon finishing its own part; the load level of the remaining operating element can change at the time of the failure, which further affects its performance, failure behavior and operation cost. Considering these dynamics, mission success probability (MSP), expected mission completion time (EMCT) and expected cost of successful mission (ECSM) are first derived. Further, optimization problems are formulated and solved, which find optimal task partition and element load levels maximizing MSP, minimizing EMCT or minimizing ECSM. Effects of element reliability, performance, operation cost on the optimal solutions are also investigated through examples. Results of this work can facilitate a tradeoff analysis of different mission performance indices for heterogeneous work-sharing systems. - Highlights: • A heterogeneous work-sharing system with two non-repairable elements is considered. • The optimal work distribution and element loading problem is formulated and solved. • Effects of element reliability, performance, operation cost on the optimal solutions are investigated.

  6. Structural analysis of reactor fuel elements

    International Nuclear Information System (INIS)

    Weeks, R.W.

    1977-01-01

    An overview of fuel-element modeling is presented that traces the development of codes for the prediction of light-water-reactor and fast-breeder-reactor fuel-element performance. It is concluded that although the mathematical analysis is now far advanced, the development and incorporation of mechanistic constitutive equations has not kept pace. The resultant reliance on empirical correlations severely limits the physical insight that can be gained from code extrapolations. Current efforts include modeling of alternate fuel systems, analysis of local fuel-cladding interactions, and development of a predictive capability for off-normal behavior. Future work should help remedy the current constitutive deficiencies and should include the development of deterministic failure criteria for use in design

  7. Elements of real analysis

    CERN Document Server

    Sprecher, David A

    2010-01-01

    This classic text in introductory analysis delineates and explores the intermediate steps between the basics of calculus and the ultimate stage of mathematics: abstraction and generalization.Since many abstractions and generalizations originate with the real line, the author has made it the unifying theme of the text, constructing the real number system from the point of view of a Cauchy sequence (a step which Dr. Sprecher feels is essential to learn what the real number system is).The material covered in Elements of Real Analysis should be accessible to those who have completed a course in

  8. Meso-Scale Finite Element Analysis of Mechanical Behavior of 3D Braided Composites Subjected to Biaxial Tension Loadings

    Science.gov (United States)

    Zhang, Chao; Curiel-Sosa, Jose L.; Bui, Tinh Quoc

    2018-04-01

    In many engineering applications, 3D braided composites are designed for primary loading-bearing structures, and they are frequently subjected to multi-axial loading conditions during service. In this paper, a unit-cell based finite element model is developed for assessment of mechanical behavior of 3D braided composites under different biaxial tension loadings. To predict the damage initiation and evolution of braiding yarns and matrix in the unit-cell, we thus propose an anisotropic damage model based on Murakami damage theory in conjunction with Hashin failure criteria and maximum stress criteria. To attain exact stress ratio, force loading mode of periodic boundary conditions which never been attempted before is first executed to the unit-cell model to apply the biaxial tension loadings. The biaxial mechanical behaviors, such as the stress distribution, tensile modulus and tensile strength are analyzed and discussed. The damage development of 3D braided composites under typical biaxial tension loadings is simulated and the damage mechanisms are revealed in the simulation process. The present study generally provides a new reference to the meso-scale finite element analysis (FEA) of multi-axial mechanical behavior of other textile composites.

  9. BATMAN: Bayesian Technique for Multi-image Analysis

    Science.gov (United States)

    Casado, J.; Ascasibar, Y.; García-Benito, R.; Guidi, G.; Choudhury, O. S.; Bellocchi, E.; Sánchez, S. F.; Díaz, A. I.

    2017-04-01

    This paper describes the Bayesian Technique for Multi-image Analysis (BATMAN), a novel image-segmentation technique based on Bayesian statistics that characterizes any astronomical data set containing spatial information and performs a tessellation based on the measurements and errors provided as input. The algorithm iteratively merges spatial elements as long as they are statistically consistent with carrying the same information (I.e. identical signal within the errors). We illustrate its operation and performance with a set of test cases including both synthetic and real integral-field spectroscopic data. The output segmentations adapt to the underlying spatial structure, regardless of its morphology and/or the statistical properties of the noise. The quality of the recovered signal represents an improvement with respect to the input, especially in regions with low signal-to-noise ratio. However, the algorithm may be sensitive to small-scale random fluctuations, and its performance in presence of spatial gradients is limited. Due to these effects, errors may be underestimated by as much as a factor of 2. Our analysis reveals that the algorithm prioritizes conservation of all the statistically significant information over noise reduction, and that the precise choice of the input data has a crucial impact on the results. Hence, the philosophy of BaTMAn is not to be used as a 'black box' to improve the signal-to-noise ratio, but as a new approach to characterize spatially resolved data prior to its analysis. The source code is publicly available at http://astro.ft.uam.es/SELGIFS/BaTMAn.

  10. Analysis and design of lumped element Marchand baluns

    DEFF Research Database (Denmark)

    Johansen, Tom Keinicke; Krozer, Viktor

    2008-01-01

    In this paper a novel design procedure for lumped element Marchand baluns is proposed. An analysis is performed on the balun structure in order to determine the conditions for ideal balun performance in terms of the lumped element values. The analysis is verified by two broadband designs centered...... around 22.75 GHz and differing only in terms of their impedance transformation ratio. EM simulation results on our proposed lumped element Marchand balun structure predicts an insertion loss of 4 dB and return loss of 40 dB at the design frequency of 22.75 GHz. The amplitude and phase imbalance...

  11. Multi-element analyses of earthworms for radioecology

    International Nuclear Information System (INIS)

    Yoshida, Satoshi; Muramatsu, Yasuyuki; Peijnenburg, W.

    2004-01-01

    Increasing attention on the environmental radiation protection realizes that more information is required on the transfer and accumulation of radionuclides in the biological compartments of the ecosystems. Earthworms play an important role in ecosystems, and might be a good indicator of soil contamination and its effect on the ecosystem. The elemental composition of earthworms gives useful information on background levels and possible accumulation of metals as well as related radionuclides. However, data for the elemental composition of earthworms are limited except for some specific heavy metals such as Cd, Zn, Pb and Cu. In this study, earthworms and their growth media were analyzed for 35 elements, including radionuclide related elements such as Cs, Sr, Th and U, in order to obtain the basic information on the transfer parameters of the elements. The earthworms analyzed were fed in the laboratory or collected in the environment. The concentrations and transfer factors (TFs) of the elements were determined both for laboratory and natural conditions. Relatively high TFs were observed for Na, Mg, P, K, Ca, Co, Ni, Cu, Zn, As, Se, Rb, Mo and Cd. The TFs for Al, Sc, Ti, Y, Nb and lanthanide elements were low. The TFs of Cs were different depending on the medium (soil type), indicating that bioavailability of Cs in the medium might be one of the important controlling factors of Cs concentration in earthworm. (author)

  12. An economic analysis of a multi-commodity fruit and vegetable irradiator

    International Nuclear Information System (INIS)

    Brown, M.D.; Eakin, D.E.; Young, J.K.; Tingey, G.L.

    1987-07-01

    Although irradiation of foods has been studied since the late 1940's and irradiation of grains and potatoes has been approved for years, only recently has the Food and Drug Administration approved irradiation of pork, fresh fruits and vegetables at doses up to 100 krad for commercial sale. A key element in commercializing irradiation technology by the food processing industry is economic viability. This paper presents an economic analysis for a multi-commodity fruit and vegetable irradiator processing apples, cherries, pears, asparagus, onions, and potatoes. Dose, throughput, and the schedule were examined. Design information and capital and operating costs for various sizes of irradiators are presented. The economics look promising, with typical costs in larger facilities in the range of a few cents per pound of product. 12 refs., 7 tabs

  13. Free vibration analysis of multi-span pipe conveying fluid with dynamic stiffness method

    International Nuclear Information System (INIS)

    Li Baohui; Gao Hangshan; Zhai Hongbo; Liu Yongshou; Yue Zhufeng

    2011-01-01

    Research highlights: → The dynamic stiffness method was proposed to analysis the free vibration of multi-span pipe conveying fluid. → The main advantage of the proposed method is that it can hold a high precision even though the element size is large. → The flowing fluid can weaken the pipe stiffness, when the fluid velocity increases, the natural frequencies of pipe are decreasing. - Abstract: By taking a pipe as Timoshenko beam, in this paper the original 4-equation model of pipe conveying fluid was modified by taking the dynamic effects of fluid into account. The shape function that always used in the finite element method was replaced by the exact wave solution of the modified four equations. And then the dynamic stiffness was deduced for the free vibration of pipe conveying fluid. The proposed method was validated by comparing the results of critical velocity with analytical solution for a simply supported pipe at both ends. In the example, the proposed method was applied to calculate the first three natural frequencies of a three span pipe with twelve meters long in three different cases. The results of natural frequency for the pipe conveying stationary fluid fitted well with that calculated by finite element software Abaqus. It was shown that the dynamic stiffness method can still hold high precision even though the element's size was quite large. And this is the predominant advantage of the proposed method comparing with conventional finite element method.

  14. Characteristic Elemental Composition of Oil Pigments using Instrumental Neutron Activation Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Yong Sam; Kim, Sun Ha; Sun, Gwang Min; Lim, Jong Myung; Moon, Jong Hwa; Kim, Young Jin [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of); Lim, Sung Jin; Song, Yu Na; Kim, Ken [National Museum of Contemporary Art, Gwacheon (Korea, Republic of)

    2009-10-15

    non-destructive, simultaneously multi-elemental analysis with high accuracy and sensitivity. In order to characterize the elemental contents of art objects, the quantitative analysis of oil pigment series was carried out using NAA facilities of the HANARO research reactor at the Korea Atomic Energy Research Institute in collaboration with the National Museum of Contemporary Art in Korea.

  15. A computational intelligent approach to multi-factor analysis of violent crime information system

    Science.gov (United States)

    Liu, Hongbo; Yang, Chao; Zhang, Meng; McLoone, Seán; Sun, Yeqing

    2017-02-01

    Various scientific studies have explored the causes of violent behaviour from different perspectives, with psychological tests, in particular, applied to the analysis of crime factors. The relationship between bi-factors has also been extensively studied including the link between age and crime. In reality, many factors interact to contribute to criminal behaviour and as such there is a need to have a greater level of insight into its complex nature. In this article we analyse violent crime information systems containing data on psychological, environmental and genetic factors. Our approach combines elements of rough set theory with fuzzy logic and particle swarm optimisation to yield an algorithm and methodology that can effectively extract multi-knowledge from information systems. The experimental results show that our approach outperforms alternative genetic algorithm and dynamic reduct-based techniques for reduct identification and has the added advantage of identifying multiple reducts and hence multi-knowledge (rules). Identified rules are consistent with classical statistical analysis of violent crime data and also reveal new insights into the interaction between several factors. As such, the results are helpful in improving our understanding of the factors contributing to violent crime and in highlighting the existence of hidden and intangible relationships between crime factors.

  16. Heat conduction analysis of multi-layered FGMs considering the finite heat wave speed

    International Nuclear Information System (INIS)

    Rahideh, H.; Malekzadeh, P.; Golbahar Haghighi, M.R.

    2012-01-01

    Highlights: ► Using a layerwise-incremental differential quadrature for heat transfer of FGMs. ► Superior accuracy with fewer degrees of freedom of the method with respect to FEM. ► Considering multi-layered functionally graded materials. ► Hyperbolic heat transfer analysis of thermal system with heat generation. ► Showing the effect of heat wave speed on thermal characteristic of the system. - Abstract: In this work, the heat conduction with finite wave heat speed of multi-layered domain made of functionally graded materials (FGMs) subjected to heat generation is simulated. For this purpose, the domain is divided into a set of mathematical layers, the number of which can be equal or greater than those of the physical layers. Then, in each mathematical layer, the non-Fourier heat transfer equations are employed. Since, the governing equations have variable coefficients due to FGM properties, as an efficient and accurate method the differential quadrature method (DQM) is adopted to discretize both spatial and temporal domains in each layer. This results in superior accuracy with fewer degrees of freedom than conventional finite element method (FEM). To verify this advantages through some comparison studies, a finite element solution are also obtained. After demonstrating the convergence and accuracy of the method, the effects of heat wave speed for two different set of boundary conditions on the temperature distribution and heat flux of the domain are studied.

  17. Prediction and phylogenetic analysis of mammalian short interspersed elements (SINEs).

    Science.gov (United States)

    Rogozin, I B; Mayorov, V I; Lavrentieva, M V; Milanesi, L; Adkison, L R

    2000-09-01

    The presence of repetitive elements can create serious problems for sequence analysis, especially in the case of homology searches in nucleotide sequence databases. Repetitive elements should be treated carefully by using special programs and databases. In this paper, various aspects of SINE (short interspersed repetitive element) identification, analysis and evolution are discussed.

  18. Obtaining Approximate Values of Exterior Orientation Elements of Multi-Intersection Images Using Particle Swarm Optimization

    Science.gov (United States)

    Li, X.; Li, S. W.

    2012-07-01

    In this paper, an efficient global optimization algorithm in the field of artificial intelligence, named Particle Swarm Optimization (PSO), is introduced into close range photogrammetric data processing. PSO can be applied to obtain the approximate values of exterior orientation elements under the condition that multi-intersection photography and a small portable plane control frame are used. PSO, put forward by an American social psychologist J. Kennedy and an electrical engineer R.C. Eberhart, is a stochastic global optimization method based on swarm intelligence, which was inspired by social behavior of bird flocking or fish schooling. The strategy of obtaining the approximate values of exterior orientation elements using PSO is as follows: in terms of image coordinate observed values and space coordinates of few control points, the equations of calculating the image coordinate residual errors can be given. The sum of absolute value of each image coordinate is minimized to be the objective function. The difference between image coordinate observed value and the image coordinate computed through collinear condition equation is defined as the image coordinate residual error. Firstly a gross area of exterior orientation elements is given, and then the adjustment of other parameters is made to get the particles fly in the gross area. After iterative computation for certain times, the satisfied approximate values of exterior orientation elements are obtained. By doing so, the procedures like positioning and measuring space control points in close range photogrammetry can be avoided. Obviously, this method can improve the surveying efficiency greatly and at the same time can decrease the surveying cost. And during such a process, only one small portable control frame with a couple of control points is employed, and there are no strict requirements for the space distribution of control points. In order to verify the effectiveness of this algorithm, two experiments are

  19. OBTAINING APPROXIMATE VALUES OF EXTERIOR ORIENTATION ELEMENTS OF MULTI-INTERSECTION IMAGES USING PARTICLE SWARM OPTIMIZATION

    Directory of Open Access Journals (Sweden)

    X. Li

    2012-07-01

    Full Text Available In this paper, an efficient global optimization algorithm in the field of artificial intelligence, named Particle Swarm Optimization (PSO, is introduced into close range photogrammetric data processing. PSO can be applied to obtain the approximate values of exterior orientation elements under the condition that multi-intersection photography and a small portable plane control frame are used. PSO, put forward by an American social psychologist J. Kennedy and an electrical engineer R.C. Eberhart, is a stochastic global optimization method based on swarm intelligence, which was inspired by social behavior of bird flocking or fish schooling. The strategy of obtaining the approximate values of exterior orientation elements using PSO is as follows: in terms of image coordinate observed values and space coordinates of few control points, the equations of calculating the image coordinate residual errors can be given. The sum of absolute value of each image coordinate is minimized to be the objective function. The difference between image coordinate observed value and the image coordinate computed through collinear condition equation is defined as the image coordinate residual error. Firstly a gross area of exterior orientation elements is given, and then the adjustment of other parameters is made to get the particles fly in the gross area. After iterative computation for certain times, the satisfied approximate values of exterior orientation elements are obtained. By doing so, the procedures like positioning and measuring space control points in close range photogrammetry can be avoided. Obviously, this method can improve the surveying efficiency greatly and at the same time can decrease the surveying cost. And during such a process, only one small portable control frame with a couple of control points is employed, and there are no strict requirements for the space distribution of control points. In order to verify the effectiveness of this algorithm

  20. Toenail elemental analysis of Korean young adults by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Lee, O.

    2016-01-01

    The element contents in toenail clippings of healthy Korean young adults were measured using an instrumental neutron activation analysis. The average contents of elements such as Na, K, Cl, Ca, Fe, Se, and Zn are 449, 474, 1024, 1677, 66, 0.7 and 94 mg/kg in men, whereas those contents in women respectively 332, 476, 836, 1097, 66, 0.8 and 104 mg/kg. The correlation analysis of toenail elements with chronic disease risks showed positive associations between Na and serum HDL-cholesterol, blood pressure, and negative associations between Se and Hs-CRP, between Zn and hemoglobin level. (author)

  1. Finite element analysis of FRP-strengthened RC beams

    Directory of Open Access Journals (Sweden)

    Teeraphot Supaviriyakit

    2004-05-01

    Full Text Available This paper presents a non-linear finite element analysis of reinforced concrete beam strengthened with externally bonded FRP plates. The finite element modeling of FRP-strengthened beams is demonstrated. Concrete and reinforcing bars are modeled together as 8-node isoparametric 2D RC element. The FRP plate is modeled as 8-node isoparametric 2D elastic element. The glue is modeled as perfect compatibility by directly connecting the nodes of FRP with those of concrete since there is no failure at the glue layer. The key to the analysis is the correct material models of concrete, steel and FRP. Cracks and steel bars are modeled as smeared over the entire element. Stress-strain properties of cracked concrete consist of tensile stress model normal to crack, compressive stress model parallel to crack and shear stress model tangential to crack. Stressstrain property of reinforcement is assumed to be elastic-hardening to account for the bond between concrete and steel bars. FRP is modeled as elastic-brittle material. From the analysis, it is found that FEM can predict the load-displacement relation, ultimate load and failure mode of the beam correctly. It can also capture the cracking process for both shear-flexural peeling and end peeling modes similar to the experiment.

  2. Multi-Year Program under Budget Constraints Using Multi-Criteria Analysis

    Directory of Open Access Journals (Sweden)

    Surya Adiguna

    2017-09-01

    Full Text Available Road investment appraisal requires joint consideration of multiple criteria which are related to engineering, economic, social and environmental impacts. The investment consideration could be based on the economic analysis but however for some factors, such as environmental, social, and political, are difficult to quantify in monetary term. The multi-criteria analysis is the alternative tool which caters the requirements of the issues above. The research, which is based on 102 class D and class E paved road sections in Kenya, is about to optimize road network investment under budget constraints by applying a multi-criteria analysis (MCA method and compare it with the conventional economic analysis. The MCA is developed from hierarchy structure which is considered as the analytical framework. The framework is based on selected criteria and weights which are assigned from Kenya road policy. The HDM-4 software is applied as decision-making tool to obtain the best investment alternatives and road work programs from both MCA and economic analysis. The road work programs will be the results from the analysis using both MCA and economic analysis within HDM-4 software to see the difference and compare the results between both programs. The results from MCA show 51 road sections need periodic work, which is overlay or resealing. Meanwhile, 51 others need rehabilitation or reconstruction. The five years road work program which based on economic analysis result shows that it costs almost Kenyan Shilling (KES 130 billion to maintain the class D and E paved road in Kenya. Meanwhile, the MCA only requires KES 59.5 billion for 5 years program. These results show huge margin between two analyses and somehow MCA result provides more efficient work program compared to economic analysis.

  3. Multi-element analysis of wheat flour and white bread by neutron activation.; Analisis multielemental en harina de trigo y pan blanco por activacion neutronica.

    Energy Technology Data Exchange (ETDEWEB)

    Godinez A, M A

    1994-12-31

    One of the best source of feeding even for the human being as for animals are the Cereals. Although they are mainly energetic aliment, due to its composition in starch, they are a very important source of proteins and amino acids. They contribute mineral elements to the diet. Even those elements constitute a very small part of the total diet, they take a very important place in many human metabolic processes. To make a multielemental analysis of an aliment is very important that we are based on a very sensible analytic technique so we are able to find them, just as the Neutronic Activation. This Nuclear technique allows you to make a qualitative and quantitative analysis of the elements that are in a sample, but it does n`t show the way in which the elements are presented. It is based in turning those elements into radioactive ones through its exposition to an uniform and constant fluid of neutrons, so then its radioactivity can be determined. The present work has as a main purpose to make a multielemental analysis of the wheat flour and white bread through the Neutronic Activation Technique, using the comparator method and establishing previously the most appropriate work conditions as much irradiation as digestion and measuring of the radioactivity of the sample. In this way, it was able to know that the wheat flour has potassium, chlorine, magnesium, sodium, iron, zinc, manganese, rubidium and selenium elements in a concentration of 2000, 700, 500, 25, 18, 13, 5.5, 0.9 and 0.01 - 0.3 mg/g respectively. In an other hand it was found that the white bread has the same elements than the wheat flour but its concentration was: 1700, 9000, 400, 7000, 52, 13, 6, 1 and 0.05 - 0.3 mg/g respectively. (Author).

  4. A General Finite Element Scheme for Limit State Analysis and Optimization

    DEFF Research Database (Denmark)

    Damkilde, Lars

    1999-01-01

    Limit State analysis which is based on a perfect material behaviour is used in many different applications primarily within Structural Engineering and Geotechnics. The calculation methods have not reached the same level of automation such as Finite Element Analysis for elastic structures....... The computer based systems are more ad hoc based and are typically not well-integrated with pre- and postprocessors well-known from commercial Finite Element codes.A finite element based formulation of limit state analysis is presented which allows an easy integration with standard Finite Element codes...... for elastic analysis. In this way the user is able to perform a limit state analysis on the same model used for elastic analysis only adding data for the yield surface.The method is based on the lower-bound theorem and uses stress-based elements with a linearized yield surface. The mathematical problem...

  5. Multi-elemental characterization of Cuban natural zeolites

    International Nuclear Information System (INIS)

    Rizo, O.D.; Peraza, E.F.H.

    1997-01-01

    Concentration of 38 elements in samples from four important Cuban zeolite beds have been obtained by Instrumental Neutron Activation (INAA) and X-ray Fluorescence analyses (XRFA). In comparison with other analytical techniques good agreement was reached. The concentration values of minor element Ba, Sr, Zn and Mn and 25 trace element (including 9 REE) are at the first time reported in Cuban zeolite. It is important for the zeolite evaluation in different industrial uses. (author)

  6. Is Preventative Long-Segment Surgery for Multi-Level Spondylolysis Necessary? A Finite Element Analysis Study.

    Directory of Open Access Journals (Sweden)

    Jianqiang Mo

    Full Text Available For multi-level spondylolysis patients, surgeons commonly choose to fix all the segments with pars interarticularis defect even those without slippage and not responsible for clinical symptoms. In this study, we tried to study the necessity of the preventative long-segment surgery for the defected segment without slippage in treatment of multi-level spondylolysis patients from a biomechanical perspective.We established a bi-level spondylolysis model with pars defects at L4 and L5 segments, and simulated posterior lumbar interbody fusion (PLIF and pedicle screw fixation at L5-S1 level. Then we compared the biomechanical changes at L4 segment before and after surgery in neutral, flexion, extension, lateral bending and axial rotation position.The stress on L4 pars interarticularis was very similar before and after surgery, and reached the highest in axial rotation. The L3-L4 intradiscal pressure was almost the same, while L4-L5 intradiscal pressure changed a little in lateral bending (increase from 1.993 to 2.160 MPa and axial rotation (decrease from 1.639 to 1.307 MPa after surgery. The PLIF surgery caused a little increase of range of motion at adjacent L4-L5 and L3-L4 levels, but the change is very tiny (1 degree.The PLIF surgery will not cause significant biomechanical change at adjacent segment with pars defect in multi-level spondylolysis. On the contrary, excessive long-segment surgery will damage surrounding soft tissues which are important for maintaining the stability of spine. So a preventative long-segment surgery is not necessary for multi-level spondylolysis as long as there are no soft tissue degeneration signs at adjacent level.

  7. Is Preventative Long-Segment Surgery for Multi-Level Spondylolysis Necessary? A Finite Element Analysis Study.

    Science.gov (United States)

    Mo, Jianqiang; Zhang, Wen; Zhong, Dongyan; Xu, Hao; Wang, Lan; Yu, Jia; Luo, Zongping

    2016-01-01

    For multi-level spondylolysis patients, surgeons commonly choose to fix all the segments with pars interarticularis defect even those without slippage and not responsible for clinical symptoms. In this study, we tried to study the necessity of the preventative long-segment surgery for the defected segment without slippage in treatment of multi-level spondylolysis patients from a biomechanical perspective. We established a bi-level spondylolysis model with pars defects at L4 and L5 segments, and simulated posterior lumbar interbody fusion (PLIF) and pedicle screw fixation at L5-S1 level. Then we compared the biomechanical changes at L4 segment before and after surgery in neutral, flexion, extension, lateral bending and axial rotation position. The stress on L4 pars interarticularis was very similar before and after surgery, and reached the highest in axial rotation. The L3-L4 intradiscal pressure was almost the same, while L4-L5 intradiscal pressure changed a little in lateral bending (increase from 1.993 to 2.160 MPa) and axial rotation (decrease from 1.639 to 1.307 MPa) after surgery. The PLIF surgery caused a little increase of range of motion at adjacent L4-L5 and L3-L4 levels, but the change is very tiny (1 degree). The PLIF surgery will not cause significant biomechanical change at adjacent segment with pars defect in multi-level spondylolysis. On the contrary, excessive long-segment surgery will damage surrounding soft tissues which are important for maintaining the stability of spine. So a preventative long-segment surgery is not necessary for multi-level spondylolysis as long as there are no soft tissue degeneration signs at adjacent level.

  8. Elemental analysis: Reduction to SI units; Rueckfuehrung in der Elementanalytik

    Energy Technology Data Exchange (ETDEWEB)

    Rienitz, O.; Jaehrling, R.; Schiel, D. [PTB-Arbeitsgruppe ' ' Anorganische Analytik' ' , Braunschweig (Germany); Matschat, R.; Kipphardt, H. [Bundesanstalt fuer Materialforschung und -pruefung, Berlin (Germany); Gernand, W.; Oeter, D. [MercK KGaA (Germany)

    2005-12-15

    In a joint project, PTB, BAM and Merck KGaA worked on a metrological reduction system for all elements relevant to analysis. The BAM certified primary pure substances with a relative error of U{sub rel} {<=} 0.01% for the mass of the main element. This was achieved by measuring the mass components of all potential impurities, i.e. practically all elements of the periodic system except the main element. These pure substances are the national reference standards of elemental analysis. From them, PTB produces primary elementa solutions and transfer solutions which are passed on as reference standards. The industrial partner constructed the DKD calibration laboratory, which certifies commercial secondary calibration solutions on the basis of the reference standard solutions produced by PTB. With this final product, measurements in elemental analysis can be reduced to the SI units system as a routine procedure. (orig.)

  9. Analysis of a yearly multi-round, multi-period, multi-product transmission rights auction

    International Nuclear Information System (INIS)

    Ziogos, N.P.; Bakirtzis, A.G.

    2008-01-01

    A yearly multi-round, multi-period, multi-product transmission rights (TR) auction issuing both point-to-point Financial Transmission Rights (FTRs) and Flow-Gate Rights (FGRs) is studied in this paper. In each round the TR market participants (buyers or sellers) submit their bid or offer prices based on past energy market performance. A Locational Marginal Pricing (LMP) based energy market is assumed. The TR market participants' bid or offer prices reflect their expectation of the average annual LMP differences between withdrawal and injections points for FTRs and of the transmission link capacity prices for FGRs. The TR auction is performed in four rounds; in each round 25% of the entire system capability is awarded. TRs that are awarded in one round are modeled as fixed injections in subsequent rounds. Market participants that have acquired TRs in one round can sell them in subsequent rounds. A market participant can submit bids or offers for on-peak, off-peak or 24-h TRs. A three-area, nine-bus test system with six TR market participants is used for the analysis of the TR auction. (author)

  10. Multi-focus and multi-level techniques for visualization and analysis of networks with thematic data

    Science.gov (United States)

    Cossalter, Michele; Mengshoel, Ole J.; Selker, Ted

    2013-01-01

    Information-rich data sets bring several challenges in the areas of visualization and analysis, even when associated with node-link network visualizations. This paper presents an integration of multi-focus and multi-level techniques that enable interactive, multi-step comparisons in node-link networks. We describe NetEx, a visualization tool that enables users to simultaneously explore different parts of a network and its thematic data, such as time series or conditional probability tables. NetEx, implemented as a Cytoscape plug-in, has been applied to the analysis of electrical power networks, Bayesian networks, and the Enron e-mail repository. In this paper we briefly discuss visualization and analysis of the Enron social network, but focus on data from an electrical power network. Specifically, we demonstrate how NetEx supports the analytical task of electrical power system fault diagnosis. Results from a user study with 25 subjects suggest that NetEx enables more accurate isolation of complex faults compared to an especially designed software tool.

  11. Comparative Study on Interface Elements, Thin-Layer Elements, and Contact Analysis Methods in the Analysis of High Concrete-Faced Rockfill Dams

    Directory of Open Access Journals (Sweden)

    Xiao-xiang Qian

    2013-01-01

    Full Text Available This paper presents a study on the numerical performance of three contact simulation methods, namely, the interface element, thin-layer element, and contact analysis methods, through the analysis of the contact behavior between the concrete face slab and the dam body of a high concrete-faced rockfill dam named Tianshengqiao-I in China. To investigate the accuracy and limitations of each method, the simulation results are compared in terms of the dam deformation, contact stress along the interface, stresses in the concrete face slab, and separation of the concrete face slab from the cushion layer. In particular, the predicted dam deformation and slab separation are compared with the in-situ observation data to classify these methods according to their agreement with the in-situ observations. It is revealed that the interface element and thin-layer element methods have their limitations in predicting contact stress, slab separation, and stresses in the concrete face slab if a large slip occurs. The contact analysis method seems to be the best choice whether the separation is finite or not.

  12. Alphavirus replicon approach to promoterless analysis of IRES elements.

    Science.gov (United States)

    Kamrud, K I; Custer, M; Dudek, J M; Owens, G; Alterson, K D; Lee, J S; Groebner, J L; Smith, J F

    2007-04-10

    Here we describe a system for promoterless analysis of putative internal ribosome entry site (IRES) elements using an alphavirus (family Togaviridae) replicon vector. The system uses the alphavirus subgenomic promoter to produce transcripts that, when modified to contain a spacer region upstream of an IRES element, allow analysis of cap-independent translation of genes of interest (GOI). If the IRES element is removed, translation of the subgenomic transcript can be reduced >95% compared to the same transcript containing a functional IRES element. Alphavirus replicons, used in this manner, offer an alternative to standard dicistronic DNA vectors or in vitro translation systems currently used to analyze putative IRES elements. In addition, protein expression levels varied depending on the spacer element located upstream of each IRES. The ability to modulate the level of expression from alphavirus vectors should extend the utility of these vectors in vaccine development.

  13. How Good Is Multi-Pivot Quicksort?

    DEFF Research Database (Denmark)

    Aumüller, Martin; Dietzfelbinger, Martin; Klaue, Pascal

    2016-01-01

    of the partitioning cost is caused by rearranging elements. A rigorous analysis of an algorithm for rearranging elements in the partitioning step is carried out, observing mainly how often array cells are accessed during partitioning. The algorithm behaves best if three to five pivots are used. Experiments show...... that this translates into good cache behavior and is closest to predicting observed running times of multi-pivot quicksort algorithms. Finally, it is studied how choosing pivots from a sample affects sorting cost. The study is theoretical in the sense that although the findings motivate design recommendations...... as the standard sorting algorithm in Sun’s Java 7. In 2014 at ALENEX, Kushagra et al. introduced an even faster algorithm that uses three pivots. This article studies what possible advantages multi-pivot quicksort might offer in general. The contributions are as follows: Natural comparison-optimal algorithms...

  14. Correct use of Membrane Elements in Structural Analysis

    Directory of Open Access Journals (Sweden)

    Rothman Timothy

    2016-01-01

    Full Text Available Structural analysis of consumer electronic devices such as phones and tablets involves Finite Element Analysis (FEA. Dynamic loading conditions such as device dropping and bending dictate accurate FEA models to reduce design risk in many areas. The solid elements typically used in structural analysis do not have integration points on the surface. The outer surface is of most interest because that is where the cracks start. Analysts employ a post processing trick through using membranes to bring accurate stress/strain results to the surface. This paper explains numerical issues with implementation of membranes and recommends a methodology for accurate structural analysis.

  15. The 3"r"d inter laboratory comparison in the determination of elements in foodstuff with neutron activation analysis method

    International Nuclear Information System (INIS)

    Muji Wiyono; Dadong Iskandar; Wahyudi

    2010-01-01

    The 3"r"d inter laboratory comparison in the determination of elements in the foodstuff with NAA method held by PTBIN-BATAN Laboratory has been carried out. Six laboratories in BATAN were participated in the program with each code were: Lab. 01, Lab. 02, Lab. 03, Lab. 04, Lab. 05 and Lab. 06. Lab KKL PTKMR-BATAN was a participant with Lab. 06 code number. The received samples of foodstuff were prepared and irradiated in the RS-03 rabbit system of GA. Siwabessy multi purpose reactor. The irradiated samples were counted by using gamma spectrometer with HPGe detector to determine the content of elements. Result of the analysis was reported to the coordinator to be evaluated whether the sample was passed or rejected. Result of the coordinator laboratory evaluated that, 9 elements identified by Lab. KKL PTKMR-BATAN had four elements such as; Al, K, Cu and Se were passed (accepted) and other elements such as; Mn, Na, Ca, Fe and Zn were rejected. The elements number that passed in the 3"r"d inter laboratory comparison was less than those of earlier inter laboratory comparison, this was due to elemental content in the analyzed samples was very low. (author)

  16. Elemental analysis of cotton by laser-induced breakdown spectroscopy

    Energy Technology Data Exchange (ETDEWEB)

    Schenk, Emily R.; Almirall, Jose R.

    2010-05-01

    Laser-induced breakdown spectroscopy (LIBS) has been applied to the elemental characterization of unprocessed cotton. This research is important in forensic and fraud detection applications to establish an elemental fingerprint of U.S. cotton by region, which can be used to determine the source of the cotton. To the best of our knowledge, this is the first report of a LIBS method for the elemental analysis of cotton. The experimental setup consists of a Nd:YAG laser that operates at the fundamental wavelength as the LIBS excitation source and an echelle spectrometer equipped with an intensified CCD camera. The relative concentrations of elements Al, Ba, Ca, Cr, Cu, Fe, Mg, and Sr from both nutrients and environmental contributions were determined by LIBS. Principal component analysis was used to visualize the differences between cotton samples based on the elemental composition by region in the U.S. Linear discriminant analysis of the LIBS data resulted in the correct classification of >97% of the cotton samples by U.S. region and >81% correct classification by state of origin.

  17. Fully automated dissolution and separation methods for inductively coupled plasma atomic emission spectrometry rock analysis. Application to the determination of rare earth elements

    International Nuclear Information System (INIS)

    Govindaraju, K.; Mevelle, G.

    1987-01-01

    In rock analysis laboratories, sample preparation is a serious problem, or even an enormous bottleneck. Because this laboratory is production-oriented, this problem was attacked by automating progressively, different steps in rock analysis for major, minor and trace elements. This effort has been considerably eased by the fact that all sample preparation schemes in this laboratory for the past three decades have been based on an initial lithium borate fusion of rock samples and all analytical methods based on multi-element atomic emission spectrometry, with switch-over from solid analysis by arc/spark excitation to solution analysis by plasma excitation in 1974. The sample preparation steps which have been automated are: weighing of samples and fluxes, lithium borate fusion, dissolution and dilution of fusion products and ion-exchange separation of difficult trace elements such as rare earth elements (REE). During 1985 and 1986, these different unit operations have been assembled together as peripheral units in the form of a workstation, called LabRobStation. A travelling robot is the master of LabRobStation, with all peripheral units at its reach in 10 m 2 workspace. As an example of real application, the automated determination of REE, based on more than 8000 samples analysed during 1982 and 1986, is presented. (author)

  18. Elemental analysis of bottom ash from municipal incinerator by neutron activation analysis

    International Nuclear Information System (INIS)

    Kim, S. H.; Jang, S. H.; Moon, J. H.; Jung, Y. S.; Kim, Y. J.

    2003-01-01

    Elemental analysis of bottom ash generated from municipal solid waste incinerator was performed by neutron activation analysis. For this study, ash samples monthly collected from incinerator in D city were sieved with 5 mm mesh size, dried, pulverized by agate mortar and finally re-sieved with 200μ mesh size. Prepared samples were irradiated by neutrons using NAA No.1 irradiation hole in Korea Atomic Energy Research Institute. Activated samples were measured by gamma-ray spectrometer according to the relevant nuclear properties of target nuclides and the concentration of 33 elements were determined from the collected ash samples. Quality control was conducted by comparative analysis with two NIST standard reference materials simultaneously. Mean values and standard deviations of hazardous elements such as As, Cr, Cu, Fe, Mn, Sb and Zn among the determined elements were 3.8±6.9mg/kg, 620±0.12 %, 4.76±0.37 %, 0.26±0.10 %, 115±29 mg/kg and 0.71±0.19 %, respectively

  19. The quantitative determination of trace elements in giant unicellular plants by particle-induced X-ray emission

    International Nuclear Information System (INIS)

    Navarrete-Dominguez, V.R.; Yoshihara, K.; Tanaka, N.

    1982-01-01

    Particle-induced X-ray emission (PIXE) was applied for the determination of trace elements in biologically interesting materials, giant unicellular plants. It was found that the PIXE method had advantages in multi-element trace analysis of a single cell of the sample plant. (author)

  20. An adaptive multi-element probabilistic collocation method for statistical EMC/EMI characterization

    KAUST Repository

    Yücel, Abdulkadir C.

    2013-12-01

    An adaptive multi-element probabilistic collocation (ME-PC) method for quantifying uncertainties in electromagnetic compatibility and interference phenomena involving electrically large, multi-scale, and complex platforms is presented. The method permits the efficient and accurate statistical characterization of observables (i.e., quantities of interest such as coupled voltages) that potentially vary rapidly and/or are discontinuous in the random variables (i.e., parameters that characterize uncertainty in a system\\'s geometry, configuration, or excitation). The method achieves its efficiency and accuracy by recursively and adaptively dividing the domain of the random variables into subdomains using as a guide the decay rate of relative error in a polynomial chaos expansion of the observables. While constructing local polynomial expansions on each subdomain, a fast integral-equation-based deterministic field-cable-circuit simulator is used to compute the observable values at the collocation/integration points determined by the adaptive ME-PC scheme. The adaptive ME-PC scheme requires far fewer (computationally costly) deterministic simulations than traditional polynomial chaos collocation and Monte Carlo methods for computing averages, standard deviations, and probability density functions of rapidly varying observables. The efficiency and accuracy of the method are demonstrated via its applications to the statistical characterization of voltages in shielded/unshielded microwave amplifiers and magnetic fields induced on car tire pressure sensors. © 2013 IEEE.

  1. Development of an accurate, sensitive, and robust isotope dilution laser ablation ICP-MS method for simultaneous multi-element analysis (chlorine, sulfur, and heavy metals) in coal samples

    International Nuclear Information System (INIS)

    Boulyga, Sergei F.; Heilmann, Jens; Heumann, Klaus G.; Prohaska, Thomas

    2007-01-01

    A method for the direct multi-element determination of Cl, S, Hg, Pb, Cd, U, Br, Cr, Cu, Fe, and Zn in powdered coal samples has been developed by applying inductively coupled plasma isotope dilution mass spectrometry (ICP-IDMS) with laser-assisted introduction into the plasma. A sector-field ICP-MS with a mass resolution of 4,000 and a high-ablation rate laser ablation system provided significantly better sensitivity, detection limits, and accuracy compared to a conventional laser ablation system coupled with a quadrupole ICP-MS. The sensitivity ranges from about 590 cps for 35 Cl + to more than 6 x 10 5 cps for 238 U + for 1 μg of trace element per gram of coal sample. Detection limits vary from 450 ng g -1 for chlorine and 18 ng g -1 for sulfur to 9.5 pg g -1 for mercury and 0.3 pg g -1 for uranium. Analyses of minor and trace elements in four certified reference materials (BCR-180 Gas Coal, BCR-331 Steam Coal, SRM 1632c Trace Elements in Coal, SRM 1635 Trace Elements in Coal) yielded good agreement of usually not more than 5% deviation from the certified values and precisions of less than 10% relative standard deviation for most elements. Higher relative standard deviations were found for particular elements such as Hg and Cd caused by inhomogeneities due to associations of these elements within micro-inclusions in coal which was demonstrated for Hg in SRM 1635, SRM 1632c, and another standard reference material (SRM 2682b, Sulfur and Mercury in Coal). The developed LA-ICP-IDMS method with its simple sample pretreatment opens the possibility for accurate, fast, and highly sensitive determinations of environmentally critical contaminants in coal as well as of trace impurities in similar sample materials like graphite powder and activated charcoal on a routine basis. (orig.)

  2. Development of an accurate, sensitive, and robust isotope dilution laser ablation ICP-MS method for simultaneous multi-element analysis (chlorine, sulfur, and heavy metals) in coal samples.

    Science.gov (United States)

    Boulyga, Sergei F; Heilmann, Jens; Prohaska, Thomas; Heumann, Klaus G

    2007-10-01

    A method for the direct multi-element determination of Cl, S, Hg, Pb, Cd, U, Br, Cr, Cu, Fe, and Zn in powdered coal samples has been developed by applying inductively coupled plasma isotope dilution mass spectrometry (ICP-IDMS) with laser-assisted introduction into the plasma. A sector-field ICP-MS with a mass resolution of 4,000 and a high-ablation rate laser ablation system provided significantly better sensitivity, detection limits, and accuracy compared to a conventional laser ablation system coupled with a quadrupole ICP-MS. The sensitivity ranges from about 590 cps for (35)Cl+ to more than 6 x 10(5) cps for (238)U+ for 1 microg of trace element per gram of coal sample. Detection limits vary from 450 ng g(-1) for chlorine and 18 ng g(-1) for sulfur to 9.5 pg g(-1) for mercury and 0.3 pg g(-1) for uranium. Analyses of minor and trace elements in four certified reference materials (BCR-180 Gas Coal, BCR-331 Steam Coal, SRM 1632c Trace Elements in Coal, SRM 1635 Trace Elements in Coal) yielded good agreement of usually not more than 5% deviation from the certified values and precisions of less than 10% relative standard deviation for most elements. Higher relative standard deviations were found for particular elements such as Hg and Cd caused by inhomogeneities due to associations of these elements within micro-inclusions in coal which was demonstrated for Hg in SRM 1635, SRM 1632c, and another standard reference material (SRM 2682b, Sulfur and Mercury in Coal). The developed LA-ICP-IDMS method with its simple sample pretreatment opens the possibility for accurate, fast, and highly sensitive determinations of environmentally critical contaminants in coal as well as of trace impurities in similar sample materials like graphite powder and activated charcoal on a routine basis.

  3. Chemical analysis of useful trace elements in sea water

    International Nuclear Information System (INIS)

    Katoh, Shunsaku; Fujii, Ayako; Miyai, Yoshitaka; Sakane, Kohji; Ogata, Noboru.

    1983-01-01

    The methods for the analysis of useful trace elements in sea water which have been tried so far are reviewed, and these methods are described briefly from the standpoint of studying the collection of resources. Ag and Au can be determined by concentrating sea water by ion-exchange method, solvent extraction method and electrodeposition method, then the elements are measured quantitatively by activation analysis and atomic absorption spectrochemical analysis. Sr, B and Li, which exist in relatively high concentration in sea water, are determined easily by atomic absorption spectrochemical analysis and absorption spectrometry. U, Mo and V are measured suitably by concentrating the elements by coprecipitation or solvent extraction method, and measuring by fluorescence analysis and arsenazo-3 method for U and through graphite-atomic absorption analysis for Mo and V. It has been revealed that the concentration of Ag and Au in sea water is extremely low, accordingly the recovery study is not conducted recently. On the other hand, the adsorption method using hydrated titanium oxide and amidoxim adsorbents for U, Mo and V, the adsorption method using aluminum adsorbent for Li, and the adsorption method using magnesium oxide and zirconium hydroxide and the solvent extraction method for B are hopeful to recover these elements. (Yoshitake, I.)

  4. Nonlinear Finite Element Analysis of Shells with Large Aspect Ratio

    Science.gov (United States)

    Chang, T. Y.; Sawamiphakdi, K.

    1984-01-01

    A higher order degenerated shell element with nine nodes was selected for large deformation and post-buckling analysis of thick or thin shells. Elastic-plastic material properties are also included. The post-buckling analysis algorithm is given. Using a square plate, it was demonstrated that the none-node element does not have shear locking effect even if its aspect ratio was increased to the order 10 to the 8th power. Two sample problems are given to illustrate the analysis capability of the shell element.

  5. An approach to multi-attribute utility analysis under parametric uncertainty

    International Nuclear Information System (INIS)

    Kelly, M.; Thorne, M.C.

    2001-01-01

    The techniques of cost-benefit analysis and multi-attribute analysis provide a useful basis for informing decisions in situations where a number of potentially conflicting opinions or interests need to be considered, and where there are a number of possible decisions that could be adopted. When the input data to such decision-making processes are uniquely specified, cost-benefit analysis and multi-attribute utility analysis provide unambiguous guidance on the preferred decision option. However, when the data are not uniquely specified, application and interpretation of these techniques is more complex. Herein, an approach to multi-attribute utility analysis (and hence, as a special case, cost-benefit analysis) when input data are subject to parametric uncertainty is presented. The approach is based on the use of a Monte Carlo technique, and has recently been applied to options for the remediation of former uranium mining liabilities in a number of Central and Eastern European States

  6. Finite element analysis of structures through unified formulation

    CERN Document Server

    Carrera, Erasmo; Petrolo, Marco; Zappino, Enrico

    2014-01-01

    The finite element method (FEM) is a computational tool widely used to design and analyse  complex structures. Currently, there are a number of different approaches to analysis using the FEM that vary according to the type of structure being analysed: beams and plates may use 1D or 2D approaches, shells and solids 2D or 3D approaches, and methods that work for one structure are typically not optimized to work for another. Finite Element Analysis of Structures Through Unified Formulation deals with the FEM used for the analysis of the mechanics of structures in the case of linear elasticity. The novelty of this book is that the finite elements (FEs) are formulated on the basis of a class of theories of structures known as the Carrera Unified Formulation (CUF). It formulates 1D, 2D and 3D FEs on the basis of the same ''fundamental nucleus'' that comes from geometrical relations and Hooke''s law, and presents both 1D and 2D refined FEs that only have displacement variables as in 3D elements. It also covers 1D...

  7. PIXE - a new method for elemental analysis

    International Nuclear Information System (INIS)

    Johansson, S.A.E.

    1983-01-01

    With elemental analysis we mean the determination of which chemical elements are present in a sample and of their concentration. This is an old and important problem in chemistry. The earliest methods were purely chemical and many such methods are still used. However, various methods based on physical principles have gradually become more and more important. One such method is neutron activation. When the sample is bombarded with neutrons it becomes radioactive and the various radioactive isotopes produced can be identified by the radiation they emit. From the measured intensity of the radiation one can calculate how much of a certain element that is present in the sample. Another possibility is to study the light emitted when the sample is excited in various ways. A spectroscopic investigation of the light can identify the chemical elements and allows also a determination of their concentration in the sample. In the same way, if a sample can be brought to emit X-rays, this radiation is also characteristic for the elements present and can be used to determine the elemental concentration. One such X-ray method which has been developed recently is PIXE. The name is an acronym for Particle Induced X-ray Emission and indicates the principle of the method. Particles in this context means heavy, charged particles such as protons and a-particles of rather high energy. Hence, in PIXE-analysis the sample is irradiated in the beam of an accelerator and the emitted X-rays are studied. (author)

  8. Multi-element determination of soil solution by INAA

    International Nuclear Information System (INIS)

    Qian Qinfang; Wu Shuiqing; Tian Jibing

    1992-01-01

    One of the factors influencing crop growth is the effective elemental contents, especially trace elements, under the circumstances of the same concentrations of N, P and K in soil. In order to obtain the data of effective elemental contents in soil, a novel method was introduced. In this method, soil solution was extracted by a squeezer. The concentrations of elements in soil solution were determined by INAA. Study on the compositions and the contents of elements in soil solution will provide information on making a suitable soil environment for plant growth and on rational and economical manuring

  9. A refined element-based Lagrangian shell element for geometrically nonlinear analysis of shell structures

    Directory of Open Access Journals (Sweden)

    Woo-Young Jung

    2015-04-01

    Full Text Available For the solution of geometrically nonlinear analysis of plates and shells, the formulation of a nonlinear nine-node refined first-order shear deformable element-based Lagrangian shell element is presented. Natural co-ordinate-based higher order transverse shear strains are used in present shell element. Using the assumed natural strain method with proper interpolation functions, the present shell element generates neither membrane nor shear locking behavior even when full integration is used in the formulation. Furthermore, a refined first-order shear deformation theory for thin and thick shells, which results in parabolic through-thickness distribution of the transverse shear strains from the formulation based on the third-order shear deformation theory, is proposed. This formulation eliminates the need for shear correction factors in the first-order theory. To avoid difficulties resulting from large increments of the rotations, a scheme of attached reference system is used for the expression of rotations of shell normal. Numerical examples demonstrate that the present element behaves reasonably satisfactorily either for the linear or for geometrically nonlinear analysis of thin and thick plates and shells with large displacement but small strain. Especially, the nonlinear results of slit annular plates with various loads provided the benchmark to test the accuracy of related numerical solutions.

  10. Evaluation of thermal conductivity of multi-component and multi-phase nuclear fuels by the finite element method

    International Nuclear Information System (INIS)

    Kurosaki, K.

    2015-01-01

    The effects of the shape and distribution state of voids on the thermal conductivity of UO 2 , and the temperature distribution and heat flow within the irradiated MOX fuel were evaluated by finite element analysis. Although the work is still in progress, some preliminary results are presented. (author)

  11. Containment penetration design and analysis by finite element methods

    International Nuclear Information System (INIS)

    Perry, R.F.; Rigamonti, G.; Dainora, J.

    1975-01-01

    Containment penetration designs which provide complete support to process piping containing high pressure and high temperature fluids and which do not employ cooling coils, require special provisions to sustain loadings associated with normal/abnormal conditions and to limit maximum temperature transmitted to the containment concrete wall. In order to accomodate piping loads and fluid temperatures within code and regulatory limitations, the containment penetration designs require careful analysis of two critical regions: 1) the portion of the penetration sleeve which is exposed to containment ambient conditions and 2) the portion of the penetration which connects the sleeve to process piping (flued head). Analytical models using finite element representation of process piping, penetration flued head, and exposed sleeve were employed to investigate the penetration assembly design. By application of flexible multi-step analyses, different penetration configurations were evaluated to determine the effects of key design parameters. Among the parameters studied were flued head angles with the process piping, sleeve length and wall thickness. Special designs employing fins welded to the sleeve to further lower the temperature at the concrete wall interface were also investigated and fin geometry effects reported. (Auth.)

  12. Dual-Section DFB-QCLs for Multi-Species Trace Gas Analysis

    Directory of Open Access Journals (Sweden)

    Martin J. Süess

    2016-04-01

    Full Text Available We report on the dynamic behavior of dual-wavelength distributed feedback (DFB quantum cascade lasers (QCLs in continuous wave and intermittent continuous wave operation. We investigate inherent etaloning effects based on spectrally resolved light-current-voltage (LIV characterization and perform time-resolved spectral analysis of thermal chirping during long (>5 µs current pulses. The theoretical aspects of the observed behavior are discussed using a combination of finite element method simulations and transfer matrix method calculations of dual-section DFB structures. Based on these results, we demonstrate how the internal etaloning can be minimized using anti-reflective (AR coatings. Finally, the potential and benefits of these devices for high precision trace gas analysis are demonstrated using a laser absorption spectroscopic setup. Thereby, the atmospherically highly relevant compounds CO2 (including its major isotopologues, CO and N2O are simultaneously determined with a precision of 0.16 ppm, 0.22 ppb and 0.26 ppb, respectively, using a 1-s integration time and an optical path-length of 36 m. This creates exciting new opportunities in the development of compact, multi-species trace gas analyzers.

  13. Analysis of trace elements in serum from human eating irradiated food

    International Nuclear Information System (INIS)

    Huang Zongzhi; Zhou Hongdi; Chen Shijie; Gao Sumei

    1987-01-01

    A method of trace element analysis by Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AEC) in serum from human eating food preserved by irradiation is described. Trace element analysis in human serum is one of the research projects concerning the wholesomeness. 78 serum samples of the human eating food preserved by irradiation were collected. After ashing and solving ICP-AES analysis of serum is performed for detecting 12 trace elements in specimen solution. The detection limitations are in the range of 10 -2 - 10 -3 ppm for differemt elements. The recoveries of elements are over 73%. Concentrations of 12 trace elements in 78 human serum has been calculated with F and t tests at PDP 11/70 computer and it was concluded that there is no significant difference between testing group and control group

  14. A computer program for structural analysis of fuel elements

    International Nuclear Information System (INIS)

    Hayashi, I.M.V.; Perrotta, J.A.

    1988-01-01

    It's presented the code ELCOM for the matrix analysis of tubular structures coupled by rigid spacers, typical of PWR's fuel elements. The code ELCOM makes a static structural analysis, where the displacements and internal forces are obtained for each structure at the joints with the spacers, and also, the natural frequencies and vibrational modes of an equivalent integrated structure are obtained. The ELCOM result is compared to a PWR fuel element structural analysis obtained in published paper. (author) [pt

  15. Development of a procedure for the multi-element determination of trace elements in wine by ICP-MS

    Energy Technology Data Exchange (ETDEWEB)

    Castineira, M.M.; Brandt, R.; von Bohlen, A.; Jakubowski, N. [Institut fuer Spektrochemie und Angewandte Spektroskopie e.V., Dortmund (Germany)

    2001-07-01

    An inductively coupled plasma mass spectrometric (ICP-MS) procedure has been developed for the determination of trace elements in wine. The procedure consists in simple 1+1 dilution of the wine and semi-quantitative analysis (without external calibration) using In as internal standard. Thirty-one elements at concentrations ranging from 0.1 mg mL{sup -1} to 0.5 ng mL{sup -1} can be determined by ICP-MS analysis with and without digestion. It was investigated whether a matrix effect observed for EtOH in the wine matrix can be overcome by application of a micro-concentric nebulizer with a membrane desolvator (MCN 6000). The results obtained for the MCN 6000 are compared with those obtained by use of a conventional Meinhard nebulizer. It is shown that the observed matrix effect can only be compensated by use of an internal standard for the Meinhard nebulizer, but not for the MCN 6000. Results for ICP-MS are compared with those obtained by total reflection X-ray fluorescence spectrometry (TXRF). (orig.)

  16. Multi-scale Analysis of MEMS Sensors Subject to Drop Impacts

    Directory of Open Access Journals (Sweden)

    Sarah Zerbini

    2007-09-01

    Full Text Available The effect of accidental drops on MEMS sensors are examined within the frame-work of a multi-scale finite element approach. With specific reference to a polysilicon MEMSaccelerometer supported by a naked die, the analysis is decoupled into macro-scale (at dielength-scale and meso-scale (at MEMS length-scale simulations, accounting for the verysmall inertial contribution of the sensor to the overall dynamics of the device. Macro-scaleanalyses are adopted to get insights into the link between shock waves caused by the impactagainst a target surface and propagating inside the die, and the displacement/acceleration his-tories at the MEMS anchor points. Meso-scale analyses are adopted to detect the most stresseddetails of the sensor and to assess whether the impact can lead to possible localized failures.Numerical results show that the acceleration at sensor anchors cannot be considered an ob-jective indicator for drop severity. Instead, accurate analyses at sensor level are necessary toestablish how MEMS can fail because of drops.

  17. Numerical analysis for multi-group neutron-diffusion equation using Radial Point Interpolation Method (RPIM)

    International Nuclear Information System (INIS)

    Kim, Kyung-O; Jeong, Hae Sun; Jo, Daeseong

    2017-01-01

    Highlights: • Employing the Radial Point Interpolation Method (RPIM) in numerical analysis of multi-group neutron-diffusion equation. • Establishing mathematical formation of modified multi-group neutron-diffusion equation by RPIM. • Performing the numerical analysis for 2D critical problem. - Abstract: A mesh-free method is introduced to overcome the drawbacks (e.g., mesh generation and connectivity definition between the meshes) of mesh-based (nodal) methods such as the finite-element method and finite-difference method. In particular, the Point Interpolation Method (PIM) using a radial basis function is employed in the numerical analysis for the multi-group neutron-diffusion equation. The benchmark calculations are performed for the 2D homogeneous and heterogeneous problems, and the Multiquadrics (MQ) and Gaussian (EXP) functions are employed to analyze the effect of the radial basis function on the numerical solution. Additionally, the effect of the dimensionless shape parameter in those functions on the calculation accuracy is evaluated. According to the results, the radial PIM (RPIM) can provide a highly accurate solution for the multiplication eigenvalue and the neutron flux distribution, and the numerical solution with the MQ radial basis function exhibits the stable accuracy with respect to the reference solutions compared with the other solution. The dimensionless shape parameter directly affects the calculation accuracy and computing time. Values between 1.87 and 3.0 for the benchmark problems considered in this study lead to the most accurate solution. The difference between the analytical and numerical results for the neutron flux is significantly increased in the edge of the problem geometry, even though the maximum difference is lower than 4%. This phenomenon seems to arise from the derivative boundary condition at (x,0) and (0,y) positions, and it may be necessary to introduce additional strategy (e.g., the method using fictitious points and

  18. Multi scale analysis of ITER pre-compression rings

    Energy Technology Data Exchange (ETDEWEB)

    Park, Ben, E-mail: ben.park@sener.es [SENER Ingeniería y Sistemas S.A., Barcelona (Spain); Foussat, Arnaud [ITER Organization, St. Paul-Lez-Durance (France); Rajainmaki, Hannu [Fusion for Energy, Barcelona (Spain); Knaster, Juan [IFMIF, Aomori (Japan)

    2013-10-15

    Highlights: • A multi-scale analysis approach employing various scales of ABAQUS FEM models have been used to calculate the response and performance of the rings. • We have studied the effects of various defects on the performance of the rings under the operating temperatures and loading that will be applied to the PCRs. • The multi scale analysis results are presented here. -- Abstract: The Pre-compression Rings of ITER (PCRs) represent one of the largest and most highly stressed composite structures ever designed for long term operation at 4 K. Six rings, each 5 m in diameter and 337 mm × 288 mm in cross-section, will be manufactured from S2 fiber-glass/epoxy composite and installed three at the top and three at the bottom of the eighteen D shaped toroidal field (TF) coils to apply a total centripetal pre-load of 70 MN per TF coil. The composite rings will be fabricated with a high content (65% by volume) of S2 fiber-glass in an epoxy resin matrix. During the manufacture emphasis will be placed on obtaining a structure with a very low void content and minimal presence of critical defects, such as delaminations. This paper presents a unified framework for the multi-scale analysis of the composite structure of the PCRs. A multi-scale analysis approach employing various scales of ABAQUS FEM models and other analysis tools have been used to calculate the response and performance of the rings over the design life of the structure. We have studied the effects of various defects on the performance of the rings under the operating temperatures and loading that will be applied to the PCRs. The results are presented here.

  19. Integral finite element analysis of turntable bearing with flexible rings

    Science.gov (United States)

    Deng, Biao; Liu, Yunfei; Guo, Yuan; Tang, Shengjin; Su, Wenbin; Lei, Zhufeng; Wang, Pengcheng

    2018-03-01

    This paper suggests a method to calculate the internal load distribution and contact stress of the thrust angular contact ball turntable bearing by FEA. The influence of the stiffness of the bearing structure and the plastic deformation of contact area on the internal load distribution and contact stress of the bearing is considered. In this method, the load-deformation relationship of the rolling elements is determined by the finite element contact analysis of a single rolling element and the raceway. Based on this, the nonlinear contact between the rolling elements and the inner and outer ring raceways is same as a nonlinear compression spring and bearing integral finite element analysis model including support structure was established. The effects of structural deformation and plastic deformation on the built-in stress distribution of slewing bearing are investigated on basis of comparing the consequences of load distribution, inner and outer ring stress, contact stress and other finite element analysis results with the traditional bearing theory, which has guiding function for improving the design of slewing bearing.

  20. Landslide risk analysis: a multi-disciplinary methodological approach

    Directory of Open Access Journals (Sweden)

    S. Sterlacchini

    2007-11-01

    Full Text Available This study describes an analysis carried out within the European community project "ALARM" (Assessment of Landslide Risk and Mitigation in Mountain Areas, 2004 on landslide risk assessment in the municipality of Corvara in Badia, Italy. This mountainous area, located in the central Dolomites (Italian Alps, poses a significant landslide hazard to several man-made and natural objects. Three parameters for determining risk were analysed as an aid to preparedness and mitigation planning: event occurrence probability, elements at risk, and the vulnerability of these elements. Initially, a landslide hazard scenario was defined; this step was followed by the identification of the potential vulnerable elements, by the estimation of the expected physical effects, due to the occurrence of a damaging phenomenon, and by the analysis of social and economic features of the area. Finally, a potential risk scenario was defined, where the relationships between the event, its physical effects, and its economic consequences were investigated. People and public administrators with training and experience in local landsliding and slope processes were involved in each step of the analysis.

    A "cause-effect" correlation was applied, derived from the "dose-response" equation initially used in the biological sciences and then adapted by economists for the assessment of environmental risks. The relationship was analysed from a physical point of view and the cause (the natural event was correlated to the physical effects, i.e. the aesthetic, functional, and structural damage. An economic evaluation of direct and indirect damage was carried out considering the assets in the affected area (i.e., tourist flows, goods, transport and the effect on other social and economic activities. This study shows the importance of indirect damage, which is as significant as direct damage. The total amount of direct damage was estimated in 8 913 000 €; on the contrary, indirect

  1. Landslide risk analysis: a multi-disciplinary methodological approach

    Science.gov (United States)

    Sterlacchini, S.; Frigerio, S.; Giacomelli, P.; Brambilla, M.

    2007-11-01

    This study describes an analysis carried out within the European community project "ALARM" (Assessment of Landslide Risk and Mitigation in Mountain Areas, 2004) on landslide risk assessment in the municipality of Corvara in Badia, Italy. This mountainous area, located in the central Dolomites (Italian Alps), poses a significant landslide hazard to several man-made and natural objects. Three parameters for determining risk were analysed as an aid to preparedness and mitigation planning: event occurrence probability, elements at risk, and the vulnerability of these elements. Initially, a landslide hazard scenario was defined; this step was followed by the identification of the potential vulnerable elements, by the estimation of the expected physical effects, due to the occurrence of a damaging phenomenon, and by the analysis of social and economic features of the area. Finally, a potential risk scenario was defined, where the relationships between the event, its physical effects, and its economic consequences were investigated. People and public administrators with training and experience in local landsliding and slope processes were involved in each step of the analysis. A "cause-effect" correlation was applied, derived from the "dose-response" equation initially used in the biological sciences and then adapted by economists for the assessment of environmental risks. The relationship was analysed from a physical point of view and the cause (the natural event) was correlated to the physical effects, i.e. the aesthetic, functional, and structural damage. An economic evaluation of direct and indirect damage was carried out considering the assets in the affected area (i.e., tourist flows, goods, transport and the effect on other social and economic activities). This study shows the importance of indirect damage, which is as significant as direct damage. The total amount of direct damage was estimated in 8 913 000 €; on the contrary, indirect damage ranged considerably

  2. Analysis of Brick Masonry Wall using Applied Element Method

    Science.gov (United States)

    Lincy Christy, D.; Madhavan Pillai, T. M.; Nagarajan, Praveen

    2018-03-01

    The Applied Element Method (AEM) is a versatile tool for structural analysis. Analysis is done by discretising the structure as in the case of Finite Element Method (FEM). In AEM, elements are connected by a set of normal and shear springs instead of nodes. AEM is extensively used for the analysis of brittle materials. Brick masonry wall can be effectively analyzed in the frame of AEM. The composite nature of masonry wall can be easily modelled using springs. The brick springs and mortar springs are assumed to be connected in series. The brick masonry wall is analyzed and failure load is determined for different loading cases. The results were used to find the best aspect ratio of brick to strengthen brick masonry wall.

  3. Elements of abstract harmonic analysis

    CERN Document Server

    Bachman, George

    2013-01-01

    Elements of Abstract Harmonic Analysis provides an introduction to the fundamental concepts and basic theorems of abstract harmonic analysis. In order to give a reasonably complete and self-contained introduction to the subject, most of the proofs have been presented in great detail thereby making the development understandable to a very wide audience. Exercises have been supplied at the end of each chapter. Some of these are meant to extend the theory slightly while others should serve to test the reader's understanding of the material presented. The first chapter and part of the second give

  4. Multi-element determinations of N,N-dimethylformamide (DMF) coal slurries using ICP-OES

    Energy Technology Data Exchange (ETDEWEB)

    M. Mujuru; R.I. McCrindle; B.M. Botha; P.P. Ndibewu [Tshwane University of Technology, Pretoria (South Africa). Department of Chemistry

    2009-04-15

    A slurry nebulisation technique was applied for elemental analysis of bituminous coals SARM 18, SARM 19 and four coals from three different seams in Witbank, South Africa, by inductively coupled plasma optical emission spectroscopy (ICP-OES). Major elements (Al, Ca, Fe, Mg, S, Si and Ti) and trace elements (Ba, Cr, Mn, Ni, Sr, V, Zn and Zr) in coal were determined. Various slurry preparations were evaluated using two dispersants (glycerol and Triton X-100) and by varying the concentration of dispersants, between 0.1% and 1.0% (v/v). The effect of initially solubilising the ground coal in N,N-dimethylformamide (DMF) was investigated by varying the volume of DMF added. The effect of wet grinding with DMF was investigated. Wet grinding with DMF was shown to drastically reduce particle sizes (50.0% < 0.28 m and 90.0% < 6.17 {mu}m) as compared to dry grinding (50.0% < 5.25 {mu}m and 90.0% < 11.1 {mu}m). The reduced particle sizes and increased transport efficiency of the coal slurries led to improved analytical recoveries of elements in the reference coal, SARM 18. The best analytical recoveries for all elements were achieved using 0.1% Triton X-100 with 10.0% DMF. Results obtained by ICP-OES after wet grinding of the coal with DMF, using 0.1% Triton X-100, also gave excellent recoveries (Al, 100%; Ca, 103%; Cr, 106%; Fe, 102%; Mg, 100%; Mn, 104%; Ni, 109%; Si, 102%; Ti, 95.0%; and V, 108%). The results obtained with 10.0% DMF and 0.1% Triton X-100 were in agreement with certified values for all selected elements according to paired t-test at the 95.0% confidence level. Selected elements (Al, Ca, Fe, Mg, Mn, Si, Ti and V) were also analysed with X-ray fluorescence for comparison with results obtained from ICP-OES. Analysis by ICP-OES of microwave digested coal was also carried out. It is suggested that the DMF slurry technique could be used for routine analysis of bituminous coals. 27 refs., 4 figs., 4 tabs.

  5. Complex finite element sensitivity method for creep analysis

    International Nuclear Information System (INIS)

    Gomez-Farias, Armando; Montoya, Arturo; Millwater, Harry

    2015-01-01

    The complex finite element method (ZFEM) has been extended to perform sensitivity analysis for mechanical and structural systems undergoing creep deformation. ZFEM uses a complex finite element formulation to provide shape, material, and loading derivatives of the system response, providing an insight into the essential factors which control the behavior of the system as a function of time. A complex variable-based quadrilateral user element (UEL) subroutine implementing the power law creep constitutive formulation was incorporated within the Abaqus commercial finite element software. The results of the complex finite element computations were verified by comparing them to the reference solution for the steady-state creep problem of a thick-walled cylinder in the power law creep range. A practical application of the ZFEM implementation to creep deformation analysis is the calculation of the skeletal point of a notched bar test from a single ZFEM run. In contrast, the standard finite element procedure requires multiple runs. The value of the skeletal point is that it identifies the location where the stress state is accurate, regardless of the certainty of the creep material properties. - Highlights: • A novel finite element sensitivity method (ZFEM) for creep was introduced. • ZFEM has the capability to calculate accurate partial derivatives. • ZFEM can be used for identification of the skeletal point of creep structures. • ZFEM can be easily implemented in a commercial software, e.g. Abaqus. • ZFEM results were shown to be in excellent agreement with analytical solutions

  6. A proposal for a determination method of element division on an analytical model for finite element elastic waves propagation analysis

    International Nuclear Information System (INIS)

    Ishida, Hitoshi; Meshii, Toshiyuki

    2010-01-01

    This study proposes an element size selection method named the 'Impact-Meshing (IM) method' for a finite element waves propagation analysis model, which is characterized by (1) determination of element division of the model with strain energy in the whole model, (2) static analysis (dynamic analysis in a single time step) with boundary conditions which gives a maximum change of displacement in the time increment and inertial (impact) force caused by the displacement change. In this paper, an example of application of the IM method to 3D ultrasonic wave propagation problem in an elastic solid is described. These examples showed an analysis result with a model determined by the IM method was convergence and calculation time for determination of element subdivision was reduced to about 1/6 by the IM Method which did not need determination of element subdivision by a dynamic transient analysis with 100 time steps. (author)

  7. Multi-flexible-body analysis for application to wind turbine control design

    Science.gov (United States)

    Lee, Donghoon

    The objective of the present research is to build a theoretical and computational framework for the aeroelastic analysis of flexible rotating systems, more specifically with special application to a wind turbine control design. The methodology is based on the integration of Kane's approach for the analysis of the multi-rigid-body subsystem and a mixed finite element method for the analysis of the flexible-body subsystem. The combined analysis is then strongly coupled with an aerodynamic model based on Blade Element Momentum theory for inflow model. The unified framework from the analysis of subsystems is represented as, in a symbolic manner, a set of nonlinear ordinary differential equations with time-variant, periodic coefficients, which describe the aeroelastic behavior of whole system. The framework can be directly applied to control design due to its symbolic characteristics. The solution procedures for the equations are presented for the study of nonlinear simulation, periodic steady-state solution, and Floquet stability of the linearized system about the steady-state solution. Finally the linear periodic system equation can be obtained with both system and control matrices as explicit functions of time, which can be directly applicable to control design. The structural model is validated by comparison of its results with those from software, some of which is commercial. The stability of the linearized system about periodic steady-state solution is different from that obtained about a constant steady-state solution, which have been conventional in the field of wind turbine dynamics. Parametric studies are performed on a wind turbine model with various pitch angles, precone angles, and rotor speeds. Combined with composite material, their effects on wind turbine aeroelastic stability are investigated. Finally it is suggested that the aeroelastic stability analysis and control design for the whole system is crucial for the design of wind turbines, and the

  8. Evaluasi Ketidakpastian Pengukuran Multi-Unsur Dalam Mineral Zirkon Dengan Metode Analisis Aktivasi Neutron

    Directory of Open Access Journals (Sweden)

    Sukirno

    2015-05-01

    Full Text Available The evaluation of multi-elements analysis has been carried out with calculation of element uncertainy in the zircon mineral from Sampit (Central Kalimantan dan Bangka has been evaluated by the Neutron Activation Analysis (NAA method. The purpose of this research is determination of composition and value of multi-elements uncertainty in the mineral of zircon to fulfil the requirements of ISO/IEC guide 17025-2008 that applied at NAA laboratory. The result of analysis using gamma spectrometry with a HPGe detector showed of 21 detected elements, divided into three groups (major, minor, and trace. Evaluation of uncertainty estimation should be done to increase quality and confidence rate of analysis results. The result of testing are not mean without calculation of uncertainty. Therefore, it was assessed the uncertainty measurement of all elements analysis in zircon mineral. The results of quantitative analysis is Zr with the highest concentration value of 38.986% and value of uncertainty is 0.331% so that value of real concentration is 38.986 ± 0.331%. In the form of oxide (ZrO2 has concentration of 52.661±0.45%. Sb element is the lowest element detected with value of concentration and uncertainty is 7±0,3 µg/g. In the form of oxide (Sb2O3 has concentration is 17±0.9 µg/g. The oxide composition and the must important of chemicals in the zircon sand mineral more significant from Sampit which quantitative composition areZrO2+HfO2 (53-55%, F2O3 (5-6%, TiO2 (13-14%, Al2O3 (1.5-2% and SiO2. Elements ofSi(SiO2 can not be determined by NAA method because Si cross-sections is verysmall.

  9. High accuracy 3D electromagnetic finite element analysis

    International Nuclear Information System (INIS)

    Nelson, Eric M.

    1997-01-01

    A high accuracy 3D electromagnetic finite element field solver employing quadratic hexahedral elements and quadratic mixed-order one-form basis functions will be described. The solver is based on an object-oriented C++ class library. Test cases demonstrate that frequency errors less than 10 ppm can be achieved using modest workstations, and that the solutions have no contamination from spurious modes. The role of differential geometry and geometrical physics in finite element analysis will also be discussed

  10. High accuracy 3D electromagnetic finite element analysis

    International Nuclear Information System (INIS)

    Nelson, E.M.

    1996-01-01

    A high accuracy 3D electromagnetic finite element field solver employing quadratic hexahedral elements and quadratic mixed-order one-form basis functions will be described. The solver is based on an object-oriented C++ class library. Test cases demonstrate that frequency errors less than 10 ppm can be achieved using modest workstations, and that the solutions have no contamination from spurious modes. The role of differential geometry and geometrical physics in finite element analysis will also be discussed

  11. The Review of Visual Analysis Methods of Multi-modal Spatio-temporal Big Data

    Directory of Open Access Journals (Sweden)

    ZHU Qing

    2017-10-01

    Full Text Available The visual analysis of spatio-temporal big data is not only the state-of-art research direction of both big data analysis and data visualization, but also the core module of pan-spatial information system. This paper reviews existing visual analysis methods at three levels:descriptive visual analysis, explanatory visual analysis and exploratory visual analysis, focusing on spatio-temporal big data's characteristics of multi-source, multi-granularity, multi-modal and complex association.The technical difficulties and development tendencies of multi-modal feature selection, innovative human-computer interaction analysis and exploratory visual reasoning in the visual analysis of spatio-temporal big data were discussed. Research shows that the study of descriptive visual analysis for data visualizationis is relatively mature.The explanatory visual analysis has become the focus of the big data analysis, which is mainly based on interactive data mining in a visual environment to diagnose implicit reason of problem. And the exploratory visual analysis method needs a major break-through.

  12. Simultaneous multi-element atomic absorption system using photodiode array detector

    International Nuclear Information System (INIS)

    Tong, S.L.; Chin, K.S.

    1994-01-01

    A photodiode array (PDA) detector-multichannel analyser (MCA) system has been coupled to a flame and a graphite furnace atomiser and tested for simultaneous multielement atomic absorption analysis. Multielement hollow cathode lamps (HCL) are used as light source. Spectral lines are dispersed through a spectrograph with triple gratings and detected by a 25.4 mm PDA detector consisting of 1024 elements. The optical MCA system is capable of recording multiple spectra spanned by the spectrograph/PDA. The transmitted intensity spectra obtained for the standard and analyte solutions during flame or graphite furnace atomisation are converted to absorbance spectra using the MCA software provided. Results from the comparison studies show that the linear range and sensitivities for Ni-Co-Fe and Cu-Cr obtained from the simultaneous measurements are within the same order of magnitudes as those from conventional single element determinations using photomultiplier tube detection. The study also shows that non-atomic absorption can be readily corrected by a two-line method where non-atomic absorption lines can be chosen from the spectra recorded simultaneously. The proposed system has been evaluated for the determination of trace elements using NBS standard reference water SRM 1643b

  13. Game meat authentication through rare earth elements fingerprinting.

    Science.gov (United States)

    Danezis, G P; Pappas, A C; Zoidis, E; Papadomichelakis, G; Hadjigeorgiou, I; Zhang, P; Brusic, V; Georgiou, C A

    2017-10-23

    Accurate labelling of meat (e.g. wild versus farmed, geographical and genetic origin, organic versus conventional, processing treatment) is important to inform the consumers about the products they buy. Meat and meat products declared as game have higher commercial value making them target to fraudulent labelling practices and replacement with non-game meat. We have developed and validated a new method for authentication of wild rabbit meat using elemental metabolomics approach. Elemental analysis was performed using rapid ultra-trace multi-element measurement by inductively coupled plasma mass spectrometry (ICP-MS). Elemental signatures showed excellent ability to discriminate the wild rabbit from non-wild rabbit meat. Our results demonstrate the usefulness of metabolic markers -rare earth signatures, as well as other trace element signatures for game meat authentication. Copyright © 2017 Elsevier B.V. All rights reserved.

  14. Neutron activation analysis of trace elements in IAEA reference materials

    International Nuclear Information System (INIS)

    Cheema, M.N.; Hasany, S.M.; Hanif, I.; Chaudhry, M.S.; Qureshi, I.H.

    1978-09-01

    Analytical Chemistry Group of Nuclear Chemistry Division at PINSTECH has been participating in IAEA Intercomparison programme of analytical quality control since 1972. So far fifteen samples of a variety of materials received from the Agency have been analyzed for different minor and trace elements. Mostly destructive and non-destructive neutron activation analysis techniques have been used for elemental analysis. In this report the description of the samples and the experimental procedures employed have been mentioned. The results of elemental analysis have been reported and compared with IAEA values which are based on the average computed from the results of different participating laboratories. (authors)

  15. Application of trace element analysis to determine trace element concentrations in the field of medicine

    International Nuclear Information System (INIS)

    Kasperek, K.; Feinendegen, L.E.

    1976-01-01

    Applied trace elements research in medicine requires a sensitive and efficient technique of trace elements analysis such as, e.g., neutron activation analysis. Essential trace elements act as stabilisators (iron in haem), structural elements (silicium in fibrous tissue), in hormones (iodine in thyroid hormone), in vitamins (cobalt in vitamin B 12), and in enzymes. Most of the essential trace elements act as coenzymes or in coenzymes or directly as metabolic catalysators. For example, selenium deficiency in PKU and maple syrup patients receiving dietary treatment can be detected by determining the selenium content of the serum, while low selenium values in the whole blood indicate liver cirrhosis. Acrodermatitis enteropathica can be diagnosed by determinig zinc in the serum, and pancreatic insufficiency by determining zinc in the pancreatic juice. Zinc also plays a part in disturbances of growth, in the healing of wounds, and in the insulin metabolism. Cobalt is important in some types of anaemia and in myocardiopathies. Trace elements are also necessary in the treatment of diseases, e.g. iron cobalt in some types of anaemia, and zinc in the delayed healing of wounds in the postoperative phase and in acrodermatitis enteropathica. Chromium is now being tested for the treatment of diabetes mellitus, and fluorides may be of interest in the treatment of osteoporosis. Finally, trace elements are important in the aetiology of acute poisoning, in nutrition, and in environmental protection. (orig./AK) [de

  16. Dynamic relaxation method in analysis of reinforced concrete bent elements

    Directory of Open Access Journals (Sweden)

    Anna Szcześniak

    2015-12-01

    Full Text Available The paper presents a method for the analysis of nonlinear behaviour of reinforced concrete bent elements subjected to short-term static load. The considerations in the range of modelling of deformation processes of reinforced concrete element were carried out. The method of structure effort analysis was developed using the finite difference method. The Dynamic Relaxation Method, which — after introduction of critical damping — allows for description of the static behaviour of a structural element, was used to solve the system of nonlinear equilibrium equations. In order to increase the method effectiveness in the range of the post-critical analysis, the Arc Length Parameter on the equilibrium path was introduced into the computational procedure.[b]Keywords[/b]: reinforced concrete elements, physical nonlinearity, geometrical nonlinearity, dynamic relaxation method, arc-length method

  17. Multi-Core Processor Memory Contention Benchmark Analysis Case Study

    Science.gov (United States)

    Simon, Tyler; McGalliard, James

    2009-01-01

    Multi-core processors dominate current mainframe, server, and high performance computing (HPC) systems. This paper provides synthetic kernel and natural benchmark results from an HPC system at the NASA Goddard Space Flight Center that illustrate the performance impacts of multi-core (dual- and quad-core) vs. single core processor systems. Analysis of processor design, application source code, and synthetic and natural test results all indicate that multi-core processors can suffer from significant memory subsystem contention compared to similar single-core processors.

  18. Isogeometric finite element analysis of poroelasticity

    NARCIS (Netherlands)

    Irzal, F.; Remmers, J.J.C.; Verhoosel, C.V.; Borst, de R.

    2013-01-01

    We present an alternative numerical approach for predicting the behaviour of a deformable fluid-saturated porous medium. The conventional finite element technology is replaced by isogeometric analysis that uses non-uniform rational B-splines. The ability of these functions to provide higher-order

  19. Multi-Dimensional Customer Data Analysis in Online Auctions

    Institute of Scientific and Technical Information of China (English)

    LAO Guoling; XIONG Kuan; QIN Zheng

    2007-01-01

    In this paper, we designed a customer-centered data warehouse system with five subjects: listing, bidding, transaction,accounts, and customer contact based on the business process of online auction companies. For each subject, we analyzed its fact indexes and dimensions. Then take transaction subject as example,analyzed the data warehouse model in detail, and got the multi-dimensional analysis structure of transaction subject. At last, using data mining to do customer segmentation, we divided customers into four types: impulse customer, prudent customer, potential customer, and ordinary customer. By the result of multi-dimensional customer data analysis, online auction companies can do more target marketing and increase customer loyalty.

  20. Welding Residual Stress Analysis and Fatigue Strength Assessment at Elevated Temperature for Multi-pass Dissimilar Material Weld Between Alloy 617 and P92 Steel

    Science.gov (United States)

    Lee, Juhwa; Hwang, Jeongho; Bae, Dongho

    2018-03-01

    In this paper, welding residual stress analysis and fatigue strength assessment were performed at elevated temperature for multi-pass dissimilar material weld between Alloy 617 and P92 steel, which are used in thermal power plant. Multi-pass welding between Alloy 617 and P92 steel was performed under optimized welding condition determined from repeated pre-test welding. In particular, for improving dissimilar material weld-ability, the buttering welding technique was applied on the P92 steel side before multi-pass welding. Welding residual stress distribution at the dissimilar material weld joint was numerically analyzed by using the finite element method, and compared with experimental results which were obtained by the hole-drilling method. Additionally, fatigue strength of dissimilar material weld joint was assessed at the room temperature (R.T), 300, 500, and 700 °C. In finite element analysis results, numerical peak values; longitudinal (410 MPa), transverse (345 MPa) were higher than those of experiments; longitudinal (298 MPa), transverse (245 MPa). There are quantitatively big differences between numerical and experimental results, due to some assumption about the thermal conductivity, specific heat, effects of enforced convection of the molten pool, dilution, and volume change during phase transformation caused by actual shield gas. The low fatigue limit at R.T, 300 °C, 500 °C and 700 °C was assessed to be 368, 276, 173 and 137 MPa respectively.

  1. Welding Residual Stress Analysis and Fatigue Strength Assessment at Elevated Temperature for Multi-pass Dissimilar Material Weld Between Alloy 617 and P92 Steel

    Science.gov (United States)

    Lee, Juhwa; Hwang, Jeongho; Bae, Dongho

    2018-07-01

    In this paper, welding residual stress analysis and fatigue strength assessment were performed at elevated temperature for multi-pass dissimilar material weld between Alloy 617 and P92 steel, which are used in thermal power plant. Multi-pass welding between Alloy 617 and P92 steel was performed under optimized welding condition determined from repeated pre-test welding. In particular, for improving dissimilar material weld-ability, the buttering welding technique was applied on the P92 steel side before multi-pass welding. Welding residual stress distribution at the dissimilar material weld joint was numerically analyzed by using the finite element method, and compared with experimental results which were obtained by the hole-drilling method. Additionally, fatigue strength of dissimilar material weld joint was assessed at the room temperature (R.T), 300, 500, and 700 °C. In finite element analysis results, numerical peak values; longitudinal (410 MPa), transverse (345 MPa) were higher than those of experiments; longitudinal (298 MPa), transverse (245 MPa). There are quantitatively big differences between numerical and experimental results, due to some assumption about the thermal conductivity, specific heat, effects of enforced convection of the molten pool, dilution, and volume change during phase transformation caused by actual shield gas. The low fatigue limit at R.T, 300 °C, 500 °C and 700 °C was assessed to be 368, 276, 173 and 137 MPa respectively.

  2. Biomonitoring of air pollution through trace element analysis

    International Nuclear Information System (INIS)

    Bamford, S.A.; Osae, E.K.; Aboh, I.J.; Serfor-Armah, Y.; Nyarko, B.; Odamtten, G.T.

    1999-01-01

    Studies are being carried out to determine the potential and reliability in the use of local lichen species for biomonitoring air pollution in Ghana. The location of most of the gold mines in forest areas of the country presents the gold mining industry as a suitable setting for such investigations. The nuclear-related techniques being used in the multielement analysis of lichen samples and air filter samples are instrumental neutron activation analysis (Miniature Neutron Source Reactor) and energy dispersive x-ray fluorescence analysis (tube-excitation). Validation of the quantitative methods of the INAA through analysis of standard and certified reference materials of orchard leaves NBS SRM 1571 and BCR-CRM No. 279 gave very good results for most elements analyzed. Elemental analysis of identified lichen samples will be done beating in mind microclimatic factors, specie type and nature of soil. (author)

  3. Biomonitoring of air pollution through trace element analysis

    International Nuclear Information System (INIS)

    Bamford, S.A.; Osae, E.K.; Aboh, I. J.; Serfor-Armah, Y.; Nyarko, B.; Ofosu, F.; Odamtten, G.T.

    1999-04-01

    Studies are being carried out to determine the potential and reliability in the use of local lichen species for biomonitoring air pollution in Ghana. The location of most of the gold mines in forest areas of the country presents the gold mining industry as a suitable setting for such investigations. The nuclear-related techniques being used in the multielement analysis of lichen samples and air filter samples are instrumental neutron activation analysis (Miniature Neutron Source Reactor) and energy dispersive x-ray fluorescence analysis (tube-excitation). Validation of the quantitative methods of the INAA through analysis of standard certified reference materials of orchard leaves NBS SRM 1571 and BCR-CRM No. 279 gave very good results for most elements analyzed. Elemental analysis of identified lichen samples will be done bearing in mind microclimatic factors, specie type and nature of soil. (author)

  4. Elemental analysis of granite by instrumental neutron activation analysis (INAA) and X-ray fluorescence analysis (XRF)

    International Nuclear Information System (INIS)

    El-Taher, A.

    2012-01-01

    The instrumental neutron activation analysis technique (INAA) was used for qualitative and quantitative analysis of granite samples collected from four locations in the Aswan area in South Egypt. The samples were prepared together with their standards and simultaneously irradiated in a neutron flux of 7×10 11 n/cm 2 s in the TRIGA Mainz research reactor. Gamma-ray spectra from an hyper-pure germanium detector were analyzed. The present study provides the basic data of elemental concentrations of granite rocks. The following elements have been determined Na, Mg, K, Fe, Mn, Sc, Cr, Ti, Co, Zn, Ga, Rb, Zr, Nb, Sn, Ba, Cs, La, Ce, Nd, Sm, Eu, Yb, Lu, Hf, Ta, Th and U. The X-ray fluorescence (XRF) was used for comparison and to detect elements, which can be detected only by XRF such as F, S, Cl, Co, Cu, Mo, Ni, Pb, Se and V. The data presented here are our contribution to understanding the elemental composition of the granite rocks. Because there are no existing databases for the elemental analysis of granite, our results are a start to establishing a database for the Egyptian granite. It is hoped that the data presented here will be useful to those dealing with geochemistry, granite chemistry and related fields. - Highlights: ► Instrumental neutron activation analysis technique (INAA) was used for qualitative and quantitative analysis of granite. ► The samples were prepared together with their standards and simultaneously irradiated in a neutron flux of 7×10 11 n/cm 2 s in the TRIGA Mainz research reactor. ► Following elements have been determined Na, Mg, K, Fe, Mn, Sc, Cr, Ti, Co, Zn, Ga, Rb, Zr, Nb, Sn, Ba, Cs, La, Ce, Nd, Sm, Eu, Yb, Lu, Hf, Ta, Th and U.

  5. Optimization and Openmp Parallelization of a Discrete Element Code for Convex Polyhedra on Multi-Core Machines

    Science.gov (United States)

    Chen, Jian; Matuttis, Hans-Georg

    2013-02-01

    We report our experiences with the optimization and parallelization of a discrete element code for convex polyhedra on multi-core machines and introduce a novel variant of the sort-and-sweep neighborhood algorithm. While in theory the whole code in itself parallelizes ideally, in practice the results on different architectures with different compilers and performance measurement tools depend very much on the particle number and optimization of the code. After difficulties with the interpretation of the data for speedup and efficiency are overcome, respectable parallelization speedups could be obtained.

  6. Finite element analysis of plastic recycling machine designed for ...

    African Journals Online (AJOL)

    ... design was evaluated using finite element analysis (FEA) tool in Solid Works Computer ... Also, a minimum factor of safety value of 5.3 was obtained for shredder shaft ... Machine; Design; Recycling; Sustainability; Finite Element; Simulation ...

  7. Analysis of multi-bunch instabilities at the Diamond storage ring

    CERN Document Server

    Bartolini, Riccardo; Rehm, Guenther; Smaluk, Victor

    2017-01-01

    We present the result of the analytical, numerical and experimental analysis of multi-bunch instabilities at the Diamond storage ring. This work compares the impedance estimates with CST with the analysis of the growth rates of the excited multi-bunch modes in different machine configurations. The contribution of a number of wakefield sources has been identified with very high precision thanks to high quality data provided by the existing TMBF diagnostics.

  8. Multivariant analyses of trace element patterns for environmental tracking

    International Nuclear Information System (INIS)

    Jervis, R.E.; Ko, M.M.C.; Junliang Tian; Puling Liu

    1993-01-01

    Nuclear-based analytical techniques: INAA, PIXE and photon activation permit simultaneous multielemental determination of concentrations in environmental materials, which data are often found sufficiently precise and free of uncontrolled, random errors among the various elements such that the data sets can yield valuable information on elemental communality through multi-variant statistical 'factor' analysis. Characteristic factor patterns obtained in this way can provide clues to the likely sources in the environment of various components. Recent studies in three different environmental situations: solid waste incinerators , Chinese soils, and iron and steel industry, involving measurements of 30-35 elements, have yielded distinct elemental patterns or, environmental signatures, with factor loading coefficients ranging mostly in the ranges: 0.7-0.96. (author) 10 refs.; 2 figs.; 9 tabs

  9. A Study on the Effect of Cohesive Laws on Finite Element Analysis of Crack Propagation Using Cohesive Elements

    Energy Technology Data Exchange (ETDEWEB)

    Seo, Hyeongseok; Baek, Hyungchan; Kim, Hyungyu [Seoul Nat' l Univ. of Sci. and Tech., Seoul (Korea, Republic of)

    2014-04-15

    In this paper, the effect of cohesive laws on the finite element analysis of crack propagation using cohesive elements is investigated through three-point bending and double cantilever beam problems. The cohesive elements are implemented into ABAQUS/Standard user subroutines(UEL), and the shape of cohesive law is varied by changing parameters in polynomial functions of cohesive traction-separation relations. In particular, crack propagation behaviors are studied by comparing load-displacement curves of the analysis models which have different shapes of cohesive laws with the same values of fracture energy and cohesive strength. Furthermore, the influence of the element size on crack propagation is discussed in this study.

  10. High accuracy 3D electromagnetic finite element analysis

    International Nuclear Information System (INIS)

    Nelson, E.M.

    1997-01-01

    A high accuracy 3D electromagnetic finite element field solver employing quadratic hexahedral elements and quadratic mixed-order one-form basis functions will be described. The solver is based on an object-oriented C++ class library. Test cases demonstrate that frequency errors less than 10 ppm can be achieved using modest workstations, and that the solutions have no contamination from spurious modes. The role of differential geometry and geometrical physics in finite element analysis will also be discussed. copyright 1997 American Institute of Physics

  11. A site-specific and multi-element isotopic approach to origin inference of sugars in foods and beverages

    International Nuclear Information System (INIS)

    Martin, M.L.; Martin, G.J.; Guillou, C.

    1991-01-01

    A strategy is presented for the characterization of sugars according to their botanical origin. The samples fermented in standardized conditions can be described in the multi-dimensional space of the overall carbon isotope ratio of ethanol measured by isotope ratio mass spectrometry (IRMS) and of the specific hydrogen isotope parameters of the methyl and methylene sites derived from nuclear magnetic resonance investigation of site-specific natural isotope fractionation (SNIF-NMR method). In the comparison of natural juices, the deuterium and oxygen-18 parameters of water extracted from the juice and from the end fermentation medium also contain information on the origin of the product. The isotopic effects of the concentration processes leading to concentrated juices, musts and syrups can be estimated and taken into account in interpreting the data. The classification power of this multi-element and multi-site approach is illustrated by discriminant analyses involving selected isotopic variables associated with pineapple, apple and barley sugars, compared to beet and cane sugars which are common sources of enrichment. The ability of the method to detect adulteration by exogenous sugars is improved when environmental conditions can be taken into account. (authors)

  12. Progress and challenges in the development and qualification of multi-level multi-physics coupled methodologies for reactor analysis

    International Nuclear Information System (INIS)

    Ivanov, K.; Avramova, M.

    2007-01-01

    Current trends in nuclear power generation and regulation as well as the design of next generation reactor concepts along with the continuing computer technology progress stimulate the development, qualification and application of multi-physics multi-scale coupled code systems. The efforts have been focused on extending the analysis capabilities by coupling models, which simulate different phenomena or system components, as well as on refining the scale and level of detail of the coupling. This paper reviews the progress made in this area and outlines the remaining challenges. The discussion is illustrated with examples based on neutronics/thermohydraulics coupling in the reactor core modeling. In both fields recent advances and developments are towards more physics-based high-fidelity simulations, which require implementation of improved and flexible coupling methodologies. First, the progresses in coupling of different physics codes along with the advances in multi-level techniques for coupled code simulations are discussed. Second, the issues related to the consistent qualification of coupled multi-physics and multi-scale code systems for design and safety evaluation are presented. The increased importance of uncertainty and sensitivity analysis are discussed along with approaches to propagate the uncertainty quantification between the codes. The incoming OECD LWR Uncertainty Analysis in Modeling (UAM) benchmark is the first international activity to address this issue and it is described in the paper. Finally, the remaining challenges with multi-physics coupling are outlined. (authors)

  13. Progress and challenges in the development and qualification of multi-level multi-physics coupled methodologies for reactor analysis

    Energy Technology Data Exchange (ETDEWEB)

    Ivanov, K.; Avramova, M. [Pennsylvania State Univ., University Park, PA (United States)

    2007-07-01

    Current trends in nuclear power generation and regulation as well as the design of next generation reactor concepts along with the continuing computer technology progress stimulate the development, qualification and application of multi-physics multi-scale coupled code systems. The efforts have been focused on extending the analysis capabilities by coupling models, which simulate different phenomena or system components, as well as on refining the scale and level of detail of the coupling. This paper reviews the progress made in this area and outlines the remaining challenges. The discussion is illustrated with examples based on neutronics/thermohydraulics coupling in the reactor core modeling. In both fields recent advances and developments are towards more physics-based high-fidelity simulations, which require implementation of improved and flexible coupling methodologies. First, the progresses in coupling of different physics codes along with the advances in multi-level techniques for coupled code simulations are discussed. Second, the issues related to the consistent qualification of coupled multi-physics and multi-scale code systems for design and safety evaluation are presented. The increased importance of uncertainty and sensitivity analysis are discussed along with approaches to propagate the uncertainty quantification between the codes. The incoming OECD LWR Uncertainty Analysis in Modeling (UAM) benchmark is the first international activity to address this issue and it is described in the paper. Finally, the remaining challenges with multi-physics coupling are outlined. (authors)

  14. Development of an accurate, sensitive, and robust isotope dilution laser ablation ICP-MS method for simultaneous multi-element analysis (chlorine, sulfur, and heavy metals) in coal samples

    Energy Technology Data Exchange (ETDEWEB)

    Boulyga, Sergei F. [University of Natural Resources and Applied Life Sciences, Department of Chemistry, Division of Analytical Chemistry-VIRIS Laboratory, Vienna (Austria); Johannes Gutenberg-University, Institute of Inorganic Chemistry and Analytical Chemistry, Mainz (Germany); Heilmann, Jens; Heumann, Klaus G. [Johannes Gutenberg-University, Institute of Inorganic Chemistry and Analytical Chemistry, Mainz (Germany); Prohaska, Thomas [University of Natural Resources and Applied Life Sciences, Department of Chemistry, Division of Analytical Chemistry-VIRIS Laboratory, Vienna (Austria)

    2007-10-15

    A method for the direct multi-element determination of Cl, S, Hg, Pb, Cd, U, Br, Cr, Cu, Fe, and Zn in powdered coal samples has been developed by applying inductively coupled plasma isotope dilution mass spectrometry (ICP-IDMS) with laser-assisted introduction into the plasma. A sector-field ICP-MS with a mass resolution of 4,000 and a high-ablation rate laser ablation system provided significantly better sensitivity, detection limits, and accuracy compared to a conventional laser ablation system coupled with a quadrupole ICP-MS. The sensitivity ranges from about 590 cps for {sup 35}Cl{sup +} to more than 6 x 10{sup 5} cps for {sup 238}U{sup +} for 1 {mu}g of trace element per gram of coal sample. Detection limits vary from 450 ng g{sup -1} for chlorine and 18 ng g{sup -1} for sulfur to 9.5 pg g{sup -1} for mercury and 0.3 pg g{sup -1} for uranium. Analyses of minor and trace elements in four certified reference materials (BCR-180 Gas Coal, BCR-331 Steam Coal, SRM 1632c Trace Elements in Coal, SRM 1635 Trace Elements in Coal) yielded good agreement of usually not more than 5% deviation from the certified values and precisions of less than 10% relative standard deviation for most elements. Higher relative standard deviations were found for particular elements such as Hg and Cd caused by inhomogeneities due to associations of these elements within micro-inclusions in coal which was demonstrated for Hg in SRM 1635, SRM 1632c, and another standard reference material (SRM 2682b, Sulfur and Mercury in Coal). The developed LA-ICP-IDMS method with its simple sample pretreatment opens the possibility for accurate, fast, and highly sensitive determinations of environmentally critical contaminants in coal as well as of trace impurities in similar sample materials like graphite powder and activated charcoal on a routine basis. (orig.)

  15. Application of trace element analysis to determine trace element concentrations in the field of medicine. [Neutrons

    Energy Technology Data Exchange (ETDEWEB)

    Kasperek, K; Feinendegen, L E

    1976-01-01

    Applied trace elements research in medicine requires a sensitive and efficient technique of trace elements analysis, such as neutron activation analysis. Essential trace elements act as stabilizators (iron in haem), structural elements (silicon in fibrous tissue), in hormones (iodine in thyroid hormone), in vitamins (cobalt in vitamin B 12), and in enzymes. Most of the essential trace elements act as coenzymes or in coenzymes or directly as metabolic catalyzers. For example, selenium deficiency in PKU and maple syrup patients receiving dietary treatment can be detected by determining the selenium content of the serum, while low selenium values in the whole blood indicate liver cirrhosis. Acrodermatitis enteropathica can be diagnosed by determinig zinc in the serum, and pancreatic insufficiency by determining zinc in the pancreatic juice. Zinc also plays a part in disturbances of growth, in the healing of wounds, and in the insulin metabolism. Cobalt is important in some types of anaemia and in myocardiopathies. Trace elements are also necessary in the treatment of diseases, e.g. iron cobalt in some types of anaemia, and zinc in the delayed healing of wounds in the postoperative phase and in acrodermatitis enteropathica. Chromium is now being tested for the treatment of diabetes mellitus, and fluorides may be of interest in the treatment of osteoporosis. Finally, trace elements are important in the aetiology of acute poisoning, in nutrition, and in environmental protection.

  16. Application of activation analysis for determination of some elements in cassiterite samples

    International Nuclear Information System (INIS)

    Armelin, Maria Jose Aguirre

    1978-01-01

    This work consists in the development of an analytical method using activation by thermal neutrons for the determination of some minor elements and traces present in cassiterite (tin ore). This method was then applied to determine these elements in samples of cassiterite from different regions of Brazil. An analysis was made of the mineralogy characteristic of cassiterite as well as of the minerals most commonly associated with it. Four main types of interference were found to occur in the analysis by activation of trace elements in samples of cassiterite. The method involves the analysis without chemical separation for the determination of some elements and the analysis with chemical separation for the determination of other elements. The steps involved in both types of analysis are described. In the analysis with chemical separation the matrix element (tin) is separated by distillation in an H 2 SO 4 -HBr medium, after fusion of the ore with Na 2 O 2 . Arsine and antimony are determined in the distilled, whereas some lanthanide elements and uranium are determined in the distillation residue by separating them as a group by precipitation with lanthanum fluoride. A discussion on the precision, accuracy and sensibility of the method is also included. (author)

  17. Orthodontic treatment: Introducing finite element analysis

    NARCIS (Netherlands)

    Driel, W.D. van; Leeuwen, E.J. van

    1998-01-01

    The aim of orthodontic treatment is the displacement of teeth by means ofspecial appliances, like braces and brackets. Through these appliances the orthodontist can apply a set of forces to the teeth which wilt result in its displacement through the jawbone. Finite Element analysis of this process

  18. A study on the nonlinear finite element analysis of reinforced concrete structures: shell finite element formulation

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Sang Jin; Seo, Jeong Moon

    2000-08-01

    The main goal of this research is to establish a methodology of finite element analysis of containment building predicting not only global behaviour but also local failure mode. In this report, we summerize some existing numerical analysis techniques to be improved for containment building. In other words, a complete description of the standard degenerated shell finite element formulation is provided for nonlinear stress analysis of nuclear containment structure. A shell finite element is derived using the degenerated solid concept which does not rely on a specific shell theory. Reissner-Mindlin assumptions are adopted to consider the transverse shear deformation effect. In order to minimize the sensitivity of the constitutive equation to structural types, microscopic material model is adopted. The four solution algorithms based on the standard Newton-Raphson method are discussed. Finally, two numerical examples are carried out to test the performance of the adopted shell medel.

  19. A study on the nonlinear finite element analysis of reinforced concrete structures: shell finite element formulation

    International Nuclear Information System (INIS)

    Lee, Sang Jin; Seo, Jeong Moon

    2000-08-01

    The main goal of this research is to establish a methodology of finite element analysis of containment building predicting not only global behaviour but also local failure mode. In this report, we summerize some existing numerical analysis techniques to be improved for containment building. In other words, a complete description of the standard degenerated shell finite element formulation is provided for nonlinear stress analysis of nuclear containment structure. A shell finite element is derived using the degenerated solid concept which does not rely on a specific shell theory. Reissner-Mindlin assumptions are adopted to consider the transverse shear deformation effect. In order to minimize the sensitivity of the constitutive equation to structural types, microscopic material model is adopted. The four solution algorithms based on the standard Newton-Raphson method are discussed. Finally, two numerical examples are carried out to test the performance of the adopted shell medel

  20. Modeling and Finite Element Analysis of Load-Carrying Performance of a Wind Turbine Considering the Influence of Assembly Factors

    Directory of Open Access Journals (Sweden)

    Jianmei Wang

    2017-03-01

    Full Text Available In this work, a wind turbine shrink disk is used as the research object to investigate load-carrying performance of a multi-layer interference fit, and the theoretical model and finite element model are constructed. According to those models, a MW-level turbine shrink disk is designed, and a test device is developed to apply torque to this turbine shrink disk by hydraulic jack. Then, the circumferential slip between the contact surfaces is monitored and the slip of all contact surfaces is zero. This conclusion verifies the reasonability of the proposed models. The effect of the key influencing factors, such as machining deviation, assembly clearance and propel stroke, were analyzed. The contact pressure and load torque of the mating surfaces were obtained by building typical models with different parameters using finite element analysis (FEA. The results show that the minimum assembly clearance and the machining deviation within the machining range have little influence on load-carrying performance of multi-layer interference fit, while having a greater influence on the maximum assembly clearance and the propel stroke. The results also show that the load-carrying performance of a multiple-layer interference fit can be ensured only if the key factors are set within a reasonable design range. To avoid the abnormal operation of equipment caused by insufficient load torque, the propel stroke during practical assembly should be at least 0.95 times the designed propel stroke, which is significant in guiding the design and assembly of the multi-layer interference fit.

  1. The multi-level perspective analysis: Indonesia geothermal energy transition study

    Science.gov (United States)

    Wisaksono, A.; Murphy, J.; Sharp, J. H.; Younger, P. L.

    2018-01-01

    The study adopts a multi-level perspective in technology transition to analyse how the transition process in the development of geothermal energy in Indonesia is able to compete against the incumbent fossil-fuelled energy sources. Three levels of multi-level perspective are socio-technical landscape (ST-landscape), socio-technical regime (ST-regime) and niche innovations in Indonesia geothermal development. The identification, mapping and analysis of the dynamic relationship between each level are the important pillars of the multi-level perspective framework. The analysis considers the set of rules, actors and controversies that may arise in the technological transition process. The identified geothermal resource risks are the basis of the emerging geothermal technological innovations in Indonesian geothermal. The analysis of this study reveals the transition pathway, which yields a forecast for the Indonesian geothermal technology transition in the form of scenarios and probable impacts.

  2. Introduction to nonlinear finite element analysis

    CERN Document Server

    Kim, Nam-Ho

    2015-01-01

    This book introduces the key concepts of nonlinear finite element analysis procedures. The book explains the fundamental theories of the field and provides instructions on how to apply the concepts to solving practical engineering problems. Instead of covering many nonlinear problems, the book focuses on three representative problems: nonlinear elasticity, elastoplasticity, and contact problems. The book is written independent of any particular software, but tutorials and examples using four commercial programs are included as appendices: ANSYS, NASTRAN, ABAQUS, and MATLAB. In particular, the MATLAB program includes all source codes so that students can develop their own material models, or different algorithms. This book also: ·         Presents clear explanations of nonlinear finite element analysis for elasticity, elastoplasticity, and contact problems ·         Includes many informative examples of nonlinear analyses so that students can clearly understand the nonlinear theory ·    ...

  3. Three dimensional finite element linear analysis of reinforced concrete structures

    International Nuclear Information System (INIS)

    Inbasakaran, M.; Pandarinathan, V.G.; Krishnamoorthy, C.S.

    1979-01-01

    A twenty noded isoparametric reinforced concrete solid element for the three dimensional linear elastic stress analysis of reinforced concrete structures is presented. The reinforcement is directly included as an integral part of the element thus facilitating discretization of the structure independent of the orientation of reinforcement. Concrete stiffness is evaluated by taking 3 x 3 x 3 Gauss integration rule and steel stiffness is evaluated numerically by considering three Gaussian points along the length of reinforcement. The numerical integration for steel stiffness necessiates the conversion of global coordiantes of the Gaussian points to nondimensional local coordinates and this is done by Newton Raphson iterative method. Subroutines for the above formulation have been developed and added to SAP and STAP routines for solving the examples. The validity of the reinforced concrete element is verified by comparison of results from finite element analysis and analytical results. It is concluded that this finite element model provides a valuable analytical tool for the three dimensional elastic stress analysis of concrete structures like beams curved in plan and nuclear containment vessels. (orig.)

  4. Statistical Energy Analysis (SEA) and Energy Finite Element Analysis (EFEA) Predictions for a Floor-Equipped Composite Cylinder

    Science.gov (United States)

    Grosveld, Ferdinand W.; Schiller, Noah H.; Cabell, Randolph H.

    2011-01-01

    Comet Enflow is a commercially available, high frequency vibroacoustic analysis software founded on Energy Finite Element Analysis (EFEA) and Energy Boundary Element Analysis (EBEA). Energy Finite Element Analysis (EFEA) was validated on a floor-equipped composite cylinder by comparing EFEA vibroacoustic response predictions with Statistical Energy Analysis (SEA) and experimental results. Statistical Energy Analysis (SEA) predictions were made using the commercial software program VA One 2009 from ESI Group. The frequency region of interest for this study covers the one-third octave bands with center frequencies from 100 Hz to 4000 Hz.

  5. Multi-spectral Image Analysis for Astaxanthin Coating Classification

    DEFF Research Database (Denmark)

    Ljungqvist, Martin Georg; Ersbøll, Bjarne Kjær; Nielsen, Michael Engelbrecht

    2011-01-01

    Industrial quality inspection using image analysis on astaxanthin coating in aquaculture feed pellets is of great importance for automatic production control. In this study multi-spectral image analysis of pellets was performed using LDA, QDA, SNV and PCA on pixel level and mean value of pixels...

  6. PIXE analysis for bioaccumulation studies of trace elements

    International Nuclear Information System (INIS)

    Iwata, Y.; Satoh, A.; Sasaki, Y.; Ito, R.; Kuramachi, K.

    2005-01-01

    Bioaccumulation by micro-alga in the ocean was simulated in nutritive seawater containing known amounts of trace metals, and the concentration factors for Fe, Zn and Cd were measured by PIXE. Trace transition metals in nearshore seawater were removed by Chelex-100. Then a culture solution was prepared by adding known amounts of trace metals and nutritive salts to the purified seawater. Marine micro-algae (Nannochloropsis sp., and Phaeodactylum sp.,) were purely cultured in the culture solution. An interested metal ion was added to the culture solution (0.01-5.0 mg/l). Alga in 10 ml of the culture solution was collected on a polycarbonate filter (pore size: 1.0 ) by suction filtration and subjected to 2.9 MeV proton bombardment. Na, Mg, Al, Si, P, S, Cl, K, Ca, Cr, Mn, Fe, Zn and Cd were simultaneously determined. PIXE multi-element analysis was possible using less than 1 mg of analytical sample. The quantity of the metal in the alga was increased in proportion to the concentration in the culture solution. The concentration factors for Zn, Fe and Cd were measured, e.g., 10200 ± 300 ml/g to Zn for Phaeodactylum. The trend of the affinity for the trace metals in the case of Nannochloropsis was Fe 3+ > Zn 2+ > Pb 2+ > Cd 2+ . (author)

  7. Prediction of residual stress distribution in multi-stacked thin film by curvature measurement and iterative FEA

    International Nuclear Information System (INIS)

    Choi, Hyeon Chang; Park, Jun Hyub

    2005-01-01

    In this study, residual stress distribution in multi-stacked film by MEMS (Micro-Electro Mechanical System) process is predicted using Finite Element Method (FEM). We develop a finite element program for REsidual Stress Analysis (RESA) in multi-stacked film. The RESA predicts the distribution of residual stress field in multi-stacked film. Curvatures of multi-stacked film and single layers which consist of the multi-stacked film are used as the input to the RESA. To measure those curvatures is easier than to measure a distribution of residual stress. To verify the RESA, mean stresses and stress gradients of single and multilayers are measured. The mean stresses are calculated from curvatures of deposited wafer by using Stoney's equation. The stress gradients are calculated from the vertical deflection at the end of cantilever beam. To measure the mean stress of each layer in multi-stacked film, we measure the curvature of wafer with the film after etching layer by layer in multi-stacked film

  8. Study of lattice strain evolution during biaxial deformation of stainless steel using a finite element and fast Fourier transform based multi-scale approach

    International Nuclear Information System (INIS)

    Upadhyay, M.V.; Van Petegem, S.; Panzner, T.; Lebensohn, R.A.; Van Swygenhoven, H.

    2016-01-01

    A multi-scale elastic-plastic finite element and fast Fourier transform based approach is proposed to study lattice strain evolution during uniaxial and biaxial loading of stainless steel cruciform shaped samples. At the macroscale, finite element simulations capture the complex coupling between applied forces in the arms and gauge stresses induced by the cruciform geometry. The predicted gauge stresses are used as macroscopic boundary conditions to drive a mesoscale elasto-viscoplastic fast Fourier transform model, from which lattice strains are calculated for particular grain families. The calculated lattice strain evolution matches well with experimental values from in-situ neutron diffraction measurements and demonstrates that the spread in lattice strain evolution between different grain families decreases with increasing biaxial stress ratio. During equibiaxial loading, the model reveals that the lattice strain evolution in all grain families, and not just the 311 grain family, is representative of the polycrystalline response. A detailed quantitative analysis of the 200 and 220 grain family reveals that the contribution of elastic and plastic anisotropy to the lattice strain evolution significantly depends on the applied stress ratio.

  9. Multi-recycling of transuranic elements in a PWR assembly with reduced fuel rod diameter

    International Nuclear Information System (INIS)

    Chambers, Alex; Ragusa, Jean C.

    2014-01-01

    Highlights: • Study of multiple recycling passes of transuranic elements: (a) without exceeding 5 wt.% on U-235 enrichment; (b) using PWR fuel assemblies compatible with current reactor core internals. • Isotopic concentrations tend towards an equilibrium after 15 recycle passes, suggesting that thermal recycling may be continued beyond that point. • Radiotoxicity comparisons for once-through UOX, once-recycle MOX-Pu, and multiple recycle passes of MOX-PuNpAm and MOX-PuNpAmCm are presented. - Abstract: This paper examines the multi-recycling of transuranic (TRU) elements (Pu-Np-Am-Cm) in standard Pressurized Water Reactor (PWR) assemblies. The original feed of TRU comes from legacy spent UOX fuel. For all subsequent recycling passes, TRU elements from the previous generation are employed, supplemented by TRU from legacy UOX fuel, as needed. The design criteria include: 235 U enrichment requirements to remain below 5 w/o, TRU loading limits to avoid return to criticality under voided conditions, and assembly power peaking factors. In order to carry out multiple recycling passes within the design envelope, additional neutron moderation is required and achieved by reducing the fuel pellet diameter by about 13%, thus keeping the assembly design compatible with current PWR core internals. TRU transmutation rates and long-term ingestion radiotoxicity results are presented for 15 recycling passes and compared to standard UOX and MOX once-through cycles. The results also show that TRU fuel isotopics and radiotoxicity tend towards an equilibrium, enabling further additional recycling passes

  10. Fundamentals of multi-element analysis with electron and beta radiation. 3

    International Nuclear Information System (INIS)

    Thuemmel, H.W.

    1977-01-01

    Mass attenuation coefficients obtained from calculations with the empirical formula μsub(Σ) = Σ psub(i).μsub(i) have been compared with the theoretical Schmidt formula (1906), in which the effective mass attenuation coefficient μsub(th) of a mixture of substances is the product of a true effective mass attenuation coefficient μ 0 and an effective by-pass coefficient U. Numerical results obtained from many substances of strongly varying composition show that for mixtures of components with atomic numbers Zsub(i) differing not too much from each other (contents psub(i), mass attenuation coefficients μsub(i) μ(Zsub(i)) μsub(Σ) is an approximation of μsub(th). This limitation is the less important, the less the curvature of the dependence of the mass attenuation coefficients of all elements on the atomic number (author)

  11. Statistical Analysis of the Spatial Distribution of Multi-Elements in an Island Arc Region: Complicating Factors and Transfer by Water Currents

    Directory of Open Access Journals (Sweden)

    Atsuyuki Ohta

    2017-01-01

    Full Text Available The compositions and transfer processes affecting coastal sea sediments from the Seto Inland Sea and the Pacific Ocean are examined through the construction of comprehensive terrestrial and marine geochemical maps for western Japan. Two-way analysis of variance (ANOVA suggests that the elemental concentrations of marine sediments vary with particle size, and that this has a greater effect than the regional provenance of the terrestrial material. Cluster analysis is employed to reveal similarities and differences in the geochemistry of coastal sea and stream sediments. This analysis suggests that the geochemical features of fine sands and silts in the marine environment reflect those of stream sediments in the adjacent terrestrial areas. However, gravels and coarse sands do not show this direct relationship, which is likely a result of mineral segregation by strong tidal currents and the denudation of old basement rocks. Finally, the transport processes for the fine-grained sediments are discussed, using the spatial distribution patterns of outliers for those elements enriched in silt and clay. Silty and clayey sediments are found to be transported and dispersed widely by a periodic current in the inner sea, and are selectively deposited at the boundary of different water masses in the outer sea.

  12. Multi-element fingerprinting as a tool in origin authentication of four east China marine species.

    Science.gov (United States)

    Guo, Lipan; Gong, Like; Yu, Yanlei; Zhang, Hong

    2013-12-01

    The contents of 25 elements in 4 types of commercial marine species from the East China Sea were determined by inductively coupled plasma mass spectrometry and atomic absorption spectrometry. The elemental composition was used to differentiate marine species according to geographical origin by multivariate statistical analysis. The results showed that principal component analysis could distinguish samples from different areas and reveal the elements which played the most important role in origin diversity. The established models by partial least squares discriminant analysis (PLS-DA) and by probabilistic neural network (PNN) can both precisely predict the origin of the marine species. Further study indicated that PLS-DA and PNN were efficacious in regional discrimination. The models from these 2 statistical methods, with an accuracy of 97.92% and 100%, respectively, could both distinguish samples from different areas without the need for species differentiation. © 2013 Institute of Food Technologists®

  13. Cost-effectiveness Analysis in R Using a Multi-state Modeling Survival Analysis Framework: A Tutorial.

    Science.gov (United States)

    Williams, Claire; Lewsey, James D; Briggs, Andrew H; Mackay, Daniel F

    2017-05-01

    This tutorial provides a step-by-step guide to performing cost-effectiveness analysis using a multi-state modeling approach. Alongside the tutorial, we provide easy-to-use functions in the statistics package R. We argue that this multi-state modeling approach using a package such as R has advantages over approaches where models are built in a spreadsheet package. In particular, using a syntax-based approach means there is a written record of what was done and the calculations are transparent. Reproducing the analysis is straightforward as the syntax just needs to be run again. The approach can be thought of as an alternative way to build a Markov decision-analytic model, which also has the option to use a state-arrival extended approach. In the state-arrival extended multi-state model, a covariate that represents patients' history is included, allowing the Markov property to be tested. We illustrate the building of multi-state survival models, making predictions from the models and assessing fits. We then proceed to perform a cost-effectiveness analysis, including deterministic and probabilistic sensitivity analyses. Finally, we show how to create 2 common methods of visualizing the results-namely, cost-effectiveness planes and cost-effectiveness acceptability curves. The analysis is implemented entirely within R. It is based on adaptions to functions in the existing R package mstate to accommodate parametric multi-state modeling that facilitates extrapolation of survival curves.

  14. Completely non-destructive elemental analysis of bulky samples by PGA

    International Nuclear Information System (INIS)

    Oura, Y.; Nakahara, H.; Sueki, K.; Sato, W.; Tomizawa, T.

    1998-01-01

    A new non-destructive method is proposed for the elemental analysis of bulk samples. It is essentially a combination of PGA and NAA by a single neutron irradiation, and allows determinations of elemental contents of both major and minor constituents relative to that of some reference element. Major elements and some trace elements such as B, Sm, and Gd are mostly determined by the measurement of prompt gamma rays emitted when a bulky sample in its original form, namely, without any reduction of the sample size, is placed in the beam of neutrons guided from a nuclear reactor. Minor elements are then determined by the off-line measurements of gamma rays emitted from the radioactive nuclides produced within the sample by neutron capture reactions. As the radioactivity remaining in the sample becomes negligibly small after a few weeks cooling, the proposed method will be most usefully applied for the elemental analysis of bulky precious samples such as archaeological samples, and arts and crafts. In this presentation, applicability of the method will be demonstrated for porcelain and bronze samples. (author)

  15. Game meat authentication through rare earth elements fingerprinting

    International Nuclear Information System (INIS)

    Danezis, G.P.; Pappas, A.C.; Zoidis, E.; Papadomichelakis, G.; Hadjigeorgiou, I.; Zhang, P.; Brusic, V.; Georgiou, C.A.

    2017-01-01

    Accurate labelling of meat (e.g. wild versus farmed, geographical and genetic origin, organic versus conventional, processing treatment) is important to inform the consumers about the products they buy. Meat and meat products declared as game have higher commercial value making them target to fraudulent labelling practices and replacement with non-game meat. We have developed and validated a new method for authentication of wild rabbit meat using elemental metabolomics approach. Elemental analysis was performed using rapid ultra-trace multi-element measurement by inductively coupled plasma mass spectrometry (ICP-MS). Elemental signatures showed excellent ability to discriminate the wild rabbit from non-wild rabbit meat. Our results demonstrate the usefulness of metabolic markers -rare earth signatures, as well as other trace element signatures for game meat authentication. - Highlights: • Elemental metabolomics is a powerful new methodology for authentication of game rabbit meat. • New method for meat authentication utilizing rare earths elemental signatures. • Samples are compared to group signatures using angular and Euclidean distances. • Meat reference materials (>70 elements) can be used for cross-comparison between studies.

  16. Noncoding Elements: Evolution and Epigenetic Regulation

    KAUST Repository

    Seridi, Loqmane

    2016-03-09

    When the human genome project was completed, it revealed a surprising result. 98% of the genome did not code for protein of which more than 50% are repeats— later known as ”Junk DNA”. However, comparative genomics unveiled that many noncoding elements are evolutionarily constrained; thus luckily to have a role in genome stability and regulation. Though, their exact functions remained largely unknown. Several large international consortia such as the Functional Annotation of Mammalian Genomes (FANTOM) and the Encyclopedia of DNA Elements (ENCODE) were set to understand the structure and the regulation of the genome. Specifically, these endeavors aim to measure and reveal the transcribed components and functional elements of the genome. One of the most the striking findings of these efforts is that most of the genome is transcribed, including non-conserved noncoding elements and repeat elements. Specifically, we investigated the evolution and epigenetic properties of noncoding elements. 1. We compared genomes of evolutionarily distant species and showed the ubiquity of constrained noncoding elements in metazoa. 2. By integrating multi-omic data (such as transcriptome, nucleosome profiling, histone modifications), I conducted a comprehensive analysis of epigenetic properties (chromatin states) of conserved noncoding elements in insects. We showed that those elements have distinct and protective sequence features, undergo dynamic epigenetic regulation, and appear to be associated with the structural components of the chromatin, replication origins, and nuclear matrix. 3. I focused on the relationship between enhancers and repetitive elements. Using Cap Analysis of Gene Expression (CAGE) and RNASeq, I compiled a full catalog of active enhancers (a class of noncoding elements) during myogenesis of human primary cells of healthy donors and donors affected by Duchenne muscular dystrophy (DMD). Comparing the two time-courses, a significant change in the epigenetic

  17. MultiSpec—a tool for multispectral hyperspectral image data analysis

    Science.gov (United States)

    Biehl, Larry; Landgrebe, David

    2002-12-01

    MultiSpec is a multispectral image data analysis software application. It is intended to provide a fast, easy-to-use means for analysis of multispectral image data, such as that from the Landsat, SPOT, MODIS or IKONOS series of Earth observational satellites, hyperspectral data such as that from the Airborne Visible-Infrared Imaging Spectrometer (AVIRIS) and EO-1 Hyperion satellite system or the data that will be produced by the next generation of Earth observational sensors. The primary purpose for the system was to make new, otherwise complex analysis tools available to the general Earth science community. It has also found use in displaying and analyzing many other types of non-space related digital imagery, such as medical image data and in K-12 and university level educational activities. MultiSpec has been implemented for both the Apple Macintosh ® and Microsoft Windows ® operating systems (OS). The effort was first begun on the Macintosh OS in 1988. The GLOBE ( http://www.globe.gov) program supported the development of a subset of MultiSpec for the Windows OS in 1995. Since then most (but not all) of the features in the Macintosh OS version have been ported to the Windows OS version. Although copyrighted, MultiSpec with its documentation is distributed without charge. The Macintosh and Windows versions and documentation on its use are available from the World Wide Web at URL: http://dynamo.ecn.purdue.edu/˜biehl/MultiSpec/ MultiSpec is copyrighted (1991-2001) by Purdue Research Foundation, West Lafayette, Indiana 47907.

  18. Finite element analysis of car hood for impact test by using ...

    African Journals Online (AJOL)

    Finite element analysis of car hood for impact test by using solidworks software ... high safety and at the same time can be built according to market demands. ... Keywords: finite element analysis; impact test; Solidworks; automation, car hood.

  19. Front-end vision and multi-scale image analysis multi-scale computer vision theory and applications, written in Mathematica

    CERN Document Server

    Romeny, Bart M Haar

    2008-01-01

    Front-End Vision and Multi-Scale Image Analysis is a tutorial in multi-scale methods for computer vision and image processing. It builds on the cross fertilization between human visual perception and multi-scale computer vision (`scale-space') theory and applications. The multi-scale strategies recognized in the first stages of the human visual system are carefully examined, and taken as inspiration for the many geometric methods discussed. All chapters are written in Mathematica, a spectacular high-level language for symbolic and numerical manipulations. The book presents a new and effective

  20. Uncertainty Flow Facilitates Zero-Shot Multi-Label Learning in Affective Facial Analysis

    Directory of Open Access Journals (Sweden)

    Wenjun Bai

    2018-02-01

    Full Text Available Featured Application: The proposed Uncertainty Flow framework may benefit the facial analysis with its promised elevation in discriminability in multi-label affective classification tasks. Moreover, this framework also allows the efficient model training and between tasks knowledge transfer. The applications that rely heavily on continuous prediction on emotional valance, e.g., to monitor prisoners’ emotional stability in jail, can be directly benefited from our framework. Abstract: To lower the single-label dependency on affective facial analysis, it urges the fruition of multi-label affective learning. The impediment to practical implementation of existing multi-label algorithms pertains to scarcity of scalable multi-label training datasets. To resolve this, an inductive transfer learning based framework, i.e.,Uncertainty Flow, is put forward in this research to allow knowledge transfer from a single labelled emotion recognition task to a multi-label affective recognition task. I.e., the model uncertainty—which can be quantified in Uncertainty Flow—is distilled from a single-label learning task. The distilled model uncertainty ensures the later efficient zero-shot multi-label affective learning. On the theoretical perspective, within our proposed Uncertainty Flow framework, the feasibility of applying weakly informative priors, e.g., uniform and Cauchy prior, is fully explored in this research. More importantly, based on the derived weight uncertainty, three sets of prediction related uncertainty indexes, i.e., soft-max uncertainty, pure uncertainty and uncertainty plus are proposed to produce reliable and accurate multi-label predictions. Validated on our manual annotated evaluation dataset, i.e., the multi-label annotated FER2013, our proposed Uncertainty Flow in multi-label facial expression analysis exhibited superiority to conventional multi-label learning algorithms and multi-label compatible neural networks. The success of our

  1. Probing Trace-elements in Bitumen by Neutron Activation Analysis

    NARCIS (Netherlands)

    Nahar, S.N.; Schmets, A.J.M.; Scarpas, Athanasios

    Trace elements and their concentrations play an important role in both chemical and physical properties of bitumen. Instrumental Neutron Activation Analysis (INAA) has been applied to determine the concentration of trace elements in bitumen. This method requires irradiation of the material with

  2. Multi-criteria analysis for site selection for the reuse of reclaimed water and biosolids

    Directory of Open Access Journals (Sweden)

    António Albuquerque

    2015-01-01

    Full Text Available Low pH soils with insufficient organic matter can benefit from the application of reclaimed water (RW and biosolids. The presence of nutrients also aids plant growth. This paper presents the results of two integrated research studies, both carried out in the Beira Interior Region (Covilhã, Portugal; one used RW for irrigation, the other applied paper mill sludge to agricultural land. In both cases, multiple criteria based on GIS tools were used for site selection. In the first study, the characteristics of RW analyzed over 2 years were found suitable for crop irrigation. The RW had moderate organic content, low electrical conductivity (CE, high nutrient content (N, P, and low concentrations of nitrate, metals and phytotoxic elements (Al, B, Cl and Na. The multi-criteria analysis was carried out taking into account environmental, technical and economic criteria and a suitable area of 30.5 ha was found for RW irrigation. In the second work, the paper mill sludge was considered suitable for application to agricultural land. Its concentrations of N, P and heavy metals did not a present risk for soil contamination and were suitable for soil improvement and crop production. A multi-criteria analysis based on similar criteria was conducted and a suitable area of 253 ha was found for sludge application.

  3. Generalized Multi-Edge Analysis for K-Edge Densitometry

    International Nuclear Information System (INIS)

    Collins, M.

    1998-01-01

    In K-edge densitometry (KED), a continuous-energy x-ray beam is transmitted through a liquid sample. The actinide content of the sample can be measured through analysis of the transmitted portion of the x-ray beam. Traditional methods for KED analysis allow the simultaneous calculation of, at most, two actinide concentrations. A generalized multi-edge KED analytical method is presented, allowing up to six actinide concentrations to be calculated simultaneously. Applications of this method for hybrid KED/x-ray fluorescence (HKED) systems are discussed. Current HKED systems require the operator to know the approximate actinide content of each sample, and manually select the proper analysis mode. The new multi-edge KED technique allows rapid identification of the major actinide components in a sample, independent of actinide content. The proper HKED analysis mode can be selected automatically, without requiring sample content information from the user. Automatic HKED analysis would be especially useful in an analytical laboratory setting, where samples with truly unknown characteristics are encountered. Because this technique requires no hardware modifications, several facilities that use HKED may eventually benefit from this approach

  4. PIXE methodology of rare earth element analysis and its applications

    International Nuclear Information System (INIS)

    Ma Xinpei

    1992-01-01

    The Proton Induced X-ray Emission (PIXE) methodology of rare earth element (REEs) analysis is discussed, including the significance of REE analysis, the principle of PIXE applied to REE, selection of characteristic X-ray for Lanthanide series elements, deconvolution of highly over lapped PIXE spectrum and minimum detection limit (MDL) of REEs. Some practical applications are presented. And the specialities of PIXE analysis to the high pure REE chemicals are discussed. (author)

  5. Analysis of elements present in beers and brewing waters by neutron activation analysis

    International Nuclear Information System (INIS)

    Krausova, Ivana; Kucera, Jan; Dostalek, Pavel; Potesil, Vaclav

    2011-01-01

    Neutron activation analysis (NAA) was used for determination of Si, Na, K, Ca, Sc, V, Cr, Mn, Fe, Co, Zn, Rb, Cs, and La in Czech beers and brewing waters. The Si concentration in beer determined by the reaction 29 Si(n,p) 29 Al with fast neutrons confirmed that beer is an important Si source in human diet. Determination of other trace elements by NAA with the whole spectrum of reactor neutrons aimed at the feasibility of identification of Gambrinus beers brewed in various breweries. The elements Ca and V appeared to be the best candidates for this purpose. The concentrations of elements determined by NAA were also compared with the recommended daily element intake for humans. The accuracy of the method was proved by analysis of reference materials, specifically NIST SRM 2704 Buffalo River Sediment, NIST SRM 1633b Coal Fly Ash, and NIST SRM 1515 Apple Leaves. (author)

  6. Multi-dimensional Fokker-Planck equation analysis using the modified finite element method

    Czech Academy of Sciences Publication Activity Database

    Náprstek, Jiří; Král, Radomil

    2016-01-01

    Roč. 744, č. 1 (2016), č. článku 012177. ISSN 1742-6588. [International Conference on Motion and Vibration Control (MOVIC 2016) /13./ and International Conference on Recent Advances in Structural Dynamics (RASD 2016) /12./. Southampton, 04.07.2016-06.07.2016] R&D Projects: GA ČR(CZ) GP14-34467P; GA ČR(CZ) GA15-01035S Institutional support: RVO:68378297 Keywords : Fokker-Planck equation * finite element method * single degree of freedom systems (SDOF) Subject RIV: JM - Building Engineering http://iopscience.iop.org/article/10.1088/1742-6596/744/1/012177

  7. Introduction to finite element analysis using MATLAB and Abaqus

    CERN Document Server

    Khennane, Amar

    2013-01-01

    There are some books that target the theory of the finite element, while others focus on the programming side of things. Introduction to Finite Element Analysis Using MATLAB(R) and Abaqus accomplishes both. This book teaches the first principles of the finite element method. It presents the theory of the finite element method while maintaining a balance between its mathematical formulation, programming implementation, and application using commercial software. The computer implementation is carried out using MATLAB, while the practical applications are carried out in both MATLAB and Abaqus. MA

  8. Structural weights analysis of advanced aerospace vehicles using finite element analysis

    Science.gov (United States)

    Bush, Lance B.; Lentz, Christopher A.; Rehder, John J.; Naftel, J. Chris; Cerro, Jeffrey A.

    1989-01-01

    A conceptual/preliminary level structural design system has been developed for structural integrity analysis and weight estimation of advanced space transportation vehicles. The system includes a three-dimensional interactive geometry modeler, a finite element pre- and post-processor, a finite element analyzer, and a structural sizing program. Inputs to the system include the geometry, surface temperature, material constants, construction methods, and aerodynamic and inertial loads. The results are a sized vehicle structure capable of withstanding the static loads incurred during assembly, transportation, operations, and missions, and a corresponding structural weight. An analysis of the Space Shuttle external tank is included in this paper as a validation and benchmark case of the system.

  9. Capture analysis of element content of a substance with other neutron methods

    International Nuclear Information System (INIS)

    Kurbanov, B.I.

    2004-01-01

    Full text: Neutron analysis method of determining element composition have found wide range of applications in industry thanks to different types of interaction of neutron with substances /1/. With the aim of widening the range of problems to be solved, on the basis of the device /2/ for determining the element content of substance, possibilities of combining the method based on the use of neutron capture gamma-ray spectrometry with other neutron methods, in particular neutron activation analysis and neutron absorption analysis were studied. In this radionuclide source ( 252 Cf) with the yield of 1,5 x 10 7 neutron/sec is used. By means of using neutron capture gamma radiation spectrometry the possibilities of determining some elements (H, B, N, S etc. ), which are not determined by very widely used method, activation analysis. These elements can be determined by both the semiconductor and scintillation detectors with parameters fitting the manufacturing requirements. And for a number of elements ( B, Cl, Cd, Sm, Gd) very high limits of determination ( up to 10- 5 %) are possible using semiconductor Ge (Li) -detectors with high resolution. Possibility of determination of some 'well' activated elements ( K, Al, Fe, Mn, Ti, Sc etc.) in samples of ore and products of their processing using the neutron-activation analysis. For 1 hour of irradiation on the experimental device quite accurate analytical peak, of these elements are obtained, allowing to determine them qualitatively. However, with decreasing neutron yield of radionuclide source it becomes more difficult to achieve the necessary parameters both in neutron capture and activation analysis. Experimental works on determination of some elements with large cross-sections of capture ( B, Cd, Sm ) by absorption of neutrons in the investigated substance, i.e. using the neutron absorption analysis method with absence of other large capture cross section elements in the samples being studied

  10. Scanning Electron Microscope-Cathodoluminescence Analysis of Rare-Earth Elements in Magnets.

    Science.gov (United States)

    Imashuku, Susumu; Wagatsuma, Kazuaki; Kawai, Jun

    2016-02-01

    Scanning electron microscope-cathodoluminescence (SEM-CL) analysis was performed for neodymium-iron-boron (NdFeB) and samarium-cobalt (Sm-Co) magnets to analyze the rare-earth elements present in the magnets. We examined the advantages of SEM-CL analysis over conventional analytical methods such as SEM-energy-dispersive X-ray (EDX) spectroscopy and SEM-wavelength-dispersive X-ray (WDX) spectroscopy for elemental analysis of rare-earth elements in NdFeB magnets. Luminescence spectra of chloride compounds of elements in the magnets were measured by the SEM-CL method. Chloride compounds were obtained by the dropwise addition of hydrochloric acid on the magnets followed by drying in vacuum. Neodymium, praseodymium, terbium, and dysprosium were separately detected in the NdFeB magnets, and samarium was detected in the Sm-Co magnet by the SEM-CL method. In contrast, it was difficult to distinguish terbium and dysprosium in the NdFeB magnet with a dysprosium concentration of 1.05 wt% by conventional SEM-EDX analysis. Terbium with a concentration of 0.02 wt% in an NdFeB magnet was detected by SEM-CL analysis, but not by conventional SEM-WDX analysis. SEM-CL analysis is advantageous over conventional SEM-EDX and SEM-WDX analyses for detecting trace rare-earth elements in NdFeB magnets, particularly dysprosium and terbium.

  11. Probabilistic finite elements for transient analysis in nonlinear continua

    Science.gov (United States)

    Liu, W. K.; Belytschko, T.; Mani, A.

    1985-01-01

    The probabilistic finite element method (PFEM), which is a combination of finite element methods and second-moment analysis, is formulated for linear and nonlinear continua with inhomogeneous random fields. Analogous to the discretization of the displacement field in finite element methods, the random field is also discretized. The formulation is simplified by transforming the correlated variables to a set of uncorrelated variables through an eigenvalue orthogonalization. Furthermore, it is shown that a reduced set of the uncorrelated variables is sufficient for the second-moment analysis. Based on the linear formulation of the PFEM, the method is then extended to transient analysis in nonlinear continua. The accuracy and efficiency of the method is demonstrated by application to a one-dimensional, elastic/plastic wave propagation problem. The moments calculated compare favorably with those obtained by Monte Carlo simulation. Also, the procedure is amenable to implementation in deterministic FEM based computer programs.

  12. Multi-element Analysis of variable sample matrices using collision/reaction cell inductively coupled plasma mass spectrometry

    International Nuclear Information System (INIS)

    Zahran, N.F.; Helal, A.I.; Amr, M.A.; Amr, M.A.; Al-saad, K.A.

    2008-01-01

    An ICP-MS with an octopole reaction/collision cell is used for the multielement determination of trace elements in water, plants, and soil samples. The use of a reaction or collision gas reduces serious spectral interferences from matrix elements such as Ar Cl or Ar Na. The background equivalent concentration (BEC) is reduced one order of magnitude at helium flow rate of 1 mL/min. Certified reference material namely , NIST Water-1643d, Tomato leaves 1573a, and Montana soil 2711 are used. The trace elements Mn, Fe, Co, Ni, Cu, Zn, As, Mo, Cd and Pb are determined in the different matrices with a accuracy better than 8% to the certified values

  13. Multi-resolution simulation of focused ultrasound propagation through ovine skull from a single-element transducer

    Science.gov (United States)

    Yoon, Kyungho; Lee, Wonhye; Croce, Phillip; Cammalleri, Amanda; Yoo, Seung-Schik

    2018-05-01

    Transcranial focused ultrasound (tFUS) is emerging as a non-invasive brain stimulation modality. Complicated interactions between acoustic pressure waves and osseous tissue introduce many challenges in the accurate targeting of an acoustic focus through the cranium. Image-guidance accompanied by a numerical simulation is desired to predict the intracranial acoustic propagation through the skull; however, such simulations typically demand heavy computation, which warrants an expedited processing method to provide on-site feedback for the user in guiding the acoustic focus to a particular brain region. In this paper, we present a multi-resolution simulation method based on the finite-difference time-domain formulation to model the transcranial propagation of acoustic waves from a single-element transducer (250 kHz). The multi-resolution approach improved computational efficiency by providing the flexibility in adjusting the spatial resolution. The simulation was also accelerated by utilizing parallelized computation through the graphic processing unit. To evaluate the accuracy of the method, we measured the actual acoustic fields through ex vivo sheep skulls with different sonication incident angles. The measured acoustic fields were compared to the simulation results in terms of focal location, dimensions, and pressure levels. The computational efficiency of the presented method was also assessed by comparing simulation speeds at various combinations of resolution grid settings. The multi-resolution grids consisting of 0.5 and 1.0 mm resolutions gave acceptable accuracy (under 3 mm in terms of focal position and dimension, less than 5% difference in peak pressure ratio) with a speed compatible with semi real-time user feedback (within 30 s). The proposed multi-resolution approach may serve as a novel tool for simulation-based guidance for tFUS applications.

  14. Evaluation of trace elements in some northern-Nigeria traditional medicinal plants using INAA technique

    International Nuclear Information System (INIS)

    Oladipo, M.O.A.; Njinga, R.L.; Baba, A.; Muhammad, H.L.

    2012-01-01

    Instrumental neutron activation analysis was used for multi-trace elemental determination of six medicinal plants: Boerhavia diffusa, Euphoria hirta, Senna occidentalis, Senna obtusofolia, Cyprus dilatatus and Mitracarpus villosu. These plants were irradiated in the Nigeria Research reactor-1, at flux levels of 2.25E+11 ncm −2 s −1 in the outer channel and 5.0E+11 ncm −2 s −1 in the inner channel. A total of the twenty one elemental concentrations were evaluated highlighted the similarity between the elements obtained for the six plants. It was found that Euphoria hirta and Senna occidentalis have similar concentrations of elements. Boerhavia difusa, Mitracarpus villosus, Cyprus dilatalus and Senna obttusifolia were also similar in elemental content to each other, while Boerhavia difusa was the only exceptional outlier. The accuracy of measurements was evaluated by analyzing IAEA-359 cabbage references standard materials and the results show good agreement with certified or literature values within ±0.01% to ±0.87%. - Highlights: ► Application of neutron activation analysis. ► Multi-trace elemental determination of six medicinal plants in northern Nigeria. ► Accuracy of the measurements was based on analyzing IAEA-359 cabbage, a standard reference material. ► Results showed good agreement with certified values within ±0.01 % to ±0.87%.

  15. Review of multi-physics temporal coupling methods for analysis of nuclear reactors

    International Nuclear Information System (INIS)

    Zerkak, Omar; Kozlowski, Tomasz; Gajev, Ivan

    2015-01-01

    Highlights: • Review of the numerical methods used for the multi-physics temporal coupling. • Review of high-order improvements to the Operator Splitting coupling method. • Analysis of truncation error due to the temporal coupling. • Recommendations on best-practice approaches for multi-physics temporal coupling. - Abstract: The advanced numerical simulation of a realistic physical system typically involves multi-physics problem. For example, analysis of a LWR core involves the intricate simulation of neutron production and transport, heat transfer throughout the structures of the system and the flowing, possibly two-phase, coolant. Such analysis involves the dynamic coupling of multiple simulation codes, each one devoted to the solving of one of the coupled physics. Multiple temporal coupling methods exist, yet the accuracy of such coupling is generally driven by the least accurate numerical scheme. The goal of this paper is to review in detail the approaches and numerical methods that can be used for the multi-physics temporal coupling, including a comprehensive discussion of the issues associated with the temporal coupling, and define approaches that can be used to perform multi-physics analysis. The paper is not limited to any particular multi-physics process or situation, but is intended to provide a generic description of multi-physics temporal coupling schemes for any development stage of the individual (single-physics) tools and methods. This includes a wide spectrum of situation, where the individual (single-physics) solvers are based on pre-existing computation codes embedded as individual components, or a new development where the temporal coupling can be developed and implemented as a part of code development. The discussed coupling methods are demonstrated in the framework of LWR core analysis

  16. Determination of uranium isotopes (235U, 238U) and trace elements (Cd, Pb, Cu and As) in bottled drinking water by Icp-SFMS

    International Nuclear Information System (INIS)

    Lara A, N.; Hernandez M, H.; Romero G, E. T.; Kuri de la C, A.; Perez B, M. A.

    2016-09-01

    In the present work we propose an optimized method for the quantification of uranium isotopes ( 235 U, 2 38 U) and the elements Cd, Pb, Cu and As in bottled water for drinking at trace levels of concentration. Based on the multi-element detection capability, the high sensitivity and resolution that the Mass Spectrometry with Magnetic Sector with Inductively Coupled Plasma Source (Icp-SFMS) technique offers; the high, medium and low resolution analysis conditions for the elements under study were established and optimized using and Element 2/Xr equipment and the 23 multi-elemental Certified Reference Material (CRM). The analysis method was validated using the standard reference material Nist 1643d and CRM mono-elemental s as external standards for the quantification of the analytes. Samples, targets and CRM were acidified with 2% of HNO 3 and analyzed without pretreatment under the established analysis conditions. The results obtained show concentrations of 235 U, 238 U, 111 Cd, 208 Pb, 63 Cu and 75 As in the range of μg L -1 , the linearity obtained from the calibration curves for each element has correlation coefficients < 0.99 in all cases, the accuracy of the method in terms of percent relative standard deviation (RSD %) was less than 5%, the mean recovery rate of Nist 1643d ranged from 96.46% to 101.12%. The optimization of the method guarantees the stability and calibration of the equipment throughout the analysis, as well as the ability to resolve interferences. In conclusion, the method proposed using Icp-SFMS offers the advantages of being fast and simple for the multi-elemental analysis in water at trace levels, with low limits of quantification and detection, with good linearity, accuracy, precision and reproducibility to a degree of reliability of 95%. (Author)

  17. Cost Analysis In A Multi-Mission Operations Environment

    Science.gov (United States)

    Newhouse, M.; Felton, L.; Bornas, N.; Botts, D.; Roth, K.; Ijames, G.; Montgomery, P.

    2014-01-01

    Spacecraft control centers have evolved from dedicated, single-mission or single missiontype support to multi-mission, service-oriented support for operating a variety of mission types. At the same time, available money for projects is shrinking and competition for new missions is increasing. These factors drive the need for an accurate and flexible model to support estimating service costs for new or extended missions; the cost model in turn drives the need for an accurate and efficient approach to service cost analysis. The National Aeronautics and Space Administration (NASA) Huntsville Operations Support Center (HOSC) at Marshall Space Flight Center (MSFC) provides operations services to a variety of customers around the world. HOSC customers range from launch vehicle test flights; to International Space Station (ISS) payloads; to small, short duration missions; and has included long duration flagship missions. The HOSC recently completed a detailed analysis of service costs as part of the development of a complete service cost model. The cost analysis process required the team to address a number of issues. One of the primary issues involves the difficulty of reverse engineering individual mission costs in a highly efficient multimission environment, along with a related issue of the value of detailed metrics or data to the cost model versus the cost of obtaining accurate data. Another concern is the difficulty of balancing costs between missions of different types and size and extrapolating costs to different mission types. The cost analysis also had to address issues relating to providing shared, cloud-like services in a government environment, and then assigning an uncertainty or risk factor to cost estimates that are based on current technology, but will be executed using future technology. Finally the cost analysis needed to consider how to validate the resulting cost models taking into account the non-homogeneous nature of the available cost data and the

  18. Challenges from variation across regions in cost effectiveness analysis in multi-regional clinical trials

    Directory of Open Access Journals (Sweden)

    Yunbo Chu

    2016-10-01

    Full Text Available Economic evaluation in the form of cost-effectiveness analysis has become a popular means to inform decisions in healthcare. With multi-regional clinical trials in a global development program becoming a new venue for drug efficacy testing in recent decades, questions in methods for cost-effectiveness analysis in the multi-regional clinical trials setting also emerge. This paper addresses some challenges from variation across regions in cost effectiveness analysis in multi-regional clinical trials. Several discussion points are raised for further attention and a multi-regional clinical trial example is presented to illustrate the implications in industrial application. A general message is delivered to call for a depth discussion by all stakeholders to reach an agreement on a good practice in cost-effectiveness analysis in the multi-regional clinical trials. Meanwhile, we recommend an additional consideration of cost-effectiveness analysis results based on the clinical evidence from a certain homogeneous population as sensitivity or scenario analysis upon data availability.

  19. Investigation of the Behavior of Steel Shear Walls Using Finite Elements Analysis

    Directory of Open Access Journals (Sweden)

    K. Abubakri

    2016-10-01

    Full Text Available Currently, steel shear walls are considered by engineers as an economic method against lateral loads imposed by wind and earthquake in tall structures. Accordingly, there is a growing need to develop accurate methods alongside approximation methods to estimate the behavior of these structural elements. The finite element technique is one of the strongest numerical methods in analysis of solid mechanics problems. Finite element analysis however requires high technical knowledge of the behavioral models of materials. Therefore, it is less used by designers for certain structural elements such as steel shear walls. This study examines the failure mechanism of steel shear walls using finite elements analysis and validates this modeling by comparing the results with experimental studies.

  20. Trace Elements in Apple Fruits of Several Regions in the Republic of Macedonia

    International Nuclear Information System (INIS)

    Boev, Blazho; Lepitkova, Sonja; Paneva-Zajkova, Vesna; Georgiev, Lazar

    2006-01-01

    Determination of macro elements and trace elements in apple fruits was carried out by ICP-AES method. Apples were picked up fresh in December 2005. Seven different types of apples from different parts of the country were selected. Apples were sliced into large pieces, dried, and after grinding were dissolved in nitric acid (HNO 3 ) and hydroperoxide (H 2 O 2 ). After digestion, multi-element analysis was carried out. Data obtained were compared to published values for trace elements in apples in other regions of the world. Data obtained indicated that the concentration of trace elements in apples were within the values and data in other regions of the world. (Author)

  1. Multi-terminal direct-current grids modeling, analysis, and control

    CERN Document Server

    Chaudhuri, Nilanjan; Majumder, Rajat; Yazdani, Amirnaser

    2014-01-01

    A comprehensive modeling, analysis, and control design framework for multi-terminal direct current (MTDC) grids is presented together with their interaction with the surrounding AC networks and the impact on overall stability. The first book of its kind on the topic of multi-terminal DC (MTDC) grids  Presents a comprehensive modeling framework for MTDC grids which is compatible with the standard AC system modeling for stability studies Includes modal analysis and study of the interactions between the MTDC grid and the surrounding AC systems Addresses the problems of autonomous power sharing an

  2. Rayleigh-based, multi-element coral thermometry: A biomineralization approach to developing climate proxies

    Science.gov (United States)

    Gaetani, G.A.; Cohen, A.L.; Wang, Z.; Crusius, John

    2011-01-01

    This study presents a new approach to coral thermometry that deconvolves the influence of water temperature on skeleton composition from that of “vital effects”, and has the potential to provide estimates of growth temperatures that are accurate to within a few tenths of a degree Celsius from both tropical and cold-water corals. Our results provide support for a physico-chemical model of coral biomineralization, and imply that Mg2+ substitutes directly for Ca2+ in biogenic aragonite. Recent studies have identified Rayleigh fractionation as an important influence on the elemental composition of coral skeletons. Daily, seasonal and interannual variations in the amount of aragonite precipitated by corals from each “batch” of calcifying fluid can explain why the temperature dependencies of elemental ratios in coral skeleton differ from those of abiogenic aragonites, and are highly variable among individual corals. On the basis of this new insight into the origin of “vital effects” in coral skeleton, we developed a Rayleigh-based, multi-element approach to coral thermometry. Temperature is resolved from the Rayleigh fractionation signal by combining information from multiple element ratios (e.g., Mg/Ca, Sr/Ca, Ba/Ca) to produce a mathematically over-constrained system of Rayleigh equations. Unlike conventional coral thermometers, this approach does not rely on an initial calibration of coral skeletal composition to an instrumental temperature record. Rather, considering coral skeletogenesis as a biologically mediated, physico-chemical process provides a means to extract temperature information from the skeleton composition using the Rayleigh equation and a set of experimentally determined partition coefficients. Because this approach is based on a quantitative understanding of the mechanism that produces the “vital effect” it should be possible to apply it both across scleractinian species and to corals growing in vastly different environments. Where

  3. Elemental analysis of biological materials. Current problems and techniques with special reference to trace elements

    International Nuclear Information System (INIS)

    1980-01-01

    Selected techniques were reviewed for the assay of trace and minor elements in biological materials. Other relevant information is also presented on the need for such analyses, sampling, sample preparation and analytical quality control. In order to evaluate and compare the applicability of the various analytical techniques on a meaningful and objective basis, the materials chosen for consideration were intended to be typical of a wide range of biological matrics of different elemental compositions, namely Bowen's kale, representing a plant material, and NBS bovine liver, IAEA animal muscle, and blood serum, representing animal tissues. The subject is reviewed under the following headings: on the need for trace element analyses in the life sciences (4 papers); sampling and sample preparation for trace element analysis (2 papers); analytical techniques for trace and minor elements in biological materials (7 papers); analytical quality control (2 papers)

  4. Effects of Process Parameters on Copper Powder Compaction Process Using Multi-Particle Finite Element Method

    Science.gov (United States)

    Güner, F.; Sofuoğlu, H.

    2018-01-01

    Powder metallurgy (PM) has been widely used in several industries; especially automotive and aerospace industries and powder metallurgy products grow up every year. The mechanical properties of the final product that is obtained by cold compaction and sintering in powder metallurgy are closely related to the final relative density of the process. The distribution of the relative density in the die is affected by parameters such as compaction velocity, friction coefficient and temperature. Moreover, most of the numerical studies utilizing finite element approaches treat the examined environment as a continuous media with uniformly homogeneous porosity whereas Multi-Particle Finite Element Method (MPFEM) treats every particles as an individual body. In MPFEM, each of the particles can be defined as an elastic- plastic deformable body, so the interactions of the particles with each other and the die wall can be investigated. In this study, each particle was modelled and analyzed as individual deformable body with 3D tetrahedral elements by using MPFEM approach. This study, therefore, was performed to investigate the effects of different temperatures and compaction velocities on stress distribution and deformations of copper powders of 200 µm-diameter in compaction process. Furthermore, 3-D MPFEM model utilized von Mises material model and constant coefficient of friction of μ=0.05. In addition to MPFEM approach, continuum modelling approach was also performed for comparison purposes.

  5. Resonant Quasi-Optical Systems with Multi-Row Periodic Structures

    DEFF Research Database (Denmark)

    Oleksandr, Rybalko; Rybalko, Yu A.; Buriak, I. A.

    2017-01-01

    Selective properties of resonant quasi-optical systems with periodical multi-row structures in millimeter wavelength range are described. The possibility of selection fluctuations in the volume of open resonator using double-row periodic elements was shown in the experiment at 70-80 GHz. Advantages...... and possibility of control the energy characteristics of such structures are also described. The obtained experimental data is used to confirm the results of computational analysis previously described in the literature. Implementation of resonant quasi-optical systems with multi-row periodic structures...

  6. Implementation of Grid-computing Framework for Simulation in Multi-scale Structural Analysis

    Directory of Open Access Journals (Sweden)

    Data Iranata

    2010-05-01

    Full Text Available A new grid-computing framework for simulation in multi-scale structural analysis is presented. Two levels of parallel processing will be involved in this framework: multiple local distributed computing environments connected by local network to form a grid-based cluster-to-cluster distributed computing environment. To successfully perform the simulation, a large-scale structural system task is decomposed into the simulations of a simplified global model and several detailed component models using various scales. These correlated multi-scale structural system tasks are distributed among clusters and connected together in a multi-level hierarchy and then coordinated over the internet. The software framework for supporting the multi-scale structural simulation approach is also presented. The program architecture design allows the integration of several multi-scale models as clients and servers under a single platform. To check its feasibility, a prototype software system has been designed and implemented to perform the proposed concept. The simulation results show that the software framework can increase the speedup performance of the structural analysis. Based on this result, the proposed grid-computing framework is suitable to perform the simulation of the multi-scale structural analysis.

  7. Elemental analysis of soil and hair sample by instrumental neutron activation analysis

    International Nuclear Information System (INIS)

    Chung, Yong Sam; Quraishi, Shamshad Begum; Moon, Jong Hwa; Kim, Sun Ha; Baek, Sung Yeoil; Kang, Sang Hoon; Lim, Jong Myoung; Cho, Hyun Je; Kim, Young Jin

    2004-03-01

    Myanmar soil sample was analyzed by using the instrumental neutron activation analysis. The elemental concentrations in the sample, altogether 34 elements, Al As, Ba, Ce, Co, Cr, Cs, Eu, Fe, Ga, Gd, Hf, Ir, K, La, Lu, Mn, Na, Nd, Rb, Sb, Sc, Se, Sm, Th, Ti, V, Yb, Zn and Zr were determined. The concentration of 17 elements (Al, Au, Br, Ca, Cl, Cr, Cu, Co, Fe, Hg, K, Na, Mn, Mg, Sb, Se, Zn) in human hair samples were determined by INAA For quality control of analytical method, certified reference material was used

  8. Elemental analysis of soil and hair sample by instrumental neutron activation analysis

    Energy Technology Data Exchange (ETDEWEB)

    Chung, Yong Sam; Quraishi, Shamshad Begum; Moon, Jong Hwa; Kim, Sun Ha; Baek, Sung Yeoil; Kang, Sang Hoon; Lim, Jong Myoung; Cho, Hyun Je; Kim, Young Jin

    2004-03-01

    Myanmar soil sample was analyzed by using the instrumental neutron activation analysis. The elemental concentrations in the sample, altogether 34 elements, Al As, Ba, Ce, Co, Cr, Cs, Eu, Fe, Ga, Gd, Hf, Ir, K, La, Lu, Mn, Na, Nd, Rb, Sb, Sc, Se, Sm, Th, Ti, V, Yb, Zn and Zr were determined. The concentration of 17 elements (Al, Au, Br, Ca, Cl, Cr, Cu, Co, Fe, Hg, K, Na, Mn, Mg, Sb, Se, Zn) in human hair samples were determined by INAA For quality control of analytical method, certified reference material was used.

  9. Output signal analysis for a variation of the R-C passive elements in a 4-2 mA R-L-C equivalent circuit modeling under a high temperature accident condition in NPPs

    International Nuclear Information System (INIS)

    Kil-Mo, Koo; Sang-Baik, Kim; Hee-Dong, Kim; Gyu-Tae, Kim

    2007-01-01

    An electrical signal should be checked to see whether it lies within its expected electrical range when there is a doubtful condition. The normal signal level for pressure, flow, level and resistance temperature detector sensors is 4-20 mA in most industrial process controls. In the case of an abnormal signal level from an instrument under a severe accident condition, it is necessary to obtain a more accurate signal validation to operate a system in a control room in NPPs. Diagnostics and analysis for some abnormal signals have been performed through an important equivalent circuits modeling for passive elements under severe accident conditions. Unlike the design basis accidents, there are some inherent uncertainties for the instrumentation capabilities under severe accident conditions. In this paper, to implement a diagnostic analysis for an equivalent circuits modeling, a kind of linked LabVIEW program for each PSpice and MULTI-SIM code is introduced as a one body order system, which can obtain some abnormal signal patterns by a special function such as an advanced simulation tool for each PSpice and Multi-SIM code as a means of a function for a PC based ASSA (Abnormal Signal Simulation Analyzer) module. The output signal can be analyzed by a comparative analysis of each PSpice and Multi-SIM code for a 4-20 mA circuit modeling which is by a composition of an R-L-C passive circuit as an alternating range of the elements for the temperature accident condition. In this simulation, a new simulator through an analysis of the important equivalent circuits modeling has been designed, the designed simulator is composed of the LabVIEW code as a main tool and the out-put file of each PSpice code and a Multi-SIM engine code as an engine tool is exported to the in-put file of the LabVIEW code. There are 3 main function units of the ASSA module, the first one is individual PSpice and Multi-SIM engine code units to comprise an equivalent circuit element, the second one is the

  10. Elemental misinterpretation in automated analysis of LIBS spectra.

    Science.gov (United States)

    Hübert, Waldemar; Ankerhold, Georg

    2011-07-01

    In this work, the Stark effect is shown to be mainly responsible for wrong elemental allocation by automated laser-induced breakdown spectroscopy (LIBS) software solutions. Due to broadening and shift of an elemental emission line affected by the Stark effect, its measured spectral position might interfere with the line position of several other elements. The micro-plasma is generated by focusing a frequency-doubled 200 mJ pulsed Nd/YAG laser on an aluminum target and furthermore on a brass sample in air at atmospheric pressure. After laser pulse excitation, we have measured the temporal evolution of the Al(II) ion line at 281.6 nm (4s(1)S-3p(1)P) during the decay of the laser-induced plasma. Depending on laser pulse power, the center of the measured line is red-shifted by 130 pm (490 GHz) with respect to the exact line position. In this case, the well-known spectral line positions of two moderate and strong lines of other elements coincide with the actual shifted position of the Al(II) line. Consequently, a time-resolving software analysis can lead to an elemental misinterpretation. To avoid a wrong interpretation of LIBS spectra in automated analysis software for a given LIBS system, we recommend using larger gate delays incorporating Stark broadening parameters and using a range of tolerance, which is non-symmetric around the measured line center. These suggestions may help to improve time-resolving LIBS software promising a smaller probability of wrong elemental identification and making LIBS more attractive for industrial applications.

  11. MultiElec: A MATLAB Based Application for MEA Data Analysis.

    Science.gov (United States)

    Georgiadis, Vassilis; Stephanou, Anastasis; Townsend, Paul A; Jackson, Thomas R

    2015-01-01

    We present MultiElec, an open source MATLAB based application for data analysis of microelectrode array (MEA) recordings. MultiElec displays an extremely user-friendly graphic user interface (GUI) that allows the simultaneous display and analysis of voltage traces for 60 electrodes and includes functions for activation-time determination, the production of activation-time heat maps with activation time and isoline display. Furthermore, local conduction velocities are semi-automatically calculated along with their corresponding vector plots. MultiElec allows ad hoc signal suppression, enabling the user to easily and efficiently handle signal artefacts and for incomplete data sets to be analysed. Voltage traces and heat maps can be simply exported for figure production and presentation. In addition, our platform is able to produce 3D videos of signal progression over all 60 electrodes. Functions are controlled entirely by a single GUI with no need for command line input or any understanding of MATLAB code. MultiElec is open source under the terms of the GNU General Public License as published by the Free Software Foundation, version 3. Both the program and source code are available to download from http://www.cancer.manchester.ac.uk/MultiElec/.

  12. Downhole Elemental Analysis with LIBS

    Science.gov (United States)

    Moreschini, Paolo; Zacny, Kris; Rickman, Doug

    2011-01-01

    In this paper we discuss a novel instrument, currently under development at Honeybee Robotics with SBIR funding from NASA. The device is designed to characterize elemental composition as a function of depth in non-terrestrial geological formations. The instrument consists of a miniaturized laser-induced breakdown spectrometer (LIBS) analyzer integrated in a 2" diameter drill string. While the drill provides subsurface access, the LIBS analyzer provides information on the elemental composition of the borehole wall. This instrument has a variety of space applications ranging from exploration of the Moon for which it was originally designed, to Mars, as well as a variety of terrestrial applications. Subsurface analysis is usually performed by sample acquisition through a drill or excavator, followed by sample preparation and subsequent sample presentation to an instrument or suite of instruments. An alternative approach consisting in bringing a miniaturized version of the instrument to the sample has many advantages over the traditional methodology, as it allows faster response, reduced probability of cross-contamination and a simplification in the sampling mechanisms. LIBS functions by focusing a high energy laser on a material inducing a plasma consisting of a small fraction of the material under analysis. Optical emission from the plasma, analyzed by a spectrometer, can be used to determine elemental composition. A triangulation sensor located in the sensor head determines the distance of the sensor from the borehole wall. An actuator modifies the position of the sensor accordingly, in order to compensate for changes due to the profile of the borehole walls. This is necessary because LIBS measurements are negatively affected by changes in the relative position of the focus of the laser with respect to the position of the sample (commonly referred to as the "lens to sample distance"). Profiling the borehole is done by adjusting the position of the sensor with a

  13. Static Analysis of Steel Fiber Concrete Beam With Heterosis Finite Elements

    Directory of Open Access Journals (Sweden)

    James H. Haido

    2014-08-01

    Full Text Available Steel fiber is considered as the most commonly used constructional fibers in concrete structures. The formulation of new nonlinearities to predict the static performance of steel fiber concrete composite structures is considered essential. Present study is devoted to investigate the efficiency of utilizing heterosis finite elements analysis in static analysis of steel fibrous beams. New and simple material nonlinearities are proposed and used in the formulation of these elements. A computer program coded in FORTRAN was developed to perform current finite element static analysis with considering four cases of elements stiffness matrix determination. The results are compared with the experimental data available in literature in terms of central deflections, strains, and failure form, good agreement was found. Suitable outcomes have been observed in present static analysis with using of tangential stiffness matrix and stiffness matrix in second iteration of the load increment.

  14. Statistical Projections for Multi-resolution, Multi-dimensional Visual Data Exploration and Analysis

    Energy Technology Data Exchange (ETDEWEB)

    Nguyen, Hoa T. [Univ. of Utah, Salt Lake City, UT (United States); Stone, Daithi [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Bethel, E. Wes [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)

    2016-01-01

    An ongoing challenge in visual exploration and analysis of large, multi-dimensional datasets is how to present useful, concise information to a user for some specific visualization tasks. Typical approaches to this problem have proposed either reduced-resolution versions of data, or projections of data, or both. These approaches still have some limitations such as consuming high computation or suffering from errors. In this work, we explore the use of a statistical metric as the basis for both projections and reduced-resolution versions of data, with a particular focus on preserving one key trait in data, namely variation. We use two different case studies to explore this idea, one that uses a synthetic dataset, and another that uses a large ensemble collection produced by an atmospheric modeling code to study long-term changes in global precipitation. The primary findings of our work are that in terms of preserving the variation signal inherent in data, that using a statistical measure more faithfully preserves this key characteristic across both multi-dimensional projections and multi-resolution representations than a methodology based upon averaging.

  15. Multi-trace element levels and arsenic speciation in urine of e-waste recycling workers from Agbogbloshie, Accra in Ghana

    International Nuclear Information System (INIS)

    Asante, Kwadwo Ansong; Agusa, Tetsuro; Biney, Charles Augustus; Agyekum, William Atuobi; Bello, Mohammed; Otsuka, Masanari; Itai, Takaaki; Takahashi, Shin; Tanabe, Shinsuke

    2012-01-01

    To understand human contamination by multi-trace elements (TEs) in electrical and electronic waste (e-waste) recycling site at Agbogbloshie, Accra in Ghana, this study analyzed TEs and As speciation in urine of e-waste recycling workers. Concentrations of Fe, Sb, and Pb in urine of e-waste recycling workers were significantly higher than those of reference sites after consideration of interaction by age, indicating that the recycling workers are exposed to these TEs through the recycling activity. Urinary As concentration was relatively high, although the level in drinking water was quite low. Speciation analysis of As in human urine revealed that arsenobetaine and dimethylarsinic acid were the predominant As species and concentrations of both species were positively correlated with total As concentration as well as between each other. These results suggest that such compounds may be derived from the same source, probably fish and shellfish and greatly influence As exposure levels. To our knowledge, this is the first study on human contamination resulting from the primitive recycling of e-waste in Ghana. This study will contribute to the knowledge about human exposure to trace elements from an e-waste site in a less industrialized region so far scantly covered in the literature. - Highlights: ► Exposure status of trace elements in e-waste recycling workers was assessed in Ghana. ► Concentrations of Fe, Sb, and Pb in urine of e-waste workers were significantly higher than those of the reference subjects. ► This study is the first to investigate human contamination arising from primitive recycling of e-waste arguably from Africa.

  16. Multi-trace element levels and arsenic speciation in urine of e-waste recycling workers from Agbogbloshie, Accra in Ghana

    Energy Technology Data Exchange (ETDEWEB)

    Asante, Kwadwo Ansong [Center for Marine Environmental Studies (CMES), Ehime University, Bunkyo-cho 2-5, Matsuyama 790-8577 (Japan); CSIR Water Research Institute, P. O. Box AH 38, Achimota, Accra (Ghana); Agusa, Tetsuro [Center for Marine Environmental Studies (CMES), Ehime University, Bunkyo-cho 2-5, Matsuyama 790-8577 (Japan); Biney, Charles Augustus [Volta Basin Authority (VBA), 10 P. O. Box 13621, Ouagadougou 10 (Burkina Faso); Agyekum, William Atuobi; Bello, Mohammed [CSIR Water Research Institute, P. O. Box AH 38, Achimota, Accra (Ghana); Otsuka, Masanari [Center for Marine Environmental Studies (CMES), Ehime University, Bunkyo-cho 2-5, Matsuyama 790-8577 (Japan); Ehime Prefectural Institute of Public Health and Environmental Science, 8-234 Sanban-cho, Matsuyama 790-0003 (Japan); Itai, Takaaki; Takahashi, Shin [Center for Marine Environmental Studies (CMES), Ehime University, Bunkyo-cho 2-5, Matsuyama 790-8577 (Japan); Tanabe, Shinsuke, E-mail: shinsuke@agr.ehime-u.ac.jp [Center for Marine Environmental Studies (CMES), Ehime University, Bunkyo-cho 2-5, Matsuyama 790-8577 (Japan)

    2012-05-01

    To understand human contamination by multi-trace elements (TEs) in electrical and electronic waste (e-waste) recycling site at Agbogbloshie, Accra in Ghana, this study analyzed TEs and As speciation in urine of e-waste recycling workers. Concentrations of Fe, Sb, and Pb in urine of e-waste recycling workers were significantly higher than those of reference sites after consideration of interaction by age, indicating that the recycling workers are exposed to these TEs through the recycling activity. Urinary As concentration was relatively high, although the level in drinking water was quite low. Speciation analysis of As in human urine revealed that arsenobetaine and dimethylarsinic acid were the predominant As species and concentrations of both species were positively correlated with total As concentration as well as between each other. These results suggest that such compounds may be derived from the same source, probably fish and shellfish and greatly influence As exposure levels. To our knowledge, this is the first study on human contamination resulting from the primitive recycling of e-waste in Ghana. This study will contribute to the knowledge about human exposure to trace elements from an e-waste site in a less industrialized region so far scantly covered in the literature. - Highlights: Black-Right-Pointing-Pointer Exposure status of trace elements in e-waste recycling workers was assessed in Ghana. Black-Right-Pointing-Pointer Concentrations of Fe, Sb, and Pb in urine of e-waste workers were significantly higher than those of the reference subjects. Black-Right-Pointing-Pointer This study is the first to investigate human contamination arising from primitive recycling of e-waste arguably from Africa.

  17. Investigation of faulted tunnel models by combined photoelasticity and finite element analysis

    International Nuclear Information System (INIS)

    Ladkany, S.G.; Huang, Yuping

    1994-01-01

    Models of square and circular tunnels with short faults cutting through their surfaces are investigated by photoelasticity. These models, when duplicated by finite element analysis can predict the stress states of square or circular faulted tunnels adequately. Finite element analysis, using gap elements, may be used to investigate full size faulted tunnel system

  18. In-vivo elemental analysis at Birmingham 1968-1981

    International Nuclear Information System (INIS)

    Chettle, D.R.; Scott, M.C.

    1986-01-01

    Techniques have been developed to measure a number of elements in-vivo. Some have been measured by producing a radioactive isotope in the body by neutron bombardment and subsequently counting γ-rays given off during its decay. Measurements of calcium and sodium have been those most frequently used; copper, iron and phosphorus have also been measured in this way. Gamma-rays emitted 10 -18 s-10 -12 s following neutron capture have also been used for elemental analysis. This method, which involved detectors being in position by the subject during the neutron irradiation, has been widely applied to measurements of both nitrogen and cadmium. Preliminary studies of nuclear resonance scattering have suggested that this could be used for in-vivo elemental analysis, provided technical difficulties in source preparation could be overcome. Recently the use of X-ray fluorescence has been investigated for in-vivo analyses of lead in bone; the extension of this technique to measure mercury in the kidney is under consideration. (author)

  19. Discrimination of wine from grape cultivated in Japan, imported wine, and others by multi-elemental analysis.

    Science.gov (United States)

    Shimizu, Hideaki; Akamatsu, Fumikazu; Kamada, Aya; Koyama, Kazuya; Okuda, Masaki; Fukuda, Hisashi; Iwashita, Kazuhiro; Goto-Yamamoto, Nami

    2018-04-01

    Differences in mineral concentrations were examined among three types of wine in the Japanese market place: Japan wine, imported wine, and domestically produced wine mainly from foreign ingredients (DWF), where Japan wine has been recently defined by the National Tax Agency as domestically produced wine from grapes cultivated in Japan. The main objective of this study was to examine the possibility of controlling the authenticity of Japan wine. The concentrations of 18 minerals (Li, B, Na, Mg, Si, P, S, K, Ca, Mn, Co, Ni, Ga, Rb, Sr, Mo, Ba, and Pb) in 214 wine samples were determined by inductively coupled-plasma mass spectrometry (ICP-MS) and ICP-atomic emission spectrometry (ICP-AES). In general, Japan wine had a higher concentration of potassium and lower concentrations of eight elements (Li, B, Na, Si, S, Co, Sr, and Pb) as compared with the other two groups of wine. Linear discriminant analysis (LDA) models based on concentrations of the 18 minerals facilitated the identification of three wine groups: Japan wine, imported wine, and DWF with a 91.1% classification score and 87.9% prediction score. In addition, an LDA model for discrimination of wine from four domestic geographic origins (Yamanashi, Nagano, Hokkaido, and Yamagata Prefectures) using 18 elements gave a classification score of 93.1% and a prediction score of 76.4%. In summary, we have shown that an LDA model based on mineral concentrations is useful for distinguishing Japan wine from other wine groups, and can contribute to classification of the four main domestic wine-producing regions of Japan. Copyright © 2017 The Society for Biotechnology, Japan. Published by Elsevier B.V. All rights reserved.

  20. Nonlinear nonstationary analysis with the finite element method

    International Nuclear Information System (INIS)

    Vaz, L.E.

    1981-01-01

    In this paper, after some introductory remarks on numerical methods for the integration of initial value problems, the applicability of the finite element method for transient diffusion analysis as well as dynamic and inelastic analysis is discussed, and some examples are presented. (RW) [de

  1. Multi-trace elements level in drinking water and the prevalence of multi-chronic arsenical poisoning in residents in the west area of Iran

    International Nuclear Information System (INIS)

    Barati, A.H.; Maleki, A.; Alasvand, M.

    2010-01-01

    First, we determined the levels of 8 trace elements (As, Se, Hg, Cd, Ag, Mn, Cr and Pb) in 530 village drinking water sources by graphite furnace or flame atomic absorption spectroscopy method, in Kurdistan Province in the west of Iran. The results showed that the level of As, Cd and Se in 28 village drinking water sources exceeded WHO or National Standard limits. The levels of concentration of arsenic in drinking water ranged from 42 to 1500 μg/L. Then in a cross-sectional survey, 587 people from 211 households were chosen for clinical examinations of multi-chronic arsenical poisoning including pigment disorders, keratosis of palms and soles, Mee's line in fingers and nails and the gangrene as a systemic manifestation. Of 587 participants, 180 (30.7%) participants were affected by representing the type of chronic arsenical poisoning. The prevalence of Mee's line, keratosis, and pigment disorders were 86.1%, 77.2% and 67.8% respectively. Therefore, the prevalence of Mee's line between inhabitants was higher than the other disorders. The results show a strong linear relationship between arsenic exposure and occurrence of multi-chronic arsenical poisoning (R 2 = 0.76). The association between age for more than 40 years and gender for more than 60 years with chronic arsenical poisoning is significant (p < 0.05). Also, there is a relationship between subjects who were affected with disorders and duration of living in the village. Except for gangrene disorder, the odds ratio of prevalence of other disorders with arsenic exposure level in drinking water show a highly significant relationship between arsenic content and the risk of chronic disorders (p < 0.01). These results confirm the need to further study trace elements in drinking waters, food products and other samples in this area and the relationship to other chronic diseases arising out of arsenicosis.

  2. Adjusting to Social Change - A Multi-Level Analysis in Three Cultures

    Science.gov (United States)

    2013-08-01

    example, coping may be more collective in collectivist , compared to individualist , societies (Chang & Sivam, 2004). Some cultures have a greater sense...AFRL-AFOSR-UK-TR-2013-0041 Adjusting to Social Change - A multi-level Analysis in three cultures Prof Robin Goodwin...COVERED (From – To) 23 May 2012 – 22 May 2013 4. TITLE AND SUBTITLE Adjusting to Social Change - A multi-level Analysis in three cultures

  3. Determination of mutually interfering elements in activation analysis

    International Nuclear Information System (INIS)

    Figueiredo, A.M.G.

    1979-01-01

    The determination of the elements present in the groups scandium-zinc, mercury-selenium and arsenic-antimony-bromine represents a classical problem in thermal neutron activation analysis because the gamma-ray peaks of the radioisotopes produced from these elements by activation appear very close in the spectrum. A study is made of the possibility of simultaneous instrumental determination of these elements by means of the spectrum stripping technique, using a 400-channel analyser coupled to a Nal(Tl) detector and a 4096-channel analyser coupled to a Ge(Li) detector. Artificial mixtures of the interfering elements in varying proportions are prepared, so as to reproduce possible real samples, where the elements may be present at several concentrations. Radiochemical separation techniques for the cited elements are studied with the use of tracers. For the separation of scadium and zinc, the technique of extraction chromatography is applied. The separation of mercury and selenium is accomplished by means of ion exchange. The technique of coprecipitation is used to separate bromine from arsenic and antimony followed by ion exchange to isolate these two elements from each other. The precision and the accuracy of the results are discussed. (Author) [pt

  4. Proposal for element size and time increment selection guideline by 3-D finite element method for elastic waves propagation analysis

    International Nuclear Information System (INIS)

    Ishida, Hitoshi; Meshii, Toshiyuki

    2008-01-01

    This paper proposes a guideline for selection of element size and time increment by 3-D finite element method, which is applied to elastic wave propagation analysis for a long distance of a large structure. An element size and a time increment are determined by quantitative evaluation of strain, which must be 0 on the analysis model with a uniform motion, caused by spatial and time discretization. (author)

  5. OpenSeesPy: Python library for the OpenSees finite element framework

    Science.gov (United States)

    Zhu, Minjie; McKenna, Frank; Scott, Michael H.

    2018-01-01

    OpenSees, an open source finite element software framework, has been used broadly in the earthquake engineering community for simulating the seismic response of structural and geotechnical systems. The framework allows users to perform finite element analysis with a scripting language and for developers to create both serial and parallel finite element computer applications as interpreters. For the last 15 years, Tcl has been the primary scripting language to which the model building and analysis modules of OpenSees are linked. To provide users with different scripting language options, particularly Python, the OpenSees interpreter interface was refactored to provide multi-interpreter capabilities. This refactoring, resulting in the creation of OpenSeesPy as a Python module, is accomplished through an abstract interface for interpreter calls with concrete implementations for different scripting languages. Through this approach, users are able to develop applications that utilize the unique features of several scripting languages while taking advantage of advanced finite element analysis models and algorithms.

  6. Multi-criteria multi-stakeholder decision analysis using a fuzzy-stochastic approach for hydrosystem management

    Science.gov (United States)

    Subagadis, Y. H.; Schütze, N.; Grundmann, J.

    2014-09-01

    The conventional methods used to solve multi-criteria multi-stakeholder problems are less strongly formulated, as they normally incorporate only homogeneous information at a time and suggest aggregating objectives of different decision-makers avoiding water-society interactions. In this contribution, Multi-Criteria Group Decision Analysis (MCGDA) using a fuzzy-stochastic approach has been proposed to rank a set of alternatives in water management decisions incorporating heterogeneous information under uncertainty. The decision making framework takes hydrologically, environmentally, and socio-economically motivated conflicting objectives into consideration. The criteria related to the performance of the physical system are optimized using multi-criteria simulation-based optimization, and fuzzy linguistic quantifiers have been used to evaluate subjective criteria and to assess stakeholders' degree of optimism. The proposed methodology is applied to find effective and robust intervention strategies for the management of a coastal hydrosystem affected by saltwater intrusion due to excessive groundwater extraction for irrigated agriculture and municipal use. Preliminary results show that the MCGDA based on a fuzzy-stochastic approach gives useful support for robust decision-making and is sensitive to the decision makers' degree of optimism.

  7. PUMA Development through a Multi physics Approach

    International Nuclear Information System (INIS)

    Cheon, Jinsik; Kim, Junehyung; Lee, Byoungoon; Lee, Chanbock

    2013-01-01

    Meanwhile advances of numerical methods make it possible for the multi physics problem to be solved in a fully coupled way. In addition to a multidimensional, multi physical approach, a nuclear fuel performance analysis code, which is 1D code, should be improved by accommodating the state-of-the-art in the numerical analysis to support current fuel design and performance analysis. In particular, the coupling between the mechanical equilibrium equation and a set of numerically stiff kinetics equations for fission gas release is of great importance for a multi physics simulation of nuclear fuel. Instead, coupling between temperature and fuel constituent was found to be made with a relative ease by employing an ordinary differential equations solver. As an effort for a new SFR metal fuel performance analysis code, called PUMA (Performance of Uranium Metal fuel rod Analysis code), the deformation of U-Zr fuel for SFR in connection with a fission gas release model is analyzed. A finite element analyses for purely mechanical problems are performed using a backward differentiation formula, and are subjected to scrupulous verification with Abaqus. Then mechanical equilibrium equation and the equations for fission gas release are coupled with the same differential-algebraic equations (DAE) solver

  8. Determination of some trace elements in biological samples using XRF and TXRF techniques

    International Nuclear Information System (INIS)

    Khuder, A.; Karjou, J.; Sawan, M. K.

    2006-07-01

    XRF and TXRF techniques were successfully used for the multi-element determination of trace elements in whole blood and human head hair samples. This was achieved by the direct analysis using XRF technique with different collimation units and by the optimized chemical procedures for TXRF analysis. Light element of S and P were preferably determined by XRF with primary x-ray excitation, while, elements of K, Ca, Fe, and Br were determined with a very good accuracy and precision using XRF with Cu- and Mo-secondary targets. The chemical procedure dependent on the preconcentration of trace elements by APDC was superiorly used for the determination of traces of Ni and Pb in the range of 1.0-1.7 μg/dl and 11-23 μg/dl, respectively, in whole blood samples by TXRF technique; determination of other elements as Cu and Zn was also achievable using this approach. Rb in whole blood samples was determined directly after the digestion of samples using PTFE-bomb for TXRF analysis. (author)

  9. Accuracy of multi-point boundary crossing time analysis

    Directory of Open Access Journals (Sweden)

    J. Vogt

    2011-12-01

    Full Text Available Recent multi-spacecraft studies of solar wind discontinuity crossings using the timing (boundary plane triangulation method gave boundary parameter estimates that are significantly different from those of the well-established single-spacecraft minimum variance analysis (MVA technique. A large survey of directional discontinuities in Cluster data turned out to be particularly inconsistent in the sense that multi-point timing analyses did not identify any rotational discontinuities (RDs whereas the MVA results of the individual spacecraft suggested that RDs form the majority of events. To make multi-spacecraft studies of discontinuity crossings more conclusive, the present report addresses the accuracy of the timing approach to boundary parameter estimation. Our error analysis is based on the reciprocal vector formalism and takes into account uncertainties both in crossing times and in the spacecraft positions. A rigorous error estimation scheme is presented for the general case of correlated crossing time errors and arbitrary spacecraft configurations. Crossing time error covariances are determined through cross correlation analyses of the residuals. The principal influence of the spacecraft array geometry on the accuracy of the timing method is illustrated using error formulas for the simplified case of mutually uncorrelated and identical errors at different spacecraft. The full error analysis procedure is demonstrated for a solar wind discontinuity as observed by the Cluster FGM instrument.

  10. Fast XRF analysis of mineral elements in dental composites

    International Nuclear Information System (INIS)

    Preoteasa, E. A.; Constantinescu, B.; Preoteasa, E.

    2001-01-01

    Dental composites, made of particles of glass, ceramics or quartz embedded in an organic polymer matrix, extensively replaced silver amalgam in tooth fillings and enabled new applications for restorative dentistry. Long-term alteration of dental fillings together with market pressure motivates the development of composites at a high rate, largely by progress of materials forming their mineral phase. Therefore, dental composites constantly bring at the interface with enamel and dentine new elements foreign to the organism, whose biological action has not been studied. Atomic and nuclear methods for surface multielemental analysis have been used in dental research but not for composites. X-ray fluorescence (XRF) is suited for the fast microanalytical screening of the elements and of their changes at the biomaterial's surface. The potential of radioisotope-excited XRF for the analysis of dental composites has been examined. Flat disk-shaped samples of composites have been prepared and polymerized chemically or by irradiation with intense 420-500 nm light. The measurements were performed with a spectrometric chain containing a 30 mCi source of 241 Am, a Si(Li) detector, and a multichannel analyzer. The spectra were built up for 2000-6000 sec. The characteristic X lines were integrated and normalized to source lines. The following Z ≥ 20 elements were detected in the studied composites: Ba only in Charisma (Kulzer) and Pekafill (Bayer); Zr, Ba, Yb in Tetric Ceram, and Ca, Ba, Yb together with traces of possibly Ti and Fe in Ariston (both from Vivadent); Zr, Hf in Valux Plus (3M Dental); and Sr, Ba together with some trace element, seemingly Cu, in F2000 Compomer (3M Dental) and with other trace elements like Ca, Fe in Surefil (Dentsply). Among older materials, Concise (3M Dental) contained only light (Z 3 that releases F for protection of enamel and dentine. Yb, Zr, Ba, Hf improve the radiological opacity of the materials. Some elements may accompany others as

  11. Medical and health-related trace element analysis by TXRF

    International Nuclear Information System (INIS)

    Greaves, E.D.

    2000-01-01

    The advantages offered with TXRF analysis by direct irradiation with monochromatic X-rays of tissue homogenates and body fluids make the technique appropriate for a number of medical and health related applications. The ability to detect low levels of toxic heavy elements is being used as an aid in accidental poisoning diagnosis and treatment, in treatment-induced toxicity control and as an accessory in medical and health research. Thus lead-in-whole-blood analysis is used in confirmation of diagnosis of victims of poisoning, or monitoring the evolution and efficiency of the clinical treatment. Measurement and control of plasma platinum levels of cancer patients undergoing chemotherapy with Pt-containing drugs includes: establishment of the drug level-tumor remission response, measurement of Pt plasma level curves and establishment of optimum dosage to minimize the nephrotoxicity of platinum, and bioequivalence comparisons of different commercially available platinum containing anticancer drugs. Analysis as an aid in clinical research applications includes: trace element determination of amniotic fluid in fetus malformation studies; analysis of brain specimens and cerebrospinal fluid in diagnosis of central nervous system disorders; the influence of trace elements in cataract genesis and the influence of heavy elements in semen quality in human reproduction studies. Human body samples require the use of monochromatized beams of x-rays in order to derive the special advantage of its use: i) The reduction in the spectrum background allowing direct irradiation of organic matter specimens. Hence human tissue and body fluids are prepared by simple procedures involving dilution, homogenization and standard addition avoiding the need for specimen digestion. This results in faster, cheaper methods that decrease sample contamination problems. ii) The presence of a large Compton scattered signal in the spectrum and its use as an internal standard reference allows further

  12. Finite element stress analysis of brick-mortar masonry under ...

    African Journals Online (AJOL)

    Stress analysis of a brick-mortar couplet as a substitute for brick wall structure has been performed by finite element method, and algorithm for determining the element stiffness matrix for a plane stress problem using the displacement approach was developed. The nodal displacements were derived for the stress in each ...

  13. Multi-recycling of transuranic elements in a PWR assembly with reduced fuel rod diameter

    Energy Technology Data Exchange (ETDEWEB)

    Chambers, Alex, E-mail: acchamb@gmail.com; Ragusa, Jean C., E-mail: jean.ragusa@tamu.edu

    2014-04-01

    Highlights: • Study of multiple recycling passes of transuranic elements: (a) without exceeding 5 wt.% on U-235 enrichment; (b) using PWR fuel assemblies compatible with current reactor core internals. • Isotopic concentrations tend towards an equilibrium after 15 recycle passes, suggesting that thermal recycling may be continued beyond that point. • Radiotoxicity comparisons for once-through UOX, once-recycle MOX-Pu, and multiple recycle passes of MOX-PuNpAm and MOX-PuNpAmCm are presented. - Abstract: This paper examines the multi-recycling of transuranic (TRU) elements (Pu-Np-Am-Cm) in standard Pressurized Water Reactor (PWR) assemblies. The original feed of TRU comes from legacy spent UOX fuel. For all subsequent recycling passes, TRU elements from the previous generation are employed, supplemented by TRU from legacy UOX fuel, as needed. The design criteria include: {sup 235}U enrichment requirements to remain below 5 w/o, TRU loading limits to avoid return to criticality under voided conditions, and assembly power peaking factors. In order to carry out multiple recycling passes within the design envelope, additional neutron moderation is required and achieved by reducing the fuel pellet diameter by about 13%, thus keeping the assembly design compatible with current PWR core internals. TRU transmutation rates and long-term ingestion radiotoxicity results are presented for 15 recycling passes and compared to standard UOX and MOX once-through cycles. The results also show that TRU fuel isotopics and radiotoxicity tend towards an equilibrium, enabling further additional recycling passes.

  14. Investigation of Shear Stud Performance in Flat Plate Using Finite Element Analysis

    Directory of Open Access Journals (Sweden)

    T.S. Viswanathan

    2014-09-01

    Full Text Available Three types of shear stud arrangement, respectively featuring an orthogonal, a radial and a critical perimeter pattern, were evaluated numerically. A numerical investigation was conducted using the finite element software ABAQUS to evaluate their ability to resist punching shear in a flat plate. The finite element analysis here is an application of the nonlinear analysis of reinforced concrete structures using three-dimensional solid finite elements. The nonlinear characteristics of concrete were achieved by employing the concrete damaged plasticity model in the finite element program. Transverse shear stress was evaluated using finite element analysis in terms of shear stress distribution for flat plate with and without shear stud reinforcement. The model predicted that shear studs placed along the critical perimeter are more effective compared to orthogonal and radial patterns.

  15. Proton induced X-Ray fluorescence study as a tool trace element analysis

    International Nuclear Information System (INIS)

    El-Kady, Ahmed A.

    1978-01-01

    Usefulness and limitations of trace elemental analysis by high energy charged particles and photon induced X-ray have been discussed. Comparison with the well established neutron activation analysis technique is also given. Back-ground radiation due to bremsstrahlung from secondary electrons and due to charged particle bremsstrahlung have been reviewed for different projectiles. The sensitivity of elemental analysis by proton induced X-ray fluorescence have been examined by measuring the characteristic X-ray emission cross section for K and L transitions of many elements and for different proton energies and compared with theroretical values. The discussion given in this report show that with suitable proton generator and a high resolution X-ray detector, proton X-ray fluorescence technique is capable of analyzing many elements simultaneously at the part per million level and offers a rapid and reliable method for trace element analysis. Data on water, blood and tissue samples given in this report are few examples of many possible applications

  16. Trace elements in Australian opals using neutron activation analysis

    International Nuclear Information System (INIS)

    McOrist, G.D.; Fardy, J.J.

    1994-01-01

    Neutron activation analysis was used to determine the concentration of trace elements in 42 samples of black, grey and white opals taken from a number of recognised Australian field. The results were evaluated to determine if a relationship exited between trace element content and opal colour. (author) 12 refs.; 12 figs.; 3 tabs

  17. Multi-level approach for parametric roll analysis

    Science.gov (United States)

    Kim, Taeyoung; Kim, Yonghwan

    2011-03-01

    The present study considers multi-level approach for the analysis of parametric roll phenomena. Three kinds of computation method, GM variation, impulse response function (IRF), and Rankine panel method, are applied for the multi-level approach. IRF and Rankine panel method are based on the weakly nonlinear formulation which includes nonlinear Froude- Krylov and restoring forces. In the computation result of parametric roll occurrence test in regular waves, IRF and Rankine panel method show similar tendency. Although the GM variation approach predicts the occurrence of parametric roll at twice roll natural frequency, its frequency criteria shows a little difference. Nonlinear roll motion in bichromatic wave is also considered in this study. To prove the unstable roll motion in bichromatic waves, theoretical and numerical approaches are applied. The occurrence of parametric roll is theoretically examined by introducing the quasi-periodic Mathieu equation. Instability criteria are well predicted from stability analysis in theoretical approach. From the Fourier analysis, it has been verified that difference-frequency effects create the unstable roll motion. The occurrence of unstable roll motion in bichromatic wave is also observed in the experiment.

  18. Elemental analysis of hair using PIXE-tomography and INAA

    International Nuclear Information System (INIS)

    Beasley, D.; Gomez-Morilla, I.; Spyrou, N.

    2008-01-01

    3D quantitative elemental maps of a section of a strand of hair were produced using a combination of PIXE-Tomography and simultaneous On/Off Axis STIM-Tomography at the University of Surrey Ion Beam Centre. The distributions of S, K, Cl, Ca, Fe and Zn were determined using the PIXE-T reconstruction package DISRA. The results were compared with conventional bulk PIXE analysis of tomographic data as determined using Dan32. The overall concentrations determined by PIXE were compared with elemental concentrations held in the University of Surrey Hair Database. All the entries currently in the database were produced using INAA. The merits and possible contributions of tomographic PIXE analysis to analysis of hair are discussed. The conclusions drawn from the PIXE-Tomography analysis can be used to argue for more stringent procedures for hair analysis at the University of Surrey. (author)

  19. Multi-dimensional Code Development for Safety Analysis of LMR

    International Nuclear Information System (INIS)

    Ha, K. S.; Jeong, H. Y.; Kwon, Y. M.; Lee, Y. B.

    2006-08-01

    A liquid metal reactor loaded a metallic fuel has the inherent safety mechanism due to the several negative reactivity feedback. Although this feature demonstrated through experiments in the EBR-II, any of the computer programs until now did not exactly analyze it because of the complexity of the reactivity feedback mechanism. A multi-dimensional detail program was developed through the International Nuclear Energy Research Initiative(INERI) from 2003 to 2005. This report includes the numerical coupling the multi-dimensional program and SSC-K code which is used to the safety analysis of liquid metal reactors in KAERI. The coupled code has been proved by comparing the analysis results using the code with the results using SAS-SASSYS code of ANL for the UTOP, ULOF, and ULOHS applied to the safety analysis for KALIMER-150

  20. Multi-element analyses of earthworms for radioecology and ecotoxicology

    International Nuclear Information System (INIS)

    Yoshida, S.; Peijnenburg, W.; Muramatsu, Y.

    2004-01-01

    Increasing concern about environmental radiation protection has raised awareness that more information is required on the transfer and accumulation of radionuclides in the biological compartments of ecosystems. ICRP (International Commission on Radiological Protection) selected earthworm as one of the reference organisms in their radiation protection recommendations. Earthworms play an important role in ecosystems, and might be a good indicator of soil contamination and its effect on the ecosystem. The elemental composition of earthworms gives useful information on background levels and possible accumulation of metals as well as related radionuclides. In addition, a change of the elemental composition itself might be a possible indicator of the effect on the earthworm and/or ecosystem. However, data for the elemental composition of earthworms are limited except for some specific heavy metals such as Cd, Zn, Pb and Cu. In this study, earthworms and their growth media were analyzed for more than 30 elements, including radionuclide related elements such as Cs, Sr, Th and U, in order to obtain the basic information on the transfer parameters of the elements. The earthworms analyzed were fed in the laboratory or collected in the environment. The concentrations and transfer factors of the elements were determined both for laboratory and natural conditions. The controlling factors on the transfer parameters such as the bioavailability of the elements in the soils will also be discussed. (author)

  1. Extended depth of field integral imaging using multi-focus fusion

    Science.gov (United States)

    Piao, Yongri; Zhang, Miao; Wang, Xiaohui; Li, Peihua

    2018-03-01

    In this paper, we propose a new method for depth of field extension in integral imaging by realizing the image fusion method on the multi-focus elemental images. In the proposed method, a camera is translated on a 2D grid to take multi-focus elemental images by sweeping the focus plane across the scene. Simply applying an image fusion method on the elemental images holding rich parallax information does not work effectively because registration accuracy of images is the prerequisite for image fusion. To solve this problem an elemental image generalization method is proposed. The aim of this generalization process is to geometrically align the objects in all elemental images so that the correct regions of multi-focus elemental images can be exacted. The all-in focus elemental images are then generated by fusing the generalized elemental images using the block based fusion method. The experimental results demonstrate that the depth of field of synthetic aperture integral imaging system has been extended by realizing the generation method combined with the image fusion on multi-focus elemental images in synthetic aperture integral imaging system.

  2. Credible baseline analysis for multi-model public policy studies

    Energy Technology Data Exchange (ETDEWEB)

    Parikh, S.C.; Gass, S.I.

    1981-01-01

    The nature of public decision-making and resource allocation is such that many complex interactions can best be examined and understood by quantitative analysis. Most organizations do not possess the totality of models and needed analytical skills to perform detailed and systematic quantitative analysis. Hence, the need for coordinated, multi-organization studies that support public decision-making has grown in recent years. This trend is expected not only to continue, but to increase. This paper describes the authors' views on the process of multi-model analysis based on their participation in an analytical exercise, the ORNL/MITRE Study. One of the authors was the exercise coordinator. During the study, the authors were concerned with the issue of measuring and conveying credibility of the analysis. This work led them to identify several key determinants, described in this paper, that could be used to develop a rating of credibility.

  3. Detecting bots using multi-level traffic analysis

    DEFF Research Database (Denmark)

    Stevanovic, Matija; Pedersen, Jens Myrup

    2016-01-01

    introduces a novel multi-level botnet detection approach that performs network traffic analysis of three protocols widely considered as the main carriers of botnet Command and Control (C&C) and attack traffic, i.e. TCP, UDP and DNS. The proposed method relies on supervised machine learning for identifying...

  4. A procedure for multi-objective optimization of tire design parameters

    Directory of Open Access Journals (Sweden)

    Nikola Korunović

    2015-04-01

    Full Text Available The identification of optimal tire design parameters for satisfying different requirements, i.e. tire performance characteristics, plays an essential role in tire design. In order to improve tire performance characteristics, formulation and solving of multi-objective optimization problem must be performed. This paper presents a multi-objective optimization procedure for determination of optimal tire design parameters for simultaneous minimization of strain energy density at two distinctive zones inside the tire. It consists of four main stages: pre-analysis, design of experiment, mathematical modeling and multi-objective optimization. Advantage of the proposed procedure is reflected in the fact that multi-objective optimization is based on the Pareto concept, which enables design engineers to obtain a complete set of optimization solutions and choose a suitable tire design. Furthermore, modeling of the relationships between tire design parameters and objective functions based on multiple regression analysis minimizes computational and modeling effort. The adequacy of the proposed tire design multi-objective optimization procedure has been validated by performing experimental trials based on finite element method.

  5. Simultaneous Multi-Element Electrothermal Atomic Absorption ...

    African Journals Online (AJOL)

    width of transmittance profile 120 pm, a linear CCD array attached to a PC and a tube atomizer furnished with a carbon fibre collector. In the experiments simultaneous determination of 18 elements was performed in the mixed solutions at the mg ...

  6. Three-dimensional fabric analysis for anisotropic material using multi-directional scanning line. Application to x-ray CI image

    International Nuclear Information System (INIS)

    Takemura, Takato; Takahashi, Manabu; Oda, Masanobu; Hirai, Hidekazu; Murakoshi, Atsushi; Miura, Makoto

    2007-01-01

    In microscopic analysis, materials are characterized by a three-dimensional (3D) microstructure which is composed of constituent elements such as pores, voids and cracks. A material's mechanical and hydrological properties are strongly dependent on its microstructure. In order to discuss the mechanics of geomaterials on a microstructural level, detailed information on their 3D macrostructure is required. X-ray computed tomography is a powerful non-destructive method for determining the microstructure, however it can be difficult to determine a material's microstructure from the reconstructed 3D image. We successfully evaluated the 3D microstructural anisotropy of porous and fibrous materials using a multi-directional scanning line method that employs straightforward image analysis, and its results were visualized using stereonet projection. (author)

  7. Development and utilization of irradiational capsule - Mechanical and thermal performance analysis and development of design program on the cylindrical structures with multi-holes

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Young Shin; Choi, M. H.; Shin, D. S. [Chungnam National University, Taejon (Korea)

    2000-04-01

    Irradiation tests in the research reactor are used with the specially designed capsules for irradiation test and loop. Accordingly, suitable instrumented capsule for HANARO must be designed and manufactured. To satisfy the requirements of users and to conduct irradiation test effectively, the accurate informations on the thermal and mechanical characteristics of capsule should be understood. The structural analysis results show that stress characteristics of the cylinder with multi-holes is not significantly effected by the sizes of specimen hole, numbers of specimen and eccentric characteristics. The thermal and structural analysis of the capsule with multi-holes under thermal loading shows that the peak temperature in the circular cylinder is occurred in the specimens inserted in the center or specimen holes and is significantly effected by gap size between the holder and the external tube. In this study, CAPSYS program is developed by interfacing finite element analysis program, ANSYS with graphic user interface program, VISUAL C++. This program will be useful on the design and safety analysis of the capsule for material irradiation test. 20 refs., 37 figs., 9 tabs. (Author)

  8. Elemental content of Vietnamese rice. Part 2. Multivariate data analysis.

    Science.gov (United States)

    Kokot, S; Phuong, T D

    1999-04-01

    Rice samples were obtained from the Red River region and some other parts of Vietnam as well as from Yanco, Australia. These samples were analysed for 14 elements (P, K, Mg, Ca, Mn, Zn, Fe, Cu, Al, Na, Ni, As, Mo and Cd) by ICP-AES, ICP-MS and FAAS as described in Part 1. This data matrix was then submitted to multivariate data analysis by principal component analysis to investigate the influences of environmental and crop cultivation variables on the elemental content of rice. Results revealed that geographical location, grain variety, seasons and soil conditions are the most likely significant factors causing changes in the elemental content between the rice samples. To assess rice quality according to its elemental content and physio-biological properties, a multicriteria decision making method (PROMETHEE) was applied. With the Vietnamese rice, the sticky rice appeared to contain somewhat higher levels of nutritionally significant elements such as P, K and Mg than the non-sticky rice. Also, rice samples grown during the wet season have better levels of nutritionally significant mineral elements than those of the dry season, but in general, the wet season seemed to provide better overall elemental and physio-biological rice quality.

  9. Thermo-mechanical analysis for multi-level HLW repository concept

    International Nuclear Information System (INIS)

    Kwon, Sang Ki; Choi, Jong Won

    2004-01-01

    This work aims to investigate the influence of design parameters for the underground high-level nuclear waste repository with multi-level concept. B. Necessity o In order to construct an HLW repository in deep underground, it is required to select a site, which is far from major discontinuities. To dispose the whole spent fuels generated from the Korean nuclear power plants in a repository, the underground area of about 4km 2 is required. This would be a constraints for selecting an adequate repository site. It is recommended to dispose the two different spent fuels, PWR and CANDU, in different areas at the operation efficiency point of view. It is necessary to investigate the influence of parameters, which can affect the stability of multi-level repository. It is also needed to consider the influence of heat generated from the HLW and the high in situ stress in deep location. Therefore, thermo-mechanical coupling analysis should be carried out and the results should be compared with the results from single-level repository concept. Three-dimensional analysis is required to model the disposal tunnel and deposition hole. It is recommended to use the Korean geological condition and actually measured rock properties in Korea in order to achieve reliable modeling results. A FISH routine developed for effective modeling of Thermal-Mechanical coupling was implemented in the modeling using FLAC3D, which is a commercial three-dimensional FDM code. The thermal and mechanical properties of rock and rock mass achieved from Yusung drilling site, were used for the computer modeling. Different parameters such as level distance, waste type disposed on different levels, and time interval between the operation on different levels, were considered in the three-dimensional analysis. From the analysis, it was possible to derive adequate multi-level repository concept. Results and recommendations for application From the thermal-mechanical analysis for the multi-level repository

  10. Advanced chemical analysis service for elements, radionuclides and phases

    International Nuclear Information System (INIS)

    Sansoni, B.

    1986-01-01

    A review is given on the structure, organisation and performance of the chemical analysis service of the Central Department for Chemical Analysis at the Kernforschungsanlage Juelich GmbH. The research and development programs together with the infrastructure of the Centre afford to analyse almost all stable elements of the periodical table in almost any material. The corresponding chemical analysis service has been organized according to a new modular system of analytical steps. According to this, the most complicated and, therefore, most general case of an analytical scheme for element and radionuclide analysis in any type of material can be differentiated into about 14 different steps, the modules. They are more or less independent of the special problem. The laboratory is designed and organized according to these steps. (orig./PW) [de

  11. COMPARATIVE ANALYSIS OF INNOVATION ASPECT EVIDENCE IN CONSTRUCTION AND MULTI-SECTOR COMPANIES

    OpenAIRE

    Ricardo Floriani; Ilse Maria Beuren; Nelson Hein

    2010-01-01

    The goal of this study is to make a comparative analysis of innovation aspect evidence among construction and multi-sector companies. Descriptive research was done through a content analysis of administration reports from 2005 to 2007. From the researched material, 14 aspects of innovations were extracted, which offer the basis to the content analysis. Two non-probability samples were developed, the first consisting of 22 multi-sector businesses, within 18 economic sectors, which comprises th...

  12. LASER SPECTROSCOPY AND TRACE ELEMENT ANALYSIS Chapter from the Energy and Environment Division Annual Report 1980

    Energy Technology Data Exchange (ETDEWEB)

    Various, Authors

    1981-05-01

    In order to control pollutants resulting from energy production and utilization, adequate methods are required for monitoring the level of various substances often present at low concentrations. The Energy and Environment Division Applied Research in Laser Spectroscopy & Analytical Techniques Program is directed toward meeting these needs, Emphasis is on the development of physical methods, as opposed to conventional chemical analysis techniques. The advantages, now widely recognized, include ultra-high sensitivity coupled with minimal sample preparation. In some instances physical methods provide multi-parameter measurements which often provide the only means of achiev·ing the sensitivity necessary for the detection of trace contaminants. Work is reported in these areas: APPLIED PHYSICS AND LASER SPECTROSCOPY RESEARCH; MICROPROCESSOR CONTROLLER ANODIC STRIPPING VOLTAMETER FOR TRACE METALS ANALYSIS IN WATER; THE SURVEY OF INSTRUMENTATION FOR ENVIRONMENTAL MONITORING; THE POSSIBLE CHRONDRITIC NATURE OF THE DANISH CRETACEOUS~TERTIARY BOUNDARY; IMPROVEMENT OF THE SENSITIVITY AND PRECISION OF NEUTRON ACTIVATION ANALYSIS OF SOME ELEMENTS IN PLANKTON AND PLANKTONIC FISH; and SOURCES OF SOME SECONDARILY WORKED OBSIDIAN ARTIFACTS FROM TIKAL, GUATEMALA.

  13. Element analysis of Japanese traditional papers by PIXE method

    International Nuclear Information System (INIS)

    Suzuki, Tatsuya; Yasuda, Keisuke; Tani, Teruhiro

    2000-01-01

    The Japanese papers, 'washi', are made from the bast fibers of the plants. Since washi have the informations of the raw material plants, there is potentiality of the identification of the production place by the element analysis of the washi. Three kinds of washi made of kozo, which have different habitats, were prepared. The elements in their washi were measured by the PIXE. It was confirmed that the amount of elements included in the washi depend on the habitats of their raw material plants. (author)

  14. Using Spatial Multi-Criteria Analysis and Ranking Tool (SMART in earthquake risk assessment: a case study of Delhi region, India

    Directory of Open Access Journals (Sweden)

    Nishant Sinha

    2016-03-01

    Full Text Available This article is aimed at earthquake hazard, vulnerability and risk assessment as a case study to demonstrate the applicability of Spatial Multi-Criteria Analysis and Ranking Tool (SMART, which is based on Saaty's multi-criteria decision analysis (MCDA technique. The three specific study sites of Delhi were chosen for research as it corresponds to a typical patch of the urban environs, completely engrossed with residential, commercial and industrial units. The earthquake hazard affecting components are established in the form of geographic information system data-set layers including seismic zone, peak ground acceleration (PGA, soil characteristics, liquefaction potential, geological characteristics, land use, proximity to fault and epicentre. The physical vulnerability layers comprising building information, namely number of stories, year-built range, area, occupancy and construction type, derived from remote sensing imagery, were only considered for the current research. SMART was developed for earthquake risk assessment, and weights were derived both at component and its element level. Based on weighted overlay techniques, the earthquake hazard and vulnerability layers were created from which the risk maps were derived through multiplicative analysis. The developed risk maps may prove useful in decision-making process and formulating risk mitigation measures.

  15. Numerical solutions of multi-dimensional solidification/melting problems by the dual reciprocity boundary element method

    International Nuclear Information System (INIS)

    Jo, Jong Chull; Shin, Won Ky

    1997-01-01

    This paper presents an effective and simple procedure for the simulation of the motion of the solid-liquid interfacial boundary and the transient temperature field during phase change process. To accomplish this purpose, an iterative implicit solution algorithm has been developed by employing the dual reciprocity boundary element method. The dual reciprocity boundary element approach provided in this paper is much simpler than the usual boundary element method applying a reciprocity principle and an available technique for dealing with domain integral of boundary element formulation simultaneously. The effectiveness of the present analysis method have been illustrated through comparisons of the calculation results of an example with its semi-analytical or other numerical solutions where available

  16. Multi-element sewer slime impact pattern--a quantitative characteristic enabling identification of the source of heavy metal discharges into sewer systems.

    Science.gov (United States)

    Kintrup, J; Wünsch, G

    2001-11-01

    The capability of sewer slime to accumulate heavy metals from municipal wastewater can be exploited to identify the sources of sewage sludge pollution. Former investigations of sewer slime looked for a few elements only and could, therefore, not account for deviations of the enrichment efficiency of the slime or for irregularities from sampling. Results of ICP-MS multi element determinations were analyzed by multivariate statistical methods. A new dimensionless characteristic "sewer slime impact" is proposed, which is zero for unloaded samples. Patterns expressed in this data format specifically extract the information required to identify the type of pollution and polluter quicker and with less effort and cost than hitherto.

  17. PIXE analysis of trace and other mineral elements in phytopharmaceutical drugs

    International Nuclear Information System (INIS)

    Preoteasa, E. A.; Harangus, Livia; Iordan, Andreea; Gugiu, M.

    2002-01-01

    Despite of ongoing progress in the biochemistry of phytopharmaceutical drugs, their mineral micro- and trace elements have not been studied in detail. These elements may have therapeutic or toxic activity which should be assessed by sensitive investigations. The latter can be done by multielemental analysis with nuclear and atomic methods. We previously found 28 elements in some Romanian plant drugs by nuclear activation analysis. The availability of this method is, however, limited by the access to a nuclear reactor. Particle-induced X-ray emission (PIXE) is an alternative method with high performances in biomedicine and requiring no sample preparation for drugs' studies. We applied PIXE in the qualitative analysis of three plant drugs - Liv52, Mentat, and Geriforte - used as invigorators, protectors and prophylactics in oxidative stress diseases. Measurements with 3 MeV protons at the 8.5 MV NIPNE-HH (Horia Hulubei National Institute for Physics and Nuclear Engineering) tandem accelerator, using a hyper-pure Ge detector and no additional absorber foil, evidenced unusually complex elemental compositions of drugs. Up to 31 elements with Z > 15 were found: P, S, Cl, K, Ca, Sc, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ga, Br, Rb, Sr, Y, Zr, Cs, Ba, La, Ce, Pr, Nd, Sm, Eu, Hg, and As and/or Pb, from major to trace levels. The three drugs' qualitative composition were found to be rather similar. Relative concentrations were well evaluated with X-ray yields calculated for another kind of light element thick target. Drug's toxic elements - As and/or Pb, Hg, and possibly Ga - were all at trace levels, but their accumulation might be harmful. Some essential elements like K, Ca, Cr, Fe, Cu, Zn, Br, Rb, Sr can be biologically useful. X-ray yields improvement and other ways for PIXE quantitative analysis of the phytotherapeutic drugs are outlined. (authors)

  18. Beyond reliability, multi-state failure analysis of satellite subsystems: A statistical approach

    International Nuclear Information System (INIS)

    Castet, Jean-Francois; Saleh, Joseph H.

    2010-01-01

    Reliability is widely recognized as a critical design attribute for space systems. In recent articles, we conducted nonparametric analyses and Weibull fits of satellite and satellite subsystems reliability for 1584 Earth-orbiting satellites launched between January 1990 and October 2008. In this paper, we extend our investigation of failures of satellites and satellite subsystems beyond the binary concept of reliability to the analysis of their anomalies and multi-state failures. In reliability analysis, the system or subsystem under study is considered to be either in an operational or failed state; multi-state failure analysis introduces 'degraded states' or partial failures, and thus provides more insights through finer resolution into the degradation behavior of an item and its progression towards complete failure. The database used for the statistical analysis in the present work identifies five states for each satellite subsystem: three degraded states, one fully operational state, and one failed state (complete failure). Because our dataset is right-censored, we calculate the nonparametric probability of transitioning between states for each satellite subsystem with the Kaplan-Meier estimator, and we derive confidence intervals for each probability of transitioning between states. We then conduct parametric Weibull fits of these probabilities using the Maximum Likelihood Estimation (MLE) approach. After validating the results, we compare the reliability versus multi-state failure analyses of three satellite subsystems: the thruster/fuel; the telemetry, tracking, and control (TTC); and the gyro/sensor/reaction wheel subsystems. The results are particularly revealing of the insights that can be gleaned from multi-state failure analysis and the deficiencies, or blind spots, of the traditional reliability analysis. In addition to the specific results provided here, which should prove particularly useful to the space industry, this work highlights the importance

  19. Semianalytic Design Sensitivity Analysis of Nonlinear Structures With a Commercial Finite Element Package

    International Nuclear Information System (INIS)

    Lee, Tae Hee; Yoo, Jung Hun; Choi, Hyeong Cheol

    2002-01-01

    A finite element package is often used as a daily design tool for engineering designers in order to analyze and improve the design. The finite element analysis can provide the responses of a system for given design variables. Although finite element analysis can quite well provide the structural behaviors for given design variables, it cannot provide enough information to improve the design such as design sensitivity coefficients. Design sensitivity analysis is an essential step to predict the change in responses due to a change in design variables and to optimize a system with the aid of the gradient-based optimization techniques. To develop a numerical method of design sensitivity analysis, analytical derivatives that are based on analytical differentiation of the continuous or discrete finite element equations are effective but analytical derivatives are difficult because of the lack of internal information of the commercial finite element package such as shape functions. Therefore, design sensitivity analysis outside of the finite element package is necessary for practical application in an industrial setting. In this paper, the semi-analytic method for design sensitivity analysis is used for the development of the design sensitivity module outside of a commercial finite element package of ANSYS. The direct differentiation method is employed to compute the design derivatives of the response and the pseudo-load for design sensitivity analysis is effectively evaluated by using the design variation of the related internal nodal forces. Especially, we suggest an effective method for stress and nonlinear design sensitivity analyses that is independent of the commercial finite element package is also discussed. Numerical examples are illustrated to show the accuracy and efficiency of the developed method and to provide insights for implementation of the suggested method into other commercial finite element packages

  20. Multi-scale damage modelling in a ceramic matrix composite using a finite-element microstructure meshfree methodology

    Science.gov (United States)

    2016-01-01

    The problem of multi-scale modelling of damage development in a SiC ceramic fibre-reinforced SiC matrix ceramic composite tube is addressed, with the objective of demonstrating the ability of the finite-element microstructure meshfree (FEMME) model to introduce important aspects of the microstructure into a larger scale model of the component. These are particularly the location, orientation and geometry of significant porosity and the load-carrying capability and quasi-brittle failure behaviour of the fibre tows. The FEMME model uses finite-element and cellular automata layers, connected by a meshfree layer, to efficiently couple the damage in the microstructure with the strain field at the component level. Comparison is made with experimental observations of damage development in an axially loaded composite tube, studied by X-ray computed tomography and digital volume correlation. Recommendations are made for further development of the model to achieve greater fidelity to the microstructure. This article is part of the themed issue ‘Multiscale modelling of the structural integrity of composite materials’. PMID:27242308