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Sample records for monolithic vcsel array

  1. Optimal parameters of monolithic high-index contrast grating VCSELs

    Science.gov (United States)

    Marciniak, Magdalena; Gebski, Marcin; Dems, Maciej; Czyszanowski, Tomasz

    2016-04-01

    Monolithic High refractive index Contrast Grating (MHCG) allows several-fold size reduction of epitaxial structure of VCSEL and facilitates VCSEL fabrication in all photonic material systems. MHCGs can be fabricated of material which refractive index is higher than 1.75 without the need of the combination of low and high refractive index materials. MHCGs have a great application potential in optoelectronic devices, especially in phosphide- and nitride-based VCSELs, which suffer from the lack of efficient monolithically integrated DBR mirrors. MHCGs can simplify the construction of VCSELs, reducing their epitaxial design to monolithic wafer with carrier confinement and active region inside and etched stripes on both surfaces in post processing. In this paper we present results of numerical analysis of MHCGs as a high reflective mirrors for broad range of refractive indices that corresponds to plethora of materials typically used in optoelectronics. Our calculations base on a three-dimensional, fully vectorial optical model. We investigate the reflectance of the MHCG mirrors of different design as the function of the refractive index and we show the optimal geometrical parameters of MHCG enabling nearly 100% reflectance and broad reflection stop-band. We show that MHCG can be designed based on most of semiconductors materials and for any incident light wavelength from optical spectrum.

  2. 1060-nm Tunable Monolithic High Index Contrast Subwavelength Grating VCSEL

    DEFF Research Database (Denmark)

    Ansbæk, Thor; Chung, Il-Sug; Semenova, Elizaveta

    2013-01-01

    We present the first tunable vertical-cavity surface-emitting laser (VCSEL) where the top distributed Bragg reflector has been completely substituted by an air-cladded high-index-contrast subwavelength grating (HCG) mirror. In this way, an extended cavity design can be realized by reducing...... the reflection at the semiconductor #x2013;air interface using an anti-reflective coating (ARC). We demonstrate how the ARC can be integrated in a monolithic structure by oxidizing AlGaAs with high Al-content. The HCG VCSEL has the potential to achieve polarization stable single-mode output with high tuning...

  3. Monolithic subwavelength high refractive-index-contrast grating VCSELs

    Science.gov (United States)

    Gebski, Marcin; Dems, Maciej; Lott, James A.; Czyszanowski, Tomasz

    2016-03-01

    In this paper we present optical design and simulation results of vertical-cavity surface-emitting lasers (VCSELs) that incorporate monolithic subwavelength high refractive-index-contrast grating (MHCG) mirrors - a new variety of HCG mirror that is composed of high index material surrounded only on one side by low index material. We show the impact of an MHCG mirror on the performance of 980 nm VCSELs designed for high bit rate and energy-efficient optical data communications. In our design, all or part of the all-semiconductor top coupling distributed Bragg reflector mirror is replaced by an undoped gallium-arsenide MHCG. We show how the optical field intensity distribution of the VCSEL's fundamental mode is controlled by the combination of the number of residual distributed Bragg reflector (DBR) mirror periods and the physical design of the topmost gallium-arsenide MHCG. Additionally, we numerically investigate the confinement factors of our VCSELs and show that this parameter for the MHCG DBR VCSELs may only be properly determined in two or three dimensions due to the periodic nature of the grating mirror.

  4. Analysis of VCSEL Array Module Using a Simple Microlens Array

    Institute of Scientific and Technical Information of China (English)

    Hen-Wai; Tsao; Shyh-Lin; Tsao

    2003-01-01

    A simple microlens array is designed between VCSEL array and fiber array for integration of array module. We increase the optical coupling efficiency from -32.057 dBm to -0.9054 dBm by using our designed microlens array.

  5. Analysis of VCSEL Array Module Using a Simple Microlens Array

    Institute of Scientific and Technical Information of China (English)

    Wen-Ming Cheng; Hen-Wai Tsao; Shyh-Lin Tsao

    2003-01-01

    A simple microlens array is designed between VCSEL array and fiber array for integration of array module. We increase the optical coupling efficiency from-32.057 dBm to-0.9054 dBm by using our designed microlens array.

  6. Comparison of fabrication approaches for selectively oxidized VCSEL arrays

    Energy Technology Data Exchange (ETDEWEB)

    GEIB,KENT M.; CHOQUETTE,KENT D.; ALLERMAN,ANDREW A.; BRIGGS,RONALD D.; HINDI,JANA JO

    2000-04-18

    The impressive performance improvements of laterally oxidized VCSELs come at the expense of increased fabrication complexity for 2-dimensional arrays. Since the epitaxial layers to be wet-thermally oxidized must be exposed, non-planarity can be an issue. This is particularly important in that electrical contact to both the anode and cathode of the diode must be brought out to a package. They have investigated four fabrication sequences suitable for the fabrication of 2-dimensional VCSEL arrays. These techniques include: mesa etched polymer planarized, mesa etched bridge contacted, mesa etched oxide isolated (where the electrical trace is isolated from the substrate during the oxidation) and oxide/implant isolation (oxidation through small via holes) all of which result in VCSELs with outstanding performance. The suitability of these processes for manufacturing are assessed relative to oxidation uniformity, device capacitance, and structural ruggedness for packaging.

  7. Simulation of transient dynamic behavior in laterally coupled VCSEL arrays

    Science.gov (United States)

    Riyopoulos, Spilios

    2002-06-01

    A novel, fast simulation tool for transient response is developed to study jitter and noise caused by lateral cavity interactions in VCSEL arrays. The cavity mode profiles, obtained from a paraxial eigenmode analysis, are used to derive fast 1-D rate equations that implement gain confinement, edge clipping, wide angle scattering and diffraction (self-interference) losses. These equations are augmented by lateral coupling terms describing the interactions among nearest neighbor cavities. Slow time scale coupling describes interactions of phase-shifted cavities via mutually induced electric polarization, cross-hole burning and cross-cavity gain due to optical fringe-field interactions. The tool is used to study cavity cross-talk, lateral bit pattern error effects, and the possibility of excitation of long range modulations over the array. Conclusions relating VCSEL packing density to BER, bit suppression by neighboring cavities, and array phase locking are given.

  8. Monolithic 1310nm buried heterostructure VCSEL using InGaAsP/InP DBR reflectors

    Science.gov (United States)

    Francis, Daniel A.; Young, David B.; Walker, Jeff; Verma, Ashish; Gold, Dave; Decker, Chris

    2005-10-01

    We report on the first monolithic 1310 nm Vertical Cavity Surface Emitting Lasers (VCSELs) with top and bottom InGaAsP/InP distributed Bragg reflectors (DBRs). The lasers show single mode powers over 1.0 mW at room temperature and single mode powers up to 0.5 mW at 85 °C. The lasers, designed to be single mode, have side mode suppression ratios exceeding 45 dB over all temperatures and all powers.

  9. Monolithic Time Delay Integrated APD Arrays Project

    Data.gov (United States)

    National Aeronautics and Space Administration — The overall goal of the proposed program by Epitaxial Technologies is to develop monolithic time delay integrated avalanche photodiode (APD) arrays with sensitivity...

  10. Development of a monolithic ferrite memory array

    Science.gov (United States)

    Heckler, C. H., Jr.; Bhiwandker, N. C.

    1972-01-01

    The results of the development and testing of ferrite monolithic memory arrays are presented. This development required the synthesis of ferrite materials having special magnetic and physical characteristics and the development of special processes; (1) for making flexible sheets (laminae) of the ferrite composition, (2) for embedding conductors in ferrite, and (3) bonding ferrite laminae together to form a monolithic structure. Major problems encountered in each of these areas and their solutions are discussed. Twenty-two full-size arrays were fabricated and fired during the development of these processes. The majority of these arrays were tested for their memory characteristics as well as for their physical characteristics and the results are presented. The arrays produced during this program meet the essential goals and demonstrate the feasibility of fabricating monolithic ferrite memory arrays by the processes developed.

  11. Image fiber optic space-CDMA parallel transmission experiment using 8 x 8 VCSEL/PD arrays.

    Science.gov (United States)

    Nakamura, Moriya; Kitayama, Ken-ichi; Igasaki, Yasunori; Shamoto, Naoki; Kaneda, Keiji

    2002-11-10

    We experimentally demonstrate space-code-division multiple access (space-CDMA) based twodimensional (2-D) parallel optical interconnections by using image fibers and 8 x 8 vertical-cavity surface-emitting laser (VCSEL)/photo diode (PD) arrays. Two spatially encoded four-bit (2 x 2) parallel optical signals were emitted fiom 2-D VCSEL arrays and transmitted through image fibers. The encoded signals were multiplexed by an image-fiber coupler and detected by a 2-D PD array on the receiver side. The receiver recovered the intended parallel signal by decoding the signal. The transmission speed was 64 Mbps/ch (total throughput: 512 Mbps). Bit-error-rate (BER) measurement with a laterally misaligned PD array showed the array had a misalignment tolerance of 25 microm for a BER performance of 10(-9).

  12. Lithographic VCSEL array multimode and single mode sources for sensing and 3D imaging

    Science.gov (United States)

    Leshin, J.; Li, M.; Beadsworth, J.; Yang, X.; Zhang, Y.; Tucker, F.; Eifert, L.; Deppe, D. G.

    2016-05-01

    Sensing applications along with free space data links can benefit from advanced laser sources that produce novel radiation patterns and tight spectral control for optical filtering. Vertical-cavity surface-emitting lasers (VCSELs) are being developed for these applications. While oxide VCSELs are being produced by most companies, a new type of oxide-free VCSEL is demonstrating many advantages in beam pattern, spectral control, and reliability. These lithographic VCSELs offer increased power density from a given aperture size, and enable dense integration of high efficiency and single mode elements that improve beam pattern. In this paper we present results for lithographic VCSELs and describes integration into military systems for very low cost pulsed applications, as well as continuouswave applications in novel sensing applications. The VCSELs are being developed for U.S. Army for soldier weapon engagement simulation training to improve beam pattern and spectral control. Wavelengths in the 904 nm to 990 nm ranges are being developed with the spectral control designed to eliminate unwanted water absorption bands from the data links. Multiple beams and radiation patterns based on highly compact packages are being investigated for improved target sensing and transmission fidelity in free space data links. These novel features based on the new VCSEL sources are also expected to find applications in 3-D imaging, proximity sensing and motion control, as well as single mode sensors such as atomic clocks and high speed data transmission.

  13. VCSEL reliability: a user's perspective

    Science.gov (United States)

    McElfresh, David K.; Lopez, Leoncio D.; Melanson, Robert; Vacar, Dan

    2005-03-01

    VCSEL arrays are being considered for use in interconnect applications that require high speed, high bandwidth, high density, and high reliability. In order to better understand the reliability of VCSEL arrays, we initiated an internal project at SUN Microsystems, Inc. In this paper, we present preliminary results of an ongoing accelerated temperature-humidity-bias stress test on VCSEL arrays from several manufacturers. This test revealed no significant differences between the reliability of AlGaAs, oxide confined VCSEL arrays constructed with a trench oxide and mesa for isolation. This test did find that the reliability of arrays needs to be measured on arrays and not be estimated with the data from singulated VCSELs as is a common practice.

  14. A Ferrite LTCC-Based Monolithic SIW Phased Antenna Array

    KAUST Repository

    Nafe, Ahmed

    2016-11-17

    In this work, we present a novel configuration for realizing monolithic SIW-based phased antenna arrays using Ferrite LTCC technology. Unlike the current common schemes for realizing SIW phased arrays that rely on surface-mount component (p-i-n diodes, etc) for controlling the phase of the individual antenna elements, here the phase is tuned by biasing of the ferrite filling of the SIW. This approach eliminates the need for mounting of any additional RF components and enables seamless monolithic integration of phase shifters and antennas in SIW technology. As a proof of concept, a two-element slotted SIW-based phased array is designed, fabricated and measured. The prototype exhibits a gain of 4.9 dBi at 13.2 GHz and a maximum E-plane beam-scanning of 28 degrees using external windings for biasing the phase shifters. Moreover, the array can achieve a maximum beam-scanning of 19 degrees when biased with small windings that are embedded in the package. This demonstration marks the first time a fully monolithic SIW-based phased array is realized in Ferrite LTCC technology and paves the way for future larger-size implementations.

  15. Parallel pipeline networking and signal processing with field-programmable gate arrays (FPGAs) and VCSEL-MSM smart pixels

    Science.gov (United States)

    Kuznia, C. B.; Sawchuk, Alexander A.; Zhang, Liping; Hoanca, Bogdan; Hong, Sunkwang; Min, Chris; Pansatiankul, Dhawat E.; Alpaslan, Zahir Y.

    2000-05-01

    We present a networking and signal processing architecture called Transpar-TR (Translucent Smart Pixel Array-Token- Ring) that utilizes smart pixel technology to perform 2D parallel optical data transfer between digital processing nodes. Transpar-TR moves data through the network in the form of 3D packets (2D spatial and 1D time). By utilizing many spatial parallel channels, Transpar-TR can achieve high throughput, low latency communication between nodes, even with each channel operating at moderate data rates. The 2D array of optical channels is created by an array of smart pixels, each with an optical input and optical output. Each smart pixel consists of two sections, an optical network interface and ALU-based processor with local memory. The optical network interface is responsible for transmitting and receiving optical data packets using a slotted token ring network protocol. The smart pixel array operates as a single-instruction multiple-data processor when processing data. The Transpar-TR network, consisting of networked smart pixel arrays, can perform pipelined parallel processing very efficiently on 2D data structures such as images and video. This paper discusses the Transpar-TR implementation in which each node is the printed circuit board integration of a VCSEL-MSM chip, a transimpedance receiver array chip and an FPGA chip.

  16. Developments of two 4 × 10 Gb/s VCSEL array drivers in 65 nm CMOS for HEP experiments

    Science.gov (United States)

    Guo, D.; Gong, D.; Xiang, A. C.; Moreira, P.; Kulis, S.; Chen, J.; Hou, S.; Liu, C.; Liu, T.; Prosser, A.; He, H.; Sun, Q.; Wang, J.; Yang, D.; Ye, J.; Zhou, W.

    2017-02-01

    This paper presents the designs and test results of two radiation tolerant 4 × 10 Gb/s vertical cavity surface emitting laser (VCSEL) array drivers VLAD and lpVLAD, both fabricated in a 1.2 V 65 nm CMOS technology. VLAD adopts a power efficient bandwidth-boost technology, and lpVLAD employs a novel high-efficiency output structure to achieve an ultra-low power consumption of 2.2 mW/Gb/ch with 2 mA bias current and 6 mA modulation current. Both drivers are optically tested passing 10 Gb/s eye mask with all channels active under the radiation of a total dose up to 350 Mrad(SiO2).

  17. Monolithic microwave integrated circuit devices for active array antennas

    Science.gov (United States)

    Mittra, R.

    1984-01-01

    Two different aspects of active antenna array design were investigated. The transition between monolithic microwave integrated circuits and rectangular waveguides was studied along with crosstalk in multiconductor transmission lines. The boundary value problem associated with a discontinuity in a microstrip line is formulated. This entailed, as a first step, the derivation of the propagating as well as evanescent modes of a microstrip line. The solution is derived to a simple discontinuity problem: change in width of the center strip. As for the multiconductor transmission line problem. A computer algorithm was developed for computing the crosstalk noise from the signal to the sense lines. The computation is based on the assumption that these lines are terminated in passive loads.

  18. Monolithic Microwave Integrated Circuit (MMIC) Phased Array Demonstrated With ACTS

    Science.gov (United States)

    1996-01-01

    Monolithic Microwave Integrated Circuit (MMIC) arrays developed by the NASA Lewis Research Center and the Air Force Rome Laboratory were demonstrated in aeronautical terminals and in mobile or fixed Earth terminals linked with NASA's Advanced Communications Technology Satellite (ACTS). Four K/Ka-band experimental arrays were demonstrated between May 1994 and May 1995. Each array had GaAs MMIC devices at each radiating element for electronic beam steering and distributed power amplification. The 30-GHz transmit array used in uplinks to ACTS was developed by Lewis and Texas Instruments. The three 20-GHz receive arrays used in downlinks from ACTS were developed in cooperation with the Air Force Rome Laboratory, taking advantage of existing Air Force integrated-circuit, active-phased-array development contracts with the Boeing Company and Lockheed Martin Corporation. Four demonstrations, each related to an application of high interest to both commercial and Department of Defense organizations, were conducted. The location, type of link, and the data rate achieved for each of the applications is shown. In one demonstration-- an aeronautical terminal experiment called AERO-X--a duplex voice link between an aeronautical terminal on the Lewis Learjet and ACTS was achieved. Two others demonstrated duplex voice links (and in one case, interactive video links as well) between ACTS and an Army high-mobility, multipurpose wheeled vehicle (HMMWV, or "humvee"). In the fourth demonstration, the array was on a fixed mount and was electronically steered toward ACTS. Lewis served as project manager for all demonstrations and as overall system integrator. Lewis engineers developed the array system including a controller for open-loop tracking of ACTS during flight and HMMWV motion, as well as a laptop data display and recording system used in all demonstrations. The Jet Propulsion Laboratory supported the AERO-X program, providing elements of the ACTS Mobile Terminal. The successful

  19. Vcsel structure

    DEFF Research Database (Denmark)

    2015-01-01

    The invention relates to a VCSEL structure based on a novel grating reflector. The grating reflector comprises a grating layer with a contiguous core grating region having a grating structure, wherein an index of refraction of high-index sections of the grating structure is at least 2.......5, and wherein an index of refraction of low-index sections of the grating structure is less than 2. The core grating region defines a projection in a direction normal to the grating layer. The grating reflector further comprises a cap layer abutting the grating layer, and an index of refraction of the cap layer...... the projection of the core grating region, the grating layer is also abutted by a second low-index layer and/or by air, an index of refraction of the second low-index layer or air being less than 2. The VCSEL structure furthermore comprises a first reflector and an active region for providing a cavity...

  20. Analysis of waveguiding properties of VCSEL structures

    Energy Technology Data Exchange (ETDEWEB)

    Erteza, I.A. [Sandia National Labs., Albuquerque, NM (United States). Exploratory Systems Development Center

    1996-09-01

    In this paper, the authors explore the feasibility of using the distributed Bragg reflector, grown on the substrate for a VCSEL (Vertical Cavity Surface Emitting Laser), to provide waveguiding within the substrate. This waveguiding could serve as an interconnection among VCSELs in an array. Before determining the feasibility of waveguide interconnected VCSELs, two analysis methods are presented and evaluated for their applicability to this problem. The implementations in Mathematica of both these methods are included. Results of the analysis show that waveguiding in VCSEL structures is feasible. Some of the many possible uses of waveguide interconnected VCSELs are also briefly discussed. The tools and analysis presented in this report can be used to evaluate such system concepts and to do detailed design calculations.

  1. Advances in Red VCSEL Technology

    Directory of Open Access Journals (Sweden)

    Klein Johnson

    2012-01-01

    Full Text Available Red VCSELs offer the benefits of improved performance and lower power consumption for medical and industrial sensing, faster printing and scanning, and lower cost, higher speed interconnects based upon plastic optical fiber (POF. However, materials challenges make it more difficult to achieve the desired performance than at the well-developed wavelength of 850 nm. This paper will describe the state of the art of red VCSEL performance and the results of development efforts to achieve improved output power and a broader temperature range of operation. It will also provide examples of the applications of red VCSELs and the benefits they offer. In addition, the packaging flexibility offered by VCSELs, and some examples of non-Hermetic package demonstrations will be discussed. Some of the red VCSEL performance demonstrations include output power of 14 mW CW at room temperature, a record maximum temperature of 115∘C for CW operation at an emission wavelength of 689 nm, time to 1% failure at room temperature of approximately 200,000 hours, lifetime in a 50∘C, 85% humidity environment in excess of 3500 hours, digital data rate of 3 Gbps, and peak pulsed array power of greater than 100 mW.

  2. Monolithic blue LED series arrays for high-voltage AC operation

    Energy Technology Data Exchange (ETDEWEB)

    Ao, Jin-Ping [Satellite Venture Business Laboratory, University of Tokushima, Tokushima 770-8506 (Japan); Sato, Hisao; Mizobuchi, Takashi; Morioka, Kenji; Kawano, Shunsuke; Muramoto, Yoshihiko; Sato, Daisuke; Sakai, Shiro [Nitride Semiconductor Co. Ltd., Naruto, Tokushima 771-0360 (Japan); Lee, Young-Bae; Ohno, Yasuo [Department of Electrical and Electronic Engineering, University of Tokushima, Tokushima 770-8506 (Japan)

    2002-12-16

    Design and fabrication of monolithic blue LED series arrays that can be operated under high ac voltage are described. Several LEDs, such as 3, 7, and 20, are connected in series and in parallel to meet ac operation. The chip size of a single device is 150 {mu}m x 120 {mu}m and the total size is 1.1 mm x 1 mm for a 40(20+20) LED array. Deep dry etching was performed as device isolation. Two-layer interconnection and air bridge are utilized to connect the devices in an array. The monolithic series array exhibit the expected operation function under dc and ac bias. The output power and forward voltage are almost proportional to LED numbers connected in series. On-wafer measurement shows that the output power is 40 mW for 40(20+20) LED array under ac 72 V. (Abstract Copyright [2002], Wiley Periodicals, Inc.)

  3. Integration of GaAs-based VCSEL array on SiN platform with HCG reflectors for WDM applications

    Science.gov (United States)

    Kumari, Sulakshna; Gustavsson, Johan S.; Wang, Ruijun; Haglund, Emanuel P.; Westbergh, Petter; Sanchez, Dorian; Haglund, Erik; Haglund, Åsa; Bengtsson, Jörgen; Le Thomas, Nicolas; Roelkens, Gunther; Larsson, Anders; Baets, Roel

    2015-02-01

    We present a GaAs-based VCSEL structure, BCB bonded to a Si3N4 waveguide circuit, where one DBR is substituted by a free-standing Si3N4 high-contrast-grating (HCG) reflector realized in the Si3N4 waveguide layer. This design enables solutions for on-chip spectroscopic sensing, and the dense integration of 850-nm WDM data communication transmitters where individual channel wavelengths are set by varying the HCG parameters. RCWA shows that a 300nm-thick Si3N4 HCG with 800nm period and 40% duty cycle reflects strongly (HCG's influence on the VCSEL wavelength, allowing for a 15-nm-wide wavelength setting range with low threshold gain (<1000 cm-1).

  4. Phased-Array Monolithic PEM for FT Spectrometry With Applications in Explosive Detection and CB Defense

    Science.gov (United States)

    2008-12-01

    1 PHASED-ARRAY MONOLITHIC PEM FOR FT SPECTROMETRY WITH APPLICATIONS IN EXPLOSIVE DETECTION AND CB DEFENSE Tudor N. Buican* Semiotic ...PERFORMING ORGANIZATION NAME(S) AND ADDRESS(ES) Semiotic Engineering Associates LLC Albuquerque, NM 87108 8. PERFORMING ORGANIZATION REPORT NUMBER 9

  5. Designing of TJ VCSEL based on nitride materials

    Science.gov (United States)

    Sarzała, R. P.; Pijanowski, K.; Gebski, M.; Marciniak, M.; Nakwaski, W.

    2016-12-01

    Different structures of nitride Vertical-Cavity Surface-Emitting Lasers (VCSELs) have been developed in recent years. However there is still many problems with such constructions, especially with electrical and optical confinement, current injection and construction and fabrication of mirrors. In this paper we present novel approach to nitride VCSEL designing. We investigated structure with tunnel junction (TJ) and top and bottom dielectric distributed Bragg reflectors (DBRs). Using our three-dimensional self-consistent model we investigated thermal and electrical properties of such laser. We also proposed replacing bottom DBR by monolithic high contrast grating mirror (MHCG) and presented optical properties of VCSEL with such mirrors.

  6. Effect of the presence of an ordered micro-pillar array on the formation of silica monoliths

    NARCIS (Netherlands)

    Detobel, Frederik; Eghbali, Hamed; De Bruyne, Selm; Terryn, Herman; Gardeniers, Han; Desmet, Gert

    2009-01-01

    We report on the synthesis of siloxane-based monoliths in the presence of a two-dimensional, perfectly ordered array of micro-pillars. Both methyltrimethoxysilane- and tetramethoxysilane-based monoliths were considered. The obtained structures were analyzed using scanning-electron microscopy and can

  7. A design concept for an MMIC (Monolithic Microwave Integrated Circuit) microstrip phased array

    Science.gov (United States)

    Lee, Richard Q.; Smetana, Jerry; Acosta, Roberto

    1987-02-01

    A conceptual design for a microstrip phased array with monolithic microwave integrated circuit (MMIC) amplitude and phase controls is described. The MMIC devices used are 20 GHz variable power amplifiers and variable phase shifters recently developed by NASA contractors for applications in future Ka proposed design, which concept is for a general NxN element array of rectangular lattice geometry. Subarray excitation is incorporated in the MMIC phased array design to reduce the complexity of the beam forming network and the number of MMIC components required.

  8. A design concept for an MMIC (Monolithic Microwave Integrated Circuit) microstrip phased array

    Science.gov (United States)

    Lee, Richard Q.; Smetana, Jerry; Acosta, Roberto

    1987-01-01

    A conceptual design for a microstrip phased array with monolithic microwave integrated circuit (MMIC) amplitude and phase controls is described. The MMIC devices used are 20 GHz variable power amplifiers and variable phase shifters recently developed by NASA contractors for applications in future Ka proposed design, which concept is for a general NxN element array of rectangular lattice geometry. Subarray excitation is incorporated in the MMIC phased array design to reduce the complexity of the beam forming network and the number of MMIC components required.

  9. Monolithic LaBr3 : Ce crystals on silicon photomultiplier arrays for time-of-flight positron emission tomography

    NARCIS (Netherlands)

    Seifert, Stefan; van Dam, Herman T.; Huizenga, Jan; Vinke, Ruud; Dendooven, Peter; Löhner, Herbert; Schaart, Dennis R.

    2012-01-01

    Positron emission tomography detectors based on monolithic scintillation crystals exhibit good spatial and energy resolution, intrinsically provide depth-of-interaction information, have high gamma-photon capture efficiency, and may reduce the manufacturing costs compared to pixelated crystal arrays

  10. A linear monolithic 4-6 on silicon IR detector array

    Science.gov (United States)

    Vandamme, J.; Vermeiren, J.; Zogg, H.; Masek, J.; Fabbricotti, M.

    1992-12-01

    A linear array of monolithically grown PbTe and PbSnSe detectors on (111)-Si for MWIR and TIR imaging applications was designed and processed. The array consists of a staggered row of 2 by 128 detectors on a 100 micrometers pitch. The readout circuitry, integrated on the Si substrate consists of a COS multiplexer with a direct injection input stage, a charge reduction stage and charge to voltage conversion stage for each individual detector. This XDI (MultipeXed Direct Injection) circuit also allows for on-chip nonuniformity compensation with a switched capacitor network.

  11. Progress toward a monolithically integrated coherent diode laser array

    Science.gov (United States)

    Evans, G. A.; Garmire, E. M.; Stoll, H. M.; Osmer, J. A.; Soady, W. E.; Lee, A. B.; Ziegler, M. P.

    1981-02-01

    Progress toward the design and fabrication of a GaAlAs semiconductor laser array capable of high average power levels (0.1 to 1.0 watt) and low (approx 1 millirad) beam divergence is reported. A large optical cavity (LOC) configuration is grown by liquid phase epitaxy. The LOC structure is characterized by photoluminescence scans, ion microprobe mass analysis (IMMA), and optical waveguiding measurements. Fabry-Perot, active-passive, and DBR lasers are fabricated using chemical and ion beam etching. Gratings formed using holographic and ion beam etching techniques provide third order feedback for the DBR lasers, and are also used as distributed beam deflectors (DBDs) and output couplers. Comparisons of the results of experiments performed on DBR lasers, DBDs, and coupled lasers are made with theoretical models. Details of the material growth, material characterization, device fabrication, experiments, and theoretical models are presented in this report.

  12. Comparison of polystyrene scintillator fiber array and monolithic polystyrene for neutron imaging and radiography

    Science.gov (United States)

    Simpson, R.; Cutler, T. E.; Danly, C. R.; Espy, M. A.; Goglio, J. H.; Hunter, J. F.; Madden, A. C.; Mayo, D. R.; Merrill, F. E.; Nelson, R. O.; Swift, A. L.; Wilde, C. H.; Zocco, T. G.

    2016-11-01

    The neutron imaging diagnostic at the National Ignition Facility has been operating since 2011 generating neutron images of deuterium-tritium (DT) implosions at peak compression. The current design features a scintillating fiber array, which allows for high imaging resolution to discern small-scale structure within the implosion. In recent years, it has become clear that additional neutron imaging systems need to be constructed in order to provide 3D reconstructions of the DT source and these additional views need to be on a shorter line of sight. As a result, there has been increased effort to identify new image collection techniques that improve upon imaging resolution for these next generation neutron imaging systems, such as monolithic deuterated scintillators. This work details measurements performed at the Weapons Neutron Research Facility at Los Alamos National Laboratory that compares the radiographic abilities of the fiber scintillator with a monolithic scintillator, which may be featured in a future short line of sight neutron imaging systems.

  13. Single-Mode VCSELs

    Science.gov (United States)

    Larsson, Anders; Gustavsson, Johan S.

    The only active transverse mode in a truly single-mode VCSEL is the fundamental mode with a near Gaussian field distribution. A single-mode VCSEL produces a light beam of higher spectral purity, higher degree of coherence and lower divergence than a multimode VCSEL and the beam can be more precisely shaped and focused to a smaller spot. Such beam properties are required in many applications. In this chapter, after discussing applications of single-mode VCSELs, we introduce the basics of fields and modes in VCSELs and review designs implemented for single-mode emission from VCSELs in different materials and at different wavelengths. This includes VCSELs that are inherently single-mode as well as inherently multimode VCSELs where higher-order modes are suppressed by mode selective gain or loss. In each case we present the current state-of-the-art and discuss pros and cons. At the end, a specific example with experimental results is provided and, as a summary, the most promising designs based on current technologies are identified.

  14. VCSEL Based Coherent PONs

    DEFF Research Database (Denmark)

    Jensen, Jesper Bevensee; Rodes, Roberto; Caballero Jambrina, Antonio;

    2014-01-01

    We present a review of research performed in the area of coherent access technologies employing vertical cavity surface emitting lasers (VCSELs). Experimental demonstrations of optical transmission over a passive fiber link with coherent detection using VCSEL local oscillators and directly modula...

  15. Three-dimensional integration of VCSEL-based optoelectronics

    Science.gov (United States)

    Louderback, Duane A.; Lin, Hung-Cheng; Fish, Melanie A.; Cheng, Julien; Guilfoyle, Peter S.

    2005-03-01

    A monolithic optoelectronic device structure with the potential to enable VCSEL-based photonic integrated circuits on GaAs is presented. Using integrated diffraction gratings, the device structure enables the optical output of VCSELs to be coupled to an internal horizontal waveguide, while the optical signals in the waveguide are tapped off to resonant cavity detectors. Since horizontal waveguides are used to route the optical signals between devices, the output mirror transmission of the VCSELs can be eliminated, although we have chosen to retain a small amount of transmission in the top DBR to enable on-wafer testing. The design and fabrication of the monolithically integrated structure, including epitaxial regrowth, is discussed and initial device characteristics are presented.

  16. Diffraction coupled phase-locked arrays of quantum cascade lasers with monolithically integrated Talbot cavities

    CERN Document Server

    Wang, Lei; Jia, Zhi-Wei; Zhao, Yue; Liu, Chuan-Wei; Liu, Ying-Hui; Zhai, Shen-Qiang; Zhuo, Ning; Liu, Feng-Qi; Xu, Xian-Gang

    2016-01-01

    Diffraction coupled arrays of quantum cascade laser are presented. The phase-locked behavior is achieved through monolithic integration of a Talbot cavity at one side of the laser array. The principle is based on fractional Talbot effect. By controlling length of Talbot cavity to be a quarter of Talbot distance (Zt/4), in-phase mode operation is selected. Measured far-field radiation patterns reflect stable in-phase mode operation under different injection currents, from threshold current to full power current. Diffraction-limited performance is shown from the lateral far-field, where three peaks can be obtained and main peak and side peak interval is 10.5{\\deg}. The phase-locked arrays with in-phase mode operation may be a feasible solution to get higher output power and maintain well beam quality meanwhile.

  17. VCSELs as light source for time-of-flight sensors

    Science.gov (United States)

    Moench, Holger; Frey, Manuel; Grabherr, Martin; Gronenborn, Stephan; Gudde, Ralph; Kolb, Johanna; Miller, Michael; Weigl, Alexander

    2017-02-01

    VCSELs and VCSEL arrays are an ideal light source for time-of-flight based sensors. The narrow emission spectrum and the ability for short pulses make them superior to LEDs. Combined with fast photodiodes or special camera chips spatial 3D information can be obtained which is needed in diverse applications like camera autofocus, indoor navigation, 3Dobject recognition or even autonomously driving vehicles. VCSEL arrays are the way to tailor the output power. For pulse operation at low duty cycle average heat dissipation is no longer the upper limit to the operating point of VCSELs but over-pulsing becomes possible. Taking into account electrical boundary conditions and optimum conversion efficiency arrays can be designed for specific operating conditions. Measurements of arrays under short pulse operation are presented using a package with integrated driver.

  18. Detector block based on arrays of 144 SiPMs and monolithic scintillators: A performance study

    Energy Technology Data Exchange (ETDEWEB)

    González, A.J.; Conde, P.; Iborra, A. [Institute for Instrumentation in Molecular Imaging (I3M), Universidad Politécnica de Valencia – CSIC – CIEMAT (Spain); Aguilar, A. [Communications and Digital Systems Design Group (DSDC), Universidad de Valencia (Spain); Bellido, P. [Institute for Instrumentation in Molecular Imaging (I3M), Universidad Politécnica de Valencia – CSIC – CIEMAT (Spain); García-Olcina, R. [Communications and Digital Systems Design Group (DSDC), Universidad de Valencia (Spain); Hernández, L.; Moliner, L.; Rigla, J.P.; Rodríguez-Álvarez, M.J.; Sánchez, F.; Seimetz, M.; Soriano, A. [Institute for Instrumentation in Molecular Imaging (I3M), Universidad Politécnica de Valencia – CSIC – CIEMAT (Spain); Torres, J. [Communications and Digital Systems Design Group (DSDC), Universidad de Valencia (Spain); Vidal, L.F.; Benlloch, J.M. [Institute for Instrumentation in Molecular Imaging (I3M), Universidad Politécnica de Valencia – CSIC – CIEMAT (Spain)

    2015-07-01

    We have developed a detector block composed by a monolithic LYSO scintillator coupled to a custom made 12×12 SiPMs array. The design is mainly focused to applications such as Positron Emission Tomography. The readout electronics is based on 3 identical and scalable Application Specific Integrated Circuits (ASIC). We have determined the main performance of the detector block namely spatial, energy, and time resolution but also the system capability to determine the photon depth of interaction, for different crystal surface treatments. Intrinsic detector spatial resolution values as good as 1.7 mm FWHM and energies of 15% for black painted crystals were measured.

  19. Advances and new functions of VCSEL photonics

    Science.gov (United States)

    Koyama, Fumio

    2014-11-01

    A vertical cavity surface emitting laser (VCSEL) was born in Japan. The 37 years' research and developments opened up various applications including datacom, sensors, optical interconnects, spectroscopy, optical storages, printers, laser displays, laser radar, atomic clock and high power sources. A lot of unique features have been already proven, such as low power consumption, a wafer level testing and so on. The market of VCSELs has been growing up rapidly and they are now key devices in local area networks based on multi-mode optical fibers. Optical interconnections in data centers and supercomputers are attracting much interest. In this paper, the advances on VCSEL photonics will be reviewed. We present the high-speed modulation of VCSELs based on a coupled cavity structure. For further increase in transmission capacity per fiber, the wavelength engineering of VCSEL arrays is discussed, which includes the wavelength stabilization and wavelength tuning based on a micro-machined cantilever structure. We also address a lateral integration platform and new functions, including high-resolution beam scanner, vortex beam creation and large-port free space wavelength selective switch with a Bragg reflector waveguide.

  20. Development of silicon monolithic arrays for dosimetry in external beam radiotherapy

    Energy Technology Data Exchange (ETDEWEB)

    Bisello, Francesca, E-mail: francesca.bisello@iba-group.com [IBA Dosimetry GmbH, Schwarzenbruck (Germany); Friedrich-Alexander Universität Erlangen—Nürnberg, Erlangen (Germany); Menichelli, David [IBA Dosimetry GmbH, Schwarzenbruck (Germany); Scaringella, Monica [University of Florence, Firenze (Italy); INFN—Florence Division, Sesto Fiorentino (Italy); Talamonti, Cinzia; Zani, Margherita; Bucciolini, Marta [University of Florence, Firenze (Italy); Azienda Ospedaliera Unversitaria Careggi, Firenze (Italy); Bruzzi, Mara [University of Florence, Firenze (Italy); INFN—Florence Division, Sesto Fiorentino (Italy)

    2015-10-01

    New tools for dosimetry in external beam radiotherapy have been developed during last years in the framework of the collaboration among the University of Florence, INFN Florence and IBA Dosimetry. The first step (in 2007) was the introduction in dosimetry of detector solutions adopted from high energy physics, namely epitaxial silicon as the base detector material and a guard ring in diode design. This allowed obtaining state of the art radiation hardness, in terms of sensitivity dependence on accumulated dose, with sensor geometry particularly suitable for the production of monolithic arrays with modular design. Following this study, a 2D monolithic array has been developed, based on 6.3×6.3 cm{sup 2} modules with 3 mm pixel pitch. This prototype has been widely investigated and turned out to be a promising tool to measure dose distributions of small and IMRT fields. A further linear array prototype has been recently design with improve spatial resolution (1 mm pitch) and radiation hardness. This 24 cm long device is constituted by 4×64 mm long modules. It features low sensitivity changes with dose (0.2%/kGy) and dose per pulse (±1% in the range 0.1–2.3 mGy/pulse, covering applications with flattened and unflattened photon fields). The detector has been tested with very satisfactory results as a tool for quality assurance of linear accelerators, with special regards to small fields, and proton pencil beams. In this contribution, the characterization of the linear array with unflattened MV X-rays, {sup 60}Co radiation and 226 MeV protons is reported. - Highlights: • A silicon monolithic 1D array with 1 mm pixel pitch was developed. • The detector was characterized with {sup 60}Co, unflattened MV X-rays, 226 MeV protons. • Dose linearity in clinical relevance range and dose profiles were measured. • The detector performs good agreement with reference detectors. • The technology is suitable in dose profiling in MV X-ray and proton therapy.

  1. Nanoporous Monolithic Microsphere Arrays Have Anti-Adhesive Properties Independent of Humidity

    Directory of Open Access Journals (Sweden)

    Anna Eichler-Volf

    2016-05-01

    Full Text Available Bioinspired artificial surfaces with tailored adhesive properties have attracted significant interest. While fibrillar adhesive pads mimicking gecko feet are optimized for strong reversible adhesion, monolithic microsphere arrays mimicking the slippery zone of the pitchers of carnivorous plants of the genus Nepenthes show anti-adhesive properties even against tacky counterpart surfaces. In contrast to the influence of topography, the influence of relative humidity (RH on adhesion has been widely neglected. Some previous works deal with the influence of RH on the adhesive performance of fibrillar adhesive pads. Commonly, humidity-induced softening of the fibrils enhances adhesion. However, little is known on the influence of RH on solid anti-adhesive surfaces. We prepared polymeric nanoporous monolithic microsphere arrays (NMMAs with microsphere diameters of a few 10 µm to test their anti-adhesive properties at RHs of 2% and 90%. Despite the presence of continuous nanopore systems through which the inner nanopore walls were accessible to humid air, the topography-induced anti-adhesive properties of NMMAs on tacky counterpart surfaces were retained even at RH = 90%. This RH-independent robustness of the anti-adhesive properties of NMMAs significantly contrasts the adhesion enhancement by humidity-induced softening on nanoporous fibrillar adhesive pads made of the same material.

  2. Phased array of high-power, coherent, monolithic flared amplifier master oscillator power amplifiers

    Science.gov (United States)

    Osinski, J. S.; Mehuys, D.; Welch, D. F.; Waarts, R. G.; Major, J. S., Jr.; Dzurko, K. M.; Lang, R. J.

    1995-01-01

    A monolithically integrated array of InGaAs/AlGaAs flared amplifiers driven by a single DBR laser through a power splitter network and individually addressed phase modulators is described. Phase adjustment of ≳2π per element by free-carrier effects is verified by monitoring the interference pattern of all four emitters, and typically requires <15 mA of current to obtain a 2π phase shift. Phase matching is achieved among all four diffraction-limited emitters at a pulsed output power of ≳5 W, and, combined with the proper external lensing, could therefore result in an ultranarrow, single-lobed far-field pattern whose width is determined by the extended aperture of the array.

  3. EML Array fabricated by SAG technique monolithically integrated with a buried ridge AWG multiplexer

    Science.gov (United States)

    Xu, Junjie; Liang, Song; Zhang, Zhike; An, Junming; Zhu, Hongliang; Wang, Wei

    2017-06-01

    We report the fabrication of a ten channel electroabsorption modulated DFB laser (EML) array. Different emission wavelengths of the laser array are obtained by selective area growth (SAG) technique, which is also used for the integration of electroabsorption modulators (EAM) with the lasers. An arrayed waveguide grating (AWG) combiner is integrated monolithically with the laser array by butt-joint regrowth (BJR) technique. A buried ridge waveguide structure is adopted for the AWG combiner. A self aligned fabrication procedure is adopted for the fabrication of the waveguide structure of the device to eliminate the misalignment between the laser active waveguide and the passive waveguide. A Ti thin film heater is integrated for each laser in the array. With the help of the heaters, ten laser emissions with 1.8 nm channel spacing are obtained. The integrated EAM has a larger than 11 dB static extinction ratios and larger than 8 GHz small signal modulation bandwidths. The light power collected in the output waveguide of the AWG is larger than -13 dBm for each wavelength.

  4. Results of a combined monolithic crystal and an array of ASICs controlled SiPMs

    Energy Technology Data Exchange (ETDEWEB)

    Conde, P.; González, A.J., E-mail: agonzalez@i3m.upv.es; Hernández, L.; Bellido, P.; Iborra, A.; Crespo, E.; Moliner, L.; Rigla, J.P.; Rodríguez-Álvarez, M.J.; Sánchez, F.; Seimetz, M.; Soriano, A.; Vidal, L.F.; Benlloch, J.M.

    2014-01-11

    In this work we present the energy and spatial resolutions we have obtained for a γ-ray detector based on a monolithic LYSO crystal coupled to an array of 256 SiPMs. Two crystal configurations of the same trapezoidal shape have been tried. In one approach all surfaces were black painted but the exit one facing the photosensor array which was polished. The other approach included a retroreflector (RR) layer coupled to the entrance face of the crystal powering the amount of transmitted light to the photosensors. Two coupling media between the scintillator and the SiPM array were used, namely direct coupling by means of optical grease and coupling through an array of light guides. Since the same operational voltage was supplied to the entire array, it was needed to equalize their gains before feeding their signals to the Data Acquisition system. Such a job was performed by means of 4 scalable Application Specific Circuits (ASICs). An energy resolution of about 24.4% has been achieved for the direct coupling with the RR layer together with a spatial resolution of approximately 2.9 mm at the detector center. With the light guides coupling the effects of image compression at the edges are significantly minimized, but worsening the energy resolution to about 33.1% with a spatial resolution nearing 4 mm at the detector center.

  5. Spectroscopic benzene detection using a broadband monolithic DFB-QCL array

    Science.gov (United States)

    Lewicki, Rafał; Witinski, Mark; Li, Biao; Wysocki, Gerard

    2016-03-01

    Quantitative laser spectroscopic measurements of complex molecules that have a broad absorption spectra require broadly tunable laser sources operating preferably in the mid-infrared molecular fingerprint region. In this paper a novel broadband mid-infrared laser source comprising of an array of single-mode distributed feedback quantum cascade lasers was used to target a broadband absorption feature of benzene (C6H6), a toxic and carcinogenic atmospheric pollutant. The DFB-QCL array is a monolithic semiconductor device with no opto-mechanical components, which eliminates issues with mechanical vibrations. The DFB-QCLs array used in this work provides spectral coverage from 1022.5 cm-1 to 1053.3 cm-1, which is sufficient to access the absorption feature of benzene at 1038 cm-1 (9.64 μm). A sensor prototype based on a 76 m multipass cell (AMAC-76LW, Aerodyne Research) and a dispersive DFB-QCL array beam combiner was developed and tested. The Allan deviation analysis of the retrieved benzene concentration data yields a short-term precision of 100 ppbv/Hz1/2 and a minimum detectable concentration of 12 ppbv for 200 s averaging time. The system was also tested by sampling atmospheric air as well as vapors of different chemical products that contained traces of benzene.

  6. Cantilever RF-MEMS for monolithic integration with phased array antennas on a PCB

    Science.gov (United States)

    Aguilar-Armenta, C. J.; Porter, S. J.

    2015-12-01

    This article presents the development and operation of a novel electrostatic metal-to-metal contact cantilever radio-frequency microelectromechanical system (RF-MEMS) switch for monolithic integration with microstrip phased array antennas (PAAs) on a printed circuit board. The switch is fabricated using simple photolithography techniques on a Rogers 4003c substrate, with a footprint of 200 µm × 100 µm, based on a 1 µm-thick copper cantilever. An alternative wet-etching technique for effectively releasing the cantilever is described. Electrostatic and electromagnetic measurements show that the RF-MEMS presents an actuation voltage of 90 V for metal-to-metal contact, an isolation of -8.7 dB, insertion loss of -2.5 dB and a return loss of -15 dB on a 50 Ω microstrip line at 12.5 GHz. For proof-of-concept, a beam-steering 2 × 2 microstrip PAA, based on two 1-bit phase shifters suitable for the monolithic integration of the RF-MEMS, has been designed and measured at 12.5 GHz. Measurements show that the beam-steering system presents effective radiation characteristics with scanning capabilities from broadside towards 29° in the H-plane.

  7. Subwavelength grating as both emission mirror and electrical contact for VCSELs in any material system

    Science.gov (United States)

    Czyszanowski, Tomasz; Gebski, Marcin; Dems, Maciej; Wasiak, Michał; Sarzała, Robert; Panajotov, Krassimir

    2017-01-01

    Semiconductor-metal subwavelength grating (SMSG) can serve a dual purpose in vertical-cavity surface-emitting lasers (VCSELs), as both optical coupler and current injector. SMSGs provide optical as well as lateral current confinement, eliminating the need for ring contacts and lateral build-in optical and current confinement, allowing their implementation on arbitrarily large surfaces. Using an SMSG as the top mirror enables fabrication of monolithic VCSELs from any type of semiconductor crystal. The construction of VCSELs with SMSGs requires significantly less p-type material, in comparison to conventional VCSELs. In this paper, using a three-dimensional, fully vectorial optical model, we analyse the properties of the stand-alone SMSG in a number of semiconductor materials for a broad range of wavelengths. Integrating the optical model with thermal and electrical numerical models, we then simulate the threshold operation of an exemplary SMSG VCSEL. PMID:28079149

  8. Subwavelength grating as both emission mirror and electrical contact for VCSELs in any material system

    Science.gov (United States)

    Czyszanowski, Tomasz; Gebski, Marcin; Dems, Maciej; Wasiak, Michał; Sarzała, Robert; Panajotov, Krassimir

    2017-01-01

    Semiconductor-metal subwavelength grating (SMSG) can serve a dual purpose in vertical-cavity surface-emitting lasers (VCSELs), as both optical coupler and current injector. SMSGs provide optical as well as lateral current confinement, eliminating the need for ring contacts and lateral build-in optical and current confinement, allowing their implementation on arbitrarily large surfaces. Using an SMSG as the top mirror enables fabrication of monolithic VCSELs from any type of semiconductor crystal. The construction of VCSELs with SMSGs requires significantly less p-type material, in comparison to conventional VCSELs. In this paper, using a three-dimensional, fully vectorial optical model, we analyse the properties of the stand-alone SMSG in a number of semiconductor materials for a broad range of wavelengths. Integrating the optical model with thermal and electrical numerical models, we then simulate the threshold operation of an exemplary SMSG VCSEL.

  9. Monolithic electrically injected nanowire array edge-emitting laser on (001) silicon

    KAUST Repository

    Frost, Thomas

    2014-08-13

    A silicon-based laser, preferably electrically pumped, has long been a scientific and engineering goal. We demonstrate here, for the first time, an edge-emitting InGaN/GaN disk-in-nanowire array electrically pumped laser emitting in the green (λ = 533 nm) on (001) silicon substrate. The devices display excellent dc and dynamic characteristics with values of threshold current density, differential gain, T0 and small signal modulation bandwidth equal to 1.76 kA/cm2, 3 × 10-17 cm2, 232 K, and 5.8 GHz respectively under continuous wave operation. Preliminary reliability measurements indicate a lifetime of 7000 h. The emission wavelength can be tuned by varying the alloy composition in the quantum disks. The monolithic nanowire laser on (001)Si can therefore address wide-ranging applications such as solid state lighting, displays, plastic fiber communication, medical diagnostics, and silicon photonics. © 2014 American Chemical Society.

  10. Front-end receiver electronics for high-frequency monolithic CMUT-on-CMOS imaging arrays.

    Science.gov (United States)

    Gurun, Gokce; Hasler, Paul; Degertekin, F

    2011-08-01

    This paper describes the design of CMOS receiver electronics for monolithic integration with capacitive micromachined ultrasonic transducer (CMUT) arrays for highfrequency intravascular ultrasound imaging. A custom 8-inch (20-cm) wafer is fabricated in a 0.35-μm two-poly, four-metal CMOS process and then CMUT arrays are built on top of the application specific integrated circuits (ASICs) on the wafer. We discuss advantages of the single-chip CMUT-on-CMOS approach in terms of receive sensitivity and SNR. Low-noise and high-gain design of a transimpedance amplifier (TIA) optimized for a forward-looking volumetric-imaging CMUT array element is discussed as a challenging design example. Amplifier gain, bandwidth, dynamic range, and power consumption trade-offs are discussed in detail. With minimized parasitics provided by the CMUT-on-CMOS approach, the optimized TIA design achieves a 90 fA/√Hz input-referred current noise, which is less than the thermal-mechanical noise of the CMUT element. We show successful system operation with a pulseecho measurement. Transducer-noise-dominated detection in immersion is also demonstrated through output noise spectrum measurement of the integrated system at different CMUT bias voltages. A noise figure of 1.8 dB is obtained in the designed CMUT bandwidth of 10 to 20 MHz.

  11. Red Emitting VCSEL

    Science.gov (United States)

    Jetter, Michael; Roßbach, Robert; Michler, Peter

    This chapter describes the progress in development of vertical-cavity surface-emitting lasers (VCSEL) emitting in the red spectral region around 650 nm for data transmission over polymer optical fibers (POF). First, growth issues of red VCSEL using two different material systems, namely AlGaAs and AlGaInP, are introduced. In particular, the optical and electrical state-of-the-art characteristics as low threshold currents ({≤} 1 mA) and high output powers (several mW) are presented with a special focus on emission wavelength. Also the thermal budget and heat removal in the devices are pointed out with regard to the geometry of the VCSEL. Small-signal modulation response in terms of maximum resonance frequency in dependance on temperature behavior are discussed. Applications of these devices in optical interconnects are described and digital data transmission at data rates up to 2.1 Gbit/s over step-index POF is reported. These properties make red emitting VCSEL perfectly suited for high-speed low power consuming light sources for optical data communication via POF. By introducing InP quantum dots as gain material in red emitting VCSEL nearly temperature independent record low threshold current densities of around 10 A/cm2 could be observed.

  12. A novel, SiPM-array-based, monolithic scintillator detector for PET.

    Science.gov (United States)

    Schaart, Dennis R; van Dam, Herman T; Seifert, Stefan; Vinke, Ruud; Dendooven, Peter; Löhner, Herbert; Beekman, Freek J

    2009-06-07

    Silicon photomultipliers (SiPMs) are of great interest to positron emission tomography (PET), as they enable new detector geometries, for e.g., depth-of-interaction (DOI) determination, are MR compatible, and offer faster response and higher gain than other solid-state photosensors such as avalanche photodiodes. Here we present a novel detector design with DOI correction, in which a position-sensitive SiPM array is used to read out a monolithic scintillator. Initial characterization of a prototype detector consisting of a 4 x 4 SiPM array coupled to either the front or back surface of a 13.2 mm x 13.2 mm x 10 mm LYSO:Ce(3+) crystal shows that front-side readout results in significantly better performance than conventional back-side readout. Spatial resolutions <1.6 mm full-width-at-half-maximum (FWHM) were measured at the detector centre in response to an approximately 0.54 mm FWHM diameter test beam. Hardly any resolution losses were observed at angles of incidence up to 45 degrees , demonstrating excellent DOI correction. About 14% FWHM energy resolution was obtained. The timing resolution, measured in coincidence with a BaF(2) detector, equals 960 ps FWHM.

  13. A novel, SiPM-array-based, monolithic scintillator detector for PET

    Energy Technology Data Exchange (ETDEWEB)

    Schaart, Dennis R; Dam, Herman T van; Seifert, Stefan; Beekman, Freek J [Delft University of Technology, Radiation Detection and Medical Imaging, Mekelweg 15, 2629 JB Delft (Netherlands); Vinke, Ruud; Dendooven, Peter; Loehner, Herbert [Kernfysisch Versneller Instituut, University of Groningen, Zernikelaan 25, 9747 AA, Groningen (Netherlands)], E-mail: d.r.schaart@tudelft.nl

    2009-06-07

    Silicon photomultipliers (SiPMs) are of great interest to positron emission tomography (PET), as they enable new detector geometries, for e.g., depth-of-interaction (DOI) determination, are MR compatible, and offer faster response and higher gain than other solid-state photosensors such as avalanche photodiodes. Here we present a novel detector design with DOI correction, in which a position-sensitive SiPM array is used to read out a monolithic scintillator. Initial characterization of a prototype detector consisting of a 4 x 4 SiPM array coupled to either the front or back surface of a 13.2 mm x 13.2 mm x 10 mm LYSO:Ce{sup 3+} crystal shows that front-side readout results in significantly better performance than conventional back-side readout. Spatial resolutions <1.6 mm full-width-at-half-maximum (FWHM) were measured at the detector centre in response to an {approx}0.54 mm FWHM diameter test beam. Hardly any resolution losses were observed at angles of incidence up to 45 deg., demonstrating excellent DOI correction. About 14% FWHM energy resolution was obtained. The timing resolution, measured in coincidence with a BaF{sub 2} detector, equals 960 ps FWHM.

  14. Effect of the presence of an ordered micro-pillar array on the formation of silica monoliths.

    Science.gov (United States)

    Detobel, Frederik; Eghbali, Hamed; De Bruyne, Selm; Terryn, Herman; Gardeniers, Han; Desmet, Gert

    2009-10-30

    We report on the synthesis of siloxane-based monoliths in the presence of a two-dimensional, perfectly ordered array of micro-pillars. Both methyltrimethoxysilane- and tetramethoxysilane-based monoliths were considered. The obtained structures were analyzed using scanning-electron microscopy and can be explained from the general theory of surface-directed phase separation in confined spaces. The formed structures are to a large extent nearly exclusively determined by the ratio between the bulk domain size of the monolith on the one hand and the distance between the micro-pillars on the other hand. When this ratio is small, the presence of the pillars has nearly no effect on the morphology of the produced monoliths. However, when the ratio approaches unity and ascends above it, some new types of monolith morphologies are induced, two of which appear to have interesting properties for use as novel chromatographic supports. One of these structures (obtained when the domain size/inter-pillar distance ratio is around unity) is a 3D network of linear interconnections between the pillars, organized such that all skeleton branches are oriented perpendicular to the micro-pillar surface. A second interesting structure is obtained at even higher values of the domain size/inter-pillar distance ratio. In this case, each individual micro-pillar is uniformly coated with a mesoporous shell.

  15. Single-mode and tunable VCSELs in the near- to mid-infraredInvited Paper

    Institute of Scientific and Technical Information of China (English)

    Markus-Christian Amann; Werner Hofmann

    2008-01-01

    @@ Single-mode, long-wavelength vertical-cavity surface-emitting lasers (VCSELs) in the near- to mid-infrared covering the wavelength range from 1.3 to 2.3μm are presented. This wide spectral emission range opens applications in gas sensing and optical interconnects. All these lasers are monolithically grown in the InGaA1As-InP material system utilizing a buried tunnel junction (BTJ) as current aperture. Fabricated with a novel high-speed design with reduced parasitics, bandwidths in excess of 10 GHz at 1.3 and 1.55 μm have been achieved. Therefore, the coarse wavelength division multiplexing (CWDM) wavelength range of 1.3 to 1.6 μm at 10 Gb/s can be accomplished with one technology. Error-free data-transmission at 10 Gb/s over a fiber link of 20 km is demonstrated. One-dimensional arrays have been fabricated with emission wavelengths addressable by current tuning. Micro-electro-mechanical system (MEMS) tunable devices provide an extended tuning range in excess of 50 nm with high spectral purity. All these devices feature continuous-wave (CW) operation with typical single-mode output powers exceeding 1 mW. The operation voltage is around 1 - 1.5 V and power consumption is as low as 10 - 20 mW. Furthermore, we have also developed VCSELs based on GaSb, targeting at the wavelength range from 2.3 to 3.0 μm. The functionality of tunable diode laser spectroscopy (TDLS) systems is shown by presenting a laser hygrometer applying a 1.84-μm VCSEL.

  16. Monolithic, High-Speed Fiber-Optic Switching Array for Lidar

    Science.gov (United States)

    Suckow, Will; Roberts, Tony; Switzer, Gregg; Terwilliger, Chelle

    2011-01-01

    Current fiber switch technologies use mechanical means to redirect light beams, resulting in slow switch time, as well as poor reliability due to moving parts wearing out quickly at high speeds. A non-mechanical ability to switch laser output into one of multiple fibers within a fiber array can provide significant power, weight, and costs savings to an all-fiber system. This invention uses an array of crystals that act as miniature prisms to redirect light as an electric voltage changes the prism s properties. At the heart of the electro-optic fiber-optic switch is an electro- optic crystal patterned with tiny prisms that can deflect the beam from the input fiber into any one of the receiving fibers arranged in a linear array when a voltage is applied across the crystal. Prism boundaries are defined by a net dipole moment in the crystal lattice that has been poled opposite to the surrounding lattice fabricated using patterned, removable microelectrodes. When a voltage is applied across the crystal, the resulting electric field changes the index of refraction within the prism boundaries relative to the surrounding substrate, causing light to deflect slightly according to Snell s Law. There are several materials that can host the necessary monolithic poled pattern (including, but not limited to, SLT, KTP, LiNbO3, and Mg:LiNbO3). Be cause this is a solid-state system without moving parts, it is very fast, and does not wear down easily. This invention is applicable to all fiber networks, as well as industries that use such networks. The unit comes in a compact package, can handle both low and high voltages, and has a high reliability (100,000 hours without maintenance).

  17. Design and fabrication of multi-channel photodetector array monolithic with arrayed waveguide grating

    Science.gov (United States)

    Qian-Qian, Lv; Pan, Pan; Han, Ye; Dong-Dong, Yin; Yu-Bing, Wang; Xiao-Hong, Yang; Qin, Han

    2016-03-01

    We have provided optical simulations of the evanescently coupled waveguide photodiodes integrated with a 13-channels AWGs. The photodiode could exhibit high internal efficiency by appropriate choice of layers geometry and refractive index. Aseamless joint structure has been designed and fabricated for integrating the output waveguides of AWGs with the evanescently coupled waveguide photodiode array. The highest simulation quantum efficiency could achieve 92% when the matching layer thickness of the PD is 120 nm and the insertion length is 2 μm. The fabricated PD with 320-nm-thick matching layer and 2-μm-length insertion matching layer present a responsivity of 0.87 A/W. Project supported by the National High Technology Research and Development Program of China (Grant Nos. 2013AA031401, 2015AA016902, and 2015AA016904), the National Natural Science Foundation of China (Grant Nos. 61176053, 61274069, and 61435002), and the National Basic Research Program of China (Grant Nos. 2012CB933503 and 2013CB932904).

  18. A new monolithic approach for mid-IR focal plane arrays

    Science.gov (United States)

    Xie, Chengzhi; Pusino, Vincenzo; Khalid, Ata; Aziz, Mohsin; Steer, Matthew J.; Cumming, David R. S.

    2016-10-01

    Antimonide-based photodetectors have recently been grown on a GaAs substrate by molecular beam epitaxy (MBE) and reported to have comparable performance to the devices grown on more expensive InSb and GaSb substrates. We demonstrated that GaAs, in addition to providing a cost saving substrate for antimonide-based semiconductor growth, can be used as a functional material to fabricate transistors and realize addressing circuits for the heterogeneously grown photodetectors. Based on co-integration of a GaAs MESFET with an InSb photodiode, we recently reported the first demonstration of a switchable and mid-IR sensible photo-pixel on a GaAs substrate that is suitable for large-scale integration into a focal plane array. In this work we report on the fabrication steps that we had to develop to deliver the integrated photo-pixel. Various highly controllable etch processes, both wet and dry etch based, were established for distinct material layers. Moreover, in order to avoid thermally-induced damage to the InSb detectors, a low temperature annealed Ohmic contact was used, and the processing temperature never exceeded 180 °C. Furthermore, since there is a considerable etch step (> 6 μm) that metal must straddle in order to interconnect the fabricated devices, we developed an intermediate step using polyimide to provide a smoothing section between the lower MESFET and upper photodiode regions of the device. This heterogeneous technology creates great potential to realize a new type of monolithic focal plane array of addressable pixels for imaging in the medium wavelength infrared range without the need for flip-chip bonding to a CMOS readout chip.

  19. High-power coherent phased array of monolithic flared amplifier-master oscillator power amplifiers (MFA-MOPAs)

    Science.gov (United States)

    Osinski, Jules S.; Mehuys, David G.; Welch, David F.; Dzurko, Kenneth M.; Lang, Robert J.

    1995-04-01

    A monolithically integrated array of InGaAs/AlGaAs flared amplifiers driven by a single DBR laser through a power splitter network and individually addressed phase modulators is described. Phase adjustment of > 2(pi) per element by free-carrier effects is verified by monitoring the interference pattern of 4 emitters, and typically requires 5 W, and, combined with the proper external lensing, could therefore result in an ultra-narrow, single-lobed far-field pattern whose width is determined by the extended aperture of the array. This architecture is capable of providing single-mode, diffraction-limited performance from each emitter and is scalable to unprecedented power levels. Over 20 W of pulsed, spectrally coherent emission is generated at 955 nm from a 4-element array, and 39 W is obtained from an 8-element array.

  20. VCSEL-based sensors for distance and velocity

    Science.gov (United States)

    Moench, Holger; Carpaij, Mark; Gerlach, Philipp; Gronenborn, Stephan; Gudde, Ralph; Hellmig, Jochen; Kolb, Johanna; van der Lee, Alexander

    2016-03-01

    VCSEL based sensors can measure distance and velocity in three dimensional space and are already produced in high quantities for professional and consumer applications. Several physical principles are used: VCSELs are applied as infrared illumination for surveillance cameras. High power arrays combined with imaging optics provide a uniform illumination of scenes up to a distance of several hundred meters. Time-of-flight methods use a pulsed VCSEL as light source, either with strong single pulses at low duty cycle or with pulse trains. Because of the sensitivity to background light and the strong decrease of the signal with distance several Watts of laser power are needed at a distance of up to 100m. VCSEL arrays enable power scaling and can provide very short pulses at higher power density. Applications range from extended functions in a smartphone over industrial sensors up to automotive LIDAR for driver assistance and autonomous driving. Self-mixing interference works with coherent laser photons scattered back into the cavity. It is therefore insensitive to environmental light. The method is used to measure target velocity and distance with very high accuracy at distances up to one meter. Single-mode VCSELs with integrated photodiode and grating stabilized polarization enable very compact and cost effective products. Besides the well know application as computer input device new applications with even higher accuracy or for speed over ground measurement in automobiles and up to 250km/h are investigated. All measurement methods exploit the known VCSEL properties like robustness, stability over temperature and the potential for packages with integrated optics and electronics. This makes VCSEL sensors ideally suited for new mass applications in consumer and automotive markets.

  1. Double high refractive-index contrast grating VCSEL

    Science.gov (United States)

    Gebski, Marcin; Dems, Maciej; Wasiak, Michał; Sarzała, Robert P.; Lott, J. A.; Czyszanowski, Tomasz

    2015-03-01

    Distributed Bragg reflectors (DBRs) are typically used as the highly reflecting mirrors of vertical-cavity surface-emitting lasers (VCSELs). In order to provide optical field confinement, oxide apertures are often incorporated in the process of the selective wet oxidation of high aluminum-content DBR layers. This technology has some potential drawbacks such as difficulty in controlling the uniformity of the oxide aperture diameters across a large-diameter (≥ 6 inch) production wafers, high DBR series resistance especially for small diameters below about 5 μm despite elaborate grading and doping schemes, free carrier absorption at longer emission wavelengths in the p-doped DBRs, reduced reliability for oxide apertures placed close to the quantum wells, and low thermal conductivity for transporting heat away from the active region. A prospective alternative mirror is a high refractive index contrast grating (HCG) monolithically integrated with the VCSEL cavity. Two HCG mirrors potentially offer a very compact and simplified VCSEL design although the problems of resistance, heat dissipation, and reliability are not completely solved. We present an analysis of a double HCG 980 nm GaAs-based ultra-thin VCSEL. We analyze the optical confinement of such a structure with a total optical thickness is ~1.0λ including the optical cavity and the two opposing and parallel HCG mirrors.

  2. MT-compatible red VCSEL module for parallel optical interconnections

    Science.gov (United States)

    Van Hove, An; Van de Putte, Koen; Naessens, Kris; Dhoedt, Bart; Baets, Roel G.; Van Daele, Peter

    2000-04-01

    In this paper we present the design, fabrication and characterization of a module which directly connectorizes a 1 by 8 red VCSEL array to a small diameter polymer optical fiber array, using a standard MT ferrule. The facets of the POF are prepared by a hot knife cutting, followed by a short polishing step. First coupling results show total losses in the range of 1.1 dB/channel for a 30 cm POF link. Optical crosstalk between adjacent channels is below -45 dB. Plastic micromachined parts surrounding the VCSEL chip ensure the correct alignment of the connector, using the connector, using the connector guiding points. The parts themselves are aligned to the chip with a n index-alignment technique, using an excimer laser ablated mastertool. In a deconnectorizable version of the module, a thin, flat glue layer on the chip acts as a window between the VCSEL chip and the MT terminated POF array. Integrated in a standard ceramic package, clear eye diagrams have been measured at 150 MHz for a 10m POF link, coupled to the VCSEL array. Further efforts on higher speed measurements using dedicated drivers, will also be presented.

  3. Reconfigurable optical switches with monolithic electrical-to-optical interfaces

    Energy Technology Data Exchange (ETDEWEB)

    Cheng, J.; Zhou, P. [New Mexico Univ., Albuquerque, NM (United States). Center for High Technology Materials; Zolper, J.C.; Lear, K.L.; Vawter, G.A. [Sandia National Labs., Albuquerque, NM (United States); Leibenguth, R.E.; Adams, A.C. [AT and T Bell Labs., Breinigsville, PA (United States)

    1994-03-01

    Vertical cavity surface-emitting lasers (VCSELs) can be integrated with heterojunction phototransistors (HPTs) and heterojunction bipolar transistors (HBTs) on the same wafer to form high speed optical and optoelectronic switches, respectively, that can be optically or electrically addressed. This permits the direct communication and transmission of data between distributed electronic processors through an optical switching network. The experimental demonstration of an integrated optoelectronic HBT/VCSEL switch combining a GaAs/AlGaAs heterojunction bipolar transistor (HBT) with a VCSEL is described below, using the same epilayer structure upon which binary HPT/VCSEL optical switches are also built. The monolithic HBT/VCSEL switch has high current gain, low power dissipation, and a high optical to electrical conversion efficiency. Its modulation has been measured and modeled.

  4. Monolithic LaBr₃:Ce crystals on silicon photomultiplier arrays for time-of-flight positron emission tomography.

    Science.gov (United States)

    Seifert, Stefan; van Dam, Herman T; Huizenga, Jan; Vinke, Ruud; Dendooven, Peter; Löhner, Herbert; Schaart, Dennis R

    2012-04-21

    Positron emission tomography detectors based on monolithic scintillation crystals exhibit good spatial and energy resolution, intrinsically provide depth-of-interaction information, have high γ-photon capture efficiency, and may reduce the manufacturing costs compared to pixelated crystal arrays. Here, we present the characterization of a detector consisting of a 18.0 mm×16.2 mm×10.0 mm monolithic LaBr₃:5%Ce scintillator directly coupled to a 4×4 array of silicon photomultipliers. An energy resolution of 6.4% full-width-at-half-maximum (FWHM) was obtained. The point-spread-function (PSF) was determined for different regions of the detector. The full-width-at-half-maximum (FWHM) of the PSF was measured to be <1.5 mm at the center of the detector and <1.7 mm averaged over the entire crystal. Both values are not corrected for the ~0.6 mm FWHM test beam diameter. Furthermore, the influence of edge effects was investigated. We found that near the edges of the detector the spatial resolution degrades to 2.2 mm (FWHM), and a bias in the position estimates, up to 1.5 mm, was observed. Moreover, the coincidence resolving time for two identical detectors in coincidence was measured to be as small as ~198 ps FWHM.

  5. Monolithic Multi-Colour 40 GHz Mode-Locked Laser Array

    OpenAIRE

    Hou, Lianping; Eddie, Iain; Marsh, John

    2016-01-01

    The monolithic integration of four 40 GHz multi-colored mode-locked lasers with a 4×1 MMI, four electroabsorption modulators and an SOA has been demonstrated. The shortest pulse widths are between 2.63 and 2.85 ps.

  6. 1550-nm wavelength-tunable HCG VCSELs

    Science.gov (United States)

    Chase, Christopher; Rao, Yi; Huang, Michael; Chang-Hasnain, Connie

    2014-02-01

    We demonstrate wavelength-tunable VCSELs using high contrast gratings (HCGs) as the top output mirror on VCSELs, operating at 1550 nm. Tunable HCG VCSELs with a ~25 nm mechanical tuning range as well as VCSELs with 2 mW output power were realized. Error-free operation of an optical link using directly-modulated tunable HCG VCSELs transmitting at 1.25 Gbps over 18 channels spaced by 100 GHz and transmitted over 20 km of single mode fiber is demonstrated, showing the suitability of the HCG tunable VCSEL as a low cost source for WDM communications systems.

  7. Monolithic watt-level millimeter-wave diode-grid frequency tripler array

    Science.gov (United States)

    Hwu, R. J.; Luhmann, N. C., Jr.; Rutledge, D. B.; Hancock, B.; Lieneweg, U.

    1988-01-01

    In order to provide watt-level CW output power throughout the millimeter and submillimeter wave region, thousands of solid-state diodes have been monolithically integrated using a metal grid to produce a highly efficient frequency multiplier. Devices considered include GaAs Schottky diodes, thin MOS diodes, and GaAs Barrier-Intrinsic-N(+)diodes. The performance of the present compact low-cost device has been theoretically and experimentally validated.

  8. Multiplexed gas spectroscopy using tunable VCSELs

    Energy Technology Data Exchange (ETDEWEB)

    Bond, T; Bond, S; McCarrick, J; Zumstein, J; Chang, A; Moran, B; Benett, W J

    2012-04-10

    Detection and identification of gas species using tunable laser diode laser absorption spectroscopy has been performed using vertical cavity surface emitting lasers (VCSEL). Two detection methods are compared: direct absorbance and wavelength modulation spectroscopy (WMS). In the first, the output of a DC-based laser is directly monitored to detect for any quench at the targeted specie wavelength. In the latter, the emission wavelength of the laser is modulated by applying a sinusoidal component on the drive current of frequency {omega}, and measuring the harmonics component (2{omega}) of the photo-detected current. This method shows a better sensitivity measured as signal to noise ratio, and is less susceptible to interference effects such as scattering or fouling. Gas detection was initially performed at room temperature and atmospheric conditions using VCSELs of emission wavelength 763 nm for oxygen and 1392 nm for water, scanning over a range of approximately 10 nm, sufficient to cover 5-10 gas specific absorption lines that enable identification and quantization of gas composition. The amplitude and frequency modulation parameters were optimized for each detected gas species, by performing two dimensional sweeps for both tuning current and either amplitude or frequency, respectively. We found that the highest detected signal is observed for a wavelength modulation amplitude equal to the width of the gas absorbance lines, in good agreement with theoretical calculations, and for modulation frequencies below the time response of the lasers (<50KHz). In conclusion, we will discuss limit of detection studies and further implementation and packaging of VCSELs in diode arrays for continuous and simultaneous monitoring of multiple species in gaseous mixtures.

  9. A 1.55-μm laser array monolithically integrated with an MMI combiner

    Institute of Scientific and Technical Information of China (English)

    Ma Li; Zhu Hongliang; Liang Song; Wang Baojun; Zhang Can; Zhao Lingjuan; Bian Jing

    2013-01-01

    The monolithic integration of four 1.55-μm range InGaAsP/InP distributed feedback lasers with a 4 × 1multimode-interference (MMI) optical combiner using the varied width ridge method is proposed and demonstrated.The average output power is 1.5 mW when the current of LD is 100 mA and the threshold current is 30-35 mA at 25 ℃.The lasing wavelength is 1.55-μm range and 40 dB sidemode suppression ratio is obtained.The four channels can operate separately or simultaneously.

  10. On the Application of a Monolithic Array for Detecting Intensity-Correlated Photons Emitted by Different Source Types

    CERN Document Server

    Boiko, D L; Brauer, N; Sergio, M; Niclass, C; Beretta, G B; Charbon, E

    2009-01-01

    It is not widely appreciated that many subtleties are involved in the accurate measurement of intensity-correlated photons; even for the original experiments of Hanbury Brown and Twiss (HBT). Using a monolithic 4x4 array of single-photon avalanche diodes (SPADs), together with an off-chip algorithm for processing streaming data, we investigate the difficulties of measuring second-order photon correlations g2 in a wide variety of light fields that exhibit dramatically different correlation statistics: a multimode He-Ne laser, an incoherent intensity-modulated lamp-light source and a thermal light source. Our off-chip algorithm treats multiple photon-arrivals at pixel-array pairs, in any observation interval, with photon fluxes limited by detector saturation, in such a way that a correctly normalized g2 function is guaranteed. The impact of detector background correlations between SPAD pixels and afterpulsing effects on second-order coherence measurements is discussed. These results demonstrate that our monolit...

  11. Monolithic millimeter-wave diode array beam controllers: Theory and experiment

    Science.gov (United States)

    Sjogren, L. B.; Liu, H.-X. L.; Wang, F.; Liu, T.; Wu, W.; Qin, X.-H.; Chung, E.; Domier, C. W.; Luhmann, N. C., Jr.; Maserjian, J.

    1992-01-01

    In the current work, multi-function beam control arrays have been fabricated and have successfully demonstrated amplitude control of transmitted beams in the W and D bands (75-170 GHz). While these arrays are designed to provide beam control under DC bias operation, new designs for high-speed electronic and optical control are under development. These arrays will fill a need for high-speed watt-level beam switches in pulsed reflectometer systems under development for magnetic fusion plasma diagnostics. A second experimental accomplishment of the current work is the demonstration in the 100-170 GHz (D band) frequency range of a new technique for the measurement of the transmission phase as well as amplitude. Transmission data can serve as a means to extract ('de-embed') the grid parameters; phase information provides more complete data to assist in this process. Additional functions of the array beam controller yet to be tested include electronically controlled steering and focusing of a reflected beam. These have application in the areas of millimeter-wave electronic scanning radar and reflectometry, respectively.

  12. Cobalt phosphide nanowall arrays supported on carbon cloth: an efficient monolithic non-noble-metal hydrogen evolution catalyst

    Science.gov (United States)

    Yang, Libin; Wang, Kunyang; Du, Gu; Zhu, Wenxin; Cui, Liang; Zhang, Chengxiao; Sun, Xuping; Asiri, Abdullah M.

    2016-11-01

    Hydrogen has been considered as an ideal energy carrier for replacing fossil fuels to mitigate global energy crises. Hydrolysis of sodium borohydride (NaBH4) is simple and effective for hydrogen production but needs active and durable catalysts to accelerate the kinetics. In this paper, we demonstrate that cobalt phosphide nanowall arrays supported on carbon cloth (CoP NAs/CC) efficiently catalyze the hydrolytic dehydrogenation of NaBH4 with an activation energy of 42.1 kJ mol-1 in alkaline media. These monolithic CoP NAs/CC show a maximum hydrogen generation rate of 5960 {{ml}} {{{\\min }}}-1 {{{{g}}}-1}({{CoP})} and are robust with superior durability and reusability. They are also excellent in activity and durability for electrochemical hydrogen evolution in 1.0 M KOH, with the need of an overpotential of only 80 mV to drive 10 mA cm-2. They offer us a promising low-cost hydrogen-generating catalyst for applications.

  13. Coincidence detection of spatially correlated photon pairs with a monolithic time-resolving detector array

    CERN Document Server

    Unternährer, Manuel; Gasparini, Leonardo; Stoppa, David; Stefanov, André

    2016-01-01

    We demonstrate coincidence measurements of spatially entangled photons by means of a novel type of multi-pixel based detection array. The adopted sensor is a fully digital 8$\\times$16 silicon photomultiplier array allowing not only photon counting but also per-pixel time stamping of the arrived photons with a resolution of 65 ps. Together with a frame rate of 500 kfps, this property exceeds the capabilities of conventional charge-coupled device cameras which have become of growing interest for the detection of transversely correlated photon pairs. The sensor is used to measure a second-order correlation function for various non-collinear configurations of entangled photons generated by spontaneous parametric down-conversion. The experimental results are compared to theory.

  14. Monolithic photovotaic PbS-on-Si infrared-sensor array

    Energy Technology Data Exchange (ETDEWEB)

    Masek, J.; Zogg, H.; Maissen, C.; Blunier, S. (Arbeitsgemeinschaft fur Industrielle Forschung, Swiss Federal Inst. of Tech., ETH-Honggerberg, CH-8093 Zurich (CH)); Ishida, A. (Shizuoka Univ., Hamamatsu (Japan). Faculty of Engineering)

    1990-01-01

    The authors have grown epitaxial narrow-gap PbS-on-Si substrates using a stacked CaF{sub 2}-BaF{sub 2} intermediate buffer layer, and have fabricated linear arrays of photovoltaic infrared (IR) sensors in the PbS layer for the first time. The sensors of the array exhibit resistance-area products at zero bias of 3{Omega}{center dot}cm{sup 2} at 200 K (3.4-{mu}m cutoff wavelength) and 2{center dot}10{sup 5} {Omega}{center dot}cm{sup 2} at 84 K (4-{mu}m cutoff), with corresponding detectivities of 2{center dot}10{sup 10} and 1{center dot}10{sup 13}cm{center dot}{radical}Hz/W, respectively.

  15. Study of the Radiation-Hardness of VCSEL and PIN

    CERN Document Server

    Gan, K K; Fernando, W; Kagan, H P; Kass, R D; Lebbai, M R M; Merritt, H; Moore, J R; Nagarkar, A; Rizatdinova, F; Skubic, P L; Smith, D S; Strang, M

    2009-01-01

    The silicon trackers of the ATLAS experiment at the Large Hadron Collider (LHC) at CERN (Geneva) use optical links for data transmission. An upgrade of the trackers is planned for the Super LHC (SLHC), an upgraded LHC with ten times higher luminosity. We study the radiation-hardness of VCSELs (Vertical-Cavity Surface-Emitting Laser) and GaAs and silicon PINs using 24 GeV/c protons at CERN for possible application in the data transmission upgrade. The optical power of VCSEL arrays decreases significantly after the irradiation but can be partially annealed with high drive currents. The responsivities of the PIN diodes also decrease significantly after irradiation, but can be recovered by operating at higher bias voltage. This provides a simple mechanism to recover from the radiation damage.

  16. Developments of VCSELs for printers and optical communications at Fuji Xerox

    Science.gov (United States)

    Kondo, Takashi; Takeda, Kazutaka; Otoma, Hiromi; Murakami, Akemi; Sakurai, Jun; Nakayama, Hideo; Gu, Xiaodong; Koyama, Fumio

    2016-03-01

    We review the characteristics of vertical-cavity surface-emitting lasers (VCSELs) for use in printers and optical communications. In 2003, we launched the world's first laser printer with a 780-nm single-mode 8×4 VCSEL array introduced to the light exposure system in order to meet the market demands for improving the image quality and speed for laser printers. The design of the VCSEL array enabled us to increase the pixel density and the printing speed by projecting 32 beams at a time to the photoconductor in the exposure process. High uniformity with less than 5% of variation has been achieved for both the optical output and the divergence angle. Currently, our high-end color printer is capable of producing the resolution of 2400 dpi (dots per inch) at the speed of 137 ppm (pages per minute). In the field of optical interconnections and networks, 850-nm VCSELs are needed as high-speed optical transmitters (>=10Gbps). In order to address communication traffic that will increase further as well as to reduce their power consumption to an even lower level, we assessed the lasing characteristics of 850-nm VCSELs with InGaAs strained quantum-well (QW) active layers by changing the ratio of Indium composition. As a result, we succeeded in reducing the power consumption per bit to 43 fJ/bit at 10-Gbps, which is much lower than that of commercial GaAs QW VCSELs. Also, we studied 850-nm transverse-coupled-cavity VCSELs, which enabled us to achieve a high 3dB modulation bandwidth (>23 GHz) and realize eye-openings at the large-signal modulation rate of 36 Gbps.

  17. Monolithic LaBr3 : Ce crystals on silicon photomultiplier arrays for time-of-flight positron emission tomography

    NARCIS (Netherlands)

    Seifert, Stefan; van Dam, Herman T.; Huizenga, Jan; Vinke, Ruud; Dendooven, Peter; Löhner, Herbert; Schaart, Dennis R.

    2012-01-01

    Positron emission tomography detectors based on monolithic scintillation crystals exhibit good spatial and energy resolution, intrinsically provide depth-of-interaction information, have high gamma-photon capture efficiency, and may reduce the manufacturing costs compared to pixelated crystal

  18. Chip-based molecularly imprinted monolithic capillary array columns coated GO/SiO2 for selective extraction and sensitive determination of rhodamine B in chili powder.

    Science.gov (United States)

    Zhai, Haiyun; Huang, Lu; Chen, Zuanguang; Su, Zihao; Yuan, Kaisong; Liang, Guohuan; Pan, Yufang

    2017-01-01

    A novel solid-phase extraction chip embedded with array columns of molecularly imprinted polymer-coated silanized graphene oxide (GO/SiO2-MISPE) was established to detect trace rhodamine B (RB) in chili powder. GO/SiO2-MISPE monolithic columns for RB detection were prepared by optimizing the supporting substrate, template, and polymerizing monomer under mild water bath conditions. Adsorption capacity and specificity, which are critical properties for the application of the GO/SiO2-MISPE monolithic column, were investigated. GO/SiO2-MIP was examined by scanning electron microscopy (SEM) and Fourier transform-infrared spectroscopy. The recovery and the intraday and interday relative standard deviations for RB ranged from 83.7% to 88.4% and 2.5% to 4.0% and the enrichment factors were higher than 110-fold. The chip-based array columns effectively eliminated impurities in chili powder, indicating that the chip-based GO/SiO2-MISPE method was reliable for RB detection in food samples using high-performance liquid chromatography. Accordingly, this method has direct applications for monitoring potentially harmful dyes in processed food.

  19. 130-nm tunable grating-mirror VCSEL

    DEFF Research Database (Denmark)

    Chung, Il-Sug; Mørk, Jesper

    2014-01-01

    We have reported that a combination of the high-index-contrast grating (HCG) mirror as movable mirror and the extended cavity configuration with an antireflection layer can provide a tuning wavelength range of 100 nm for tunable VCSELs. Here, we report that using the air-coupled cavity configurat......We have reported that a combination of the high-index-contrast grating (HCG) mirror as movable mirror and the extended cavity configuration with an antireflection layer can provide a tuning wavelength range of 100 nm for tunable VCSELs. Here, we report that using the air-coupled cavity...... configuration instead of the extended cavity configuration can bring 130-nm tuning range around 1330-nm wavelength. The air-coupled cavity is known to reduce the quantum confinement factor in VCSELs, increasing threshold. In our air-coupled cavity HCG VCSEL case, the very short power penetration length...

  20. SU-E-T-163: Characterization of a Novel High Resolution 1D Silicon Monolithic Array for Small Field Commissioning and Quality Assurance

    Energy Technology Data Exchange (ETDEWEB)

    Bisello, F [FAU University Erlangen-Nuernberg, Erlangen, DE (Germany); IBA Dosimetry, Schwarzenbruck, DE (United States); McGlade, J; Wang, P; Kralik, J; Kosterin, P; Mooij, R; Solberg, T [University of Pennsylvenia, Philadelphia, PA (United States); Menichelli, D; Celi, J [IBA Dosimetry, Schwarzenbruck, DE (United States)

    2015-06-15

    Purpose: To study the suitability of a novel 1D silicon monolithic array for dosimetry of small radiation fields and for QA of high dose gradient treatment modalities (IMRT and SBRT). Methods: A 1D array composed of 4 monolithic silicon modules of 64 mm length and 1 mm pixel pitch was developed by IBA Dosimetry. Measurements were carried out for 6MV and 15MV photons on two commercial different linacs (TrueBeam and Clinac iX, Varian Medical Systems, Palo Alto, CA) and for a CyberKnife G4 (Accuray Inc., Sunnyvale, CA). The 1D array was used to measure output factors (OF), profiles and off axis correction factors (OACF) for the Iris CyberKnife variable collimator (5–60 mm). In addition, dose profiles (at the isocenter plane) were measured for multiple IMRT and SBRT treatment plans and compared with those obtained using EDR2radiographic film (Carestream Health, Rochester NY), a commercial 2D diode array and with the dose distribution calculated using a commercial TPS (Eclipse, Varian Medical Systems, Palo Alto, CA). Results: Due to the small pixel pitch of the detector, IMRT and SBRT plan profiles deviate from film measurements by less than 2%. Similarly, the 1D array exhibits better performance than the 2D diode array due to the larger (7 mm) pitch of that device. Iris collimator OFs measured using the 1D silicon array are in good agreement with the commissioning values obtained using a commercial stereotactic diode as well as with published data. Maximum deviations are < 3% for the smallest field (5 and 7.5mm) and below 1% for all other dimensions. Conclusion: We have demonstrated good performances of the array for commissioning of small photon fields and in patient QA, compared with diodes and film typically used in these clinical applications. The technology compares favorably with existing commercial solutions The presenting author is founded by a Marie Curie Early Initial Training Network Fellowship of the European Communitys Seventh Framework Programme under

  1. VCSELs for optical communication at Fuji Xerox

    Science.gov (United States)

    Kondo, Takashi; Hayakawa, Junichiro; Jogan, Naoki; Murakami, Akemi; Sakurai, Jun; Gu, Xiaodong; Koyama, Fumio

    2017-02-01

    We introduce the characteristics of vertical-cavity surface-emitting lasers (VCSELs) for use in optical communications. In the field of optical interconnections and networks, 850 nm VCSELs are key optical transmitters due to their high-speed modulation and low power consumption. One promising candidate for achieving high-speed modulations exceeding 50 Gbps is the transverse-coupled-cavity (TCC) VCSEL. In this talk, we demonstrate the characteristics of 850 nm transverse-coupled-cavity VCSELs, which helped us achieve a high 3dB modulation bandwidth (30 GHz) at 0 °C and realize eye-opening at the large-signal modulation rate of 48 Gbps. The VCSEL's epilayer structure was grown by MOCVD. The active region consists of three strained InGaAs QWs surrounded by AlGaAs barriers. The n-type and p-type DBRs are composed of AlGaAs/AlGaAs, respectively. A line-shaped H+ ion was implanted at the center of the bowtie-shaped post, dividing it into two cavities. The threshold current of the TCC VCSEL with an oxide aperture of 3.6 μm is 0.33 mA. Only the left-side cavity is pumped, while the right cavity is unpumped. The effect of modulation bandwidth enhancement was observed over a wide temperature range of 120K thanks to an optical feedback in the coupled cavities. These results show the possibility of achieving high-speed VCSELs without any temperature or bias control. We also demonstrate an ultra-compact photodetector-integrated VCSEL with two laterally-coupled cavities. An output power and a photocurrent exhibit similar tendencies under a wide range of temperature changes. This device could be also used for monitoring output power without a conventional photodetector mounted separately.

  2. Development of a large-area monolithic 4x4 MPPC array for a future PET scanner employing pixelized Ce:LYSO and Pr:LuAG crystals

    Energy Technology Data Exchange (ETDEWEB)

    Kato, T., E-mail: katou.frme.8180@asagi.waseda.j [Research Institute for Science and Engineering, Waseda University, 3-4-1, Ohkubo, Shinjuku, Tokyo (Japan); Kataoka, J.; Nakamori, T.; Miura, T.; Matsuda, H. [Research Institute for Science and Engineering, Waseda University, 3-4-1, Ohkubo, Shinjuku, Tokyo (Japan); Sato, K.; Ishikawa, Y.; Yamamura, K.; Kawabata, N. [Solid State Division, Hamamatsu Photonics K. K., 1126-1, Ichino-cho, Hamamatsu, Shizuoka (Japan); Ikeda, H.; Sato, G. [ISAS/JAXA, 3-1-1, Yoshinodai, Chuo-ku, Sagamihara-shi, Kanagawa (Japan); Kamada, K. [Materials Research Laboratory, Furukawa Co., Ltd., 1-25-13, Kannondai, Tsukuba, Ibaraki 305-0856 (Japan)

    2011-05-11

    We have developed a new type of large-area monolithic Multi-Pixel Photon Counter (MPPC) array consisting of a 4x4 matrix of 3x3 mm{sup 2} pixels. Each pixel comprises 3600 Geiger mode avalanche photodiodes (APDs) that achieve an average gain of 9.68x10{sup 5} at 71.9 V at 0 {sup o}C with variations of only {+-}7.2% over 4x4 pixels. Excellent uniformity was also obtained for photon detection efficiencies (PDE) of {+-}6.4%, whilst dark count rates at the single photoelectron (1 p.e.) level amounted to {approx_equal}2Mcps/pixel, measured at 0 {sup o}C. As the first step toward using the device in scintillation photon detectors, we fabricated a prototype gamma-ray camera consisting of an MPPC array optically coupled with a scintillator matrix, namely a 4x4 array of 3x3 x10 mm{sup 3} crystals. Specifically, we tested the performance with Ce-doped (Lu, Y){sub 2}(SiO{sub 4})O (Ce:LYSO), Pr-doped Lu{sub 3}Al{sub 5}O{sub 12} (Pr:LuAG) and 'surface coated' Pr:LuAG (Pr:LuAG (WLS)) matrices whereby the emission peak of Pr:LuAG was shifted from 310 to 420 nm via a wavelength shifter (WLS). Average energy resolutions of 13.83%, 14.70% and 13.96% (FWHM) were obtained for 662 keV gamma-rays, as measured at 0 {sup o}C with Ce:LYSO, Pr:LuAG and Pr:LuAG (WLS) scintillator matrices, respectively. We confirmed that the effective PDE for Pr:LuAG (WLS) had improved by more than 30% compared to original, non-coated Pr:LuAG matrix. These results suggest that a large-area monolithic MPPC array developed here could be promising for future medical imaging, particularly in positron emission tomography (PET).

  3. Monolithic Integration of GaN-based LEDs

    Energy Technology Data Exchange (ETDEWEB)

    Ao, Jin-Ping, E-mail: jpao@ee.tokushima-u.ac.jp [Institute of Technology and Science, University of Tokushima 2-1 Minami-Josanjima, Tokushima 770-8506 (Japan)

    2011-02-01

    The technology of monolithically integrated GaN-based light-emitting diodes (LEDs) is reported. First, the technology details to realize monolithic integration are described, including the circuit design for high-voltage and alternating current (AC) operation and the technologies for device isolation. The performances of the fabricated monolithic LED arrays are then demonstrated. A monolithic series array with totally 40 LEDs exhibited expected operation function under AC bias. The operation voltage of the array is 72 V when 20 LEDs were connected in series. Some modified circuit designs for high-voltage operation and other monolithic LED arrays are finally reviewed.

  4. Solution-based photodetectors for monolithically integrated low-cost short-wave infrared focal plane arrays

    Science.gov (United States)

    Heves, Emre; Kayahan, Huseyin; Gurbuz, Yasar

    2013-05-01

    In this work, PbS Colloidal Quantum Dots (CQD) based photodiodes are realized on both silicon substrates and on the replicas of the ROICs in order to demonstrate fully integrated FPAs. Careful optimization of PbS CQD film formation and ligand exchange process, together with optimization of IC integrable process steps resulted in high performance, monolithically integrable photodiodes. High quantum efficiencies such as 32% is achieved for photodiodes on Si substrates and high responsivities up to 5,73 A/W is achieved for photodiodes on ROIC replicas. Also these detectors achieved very high normalized detectivities such as; 1.36 x 1011 Jones and 1.42 x 1012 Jones under 1V and 2V reverse bias respectively, which is close to conventional InGaAS SWIR detectors.

  5. Modulator and VCSEL-MSM smart pixels for parallel pipeline networking and signal processing

    Science.gov (United States)

    Chen, C.-H.; Hoanca, Bogdan; Kuznia, C. B.; Pansatiankul, Dhawat E.; Zhang, Liping; Sawchuk, Alexander A.

    1999-07-01

    TRANslucent Smart Pixel Array (TRANSPAR) systems perform high performance parallel pipeline networking and signal processing based on optical propagation of 3D data packets. The TRANSPAR smart pixel devices use either self-electro- optic effect GaAs multiple quantum well modulators or CMOS- VCSEL-MSM (CMOS-Vertical Cavity Surface Emitting Laser- Metal-Semiconductor-Metal) technology. The data packets transfer among high throughput photonic network nodes using multiple access/collision detection or token-ring protocols.

  6. Speed enhancement in VCSELs employing grating mirrors

    DEFF Research Database (Denmark)

    Chung, Il-Sug; Mørk, Jesper

    2013-01-01

    In recent years, various approaches to improve the speed of directly modulated vertical-cavity surface-emitting lasers (VCSELs) have been reported and demonstrated good improvement. In this paper, we propose and numerically investigate a new possibility of using high-index-contrast grating (HCG...

  7. Polarization properties of localized structures in VCSELs

    Science.gov (United States)

    Averlant, Etienne; Tlidi, Mustapha; Ackemann, Thorsten; Thienpont, Hugo; Panajotov, Krassimir

    2016-04-01

    Broad area Vertical-Cavity Surface-Emitting Lasers (VCSELs) have peculiar polarization properties which are a field of study by itself.1-3 These properties have already been used for localized structure generation, in a simple configuration, where only one polarization component was used.4 Here, we present new experimental and theoretical results on the complex polarization behavior of localized structures generated in an optically-injected broad area VCSEL. A linear stability analysis of the spin-flip VCSEL model is performed for the case of broad area devices, in a restrained and experimentally relevant parameter set. Numerical simulations are performed, in one and two dimensions. They reveal existence of vector localized structures. These structures have a complex polarization state, which is not simply a linear polarization following the one of the optical injection. Experimental results confirm theoretical predictions. Applications of this work can lead to the encoding of small color images in the polarization state of an ensemble of localized structures at the surface of a broad area VCSEL.

  8. A novel gamma-ray detector with submillimeter resolutions using a monolithic MPPC array with pixelized Ce:LYSO and Ce:GGAG crystals

    Energy Technology Data Exchange (ETDEWEB)

    Kato, T., E-mail: katou.frme.8180@asagi.waseda.jp [Research Institute for Science and Engineering, Waseda University, 3-4-1, Ohkubo, Shinjuku, Tokyo (Japan); Kataoka, J.; Nakamori, T.; Miura, T.; Matsuda, H.; Kishimoto, A. [Research Institute for Science and Engineering, Waseda University, 3-4-1, Ohkubo, Shinjuku, Tokyo (Japan); Sato, K.; Ishikawa, Y.; Yamamura, K.; Nakamura, S.; Kawabata, N. [Solid State Division, Hamamatsu Photonics K. K., 1126-1, Ichino-cho, Hamamatsu, Shizuoka (Japan); Ikeda, H. [ISAS/JAXA, 3-1-1, Yoshinodai, Chuo-ku, Sagamihara-shi, Kanagawa (Japan); Yamamoto, S. [Kobe City College of Technology, 8-3, Gakuenhigashimati, Nishi-ku, Kobe-shi, Hyougo 651-2194 (Japan); Kamada, K. [Materials Research Laboratory, Furukawa Co., Ltd., 1-25-13, Kannondai, Tsukuba, Ibaraki 305-0856 (Japan)

    2013-01-21

    We have developed a large-area monolithic Multi-Pixel Photon Counter (MPPC) array consisting of 4×4 channels with a three-side buttable package. Each channel has a photosensitive area of 3×3 mm{sup 2} and 3600 Geiger mode avalanche photodiodes (APDs). For typical operational gain of 7.5×10{sup 5} at +20 °C, gain fluctuation over the entire MPPC device is only ±5.6%, and dark count rates (as measured at the 1 p.e. level) amount to ≤400kcps per channel. We first fabricated a gamma-ray camera consisting of the MPPC array with one-to-one coupling to a Ce-doped (Lu,Y){sub 2}(SiO{sub 4})O (Ce:LYSO) crystal array (4×4 array of 3×3×10 mm{sup 3} crystals). Energy and time resolutions of 11.5±0.5% (FWHM at 662 keV) and 493±22ps were obtained, respectively. When using the charge division resistor network, which compiles signals into four position-encoded analog outputs, the ultimate positional resolution is estimated as 0.19 mm in both X and Y directions, while energy resolution of 10.2±0.4% (FWHM) was obtained. Finally, we fabricated submillimeter Ce:LYSO and Ce-doped Gd{sub 3}Ga{sub 3}Al{sub 2}O{sub 12} (Ce:GGAG) scintillator matrices each consisting of 1.0×1.0, 0.7×0.7 and 0.5×0.5 mm{sup 2} pixels, to further improve the spatial resolution. In all types of Ce:LYSO and Ce:GGAG matrices, each crystal was clearly resolved in the position histograms when irradiated by a {sup 137}Cs source. The energy resolutions for 662 keV gamma-rays for each Ce:LYSO and Ce:GGAG scintillator matrix were ≤14.3%. These results suggest excellent potential for its use as a high spatial medical imaging device, particularly in positron emission tomography (PET). -- Highlights: ► We developed a newly designed large-area monolithic MPPC array. ► We obtained fine gain uniformity, and good energy and time resolutions when coupled to the LYSO scintillator. ► We fabricated gamma-ray camera consisting of the MPPC array and submillimeter pixelized LYSO and GGAG scintillators. ► In

  9. Monolithic spectrometer

    Science.gov (United States)

    Rajic, Slobodan; Egert, Charles M.; Kahl, William K.; Snyder, Jr., William B.; Evans, III, Boyd M.; Marlar, Troy A.; Cunningham, Joseph P.

    1998-01-01

    A monolithic spectrometer is disclosed for use in spectroscopy. The spectrometer is a single body of translucent material with positioned surfaces for the transmission, reflection and spectral analysis of light rays.

  10. Numerical methods for modeling photonic-crystal VCSELs

    DEFF Research Database (Denmark)

    Dems, Maciej; Chung, Il-Sug; Nyakas, Peter

    2010-01-01

    We show comparison of four different numerical methods for simulating Photonic-Crystal (PC) VCSELs. We present the theoretical basis behind each method and analyze the differences by studying a benchmark VCSEL structure, where the PC structure penetrates all VCSEL layers, the entire top-mirror DBR...... to the effective index method. The simulation results elucidate the strength and weaknesses of the analyzed methods; and outline the limits of applicability of the different models....

  11. Comparison of Stability-Indicating LC Methods Using Light Scattering and Photodiode Array Detection with Monolithic Column for Determination of Quinapril and Hydrochlorothiazide.

    Science.gov (United States)

    de Diego, Marta; Godoy, Ricardo; Mennickent, Sigrid; Vergara, Carola; Charnock, Henry; Hernández, Camilo

    2016-09-01

    Rapid stability-indicating LC methods for simultaneous analysis of quinapril and hydrochlorothiazide were developed, validated and compared using evaporative light scattering detection (ELSD) and diode array detection (DAD). For the separation of quinapril, hydrochlorothiazide and its major degradation products, a monolithic column was used and the analytes were eluted within 7 min, applying gradient mobile phase in both methods. Quinapril was subjected to hydrolytic, oxidative, thermal, humidity and photolytic stress conditions. Degradation products were well resolved from main peaks and from each other, proving the stability-indicating power of the methods. The response with DAD was linear and the response with ELSD was fitted to a power function, for quinapril and hydrochlorothiazide concentrations of 20-160 and 12.5-100 µg mL(-1), respectively. DAD method achieved better precision than ELSD method, the LOQ of DAD was lower and the accuracy of the methods was similar. Quinapril degrade by hydrolysis and thermal stress, showing the formation of quinaprilat and quinapril diketopiperazine as degradants, which were identified by MS-MS. The methods were successfully applied to quantify quinapril and hydrochlorothiazide in commercial tablets. LC-DAD and LC-ELSD methods are suitable to assess the stability and routine analysis of quinapril and hydrochlorothiazide in pharmaceutical industry.

  12. Monolithic integration of a silicon nanowire field-effect transistors array on a complementary metal-oxide semiconductor chip for biochemical sensor applications.

    Science.gov (United States)

    Livi, Paolo; Kwiat, Moria; Shadmani, Amir; Pevzner, Alexander; Navarra, Giulio; Rothe, Jörg; Stettler, Alexander; Chen, Yihui; Patolsky, Fernando; Hierlemann, Andreas

    2015-10-06

    We present a monolithic complementary metal-oxide semiconductor (CMOS)-based sensor system comprising an array of silicon nanowire field-effect transistors (FETs) and the signal-conditioning circuitry on the same chip. The silicon nanowires were fabricated by chemical vapor deposition methods and then transferred to the CMOS chip, where Ti/Pd/Ti contacts had been patterned via e-beam lithography. The on-chip circuitry measures the current flowing through each nanowire FET upon applying a constant source-drain voltage. The analog signal is digitized on chip and then transmitted to a receiving unit. The system has been successfully fabricated and tested by acquiring I-V curves of the bare nanowire-based FETs. Furthermore, the sensing capabilities of the complete system have been demonstrated by recording current changes upon nanowire exposure to solutions of different pHs, as well as by detecting different concentrations of Troponin T biomarkers (cTnT) through antibody-functionalized nanowire FETs.

  13. 10 Gb/s 1550 nm VCSEL transmission over 23.6 km SMF with no Dispersion Compensation and no Injection Locking for WDM PONs

    DEFF Research Database (Denmark)

    Gibbon, Timothy Braidwood; Prince, Kamau; Neumeyer, Christian;

    2010-01-01

    demonstrate 10Gb/s VCSEL transmission for WDM PON over 23.6km single mode fiber. Dispersion penalty is limited to 2.9dB by introducing a wavelength offset with respect to the remote array waveguide grating to reduce chirp.......demonstrate 10Gb/s VCSEL transmission for WDM PON over 23.6km single mode fiber. Dispersion penalty is limited to 2.9dB by introducing a wavelength offset with respect to the remote array waveguide grating to reduce chirp....

  14. 30 Gbps bottom-emitting 1060 nm VCSEL

    DEFF Research Database (Denmark)

    Tatarczak, Anna; Zheng, Y.; Rodes, G. A.

    2014-01-01

    1060 nm VCSEL-based data transmission over 50 m OM3 MMF at 30 Gbit/s is experimentally demonstrated. A highly-strained bottom-emitting QW VCSEL with p-type modulation doping is used with 3.77 mA bias and 0.55 V data amplitude.......1060 nm VCSEL-based data transmission over 50 m OM3 MMF at 30 Gbit/s is experimentally demonstrated. A highly-strained bottom-emitting QW VCSEL with p-type modulation doping is used with 3.77 mA bias and 0.55 V data amplitude....

  15. A novel gamma-ray detector with submillimeter resolutions using a monolithic MPPC array with pixelized Ce:LYSO and Ce:GGAG crystals

    Science.gov (United States)

    Kato, T.; Kataoka, J.; Nakamori, T.; Miura, T.; Matsuda, H.; Kishimoto, A.; Sato, K.; Ishikawa, Y.; Yamamura, K.; Nakamura, S.; Kawabata, N.; Ikeda, H.; Yamamoto, S.; Kamada, K.

    2013-01-01

    We have developed a large-area monolithic Multi-Pixel Photon Counter (MPPC) array consisting of 4×4 channels with a three-side buttable package. Each channel has a photosensitive area of 3×3 mm2 and 3600 Geiger mode avalanche photodiodes (APDs). For typical operational gain of 7.5×105 at +20 °C, gain fluctuation over the entire MPPC device is only ±5.6%, and dark count rates (as measured at the 1 p.e. level) amount to ≤400 kcps per channel. We first fabricated a gamma-ray camera consisting of the MPPC array with one-to-one coupling to a Ce-doped (Lu, Y)2(SiO4)O (Ce:LYSO) crystal array (4×4 array of 3×3×10 mm3 crystals). Energy and time resolutions of 11.5±0.5% (FWHM at 662 keV) and 493±22 ps were obtained, respectively. When using the charge division resistor network, which compiles signals into four position-encoded analog outputs, the ultimate positional resolution is estimated as 0.19 mm in both X and Y directions, while energy resolution of 10.2±0.4% (FWHM) was obtained. Finally, we fabricated submillimeter Ce:LYSO and Ce-doped Gd3Ga3Al2O12 (Ce:GGAG) scintillator matrices each consisting of 1.0×1.0, 0.7×0.7 and 0.5×0.5 mm2 pixels, to further improve the spatial resolution. In all types of Ce:LYSO and Ce:GGAG matrices, each crystal was clearly resolved in the position histograms when irradiated by a 137Cs source. The energy resolutions for 662 keV gamma-rays for each Ce:LYSO and Ce:GGAG scintillator matrix were ≤14.3%. These results suggest excellent potential for its use as a high spatial medical imaging device, particularly in positron emission tomography (PET).

  16. Physical and chemical sensing using monolithic semiconductor optical transducers

    Science.gov (United States)

    Zappe, Hans P.; Hofstetter, Daniel; Maisenhoelder, Bernd; Moser, Michael; Riel, Peter; Kunz, Rino E.

    1997-09-01

    We present two monolithically integrated optical sensor systems based on semiconductor photonic integrated circuits. These compact, robust and highly functional transducers perform all necessary optical and electro-optical functions on-chip; extension to multi-sensor arrays is easily envisaged. A monolithic Michelson interferometer for high-resolution displacement measurement and a monolithic Mach-Zehnder interferometer for refractometry are discussed.

  17. 100 Gb/s single VCSEL data transmission link

    DEFF Research Database (Denmark)

    Rodes Lopez, Roberto; Estaran Tolosa, Jose Manuel; Li, Bomin

    2012-01-01

    100 Gb/s optical fiber transmission link with a single 1.5 um VCSEL has been experimentally demonstrated using 4-level pulse amplitude modulation.......100 Gb/s optical fiber transmission link with a single 1.5 um VCSEL has been experimentally demonstrated using 4-level pulse amplitude modulation....

  18. Fabrication, Packaging, and Performance of VCSELs and Photodetectors for Space Applications

    Energy Technology Data Exchange (ETDEWEB)

    Armendariz, M.G.; Briggs, R.D.; Choquette, K.D.; Geib, K.M.; Serkland, D.K.

    1999-03-09

    Optocouplers are used for a variety of applications aboard spacecraft including electrical isolation, switching and power transfer. Commercially available light emitting diode (LED)-based optocouplers have experienced severe degradation of light output due to extensive displacement damage occurring in the semiconductor lattice caused by energetic proton bombardment. A new optocoupler has been designed and fabricated which utilizes vertical cavity surface emitting laser (VCSEL) and resonant cavity photodetector (RCPD) technologies for the optocoupler emitter and detector, respectively. Linear arrays of selectively oxidized GaAs/AlGaAs VCSELS and RCPDS, each designed to operate at a wavelength of 850nm, were fabricated using an airbridge contacting scheme. The airbridged contacts were designed to improve packaging yields and device reliability by eliminating the use of a polyimide planarizing layer which provided poor adhesion to the bond pad metallization. Details of the airbridged optocoupler fabrication process are reported. Discrete VCSEL and RCPD devices were characterized at temperatures between {minus}100 to 100 C. Devices were packaged in a face-to-face configuration to form a single channel optocoupler and its performance was evaluated under conditions of high-energy proton bombardment.

  19. Performance of a monolithic LaBr{sub 3}:Ce crystal coupled to an array of silicon photomultipliers

    Energy Technology Data Exchange (ETDEWEB)

    Ulyanov, Alexei, E-mail: alexey.uliyanov@ucd.ie [School of Physics, University College Dublin, Belfield, Dublin 4 (Ireland); Morris, Oran [School of Physics, University College Dublin, Belfield, Dublin 4 (Ireland); Department of Computer Science & Applied Physics, Galway-Mayo Institute of Technology, Galway (Ireland); Hanlon, Lorraine; McBreen, Sheila; Foley, Suzanne; Roberts, Oliver J.; Tobin, Isaac; Murphy, David; Wade, Colin [School of Physics, University College Dublin, Belfield, Dublin 4 (Ireland); Nelms, Nick; Shortt, Brian [European Space Agency, ESTEC, 2200 AG Noordwijk (Netherlands); Slavicek, Tomas; Granja, Carlos; Solar, Michael [Institute of Experimental and Applied Physics, Czech Technical University in Prague, 12800 Prague 2 (Czech Republic)

    2016-02-21

    A gamma-ray detector composed of a single 28×28×20 mm{sup 3} LaBr{sub 3}:Ce crystal coupled to a custom built 4×4 array of silicon photomultipliers was tested over an energy range of 30 keV to 9.3 MeV. The silicon photomultipliers were initially calibrated using 20 ns light pulses generated by a light emitting diode. The photodetector responses measured as a function of the number of incident photons were found to be non-linear and consistent with model predictions. Using corrections for the non-linearity of the silicon photomultipliers, the detector showed a linear response to gamma-rays with energies from 100 keV to the maximum available energy of 9.3 MeV. The energy resolution was found to be 4% FWHM at 662 keV. Despite the large thickness of the scintillator (20 mm) and a 5 mm thick optical window, the detector was capable of measuring the positions of the gamma-ray interaction points. The position resolution was measured at 356 keV and was found to be 8 mm FWHM in the detector plane and 11 mm FWHM for the depth of interaction. The detector can be used as a building block of a larger calorimeter system that is capable of measuring gamma-ray energies up to tens of MeV.

  20. Cavity structures for low loss oxide-confined VCSELs

    Energy Technology Data Exchange (ETDEWEB)

    Choquette, K.D.; Hadley, G.R.; Chow, W.W.; Hou, H.Q.; Geib, K.M.; Hammons, B.E. [Sandia National Labs., Albuquerque, NM (United States). Center for Compound Semiconductor Science and Technology; Mathes, D.; Hull, R. [Univ. of Virginia, Charlottesville, VA (United States). Dept. of Materials Science

    1997-05-01

    The authors examine the threshold characteristics of selectively oxidized VCSELs as a function of the number, thickness, and placement of the buried oxide apertures. The threshold current density for small area VCSELs is shown to increase with the number of oxide apertures in the cavity due to increased optical loss, while the threshold current density for broad area VCSELs decreases with increasing number of apertures due to more uniform current injection. Reductions of the threshold gain and optical loss are achieved for small area VCSELs using thin oxide apertures which are displaced longitudinally away from te optical cavity. They show that the optical loss can be sufficiently reduced to allow lasing in VCSELs with aperture area as small as 0.25 {micro}m{sup 2}.

  1. Progress and challenges in electrically pumped GaN-based VCSELs

    Science.gov (United States)

    Haglund, A.; Hashemi, E.; Bengtsson, J.; Gustavsson, J.; Stattin, M.; Calciati, M.; Goano, M.

    2016-04-01

    ABSTRACT The Vertical-Cavity Surface-Emitting Laser (VCSEL) is an established optical source in short-distance optical communication links, computer mice and tailored infrared power heating systems. Its low power consumption, easy integration into two-dimensional arrays, and low-cost manufacturing also make this type of semiconductor laser suitable for application in areas such as high-resolution printing, medical applications, and general lighting. However, these applications require emission wavelengths in the blue-UV instead of the established infrared regime, which can be achieved by using GaN-based instead of GaAs-based materials. The development of GaN-based VCSELs is challenging, but during recent years several groups have managed to demonstrate electrically pumped GaN-based VCSELs with close to 1 mW of optical output power and threshold current densities between 3-16 kA/cm2. The performance is limited by challenges such as achieving high-reflectivity mirrors, vertical and lateral carrier confinement, efficient lateral current spreading, accurate cavity length control and lateral optical mode confinement. This paper summarizes different strategies to solve these issues in electrically pumped GaN-VCSELs together with state-of-the-art results. We will highlight our work on combined transverse current and optical mode confinement, where we show that many structures used for current confinement result in unintentionally optically anti-guided resonators. Such resonators can have a very high optical loss, which easily doubles the threshold gain for lasing. We will also present an alternative to the use of distributed Bragg reflectors as high-reflectivity mirrors, namely TiO2/air high contrast gratings (HCGs). Fabricated HCGs of this type show a high reflectivity (>95%) over a 25 nm wavelength span.

  2. Intracavity contacts for nitride based monolithic surface emitters by focused ion beam processing

    Energy Technology Data Exchange (ETDEWEB)

    Fandrich, Malte; Dartsch, Heiko; Tessarek, Christian; Aschenbrenner, Timo; Hommel, Detlef [Institut fuer Festkoerperphysik - Halbleiterepitaxie, Universitaet Bremen (Germany)

    2010-07-01

    The realization of electrically driven nitride based vertical-cavity surface-emitting lasers (VCSELs) is challenging due to limitations in the conductivity of the distributed Bragg reflectors (DBRs). Therefore monolithic approaches are based on a doped cavity and one or two undoped DBRs. This requires the use of technologically complex intracavity contacts. The presented process yields intracavity contacts applicable to monolithically grown VCSEL structures. Initially mesas are structured by photolithography and chemical assisted ion beam etching. The precise structuring of the prestructured mesas is performed in a focused ion beam system (FIB), where the micropillars are thinned stepwise down to a diameter of 0.5-5 {mu}m. The contacting of the pillars is realized by FIB deposited metal and insulator structures. Insulator separated Pt ring-contacts connect the micropillars with large-scale contact pads. This procedure was applied to a VCSEL structure consisting of a bottom AlInN/GaN-DBR with 40 pairs, a p/n-doped 5 {lambda} GaN-cavity with embedded InGaN quantum dots and a top 10 pair AlInN/GaN-DBR. The developed contacting structure enables a current up to 15 mA through the cavity which documents the capability for the electrical operation of VCSEL devices.

  3. Monolithic III-V and hybrid polysilicon-III-V microelectromechanical tunable vertical-cavity surface-emitting lasers

    Science.gov (United States)

    Ochoa, Edward M.; Lott, James A.; Nelson, Thomas R., Jr.; Harvey, M. C.; Raley, J. A.; Stintz, Andreas; Malloy, Kevin J.

    2003-04-01

    We report our progress on the design and fabrication of electrostatically-actuated microelectromechanical (MEM) tunable wavelength filters and vertical cavity surface-emitting lasers (VCSELs). We investigate both an all-semiconductor monolithic approach and a hybrid approach based on the combination of conventional polysilicon microelectromechanical systems (MEMS) and III-V semiconductor thin-film distributed Bragg reflector (DBR) and VCSEL structures. In the tunable hybrid structures the III-V semiconductor layers are flip-bonded onto specially designed polysilicon foundry MEMS structures and separated from their lattice-matched parent substrates by a novel post-bonding lift-off process.

  4. AIN Monolithic Microchannel Cooled Heatsink for High Power Laser Diode Array%应用于大功率激光二极管列阵的单片集成微通道制冷热沉

    Institute of Scientific and Technical Information of China (English)

    马杰慧; 方高瞻; 蓝永生; 马骁宇

    2005-01-01

    介绍了一种应用于大功率激光二极管列阵的新型单片集成微通道制冷热沉.这种热沉已制造并经过测试.10叠层的激光二极管列阵的热阻为0.121℃/W.相邻两个激光条的间距是1.17mm.在20%高占空比条件下,波长为808nm左右,峰值功率可以达到611W.%A novel AIN monolithic microchannel cooled heatsink for high power laser diode array is introduced.The high power stack laser diode array with an AIN monolithic microchannel heatsink is fabricated and tested.The thermal impedance of a 10 stack laser diode array is 0.121℃/W.The pitch between two adjacent bars is 1.17mm.The power level of 611W is achieved under the 20% duty factor condition at an emission wavelength around 808nm.

  5. VCSEL Transmission at 10 Gb/s for 20 km Single Mode Fiber WDM-PON without Dispersion Compensation or Injection Locking

    DEFF Research Database (Denmark)

    Gibbon, Timothy Braidwood; Prince, Kamau; Pham, Tien Thang;

    2011-01-01

    how off-center wavelength filtering of the VCSEL spectrum at an array waveguide grating can be used to mitigate the effect of chirp and the dispersion penalty. Transmission at 10Gb/s VCSEL over 23.6 km of single mode fiber is experimentally demonstrated, with a dispersion penalty of only 2.9 d......B. Simulated results are also presented which show that off-center wavelength filtering can extend the 10 Gb/s network reach from 11.7 km to 25.8 km for a 4 dB dispersion penalty. This allows for cheap and simple dispersion mitigation in next generation VCSEL based optical access networks....

  6. Single-Fiber Bidirectional Optical Data Links with Monolithic Transceiver Chips

    OpenAIRE

    Alexander Kern; Sujoy Paul; Dietmar Wahl; Ahmed Al-Samaneh; Rainer Michalzik

    2012-01-01

    We report the monolithic integration, fabrication, and electrooptical properties of AlGaAs-GaAs-based transceiver (TRx) chips for 850 nm wavelength optical links with data rates of multiple Gbit/s. Using a single butt-coupled multimode fiber (MMF), low-cost bidirectional communication in half- and even full-duplex mode is demonstrated. Two design concepts are presented, based on a vertical-cavity surface-emitting laser (VCSEL) and a monolithically integrated p-doped-intrinsic-n-doped (PIN) or...

  7. VCSEL structures used to suppress higher-order transverse modes

    National Research Council Canada - National Science Library

    Nakwaski, W

    2011-01-01

    .... It is well known that, because of a nearly uniform current injection into their active regions, small-aperture VCSELs without any modification offer quite high single-fundamental-mode (SFM) output...

  8. Bidirectional uncompressed HD video distribution over fiber employing VCSELs

    DEFF Research Database (Denmark)

    Estaran Tolosa, Jose Manuel; Vegas Olmos, Juan José; Rodes, G. A.;

    2012-01-01

    We report on a bidirectional system in which VCSELs are simultaneously modulated with two uncompressed HD video signals. The results show a large power budget and a negligible penalty over 10 km long transmission links.......We report on a bidirectional system in which VCSELs are simultaneously modulated with two uncompressed HD video signals. The results show a large power budget and a negligible penalty over 10 km long transmission links....

  9. Advanced vectorial simulation of VCSELs with nano structures invited paper

    DEFF Research Database (Denmark)

    Chung, Il-Sug; Mørk, Jesper

    2009-01-01

    The single-mode properties and design issues of three vertical-cavity surface-emitting laser (VCSEL) structures incorporating nano structures are rigorously investigated. Nano structuring enables to deliver selective pumping or loss to the fundamental mode as well as stabilizing the output...... polarization state. Comparison of three vectorial simulation methods reveals that the modal expansion method is suitable for treating the nano structured VCSEL designs....

  10. Fabrication issues of oxide-confined VCSELs

    Energy Technology Data Exchange (ETDEWEB)

    Geib, K.M.; Choquette, K.D.; Hou, H.Q.; Hammons, B.E.

    1997-04-01

    To insert high-performance oxide-confined vertical-cavity surface- emitting lasers (VCSELs) into the manufacturing arena, we have examined the critical parameters that must be controlled to establish a repeatable and uniform wet thermal oxidation process for AlGaAs. These parameters include the AlAs mole fraction, sample temperature, carrier gas flow, and bubbler water temperature. Knowledge of these parameters has enable the compilation of oxidation rate data for AlGaAs which exhibits an Arrhenius rate dependence. The compositionally dependent activation energies for Al{sub x}Ga{sub 1-x}As layers of x=1.00, 0.98, and 0.92 are found to be 1.24, 1.75, and 1.88 eV, respectively. 7 figs, 1 tab, 14 refs.

  11. High-index-contrast subwavelength grating VCSEL

    DEFF Research Database (Denmark)

    Gilet, Philippe; Olivier, Nicolas; Grosse, Philippe

    2010-01-01

    In this article, we report our results on 980nm high-index-contrast subwavelength grating (HCG) VCSELs for optical interconnection applications. In our structure, a thin undoped HCG layer replaces a thick p-type Bragg mirror. The HCG mirror can feasibly achieve polarization-selective reflectivities...... close to 100%. The investigated structure consists of a HCG mirror with an underneath /4-thick oxide gap, four p-type GaAlAs/GaAs pairs for current spreading, three InGaAs/GaAs quantum wells, and an n-type GaAlAs/GaAs Bragg mirror. The HCG structure was defined by e-beam lithography and dry etching....... The current oxide aperture and the oxide gap underneath the HCG were simultaneously formed by the selective wet oxidation process. Compared to air-gap high contrast grating mirrors demonstrated elsewhere, our grating mirrors are particular since they are supported by thinner /4 aluminium oxide layer, and thus...

  12. High-frequency signal generation using 1550 nm VCSEL subject to two-frequency optical injection

    Science.gov (United States)

    Consoli, Antonio; Quirce, Ana; Valle, Angel; Esquivias, Ignacio; Pesquera, Luis; García Tijero, Jose Manuel

    2013-03-01

    We experimentally investigate high-frequency microwave signal generation using a 1550 nm single-mode VCSEL subject to two-frequency optical injection. We first consider a situation in which the injected signals come from two similar VCSELs. The polarization of the injected light is parallel to that of the injected VCSEL. We obtain that the VCSEL can be locked to one of the injected signals, but the observed microwave signal is originated by beating at the photodetector. In a second situation we consider injected signals that come from two external cavity tunable lasers with a significant increase of the injected power with respect to the VCSEL-by-VCSEL injection case. The polarization of the injected light is orthogonal to that of the free-running slave VCSEL. We show that in this case it is possible to generate a microwave signal inside the VCSEL cavity.

  13. Dynamic Self-Locking of an OEO Containing a VCSEL

    Science.gov (United States)

    Strekalov, Dmitry; Matsko, Andrey; Yu, Nan; Savchenkov, Anatoliy; Maleki, Lute

    2009-01-01

    A method of dynamic self-locking has been demonstrated to be effective as a means of stabilizing the wavelength of light emitted by a vertical-cavity surface-emitting laser (VCSEL) that is an active element in the frequency-control loop of an optoelectronic oscillator (OEO) designed to implement an atomic clock based on an electromagnetically- induced-transparency (EIT) resonance. This scheme can be considered an alternative to the one described in Optical Injection Locking of a VCSEL in an OEO (NPO-43454), NASA Tech Briefs, Vol. 33, No. 7 (July 2009), page 33. Both schemes are expected to enable the development of small, low-power, high-stability atomic clocks that would be suitable for use in applications involving precise navigation and/or communication. To recapitulate from the cited prior article: In one essential aspect of operation of an OEO of the type described above, a microwave modulation signal is coupled into the VCSEL. Heretofore, it has been well known that the wavelength of light emitted by a VCSEL depends on its temperature and drive current, necessitating thorough stabilization of these operational parameters. Recently, it was discovered that the wavelength also depends on the microwave power coupled into the VCSEL. This concludes the background information. From the perspective that led to the conception of the optical injection-locking scheme described in the cited prior article, the variation of the VCSEL wavelength with the microwave power circulating in the frequency-control loop is regarded as a disadvantage and optical injection locking is a solution of the problem of stabilizing the wavelength in the presence of uncontrolled fluctuations in the microwave power. The present scheme for dynamic self-locking emerges from a different perspective, in which the dependence of VCSEL wavelength on microwave power is regarded as an advantageous phenomenon that can be exploited as a means of controlling the wavelength. The figure schematically depicts

  14. Monolithic microchannel heatsink

    Science.gov (United States)

    Benett, William J.; Beach, Raymond J.; Ciarlo, Dino R.

    1996-01-01

    A silicon wafer has slots sawn in it that allow diode laser bars to be mounted in contact with the silicon. Microchannels are etched into the back of the wafer to provide cooling of the diode bars. To facilitate getting the channels close to the diode bars, the channels are rotated from an angle perpendicular to the diode bars which allows increased penetration between the mounted diode bars. This invention enables the fabrication of monolithic silicon microchannel heatsinks for laser diodes. The heatsinks have low thermal resistance because of the close proximity of the microchannels to the laser diode being cooled. This allows high average power operation of two-dimensional laser diode arrays that have a high density of laser diode bars and therefore high optical power density.

  15. Single-Fiber Bidirectional Optical Data Links with Monolithic Transceiver Chips

    Directory of Open Access Journals (Sweden)

    Alexander Kern

    2012-01-01

    fiber (MMF, low-cost bidirectional communication in half- and even full-duplex mode is demonstrated. Two design concepts are presented, based on a vertical-cavity surface-emitting laser (VCSEL and a monolithically integrated p-doped-intrinsic-n-doped (PIN or metal-semiconductor-metal (MSM photodetector. Whereas the VCSEL-PIN photodiode (PD chips are used for high-speed bidirectional data transmission over 62.5 and 50 μm core diameter MMFs, MSM TRx chips are employed for 100 or 200 μm large-area fibers. Such a monolithic transceiver design based on a well-established material system and avoiding the use of external fiber coupling optics is well suited for inexpensive and compact optical interconnects over distances of a few hundred meters. Standard MMF networks can thus be upgraded using high-speed VCSEL-PIN transceiver chips which are capable to handle data rates of up to 10 Gbit/s.

  16. Monoliths in Bioprocess Technology

    Directory of Open Access Journals (Sweden)

    Vignesh Rajamanickam

    2015-04-01

    Full Text Available Monolithic columns are a special type of chromatography column, which can be used for the purification of different biomolecules. They have become popular due to their high mass transfer properties and short purification times. Several articles have already discussed monolith manufacturing, as well as monolith characteristics. In contrast, this review focuses on the applied aspect of monoliths and discusses the most relevant biomolecules that can be successfully purified by them. We describe success stories for viruses, nucleic acids and proteins and compare them to conventional purification methods. Furthermore, the advantages of monolithic columns over particle-based resins, as well as the limitations of monoliths are discussed. With a compilation of commercially available monolithic columns, this review aims at serving as a ‘yellow pages’ for bioprocess engineers who face the challenge of purifying a certain biomolecule using monoliths.

  17. Widely tunable narrow-linewidth 1.5 μm light source based on a monolithically integrated quantum dot laser array

    Science.gov (United States)

    Becker, A.; Sichkovskyi, V.; Bjelica, M.; Rippien, A.; Schnabel, F.; Kaiser, M.; Eyal, O.; Witzigmann, B.; Eisenstein, G.; Reithmaier, J. P.

    2017-05-01

    A monolithically integrated widely tunable narrow-linewidth light source was realized on an InP-based quantum dot (QD) gain material. The quasi zero-dimensional nature of QDs and the resulting low linewidth enhancement factor enabled standalone distributed feedback (DFB) lasers with intrinsic linewidths as low as 110 kHz. An integrated device comprising four DFB lasers with on-chip micro-heaters, a 3 dB-coupler network, and a semiconductor optical amplifier (SOA), which covers the entire C+ telecom band, exhibits a linewidth of below 200 kHz independent of the SOA operation current.

  18. Synchronization of chaotic VCSELs by external chaotic signal parameter modulation

    Institute of Scientific and Technical Information of China (English)

    Wei Wang; Shenghai Zhang; Xingzhong Qian; Yanbin Wang

    2009-01-01

    Synchronization of chaotic vertical-cavity surface-emitting lasers (VCSELs) is achieved by external chaotic signal modulation successfully.Simulation indicates that we can get chaos synchronization if the intensity of external chaotic signal is large enough.First of all,we use direct current modulation to achieve the chaos of VCSELs,and determine the laser's chaotic state by analyzing time series of the output and the corresponding power spectrum.And then we achieve synchronization of the two chaotic systems by external chaotic signal parameter modulation.We also find that the larger the modulation intensity is,the easier it is to achieve synchronization for chaotic VCSELs.This approach can also be applied to systems with a number of modulated lasers.

  19. Highly reflective Bragg mirrors for VCSEL applications at 1.3 and 1.55μm

    Science.gov (United States)

    Linnik, Maria; Christou, Aristos

    2000-07-01

    Quaternary semiconductor alloy material systems for applications as highly efficient Distributed Bragg Reflectors were investigated for two operating wavelengths of 1.3 and 1.55 micrometer. Based on the calculations of the material's energy bandgaps and indices of refraction for the entire composition range and for the corresponding incident wavelength, four quaternary alloys have been selected from which the refractive index difference between two adjacent layers of 0.65 has been obtained. All quaternary alloys were lattice matched to InP substrate. The reflectivity calculations show that for the DBR with a large index of refraction contrast, 16 pairs of layers would result in a reflectivity of 99%. The resulting monolithic VCSEL structure would consist of fewer DBR layers, interface roughness would be reduced, and, therefore, reliability of the device would be improved.

  20. Optical Injection Locking of a VCSEL in an OEO

    Science.gov (United States)

    Strekalov, Dmitry; Matsko, Andrey; Savchenkov, Anatoliy; Yu, Nan; Maleki, Lute

    2009-01-01

    Optical injection locking has been demonstrated to be effective as a means of stabilizing the wavelength of light emitted by a vertical-cavity surface- emitting laser (VCSEL) that is an active element in the frequency-control loop of an opto-electronic oscillator (OEO) designed to implement an atomic clock based on an electromagnetically- induced-transparency resonance. This particular optical-injection- locking scheme is expected to enable the development of small, low-power, high-stability atomic clocks that would be suitable for use in applications involving precise navigation and/or communication. In one essential aspect of operation of an OEO of the type described above, a microwave modulation signal is coupled into the VCSEL. Heretofore, it has been well known that the wavelength of light emitted by a VCSEL depends on its temperature and drive current, necessitating thorough stabilization of these operational parameters. Recently, it was discovered that the wavelength also depends on the microwave power coupled into the VCSEL. Inasmuch as the microwave power circulating in the frequency-control loop is a dynamic frequency-control variable (and, hence, cannot be stabilized), there arises a need for another means of stabilizing the wavelength. The present optical-injection-locking scheme satisfies the need for a means to stabilize the wavelength against microwave- power fluctuations. It is also expected to afford stabilization against temperature and current fluctuations. In an experiment performed to demonstrate this scheme, wavelength locking was observed when about 200 W of the output power of a commercial tunable diode laser was injected into a commercial VCSEL, designed to operate in the wavelength range of 795+/-3 nm, that was generating about 200 microW of optical power. (The use of relatively high injection power levels is a usual practice in injection locking of VCSELs.)

  1. VCSELs Fundamentals, Technology and Applications of Vertical-Cavity Surface-Emitting Lasers

    CERN Document Server

    2013-01-01

    The huge progress which has been achieved in the field is covered here, in the first comprehensive monograph on vertical-cavity surface-emitting lasers (VCSELs) since eight years. Apart from chapters reviewing the research field and the laser fundamentals, there are comprehensive updates on red and blue emitting VCSELs, telecommunication VCSELs, optical transceivers, and parallel-optical links for computer interconnects. Entirely new contributions are made to the fields of vectorial three-dimensional optical modeling, single-mode VCSELs, polarization control, polarization dynamics, very-high-speed design, high-power emission, use of high-contrast gratings, GaInNAsSb long-wavelength VCSELs, optical video links, VCSELs for optical mice and sensing, as well as VCSEL-based laser printing. The book appeals to researchers, optical engineers and graduate students.

  2. Self-mixing interferometry in VCSELs for nanomechanical cantilever sensing

    DEFF Research Database (Denmark)

    Larsson, David; Greve, Anders; Hvam, Jørn Märcher

    2009-01-01

    We have investigated optical read-out of uncoated polymer micrometer-sized cantilever sensors by self-mixing interference in VCSELs for single-molecule gas sensing. A resolution ~0.2 nm is measured, which is much better than current methods.......We have investigated optical read-out of uncoated polymer micrometer-sized cantilever sensors by self-mixing interference in VCSELs for single-molecule gas sensing. A resolution ~0.2 nm is measured, which is much better than current methods....

  3. Green monolithic II-VI vertical-cavity surface-emitting laser operating at room temperature

    Science.gov (United States)

    Kruse, C.; Ulrich, S. M.; Alexe, G.; Roventa, E.; Kröger, R.; Brendemühl, B.; Michler, P.; Gutowski, J.; Hommel, D.

    2004-02-01

    The realization of a monolithic all II-VI-based vertical cavity surface emitting laser (VCSEL) for the green spectral region is reported. Optically pumped lasing operation was achieved up to room temperature using a planar VCSEL structure. Taking advantage of distributed Bragg-reflectors based on MgS/Zn(Cd)Se superlattices as the low-refractive index material and ZnS0.06Se0.94 layers as the high-index material with a refractive index contrast of n = 0.6, a quality factor exceeding Q = 2000 is reached by using only 18 Bragg periods for the bottom DBR and 15 Bragg periods for the top DBR. The threshold power density is 0.32 MW/cm2 at a temperature of 10 K (emission wavelength 498.5 nm) and 1.9 MW/cm2 at room temperature (emission wavelength 502.3 nm).

  4. Monolithic CMOS pixel detector for international linear collider vertex detection

    Indian Academy of Sciences (India)

    J E Brau; O Igonkina; N Sinew; D Strom; C Baltay; W Emmet; H Neal; D Rabinowitz

    2007-12-01

    A monolithic CMS pixel detector is under development for an ILC experiment. This chronopixel array provides a time stamp resolution of one bunch crossing, a critical feature for background suppression. The status of this effort is summarized.

  5. Modulation properties of VCSEL with intracavity modulator

    Science.gov (United States)

    van Eisden, J.; Yakimov, M.; Tokranov, V.; Varanasi, M.; Mohammed, E. M.; Young, I. A.; Oktyabrsky, S.

    2007-02-01

    We have studied the modulation properties of VCSEL with intracavity multiple quantum well (MQW) electroabsorption modulator integrated into the top distributed Bragg reflector (DBR) [1]. Small signal analysis of rate equations for loss modulation shows an intrinsic high-frequency roll-off slope of 1/ω instead of 1/ω2 in directly modulated laser diodes, and consequently bandwidths in excess of 40 GHz are obtainable with this configuration [2]. Possible limiting factors to high bandwidth were examined by fitting high frequency characteristics to a multi-pole transfer function, and include RC delay and carrier drift-limited time of flight (TOF) in the modulator intrinsic region. Intracavity loss modulation shows a strong (+20dB) relaxation oscillation resonant feature in both theory and experiment. As demonstrated, this feature can be significantly reduced in amplitude using parasitics. We have extracted relative contribution of TOF and parasitic capacitance by varying the modulator intrinsic region width (105 and 210 nm) and lateral size of the modulator (18 and 12μm). It was estimated that the small size modulator exhibits parasitics f -3dB at 8GHz. To estimate the carrier TOF contribution to bandwidth limits, low temperature growth of a 210 nm absorber i-region and MQW was employed to reduce photogenerated carrier lifetime. Bandwidth limitations were found to be mostly due to diode and metallization capacitances, in addition to one pole set by the optoelectronic resonance frequency. We have used p-modulation doping of the gain region to increase the relaxation frequency. Pronounced active Q-switching was observed, yielding pulse widths of 40 ps at a 4 GHz rate.

  6. Extraction of amphetamines and methylenedioxyamphetamines from urine using a monolithic silica disk-packed spin column and high-performance liquid chromatography-diode array detection.

    Science.gov (United States)

    Namera, Akira; Nakamoto, Akihiro; Nishida, Manami; Saito, Takeshi; Kishiyama, Izumi; Miyazaki, Shota; Yahata, Midori; Yashiki, Mikio; Nagao, Masataka

    2008-10-24

    To overcome the limitations of solid-phase extraction, we developed a device comprising a spin column packed with octadecyl silane-bonded monolithic silica for extracting amphetamines and methylenedioxyamphetamines from urine. Urine (0.5mL), buffer (0.4mL), and methoxyphenamine (internal standard) were directly put into the preactivated column. The column was centrifuged (3000rpm, 5min) for sample loading and washed. The adsorbed analytes were eluted and analyzed by high-performance liquid chromatography, without evaporation. The results were as follows: linear curves (drug concentrations of 0.2-20microg/mL); correlation coefficients >0.99; detection limit, 0.1microg/mL. The proposed method is not only useful for drugs from biological materials but also highly reproducible for the analysis of these drugs in urine.

  7. On high speed transmission with the 850nm VCSELs

    Science.gov (United States)

    Turkiewicz, Jarosław P.; Chorchos, Łukasz; Puerta Ramirez, Rafael; Vegas Olmos, Juan Jose; Ledentsov, Nikolay

    2016-09-01

    One of the key research challenges is development of energy efficient high bit rate data interconnects. The most promising solutions are based on 850 nm vertical cavity surface emitting lasers (VCSEL) and multi mode fibre (MMF). In this paper options to realize energy efficient 850 nm data interconnects are discussed and evaluated.

  8. On high speed transmission with the 850 nm VCSELs

    DEFF Research Database (Denmark)

    Turkiewicz, Jarosław P.; Chorchos, Łukasz; Puerta Ramírez, Rafael

    2016-01-01

    One of the key research challenges is development of energy efficient high bit rate data interconnects. The most promising solutions are based on 850 nm vertical cavity surface emitting lasers (VCSEL) and multi mode fibre (MMF). In this paper options to realize energy efficient 850 nm data...

  9. Optically pumped 1550nm wavelength tunable MEMS VCSEL

    DEFF Research Database (Denmark)

    Sahoo, Hitesh Kumar; Ansbæk, Thor; Ottaviano, Luisa

    2016-01-01

    The paper presents the design and fabrication of an optically pumped 1550nm tunable MEMS VCSEL with anenclosed MEMS. The MEMS is defined in SOI and the active material, an InP wafer with quantum wells arebonded to the SOI and the last mirror is made from the deposition of dielectric materials...

  10. Transverse-Mode Control of VCSELs With Convex Mirror

    Institute of Scientific and Technical Information of China (English)

    2003-01-01

    We propose the transverse-mode control of vertical-cavity surface-emitting lasers (VCSELs) with a convex mirror. A possibility of improvements on single-mode output power and higher-order mode suppression is presented by optimizing a convex mirror.

  11. Long-wavelength oxide-confined VCSEL using InGaAsN quantum wells

    Science.gov (United States)

    Lai, H. C.; Pan, J. S.; Li, Alice C. F.; Tang, M. C.; Wu, C. C.; Lee, Tsin-Dong; Huang, K. F.

    2004-05-01

    Characteristics of oxide-confined vertical-cavity surface emitting laser emitting at 1289nm will be presented in this paper. The wafer is monolithically grown using InGaAsN/GaAs QWs as active layer and GaAs/AlGaAs conventional DBRs. In the structure, the laser employs 39 pairs N-GaAs/Al0.9GaAs and 23 pairs P-GaAs/Al0.9GaAs with a selectively oxide layer located at first DBR close to active region, providing the current and optical confinement. The device processing is similar to the fabrication for current 850nm oxVCSELs. Mesa etching is used to expose the Al-rich AlGaAs layer and followed by oxidation to form the current confinement. The maximum light output power is around 950uW at room temperature under CW operation with a threshold current around 6mA for 10um aperture size devices. The device can still lase at 1000C with a maximum power of 0.14mW. Slope efficiency is 0.133(W/A) and side mode suppression ratio (SMSR) is around 20dB at 10mA operation. The aging data and speed transmission experimental data will also be presented.

  12. Phase-locked arrays of vertical-cavity surface-emitting lasers

    Energy Technology Data Exchange (ETDEWEB)

    Warren, M.E.; Hadley, G.R.; Lear, K.L.; Gourley, P.L.; Vawter, G.A.; Zolper, J.C.; Brennan, T.M.; Hammons, B.E.

    1994-05-01

    Vertical Cavity Surface-Emitting Lasers (VCSELs) are of increasing interest to the photonics community because of their surface-emitting structure, simple fabrication and packaging, wafer-level testability and potential for low cost. Scaling VCSELs to higher power outputs requires increasing the device area, which leads to transverse mode control difficulties if devices become larger than 10-15 microns. One approach to increasing the device size while maintaining a well controlled transverse mode profile is to form coupled or phase-locked, two-dimensional arrays of VCSELs that are individually single-transverse mode. The authors have fabricated and characterized both photopumped and electrically injected two-dimensional VCSEL arrays with apertures over 100 microns wide. Their work has led to an increased understanding of these devices and they have developed new types of devices, including hybrid semiconductor/dielectric mirror VCSEL arrays, VCSEL arrays with etched trench, self-aligned, gold grid contacts and arrays with integrated phase-shifters to correct the far-field pattern.

  13. Imaging Properties of Planar Microlens Arrays

    Institute of Scientific and Technical Information of China (English)

    2003-01-01

    The planar microlens arrays is a two-dimensional array of optical component which is fabricated monolithically available. Imaging properties of planar microlens arrays are described, which provide both image multiplexer and erect, unit magnification images.

  14. Nanosecond monolithic CMOS readout cell

    Science.gov (United States)

    Souchkov, Vitali V.

    2004-08-24

    A pulse shaper is implemented in monolithic CMOS with a delay unit formed of a unity gain buffer. The shaper is formed of a difference amplifier having one input connected directly to an input signal and a second input connected to a delayed input signal through the buffer. An elementary cell is based on the pulse shaper and a timing circuit which gates the output of an integrator connected to the pulse shaper output. A detector readout system is formed of a plurality of elementary cells, each connected to a pixel of a pixel array, or to a microstrip of a plurality of microstrips, or to a detector segment.

  15. New functions of VCSEL-based optical devicesInvited Paper

    Institute of Scientific and Technical Information of China (English)

    Fumio Koyama

    2008-01-01

    @@ We have seen a lot of unique features off vertical cavity surface emitting lasers (VCSELs), such as low power consumption, wafer-level testing, small packaging capability, and so on. The market of VCSELs has been growing up rapidly in recent years and they are now the key devices in local area networks using multi-mode optical fibers. In addition, new functions on VCSELs have been demonstrated. In this paper, the recent advances of VCSEL photonics will be reviewed, which include the wavelength engineering and the athermal operation based on microelectro mechanical system (MEMS) technologies. Also, this paper explores the potential and challenges for new functions of VCSELs, including high-speed control of optical phase, slow light devices, plasmonic VCSELs, and so on.

  16. Towards 100 Gbps over 100m MMF using a 850nm VCSEL

    DEFF Research Database (Denmark)

    Iglesias Olmedo, Miguel; Tatarczak, Anna; Zuo, Tianjian

    2014-01-01

    Employing MultiCAP signaling, successful 70.4 Gbps transmission over 100m of OM3 MMF using off-the-shelf 850 nm VCSEL with 10.1 GHz 3-dB bandwidth is experimentally demonstrated indicating the feasibility of achieving 100 Gbps with a single 25 GHz VCSEL. © 2014 OSA.......Employing MultiCAP signaling, successful 70.4 Gbps transmission over 100m of OM3 MMF using off-the-shelf 850 nm VCSEL with 10.1 GHz 3-dB bandwidth is experimentally demonstrated indicating the feasibility of achieving 100 Gbps with a single 25 GHz VCSEL. © 2014 OSA....

  17. Signal Quality Enhancement of Directly- Modulated VCSELs Using a Micro-Ring Resonator Transfer Function

    DEFF Research Database (Denmark)

    An, Yi; Muller, M.; Estaran Tolosa, Jose Manuel

    2013-01-01

    A micro-ring resonator transfer function is used to enhance the quality of signals generated using directly modulated VCSELs. The scheme is demonstrated up to 25 Gbit/s with a 17.6-GHz VCSEL, with up to 10 dB sensitivity improvement.......A micro-ring resonator transfer function is used to enhance the quality of signals generated using directly modulated VCSELs. The scheme is demonstrated up to 25 Gbit/s with a 17.6-GHz VCSEL, with up to 10 dB sensitivity improvement....

  18. Free-Space Optical Interconnect Employing VCSEL Diodes

    Science.gov (United States)

    Simons, Rainee N.; Savich, Gregory R.; Torres, Heidi

    2009-01-01

    Sensor signal processing is widely used on aircraft and spacecraft. The scheme employs multiple input/output nodes for data acquisition and CPU (central processing unit) nodes for data processing. To connect 110 nodes and CPU nodes, scalable interconnections such as backplanes are desired because the number of nodes depends on requirements of each mission. An optical backplane consisting of vertical-cavity surface-emitting lasers (VCSELs), VCSEL drivers, photodetectors, and transimpedance amplifiers is the preferred approach since it can handle several hundred megabits per second data throughput.The next generation of satellite-borne systems will require transceivers and processors that can handle several Gb/s of data. Optical interconnects have been praised for both their speed and functionality with hopes that light can relieve the electrical bottleneck predicted for the near future. Optoelectronic interconnects provide a factor of ten improvement over electrical interconnects.

  19. High Power VCSEL Device with Periodic Gain Active Region

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    High power vertical cavity surface emitting lasers(VCSEKLs) with large aperture have been fabricated through improving passivation, lateral oxidation and heat dissipation techniques. Different from conventional three quantum well structures, a periodic gain active region with nine quantum wells was incorporated into the VCSEL structure, with which high efficiency and high power operation were expected. The nine quantum wells were divided into three groups with each of them located at the antinodes of the ca...

  20. True photonic band-gap mode-control in VCSEL structures

    DEFF Research Database (Denmark)

    Romstad, F.; Madsen, M.; Birkedal, Dan;

    2003-01-01

    Photonic band-gap mode confinement in novel nano-structured large area VCSEL structures is confirmed by the amplified spontaneous emission spectrum. Both guide and anti-guide VCSEL structures are experimentally characterised to verify the photonic band-gap effect....

  1. Long-wavelength VCSELs with AlGaAsSb/AlAsSb Bragg mirrors lattice-matched on InP substrates

    Science.gov (United States)

    Almuneau, Guilhem; Hall, Eric M.; Nakagawa, Shigeru; Kim, Jin K.; Coldren, Larry A.

    2000-05-01

    The characterization of 1.55 micrometer room temperature (RT) electrically pumped monolithic vertical cavity surface emitting lasers (VCSELs) on InP is reported. By combining high refractive index-contrast AlGaAsSb/AlAsSb distributed Bragg mirrors (DBRs) and Esaki-junction-based active region, these results demonstrate that VCSELs operating at 1.55 micrometer and employing a reasonable number of mirror periods can be grown in a single epitaxial step. Regarding our first results with the same type of structure, some improvements have been achieved on the threshold current density (approximately equals 1 kA/cm2), and on the voltage drop in the DBRs. We also present in this paper the thermal conductivity of the As- Sb materials measured on both bulk layers and DBR stacks. The main performance-limiting factor appears to be the combination between the low thermal conduction of the quaternary alloys lattice-matched to InP, and the high energy-band offset between the high- and the low-index materials.

  2. A linear optical link using radiation hard VCSELs

    CERN Document Server

    Lozano-Bahilo, J; Zsenei, A

    2001-01-01

    A four-channel linear optical link has been developed to enable analogue data transmission in LHC experiments for the analogue front- end chip SCT128A. Signals from a prototype ATLAS SCT module, consisting of 12 cm long silicon strip detectors, connected to six 128 channel SCTA chips, have been transmitted at 40 MHz using the Mitel 4D469 VCSEL and matching PIN diode at a wavelength of 850 nm. Results are presented showing static and dynamic linearity, frequency response and noise. The overall performance of the complete chain is shown for /sup 241/Am spectra. (4 refs).

  3. Final report on LDRD project : narrow-linewidth VCSELs for atomic microsystems.

    Energy Technology Data Exchange (ETDEWEB)

    Chow, Weng Wah; Geib, Kent Martin; Peake, Gregory Merwin; Serkland, Darwin Keith

    2011-09-01

    Vertical-cavity surface-emitting lasers (VCSELs) are well suited for emerging photonic microsystems due to their low power consumption, ease of integration with other optical components, and single frequency operation. However, the typical VCSEL linewidth of 100 MHz is approximately ten times wider than the natural linewidth of atoms used in atomic beam clocks and trapped atom research, which degrades or completely destroys performance in those systems. This report documents our efforts to reduce VCSEL linewidths below 10 MHz to meet the needs of advanced sub-Doppler atomic microsystems, such as cold-atom traps. We have investigated two complementary approaches to reduce VCSEL linewidth: (A) increasing the laser-cavity quality factor, and (B) decreasing the linewidth enhancement factor (alpha) of the optical gain medium. We have developed two new VCSEL devices that achieved increased cavity quality factors: (1) all-semiconductor extended-cavity VCSELs, and (2) micro-external-cavity surface-emitting lasers (MECSELs). These new VCSEL devices have demonstrated linewidths below 10 MHz, and linewidths below 1 MHz seem feasible with further optimization.

  4. Progress on High-Speed 980 nm VCSELs for Short-Reach Optical Interconnects

    Directory of Open Access Journals (Sweden)

    Alex Mutig

    2011-01-01

    Full Text Available Progress of high-speed vertical cavity surface emitting lasers (VCSEL operating around 980 nm is reviewed. A special focus is on their applications for future short-reach optical interconnects, for example, in high-performance computers (HPC. The wavelength of 980 nm has fundamental advantages for these applications and plays a significant role in VCSEL research today. The present data rates of 980 nm VCSELs exceed 40 Gbit/s, and excellent temperature stability has been reported. The major concepts leading to these impressive developments are presented.

  5. All-optical tunable mirror of VCSEL using electromagnetically induced transparency

    Science.gov (United States)

    Rostami, A.; Abbasian, K.; Khodashenas, P. S.; Janabi-Sharifi, F.

    2008-11-01

    A new and efficient proposal for all-optical tunable mirror of VCSEL using electromagnetically induced transparency (EIT) is proposed. For this purpose a slab doped with quantum dots for realization of 3-level atomic system is considered. Density matrix formulation for time evaluation of the proposed structure is used. The reflection and transmission coefficients of the considered slab are calculated and time development of the related amplitude and output power and threshold current density of VCSEL laser studied. We show that some nanometer tuning can be obtained. So, the proposed idea can open a new realization method of all-optical tunable VCSEL lasers.

  6. Flip-chip assembly of VCSELs to silicon grating couplers via laser fabricated SU8 prisms.

    Science.gov (United States)

    Kaur, K S; Subramanian, A Z; Cardile, P; Verplancke, R; Van Kerrebrouck, J; Spiga, S; Meyer, R; Bauwelinck, J; Baets, R; Van Steenberge, G

    2015-11-02

    This article presents the flip-chip bonding of vertical-cavity surface-emitting lasers (VCSELs) to silicon grating couplers (GCs) via SU8 prisms. The SU8 prisms are defined on top of the GCs using non-uniform laser ablation process. The prisms enable perfectly vertical coupling from the bonded VCSELs to the GCs. The VCSELs are flip-chip bonded on top of the silicon GCs employing the laser-induced forward transfer (LIFT)-assisted thermocompression technique. An excess loss of transmission experiments performed on the bonded assemblies with clear eye openings up to 20 Gb/s are also presented.

  7. Monolithic microwave integrated circuits

    Science.gov (United States)

    Pucel, R. A.

    Monolithic microwave integrated circuits (MMICs), a new microwave technology which is expected to exert a profound influence on microwave circuit designs for future military systems as well as for the commercial and consumer markets, is discussed. The book contains an historical discussion followed by a comprehensive review presenting the current status in the field. The general topics of the volume are: design considerations, materials and processing considerations, monolithic circuit applications, and CAD, measurement, and packaging techniques. All phases of MMIC technology are covered, from design to testing.

  8. Phase-locked arrays of vertical-cavity surface-emitting lasers

    Energy Technology Data Exchange (ETDEWEB)

    Warren, M.E.; Lear, K.L.; Gourley, P.L.; Hadley, G.R.; Vawter, G.A.; Brennan, T.M.; Hammons, B.E.; Zolper, J.C. [Sandia National Labs., Albuquerque, NM (United States); Lott, J.A. [Air Force Institute of Technology, Wright Patterson Air Force Base, OH (United States); Chalmers, S.A. [Optical Solutions, Albany, CA (United States)

    1994-04-01

    Vertical-Cavity Surface-Emitting Lasers (VCSELS) are of increasing interest to the photonics community because of their surface-emitting structure, simple fabrication and packaging, wafer-level testability, and potential for low cost manufacture. Scaling VCSELs to higher power outputs requires increasing the device area, which leads to transverse mode control difficulties if devices become larger than about 5 microns. One approach to increasing the device size while maintaining a well controlled transverse mode profile is formation of coupled or phase-locked two-dimensional arrays of VCSELs that are individually single-transverse mode. Such arrays have unique optical properties, not all of which are desirable. This paper covers some of the basic principles of these devices and reviews recent work on device designs, fabrication and operation. A technique for improving the far-field properties of the arrays is demonstrated and performance limitations are discussed.

  9. Monolithic Gradient Index Phase Plate Array Project

    Data.gov (United States)

    National Aeronautics and Space Administration — The "piston errors" and aberrations of the mirror segments used in large telescopes, are typically measured with on-board optical instruments, usually a dispersed...

  10. Embedded-monolith armor

    Science.gov (United States)

    McElfresh, Michael W.; Groves, Scott E; Moffet, Mitchell L.; Martin, Louis P.

    2016-07-19

    A lightweight armor system utilizing a face section having a multiplicity of monoliths embedded in a matrix supported on low density foam. The face section is supported with a strong stiff backing plate. The backing plate is mounted on a spall plate.

  11. Reach Extension and Capacity Enhancement of VCSEL-Based Transmission Over Single-Lane MMF Links

    DEFF Research Database (Denmark)

    Tatarczak, Anna; Motaghiannezam, S. M. Reza; Kocot, Chris

    2017-01-01

    This paper reviews and examines several techniques for expanding the carrying capacity of multimode fiber (MMF) using vertical cavity surface emitting lasers (VCSELs). The first approach utilizes short wavelength division multiplexing in combination with MMF optimized for operation between 850...

  12. Scalabilities of LEDs and VCSELs with tunnel-regenerated multi-active region structure

    Institute of Scientific and Technical Information of China (English)

    Xia GUO; Xinxin LUAN; Wenjuan WANG; Chunwei GUO; Guangdi SHEN

    2013-01-01

    Scalabilities of light-emitting diodes (LEDs) and vertical-cavity surface-emitting lasers (VCSELs) with tunnel-regenerated multi-active-region (TRMAR) structure were investigated. It was found that the output optical power and quantum efficiency of these new LEDs with TRMAR increased with the number of its active regions, but the threshold gain and threshold current density decreased. However, for VCSELs with TRMAR, the differential quantum efficiency and optical power increased with the number of the active region. The results suggest that LEDs and VCSELs with the TRMAR structure have some potential advantages over the conventional LEDs or VCSELs in high internal quantum efficiency, low heat generation, high round-trip gain, and so on. These advantages will make TRMAR LEDs or VCSELs more attractive for the industrial application.

  13. Modelling of photonic-crystal VCSELs with semi-vectorial and vectorial models

    DEFF Research Database (Denmark)

    Dems, Maciej; Chung, Il-Sug; Nyakas, Peter

    2011-01-01

    of the top-mirror DBR or just the VCSEL cavity. The different models are evaluated by comparing the predicted resonance wavelengths and threshold gains for different hole diameters and pitches of the PC. The agreement between the models is relatively good, with an exception of one case, which corresponds...... to the effective index method. The simulation results elucidate the strength and weaknesses of the analyzed methods and outline the limits of applicability of different models.......In the talk the results of the COST MP0702 exercise on modeling photonic- crystal (PC) VCSELs are presented. Four different numerical methods are compared through an analysis of a benchmark VCSEL structure, where the PC structure penetrates all VCSEL layers, the entire top-mirror DBR, a fraction...

  14. Flip-chip integration of tilted VCSELs onto a silicon photonic integrated circuit.

    Science.gov (United States)

    Lu, Huihui; Lee, Jun Su; Zhao, Yan; Scarcella, Carmelo; Cardile, Paolo; Daly, Aidan; Ortsiefer, Markus; Carroll, Lee; O'Brien, Peter

    2016-07-25

    In this article we describe a cost-effective approach for hybrid laser integration, in which vertical cavity surface emitting lasers (VCSELs) are passively-aligned and flip-chip bonded to a Si photonic integrated circuit (PIC), with a tilt-angle optimized for optical-insertion into standard grating-couplers. A tilt-angle of 10° is achieved by controlling the reflow of the solder ball deposition used for the electrical-contacting and mechanical-bonding of the VCSEL to the PIC. After flip-chip integration, the VCSEL-to-PIC insertion loss is -11.8 dB, indicating an excess coupling penalty of -5.9 dB, compared to Fibre-to-PIC coupling. Finite difference time domain simulations indicate that the penalty arises from the relatively poor match between the VCSEL mode and the grating-coupler.

  15. Colorless ONU Based on All-VCSEL Sources with Remote Optical Injection for WDM-PON

    DEFF Research Database (Denmark)

    Deng, Lei; Zhao, Ying; Pang, Xiaodan;

    2011-01-01

    We propose a novel low-cost and colorless WDM-PON architecture by using all VCSELs-based optical injection locking technique. A bidirectional transmission system over 26 km SMF at 5 Gbps without optical amplification is successfully achieved....

  16. Investigation of utilizing a VCSEL diode to work as a tunable optical bandpass filter

    Science.gov (United States)

    Chang, Ching-Hung; Huang, Yi-Syuan; Li, Chung-Yi

    2017-04-01

    Tunable optical band-pass filter (TOBPF) composed of a vertical-cavity surface-emitting laser (VCSEL) is proposed for multi-wavelength optical fiber transport systems. Experimental results prove that through properly adjusting VCSEL driving current, one of multiple injected lightwaves can properly flow through the proposed optical filter and others will be attenuated roughly 12 dB. Furthermore, by changing the VCSEL driving current, the pass-band window of the VCSEL-based TOBPF can be shifted to align with different designated injected lightwave and to block the others. By employing the TOBPF in multi-wavelength optical fiber transport systems, proper eye diagrams are experimentally observed for each dedicated optical signal. The proposed scheme is shown to be a practical and flexible component for multi-wavelength optical fiber transport systems.

  17. Colorless ONU Based on All-VCSEL Sources with Remote Optical Injection for WDM-PON

    DEFF Research Database (Denmark)

    Deng, Lei; Zhao, Ying; Pang, Xiaodan

    2011-01-01

    We propose a novel low-cost and colorless WDM-PON architecture by using all VCSELs-based optical injection locking technique. A bidirectional transmission system over 26 km SMF at 5 Gbps without optical amplification is successfully achieved....

  18. Improving the capacity of short-reach VCSEL-based MMF optical links

    DEFF Research Database (Denmark)

    Tatarczak, Anna; Lu, Xiaofeng; Tafur Monroy, Idelfonso

    2016-01-01

    We summarize strategies for increasing a capacity of short-reach links that base on an 850 nm VCSEL and an MMF. Presented methods include advanced modulation formats, equalization, WDM, quasi-single mode sources and a selective mode launch.......We summarize strategies for increasing a capacity of short-reach links that base on an 850 nm VCSEL and an MMF. Presented methods include advanced modulation formats, equalization, WDM, quasi-single mode sources and a selective mode launch....

  19. Real time algorithm temperature compensation in tunable laser / VCSEL based WDM-PON system

    DEFF Research Database (Denmark)

    Iglesias Olmedo, Miguel; Rodes Lopez, Roberto; Pham, Tien Thang

    2012-01-01

    We report on a real time experimental validation of a centralized algorithm for temperature compensation of tunable laser/VCSEL at ONU and OLT, respectively. Locking to a chosen WDM channel is shown for temperature changes over 40°C.......We report on a real time experimental validation of a centralized algorithm for temperature compensation of tunable laser/VCSEL at ONU and OLT, respectively. Locking to a chosen WDM channel is shown for temperature changes over 40°C....

  20. An electrical model of VCSEL as optical transmitter for optical printed circuit board

    Science.gov (United States)

    Kim, Do-Kyoon; Yoon, Young-Seol; Choi, Jin-Ho; Kim, Kyung-Min; Choi, Young-Wan; Lee, Seok

    2005-03-01

    Optical interconnection is recent issue for high-speed data transmission. The limitation of high-speed electrical data transmission is caused by impedance mismatching, electric field coupling, microwave loss, and different length of the electrical signal lines. To overcome these limitations, the electrical signal in the current electrical system has to be changed by the optical signal. The most suitable optical source in the OPCB (Optical Printed Circuit Board) is VCSEL (Vertical Cavity Surface Emitting Lasers) that is low-priced and has the characteristic of vertical surface emitting. In this paper, we propose an electrical model of the VCSEL as E/O converting devices for the OPCB. The equivalent circuit of the VCSEL based on the rate equations includes carrier dynamics and material properties. The rate equation parameters are obtained by full analysis based on rate equation and experiment results. The electrical model of the VCSEL has the series resistance determined by I-V characteristic curve, and the parallel capacitance by the parasitic response of the VCSEL chip. The bandwidth of the optical interconnection is analyzed considering those parameters. We design and fabricate the optical transmitter for OPCB considering proposed electrical model of VCSEL.

  1. Monolithic MACS micro resonators

    Science.gov (United States)

    Lehmann-Horn, J. A.; Jacquinot, J.-F.; Ginefri, J. C.; Bonhomme, C.; Sakellariou, D.

    2016-10-01

    Magic Angle Coil Spinning (MACS) aids improving the intrinsically low NMR sensitivity of heterogeneous microscopic samples. We report on the design and testing of a new type of monolithic 2D MACS resonators to overcome known limitations of conventional micro coils. The resonators' conductors were printed on dielectric substrate and tuned without utilizing lumped element capacitors. Self-resonance conditions have been computed by a hybrid FEM-MoM technique. Preliminary results reported here indicate robust mechanical stability, reduced eddy currents heating and negligible susceptibility effects. The gain in B1 /√{ P } is in agreement with the NMR sensitivity enhancement according to the principle of reciprocity. A sensitivity enhancement larger than 3 has been achieved in a monolithic micro resonator inside a standard 4 mm rotor at 500 MHz. These 2D resonators could offer higher performance micro-detection and ease of use of heterogeneous microscopic substances such as biomedical samples, microscopic specimens and thin film materials.

  2. The MONOLITH prototype

    CERN Document Server

    Ambrosio, M; Bencivenni, G; Candela, A M; Chiarini, A; Chignoli, F; De Deo, M; D'Incecco, M; Gerli, S; Giusti, P; Gómez, F; Gustavino, C; Lindozzi, M; Mannocchi, G; Menghetti, H; Morello, C; Murtas, F; Paoluzzi, G; Pilastrini, R; Redaelli, N G; Santoni, M; Sartorelli, G; Terranova, F; Trinchero, G C

    2000-01-01

    MONOLITH (Massive Observatory for Neutrino Oscillation or LImits on THeir existence) is the project of an experiment to study atmospheric neutrino oscillations with a massive magnetized iron detector. The baseline option is a 34 kt iron detector based on the use of about 50000 m/sup 2/ of the glass Resistive Plate Chambers (glass RPCs) developed at the Laboratori Nazionali del Gran Sasso (LNGS). An 8 ton prototype equipped with 23 m/sup 2/ of glass RPC has been realized and tested at the T7-PS beam at CERN. The energy resolution for pions follows a 68%/ square root (E(GeV))+2% law for orthogonally incident particles, in the energy range between 2 and 10 GeV. The time resolution and the tracking capability of the glass RPC are suitable for the MONOLITH experiment. (7 refs).

  3. Comparing 52 Gbps Duobinary and 4-PAM Transmission Over 100m OM-3 Fiber With 25GHz Class VCSELs

    DEFF Research Database (Denmark)

    Suhr, Lau Frejstrup; Lyubomirsky, Ilya; Daghighian, Henry M.

    This paper compares VCSEL based transmission of 52 Gbps duobinary-NRZ and 4-PAM over 100m OM-3 fiber employing a linear equalizer in the receiver.......This paper compares VCSEL based transmission of 52 Gbps duobinary-NRZ and 4-PAM over 100m OM-3 fiber employing a linear equalizer in the receiver....

  4. Long-distance multi-channel bidirectional chaos communication based on synchronized VCSELs subject to chaotic signal injection

    Science.gov (United States)

    Xie, Yi-Yuan; Li, Jia-Chao; He, Chao; Zhang, Zhen-Dong; Song, Ting-Ting; Xu, Chang-Jun; Wang, Gui-Jin

    2016-10-01

    A novel long-distance multi-channel bidirectional chaos communication system over multiple paths based on two synchronized 1550 nm vertical-cavity surface-emitting lasers (VCSELs) is proposed and studied theoretically. These two responding VCSELs (R-VCSELs) can output similar chaotic signals served as chaotic carrier in two linear polarization (LP) modes with identical signal injection from a driving VCSEL (D-VCSEL), which is subject to optical feedback and optical injection, simultaneously. Through the numerical simulations, high quality chaos synchronization between the two R-VCSELs can be obtained. Besides, the effects of varied qualities of chaos synchronization on communication performances in 20 km single mode fiber (SMF) channels are investigated by regulating different internal parameters mismatch after adopting chaos masking (CMS) technique. With the decrease of the maximum cross correlation coefficient (Max-C) between the two R-VCSELs, the bit error rate (BER) of decoded message increase. Meanwhile, the BER can still be less than 10-9 when the Max-C degrades to 0.982. Based on high quality synchronization, when the dispersion compensating fiber (DCF) links are introduced, 4n messages of 10 Gbit/s can transmit in 180 km SMF channels over n coupling paths, bidirectionally and simultaneously. Thorough tests are carried out with detailed analysis, demonstrating long-distance, multi-channel, bidirectional chaos communication based on VCSELs with chaotic signal injection.

  5. Bioaffinity chromatography on monolithic supports

    NARCIS (Netherlands)

    Tetala, K.K.R.; Beek, van T.A.

    2010-01-01

    Affinity chromatography on monolithic supports is a powerful analytical chemical platform because it allows for fast analyses, small sample volumes, strong enrichment of trace biomarkers and applications in microchips. In this review, the recent research using monolithic materials in the field of bi

  6. Bioaffinity chromatography on monolithic supports

    NARCIS (Netherlands)

    Tetala, K.K.R.; Beek, van T.A.

    2010-01-01

    Affinity chromatography on monolithic supports is a powerful analytical chemical platform because it allows for fast analyses, small sample volumes, strong enrichment of trace biomarkers and applications in microchips. In this review, the recent research using monolithic materials in the field of bi

  7. Demonstration of Raman-based, dispersion-managed VCSEL technology for fibre-to-the-hut application

    Science.gov (United States)

    Rotich Kipnoo, E. K.; Kiboi Boiyo, D.; Isoe, G. M.; Chabata, T. V.; Gamatham, R. R. G.; Leitch, A. W. R.; Gibbon, T. B.

    2017-03-01

    For the first time, we experimentally investigate the use of vertical cavity surface emitting lasers (VCSELs) in the fibre-to-the-home (FTTH) flavour for Africa, known as fibre-to-the-hut. Fibre-to-the-hut is a VCSEL based passive optical network technology designed and optimized for African continent. VCSELs have attracted attention in optical communication due to its vast advantages; low power consumption, relatively cheap costs among others. A 4.25 Gb/s uncooled VCSEL is used in a dispersion managed, Raman assisted network achieving beyond 100 km of error free transmission suited for FTTHut scenario. Energy-efficient high performance VCSEL is modulated using a 27-1 PRBS pattern and the signal transmitted on a G.655 fibre utilizing the minimum attenuation window.

  8. Design of monoliths through their mechanical properties.

    Science.gov (United States)

    Podgornik, Aleš; Savnik, Aleš; Jančar, Janez; Krajnc, Nika Lendero

    2014-03-14

    Chromatographic monoliths have several interesting properties making them attractive supports for analytics but also for purification, especially of large biomolecules and bioassemblies. Although many of monolith features were thoroughly investigated, there is no data available to predict how monolith mechanical properties affect its chromatographic performance. In this work, we investigated the effect of porosity, pore size and chemical modification on methacrylate monolith compression modulus. While a linear correlation between pore size and compression modulus was found, the effect of porosity was highly exponential. Through these correlations it was concluded that chemical modification affects monolith porosity without changing the monolith skeleton integrity. Mathematical model to describe the change of monolith permeability as a function of monolith compression modulus was derived and successfully validated for monoliths of different geometries and pore sizes. It enables the prediction of pressure drop increase due to monolith compressibility for any monolith structural characteristics, such as geometry, porosity, pore size or mobile phase properties like viscosity or flow rate, based solely on the data of compression modulus and structural data of non-compressed monolith. Furthermore, it enables simple determination of monolith pore size at which monolith compressibility is the smallest and the most robust performance is expected. Data of monolith compression modulus in combination with developed mathematical model can therefore be used for the prediction of monolith permeability during its implementation but also to accelerate the design of novel chromatographic monoliths with desired hydrodynamic properties for particular application.

  9. Radiation-hard/high-speed array-based optical engine

    Science.gov (United States)

    Gan, K. K.; Buchholz, P.; Heidbrink, S.; Kagan, H. P.; Kass, R. D.; Moore, J.; Smith, D. S.; Vogt, M.; Ziolkowski, M.

    2016-12-01

    We have designed and fabricated a compact array-based optical engine for transmitting data at 10 Gb/s. The device consists of a 4-channel ASIC driving a VCSEL (Vertical Cavity Surface Emitting Laser) array in an optical package. The ASIC is designed using only core transistors in a 65 nm CMOS process to enhance the radiation-hardness. The ASIC contains an 8-bit DAC to control the bias and modulation currents of the individual channels in the VCSEL array. The DAC settings are stored in SEU (single event upset) tolerant registers. Several devices were irradiated with 24 GeV/c protons and the performance of the devices is satisfactory after the irradiation.

  10. Porous polymer monolithic col

    Directory of Open Access Journals (Sweden)

    Lydia Terborg

    2015-05-01

    Full Text Available A new approach has been developed for the preparation of mixed-mode stationary phases to separate proteins. The pore surface of monolithic poly(glycidyl methacrylate-co-ethylene dimethacrylate capillary columns was functionalized with thiols and coated with gold nanoparticles. The final mixed mode surface chemistry was formed by attaching, in a single step, alkanethiols, mercaptoalkanoic acids, and their mixtures on the free surface of attached gold nanoparticles. Use of these mixtures allowed fine tuning of the hydrophobic/hydrophilic balance. The amount of attached gold nanoparticles according to thermal gravimetric analysis was 44.8 wt.%. This value together with results of frontal elution enabled calculation of surface coverage with the alkanethiol and mercaptoalkanoic acid ligands. Interestingly, alkanethiols coverage in a range of 4.46–4.51 molecules/nm2 significantly exceeded that of mercaptoalkanoic acids with 2.39–2.45 molecules/nm2. The mixed mode character of these monolithic stationary phases was for the first time demonstrated in the separations of proteins that could be achieved in the same column using gradient elution conditions typical of reverse phase (using gradient of acetonitrile in water and ion exchange chromatographic modes (applying gradient of salt in water, respectively.

  11. Optical chaos synchronization and encrypted communications of VCSEL by direct optical injection

    Science.gov (United States)

    Hosomi, Naohito; Sasaki, Wakao

    2014-09-01

    In this work, we propose electro-optical nonlinear delayed feedback systems (NDFS) for optical secure communications using VCSEL for the first time. Its optical output can perform more sensitive chaotic dynamics by varying only a few mA of injection current range resulting in very significant charges of VCSEL's operation conditions from threshold to maximum rating. This enables us to vary chaotic output dynamically by a slight difference of initial values in NDFS. We have proposed a chaos synchronization system using two identical NDFS's of VCSEL, and realized chaos synchronization by optical injection. As a result of experiment the correlation coefficient up to about 0.88 was obtained. Moreover, by varying the delay time and feedback gain in the parameters of NDFSs, we have confirmed that the variations of these parameters may affect variations of correlation.

  12. Coherent Detection for 1550 nm, 5 Gbit/s VCSEL Based 40 km Bidirectional PON Transmission

    DEFF Research Database (Denmark)

    Jensen, Jesper Bevensee; Rodes Lopez, Roberto; Zibar, Darko;

    2011-01-01

    Coherent detection of directly modulated 1550nm VCSELs in 5Gbit/s bidirectional 40km SSMF PON-links is presented. Receiver sensitivity of –37.3dBm after transmission is achieved with 30dB system margin, corresponding to 1:1024 passive powersplitting.......Coherent detection of directly modulated 1550nm VCSELs in 5Gbit/s bidirectional 40km SSMF PON-links is presented. Receiver sensitivity of –37.3dBm after transmission is achieved with 30dB system margin, corresponding to 1:1024 passive powersplitting....

  13. Half-cycle QAM modulation for VCSEL-based optical links

    DEFF Research Database (Denmark)

    Pham, Tien Thang; Rodes Lopez, Roberto; Jensen, Jesper Bevensee;

    2012-01-01

    Abstract (40-Word Limit): Novel spectrally efficient half-cycle QAM modulation is experimentally demonstrated. 10 Gbps 4-QAM signal in 7.5-GHz bandwidth was successfully transmitted over 20 km SMF using an un-cooled 1.5 µm VCSEL with no equalization applied.......Abstract (40-Word Limit): Novel spectrally efficient half-cycle QAM modulation is experimentally demonstrated. 10 Gbps 4-QAM signal in 7.5-GHz bandwidth was successfully transmitted over 20 km SMF using an un-cooled 1.5 µm VCSEL with no equalization applied....

  14. VCSEL sources for optical fiber-wireless composite data links at 60GHz

    DEFF Research Database (Denmark)

    Vegas Olmos, Juan José; Pang, Xiaodan; Lebedev, Alexander

    2013-01-01

    This paper presents a performance assessment of 60-GHz mm-wave signal generation using photonic upconversion employing a VCSEL as source. The system reaches 10−9 BER over a variety of optical fibers for data rates of 1.25-Gbit/s.......This paper presents a performance assessment of 60-GHz mm-wave signal generation using photonic upconversion employing a VCSEL as source. The system reaches 10−9 BER over a variety of optical fibers for data rates of 1.25-Gbit/s....

  15. Performance Evaluation for DFB and VCSEL-based 60 GHz Radio-over-Fiber System

    DEFF Research Database (Denmark)

    Pang, Xiaodan; Lebedev, Alexander; Vegas Olmos, Juan José

    2013-01-01

    In this paper, we report on a detailed analysis and performance comparison work between 60 GHz radio-over-fiber systems based on a DFB laser and a C-band VCSEL. Coherent photonic up-conversion method is applied for the 60 GHz millimeter-wave signal generation. The generated signals are evaluated...... by means of phase noise and bit error rate for different transmission scenarios. The results show a positive potential to adopt both DFB lasers and VCSELs for the next generation 60 GHz hybrid fiber-wireless access networks....

  16. Adaptive MultiCAP modulation for short range VCSEL based transmissions

    DEFF Research Database (Denmark)

    Puerta Ramírez, Rafael; Vegas Olmos, Juan José; Tafur Monroy, Idelfonso

    2016-01-01

    We propose an adaptive approach for multi-band carrierless amplitude/phase modulation, with advantages of adaptive bit rate and energy savings. Successful performance is demonstrated on 850 nm multi-mode VCSEL based transmissions achieving up to 40.6 Gb/s.......We propose an adaptive approach for multi-band carrierless amplitude/phase modulation, with advantages of adaptive bit rate and energy savings. Successful performance is demonstrated on 850 nm multi-mode VCSEL based transmissions achieving up to 40.6 Gb/s....

  17. Optimization of self-mixing modulation in VCSELs for sensing applications

    DEFF Research Database (Denmark)

    Larsson, David; Yvind, Kresten; Hvam, Jørn Märcher

    2009-01-01

    This paper numerically investigates, SMI in an oxide aperture VCSEL to optimize the epitaxial structure for higher performance. The standard investigated structure is emitting light at 970 nm from In0.17Ga0.83As-GaAsP QWs sandwiched between 36 pairs of bottom mirror and 23 pairs of top mirror (Alx......Ga1-xAs). The calculations are based on matrix multiplication for calculating effective reflectivity and transmission with external feedback, combined with a logarithmic gain model and standard laser rate equations. To improve the sensitivity towards self-mixing interference in VCSELs by simple...

  18. Biobased monoliths for adenovirus purification.

    Science.gov (United States)

    Fernandes, Cláudia S M; Gonçalves, Bianca; Sousa, Margarida; Martins, Duarte L; Barroso, Telma; Pina, Ana Sofia; Peixoto, Cristina; Aguiar-Ricardo, Ana; Roque, A Cecília A

    2015-04-01

    Adenoviruses are important platforms for vaccine development and vectors for gene therapy, increasing the demand for high titers of purified viral preparations. Monoliths are macroporous supports regarded as ideal for the purification of macromolecular complexes, including viral particles. Although common monoliths are based on synthetic polymers as methacrylates, we explored the potential of biopolymers processed by clean technologies to produce monoliths for adenovirus purification. Such an approach enables the development of disposable and biodegradable matrices for bioprocessing. A total of 20 monoliths were produced from different biopolymers (chitosan, agarose, and dextran), employing two distinct temperatures during the freezing process (-20 °C and -80 °C). The morphological and physical properties of the structures were thoroughly characterized. The monoliths presenting higher robustness and permeability rates were further analyzed for the nonspecific binding of Adenovirus serotype 5 (Ad5) preparations. The matrices presenting lower nonspecific Ad5 binding were further functionalized with quaternary amine anion-exchange ligand glycidyltrimethylammonium chloride hydrochloride by two distinct methods, and their performance toward Ad5 purification was assessed. The monolith composed of chitosan and poly(vinyl) alcohol (50:50) prepared at -80 °C allowed 100% recovery of Ad5 particles bound to the support. This is the first report of the successful purification of adenovirus using monoliths obtained from biopolymers processed by clean technologies.

  19. Two stage dual gate MESFET monolithic gain control amplifier for Ka-band

    Science.gov (United States)

    Sokolov, V.; Geddes, J.; Contolatis, A.

    A monolithic two stage gain control amplifier has been developed using submicron gate length dual gate MESFETs fabricated on ion implanted material. The amplifier has a gain of 12 dB at 30 GHz with a gain control range of over 30 dB. This ion implanted monolithic IC is readily integrable with other phased array receiver functions such as low noise amplifiers and phase shifters.

  20. SC-FDE for MMF short reach optical interconnects using directly modulated 850 nm VCSELs

    DEFF Research Database (Denmark)

    Teichmann, Victor S. C.; Barreto, Andre N.; Pham, Tien Thang

    2012-01-01

    We propose the use of single-carrier frequency-domain equalization (SC-FDE) for the compensation of modal dispersion in short distance optical links using multimode fibers and 850 nm VCSELs. By post-processing of experimental data, we demonstrate, at 7.9% overhead, the error-free transmission (ov...

  1. Observation of electro-activated localized structures in broad area VCSELs

    CERN Document Server

    Parravicini, J; Columbo, L; Prati, F; Rizza, C; Tissoni, G; Agranat, A J; DelRe, E

    2014-01-01

    We demonstrate experimentally the electro-activation of a localized optical structure in a coherently driven broad-area vertical-cavity surface-emitting laser (VCSEL) operated below threshold. Control is achieved by electro-optically steering a writing beam through a pre-programmable switch based on a photorefractive funnel waveguide.

  2. Real time 1.55 μm VCSEL-based coherent detection link

    DEFF Research Database (Denmark)

    Rodes Lopez, Roberto; Parekh, D.; Jensen, Jesper Bevensee

    2012-01-01

    This paper presents an experimental demonstration of VCSEL-based PON with simplified real-time coherent receiver at 2.5 Gbps. Receiver sensitivity of −37 dBm is achieved proving splitting ratio up to 2048 after 17 km fiber transmission....

  3. Radiation hardness and lifetime studies of the VCSELs for the ATLAS SemiConductor Tracker

    CERN Document Server

    Teng, P K; Chu, M L; Duh, T S; Gregor, I M; Hou, L S; Lee, S C; Song, P S; Su, D S

    2003-01-01

    Studies have been performed on the radiation hardness of the type of VCSELs**2 Vertical Cavity Surface Emitting Lasers. that will be used in the ATLAS SemicConductor Tracker. The measurements were made using 30 MeV proton beams, 24 GeV/c proton beams and a gamma source. The lifetime of the devices after irradiation was studied.

  4. Polarization and dynamical properties of VCSELs-based photonic neuron subject to optical pulse injection

    Science.gov (United States)

    Xiang, Shuiying; Wen, Aijun; Zhang, Hao; Li, Jiafu; Guo, Xingxing; Shang, Lei; Lin, Lin

    2016-11-01

    The polarization-resolved nonlinear dynamics of vertical-cavity surface-emitting lasers (VCSELs) subject to orthogonally polarized optical pulse injection are investigated numerically based on the spin flip model. By extensive numerical bifurcation analysis, the responses dynamics of photonic neuron based on VCSELs under the arrival of external stimuli of orthogonally polarized optical pulse injection are mainly discussed. It is found that, several neuron-like dynamics, such as phasic spiking of a single abrupt large amplitude pulse followed with or without subthreshold oscillation, and tonic spiking with multiple periodic pulses, are successfully reproduced in the numerical model of VCSELs. Besides, the effects of stimuli strength, pump current, frequency detuning, as well as the linewidth enhancement factor on the neuron-like response dynamics are examined carefully. The operating parameters ranges corresponding to different neuron-like dynamics are further identified. Thus, the numerical model and simulation results are very useful and interesting for the ultrafast brain-inspired neuromorphic photonics systems based on VCSELs.

  5. 10 Gb/s Real-Time All-VCSEL Low Complexity Coherent scheme for PONs

    DEFF Research Database (Denmark)

    Rodes Lopez, Roberto; Cheng, Ning; Jensen, Jesper Bevensee;

    2012-01-01

    Real time demodulation of a 10 Gb/s all-VCSEL based coherent PON link with a simplified coherent receiver scheme is demonstrated. Receiver sensitivity of −33 dBm is achieved providing high splitting ratio and link reach....

  6. 980-nm VCSELs for optical interconnects at bandwidths beyond 40 Gb/s

    Science.gov (United States)

    Hofmann, W. H.; Moser, P.; Wolf, P.; Larisch, G.; Unrau, W.; Bimberg, D.

    2012-03-01

    The copper-induced communication bottleneck is inhibiting performance and environmental acceptance of today's supercomputers. Vertical-cavity surface-emitting lasers (VCSELs) are ideally suited to solve this dilemma. Indeed global players like Google, Intel, HP or IBM are now going for optical interconnects based on VCSELs. The required bandwidth per link, however, is fixed by the architecture of the data center. According to Google, a bandwidth of 40 Gb/s has to be accommodated. We recently realized ultra-high speed VCSELs suited for optical interconnects in data centers with record-high performance. The 980-nm wavelength was chosen to be able to realize densely-packed, bottom-emitting devices particularly advantageous for interconnects. These devices show error-free transmission at temperatures up to 155°C. Serial data-rates of 40 Gb/s were achieved up to 75° C. Peltier-cooled devices were modulated up to 50 Gb/s. These results were achieved from the sender side by a VCSEL structure with important improvements and from the receiver side by a receiver module supplied by u2t with some 30 GHz bandwidth. The novel VCSELs feature a new active region, a very short laser cavity, and a drastically improved thermal resistance by the incorporation of a binary bottom mirror. As these devices might be of industrial interest we had the epi-growth done by metal-organic chemical-vapor deposition at IQE Europe. Consequently, the devices were fabricated using a three-inch wafer process, and the apertures were formed by proprietary in-situ controlled selective wet oxidation. All device data were measured, mapped and evaluated by our fully automated probe station. Furthermore, these devices enable record-efficient data-transmission beyond 30 Gb/s, which is crucial for green photonics.

  7. Solid oxide fuel cell having monolithic core

    Science.gov (United States)

    Ackerman, J. P.; Young, J. E.

    1983-10-01

    A solid oxide fuel cell is described for electrochemically combining fuel and oxidant for generating galvanic output, wherein the cell core has an array of electrolyte and interconnect walls that are substantially devoid of any composite inert materials for support. The core is monolithic, where each electrolyte wall consists of thin layers of cathode and anode materials sandwiching a thin layer of electrolyte material. The electrolyte walls are arranged and backfolded between adjacent interconnect walls operable to define a plurality of core passageways alternately arranged where the inside faces have only the anode material or only the cathode material exposed. Each layer of the electrolyte and interconnect materials 0.002 to 0.01 cm thick; and each layer of the cathode and anode materials is 0.002 to 0.05 cm thick.

  8. VCSEL-based, high-speed, in situ TDLAS for in-cylinder water vapor measurements in IC engines

    National Research Council Canada - National Science Library

    Witzel, O; Klein, A; Meffert, C; Wagner, S; Kaiser, S; Schulz, C; Ebert, V

    2013-01-01

    We report the first application of a vertical-cavity surfaceemitting laser (VCSEL) for calibration- and sampling-free, high-speed, in situ H2O concentration measurements in IC engines using direct TDLAS...

  9. High-speed tunable and fixed-wavelength VCSELs for short-reach optical links and interconnects

    Science.gov (United States)

    Larsson, A.; Gustavsson, J. S.; Haglund, Å.; Kögel, B.; Bengtsson, J.; Westbergh, P.; Haglund, E.; Baveja, P. P.

    2012-03-01

    This paper presents a review of recent work on high speed tunable and fixed wavelength vertical cavity surface emitting lasers (VCSELs) at Chalmers University of Technology. All VCSELs are GaAs-based, employ an oxide aperture for current and/or optical confinement, and emit around 850 nm. With proper active region and cavity designs, and techniques for reducing capacitance and thermal impedance, our fixed wavelength VCSELs have reached a modulation bandwidth of 23 GHz, which has enabled error-free 40 Gbps back-to-back transmission and 35 Gbps transmission over 100 m of multimode fiber. A MEMS-technology for wafer scale integration of tunable high speed VCSELs has also been developed. A tuning range of 24 nm and a modulation bandwidth of 6 GHz have been achieved, enabling error-free back-to-back transmission at 5 Gbps.

  10. Energy-efficient VCSEL-based multiGigabit IR-UWB over Fiber with Airlink Transmission System

    DEFF Research Database (Denmark)

    Rodes Lopez, Roberto; Pham, Tien Thang; Jensen, Jesper Bevensee;

    2010-01-01

    We propose VCSEL based impulse-radio ultrawideband technology for energy efficient high-speed wireless networks; with full passive signal distribution, from the central office to the home with high-speed wireless connection to the final user.......We propose VCSEL based impulse-radio ultrawideband technology for energy efficient high-speed wireless networks; with full passive signal distribution, from the central office to the home with high-speed wireless connection to the final user....

  11. 8-dimensional lattice optimized formats in 25-GBaud/s VCSEL based IM/DD optical interconnections

    DEFF Research Database (Denmark)

    Lu, Xiaofeng; Tafur Monroy, Idelfonso

    2015-01-01

    Temporally combined 4- and 8-dimensional lattice grids optimized modulation formats for VCSEL based IM/DD short-reach optical inter-connections has been proposed and investigated numerically together with its conventional counterpart PAM-4. © 2015 OSA.......Temporally combined 4- and 8-dimensional lattice grids optimized modulation formats for VCSEL based IM/DD short-reach optical inter-connections has been proposed and investigated numerically together with its conventional counterpart PAM-4. © 2015 OSA....

  12. Reconfigurable high-speed optical fibre networks: Optical wavelength conversion and switching using VCSELs to eliminate channel collisions

    Science.gov (United States)

    Boiyo, Duncan Kiboi; Chabata, T. V.; Kipnoo, E. K. Rotich; Gamatham, R. R. G.; Leitch, A. W. R.; Gibbon, T. B.

    2017-01-01

    We experimentally provide an alternative solution to channel collisions through up-wavelength conversion and switching by using vertical cavity surface-emitting lasers (VCSELs). This has been achieved by utilizing purely optical wavelength conversion on VCSELs at the low attenuation, 1550 nm transmission window. The corresponding transmission and bit error-rate (BER) performance evaluation is also presented. In this paper, two 1550 nm VCSELs with 50-150 GHz channel spacing are modulated with a 10 Gb/s NRZ PRBS 27-1 data and their interferences investigated. A channel interference penalty range of 0.15-1.63 dB is incurred for 150-50 GHz channel spacing without transmission. To avoid channel collisions and to minimize high interference penalties, the transmitting VCSEL with data is injected into the side-mode of a slave VCSEL to obtain a new up converted wavelength. A 16 dB extinction ratio of the incoming wavelength is achieved when a 15 dBm transmitting beam is injected into the side-mode of a -4.5 dBm slave VCSEL. At 8.5 Gb/s, a 1.1 dB conversion and a 0.5 dB transmission penalties are realized when the converted wavelength is transmitted over a 24.7 km G.655 fibre. This work offers a low-cost, effective wavelength conversion and channel switching to reduce channel collision probability by reconfiguring channels at the node of networks.

  13. Non-Hermitian engineering of single mode two dimensional laser arrays

    CERN Document Server

    Teimourpour, Mohammad H; Christodoulides, Demetrios N; El-Ganainy, Ramy

    2016-01-01

    A new scheme for building two dimensional laser arrays that operate in the single supermode regime is proposed. This is done by introducing an optical coupling between the laser array and a lossy pseudo-isospectral chain of photonic resonators. The spectrum of this discrete reservoir is tailored to suppress all the supermodes of the main array except the fundamental one. This spectral engineering is facilitated by employing the Householder transformation in conjunction with discrete supersymmetry. The proposed scheme is general and can in principle be used in different platforms such as VCSEL arrays and photonic crystal laser arrays.

  14. 107.5 Gb/s 850 nm multi- and single-mode VCSEL transmission over 10 and 100 m of multi-mode fiber

    DEFF Research Database (Denmark)

    Puerta Ramírez, Rafael; Agustin, M.; Chorchos, L.

    2016-01-01

    First time successful 107.5 Gb/s MultiCAP 850 nm OM4 MMF transmissions over 10 m with multi-mode VCSEL and up to 100 m with single-mode VCSEL are demonstrated, with BER below 7% overhead FEC limit measured for each case.......First time successful 107.5 Gb/s MultiCAP 850 nm OM4 MMF transmissions over 10 m with multi-mode VCSEL and up to 100 m with single-mode VCSEL are demonstrated, with BER below 7% overhead FEC limit measured for each case....

  15. Polarization-locked VCSEL with PM fiber pigtail for quantum communication

    Institute of Scientific and Technical Information of China (English)

    Guofeng Xin; Zujie Fang; Weibiao Chen; Li Shen; Haoyang Pi; Dijun Chen; Haiwen Cai; Huizhong Feng; Jianxin Geng; Ronghui Qu; Gaoting Chen

    2012-01-01

    Quantum communication is a new technology requiring a stable and reliable laser source for communication security.A new kind of polarization-locked vertical-cavity surface-emitting laser (VCSEL) with polarization maintaining (PM) fiber pigtail is fabricated as a decoy state laser source.The VCSEL is packaged in a standard butterfly box integrated with thermoelectric coder (TEC) and thermistor.The optical pulse width of full-width at half-maximum (FWHM) is smaller than 400 ps with a 100-MHz on/off modulation frequency.The results reveal that modulation range is better than 4.Moreover,the polarization is stable,and the power extinction ratio is larger than 25.The center wavelength is 850 nm,and the SMSR is better than 40 dB.

  16. Dynamics of dual-polarization VCSEL-based optical frequency combs under optical injection locking.

    Science.gov (United States)

    Prior, E; de Dios, C; Criado, R; Ortsiefer, M; Meissner, P; Acedo, P

    2016-09-01

    The present experimental work studies the dynamics of dual-polarization optical frequency combs (OFCs) based on gain switching (GS) vertical-cavity surface-emitting laser (VCSEL) diodes under optical injection locking (OIL). This study presents two main results. First, we have obtained an overall comb formed by two orthogonally polarized sub-combs with comparable span and power. The overall comb shows enhanced optical span and flatness and high coherence between its modes. The second result is that we have been able to control the polarization state of the overall comb by tuning the polarization state of the injected light by locking the same single teeth of the comb. This produces an overall comb with single polarization that is parallel or orthogonal. These are novel findings that provide for the development of efficient and compact OFCs based on GS VCSEL sources with versatile polarization dynamics.

  17. Fabrication and characterization of monolithic solid oxide fuel cells

    Science.gov (United States)

    Minh, N. Q.; Horne, C. R.; Liu, F. S.; Moffatt, D. M.; Staszak, P. R.

    The monolithic solid oxide fuel cell (MSOFC) is an all-ceramic structure in which cell components are configured in a compact corrugated array. The MSOFC shows promise for use in a wide range of sizes (kilowatt to megawatt) and a broad spectrum of applications (electric utility, cogeneration, on-site, and aerospace power). A process based on the tape calendering technique is being developed for the fabrication of the MSOFC. MSOFC single cells have been fabricated by this process without cracking or delamination. Stacks of various sizes have been formed and processed to demonstrate fabricability of the monolithic structure. Extensive physical, chemical, electrical, and electrochemical characterization of fabricated samples has been carried out to confirm the required properties of each cell component. The characterization results reported have been used to support material and fabrication improvements.

  18. Microfabricated ion trap array

    Science.gov (United States)

    Blain, Matthew G.; Fleming, James G.

    2006-12-26

    A microfabricated ion trap array, comprising a plurality of ion traps having an inner radius of order one micron, can be fabricated using surface micromachining techniques and materials known to the integrated circuits manufacturing and microelectromechanical systems industries. Micromachining methods enable batch fabrication, reduced manufacturing costs, dimensional and positional precision, and monolithic integration of massive arrays of ion traps with microscale ion generation and detection devices. Massive arraying enables the microscale ion traps to retain the resolution, sensitivity, and mass range advantages necessary for high chemical selectivity. The reduced electrode voltage enables integration of the microfabricated ion trap array with on-chip circuit-based rf operation and detection electronics (i.e., cell phone electronics). Therefore, the full performance advantages of the microfabricated ion trap array can be realized in truly field portable, handheld microanalysis systems.

  19. Optical injection induced polarization mode switching and correlation analysis on a VCSEL

    CERN Document Server

    Damodarakurup, Sajeev; Vudayagiri, Ashok

    2015-01-01

    Vertical cavity Surface Emitting Laser (VCSEL) diodes emit light in two polarization modes. The amount of optical feedback is found to influence the intensities of the emitted modes. We investigate the effect of the amount of total output polarization feedback and polarization selective feedback on the intensities of the two emitted polarization modes. A 40 micro seconds resolution time series correlation analysis is done for different feedback conditions and investigate the power spectral continuity and onset of chaos on two polarization modes

  20. In situ Fabrication of Monolithic Copper Azide

    Science.gov (United States)

    Li, Bing; Li, Mingyu; Zeng, Qingxuan; Wu, Xingyu

    2016-04-01

    Fabrication and characterization of monolithic copper azide were performed. The monolithic nanoporous copper (NPC) with interconnected pores and nanoparticles was prepared by decomposition and sintering of the ultrafine copper oxalate. The preferable monolithic NPC can be obtained through decomposition and sintering at 400°C for 30 min. Then, the available monolithic NPC was in situ reacted with the gaseous HN3 for 24 h and the monolithic NPC was transformed into monolithic copper azide. Additionally, the copper particles prepared by electrodeposition were also reacted with the gaseous HN3 under uniform conditions as a comparison. The fabricated monolithic copper azide was characterized by Fourier transform infrared (FTIR), inductively coupled plasma-optical emission spectrometry (ICP-OES), and differential scanning calorimetry (DSC).

  1. Dedicated monolithic infrared spectrometer for process monitoring

    Science.gov (United States)

    Chadha, Suneet; Kyle, William; Bolduc, Roy A.; Curtiss, Lawrence E.

    1999-12-01

    Foster-Miller has leveraged its innovations in IR fiber- optic probes and the recent development of a miniature spectrometer to build a novel IR sensor system for process applications. The developed sensor systems is a low-cost alternative to process FTIR and filter based systems. A monolithic wedge-grating optic provides the spectral dispersion with low cost thermopile point or array detectors picking off the diffracted wavelengths from the optic. The integrated optic provides spectral discrimination between 3- 12 micrometers with resolution at 8 cm-1 or better and high overall optical throughput. The device has a fixed cylindrical grating uniquely bonded to the edge of a ZnSe conditioning 'wedge'. The conditioning optic overcomes limitations of concave gratings as it accepts high angle light at the narrow end of the wedge and progressively conditions it to be near normal to the grating. On return, the diffracted wavelengths are concentrated on the discrete or array detector elements by the wedge, providing throughput comparable to that of an FTIR. The miniature spectrometer coupled to flow through liquid cells or multipass gas cells provides significant cost advantage over conventional sampling methodologies. Currently, we are investigating process applications for the petroleum and dairy markets. The sensor system eliminates the cost, complexity, reliability and bandwidth/resolution problems associated with either Fabry Perot or Michelson Interferometer based approaches for low-cost process applications.

  2. 14 MeV neutron-induced transverse mode shifts in multimode VCSELs

    CERN Document Server

    Pailharey, E; D'Hose, C; Musseau, O

    2000-01-01

    Research on optical communication behavior in radiative environments is a key point for the design of diagnostic links for the large physical instruments (Laser MegaJoule at CEA, Large Hadron Collider at CERN). For years, the radiation tolerance of several types of emitters (LED and LD) have been tested with promising results for the LDs. New technologies and devices (VCSEL) have recently appeared as promising candidates to replace conventional edge emitting LDs. The shorter wavelength VCSELs (below 1 mu m) are well adapted for short distance data links, due to their low threshold current, high efficiency and large possibilities for integration. 850 nm VCSELs are tested under 14 MeV neutron irradiation. Three different aperture (8 mu m monomode, 15 mu m and 20 mu m multimode) COTS devices are irradiated up to 3.4*10/sup 13/ n/cm/sup 2/. Transverse pattern behavior is studied using infrared camera imaging, while optical power modifications are measured as a function of bias current. Displacement damage induces...

  3. Detection of ochratoxin A in beer samples with a label-free monolithically integrated optoelectronic biosensor

    NARCIS (Netherlands)

    Pagkali, Varvara; Petrou, Panagiota S.; Salapatas, Alexandros; Makarona, Eleni; Peters, Jeroen; Haasnoot, Willem; Jobst, Gerhard; Economou, Anastasios; Misiakos, Konstantinos; Raptis, Ioannis; Kakabakos, Sotirios E.

    2016-01-01

    An optical biosensor for label-free detection of ochratoxin A (OTA) in beer samples is presented. The biosensor consists of an array of ten Mach-Zehnder interferometers (MZIs) monolithically integrated along with their respective broad-band silicon light sources on the same Si chip (37mm2

  4. Detection of ochratoxin A in beer samples with a label-free monolithically integrated optoelectronic biosensor

    NARCIS (Netherlands)

    Pagkali, Varvara; Petrou, Panagiota S.; Salapatas, Alexandros; Makarona, Eleni; Peters, Jeroen; Haasnoot, Willem; Jobst, Gerhard; Economou, Anastasios; Misiakos, Konstantinos; Raptis, Ioannis; Kakabakos, Sotirios E.

    2017-01-01

    An optical biosensor for label-free detection of ochratoxin A (OTA) in beer samples is presented. The biosensor consists of an array of ten Mach-Zehnder interferometers (MZIs) monolithically integrated along with their respective broad-band silicon light sources on the same Si chip (37mm2

  5. Fully integrated monolithic opoelectronic transducer for real.time protein and DNA detection

    DEFF Research Database (Denmark)

    Misiakos, Konstatinos; S. Petrou, Panagiota; E. Kakabakos, Sotirios

    2010-01-01

    The development and testing of a portable bioanalytical device which was capable for real-time monitoring of binding assays was demonstrated. The device was based on arrays of nine optoelectronic transducers monolithically integrated on silicon chips. The optocouplers consisted of nine silicon av...

  6. Thick monolithic scintillation crystals for TOF-PET with depth-of-interaction measurement

    NARCIS (Netherlands)

    Vinke, Ruud; van Dam, Herman T.; Seifert, Stefan; Beekman, Freek J.; Lohner, Herbert; Schaart, Dennis R.; Dendooven, Peter

    2010-01-01

    Positron emission tomography (PET) detectors based on monolithic scintillation crystals show excellent intrinsic spatial resolution and allow depth-of-interaction (DOI) reconstruction using a single photosensor array. The inclusion of time-of-flight (TOF) information in the image reconstruction

  7. Monolithic Fuel Fabrication Process Development

    Energy Technology Data Exchange (ETDEWEB)

    C. R. Clark; N. P. Hallinan; J. F. Jue; D. D. Keiser; J. M. Wight

    2006-05-01

    The pursuit of a high uranium density research reactor fuel plate has led to monolithic fuel, which possesses the greatest possible uranium density in the fuel region. Process developments in fabrication development include friction stir welding tool geometry and cooling improvements and a reduction in the length of time required to complete the transient liquid phase bonding process. Annealing effects on the microstructures of the U-10Mo foil and friction stir welded aluminum 6061 cladding are also examined.

  8. Pressure drop in CIM disk monolithic columns.

    Science.gov (United States)

    Mihelic, Igor; Nemec, Damjan; Podgornik, Ales; Koloini, Tine

    2005-02-11

    Pressure drop analysis in commercial CIM disk monolithic columns is presented. Experimental measurements of pressure drop are compared to hydrodynamic models usually employed for prediction of pressure drop in packed beds, e.g. free surface model and capillary model applying hydraulic radius concept. However, the comparison between pressure drop in monolith and adequate packed bed give unexpected results. Pressure drop in a CIM disk monolithic column is approximately 50% lower than in an adequate packed bed of spheres having the same hydraulic radius as CIM disk monolith; meaning they both have the same porosity and the same specific surface area. This phenomenon seems to be a consequence of the monolithic porous structure which is quite different in terms of the pore size distribution and parallel pore nonuniformity compared to the one in conventional packed beds. The number of self-similar levels for the CIM monoliths was estimated to be between 1.03 and 2.75.

  9. Graphene-supported metal oxide monolith

    Energy Technology Data Exchange (ETDEWEB)

    Worsley, Marcus A.; Baumann, Theodore F.; Biener, Juergen; Biener, Monika A.; Wang, Yinmin; Ye, Jianchao; Tylski, Elijah

    2017-01-10

    A composition comprising at least one graphene-supported metal oxide monolith, said monolith comprising a three-dimensional structure of graphene sheets crosslinked by covalent carbon bonds, wherein the graphene sheets are coated by at least one metal oxide such as iron oxide or titanium oxide. Also provided is an electrode comprising the aforementioned graphene-supported metal oxide monolith, wherein the electrode can be substantially free of any carbon-black and substantially free of any binder.

  10. Graphene-supported metal oxide monolith

    Science.gov (United States)

    Worsley, Marcus A.; Baumann, Theodore F.; Biener, Juergen; Biener, Monika A.; Wang, Yinmin; Ye, Jianchao; Tylski, Elijah

    2017-01-10

    A composition comprising at least one graphene-supported metal oxide monolith, said monolith comprising a three-dimensional structure of graphene sheets crosslinked by covalent carbon bonds, wherein the graphene sheets are coated by at least one metal oxide such as iron oxide or titanium oxide. Also provided is an electrode comprising the aforementioned graphene-supported metal oxide monolith, wherein the electrode can be substantially free of any carbon-black and substantially free of any binder.

  11. Study on differences between high contrast grating reflectors for TM and TE polarizations and their impact on VCSEL designs

    CERN Document Server

    Chung, Il-Sug

    2015-01-01

    A theoretical study of differences in broadband high-index-contrast grating (HCG) reflectors for TM and TE polarizations is presented, covering various grating parameters and properties of HCGs. It is shown that the HCG reflectors for TM polarization (TM HCG reflectors) have much thicker grating thicknesses and smaller grating periods than the TE HCG reflectors. This difference is found to originate from the different boundary conditions met for the electric field of each polarization. Due to this difference, the TM HCG reflectors have much shorter evanescent extension of HCG modes into low-refractive-index media surrounding the HCG. This enables to achieve a very short effective cavity length for VCSELs, which is essential for ultrahigh speed VCSELs and MEMS-tunable VCSELs. The obtained understandings on polarization dependences will be able to serve as important design guidelines for various HCG-based devices.

  12. Preparation and applications of monolithic structures containing metal-organic frameworks.

    Science.gov (United States)

    Lv, Yongqin; Tan, Xinyi; Svec, Frantisek

    2017-01-01

    Metal-organic frameworks are a new category of advanced porous materials with large surface areas and porosities, uniform pore sizes, tunable surface chemistry, and structural diversity. In combination with monoliths, they allow the fine tuning of desired interactions required in a variety of applications. This review article summarizes results of recent studies focused on synthetic strategies enabling incorporation of metal-organic frameworks in monolithic structures. A diverse array of applications including chromatographic separation, solid-phase microextraction, sample enrichment, heterogeneous catalysis, and enzymatic catalysis are also described. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  13. In-building Unlicensed WiFi Band OFDM Signal Distribution over MMF&BIF Using VCSEL

    DEFF Research Database (Denmark)

    Deng, Lei; Jensen, Jesper Bevensee; Yu, Xianbin

    2011-01-01

    For in-building applications, an OFDM-VCSEL RoF system operating in unlicensed WiFi band is experimentally tested using MMF and bend insensitive fiber (BIF). A spectral efficiency of 4.32 bit/s/Hz with 0.9 Gbps data rate is achieved.......For in-building applications, an OFDM-VCSEL RoF system operating in unlicensed WiFi band is experimentally tested using MMF and bend insensitive fiber (BIF). A spectral efficiency of 4.32 bit/s/Hz with 0.9 Gbps data rate is achieved....

  14. Robust design of Si/Si3N4 high contrast grating mirror for mid-infrared VCSEL application

    CERN Document Server

    Chevallier, Christyves; Genty, Frédéric; Jacquet, Joel

    2012-01-01

    A Si/Si3N4 high contrast grating mirror has been designed for a VCSEL integration in mid-infrared ({\\lambda} = 2.65 $\\mu$m). The use of an optimization algorithm which maximizes a VCSEL mirror quality factor allowed the adjustment of the grating parameters while keeping large and shallow grating pattern. The robustness with respect to fabrication error has been enhanced thanks to a precise study of the grating dimension tolerances. The final mirror exhibits large high reflectivity bandwidth with a polarization selectivity and several percent of tolerance on the grating dimensions.

  15. Free-Running 1550 nm VCSEL for 10.7 Gb/s Transmission in 99.7 km PON

    DEFF Research Database (Denmark)

    Prince, Kamau; Ma, Ming; Gibbon, Timothy Braidwood;

    2011-01-01

    We present a cooler-less, free-running 1550 nm vertical cavity surface emitting laser (VCSEL) directly modulated at 10.7 Gb/s. We also report on error-free transmission through 40 km of standard single-mode optical fiber, achieved without the use of dispersion-mitigation or mid-span amplification....... Inverse-dispersion fiber was utilized to realize a dispersion-matched 99.7 km optical access uplink supporting error-free transmission with 27 dB loss margin. These results indicate the feasibility of implementing cooler-less long-wavelength VCSEL devices in long-reach optical access networks....

  16. Directly-Modulated VCSELs for 2x2 MIMO-OFDM Radio over Fiber in WDM-PON

    DEFF Research Database (Denmark)

    Binti Othman, Maisara; Deng, Lei; Pang, Xiaodan;

    2011-01-01

    We demonstrate directly- modulated VCSELs supporting 2x2 MIMO-OFDM 5.6-GHz radio over fiber signaling over 20-km WDM-PON. Error-free signal demodulation of 64-subcarrier 4-QAM signals modulated at 198.5-Mb/s is achieved after fiber and 2-m indoor wireless transmission.......We demonstrate directly- modulated VCSELs supporting 2x2 MIMO-OFDM 5.6-GHz radio over fiber signaling over 20-km WDM-PON. Error-free signal demodulation of 64-subcarrier 4-QAM signals modulated at 198.5-Mb/s is achieved after fiber and 2-m indoor wireless transmission....

  17. VCSEL-Based DWDM PON With 4 BIT/S/HZ Spectral Efficiency Using Carrierless Amplitude Phase Modulation

    DEFF Research Database (Denmark)

    Rodes Lopez, Roberto; Wieckowski, Marcin; Pham, Tien Thang

    2011-01-01

    We experimental demonstrate successful performance of VCSEL-based WDM link supporting advanced 16-level carrierless amplitude/phase modulation up to 1.25 Gbps, over 26 km SSMF with spectral efficiency of 4 bit/s/Hz for application in high capacity PONs.......We experimental demonstrate successful performance of VCSEL-based WDM link supporting advanced 16-level carrierless amplitude/phase modulation up to 1.25 Gbps, over 26 km SSMF with spectral efficiency of 4 bit/s/Hz for application in high capacity PONs....

  18. VCSEL-based gigabit impulse radio UWB for converged wireless sensor and communication in-building networks

    DEFF Research Database (Denmark)

    Gibbon, Timothy Braidwood; Pham, Tien Thang; Neumeyr, C.

    2010-01-01

    A 1550nm VCSEL-generated UWB signal is used for simultaneous 2Gb/s wireless data transfer and to measuring the rotational speed of a blade spinning between 18-29Hz, with up to 50km distribution over single mode fibre.......A 1550nm VCSEL-generated UWB signal is used for simultaneous 2Gb/s wireless data transfer and to measuring the rotational speed of a blade spinning between 18-29Hz, with up to 50km distribution over single mode fibre....

  19. SC-FDE for MMF short reach optical interconnects using directly modulated 850 nm VCSELs.

    Science.gov (United States)

    Teichmann, Victor S C; Barreto, Andre N; Pham, Tien-Thang; Rodes, Roberto; Monroy, Idelfonso T; Mello, Darli A A

    2012-11-05

    We propose the use of single-carrier frequency-domain equalization (SC-FDE) for the compensation of modal dispersion in short distance optical links using multimode fibers and 850 nm VCSELs. By post-processing of experimental data, we demonstrate, at 7.9% overhead, the error-free transmission (over a 4 Mbit sequence) of OOK-modulated 5 Gbps over 2443 meters of OM3 fiber (with a nominal 3300 MHz×km bandwidth). The proposed solution may be applied as a low cost alternative for data center and supercomputer interconnects.

  20. 30 Gbps 4-PAM transmission over 200 m of MMF using an 850 nm VCSEL.

    Science.gov (United States)

    Szczerba, Krzysztof; Westbergh, Petter; Karout, Johnny; Gustavsson, Johan; Haglund, Åsa; Karlsson, Magnus; Andrekson, Peter; Agrell, Erik; Larsson, Anders

    2011-12-12

    We present high speed real time, error free 4-PAM transmission for short range optical links based on a VCSEL operating at 850 nm, a multimode fibre and a simple intensity detector. Transmission speeds of 25 Gbps and 30 Gbps are demonstrated, and the maximum fibre reaches were 300 m and 200 m, respectively. The 4-PAM is also compared with OOK transmission at 25 Gbps, and we find that at this bit rate 4-PAM increases the error free transmission distance in the multimode fibre by 100 m, compared to OOK.

  1. Design and optimization of DBR in 980 nm bottom-emitting VCSEL

    Institute of Scientific and Technical Information of China (English)

    LI Te; NING YongQiang; HAO ErJuan; CUI JinJiang; ZHANG Yan; LIU GuangYu; QIN Li; LIU Yun; WANG LiJun; CUI DaFu; XU ZuYan

    2009-01-01

    According to the theory of DBR, with the P-type DBR as an example, the electrical characteristics and optical reflection of the DBR are analyzed by studying the energy band structure with various graded region widths and doping densities. The width and doping density of graded region are decided through a comparative study. The P-type DBR of 980 nm VCSELs is designed with Al0.9Ga0.1As and AI0.1Ga0.9As selected as the high and low refractive index material for the DBR. The 980 nm bottom VCSELs, which consists of 30 pairs P-type DBR and 28 pairs N-type DBR, are then fabricated. In P-type DBR, the width of graded region is 0.02 μm and the uniformity doping concentration is 2.5×1018cm-3. Its reflectivity is 99.9%. In N-type DBR, the width of graded region is also 0.02 μm and the uniformity doping concentration is 2×1018cm-3. Its reflectivity is 99.3%. The I-V curve shows that the series resistance of the device is about 0.05 Ω. According to the theory of DBR, with the P-type DBR as an example, the electrical characteristics and optical reflection of the DBR are analyzed by studying the energy band structure with various graded region widths and doping densities. The width and doping density of graded region are decided through a comparative study. The P-type DBR of 980 nm VCSELs is designed, with Al0.9Ga0.1As and Al0.1Ga0.9As selected as the high and low refractive index material for the DBR. The 980 nm bottom VCSELs, which consist of 30 pairs P-type DBR and 28 pairs N-type DBR, are then fabricated. In P-type DBR, the width of graded region is 0.02 μm and the uniformity doping concentration is 2.5×1018cm-3. Its reflectivity is 99.9%. In N-type DBR, the width of graded region is also 0.02 μm and the uniformity doping concentration is 2×1018cm-3. Its reflectivity is 99.3%. The I-V curve shows that the series resistance of the device is about 0.05 Ω.

  2. Large Aperture Low Threshold Current 980nm VCSELs Fabricated with Pulsed Anodic Oxidation

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    Pulsed anodic oxidation technique, a new way of forming current blocking layers, was successfully used in ridge-waveguide QW laser fabrication. This method was applied in 980 nm VCSELs fabrication to form a high-quality native oxide current blocking layer, which simplifies the device process. A significant reduction of threshold current and a distinguished device performance are achieved. The 500 μm diameter device has a current threshold as low as 0.48 W. The maximum CW operation output power at room tempe...

  3. Sub-cycle QAM modulation for VCSEL-based optical fiber links

    DEFF Research Database (Denmark)

    Pham, Tien-Thang; Rodes Lopez, Roberto; Jensen, Jesper Bevensee;

    2013-01-01

    QAM modulation utilizing subcarrier frequency lower than the symbol rate is both theoretically and experimentally investigated. High spectral efficiency and concentration of power in low frequencies make sub-cycle QAM signals attractive for optical fiber links with direct modulated light sources....... Real-time generated 10-Gbps 4-level QAM signal in a 7.5-GHz bandwidth utilizing subcarrier frequency at a half symbol rate was successfully transmitted over 20-km SMF using an un-cooled 1.5-μm VCSEL. Only 2.5-dB fiber transmission power penalty was observed with no equalization applied....

  4. Monolithically integrated absolute frequency comb laser system

    Energy Technology Data Exchange (ETDEWEB)

    Wanke, Michael C.

    2016-07-12

    Rather than down-convert optical frequencies, a QCL laser system directly generates a THz frequency comb in a compact monolithically integrated chip that can be locked to an absolute frequency without the need of a frequency-comb synthesizer. The monolithic, absolute frequency comb can provide a THz frequency reference and tool for high-resolution broad band spectroscopy.

  5. Compact monolithic capacitive discharge unit

    Science.gov (United States)

    Roesler, Alexander W.; Vernon, George E.; Hoke, Darren A.; De Marquis, Virginia K.; Harris, Steven M.

    2007-06-26

    A compact monolithic capacitive discharge unit (CDU) is disclosed in which a thyristor switch and a flyback charging circuit are both sandwiched about a ceramic energy storage capacitor. The result is a compact rugged assembly which provides a low-inductance current discharge path. The flyback charging circuit preferably includes a low-temperature co-fired ceramic transformer. The CDU can further include one or more ceramic substrates for enclosing the thyristor switch and for holding various passive components used in the flyback charging circuit. A load such as a detonator can also be attached directly to the CDU.

  6. Monolithic crystals for PET devices: Optical coupling optimization

    Energy Technology Data Exchange (ETDEWEB)

    González, A.J., E-mail: agonzalez@i3m.upv.es; Peiró, A.; Conde, P.; Hernández, L.; Moliner, L.; Orero, A.; Rodríguez-Álvarez, M.J.; Sánchez, F.; Soriano, A.; Vidal, L.F.; Benlloch, J.M.

    2013-12-11

    In this work we present a method to efficiently collect scintillation light when using monolithic scintillator crystals. The acceptance angle of the scintillation light has been reduced by means of optical devices reducing the border effect which typically affects continuous crystals. We have applied this procedure on gamma detectors for PET systems using both position sensitive PMTs and arrays of SiPMs. In the case of using SiPMs, this approach also helps to reduce the photosensor active area. We evaluated the method using PMTs with a variety of different crystals with thicknesses ranging from 10 to 24 mm. We found that our design allows the use of crystal blocks with a thickness of up to 18 mm without degrading the spatial resolution caused by edge effects and without a significant detriment to the energy resolution. These results were compared with simulated data. The first results of monolithic LYSO crystals coupled to an array of 256 SiPMs by means of individual optical light guides are also presented. -- Highlights: •Acceptance angle reduction decreases border effect in continuous crystals. •Experimental measurements with PMTs correlate well with simulated data. •Optical devices called faceplates serve to control the scintillation light angle. •Simulation on the light propagation for SiPMs requires exhaustive modeling.

  7. Polymer monolith microextraction using poly(butyl methacrylate-co-1,6-hexanediol ethoxylate diacrylate) monolithic sorbent for determination of phenylurea herbicides in water samples.

    Science.gov (United States)

    Lin, Shu-Ling; Wu, Yu-Ru; Fuh, Ming-Ren

    2016-01-15

    In this study, recently developed 1,6-hexanediol ethoxylate diacrylate (HEDA)-based polymeric monoliths were utilized as sorbents for efficient extraction of phenylurea herbicides (PUHs) from water samples. The HEDA-based monolithic sorbents were prepared in a fused silica capillary (0.7mm i.d., 4.5-cm long) for polymer monolith microextraction (PMME). The experimental parameters of PMME microextraction including sample loading speed, pH of sample solution, composition of elution solvent, and addition of salt were optimized to efficiently extract PUHs from environmental water samples. The extracted PUHs were determined using ultra-high performance liquid chromatography (UHPLC) with UV-photodiode array detection. The extraction recoveries for PUHs-spiked water samples were 91.1-108.1% with relative standard deviations lower than 5%. The linearity range was 0.025-25ngmL(-1) for each PUH and the detection limits of PUHs were estimated at 0.006-0.019ng mL(-1). In addition, good intra-day/inter-day precision (0.1-8.7%/0.2-8.9%) and accuracy (92.0-108.0%/96.5-105.2%) of the proposed method were obtained. The extraction capacity of the monolith-filled capillary was also determined to be approximately 1μg. Moreover, each monolith-filled capillary could be reused up to 8 times without carry-over. According to the European Union regulations, the allowed permissible limit of any single herbicide in drinking water is 0.1ng mL(-1). This permissible level fell in the linear range examined in this study. In addition, the proposed method provided detection limits lower than the allowed permissible level, which demonstrated the feasibility of utilizing the HEDA-based monolithic sorbent to perform PMME for determining contaminants, such as PUHs, in environmental application.

  8. Initial results for the silicon monolithically interconnected solar cell product

    Science.gov (United States)

    Dinetta, L. C.; Shreve, K. P.; Cotter, J. E.; Barnett, A. M.

    1995-01-01

    This proprietary technology is based on AstroPower's electrostatic bonding and innovative silicon solar cell processing techniques. Electrostatic bonding allows silicon wafers to be permanently attached to a thermally matched glass superstrate and then thinned to final thicknesses less than 25 micron. These devices are based on the features of a thin, light-trapping silicon solar cell: high voltage, high current, light weight (high specific power) and high radiation resistance. Monolithic interconnection allows the fabrication costs on a per watt basis to be roughly independent of the array size, power or voltage, therefore, the cost effectiveness to manufacture solar cell arrays with output powers ranging from milliwatts up to four watts and output voltages ranging from 5 to 500 volts will be similar. This compares favorably to conventionally manufactured, commercial solar cell arrays, where handling of small parts is very labor intensive and costly. In this way, a wide variety of product specifications can be met using the same fabrication techniques. Prototype solar cells have demonstrated efficiencies greater than 11%. An open-circuit voltage of 5.4 volts, fill factor of 65%, and short-circuit current density of 28 mA/sq cm at AM1.5 illumination are typical. Future efforts are being directed to optimization of the solar cell operating characteristics as well as production processing. The monolithic approach has a number of inherent advantages, including reduced cost per interconnect and increased reliability of array connections. These features make this proprietary technology an excellent candidate for a large number of consumer products.

  9. Active inductor shunt peaking in high-speed VCSEL driver design

    CERN Document Server

    Liang, Futian; Hou, Suen; Liu, Chonghan; Liu, Tiankuan; Su, Da-Shung; Teng, Ping-Kun; Xiang, Annie; Ye, Jingbo; Jin, Ge

    2013-01-01

    An all transistor active inductor shunt peaking structure has been used in a prototype of 8-Gbps high-speed VCSEL driver which is designed for the optical link in ATLAS liquid Argon calorimeter upgrade. The VCSEL driver is fabricated in a commercial 0.25-um Silicon-on-Sapphire (SoS) CMOS process for radiation tolerant purpose. The all transistor active inductor shunt peaking is used to overcome the bandwidth limitation from the CMOS process. The peaking structure has the same peaking effect as the passive one, but takes a small area, does not need linear resistors and can overcome the process variation by adjust the peaking strength via an external control. The design has been tapped out, and the prototype has been proofed by the preliminary electrical test results and bit error ratio test results. The driver achieves 8-Gbps data rate as simulated with the peaking. We present the all transistor active inductor shunt peaking structure, simulation and test results in this paper.

  10. Half-cycle modulation for VCSEL based 6-Gbaud 4-QAM transmission over 1 km multimode fibre link

    DEFF Research Database (Denmark)

    Pham, Tien Thang; Rodes Lopez, Roberto; Estaran Tolosa, Jose Manuel

    2012-01-01

    A subcarrier multiplexing system with the subcarrier frequency at half the baud rate to improve the spectral efficiency is demonstrated. A 12 Gbit/s 4-QAM signal in 9GHz bandwidth was successfully transmitted over a 1 km OM4 MMF 850 nm VCSEL without any equalisation method. The 1.5 dB power penalty...

  11. Temperature stable mid-infrared GaInAsSb/GaSb Vertical Cavity Surface Emitting Lasers (VCSELs)

    Science.gov (United States)

    Ikyo, A. B.; Marko, I. P.; Hild, K.; Adams, A. R.; Arafin, S.; Amann, M.-C.; Sweeney, S. J.

    2016-01-01

    GaInAsSb/GaSb based quantum well vertical cavity surface emitting lasers (VCSELs) operating in mid-infrared spectral range between 2 and 3 micrometres are of great importance for low cost gas monitoring applications. This paper discusses the efficiency and temperature sensitivity of the VCSELs emitting at 2.6 μm and the processes that must be controlled to provide temperature stable operation. We show that non-radiative Auger recombination dominates the threshold current and limits the device performance at room temperature. Critically, we demonstrate that the combined influence of non-radiative recombination and gain peak – cavity mode de-tuning determines the overall temperature sensitivity of the VCSELs. The results show that improved temperature stable operation around room temperature can only be achieved with a larger gain peak – cavity mode de-tuning, offsetting the significant effect of increasing non-radiative recombination with increasing temperature, a physical effect which must be accounted for in mid-infrared VCSEL design.

  12. Carrierless amplitude phase modulation of VCSEL with 4 bit/s/Hz spectral efficiency for use in WDM-PON

    DEFF Research Database (Denmark)

    Rodes Lopez, Roberto; Wieckowski, Marcin; Pham, Tien Thang

    2011-01-01

    We experimentally demonstrate successful performance of VCSEL-based WDM link supporting advanced 16-level carrierless amplitude/phase modulation up to 1.25 Gbps, over 26 km SSMF with spectral efficiency of 4 bit/s/Hz for application in high capacity PONs. © 2011 Optical Society of America....

  13. Microfluidic devices and methods including porous polymer monoliths

    Science.gov (United States)

    Hatch, Anson V; Sommer, Gregory J; Singh, Anup K; Wang, Ying-Chih; Abhyankar, Vinay V

    2014-04-22

    Microfluidic devices and methods including porous polymer monoliths are described. Polymerization techniques may be used to generate porous polymer monoliths having pores defined by a liquid component of a fluid mixture. The fluid mixture may contain iniferters and the resulting porous polymer monolith may include surfaces terminated with iniferter species. Capture molecules may then be grafted to the monolith pores.

  14. Monolithic Continuous-Flow Bioreactors

    Science.gov (United States)

    Stephanopoulos, Gregory; Kornfield, Julia A.; Voecks, Gerald A.

    1993-01-01

    Monolithic ceramic matrices containing many small flow passages useful as continuous-flow bioreactors. Ceramic matrix containing passages made by extruding and firing suitable ceramic. Pores in matrix provide attachment medium for film of cells and allow free movement of solution. Material one not toxic to micro-organisms grown in reactor. In reactor, liquid nutrients flow over, and liquid reaction products flow from, cell culture immobilized in one set of channels while oxygen flows to, and gaseous reaction products flow from, culture in adjacent set of passages. Cells live on inner surfaces containing flowing nutrient and in pores of walls of passages. Ready access to nutrients and oxygen in channels. They generate continuous high yield characteristic of immobilized cells, without large expenditure of energy otherwise incurred if necessary to pump nutrient solution through dense biomass as in bioreactors of other types.

  15. GaAs optoelectronic neuron arrays

    Science.gov (United States)

    Lin, Steven; Grot, Annette; Luo, Jiafu; Psaltis, Demetri

    1993-01-01

    A simple optoelectronic circuit integrated monolithically in GaAs to implement sigmoidal neuron responses is presented. The circuit integrates a light-emitting diode with one or two transistors and one or two photodetectors. The design considerations for building arrays with densities of up to 10,000/sq cm are discussed.

  16. Monolithic Micromachined Quartz Resonator based Infrared Focal Plane Arrays

    Science.gov (United States)

    2012-05-05

    etching of glass using nitrogen trifluoride based gas . MEMS Personnel Working on the Project • Dr. Srinivas Tadigadapa, Professor, Penn State...source could be varied. • The RF power supplied operated at 13.56 MHz. RF Power Supply RF Matching Network Gas Inlet ICP Source Antenna Magnetic...500-2000 Substrate Power Watts 100-475 O2 Flow Rate sccm 5-100 SF6 Flow Rate sccm 5-50 C4F8 Flow Rate sccm 5-50 CH4 Flow Rate sccm 5-50 Ar Flow

  17. Application of Uncooled Monolithic Thermoelectric Linear Arrays to Imaging Radiometers

    Science.gov (United States)

    Kruse, Paul W.

    Introduction Identification of Incipient Failure of Railcar Wheels Technical Description of the Model IR 1000 Imaging Radiometer Performance of the Model IR 1000 Imaging Radiometer Initial Application Summary Imaging Radiometer for Predictive and Preventive Maintenance Description Operation Specifications Summary References INDEX CONTENTS OF VOLUMES IN THIS SERIES

  18. Progress Toward a Monolithically Integrated Coherent Diode Laser Array.

    Science.gov (United States)

    1981-02-20

    B-i C. DBR AND ACTIVE-PASSIVE LASER FABRICATION PROCEDURE ............... C-I D. ELECTROCHEMICAL DEPOSITION OF OHMIC CONTACTS FOR DIODE... LASER FABRICATION PROCEDURE C.1 SAMPLE EXAMINATION 1. Etch sample in 1:1:8 A-B etch (A:B:H 20 mp) for 5 sec. 2. Photograph all four corners of sample to...GaAlAs waveguide att ,uation coeffi- cients; 1 6 the assumption that K remains the same for both DBRs simplifies con- siderably the actual DBR laser

  19. Anisotropically structured magnetic aerogel monoliths

    Science.gov (United States)

    Heiligtag, Florian J.; Airaghi Leccardi, Marta J. I.; Erdem, Derya; Süess, Martin J.; Niederberger, Markus

    2014-10-01

    Texturing of magnetic ceramics and composites by aligning and fixing of colloidal particles in a magnetic field is a powerful strategy to induce anisotropic chemical, physical and especially mechanical properties into bulk materials. If porosity could be introduced, anisotropically structured magnetic materials would be the perfect supports for magnetic separations in biotechnology or for magnetic field-assisted chemical reactions. Aerogels, combining high porosity with nanoscale structural features, offer an exceptionally large surface area, but they are difficult to magnetically texture. Here we present the preparation of anatase-magnetite aerogel monoliths via the assembly of preformed nanocrystallites. Different approaches are proposed to produce macroscopic bodies with gradient-like magnetic segmentation or with strongly anisotropic magnetic texture.Texturing of magnetic ceramics and composites by aligning and fixing of colloidal particles in a magnetic field is a powerful strategy to induce anisotropic chemical, physical and especially mechanical properties into bulk materials. If porosity could be introduced, anisotropically structured magnetic materials would be the perfect supports for magnetic separations in biotechnology or for magnetic field-assisted chemical reactions. Aerogels, combining high porosity with nanoscale structural features, offer an exceptionally large surface area, but they are difficult to magnetically texture. Here we present the preparation of anatase-magnetite aerogel monoliths via the assembly of preformed nanocrystallites. Different approaches are proposed to produce macroscopic bodies with gradient-like magnetic segmentation or with strongly anisotropic magnetic texture. Electronic supplementary information (ESI) available: Digital photographs of dispersions and gels with different water-to-ethanol ratios; magnetic measurements of an anatase aerogel containing 0.25 mol% Fe3O4 nanoparticles; XRD patterns of the iron oxide and

  20. Monolithic cells for solar fuels.

    Science.gov (United States)

    Rongé, Jan; Bosserez, Tom; Martel, David; Nervi, Carlo; Boarino, Luca; Taulelle, Francis; Decher, Gero; Bordiga, Silvia; Martens, Johan A

    2014-12-07

    Hybrid energy generation models based on a variety of alternative energy supply technologies are considered the best way to cope with the depletion of fossil energy resources and to limit global warming. One of the currently missing technologies is the mimic of natural photosynthesis to convert carbon dioxide and water into chemical fuel using sunlight. This idea has been around for decades, but artificial photosynthesis of organic molecules is still far away from providing real-world solutions. The scientific challenge is to perform in an efficient way the multi-electron transfer reactions of water oxidation and carbon dioxide reduction using holes and single electrons generated in an illuminated semiconductor. In this tutorial review the design of photoelectrochemical (PEC) cells that combine solar water oxidation and CO2 reduction is discussed. In such PEC cells simultaneous transport and efficient use of light, electrons, protons and molecules has to be managed. It is explained how efficiency can be gained by compartmentalisation of the water oxidation and CO2 reduction processes by proton exchange membranes, and monolithic concepts of artificial leaves and solar membranes are presented. Besides transferring protons from the anode to the cathode compartment the membrane serves as a molecular barrier material to prevent cross-over of oxygen and fuel molecules. Innovative nano-organized multimaterials will be needed to realise practical artificial photosynthesis devices. This review provides an overview of synthesis techniques which could be used to realise monolithic multifunctional membrane-electrode assemblies, such as Layer-by-Layer (LbL) deposition, Atomic Layer Deposition (ALD), and porous silicon (porSi) engineering. Advances in modelling approaches, electrochemical techniques and in situ spectroscopies to characterise overall PEC cell performance are discussed.

  1. Effective 100 Gb/s IM/DD 850-nm Multi- and Single-Mode VCSEL Transmission Through OM4 MMF

    DEFF Research Database (Denmark)

    Puerta Ramírez, Rafael; Agustin, Mikel; Chorchos, Lukasz

    2017-01-01

    of OM4 multimode fiber (MMF) using a multimode VCSEL at 850 nm, and up to 100 m of OM4 MMF using a single-mode VCSEL at 850 nm. Measured bit error rates were below 7% overhead forward error correction limit of 3.8e−03, thus, achieving an effective bit rate of 100.5 Gb/s. These successful transmissions...

  2. On-chip generation and demultiplexing of quantum correlated photons using a silicon-silica monolithic photonic integration platform.

    Science.gov (United States)

    Matsuda, Nobuyuki; Karkus, Peter; Nishi, Hidetaka; Tsuchizawa, Tai; Munro, William J; Takesue, Hiroki; Yamada, Koji

    2014-09-22

    We demonstrate the generation and demultiplexing of quantum correlated photons on a monolithic photonic chip composed of silicon and silica-based waveguides. Photon pairs generated in a nonlinear silicon waveguide are successfully separated into two optical channels of an arrayed-waveguide grating fabricated on a silica-based waveguide platform.

  3. High-speed highly temperature stable 980 nm VCSELs operating at 25 Gb/s at up to 85 °C for short reach optical interconnects

    Science.gov (United States)

    Mutig, Alex; Lott, James A.; Blokhin, Sergey A.; Moser, Philip; Wolf, Philip; Hofmann, Werner; Nadtochiy, Alexey M.; Bimberg, Dieter

    2011-03-01

    The progressive penetration of optical communication links into traditional copper interconnect markets greatly expands the applications of vertical cavity surface emitting lasers (VCSELs) for the next-generation of board-to-board, moduleto- module, chip-to-chip, and on-chip optical interconnects. Stability of the VCSEL parameters at high temperatures is indispensable for such applications, since these lasers typically reside directly on or near integrated circuit chips. Here we present 980 nm oxide-confined VCSELs operating error-free at bit rates up to 25 Gbit/s at temperatures as high as 85 °C without adjustment of the drive current and peak-to-peak modulation voltage. The driver design is therefore simplified and the power consumption of the driver electronics is lowered, reducing the production and operational costs. Small and large signal modulation experiments at various temperatures from 20 up to 85 °C for lasers with different oxide aperture diameters are presented in order to analyze the physical processes controlling the performance of the VCSELs. Temperature insensitive maximum -3 dB bandwidths of around 13-15 GHz for VCSELs with aperture diameters of 10 μm and corresponding parasitic cut-off frequencies exceeding 22 GHz are observed. Presented results demonstrate the suitability of our VCSELs for practical high speed and high temperature stable short-reach optical links.

  4. Monolithic multinozzle emitters for nanoelectrospray mass spectrometry

    Science.gov (United States)

    Wang, Daojing; Yang, Peidong; Kim, Woong; Fan, Rong

    2011-09-20

    Novel and significantly simplified procedures for fabrication of fully integrated nanoelectrospray emitters have been described. For nanofabricated monolithic multinozzle emitters (NM.sup.2 emitters), a bottom up approach using silicon nanowires on a silicon sliver is used. For microfabricated monolithic multinozzle emitters (M.sup.3 emitters), a top down approach using MEMS techniques on silicon wafers is used. The emitters have performance comparable to that of commercially-available silica capillary emitters for nanoelectrospray mass spectrometry.

  5. Large Aperture Low Threshold Current 980 nm VCSELs Fabricated with Pulsed Anodic Oxidation

    Institute of Scientific and Technical Information of China (English)

    CUI Jin-jiang; NING Yong-qiang; LI Te; LIU Guang-yu; ZHANG Yan; PENG Biao; SUN Yan-fang; WANG Li-jun

    2007-01-01

    Pulsed anodic oxidation technique, a new way of forming current blocking layers, was successfully used in ridge-waveguide QW laser fabrication. This method was applied in 980 nm VCSELs fabrication to form a high-quality native oxide current blocking layer, which simplifies the device process. A significant reduction of threshold current and a distinguished device performance are achieved. The 500 μm diameter device has a current threshold as low as 048 W. The maximum CW operation output power at room temperature is 1.48 W. The lateral divergence angle θ‖ and vertical divergence angle θ⊥ are as low as 15.3° and 13.8° without side-lobes at a current of 6 A.

  6. A 1.3 Tb/s parallel optics VCSEL link

    Science.gov (United States)

    Hasharoni, Kobi; Benjamin, Shuki; Geron, Amir; Stepanov, Stanislav; Katz, Gideon; Epstein, Itai; Margalit, Niv; Chairman, David; Mesh, Michael

    2014-03-01

    A high bandwidth optical interconnect is designed based on parallel optical VCSEL links. Large matrices with 168 data channels are utilized exhibiting the highest reported full duplex aggregate bandwidth of 1.34Tb/s. Optical links of 300m are measured with BER Optical packaging is enabled using fiber bundle matrices whose dimensions are identical to those of the optoelectronic chips. The entire chip is assembled onto a system PCB in telecom and datacom applications. The backplane of the system becomes passive optical backplane and is entirely fiber based. The hybrid integration allows for a 3-fold increase in the number of SerDes available on a single package to about 500 lanes.

  7. Activated Carbon Fiber Monoliths as Supercapacitor Electrodes

    Directory of Open Access Journals (Sweden)

    Gelines Moreno-Fernandez

    2017-01-01

    Full Text Available Activated carbon fibers (ACF are interesting candidates for electrodes in electrochemical energy storage devices; however, one major drawback for practical application is their low density. In the present work, monoliths were synthesized from two different ACFs, reaching 3 times higher densities than the original ACFs’ apparent densities. The porosity of the monoliths was only slightly decreased with respect to the pristine ACFs, the employed PVDC binder developing additional porosity upon carbonization. The ACF monoliths are essentially microporous and reach BET surface areas of up to 1838 m2 g−1. SEM analysis reveals that the ACFs are well embedded into the monolith structure and that their length was significantly reduced due to the monolith preparation process. The carbonized monoliths were studied as supercapacitor electrodes in two- and three-electrode cells having 2 M H2SO4 as electrolyte. Maximum capacitances of around 200 F g−1 were reached. The results confirm that the capacitance of the bisulfate anions essentially originates from the double layer, while hydronium cations contribute with a mixture of both, double layer capacitance and pseudocapacitance.

  8. High finesse external cavity VCSELs: from very low noise lasers to dual frequency lasers

    Science.gov (United States)

    Baili, Ghaya; Alouini, Medhi; Morvan, Loic; Bretenaker, Fabien; Sagnes, Isabelle; Garnache, Arnaud; Dolfi, Daniel

    2011-01-01

    Low noise-level optical sources are required for numerous applications such as microwave photonics, fiber-optic sensing and time/frequency references distribution. In this paper, we demonstrate how inserting a SC active medium into a centimetric high-Q external cavity is a simple way to obtain a shot-noise-limited laser source over a very wide frequency bandwidth. This approach ensures, with a compact design, a sufficiently long photon lifetime to reach the oscillation-relaxation- free class-A regime. This concept has been illustrated by inserting a 1/2-VCSEL in an external cavity including an etalon filter. A -156dB/Hz relative intensity noise level is obtained over the 100 MHz to 18 GHz bandwidth of interest. This is several orders of magnitude better than the noise, previously observed in VCSELs, belonging to the class-B regime. The optimization, in terms of noise, is shown to be a trade-off between the cavity length and the laser mode filtering. The transition between the class-B and class-A dynamical behaviors is directly observed by continuously controlling the photon lifetime is a sub-millimetric to a centimetric cavity length. It's proven that the transition occurs progressively, without any discontinuity. Based on the same laser architecture, tunable dual-frequency oscillation is demonstrated by reducing the polarized eigenstates overlap in the gain medium. The class-A dynamics of such a laser, free of relaxation oscillations, enables to suppress the electrical phase noise in excess, usually observed in the vicinity of the beat note. An original technique for jitter reduction in mode-locked VECSELs is also investigated. Such lasers are needed for photonic analog to digital converters.

  9. Experimental Analysis of 60-GHz VCSEL and ECL Photonic Generation and Transmission of Impulse-Radio Ultra-Wideband Signals

    DEFF Research Database (Denmark)

    Beltran, Marta; Jensen, Jesper Bevensee; Llorente, Roberto

    2011-01-01

    Optical generation of impulse-radio ultra-wideband (UWB) signals in the 60-GHz band is proposed and experimentally demonstrated. External-cavity laser (ECL) and vertical-cavity surface-emitting laser (VCSEL) is employed for frequency up-conversion by heterodyne mixing with a UWB optical signal...... for comparison purposes. Real-time bit-error-rate (BER) performance of generated signals at 3.125 Gb/s is evaluated combining fiber and 2-m wireless transmission. Different optical fiber types including 1-km bend-insensitive single-mode fiber and 20-km nonzero dispersion-shifted fiber is evaluated. $\\hbox......{BER} for the ECL and $\\hbox{BER} for the VCSEL requiring higher received optical power than the ECL is demonstrated employing electrical power detection....

  10. Narrow-linewidth photonic microwave generation based on an optically injected 1550 nm VCSEL subject to optoelectronic feedback

    Science.gov (United States)

    Liang, Qing; Fan, Li; Yang, Ji-Yun; Wang, Zhen-Zhen; Wu, Zheng-Mao; Xia, Guang-Qiong

    2016-11-01

    High-quality photonic microwave generation is experimentally demonstrated based on the period-one (P1) dynamical state output from an optically injected 1550 nm vertical-cavity surface-emitting laser (1550 nm-VCSEL) subject to optoelectronic negative feedback. The experimental results show that, under suitable injection condition, the 1550 nm-VCSEL can generate a photonic microwave signal with single sideband optical spectrum structure, but the linewidth of the microwave signal is relatively wide (on the order of MHz). After further introducing optoelectronic negative feedback, the linewidth of the microwave signal can be narrowed two orders of magnitude to 105.7 kHz. Furthermore, for the case that the feedback strength is set at an optimized value, the frequency of the microwave signal can be tuned continuously within a certain range through simply adjusting the injection strength.

  11. VCSEL-based, high-speed, in situ TDLAS for in-cylinder water vapor measurements in IC engines.

    Science.gov (United States)

    Witzel, O; Klein, A; Meffert, C; Wagner, S; Kaiser, S; Schulz, C; Ebert, V

    2013-08-26

    We report the first application of a vertical-cavity surfaceemitting laser (VCSEL) for calibration- and sampling-free, high-speed, in situ H2O concentration measurements in IC engines using direct TDLAS (tunable diode laser absorption spectroscopy). Measurements were performed in a single-cylinder research engine operated under motored conditions with a time resolution down to 100 μs (i.e., 1.2 crank angle degrees at 2000 rpm). Signal-to-noise ratios (1σ) up to 29 were achieved, corresponding to a H2O precision of 0.046 vol.% H2O or 39 ppm · m. The modulation frequency dependence of the performance was investigated at different engine operating points in order to quantify the advantages of VCSEL against DFB lasers.

  12. Evaluation of the frequency stability of a VCSEL locked to a micro-fabricated Rubidium vapour cell

    Science.gov (United States)

    Di Francesco, J.; Gruet, F.; Schori, C.; Affolderbach, C.; Matthey, R.; Mileti, G.; Salvadé, Y.; Petremand, Y.; De Rooij, N.

    2010-04-01

    We present our evaluation of a compact laser system made of a 795 nm VCSEL locked to the Rubidium absorption line of a micro-fabricated absorption cell. The spectrum of the VCSEL was characterised, including its RIN, FM noise and line-width. We optimised the signal-to-noise ratio and determined the frequency shifts versus the cell temperature and the incident optical power. The frequency stability of the laser (Allan deviation) was measured using a high-resolution wavemeter and an ECDL-based reference. Our results show that a fractional instability of anodic bonding. The overall thickness of the reference cell is 1.5 mm. No buffer gas was added. The potential applications of this compact and low-consumption system range from optical interferometers to basic laser spectroscopy. It is particularly attractive for mobile and space instruments where stable and accurate wavelength references are needed.

  13. VCSEL-based gigabit IR-UWB link for converged communication and sensing applications in optical metro-access networks

    DEFF Research Database (Denmark)

    Pham, Tien Thang; Gibbon, Timothy Braidwood; Tafur Monroy, Idelfonso

    2012-01-01

    We report on experimental demonstration of an impulse radio ultrawideband (IR-UWB) based converged communication and sensing system. A 1550-nm VCSEL-generated IR-UWB signal is used for 2-Gbps wireless data distribution over 800-m and 50-km single mode fiber links which present short-range in......-building and long-reach access network applications. The IR-UWB signal is also used to simultaneously measure the rotational speed of a blade spinning between 18 and 30 Hz. To the best of our knowledge, this is the very first demonstration of a simultaneous gigabit UWB telecommunication and wireless UWB sensing...... application, paving the way forward for the development and deployment of converged UWB VCSEL-based technologies in access and in-building networks of the future....

  14. Monolithically integrated Ge CMOS laser

    Science.gov (United States)

    Camacho-Aguilera, Rodolfo

    2014-02-01

    Ge-on-Si devices are explored for photonic integration. Through the development of better growth techniques, monolithic integration, laser design and prototypes, it was possible to probe Ge light emitters with emphasis on lasers. Preliminary worked shows thermal photonic behavior capable of enhancing lamination at high temperatures. Increase luminescence is observed up to 120°C from L-band contribution. Higher temperatures show contribution from Δ -band. The increase carrier thermal contribution suggests high temperature applications for Ge light emitters. A Ge electrically pumped laser was probed under 0.2% biaxial strain and doping concentration ~4.5×1019cm-3 n-type. Ge pnn lasers exhibit a gain >1000cm-1 with 8mW power output, presenting a spectrum range of over 200nm, making Ge the ideal candidate for Si photonics. Large temperatures fluctuations and process limit the present device. Theoretically a gain of >4000cm- gain is possible with a threshold of as low as 1kA/cm2. Improvements in Ge work

  15. Eight-wavelength distributed-Bragg-reflector (DBR) laser array transmitter for WDM applications

    Science.gov (United States)

    Fallahi, Mahmoud; McGreer, K. A.; Delage, Andre; Neophytou, A.; Templeton, Ian M.; Champion, Garth; Chatenoud, F.; Barber, Richard A.; Wang, Weijian; He, Jian Jun; Koteles, Emil S.

    1995-03-01

    We report on the design, growth, fabrication and characterization of monolithic wavelength division multiplexed (WDM) laser array transmitter and receiver chips produced by the Canadian Solid State Optoelectronics Consortium. The transmitter chip includes multiple, discrete wavelength, distributed Bragg reflector (DBR) laser diodes monolithically integrated with waveguide combiners fabricated using an InGaAs/GaAs heterostructure. The corresponding wavelength demultiplexer unit is based on a Rowland circle grating spectrometer monolithically integrated with a metal-semiconductor-metal (MSM) detector array fabricated on an InGaAs/AlGaAs/GaAs heterostructure. The epitaxial layer wafers for both transmitter and receiver modules were grown in single molecular beam epitaxy (MBE) runs.

  16. Photonic heterostructure High Contrast Grating as a novel polarization control and light confinement system in HCG VCSEL

    Science.gov (United States)

    Gebski, M.; Dems, M.; Chen, J.; Qijie, W.; Dao Hua, Z.; Czyszanowski, T.

    2014-05-01

    In this paper we present results of computer optical simulations of VCSEL with modified high refractive index contrast grating (HCG) as a top mirror. We consider the HCG of two different designs which determine the lateral aperture. Such HCG mirror provides selective guiding effect. We show that proper design of aperture of HCG results in almost sixfold increase in cavity Q-factor for zero order mode and a discrimination of higher order modes.

  17. A High Resolution Monolithic Crystal, DOI, MR Compatible, PET Detector

    Energy Technology Data Exchange (ETDEWEB)

    Robert S Miyaoka

    2012-03-06

    The principle objective of this proposal is to develop a positron emission tomography (PET) detector with depth-of-interaction (DOI) positioning capability that will achieve state of the art spatial resolution and sensitivity performance for small animal PET imaging. When arranged in a ring or box detector geometry, the proposed detector module will support <1 mm3 image resolution and >15% absolute detection efficiency. The detector will also be compatible with operation in a MR scanner to support simultaneous multi-modality imaging. The detector design will utilize a thick, monolithic crystal scintillator readout by a two-dimensional array of silicon photomultiplier (SiPM) devices using a novel sensor on the entrance surface (SES) design. Our hypothesis is that our single-ended readout SES design will provide an effective DOI positioning performance equivalent to more expensive dual-ended readout techniques and at a significantly lower cost. Our monolithic crystal design will also lead to a significantly lower cost system. It is our goal to design a detector with state of the art performance but at a price point that is affordable so the technology can be disseminated to many laboratories. A second hypothesis is that using SiPM arrays, the detector will be able to operate in a MR scanner without any degradation in performance to support simultaneous PET/MR imaging. Having a co-registered MR image will assist in radiotracer localization and may also be used for partial volume corrections to improve radiotracer uptake quantitation. The far reaching goal of this research is to develop technology for medical research that will lead to improvements in human health care.

  18. Preparation, characterization and application of organic-inorganic hybrid caffeine imprinted monolith.

    Science.gov (United States)

    Liu, Xiaofang; Sun, Na; Zhu, Quanfei; Wu, Mei; Ye, Yong; Chen, Huaixia

    2013-08-23

    The present work aims to synthesize an organic-inorganic hybrid caffeine imprinted monolith using one-step method. The synthesis conditions such as the type of inorganic precursor and porogenic solvent, the molar ratios of the monomer and cross-linker, the volume ratio of the inorganic alcoholysate and organic part were optimized. The morphology of the monolith was studied by scanning electron microscopy and Fourier transform infrared spectra. The imprinted factor of the monolith for caffeine reached 3.02. A simple, rapid and sensitive method for the determination of caffeine in children's milk using the organic-inorganic hybrid caffeine imprinted polymer monolith microextraction combined with high-performance liquid chromatography-photodiodes array detector was developed. Several parameters affecting the sample pretreatment were investigated, including the type, flow rate and volume of eluent, the flow rate and volume of sample solution. The assay exhibited a linear dynamic range of 8-500μgL(-1) with the correlation coefficient above 0.9987. Lower limits of detection (LOD, at S/N=3) and quantification (LOQ, at S/N=10) in children's milk samples were 2.7 and 8μgL(-1). Recoveries of caffeine from spiked children's milk ranged from 85 to 104% with relative standard deviations of less than 8.9%.

  19. Radiation hardness and lifetime studies of LEDs and VCSELs for the optical readout of the ATLAS SCT

    CERN Document Server

    Beringer, J; Mommsen, R K; Nickerson, R B; Weidberg, A R; Monnier, E; Hou, H Q; Lear, K L

    1999-01-01

    We study the radiation hardness and the lifetime of Light Emitting Diodes (LEDs) and Vertical Cavity Surface Emitting Laser diodes (VCSELs) in the context of the development of the optical readout for the ATLAS SemiConductor Tracker (SCT) at LHC. About 170 LEDs from two different manufacturers and about 130 VCSELs were irradiated with neutron and proton fluences equivalent to (and in some cases more than twice as high as) the combined neutral and charged particle fluence of about 5x10 sup 1 sup 4 n (1 MeV eq. in GaAs)/cm sup 2 expected in the ATLAS inner detector. We report on the radiation damage and the conditions required for its partial annealing under forward bias, we calculate radiation damage constants, and we present post-irradiation failure rates for LEDs and VCSELs. The lifetime after irradiation was investigated by operating the diodes at an elevated temperature of 50 degree sign C for several months, resulting in operating times corresponding to up to 70 years of operation in the ATLAS SCT. From o...

  20. Synthesis of monolithic graphene – graphite integrated electronics

    Science.gov (United States)

    Park, Jang-Ung; Nam, SungWoo; Lee, Mi-Sun; Lieber, Charles M.

    2013-01-01

    Encoding electronic functionality into nanoscale elements during chemical synthesis has been extensively explored over the past decade as the key to developing integrated nanosystems1 with functions defined by synthesis2-6. Graphene7-12 has been recently explored as a two-dimensional nanoscale material, and has demonstrated simple device functions based on conventional top-down fabrication13-20. However, the synthetic approach to encoding electronic functionality and thus enabling an entire integrated graphene electronics in a chemical synthesis had not previously been demonstrated. Here we report an unconventional approach for the synthesis of monolithically-integrated electronic devices based on graphene and graphite. Spatial patterning of heterogeneous catalyst metals permits the selective growth of graphene and graphite, with controlled number of graphene layers. Graphene transistor arrays with graphitic electrodes and interconnects were formed from synthesis. These functional, all-carbon structures were transferrable onto a variety of substrates. The integrated transistor arrays were used to demonstrate real-time, multiplexed chemical sensing, and more significantly, multiple carbon layers of the graphene-graphite device components were vertically assembled to form a three-dimensional flexible structure which served as a top-gate transistor array. These results represent a substantial progress towards encoding electronic functionality via chemical synthesis and suggest future promise for one-step integration of graphene-graphite based electronics. PMID:22101813

  1. Synthesis of monolithic graphene-graphite integrated electronics.

    Science.gov (United States)

    Park, Jang-Ung; Nam, SungWoo; Lee, Mi-Sun; Lieber, Charles M

    2011-11-20

    Encoding electronic functionality into nanoscale elements during chemical synthesis has been extensively explored over the past decade as the key to developing integrated nanosystems with functions defined by synthesis. Graphene has been recently explored as a two-dimensional nanoscale material, and has demonstrated simple device functions based on conventional top-down fabrication. However, the synthetic approach to encoding electronic functionality and thus enabling an entire integrated graphene electronics in a chemical synthesis had not previously been demonstrated. Here we report an unconventional approach for the synthesis of monolithically integrated electronic devices based on graphene and graphite. Spatial patterning of heterogeneous metal catalysts permits the selective growth of graphene and graphite, with a controlled number of graphene layers. Graphene transistor arrays with graphitic electrodes and interconnects were formed from the synthesis. These functional, all-carbon structures were transferable onto a variety of substrates. The integrated transistor arrays were used to demonstrate real-time, multiplexed chemical sensing and more significantly, multiple carbon layers of the graphene-graphite device components were vertically assembled to form a three-dimensional flexible structure which served as a top-gate transistor array. These results represent substantial progress towards encoding electronic functionality through chemical synthesis and suggest the future promise of one-step integration of graphene-graphite based electronics.

  2. 3D photon impact determination in monolithic crystals based on autocorrelation filters and RTP methods

    Energy Technology Data Exchange (ETDEWEB)

    Conde, Pablo; Gonzalez, Antonio [Institute for Instrumentation in Molecular Imaging, I3M-CSIC, Valencia (Spain); Bettiol, Marco; Fabbri, Andrea; Pani, Roberto [Department of Molecular Medicine, Sapienza University of Rome (Italy); Benlloch Baviera, José María; Talens Aguilar, Albert; Hernandez, Liczandro; Sanchez, Filomeno [Institute for Instrumentation in Molecular Imaging, I3M-CSIC, Valencia (Spain)

    2015-05-18

    In PET detectors based on monolithic scintillators, the photon impact position can be estimated from the light intensity distribution (LD) on the photodetector pixels. Typically, there is a poor estimation of the interaction positions towards the edges when linear algorithms such as Center of Gravity (CoG) are used. We present a novel method to determine the interaction coordinates in thick monolithic crystals filtering the digitized LDs from each gamma-event by means of an autocorrelation filter and the raise to power (RTP) positioning algorithm to reduce the border effects. The experimental setup was based on two detector blocks based on monolithic LYSO scintillator crystals (50x50x20 mm{sup 3}). Each crystal is coupled to a SiPMs array as 12x12 photosensors and an electronic readout that outputs information of each SiPM row and column. Between the detector blocks, a collimated array of 9x9 {sup 22}Na sources, separated 5 mm each other, was placed. The optimum power to use in the RTP positioning algorithm was determined using the third order intercept point (IP3) from plots of the measured coordinates versus known positions. After applying the autocorrelation and RTP fifth to the data, we found an improvement of the spatial resolution from 2.5 mm when CoG is used, to 1.2 mm in the crystal center region. In this work we show how to accurately resolve 3D photon impact coordinates in thick monolithic crystals using autocorrelation filters merged with RTP methods. After applying the new approach it is possible to accurately resolve impacts close to the entrance of 20 mm thick LYSO scintillators. The reached spatial resolution at any photon depth of interaction is comparable with state-of-the-art crystal array approaches with the advantage of the proposed work to also provide continuous depth of interaction information.

  3. Modified monolithic silica capillary for preconcentration of catecholamines

    Institute of Scientific and Technical Information of China (English)

    Wei Chang; Tusyo-shi Komazu

    2009-01-01

    Preconcentration of catecholamines by the modified monolithic silica in the capillary was investigated in this study. In order to achieve a microchip-based method for determining catecholamines in the saliva, the monolithic silica was fabricated in the capillary and the monolithic silica was chemically modified by on-column reaction with phenylboronate. Different modified methods were compared. The concentration conditions were optimized. This study indicates the applicability of the modified monolithic silica capillary when it was used to concentrate catecholamines.

  4. Modified monolithic silica capillary for preconcentration of catecholamines

    Institute of Scientific and Technical Information of China (English)

    2009-01-01

    Preconcentration of catecholamines by the modified monolithic silica in the capillary was investigated in this study. In order to achieve a microchip-based method for determining catecholamines in the saliva,the monolithic silica was fabricated in the capillary and the monolithic silica was chemically modified by on-column reaction with phenylboronate. Different modified methods were compared. The concentration conditions were optimized. This study indicates the applicability of the modified monolithic sili...

  5. Fracture resistance of monolithic zirconia molar crowns with reduced thickness

    OpenAIRE

    Nakamura, Keisuke; Harada, A.; Inagaki, R.; Kanno, Taro; Niwano, Y; Milleding, Percy; Ørtengren, Ulf Thore

    2015-01-01

    This is the accepted manuscript version. Published version is available at Acta Odontologica Scandinavica Objectives. The purpose of the present study was to analyze the relationship between fracture load of monolithic zirconia crowns and axial/occlusal thickness, and to evaluate the fracture resistance of monolithic zirconia crowns with reduced thickness in comparison with that of monolithic lithium disilicate crowns with regular thickness. Materials and methods. Monolithic zi...

  6. Effect of Distributor Design on Gas-Liquid Distribution in Monolithic Bed at High Gas/Liquid Ratios

    Institute of Scientific and Technical Information of China (English)

    周媛; AL-DAHHAN Muthanna; DUDUKOVIC Milorad; 刘辉

    2012-01-01

    Experiments were carried out to investigate the liquid flow distribution at high gas/liquid ratios in a cold model monolith bed of a 0.048 m diameter with 62 cells per cm2.Three types of distributor for the liquid distribu-tion were used to evaluate their distribution performance.Local liquid saturation in individual channels was meas-ured using 16 single-point optical fiber probes mounted inside the channels.The results indicate that 1) The optical fiber probe technique can measure phase distribution in the monolith bed;2) Liquid saturation distribution along the radial direction of the monolith bed is not uniform and the extent of non-uniformity depends on the distributor de-sign and phase velocities;and 3) The tube array distributor provides superior liquid distribution performance over the showerhead and nozzle distributors.

  7. Carbon Fiber Composite Monoliths as Catalyst Supports

    Energy Technology Data Exchange (ETDEWEB)

    Contescu, Cristian I [ORNL; Gallego, Nidia C [ORNL; Pickel, Joseph M [ORNL; Blom, Douglas Allen [ORNL; Burchell, Timothy D [ORNL

    2006-01-01

    Carbon fiber composite monoliths are rigid bodies that can be activated to a large surface area, have tunable porosity, and proven performance in gas separation and storage. They are ideal as catalyst supports in applications where a rigid support, with open structure and easy fluid access is desired. We developed a procedure for depositing a dispersed nanoparticulate phase of molybdenum carbide (Mo2C) on carbon composite monoliths in the concentration range of 3 to 15 wt% Mo. The composition and morphology of this phase was characterized using X-ray diffraction and electron microscopy, and a mechanism was suggested for its formation. Molybdenum carbide is known for its catalytic properties that resemble those of platinum group metals, but at a lower cost. The materials obtained are expected to demonstrate catalytic activity in a series of hydrocarbon reactions involving hydrogen transfer. This project demonstrates the potential of carbon fiber composite monoliths as catalyst supports.

  8. Carbon Fiber Composite Monoliths for Catalyst Supports

    Energy Technology Data Exchange (ETDEWEB)

    Contescu, Cristian I [ORNL; Gallego, Nidia C [ORNL; Pickel, Joseph M [ORNL; Blom, Douglas Allen [ORNL; Burchell, Timothy D [ORNL

    2006-01-01

    Carbon fiber composite monoliths are rigid bodies that can be activated to a large surface area, have tunable porosity, and proven performance in gas separation and storage. They are ideal as catalyst supports in applications where a rigid support, with open structure and easy fluid access is desired. We developed a procedure for depositing a dispersed nanoparticulate phase of molybdenum carbide (Mo2C) on carbon composite monoliths in the concentration range of 3 to 15 wt% Mo. The composition and morphology of this phase was characterized using X-ray diffraction and electron microscopy, and a mechanism was suggested for its formation. Molybdenum carbide is known for its catalytic properties that resemble those of platinum group metals, but at a lower cost. The materials obtained are expected to demonstrate catalytic activity in a series of hydrocarbon reactions involving hydrogen transfer. This project demonstrates the potential of carbon fiber composite monoliths as catalyst supports.

  9. Eigenpolarization theory of monolithic nonplanar ring oscillators

    Science.gov (United States)

    Nilsson, Alan C.; Gustafson, Eric K.; Byer, Robert L.

    1989-01-01

    Diode-laser-pumped monolithic nonplanar ring oscillators (NPROs) in an applied magnetic field can operate as unidirectional traveling-wave lasers. The diode laser pumping, monolithic construction, and unidirectional oscillation lead to narrow linewidth radiation. Here, a comprehensive theory of the eigenpolarizations of a monolithic NPRO is presented. It is shown how the properties of the integral optical diode that forces unidirectional operation depend on the choice of the gain medium, the applied magnetic field, the output coupler, and the geometry of the nonplanar ring light path. Using optical equivalence theorems to gain insight into the polarization characteristics of the NPRO, a strategy for designing NPROs with low thresholds and large loss nonreciprocities is given. An analysis of the eigenpolarizations for one such NPRO is presented, alternative optimization approaches are considered, and the prospects for further reducing the linewidths of these lasers are briefly discussed.

  10. Increased thermal conductivity monolithic zeolite structures

    Science.gov (United States)

    Klett, James; Klett, Lynn; Kaufman, Jonathan

    2008-11-25

    A monolith comprises a zeolite, a thermally conductive carbon, and a binder. The zeolite is included in the form of beads, pellets, powders and mixtures thereof. The thermally conductive carbon can be carbon nano-fibers, diamond or graphite which provide thermal conductivities in excess of about 100 W/mK to more than 1,000 W/mK. A method of preparing a zeolite monolith includes the steps of mixing a zeolite dispersion in an aqueous colloidal silica binder with a dispersion of carbon nano-fibers in water followed by dehydration and curing of the binder is given.

  11. Characterization of CIM monoliths as enzyme reactors.

    Science.gov (United States)

    Vodopivec, Martina; Podgornik, Ales; Berovic, Marin; Strancar, Ales

    2003-09-25

    The immobilization of the enzymes citrate lyase, malate dehydrogenase, isocitrate dehydrogenase and lactate dehydrogenase to CIM monolithic supports was performed. The long-term stability, reproducibility, and linear response range of the immobilized enzyme reactors were investigated along with the determination of the kinetic behavior of the enzymes immobilized on the CIM monoliths. The Michaelis-Menten constant K(m) and the turnover number k(3) of the immobilized enzymes were found to be flow-unaffected. Furthermore, the K(m) values of the soluble and immobilized enzyme were found to be comparable. Both facts indicate the absence of a diffusional limitation in immobilized CIM enzyme reactors.

  12. Monolithically integrated optoelectronic down-converter (MIOD)

    Science.gov (United States)

    Portnoi, Efrim L.; Venus, G. B.; Khazan, A. A.; Gorfinkel, Vera B.; Kompa, Guenter; Avrutin, Evgenii A.; Thayne, Iain G.; Barrow, David A.; Marsh, John H.

    1995-06-01

    Optoelectronic down-conversion of very high-frequency amplitude-modulated signals using a semiconductor laser simultaneously as a local oscillator and a mixer is proposed. Three possible constructions of a monolithically integrated down-converter are considered theoretically: a four-terminal semiconductor laser with dual pumping current/modal gain control, and both a passively mode-locked and a passively Q-switched semiconductor laser monolithically integrated with an electroabsorption or pumping current modulator. Experimental verification of the feasibility of the concept of down conversion in a laser diode is presented.

  13. Monolithic Silicon Photodetector - Detector of Ionizing Radiation Based on Functional Integrated MOS Structures

    Directory of Open Access Journals (Sweden)

    S.A. Legotin

    2014-07-01

    Full Text Available This paper describes the principle of operation, construction, architecture and fabrication of a new type of monolithic silicon coordinate photodetector - detector of optical and ionizing radiation (MSCP on the basis of functional integrated MOS structures. The analytical estimation of electrophysical characteristics MSCP is given. It is shown that MSCP is a specialized monolithic silicon VLSI containing two-dimensional pixel array with high and low voltage functionally integrated structures (FIS and peripheral electronic circuits of amplification and signal processing matrix. Estimations and presents comparative characteristics are presented. They show potential MSCP possibilities for registration of optical and ionizing radiation. Experimental results of α-particles and electrons registration. The possible areas of application, with the possibility of its use in a wide X-ray panels medical supplies, X-rays, etc are considered.

  14. A novel monolithic ultraviolet image sensor based on a standard CMOS process

    Institute of Scientific and Technical Information of China (English)

    Li Guike; Feng Peng; Wu Nanjian

    2011-01-01

    We present a monolithic ultraviolet (UV) image sensor based on a standard CMOS process.A compact UV sensitive device structure is designed as a pixel for the image sensor.This UV image sensor consists ofa CMOS pixel array,high-voltage switches,a readout circuit and a digital control circuit.A 16 × 16 image sensor prototype chip is implemented in a 0.18 μm standard CMOS logic process.The pixel and image sensor were measured.Experimental results demonstrate that the image sensor has a high sensitivity of 0.072 V/(mJ/cm2) and can capture a UV image.It is suitable for large-scale monolithic bio-medical and space applications.

  15. MONOLITHIC ACTIVE PIXEL MATRIX WITH BINARY COUNTERS IN AN SOI PROCESS.

    Energy Technology Data Exchange (ETDEWEB)

    DUPTUCH,G.; YAREMA, R.

    2007-06-07

    The design of a Prototype monolithic active pixel matrix, designed in a 0.15 {micro}m CMOS SOI Process, is presented. The process allowed connection between the electronics and the silicon volume under the layer of buried oxide (BOX). The small size vias traversing through the BOX and implantation of small p-type islands in the n-type bulk result in a monolithic imager. During the acquisition time, all pixels register individual radiation events incrementing the counters. The counting rate is up to 1 MHz per pixel. The contents of counters are shifted out during the readout phase. The designed prototype is an array of 64 x 64 pixels and the pixel size is 26 x 26 {micro}m{sup 2}.

  16. Multianalyte electrochemical biosensor on a monolith electrode by optically scanning the electrical double layer.

    Science.gov (United States)

    Lee, Seung-Woo; Saraf, Ravi F

    2014-07-15

    Redox on an electrode is an interfacial phenomenon that modulates the charge in the electrical double layer (EDL). A novel instrument, the Scanning Electrometer for Electrical Double-layer (SEED) has been developed to measure multiple enzyme reactions on a monolith electrode due to immunospecific binding with a mixture of respective analytes. SEED quantitatively maps the local redox reaction by scanning a laser on the array of enzyme monolayer spots immobilized on the monolith electrode. SEED measures the change in local charge state of the EDL that abruptly changes due to the redox reaction. The measurement spot size defined by the size of the laser beam is ~10 µm. The SEED signal is linearly proportional to the local redox current density and analyte concentration. The specificity is close to 100%. The SEED readout is compatible with microfluidics platform where the signal degrades less than 2% due to the poly(dimethyl siloxane) (PDMS) body.

  17. VCSEL based Faraday rotation spectroscopy at 762nm for battery powered trace molecular oxygen detection

    Science.gov (United States)

    So, Stephen; Wysocki, Gerard

    2010-02-01

    Faraday Rotation Spectroscopy (FRS) is a polarization based spectroscopic technique which can provide higher sensitivity concentration measurements of paramagnetic gases and free radicals than direct absorption spectroscopic techniques. We have developed sensor systems which require only 0.2W to perform TDLAS (tunable diode laser absorption spectroscopy), and can additionally be quickly duty cycled, enabling operation in wireless sensor networks of laser-based trace gas sensors We adapted our integrated TDLAS electronics to perform FRS in a compact and more sensitive system for quantification of molecular oxygen (O2) using a 762.3nm VCSEL in the A band. Using an AC magnetic field, we demonstrate detector noise dominated performance, achieving 2.1×10-6/Hz1/2 equivalent detectable fractional absorption and a minimum detection limit of 462 ppmv O2 in 1 second in a 15cm path. At longer paths and integration times, such a sensor will enable oxygen measurements at biotic respiration levels (CO2 - O2 exchange for mapping natural exchange of greenhouse gases. Potential improvement of detection limits by increasing various system performance parameters is described.

  18. Volumetric cutaneous microangiography of human skin in vivo by VCSEL swept-source optical coherence tomography

    Energy Technology Data Exchange (ETDEWEB)

    Woo June Choi; Wang, R K [University of Washington, Department of Bioengineering, Seattle, Washington 98195 (United States)

    2014-08-31

    We demonstrate volumetric cutaneous microangiography of the human skin in vivo that utilises 1.3-μm high-speed sweptsource optical coherence tomography (SS-OCT). The swept source is based on a micro-electro-mechanical (MEMS)-tunable vertical cavity surface emission laser (VCSEL) that is advantageous in terms of long coherence length over 50 mm and 100 nm spectral bandwidth, which enables the visualisation of microstructures within a few mm from the skin surface. We show that the skin microvasculature can be delineated in 3D SS-OCT images using ultrahigh-sensitive optical microangiography (UHS-OMAG) with a correlation mapping mask, providing a contrast enhanced blood perfusion map with capillary flow sensitivity. 3D microangiograms of a healthy human finger are shown with distinct cutaneous vessel architectures from different dermal layers and even within hypodermis. These findings suggest that the OCT microangiography could be a beneficial biomedical assay to assess cutaneous vascular functions in clinic. (laser biophotonics)

  19. VCSEL-powered and polarization-maintaining fiber-optic grating vector rotation sensor.

    Science.gov (United States)

    Guo, Tuan; Liu, Fu; Du, Fa; Zhang, Zhaochuan; Li, Chunjie; Guan, Bai-Ou; Albert, Jacques

    2013-08-12

    A compact fiber-optic vector rotation sensor in which a short section of polarization-maintaining (PM) fiber stub containing a straight fiber Bragg grating (FBG) is spliced to another single mode fiber without any lateral offset is proposed and experimentally demonstrated. Due to the intrinsic birefringence of the PM fiber, two well-defined resonances (i.e. orthogonally polarized FBG core modes) with wavelength separation of 0.5 nm have been achieved in reflection, and they exhibit a high sensitivity to fiber rotation. Both the orientation and the angle of rotation can be determined unambiguously via simple power detection of the relative amplitudes of the orthogonal core reflections. Meanwhile, instead of using a broadband source (BBS), the sensor is powered by a commercial vertical cavity surface emitting laser (VCSEL) with the laser wavelength matched to the PM-FBG core modes, which enables the sensor to work at much higher power levels (~15 dB better than BBS). This improves the signal-to-noise ratio considerably (~50 dB), and makes a demodulation filter unnecessary. Vector rotation measurement with a sensitivity of 0.09 dB/deg has been achieved via cost-effective single detector real time power measurement, and the unwanted power fluctuations and temperature perturbations can be effectively referenced out.

  20. Ultrahigh speed endoscopic swept source optical coherence tomography using a VCSEL light source and micromotor catheter

    Science.gov (United States)

    Tsai, Tsung-Han; Ahsen, Osman O.; Lee, Hsiang-Chieh; Liang, Kaicheng; Giacomelli, Michael G.; Potsaid, Benjamin M.; Tao, Yuankai K.; Jayaraman, Vijaysekhar; Kraus, Martin F.; Hornegger, Joachim; Figueiredo, Marisa; Huang, Qin; Mashimo, Hiroshi; Cable, Alex E.; Fujimoto, James G.

    2014-03-01

    We developed an ultrahigh speed endoscopic swept source optical coherence tomography (OCT) system for clinical gastroenterology using a vertical-cavity surface-emitting laser (VCSEL) and micromotor based imaging catheter, which provided an imaging speed of 600 kHz axial scan rate and 8 μm axial resolution in tissue. The micromotor catheter was 3.2 mm in diameter and could be introduced through the 3.7 mm accessory port of an endoscope. Imaging was performed at 400 frames per second with an 8 μm spot size using a pullback to generate volumetric data over 16 mm with a pixel spacing of 5 μm in the longitudinal direction. Three-dimensional OCT (3D-OCT) imaging was performed in patients with a cross section of pathologies undergoing standard upper and lower endoscopy at the Veterans Affairs Boston Healthcare System (VABHS). Patients with Barrett's esophagus, dysplasia, and inflammatory bowel disease were imaged. The use of distally actuated imaging catheters allowed OCT imaging with more flexibility such as volumetric imaging in the terminal ileum and the assessment of the hiatal hernia using retroflex imaging. The high rotational stability of the micromotor enabled 3D volumetric imaging with micron scale volumetric accuracy for both en face and cross-sectional imaging. The ability to perform 3D OCT imaging in the GI tract with microscopic accuracy should enable a wide range of studies to investigate the ability of OCT to detect pathology as well as assess treatment response.

  1. Experimental investigation on nonlinear dynamics of 1550 nm VCSEL simultaneously subject to orthogonal optical injection and negative optoelectronic feedback

    Science.gov (United States)

    Deng, Tao; Xia, Guang-Qiong; Chen, Jian-Jun; Tang, Xi; Lin, Xiao-Dong; Yang, Xin; Huang, Shou-Wen; Wu, Zheng-Mao

    2017-04-01

    Nonlinear dynamic characteristics of a 1550 nm vertical-cavity surface-emitting laser (1550 nm VCSEL) simultaneously subject to orthogonal optical injection and negative optoelectronic feedback are experimentally investigated. The results show that, under suitable orthogonal optical injection the VCSEL can exhibit rich nonlinear dynamic behaviors such as stable state (S), period-one (P1), period-two (P2), chaos (CO), stable injection locking (SIL) and polarization switching (PS). After further introducing negative optoelectronic feedback with a certain feedback delay time, the dynamic distribution of the orthogonal optical injection 1550 nm VCSEL is significantly affected, and some new phenomena including three-frequency quasiperiodic (Q3) state can be observed. With the increase of optoelectronic feedback strength, the S and SIL regions typically are shrank, while the quasiperiodic (QP) and CO regions are enlarged.

  2. Monolithic resonant optical reflector laser diodes

    Science.gov (United States)

    Hirata, T.; Suehiro, M.; Maeda, M.; Hihara, M.; Hosomatsu, H.

    1991-10-01

    The first monolithic resonant optical reflector laser diode that has a waveguide directional coupler and two DBR reflectors integrated by compositional disordering of quantum-well heterostructures is described. A linewidth of 440 kHz was obtained, and this value is expected to be greatly decreased by reducing the propagation loss in the integrated waveguide.

  3. Constant capacitance in nanopores of carbon monoliths.

    Science.gov (United States)

    García-Gómez, Alejandra; Moreno-Fernández, Gelines; Lobato, Belén; Centeno, Teresa A

    2015-06-28

    The results obtained for binder-free electrodes made of carbon monoliths with narrow micropore size distributions confirm that the specific capacitance in the electrolyte (C2H5)4NBF4/acetonitrile does not depend significantly on the micropore size and support the foregoing constant result of 0.094 ± 0.011 F m(-2).

  4. Pilot tests of a PET detector using the TOF-PET ASIC based on monolithic crystals and SiPMs

    Science.gov (United States)

    Aguilar, A.; González-Montoro, A.; González, A. J.; Hernández, L.; Monzó, J. M.; Bugalho, R.; Ferramacho, L.; Benlloch, J. M.

    2016-12-01

    In this work we show pilot tests of PET detector blocks using the TOF-PET ASIC, coupled to SiPM detector arrays and different crystal configurations. We have characterized the main ASIC features running calibration processes to compensate the time dispersion among the different ASIC/SiPM paths as well as for the time walk on the arrival of optical photons. The aim of this work is to use of LYSO monolithic crystals and explore their photon Depth of Interaction (DOI) capabilities, keeping good energy and spatial resolutions. First tests have been carried out with crystal arrays. Here we made it possible to reach a coincidence resolving times (CRT) of 370 ps FWHM, with energy resolutions better than 20% and resolving well 2 mm sized crystal elements. When using monolithic crystals, a single-pixel LYSO reference crystal helped to explore the CRT performance. We studied different strategies to provide the best timestamp determination in the monolithic scintillator. Times around 1 ns FWHM have been achieved in these pilot studies. In terms of spatial and energy resolution, values of about 3 mm and better than 30% were found, respectively. We have also demonstrated the capability of this system (monolithic and ASIC) to return accurate DOI information.

  5. Performance comparison of 850-nm and 1550-nm VCSELs exploiting OOK, OFDM, and 4-PAM over SMF/MMF links for low-cost optical interconnects

    DEFF Research Database (Denmark)

    Karinou, Fotini; Deng, Lei; Rodes Lopez, Roberto

    2013-01-01

    modulation (4-PAM), for the 1550-nm transmitter over SMF and MMF links and we compare it to the data-rate equivalent NRZ-OOK. The extensive performance comparison under various transmission scenarios shows the superiority of 1550-nm single-mode VCSEL compared to its multi-mode 850-nm counterpart. Moreover......, OFDM/DD and 4-PAM in conjunction with low-cost, inexpensive VCSELs as transmitters prove to be an enabling technology for next-generation WDM, point-to-point, short-reach, SMF/MMF optical interconnects and potential candidates to substitute NRZ-OOK. Nevertheless, the sensitivity requirements are higher...

  6. IM/DD vs. 4-PAM Using a 1550-nm VCSEL over Short-Range SMF/MMF Links for Optical Interconnects

    DEFF Research Database (Denmark)

    Karinou, Fotini; Rodes Lopez, Roberto; Prince, Kamau

    2013-01-01

    We experimentally compare the performance of 10.9-Gb/s IM/DD and 5-GBd 4-PAM modulation formats over 5-km SMF and 1-km MMF links, employing a commercially-available 1550-nm VCSEL as an enabling technology for use in optical interconnects.......We experimentally compare the performance of 10.9-Gb/s IM/DD and 5-GBd 4-PAM modulation formats over 5-km SMF and 1-km MMF links, employing a commercially-available 1550-nm VCSEL as an enabling technology for use in optical interconnects....

  7. Quad 14Gbps L-Band VCSEL-based System for WDM Migration of 4-lanes 56 Gbps Optical Data Links

    DEFF Research Database (Denmark)

    Estaran Tolosa, Jose Manuel; Rodes Lopez, Roberto; Pham, Tien Thang;

    2012-01-01

    We report on migrating multiple lane link into a single WDM L-band VCSEL-based system. Experimental validation successfully achieves 10 km of SMF reach with 4x14Gbps and less than 0.5dB inter-channel crosstalk penalty.......We report on migrating multiple lane link into a single WDM L-band VCSEL-based system. Experimental validation successfully achieves 10 km of SMF reach with 4x14Gbps and less than 0.5dB inter-channel crosstalk penalty....

  8. Multicolor photonic crystal laser array

    Science.gov (United States)

    Wright, Jeremy B; Brener, Igal; Subramania, Ganapathi S; Wang, George T; Li, Qiming

    2015-04-28

    A multicolor photonic crystal laser array comprises pixels of monolithically grown gain sections each with a different emission center wavelength. As an example, two-dimensional surface-emitting photonic crystal lasers comprising broad gain-bandwidth III-nitride multiple quantum well axial heterostructures were fabricated using a novel top-down nanowire fabrication method. Single-mode lasing was obtained in the blue-violet spectral region with 60 nm of tuning (or 16% of the nominal center wavelength) that was determined purely by the photonic crystal geometry. This approach can be extended to cover the entire visible spectrum.

  9. Time-delay signatures in multi-transverse mode VCSELs subject to double-cavity polarization-rotated optical feedback

    Science.gov (United States)

    Lin, Hong; Khurram, Aliza; Hong, Yanhua

    2016-10-01

    Time delay (TD) signatures are studied experimentally in orthogonal polarizations and in individual transverse modes respectively in a VCSEL operating with three transverse modes. Different types of concealment of the TD signatures are observed when the polarization of feedback is rotated through large angles. Effects of feedback strength and external cavity length on the TD signatures are investigated. Weak feedback leads to better concealment of the TD signatures in the dominant polarization. When the round-trip time difference between the two external cavities is close to a half of the relaxation oscillation period, the TD signatures are minimized.

  10. Robust Design by Antioptimization for Parameter Tolerant GaAs/AlOx High Contrast Grating Mirror for VCSEL Application

    CERN Document Server

    Chevallier, Christyves; Fressengeas, Nicolas; Jacquet, Joel

    2013-01-01

    A GaAs/AlOx high contrast grating structure design which exhibits a 99.5% high reflectivity for a 425nm large bandwidth is reported. The high contrast grating (HCG) structure has been designed in order to enhance the properties of mid-infrared VCSEL devices by replacing the top Bragg mirror of the cavity. A robust optimization algorithm has been implemented to design the HCG structure not only as an efficient mirror but also as a robust structure against the imperfections of fabrication. The design method presented here can be easily adapted for other HCG applications at different wavelengths.

  11. Performance analysis of communication links based on VCSEL and silicon photonics technology for high-capacity data-intensive scenario.

    Science.gov (United States)

    Boletti, A; Boffi, P; Martelli, P; Ferrario, M; Martinelli, M

    2015-01-26

    To face the increased demand for bandwidth, cost-effectiveness and simplicity of future Ethernet data communications, a comparison between two different solutions based on directly-modulated VCSEL sources and Silicon Photonics technologies is carried out. Also by exploiting 4-PAM modulation, the transmission of 50-Gb/s and beyond capacity per channel is analyzed by means of BER performance. Applications for optical backplane, very short reach and in case of client-optics networks and intra and inter massive data centers communications (up to 10 km) are taken into account. A comparative analysis based on the power consumption is also proposed.

  12. Spatial characterization of monolithic multi-element Silicon-Drift-Detectors for X-ray spectroscopic applications

    CERN Document Server

    Kappen, P; Hansen, K; Reckleben, C; Lechner, P; Strüder, L; Materlik, G

    2001-01-01

    Spatially resolved spectroscopic measurements with a 10 and 20 mu m pencil beam have been performed on a monolithic 7-element Silicon-Drift-Detector (SDD). Detailed studies are shown of the modification of the spectroscopic response at pixel edges and pixel centre. The results give quantitative insight into the local SDD performance. A simple model predicts global properties (e.g. peak-to-background ratio) of larger SDD arrays, like the 61-element detector currently under development.

  13. A monolithic integrated photonic microwave filter

    Science.gov (United States)

    Fandiño, Javier S.; Muñoz, Pascual; Doménech, David; Capmany, José

    2016-12-01

    Meeting the increasing demand for capacity in wireless networks requires the harnessing of higher regions in the radiofrequency spectrum, reducing cell size, as well as more compact, agile and power-efficient base stations that are capable of smoothly interfacing the radio and fibre segments. Fully functional microwave photonic chips are promising candidates in attempts to meet these goals. In recent years, many integrated microwave photonic chips have been reported in different technologies. To the best of our knowledge, none has monolithically integrated all the main active and passive optoelectronic components. Here, we report the first demonstration of a tunable microwave photonics filter that is monolithically integrated into an indium phosphide chip. The reconfigurable radiofrequency photonic filter includes all the necessary elements (for example, lasers, modulators and photodetectors), and its response can be tuned by means of control electric currents. This is an important step in demonstrating the feasibility of integrated and programmable microwave photonic processors.

  14. Macroporous Monolithic Polymers: Preparation and Applications

    Directory of Open Access Journals (Sweden)

    Cecilia Inés Alvarez Igarzabal

    2009-12-01

    Full Text Available In the last years, macroporous monolithic materials have been introduced as a new and useful generation of polymers used in different fields. These polymers may be prepared in a simple way from a homogenous mixture into a mold and contain large interconnected pores or channels allowing for high flow rates at moderate pressures. Due to their porous characteristics, they could be used in different processes, such as stationary phases for different types of chromatography, high-throughput bioreactors and in microfluidic chip applications. This review reports the contributions of several groups working in the preparation of different macroporous monoliths and their modification by immobilization of specific ligands on the products for specific purposes.

  15. Monolithic pixel detectors for high energy physics

    CERN Document Server

    Snoeys, W

    2013-01-01

    Monolithic pixel detectors integrating sensor matrix and readout in one piece of silicon have revolutionized imaging for consumer applications, but despite years of research they have not yet been widely adopted for high energy physics. Two major requirements for this application, radiation tolerance and low power consumption, require charge collection by drift for the most extreme radiation levels and an optimization of the collected signal charge over input capacitance ratio ( Q / C ). It is shown that monolithic detectors can achieve Q / C for low analog power consumption and even carryout the promise to practically eliminate analog power consumption, but combining suf fi cient Q / C , collection by drift, and integration of readout circuitry within the pixel remains a challenge. An overview is given of different approaches to address this challenge, with possible advantages and disadvantages.

  16. Update On Monolithic Fuel Fabrication Development

    Energy Technology Data Exchange (ETDEWEB)

    C. R Clark; J. M. Wight; G. C. Knighton; G. A. Moore; J. F. Jue

    2005-11-01

    Efforts to develop a viable monolithic research reactor fuel plate have continued at Idaho National Laboratory. These efforts have concentrated on both fabrication process refinement and scale-up to produce full sized fuel plates. Advancements have been made in the production of U-Mo foil including full sized foils. Progress has also been made in the friction stir welding and transient liquid phase bonding fabrication processes resulting in better bonding, more stable processes and the ability to fabricate larger fuel plates.

  17. FLUIDIZED BED STEAM REFORMER MONOLITH FORMATION

    Energy Technology Data Exchange (ETDEWEB)

    Jantzen, C

    2006-12-22

    Fluidized Bed Steam Reforming (FBSR) is being considered as an alternative technology for the immobilization of a wide variety of aqueous high sodium containing radioactive wastes at various DOE facilities in the United States. The addition of clay, charcoal, and a catalyst as co-reactants converts aqueous Low Activity Wastes (LAW) to a granular or ''mineralized'' waste form while converting organic components to CO{sub 2} and steam, and nitrate/nitrite components, if any, to N{sub 2}. The waste form produced is a multiphase mineral assemblage of Na-Al-Si (NAS) feldspathoid minerals with cage-like structures that atomically bond radionuclides like Tc-99 and anions such as SO{sub 4}, I, F, and Cl. The granular product has been shown to be as durable as LAW glass. Shallow land burial requires that the mineralized waste form be able to sustain the weight of soil overburden and potential intrusion by future generations. The strength requirement necessitates binding the granular product into a monolith. FBSR mineral products were formulated into a variety of monoliths including various cements, Ceramicrete, and hydroceramics. All but one of the nine monoliths tested met the <2g/m{sup 2} durability specification for Na and Re (simulant for Tc-99) when tested using the Product Consistency Test (PCT; ASTM C1285). Of the nine monoliths tested the cements produced with 80-87 wt% FBSR product, the Ceramicrete, and the hydroceramic produced with 83.3 wt% FBSR product, met the compressive strength and durability requirements for an LAW waste form.

  18. Monolithically integrated interferometer for optical displacement measurement

    Science.gov (United States)

    Hofstetter, Daniel; Zappe, Hans P.

    1996-01-01

    We discuss the fabrication of a monolithically integrated optical displacement sensors using III-V semiconductor technology. The device is configured as a Michelson interferometer and consists of a distributed Bragg reflector laser, a photodetector and waveguides forming a directional coupler. Using this interferometer, displacements in the 100 nm range could be measured at distances of up to 45 cm. We present fabrication, device results and characterization of the completed interferometer, problems, limitations and future applications will also be discussed.

  19. Monolithic circuits for barium fluoride detectors used in nuclear physics experiments. CRADA final report

    Energy Technology Data Exchange (ETDEWEB)

    Varner, R.L.; Blankenship, J.L.; Beene, J.R. [Oak Ridge National Lab., TN (United States); Todd, R.A. [RIS Corp., Oak Ridge, TN (United States)

    1998-02-01

    Custom monolithic electronic circuits have been developed recently for large detector applications in high energy physics where subsystems require tens of thousands of channels of signal processing and data acquisition. In the design and construction of these enormous detectors, it has been found that monolithic circuits offer significant advantages over discrete implementations through increased performance, flexible packaging, lower power and reduced cost per channel. Much of the integrated circuit design for the high energy physics community is directly applicable to intermediate energy heavy-ion and electron physics. This STTR project conducted in collaboration with researchers at the Holifield Radioactive Ion Beam Facility (HRIBF) at Oak Ridge National Laboratory, sought to develop a new integrated circuit chip set for barium fluoride (BaF{sub 2}) detector arrays based upon existing CMOS monolithic circuit designs created for the high energy physics experiments. The work under the STTR Phase 1 demonstrated through the design, simulation, and testing of several prototype chips the feasibility of using custom CMOS integrated circuits for processing signals from BaF{sub 2} detectors. Function blocks including charge-sensitive amplifiers, comparators, one shots, time-to-amplitude converters, analog memory circuits and buffer amplifiers were implemented during Phase 1 effort. Experimental results from bench testing and laboratory testing with sources were documented.

  20. Magnetism-Enhanced Monolith-Based In-Tube Solid Phase Microextraction.

    Science.gov (United States)

    Mei, Meng; Huang, Xiaojia; Luo, Qing; Yuan, Dongxin

    2016-02-02

    Monolith-based in-tube solid phase microextraction (MB/IT-SPME) has received wide attention because of miniaturization, automation, expected loading capacity, and environmental friendliness. However, the unsatisfactory extraction efficiency becomes the main disadvantage of MB/IT-SPME. To overcome this circumstance, magnetism-enhanced MB/IT-SPME (ME-MB/IT-SPME) was developed in the present work, taking advantage of magnetic microfluidic principles. First, modified Fe3O4 nanoparticles were mixed with polymerization solution and in situ polymerized in the capillary to obtain a magnetic monolith extraction phase. After that, the monolithic capillary column was placed inside a magnetic coil that allowed the exertion of a variable magnetic field. The effects of intensity of magnetic field, adsorption and desorption flow rate, volume of sample, and desorption solvent on the performance of ME-MB/IT-SPME were investigated in detail. The analysis of six steroid hormones in water samples by the combination of ME-MB/IT-SPME with high-performance liquid chromatography with diode array detection was selected as a paradigm for the practical evaluation of ME-MB/IT-SPME. The application of a controlled magnetic field resulted in an obvious increase of extraction efficiencies of the target analytes between 70% and 100%. The present work demonstrated that application of different magnetic forces in adsorption and desorption steps can effectively enhance extraction efficiency of MB/IT-SPME systems.

  1. Monolithic phononic crystals with a surface acoustic band gap from surface phonon-polariton coupling.

    Science.gov (United States)

    Yudistira, D; Boes, A; Djafari-Rouhani, B; Pennec, Y; Yeo, L Y; Mitchell, A; Friend, J R

    2014-11-21

    We theoretically and experimentally demonstrate the existence of complete surface acoustic wave band gaps in surface phonon-polariton phononic crystals, in a completely monolithic structure formed from a two-dimensional honeycomb array of hexagonal shape domain-inverted inclusions in single crystal piezoelectric Z-cut lithium niobate. The band gaps appear at a frequency of about twice the Bragg band gap at the center of the Brillouin zone, formed through phonon-polariton coupling. The structure is mechanically, electromagnetically, and topographically homogeneous, without any physical alteration of the surface, offering an ideal platform for many acoustic wave applications for photonics, phononics, and microfluidics.

  2. An overview of monolithic zirconia in dentistry

    Directory of Open Access Journals (Sweden)

    Özlem Malkondu

    2016-07-01

    Full Text Available Zirconia restorations have been used successfully for years in dentistry owing to their biocompatibility and good mechanical properties. Because of their lack of translucency, zirconia cores are generally veneered with porcelain, which makes restorations weaker due to failure of the adhesion between the two materials. In recent years, all-ceramic zirconia restorations have been introduced in the dental sector with the intent to solve this problem. Besides the elimination of chipping, the reduced occlusal space requirement seems to be a clear advantage of monolithic zirconia restorations. However, scientific evidence is needed to recommend this relatively new application for clinical use. This mini-review discusses the current scientific literature on monolithic zirconia restorations. The results of in vitro studies suggested that monolithic zirconia may be the best choice for posterior fixed partial dentures in the presence of high occlusal loads and minimal occlusal restoration space. The results should be supported with much more in vitro and particularly in vivo studies to obtain a final conclusion.

  3. Temperature-Modulated Array High-Performance Liquid Chromatography

    OpenAIRE

    Premstaller, Andreas; Xiao, Wenzhong; Oberacher, Herbert; O'Keefe, Matthew; Stern, David; Willis, Thomas; Huber, Christian G.; Peter J. Oefner

    2001-01-01

    Using novel monolithic poly(styrene-divinylbenzene) capillary columns with an internal diameter of 0.2 mm, we demonstrate for the first time the feasibility of constructing high-performance liquid chromatography arrays for the detection of mutations by heteroduplex analysis under partially denaturing conditions. In one embodiment, such an array can be used to analyze one sample simultaneously at different temperatures to maximize the detection of mutations in DNA fragments containing multiple...

  4. Controllable all-optical stochastic logic gates and their delay storages based on the cascaded VCSELs with optical-injection

    Science.gov (United States)

    Zhong, Dongzhou; Luo, Wei; Xu, Geliang

    2016-09-01

    Using the dynamical properties of the polarization bistability that depends on the detuning of the injected light, we propose a novel approach to implement reliable all-optical stochastic logic gates in the cascaded vertical cavity surface emitting lasers (VCSELs) with optical-injection. Here, two logic inputs are encoded in the detuning of the injected light from a tunable CW laser. The logic outputs are decoded from the two orthogonal polarization lights emitted from the optically injected VCSELs. For the same logic inputs, under electro-optic modulation, we perform various digital signal processing (NOT, AND, NAND, XOR, XNOR, OR, NOR) in the all-optical domain by controlling the logic operation of the applied electric field. Also we explore their delay storages by using the mechanism of the generalized chaotic synchronization. To quantify the reliabilities of these logic gates, we further demonstrate their success probabilities. Project supported by the National Natural Science Foundation of China (Grant No. 61475120) and the Innovative Projects in Guangdong Colleges and Universities, China (Grant Nos. 2014KTSCX134 and 2015KTSCX146).

  5. Quad 14 Gbps L-band VCSEL-based system for WDM migration of 4-lanes 56 Gbps optical data links

    DEFF Research Database (Denmark)

    Estaran Tolosa, Jose Manuel; Rodes Lopez, Roberto; Pham, Tien Thang;

    2012-01-01

    We report on migrating multiple-lane link into an L-band VCSEL-based WDM system. Experimental validation achieves successful transmission over 10 km of SMF at 4x14Gbps. Inter-channel crosstalk penalty is observed to be less than 0.5 dB and a transmission penalty around 1 dB. The power budget margin...

  6. Laser self-mixing interferometry in VCSELs - an ultra-compact and massproduceable deflection detection system for nanomechanical polymer cantilever sensors

    DEFF Research Database (Denmark)

    Larsson, David; Yvind, Kresten; Hvam, Jørn Märcher;

    2008-01-01

    We have realised an ultra-compact deflection detection system based on laser self-mixing interferometry in a Vertical-Cavity Surface-Emitting Laser (VCSEL). The system can be used together with polymer nanomechanical cantilevers to form chemical sensors capable of detecting less than 1nm deflection....

  7. Comparison of 850-nm and 1550-nm VCSELs for low-cost short-reach IM/DD and OFDM SMF/MMF links

    DEFF Research Database (Denmark)

    Karinou, Fotini; Deng, Lei; Rodes Lopez, Roberto

    2013-01-01

    In this paper, we experimentally compare the suitability of two VCSEL designs of different wavelength and technology as inexpensive, off-the-shelf transmitter components to enable low-cost and energy-efficient optical interconnects employing conventional (NRZ IM/DD) and advanced (OFDM) modulation...

  8. Preparation of imprinted monolithic column under molecular crowding conditions

    Institute of Scientific and Technical Information of China (English)

    Xiao Xia Li; Xin Liu; Li Hong Bai; Hong Quan Duan; Yan Ping Huang; Zhao Sheng Liu

    2011-01-01

    Molecular crowding is a new concept to obtain molecularly imprinted polymers (MIPs) with greater capacity and selectivity. In this work, molecular crowding agent was firstly applied to the preparation of MIPs monolithic column. A new polymerization system based on molecular crowding surrounding was developed to prepare enrofloxacin-imprinted monolith, which was composed of polystyrene and tetrahydrofuran. The result showed that the monolithic MIPs under molecular crowding conditions presented good molecular recognition for enrofloxacin with an imprinting factor of 3.03.

  9. Monolithic Lumped Element Integrated Circuit (M2LEIC) Transistors.

    Science.gov (United States)

    INTEGRATED CIRCUITS, *MONOLITHIC STRUCTURES(ELECTRONICS), *TRANSISTORS, CHIPS(ELECTRONICS), FABRICATION, EPITAXIAL GROWTH, ULTRAHIGH FREQUENCY, POLYSILICONS, PHOTOLITHOGRAPHY, RADIOFREQUENCY POWER, IMPEDANCE MATCHING .

  10. 基于同轴结构的高速VCSEL管座设计方法%An optimized design based on coaxial packaging of the high speed VCSEL

    Institute of Scientific and Technical Information of China (English)

    柴广跃; 刘强; 徐光辉; 段子刚

    2014-01-01

    基于垂直腔面发射激光器( vertical cavity surface emitting laser, VCSEL)的同轴管壳封装等效电路模型,分析影响器件高频性能的封装寄生参量。结合量产要求,通过调节管壳的部分结构参数与介质材料的介电常数,提高器件频率响应。分析结果表明,优化设计后的器件高频性能得到显著提高。%The high speed, low cost vertical cavity surface emitting laser ( VCSEL) is widely used in many fields such as the storage area network. According to the recent news release of the Fabre Channel Industry Association, the transmission rate of the fiber channel standard has reached 16 Gbit/s. Because of its low cost and suitability for mass production, through-hole ( TO) tube has been widely used in the VCSEL whose rate is less than 10 Gbit/s. Packaging is an important step to achieve the high-frequency performance for the VCSEL. Based on the equivalent circuit model of VCSEL coaxial package, this paper analyses some package parasitic parameters that can affect the high-frequency performances of devices. And to meet with the mass production requirements in factories, the device frequency response is optimized by adjusting parts of structure parameters and the relative permittivity of filling mate-rials. The results show that the high-frequency performances of devices are improved remarkably after the optimiza-tion design.

  11. Selective oxidation of cyclohexene through gold functionalized silica monolith microreactors

    Science.gov (United States)

    Alotaibi, Mohammed T.; Taylor, Martin J.; Liu, Dan; Beaumont, Simon K.; Kyriakou, Georgios

    2016-04-01

    Two simple, reproducible methods of preparing evenly distributed Au nanoparticle containing mesoporous silica monoliths are investigated. These Au nanoparticle containing monoliths are subsequently investigated as flow reactors for the selective oxidation of cyclohexene. In the first strategy, the silica monolith was directly impregnated with Au nanoparticles during the formation of the monolith. The second approach was to pre-functionalize the monolith with thiol groups tethered within the silica mesostructure. These can act as evenly distributed anchors for the Au nanoparticles to be incorporated by flowing a Au nanoparticle solution through the thiol functionalized monolith. Both methods led to successfully achieving even distribution of Au nanoparticles along the length of the monolith as demonstrated by ICP-OES. However, the impregnation method led to strong agglomeration of the Au nanoparticles during subsequent heating steps while the thiol anchoring procedure maintained the nanoparticles in the range of 6.8 ± 1.4 nm. Both Au nanoparticle containing monoliths as well as samples with no Au incorporated were tested for the selective oxidation of cyclohexene under constant flow at 30 °C. The Au free materials were found to be catalytically inactive with Au being the minimum necessary requirement for the reaction to proceed. The impregnated Au-containing monolith was found to be less active than the thiol functionalized Au-containing material, attributable to the low metal surface area of the Au nanoparticles. The reaction on the thiol functionalized Au-containing monolith was found to depend strongly on the type of oxidant used: tert-butyl hydroperoxide (TBHP) was more active than H2O2, likely due to the thiol induced hydrophobicity in the monolith.

  12. Monolithic microwave integrated circuits for sensors, radar, and communications systems; Proceedings of the Meeting, Orlando, FL, Apr. 2-4, 1991

    Science.gov (United States)

    Leonard, Regis F. (Editor); Bhasin, Kul B. (Editor)

    1991-01-01

    Consideration is given to MMICs for airborne phased arrays, monolithic GaAs integrated circuit millimeter wave imaging sensors, accurate design of multiport low-noise MMICs up to 20 GHz, an ultralinear low-noise amplifier technology for space communications, variable-gain MMIC module for space applications, a high-efficiency dual-band power amplifier for radar applications, a high-density circuit approach for low-cost MMIC circuits, coplanar SIMMWIC circuits, recent advances in monolithic phased arrays, and system-level integrated circuit development for phased-array antenna applications. Consideration is also given to performance enhancement in future communications satellites with MMIC technology insertion, application of Ka-band MMIC technology for an Orbiter/ACTS communications experiment, a space-based millimeter wave debris tracking radar, low-noise high-yield octave-band feedback amplifiers to 20 GHz, quasi-optical MESFET VCOs, and a high-dynamic-range mixer using novel balun structure.

  13. Energy Absorption of Monolithic and Fibre Reinforced Aluminium Cylinders

    NARCIS (Netherlands)

    De Kanter, J.L.C.G.

    2006-01-01

    Summary accompanying the thesis: Energy Absorption of Monolithic and Fibre Reinforced Aluminium Cylinders by Jens de Kanter This thesis presents the investigation of the crush behaviour of both monolithic aluminium cylinders and externally fibre reinforced aluminium cylinders. The research is based

  14. Time-based position estimation in monolithic scintillator detectors

    NARCIS (Netherlands)

    Tabacchini, V.; Borghi, G.; Schaart, D.R.

    2015-01-01

    Gamma-ray detectors based on bright monolithic scintillation crystals coupled to pixelated photodetectors are currently being considered for several applications in the medical imaging field. In a typical monolithic detector, both the light intensity and the time of arrival of the earliest

  15. Time-based position estimation in monolithic scintillator detectors

    NARCIS (Netherlands)

    Tabacchini, V.; Borghi, G.; Schaart, D.R.

    2015-01-01

    Gamma-ray detectors based on bright monolithic scintillation crystals coupled to pixelated photodetectors are currently being considered for several applications in the medical imaging field. In a typical monolithic detector, both the light intensity and the time of arrival of the earliest scintilla

  16. Time-based position estimation in monolithic scintillator detectors

    NARCIS (Netherlands)

    Tabacchini, V.; Borghi, G.; Schaart, D.R.

    2015-01-01

    Gamma-ray detectors based on bright monolithic scintillation crystals coupled to pixelated photodetectors are currently being considered for several applications in the medical imaging field. In a typical monolithic detector, both the light intensity and the time of arrival of the earliest scintilla

  17. A Monolithic Perovskite Structure for Use as a Magnetic Regenerator

    DEFF Research Database (Denmark)

    Pryds, Nini; Clemens, Frank; Menon, Mohan

    2011-01-01

    A La0.67Ca0.26Sr0.07Mn1.05O3 (LCSM) perovskite was prepared for the first time as a ceramic monolithic regenerator used in a regenerative magnetic refrigeration device. The parameters influencing the extrusion process and the performance of the regenerator, such as the nature of the monolith paste...

  18. Energy Absorption of Monolithic and Fibre Reinforced Aluminium Cylinders

    NARCIS (Netherlands)

    De Kanter, J.L.C.G.

    2006-01-01

    Summary accompanying the thesis: Energy Absorption of Monolithic and Fibre Reinforced Aluminium Cylinders by Jens de Kanter This thesis presents the investigation of the crush behaviour of both monolithic aluminium cylinders and externally fibre reinforced aluminium cylinders. The research is based

  19. Hydrogel coated monoliths for enzymatic hydrolysis of penicillin G

    NARCIS (Netherlands)

    De Lathouder, K.M.; Smeltink, M.W.; Straathof, A.J.J.; Paasman, M.A.; Van de Sandt, E.J.A.X.; Kapteijn, F.; Moulijn, J.A.

    2008-01-01

    The objective of this work was to develop a hydrogel-coated monolith for the entrapment of penicillin G acylase (E. coli, PGA). After screening of different hydrogels, chitosan was chosen as the carrier material for the preparation of monolithic biocatalysts. This protocol leads to active immobilize

  20. A new large area monolithic silicon telescope

    CERN Document Server

    Tudisco, S; Cabibbo, M; Cardella, G; De Geronimo, G; Di Pietro, A; Fallica, G; Figuera, P; Musumarra, A; Papa, M; Pappalardo, G S; Rizzo, F; Valvo, G

    1999-01-01

    A new prototype of large area (20x20 mm sup 2) monolithic silicon telescope with an ultrathin DELTA E stage (1 mu m) has been built and tested. A particular mask for the ground electrode has been developed to improve the charge collection reducing the induction between the E and DELTA E stages. A special designed preamplifier has been used for the readout of the signal from the DELTA E stage to overcome the problem of the large input capacitance (40 nF). A rather low energy threshold charge discrimination has been obtained. Small side effects due to the electric field deformation near the ground electrode were observed and quantified.

  1. Monolithic aerogels with nanoporous crystalline phases

    Science.gov (United States)

    Daniel, Christophe; Guerra, Gaetano

    2015-05-01

    High porosity monolithic aerogels with nanoporous crystalline phases can be obtained from syndiotactic polystyrene and poly(2,6-dimethyl-1,4-phenylene)oxide thermoreversible gels by removing the solvent with supercritical CO2. The presence of crystalline nanopores in the aerogels based on these polymers allows a high uptake associated with a high selectivity of volatile organic compounds from vapor phase or aqueous solutions even at very low activities. The sorption and the fast kinetics make these materials particularly suitable as sorption medium to remove traces of pollutants from water and moist air.

  2. Growth and Transfer of Monolithic Horizontal ZnO Nanowire Superstructures onto Flexible Substrates

    KAUST Repository

    Xu, Sheng

    2010-04-28

    A method of fabricating horizontally aligned ZnO nanowire (NW) arrays with full control over the width and length is demonstrated. A cross-sectional view of the NWs by transmission electron microscopy shows a "mushroom-like" structure. Novel monolithic multisegment superstructures are fabricated by making use of the lateral overgrowth. Ultralong horizontal ZnO NWs of an aspect ratio on the order often thousand are also demonstrated. These horizontal NWs are lifted off and transferred onto a flexible polymer substrate, which may have many great applications in horizontal ZnO NW-based nanosensor arrays, light-emitting diodes, optical gratings, integrated circuit interconnects, and high-output-power alternating-current nanogenerators. © 2010 WILEY-VCH Verlag GmbH & Co. KGaA.

  3. SiGe BiCMOS front-end circuits for X-Band phased arrays

    OpenAIRE

    2012-01-01

    The current Transmit/Receive (T/R) modules have typically been implemented using GaAs- and InP-based discrete monolithic microwave integrated circuits (MMIC) to meet the high performance requirement of the present X-Band phased arrays. However their cost, size, weight, power consumption and complexity restrict phased array technology only to certain military and satellite applications which can tolerate these limitations. Therefore, next generation X-Band phased array radar systems aim to use...

  4. A multiple-input-multiple-output visible light communication system based on VCSELs and spatial light modulators.

    Science.gov (United States)

    Lu, Hai-Han; Lin, Ying-Pyng; Wu, Po-Yi; Chen, Chia-Yi; Chen, Min-Chou; Jhang, Tai-Wei

    2014-02-10

    A multiple-input-multiple-output (MIMO) visible light communication (VLC) system employing vertical cavity surface emitting laser (VCSEL) and spatial light modulators (SLMs) with 16-quadrature amplitude modulation (QAM)-orthogonal frequency-division multiplexing (OFDM) modulating signal is proposed and experimentally demonstrated. The transmission capacity of system is significantly increased by space-division demultiplexing scheme. With the assistance of low noise amplifier (LNA) and data comparator, good bit error rate (BER) performance, clear constellation map, and clear eye diagram are achieved for each optical channel. Such a MIMO VLC system would be attractive for providing services including data and telecommunication services. Our proposed system is suitably applicable to the lightwave communication system in wireless transmission.

  5. Real-time, continuous, fluorescence sensing in a freely-moving subject with an implanted hybrid VCSEL/CMOS biosensor

    Science.gov (United States)

    O’Sullivan, Thomas D.; Heitz, Roxana T.; Parashurama, Natesh; Barkin, David B.; Wooley, Bruce A.; Gambhir, Sanjiv S.; Harris, James S.; Levi, Ofer

    2013-01-01

    Performance improvements in instrumentation for optical imaging have contributed greatly to molecular imaging in living subjects. In order to advance molecular imaging in freely moving, untethered subjects, we designed a miniature vertical-cavity surface-emitting laser (VCSEL)-based biosensor measuring 1cm3 and weighing 0.7g that accurately detects both fluorophore and tumor-targeted molecular probes in small animals. We integrated a critical enabling component, a complementary metal-oxide semiconductor (CMOS) read-out integrated circuit, which digitized the fluorescence signal to achieve autofluorescence-limited sensitivity. After surgical implantation of the lightweight sensor for two weeks, we obtained continuous and dynamic fluorophore measurements while the subject was un-anesthetized and mobile. The technology demonstrated here represents a critical step in the path toward untethered optical sensing using an integrated optoelectronic implant. PMID:24009996

  6. Monolithic columns in plant proteomics and metabolomics.

    Science.gov (United States)

    Rigobello-Masini, Marilda; Penteado, José Carlos Pires; Masini, Jorge Cesar

    2013-03-01

    Since "omics" techniques emerged, plant studies, from biochemistry to ecology, have become more comprehensive. Plant proteomics and metabolomics enable the construction of databases that, with the help of genomics and informatics, show the data obtained as a system. Thus, all the constituents of the system can be seen with their interactions in both space and time. For instance, perturbations in a plant ecosystem as a consequence of application of herbicides or exposure to pollutants can be predicted by using information gathered from these databases. Analytical chemistry has been involved in this scientific evolution. Proteomics and metabolomics are emerging fields that require separation, identification, and quantification of proteins, peptides, and small molecules of metabolites in complex biological samples. The success of this work relies on efficient chromatographic and electrophoretic techniques, and on mass spectrometric detection. This paper reviews recent developments in the use of monolithic columns, focusing on their applications in "top-down" and "bottom-up" approaches, including their use as supports for immobilization of proteolytic enzymes and their use in two-dimensional and multidimensional chromatography. Whereas polymeric columns have been predominantly used for separation of proteins and polypeptides, silica-based monoliths have been more extensively used for separation of small molecules of metabolites. Representative applications in proteomics and in analysis of plant metabolites are given and summarized in tables.

  7. Growth techniques for monolithic YBCO solenoidal magnets

    Energy Technology Data Exchange (ETDEWEB)

    Scruggs, S.J. [Texas Center for Superconductivity at University of Houston, 4800 Calhoun, Houston, TX 77204 (United States)]. E-mail: Sscruggs2@uh.edu; Putman, P.T. [Texas Center for Superconductivity at University of Houston, 4800 Calhoun, Houston, TX 77204 (United States); Fang, H. [Texas Center for Superconductivity at University of Houston, 4800 Calhoun, Houston, TX 77204 (United States); Alessandrini, M. [Texas Center for Superconductivity at University of Houston, 4800 Calhoun, Houston, TX 77204 (United States); Salama, K. [Texas Center for Superconductivity at University of Houston, 4800 Calhoun, Houston, TX 77204 (United States)

    2006-10-01

    The possibility of growing large single domain YBCO solenoids by the use of a large seed has been investigated. There are two known methods for producing a similar solenoid. This first is a conventional top seeded melt growth process followed by a post processing machining step to create the bore. The second involves using multiple seeds spaced around the magnet bore. The appeal of the new technique lies in decreasing processing time compared to the single seed technique, while avoiding alignment problems found in the multiple seeding technique. By avoiding these problems, larger diameter monoliths can be produced. Large diameter monoliths are beneficial because the maximum magnetic field produced by a trapped field magnet is proportional to the radius of the sample. Furthermore, the availability of trapped field magnets with large diameter could enable their use in applications that traditionally have been considered to require wound electromagnets, such as beam bending magnets for particle accelerators or electric propulsion. A comparison of YBCO solenoids grown by the use of a large seed and grown by the use of two small seeds simulating multiple seeding is made. Trapped field measurements as well as microstructure evaluation were used in characterization of each solenoid. Results indicate that high quality growth occurs only in the vicinity of the seeds for the multiple seeded sample, while the sample with the large seeded exhibited high quality growth throughout the entire sample.

  8. High surface area, high permeability carbon monoliths

    Energy Technology Data Exchange (ETDEWEB)

    Lagasse, R.R.; Schroeder, J.L. [Sandia National Labs., Albuquerque, NM (United States). Organic Materials Processing Dept.

    1994-12-31

    The goal of this work is to prepare carbon monoliths having precisely tailored pore size distribution. Prior studies have demonstrated that poly(acrylonitrile) can be processed into a precursor having tailored macropore structure. Since the macropores were preserved during pyrolysis, this synthetic process provided a route to porous carbon having macropores with size =0.1 to 10{mu}m. No micropores of size <2 nm could be detected in the carbon, however, by nitrogen adsorption. In the present work, the authors have processed a different polymer, poly(vinylidene chloride) into a macroporous precursor, Pyrolysis produced carbon monoliths having macropores derived from the polymer precursor as well as extensive microporosity produced during the pyrolysis of the polymer. One of these carbons had BET surface area of 1,050 m{sup 2}/g and about 1.2 cc/g total pore volume, with about 1/3 of the total pore volume in micropores and the remainder in 1{mu}m macropores. No mesopores in the intermediate size range could be detected by nitrogen adsorption. Carbon materials having high surface area as well as micron size pores have potential applications as electrodes for double layer supercapacitors containing liquid electrolyte, or as efficient media for performing chemical separations.

  9. Hydrothermal method for preparing calcium phosphate monoliths

    Directory of Open Access Journals (Sweden)

    García Carrodeguas Raúl

    2003-01-01

    Full Text Available A new hydrothermal route for preparing biphasic calcium phosphate monoliths is proposed. Firstly, a slurry of beta-tricalcium phosphate/ortho-phosphoric acid (b-TCP/H3PO4 is cast into the desired final shape and size to obtain a block composed of dicalcium phosphate dihydrate (DCPD and b-TCP. This block is then treated in 1.0 M Na2HPO4 at 60 °C in order to hydrolyze the DCPD into Ca10-x(HPO4x(PO4 6-x(OH2-x (CDHA and Ca8H2(PO46 .5H2O (OCP. The result is a monolithic piece which preserves the initial shape and size, but which is composed instead of CDHA, OCP, and b-TCP. During the initial stage, when the pH is slightly alkaline, the product of DCPD hydrolysis is CDHA. However, when a neutral or slightly acidic pH is reached OCP is formed. Test samples processed by this method showed complete conversion of DCPD into CDHA and OCP after 112 h of hydrolysis, and with a compressive strength of 16.2 MPa, similar to cancellous bone.

  10. Catastrophic failure of a monolithic zirconia prosthesis.

    Science.gov (United States)

    Chang, Jae-Seung; Ji, Woon; Choi, Chang-Hoon; Kim, Sunjai

    2015-02-01

    Recently, monolithic zirconia restorations have received attention as an alternative to zirconia veneered with feldspathic porcelain to eliminate chipping failures of veneer ceramics. In this clinical report, a patient with mandibular edentulism received 4 dental implants in the interforaminal area, and a screw-retained monolithic zirconia prosthesis was fabricated. The patient also received a maxillary complete removable dental prosthesis over 4 anterior roots. At the 18-month follow-up, all of the zirconia cylinders were seen to be fractured, and the contacting abutment surfaces had lost structural integrity. The damaged abutments were replaced with new abutments, and a new prosthesis was delivered with a computer-assisted design and computer-assisted manufacturing fabricated titanium framework with denture teeth and denture base resins. At the 6-month recall, the patient did not have any problems. Dental zirconia has excellent physical properties; however, care should be taken to prevent excessive stresses on the zirconia cylinders when a screw-retained zirconia restoration is planned as a definitive prosthesis.

  11. Fabrication of four-channel DFB laser array using nanoimprint technology for 1.3 μm CWDM systems

    Institute of Scientific and Technical Information of China (English)

    Zhao Jianyi; Chen Xin; Zhou Ning; Huang Xiaodong; Liu Wen

    2014-01-01

    Four-channel monolithically integrated index-coupled distributed-feedback laser array has been fabricated using nanoimprint technology for 1.3 μm CWDM system.Selective lasing wavelength with 20 nm wavelength space is obtained.The present results show that the nanoimprint technology is mature and reliable in the fabrication of DFB laser array.

  12. Monolithically interconnected GaAs solar cells: A new interconnection technology for high voltage solar cell output

    Science.gov (United States)

    Dinetta, L. C.; Hannon, M. H.

    1995-01-01

    Photovoltaic linear concentrator arrays can benefit from high performance solar cell technologies being developed at AstroPower. Specifically, these are the integration of thin GaAs solar cell and epitaxial lateral overgrowth technologies with the application of monolithically interconnected solar cell (MISC) techniques. This MISC array has several advantages which make it ideal for space concentrator systems. These are high system voltage, reliable low cost monolithically formed interconnections, design flexibility, costs that are independent of array voltage, and low power loss from shorts, opens, and impact damage. This concentrator solar cell will incorporate the benefits of light trapping by growing the device active layers over a low-cost, simple, PECVD deposited silicon/silicon dioxide Bragg reflector. The high voltage-low current output results in minimal 12R losses while properly designing the device allows for minimal shading and resistance losses. It is possible to obtain open circuit voltages as high as 67 volts/cm of solar cell length with existing technology. The projected power density for the high performance device is 5 kW/m for an AMO efficiency of 26% at 1 5X. Concentrator solar cell arrays are necessary to meet the power requirements of specific mission platforms and can supply high voltage power for electric propulsion systems. It is anticipated that the high efficiency, GaAs monolithically interconnected linear concentrator solar cell array will enjoy widespread application for space based solar power needs. Additional applications include remote man-portable or ultra-light unmanned air vehicle (UAV) power supplies where high power per area, high radiation hardness and a high bus voltage or low bus current are important. The monolithic approach has a number of inherent advantages, including reduced cost per interconnect and increased reliability of array connections. There is also a high potential for a large number of consumer products. Dual

  13. Preparation and Characterization of Temperature-responsive Porous Monoliths

    Institute of Scientific and Technical Information of China (English)

    ZHANG, Rongyue; QI, Li; XIN, Peiyong; YANG, Gengliang; CHEN, Yi

    2009-01-01

    A new temperature-responsive porous monolith has been prepared by surface-initiated activators generated by electron transfer atom transfer radical polymerization (AGET ATRP) grafting poly(N-isopropylacrylamide) (PNIPAAm) within the pores of the porous polymer monolith. The grafting copolymerization was carried out by a method based on a continuous flow-through technique without special deoxygenation procedure needed in the general ATRP. The addition of ascorbic acid could counteract the oxidation effect of oxygen diffusing into the reaction system. The resulting grafted monolith was characterized by a mercury intrusion method and the size of macropore was 3.65 μm, which was suitable for flow through the monolith for HPLC. The thermally responsive property of the grafted monolith was evaluated by HPLC using steroids with various hydrophobicities as probes. Through determination of retention factor of each steroid on the grafted monolith at different temperatures using water as mobile phase, it was found that the slope of the plot of retention factor of each steroid versus the temperature changed around the low critical solution temperature (LCST, 32 ℃) of PNIPAAm in water. It was relative to the grafted PNIPAAm temperature sensitivity that a hydrophobic and hydrophilic alternation would take place around its LCST.Based on this thermally responsive property, the grafted monolith was used as stationary phase for HPLC and to separate the steroids using water as mobile phase by changing the column temperature. As a mobile phase, water is much better than organic solvents concerning the environment.

  14. Influence of different carbon monolith preparation parameters on pesticide adsorption

    Directory of Open Access Journals (Sweden)

    Vukčević Marija

    2013-01-01

    Full Text Available The capacity of carbon monolith for pesticide removal from water, and the mechanism of pesticide interaction with carbon surface were examined. Different carbon monolith samples were obtained by varying the carbonization and activation parameters. In order to examine the role of surface oxygen groups in pesticide adsorption, carbon monolith surface was functionalized by chemical treatment in HNO3, H2O2 and KOH. The surface properties of the obtained samples were investigated by BET surface area, pore size distribution and temperature-programmed desorption. Adsorption of pesticides from aqueous solution onto activated carbon monolith samples was studied by using five pesticides belonging to different chemical groups (acetamiprid, dimethoate, nicosulfuron, carbofuran and atrazine. Presented results show that higher temperature of carbonization and the amount of activating agent allow obtaining microporous carbon monolith with higher amount of surface functional groups. Adsorption properties of the activated carbon monolith were more readily affected by the amount of the surface functional groups than by specific surface area. Results obtained by carbon monolith functionalisation showed that π-π interactions were the main force for adsorption of pesticides with aromatic structure, while acidic groups play an important role in adsorption of pesticides with no aromatic ring in the chemical structure.

  15. Close to 100 Gbps discrete multitone transmission over 100m of multimode fiber using a single transverse mode 850nm VCSEL

    Science.gov (United States)

    Wu, Bo; Zhou, Xian; Ma, Yanan; Luo, Jun; Zhong, Kangping; Qiu, Shaofeng; Feng, Zhiyong; Luo, Yazhi; Agustin, Mikel; Ledentsov, Nikolay; Kropp, Joerg; Shchukin, Vitaly; Ledentsov, Nikolay N.; Eddie, Iain; Chao, Lu

    2016-03-01

    Discrete Multitone Transmission (DMT) transmission over standard multimode fiber (MMF) using high-speed single (SM) and multimode (MM) Vertical-Cavity Surface-Emitting Lasers (VCSELs) is studied. Transmission speed in the range of 72Gbps to 82Gbps over 300m -100m distances of OM4 fiber is realized, respectively, at Bit-Error-Ratio (BER) 100Gbps data transmission over >300m MMF distances at the BER levels matching the industry standards will become possible.

  16. Preliminary comparison of monolithic and aperture optics for XRMF

    Energy Technology Data Exchange (ETDEWEB)

    Havrilla, G.J.; Worley, C.G.

    1997-08-01

    Comparisons between standard aperture optics and a custom designed monolithic capillary x-ray optic for the Kevex Omicron are presented. The results demonstrate the feasibility of retrofitting an Omicron with a monolithic capillary. Increased flux is observed especially at lower energies which results in an increase in sensitivity and potentially an increase in spatial resolution. Alignment is a critical factor in achieving optimal performance of the monolithic capillary. Further improvements in flux output, spot size and overall sensitivity are expected with better alignment.

  17. On monolithic stability and reinforcement analysis of high arch dams

    Institute of Scientific and Technical Information of China (English)

    2007-01-01

    Monolithic stability safety and reinforcement based on monolithic stability are very important for arch dam design.In this paper,the issue is addressed based on deformation reinforcement theory.In this approach,plastic complementary energy norm can be taken as safety Index for monolithic stability.According to deformation reinforcement theory,the areas where unbalanced force exists require reinforcement,and the required reinforcement forces are just the unbalanced forces with opposite direction.Results show that areas with unbalanced force mainly concentrate in dam-toes,dam-heels and faults.

  18. Hierarchically Structured Monolithic ZSM-5 through Macroporous Silica Gel Zeolitization

    Institute of Scientific and Technical Information of China (English)

    Lei Qian; Zhao Tianbo; Li Fengyan; Zong Baoning; Tong Yangchuan

    2006-01-01

    The hierarchically structured ZSM-5 monolith was prepared through transforming the skeletons of the macroporous silica gel into ZSM-5 by the steam-assisted conversion method. The morphology and monolithic shapes of macroporous silica gel were well preserved. The hierarchically structured ZSM-5 monolith exhibited the hierarchical porosity, with mesopores and macropores existing inside the macroporous silica gel, and micropores formed by the ZSM-5. The products have been characterized properly by using the XRD, SEM and N2 adsorption-desorption methods.

  19. Preparation of carbon monoliths from orange peel for NOx retention

    Directory of Open Access Journals (Sweden)

    Liliana Giraldo

    2014-12-01

    Full Text Available A series of monoliths are prepared from orange peels and chemically activated with H3PO4, KOH, ZnCl2, and water vapor without a binder. The monoliths were characterized by N2 adsorption-desorption isotherms at 77 K, Boehm titrations and XPS. Thereafter, monoliths were tested for their ability to establish NOx retention. The results show that the retention capacities of NOx were a function of the textural properties and chemistries. The carbons synthesized with ZnCl2 and KOH retained similar amounts of NOx.

  20. A decoupled monolithic projection method for natural convection problems

    Science.gov (United States)

    Pan, Xiaomin; Kim, Kyoungyoun; Lee, Changhoon; Choi, Jung-Il

    2016-06-01

    We propose an efficient monolithic numerical procedure based on a projection method for solving natural convection problems. In the present monolithic method, the buoyancy, linear diffusion, and nonlinear convection terms are implicitly advanced by applying the Crank-Nicolson scheme in time. To avoid an otherwise inevitable iterative procedure in solving the monolithic discretized system, we use a linearization of the nonlinear convection terms and approximate block lower-upper (LU) decompositions along with approximate factorization. Numerical simulations demonstrate that the proposed method is more stable and computationally efficient than other semi-implicit methods, preserving temporal second-order accuracy.

  1. Monolithically Peltier-cooled laser diodes

    Energy Technology Data Exchange (ETDEWEB)

    Hava, S.; Hunsperger, R.G.; Sequeira, H.B.

    1984-04-01

    A new method of cooling a GaAs/GaAlAs laser in an optical integrated circuit or on a discrete chip, by adding an integral thermoelectric (Peltier) cooling and heat spreading device to the laser, is presented. This cooling both reduces and stabilizes the laser junction temperature to minimize such deleterious effects as wavelength drift due to heating. A unified description of the electrical and thermal properties of a monolithic semiconductor mesa structure is given. Here it is shown that an improvement in thermal characteristics is obtained by depositing a relatively thick metallic layer, and by using this layer as a part of an active Peltier structure. Experimental results reveal a 14-percent increase in emitted power (external quantum efficiency) due to passive heat spreading and a further 8-percent if its Peltier cooler is operated. Fabrication techniques used to obtain devices exhibiting the above performance characteristics are given. 21 references.

  2. LSST primary/tertiary monolithic mirror

    Science.gov (United States)

    Sebag, J.; Gressler, W.; Liang, M.; Neill, D.; Araujo-Hauck, C.; Andrew, J.; Angeli, G.; Cho, M.; Claver, C.; Daruich, F.; Gessner, C.; Hileman, E.; Krabbendam, V.; Muller, G.; Poczulp, G.; Repp, R.; Wiecha, O.; Xin, B.; Kenagy, K.; Martin, H. M.; Tuell, M. T.; West, S. C.

    2016-08-01

    At the core of the Large Synoptic Survey Telescope (LSST) three-mirror optical design is the primary/tertiary (M1M3) mirror that combines these two large mirrors onto one monolithic substrate. The M1M3 mirror was spin cast and polished at the Steward Observatory Mirror Lab at The University of Arizona (formerly SOML, now the Richard F. Caris Mirror Lab at the University of Arizona (RFCML)). Final acceptance of the mirror occurred during the year 2015 and the mirror is now in storage while the mirror cell assembly is being fabricated. The M1M3 mirror will be tested at RFCML after integration with its mirror cell before being shipped to Chile.

  3. A monolithic thin film electrochromic window

    Energy Technology Data Exchange (ETDEWEB)

    Goldner, R.B.; Arntz, F.O.; Berera, G.; Haas, T.E.; Wong, K.K. (Tufts Univ., Medford, MA (United States). Electro-Optics Technology Center); Wei, G. (Mobil Solar Energy Corp., Billerica, MA (United States)); Yu, P.C. (PPG Industries, Inc., Monroeville, PA (United States))

    1991-01-01

    Three closely related thin film solid state ionic devices that are potentially important for applications are: electrochromic smart windows, high energy density thin film rechargeable batteries, and thin film electrochemical sensors. Each usually has at least on mixed ion/electron conductor, an electron-blocking ion conductor, and an ion-blocking electron conductor, and many of the technical issues associated with thin film solid state ionics are common to all three devices. Since the electrochromic window has the added technical requirement of electrically-controlled optical modulation, (over the solar spectrum), and since research at the authors' institution has focused primarily on the window structure, this paper will address the electrochromic window, and particularly a monolithic variable reflectivity electrochromic window, as an illustrative example of some of the challenges and opportunities that are confronting the thin film solid state ionics community. 33 refs.

  4. A monolithic thin film electrochromic window

    Energy Technology Data Exchange (ETDEWEB)

    Goldner, R.B.; Arntz, F.O.; Berera, G.; Haas, T.E.; Wong, K.K. [Tufts Univ., Medford, MA (United States). Electro-Optics Technology Center; Wei, G. [Mobil Solar Energy Corp., Billerica, MA (United States); Yu, P.C. [PPG Industries, Inc., Monroeville, PA (United States)

    1991-12-31

    Three closely related thin film solid state ionic devices that are potentially important for applications are: electrochromic smart windows, high energy density thin film rechargeable batteries, and thin film electrochemical sensors. Each usually has at least on mixed ion/electron conductor, an electron-blocking ion conductor, and an ion-blocking electron conductor, and many of the technical issues associated with thin film solid state ionics are common to all three devices. Since the electrochromic window has the added technical requirement of electrically-controlled optical modulation, (over the solar spectrum), and since research at the authors` institution has focused primarily on the window structure, this paper will address the electrochromic window, and particularly a monolithic variable reflectivity electrochromic window, as an illustrative example of some of the challenges and opportunities that are confronting the thin film solid state ionics community. 33 refs.

  5. Machining distortion prediction of aerospace monolithic components

    Institute of Scientific and Technical Information of China (English)

    Yun-bo BI; Qun-lin CHENG; Hui-yue DONG; Ying-lin KE

    2009-01-01

    To predict the distortion of aerospace monolithic components.a model is established to simulate the numerical control (NC)milling process using 3D finite element method(FEM).In this model,the cutting layer is simplified firstly.Then,the models of cutting force and cutting temperature are established to gain the cutting loads,which are applied to the mesh model of the part.Finally,a prototype of machining simulation environment is developed to simulate the milling process of a spar.Key factors influencing the distortion,such as initial residual stress,cutting loads,fixture layout,cutting sequence,and tool path are considered all together.The total distortion of the spar is predicted and an experiment is conducted to validate the numerical results.It is found that the maximum discrepancy between the simulation results and experiment values is 19.0%

  6. Silver deposition on chemically treated carbon monolith

    Directory of Open Access Journals (Sweden)

    Jovanović Zoran M.

    2009-01-01

    Full Text Available Carbon monolith was treated with HNO3, KOH and H2O2. Effects of these treatments on the surface functional groups and on the amount of silver deposited on the CM surface were studied by temperature programmed desorption (TPD and atomic absorption spectrometry (AAS. As a result of chemical treatment there was an increase in the amount of surface oxygen complexes. The increase in the amount of silver deposit is proportional to the amount of surface groups that produce CO under decomposition. However, the high amount of CO groups, decomposing above 600°C, induces the smaller Ag crystallite size. Therefore, the high temperature CO evolving oxides are, most likely, the initial centers for Ag deposition.

  7. A Low Phase Noise Fully Monolithic 6 GHz Differential Coupled NMOS LC-VCO

    Science.gov (United States)

    Moalla, Dorra Mellouli; Cordeau, David; Mnif, Hassene; Paillot, Jean-Marie; Loulou, Mourad

    2016-01-01

    A fully monolithic 6 GHz low-phase noise Voltage-Controlled-Oscillator (VCO) is presented in this paper. It consists in two LC-NMOS differential VCOs coupled through a resistive network and is implemented on a 0.25 µm BiCMOS SiGe process. This proposed integrated VCO can be used also for phased-array applications to steer the beam over the entire spatial range. In this case, the radiation pattern of the phased antenna array is steered in a particular direction by establishing a constant phase progression in the oscillator chain which can be obtained by detuning the free-running frequencies of the two oscillators in the array. At 2.5 V power supply voltage and a power dissipation of 62.5 mW, the coupled VCO array features a measured worst case phase noise of -102.4 dBc/Hz and -125.64 dBc/Hz at 100 kHz and 1 MHz frequency offset respectively from a 6 GHz carrier. The tuning range is about 400 MHz, from 5.85 to 6.25 GHz, for a tuning voltage varying from 0 to 2.5 V.

  8. Monolithic Rare Earth Doped PTR Glass Laser Project

    Data.gov (United States)

    National Aeronautics and Space Administration — The main goal of the project is to demonstrate the feasibility of a monolithic solid state laser on the basis of PTR glass co-doped with luminescent rare earth ions....

  9. Plant oil-based shape memory polymer using acrylic monolith

    Directory of Open Access Journals (Sweden)

    T. Tsujimoto

    2015-09-01

    Full Text Available This article deals with the synthesis of a plant oil-based material using acrylic monolith. An acrylic monolith bearing oxirane groups was prepared via simple technique that involved the dissolution of poly(glycidyl methacrylate-comethyl methacrylate (PGMA in ethanolic – aqueous solution by heating and subsequent cooling. The PGMA monolith had topologically porous structure, which was attributed to the phase separation of the polymer solution. The PGMA monolith was impregnated by epoxidized soybean oil (ESO containing thermally-latent catalyst, and the subsequent curing produced a crosslinked material with relatively good transparency. The Young’s modulus and the tensile strength of polyESO/PGMA increased compared with the ESO homopolymer. The strain at break of polyESO/PGMA was larger than that of the ESO homopolymer and crosslinked PGMA. Furthermore, polyESO/PGMA exhibited good shape memory-recovery behavior.

  10. Application of monolithic chromatographic supports in virus research.

    Science.gov (United States)

    Krajacic, Mladen; Ravnikar, Maja; Štrancar, Aleš; Gutiérrez-Aguirre, Ion

    2017-05-12

    Key properties of monolithic chromatographic supports, make them suitable for separation and/or concentration of large biomolecules, especially virus particles and viral genomes. One by one, the studies that have been completed so far, contributed to the knowledge that monolith chromatography has hardly any limitation to be applied in virus research. Viruses of different sizes, possessing icosahedral structure and symmetrical morphology, as well as rod-shaped or filamentous viruses with helical structure, even enveloped ones, all of them could be successfully managed by means of monolith chromatography. Same is true for viral genomes, primarily when being distinct from other nucleic acid forms present in a host cell. This review is exclusively focused on viruses. It describes the application of monolith chromatography to different problematics within the virus research field. The reviewed achievements offer new possibilities and trigger new aspects in virology. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  11. Monolithic Perovskite Silicon Tandem Solar Cells with Advanced Optics

    Energy Technology Data Exchange (ETDEWEB)

    Goldschmidt, Jan C.; Bett, Alexander J.; Bivour, Martin; Blasi, Benedikt; Eisenlohr, Johannes; Kohlstadt, Markus; Lee, Seunghun; Mastroianni, Simone; Mundt, Laura; Mundus, Markus; Ndione, Paul; Reichel, Christian; Schubert, Martin; Schulze, Patricia S.; Tucher, Nico; Veit, Clemens; Veurman, Welmoed; Wienands, Karl; Winkler, Kristina; Wurfel, Uli; Glunz, Stefan W.; Hermle, Martin

    2016-11-14

    For high efficiency monolithic perovskite silicon tandem solar cells, we develop low-temperature processes for the perovskite top cell, rear-side light trapping, optimized perovskite growth, transparent contacts and adapted characterization methods.

  12. Effect of accelerated aging on translucency of monolithic zirconia

    Directory of Open Access Journals (Sweden)

    O. Abdelbary

    2016-12-01

    Conclusion: Thickness of zirconia has significant effect on translucency. Aging has significant effect on thinner sections of zirconia. More research is required on zirconia towards making the material more translucent for its potential use as esthetic monolithic restoration.

  13. Performance characteristics between monolithic and microservice-based systems

    OpenAIRE

    Flygare, Robin; Holmqvist, Anthon

    2017-01-01

    A new promising technology to face the problem of scalability and availability is the microservice architecture. The problem with this architecture is that there is no significant study that clearly proves the performance differences compared to the monolithic architecture. Our thesis aims to provide a more conclusive answer of how the microservice architecture differs performance wise compared to the monolithic architecture. In this study, we conducted several experiments on a self-developed...

  14. Sol-Gel Synthesis of Non-Silica Monolithic Materials

    Directory of Open Access Journals (Sweden)

    Bartłomiej Gaweł

    2010-04-01

    Full Text Available Monolithic materials have become very popular because of various applications, especially within chromatography and catalysis. Large surface areas and multimodal porosities are great advantages for these applications. New sol-gel preparation methods utilizing phase separation or nanocasting have opened the possibility for preparing materials of other oxides than silica. In this review, we present different synthesis methods for inorganic, non-silica monolithic materials. Some examples of application of the materials are also included.

  15. Reliability Analysis and Optimal Design of Monolithic Vertical Wall Breakwaters

    DEFF Research Database (Denmark)

    Sørensen, John Dalsgaard; Burcharth, Hans F.; Christiani, E.

    1994-01-01

    Reliability analysis and reliability-based design of monolithic vertical wall breakwaters are considered. Probabilistic models of the most important failure modes, sliding failure, failure of the foundation and overturning failure are described . Relevant design variables are identified and relia......Reliability analysis and reliability-based design of monolithic vertical wall breakwaters are considered. Probabilistic models of the most important failure modes, sliding failure, failure of the foundation and overturning failure are described . Relevant design variables are identified...

  16. Extended Leach Testing of Simulated LAW Cast Stone Monoliths

    Energy Technology Data Exchange (ETDEWEB)

    Serne, R. Jeffrey [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Westsik, Joseph H. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Williams, Benjamin D. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Jung, H. B. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Wang, Guohui [Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

    2015-07-09

    This report describes the results from long-term laboratory leach tests performed at Pacific Northwest National Laboratory (PNNL) for Washington River Protection Solutions (WRPS) to evaluate the release of key constituents from monoliths of Cast Stone prepared with four simulated low-activity waste (LAW) liquid waste streams. Specific objectives of the Cast Stone long-term leach tests described in this report focused on four activities: 1. Extending the leaching times for selected ongoing EPA-1315 tests on monoliths made with LAW simulants beyond the conventional 63-day time period up to 609 days reported herein (with some tests continuing that will be documented later) in an effort to evaluate long-term leaching properties of Cast Stone to support future performance assessment activities. 2. Starting new EPA-1315 leach tests on archived Cast Stone monoliths made with four LAW simulants using two leachants (deionized water [DIW] and simulated Hanford Integrated Disposal Facility (IDF) Site vadose zone pore water [VZP]). 3. Evaluating the impacts of varying the iodide loading (starting iodide concentrations) in one LAW simulant (7.8 M Na Hanford Tank Waste Operations Simulator (HTWOS) Average) by manufacturing new Cast Stone monoliths and repeating the EPA-1315 leach tests using DIW and the VZP leachants. 4. Evaluating the impacts of using a non-pertechnetate form of Tc that is present in some Hanford tanks. In this activity one LAW simulant (7.8 M Na HTWOS Average) was spiked with a Tc(I)-tricarbonyl gluconate species and then solidified into Cast Stone monoliths. Cured monoliths were leached using the EPA-1315 leach protocol with DIW and VZP. The leach results for the Tc-Gluconate Cast Stone monoliths were compared to Cast Stone monoliths pertechnetate.

  17. Depth of interaction determination in monolithic scintillator with double side SiPM readout.

    Science.gov (United States)

    Morrocchi, Matteo; Ambrosi, Giovanni; Bisogni, Maria Giuseppina; Bosi, Filippo; Boretto, Marco; Cerello, Piergiorgio; Ionica, Maria; Liu, Ben; Pennazio, Francesco; Piliero, Maria Antonietta; Pirrone, Giovanni; Postolache, Vasile; Wheadon, Richard; Del Guerra, Alberto

    2017-12-01

    Monolithic scintillators read out by arrays of photodetectors represent a promising solution to obtain high spatial resolution and the depth of interaction (DOI) of the annihilation photon. We have recently investigated a detector geometry composed of a monolithic scintillator readout on two sides by silicon photomultiplier (SiPM) arrays, and we have proposed two parameters for the DOI determination: the difference in the number of triggered SiPMs on the two sides of the detector and the difference in the maximum collected signal on a single SiPM on each side. This work is focused on the DOI calibration and on the determination of the capability of our detector. For the DOI calibration, we studied a method which can be implemented also in detectors mounted in a full PET scanner. We used a PET detector module composed of a monolithic 20 × 20 × 10 mm(3) LYSO scintillator crystal coupled on two opposite faces to two arrays of SiPMs. On each side, the scintillator was coupled to 6 × 6 SiPMs. In this paper, the two parameters previously proposed for the DOI determination were calibrated with two different methods. The first used a lateral scan of the detector with a collimated 511 keV pencil beam at steps of 0.5 mm to study the detector DOI capability, while the second used the background radiation of the (176)Lu in the scintillator. The DOI determination capability was tested on different regions of the detector using each parameter and the combination of the two. With both parameters for the DOI determination, in the lateral scan, the bias between the mean reconstructed DOI and the real beam position was lower than 0.3 mm, and the DOI distribution had a standard deviation of about 1.5 mm. When using the calibration with the radioactivity of the LYSO, the mean bias increased of about 0.2 mm but with no degradation of the standard deviation of the DOI distribution. The two parameters allow to achieve a DOI resolution comparable with the state of the

  18. Performance of a SiPM based semi-monolithic scintillator PET detector

    Science.gov (United States)

    Zhang, Xianming; Wang, Xiaohui; Ren, Ning; Kuang, Zhonghua; Deng, Xinhan; Fu, Xin; Wu, San; Sang, Ziru; Hu, Zhanli; Liang, Dong; Liu, Xin; Zheng, Hairong; Yang, Yongfeng

    2017-10-01

    A depth encoding PET detector module using semi-monolithic scintillation crystal single-ended readout by a SiPM array was built and its performance was measured. The semi-monolithic scintillator detector consists of 11 polished LYSO slices measuring 1  ×  11.6  ×  10 mm3. The slices are glued together with enhanced specular reflector (ESR) in between and outside of the slices. The bottom surface of the slices is coupled to a 4  ×  4 SiPM array with a 1 mm light guide and silicon grease between them. No reflector is used on the top surface and two sides of the slices to reduce the scintillation photon reflection. The signals of the 4  ×  4 SiPM array are grouped along rows and columns separately into eight signals. Four SiPM column signals are used to identify the slices according to the center of the gravity of the scintillation photon distribution in the pixelated direction. Four SiPM row signals are used to estimate the y (monolithic direction) and z (depth of interaction) positions according to the center of the gravity and the width of the scintillation photon distribution in the monolithic direction, respectively. The detector was measured with 1 mm sampling interval in both the y and z directions with electronic collimation by using a 0.25 mm diameter 22Na point source and a 1  ×  1  ×  20 mm3 LYSO crystal detector. An average slice based energy resolution of 14.9% was obtained. All slices of 1 mm thick were clearly resolved and a detector with even thinner slices could be used. The y positions calculated with the center of gravity method are different for interactions happening at the same y, but different z positions due to depth dependent edge effects. The least-square minimization and the maximum likelihood positioning algorithms were developed and both methods improved the spatial resolution at the edges of the detector as compared with the center of gravity method. A mean absolute error

  19. Mechanically stable, hierarchically porous Cu3(btc)2 (HKUST-1) monoliths via direct conversion of copper(II) hydroxide-based monoliths.

    Science.gov (United States)

    Moitra, Nirmalya; Fukumoto, Shotaro; Reboul, Julien; Sumida, Kenji; Zhu, Yang; Nakanishi, Kazuki; Furukawa, Shuhei; Kitagawa, Susumu; Kanamori, Kazuyoshi

    2015-02-28

    The synthesis of highly crystalline macro-meso-microporous monolithic Cu3(btc)2 (HKUST-1; btc(3-) = benzene-1,3,5-tricarboxylate) is demonstrated by direct conversion of Cu(OH)2-based monoliths while preserving the characteristic macroporous structure. The high mechanical strength of the monoliths is promising for possible applications to continuous flow reactors.

  20. Towards monolithic scintillator based TOF-PET systems: practical methods for detector calibration and operation

    Science.gov (United States)

    Borghi, Giacomo; Tabacchini, Valerio; Schaart, Dennis R.

    2016-07-01

    Gamma-ray detectors based on thick monolithic scintillator crystals can achieve spatial resolutions  published k-NN 1D method. Also, the procedures for estimating the DOI and time of interaction are revised to enable full detector calibration by means of fan-beam or flood irradiations only. Moreover, a new technique is presented to allow the use of events in which some of the photosensor pixel values and/or timestamps are missing (e.g. due to dead time), so as to further increase system sensitivity. The accelerated methods were tested on a monolithic scintillator detector specifically developed for clinical PET applications, consisting of a 32 mm  ×  32 mm  ×  22 mm LYSO : Ce crystal coupled to a digital photon counter (DPC) array. This resulted in a spatial resolution of 1.7 mm FWHM, an average DOI resolution of 3.7 mm FWHM, and a CRT of 214 ps. Moreover, the possibility of using events missing the information of up to 16 out of 64 photosensor pixels is shown. This results in only a small deterioration of the detector performance.

  1. Integrated optical and nuclear simulation of a monolithic LYSO:Ce based PET detector module

    Science.gov (United States)

    Játékos, B.; Patay, G.; Lőrincz, E.; Erdei, G.

    2017-05-01

    In the recent years new digital photon counter devices (also known as silicon photomultipliers, SiPMs) were designed and manufactured to be used specifically in positron emission tomography (PET) scanners. Finely pixelated SiPM arrays have opened new opportunities in PET detector development, such as the utilization of monolithic scintillator crystals. We worked out a simulation tool (SCOPE2) to assist the optimization and characterization of such PET detector modules. In the present paper we report the first application of SCOPE2 on the performance evaluation of a prototype PET detector module. The PET detector is based on monolithic LYSO:Ce scintillator crystal and a fully digital, silicon photon-counter, SPADnet-I. A new interface has been developed for SCOPE2 to access GATE simulation results. A combination of GATE and SCOPE2 was used to simulate excitation of the prototype PET detector with an electronically collimated γ -beam. Measurement results from the collimated γ-beam experiment were compared with the combined simulation. A good agreement was observed in the tendencies of total count spectrum and point of interaction distribution. We used the performance evaluation to understand and explain the measurement results in detail.

  2. Multi-channel monolithic integrated optic fiber Bragg grating sensor interrogator

    Science.gov (United States)

    Mendoza, Edgar A.; Esterkin, Yan; Kempen, Cornelia; Sun, Zongjian

    2011-09-01

    Fiber Bragg grating (FBG) is a mature sensing technology for the measurement of strain, vibration, acoustics, acceleration, pressure, temperature, moisture, and corrosion. It has gained rapid acceptance in civil, aerospace, chemical and petrochemical, medicine, aviation and automotive industries. The most prominent advantages of FBG are: small size and light weight, distributed array of FBG transducers on a single fiber, and immunity to radio frequency interference. However, a major disadvantage of FBG technology is that conventional state-of-the-art FBG interrogation system is typically bulky, heavy, and costly bench top instruments that are typically assembled from off-the-shelf fiber optic and optical components integrated with a signal electronics board into an instrument console. Based on the industrial need for a compact FBG interrogation system, this paper describes recent progress towards the development of miniature fiber Bragg grating sensor interrogator (FBG-Transceiver™) system based on multi-channel monolithic integrated optic sensor microchip technology. The integrated optic microchip technology enables monolithic integration of all functionalities, both passive and active, of conventional bench top FBG sensor interrogator system, packaged in a miniaturized, low power operation, 2 cm×5 cm small form factor (SFF) package suitable for long-term structural health monitoring in applications where size, weight, and power are critical for operation.

  3. Monolithically Integrated Microelectromechanical Systems for On-Chip Strain Engineering of Quantum Dots.

    Science.gov (United States)

    Zhang, Yang; Chen, Yan; Mietschke, Michael; Zhang, Long; Yuan, Feifei; Abel, Stefan; Hühne, Ruben; Nielsch, Kornelius; Fompeyrine, Jean; Ding, Fei; Schmidt, Oliver G

    2016-09-14

    Elastic strain fields based on single crystal piezoelectric elements represent an effective way for engineering the quantum dot (QD) emission with unrivaled precision and technological relevance. However, pioneering researches in this direction were mainly based on bulk piezoelectric substrates, which prevent the development of chip-scale devices. Here, we present a monolithically integrated Microelectromechanical systems (MEMS) device with great potential for on-chip quantum photonic applications. High-quality epitaxial PMN-PT thin films have been grown on SrTiO3 buffered Si and show excellent piezoelectric responses. Dense arrays of MEMS with small footprints are then fabricated based on these films, forming an on-chip strain tuning platform. After transferring the QD-containing nanomembranes onto these MEMS, the nonclassical emissions (e.g., single photons) from single QDs can be engineered by the strain fields. We envision that the strain tunable QD sources on the individually addressable and monolithically integrated MEMS pave the way toward complex quantum photonic applications on chip.

  4. Monoliths: A Review of the Basics, Preparation Methods and Their Relevance to Oxidation

    Directory of Open Access Journals (Sweden)

    Sandeeran Govender

    2017-02-01

    Full Text Available Considerable research has been conducted on monolithic catalysts for various applications. Strategies toward coating monoliths are of equal interest and importance. In this paper, the preparation of monoliths and monolithic catalysts have been summarized. More specifically, a brief explanation for the manufacturing of ceramic and metallic monoliths has been provided. Also, different methods for coating γ-alumina, as a secondary support, are included. Techniques used to deposit metal-based species, zeolites and carbon onto monoliths are discussed. Furthermore, monoliths extruded with metal oxides, zeolites and carbon are described. The main foci are on the reasoning and understanding behind the preparation of monolithic catalysts. Ideas and concerns are also contributed to encourage better approaches when designing these catalysts. More importantly, the relevance of monolithic structures to reactions, such as the selective oxidation of alkanes, catalytic combustion for power generation and the preferential oxidation of carbon monoxide, has been described.

  5. Polymethacrylate monolithic and hybrid particle-monolithic columns for reversed-phase and hydrophilic interaction capillary liquid chromatography.

    Science.gov (United States)

    Jandera, Pavel; Urban, Jirí; Skeríková, Veronika; Langmaier, Pavel; Kubícková, Romana; Planeta, Josef

    2010-01-01

    We prepared hybrid particle-monolithic polymethacrylate columns for micro-HPLC by in situ polymerization in fused silica capillaries pre-packed with 3-5microm C(18) and aminopropyl silica bonded particles, using polymerization mixtures based on laurylmethacrylate-ethylene dimethacrylate (co)polymers for the reversed-phase (RP) mode and [2-(methacryloyloxy)ethyl]-dimethyl-(3-sulfopropyl) zwitterionic (co)polymers for the hydrophilic interaction (HILIC) mode. The hybrid particle-monolithic columns showed reduced porosity and hold-up volumes, approximately 2-2.5 times lower in comparison to the pure monolithic columns prepared in the whole volume of empty capillaries. The elution volumes of sample compounds are also generally lower in comparison to packed or pure monolithic columns. The efficiency and permeability of the hybrid columns are intermediate in between the properties of the reference pure monolithic and particle-packed columns. The chemistries of the embedded solid particles and of the interparticle monolithic moiety in the hybrid capillary columns contribute to the retention to various degrees, affecting the selectivity of separation. Some hybrid columns provided improved separations of proteins in comparison to the reference particle-packed columns in the reversed-phase mode. Zwitterionic hybrid particle-monolithic columns show dual mode retention HILIC/RP behaviour depending on the composition of the mobile phase and allow separations of polar compounds such as phenolic acids in the HILIC mode at lower concentrations of acetonitrile and, often in shorter analysis time in comparison to particle-packed and full-volume monolithic columns.

  6. Biasable, Balanced, Fundamental Submillimeter Monolithic Membrane Mixer

    Science.gov (United States)

    Siegel, Peter; Schlecht, Erich; Mehdi, Imran; Gill, John; Velebir, James; Tsang, Raymond; Dengler, Robert; Lin, Robert

    2010-01-01

    This device is a biasable, submillimeter-wave, balanced mixer fabricated using JPL s monolithic membrane process a simplified version of planar membrane technology. The primary target application is instrumentation used for analysis of atmospheric constituents, pressure, temperature, winds, and other physical and chemical properties of the atmospheres of planets and comets. Other applications include high-sensitivity gas detection and analysis. This innovation uses a balanced configuration of two diodes allowing the radio frequency (RF) signal and local oscillator (LO) inputs to be separated. This removes the need for external diplexers that are inherently narrowband, bulky, and require mechanical tuning to change frequency. Additionally, this mixer uses DC bias-ability to improve its performance and versatility. In order to solve problems relating to circuit size, the GaAs membrane process was created. As much of the circuitry as possible is fabricated on-chip, making the circuit monolithic. The remainder of the circuitry is precision-machined into a waveguide block that holds the GaAs circuit. The most critical alignments are performed using micron-scale semiconductor technology, enabling wide bandwidth and high operating frequencies. The balanced mixer gets superior performance with less than 2 mW of LO power. This can be provided by a simple two-stage multiplier chain following an amplifier at around 90 GHz. Further, the diodes are arranged so that they can be biased. Biasing pushes the diodes closer to their switching voltage, so that less LO power is required to switch the diodes on and off. In the photo, the diodes are at the right end of the circuit. The LO comes from the waveguide at the right into a reduced-height section containing the diodes. Because the diodes are in series to the LO signal, they are both turned on and off simultaneously once per LO cycle. Conversely, the RF signal is picked up from the RF waveguide by the probe at the left, and flows

  7. Tracking antenna arrays for near-millimeter waves

    Science.gov (United States)

    Tong, P. P.; Neikirk, D. P.; Psaltis, D.; Rutledge, D. B.; Wagner, K.; Young, P. E.

    1983-01-01

    A two-dimensional monolithic array has been developed that gives the elevation and azimuth of point source targets. The array is an arrangement of rows and columns of antennas and bismuth bolometer detectors on a fused quartz substrate. Energy is focused onto the array through a lens placed on the back side of the substrate. At 1.38 mm with a 50 mm diameter objective lens, the array has demonstrated a positioning accuracy of 26 arcmin. In a differential mode this precision improves to 9 arcsec, limited by the mechanics of the rotating stage. This tracking could be automated to a fast two-step procedure where a source is first located to the nearest row and column, and then precisely located by scanning. With signal processing the array should be able to track multiple sources.

  8. Design of a High Resolution, Monolithic Crystal, PET/MRI Detector with DOI Positioning Capability.

    Science.gov (United States)

    Miyaoka, Robert S; Li, Xiaoli; Lockhart, Cate; Lewellen, Tom K

    2008-10-01

    We report on a high resolution, monolithic crystal PET detector design concept that provides depth of interaction (DOI) positioning within the crystal and is compatible for operation in a MRI scanner to support multimodal anatomic and functional imaging. Our design utilizes a novel sensor on the entrance surface (SES) approach combined with a maximum likelihood positioning algorithm. The sensor will be a two-dimensional array of micro-pixel avalanche photodiodes (MAPD). MAPDs are a new type of solid-state photodetector with Geiger mode operation that can provide signal gain similar to a photomltipiler tube (PMT). In addition, they can be operated in high magnetic fields to support PET/MR imaging. Utilizing a multi-step simulation process, we determined the intrinsic spatial resolution characteristics for a variety of detector configurations. The crystal was always modeled as a 48.8 mm by 48.8 mm by 15 mm monolithic slab of a lutetium-based scintillator. The SES design was evaluated via simulation for three different two-dimensional MAPD array sizes: 8×8 with 5.8×5.8 mm(2) pads; 12×12 with 3.8×3.8 mm(2) pads; and 16×16 with 2.8×2.8 mm(2) pads. To reduce the number of signal channels row-column summing readout was explored for the 12×12 and 16×16 channel array devices. The intrinsic spatial resolution for the 8×8 MAPD array is 0.88 mm FWHM in X and Y, and 1.83 mm FWHM in Z (i.e., DOI). Comparing the results versus using a conventional design with the photosensors on the backside of the crystal, an average improvement of ~24% in X and Y and 20% in Z is achieved. The X, Y intrinsic spatial resolution improved to 0.66 mm and 0.65 mm FWHM for the 12×12 and 16×16 MAPDs using row-column readout. Using the 12×12 and 16×16 arrays also led to a slight improvement in the DOI positioning accuracy.

  9. Compact 4-channel AWGs for CWDM and LAN WDM in data center monolithic applications

    Science.gov (United States)

    Pan, Pan; An, Junming; Wang, Yue; Zhang, Jiashun; Wang, Liangliang; Qi, Ying; Han, Qin; Hu, Xiongwei

    2015-12-01

    InP-based 4-channel AWGs for Coarse Wavelength Division Multiplexing (CWDM) with channel spacing of 20 nm and Local Area Network (LAN) WDM with channel spacing of 800 GHz are designed and fabricated. The deep-ridge waveguide is used to make the chip compact, chip size of AWG for CWDM is 0.55×3.9 mm2 and for LAN WDM is 1.6×3 mm2. The measured results indicate that, the insertion losses are -5 dB and -7 dB, crosstalk levels are below -25 dB and -24 dB for AWG with 20 nm channel spacing and 800 GHz channel spacing, respectively. These AWGs can be integrated with lasers and detectors array monolithically for data center applications.

  10. Multiport InP monolithically integrated all-optical wavelength router.

    Science.gov (United States)

    Zheng, Xiu; Raz, Oded; Calabretta, Nicola; Zhao, Dan; Lu, Rongguo; Liu, Yong

    2016-08-15

    An indium phosphide-based monolithically integrated wavelength router is demonstrated in this Letter. The wavelength router has four input ports and four output ports, which integrate four wavelength converters and a 4×4 arrayed-waveguide grating router. Each wavelength converter is achieved based on cross-gain modulation and cross-phase modulation effects in a semiconductor optical amplifier. Error-free wavelength switching for a non-return-to-zero 231-1 ps eudorandom binary sequence at 40 Gb/s data rate is performed. Both 1×4 and 3×1 all-optical routing functions of this chip are demonstrated for the first time with power penalties as low as 3.2 dB.

  11. Fully integrated monolithic opoelectronic transducer for real.time protein and DNA detection

    DEFF Research Database (Denmark)

    Misiakos, Konstatinos; S. Petrou, Panagiota; E. Kakabakos, Sotirios

    2010-01-01

    scheme through a board-to-board receptacle was developed and combined with a portable customized readout and control instrument. Real-time detection of deleterious mutations in BRCA1 gene related to predisposition to hereditary breast/ovarian cancer was performed with the instrument developed using PCR......The development and testing of a portable bioanalytical device which was capable for real-time monitoring of binding assays was demonstrated. The device was based on arrays of nine optoelectronic transducers monolithically integrated on silicon chips. The optocouplers consisted of nine silicon...... products. Detection was based on waveguided photons elimination through interaction with fluorescently labeled PCR products. Detection of single biomolecular binding events was also demonstrated using nanoparticles as labels. In addition, label-free monitoring of bioreactions in real time was achieved...

  12. The Advanced Virgo monolithic fused silica suspension

    Energy Technology Data Exchange (ETDEWEB)

    Aisa, D.; Aisa, S.; Campeggi, C.; Colombini, M. [University of Perugia and INFN Perugia (Italy); Conte, A. [University of Roma Sapienza and INFN Roma (Italy); Farnesini, L. [University of Perugia and INFN Perugia (Italy); Majorana, E.; Mezzani, F. [University of Roma Sapienza and INFN Roma (Italy); Montani, M. [University of Urbino and INFN Firenze (Italy); Naticchioni, L.; Perciballi, M. [University of Roma Sapienza and INFN Roma (Italy); Piergiovanni, F. [University of Urbino and INFN Firenze (Italy); Piluso, A. [University of Perugia and INFN Perugia (Italy); Puppo, P., E-mail: paola.puppo@roma1.infn.it [University of Roma Sapienza and INFN Roma (Italy); Rapagnani, P. [University of Roma Sapienza and INFN Roma (Italy); Travasso, F. [University of Perugia and INFN Perugia (Italy); Vicerè, A. [University of Urbino and INFN Firenze (Italy); Vocca, H. [University of Perugia and INFN Perugia (Italy)

    2016-07-11

    The detection of gravitational waves is one of the most challenging prospects faced by experimental physicists. Suspension thermal noise is an important noise source at operating frequencies between approximately 10 and 30 Hz, and represents a limit to the sensitivity of the ground based interferometric gravitational wave detectors. Its effects can be reduced by minimizing the losses and by optimizing the geometry of the suspension fiber as well as its attachment system. In this proceeding we will describe the mirrors double stage monolithic suspension system to be used in the Advanced Virgo (AdV) detector. We also present the results of the thermal noise study, performed with the help of a finite elements model, taking into account the precise geometry of the fibers attachment systems on the suspension elements. We shall demonstrate the suitability of this suspension for installation in AdV. - Highlights: • Suspension system design for the test masses of the gravitational wave detectors. • Finite element model studies. • Suspension thermal noise studies.

  13. Monolithic supports with unique geometries and enhanced mass transfer.

    Energy Technology Data Exchange (ETDEWEB)

    Stuecker, John Nicholas; Ferrizz, Robert Matthew; Cesarano, Joseph, III; Miller, James Edward

    2004-01-01

    The catalytic combustion of natural gas has been the topic of much research over the past decade. Interest in this technology results from a desire to decrease or eliminate the emissions of harmful nitrogen oxides (NOX) from gas turbine power plants. A low-pressure drop catalyst support, such as a ceramic monolith, is ideal for this high-temperature, high-flow application. A drawback to the traditional honeycomb monoliths under these operating conditions is poor mass transfer to the catalyst surface in the straight-through channels. 'Robocasting' is a unique process developed at Sandia National Laboratories that can be used to manufacture ceramic monoliths with alternative 3-dimensional geometries, providing tortuous pathways to increase mass transfer while maintaining low pressure drops. This report details the mass transfer effects for novel 3-dimensional robocast monoliths, traditional honeycomb-type monoliths, and ceramic foams. The mass transfer limit is experimentally determined using the probe reaction of CO oxidation over a Pt / {gamma}-Al{sub 2}O{sub 3} catalyst, and the pressure drop is measured for each monolith sample. Conversion versus temperature data is analyzed quantitatively using well-known dimensionless mass transfer parameters. The results show that, relative to the honeycomb monolith support, considerable improvement in mass transfer efficiency is observed for robocast samples synthesized using an FCC-like geometry of alternating rods. Also, there is clearly a trade-off between enhanced mass transfer and increased pressure drop, which can be optimized depending on the particular demands of a given application.

  14. Feedhorn-Coupled Transition-Edge Superconducting Bolometer Arrays for Cosmic Microwave Background Polarimetry

    Science.gov (United States)

    Hubmayr, J.; Austermann, J.; Beall, J.; Becker, D.; Cho, H.-M.; Datta, R.; Duff, S. M.; Grace, E.; Halverson, N.; Henderson, S. W.; hide

    2015-01-01

    NIST produces large-format, dual-polarization-sensitive detector arrays for a broad range of frequencies (30-1400 GHz). Such arrays enable a host of astrophysical measurements. Detectors optimized for cosmic microwave background observations are monolithic, polarization-sensitive arrays based on feedhorn and planar Nb antenna-coupled transition-edge superconducting (TES) bolometers. Recent designs achieve multiband, polarimetric sensing within each spatial pixel. In this proceeding, we describe our multichroic, feedhorn-coupled design; demonstrate performance at 70-380 GHz; and comment on current developments for implementation of these detector arrays in the advanced Atacama Cosmology Telescope receiver

  15. Advanced Gasification Mercury/Trace Metal Control with Monolith Traps

    Energy Technology Data Exchange (ETDEWEB)

    Musich, Mark; Swanson, Michael; Dunham, Grant; Stanislowski, Joshua

    2010-10-05

    Two Corning monoliths and a non-carbon-based material have been identified as potential additives for mercury capture in syngas at temperatures above 400°F and pressure of 600 psig. A new Corning monolith formulation, GR-F1-2189, described as an active sample appeared to be the best monolith tested to date. The Corning SR Liquid monolith concept continues to be a strong candidate for mercury capture. Both monolith types allowed mercury reduction to below 5-μg/m{sup 3} (~5 ppb), a current U.S. Department of Energy (DOE) goal for trace metal control. Preparation methods for formulating the SR Liquid monolith impacted the ability of the monolith to capture mercury. The Energy & Environmental Research Center (EERC)-prepared Noncarbon Sorbents 1 and 2 appeared to offer potential for sustained and significant reduction of mercury concentration in the simulated fuel gas. The Noncarbon Sorbent 1 allowed sustained mercury reduction to below 5-μg/m{sup 3} (~5 ppb). The non-carbon-based sorbent appeared to offer the potential for regeneration, that is, desorption of mercury by temperature swing (using nitrogen and steam at temperatures above where adsorption takes place). A Corning cordierite monolith treated with a Group IB metal offered limited potential as a mercury sorbent. However, a Corning carbon-based monolith containing prereduced metallic species similar to those found on the noncarbon sorbents did not exhibit significant or sustained mercury reduction. EERC sorbents prepared with Group IB and IIB selenide appeared to have some promise for mercury capture. Unfortunately, these sorbents also released Se, as was evidenced by the measurement of H2Se in the effluent gas. All sorbents tested with arsine or hydrogen selenide, including Corning monoliths and the Group IB and IIB metal-based materials, showed an ability to capture arsine or hydrogen selenide at 400°F and 600 psig. Based on current testing, the noncarbon metal-based sorbents appear to be the most

  16. ADVANCED GASIFICATION MERCURY/TRACE METAL CONTROL WITH MONOLITH TRAPS

    Energy Technology Data Exchange (ETDEWEB)

    Mark A. Musich; Michael L. Swanson; Grant E. Dunham; Joshua J. Stanislowski

    2010-07-31

    Two Corning monoliths and a non-carbon-based material have been identified as potential additives for mercury capture in syngas at temperatures above 400°F and pressure of 600 psig. A new Corning monolith formulation, GR-F1-2189, described as an active sample appeared to be the best monolith tested to date. The Corning SR Liquid monolith concept continues to be a strong candidate for mercury capture. Both monolith types allowed mercury reduction to below 5-μg/m3 (~5 ppb), a current U.S. Department of Energy (DOE) goal for trace metal control. Preparation methods for formulating the SR Liquid monolith impacted the ability of the monolith to capture mercury. The Energy & Environmental Research Center (EERC)-prepared Noncarbon Sorbents 1 and 2 appeared to offer potential for sustained and significant reduction of mercury concentration in the simulated fuel gas. The Noncarbon Sorbent 1 allowed sustained mercury reduction to below 5-μg/m3 (~5 ppb). The non-carbon-based sorbent appeared to offer the potential for regeneration, that is, desorption of mercury by temperature swing (using nitrogen and steam at temperatures above where adsorption takes place). A Corning cordierite monolith treated with a Group IB metal offered limited potential as a mercury sorbent. However, a Corning carbon-based monolith containing prereduced metallic species similar to those found on the noncarbon sorbents did not exhibit significant or sustained mercury reduction. EERC sorbents prepared with Group IB and IIB selenide appeared to have some promise for mercury capture. Unfortunately, these sorbents also released Se, as was evidenced by the measurement of H2Se in the effluent gas. All sorbents tested with arsine or hydrogen selenide, including Corning monoliths and the Group IB and IIB metal-based materials, showed an ability to capture arsine or hydrogen selenide at 400°F and 600 psig. Based on current testing, the noncarbon metal-based sorbents appear to be the most effective arsine

  17. New Graphene Form of Nanoporous Monolith for Excellent Energy Storage.

    Science.gov (United States)

    Bi, Hui; Lin, Tianquan; Xu, Feng; Tang, Yufeng; Liu, Zhanqiang; Huang, Fuqiang

    2016-01-13

    Extraordinary tubular graphene cellular material of a tetrahedrally connected covalent structure was very recently discovered as a new supermaterial with ultralight, ultrastiff, superelastic, and excellent conductive characteristics, but no high specific surface area will keep it from any next-generation energy storage applications. Herein, we prepare another new graphene monolith of mesoporous graphene-filled tubes instead of hollow tubes in the reported cellular structure. This graphene nanoporous monolith is also composed of covalently bonded carbon network possessing high specific surface area of ∼1590 m(2) g(-1) and electrical conductivity of ∼32 S cm(-1), superior to graphene aerogels and porous graphene forms self-assembled by graphene oxide. This 3D graphene monolith can support over 10 000 times its own weight, significantly superior to CNT and graphene cellular materials with a similar density. Furthermore, pseudocapacitance-active functional groups are introduced into the new nanoporous graphene monolith as an electrode material in electrochemical capacitors. Surprisingly, the electrode of 3D mesoporous graphene has a specific capacitance of 303 F g(-1) and maintains over 98% retention after 10 000 cycles, belonging to the list for the best carbon-based active materials. The macroscopic mesoporous graphene monolith suggests the great potential as an electrode for supercapacitors in energy storage areas.

  18. Recent advances in polymer monoliths for ion-exchange chromatography.

    Science.gov (United States)

    Nordborg, Anna; Hilder, Emily F

    2009-05-01

    The use of polymeric materials in ion-exchange chromatography applications is advantageous because of their typically high mechanical stability and tolerance of a wide range of pH conditions. The possibility of using polymeric monoliths in ion-exchange chromatography is therefore obvious and many of the same strategies developed for polymeric particles have been adapted for use with polymeric monoliths. In this review different strategies for the synthesis of polymeric monoliths with ion-exchange functionality are discussed. The incorporation of ion-exchange functionality by co-polymerization is included, as also are different post-polymerization alterations to the monolith surface such as grafting. The formulations and strategies presented include materials intended for use in analytical separations in ion-exchange chromatography, sample pre-treatment or enrichment applications, and materials for capillary electrochromatography. Finally, examples of the use of polymeric monoliths in ion-exchange chromatography applications are included with examples published in the years 2003 to 2008.

  19. HPLC analysis of synthetic polymers on short monolithic columns.

    Science.gov (United States)

    Maksimova, Elena; Vlakh, Evgenia; Sinitsyna, Ekaterina; Tennikova, Tatiana

    2013-12-01

    Ultrashort monolithic columns (disks) were thoroughly studied as efficient stationary phases for precipitation-dissolution chromatography of synthetic polymers. Gradient elution mode was applied in all chromatographic runs. The mixtures of different flexible chain homopolymers, such as polystyrenes, poly(methyl methacrylates), and poly(tert-butylmethacrylates) were separated according to their molecular weights on both commercial poly(styrene-co-divinylbenzene) disks (12 id × 3 mm and 5 × 5 mm) and lab-made monolithic columns (4.6 id × 50 mm) filled with supports of different hydrophobicity. The experimental conditions were optimized to reach fast and highly efficient separation. It was observed that, similar to the separation of monoliths of other classes of (macro)molecules (proteins, DNA, oligonucleotides), the length of column did not affect the peak resolution. A comparison of the retention properties of the poly(styrene-co-divinylbenzene) disk-shaped monoliths with those based on poly(lauryl methacrylate-co-ethylene dimethacrylate), poly(butyl methacrylate-co-ethylene dimethacrylate), and poly(glycidyl methacrylate-co-ethylene dimethacrylate) supports demonstrated the obvious effect of surface chemistry on the resolution factor. Additionally, the results of the discussed chromatographic mode on the fast determination of the molecular weights of homopolymers used in this study were compared to those established by SEC on columns packed with sorbent beads of a similar nature to the monoliths. © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  20. Edge chipping and flexural resistance of monolithic ceramics☆

    Science.gov (United States)

    Zhang, Yu; Lee, James J.-W.; Srikanth, Ramanathan; Lawn, Brian R.

    2014-01-01

    Objective Test the hypothesis that monolithic ceramics can be developed with combined esthetics and superior fracture resistance to circumvent processing and performance drawbacks of traditional all-ceramic crowns and fixed-dental-prostheses consisting of a hard and strong core with an esthetic porcelain veneer. Specifically, to demonstrate that monolithic prostheses can be produced with a much reduced susceptibility to fracture. Methods Protocols were applied for quantifying resistance to chipping as well as resistance to flexural failure in two classes of dental ceramic, microstructurally-modified zirconias and lithium disilicate glass–ceramics. A sharp indenter was used to induce chips near the edges of flat-layer specimens, and the results compared with predictions from a critical load equation. The critical loads required to produce cementation surface failure in monolithic specimens bonded to dentin were computed from established flexural strength relations and the predictions validated with experimental data. Results Monolithic zirconias have superior chipping and flexural fracture resistance relative to their veneered counterparts. While they have superior esthetics, glass–ceramics exhibit lower strength but higher chip fracture resistance relative to porcelain-veneered zirconias. Significance The study suggests a promising future for new and improved monolithic ceramic restorations, with combined durability and acceptable esthetics. PMID:24139756

  1. Monolithic View of Galaxy Formation and Evolution

    Directory of Open Access Journals (Sweden)

    Cesare Chiosi

    2014-07-01

    Full Text Available We review and critically discuss the current understanding of galaxy formation and evolution limited to Early Type Galaxies (ETGs as inferred from the observational data and briefly contrast the hierarchical and quasi-monolithic paradigms of formation and evolution. Since in Cold Dark Matter (CDM cosmogony small scale structures typically collapse early and form low-mass haloes that subsequently can merge to assembly larger haloes, galaxies formed in the gravitational potential well of a halo are also expected to merge thus assembling their mass hierarchically. Mergers should occur all over the Hubble time and large mass galaxies should be in place only recently. However, recent observations of high redshift galaxies tell a different story: massive ETGs are already in place at high redshift. To this aim, we propose here a revision of the quasi-monolithic scenario as an alternative to the hierarchical one, in which mass assembling should occur in early stages of a galaxy lifetime and present recent models of ETGs made of Dark and Baryonic Matter in a Λ-CDM Universe that obey the latter scheme. The galaxies are followed from the detachment from the linear regime and Hubble flow at z ≥ 20 down to the stage of nearly complete assembly of the stellar content (z ∼ 2 − 1 and beyond.  It is found that the total mass (Mh = MDM + MBM and/or initial over-density of the proto-galaxy drive the subsequent star formation histories (SFH. Massive galaxies (Mh ~ _1012M⊙ experience a single, intense burst of star formation (with rates ≥ 103M⊙/yr at early epochs, consistently with observations, with a weak dependence on the initial over-density; intermediate mass haloes (Mh~_ 1010 − 1011M⊙ have star formation histories that strongly depend on their initial over-density; finally, low mass haloes (Mh ~_ 109M⊙ always have erratic, burst-like star forming histories. The present-day properties (morphology, structure, chemistry and photometry of the

  2. Monolithic Solid Oxide Fuel Cell development

    Science.gov (United States)

    Myles, K. M.; McPheeters, C. C.

    1989-12-01

    The Monolithic Solid Oxide Fuel Cell (MSOFC) is an oxide-ceramic structure in which appropriate electronic and ionic conductors are fabricated in a honeycomb shape similar to a block of corrugated paperboard. These electronic and ionic conductors are arranged to provide short conduction paths to minimize resistive losses. The power density achievable with the MSOFC is expected to be about 8 kW/kg or 4 kW/L, at fuel efficienceis over 50 percent, because of small cell size and low resistive losses in the materials. The MSOFC operates in the range of 700 to 1000 C, at which temperatures rapid reform of hydrocarbon fuels is expected within the nickel-YSZ fuel channels. Tape casting and hot roll calendering are used to fabricate the MSOFC structure. The performance of the MSOFC has improved significantly during the course of development. The limitation of this system, based on materials resistance alone without interfacial resistances, is 0.093 ohm-sq cm area-specific resistance (ASR). The current typical performance of MSOFC single cells is characterized by ASRs of about 0.4 to 0.5 ohm-sq cm. With further development the ASR is expected to be reduced below 0.2 ohm-sq cm, which will result in power levels greater than 1.4 W/sq cm. The feasibility of the MSOFC concept was proven, and the performance was dramatically improved. The differences in thermal expansion coefficients and firing shrinkages among the fuel cell materials were minimized. As a result of good matching of these properties, the MSOFC structure was successfully fabricated with few defects, and the system shows excellent promise for development into a practical power source.

  3. Monolithic series-connected gallium arsenide converter development

    Energy Technology Data Exchange (ETDEWEB)

    Spitzer, M.B.; McClelland, R.W.; Dingle, B.D.; Dingle, J.E.; Hill, D.S. (Kopin Corp., Taunton, MA (United States)); Rose, B.H. (Sandia National Labs., Albuquerque, NM (United States))

    1991-01-01

    We report the development of monolithic GaAs photovoltaic devices intended to convert light generated by a laser or other bright source to electricity. The converters described here can provide higher operating voltage than is possible using a single-junction converter, owing to use of a monolithic circuit that forms a planar series-connected string of single-junction sub-cells. This planar monolithic circuit is arranged to deliver the desired voltage and current during operation at the maximum power point. The paper describes two-, six-, and twelve-junction converters intended for illumination by a laser diode with a wavelength of 0.8 {mu}m. Design and characterization data are presented for optical power in the range of 100 mW to 1 W. The best conversion efficiency exceeds 50%. 9 refs., 4 figs., 2 tabs.

  4. Design of Monolithic Integrator for Strain-to-Frequency Converter

    Directory of Open Access Journals (Sweden)

    Tuan Mohd. Khairi Tuan Mat

    2012-01-01

    Full Text Available Strain-to-Frequency converter (SFC is a one of the analog conditioner tools that converts any strain signal to the frequency signal. The basic concept of SFC is by detecting any changing of strains, then converting the strain to the voltage signal and converting the voltage signal to the frequency signal. This tool consists of 3 main  components which are strain gauge, differential integrator and comparator. This paper presents the designing and analysis of monolithic integrator that to be used in the Strain-toFrequency converter. The primary goal is to design and simulate the performance of monolithic integrator for SFC using GATEWAY Silvaco Electronic Design Automation (S EDA tools and EXPERT software. The performances of SFC using the designed monolithic integrator are also investigated.

  5. Molecularly imprinted macroporous monolithic materials for protein recognition

    Institute of Scientific and Technical Information of China (English)

    Qi Liang Deng; Yan Li Li; Li Hua Zhang; Yu Kui Zhang

    2011-01-01

    Synthetic materials that can specifically recognize proteins will find wide application in many fields. In this report, bovine serum albumin was chosen as the template protein. Acrylamide and N, N'-methylenebisacrylamide were employed as the functional and cross-linker monomers, respectively. Molecularly imprinted macroporous monolithic materials that can preferentially bind the template protein in an aqueous environment were prepared by combination of molecular imprinting technique and freezing/thawing preparation method. The resulted imprinted macroporous monolithic columns were evaluated by utilizing as stationary phase in high performance liquid chromatography and solid-phase extraction materials. The experimental results indicated that the imprinted macroporous monolithic column exhibited good recognition for template protein, as compared with the control protein (hemoglobin), whereas the non-imprinted polymer (prepared under the same conditions except without addition template protein) had no selective properties.

  6. A Possible Astronomically Aligned Monolith at Gardom's Edge

    Science.gov (United States)

    Brown, Daniel; Alder, Andy; Bemand, Elizabeth

    2015-05-01

    A unique triangular shaped monolith located within the Peak District National Park at Gardom's Edge could be intentionally astronomically aligned. It is set within a landscape rich in late Neolithic and Bronze Age remains. We show that the stone is most likely in its original orientation owing to its clear signs of erosion and associated to the time period of the late Neolithic. It is tilted towards south and its north side slopes at an angle equal to the maximum altitude of the Sun at mid-summer. This alignment emphasizes the changing declinations of the Sun during the seasons as well as giving an indication of mid-summers day. This functionality is achieved by an impressive display of light and shadow on the north facing side of the monolith. Together with other monuments in the close vicinity the monolith would have represented an ideal marker or social arena for seasonal gatherings for the otherwise dispersed small communities.

  7. Preliminary shielding analysis for the CSNS target station monolith

    Institute of Scientific and Technical Information of China (English)

    张斌; 陈义学; 杨寿海; 吴军; 殷雯; 梁天骄; 贾学军

    2010-01-01

    The construction of the China Spallation Neutron Source (CSNS) has been initiated at Dongguan,Guangdong,China.In spallation neutron sources the target station monolith is contaminated by a large number of fast neutrons whose energies can be as large as those of the protons of the proton beam directed towards the tungsten target.A detailed radiation transport analysis of the target station monolith is important for the construction of the CSNS.The analysis is performed using the coupled Monte Carlo and multi-dimensional discrete ordinates method.Successful elimination of the primary ray effects via the two-dimensional uncollided flux and first collision source methodology is also illustrated.The dose at the edge of the monolith is calculated.The results demonstrate that the doses received by the hall staff members are below the required standard limit.

  8. Monolithic fuel cell based power source for burst power generation

    Science.gov (United States)

    Fee, D. C.; Blackburn, P. E.; Busch, D. E.; Dees, D. W.; Dusek, J.; Easler, T. E.; Ellingson, W. A.; Flandermeyer, B. K.; Fousek, R. J.; Heiberger, J. J.

    A unique fuel cell coupled with a low power nuclear reactor presents an attractive approach for SDI burst power requirements. The monolithic fuel cell looks attractive for space applications and represents a quantum jump in fuel cell technology. Such a breakthrough in design is the enabling technology for lightweight, low volume power sources for space based pulse power systems. The monolith is unique among fuel cells in being an all solid state device. The capability for miniaturization, inherent in solid state devices, gives the low volume required for space missions. In addition, the solid oxide fuel cell technology employed in the monolith has high temperature reject heat and can be operated in either closed or open cycles. Both these features are attractive for integration into a burst power system.

  9. A Possible Astronomically Aligned Monolith at Gardom's Edge

    CERN Document Server

    Brown, D; Bemand, E

    2012-01-01

    A unique triangular shaped monolith located within the Peak District National Park at Gardom's Edge could be intentionally astronomically aligned. It is set within a landscape rich in late Neolithic and Bronze Age remains. We show that the stone is most likely in its original orientation owing to its clear signs of erosion and associated to the time period of the late Neolithic. It is tilted towards South and its North side slopes at an angle equal to the maximum altitude of the Sun at mid-summer. This alignment emphasizes the changing declinations of the Sun during the seasons as well as giving an indication of mid-summers day. This functionality is achieved by an impressive display of light and shadow on the North-facing side of the Monolith. Together with other monuments in the close vicinity the monolith would have represented an ideal marker or social arena for seasonal gatherings for the else dispersed small communities.

  10. MONOLITHIC FUEL FABRICATION PROCESS DEVELOPMENT AT THE IDAHO NATIONAL LABORATORY_

    Energy Technology Data Exchange (ETDEWEB)

    G. A. Moore; F. J. Rice; N. E. Woolstenhulme; J-F. Jue; B. H. Park; S. E. Steffler; N. P. Hallinan; M. D. Chapple; M. C. Marshall; B. L. Mackowiak; C. R. Clark; B. H. Rabin

    2009-11-01

    Full-size/prototypic U10Mo monolithic fuel-foils and aluminum clad fuel plates are being developed at the Idaho National Laboratory’s (INL) Materials and Fuels Complex (MFC). These efforts are focused on realizing Low Enriched Uranium (LEU) high density monolithic fuel plates for use in High Performance Research and Test Reactors. The U10Mo fuel foils under development afford a fuel meat density of ~16 gU/cc and thus have the potential to facilitate LEU conversions without any significant reactor-performance penalty. An overview is provided of the ongoing monolithic UMo fuel development effort, including application of a zirconium barrier layer on fuel foils, fabrication scale-up efforts, and development of complex/graded fuel foils. Fuel plate clad bonding processes to be discussed include: Hot Isostatic Pressing (HIP) and Friction Bonding (FB).

  11. Filter arrays

    Energy Technology Data Exchange (ETDEWEB)

    Page, Ralph H.; Doty, Patrick F.

    2017-08-01

    The various technologies presented herein relate to a tiled filter array that can be used in connection with performance of spatial sampling of optical signals. The filter array comprises filter tiles, wherein a first plurality of filter tiles are formed from a first material, the first material being configured such that only photons having wavelengths in a first wavelength band pass therethrough. A second plurality of filter tiles is formed from a second material, the second material being configured such that only photons having wavelengths in a second wavelength band pass therethrough. The first plurality of filter tiles and the second plurality of filter tiles can be interspersed to form the filter array comprising an alternating arrangement of first filter tiles and second filter tiles.

  12. Preparation of poly(γ-glutamic acid)/hydroxyapatite monolith via biomineralization for bone tissue engineering.

    Science.gov (United States)

    Park, Sung-Bin; Hasegawa, Urara; van der Vlies, André J; Sung, Moon-Hee; Uyama, Hiroshi

    2014-01-01

    A hybrid monolith of poly(γ-glutamic acid) and hydroxyapatite (PGA/HAp monolith) was prepared via biomineralization and used as a macroporous cell scaffold in bone tissue engineering. The PGA monolith having a bimodal pore size distribution was used as a substrate to induce biomineralization. The PGA/HAp monolith was obtained by immersing the PGA monolith in simulated body fluid. Pretreatment with CaCl2 enhanced the apatite-forming ability of the PGA monolith. Murine osteoblastic MC3T3-E1 cells efficiently attached and proliferated on the PGA/HAp monolith. MTT assay showed that both the PGA and PGA/HAp monolith did not have apparent cytotoxicity. Moreover, the PGA and PGA/HAp monoliths adsorbed bone morphogenetic protein-2 (BMP-2) by electrostatic interaction which was slowly released in the medium during cell culture. The PGA/HAp monolith enhanced BMP-2 induced alkaline phosphatase activity compared to the PGA monolith and a polystyrene culture plate. Thus, these PGA/HAp monoliths may have potential in bone tissue engineering.

  13. IRAN: interferometric remapped array nulling

    Science.gov (United States)

    Aristidi, Eric; Vakili, Farrokh; Abe, Lyu; Belu, Adrian; Lopez, Bruno; Lanteri, Henri; Schutz, A.; Menut, Jean-Luc

    2004-10-01

    This paper describes a method of beam-combination in the so-called hypertelescope imaging technique recently introduced by Labeyrie in optical interferometry. The method we propose is an alternative to the Michelson pupil reconfiguration that suffers from the loss of the classical object-image convolution relation. From elementary theory of Fourier optics we demonstrate that this problem can be solved by observing in a combined pupil plane instead of an image plane. The point-source intensity distribution (PSID) of this interferometric "image" tends towards a psuedo Airy disc (similar to that of a giant monolithic telescope) for a sufficiently large number of telescopes. Our method is applicable to snap-shot imaging of extended sources with a field comparable to the Airy pattern of single telescopes operated in a co-phased multi-aperture interferometric array. It thus allows to apply conveniently pupil plane coronagraphy. Our technique called Interferometric Remapped Array Nulling (IRAN) is particularly suitable for high dynamic imaging of extra-solar planetary companions, circumstellar nebulosities or extra-galactic objects where long baseline interferometry would closely probe the central regions of AGNs for instance.

  14. Numerical Simulation of Fluid Dynamics in a Monolithic Column

    Directory of Open Access Journals (Sweden)

    Kazuhiro Yamamoto

    2017-01-01

    Full Text Available As for the measurement of polycyclic aromatic hydrocarbons (PAHs, ultra-performance liquid chromatography (UPLC is used for PAH identification and densitometry. However, when a solvent containing a substance to be identified passes through a column of UPLC, a dedicated high-pressure-proof device is required. Recently, a liquid chromatography instrument using a monolithic column technology has been proposed to reduce the pressure of UPLC. The present study tested five types of monolithic columns produced in experiments. To simulate the flow field, the lattice Boltzmann method (LBM was used. The velocity profile was discussed to decrease the pressure drop in the ultra-performance liquid chromatography (UPLC system.

  15. A Monolithic Oxide-Based Transversal Thermoelectric Energy Harvester

    Science.gov (United States)

    Teichert, S.; Bochmann, A.; Reimann, T.; Schulz, T.; Dreßler, C.; Udich, S.; Töpfer, J.

    2016-03-01

    We report the fabrication and properties of a monolithic transversal thermoelectric energy harvester based on the combination of a thermoelectric oxide and a metal. The fabrication of the device is done with a ceramic multilayer technology using printing and co-firing processes. Five transversal devices were combined to a meander-like thermoelectric generator. Electrical measurements and finite element calculations were performed to characterize the resulting thermoelectric generator. A maximum experimental electrical power output of 30.2 mW at a temperature difference of {Δ }T = 208 K was found. The prepared monolithic thermoelectric generator provides at {Δ }T = 35 K sufficient energy to drive a simple electronic sensor application.

  16. Monolithic Michelson Interferometer as ultra stable wavelength reference

    Science.gov (United States)

    Wan, Xiaoke; Ge, Jian

    2010-07-01

    Ultra-stable Monolithic Michelson interferometer can be an ideal reference for highprecision applications such as RV measurement in planet searching and orbit study. The advantages include wide wavelength range, simple sinusoidal spectral format, and high optical efficiency. In this paper, we report that a monolithic Michelson interferometers has been in-house developed with minimized thermal sensitivity with compensation tuning. With a scanning white light interferometer, the thermal sensitivity is measured ~ 6x10-7/°C at 550 nm and it decreases to zero near 1000 nm. We expect the wideband wavelength reference source to be stabilized better than 0.3 m/s for RV experiments

  17. Synthesis of ZSM-5 Monoliths with Hierarchical Porosity

    Institute of Scientific and Technical Information of China (English)

    Tong Yangchuan; Zhao Tianbo; Li Fengyan; Zong Baoning; Wang Yue

    2006-01-01

    A new route to synthesize ZSM-5 monoliths with hierarchical pore structure has been referred to in this stud y. The successful incorporation of the macropores and mesopores within the ZSM-5 structure was achieved through transforming the skeleton of the macroporous silica gel into zeolite ZSM-5 using carbon materials as the transitional template. The ZSM-5 crystal covered part of the macroporous material, and provided micropores to the macroporous silica gel. The structure of carbon monolith was studied after dissolving the silica contained in the carbon/silica composite.

  18. Lectin-carbohydrate interactions on nanoporous gold monoliths.

    Science.gov (United States)

    Tan, Yih Horng; Fujikawa, Kohki; Pornsuriyasak, Papapida; Alla, Allan J; Ganesh, N Vijaya; Demchenko, Alexei V; Stine, Keith J

    2013-07-01

    Monoliths of nanoporous gold (np-Au) were modified with self-assembled monolayers of octadecanethiol (C18-SH), 8-mercaptooctyl α-D-mannopyranoside (αMan-C8-SH), and 8-mercapto-3,6-dioxaoctanol (HO-PEG2-SH), and the loading was assessed using thermogravimetric analysis (TGA). Modification with mixed SAMs containing αMan-C8-SH (at a 0.20 mole fraction in the SAM forming solution) with either octanethiol or HO-PEG2-SH was also investigated. The np-Au monoliths modified with αMan-C8-SH bind the lectin Concanavalin A (Con A), and the additional mass due to bound protein was assessed using TGA analysis. A comparison of TGA traces measured before and after exposure of HO-PEG2-SH modified np-Au to Con A showed that the non-specific binding of Con A was minimal. In contrast, np-Au modified with octanethiol showed a significant mass loss due to non-specifically adsorbed Con A. A significant mass loss was also attributed to binding of Con A to bare np-Au monoliths. TGA revealed a mass loss due to the binding of Con A to np-Au monoliths modified with pure αMan-C8-SH. The use of mass losses determined by TGA to compare the binding of Con A to np-Au monoliths modified by mixed SAMs of αMan-C8-SH and either octanethiol or HO-PEG2-SH revealed that binding to mixed SAM modified surfaces is specific for the mixed SAMs with HO-PEG2-SH but shows a significant contribution from non-specific adsorption for the mixed SAMs with octanethiol. Minimal adsorption of immunoglobulin G (IgG) and peanut agglutinin (PNA) towards the mannoside modified np-Au monoliths was demonstrated. A greater mass loss was found for Con A bound onto the monolith than for either IgG or PNA, signifying that the mannose presenting SAMs in np-Au retain selectivity for Con A. TGA data also provide evidence that Con A bound to the αMan-C8-SH modified np-Au can be eluted by flowing a solution of methyl α-D-mannopyranoside through the structure. The presence of Con A proteins on the modified np-Au surface was

  19. Paladin Enterprises: Monolithic particle physics models global climate.

    CERN Multimedia

    2002-01-01

    Paladin Enterprises presents a monolithic particle model of the universe which will be used by them to build an economical fusion energy system. The model is an extension of the work done by James Clerk Maxwell. Essentially, gravity is unified with electro-magnetic forces and shown to be a product of a closed loop current system, i.e. a particle - monolithic or sub atomic. This discovery explains rapid global climate changes which are evident in the geological record and also provides an explanation for recent changes in the global climate.

  20. Polyurea-Based Aerogel Monoliths and Composites

    Science.gov (United States)

    Lee, Je Kyun

    2012-01-01

    aerogel insulation material was developed that will provide superior thermal insulation and inherent radiation protection for government and commercial applications. The rubbery polyureabased aerogel exhibits little dustiness, good flexibility and toughness, and durability typical of the parent polyurea polymer, yet with the low density and superior insulation properties associated with aerogels. The thermal conductivity values of polyurea-based aerogels at lower temperature under vacuum pressures are very low and better than that of silica aerogels. Flexible, rubbery polyurea-based aerogels are able to overcome the weak and brittle nature of conventional inorganic and organic aerogels, including polyisocyanurate aerogels, which are generally prepared with the one similar component to polyurethane rubber aerogels. Additionally, with higher content of hydrogen in their structures, the polyurea rubber-based aerogels will also provide inherently better radiation protection than those of inorganic and carbon aerogels. The aerogel materials also demonstrate good hydrophobicity due to their hydrocarbon molecular structure. There are several strategies to overcoming the drawbacks associated with the weakness and brittleness of silica aerogels. Development of the flexible fiber-reinforced silica aerogel composite blanket has proven to be one promising approach, providing a conveniently fielded form factor that is relatively robust in industrial environments compared to silica aerogel monoliths. However, the flexible, silica aerogel composites still have a brittle, dusty character that may be undesirable, or even intolerable, in certain application environments. Although the cross - linked organic aerogels, such as resorcinol- formaldehyde (RF), polyisocyanurate, and cellulose aerogels, show very high impact strength, they are also very brittle with little elongation (i.e., less rubbery). Also, silica and carbon aerogels are less efficient radiation shielding materials due

  1. Constitutive Theory Developed for Monolithic Ceramic Materials

    Science.gov (United States)

    Janosik, Lesley A.

    1998-01-01

    with these service conditions by developing a multiaxial viscoplastic constitutive model that accounts for time-dependent hereditary material deformation (such as creep and stress relaxation) in monolithic structural ceramics. Using continuum principles of engineering mechanics, we derived the complete viscoplastic theory from a scalar dissipative potential function.

  2. Chromatographic comparison of bupivacaine imprinted polymers prepared in crushed monolith, microsphere, silica-based composite and capillary monolith formats.

    Science.gov (United States)

    Oxelbark, Joakim; Legido-Quigley, Cristina; Aureliano, Carla S A; Titirici, Maria-Magdalena; Schillinger, Eric; Sellergren, Börje; Courtois, Julien; Irgum, Knut; Dambies, Laurent; Cormack, Peter A G; Sherrington, David C; De Lorenzi, Ersilia

    2007-08-10

    A comprehensive comparison of five chromatographic stationary phases based on molecularly imprinted polymers is presented. Efficiency, imprinting factors, water compatibility and batch-to-batch reproducibility are discussed for crushed monolith, microspheres, two silica-based composites and capillary monoliths, all imprinted with the local anaesthetic bupivacaine. Synthesis protocol and chromatographic test conditions have been kept fixed within certain limits, in order to provide further insight into the strengths and weaknesses of the different formats. Excluding microparticles, all formats give satisfactory performance, especially in aqueous mobile phases. An assessment of batch-to-batch reproducibility in different mobile phases adds further value to this comparison study.

  3. High-power laser arrays with 100% fill factor emission facet

    Science.gov (United States)

    Yanson, Dan A.; McDougall, Stewart D.; Qiu, Bocang; Loyo-Maldonado, Valentin; Bacchin, Gianluca; Robertson, Stephen; Bon, Sébastien; Marsh, John H.

    2008-02-01

    Novel types of laser diode array with a 100% filling factor at the emission facet are reported. The arrays utilize both parallel and tapered cavity emitters that are connected via a common Laterally Unconfined Non-Absorbing Mirror (LUNAM) defined with quantum-well intermixing technology at 808 nm wavelength. Two LUNAM array types are considered: incoherent (weakly coupled) and coherent (diffraction coupled). Incoherent LUNAM arrays benefit from a reduced power density at the facet, improving reliability, and a near-uniform intensity distribution across the array aperture. Stacked laser diode arrays built with LUNAM bars deliver 950 W power under QCW operation with monolithically integrated LUNAM Talbot cavity. The devices produce a single-lobed horizontal far-field pattern over a limited current range with <10% slope efficiency penalty compared to an uncoupled case. The LUNAM arrays are promising candidates for high-power, high-brightness and high-reliability operation.

  4. Single-mode electrically pumped GaSb-based VCSELs emitting continuous-wave at 2.4 and 2.6 {mu}m

    Energy Technology Data Exchange (ETDEWEB)

    Bachmann, Alexander; Arafin, Shamsul; Kashani-Shirazi, Kaveh [Walter Schottky Institut, Technische Universitaet Muenchen, Am Coulombwall 3, 85748 Garching (Germany)], E-mail: bachmann@wsi.tum.de

    2009-12-15

    Vertical-cavity surface-emitting lasers (VCSELs) are perfect light sources for spectroscopic applications, where properties such as continuous-wave (cw) operation, single-mode emission, high lifetime and often low power consumption are crucial. For applications such as tunable diode laser absorption spectroscopy (TDLAS), there is a growing interest in laser devices emitting in the near- to mid-infrared wavelength range, where many environmentally and technologically important gases show strong absorption lines. The (AlGaIn)(AsSb) material system based on GaSb is the material of choice for covering the 2.0-3.3 {mu}m range. In this paper, we report on electrically pumped single-mode VCSELs with emission wavelengths of 2.4 and 2.6 {mu}m, operating cw at room temperature and beyond. By (electro-) thermal tuning, the emission wavelength can be tuned mode-hop free over a range of several nanometers. In addition, low threshold currents of several milliamperes promise mobile application. In the devices, a structured buried tunnel junction with subsequent overgrowth has been used in order to achieve efficient current confinement, reduced optical losses and increased electrical conductivity. Furthermore, strong optical confinement is introduced in the lasers due to laterally differing cavity lengths.

  5. A radiation hard bipolar monolithic front-end readout

    CERN Document Server

    Baschirotto, A; Cappelluti, I; Castello, R; Cermesoni, M; Gola, A; Pessina, G; Pistolesi, E; Rancoita, P G; Seidman, A

    1999-01-01

    A fast bipolar monolithic charge sensitive preamplifier (CSP), implemented in the monolithic 2 mu m BiCMOS technology (called HF2CMOS) was designed and built in a quad monolithic chip. Studies of radiation effects in the CSP $9 performance, from non-irradiated and up to neutron irradiation of 5.3*10/sup 14/ n/cm/sup 2/, have confirmed that the use of bipolar npn transistors is suitable for the radiation level of the future LHC collider environment. The CSP $9 presents a new circuit solution for obtaining adequate slew rate performances which results in an integral linearity better than 0.8554330n 5 V at 20 ns of shaping time, regardless of the bias current selected for the CSP. This way $9 the bias current of the CSP can be set for optimizing the power dissipation with respect to series and parallel noise, especially useful when the CSP is put in a radiation environment. A prototype test with a novel monolithic 20 ns $9 time constant RC-CR shaper, capable to sum up four inputs has been also realized, featurin...

  6. Carbon monolith: preparation, characterization and application as microextraction fiber.

    Science.gov (United States)

    Shi, Zhi-Guo; Chen, Fei; Xing, Jun; Feng, Yu-Qi

    2009-07-10

    A carbon monolith was synthesized via a polymerization-carbonization method, styrene and divinylbenzene being adopted as precursors and dodecanol as a porogen during polymerization. The resultant monolith had bimodal porous substructure, narrowly distributed nano skeleton pores and uniform textural pores or throughpores. The carbon monolith was directly used as an extracting fiber, taking place of the coated silica fibers in commercially available solid-phase microextraction device, for the extraction of phenols followed by gas chromatography-mass spectrometry. Under the studied conditions, the calibration curves were linear from 0.5 to 50 ng mL(-1) for phenol, o-nitrophenol, 2,4-dichlorophenol and p-chlorophenol. The limits of detection were between 0.04 and 0.43 ng mL(-1). The recoveries of the phenols spiked in real water samples at 10 ng mL(-1) were between 85% and 98% with the relative standard deviations below 10%. Compared with the commercial coated ones (e.g. PDMS, CW/DVB and DVB/CAR/PDMS), the carbon monolith-based fiber had advantages of faster extraction equilibrium and higher extraction capacity due to the superior pore connectivity and pore openness resulting from its bimodal porous substructure.

  7. Shear bond strength of indirect composite material to monolithic zirconia

    Science.gov (United States)

    2016-01-01

    PURPOSE This study aimed to evaluate the effect of surface treatments on bond strength of indirect composite material (Tescera Indirect Composite System) to monolithic zirconia (inCoris TZI). MATERIALS AND METHODS Partially stabilized monolithic zirconia blocks were cut into with 2.0 mm thickness. Sintered zirconia specimens were divided into different surface treatment groups: no treatment (control), sandblasting, glaze layer & hydrofluoric acid application, and sandblasting + glaze layer & hydrofluoric acid application. The indirect composite material was applied to the surface of the monolithic zirconia specimens. Shear bond strength value of each specimen was evaluated after thermocycling. The fractured surface of each specimen was examined with a stereomicroscope and a scanning electron microscope to assess the failure types. The data were analyzed using one-way analysis of variance (ANOVA) and Tukey LSD tests (α=.05). RESULTS Bond strength was significantly lower in untreated specimens than in sandblasted specimens (P<.05). No difference between the glaze layer and hydrofluoric acid application treated groups were observed. However, bond strength for these groups were significantly higher as compared with the other two groups (P<.05). CONCLUSION Combined use of glaze layer & hydrofluoric acid application and silanization are reliable for strong and durable bonding between indirect composite material and monolithic zirconia. PMID:27555895

  8. Cyclodextrin-Functionalized Monolithic Capillary Columns: Preparation and Chiral Applications.

    Science.gov (United States)

    Adly, Frady G; Antwi, Nana Yaa; Ghanem, Ashraf

    2016-02-01

    In this review, the recently reported approaches for the preparation of cyclodextrin-functionalized capillary monolithic columns are highlighted, with few applications in chiral separations using capillary liquid chromatography (CLC) and capillary electrochromatography (CEC). Chirality 28:97-109, 2016. © 2015 Wiley Periodicals, Inc.

  9. Monolithic natural gas storage delivery system based on sorbents

    Energy Technology Data Exchange (ETDEWEB)

    Hornbostel, Marc; Krishnan, Gopala N.; Sanjurjo, Angel

    2016-09-27

    The invention provides methods for producing a strong, light, sorbent-based storage/dispenser system for gases and fuels. The system comprises a porous monolithic material with an adherent strong impervious skin that is capable of storing a gas under pressure in a safe and usable manner.

  10. Monolithic natural gas storage delivery system based on sorbents

    Energy Technology Data Exchange (ETDEWEB)

    Hornbostel, Marc; Krishnan, Gopala N.; Sanjurjo, Angel

    2016-09-27

    The invention provides methods for producing a strong, light, sorbent-based storage/dispenser system for gases and fuels. The system comprises a porous monolithic material with an adherent strong impervious skin that is capable of storing a gas under pressure in a safe and usable manner.

  11. Multiple Quantum Well (MQW) Devices For Monolithic Integrated Optoelectronics

    Science.gov (United States)

    Wood, Thomas H.

    1988-05-01

    Semiconductor MQWs represent a new technology for opto-electronics. These MQWs have an electroabsorption effect approximately 50 times larger than conventional semiconductors. They are compatible with existing source and detector material systems and produce devices that are compact and high speed, which makes them useful for monolithic integrated optoelectronic devices.

  12. Morphosynthesis of cubic silver cages on monolithic activated carbon.

    Science.gov (United States)

    Wang, Fei; Zhao, Hong; Lai, Yijian; Liu, Siyu; Zhao, Binyuan; Ning, Yuesheng; Hu, Xiaobin

    2013-11-14

    Cubic silver cages were prepared on monolithic activated carbon (MAC) pre-absorbed with Cl(-), SO4(2-), or PO4(3-) anions. Silver insoluble salts served as templates for the morphosynthesis of silver cages. The silver ions were reduced by reductive functional groups on MAC micropores through a galvanic cell reaction mechanism.

  13. 3D-Printed MOF Monoliths for Gas Adsorption Processes.

    Science.gov (United States)

    Thakkar, Harshul; Eastman, Stephen; Al-Naddaf, Qasim; Rownaghi, Ali Asghar; Rezaei, Fateme

    2017-09-27

    Metal-Organic Frameworks (MOFs) have shown promising performance in separation, adsorption, reaction and storage of various industrial gases, however, their large-scale applications have been hampered by the lack of a proper strategy to formulate them into scalable gas-solid contactors. Herein, we report fabrication of MOF monoliths using 3D printing technique and evaluation of their adsorptive performance in CO2 removal from air. The 3D-printed MOF-74(Ni) and UTSA-16(Co) monoliths with MOF loadings as high as 80 and 85 wt %, respectively were developed and their physical and structural properties were characterized and compared with those of MOF powders. Our adsorption experiments showed that upon exposure to 5,000 ppm (0.5%) CO2 at 25 ºC, the MOF-74(Ni) and UTSA-16(Co) monoliths can adsorb CO2 with the uptake capacity of 1.35 and 1.31 mmol/g, respectively, which are 79 and 87% of the capacity of their MOF analogues under the same conditions. Furthermore, a stable performance was obtained for self-standing 3D-printed monolithic structures with relatively good adsorption kinetics. The preliminary findings reported in this investigation highlight the advantage of robocasting (3D printing) technique for shaping MOF materials into practical configurations that are suitable for various gas separation applications.

  14. From 1D to 3D - macroscopic nanowire aerogel monoliths.

    Science.gov (United States)

    Cheng, Wei; Rechberger, Felix; Niederberger, Markus

    2016-08-01

    Here we present a strategy to assemble one-dimensional nanostructures into a three-dimensional architecture with macroscopic size. With the assistance of centrifugation, we successfully gel ultrathin W18O49 nanowires with diameters of 1 to 2 nm and aspect ratios larger than 100 into 3D networks, which are transformed into monolithic aerogels by supercritical drying.

  15. Position and time resolution measurements with a microchannel plate image intensifier: A comparison of monolithic and pixelated CeBr{sub 3} scintillators

    Energy Technology Data Exchange (ETDEWEB)

    Ackermann, Ulrich, E-mail: ulrich.ackermann@unibw.de [Universität der Bundeswehr München, Institut für angewandte Physik und Messtechnik (LRT2), Werner-Heisenberg-Weg 39, 85577 Neubiberg (Germany); Eschbaumer, Stephan, E-mail: stephan.eschbaumer@unibw.de [Universität der Bundeswehr München, Institut für angewandte Physik und Messtechnik (LRT2), Werner-Heisenberg-Weg 39, 85577 Neubiberg (Germany); Bergmaier, Andreas, E-mail: andreas.bergmaier@unibw.de [Universität der Bundeswehr München, Institut für angewandte Physik und Messtechnik (LRT2), Werner-Heisenberg-Weg 39, 85577 Neubiberg (Germany); Egger, Werner, E-mail: werner.egger@unibw.de [Universität der Bundeswehr München, Institut für angewandte Physik und Messtechnik (LRT2), Werner-Heisenberg-Weg 39, 85577 Neubiberg (Germany); Sperr, Peter, E-mail: peter.sperr@unibw.de [Universität der Bundeswehr München, Institut für angewandte Physik und Messtechnik (LRT2), Werner-Heisenberg-Weg 39, 85577 Neubiberg (Germany); Greubel, Christoph, E-mail: christoph.greubel@unibw.de [Universität der Bundeswehr München, Institut für angewandte Physik und Messtechnik (LRT2), Werner-Heisenberg-Weg 39, 85577 Neubiberg (Germany); and others

    2016-07-01

    To perform Four Dimensional Age Momentum Correlation measurements in the near future, where one obtains the positron lifetime in coincidence with the three dimensional momentum of the electron annihilating with the positron, we have investigated the time and position resolution of two CeBr{sub 3} scintillators (monolithic and an array of pixels) using a Photek IPD340/Q/BI/RS microchannel plate image intensifier. The microchannel plate image intensifier has an active diameter of 40 mm and a stack of two microchannel plates in chevron configuration. The monolithic CeBr{sub 3} scintillator was cylindrically shaped with a diameter of 40 mm and a height of 5 mm. The pixelated scintillator array covered the whole active area of the microchannel plate image intensifier and the shape of each pixel was 2.5·2.5·8 mm{sup 3} with a pixel pitch of 3.3 mm. For the monolithic setup the measured mean single time resolution was 330 ps (FWHM) at a gamma energy of 511 keV. No significant dependence on the position was detected. The position resolution at the center of the monolithic scintillator was about 2.5 mm (FWHM) at a gamma energy of 662 keV. The single time resolution of the pixelated crystal setup reached 320 ps (FWHM) in the region of the center of the active area of the microchannel plate image intensifier. The position resolution was limited by the cross-section of the pixels. The gamma energy for the pixel setup measurements was 511 keV.

  16. Design, development, fabrication and delivery of register and multiplexer units. [CMOS monolithic chip development

    Science.gov (United States)

    Feller, A.; Lombardi, T.

    1978-01-01

    Several approaches for implementing the register and multiplexer unit into two CMOS monolithic chip types were evaluated. The CMOS standard cell array technique was selected and implemented. Using this design automation technology, two LSI CMOS arrays were designed, fabricated, packaged, and tested for proper static, functional, and dynamic operation. One of the chip types, multiplexer register type 1, is fabricated on a 0.143 x 0.123 inch chip. It uses nine standard cell types for a total of 54 standard cells. This involves more than 350 transistors and has the functional equivalent of 111 gates. The second chip, multiplexer register type 2, is housed on a 0.12 x 0.12 inch die. It uses 13 standard cell types, for a total of 42 standard cells. It contains more than 300 transistors, the functional equivalent of 112 gates. All of the hermetically sealed units were initially screened for proper functional operation. The static leakage and the dynamic leakage were measured. Dynamic measurements were made and recorded. At 10 V, 14 megabit shifting rates were measured on multiplexer register type 1. At 5 V these units shifted data at a 6.6 MHz rate. The units were designed to operate over the 3 to 15 V operating range and over a temperature range of -55 to 125 C.

  17. A high resolution, monolithic crystal, PET/MRI detector with DOI positioning capability.

    Science.gov (United States)

    Li, Xiaoli; Lockhart, Cate; Lewellen, Tom K; Miyaoka, Robert S

    2008-01-01

    We report on a high resolution, monolithic crystal PET detector design that provides depth of interaction (DOI) positioning within the crystal and is compatible for operation in a MRI scanner to support multimodal anatomic and functional imaging. Our design utilizes a novel sensor on the entrance surface (SES) design combined with a maximum likelihood positioning algorithm. The sensor will be a two-dimensional array of micro-pixel avalanche photodiodes (MAPD). MAPDs are a new type of solid-state photodetector with Geiger mode operation that can provide signal gain similar to a photomltipiler tube (PMT). In addition, they can be operated in high magnetic fields to support PET/MR imaging. Utilizing a multi-step simulation process, we determined the intrinsic spatial resolution characteristics of a detector using the proposed design. For a 48.8 mm by 48.8 mm by 15 mm LSO crystal detector readout by an 8 by 8 array of 5.8 mm by 5.8 mm MAPD elements the intrinsic spatial resolution is 0.83 mm FWHM in X, 0.92 mm FWHM in Y and 1.83 mm FWHM in Z (i.e., DOI) for normally incident photons. Comparing the results versus using a conventional design with the photosensors on the backside of the crystal, an average improvement of 25% in X, 23% in Y, and 20% in Z is achieved.

  18. Adaptive and mobile ground sensor array.

    Energy Technology Data Exchange (ETDEWEB)

    Holzrichter, Michael Warren; O' Rourke, William T.; Zenner, Jennifer; Maish, Alexander B.

    2003-12-01

    The goal of this LDRD was to demonstrate the use of robotic vehicles for deploying and autonomously reconfiguring seismic and acoustic sensor arrays with high (centimeter) accuracy to obtain enhancement of our capability to locate and characterize remote targets. The capability to accurately place sensors and then retrieve and reconfigure them allows sensors to be placed in phased arrays in an initial monitoring configuration and then to be reconfigured in an array tuned to the specific frequencies and directions of the selected target. This report reviews the findings and accomplishments achieved during this three-year project. This project successfully demonstrated autonomous deployment and retrieval of a payload package with an accuracy of a few centimeters using differential global positioning system (GPS) signals. It developed an autonomous, multisensor, temporally aligned, radio-frequency communication and signal processing capability, and an array optimization algorithm, which was implemented on a digital signal processor (DSP). Additionally, the project converted the existing single-threaded, monolithic robotic vehicle control code into a multi-threaded, modular control architecture that enhances the reuse of control code in future projects.

  19. Monolithic silicon photonics in a sub-100nm SOI CMOS microprocessor foundry: progress from devices to systems

    Science.gov (United States)

    Popović, Miloš A.; Wade, Mark T.; Orcutt, Jason S.; Shainline, Jeffrey M.; Sun, Chen; Georgas, Michael; Moss, Benjamin; Kumar, Rajesh; Alloatti, Luca; Pavanello, Fabio; Chen, Yu-Hsin; Nammari, Kareem; Notaros, Jelena; Atabaki, Amir; Leu, Jonathan; Stojanović, Vladimir; Ram, Rajeev J.

    2015-02-01

    We review recent progress of an effort led by the Stojanović (UC Berkeley), Ram (MIT) and Popović (CU Boulder) research groups to enable the design of photonic devices, and complete on-chip electro-optic systems and interfaces, directly in standard microelectronics CMOS processes in a microprocessor foundry, with no in-foundry process modifications. This approach allows tight and large-scale monolithic integration of silicon photonics with state-of-the-art (sub-100nm-node) microelectronics, here a 45nm SOI CMOS process. It enables natural scale-up to manufacturing, and rapid advances in device design due to process repeatability. The initial driver application was addressing the processor-to-memory communication energy bottleneck. Device results include 5Gbps modulators based on an interleaved junction that take advantage of the high resolution of the sub-100nm CMOS process. We demonstrate operation at 5fJ/bit with 1.5dB insertion loss and 8dB extinction ratio. We also demonstrate the first infrared detectors in a zero-change CMOS process, using absorption in transistor source/drain SiGe stressors. Subsystems described include the first monolithically integrated electronic-photonic transmitter on chip (modulator+driver) with 20-70fJ/bit wall plug energy/bit (2-3.5Gbps), to our knowledge the lowest transmitter energy demonstrated to date. We also demonstrate native-process infrared receivers at 220fJ/bit (5Gbps). These are encouraging signs for the prospects of monolithic electronics-photonics integration. Beyond processor-to-memory interconnects, our approach to photonics as a "More-than- Moore" technology inside advanced CMOS promises to enable VLSI electronic-photonic chip platforms tailored to a vast array of emerging applications, from optical and acoustic sensing, high-speed signal processing, RF and optical metrology and clocks, through to analog computation and quantum technology.

  20. Global Arrays

    Energy Technology Data Exchange (ETDEWEB)

    Krishnamoorthy, Sriram; Daily, Jeffrey A.; Vishnu, Abhinav; Palmer, Bruce J.

    2015-11-01

    Global Arrays (GA) is a distributed-memory programming model that allows for shared-memory-style programming combined with one-sided communication, to create a set of tools that combine high performance with ease-of-use. GA exposes a relatively straightforward programming abstraction, while supporting fully-distributed data structures, locality of reference, and high-performance communication. GA was originally formulated in the early 1990’s to provide a communication layer for the Northwest Chemistry (NWChem) suite of chemistry modeling codes that was being developed concurrently.

  1. Integrated Duo Wavelength VCSEL Using an Electrically Pumped GaInAs/AlGaAs 980 nm Cavity at the Bottom and an Optically Pumped GaInAs/AlGaInAs 1550 nm Cavity on the Top

    Science.gov (United States)

    Islam, Samiha Ishrat; Islam, Arnob; Islam, Saiful

    2014-01-01

    In this work, an integrated single chip dual cavity VCSEL has been designed which comprises an electrically pumped 980 nm bottom VCSEL section fabricated using GaInAs/AlGaAs MQW active region and a 1550 nm top VCSEL section constructed using GaInAs/AlGaInAs MQW active region but optically pumped using half of the produced 980 nm light entering into it from the electrically pumped bottom cavity. In this design, the active region of the intracavity structure 980 nm VCSEL consists of 3 quantum wells (QWs) using Ga0.847In0.153As, 2 barriers using Al0.03Ga0.97As, and 2 separate confinement heterostructures (SCH) using the same material as the barrier. The active region of the top emitting 1550 nm VCSEL consists of 3 QWs using Ga0.47In0.52As, 2 barriers using Al0.3Ga0.17In0.53As, and 2 SCHs using the same material as the barrier. The top DBR and the bottom DBR mirror systems of the 1550 nm VCSEL section plus the top and bottom DBR mirror systems of the 980 nm VCSEL section have been formed using GaAs/Al0.8Ga0.2As. Computations show that the VCSEL is capable of producing 8.5 mW of power at 980 nm from the bottom side and 2 mW of power at the 1550 nm from top side. PMID:27379335

  2. Monolithic, High-Speed Fiber-Optic Switching Array for Lidar Project

    Data.gov (United States)

    National Aeronautics and Space Administration — This NASA SBIR Phase II effort will develop a 1 x 10 prototype non-mechanical fiber optic switch for use with high power lasers. The proposed optical device is a...

  3. Monolithic, High-Speed Fiber-Optic Switching Array for Lidar Project

    Data.gov (United States)

    National Aeronautics and Space Administration — The proposed optical device is a fiber-based multi-channel switch to quickly switch a fiber-coupled laser among many possible output channels to create a fiber-based...

  4. A novel, SiPM-array-based, monolithic scintillator detector for PET

    NARCIS (Netherlands)

    Schaart, D.R.; Van Dam, H.T.; Seifert, S.; Vinke, R.; Dendooven, P.; Löhner, H.; Beekman, F.J.

    2009-01-01

    Silicon photomultipliers (SiPMs) are of great interest to positron emission tomography (PET), as they enable new detector geometries, for e.g., depth-of-interaction (DOI) determination, are MR compatible, and offer faster response and higher gain than other solid-state photosensors such as avalanche

  5. A novel, SiPM-array-based, monolithic scintillator detector for PET

    NARCIS (Netherlands)

    Schaart, Dennis R.; van Dam, Herman T.; Seifert, Stefan; Vinke, Ruud; Dendooven, Peter; Beekman, Freek J.; Löhner, H.

    2009-01-01

    Silicon photomultipliers (SiPMs) are of great interest to positron emission tomography (PET), as they enable new detector geometries, for e. g., depth-of-interaction (DOI) determination, are MR compatible, and offer faster response and higher gain than other solid-state photosensors such as

  6. The First Monolithic Silicon Carbide Active Pixel Sensor Array for Solar Blind UV Detection Project

    Data.gov (United States)

    National Aeronautics and Space Administration — This Small Business Innovation Research Phase I project will address the needs of space astronomy, military threat detection, and scientific research for image...

  7. A novel, SiPM-array-based, monolithic scintillator detector for PET

    NARCIS (Netherlands)

    Schaart, Dennis R.; van Dam, Herman T.; Seifert, Stefan; Vinke, Ruud; Dendooven, Peter; Beekman, Freek J.; Löhner, H.

    2009-01-01

    Silicon photomultipliers (SiPMs) are of great interest to positron emission tomography (PET), as they enable new detector geometries, for e. g., depth-of-interaction (DOI) determination, are MR compatible, and offer faster response and higher gain than other solid-state photosensors such as avalanch

  8. Monolithic microwave integrated circuits for sensors, radar, and communications systems; Proceedings of the Meeting, Orlando, FL, Apr. 2-4, 1991

    Science.gov (United States)

    Leonard, Regis F.; Bhasin, Kul B.

    Consideration is given to MMICs for airborne phased arrays, monolithic GaAs integrated circuit millimeter wave imaging sensors, accurate design of multiport low-noise MMICs up to 20 GHz, an ultralinear low-noise amplifier technology for space communications, variable-gain MMIC module for space applications, a high-efficiency dual-band power amplifier for radar applications, a high-density circuit approach for low-cost MMIC circuits, coplanar SIMMWIC circuits, recent advances in monolithic phased arrays, and system-level integrated circuit development for phased-array antenna applications. Consideration is also given to performance enhancement in future communications satellites with MMIC technology insertion, application of Ka-band MMIC technology for an Orbiter/ACTS communications experiment, a space-based millimeter wave debris tracking radar, low-noise high-yield octave-band feedback amplifiers to 20 GHz, quasi-optical MESFET VCOs, and a high-dynamic-range mixer using novel balun structure. (For individual items see A93-25777 to A93-25814)

  9. Piezoresistive Sensors Development Using Monolithic CMOS MEMS Technology

    Directory of Open Access Journals (Sweden)

    A. Chaehoi

    2011-04-01

    Full Text Available This paper presents the development of a monolithic CMOS-MEMS platform under the iDesign and SemeMEMS projects with the aim of jointly providing an open access “one-stop-shop” design and prototyping facility for integrated CMOS-MEMS. This work addresses the implementation of a 3-axis accelerometer and a pressure sensor using Semefab’s in-house 2-poly 1-metal CMOS process on a 380/4/15 μm SOI wafer; the membrane and the proof mass being micromachined using double-sided Deep Reactive Ion Etching (DRIE. This monolithic approach promises, in high volume production and using low complexity processes, a dramatic cost reduction over hybrid sensors. Furthermore, the embedded signal conditioning and the low-noise level in polysilicon gauges enables high performance to be achieved by implementing dedicated on-chip amplification and filtering circuitry.

  10. Low-bandgap, monolithic, multi-bandgap, optoelectronic devices

    Science.gov (United States)

    Wanlass, Mark W.; Carapella, Jeffrey J.

    2014-07-08

    Low bandgap, monolithic, multi-bandgap, optoelectronic devices (10), including PV converters, photodetectors, and LED's, have lattice-matched (LM), double-heterostructure (DH), low-bandgap GaInAs(P) subcells (22, 24) including those that are lattice-mismatched (LMM) to InP, grown on an InP substrate (26) by use of at least one graded lattice constant transition layer (20) of InAsP positioned somewhere between the InP substrate (26) and the LMM subcell(s) (22, 24). These devices are monofacial (10) or bifacial (80) and include monolithic, integrated, modules (MIMs) (190) with a plurality of voltage-matched subcell circuits (262, 264, 266, 270, 272) as well as other variations and embodiments.

  11. Design and Testing of Prototypic Elements Containing Monolithic Fuel

    Energy Technology Data Exchange (ETDEWEB)

    N.E. Woolstenhulme; M.K. Meyer; D.M. Wachs

    2011-10-01

    The US fuel development team has performed numerous irradiation tests on small to medium sized specimens containing low enriched uranium fuel designs. The team is now focused on qualification and demonstration of the uranium-molybdenum Base Monolithic Design and has entered the next generation of testing with the design and irradiation of prototypic elements which contain this fuel. The designs of fuel elements containing monolithic fuel, such as AFIP-7 (which is currently under irradiation) and RERTR-FE (which is currently under fabrication), are appropriate progressions relative to the technology life cycle. The culmination of this testing program will occur with the design, fabrication, and irradiation of demonstration products to include the base fuel demonstration and design demonstration experiments. Future plans show that design, fabrication, and testing activities will apply the rigor needed for a demonstration campaign.

  12. From 1D to 3D - macroscopic nanowire aerogel monoliths

    Science.gov (United States)

    Cheng, Wei; Rechberger, Felix; Niederberger, Markus

    2016-07-01

    Here we present a strategy to assemble one-dimensional nanostructures into a three-dimensional architecture with macroscopic size. With the assistance of centrifugation, we successfully gel ultrathin W18O49 nanowires with diameters of 1 to 2 nm and aspect ratios larger than 100 into 3D networks, which are transformed into monolithic aerogels by supercritical drying.Here we present a strategy to assemble one-dimensional nanostructures into a three-dimensional architecture with macroscopic size. With the assistance of centrifugation, we successfully gel ultrathin W18O49 nanowires with diameters of 1 to 2 nm and aspect ratios larger than 100 into 3D networks, which are transformed into monolithic aerogels by supercritical drying. Electronic supplementary information (ESI) available: Experimental details, SEM and TEM images, and digital photographs. See DOI: 10.1039/c6nr04429h

  13. Low-bandgap, monolithic, multi-bandgap, optoelectronic devices

    Energy Technology Data Exchange (ETDEWEB)

    Wanlass, Mark W.; Carapella, Jeffrey J.

    2016-01-05

    Low bandgap, monolithic, multi-bandgap, optoelectronic devices (10), including PV converters, photodetectors, and LED's, have lattice-matched (LM), double-heterostructure (DH), low-bandgap GaInAs(P) subcells (22, 24) including those that are lattice-mismatched (LMM) to InP, grown on an InP substrate (26) by use of at least one graded lattice constant transition layer (20) of InAsP positioned somewhere between the InP substrate (26) and the LMM subcell(s) (22, 24). These devices are monofacial (10) or bifacial (80) and include monolithic, integrated, modules (MIMs) (190) with a plurality of voltage-matched subcell circuits (262, 264, 266, 270, 272) as well as other variations and embodiments.

  14. Low-bandgap, monolithic, multi-bandgap, optoelectronic devices

    Energy Technology Data Exchange (ETDEWEB)

    Wanlass, Mark W.; Carapella, Jeffrey J.

    2014-07-08

    Low bandgap, monolithic, multi-bandgap, optoelectronic devices (10), including PV converters, photodetectors, and LED's, have lattice-matched (LM), double-heterostructure (DH), low-bandgap GaInAs(P) subcells (22, 24) including those that are lattice-mismatched (LMM) to InP, grown on an InP substrate (26) by use of at least one graded lattice constant transition layer (20) of InAsP positioned somewhere between the InP substrate (26) and the LMM subcell(s) (22, 24). These devices are monofacial (10) or bifacial (80) and include monolithic, integrated, modules (MIMs) (190) with a plurality of voltage-matched subcell circuits (262, 264, 266, 270, 272) as well as other variations and embodiments.

  15. Low-bandgap, monolithic, multi-bandgap, optoelectronic devices

    Energy Technology Data Exchange (ETDEWEB)

    Wanlass, Mark W.; Carapella, Jeffrey J.

    2016-03-22

    Low bandgap, monolithic, multi-bandgap, optoelectronic devices (10), including PV converters, photodetectors, and LED's, have lattice-matched (LM), double-heterostructure (DH), low-bandgap GaInAs(P) subcells (22, 24) including those that are lattice-mismatched (LMM) to InP, grown on an InP substrate (26) by use of at least one graded lattice constant transition layer (20) of InAsP positioned somewhere between the InP substrate (26) and the LMM subcell(s) (22, 24). These devices are monofacial (10) or bifacial (80) and include monolithic, integrated, modules (MIMs) (190) with a plurality of voltage-matched subcell circuits (262, 264, 266, 270, 272) as well as other variations and embodiments.

  16. Development of stable monolithic wide-field Michelson interferometers

    Science.gov (United States)

    Wan, Xiaoke; Ge, Jian; Chen, Zhiping

    2011-07-01

    Bulk wide-field Michelson interferometers are very useful for high precision applications in remote sensing and astronomy. A stable monolithic Michelson interferometer is a key element in high precision radial velocity (RV) measurements for extrasolar planets searching and studies. Thermal stress analysis shows that matching coefficients of thermal expansion (CTEs) is a critical requirement for ensuring interferometer stability. This requirement leads to a novel design using BK7 and LAK7 materials, such that the monolithic interferometer is free from thermal distortion. The processes of design, fabrication, and testing of interferometers are described in detail. In performance evaluations, the field angle is typically 23.8° and thermal sensitivity is typically -2.6×10-6/° C near 550nm, which corresponds to ˜800m/s/°C in the RV scale. Low-cost interferometer products have been commissioned in multiple RV instruments, and they are producing high stability performance over long term operations.

  17. Development of stable monolithic wide-field Michelson interferometers.

    Science.gov (United States)

    Wan, Xiaoke; Ge, Jian; Chen, Zhiping

    2011-07-20

    Bulk wide-field Michelson interferometers are very useful for high precision applications in remote sensing and astronomy. A stable monolithic Michelson interferometer is a key element in high precision radial velocity (RV) measurements for extrasolar planets searching and studies. Thermal stress analysis shows that matching coefficients of thermal expansion (CTEs) is a critical requirement for ensuring interferometer stability. This requirement leads to a novel design using BK7 and LAK7 materials, such that the monolithic interferometer is free from thermal distortion. The processes of design, fabrication, and testing of interferometers are described in detail. In performance evaluations, the field angle is typically 23.8° and thermal sensitivity is typically -2.6×10(-6)/°C near 550 nm, which corresponds to ∼800 m/s/°C in the RV scale. Low-cost interferometer products have been commissioned in multiple RV instruments, and they are producing high stability performance over long term operations.

  18. Affinity Monolith-Integrated Microchips for Protein Purification and Concentration.

    Science.gov (United States)

    Gao, Changlu; Sun, Xiuhua; Wang, Huaixin; Qiao, Wei; Hu, Bo

    2016-01-01

    Affinity chromatography is a valuable method to purify and concentrate minute amount of proteins. Monoliths with epoxy groups for affinity immobilization were prepared by direct in-situ photopolymerization of glycidyl methacrylate and ethylene glycol dimethacrylate in porogenic solvents consisting of 1-dodecanol and cyclohexanol. By integrating affinity monoliths onto a microfluidic system, targeted biomolecules can be captured and retained on affinity column, while other biomolecules having no specific interactions toward the immobilized ligands flow through the microchannel. Therefore, proteins which remain on the affinity column are purified and concentrated, and then eluted by appropriate solutions and finally, separated by microchip capillary electrophoresis. This integrated microfluidic device has been applied to the purification and separation of specific proteins (FITC-labeled human serum albumin and IgG) in a mixture.

  19. Materials and process development for the monolithic interconnected module (MIM) InGaAs/InP TPV cells

    Energy Technology Data Exchange (ETDEWEB)

    Fatemi, N.S.; Jenkins, P.P.; Hoffman, R.W. Jr.; Weizer, V.G. [Essential Research, Inc., Cleveland, OH (United States); Wilt, D.M. [National Aeronautics and Space Administration, Cleveland, OH (United States). Lewis Research Center; Murray, C.S.; Riley, D. [Westinghouse Electric Corp., West Mifflin, PA (United States)

    1997-06-01

    Four major components of a thermophotovoltaic (TPV) energy conversion system are a heat source, a graybody or a selective emitter, spectrum shaping elements such as filters, and photovoltaic (PV) cells. One approach to achieving a high voltage/low current configuration is to fabricate a device, where small area PV cells are monolithically series connected. The authors have termed this device a monolithic interconnected module (MIM). A MIM device has other advantages over conventional one-junction cells, such as simplified array interconnections and heat-sinking, and radiation recycling capability via a back surface reflector (BSR). The authors confine the contents of this article to the MIM materials, process development, and some optical results. The successful fabrication of InGaAs/InP MIM devices entails the development and optimization of several key components and processes. These include: isolation trench via geometry, selective chemical etching, contact and interconnect metallization, dielectric isolation barrier, back surface reflector (BSR), and anti-reflection (AR) coating. The selection, development, and testing of the materials and processes described above for MIM fabrication will be described.

  20. A design concept for an MMIC microstrip phased array

    Science.gov (United States)

    Lee, R. Q.; Smetana, J.; Acosta, R.

    A conceptual design for a microstrip phased array with monolithic microwave integrated circuit (MMIC) amplitude and phase controls is described. The MMIC devices used are 20 GHz variable power amplifiers and variable phase shifters recently developed by NASA contractors for applications in future Ka band advanced satellite communication antenna systems. The proposed design concept is for a general NxN element array of rectangular lattice geometry. Subarray excitation is incorporated in the MMIC phased array design to reduce the complexity of the beam forming network and the number of MMIC components required. The proposed design concept takes into consideration the RF characteristics and actual phyical dimensions of the MMIC devices. Also, solutions to spatial constraints and interconnections associated with currently available packaging designs are discussed. Finally, the design of the microstrip radiating elements and their radiation characteristics are examined.

  1. Ka-band MMIC microstrip array for high rate communications

    Science.gov (United States)

    Lee, R. Q.; Raquet, C. A.; Tolleson, J. B.; Sanzgiri, S. M.

    1991-01-01

    In a recent technology assessment of alternative communication systems for the space exploration initiative (SEI), Ka-band (18 to 40 GHz) communication technology was identified to meet the mission requirements of telecommunication, navigation, and information management. Compared to the lower frequency bands, Ka-band antennas offer higher gain and broader bandwidths; thus, they are more suitable for high data rate communications. Over the years, NASA has played an important role in monolithic microwave integrated circuit (MMIC) phased array technology development, and currently, has an ongoing contract with Texas Instrument (TI) to develop a modular Ka-band MMIC microstrip subarray (NAS3-25718). The TI contract emphasizes MMIC integration technology development and stipulates using existing MMIC devices to minimize the array development cost. The objective of this paper is to present array component technologies and integration techniques used to construct the subarray modules.

  2. Dynamic response of monolithic and laminate/particulate reactive mixtures

    OpenAIRE

    Wei, Chung-Ting

    2011-01-01

    Two dynamic compression methods were applied to a monolithic metal and reactive mixtures to investigate their responses: (a) Dynamic experiments using a split Hopkinson pressure bar were applied to reactive mixtures densified by explosive consolidation in order to establish their mechanical response and failure mechanisms. (b) Laser compression and release, which can impart high stresses, up to hundreds GPa, in times of nanoseconds and fractions thereof, was applied to establish the spalling ...

  3. Advanced on-chip divider for monolithic microwave VCO's

    Science.gov (United States)

    Peterson, Weddell C.

    1989-01-01

    High frequency division on a monolithic circuit is a critical technology required to significantly enhance the performance of microwave and millimeter-wave phase-locked sources. The approach used to meet this need is to apply circuit design practices which are essentially 'microwave' in nature to the basically 'digital' problem of high speed division. Following investigation of several promising circuit approaches, program phase 1 culminated in the design and layout of an 8.5 GHz (Deep Space Channel 14) divide by four circuit based on a dynamic mixing divider circuit approach. Therefore, during program phase 2, an 8.5 GHz VCO with an integral divider which provides a phase coherent 2.125 GHz reference signal for phase locking applications was fabricated and optimized. Complete phase locked operation of the monolithic GaAs devices (VCO, power splitter, and dynamic divider) was demonstrated both individually and as an integrated unit. The fully functional integrated unit in a suitable test fixture was delivered to NASA for engineering data correlation. Based on the experience gained from this 8.5 GHz super component, a monolithic GaAs millimeter-wave dynamic divider for operation with an external VCO was also designed, fabricated, and characterized. This circuit, which was also delivered to NASA, demonstrated coherent division by four at an input frequency of 24.3 GHz. The high performance monolithic microwave VCO with a coherent low frequency reference output described in this report and others based on this technology will greatly benefit advanced communications systems in both the DoD and commercial sectors. Signal processing and instrumentation systems based on phase-locking loops will also attain enhanced performance at potentially reduced cost.

  4. Advanced on-chip divider for monolithic microwave VCO's

    Science.gov (United States)

    Peterson, Weddell C.

    1989-05-01

    High frequency division on a monolithic circuit is a critical technology required to significantly enhance the performance of microwave and millimeter-wave phase-locked sources. The approach used to meet this need is to apply circuit design practices which are essentially 'microwave' in nature to the basically 'digital' problem of high speed division. Following investigation of several promising circuit approaches, program phase 1 culminated in the design and layout of an 8.5 GHz (Deep Space Channel 14) divide by four circuit based on a dynamic mixing divider circuit approach. Therefore, during program phase 2, an 8.5 GHz VCO with an integral divider which provides a phase coherent 2.125 GHz reference signal for phase locking applications was fabricated and optimized. Complete phase locked operation of the monolithic GaAs devices (VCO, power splitter, and dynamic divider) was demonstrated both individually and as an integrated unit. The fully functional integrated unit in a suitable test fixture was delivered to NASA for engineering data correlation. Based on the experience gained from this 8.5 GHz super component, a monolithic GaAs millimeter-wave dynamic divider for operation with an external VCO was also designed, fabricated, and characterized. This circuit, which was also delivered to NASA, demonstrated coherent division by four at an input frequency of 24.3 GHz. The high performance monolithic microwave VCO with a coherent low frequency reference output described in this report and others based on this technology will greatly benefit advanced communications systems in both the DoD and commercial sectors. Signal processing and instrumentation systems based on phase-locking loops will also attain enhanced performance at potentially reduced cost.

  5. Clinical assessment of enamel wear caused by monolithic zirconia crowns.

    Science.gov (United States)

    Stober, T; Bermejo, J L; Schwindling, F S; Schmitter, M

    2016-08-01

    The purpose of this study was to measure enamel wear caused by antagonistic monolithic zirconia crowns and to compare this with enamel wear caused by contralateral natural antagonists. Twenty monolithic zirconia full molar crowns were placed in 20 patients. Patients with high activity of the masseter muscle at night (bruxism) were excluded. For analysis of wear, vinylpolysiloxane impressions were prepared after crown incorporation and at 6-, 12-, and 24-month follow-up. Wear of the occlusal contact areas of the crowns, of their natural antagonists, and of two contralateral natural antagonists (control teeth) was measured by use of plaster replicas and a 3D laser-scanning device. Differences of wear between the zirconia crown antagonists and the control teeth were investigated by means of two-sided paired Student's t-tests and linear regression analysis. After 2 years, mean vertical loss was 46 μm for enamel opposed to zirconia, 19-26 μm for contralateral control teeth and 14 μm for zirconia crowns. Maximum vertical loss was 151 μm for enamel opposed to zirconia, 75-115 μm for control teeth and 60 μm for zirconia crowns. Statistical analysis revealed significant differences between wear of enamel by zirconia-opposed teeth and by control teeth. Gender, which significantly affected wear, was identified as a possible confounder. Monolithic zirconia crowns generated more wear of opposed enamel than did natural teeth. Because of the greater wear caused by other dental ceramics, the use of monolithic zirconia crowns may be justified.

  6. Applications of monolithic fiber interferometers and actively controlled fibers

    OpenAIRE

    Rugeland, Patrik

    2013-01-01

    The objective of this thesis was to develop applications of monolithic fiber devices and actively controlled fibers. A special twin-core fiber known as a ‘Gemini’ fiber was used to construct equal arm-length fiber interferometers, impervious to temperature and mechanical perturbations. A broadband add/drop multiplexer was constructed by inscribing fiber Bragg gratings in the arms of a Gemini Mach-Zehnder interferometer. A broadband interferometric nanosecond switch was constructed from a micr...

  7. Monolithically Integrated Ge-on-Si Active Photonics

    OpenAIRE

    Jifeng Liu

    2014-01-01

    Monolithically integrated, active photonic devices on Si are key components in Si-based large-scale electronic-photonic integration for future generations of high-performance, low-power computation and communication systems. Ge has become an interesting candidate for active photonic devices in Si photonics due to its pseudo-direct gap behavior and compatibility with Si complementary metal oxide semiconductor (CMOS) processing. In this paper, we present a review of the recent progress in Ge-on...

  8. Extended Leach Testing of Simulated LAW Cast Stone Monoliths

    Energy Technology Data Exchange (ETDEWEB)

    Serne, R. Jeffrey [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Lanigan, David C. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Westsik, Joseph H. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Williams, Benjamin D. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Jung, H. B. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Wang, Guohui [Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

    2016-08-12

    This revision to the original report adds two longer term leach sets of data to the report and provides more discussion and graphics on how to interpret the results from long-term laboratory leach tests. The leach tests were performed at Pacific Northwest National Laboratory (PNNL) for Washington River Protection Solutions (WRPS) to evaluate the release of key constituents from monoliths of Cast Stone prepared with four simulated low-activity waste (LAW) liquid waste streams.

  9. A Distributed Model of Four-Port Monolithic Transformer

    OpenAIRE

    Lee, Dong Ho; Ko, Sangsoo; Jeon, Sang-Hoon; Park, Jae-Woo; Hong, Songcheol

    2004-01-01

    This paper deals with modeling of a monolithic spiral transformer. The transformer is designed and fabricated as a symmetrical octagonal spiral structure using two-metal layer process on GaAs substrate for input balun applications of 2 GHz and 5 GHz push-pull power amplifiers. A distributed model of the transformer is developed to fit in wide frequency range with four ports. The model includes the skin effect which describes increase in series resistance with frequency. Six different se...

  10. UPDATE ON MECHANICAL ANALYSIS OF MONOLITHIC FUEL PLATES

    Energy Technology Data Exchange (ETDEWEB)

    D. E. Burkes; F. J. Rice; J.-F. Jue; N. P. Hallinan

    2008-03-01

    Results on the relative bond strength of the fuel-clad interface in monolithic fuel plates have been presented at previous RRFM conferences. An understanding of mechanical properties of the fuel, cladding, and fuel / cladding interface has been identified as an important area of investigation and quantification for qualification of monolithic fuel forms. Significant progress has been made in the area of mechanical analysis of the monolithic fuel plates, including mechanical property determination of fuel foils, cladding processed by both hot isostatic pressing and friction bonding, and the fuel-clad composite. In addition, mechanical analysis of fabrication induced residual stress has been initiated, along with a study to address how such stress can be relieved prior to irradiation. Results of destructive examinations and mechanical tests are presented along with analysis and supporting conclusions. A brief discussion of alternative non-destructive evaluation techniques to quantify not only bond quality, but also bond integrity and strength, will also be provided. These are all necessary steps to link out-of-pile observations as a function of fabrication with in-pile behaviours.

  11. Strong cation exchange monoliths for HPLC by Reactive Gelation.

    Science.gov (United States)

    Brand, Bastian; Krättli, Martin; Storti, Giuseppe; Morbidelli, Massimo

    2011-08-01

    Polymeric monolithic stationary phases for HPLC can be produced by Reactive Gelation. Unlike the conventional method of using porogens, such novel process consists of a number of separate steps, thus enabling a better control of the quality of the final material. A suspension of polymer nanoparticles in water is produced and subsequently swollen with hydrophobic monomers. The particles are then destabilised (usually by salt addition) to make them aggregate into a large percolating structure, the so-called monolith. Finally, the added monomer can then be polymerised to harden the structure. In this work, a polystyrene latex is used as the base material and functionalised by introduction of epoxide groups on the surface and subsequent reaction to sulphonic acid groups, yielding a SO3(-) density of 0.7 mmol/g dry material. Morphological investigations show 54% porosity made of 300 nm large pores. Van Deemter measurements of a large protein show no practical influence of diffusion limitations on the plate number. Finally, a preliminary separation of a test protein mixture is shown, demonstrating the potential of using ion-exchange chromatography on Reactive Gelation monoliths.

  12. Controlled porosity monolithic material as permselective ion exchange membranes.

    Science.gov (United States)

    Huang, Xiaojia; Dasgupta, Purnendu K

    2011-03-18

    Ion exchange membranes (IEMs) are used in a variety of analytical devices, including suppressors, eluent generators and other components used in ion chromatography. Such membranes are flexible and undergo substantial dimensional changes on hydration. Presently the push to miniaturization continues; a resurgent interest in open tubular ion chromatography requires microscale adaptation of these components. Incorporating IEMs in microscale devices is difficult. Although both macroporous and microporous ion exchange materials have been made for use as chromatographic packing, ion exchange material used as membranes are porous only on a molecular scale. Because such pores have vicinal ion exchange sites, ions of the same charge sign as those of the fixed sites are excluded from the IEMs. Monolithic polymers, including ion exchangers derived therefrom, are presently extensively used. When used in a separation column, such a monolithic structure contains an extensively connected porous network. We show here that by controlling the amount of porogen added during the synthesis of monolithic polymers derived from ethylene dimethacrylate - glycidyl methacrylate, which are converted to an anion exchanger by treatment with trimethylamine, it is possible to obtain rigid ion exchange polymers that behave like IEMs and allow only one charge type of ions to pass through, i.e., are permselective. We demonstrate successful open tubular cation chromatography suppressor performance.

  13. Monolithic pixels on moderate resistivity substrate and sparsifying readout architecture

    Science.gov (United States)

    Giubilato, P.; Battaglia, M.; Bisello, D.; Caselle, M.; Chalmet, P.; Demaria, L.; Ikemoto, Y.; Kloukinas, K.; Mansuy, S. C.; Mattiazzo, S.; Marchioro, A.; Mugnier, H.; Pantano, D.; Potenza, A.; Rivetti, A.; Rousset, J.; Silvestrin, L.; Snoeys, W.

    2013-12-01

    The LePix projects aim realizing a new generation monolithic pixel detectors with improved performances at lesser cost with respect to both current state of the art monolithic and hybrid pixel sensors. The detector is built in a 90 nm CMOS process on a substrate of moderate resistivity. This allows charge collection by drift while maintaining the other advantages usually offered by MAPS, like having a single piece detector and using a standard CMOS production line. The collection by drift mechanism, coupled to the low capacitance design of the collecting node made possible by the monolithic approach, provides an excellent signal to noise ratio straight at the pixel cell together with a radiation tolerance far superior to conventional un-depleted MAPS. The excellent signal-to-noise performance is demonstrated by the device ability to separate the 6 keV 55Fe double peak at room temperature. To achieve high granularity (10-20 μm pitch pixels) over large detector areas maintaining high readout speed, a completely new compressing architecture has been devised. This architecture departs from the mainstream hybrid pixel sparsification approach, which uses in-pixel logic to reduce data, by using topological compression to minimize pixel area and power consumption.

  14. Preparing silica aerogel monoliths via a rapid supercritical extraction method.

    Science.gov (United States)

    Carroll, Mary K; Anderson, Ann M; Gorka, Caroline A

    2014-02-28

    A procedure for the fabrication of monolithic silica aerogels in eight hours or less via a rapid supercritical extraction process is described. The procedure requires 15-20 min of preparation time, during which a liquid precursor mixture is prepared and poured into wells of a metal mold that is placed between the platens of a hydraulic hot press, followed by several hours of processing within the hot press. The precursor solution consists of a 1.0:12.0:3.6:3.5 x 10(-3) molar ratio of tetramethylorthosilicate (TMOS):methanol:water:ammonia. In each well of the mold, a porous silica sol-gel matrix forms. As the temperature of the mold and its contents is increased, the pressure within the mold rises. After the temperature/pressure conditions surpass the supercritical point for the solvent within the pores of the matrix (in this case, a methanol/water mixture), the supercritical fluid is released, and monolithic aerogel remains within the wells of the mold. With the mold used in this procedure, cylindrical monoliths of 2.2 cm diameter and 1.9 cm height are produced. Aerogels formed by this rapid method have comparable properties (low bulk and skeletal density, high surface area, mesoporous morphology) to those prepared by other methods that involve either additional reaction steps or solvent extractions (lengthier processes that generate more chemical waste).The rapid supercritical extraction method can also be applied to the fabrication of aerogels based on other precursor recipes.

  15. Monolithic pixels on moderate resistivity substrate and sparsifying readout architecture

    CERN Document Server

    Giubilato, P; Snoeys, W; Bisello, D; Marchioro, A; Battaglia, M; Demaria, L; Mansuy, S C; Pantano, D; Rousset, J; Mattiazzo, S; Kloukinas, K; Potenza, A; Ikemoto, Y; Rivetti, A; Chalmet, P; Mugnier, H; Silvestrin, L

    2013-01-01

    The LePix projects aim realizing a new generation monolithic pixel detectors with improved performances at lesser cost with respect to both current state of the art monolithic and hybrid pixel sensors. The detector is built in a 90 nm CMOS process on a substrate of moderate resistivity. This allows charge collection by drift while maintaining the other advantages usually offered by MAPS, like having a single piece detector and using a standard CMOS production line. The collection by drift mechanism, coupled to the low capacitance design of the collecting node made possible by the monolithic approach, provides an excellent signal to noise ratio straight at the pixel cell together with a radiation tolerance far superior to conventional un-depleted MAPS. The excellent signal-to-noise performance is demonstrated by the device ability to separate the 6 keV Fe-55 double peak at room temperature. To achieve high granularity (10-20 mu m pitch pixels) over large detector areas maintaining high readout speed, a complet...

  16. Two-way fiber-wireless convergence systems based on two-stage injection-locked VCSELs transmitter and optical interleaver.

    Science.gov (United States)

    Li, Chung-Yi; Lu, Hai-Han; Ying, Cheng-Ling; Zheng, Jun-Ren; Lin, Che-Yu; Wan, Zhi-Wei

    2015-02-23

    A two-way fiber-wireless convergence system based on a two-stage injection-locked 1.55-μm vertical-cavity surface-emitting lasers (VCSELs) transmitter and an optical interleaver (IL) to deliver intensity-modulated and phase-remodulated millimeter-wave (MMW) data signals over a 40-km single-mode fiber (SMF) and a 5-m radio frequency (RF) wireless transport is proposed and experimentally demonstrated. Bit error rate (BER) and eye diagram perform brilliantly through a serious investigation in systems. Such a two-way fiber-wireless convergence system is a promising option, it reveals a prominent one to present its advancement in integration of distribute fiber and in-house network.

  17. Preparation and characterization of polystyrene-based monolith with ordered macroporous structure

    Institute of Scientific and Technical Information of China (English)

    Quan Zhou Wu; Jian Feng He; Ji Ming Ou

    2012-01-01

    In this paper,polystyrene-based monoliths with highly ordered macroporous structure were synthesized by using SiO2 colloidal crystal as template.SEM observation shows that the macropores are highly ordered and are interconnected by small windows.The BET surface area of PS monolith is about 36.17 m2/g.The polymer monoliths can resist 5 MPa pressure,showing high mechanical and compressive strength.

  18. Photoinitiated grafting of porous polymer monoliths and thermoplastic polymers for microfluidic devices

    Science.gov (United States)

    Frechet, Jean M. J.; Svec, Frantisek; Rohr, Thomas

    2008-10-07

    A microfluidic device preferably made of a thermoplastic polymer that includes a channel or a multiplicity of channels whose surfaces are modified by photografting. The device further includes a porous polymer monolith prepared via UV initiated polymerization within the channel, and functionalization of the pore surface of the monolith using photografting. Processes for making such surface modifications of thermoplastic polymers and porous polymer monoliths are set forth.

  19. Application of Monolithic Zirconia Ceramics in Dental Practice: A Case History Report.

    Science.gov (United States)

    Kim, Hee-Kyung; Kim, Sung-Hun; Lee, Jai-Bong; Han, Jung-Suk; Yeo, In-Sung

    2016-01-01

    Monolithic zirconia restorations increasingly have been used in dental practice in recent years and demonstrate superior mechanical performance compared with porcelain-veneered zirconia restorations. Recent advances in manufacturing technology have made possible the fabrication of translucent monolithic zirconia ceramics. This case report describes three clinical examples of monolithic zirconia fixed dental prostheses being used in the anterior and posterior regions and exhibiting acceptable esthetic results.

  20. Compact stereo endoscopic camera using microprism arrays.

    Science.gov (United States)

    Yang, Sung-Pyo; Kim, Jae-Jun; Jang, Kyung-Won; Song, Weon-Kook; Jeong, Ki-Hun

    2016-03-15

    This work reports a microprism array (MPA) based compact stereo endoscopic camera with a single image sensor. The MPAs were monolithically fabricated by using two-step photolithography and geometry-guided resist reflow to form an appropriate prism angle for stereo image pair formation. The fabricated MPAs were transferred onto a glass substrate with a UV curable resin replica by using polydimethylsiloxane (PDMS) replica molding and then successfully integrated in front of a single camera module. The stereo endoscopic camera with MPA splits an image into two stereo images and successfully demonstrates the binocular disparities between the stereo image pairs for objects with different distances. This stereo endoscopic camera can serve as a compact and 3D imaging platform for medical, industrial, or military uses.

  1. Feasibility evaluation of the monolithic braided ablative nozzle

    Science.gov (United States)

    Director, Mark N.; McPherson, Douglass J., Sr.

    1992-02-01

    The feasibility of the monolithic braided ablative nozzle was evaluated as part of an independent research and development (IR&D) program complementary to the National Aeronautics and Space Administration/Marshall Space Flight Center (NASA/MSFC) Low-Cost, High-Reliability Case, Insulation and Nozzle for Large Solid Rocket Motors (LOCCIN) Program. The monolithic braided ablative nozzle is a new concept that utilizes a continuous, ablative, monolithic flame surface that extends from the nozzle entrance, through the throat, to the exit plane. The flame surface is fabricated using a Through-the-Thickness braided carbon-fiber preform, which is impregnated with a phenolic or phenolic-like resin. During operation, the braided-carbon fiber/resin material ablates, leaving the structural backside at temperatures which are sufficiently low to preclude the need for any additional insulative materials. The monolithic braided nozzle derives its potential for low life cycle cost through the use of automated processing, one-component fabrication, low material scrap, low process scrap, inexpensive raw materials, and simplified case attachment. It also has the potential for high reliability because its construction prevents delamination, has no nozzle bondlines or leak paths along the flame surface, is amenable to simplified analysis, and is readily inspectable. In addition, the braided construction has inherent toughness and is damage-tolerant. Two static-firing tests were conducted using subscale, 1.8 - 2.0-inch throat diameter, hardware. Tests were approximately 15 seconds in duration, using a conventional 18 percent aluminum/ammonium perchlorate propellant. The first of these tests evaluated the braided ablative as an integral backside insulator and exit cone; the second test evaluated the monolithic braided ablative as an integral entrance/throat/exit cone nozzle. Both tests met their objectives. Radial ablation rates at the throat were as predicted, approximately 0.017 in

  2. Comparison of perfusion media and monoliths for protein and virus-like particle chromatography.

    Science.gov (United States)

    Wu, Yige; Abraham, Dicky; Carta, Giorgio

    2016-05-20

    Structural and performance characteristics of perfusion chromatography media (POROS HS 20 and 50) and those of a polymethacrylate monolith (CIM SO3-1 tube monolith column) are compared for protein and virus-like particle chromatography using 1mL columns. Axial flow columns are used for POROS while the monolith has a radial flow configuration, which provides comparable operating pressures. The POROS beads contain a bimodal distribution of pore sizes, some as large as 0.5μm, which allow a small fraction of the mobile phase to flow within the particles, while the monolith contains 1-2μm flow channels. For proteins (lysozyme and IgG), the dynamic binding capacity of the POROS columns is more than twice that of the monolith at longer residence times. While the DBC of the POROS HS 50 column decreases at shorter residence times, the DBC of the POROS HS 20 column for IgG remains nearly twice that of the monolith at residence times at least as low as 0.2min as a result of intraparticle convection. Protein recoveries are comparable for all three columns. For VLPs, however, the eluted peaks are broader and recovery is lower for the monolith than for the POROS columns and is dependent on the direction of flow in the monolith, which is attributed to denser layer observed by SEM at the inlet surface of the monolith that appears to trap VLPs when loading in the normal flow direction.

  3. Microfluidic gene arrays for rapid genomic profiling

    Science.gov (United States)

    West, Jay A.; Hukari, Kyle W.; Hux, Gary A.; Shepodd, Timothy J.

    2004-12-01

    Genomic analysis tools have recently become an indispensable tool for the evaluation of gene expression in a variety of experiment protocols. Two of the main drawbacks to this technology are the labor and time intensive process for sample preparation and the relatively long times required for target/probe hybridization. In order to overcome these two technological barriers we have developed a microfluidic chip to perform on chip sample purification and labeling, integrated with a high density genearray. Sample purification was performed using a porous polymer monolithic material functionalized with an oligo dT nucleotide sequence for the isolation of high purity mRNA. These purified mRNA"s can then rapidly labeled using a covalent fluorescent molecule which forms a selective covalent bond at the N7 position of guanine residues. These labeled mRNA"s can then released from the polymer monolith to allow for direct hybridization with oligonucletide probes deposited in microfluidic channel. To allow for rapid target/probe hybridization high density microarray were printed in microchannels. The channels can accommodate array densities as high as 4000 probes. When oligonucleotide deposition is complete, these channels are sealed using a polymer film which forms a pressure tight seal to allow sample reagent flow to the arrayed probes. This process will allow for real time target to probe hybridization monitoring using a top mounted CCD fiber bundle combination. Using this process we have been able to perform a multi-step sample preparation to labeled target/probe hybridization in less than 30 minutes. These results demonstrate the capability to perform rapid genomic screening on a high density microfluidic microarray of oligonucleotides.

  4. Array Phase Shifters: Theory and Technology

    Science.gov (United States)

    Romanofsky, Robert R.

    2007-01-01

    While there are a myriad of applications for microwave phase shifters in instrumentation and metrology, power combining, amplifier linearization, and so on, the most prevalent use is in scanning phased-array antennas. And while this market continues to be dominated by military radar and tracking platforms, many commercial applications have emerged in the past decade or so. These new and potential applications span low-Earth-orbit (LEO) communications satellite constellations and collision warning radar, an aspect of the Intelligent Vehicle Highway System or Automated Highway System. In any case, the phase shifters represent a considerable portion of the overall antenna cost, with some estimates approaching 40 percent for receive arrays. Ferrite phase shifters continue to be the workhorse in military-phased arrays, and while there have been advances in thin film ferrite devices, the review of this device technology in the previous edition of this book is still highly relevant. This chapter will focus on three types of phase shifters that have matured in the past decade: GaAs MESFET monolithic microwave integrated circuit (MMIC), micro-electromechanical systems (MEMS), and thin film ferroelectric-based devices. A brief review of some novel devices including thin film ferrite phase shifters and superconducting switches for phase shifter applications will be provided. Finally, the effects of modulo 2 phase shift limitations, phase errors, and transient response on bit error rate degradation will be considered.

  5. Impact on the Spatial Resolution Performance of a Monolithic Crystal PET Detector Due to Different Sensor Parameters.

    Science.gov (United States)

    Li, Xiaoli; Lockhart, Cate; Lewellen, Tom K; Miyaoka, Robert S

    2009-10-24

    The performance characteristics of a monolithic crystal PET detector utilizing a novel sensor on the entrance surface (SES) design is reported. To facilitate this design, we propose to utilize a 2D silicon photomultiplier (SiPM) array device. SiPMs are a form of Geiger-Muller mode avalanche photodiodes (GMAPD) that can provide signal gain similar to a photomultiplier tube (PMT). Since these devices are still under active development, their performance parameters are changing. Using a multi-step simulation process, we investigated how different SiPM parameters affect the performance of a monolithic crystal PET detector. These parameters include gain variability between different channels; gain instability; and dark count noise. The detector simulated was a 49.6 mm by 49.6 mm by 15 mm LYSO crystal detector readout by a 16 by 16 array of 2.8 mm by 2.8 mm SiPM elements. To reduce the number of signal channels that need to be collected, the detector utilizes row-column summing. A statistics based positioning method is used for event positioning and depth of interaction (DOI) decoding. Of the variables investigated, the dark count noise had the largest impact on the intrinsic spatial resolution. Gain differences of 5-10% between detector calibration and detector testing had a modest impact on the intrinsic spatial resolution performance and led to a slight bias in positioning. There was no measurable difference with a gain variability of up to 25% between the individual SiPM channels. Based upon these results we are planning to cool our detectors below room temperature to reduce dark count noise and to actively control the temperature of the SiPMs to reduce drifts in gain over time.

  6. High brightness imaging system using vertical cavity surface-emitting laser micro-arrays- results and proposed enhancements

    Science.gov (United States)

    Mentzer, Mark A.; Ghosh, Chuni L.

    2011-05-01

    Laser illumination systems for high brightness imaging through the self-luminosity of explosive events, at Aberdeen Proving Ground and elsewhere, required complex pulse timing, extensive cooling, large-scale laser systems (frequencydoubled flash-pumped Nd:YAG, Cu-vapor, Q-switched ruby), making them difficult to implement for range test illumination in high speed videography. A Vertical Cavity Surface-Emitting Laser (VCSEL) array was designed and implemented with spectral filtering to effectively remove self-luminosity and the fireball from the image, providing excellent background discrimination in a variety of range test scenarios. Further improvements to the system are proposed for applications such as imaging through murky water or dust clouds with optimal penetration of obscurants.

  7. VCSELs for coherent PON

    DEFF Research Database (Denmark)

    Jensen, Jesper Bevensee; Rodes, Roberto; Cheng, Ning;

    2015-01-01

    Recent advances and research on coherent technologies for access networks are discussed and put into context of user demands and standardization work.......Recent advances and research on coherent technologies for access networks are discussed and put into context of user demands and standardization work....

  8. Resonant MEMS tunable VCSEL

    DEFF Research Database (Denmark)

    Ansbæk, Thor; Chung, Il-Sug; Semenova, Elizaveta;

    2013-01-01

    We demonstrate how resonant excitation of a microelectro-mechanical system can be used to increase the tuning range of a vertical-cavity surface-emitting laser two-fold by enabling both blue- and red-shifting of the wavelength. In this way a short-cavity design enabling wide tuning range can be r...

  9. Three-dimensional (3D) monolithically integrated photodetector and WDM receiver based on bulk silicon wafer.

    Science.gov (United States)

    Song, Junfeng; Luo, Xianshu; Tu, Xiaoguang; Jia, Lianxi; Fang, Qing; Liow, Tsung-Yang; Yu, Mingbin; Lo, Guo-Qiang

    2014-08-11

    We propose a novel three-dimensional (3D) monolithic optoelectronic integration platform. Such platform integrates both electrical and photonic devices in a bulk silicon wafer, which eliminates the high-cost silicon-on-insulator (SOI) wafer and is more suitable for process requirements of electronic and photonic integrated circuits (ICs). For proof-of-concept, we demonstrate a three-dimensional photodetector and WDM receiver system. The Ge is grown on a 8-inch bulk silicon wafer while the optical waveguide is defined in a SiN layer which is deposited on top of it, with ~4 µm oxide sandwiched in between. The light is directed to the Ge photodetector from the SiN waveguide vertically by using grating coupler with a Aluminum mirror on top of it. The measured photodetector responsivity is ~0.2 A/W and the 3-dB bandwidth is ~2 GHz. Using such vertical-coupled photodetector, we demonstrated an 8-channel receiver by integrating a 1 × 8 arrayed waveguide grating (AWG). High-quality optical signal detection with up to 10 Gbit/s data rate is demonstrated, suggesting a 80 Gbit/s throughput. Such receiver can be applied to on-chip optical interconnect, DRAM interface, and telecommunication systems.

  10. ZnO on nickel RF micromechanical resonators for monolithic wireless communication applications

    Science.gov (United States)

    Wei, Mian; Avila, Adrian; Rivera, Ivan; Baghelani, Masoud; Wang, Jing

    2017-05-01

    On-chip integrability of high-Q RF passives alongside CMOS transistors is crucial for the implementation of monolithic radio transceivers. One of the most significant bottlenecks in back-end-of-line (BEoL) integration of MEMS devices on CMOS processed wafers is their relatively low thermal budget, which is less than that required for typical MEMS material deposition processes. This paper investigates electroplated nickel as a structural material for piezoelectrically-transduced resonators to demonstrate ZnO-on-nickel resonators with a CMOS-compatible low temperature process for the first time. Aside from the obvious manufacturing cost benefit, electroplated nickel is a reasonable substitute for polycrystalline or single crystal silicon and thin-film microcrystalline diamond device layers, while realizing decent acoustic velocity and moderate Q. Electroplated nickel has been already adopted by MEMSCAP, a multi-user MEMS process foundry, in its MetalMUMPs process. Furthermore, it is observed that a localized annealing process through Joule heating can be exploited to significantly improve the effective mechanical quality factor for the ZnO-on-nickel resonators, which is still lower than the reported AlN resonators. This work demonstrates ZnO-on-nickel piezoelectrically-actuated MEMS resonators and resonator arrays by using an IC compatible low temperature process. There is room for performance improvement by lowering the acoustic energy losses in the ZnO and nickel layers.

  11. Preclinical positron emission tomography scanner based on a monolithic annulus of scintillator: initial design study.

    Science.gov (United States)

    Stolin, Alexander V; Martone, Peter F; Jaliparthi, Gangadhar; Raylman, Raymond R

    2017-01-01

    Positron emission tomography (PET) scanners designed for imaging of small animals have transformed translational research by reducing the necessity to invasively monitor physiology and disease progression. Virtually all of these scanners are based on the use of pixelated detector modules arranged in rings. This design, while generally successful, has some limitations. Specifically, use of discrete detector modules to construct PET scanners reduces detection sensitivity and can introduce artifacts in reconstructed images, requiring the use of correction methods. To address these challenges, and facilitate measurement of photon depth-of-interaction in the detector, we investigated a small animal PET scanner (called AnnPET) based on a monolithic annulus of scintillator. The scanner was created by placing 12 flat facets around the outer surface of the scintillator to accommodate placement of silicon photomultiplier arrays. Its performance characteristics were explored using Monte Carlo simulations and sections of the NEMA NU4-2008 protocol. Results from this study revealed that AnnPET's reconstructed spatial resolution is predicted to be [Formula: see text] full width at half maximum in the radial, tangential, and axial directions. Peak detection sensitivity is predicted to be 10.1%. Images of simulated phantoms (mini-hot rod and mouse whole body) yielded promising results, indicating the potential of this system for enhancing PET imaging of small animals.

  12. 3D position determination in monolithic crystals coupled to SiPMs for PET.

    Science.gov (United States)

    Etxebeste, Ane; Barrio, John; Muñoz, Enrique; Oliver, Josep F; Solaz, Carles; Llosá, Gabriela

    2016-05-21

    The interest in using continuous monolithic crystals in positron emission tomography (PET) has grown in the last years. Coupled to silicon photomultipliers (SiPMs), the detector can combine high sensitivity and high resolution, the two main factors to be maximized in a positron emission tomograph. In this work, the position determination capability of a detector comprised of a [Formula: see text] mm(3) LYSO crystal coupled to an [Formula: see text]-pixel array of SiPMs is evaluated. The 3D interaction position of γ-rays is estimated using an analytical model of the light distribution including reflections on the facets of the crystal. Monte Carlo simulations have been performed to evaluate different crystal reflectors and geometries. The method has been characterized and applied to different cases. Intrinsic resolution obtained with the position estimation method used in this work, applied to experimental data, achieves sub-millimetre resolution values. Average resolution over the detector surface for 5 mm thick crystal is  ∼0.9 mm FWHM and  ∼1.2 mm FWHM for 10 mm thick crystal. Depth of interaction resolution is close to 2 mm FWHM in both cases, while the FWTM is  ∼5.3 mm for 5 mm thick crystal and  ∼9.6 mm for 10 mm thick crystal.

  13. Small animal PET based on 16x16 TSV-MPPCs and monolithic crystals

    Energy Technology Data Exchange (ETDEWEB)

    Gonzalez, Antonio; Aguilar, Albert Talens; Conde, Pablo; Hernadez, Liczandro Hernadez; Vidal San Sebastian, Luis Fernando [Institute for Instrumentation in Molecular Imaging, i3M-CSIC, Valencia (Spain); Salbador, Carlos Correcher; Solsona, Cesar Molinos [Oncovision, Valencia (Spain); Junge, Sven; Lankes, Konrad [Bruker BioSpin (Germany); Benlloch, Jose Maria [Institute for Instrumentation in Molecular Imaging, i3M-CSIC, Valencia (Spain)

    2015-05-18

    In this work we present the design of a small animal PET based on 8 high-density arrays of MPPCs and monolithic scintillators. The MPPCs arrays are composed of 16x16 TSV-type (3x3 mm{sup 2}) elements covering a rough active area of 5x5 cm{sup 2}. A single LYSO block with a thickness of 10mm has been mounted on each detector. Black paint has been applied to the entrance and lateral faces of the crystal to preserve the scintillation light distribution. The axial and transaxial FOVs of one ring are 48 mm and 80 mm, respectively. Each MPPC array has been directly attached to a resistive readout circuit that provides outputs for each row and column of the array. These 32 signals are read with flexible boards 30 cm apart from the PET detector without any additional connectors in between. The PET-system is intended for in-line acquisition in front of MR scanners and as PET-insert inside the sensitive MRI volume. For this purpose, it is necessary to avoid magnetic sensible materials, such as nickel, and to prevent eddy currents in metallic structures induced by the MRI gradients. All detectors are air cooled and kept at temperatures of approximately 20{sup o}C with a variation below 0.05{sup o}C. The intrinsic resolution is 2.2 mm at the crystal center (averaged over all 2.6 mm) when Center of Gravity methods are used to resolve the impact position. This value is about a factor 1.5 better than results obtained with the H8500 PSPMT (64 PADs) and similar scintillators. With an improved collimator with holes with only 0.8mm diameter and a length of 70 mm, an intrinsic detector resolution of 1.1mm was reached. The energy resolutions of ROIs of 1x1 cm{sup 2} showed FWHM values in the range of 14%.

  14. Reprocessing of LEU U-Mo Dispersion and Monolithic Fuels

    Energy Technology Data Exchange (ETDEWEB)

    Vandegrift, G.F.; Jerden, J.; Stepinski, D.C.; Figueroa, J.; Williamson, M.A.; Kleeck, M.A. Van; Blaskovitz, R.J.; Ziegler, A.J.; Maggos, L.E.; Swanson, J.; Fortner, J.; Bakel, A.J. [Chemical Sciences and Engineering Division, Argonne National Laboratory, 9700 S. Cass Ave., Argonne, IL 60439 (United States)

    2011-07-01

    For conversion of high-performance research reactors from high-enriched uranium (HEU) to low-enriched uranium (LEU) fuel, a fuel material with a higher density than uranium aluminide is required. Development studies are underway to develop U-Mo dispersion and monolithic fuels for conversion of several high- performance reactors. For dispersion fuels, development is narrowing down to a composition of U-7Mo dispersed in an aluminium matrix containing {approx}5% silicon. For monolithic fuels to be used in high performance research reactors in the United States, a zirconium-bonded U-10Mo foil appears to be the fuel of choice. For conversion to be realized a back-end disposition path is required for both fuels; one disposition pathway is reprocessing. Argonne National Laboratory is developing a pyroprocess for reprocessing spent monolithic fuel. Pyroprocessing was chosen over conventional aqueous solvent extraction due to the necessity of adding fluoride to the fuel-dissolution solution in order to dissolve the zirconium bonding layer on the U-Mo fuel. The proposed flowsheet and development activities will be described. A literature survey points to the ability to reprocess U-Mo dispersion fuels by an aqueous process, but due to several special characteristics of the fuel, the solvent-extraction flowsheets will be a departure from that normally used for the reprocessing of power reactor fuel. Special concerns that must be addressed in reprocessing these fuels are, for example, the low solubilities of uranyl molybdate, molybdic acid, and silicic acid in nitric acid solutions. This paper will address these concerns and development activities required to overcome them. (author)

  15. 10Gbps monolithic silicon FTTH transceiver for PON

    Science.gov (United States)

    Zhang, J.; Liow, T. Y.; Lo, G. Q.; Kwong, D. L.

    2010-05-01

    We propose a new passive optical network (PON) configuration and a novel silicon photonic transceiver architecture for optical network unit (ONU), eliminating the need for an internal laser source in ONU. We adopt dual fiber network configuration. The internal light source in each of the ONUs is eliminated. Instead, an extra seed laser source in the optical line termination (OLT) operates in continuous wave mode to serve the ONUs in the PON as a shared and centralized laser source. λ1 from OLT Tx and λ2 from the seed laser are combined by using a WDM combiner and connected to serve the multiple ONUs through the downstream fibers. The ONUs receive the data in λ1. Meanwhile, the ONUs encode and transmit data in λ2, which are sent back to OLT. The monolithic ONU transceiver contains a wavelength-division-multiplexing (WDM) filter component, a silicon modulator and a Ge photo-detector. The WDM in ONU selectively guides λ1 to the Ge-PD where the data in λ1 are detected and converted to electrical signals, and λ2 to the transmitter where the light is modulated by upstream data. The modulated optical signals in λ2 from ONUs are connected back to OLT through upstream fibers. The monolithic ONU transceiver chip size is only 2mm by 4mm. The crosstalk between the Tx and Rx is measured to be less than -20dB. The transceiver chip is integrated on a SFP+ transceiver board. Both Tx and Rx demonstrated data rate capabilities of up to 10Gbps. By implementing this scheme, the ONU transceiver size can be significantly reduced and the assembly processes will be greatly simplified. The results demonstrate the feasibility of mass manufacturing monolithic silicon ONU transceivers via low cost

  16. W-band monolithic oscillator using InAlAs/InGaAs HEMT

    Science.gov (United States)

    Kwon, Y.; Pavlidis, D.; Tutt, M.; Ng, G. I.; Lai, R.

    1990-01-01

    A W-band monolithic integrated oscillator circuit was designed and fabricated using submicron HEMT technology. The oscillation frequency was around 81 GHz and the power was -7 dBm at the chip level. This is the first report of an InAlAs/InGaAs monolithic oscillator operating at the W-band.

  17. Recent advances in the preparation and application of monolithic capillary columns in separation science

    Energy Technology Data Exchange (ETDEWEB)

    Hong, Tingting; Yang, Xi; Xu, Yujing [Department of Analytical Chemistry, China Pharmaceutical University, Nanjing, 210009 (China); Key Laboratory of Drug Quality Control and Pharmacovigilance, Ministry of Education, Nanjing, 210009 (China); Ji, Yibing, E-mail: jiyibing@msn.com [Department of Analytical Chemistry, China Pharmaceutical University, Nanjing, 210009 (China); Key Laboratory of Drug Quality Control and Pharmacovigilance, Ministry of Education, Nanjing, 210009 (China)

    2016-08-10

    Novel column technologies involving various materials and efficient reactions have been investigated for the fabrication of monolithic capillary columns in the field of analytical chemistry. In addition to the development of these miniaturized systems, a variety of microscale separation applications have achieved noteworthy results, providing a stepping stone for new types of chromatographic columns with improved efficiency and selectivity. Three novel strategies for the preparation of capillary monoliths, including ionic liquid-based approaches, nanoparticle-based approaches and “click chemistry”, are highlighted in this review. Furthermore, we present the employment of state-of-the-art capillary monolithic stationary phases for enantioseparation, solid-phase microextraction, mixed-mode separation and immobilized enzyme reactors. The review concludes with recommendations for future studies and improvements in this field of research. - Highlights: • Preparation of novel monolithic capillary columns have shown powerful potential in analytical chemistry field. • Various materials including ionic liquids and nanoparticles involved into capillary monolithic micro-devices are concluded. • Click chemistry strategy applied for preparing monolithic capillary columns is reviewed. • Recent strategies utilized in constructing different capillary monoliths for enantiomeric separation are summarized. • Advancement of capillary monoliths for complex samples analysis is comprehensively described.

  18. Preparation and applications of hybrid organic-inorganic monoliths: a review.

    Science.gov (United States)

    Zhu, Tao; Row, Kyung Ho

    2012-06-01

    This review presents an overview of the properties of hybrid organic-inorganic monolithic materials and summarizes the recent developments in the preparation and applications of these hybrid monolithic materials. Hybrid monolithic materials with porosities, surface functionalities, and fast dynamic transport have developed rapidly, and have been used in a wide range of applications owing to the low cost, good stability, and excellent performance. Basically, these materials can be divided into two major types according to the chemical composition: hybrid silica-based monolith (HSM) and hybrid polymer-based monolith (HPM). Compared to the HPM, HSM monolith has been attracting most wide attentions, and it is commonly synthesized by the sol-gel process. The conventional preparation procedures of two type's hybrid organic-inorganic monoliths are addressed. Applications of hybrid organic-inorganic monoliths in optical devices, capillary microextraction (CME), capillary electrochromatography (CEC), high performance liquid chromatography (HPLC), and chiral separation are also reviewed. © 2012 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  19. Preparation of a zeolite-modified polymer monolith for identification of synthetic colorants in lipsticks

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Huiqi; Li, Zheng [College of Chemistry, Jilin University, Changchun 130012 (China); Niu, Qian [Jilin Entry-Exit Inspection and Quarantine Bureau, Changchun 130062 (China); Ma, Jiutong [College of Chemistry, Jilin University, Changchun 130012 (China); Jia, Qiong, E-mail: jiaqiong@jlu.edu.cn [College of Chemistry, Jilin University, Changchun 130012 (China)

    2015-10-30

    Graphical abstract: Poly(methacrylic acid-ethylene dimethacrylate) monolithic column embedded with zeolites was prepared and employed for the polymer monolith microextraction of colorants combined with HPLC. - Highlights: • Zeolite, as a kind of mesoporous material, was firstly combined with PMME. • Zeolite@poly(MAA-EDMA) monolith columns were prepared for the enrichment of colorants. • Zeolite@poly(MAA-EDMA) monolith columns demonstrated relatively high extraction capacity. - Abstract: A novel zeolite-modified poly(methacrylic acid-ethylenedimethacrylate) (zeolite@poly(MAA-EDMA)) monolithic column was prepared with the in situ polymerization method and employed in polymer monolith microextraction for the separation and preconcentration of synthetic colorants combined with high performance liquid chromatography. The polymer was characterized by scanning electronmicroscopy, Fourier-transform infrared spectroscopy, X-ray photoelectron spectroscopy, and thermo-gravimetric analysis. Various parameters affecting the extraction efficiency were investigated and optimized. Under the optimum experimental conditions, we obtained acceptable linearities, low limits of detection, and good intra-day/inter-day relative standard deviations. The method was applied to the determination of synthetic colorants in lipsticks with recoveries ranged from 70.7% to 109.7%. Compared with conventional methacrylic acid-based monoliths, the developed monolith exhibited high enrichment capacity because of the introduction of zeolites into the preparation process. The extraction efficiency followed the order: zeolite@poly(MAA-EDMA) > poly(MAA-EDMA) > direct HPLC analysis.

  20. Hydrophobic polymer monoliths as novel phase separators: Application in continuous liquid-liquid extraction systems

    NARCIS (Netherlands)

    Peroni, D.; Vanhoutte, D.; Vilaplana, F.; Schoenmakers, P.; de Koning, S.; Janssen, H.-G.

    2012-01-01

    Hydrophobic macroporous polymer monoliths are shown to be interesting materials for the construction of "selective solvent gates". With the appropriate surface chemistry and porous properties the monoliths can be made permeable only for apolar organic solvents and not for water. Different poly(butyl

  1. Functionalization of hybrid monolithic columns via thiol-ene click reaction for proteomics analysis.

    Science.gov (United States)

    Liu, Zhongshan; Liu, Jing; Liu, Zheyi; Wang, Hongwei; Ou, Junjie; Ye, Mingliang; Zou, Hanfa

    2017-05-19

    The vinyl-functionalized hybrid monolithic columns (75 and 150μm i.d.) were prepared via sol-gel chemistry of tetramethoxysilane (TMOS) and vinyltrimethoxysilane (VTMS). The content of accessible vinyl groups was further improved after the monolithic column was post-treated with vinyldimethylethoxysilane (VDMES). The surface properties of monolithic columns were tailored via thiol-ene click reaction by using 1-octadecanethiol, sodium 3-mercapto-1-propanesulfonate and 2,2'-(ethylenedioxy)diethanethiol/vinylphosphonic acid, respectively. The preparing octadecyl-functionalized monolithic columns were adopted for proteomics analysis in cLC-MS/MS. A 37-cm-long×75-μm-i.d. monolithic column could identify 3918 unique peptides and 1067 unique proteins in the tryptic digest of proteins from HeLa cells. When a 90-cm-long×75-μm-i.d. monolithic column was used, the numbers of unique peptides and proteins were increased by 82% and 32%, respectively. Furthermore, strong cation exchange (SCX) monolithic columns (4cm in length×150μm i.d.) were also prepared and coupled with the 37-cm-long×75-μm-i.d. octadecyl-functionalized monolithic column for two-dimensional SCX-RPLC-MS/MS analysis, which could identify 17114 unique peptides and 3211 unique proteins. Copyright © 2017 Elsevier B.V. All rights reserved.

  2. A monolithically integrated torsional CMOS-MEMS relay

    Science.gov (United States)

    Riverola, M.; Sobreviela, G.; Torres, F.; Uranga, A.; Barniol, N.

    2016-11-01

    We report experimental demonstrations of a torsional microelectromechanical (MEM) relay fabricated using the CMOS-MEMS approach (or intra-CMOS) which exploits the full foundry inherent characteristics enabling drastic reduction of the fabrication costs and batch production. In particular, the relay is monolithically integrated in the back end of line of a commercial standard CMOS technology (AMS 0.35 μm) and released by means of a simple one-step mask-less wet etching. The fabricated torsional relay exhibits an extremely steep switching behaviour symmetrical about both contact sides with an on-state contact resistance in the k Ω -range throughout the on-off cycling test.

  3. Remote Sensing with Commutable Monolithic Laser and Detector

    Science.gov (United States)

    2016-01-01

    The ubiquitous trend toward miniaturized sensing systems demands novel concepts for compact and versatile spectroscopic tools. Conventional optical sensing setups include a light source, an analyte interaction region, and a separate external detector. We present a compact sensor providing room-temperature operation of monolithic surface-active lasers and detectors integrated on the same chip. The differentiation between emitter and detector is eliminated, which enables mutual commutation. Proof-of-principle gas measurements with a limit of detection below 400 ppm are demonstrated. This concept enables a crucial miniaturization of sensing devices. PMID:27785455

  4. Inherent polarization entanglement generated from a monolithic semiconductor chip

    DEFF Research Database (Denmark)

    Horn, Rolf T.; Kolenderski, Piotr; Kang, Dongpeng

    2013-01-01

    Creating miniature chip scale implementations of optical quantum information protocols is a dream for many in the quantum optics community. This is largely because of the promise of stability and scalability. Here we present a monolithically integratable chip architecture upon which is built...... a photonic device primitive called a Bragg reflection waveguide (BRW). Implemented in gallium arsenide, we show that, via the process of spontaneous parametric down conversion, the BRW is capable of directly producing polarization entangled photons without additional path difference compensation, spectral...... as a serious contender on which to build large scale implementations of optical quantum processing devices....

  5. A Monolithic Filter Cavity for Experiments in Quantum Optics

    CERN Document Server

    Palittapongarnpim, Pantita; Lvovsky, A I

    2012-01-01

    By applying a high-reflectivity dielectric coating on both sides of a commercial plano-convex lens, we produce a stable monolithic Fabry-Perot cavity suitable for use as a narrow band filter in quantum optics experiments. The resonant frequency is selected by means of thermal expansion. Owing to the long term mechanical stability, no optical locking techniques are required. We characterize the cavity performance as an optical filter, obtaining a 45 dB suppression of unwanted modes while maintaining a transmission of 60%.

  6. A novel carbon fiber based porous carbon monolith

    Energy Technology Data Exchange (ETDEWEB)

    Burchell, T.D.; Klett, J.W.; Weaver, C.E.

    1995-06-01

    A novel porous carbon material based on carbon fibers has been developed. The material, when activated, develops a significant micro- or mesopore volume dependent upon the carbon fiber type utilized (isotropic pitch or polyacrylonitrile). The materials will find applications in the field of fluid separations or as a catalyst support. Here, the manufacture and characterization of our porous carbon monoliths are described. A novel adsorbent carbon composite material has been developed comprising carbon fibers and a binder. The material, called carbon fiber composite molecular sieve (CFCMS), was developed through a joint research program between Oak Ridge National Laboratory (ORNL) and the University of Kentucky, Center for Applied Energy Research (UKCAER).

  7. Rapid Preparation of Monolithic Columns for Capillary Electrochromatography Separation

    Institute of Scientific and Technical Information of China (English)

    Wen Jun GONG; Yi Jun ZHANG; Yu Ping ZHANG; Seong Ho CHOI

    2006-01-01

    Fritless packed silica gel columns were prepared using sol-gel technology. The part of a75 μm i.d. capillary was filled with a mixture of methacryloxypropyltrimethoxysilane, toluene and hydrochloric acid. Four different photoinitiators such as benzoin methyl ether, Irgacure 819,Irgacure 1700 and irgacure 1800 were added in the presence or absence of sodium dodecyl sulfate during the polymerization process. The above eight solutions were irradiated at 365 nm about5-10 min to prepare the porous monolithic sol-gel columns by a one-step process.

  8. Hybrid and monolithic integration of planar lightwave circuits (PLCs)

    Science.gov (United States)

    Chen, Ray T.

    2008-02-01

    In this paper, we review the status of monolithic and hybrid integration of planar lightwave circuits (PLCs). Building blocks needed for system integration based on polymeric materials, III-V semiconductor materials, LiNbO 3 and SOI on Silicon are summarized with pros and cons. Due to the maturity of silicon CMOS technology, silicon becomes the platform of choice for optical application specific integrated circuits (OASICs). However, the indirect bandgap of silicon makes the formation of electrically pumped silicon laser a remote plausibility which requires hybrid integration of laser sources made out of III-V compound semicouductor.

  9. Preparation of a biomimetic polyphosphorylcholine monolithic column for immobilized artificial membrane chromatography.

    Science.gov (United States)

    Zhao, XiangLong; Chen, WeiJia; Zhou, ZhengYin; Wang, QiQin; Liu, ZhengHua; Moaddel, Ruin; Jiang, ZhengJin

    2015-08-14

    The present work aims to prepare a novel phosphatidylcholine functionalized monolithic stationary phase by in situ co-polymerization of 12-methacryloyl dodecylphosphocholine (MDPC) and ethylene dimethacrylate (EDMA) for immobilized artificial membrane chromatography. Scanning electron microscopy, energy dispersive X-ray spectroscopy, FT-IR spectroscopy, pore size distribution analysis, ζ-potential analysis and micro-HPLC were used to evaluate the monolithic structure and physicochemical properties. Satisfactory morphology, high mechanical stability, good permeability and chromatographic performance were obtained on the optimized monolithic columns. A typical reverse-phase retention mechanism was observed over a wide range of organic solvent content (acetonitrilecolumn (IAM.PC.DD2) and poly(MDPC-co-EDMA) monolith. This novel poly(MDPC-co-EDMA) monolith exhibited good potential for studying the drug-membrane interaction.

  10. Synthesis and methane storage of binder-free porous graphene monoliths

    Institute of Scientific and Technical Information of China (English)

    Guoqing Ning; Hao Wang; Xiaoxin Zhang; Chenggen Xu; Guangjin Chen; Jinsen Gao

    2013-01-01

    Nanomesh graphene (NMG) obtained by template chemical vapor deposition was used to synthesize the binder-free graphene monoliths by simple tablet pressing.The stacking manner of the NMG sheets was crucial to the cohesion interaction between the graphene sheets,only the NMG materials with a loosely stacking manner could be pressed into binder-free monoliths.At the tableting pressure of 2-8 MPa,both the bulk densities and the specific surface areas of the monoliths keep nearly constant as the tableting pressure increases,indicating that the NMG monoliths have obvious elasticity and a porous structure due to the large corrugations and the mesh structures of the graphene sheets.As a result,an extraordinary methane storage capacity of 236 (v/v) at 9MPa was obtained in the graphene monolith prepared by tableting at 4 MPa.

  11. Monitoring catalysts at work in their final form: spectroscopic investigations on a monolithic catalyst

    DEFF Research Database (Denmark)

    Rasmussen, Søren B.; Bañares, Miguel A.; Bazin, Philippe;

    2012-01-01

    A monolithic vanadia–titania based catalyst has been subjected to studies with in situ FTIR spectroscopy coupled with mass spectrometry, during the SCR (Selective Catalytic Reduction) reaction. A device based on a transmission reactor cell for monolithic samples was constructed, dedicated to the ...... with other surface or bulk sensitive techniques, e.g. Raman and UV-vis spectroscopy.......A monolithic vanadia–titania based catalyst has been subjected to studies with in situ FTIR spectroscopy coupled with mass spectrometry, during the SCR (Selective Catalytic Reduction) reaction. A device based on a transmission reactor cell for monolithic samples was constructed, dedicated....... The observations reported here serve as a demonstration of the great potential for the application of operando spectroscopy on monolithic systems. This cross disciplinary approach aims to identify reaction pathways, active sites, intermediate- and spectator-species for catalytic reactions under truly industrial...

  12. Coupling in reflector arrays

    DEFF Research Database (Denmark)

    Appel-Hansen, Jørgen

    1968-01-01

    In order to reduce the space occupied by a reflector array, it is desirable to arrange the array antennas as close to each other as possible; however, in this case coupling between the array antennas will reduce the reflecting properties of the reflector array. The purpose of the present communic...

  13. New 3-D microarray platform based on macroporous polymer monoliths.

    Science.gov (United States)

    Rober, M; Walter, J; Vlakh, E; Stahl, F; Kasper, C; Tennikova, T

    2009-06-30

    Polymer macroporous monoliths are widely used as efficient sorbents in different, mostly dynamic, interphase processes. In this paper, monolithic materials strongly bound to the inert glass surface are suggested as operative matrices at the development of three-dimensional (3-D) microarrays. For this purpose, several rigid macroporous copolymers differed by reactivity and hydrophobic-hydrophilic properties were synthesized and tested: (1) glycidyl methacrylate-co-ethylene dimethacrylate (poly(GMA-co-EDMA)), (2) glycidyl methacrylate-co-glycerol dimethacrylate (poly(GMA-co-GDMA)), (3) N-hydroxyphthalimide ester of acrylic acid-co-glycidyl methacrylate-co-ethylene dimethacrylate (poly(HPIEAA-co-GMA-co-EDMA)), (4) 2-cyanoethyl methacrylate-co-ethylene dimethacrylate (poly(CEMA-co-EDMA)), and (5) 2-cyanoethyl methacrylate-co-2-hydroxyethyl methacrylate-co-ethylene dimethacrylate (poly(CEMA-co-HEMA-co-EDMA)). The constructed devices were used as platforms for protein microarrays construction and model mouse IgG-goat anti-mouse IgG affinity pair was used to demonstrate the potential of developed test-systems, as well as to optimize microanalytical conditions. The offered microarray platforms were applied to detect the bone tissue marker osteopontin directly in cell culture medium.

  14. Methacrylate-based monolithic layers for planar chromatography of polymers.

    Science.gov (United States)

    Maksimova, E F; Vlakh, E G; Tennikova, T B

    2011-04-29

    A series of macroporous monolithic methacrylate-based materials was synthesized by in situ free radical UV-initiated copolymerization of functional monomers, such as glycidyl methacrylate (GMA), butyl methacrylate (BuMA), 2-aminoethyl methacrylate (AEMA), 2-hydroxyethyl methacrylate (HEMA) and 2-cyanoethyl methacrylate (CEMA), with crosslinking agent, namely, ethylene glycol dimethacrylate (EDMA). The materials obtained were applied as the stationary phases in simple and robust technique - planar chromatography (PLC). The method of separation layer fabrication representing macroporous polymer monolith bound to the specially prepared glass surface was developed and optimized. The GMA-EDMA and BuMA-EDMA matrixes were successfully applied for the separation of low molecular weight compounds (the mixture of several dies), as well as poly(vinylpyrrolidone) and polystyrene homopolymers of different molecular weights using reversed-phase mechanism. The materials based on copolymers AEMA-HEMA-EDMA and CEMA-HEMA-EDMA were used for normal-phase PLC separation of 2,4-dinitrophenyl amino acids and polystyrene standards.

  15. Squeezed light from a diamond-turned monolithic cavity

    CERN Document Server

    Brieussel, A; Campbell, G; Guccione, G; Janousek, J; Hage, B; Buchler, B C; Treps, N; Fabre, C; Fang, F Z; Li, X Y; Symul, T; Lam, P K

    2016-01-01

    For some crystalline materials, a regime can be found where continuous ductile cutting is feasible. Using precision diamond turning, such materials can be cut into complex optical components with high surface quality and form accuracy. In this work we use diamond-turning to machine a monolithic, square-shaped, doubly-resonant $LiNbO_3$ cavity with two flat and two convex facets. When additional mild polishing is implemented, the Q-factor of the resonator is found to be limited only by the material absorption loss. We show how our monolithic square resonator may be operated as an optical parametric oscillator that is evanescently coupled to free-space beams via birefringent prisms. The prism arrangement allows for independent and large tuning of the fundamental and second harmonic coupling rates. We measure $2.6\\pm0.5$ dB of vacuum squeezing at 1064 nm using our system. Potential improvements to obtain higher degrees of squeezing are discussed.

  16. Fabrication of Monolithic RERTR Fuels by Hot Isostatic Pressing

    Energy Technology Data Exchange (ETDEWEB)

    Jan-Fong Jue; Blair H. Park; Curtis R. Clark; Glenn A. Moore; Dennis D. Keiser, Jr.

    2010-11-01

    The RERTR (Reduced Enrichment for Research and Test Reactors) Program is developing advanced nuclear fuels for high-power test reactors. Monolithic fuel design provides higher uranium loading than that of the traditional dispersion fuel design. Hot isostatic pressing is a promising process for low-cost batch fabrication of monolithic RERTR fuel plates for these high-power reactors. Bonding U Mo fuel foil and 6061 Al cladding by hot isostatic press bonding was successfully developed at Idaho National Laboratory. Due to the relatively high processing temperature, the interaction between fuel meat and aluminum cladding is a concern. Two different methods were employed to mitigate this effect: (1) a diffusion barrier and (2) a doping addition to the interface. Both types of fuel plates have been fabricated by hot isostatic press bonding. Preliminary results show that the direct fuel/cladding interaction during the bonding process was eliminated by introducing a thin zirconium diffusion barrier layer between the fuel and the cladding. Fuel plates were also produced and characterized with a silicon-rich interlayer between fuel and cladding. This paper reports the recent progress of this developmental effort and identifies the areas that need further attention.

  17. Macroporous monoliths for trace metal extraction from seawater

    Energy Technology Data Exchange (ETDEWEB)

    Yue, Yanfeng; Mayes, Richard; Gill, Gary A.; Kuo, Li-Jung; Wood, Jordana R.; Binder, Andrew; Brown, Suree; Dai, Sheng

    2015-05-29

    The viability of seawater-based uranium recovery depends on the uranium adsorption rate and capacity, since the concentration of uranium in the oceans is relatively low (3.3 μgL⁻¹). An important consideration for a fast adsorption is to maximize the adsorption properties of adsorbents such as surface areas and pore structures, which can greatly improve the kinetics of uranium extraction and the adsorption capacity simultaneously. Following this consideration, macroporous monolith adsorbents were prepared from the copolymerization of acrylonitrile (AN) and N,N’-methylenebis(acrylamide) (MBAAm) based on a cryogel method using both hydrophobic and hydrophilic monomers. The monolithic sorbents were tested with simulated seawater containing a high uranyl concentration (–6 ppm) and the uranium adsorption results showed that the adsorption capacities are strongly influenced by the ratio of monomer to the crosslinker, i.e., the density of the amidoxime groups. The preliminary seawater testing indicates the high salinity content of seawater does not hinder the adsorption of uranium.

  18. Monolithically Integrated Ge-on-Si Active Photonics

    Directory of Open Access Journals (Sweden)

    Jifeng Liu

    2014-07-01

    Full Text Available Monolithically integrated, active photonic devices on Si are key components in Si-based large-scale electronic-photonic integration for future generations of high-performance, low-power computation and communication systems. Ge has become an interesting candidate for active photonic devices in Si photonics due to its pseudo-direct gap behavior and compatibility with Si complementary metal oxide semiconductor (CMOS processing. In this paper, we present a review of the recent progress in Ge-on-Si active photonics materials and devices for photon detection, modulation, and generation. We first discuss the band engineering of Ge using tensile strain, n-type doping, Sn alloying, and separate confinement of Γ vs. L electrons in quantum well (QW structures to transform the material towards a direct band gap semiconductor for enhancing optoelectronic properties. We then give a brief overview of epitaxial Ge-on-Si materials growth, followed by a summary of recent investigations towards low-temperature, direct growth of high crystallinity Ge and GeSn alloys on dielectric layers for 3D photonic integration. Finally, we review the most recent studies on waveguide-integrated Ge-on-Si photodetectors (PDs, electroabsorption modulators (EAMs, and laser diodes (LDs, and suggest possible future research directions for large-scale monolithic electronic-photonic integrated circuits on a Si platform.

  19. Monolithic integrated optic fiber Bragg grating sensor interrogator

    Science.gov (United States)

    Mendoza, Edgar A.; Esterkin, Yan; Kempen, Cornelia; Sun, Songjian

    2010-04-01

    Fiber Bragg gratings (FBGs) are a mature sensing technology that has gained rapid acceptance in civil, aerospace, chemical and petrochemical, medicine, aviation and automotive industries. Fiber Bragg grating sensors can be use for a variety of measurements including strain, stress, vibration, acoustics, acceleration, pressure, temperature, moisture, and corrosion distributed at multiple locations within the structure using a single fiber element. The most prominent advantages of FBGs are: small size and light weight, multiple FBG transducers on a single fiber, and immunity to radio frequency interference. A major disadvantage of FBG technology is that conventional state-of-the-art fiber Bragg grating interrogation systems are typically bulky, heavy, and costly bench top instruments that are assembled from off-the-shelf fiber optic and optical components integrated with a signal electronics board into an instrument console. Based on the need for a compact FBG interrogation system, this paper describes recent progress towards the development of a miniature fiber Bragg grating sensor interrogator (FBG-TransceiverTM) system based on multi-channel monolithic integrated optic sensor microchip technology. The integrated optic microchip technology enables the monolithic integration of all of the functionalities, both passive and active, of conventional bench top FBG sensor interrogators systems, packaged in a miniaturized, low power operation, 2-cm x 5-cm small form factor (SFF) package suitable for the long-term structural health monitoring in applications where size, weight, and power are critical for operation.

  20. Monolithic molecularly imprinted polymeric capillary columns for isolation of aflatoxins.

    Science.gov (United States)

    Szumski, Michał; Grzywiński, Damian; Prus, Wojciech; Buszewski, Bogusław

    2014-10-17

    Monolithic molecularly imprinted polymers extraction columns have been prepared in fused-silica capillaries by UV or thermal polymerization in a two-step process. First, a poly-(trimethylolpropane trimethacrylate) (polyTRIM) core monolith was synthesized either by UV or thermal polymerization. Then it was grafted with the mixture of methacrylic acid (MAA) as a functional monomer, ethylene dimethacrylate (EDMA) as a cross-linking agent, 5,7-dimethoxycoumarin (DMC) as an aflatoxin-mimicking template, toluene as a porogen solvent and 2,2-azobis-(2-methylpropionitrile) (AIBN) as an initiator of the polymerization reaction. Different thermal condition of the photografting and different concentrations of the grafting mixture were tested during polymerization. The extraction capillary columns were evaluated in the terms of their hydrodynamic and chromatographic properties. Retention coefficients for aflatoxin B1 and DMC were used for assessment of the selectivity and imprinting factor. The obtained results indicate that the temperature of photografting and concentration of the grafting mixture are key parameters that determine the quality of the prepared MIPs. From the MIP columns characterized by the highest permeability the column of the highest imprinting factor was applied for isolation of aflatoxins B1, B2, G1 and G2 from the model aqueous sample followed by on-line chromatographic separation. The process was performed using a micro-MISPE-microLC-LIF system of a novel design, which allowed for detection of the eluates from the sample preparation part as well as from the chromatographic separation.