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Sample records for metallurgy fabrication

  1. Powder Metallurgy Fabrication of Molybdenum Accelerator Target Disks

    Energy Technology Data Exchange (ETDEWEB)

    Lowden, Richard Andrew [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Kiggans Jr., James O. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Nunn, Stephen D. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Parten, Randy J. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2015-07-01

    Powder metallurgy approaches for the fabrication of accelerator target disks are being examined to support the development of Mo-99 production by NorthStar Medical Technologies, LLC. An advantage of powder metallurgy is that very little material is wasted and, at present, dense, quality parts are routinely produced from molybdenum powder. The proposed targets, however, are thin wafers, 29 mm in diameter with a thickness of 0.5 mm, with very stringent dimensional tolerances. Although tooling can be machined to very high tolerance levels, the operations of powder feed, pressing and sintering involve complicated mechanisms, each of which affects green density and shrinkage, and therefore the dimensions and shape of the final product. Combinations of powder morphology, lubricants and pressing technique have been explored to produce target disks with minimal variations in thickness and little or no distortion. In addition, sintering conditions that produce densities for optimum target dissolvability are being determined.

  2. Investigation of a thermoplastic-powder metallurgy process for the fabrication of porous niobium rods

    International Nuclear Information System (INIS)

    Nordin, D.R.

    1978-06-01

    The feasibility of using a thermoplastic-powder metallurgy technique for the fabrication of porous niobium rods was investigated. Some early problems were overcome to successfully extrude the polymer coated niobium powder into long lengths. The effects of certain process variables were investigated. Residual porosity and extrusion pressure were found to be regulated by the polymer fraction. The procedures for taking the extruded polystyrene--niobium rods through the heat treatments to the final, tin infiltrated stage are explained

  3. Porous titanium scaffolds fabricated using a rapid prototyping and powder metallurgy technique.

    Science.gov (United States)

    Ryan, Garrett E; Pandit, Abhay S; Apatsidis, Dimitrios P

    2008-09-01

    One of the main issues in orthopaedic implant design is the fabrication of scaffolds that closely mimic the biomechanical properties of the surrounding bone. This research reports on a multi-stage rapid prototyping technique that was successfully developed to produce porous titanium scaffolds with fully interconnected pore networks and reproducible porosity and pore size. The scaffolds' porous characteristics were governed by a sacrificial wax template, fabricated using a commercial 3D-printer. Powder metallurgy processes were employed to generate the titanium scaffolds by filling around the wax template with titanium slurry. In the attempt to optimise the powder metallurgy technique, variations in slurry concentration, compaction pressure and sintering temperature were investigated. By altering the wax design template, pore sizes ranging from 200 to 400 microm were achieved. Scaffolds with porosities of 66.8 +/- 3.6% revealed compression strengths of 104.4+/-22.5 MPa in the axial direction and 23.5 +/- 9.6 MPa in the transverse direction demonstrating their anisotropic nature. Scaffold topography was characterised using scanning electron microscopy and microcomputed tomography. Three-dimensional reconstruction enabled the main architectural parameters such as pore size, interconnecting porosity, level of anisotropy and level of structural disorder to be determined. The titanium scaffolds were compared to their intended designs, as governed by their sacrificial wax templates. Although discrepancies in architectural parameters existed between the intended and the actual scaffolds, overall the results indicate that the porous titanium scaffolds have the properties to be potentially employed in orthopaedic applications.

  4. U3O8 from resin for powder-metallurgy fabrication of reactor fuel

    International Nuclear Information System (INIS)

    Mosley, W.C. Jr.

    1982-01-01

    A study was conducted to determine if cation exchange resin could be used to produce U 3 O 8 powder suitable for use in powder metallurgy fabrication of fuel tubes for production reactors at the Savannah River Plant (SRP). U 3 O 8 powders have been produced from three cation exchange resins: DOWEX (Dow Chemical Co.) 50W, AG (Bio-Rad Laboratories, Richmond, California) MP-50, and Bio-REX (Bio-Rad Laboratories, Richmond, California). This study included characterization of the thermal decomposition of uranium-loaded resins, measurement of properties of resin-based U 3 O 8 powders, and metallographic examination of U 3 O 8 -Al cores in extruded fuel tubes. Results to date show that AG MP-50 appears to be the best resin for producing U 3 O 8 powder suitable for the PM process. 20 figures

  5. Study on titanium-magnesium composites with bicontinuous structure fabricated by powder metallurgy and ultrasonic infiltration.

    Science.gov (United States)

    Jiang, S; Huang, L J; An, Q; Geng, L; Wang, X J; Wang, S

    2018-02-14

    Titanium-magnesium (Ti-Mg) composites with bicontinuous structure have been successfully fabricated by powder metallurgy and ultrasonic infiltration for biomaterial potential. In the composites, Ti phase is distributed continuously by sintering necks, while Mg phase is also continuous, distributing at the interconnected pores surrounding the Ti phase. The results showed that the fabricated Ti-Mg composites exhibited low modulus and high strength, which are very suitable for load bearing biomedical materials. The composites with 100 µm and 230 µm particle sizes exhibited Young's modulus of 37.6 GPa and 23.4 GPa, 500.7 MPa and 340 MPa of compressive strength and 631.5 MPa and 375.2 MPa of bending strength, respectively. Moreover, both of the modulus and strength of the composites increase with decreasing of Ti particle sizes. In vitro study has been done for the preliminary evaluation of the Ti-Mg composites. Copyright © 2018 Elsevier Ltd. All rights reserved.

  6. Fabrication of Fe-Cr-Mo powder metallurgy steel via a mechanical-alloying process

    Science.gov (United States)

    Park, Jooyoung; Jeong, Gowoon; Kang, Singon; Lee, Seok-Jae; Choi, Hyunjoo

    2015-11-01

    In this study, we employed a mechanical-alloying process to manufacture low-alloy CrL and CrM steel powders that have similar specifications to their water-atomized counterparts. X-ray diffraction showed that Mo and Cr are alloyed in Fe after four cycles of planetary milling for 1 h at 150 RPM with 15-min pauses between the cycles (designated as P2C4 process). Furthermore, the measured powder size was found to be similar to that of the water-atomized counterparts according to both scanning electron microscope images and laser particle size analysis. The samples were sintered at 1120 °C, after which the P2C4-milled CrL showed similar hardness to that of water-atomized CrL, whereas the P2C4-milled CrM showed about 45% lower hardness than that of its water-atomized counterpart. Water-atomized CrM consists of a well-developed lathtype microstructure (bainite or martensite), while a higher fraction of polygonal ferrite is observed in P2C4-milled CrM. This phase difference causes the reduction of hardness in the P2C4-milled CrM, implying that the phase transformation behavior of specimens produced via powder metallurgy is influenced by the powder fabrication method.

  7. Current programmes of Metallurgy Division (1991)

    International Nuclear Information System (INIS)

    1991-01-01

    Current research and development programmes of the Metallurgy Division are listed under the headings: 1)Thrust Areas, 2)High Temperature Materials Section, 3)Chemical Metallurgy Section, 4)Metallurgical Thermochemistry Section, 5)Physical Metallurgy Section, 6)Mechanical Metallurgy Section, 7)Corrosion Metallurgy Section, 8)Electrochemical Science and Technology Section, 9)Ceramics Section, and 10)Fabrication and Maintenance Group. A list of equipment in the Division and a list of sciientific personnel of the Division are also given. (M.G.B.)

  8. Fabrication of homogeneously dispersed graphene/Al composites by solution mixing and powder metallurgy

    Science.gov (United States)

    Zeng, Xiang; Teng, Jie; Yu, Jin-gang; Tan, Ao-shuang; Fu, Ding-fa; Zhang, Hui

    2018-01-01

    Graphene-reinforced aluminum (Al) matrix composites were successfully prepared via solution mixing and powder metallurgy in this study. The mechanical properties of the composites were studied using microhardness and tensile tests. Compared to the pure Al alloy, the graphene/Al composites showed increased strength and hardness. A tensile strength of 255 MPa was achieved for the graphene/Al composite with only 0.3wt% graphene, which has a 25% increase over the tensile strength of the pure Al matrix. Raman spectroscopy, Fourier transform infrared spectroscopy, scanning electron microscopy, and transmission electron microscopy were used to investigate the morphologies, chemical compositions, and microstructures of the graphene and the graphene/Al composites. On the basis of fractographic evidence, a relevant fracture mechanism is proposed.

  9. Filamentary niobium--tin superconductors fabricated by a powder metallurgy approach

    International Nuclear Information System (INIS)

    Hemachalam, K.

    1976-02-01

    Procedures are described for making superconducting tapes and wires containing filments of the A-15 compound, Nb 3 Sn, by powder metallurgy techniques. The Nb 3 Sn filaments, typically 1-5 m thick, are formed by a short heat treatment. The effects of process variables on the microstructure of the tapes and wires were investigated. Microstructural aspects were examined by optical metallography and transmission electron microscopy. A pulsed field technique was used to determine the critical current density, J/sub c/, at 4.2 0 K as a function of transverse magnetic field up to 170 kG. Satisfactory agreement was oserved between these results and data obtained under steady fields of up to 100 kG. The J/sub c/ of the conductors are related to their individual filament morphologies resulting from the different thermo-mechanical histories. The effect of heat treatment conditions on critical current and transition temperature, T/sub c/, is presented. Through process modifications, optimal values or ranges are developed for the metallugical variables in order to maximize the superconducting properties. The inductively measured T/sub c/ of the conductors is about 17.9 +- 0.1 0 . The values of J/sub c/ for the wires computed on the basis of Nb 3 Sn and niobium matrix are 2.3 x 10 5 A/cm 2 at a transverse pulse field of 50 kG, 1.1 x 10 5 A/cm 2 at 100 kG and 7.5 x 10 4 A/cm 2 at 150 kG

  10. Investigation of hydrostatic extrusion and other deformation modes for the fabrication of multifilamentary niobium--tin superconductors by a powder metallurgy approach

    International Nuclear Information System (INIS)

    MacLeod, G.E.

    1977-06-01

    Various aspects of a powder metallurgy approach to fabricate filamentary niobium-tin superconducting wire were investigated. Difficulties occurred due to lack of complete tin infiltration of the sintered niobium rod, formation of intermetallics during infiltration, and both cladding and core fracture during mechanical reduction. The influence of sintering time, infiltration temperature, and deformation mode was investigated. Progress is reported on the clarification of the role of several of the important process parameters

  11. Powder metallurgy inspired low-temperature fabrication of high-performance stereocomplexed polylactide products with good optical transparency

    Science.gov (United States)

    Bai, Dongyu; Liu, Huili; Bai, Hongwei; Zhang, Qin; Fu, Qiang

    2016-01-01

    Stereocomplexation between enantiomeric poly(l-lactide) (PLLA) and poly(d-lactide) (PDLA) provides an avenue to greatly enhance performance of eco-friendly polylactide (PLA). Unfortunately, although the manufacturing of semicrystalline polymers generally involves melt processing, it is still hugely challenging to create high-performance stereocomplexed polylactide (sc-PLA) products from melt-processed high-molecular-weight PLLA/PDLA blends due to the weak crystallization memory effect of stereocomplex (sc) crystallites after complete melting as well as the substantial degradation of PLA chains at elevated melt-processing temperatures of ca. 240–260 °C. Inspired by the concept of powder metallurgy, here we report a new facile route to address these obstacles by sintering of sc-PLA powder at temperatures as low as 180–210 °C, which is distinctly different from traditional sintering of polymer powders performed at temperatures far exceeding their melting temperatures. The enantiomeric PLA chain segments from adjacent powder particles can interdiffuse across particle interfaces and co-crystallize into new sc crystallites capable of tightly welding the interfaces during the low-temperature sintering process, and thus highly transparent sc-PLA products with outstanding heat resistance, mechanical strength, and hydrolytic stability have been successfully fabricated for the first time. PMID:26837848

  12. Investigation of the effects of particle size on the mechanical properties of porous and tin infiltrated niobium rods fabricated by a thermoplastic-powder metallurgy technique

    International Nuclear Information System (INIS)

    Noman, A.

    1978-12-01

    An investigation was made of the influence of particle size on the properties of both porous and tin infiltrated niobium rods fabricated by a thermoplastic-powder metallurgy technique. The residual porosity, extrusion pressure, tensile strength, and ductility were found to be dependent on the particle size distribution. All of these parameters were found to increase with increasing particle size. The influence of sintering time at a temperature of 2250 0 C was also studied. With increasing sintering time, the residual porosity and tensile strength decreased, whereas the ductility increased. The procedures for fabricating infiltrated niobium rods and the various tests employed to determine their properties are described

  13. Study to assess the feasibility of scaling up the powder metallurgy approach for the fabrication of commercial Nb3Sn filamentary superconductors

    International Nuclear Information System (INIS)

    1977-01-01

    A preliminary assessment was made of the feasibility of scaling up the laboratory techniques of making filamentary Nb 3 Sn superconductors using powder metallurgy to commercial fabrication process. The purpose of the effort is divided into two tasks. The first one is to demonstrate that sintered niobium rods infiltrated with tin can be reduced in area of approximately 10 4 . The second task pertains to the extrusion by conventional manner a copper billet containing several sintered rods each encapsulated in tantalum. The ultimate goal of the project is to establish optimal processing parameters that are suitable for the production of long lengths of fully stabilized, large current and high field conductors

  14. Metallurgy Department

    DEFF Research Database (Denmark)

    Risø National Laboratory, Roskilde

    The activities of the Metallurgy Department at Risø during 1981 are described. The work is presented in three chapters: General Materials Research, Technology and Materials Development, Fuel Elements. Furthermore, a survey is given of the department's participation in international collaboration...

  15. Study to assess the feasibility of scaling up the powder metallurgy approach for the fabrication of commercial Nb/sub 3/Sn filamentary superconductors

    Energy Technology Data Exchange (ETDEWEB)

    1977-12-09

    A preliminary assessment was made of the feasibility of scaling up the laboratory techniques of making filamentary Nb/sub 3/Sn superconductors using powder metallurgy to commercial fabrication process. The purpose of the effort is divided into two tasks. The first one is to demonstrate that sintered niobium rods infiltrated with tin can be reduced in area of approximately 10/sup 4/. The second task pertains to the extrusion by conventional manner a copper billet containing several sintered rods each encapsulated in tantalum. The ultimate goal of the project is to establish optimal processing parameters that are suitable for the production of long lengths of fully stabilized, large current and high field conductors.

  16. Implantation metallurgy

    International Nuclear Information System (INIS)

    Picraux, S.T.

    1975-01-01

    Important changes in the near-surface physical properties of metals were obtained by high-fluence ion implantation. Recently there have been an increasing number of studies of the behavior of implanted species with the aim of understanding the detailed physical processes that occur in an implanted metal layer. A key aspect of these implantation metallurgy studies has been the ability to form uniquely controlled systems in the near-surface regions of metals that can be studied with accurate depth resolution. Metallurgical parameters that may be difficult or impossible to obtain by other means can be measured. Also, parameters that depend on the implantation process, due to the athermal introduction of atoms and defects can be determined. Thus the dual objective of implantation metallurgy is to obtain information to improve understanding of the microscopic aspects of metallurgy and to understand how to form controlled new metallurgical systems. Examples of parameters studied include implanted impurity location, diffusion, enhanced diffusion, solubility, precipitation, and dissolution. (auth)

  17. Metallurgy Department publications 1988

    International Nuclear Information System (INIS)

    Schroeder Pedersen, A.; Bilde-Soerensen, J.B.

    1989-08-01

    A presentation (including abstracts) of scientific and technical publications and lectures by the staff of the Metallurgy Department during 1988 is given. The list comprises journal papers, conference papers, reports, lectures and poster presentations in the following catagories: Publications, Lectures and Poster Presentations. (author)

  18. Metallurgy Department publications 1989

    International Nuclear Information System (INIS)

    Horsewell, A.

    1990-08-01

    All publiclations by the staff of the Metallurgy Department during 1989 are listed. This list is divided into three sections as follows: Publications (journal and conference papers, reports); Lectures (public lecture presentations) and Posters (poster presentations at conferences and symposia). Abstracts are included. (author)

  19. Extractive metallurgy. Recent advances

    International Nuclear Information System (INIS)

    Stevenson, E.J.

    1977-01-01

    Detailed technical information derived from patents issued since 1975 on extractive metallurgy is presented. In part one, concerning copper, the major areas covered are: smelting and roasting; acid leaching; ammonia leach processes; cuprous chloride and ferric chloride; and recovery of copper values from solution. Part two covers other metals, including: nickel and cobalt; ocean floor nodules; lead, zinc, molybdenum and manganese; precious metals; and uranium titanium, tantalum, rhenium, gallium, and other metals

  20. Effect of Pre-Oxidation Treatment of Nano-SiC Particulates on Microstructure and Mechanical Properties of SiC/Mg-8Al-1Sn Composites Fabricated by Powder Metallurgy Combined with Hot Extrusion.

    Science.gov (United States)

    Li, Chuan-Peng; Wang, Zhi-Guo; Zha, Min; Wang, Cheng; Yu, Hong-Chen; Wang, Hui-Yuan; Jiang, Qi-Chuan

    2016-11-26

    Nano-SiC particulates (n-SiC p ) reinforced Mg-8Al-1Sn (AT81) composites with different pre-oxidation parameters were fabricated by powder metallurgy (P/M) process combined with hot extrusion. The effects of pre-oxidization treatment of n-SiC p on the microstructure and tensile properties of 0.5 vol % n-SiC p /AT81 composites were investigated accordingly. The distribution of n-SiC p with different pre-oxidation parameters was homogeneous in the composites. Moreover, it was found that a thin MgAl₂O₄ layer formed at the interface when the n-SiC p were pre-oxidized at 1073 K for 2 h, while the MgAl₂O₄ layer became much thicker with pre-oxidization temperature increasing to 1273 K for 2 h. After an appropriate pre-oxidization treatment of n-SiC p at 1073 K for 2 h, the as-extruded 0.5 vol % n-SiC p /AT81 composites exhibited an enhanced strength. It was found that the yield strength (YS) and ultimate tensile strength (UTS) increased from 168 MPa and 311 MPa to 255 MPa and 393 MPa compared with the as-extruded AT81 alloy, reflecting 51.8% and 26.4% increments, respectively. The improvement of mechanical properties should be mainly attributed to the grain refinement and homogeneous distribution of n-SiC p in the composites. Moreover, a well-bonded interface and the formation of an appropriate amount of interfacial product (MgAl₂O₄) benefited the material's mechanical properties.

  1. Powder metallurgy development at SRL

    International Nuclear Information System (INIS)

    Peacock, H.B.

    1978-01-01

    Fuel for Savannah River Plant (SRP) reactors consists of extruded tubes with aluminum--uranium alloy cores clad with 8001 aluminum. The 235 U in the fuel is periodically recovered and recycled in new fuel assemblies. The buildup of 236 U in the enriched uranium requires increased total uranium contents to maintain reactivity in existing assembly designs. High level waste production from these tubes is proportional to the aluminum content; therefore, appreciable radioactive waste reductions result from lower aluminum--uranium ratios and thinner clad tubes. The casting process now used for fuel cores is limited to below 40 wt % U because of the reduced fabricability of high uranium alloys. To increase tube loading and reduce aluminum, the U 3 O 8 -Al powder metallurgy (P/M) process for fuel tubes is under development. Several fabricaion and irradiaion tests have been made using production conditions. Both small scale and production tests carried out at SRL for high-density P/M fuel development are discussed

  2. Lithium extractive metallurgy

    International Nuclear Information System (INIS)

    Josa, J.M.; Merino, J.L.

    1985-01-01

    The Nuclear Fusion National Program depends on lithium supplies. Extractive metallurgy development is subordinate to the localization and evaluation of ore resources. Nowadays lithium raw materials usable with present technology consist of pegmatite ore and brine. The Instituto Geologico y Minero Espanol (IGME) found lepidolite, ambligonite and spodrimene in pegmatite ores in different areas of Spain. However, an evaluation of resources has not been made. Different Spanish surface and underground brines are to be sampled and analyzed. If none of these contain significant levels of lithium, the Junta de Energia Nuclear (JEN) will try an agreement with IGME for ENUSA (Empresa Nacional del Uranio, S.A.) to explore pegmatite-ore bodies from different locations. Different work stages, laboratory tests, pilots plants tests and commercial plant, are foreseen, if the deposits are found. (author)

  3. Metallurgy: Printing steels

    Science.gov (United States)

    Todd, Iain

    2018-01-01

    Additive manufacturing has been used to fabricate a common stainless steel, which imparts a unique microstructure to this material, making it stronger and more ductile than that produced with conventional methods.

  4. The extractive metallurgy of gold

    Energy Technology Data Exchange (ETDEWEB)

    Kongolo, K.; Mwema, M.D. [University of Lubumbashi, Zaire, Gecamines Metallurgical Research Centre, Likasi, Zaire, c/o Gecamines Brussels (Belgium)

    1998-12-15

    Moessbauer spectroscopy has been successfully used in investigation of the gold compounds present in ores and the gold species which occur during the process metallurgy of this metal. This paper is a survey of the basic recovery methods and techniques used in extractive metallurgy of gold. Process fundamentals on mineral processing, ore leaching, zinc dust cementation, adsorption on activated carbon, electrowinning and refining are examined. The recovery of gold as a by-product of the copper industry is also described. Alternative processing methods are indicated in order to shed light on new interesting research topics where Moessbauer spectroscopy could be applied.

  5. The extractive metallurgy of gold

    International Nuclear Information System (INIS)

    Kongolo, K.; Mwema, M.D.

    1998-01-01

    Moessbauer spectroscopy has been successfully used in investigation of the gold compounds present in ores and the gold species which occur during the process metallurgy of this metal. This paper is a survey of the basic recovery methods and techniques used in extractive metallurgy of gold. Process fundamentals on mineral processing, ore leaching, zinc dust cementation, adsorption on activated carbon, electrowinning and refining are examined. The recovery of gold as a by-product of the copper industry is also described. Alternative processing methods are indicated in order to shed light on new interesting research topics where Moessbauer spectroscopy could be applied

  6. Powder metallurgy development at SRL

    International Nuclear Information System (INIS)

    Peacock, H.B.

    1993-01-01

    The Savannah River Laboratory (SRL) is developing a powder metallurgy (P/M) process for manufacturing reactor-grade fuel tubes containing high wt % U 3 O 8 -Al cores clad with 8001 aluminum. The P/M cores are made by isostatic compaction. They are assembled in billets, outgassed, and hot-extruded using conventional coextrusion techniques. Cores have been compacted with up to 100% U3O 8 and tubes extruded with 80 wt % oxide cores. Irradiation tests have been made using P/M core tubes in the Savannah River reactors. These tubes contained U 3 O 8 concentrations up to 59 wt % and no significant swelling or blistering occurred. The tubes were irradiated to ∼ 40% burnup or 1.6x10 21 fissions/cc of core. This report discusses both small-scale and production tests for high-density P/M fuel development. The purpose of the P/M development program at SRL is to: determine the maximum U 3 O 8 content that can be fabricated into thin wall tubes, irradiate high-density tubes to high burnup and assess irradiation and dimensional stability, continue metal forming studies for extrusion and drawing, and evaluate hydrostatic extrusion and hydrostatically assisted drawing of P/M core tubes. Experimental results of testing the fuel assemblies performance so far indicate that: cores containing fine (-325 mesh) U 3 O 8 and aluminum powders can be made practically free of high-density areas using the outlined P/M pre blending and sieving techniques. U 3 O 8 -Al cores can be isostatically compacted with up to 100 wt U 3 O 8 and tubes successfully extruded with up to 80 wt oxide; fission gas blistering of U 3 O 8 -Al P/M tubes as indicated by the blister tests is a function of fissions/cc of U 3 O 8 in the core; Decreasing the fission density of oxide increases the threshold temperature for blister formation; U 3 O 8 -Al P/M fuel tubes with up to 59 wt U 3 O 8 have been successfully irradiated in SRP reactor to 1.6 x 10 21 fissions/cc of core or 7 x 10 20 fissions/cc of U 3 O 8 small

  7. Physical metallurgy of nickel aluminides

    Indian Academy of Sciences (India)

    A description of the important physical metallurgy aspects of Ni$_3Al and NiAl encompassing structure, crystallographic defects, slip systems and phase stability has been presented in this article. The microstructures generated in the two alloys by conventional as well as novel processing techniques have been discussed.

  8. Aluminum powder metallurgy processing

    Energy Technology Data Exchange (ETDEWEB)

    Flumerfelt, J.F.

    1999-02-12

    The objective of this dissertation is to explore the hypothesis that there is a strong linkage between gas atomization processing conditions, as-atomized aluminum powder characteristics, and the consolidation methodology required to make components from aluminum powder. The hypothesis was tested with pure aluminum powders produced by commercial air atomization, commercial inert gas atomization, and gas atomization reaction synthesis (GARS). A comparison of the GARS aluminum powders with the commercial aluminum powders showed the former to exhibit superior powder characteristics. The powders were compared in terms of size and shape, bulk chemistry, surface oxide chemistry and structure, and oxide film thickness. Minimum explosive concentration measurements assessed the dependence of explosibility hazard on surface area, oxide film thickness, and gas atomization processing conditions. The GARS aluminum powders were exposed to different relative humidity levels, demonstrating the effect of atmospheric conditions on post-atomization processing conditions. The GARS aluminum powders were exposed to different relative humidity levels, demonstrating the effect of atmospheric conditions on post-atomization oxidation of aluminum powder. An Al-Ti-Y GARS alloy exposed in ambient air at different temperatures revealed the effect of reactive alloy elements on post-atomization powder oxidation. The pure aluminum powders were consolidated by two different routes, a conventional consolidation process for fabricating aerospace components with aluminum powder and a proposed alternative. The consolidation procedures were compared by evaluating the consolidated microstructures and the corresponding mechanical properties. A low temperature solid state sintering experiment demonstrated that tap densified GARS aluminum powders can form sintering necks between contacting powder particles, unlike the total resistance to sintering of commercial air atomization aluminum powder.

  9. Metallurgi for Ingeniører

    DEFF Research Database (Denmark)

    Pedersen, Jan

    Ny gennemarbejdet udgave af den klassiske "Metallurgi for Ingeniører", først skrevet af K. Offer Andersen i 1962......Ny gennemarbejdet udgave af den klassiske "Metallurgi for Ingeniører", først skrevet af K. Offer Andersen i 1962...

  10. Power metallurgy approaches to high temperature components for gas turbine engines

    Science.gov (United States)

    Probst, H. B.

    1974-01-01

    Work conducted by NASA and NASA contractors on prealloyed superalloy powders and materials strengthened by oxide dispersion is reviewed. Fabrication, tensile strength, superplasticity, grain growth control, stress rupture life, and grain-size and dispersion-level effects are covered. Distinct strength advantages of powder metallurgy superalloys over conventional wrought alloys are noted.

  11. Powder Metallurgy Reconditioning of Food and Processing Equipment Components

    Science.gov (United States)

    Nafikov, M. Z.; Aipov, R. S.; Konnov, A. Yu.

    2017-12-01

    A powder metallurgy method is developed to recondition the worn surfaces of food and processing equipment components. A combined additive is composed to minimize the powder losses in sintering. A technique is constructed to determine the powder consumption as a function of the required metallic coating thickness. A rapid method is developed to determine the porosity of the coating. The proposed technology is used to fabricate a wear-resistant defectless metallic coating with favorable residual stresses, and the adhesive strength of this coating is equal to the strength of the base metal.

  12. Properties of porous magnesium prepared by powder metallurgy.

    Science.gov (United States)

    Čapek, Jaroslav; Vojtěch, Dalibor

    2013-01-01

    Porous magnesium-based materials are biodegradable and promising for use in orthopaedic applications, but their applications are hampered by their difficult fabrication. This work reports the preparation of porous magnesium materials by a powder metallurgy technique using ammonium bicarbonate as spacer particles. The porosity of the materials depended on the amount of ammonium bicarbonate and was found to have strong negative effects on flexural strength and corrosion behaviour. However, the flexural strength of materials with porosities of up to 28 vol.% was higher than the flexural strength of non-metallic biomaterials and comparable with that of natural bone. Copyright © 2012 Elsevier B.V. All rights reserved.

  13. A major advance in powder metallurgy

    Science.gov (United States)

    Williams, Brian E.; Stiglich, Jacob J., Jr.; Kaplan, Richard B.; Tuffias, Robert H.

    1991-01-01

    Ultramet has developed a process which promises to significantly increase the mechanical properties of powder metallurgy (PM) parts. Current PM technology uses mixed powders of various constituents prior to compaction. The homogeneity and flaw distribution in PM parts depends on the uniformity of mixing and the maintenance of uniformity during compaction. Conventional PM fabrication processes typically result in non-uniform distribution of the matrix, flaw generation due to particle-particle contact when one of the constituents is a brittle material, and grain growth caused by high temperature, long duration compaction processes. Additionally, a significant amount of matrix material is usually necessary to fill voids and create 100 percent dense parts. In Ultramet's process, each individual particle is coated with the matrix material, and compaction is performed by solid state processing. In this program, Ultramet coated 12-micron tungsten particles with approximately 5 wt percent nickel/iron. After compaction, flexure strengths were measured 50 percent higher than those achieved in conventional liquid phase sintered parts (10 wt percent Ni/Fe). Further results and other material combinations are discussed.

  14. The metallurgy, science and engineering

    International Nuclear Information System (INIS)

    Pineau, A.; Quere, Y.

    2011-01-01

    Metallurgy, the science of metals and the technical discipline concerned with the production, shaping and assembling of metals, is one of the major assets of European economy. The French metallurgy industry - from producers (steel, light alloys, ...) to users (car, aviation, nuclear industries, ...) -- has achieved in many of its sectors a world-class level of excellence, based on high-quality research centres that are recognized both for their theoretical and experimental academic work. By contrast, public research is insufficiently concerned with engineering. In 2004, this industry employed 1 800 000 persons, 220 000 of which worked as engineers and managers in 45 000 companies, with a turnover of 420 billion euros. This state of grace is starting to decline. We are undergoing, in this sector as in others, a de-industrialization that affects upstream activities: courses in these disciplines, which have been previously outstanding, have partially disappeared; laboratories have shrunk; expertise has been dispersed; students are staying away from a discipline they consider 'unfruitful', like many other engineering sciences. Simultaneously, further up in this sector, decision centres have moved away from production centres and away from our country. France still maintains a few important R and D centres within international groups in spite of France's decreasing weight in world production. However, these groups see the future of R and D as being centred in the emerging countries (China, India...). The main users (transport, energy, ...) are losing their experts as are the technical centres on which rely a large network of small and medium businesses. The consequences are alarming in view of the already noticeable loss of technical control. This trend can and must be reversed. Because of its presence in many industrial sectors and its excellence, metallurgy - including both research and industry - is an essential activity in which France should remain a major player

  15. Progress report of the Metallurgy Group

    International Nuclear Information System (INIS)

    Sundaram, C.V.; Moorthy, V.K.

    1975-01-01

    The activities of the Metallurgy Division of the Bhabha Atomic Research Centre, Bombay, during the year 1974 are reported under six sections, namely: ore dressing; extractive metallurgy; ceramics; physical metallurgy; corrosion and electrometallurgy, and radiometallurgy. The developmental programme is not only concerned with materials of nuclear interest such as uranium, thorium, plutonium, zirconium, niobium and beryllium, but also other materials of national interest such as titanium, tantalum, ceramics, corrosion-resistant alloys etc. In addition to the laboratory studies, collaborative work has also been undertaken with other units of the Department of Atomic Energy. (A.K.)

  16. [Respiratory diseases in metallurgy production workers].

    Science.gov (United States)

    Shliapnikov, D M; Vlasova, E M; Ponomareva, T A

    2012-01-01

    The authors identified features of respiratory diseases in workers of various metallurgy workshops. Cause-effect relationships are defined between occupational risk factors and respiratory diseases, with determining the affection level.

  17. Structural Description of Powder Metallurgy Prepared Materials

    Czech Academy of Sciences Publication Activity Database

    Michalcová, A.; Vojtěch, D.; Kubatík, Tomáš František; Novák, P.; Dvořák, P.

    2014-01-01

    Roč. 14, č. 3 (2014), s. 359-362 ISSN 1213-2489. [Mezinárodní konference „Mikroskopie a nedestruktivní zkoušení materiálů/3./. Litoměřice, 22.10.2014-24.10.2014] Institutional support: RVO:61389021 Keywords : SPS * Intermetallics * powder metallurgy Subject RIV: JG - Metallurgy http://journal.strojirenskatechnologie.cz/templates/obalky_casopis/XIV_2014-3.pdf

  18. Advanced powder metallurgy aluminum alloys and composites

    Science.gov (United States)

    Lisagor, W. B.; Stein, B. A.

    1982-01-01

    The differences between powder and ingot metallurgy processing of aluminum alloys are outlined. The potential payoff in the use of advanced powder metallurgy (PM) aluminum alloys in future transport aircraft is indicated. The national program to bring this technology to commercial fruition and the NASA Langley Research Center role in this program are briefly outlined. Some initial results of research in 2000-series PM alloys and composites that highlight the property improvements possible are given.

  19. The mysterious world of plutonium metallurgy: Past and future

    International Nuclear Information System (INIS)

    Hecker, S.S.; Hammel, E.F.

    1998-01-01

    The first atomic bomb detonated at the Trinity Site in New Mexico on July 16, 1945, used plutonium, a man-made element discovered < 5 yr earlier. The story of how Manhattan Project scientists and engineers tackled the mysteries of this element and fabricated it into the first atomic bomb is one of the most fascinating in the history of metallurgy and materials. The authors are currently trying to generate renewed interest in plutonium metallurgy because of the challenge posed by President Clinton, i.e., to keep the nuclear stockpile of weapons safe and reliable without nuclear testing. The stockpile stewardship challenge requires either a lifetime extension of the plutonium components or a remanufacture--neither of which can be verified by testing. In turn, this requires that one achieve a better fundamental understanding of plutonium. Of special interest is the effect of self-irradiation on the properties and on the long-term stability of plutonium and its alloys. Additional challenges arise from long-term concerns about disposing of plutonium and dealing with its environmental legacy. It is imperative to interest the next generation of students in these plutonium challenges

  20. Current programmes on physical metallurgy and related areas in BARC

    International Nuclear Information System (INIS)

    1994-01-01

    Current research and development programmes on physical metallurgy and related areas from the following Divisions of Bhabha Atomic Research Centre are included in this report : Atomic Fuels Division, High Pressure Physics Division, Metallurgy Division, Radio Metallurgy Division, Solid State Physics Division. Important publications corresponding to each activity have also been listed. (author)

  1. Ideate about building green mine of uranium mining and metallurgy

    International Nuclear Information System (INIS)

    Shi Zuyuan

    2012-01-01

    Analysing the current situation of uranium mining and metallurgy; Setting up goals for green uranium mining and metallurgy, its fundamental conditions, Contents and measures. Putting forward an idea to combine green uranium mining and metallurgy with the state target for green mining, and keeping its own characteristics. (author)

  2. An application of powder metallurgy for the LHC

    CERN Document Server

    Sgobba, Stefano

    2004-01-01

    The cold mass of the 1232 superconducting dipole magnets of LHC, operating at 1.9 K, is enclosed by a shrinking cylinder and two end covers at its extremities. The covers are structural components that must retain high strength and toughness at cryogenic temperature. They are manufactured by Metso Oy /FI in AISI 316 LN steel by Powder Metallurgy (PM) and Hot Isostatic Pressing. PM represents an attractive near net shaping technique for these components of complex geometry for which dimension tolerances, dimensional stability, weldability are key issues for magnet fabrication, and mechanical properties, ductility and leak tightness have to be guaranteed during operation. The material of the covers and its welds have been fully characterized and mechanically tested down to 4.2 K at CERN. The fine grained structure, the absence of residual stresses, the full isotropy of mechanical properties associated to the low level of Prior Particle Boundaries oxides result in superior mechanical properties and high ductilit...

  3. Biennial activity report of metallurgy programme for 1987 and 1988

    International Nuclear Information System (INIS)

    Shanmugam, V.; Rao, B.P.C.; Bhanu Sankara Rao, K.; Muralidharan, P.; Bhaduri, A.K.; Kuppusami, P.; Shyamsunder, M.T.; Sampath, N.; Sreedharan, O.M.

    1990-01-01

    The research and development (R and D) activities in the field of metallurgy at Indira Gandhi Centre for Atomic Research, Kalpakkam during 1987-1988 are reported in the form of individual summaries arranged under headings : (1) Mechanical Metallurgy Section, (2) Physical Metallurgy Section, (3) Chemical Metallurgy Section, (4) Materials Technology Section, (5) Division for PIE and NDT Development and (6) Quality Engineering Section. A list of publications by the staff scientists working in the field of metallurgy during report period is given in one of the appendices. (author). figs., tabs

  4. Study on the formation of cubic texture in Ni-7 at.% W alloy substrates by powder metallurgy routes

    DEFF Research Database (Denmark)

    Zhao, Yue; Suo, HongLi; Zhu, YongHua

    2009-01-01

    One of the main challenges for coated conductor applications is to produce sharp cubic textured alloy substrates with high strength and low magnetism. In this work, the cubic textured Ni–7 at.% W substrates were prepared from different powder metallurgy ingots by rolling-assisted biaxially textured...... substrate processing. The fabrication processes of cubic texture in the Ni–7 at.% W tapes by two powder metallurgy routes are described in detail. Through the optimized process, full width at half maximum values of 6.7° and 5.0° were obtained, as estimated by X-ray (1 1 1) phi scan and (2 0 0) rocking curve...

  5. Metallurgy department publications and lectures 1987

    International Nuclear Information System (INIS)

    Schroeder Pedersen, A.; Bilde-Soerensen, J.B.

    1988-04-01

    A presentation (including abstract) of scientific and technical publications and lectures by the staff of the Metallurgy Department during 1987 is given. The list comprises journal papers, conference papers, reports, lectures and poster presentations in the following categories: Publications, Lectures and Poster Presentations. (author)

  6. Investigations to problems of the implantation metallurgy

    International Nuclear Information System (INIS)

    Rauschenbach, B.

    1987-01-01

    Basing on processes and effects caused ion implantation of metals a review is given about the problems of the implantation metallurgy. Techniques of high-fluence ion implantation and ion beam mixing are generally confined. These techniques change the structure and the chemical composition in the near of the surface of metals. The application of these methods is demonstrated on series of examples. (author)

  7. Powder-Metallurgy Process And Product

    Science.gov (United States)

    Paris, Henry G.

    1988-01-01

    Rapid-solidification processing yields alloys with improved properties. Study undertaken to extend favorable property combinations of I/M 2XXX alloys through recently developed technique of rapid-solidification processing using powder metallurgy(P/M). Rapid-solidification processing involves impingement of molten metal stream onto rapidly-spinning chill block or through gas medium using gas atomization technique.

  8. Development and prospect of china uranium mining and metallurgy

    International Nuclear Information System (INIS)

    Que Weimin; Wang Haifeng; Niu Yuqing; Gu Wancheng; Zhang Feifeng

    2007-01-01

    The development of industry of uranium mining and metallurgy in China has been reviewed generally, emphasizing on investigation approaches and application levels of uranium mining technologies such as in-situ leaching, heap leaching, stope leaching: on the basis of analysis on status of uranium mining and metallurgy and problems existed, also considering the specific features of deposit resources, the development orientation of uranium mining and metallurgy in China is pointed out. The industry of China uranium mining and metallurgy is faced to new opportunity of development and challenge in 21st century, the only way to realize sustainable development of uranium mining and metallurgy and harmonious development between economy and environment is to develop new technology on mining, ore beneficiation and metallurgy, increase the utilization level of uranium resources, low down impact on environment caused by mining and metallurgy. (authors)

  9. Development of new metal matrix composite electrodes for electrical discharge machining through powder metallurgy process

    Directory of Open Access Journals (Sweden)

    C. Mathalai Sundaram

    2014-12-01

    Full Text Available Electrical discharge machining (EDM is one of the widely used nontraditional machining methods to produce die cavities by the erosive effect of electrical discharges. This method is popular due to the fact that a relatively soft electrically conductive tool electrode can machine hard work piece. Copper electrode is normally used for machining process. Electrode wear rate is the major drawback for EDM researchers. This research focus on fabrication of metal matrix composite (MMC electrode by mixing copper powder with titanium carbide (TiC and Tungsten carbide (WC powder through powder metallurgy process, Copper powder is the major amount of mixing proportion with TiC and WC. However, this paper focus on the early stage of the project where powder metallurgy route was used to determine suitable mixing time, compaction pressure and sintering and compacting process in producing EDM electrode. The newly prepared composite electrodes in different composition are tested in EDM for OHNS steel.

  10. Mechanical properties of metals for biomedical applications using powder metallurgy process: A review

    Science.gov (United States)

    Dewidar, Montasser Marasy; Yoon, Ho-Chel; Lim, Jae Kyoo

    2006-06-01

    The uses of biomaterials have been revolutionizing the biomedical field in deployment as implants for humans. During the past five decades, many implant materials made of metals have been put into practical use. Powder metallurgy techniques have been used to produce controlled porous structures, such as porous coatings applied for dental and orthopedic surgical implants, which allow bony tissue ingrowth within the implant surface, thereby improving fixation. This paper examines various important metals using powder metallurgy technology to produce elements of a total hip replacement. These alloys are 316L stainless steel alloy, Co-Cr-Mo alloy, and Ti-6Al-4V alloy. Also, this paper examines current information on the mechanical properties. Mechanical properties are discussed as a function of type of materials and process of fabrication. This article addresses the engineering aspects concerning the advantages and disadvantages of each type of material.

  11. Computational thermodynamics in electric current metallurgy

    DEFF Research Database (Denmark)

    Bhowmik, Arghya; Qin, R.S.

    2015-01-01

    A priori derivation for the extra free energy caused by the passing electric current in metal is presented. The analytical expression and its discrete format in support of the numerical calculation of thermodynamics in electric current metallurgy have been developed. This enables the calculation...... of electric current distribution, current induced temperature distribution and free energy sequence of various phase transitions in multiphase materials. The work is particularly suitable for the study of magnetic materials that contain various magnetic phases. The latter has not been considered in literature....... The method has been validated against the analytical solution of current distribution and experimental observation of microstructure evolution. It provides a basis for the design, prediction and implementation of the electric current metallurgy. The applicability of the theory is discussed in the derivations....

  12. Powder metallurgy bearings for advanced rocket engines

    Science.gov (United States)

    Fleck, J. N.; Killman, B. J.; Munson, H.E.

    1985-01-01

    Traditional ingot metallurgy was pushed to the limit for many demanding applications including antifriction bearings. New systems require corrosion resistance, better fatigue resistance, and higher toughness. With conventional processing, increasing the alloying level to achieve corrosion resistance results in a decrease in other properties such as toughness. Advanced powder metallurgy affords a viable solution to this problem. During powder manufacture, the individual particle solidifies very rapidly; as a consequence, the primary carbides are very small and uniformly distributed. When properly consolidated, this uniform structure is preserved while generating a fully dense product. Element tests including rolling contact fatigue, hot hardness, wear, fracture toughness, and corrosion resistance are underway on eleven candidate P/M bearing alloys and results are compared with those for wrought 440C steel, the current SSME bearing material. Several materials which offer the promise of a significant improvement in performance were identified.

  13. Metallurgy Department. Annual progress report for 1989

    International Nuclear Information System (INIS)

    Horsewell, A.; Hansen, N.

    1990-07-01

    Selected activities of the Metallurgy Department at Risoe National Laboratory during 1989 are described. The work is presented in three chapters: Materials Science, Materials Engineering and Materials Technology. A survey is given of the Department's participation in international collaboration and of its acitivities within eduation and training. Furthermore, the main figures outlining the funding and expenditure of the Department are given. Lists of staff members, visiting scientists, publicaltions, lectures and poster presentations are included. (author) 90 refs

  14. Metallurgy Department annual progress report for 1987

    International Nuclear Information System (INIS)

    Schroeder Pedersen, A.; Bilde-Soerensen, J.B.; Hansen, N.

    1988-05-01

    Selected activities of the Metallurgy Department at Risoe National Laboratory during 1987 are described. The work is presented in four chapters: Materials Science, Materials Engineering, Materials Technology and Energy Programmes. A survey is given of the Department's participation in international collaboration and of its activities within education and training. Furthermore, the main numbers illustrating the Departments's economy are given. Lists of staff members, visiting scientists, publications, lectures and poster presentations are included. 38 ills. (author)

  15. Metallurgy Department. Annual progress report for 1988

    International Nuclear Information System (INIS)

    Schroeder Pedersen, A.; Bilde-Soerensen, J.B.; Hansen, N.

    1989-05-01

    Selected activities of the Metallurgy Department at Risoe National Laboratory during 1988 are described. The work is presented in four chapters: Materials Science, Materials Engineering, Materials Technology and Energy Programmes. A survey is given of the Department's participation in international collaboration and of its activities within education and training. Furthermore, the main numbers illustrating the Department's economy are given. Lists of staff members, visiting scientists, publications, lectures and poster presentations are included. (author) 36 ills., 81 refs

  16. Powder metallurgy development at SRL

    International Nuclear Information System (INIS)

    Peacock, H.B.

    1993-01-01

    The Savannah River Laboratory (SRL) is developing a powder metallury (P/M) process for manufacturing reactor-grade fuel tubes containing high wt % U 3 O 8 -Al cores clad with 8001 aluminum. The P/M cores are made by isostatic compaction. They are assembled in billets, outgassed, and hot-extruded using conventional coextrusion techniques. Cores have been compacted with up to 100% U 3 O 8 and tubes extruded with 80 wt % oxide cores. Irradiation tests have been made using P/M core tubes in the Savannah River reactors. These tubes contained U 3 O 8 concentrations up to 59 wt % and no significant swelling or blistering occurred. The tubes were irradiated to ∼40% burnup or 1.6x10 21 fissions/cc of core. This report discusses both small-scale and production tests for high- density P/M fuel development. The purpose of the P/M development program at SRL is to: (1) determine the maximum U 3 O 8 content that can be fabricated into thin wall tubes, (2) irradiate high-density tubes to high burnup and assess irradiation and dimensional stability, (3) continue metal forming studies for extrusion and drawing, and (4) evaluate hydrostatic extrusion and hydrostatically assisted drawing of P/M core tubes

  17. Metals in Past Societies: A Global Perspective on Indigenous African Metallurgy Shadreck Chirikure

    Energy Technology Data Exchange (ETDEWEB)

    Devanathan, Ram [Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

    2015-10-01

    This slim book (166 pages) shines a spotlight on pre-industrial African metallurgy, its global connections, and anthropological implications. It integrates seemingly disparate disciplines, such as history, geology, ethnography, archeology, and metallurgy, to illustrate the diversity and innovation in metallurgy across Africa and the role of metals in the rise of socio-economic inequalities and political power. The book has 7 chapters and the focus on metals as enablers of human needs and wants is evident in each chapter. The first chapter presents the context of the work and data sources. The second chapter focuses on the origin and development of mining and metallurgy in pre-industrial Africa. Chapter 3 is dedicated to the interaction of nature and culture in the process of mining. Chapter 4 deals with the transformation of the ore into metal by smelting and the sociocultural aspects of this process. Chapter 5 explores the social and cultural roles acquired by metals as a result of fabrication into objects. Chapter 6 examines the social role of metals, trade in metals, cultural contact, proto-globalization, and technology transfer. Finally, Chapter 7 draws lessons for global anthropology from the African experience. The sources of information are adequately cited and the long list of references at the end of each chapter will be a boon to researchers in this field. The author highlights the cultural aspects and social context of the adoption of metallurgy in Africa while drawing parallels between practices in pre-industrial Africa and those in other parts of the world. The book is peppered with delightful vignettes that offer insights into the process of transforming nature into culturally significant objects. For instance, African miners, like their counterparts in Nepal and Latin America, called upon deities, spirits and ancestors to mediate between nature and humans. Women had distinct roles in this process, but there were variations in these roles and in the

  18. Low-Cobalt Powder-Metallurgy Superalloy

    Science.gov (United States)

    Harf, F. H.

    1986-01-01

    Highly-stressed jet-engine parts made with less cobalt. Udimet 700* (or equivalent) is common nickel-based superalloy used in hot sections of jet engines for many years. This alloy, while normally used in wrought condition, also gas-atomized into prealloyed powder-metallurgy (PM) product. Product can be consolidated by hot isostatically pressing (HIPPM condition) and formed into parts such as turbine disk. Such jet-engine disks "see" both high stresses and temperatures to 1,400 degrees F (760 degrees C).

  19. Borax as a lubricant in powder metallurgy

    Directory of Open Access Journals (Sweden)

    Héctor Geovanny Ariza-Suarez

    2014-12-01

    were compacted at 700 MPa in a uniaxial press of 15 tons. DSC-TGA analysis of the mixture with borax was realized. The specimens were sintered in a plasma reactor at 1000 for 30 minutes, with a combined atmosphere of hydrogen and argon. Microhardness and density of the sintered samples was haracterized. XRD analysis was realized to detect possible compounds formation by interaction of borax. This paper shows that borax can be used as a lubricant in powder metallurgy.

  20. Biaxially textured articles formed by powder metallurgy

    Science.gov (United States)

    Goyal, Amit; Williams, Robert K.; Kroeger, Donald M.

    2003-07-29

    A biaxially textured alloy article having a magnetism less than pure Ni includes a rolled and annealed compacted and sintered powder-metallurgy preform article, the preform article having been formed from a powder mixture selected from the group of mixtures consisting of: at least 60 at % Ni powder and at least one of Cr powder, W powder, V powder, Mo powder, Cu powder, Al powder, Ce powder, YSZ powder, Y powder, Mg powder, and RE powder; the article having a fine and homogeneous grain structure; and having a dominant cube oriented {100} orientation texture; and further having a Curie temperature less than that of pure Ni.

  1. Biaxially textured articles formed by power metallurgy

    Science.gov (United States)

    Goyal, Amit; Williams, Robert K.; Kroeger, Donald M.

    2003-08-26

    A biaxially textured alloy article having a magnetism less than pure Ni includes a rolled and annealed compacted and sintered powder-metallurgy preform article, the preform article having been formed from a powder mixture selected from the group of mixtures consisting of: at least 60 at % Ni powder and at least one of Cr powder, W powder, V powder, Mo powder, Cu powder, Al powder, Ce powder, YSZ powder, Y powder, Mg powder, and RE powder; the article having a fine and homogeneous grain structure; and having a dominant cube oriented {100} orientation texture; and further having a Curie temperature less than that of pure Ni.

  2. Preparation of nitinol by non-conventional powder metallurgy techniques

    Czech Academy of Sciences Publication Activity Database

    Novák, P.; Moravec, H.; Salvetr, P.; Průša, F.; Drahokoupil, Jan; Kopeček, Jaromír; Karlík, M.; Kubatík, Tomáš František

    2015-01-01

    Roč. 31, č. 15 (2015), s. 1886-1893 ISSN 0267-0836 R&D Projects: GA ČR(CZ) GA14-03044S Institutional support: RVO:68378271 ; RVO:61389021 Keywords : shape memory alloys * SHS process * SEM * powder metallurgy Subject RIV: JG - Metallurgy Impact factor: 1.008, year: 2015

  3. Metallurgy and Heat Treating. Welding Module 7. Instructor's Guide.

    Science.gov (United States)

    Missouri Univ., Columbia. Instructional Materials Lab.

    This guide is intended to assist vocational educators in teaching a three-unit module in metallurgy and heat treating. The module is part of a welding curriculum that has been designed to be totally integrated with Missouri's Vocational Instruction Management System. The basic principles of metallurgy and heat treatment and techniques for…

  4. List of unclassified documents by the staff of Metallurgy Division, AERE Harwell from January 1972 to July 1977

    International Nuclear Information System (INIS)

    Wallis, V.

    1977-11-01

    This list constitutes unclassified material published or presented between January 1972 and July 1977 by the staff of Metallurgy Division. It covers reports, memoranda, bibliographies, articles in periodicals, conference papers, books, theses and patent specifications. It is planned to issue a list annually. The publications are listed under the following titles of the research teams concerned: fast reactor fuels, advanced reactor systems, fracture studies, structural materials, radiation effects, composite materials, high voltage microscope and metals fabrication, management and administration. (U.K.)

  5. Titanium surgical implants processed by powder metallurgy

    Energy Technology Data Exchange (ETDEWEB)

    Oliveira, M.V. de [INT-DMCM, Inst. Nacional de Tecnologia, Rio de Janeiro, RJ (Brazil); Pereira, L.C. [Programa de Eng. de Materiais e Metalurgica, UFRJ-COPPE (Brazil); Schwanke, C.M.; Schaeffer, L. [Centro de Tecnologia- LdTM-INT-DMCM, UFRGS, Venezuela, CEP, Rio de Janeiro, RJ (Brazil)

    2001-07-01

    Due to their low density coupled with excellent corrosion resistance and good mechanical properties, titanium and titanium alloys have been widely used for surgical implants. They have also a relatively low young's modulus, allowing a good load transfer to the bone. The elastic modulus difference between metallic implant material and bone is large, which can lead to a fracture of the implant. To solve this problem, many implants for artificial joint and dental applications have been produced by powder metallurgy routes, obtaining a porous material with an even lower young's modulus than that of the bulk titanium. This porous structure allows bone ingrowth, as the osseous tissue invade the holes of the porous material while growing and adheres to it. Besides, near net shape technologies like powder metallurgy and injection molding techniques, can reduce the components high costs due to machining final steps, also providing a fine, uniform grain structure and lack of texture and segregation. This work outlines the characteristics, properties and some of the powder routes for producing titanium surgical implants and implant porous coatings. (orig.)

  6. Promoting energy conservation in China's metallurgy industry

    International Nuclear Information System (INIS)

    Lin, Boqiang; Du, Zhili

    2017-01-01

    China is undergoing rapid industrialization and urbanization, with consequent dramatic increase in energy demand. Given energy scarcity, environmental pollution, energy security and energy cost constraints, energy conservation will be the major strategy in China's transition to a low-carbon economy. Since the metallurgy industry is a main sector of energy consumption, the efficiency of energy conservation in this industry will affect the future prospects of energy savings. This paper analyzes the energy conservation potential of China's metallurgy industry. First, seemingly unrelated regression method is applied to investigate the relationship between energy relative price, R&D input, enterprise ownership structure, enterprise scale and energy intensity of the metallurgy industry. Then, based on the SUR results, we use the scenario analysis method to predict energy consumption and savings potential in the industry in different scenarios. This paper provides references for China's government and metallurgy industry in formulating relevant energy conservation policies. - Highlights: • Seemingly unrelated regression method is applied to analyze the energy intensity of metallurgy industry. • We use the scenario analysis method to predict energy consuming and energy saving of Chinese metallurgy industry. • Provide references for China's government and metallurgy industry in formulating relevant energy conservation policies.

  7. Biennial activity report of Metallurgy Division for 1989 and 1990

    International Nuclear Information System (INIS)

    Kamachi Mudali, U.; Muraleedharan, P.; Parameswaran, P.; Swaminathan, K.; Sreedharan, O.M.

    1993-01-01

    This is the first divisional biennial report of the Metallurgy Division of Indira Gandhi Centre for Atomic Research, for the year 1989-1990, after formation of the Metallurgy Division in September 1988. Major areas of work in the Division relate to aqueous corrosion and localised corrosion, stress corrosion cracking and liquid metal corrosion, high temperature oxidation, thermodynamic studies, physical metallurgy studies for structure-property correlations and failure analyses. The principal materials of studies have been the austenitic stainless steels, the current materials of construction in the Fast Breeder Test Reactor and the candidate materials for the Prototype Fast Breeder Reactor

  8. Chemistry and metallurgy in the Portuguese Empire

    Energy Technology Data Exchange (ETDEWEB)

    Habashi, F. [Laval Univ., Sainte-Foy, Quebec City, PQ (Canada)

    2000-10-01

    The foundation and expansion of the Portuguese Empire is sketched, with emphasis on the development of a new type of ship by Prince Henrique the Navigator (AD 1385-1460), known as the caravel. By virtue of its advanced design, it was capable of sailing the stormy seas at high speeds, and thereby was instrumental in extending Portuguese influence over vast territories in South America, Asia and Africa, extending Portuguese know-how in mining, metallurgy, chemistry and trade along with Christianity. The role played by the University of Coimbra, founded in 1306, and the contribution of the Brazilian Geological Survey, established in 1875, and of the School of Mines in Ouro Preto in Brazil in 1876, in the exploitation of the mineral wealth of the Portuguese colonies is chronicled.

  9. Thermogravimetric control of intermediate compounds in uranium metallurgy

    International Nuclear Information System (INIS)

    Gasco Sanchez, L.; Fernandez Cellini, R.

    1959-01-01

    The thermal decomposition of some intermediate compounds in the metallurgy of the uranium as uranium peroxide, ammonium uranate, uranium and ammonium penta-fluoride, uranium tetrafluoride and uranous oxide has been study by means of the Chevenard's thermo balance. Some data on pyrolysis of synthetic mixtures of intermediate compounds which may occasionally appear during the industrial process, are given. Thermogravimetric methods of control are suggested, usable in interesting products in the uranium metallurgy. (Author) 20 refs

  10. The metallurgy of superalloys part 2

    International Nuclear Information System (INIS)

    Abdelazim, M.E.; Hammad, F.H.

    1990-01-01

    This is part II of the report titled 'the metallurgy of superalloys'. It deals with the effect of heat treatment and operating conditions (thermal exposure and environment) on the mechanical properties of superalloys. The heat treatment is important in the development of superalloys through that it controls type, amount, size shape and distribution of the precipitate and the grain size of the matrix. The thermal exposure leads to reduction in the amount of the primary carbides and to precipitation of secondary carbides. Also it leads to the agglomeration and coarsening of gamma or the transformation of gamma phase to phase. The environment may lead to the internal oxidation, carburization, decarburization or sulphidization of the superalloys which may result in the degradation of their mechanical properties. This part gives also an example of applications of superalloys in the field of nuclear reactors especially high temperature-gas cooled reactors. Joined with this part a table which contains the major superalloys including its chemical analysis, creep rupture strength and some of its applications. 1 tab

  11. Copper alloys with improved properties: standard ingot metallurgy vs. powder metallurgy

    Directory of Open Access Journals (Sweden)

    Milan T. Jovanović

    2014-09-01

    Full Text Available Three copper-based alloys: two composites reinforced with Al2O3 particles and processed through powder metallurgy (P/M route, i.e. by internal oxidation (Cu-2.5Al composite and by mechanical alloying (Cu-4.7Al2O3 and Cu-0.4Cr-0.08Zr alloy produced by ingot metallurgy (vacuum melting and casting were the object of this investigation. Light microscope and scanning electron microscope (SEM equipped with electron X-ray spectrometer (EDS were used for microstructural characterization. Microhardness and electrical conductivity were also measured. Compared to composite materials, Cu-0.4Cr-0.08Zr alloy possesses highest electrical conductivity in the range from 20 to 800 ℃, whereas the lowest conductivity shows composite Cu-2.5Al processed by internal oxidation. In spite to somewhat lower electrical conductivity (probably due to inadequate density, Cu-2.5Al composite exhibits thermal stability enabling its application at much higher temperatures than materials processed by mechanical alloying or by vacuum melting and casting.

  12. Josephson junction electronics: Materials issues and fabrication techniques. Metallurgy, fabrication, and applications

    International Nuclear Information System (INIS)

    Beasley, M.R.

    1981-01-01

    The main body of this chapter is organized as follows. In Section II we review the device principles that underlie the operation of superconducting electronic devices. The emphasis is on defining the most critical and characteristic materials issues and problems. In Section III we discuss the state of the art in the LSI circuit technology being developed for the Josephson computer. The problems associated with thermally-induced stresses in Josephson junctions are discussed in Section IV, and the importance and current understanding of the science of tunneling between superconductors is discussed in Section V. Finally, in Section VI we attempt to look ahead and discuss current work on advanced superconducting materials and devices

  13. Development of processes for zircaloy chips recycling by electric arc furnace remelting and powder metallurgy

    International Nuclear Information System (INIS)

    Pereira, Luiz Alberto Tavares

    2014-01-01

    PWR reactors employ, as nuclear fuel, UO 2 pellets with Zircaloy clad. In the fabrication of fuel element parts, machining chips from the alloys are generated. As the Zircaloy chips cannot be discarded as ordinary metallic waste, the recycling of this material is important for the Brazilian Nuclear Policy, which targets the reprocess of Zircaloy residues for economic and environmental aspects. This work presents two methods developed in order to recycle Zircaloy chips. In one of the methods, Zircaloy machining chips were refused using an electric-arc furnace to obtain small laboratory ingots. The second one uses powder metallurgy techniques, where the chips were submitted to hydriding process and the resulting material was milled, isostatically pressed and vacuum sintered. The ingots were heat-treated by vacuum annealing. The microstructures resulting from both processing methods were characterized using optical and scanning electron microscopy. Chemical composition, crystal phases and hardness were also determined. The results showed that the composition of recycled Zircaloy comply with the chemical specifications and presented adequate microstructure for nuclear use. The good results of the powder metallurgy method suggest the possibility of producing small parts, like cladding end-caps, using near net shape sintering. (author)

  14. 78 FR 8202 - Meeting of the Joint ACRS Subcommittees on Thermal Hydraulic Phenomena and Materials, Metallurgy...

    Science.gov (United States)

    2013-02-05

    ... Hydraulic Phenomena and Materials, Metallurgy and Reactor Fuels; Notice of Meeting The Joint ACRS Subcommittees on Thermal Hydraulic Phenomena and Materials, Metallurgy and Reactor Fuels will hold a meeting on...

  15. The Metallurgy of some indian swords

    Directory of Open Access Journals (Sweden)

    Williams, Alan

    2007-12-01

    Full Text Available The metallurgy of Indian swords shows many differences from that of European swords. The distinction between "Damascus Steel" (or wootz and crucible steel is explained. Ten broken blades from the Armoury of the Nizams of Hyderabad were made available for microscopic examination. Six of these seem to been made from crucible steels, and are of notably high quality. By contrast, a group of six randomly collected from Private Collections in England were also examined. Only one of these was made of crucible steel, and three of the others were of very mediocre quality. This perhaps represents the quality of blades available to the average Indian soldier.

    La metalurgia de las espadas indias presenta notables diferencias en comparación con la de las europeas. Se explica la distinción entre el ‘acero de Damasco’ (o wootz y el acero de crisol. Se ha realizado un análisis microscópico de un conjunto de diez hojas rotas de espada depositadas en la Armería de los Nizams de Hyderabad. Seis de ellas parecen haber sido realizadas a partir de acero de crisol, y son de elevada calidad. En contraste, se examinó también un grupo de seis espadas de colecciones privadas en Inglaterra. Sólo una de ellas estaba fabricada con acero de crisol, y tres de las otras eran de calidad muy mediocre. Esto representa quizá la calidad de las hojas de espada al alcance del soldado medio indio.

  16. Biennial activity report of Metallurgy Programme - 1985 and 1986

    International Nuclear Information System (INIS)

    Mallika, C.; Sreenivasan, P.R.; Muraleedharan, P.; Shyamsunder, M.T.; Kuppuswami, P.; Sampath, N.; Bhaduri, A.K.; Sreedharan, O.M.

    1988-01-01

    The biennial activity report of the Metallurgy Programme of the Indira Gandhi Centre for Atomic Research covers the period of the years 1985 and 1986. Along with NDT, welding metallurgy, low cycle fatigue, creep and creep fatigue interactions, structure-property correlations, thermodynamics and corrosion metallurgy of alloy steels with respect to their compatibility with aqueous and liquid sodium environments continue to be the major thrust areas of the Programme. Some of the basic research contributions of the Programme are: the observation of uniform and homogeneous distribution of voids in cyclically deformed 304 SS, the role of grain boundaries and precipitation in dynamic strain ageing of 316 SS and the determination of the activities of component metals in 316 and 304 SS by metastable EMF method. (author)

  17. Introduction to powder metallurgy processes for titanium manufacturing

    International Nuclear Information System (INIS)

    Esteban, P. G.; Bolzoni, L.; Ruiz-Navas, E. M.; Gordo, E.

    2011-01-01

    The development of new extraction processes to produce titanium in powder form leads Powder Metallurgy to an advantage position among the manufacturing processes for titanium. The cost reduction of base material, coupled with the economy of the powder metallurgy processes, give titanium industry the chance to diversify its products, which could lead to production volumes able to stabilise the price of the metal. This work reviews some of the Powder Metallurgy techniques for the manufacturing of titanium parts, and describes the two typical approaches for titanium manufacturing: Blending Elemental and Prealloyed Powders. Among others, conventional pressing and sintering are described, which are compared with cold and hot isostatic pressing techniques. Real and potential applications are described. (Author) 71 refs.

  18. Summarizing of new techniques in uranium mining and metallurgy

    International Nuclear Information System (INIS)

    Wang Delin; Zhang Fei; Su Yanru; Zeng Yijun; Meng Jin

    2010-01-01

    According to character of national resources and uranium mining and metallurgical science and technology members research achievements, new techniques in ten scientific research area of in-situ leaching, heap leaching, multi-metal comprehensive recovery, bio-metallurgy etc. for 10 years is introduced in this paper. The level of innovation ability is shown by technical index, resources recovery and reduction capital cost etc. datum. The application bound of natural uranium resource is enlarged and production ability of national uranium is increased. It is put forward renovation and development ideas for uranium mining and metallurgy. (authors)

  19. Metallurgy and properties of plasma spray formed materials

    Science.gov (United States)

    Mckechnie, T. N.; Liaw, Y. K.; Zimmerman, F. R.; Poorman, R. M.

    1992-01-01

    Understanding the fundamental metallurgy of vacuum plasma spray formed materials is the key to enhancing and developing full material properties. Investigations have shown that the microstructure of plasma sprayed materials must evolve from a powder splat morphology to a recrystallized grain structure to assure high strength and ductility. A fully, or near fully, dense material that exhibits a powder splat morphology will perform as a brittle material compared to a recrystallized grain structure for the same amount of porosity. Metallurgy and material properties of nickel, iron, and copper base alloys will be presented and correlated to microstructure.

  20. A powder metallurgy austenitic stainless steel for application at very low temperatures

    CERN Document Server

    Sgobba, Stefano; Liimatainen, J; Kumpula, M

    2000-01-01

    The Large Hadron Collider to be built at CERN will require 1232 superconducting dipole magnets operating at 1.9 K. By virtue of their mechanical properties, weldability and improved austenite stability, nitrogen enriched austenitic stainless steels have been chosen as the material for several of the structural components of these magnets. Powder Metallurgy (PM) could represent an attractive production technique for components of complex shape for which dimension tolerances, dimensional stability, weldability are key issues during fabrication, and mechanical properties, ductility and leak tightness have to be guaranteed during operation. PM Hot Isostatic Pressed test plates and prototype components of 316LN-type grade have been produced by Santasalo Powdermet Oy. They have been fully characterized and mechanically tested down to 4.2 K at CERN. The fine grained structure, the absence of residual stresses, the full isotropy of mechanical properties associated to the low level of Prior Particle Boundaries oxides ...

  1. Microstructure, mechanical behavior and biocompatibility of powder metallurgy Nb-Ti-Ta alloys as biomedical material.

    Science.gov (United States)

    Liu, Jue; Chang, Lin; Liu, Hairong; Li, Yongsheng; Yang, Hailin; Ruan, Jianming

    2017-02-01

    Microstructures, mechanical properties, apatite-forming ability and in vitro experiments were studied for Nb-25Ti-xTa (x=10, 15, 20, 25, 35at.%) alloys fabricated by powder metallurgy. It is confirmed that the alloys could achieve a relative density over 80%. Meanwhile, the increase in Ta content enhances the tensile strength, elastic modulus and hardness of the as-sintered alloys. When increasing the sintering temperatures, the microstructure became more homogeneous for β phase, resulting in a decrease in the modulus and strength. Moreover, the alloys showed a good biocompatibility due to the absence of cytotoxic elements, and were suitable for apatite formation and cell adhesion. In conclusion, Nb-25Ti-xTa alloys are potentially useful in biomedical applications with their mechanical and biological properties being evaluated in this work. Copyright © 2016 Elsevier B.V. All rights reserved.

  2. Comparison Study on Additive Manufacturing (AM) and Powder Metallurgy (PM) AlSi10Mg Alloys

    Science.gov (United States)

    Chen, B.; Moon, S. K.; Yao, X.; Bi, G.; Shen, J.; Umeda, J.; Kondoh, K.

    2018-02-01

    The microstructural and mechanical properties of AlSi10Mg alloys fabricated by additive manufacturing (AM) and powder metallurgy (PM) routes were investigated and compared. The microstructures were examined by scanning electron microscopy assisted with electron-dispersive spectroscopy. The crystalline features were studied by x-ray diffraction and electron backscatter diffraction. Room-temperature tensile tests and Vickers hardness measurements were performed to characterize the mechanical properties. It was found that the AM alloy had coarser Al grains but much finer Si precipitates compared with the PM alloy. Consequently, the AM alloy showed more than 100% increment in strength and hardness compared with the PM alloy due to the presence of ultrafine forms of Si, while exhibiting moderate ductility.

  3. Laboratory Powder Metallurgy Makes Tough Aluminum Sheet

    Science.gov (United States)

    Royster, D. M.; Thomas, J. R.; Singleton, O. R.

    1993-01-01

    Aluminum alloy sheet exhibits high tensile and Kahn tear strengths. Rapid solidification of aluminum alloys in powder form and subsequent consolidation and fabrication processes used to tailor parts made of these alloys to satisfy such specific aerospace design requirements as high strength and toughness.

  4. The effect of powder metallurgy process parameters on mechanical ...

    African Journals Online (AJOL)

    The ever-increasing development of applying the iron pieces made by powder metallurgy in car industries and other usages depends on making pieces with high density and consequently acceptable physical and mechanical properties. Regarding the effect of decrease in the powder bits' size on improvement of the ...

  5. Chemical and Metallurgy Research (CMR) Sample Tracking System Design Document

    International Nuclear Information System (INIS)

    Bargelski, C. J.; Berrett, D. E.

    1998-01-01

    The purpose of this document is to describe the system architecture of the Chemical and Metallurgy Research (CMR) Sample Tracking System at Los Alamos National Laboratory. During the course of the document observations are made concerning the objectives, constraints and limitations, technical approaches, and the technical deliverables

  6. Damage on 316LN stainless steel transformed by powder metallurgy

    International Nuclear Information System (INIS)

    Couturier, R.; Burlet, H.

    1998-01-01

    This study deals with the 316 LN stainless steel elaboration by powder metallurgy. This method allows the realization of structures in austenitic steel less affected by the thermal aging than the cast austenitic-ferritic components. The components are performed by the method of HIP (Hot Isostatic Pressing). Mechanical tests are provided to control mechanical properties

  7. Iron Metallurgy: Technical Terminology Bulletin. Terminotech, Vol. 2, No. 7.

    Science.gov (United States)

    General Electric Co. of Canada, Ltd., Montreal, Quebec.

    This issue of a bulletin of technological terminology is devoted to iron metallurgy. Various aspects of iron production are described in both French and English. An English-French dictionary of terms comprises the bulk of the document. Explanatory illustrations are appended. (JB)

  8. [Hygienic evaluation of risk factors on powder metallurgy production].

    Science.gov (United States)

    2011-01-01

    Complex hygienic, clinical, sociologic and epidemiologic studies revealed reliable relationship between work conditions and arterial hypertension, locomotory system disorders, monocytosis in powder metallurgy production workers. Findings are more probable cardiovascular and respiratory diseases, digestive tract diseases due to influence of lifestyle factors.

  9. Effects of Thermocapillary Forces during Welding of 316L-Type Wrought, Cast and Powder Metallurgy Austenitic Stainless Steels

    CERN Document Server

    Sgobba, Stefano

    2003-01-01

    The Large Hadron Collider (LHC) is now under construction at the European Organization for Nuclear Research (CERN). This 27 km long accelerator requires 1248 superconducting dipole magnets operating at 1.9 K. The cold mass of the dipole magnets is closed by a shrinking cylinder with two longitudinal welds and two end covers at both extremities of the cylinder. The end covers, for which fabrication by welding, casting or Powder Metallurgy (PM) was considered, are dished-heads equipped with a number of protruding nozzles for the passage of the different cryogenic lines. Structural materials and welds must retain high strength and toughness at cryogenic temperature. AISI 316L-type austenitic stainless steel grades have been selected because of their mechanical properties, ductility, weldability and stability of the austenitic phase against low-temperature spontaneous martensitic transformation. 316LN is chosen for the fabrication of the end covers, while the interconnection components to be welded on the protrud...

  10. Powder metallurgy and mechanical alloying effects on the formation of thermally induced martensite in an FeMnSiCrNi SMA

    Directory of Open Access Journals (Sweden)

    Pricop Bogdan

    2015-01-01

    Full Text Available By ingot metallurgy (IM, melting, alloying and casting, powder metallurgy (PM, using as-blended elemental powders and mechanical alloying (MA of 50 % of particle volume, three types of FeMnSiCrNi shape memory alloy (SMA specimens were fabricated, respectively. After specimen thickness reduction by hot rolling, solution treatments were applied, at 973 and 1273 K, to thermally induce martensite. The resulting specimens were analysed by X-ray diffraction (XRD and scanning electron microscopy (SEM, in order to reveal the presence of ε (hexagonal close-packed, hcp and α’ (body centred cubic, bcc thermally induced martensites. The reversion of thermally induced martensites, to γ (face centred cubic, fcc austenite, during heating, was confirmed by dynamic mechanical analysis (DMA, which emphasized marked increases of storage modulus and obvious internal friction maxima on DMA thermograms. The results proved that the increase of porosity degree, after PM processing, increased internal friction, while MA enhanced crystallinity degree.

  11. Powder metallurgy at Savannah River Laboratory

    International Nuclear Information System (INIS)

    Peacock, H.B.

    1978-12-01

    Development of a powder metallurgical process for the manufacture of reactor grade fuel tubes is being carried out at the Savannah River Laboratory (SRL). Using the P/M technology, cores were isostatically compacted with 100 wt % U 3 O 8 and coextruded tubes fabricated which contain up to approx. 80% cores clad with aluminum. Irradiation tests were completed for tubes with up to 59 wt % oxide. Post-irradiation inspection showed no significant swelling for 40% burnup. Thermal testing of sections from irradiated tubes showed that the threshold temperature for blister formation increased as the fission density of oxide decreased. Procedures are discussed for making PM cores and extruded tubes at SRL. Both laboratory and full-scale tests are presented

  12. Powder Metallurgy characteristics and application: state of the art

    International Nuclear Information System (INIS)

    Zaid, A.I.O.

    2005-01-01

    Powder metallurgy process (P/M) is a near-net or net-shape manufacturing process that combines the features of shape making technology of powder compaction with the development of final material and design properties (physical and mechanical) during subsequent densification or consolidation processes, e.g. sintering. It utilizes the metal powder or powders of metal alloys. In this paper, the major historical developments in P/M are reviewed and discussed. The main parameters involved in the process and their effects on the product characteristics are presented and discussed, which include: powders and methods of their production, particle size and shape, compressibility and additives, sintering temperature and time and finishing processes. The advantages and limitations of powder metallurgy are also presented and discussed. Finally, applications and future developments of the process are outlined and discussed. (author)

  13. Uranium 2000 : International symposium on the process metallurgy of uranium

    International Nuclear Information System (INIS)

    Ozberk, E.; Oliver, A.J.

    2000-01-01

    The International Symposium on the Process Metallurgy of Uranium has been organized as the thirtieth annual meeting of the Hydrometallurgy Section of the Metallurgical Society of the Canadian Institute of Mining, Metallurgy and Petroleum (CIM). This meeting is jointly organized with the Canadian Mineral Processors Division of CIM. The proceedings are a collection of papers from fifteen countries covering the latest research, development, industrial practices and regulatory issues in uranium processing, providing a concise description of the state of this industry. Topics include: uranium industry overview; current milling operations; in-situ uranium mines and processing plants; uranium recovery and further processing; uranium leaching; uranium operations effluent water treatment; tailings disposal, water treatment and decommissioning; mine decommissioning; and international regulations and decommissioning. (author)

  14. Microstructure and Aging of Powder-Metallurgy Al Alloys

    Science.gov (United States)

    Blackburn, L. B.

    1987-01-01

    Report describes experimental study of thermal responses and aging behaviors of three new aluminum alloys. Alloys produced from rapidly solidified powders and contain 3.20 to 5.15 percent copper, 0.24 to 1.73 percent magnesium, 0.08 to 0.92 percent iron, and smaller amounts of manganese, nickel, titanium, silicon, and zinc. Peak hardness achieved at lower aging temperatures than with standard ingot-metallurgy alloys. Alloys of interest for automobile, aircraft, and aerospace applications.

  15. Powder-metallurgy superalloy strengthened by a secondary gamma phase.

    Science.gov (United States)

    Kotval, P. S.

    1971-01-01

    Description of experiments in which prealloyed powders of superalloy compositions were consolidated by extrusion after the strengthening by precipitation of a body-centered tetragonal gamma secondary Ni3 Ta phase. Thin foil electron microscopy showed that the mechanical properties of the resultant powder-metallurgy product were correlated with its microstructure. The product exhibited high strength at 1200 F without loss of ductility, after thermomechanical treatment and aging.

  16. Mechanical and microstructural characterization of powder metallurgy CoCrNi medium entropy alloy

    Czech Academy of Sciences Publication Activity Database

    Moravčík, I.; Čížek, Jan; Kováčová, Z.; Nejezchlebová, J.; Kitzmantel, M.; Neubauer, E.; Kuběna, Ivo; Horník, Vít; Dlouhý, I.

    2017-01-01

    Roč. 701, July (2017), s. 370-380 ISSN 0921-5093 Institutional support: RVO:61389021 ; RVO:68081723 Keywords : tensile test * mechanical alloying * plasticity * mechanical characterization * powder metallurgy Subject RIV: JG - Metallurgy; JG - Metallurgy (UFM-A) OBOR OECD: Materials engineering ; Materials engineering (UFM-A) Impact factor: 3.094, year: 2016 https://www.sciencedirect.com/science/article/pii/S0921509317308535

  17. Development of Cu-Be bronzes through powder metallurgy

    International Nuclear Information System (INIS)

    Abbas, M.

    2012-01-01

    Copper and copper alloys are the major group of commercial alloy. One of the important copper bronzes is Copper beryllium. This is unique among all engineering alloys. Copper beryllium alloy possesses the highest strength in all the copper base alloys. Development of copper beryllium alloy with powder metallurgy is challenging problem due to toxicity of beryllium dust. Purpose of this project to find out parameters by which copper beryllium with all unique properties should obtained. For this purpose efforts are put on development of alternative to copper beryllium system like copper-tin and copper-aluminum by powder metallurgy route. Different time of milling with uniaxial pressure of about 200 MPa and different sintering temperature according to phase diagram of alloy, with different soaking time is tried. Problems may occur like decrease in density after sintering, breaking of samples by Rockwell A, B and C indenters arid by hammering. Cold iso-static pressing at 300 MPa and sintering at above 900 degree C is used to develop copper beryllium alloy. As quenched samples are heat treated at 260 degree C, 315 degree C and 370 degree C with different soaking time of 30, 90 and 180 minutes to find out optimum time and temperature parameters. . It is observed that at aging at 260 degree C for 180 minutes, aging at 315 degree C for 180 minutes and aging at 370 degree C for 30 minutes produce optimum result. By observing these pellets by SEM, precipitates appeared in peak-aged alloy and bigger precipitates in over-aged alloy. Copper beryllium alloy developed through powder metallurgy has better prospects than other copper bronzes. (author)

  18. Welding Metallurgy and Processing Issues for Joining of Power Sources

    Energy Technology Data Exchange (ETDEWEB)

    Lienert, Thomas J. [Los Alamos National Laboratory; Reardon, Patrick T. [Los Alamos National Laboratory

    2012-08-14

    Weldability issues with the pertinent alloys have been reviewed and preliminary results of our work on Haynes 25 have been presented. Further results on the mechanical properties and metallography on the EB welds are imminent. Hot-ductility experiments will commence within a few weeks. Aging studies on the effects of heat treatment using the Gleeble are also planned. MST-6 has extensive background in the welding metallurgy of the pertinent alloys. We also have considerable experience with the various welding processes to be used.

  19. Annual report of the Metallurgy Division - period ending December 1975

    International Nuclear Information System (INIS)

    1976-01-01

    The R and D activities of the Metallurgy Division of the Bhabha Atomic Research Centre, Bombay (India) during 1975 are described. Some of the R and D programmes of particular interest to nuclear technology are: (1) flowsheet development for the production of rare metals and alloys of nuclear use e.g. hafnium, beryllium, zirconium (2) metallurgical, irradiation hardening and corrosion studies on Zr and Zr-base alloys and (3) studies of nuclear ceramic materials such as UO2 and beryllia. (M.G.B.)

  20. CURRENT STATE AND TENDENCIES OF DEVELOPMENT OF FERROUS METALLURGY IN THE EAEU COUNTRIES

    Directory of Open Access Journals (Sweden)

    N. P. Dragun

    2016-01-01

    Full Text Available The analysis of modern status and tendencies of development of ferrous metallurgy in the countries of the EAEU is described in the article. On the basis of the conducted analysis are revealed the identified systemic problems of metallurgy and the conclusions on possible ways of their solution using the potential of integration are given.

  1. Preliminary analysis about reducing production costs in uranium mining and metallurgy at Fuzhou uranium mine

    International Nuclear Information System (INIS)

    Wu Sanmao

    1999-01-01

    The production costs in uranium ming and metallurgy have been analyzed quantitatively term by term according to present production situation for The Uranium Mining and Metallurgy Corp, which is part of Fuzhou Uranium Mine. The principal factors influencing on the production costs and the main means reducing the production costs have been found

  2. Feasibility study of the production of biomedical Ti-6Al-4V alloy by powder metallurgy.

    Science.gov (United States)

    Bolzoni, L; Ruiz-Navas, E M; Gordo, E

    2015-04-01

    Titanium and its alloys are characterized by an exceptional combination of properties like high strength, good corrosion resistance and biocompatibility which makes them suitable materials for biomedical prosthesis and devices. The wrought Ti-6Al-4V alloy is generally favored in comparison to other metallic biomaterials due to its relatively low elastic modulus and it has been long used to obtain products for biomedical applications. In this work an alternative route to fabricate biomedical implants made out of the Ti-6Al-4V alloy is investigated. Specifically, the feasibility of the conventional powder metallurgy route of cold uniaxial pressing and sintering is addressed by considering two types of powders (i.e. blended elemental and prealloyed). The characterization of physical properties, chemical analysis, mechanical behavior and microstructural analysis is carried out in-depth and the properties are correlated among them. On the base of the results found, the produced alloys are promising materials for biomedical applications as well as cheaper surgical devices and tools. Copyright © 2015 Elsevier B.V. All rights reserved.

  3. Evaluation of the mechanical properties of powder metallurgy Ti-6Al-7Nb alloy.

    Science.gov (United States)

    Bolzoni, L; Ruiz-Navas, E M; Gordo, E

    2017-03-01

    Titanium and its alloys are common biomedical materials owing to their combination of mechanical properties, corrosion resistance and biocompatibility. Powder metallurgy (PM) techniques can be used to fabricate biomaterials with tailored properties because changing the processing parameters, such as the sintering temperature, products with different level of porosity and mechanical performances can be obtained. This study addresses the production of the biomedical Ti-6Al-7Nb alloy by means of the master alloy addition variant of the PM blending elemental approach. The sintering parameters investigated guarantee that the complete diffusion of the alloying elements and the homogenization of the microstructure is achieved. The sintering of the Ti-6Al-7Nb alloy induces a total shrinkage between 7.4% and 10.7% and the level of porosity decreases from 6.2% to 4.7% with the increment of the sintering temperature. Vickers hardness (280-300 HV30) and tensile properties (different combination of strength and elongation around 900MPa and 3%) are achieved. Copyright © 2016 Elsevier Ltd. All rights reserved.

  4. Characterization of TiC-FeCrMn Cermets Produced by Powder Metallurgy Method

    Directory of Open Access Journals (Sweden)

    Märt Kolnes

    2015-09-01

    Full Text Available TiC-NiMo cermets combine relatively low density with high hardness. Because nickel is known as a toxin and allergen and allergy to nickel is a phenomenon which has assumed growing importance in recent years there has been a flurry of activity to find alternatives to the nickel binder in cermets. It is also the global research and technical development trend in the powder metallurgy cermets industry. In present research TiC-based cermets with FeCrMn binder system were fabricated. Three different sintering conditions were used (vacuum sintering, sinter/HIP and sintering under low Ar pressure. Because of high vapor pressure of manganese different sintering conditions and technologies were investigated to depress the Mn-loss during sintering. Chemical composition of TiC-FeCrMn cermets after different sintering conditions were analyzed by energy-dispersive X-ray spectroscopy (EDS and mechanical properties – hardness and fracture toughness were evaluated on the samples. Results of research showed that Ni-free TiC-based CrMn-steels bonded cermets compare unfavorably with cermets bonded with CrNi austenitic steels in terms of fracture toughness and corrosion resistance. Noticeable Mn-loss during vacuum sintering can be avoided when sintering under low Ar gas pressure.DOI: http://dx.doi.org/10.5755/j01.ms.21.3.7364

  5. Deformation and energy absorption properties of powder-metallurgy produced Al foams

    International Nuclear Information System (INIS)

    Michailidis, N.; Stergioudi, F.; Tsouknidas, A.

    2011-01-01

    Highlights: → Porous Al fabricated via a dissolution and sintering method using raw cane sugar. → Different deformation mode depending on the relative density of the foams. → Enhanced energy absorption by reducing pore size and relative density of the foam. → Pore size uniformity and sintering temperature affect energy absorption. - Abstract: Al-foams with relative densities ranging from 0.30 to 0.60 and mean pore sizes of 0.35, 0.70 and 1.35 mm were manufactured by a powder metallurgy technology, based on raw cane sugar as a space-holder material. Compressive tests were carried out to investigate the deformation and energy absorbing characteristics and mechanisms of the produced Al-foams. The deformation mode of low density Al-foams is dominated by the bending and buckling of cell walls and the formation of macroscopic deformation bands whereas that of high density Al-foams is predominantly attributed to plastic yielding. The energy absorbing capacity of Al-foams rises for increased relative density and compressive strength. The sintering temperature of Al-foams having similar relative densities has a marked influence on both, energy absorbing efficiency and capacity. Pore size has a marginal effect on energy efficiency aside from Al-foams with mean pore size of 0.35 which exhibit enhanced energy absorption as a result of increased friction during deformation at lower strain levels.

  6. New alloying systems for ferrous powder metallurgy precision parts

    Directory of Open Access Journals (Sweden)

    Danninger H.

    2008-01-01

    Full Text Available Traditionally, the common alloy elements for sintered steels have been Cu and Ni. With increasing requirements towards mechanical properties, and also as a consequence of soaring prices especially for these two metals, other alloy elements have also become more and more attractive for sintered steels, which make the steels however more tricky to process through PM. Here, the chances and risks of using in particular Cr and Mn alloy steels are discussed, considering the different alloying techniques viable in powder metallurgy, and it is shown that there are specific requirements in particular for sintering process. The critical importance of chemical reactions between the metal and the atmosphere is described, and it is shown that not only O2 and H2O but also H2 and even N2 can critically affect sintering and microstructural homogenization.

  7. Stress analyses of pump gears produced by powder metallurgy

    Energy Technology Data Exchange (ETDEWEB)

    Cetinel, Hakan [Celal Bayar Univ., Mechanical Engineering Dept. (Turkey); Yilmaz, Burak

    2013-06-01

    In this study, trochoidal type (gerotor) hydraulic pump gears were produced by powder metallurgy (P/M) technique. Several gears with different mechanical properties have been obtained by changing process variables. The tooth contact stresses were calculated analytically under particular operation conditions of the hydraulic pump. The 3D models have been obtained from real gears by using Capability Maturity Model (CMM, 3D scanning) operation and SOLIDWORKS software. Stress analyses were conducted on these 3D models by using ANSYS WORKBENCH software. It was found that the density increases by the increase of sintering duration and mechanical properties were positively affected by the increase of density. Maximum deformation takes place in the region of the outer gear where failure generally occurs with the minimum cross-section area.

  8. N18, powder metallurgy superalloy for disks: Development and applications

    Energy Technology Data Exchange (ETDEWEB)

    Guedou, J.Y.; Lautridou, J.C.; Honnorat, Y. (SNECMA, Evry (France). Materials and Processes Dept.)

    1993-08-01

    The preliminary industrial development of a powder metallurgy (PM) superalloy, designated N18, for disk applications has been completed. This alloy exhibits good overall mechanical properties after appropriate processing of the material. These properties have been measured on both isothermally forged and extruded billets, as well as on specimens cut from actual parts. The temperature capability of the alloy is about 700 C for long-term applications and approximately 750 C for short-term use because of microstructural instability. Further improvements in creep and crack propagation properties, without significant reduction in tensile strength, are possible through appropriate thermomechanical processing, which results in a large controlled grain size. Spin pit tests on subscale disks have confirmed that the N18 alloy has a higher resistance than PM Astrology and is therefore an excellent alloy for modern turbine disk applications.

  9. Powder metallurgy: Solid and liquid phase sintering of copper

    Science.gov (United States)

    Sheldon, Rex; Weiser, Martin W.

    1993-01-01

    Basic powder metallurgy (P/M) principles and techniques are presented in this laboratory experiment. A copper based system is used since it is relatively easy to work with and is commercially important. In addition to standard solid state sintering, small quantities of low melting metals such as tin, zinc, lead, and aluminum can be added to demonstrate liquid phase sintering and alloy formation. The Taguchi Method of experimental design was used to study the effect of particle size, pressing force, sintering temperature, and sintering time. These parameters can be easily changed to incorporate liquid phase sintering effects and some guidelines for such substitutions are presented. The experiment is typically carried out over a period of three weeks.

  10. Advanced powder metallurgy aluminum alloys via rapid solidification technology

    Science.gov (United States)

    Ray, R.

    1984-01-01

    Aluminum alloys containing 10 to 11.5 wt. pct. of iron and 1.5 to 3 wt. pct. of chromium using the technique of rapid solidification powder metallurgy were studied. Alloys were prepared as thin ribbons (.002 inch thick) rapidly solidified at uniform rate of 10(6) C/second by the melt spinning process. The melt spun ribbons were pulverized into powders (-60 to 400 mesh) by a rotating hammer mill. The powders were consolidated by hot extrusion at a high reduction ratio of 50:1. The powder extrusion temperature was varied to determine the range of desirable processing conditions necessary to yield useful properties. Powders and consolidated alloys were characterized by SEM and optical metallography. The consolidated alloys were evaluated for (1) thermal stability, (2) tensile properties in the range, room temperature to 450 F, and (3) notch toughness in the range, room temperature to 450 F.

  11. Mechanical properties and strain effects in superconductors: Metallurgy, fabrication, and applications

    International Nuclear Information System (INIS)

    Ekin, J.W.

    1981-01-01

    This paper studies the mechanical properties and material strain effects for magnet design in superconductors. The material strain limit for typical magnet systems such as multifilamentary Nb 3 Sn, Nb 3 Sn dipoles plus small bore, pulsed NbTi:Cu, epoxy impregnated, and large SS reinforced are given, along with the limiting property, and the material limit. For each magnet type, a different mechanical property and material play the limiting role: In multifilamentary Nb 3 Sn magnets, uniaxial-strain degradation of I /SUB c/ is the limiting factor. If, in addition, the Nb 3 Sn magnet is a dipole or small bore magnet, the tight bend radius required of the conductor sets bending strain limits on the conductor thickness. In pulsed NbTi:copper magnets that will be cycled many times without anneal, fatigue degradation of the stabilizing copper matrix is the primary factor placing limits on the peak-to-peak strain amplitude. In high-current density, epoxy-impregnated magnets, excessive training caused by the low strain tolerance of epoxies at cryogenic temperatures generally plays the primary role. Finally, in large reinforced magnets, the yield properties of the structural reinforcement material set the mechanical design limits

  12. Uranium mining and metallurgy library information service under the network environment

    International Nuclear Information System (INIS)

    Tang Lilei

    2012-01-01

    This paper analyzes the effect of the network environment on the uranium mining and metallurgy of the information service. Introduces some measures such as strengthening professional characteristic literature resources construction, changing the service mode, building up information navigation, deepening service, meet the individual needs of users, raising librarian's quality, promoting the co-construction and sharing of library information resources, and puts forward the development idea of uranium mining and metallurgy library information service under the network environment. (author)

  13. Production of uranium in Navoi Mining and Metallurgy Combinat, Uzbekistan

    International Nuclear Information System (INIS)

    Kuchersky, N.; Tolstov, E.A.; Mazurkevich, A.P.; Inozemzev, S.B.

    2001-01-01

    Full text: Under the conditions of constantly increasing level of development of the nuclear power, it is inevitable that the uranium stockpiles accumulated to 1985 will soon be depleted. This consideration underlies the development concept of uranium production in the Navoi Mining and Metallurgy Combinat, Uzbekistan. Because this product has become a source of hard currency revenues for the Republic, there will be a significant increase in the processed ore and output of uranium oxide within the next few years. Uranium production in the Navoi Mining and Metallurgy Combinat represents a full-cycle operations ranging from geological survey through hydrometallurgical processing resulting in the output of uranium concentrate in the form of uranium protoxide-oxide (U 3 O 8 ). The NMMC uranium operations include the Hydrometallurgical Plant and three facilities accomplishing ISL mining facilities. A successful start on the development of the Uchkuduk deposit by ISL method in the 1960s gave rise to scientific and production approach for development of other uranium deposits of the infiltration bedded (sandstone) type. Uranium recovery by ISL has become a separate mining branch within the 30-year period of its history and the contribution of this branch in uranium production has steadily grown. Since 1995 all uranium produced by Navoi Mining and Metallurgy Combinat is attributed to ISL. During this evolution period of the ISL method, a whole range of systematic scientific research and practical works were carried out covering improvement of process flowsheets, equipment, operational methods and techniques for particular mining conditions at those specific sites. In co-operation with design and scientific research institutions, a significant number of scientific researches, test works, design and engineering projects were achieved in order to create optimal conditions for ISL mining and further processing of pregnant solutions by sorption as well as to appropriately equip

  14. Development and application of characteristic database for uranium mining and metallurgy in the library of Beijing Research Institute of Chemical Engineering and Metallurgy

    International Nuclear Information System (INIS)

    Gao Renxi

    2012-01-01

    Beijing Research Institute of Chemical Engineering and Metallurgy (BRICEM) is a multi disciplinary comprehensive research institute engaged in uranium mining, engineering design and related material researches. After 53 years of researches and development, BRICEM has accumulated a plenty of valuable data and resources. By analyzing the actual conditions of BRICEM's technological database, this thesis aims to propose the idea of building a characteristic database for uranium mining and metallurgy. It gives an in-depth analysis on content design, development status and problems of database development, in order to come up with solutions to these problems, as well as suggestions on the future development plans of the characteristic database. (author)

  15. Fabrication of a Textured Non-Magnetic Ni-12at.%V Alloy Substrate for Coated Conductors

    DEFF Research Database (Denmark)

    Gao, M. M.; Grivel, Jean-Claude; Suo, H. L.

    2011-01-01

    Ni-12at.%V alloy is a promising candidate for non-magnetic cube textured metallic substrates used for high temperature coated conductors. In this work, a textured Ni-12at.%V substrate has been fabricated by powder metallurgy route. After cold rolling and recrystallization annealing, a cube texture...

  16. Production of titanium alloys for medical implants by powder metallurgy

    Energy Technology Data Exchange (ETDEWEB)

    Henriques, V.A.R. [Dept. de Engenharia de Materiais, Faculdade de Engenharia Quimica de Lorena, Lorena SP (Brazil); Silva, C.R.M. da [Div. de Materiais, CTA-IAE-AMR, Sao Jose dos Campos SP (Brazil)

    2001-07-01

    Titanium alloys are expected to be much more widely used for implant materials in the medical and dental fields because of their superior biocompatibility, corrosion resistance and specific strength compared with other metallic implant materials. Vanadium free alloys like Ti-6Al-7Nb and Ti-5Al-2,5Fe have been recently developed for biomedical use. More recently vanadium and aluminum free alloys composed of non-toxic elements like Nb, Ta, Zr and so on with lower modulus have been started to be developed. The {beta} type alloys like Ti-15Mo are now the main target for medical materials. A blended elemental titanium powder metallurgy process has been developed to offer low cost products. The process employs hydride-dehydride (HDH) powders and near-net shape techniques. In this work, the influence of the processing parameters and chemical composition of the elementary powders on the final microstructure was investigated. The alloys were characterized by means of scanning electron microscopy, X-ray diffraction, Vickers microhardness measurements, chemical analysis and density. The results indicate that the samples presented high densification, homogeneous chemical composition and coherent microstructures. The process parameters were defined aiming to reduce the interstitial pick-up (O, N) and to avoid the grain growth. (orig.)

  17. The traces of roman metallurgy in Eastern Serbia

    Directory of Open Access Journals (Sweden)

    Petković Sofija

    2009-01-01

    Full Text Available The archaeological traces of the Roman mining and metallurgy in eastern Serbia are rather frequent but insufficiently studied and published. Three mining-metallurgical regions abounding in gold, silver, copper, iron and lead could be distinguished there: 1. the upper course of the Pek river, metalla Pincensia, 2. the area between Bor, Zlot, Crna Reka and Rgotina and 3. the area in the river basin of Beli Timok, two latter ones had been organized as territoria metallorum. The archeometallurgical sites confirmed by investigations are: Kraku lu Jordan at the confluence of the Brodica river and the Pek river, Rudna Glava, Tilva Roš in Bor, Gamzigrad - Romuliana, Rgotina near Zaječar and Timacum Minus in the village Ravna near Knjaževac. Roman mining-metallurgical activities in eastern Serbia flourished from the end of the 3rd century, were interrupted by the invasion of Huns in AD 441. and restored in the time of emperors Anastasius and Justin I, in the end of the 5th - beginning of the 6th centuries. The Roman mining-metallurgical centers functioned in the 6th century until the Slav invasion in the beginning of the 7th century.

  18. Wear mechanisms in powder metallurgy high speed steels matrix composites

    International Nuclear Information System (INIS)

    Gordo, E.; Martinez, M. A.; Torralba, J. M.; Jimenez, J. A.

    2001-01-01

    The development of metal matrix composites has a major interest for automotive and cutting tools industries since they possess better mechanical properties and wear resistance than corresponding base materials. One of the manufacturing methods for these materials includes processing by powder metallurgy techniques. in this case, blending of both, base material and reinforcement powders constitute the most important process in order to achieve a homogeneous distribution of second phase particles. in the present work, composite materials of M3/2 tool steel reinforced with 2.5,5 and 8 vol% of niobium carbide have been prepared. In order to ensure a homogeneous mix, powders of both materials were mixed by dry high-energy mechanical milling at 200 r.p.m. for 40 h. After a recovering annealing, two routes for consolidate were followed die pressing and vacuum sintering, and hot isostatic pressing (HIP). Pin-on-disc tests were carried out to evaluate wear behaviour in all the materials. Results show that ceramic particles additions improve wear resistance of base material. (Author) 9 refs

  19. TRADITIONAL METALLURGY, NANOTECHNOLOGIES AND STRUCTURAL MATERIALS: A SORBY AWARD LECTURE

    Energy Technology Data Exchange (ETDEWEB)

    Louthan, M

    2007-07-17

    Traditional metallurgical processes are among the many ''old fashion'' practices that use nanoparticles to control the behavior of materials. Many of these practices were developed long before microscopy could resolve nanoscale features, yet the practitioners learned to manipulate and control microstructural elements that they could neither see nor identify. Furthermore, these early practitioners used that control to modify microstructures and develop desired material properties. Centuries old colored glass, ancient high strength steels and medieval organ pipes derived many of their desirable features through control of nanoparticles in their microstructures. Henry Sorby was among the first to recognize that the properties of rocks, minerals, metals and organic materials were controlled by microstructure. However, Mr. Sorby was accused of the folly of trying to study mountains with a microscope. Although he could not resolve nanoscale microstructural features, Mr. Sorby's observations revolutionized the study of materials. The importance of nanoscale microstructural elements should be emphasized, however, because the present foundation for structural materials was built by manipulating those features. That foundation currently supports several multibillion dollar industries but is not generally considered when the nanomaterials revolution is discussed. This lecture demonstrates that using nanotechnologies to control the behavior of metallic materials is almost as old as the practice of metallurgy and that many of the emergent nanomaterials technologists are walking along pathways previously paved by traditional metallurgists.

  20. [Possible health effects associated with Pre-Columbian metallurgy].

    Science.gov (United States)

    Idrovo, Alvaro Javier

    2005-09-01

    In the Old World, several researchers have indicated that adverse health effects were associated with exposure to arsenic, and that this influenced a change in the use of copper-arsenic alloys to others less toxic. This hypothesis was evaluated for three Pre-Columbian metallurgy traditions: Central Andes, Intermediate Area, and West Mexico. The metal artifacts from the Central Andes showed arsenic concentrations similar to those in the Old World (0.5%-1.0%). In the Intermediate Area the values were smallest; however, in West Mexico the arsenic content was very high (7%-25%). In Central Andes arsenical bronze was used initially, but copper-tin alloys when introduced were preferred and distributed throughout the Inca Empire. Osteological and artistic evidences of foot amputations among Moche individuals from Central Andes support the presence of "black foot disease" (a condition associated with arsenic poisoning) among Pre-Columbian populations. In conclusion, the adverse effects of arsenic have been observed in the New World, and that these effects promoted a change toward the use of less toxic alloys.

  1. Indexation Rules for Metallurgy in PASCAL. Original Title: Regles d'Indexation de la Metallurgie'--Technical Note Issued by Informascience--January 1980. Translated by Marie Wallin.

    Science.gov (United States)

    Royal Inst. of Tech., Stockholm (Sweden). Library.

    The indexing rules presented are designed for use with a new French-German database on metallurgy being developed under an agreement by CNRS (Centre National de la Recherche Scientifique, Paris) and BAM (Bundesanstalt fur Materialprufung, Berlin). The new database, which will feature multilingual titles and index terms (French-German-English-) and…

  2. Fabrication Facilities

    Data.gov (United States)

    Federal Laboratory Consortium — The Fabrication Facilities are a direct result of years of testing support. Through years of experience, the three fabrication facilities (Fort Hood, Fort Lewis, and...

  3. Dual-Alloy Disks are Formed by Powder Metallurgy

    Science.gov (United States)

    Harf, F. H.; Miner, R. V.; Kortovich, C. S.; Marder, J. M.

    1982-01-01

    High-performance disks have widely varying properties from hub to rim. Dual property disk is fabricated using two nickel-base alloys, AF-115 for rim and Rene 95 for hub. Dual-alloy fabrication may find applications in automobiles, earth-moving equipment, and energy conversion systems as well as aircraft powerplants. There is potential for such applications as shafts, gears, and blades.

  4. [Atmospheric emission of PCDD/Fs from secondary aluminum metallurgy industry in the southwest area, China].

    Science.gov (United States)

    Lu, Yi; Zhang, Xiao-Ling; Guo, Zhi-Shun; Jian, Chuan; Zhu, Ming-Ji; Deng, Li; Sun, Jing; Zhang, Qin

    2014-01-01

    Five secondary aluminum metallurgy enterprises in the southwest area of China were measured for emissions of PCDD/Fs. The results indicated that the emission levels of PCDD/Fs (as TEQ) were 0.015-0.16 ng x m(-3), and the average was 0.093 ng x m(-3) from secondary aluminum metallurgy enterprises. Emission factors of PCDD/Fs (as TEQ) from the five secondary aluminum metallurgy enterprises varied between 0.041 and 4.68 microg x t(-1) aluminum, and the average was 2.01 microg x t(-1) aluminum; among them, PCDD/Fs emission factors from the crucible smelting furnace was the highest. Congener distribution of PCDD/F in stack gas from the five secondary aluminum metallurgies was very different from each other. Moreover, the R(PCDF/PCDD) was the lowest in the enterprise which was installed only with bag filters; the R(PCDF/PCDD) were 3.8-12.6 (the average, 7.7) in the others which were installed with water scrubbers. The results above indicated that the mechanism of PCDD/Fs formation was related to the types of exhaust gas treatment device. The results of this study can provide technical support for the formulation of PCDD/Fs emission standards and the best available techniques in the secondary aluminum metallurgy industry.

  5. Powder Metallurgy of Uranium Alloy Fuels for TRU-Burning Reactors Final Technical Report

    International Nuclear Information System (INIS)

    McDeavitt, Sean M.

    2011-01-01

    Overview Fast reactors were evaluated to enable the transmutation of transuranic isotopes generated by nuclear energy systems. The motivation for this was that TRU isotopes have high radiotoxicity and relatively long half-lives, making them unattractive for disposal in a long-term geologic repository. Fast reactors provide an efficient means to utilize the energy content of the TRUs while destroying them. An enabling technology that requires research and development is the fabrication metallic fuel containing TRU isotopes using powder metallurgy methods. This project focused upon developing a powder metallurgical fabrication method to produce U-Zr-transuranic (TRU) alloys at relatively low processing temperatures (500 C to 600 C) using either hot extrusion or alpha-phase sintering for charecterization. Researchers quantified the fundamental aspects of both processing methods using surrogate metals to simulate the TRU elements. The process produced novel solutions to some of the issues relating to metallic fuels, such as fuel-cladding chemical interactions, fuel swelling, volatility losses during casting, and casting mold material losses. Workscope There were two primary tasks associated with this project: (1) Hot working fabrication using mechanical alloying and extrusion - Design, fabricate, and assemble extrusion equipment - Extrusion database on DU metal - Extrusion database on U-10Zr alloys - Extrusion database on U-20xx-10Zr alloys - Evaluation and testing of tube sheath metals (2) Low-temperature sintering of U alloys - Design, fabricate, and assemble equipment - Sintering database on DU metal - Sintering database on U-10Zr alloys - Liquid assisted phase sintering on U-20xx-10Zr alloys Appendices Outline Appendix A contains a Fuel Cycle Research and Development (FCR and D) poster and contact presentation where TAMU made primary contributions. Appendix B contains MSNE theses and final defense presentations by David Garnetti and Grant Helmreich outlining the

  6. Powder Metallurgy of Uranium Alloy Fuels for TRU-Burning Reactors Final Technical Report

    Energy Technology Data Exchange (ETDEWEB)

    McDeavitt, Sean M

    2011-04-29

    Overview Fast reactors were evaluated to enable the transmutation of transuranic isotopes generated by nuclear energy systems. The motivation for this was that TRU isotopes have high radiotoxicity and relatively long half-lives, making them unattractive for disposal in a long-term geologic repository. Fast reactors provide an efficient means to utilize the energy content of the TRUs while destroying them. An enabling technology that requires research and development is the fabrication metallic fuel containing TRU isotopes using powder metallurgy methods. This project focused upon developing a powder metallurgical fabrication method to produce U-Zr-transuranic (TRU) alloys at relatively low processing temperatures (500ºC to 600ºC) using either hot extrusion or alpha-phase sintering for charecterization. Researchers quantified the fundamental aspects of both processing methods using surrogate metals to simulate the TRU elements. The process produced novel solutions to some of the issues relating to metallic fuels, such as fuel-cladding chemical interactions, fuel swelling, volatility losses during casting, and casting mold material losses. Workscope There were two primary tasks associated with this project: 1. Hot working fabrication using mechanical alloying and extrusion • Design, fabricate, and assemble extrusion equipment • Extrusion database on DU metal • Extrusion database on U-10Zr alloys • Extrusion database on U-20xx-10Zr alloys • Evaluation and testing of tube sheath metals 2. Low-temperature sintering of U alloys • Design, fabricate, and assemble equipment • Sintering database on DU metal • Sintering database on U-10Zr alloys • Liquid assisted phase sintering on U-20xx-10Zr alloys Appendices Outline Appendix A contains a Fuel Cycle Research & Development (FCR&D) poster and contact presentation where TAMU made primary contributions. Appendix B contains MSNE theses and final defense presentations by David Garnetti and Grant Helmreich

  7. Effects of Plasma ZrN Metallurgy and Shot Peening Duplex Treatment on Fretting Wear and Fretting Fatigue Behavior of Ti6Al4V Alloy.

    Science.gov (United States)

    Tang, Jingang; Liu, Daoxin; Zhang, Xiaohua; Du, Dongxing; Yu, Shouming

    2016-03-23

    A metallurgical zirconium nitride (ZrN) layer was fabricated using glow metallurgy using nitriding with zirconiuming prior treatment of the Ti6Al4V alloy. The microstructure, composition and microhardness of the corresponding layer were studied. The influence of this treatment on fretting wear (FW) and fretting fatigue (FF) behavior of the Ti6Al4V alloy was studied. The composite layer consisted of an 8-μm-thick ZrN compound layer and a 50-μm-thick nitrogen-rich Zr-Ti solid solution layer. The surface microhardness of the composite layer is 1775 HK 0.1 . A gradient in cross-sectional microhardness distribution exists in the layer. The plasma ZrN metallurgical layer improves the FW resistance of the Ti6Al4V alloy, but reduces the base FF resistance. This occurs because the improvement in surface hardness results in lowering of the toughness and increasing in the notch sensitivity. Compared with shot peening treatment, plasma ZrN metallurgy and shot peening composite treatment improves the FW resistance and enhances the FF resistance of the Ti6Al4V alloy. This is attributed to the introduction of a compressive stress field. The combination of toughness, strength, FW resistance and fatigue resistance enhance the FF resistance for titanium alloy.

  8. Influence of the chemical composition and the fabrication process on the behaviour of high temperature oxidation of Fe-Cr-Al alloys

    International Nuclear Information System (INIS)

    Clemendot, F.; Arnoldi, F.; Cerede, J.B.; Dionnet, B.; Nardou, F.; Duysen, J.C. van

    1993-01-01

    The oxidation behaviour of four industrial Fe-Cr-Al alloys was studied. Two of them were Fe-Cr-Al alloys fabricated either by melting or by powder metallurgy. The two other ones were Fe-Cr-Al-Y alloys either produced by melting or by mechanical alloying. On these alloys, we determined oxidation kinetics and observed the morphology of the oxide layer after isothermal and cyclic exposures from 1000 C up to 1300 C. The beneficial effect of yttrium on the adherence of oxide layers was confirmed. The powder metallurgy fabrication route does not improve the oxidation resistance of yttrium-free alloys. On the other hand, the association of the powder metallurgy and the addition of yttrium allow the manufacturing of alloys which present an excellent behaviour to high temperature oxidation. (orig.)

  9. Superplasticity in powder metallurgy aluminum alloys and composites

    International Nuclear Information System (INIS)

    Mishra, R.S.; Bieler, T.R.; Mukherjee, A.K.

    1995-01-01

    Superplasticity in powder metallurgy Al alloys and composites has been reviewed through a detailed analysis. The stress-strain curves can be put into 4 categories: classical well-behaved type, continuous strain hardening type, continuous strain softening type and complex type. The origin of these different types of is discussed. The microstructural features of the processed material and the role of strain have been reviewed. The role of increasing misorientation of low angle boundaries to high angle boundaries by lattice dislocation absorption is examined. Threshold stresses have been determined and analyzed. The parametric dependencies for superplastic flow in modified conventional aluminum alloys, mechanically alloyed alloys and Al alloy matrix composites is determined to elucidate the superplastic mechanism at high strain rates. The role of incipient melting has been analyzed. A stress exponent of 2, an activation energy equal to that for grain boundary diffusion and a grain size dependence of 2 generally describes superplastic flow in modified conventional Al alloys and mechanically alloyed alloys. The present results agree well with the predictions of grain boundary sliding models. This suggests that the mechanism of high strain rate superplasticity in the above-mentioned alloys is similar to conventional superplasticity. The shift of optimum superplastic strain rates to higher values is a consequence of microstructural refinement. The parametric dependencies for superplasticity in aluminum alloy matrix composites, however, is different. A true activation energy of superplasticity in aluminum alloy matrix composites, however, is different. A true activation energy of 313 kJ/mol best describes the composites having SiC reinforcements. The role of shape of the reinforcement (particle or whisker) and processing history is addressed. The analysis suggests that the mechanism for superplasticity in composites is interface diffusion controlled grain boundary sliding

  10. Corrosion inhibition of powder metallurgy Mg by fluoride treatments.

    Science.gov (United States)

    Pereda, M D; Alonso, C; Burgos-Asperilla, L; del Valle, J A; Ruano, O A; Perez, P; Fernández Lorenzo de Mele, M A

    2010-05-01

    Pure Mg has been proposed as a potential degradable biomaterial to avoid both the disadvantages of non-degradable internal fixation implants and the use of alloying elements that may be toxic. However, it shows excessively high corrosion rate and insufficient yield strength. The effects of reinforcing Mg by a powder metallurgy (PM) route and the application of biocompatible corrosion inhibitors (immersion in 0.1 and 1M KF solution treatments, 0.1M FST and 1M FST, respectively) were analyzed in order to improve Mg mechanical and corrosion resistance, respectively. Open circuit potential measurements, polarization techniques (PT), scanning electrochemical microscopy (SECM) and electrochemical impedance spectroscopy (EIS) were performed to evaluate its corrosion behavior. SECM showed that the local current of attacked areas decreased during the F(-) treatments. The corrosion inhibitory action of 0.1M FST and 1M FST in phosphate buffered solution was assessed by PT and EIS. Under the experimental conditions assayed, 0.1M FST revealed better performance. X-ray photoelectron spectroscopy, energy dispersive X-ray and X-ray diffraction analyses of Mg(PM) with 0.1M FST showed the presence of KMgF(3) crystals on the surface while a MgF(2) film was detected for 1M FST. After fluoride inhibition treatments, promising results were observed for Mg(PM) as degradable metallic biomaterial due to its higher yield strength and lower initial corrosion rate than untreated Mg, as well as a progressive loss of the protective characteristics of the F(-)-containing film which ensures the gradual degradation process. Copyright (c) 2009 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

  11. Progress report of the Metallurgy Division for the period 1978-1980

    International Nuclear Information System (INIS)

    Sharma, B.D.; Mohan, Ashok; Bose, D.K.; Rao, C.N.; Chouthai, S.S.

    1980-01-01

    The research and development (R and D) work of the Metallurgy Division of the Bhabha Atomic Research Centre at Bombay for the period 1978-1980 is reported in the form of individual summaries under the headings: extractive metallurgy section, physical metallurgy section, corrosion and electrometallurgy section, ceramics section. Progress of work of beryllium pilot plant project, programme for R-5 utilisation for materials irradiation research project, development of rare, reactive and refractory metals, and development of ceramics materials for MHD programme is surveyed. Lists of publications, deputations, visits, conferences, colloquia are given. A chart at the end shows the various sections of the Division and personnel in each section. (M.G.B.)

  12. Introduction to powder metallurgy processes for titanium manufacturing; Introduccion al procesado pulvimetalurgico del titanio

    Energy Technology Data Exchange (ETDEWEB)

    Esteban, P. G.; Bolzoni, L.; Ruiz-Navas, E. M.; Gordo, E.

    2011-07-01

    The development of new extraction processes to produce titanium in powder form leads Powder Metallurgy to an advantage position among the manufacturing processes for titanium. The cost reduction of base material, coupled with the economy of the powder metallurgy processes, give titanium industry the chance to diversify its products, which could lead to production volumes able to stabilise the price of the metal. This work reviews some of the Powder Metallurgy techniques for the manufacturing of titanium parts, and describes the two typical approaches for titanium manufacturing: Blending Elemental and Prealloyed Powders. Among others, conventional pressing and sintering are described, which are compared with cold and hot isostatic pressing techniques. Real and potential applications are described. (Author) 71 refs.

  13. 76 FR 64344 - Amended Record of Decision for the Nuclear Facility Portion of the Chemistry and Metallurgy...

    Science.gov (United States)

    2011-10-18

    ... the same sets of safety controls and key equipment. Further, as the SEIS analysis indicates, once... Nuclear Facility Portion of the Chemistry and Metallurgy Research Building Replacement Project at Los...) for the Nuclear Facility portion of the Chemistry and Metallurgy Research Building Replacement (CMRR...

  14. Modernization of the Ural Metallurgy during the Great Patriotic War (1941–1945

    Directory of Open Access Journals (Sweden)

    Vladimir V. Zaparii

    2013-09-01

    Full Text Available The article characterizes the Ural industry modernization in war footing, shows the significance of evacuation of enterprises from the Western areas of the country to the region, reveals their role in the formation of a new metallurgical center of modern metallurgy in terms of human resources and manufacture. Innovations in metallurgy, the role of human factor in solving industrial restructuring problem are examined. Forms and methods of science use for the industrial modernization are considered. Solving of human resources problem is shown. The author touches upon the problem of metallurgical sector management in wartime. The role of people’s heroism in this difficult period of Russian history is discussed.

  15. Metallurgy of high-silicon steel parts produced using Selective Laser Melting

    OpenAIRE

    Garibaldi, Michele; Ashcroft, Ian; Simonelli, Marco; Hague, Richard

    2016-01-01

    The metallurgy of high-silicon steel (6.9%wt.Si) processed using Selective Laser Melting (SLM) is presented for the first time in this study. High-silicon steel has great potential as a soft magnetic alloy, but its employment has been limited due to its poor workability. The effect of SLM-processing on the metallurgy of the alloy is investigated in this work using microscopy, X-Ray Diffraction (XRD) and Electron Backscatter Diffraction (EBSD). XRD analysis suggests that the SLM high-silicon s...

  16. [Analysis of changes in characteristics of arterial hypertension occupational risk in workers of nonferrous metallurgy].

    Science.gov (United States)

    Vlasova, E M; Shliapnikov, D M; Lebedeva, T M

    2015-01-01

    The article covers changes in occupational cardiovascular risk for workers of nonferrous,metallurgy. Findings are that exposure to noise up to 94 dB with length of service increases possible atherosclerosis and metabolic syndrome. With 5 years of service, risk of the predicted conditions increases by 40.5%. When occupational exposure lasts over 5 years, risk of arterial hypertension increases. A group of workers without exposure to occupational factors appeared to have no connection between length of service and metabolic syndrome and arterial hypertension. Risk evolution modelling proved that risk of functional disorders in nonferrous metallurgy workers becomes unacceptable after 5 years of service (cardiovascular disorders are critical).

  17. Enhanced ductility of Mg–3Al–1Zn alloy reinforced with short length multi-walled carbon nanotubes using a powder metallurgy method

    Directory of Open Access Journals (Sweden)

    Muhammad Rashad

    2015-08-01

    Full Text Available Mg–3Al–1Zn–CNTs composites, with different weight fractions (0.25–1.0 wt% of carbon nanotubes (CNTs were successfully fabricated via a powder metallurgy method. The processing parameters were adopted in such a way to have uniform dispersion of short length CNTs without any damage, as well as refined and dissolved β phases structures throughout the composite matrix. The composite exhibited impressive increase in microhardness (about +23% and tensile failure strain value (about +98% without significant compromise in tensile strength, compared to the un-reinforced Mg–3Al–1Zn alloy. The synthesized composites can be used in automotive and aerospace industries due to their low density and high specific strength.

  18. Advance on Al2O3 Particulates Reinforced Aluminum Metal Matrix Composites (Al-MMCs Manufactured by the Power Metallurgy(PM Methods- Improved PM Techniques

    Directory of Open Access Journals (Sweden)

    Xu Lina

    2016-01-01

    Full Text Available Aluminum metal matrix composites (Al-MMCs with Al2O3 particulates as reinforcement fabricated by the power metallurgy (PM methods have gained much attention due to their unique characteristics of the wide range of Al2O3 particles addition, easy-operating process and effectiveness. The improved PM techniques, such as the high energy ball milling, powder extruder and high pressure torsion were applied to further strengthening the properties or/and diminishing the agglomeration of strength particles. The formation of liquid phase assisted densification of compacts to promote the sintering of composites. Complex design of Al2O3 particles with other particles was another efficient method to tailor the properties of Al-MMCs.

  19. Data on processing of Ti-25Nb-25Zr β-titanium alloys via powder metallurgy route: Methodology, microstructure and mechanical properties.

    Science.gov (United States)

    Ueda, D; Dirras, G; Hocini, A; Tingaud, D; Ameyama, K; Langlois, P; Vrel, D; Trzaska, Z

    2018-04-01

    The data presented in this article are related to the research article entitled "Cyclic Shear behavior of conventional and harmonic structure-designed Ti-25Nb-25Zr β-titanium alloy: Back-stress hardening and twinning inhibition" (Dirras et al., 2017) [1]. The datasheet describes the methods used to fabricate two β-titanium alloys having conventional microstructure and so-called harmonic structure (HS) design via a powder metallurgy route, namely the spark plasma sintering (SPS) route. The data show the as-processed unconsolidated powder microstructures as well as the post-SPS ones. The data illustrate the mechanical response under cyclic shear loading of consolidated alloy specimens. The data show how electron back scattering diffraction(EBSD) method is used to clearly identify induced deformation features in the case of the conventional alloy.

  20. Metallurgy, environmental pollution and the decline of Etruscan civilisation.

    Science.gov (United States)

    Harrison, Adrian P; Cattani, Ilenia; Turfa, Jean M

    2010-01-01

    The Etruscans were justifiably famous in antiquity for their advanced metallurgy and for the rich mineral resources of their region (including La Tolfa, the Colline Metallifere, Mont'Amiata and Elba). We offer a new perspective on certain Iron Age and Archaic (ca. 1,000-480 BC: ) Etruscan industrial and habitation sites, and on the problem of heavy metal poisoning, still being investigated today, coincidentally in some of the same areas that originally saw Etruscan mines and workshops. This study investigates ancient sources, including literature and excavation reports, in the light of modern studies of heavy metal poisoning on human beings, plant and animal life. Furthermore, it is the first to use non-invasive Niton X-ray fluorescence analysis of samples of Etruscan (strictly ethnically Faliscan) hair (c. 350 BCE: ). The findings show the strong likelihood of heavy metal poisoning in areas of Etruscan metallurgical activity with the effects of this being responsible for or contributing to the abandonment of a number of these sites around the 6th century BC: . No thoroughly satisfactory explanation of this phenomenon has previously been offered. However, findings suggest that Faliscan women, represented by sample CG 2004-6-2, were not exposed to high levels of arsenic in life, which is not perhaps surprising for an urban aristocratic woman of the mid-4th century BC: . The reasons for the abandonment of several flourishing settlements are without doubt complex, and include political and social change. We suggest heavy metal contamination as an additional stimulus to the noted phenomenon of the peaceful abandonment, at the beginning, and at the end of the 6th century BC: , of sites in southern and northern Etruria such as Marsiliana d'Albegna (late 7th c.), Lago dell'Accesa, Acquarossa and Poggio Civitate-Murlo (late 6th c.). While the historical truth of the demise of Etruscan civilisation is much more complex, an interim set of related events, the desertion of

  1. Human alveolar bone cell proliferation, expression of osteoblastic phenotype, and matrix mineralization on porous titanium produced by powder metallurgy.

    Science.gov (United States)

    Rosa, Adalberto Luiz; Crippa, Grasiele Edilaine; de Oliveira, Paulo Tambasco; Taba, Mario; Lefebvre, Louis-Philippe; Beloti, Marcio Mateus

    2009-05-01

    This study aimed at investigating the influence of the porous titanium (Ti) structure on the osteogenic cell behaviour. Porous Ti discs were fabricated by the powder metallurgy process with the pore size typically between 50 and 400 microm and a porosity of 60%. Osteogenic cells obtained from human alveolar bone were cultured until subconfluence and subcultured on dense Ti (control) and porous Ti for periods of up to 17 days. Cultures grown on porous Ti exhibited increased cell proliferation and total protein content, and lower levels of alkaline phosphatase (ALP) activity than on dense Ti. In general, gene expression of osteoblastic markers-runt-related transcription factor 2, collagen type I, alkaline phosphatase, bone morphogenetic protein-7, and osteocalcin was lower at day 7 and higher at day 17 in cultures grown on porous Ti compared with dense Ti, a finding consistent with the enhanced growth rate for such cultures. The amount of mineralized matrix was greater on porous Ti compared with the dense one. These results indicate that the porous Ti is an appropriate substrate for osteogenic cell adhesion, proliferation, and production of a mineralized matrix. Because of the three-dimensional environment it provides, porous Ti should be considered an advantageous substrate for promoting desirable implant surface-bone interactions.

  2. Making Self-Lubricating Parts By Powder Metallurgy

    Science.gov (United States)

    Sliney, Harold E.; Dellacorte, Christopher

    1990-01-01

    Compositions and parameters of powder-metallurgical fabrication processes determined for new class of low-friction, low-wear, self-lubricating materials. Used in oxidizing or reducing atmospheres in bearings and seals, at temperatures from below 25 degrees C to as high as 900 degrees C. Thick parts made with minimal waste.

  3. Uranium mining and metallurgy library science and technology literature retrieval of network

    International Nuclear Information System (INIS)

    Tang Lilei

    2014-01-01

    This paper introduces the network resources and characteristics retrieve service of Beijing research Institute of Chemical Engineering of Metallurgy library, Analyzes the problems often encountered in the literature retrieval in science and technology, And puts forward the solution, Puts forward the thinking and Suggestions of science and technology literature retrieval. (author)

  4. Solvent Extraction of Copper: An Extractive Metallurgy Exercise for Undergraduate Teaching Laboratories

    Science.gov (United States)

    Smellie, Iain A.; Forgan, Ross S.; Brodie, Claire; Gavine, Jack S.; Harris, Leanne; Houston, Daniel; Hoyland, Andrew D.; McCaughan, Rory P.; Miller, Andrew J.; Wilson, Liam; Woodhall, Fiona M.

    2016-01-01

    A multidisciplinary experiment for advanced undergraduate students has been developed in the context of extractive metallurgy. The experiment serves as a model of an important modern industrial process that combines aspects of organic/inorganic synthesis and analysis. Students are tasked to prepare a salicylaldoxime ligand and samples of the…

  5. Metallurgy department progress report for the period 1 January to 31 December 1981

    International Nuclear Information System (INIS)

    1982-07-01

    The activities of the Metallurgy Department at Risoe during 1981 are described. The work is presented in three chapters: General Materials Research, Technology and Materials Development, Fuel Elements. Furthermore, a survey is given of the department's participation in international collaboration and of its activities within education and training. A list (with abstracts) of publications and lectures by the staff during 1981 is included. (author)

  6. Metallurgy department progress report for the period 1 January to 31 December 1982

    International Nuclear Information System (INIS)

    1983-07-01

    The activities of the Metallurgy Department at Risoe during 1982 are described. The work is presented in three chapters: General Materials Research, Technology and Materials Deveopment, Fuel Elements. Furthermore, a survey is given of the department's participation in international collaboration and of its activities within education and training. A list (with abstracts) of publications and lectures by the staff during 1982 is included. (author)

  7. Powder metallurgy preparation of Al-Cu-Fe quasicrystals using mechanical alloying and Spark Plasma Sintering

    Czech Academy of Sciences Publication Activity Database

    Novák, P.; Kubatík, Tomáš František; Vystrčil, J.; Hendrych, R.; Kříž, J.; Mlynár, J.; Vojtěch, D.

    2014-01-01

    Roč. 52, September (2014), s. 131-137 ISSN 0966-9795 Institutional support: RVO:61389021 Keywords : Nanostructure intermetallics * Ternary alloys systems * Mechanical alloying and milling * Sintering * Diffraction Subject RIV: JG - Metallurgy Impact factor: 2.131, year: 2014 http://www.sciencedirect.com/science/article/pii/S0966979514001198#

  8. Recycling of wastes from uranium mining and metallurgy and recovery of useful resources in China

    International Nuclear Information System (INIS)

    Pan Yingjie; Xue Jianxin; Chen Zhongqiu

    2012-01-01

    Recycling of wastes from uranium mining and metallurgy in China and recovery of useful resources are summarized from the aspects such as recovery of uranium from mine water, reusing of waste water, decontaminating and recycling of radioactivity contaminated metal, backfill of gangues and tailings, and comprehensive recovery and utilization of associated uranium deposits. (authors)

  9. Practical application of solid phase spectrophotometry in analysis of materials and goods of mining and metallurgy

    International Nuclear Information System (INIS)

    Duan Qunzhang

    1999-01-01

    The author reviewed recent development and practical application of solid phase spectrophotometry in analysis of materials and goods of mining-metallurgy. Separation and preconcentration and conditions of coloring determination, sensitivity and range of detection, as well as interference of corresponding method are discussed

  10. Annual report of the Metallurgy Division [for the] period ending December 1977

    International Nuclear Information System (INIS)

    Elayaperumal, K.; Sridhar Rao, Ch.; Mukhopadhyay, P.; Rao, S.V.K.

    1979-01-01

    The research and development work carried out and the various programmes underway in the Metallurgy Division of the Bhabha Atomic Research Centre, Bombay, during the calendar year 1977 have been reported. The R and D work and programmes cover extraction metallurgy, physical metallurgy, alloy development, corrosion metallurgy and ceramics. Some of the major studies and programmes are: (1) development of processes for extraction of niobium, vanadium, hafnium and nickel, (2) preparation of niobium alloys, ferro-zirconium, ceramic grade zirconia, (3) electro-refining of zircaloy scrap, (4) preparation of anhydrous beryllium fluoride from Indian beryl, (5) preparation of beryllium alloys, (6) studies on phase transformation and deformation behaviour of zirconium and zirconium-oxygen alloys, (7) self-diffusion studies in dilute Zr-Fe and Zr-Cr alloys, (8) studies on corrosion and stress corrosion cracking of zirconium base alloys and (9) sintering studies on ZrO 2 -PuO 2 and BeO. (M.G.B.)

  11. Metallurgy Department progress report for the period 1 January to 31 December 1984

    International Nuclear Information System (INIS)

    1985-04-01

    The activities of the Metallurgy Department at Risoe during 1984 are described. The work is presented in three chapters: General Materials Research, Technology and Materials Development, and Fuel Elements. A survey is given of the Department's participation in international collaboration and of its activities within education and training. A list (with abstracts) of publications and lectures by the staff during 1984 is included. (author)

  12. Powder Metallurgy Preparation of Co-Based Alloys for Biomedical Applications

    Czech Academy of Sciences Publication Activity Database

    Marek, I.; Novák, P.; Mlynár, J.; Vojtěch, D.; Kubatík, Tomáš František; Málek, J.

    2015-01-01

    Roč. 128, č. 4 (2015), s. 597-601 ISSN 0587-4246. [International Symposium on Physics of Materials (ISPMA) /13./. Prague, 31.08.2014-04.09.2014] Institutional support: RVO:61389021 Keywords : powder metallurgy * mechanical properties * biomedical applications Subject RIV: JK - Corrosion ; Surface Treatment of Materials Impact factor: 0.525, year: 2015

  13. Mechanical properties of modified low cobalt powder metallurgy Udimet 700 type alloys

    Science.gov (United States)

    Harf, Fredric H.

    1989-01-01

    Eight superalloys derived from Udimet 700 were prepared by powder metallurgy, hot isostatically pressed, heat treated and their tensile and creep rupture properties determined. Several of these alloys displayed properties superior to those of Udimet 700 similarly prepared, in one case exceeding the creep rupture life tenfold. Filter clogging by extracted gamma prime, its measurement and significance are discussed in an appendix.

  14. Ice-core evidence of earliest extensive copper metallurgy in the Andes 2700 years ago.

    Science.gov (United States)

    Eichler, A; Gramlich, G; Kellerhals, T; Tobler, L; Rehren, Th; Schwikowski, M

    2017-01-31

    The importance of metallurgy for social and economic development is indisputable. Although copper (Cu) was essential for the wealth of pre- and post-colonial societies in the Andes, the onset of extensive Cu metallurgy in South America is still debated. Comprehensive archaeological findings point to first sophisticated Cu metallurgy during the Moche culture ~200-800 AD, whereas peat-bog records from southern South America suggest earliest pollution potentially from Cu smelting as far back as ~2000 BC. Here we present a 6500-years Cu emission history for the Andean Altiplano, based on ice-core records from Illimani glacier in Bolivia, providing the first complete history of large-scale Cu smelting activities in South America. We find earliest anthropogenic Cu pollution during the Early Horizon period ~700-50 BC, and attribute the onset of intensified Cu smelting in South America to the activities of the central Andean Chiripa and Chavin cultures ~2700 years ago. This study provides for the first time substantial evidence for extensive Cu metallurgy already during these early cultures.

  15. A Guide for Planning Facilities for Occupational Preparation Programs in Metallurgy Technology. Interim Report. Research 28.

    Science.gov (United States)

    German, Carl, Jr.

    The major purpose of this guide is to elicit the information necessary for writing educational specifications for facilities to house technical education programs in metallurgy. It is organized in these parts: (1) Part I discusses the major purpose, underlying assumptions, recent instructional trends, and guiding principles utilized in the…

  16. Microstructural and mechanical properties of biodegradable iron foam prepared by powder metallurgy

    Czech Academy of Sciences Publication Activity Database

    Čapek, Jaroslav; Vojtěch, D.; Oborná, A.

    2015-01-01

    Roč. 83, Oct (2015), s. 468-482 ISSN 0261-3069 R&D Projects: GA ČR GBP108/12/G043 Institutional support: RVO:68378271 Keywords : powder metallurgy * metallic foams * biodegradable iron * mechanical properties * scaffolds Subject RIV: BM - Solid Matter Physics ; Magnetism Impact factor: 3.997, year: 2015

  17. Powder metallurgy approaches to high temperature components for gas turbine engines

    Science.gov (United States)

    Probst, H. B.

    1974-01-01

    Research is reported for the tensile strength, ductility, and heat performance characterisitics of powder metallurgy (p/m) superalloys. Oxide dispersion strengthened alloys were also evaluated for their strength during thermal processing. The mechanical attributes evident in both p/m supperalloys and dispersion strengthened alloys are discussed in terms of research into their possible combination.

  18. [Concomitant influence of occupational and social risk factors on health of workers engaged into powder metallurgy].

    Science.gov (United States)

    Shur, P Z; Zaĭtseva, N V; Kostarev, V G; Lebedeva-Nesevria, N A; Shliapnikov, D M

    2012-01-01

    Results of health risk evaluation in workers engaged into powder metallurgy, using complex of hygienic, medical, epidemiologic and sociologic studies, enable to define priority occupational and social risk factors, to assess degree of their influence on the workers' health and to identify occupationally induced diseases.

  19. Prerequisites and opportunities for repositioning of the Urals metallurgy within the Industry 4.0

    Directory of Open Access Journals (Sweden)

    O. A. Romanova

    2017-12-01

    Full Text Available The authors present the modern trends in the development of metallurgy, and classify the technological structure of metallurgical industry. The article contains specific features of the development of metallurgy in the conditions of industry formation. A special role in this process plays the pace of digitalization and robotization of the industry, the development of additive technologies, Internet of things. The authors substantiate the possibility of developing the metallurgy of the Middle Urals as a science-intensive, high-tech complex that meets the requirements of Industry 4.0. This possibility interrelates with its repositioning, one of the main tasks of which is the formation of new sales markets focused on high-tech consumer industries, as well as the preservation of traditional consumption sectors under conditions of increasing competition in the construction materials market. The authors underline the importance of international cooperation in the field of environmentally safe industrial development, with applying the best available technologies and innovative development in general. The authors propose a methodological approach for assessing the repositioning of the regional metallurgical complex. This approach is the consecutive implementation of the following stages: assessment of dynamics and the forecast of development of consumer steel products sector and its structure based on identified priority areas of technological development of metallurgy in the region; construction of a factor model describing the changes in parameters of the RMC repositioning process, and approximation of the characteristics of their nonlinear elements; building a mathematical model on the basis of neural network algorithms for assessing the process of repositioning the RMC, taking into account projected values of the RMK parameters in the process of repositioning and changing the structure of consumer markets for metal products; formation of a variable

  20. Powder-metallurgy preparation of NiTi shape-memory alloy using mechanical alloying and spark-plasma sintering.

    Czech Academy of Sciences Publication Activity Database

    Novák, P.; Moravec, H.; Vojtěch, V.; Knaislová, A.; Školáková, A.; Kubatík, Tomáš František; Kopeček, Jaromír

    2017-01-01

    Roč. 51, č. 1 (2017), s. 141-144 ISSN 1580-2949 R&D Projects: GA ČR(CZ) GA14-03044S Institutional support: RVO:61389021 ; RVO:68378271 Keywords : mechanical alloying * spark plasma sintering * NiTi * shape memory alloy Subject RIV: JG - Metallurgy; JG - Metallurgy (FZU-D) OBOR OECD: Materials engineering ; Materials engineering (FZU-D) Impact factor: 0.436, year: 2016 https://www.researchgate.net/publication/313900224_Powder-metallurgy_preparation_of_NiTi_shape-memory_alloy_using_mechanical_alloying_and_spark-plasma_sintering

  1. Digital fabrication

    CERN Document Server

    2012-01-01

    The Winter 2012 (vol. 14 no. 3) issue of the Nexus Network Journal features seven original papers dedicated to the theme “Digital Fabrication”. Digital fabrication is changing architecture in fundamental ways in every phase, from concept to artifact. Projects growing out of research in digital fabrication are dependent on software that is entirely surface-oriented in its underlying mathematics. Decisions made during design, prototyping, fabrication and assembly rely on codes, scripts, parameters, operating systems and software, creating the need for teams with multidisciplinary expertise and different skills, from IT to architecture, design, material engineering, and mathematics, among others The papers grew out of a Lisbon symposium hosted by the ISCTE-Instituto Universitario de Lisboa entitled “Digital Fabrication – A State of the Art”. The issue is completed with four other research papers which address different mathematical instruments applied to architecture, including geometric tracing system...

  2. List of unclassified documents by the staff of Metallurgy Division, AERE Harwell from January 1979 to July 1980

    International Nuclear Information System (INIS)

    Smith, N.C.

    1980-12-01

    This list constitutes unclassified material published or presented between January 1979 and July 1980, by the staff of Metallurgy Division. It covers reports, memoranda, articles in periodicals, conference papers, books and patent specifications. (author)

  3. Thermal stability and creep behaviour of MgNiYCe-rich mischmetal alloys processed by a powder metallurgy route

    Czech Academy of Sciences Publication Activity Database

    Peréz, P.; Milička, Karel; Badia, J. M.; Garcés, G.; Antoranz, J. M.; Gonzáles, S.; Dobeš, Ferdinand; Adeva, P.

    289-292, - (2009), s. 127-136 ISSN 1012-0386. [DIMAT 2008, International Conference on Diffusion in Materials /7./. Lanzarote, Canary Islands, 28.10.2008-31.10.2008] Grant - others:Ministerio de Ciencia y Tecnologia (ES) MAT2006-11731-C02 Institutional research plan: CEZ:AV0Z20410507 Keywords : magnesium alloys * powder metallurgy * microstructure * thermal stability * creep Subject RIV: JG - Metallurgy

  4. Thermogravimetric control of intermediate compounds in uranium metallurgy; Control termogravimetrico de productos intermedios de la metalurgia del uranio

    Energy Technology Data Exchange (ETDEWEB)

    Gasco Sanchez, L.; Fernandez Cellini, R.

    1959-07-01

    The thermal decomposition of some intermediate compounds in the metallurgy of the uranium as uranium peroxide, ammonium uranate, uranium and ammonium penta-fluoride, uranium tetrafluoride and uranous oxide has been study by means of the Chevenard's thermo balance. Some data on pyrolysis of synthetic mixtures of intermediate compounds which may occasionally appear during the industrial process, are given. Thermogravimetric methods of control are suggested, usable in interesting products in the uranium metallurgy. (Author) 20 refs.

  5. Hydrothermal metallurgy for recycling of slag and glass

    International Nuclear Information System (INIS)

    Tanaka, Toshihiro; Yoshikawa, Takeshi; Hirai, Nobumitsu; Katsuyama, Shigeru

    2009-01-01

    The authors have applied hydrothermal reactions to develop recycling processing of slag or glass. As an example, under hydrothermal conditions such as 200 300 deg. C and 30 40MPa with H 2 O, powders made of glass can be sintered to become solidified glass materials containing about 10mass% H 2 O. When the glass containing H 2 O is heated again under normal pressure, the glass expands releasing H 2 O to make porous microstructure. H 2 O starts to emit just above the glass transition temperature. Therefore, when we have a glass with low glass transition temperature, we can make low temperature foaming glass. The SiO 2 -Na 2 O-B 2 O 3 glass is a candidate to be such a foaming glass. In this paper, we describe our recent trial on the fabrication of the low temperature foaming glass by using hydrothermal reaction.

  6. Powder metallurgy processing of high strength turbine disk alloys

    Science.gov (United States)

    Evans, D. J.

    1976-01-01

    Using vacuum-atomized AF2-1DA and Mar-M432 powders, full-scale gas turbine engine disks were fabricated by hot isostatically pressing (HIP) billets which were then isothermally forged using the Pratt & Whitney Aircraft GATORIZING forging process. While a sound forging was produced in the AF2-1DA, a container leak had occurred in the Mar-M432 billet during HIP. This resulted in billet cracking during forging. In-process control procedures were developed to identify such leaks. The AF2-1DA forging was heat treated and metallographic and mechanical property evaluation was performed. Mechanical properties exceeded those of Astroloy, one of the highest temperature capability turbine disk alloys presently used.

  7. Structural and electrical properties of copper-nickel-aluminum alloys obtained by conventional powder metallurgy method

    Energy Technology Data Exchange (ETDEWEB)

    Monteiro, Waldemar A.; Carrio, Juan A.G.; Silveira, C.R. da; Pertile, H.K.S., E-mail: fisica.cch@mackenzie.br [Universidade Presbiteriana Mackenzie (UPM/CCH), Sao Paulo, SP (Brazil). Centro de Ciencias e Humanidades. Dept. de Fisica; Silva, L.C.E. da; Buso, S.J., E-mail: jgcarrio@mackenzie.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2009-07-01

    This work looked for to search out systematically, in scale of laboratory, copper-nickel-aluminum alloys (Cu-Ni-Al) with conventional powder metallurgy processing, in view of the maintenance of the electric and mechanical properties with the intention of getting electric connectors of high performance or high mechanical damping. After cold uniaxial pressing (1000 kPa), sintering (780 deg C) and convenient homogenization treatments (500 deg C for different times) under vacuum (powder metallurgy), the obtained Cu-Ni-Al alloys were characterized by optical microscopy, electrical conductivity, Vickers hardness. X rays powder diffraction data were collected for the sintered samples in order to a structural and microstructural analysis. The comparative analysis is based on the sintered density, hardness, macrostructures and microstructures of the samples. (author)

  8. Structural and electrical properties of copper-nickel-aluminum alloys obtained by conventional powder metallurgy method

    International Nuclear Information System (INIS)

    Monteiro, Waldemar A.; Carrio, Juan A.G.; Silveira, C.R. da; Pertile, H.K.S.

    2009-01-01

    This work looked for to search out systematically, in scale of laboratory, copper-nickel-aluminum alloys (Cu-Ni-Al) with conventional powder metallurgy processing, in view of the maintenance of the electric and mechanical properties with the intention of getting electric connectors of high performance or high mechanical damping. After cold uniaxial pressing (1000 kPa), sintering (780 deg C) and convenient homogenization treatments (500 deg C for different times) under vacuum (powder metallurgy), the obtained Cu-Ni-Al alloys were characterized by optical microscopy, electrical conductivity, Vickers hardness. X rays powder diffraction data were collected for the sintered samples in order to a structural and microstructural analysis. The comparative analysis is based on the sintered density, hardness, macrostructures and microstructures of the samples. (author)

  9. Quantifying the properties of low-cost powder metallurgy titanium alloys

    International Nuclear Information System (INIS)

    Bolzoni, L.; Ruiz-Navas, E.M.; Gordo, E.

    2017-01-01

    The extensive industrial employment of titanium is hindered by its high production costs where reduction of these costs can be achieved using cheap alloying elements and appropriate alternative processing techniques. In this work the feasibility of the production of low-cost titanium alloys is addressed by adding steel to pure titanium and processing the alloys by powder metallurgy. In particular, a spherical 4140 LCH steel powder commonly used in metal injection moulding is blended with irregular hydride-dehydride Ti. The new low-cost alloys are cold uniaxially pressed and sintered under high vacuum and show comparable properties to other wrought-equivalent and powder metallurgy titanium alloys. Differential thermal analysis and X-ray diffraction analyses confirm that Ti can tolerate the employment of iron as primary alloying element without forming detrimental TiFe-based intermetallic phases. Thus, the newly designed α+β alloys could be used for cheaper non-critical components.

  10. Preparation of Three-Dimensional Graphene Foams Using Powder Metallurgy Templates.

    Science.gov (United States)

    Sha, Junwei; Gao, Caitian; Lee, Seoung-Ki; Li, Yilun; Zhao, Naiqin; Tour, James M

    2016-01-26

    A simple and scalable method which combines traditional powder metallurgy and chemical vapor deposition is developed for the synthesis of mesoporous free-standing 3D graphene foams. The powder metallurgy templates for 3D graphene foams (PMT-GFs) consist of particle-like carbon shells which are connected by multilayered graphene that shows high specific surface area (1080 m(2) g(-1)), good crystallization, good electrical conductivity (13.8 S cm(-1)), and a mechanically robust structure. The PMT-GFs did not break under direct flushing with DI water, and they were able to recover after being compressed. These properties indicate promising applications of PMT-GFs for fields requiring 3D carbon frameworks such as in energy-based electrodes and mechanical dampening.

  11. [Investigation about prevention behavior for dust workers in machinery, ceramic, and metallurgy industry].

    Science.gov (United States)

    Shen, Fu-hai; Ma, Qing-kun; Xiao, Shu-yu; Cui, Feng-tao; Meng, Qing-di; Yang, Xiu-qing; Qi, Hui-sheng; Fan, Xue-yun; Yao, San-qiao

    2011-01-01

    The purposes of this thesis were to study the behavior about workers exposed to dust and provide scientific basis for health promotion. We designed a questionnaire and carry it on the 746 dust workers in the 3 representative corporations of Machinery, Ceramic, and Metallurgy Industry. All data were input into computer. And a database was established with Excel. SPSS11.5 statistical analysis software was used to analyze the influence on protecting behavioral between the application of qualifications, different jobs, training or protection, and other aspects etc. The rates were 94.4% and 75.3% about the regular physical examination and requirements for protective equipment. The rate of choosing an effective way of protection was generally low (15.4%). There was significant difference for among different educational background workers (P Metallurgy Industry. Those who were not educated had a lower using rate about the protection behavior, regular physical examination, and requirements for protective equipment than those educated.

  12. [Risk and features of occupational diseases in nonferrous metallurgy workers of Kolsky Transpolar area].

    Science.gov (United States)

    Siurin, S A; Chashchin, V P; Frolova, N M

    2015-01-01

    The study covered data on 977 cases of occupational diseases in 615 workers of nonferrous metallurgy in Kolsky Transpolar area. Findings are high risk of occupational diseases in workers engaged into electrolysis production of aluminium, all nickel reprocessing and pyrometallic copper reprocessing (GR 7.02-10.0). Electrolysis operators and anode operators of aluminium production are more prone to occupational diseases, with bone and muscular disorders (46.8%) prevalent in the morbidity structure. Respiratory diseases are more prevalent (68.2-100%) in the occupational morbidity structure of copper-nickelindustry workers. Conclusion is made on mandatory improvement of the work conditions and more effective individual protective means against occupational hazards in workers of nonferrous metallurgy in Kolsky Transpolar area.

  13. Estimation and characterization of polycyclic aromatic hydrocarbons from magnesium metallurgy facilities in China.

    Science.gov (United States)

    Nie, Zhiqiang; Yang, Yufei; Tang, Zhenwu; Liu, Feng; Wang, Qi; Huang, Qifei

    2014-11-01

    Field monitoring was conducted to develop a polycyclic aromatic hydrocarbon (PAH) emission inventory for the magnesium (Mg) metallurgy industry in China. PAH emissions in stack gas and fly/bottom ash samples from different smelting units of a typical Mg smelter were measured and compared. Large variations of concentrations, congener patterns, and emission factors of PAHs during the oxidation and reduction stages in the Mg smelter were observed. The measured average emission factor (166,487 μg/t Mg) was significantly higher than those of other industrial sources. Annual emission from Mg metallurgy in 2012 in China was estimated at 116 kg (514 g BaPeq) for PAHs. The results of this study suggest that PAH emission from Mg industries should be considered by local government agencies. These data may be helpful for understanding PAH levels produced by the Mg industry and in developing a PAH inventory.

  14. Metallurgy Department. Progress Report for the Period 1 January to 31 December 1984

    DEFF Research Database (Denmark)

    Risø National Laboratory, Roskilde

    The activities of the Metallurgy Department at Risø during 1984 are described. The work is presented in three chapters: General Materials Research, Technology and Materials Development, and Fuel Elements. A survey is given of the Department's participation in international collaboration and of its...... activities within education and training. A list (with abstracts) of publications and lectures by the staff during 1984 is included....

  15. Metallurgy Department progress report for the period 1 January to 31 December 1986

    International Nuclear Information System (INIS)

    Schroeder Pedersen, A.; Bilde-Soerensen, J.B.

    1987-04-01

    The activities of the Metallurgy Department at Risoe during 1986 are described. The work is presented in four chapters: General Materials Research, Technology and Materials Development, Chemical and Electrochemical Energy Research and Development, and Fuel Elements. A survey is given of the Department's participation in international collaboration and of its activities within education and training. A list (with abstracts) of publications and lectures by the staff during 1986 is included. (editors)

  16. Characterization of Powder Metallurgy Processed Pure Magnesium Materials for Biomedical Applications

    Czech Academy of Sciences Publication Activity Database

    Březina, M.; Minda, J.; Doležal, P.; Krystýnová, M.; Fintová, Stanislava; Zapletal, J.; Wasserbauer, J.; Ptáček, P.

    2017-01-01

    Roč. 7, č. 11 (2017), č. článku 461. ISSN 2075-4701 Institutional support: RVO:68081723 Keywords : magnesium * powder metallurgy * cold pressing * hot pressing * EIS (Electrochemical impedance spectroscopy) * three-point bending test * corrosion Subject RIV: JK - Corrosion ; Surface Treatment of Materials OBOR OECD: Coating and films Impact factor: 1.984, year: 2016 http://www.mdpi.com/2075-4701/7/11/461

  17. Metallurgy department progress report for the period 1 January to 31 December 1977

    International Nuclear Information System (INIS)

    1978-03-01

    The activities of the Metallurgy Department at Risoe during 1977 are described. The work is presented in four chapters: General Materials Research, Technology and Materials Development, Fuel elements, and Non-Destructive Testing. Furthermore, a survey is given of the department's participation in international collaboration and of its activities within education and training. A list (with abstracts) of publications and lectures by the staff during 1977 is included. (author)

  18. Metallurgy Department progress report for the period 1 January to 31 December 1985

    International Nuclear Information System (INIS)

    Schroeder Pedersen, A.; Bilde Soerensen, J.B.

    1986-04-01

    The activities of the Metallurgy department at Risoe during 1985 are described. The work is presented in four chapters: General Materials Research, Technology and Materials Development, Chemical and Electrochemical Energy Research and Development, and Fuel elements. A survey is given of the Department's participation in international collaboration and of its activities within education and training. A list (with abstracts) of publications and lectures by the staff during 1985 is included. (author)

  19. Production of titanium alloys for advanced aerospace systems by powder metallurgy

    OpenAIRE

    Henriques, Vinicius André Rodrigues; Campos, Pedro Paulo de; Cairo, Carlos Alberto Alves; Bressiani, José Carlos

    2005-01-01

    Titanium alloys parts are ideally suited for advanced aerospace systems because of their unique combination of high specific strength at both room temperature and moderately elevated temperature, in addition to excellent corrosion resistance. Despite these features, use of titanium alloys in engines and airframes is limited by cost. The alloys processing by powder metallurgy eases the obtainment of parts with complex geometry. In this work, results of the Ti-6Al-4V and Ti-13Nb-13Zr alloys pro...

  20. Production of a low young modulus titanium alloy by powder metallurgy

    OpenAIRE

    Santos,Dalcy Roberto dos; Henriques,Vinicius André Rodrigues; Cairo,Carlos Alberto Alves; Pereira,Marcelo dos Santos

    2005-01-01

    Titanium alloys have several advantages over ferrous and non-ferrous metallic materials, such as high strengthto-weight ratio and excellent corrosion resistance. A blended elemental titanium powder metallurgy process has been developed to offer low cost commercial products. The process employs hydride-dehydride (HDH) powders as raw material. In this work, results of the Ti-35Nb alloy sintering are presented. This alloy due to its lower modulus of elasticity and high biocompatibility is a prom...

  1. A Comparison of the Plastic Flow Response of a Powder Metallurgy Nickel Base Superalloy (Postprint)

    Science.gov (United States)

    2017-04-01

    Materials The nickel-base, powder-metallurgy (PM) cc¢ super- alloy LSHR was used to establish the effect of test method on plastic -flow response under hot...of friction was estimated to lead to maximum errors in flow stress of the order of 3 pct for the sample geometry and height reduction used in the... plastic -flow behavior of LSHR (in effective stress-strain terms) was described using a phenomeno- logical relationship typical of those for

  2. Metallurgy department progress report for the period 1 January to 31 December 1980

    International Nuclear Information System (INIS)

    1981-07-01

    The activities of the Metallurgy Department at Risoe during 1980 are described. The work is presented in four chapters: General Materials Research, Technology and Materials Development, Fuel Elements, Non-Destructive Testing. Furthermore, a survey is given of the department's participation in international collaboration and of its activities within education and training. A list (with abstracts) of publications and lectures by the staff during 1980 is included. (Author)

  3. Review of some past and present powder metallurgy programs at the Los Alamos Scientific Laboratory

    International Nuclear Information System (INIS)

    Sheinberg, H.

    1977-01-01

    Powder metallurgy programs at LASL are reviewed. Topics covered include: KIWI reactor fuel elements; Phoebus reactor fuel elements, criticality control and poison plate material, structural composites for fuel element supports, and heat shields for fuel element supports; thermionic emitter reactor uranium carbide--zirconium carbide fuel pins, and molybdenum--uranium oxide fuel pins; laser and electron beam fusion targets; and current work in MHD components

  4. Situation of radioactive wastes and their prevention and treatment measures in China's uranium mining and metallurgy

    International Nuclear Information System (INIS)

    Li Renjie.

    1988-01-01

    The sorts of radioactive wastes produced in uranium mining and metallurgy and their hazards are discribed in this paper. The characteristics of the radioactive wastes are discussed. The measurements and results are introduced for treatment and disposal of the radioactive wastes. The way to deal with prevention and treatment of radioactive wastes is presented in the stages of engineering design, construction, production and decommission of uranium mines and plants

  5. Extractive metallurgy of the beryllium; Fundamentos da metalurgia extrativa do berilio

    Energy Technology Data Exchange (ETDEWEB)

    Alonso, Neusa; Capocchi, Jose Deodoro Trani [Sao Paulo Univ., SP (Brazil). Escola Politecnica

    1995-07-01

    A bibliographic review is performed on the beryllium extractive metallurgy. The work describes the main type of ores and processes applied to the metallic beryllium production, beryllium oxide production using fluoride, sulfide and direct chlorination. The thermodynamic consideration are made on beryllium reduction processes, discussing the viability of the beryllium oxide and hallide reduction processes. Under the technological viewpoint, the Cu-Be alloys main production processes are discussed, and the main toxicity problems related with beryllium are mentioned 15 refs..

  6. Metallurgy department progress report for the period 1 January to 31 December 1978

    International Nuclear Information System (INIS)

    1979-04-01

    The activities of the metallurgy department at Risoe during 1978 are described. The work is presented in four chapters: General materials research, technology and materials development, fuel elements, and non-destructive testing. Furthermore, a survey is given of the depratment's participation in international collaboration and of its activities within education and training. A list (with abstracts) of publications and lectures by the staff during 1978 is included. (author)

  7. Metallurgy department progress report for the period 1 January to 31 December 1983

    International Nuclear Information System (INIS)

    1984-06-01

    The activities of the Metallurgy Department at Risoe during 1983 are described. The work is presented in three chapters: General Materials Research, Technology and Materials Development, and Fuel Elements. Furthermore, a survey is given of the Department's participation in international collaboration and of its activities within education and training. A list (with abstracts) of publications and lectures by the staff during 1983 is included. (author)

  8. Effect of repressing on the mechanical properties of the valve guides manufactured by powder metallurgy

    Directory of Open Access Journals (Sweden)

    Andrés Rodríguez-Spitia

    2017-03-01

    Full Text Available Characterization of hardness, mass loss, and friction coefficient, was carried out on valve guides for internal combustion engines, manufactured by powder metallurgy, with the aim of finding out if they fulfill the requirements of an internal combustion engine and to be mass produced. Currently available brass casting valve guides were used as comparative parameter. It was analyzed whether properties were present in a homogeneous way in the piece lengthwise; the additional repressing process carried out in the production line with respect to the sintered guides was evaluated. Therefore, Brinell, Vickers and dry slip pin-on-disk tests were done in order to determine the friction coefficient and the wear rate. Scanning electron microscopy SEM and the metallographic analysis were used to study the wear mechanism, chemical composition of the guides, and the effect of repressing -quantifying the porosity. It was clear that these pieces manufactured by powder metallurgy process showed lower values in their mechanical-tribological properties compared to commercially available valve guides taken as reference. With these results, the company which manufactures the guides by powder metallurgy will make some adjustments suggested for the parameters at the guide’s production line.

  9. Manufacture of good-weldable low oxygen molybdenum by powder metallurgy

    International Nuclear Information System (INIS)

    Hiraoka, Yutaka; Okada, Masatoshi; Akiyama, Takashi; Yamafuchi, Yasuo.

    1984-01-01

    In general most of commercial molybdenum is produced by the powder metallurgy method and is utilized as a superior heat-resisting material in many fields. Moreover, molybdenum is expected to be used as the first-wall components of JT-60 (JAERI Tokamak-60). However, one of major problems on molybdenum, particularly on powder metallurgy molybdenum, is that any sound welded joint is hard to be obtainable. In many cases weld pores are formed on welding and, therefore, ductility of the welded joint is severely degraded. The object of the present work is to get a sound welded joint without any weld pores by reducing impurity levels in the material. The materials were produced by modifying one or several parts in the ordinary manufacturing process of powder metallurgy molybdenum. Oxygen, nitrogen, carbon and other principal metallic impurities were chemically analysed. The above materials were then subjected to electron-beam-welding by using a melt-run technique, and the soundness of the welded joints was examined by optical microscopy. (author)

  10. Properties of WZ21 (%wt) alloy processed by a powder metallurgy route.

    Science.gov (United States)

    Cabeza, Sandra; Garcés, Gerardo; Pérez, Pablo; Adeva, Paloma

    2015-06-01

    Microstructure, mechanical properties and corrosion behaviour of WZ21 (%wt) alloy prepared by a powder metallurgy route from rapidly solidified powders have been studied. Results were compared to those of the same alloy prepared through a conventional route of casting and extrusion. The microstructure of the extruded ingot consisted of α-Mg grains and Mg3Zn3Y2 (W-phase) and LPSO-phase particles located at grain boundaries. Moreover, stacking faults were also observed within α-Mg grains. The alloy processed by the powder metallurgy route exhibited a more homogeneous and finer microstructure, with a grain size of 2 μm. In this case W-phase and Mg24Y5 phase were identified, but not the LPSO-phase. The microstructural refinement induced by the use of rapidly solidified powders strengthened the alloy at room temperature and promoted superplasticity at higher strain rates. Corrosion behaviour in PBS medium evidenced certain physical barrier effect of the almost continuous arrangements of second phases aligned along the extrusion direction in conventionally processed WZ21 alloy, with a stable tendency around 7 mm/year. On the other hand, powder metallurgy processing promoted significant pitting corrosion, inducing accelerated corrosion rate during prolonged immersion times. Copyright © 2015 Elsevier Ltd. All rights reserved.

  11. A millennium of metallurgy recorded by lake sediments from Morococha, Peruvian Andes.

    Science.gov (United States)

    Cooke, Colin A; Abbott, Mark B; Wolfe, Alexander P; Kittleson, John L

    2007-05-15

    To date, information concerning pre-Colonial metallurgy in South America has largely been limited to the archaeological record of artifacts. Here, we reconstruct a millennium of smelting activity in the Peruvian Andes using the lake-sediment stratigraphy of atmospherically derived metals (Pb, Zn, Cu, Ag, Sb, Bi, and Ti) and lead isotopic ratios (206Pb/ 207Pb) associated with smelting from the Morococha mining region in the central Peruvian Andes. The earliest evidence for metallurgy occurs ca. 1000 A.D., coinciding with the fall of the Wari Empire and decentralization of local populations. Smelting during this interval appears to have been aimed at copper and copper alloys, because of large increases in Zn and Cu relative to Pb. A subsequent switch to silver metallurgy under Inca control (ca. 1450 to conquest, 1533 A.D.) is indicated by increases in Pb, Sb, and Bi, a conclusion supported by further increases of these metals during Colonial mining, which targeted silver extraction. Rapid development of the central Andes during the 20th century raised metal burdens by an order of magnitude above previous levels. Our results represent the first evidence for pre-Colonial smelting in the central Peruvian Andes, and corroborate the sensitivity of lake sediments to pre-Colonial metallurgical activity suggested by earlier findings from Bolivia.

  12. Lateral and axial cutting efficiency of instruments manufactured with conventional nickel-titanium and novel gold metallurgy.

    Science.gov (United States)

    Vasconcelos, R A; Arias, A; Peters, O A

    2017-07-26

    To isolate the effect of metallurgy in lateral and axial cutting efficacy against plastic and bovine dentine substrates by comparing two rotary systems with identical design but manufactured with either conventional nickel-titanium or heat-treated gold alloy. A total of 258 ProTaper Universal (PTU) and ProTaper Gold (PTG) Shaping instruments were used. Bending behaviour was assessed to determine the appropriate displacement associated with a 2 N force in lateral cutting. Ten instruments of each type were used in lateral action for 60 s against bovine dentine or plastic substrates four consecutive times producing four notches in each specimen. Ten further instruments of each type were used in on axial action in four standardized simulated root canals fabricated from 4-mm thick plastic or dentine discs. Both tests were performed at 300 rpm in a computer-controlled testing platform. Notch area and torsional load were compared with Student's t-tests. Repeated measures ANOVA was used to compare cutting efficiency across the four different time-points. Pearson correlation coefficients between substrates were also determined. For lateral action, all three PTG instruments cut significantly more effectively (P < 0.05) than PTU on the plastic substrate. S1 and S2 PTG cut significantly more after 120 and 180 s (P < 0.05) on bovine dentine substrate. For axial action, S1 and S2 PTG were significantly more efficient in cutting at 180 s on plastic and 120 s on bovine dentine (P < 0.05). Instruments made from heat-treated nickel-titanium gold alloy had equal or greater cutting efficiency when compared to those made from conventional nickel-titanium. © 2017 International Endodontic Journal. Published by John Wiley & Sons Ltd.

  13. Quarterly Progress Report Metallurgy Development Operation: January - March 1964

    Energy Technology Data Exchange (ETDEWEB)

    Wick, O. J. [Hanford Site (HNF), Richland, WA (United States). Metallurgy Development Operation; Last, G. A. [Hanford Site (HNF), Richland, WA (United States). Metallurgy Development Operation. Fuels Design; Minor, J. E. [Hanford Site (HNF), Richland, WA (United States). Metallurgy Development Operation. Metal Fabrication Development; Nelson, T. C. [Hanford Site (HNF), Richland, WA (United States). Metallurgy Development Operation. Plutonium Product Development; Stewart, R. W. [Hanford Site (HNF), Richland, WA (United States). Metallurgy Development Operation. Plutonium Metallurgy Development

    1964-05-20

    This progress report focuses on two topics: Metallic Fuels Technology and Metallic Fuel Development. Within Metallic Fuels Technology, the following subtopics are covered: new fuels design, fabrication development, and fuel evaluation. The addition of recently obtained swelling data on tubular fuel elements to the previously accumulated information has prompted a refinement to the swelling model. Analysis of data for the N-outer tube, the N-inner tube and the K-single tube geometries has led to separate empirical expressions for each of the three shapes in place of the single expression formerly used for all geometries. Within Metallic Fuel Development, the irradiation of thorium fuel continued. Three tubular elements containing 2.35 wt% U235 and 1 wt% Zr have reached an exposure of 5200 Mwd/ton in the ETR P-7 facility. Weight measurements indicate that the elements have undergone 0.8% volume increase. This figure is very close to the theoretical minimum volume expansion expected from fission product production.

  14. Microstructures and Properties of 40Cu/Ag(Invar) Composites Fabricated by Powder Metallurgy and Subsequent Thermo-Mechanical Treatment

    Science.gov (United States)

    Zhang, Xin; Huang, Yingqiu; Liu, Xiangyu; Yang, Lei; Shi, Changdong; Wu, Yucheng; Tang, Wenming

    2018-03-01

    Composites of 40Cu/Ag(Invar) were prepared via pressureless sintering and subsequent thermo-mechanical treatment from raw materials of electroless Ag-plated Invar alloy powder and electrolytic Cu powder. Microstructures and properties of the prepared composites were studied to evaluate the effect of the Ag layer on blocking Cu/Invar interfacial diffusion in the composites. The electroless-plated Ag layer was dense, uniform, continuous, and bonded tightly with the Invar alloy substrate. During sintering of the composites, the Ag layer effectively prevented Cu/Invar interfacial diffusion. During cold-rolling, the Ag layer was deformed uniformly with the Invar alloy particles. The composites exhibited bi-continuous network structure and considerably improved properties. After sintering at 775 °C and subsequent thermo-mechanical treatment, the 40Cu/Ag(Invar) composites showed satisfactory comprehensive properties: relative density of 99.0 pct, hardness of HV 253, thermal conductivity of 55.7 W/(m K), and coefficient of thermal expansion of 11.2 × 10-6/K.

  15. On possibility of fabrication of monolith composite materials on niobium carbide base

    International Nuclear Information System (INIS)

    Ploshkin, V.V.; Ul'yanina, I.Yu.; Filonenko, V.P.

    1984-01-01

    An attempt was made to fabricate the composite material on niobium carbide base possessing the elevated heat resistance, erosion and chemical resistance in special media, as well as capable of withstanding sufficient thermal shocks. Powder of niobium carbide of 10 μm fraction was used as base material, the powder of pure copper of 10...12 μm fraction - as binder. It was shown that samples of composite mateiral on niobium carbide base fabricated by the method of hydrostatic pressing possessed the minimal porosity as compared to samples fabricated by usual methods of powder metallurgy. The basic phases of composite material-copper and niobium carbide - distribute uniformly over sample cross-section and don't interact with each other under any conditions. The fabricated composite material possesses sufficient thermal shock resistance and isn't subjected to brittle fracture

  16. Fabrication of cermet fuel for fast reactor

    International Nuclear Information System (INIS)

    Mishra, Sudhir; Kumar, Arun; Kutty, T.R.G.; Kamath, H.S.

    2011-01-01

    Mixed oxide (MOX) (U,Pu)O 2 , and metallic (U,Pu ,Zr) fuels are considered promising fuels for the fast reactor. The fuel cycle of MOX is well established. The advantages of the oxide fuel are its easy fabricability, good performance in the reactor and a well established reprocessing technology. However the problems lie in low thermal conductivity , low density of the fuel leading to low breeding ratio and consequently longer doubling time. The metallic fuel has the advantages of high thermal conductivity, higher metal density and higher coefficient of linear expansion. The higher coefficient of linear expansion is good from the safety consideration (negative reactivity factor). Because of higher metal density it offers highest breeding ratio and shortest doubling time. Metallic fuel disadvantages comprise large swelling at high burnup, fuel cladding interaction and lower margin between operating and melting temperature. The optimal solution may lie in cermet fuel (U, PuO 2 ), where PuO 2 is dispersed in U metal matrix and combines the favorable features of both the fuel types. The advantages of this fuel include high thermal conductivity, larger margin between melting and operating temperature, ability to retain fission product etc. The matrix being of high density metal the advantage of high breeding ratio is also maintained. In this report some results of fabrication of cermet pellet comprising of UO 2 /PuO 2 dispersed in U metal powder through classical powder metallurgy route and characterization are presented. (author)

  17. Functional dependency between the logistics security system and the MySAP ERP in metallurgy

    Directory of Open Access Journals (Sweden)

    P. Ranitović

    2013-10-01

    Full Text Available MySAP ERP - Enterprise Resource Planning (system - solution which provides a whole set of functions for the business analytics, finance, human resources management, logistics and corporate services has developed from SAP R/3. It is one of the main products of the SAP AG German multinational company and as such, it is a very important element of the international industrial and technological security system. By defining the functional dependency between the security systems (logistics security systems and the IT (My SAP ERP systems in metallurgy, a concept for designing MY SAP ERP system in metallurgic industry is defined, based on the security aspects.

  18. Physical metallurgy: Scientific school of the Academician V.M. Schastlivtsev

    Science.gov (United States)

    Tabatchikova, T. I.

    2016-04-01

    This paper is to honor Academician Vadim Mikhailovich Schastlivtsev, a prominent scientist in the field of metal physics and materials science. The article comprises an analysis of the topical issues of the physical metallurgy of the early 21st century and of the contribution of V.M. Schastlivtsev and of his school to the science of phase and structural transformations in steels. In 2015, Vadim Mikhailovich celebrates his 80th birthday, and this paper is timed to this honorable date. The list of his main publications is given in it.

  19. Metallurgy of mercury in Almaden: from aludel furnaces until Pacific furnaces

    International Nuclear Information System (INIS)

    Tejero-Manzanares, J.; Garrido Saenz, I.; Mata Cabrera, F.; Rubio Mesas, M. L.

    2014-01-01

    This paper shows the different types of furnaces for roasting cinnabar, used in the metallurgy of quicksilver over the centuries of exploitation of the Almaden Mines (Spain). Some of these techniques are part of our industrial heritage. They have contributed to name UNESCO World Heritage Site the vast technological legacy of these mines recently. This research contributes to close the long way of metallurgical activity from aludel furnaces until Pacif furnaces, first and lasted technology to produce on an industrial scale. It is delved into the most relevant aspects having to do with the type, evolution and number of furnaces existing on each of the periods. (Author)

  20. Proceedings of the III International Congress of Mining and Metallurgy MINEMETAL 2016

    International Nuclear Information System (INIS)

    2016-10-01

    The III International Congress of Mining and Metallurgy was inaugurated at the Plaza América Convention Center in Varadero. Professionals from 16 countries come together to promote scientific exchange for sustainable mining and to make concrete future investments to boost the development of this important sector in Cuba. Among the topics that will occupy the agenda of these days of congress stand out the development of geology, new technological processes, advances in the application of zeolite, sustainable development and care of the environment.

  1. Metallurgy department progress report for the period 1 January to 31 December 1979

    International Nuclear Information System (INIS)

    1980-07-01

    The activities of the Metallurgy Department at Risoe during 1979 are described. The work is presented in four chapters: General material research, technology and materials development, fuel elements, non-destructive testing. An article on wingblades of glass fibre reinforced polyester for a 630 kW windturbine is also included. Furthermore, a survey is given of the department's participation in international collaboration and of its activities within education and training. A list (with abstracts) of publications and lectures by the staff during 1979 is included. (author)

  2. Accelerated Near-Threshold Fatigue Crack Growth Behavior of an Aluminum Powder Metallurgy Alloy

    Science.gov (United States)

    Piascik, Robert S.; Newman, John A.

    2002-01-01

    Fatigue crack growth (FCG) research conducted in the near threshold regime has identified a room temperature creep crack growth damage mechanism for a fine grain powder metallurgy (PM) aluminum alloy (8009). At very low DK, an abrupt acceleration in room temperature FCG rate occurs at high stress ratio (R = Kmin/Kmax). The near threshold accelerated FCG rates are exacerbated by increased levels of Kmax (Kmax less than 0.4 KIC). Detailed fractographic analysis correlates accelerated FCG with the formation of crack-tip process zone micro-void damage. Experimental results show that the near threshold and Kmax influenced accelerated crack growth is time and temperature dependent.

  3. The synthesis and characterization of Mg-Zn-Ca alloy by powder metallurgy process

    Energy Technology Data Exchange (ETDEWEB)

    Annur, Dhyah; Franciska, P.L.; Erryani, Aprilia; Amal, M. Ikhlasul; Kartika, Ika, E-mail: pepeng2000@yahoo.com [Research center for Metallurgy and Material, Indonesian Institute of Science (Indonesia); Sitorus, Lyandra S. [Sultan Ageng Tirtayasa University (Indonesia)

    2016-04-19

    Known for its biodegradation and biocompatible properties, magnesium alloys have gained many interests to be researched as implant material. In this study, Mg-3Zn-1Ca, Mg-29Zn-1Ca, and Mg-53Zn-4.3Ca (in wt%) were synthesized by means of powder metallurgy method. The compression strength and corrosion resistance of magnesium alloy were thoroughly examined. The microstructures of the alloy were characterized using optical microscopy, Scanning Electron Microscope, and also X-ray diffraction analysis. The corrosion resistance were evaluated using electrochemical analysis. The result indicated that Mg- Zn- Ca alloy could be synthesized using powder metallurgy method. This study showed that Mg-29Zn-1Ca would make the highest mechanical strength up to 159.81 MPa. Strengthening mechanism can be explained by precipitation hardening and grain refinement mechanism. Phase analysis had shown the formation of α Mg, MgO, and intermetallic phases: Mg2Zn11 and also Ca2Mg6Zn3. However, when the composition of Zn reach 53% weight, the mechanical strength will be decreasing. In addition, all of Mg-Zn-Ca alloy studied here had better corrosion resistance (Ecorr around -1.4 VSCE) than previous study of Mg. This study indicated that Mg- 29Zn- 1Ca alloy can be further analyzed to be a biodegradable implant material.

  4. Microstructural and electrical investigation of Cu-Ni-Cr alloys obtained by powder metallurgy method

    Energy Technology Data Exchange (ETDEWEB)

    Carrio, Juan A.G.; Carvalhal, M.A.; Ayabe, L.M.; Monteiro, W.A., E-mail: jgcarrio@mackenzie.br [Universidade Presbiteriana Mackenzie (UPM/CCH), Sao Paulo, SP (Brazil). Centro de Ciencias e Humanidades. Dept. de Fisica; Silva, L.C.E. da; Silva Junior, R.V., E-mail: fisica.cch@mackenzie.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2009-07-01

    The aim of this work, using the powder metallurgy process, is to synthesize metallic alloys with high mechanical strength and high electric conductivity, after melting optimizing and thermal treatments. The Cu-Ni-Cr (wt%) alloys are characterized in their mechanical and electrical properties as well as the obtained microstructure. Through the process of powder metallurgy, contacts and structural parts can be obtained. The alloys elements are added to copper with the intention to improve their strength, ductility and thermal stability, without causing considerable damages in their form, electrical and thermal conductivity, and corrosion resistance. The metallic powders were mixed for a suitable time and then they were pressed in a cold uniaxial pressing (1000 kPa). Afterwards, the specimens were sintered in temperatures varying from 700 up to 800 deg C under vacuum. At last, the samples were homogenized at 550 deg C under vacuum, for special times. The comparative analysis is based on the sintered density, densification parameter, hardness, macrostructures and microstructures of the samples. The alloys were characterized by optical microscopy, X-rays powder diffraction, electrical conductivity and Vickers hardness. (author)

  5. Summary of NRC LWR safety research programs on fuel behavior, metallurgy/materials and operational safety

    International Nuclear Information System (INIS)

    Bennett, G.L.

    1979-09-01

    The NRC light-water reactor safety-research program is part of the NRC regulatory program for ensuring the safety of nuclear power plants. This paper summarizes the results of NRC-sponsored research into fuel behavior, metallurgy and materials, and operational safety. The fuel behavior research program provides a detailed understanding of the response of nuclear fuel assemblies to postulated off-normal or accident conditions. Fuel behavior research includes studies of basic fuel rod properties, in-reactor tests, computer code development, fission product release and fuel meltdown. The metallurgy and materials research program provides independent confirmation of the safe design of reactor vessels and piping. This program includes studies on fracture mechanics, irradiation embrittlement, stress corrosion, crack growth, and nondestructive examination. The operational safety research provides direct assistance to NRC officials concerned with the operational and operational-safety aspects of nuclear power plants. The topics currently being addressed include qualification testing evaluation, fire protection, human factors, and noise diagnostics

  6. Acoustic harmonic generation measurement applications: Detection of tight cracks in powder metallurgy compacts

    International Nuclear Information System (INIS)

    Barnard, D.J.; Foley, J.C.

    2000-01-01

    Standard linear ultrasonic testing techniques have long been employed for locating and characterizing relatively open cracks in a wide variety of materials, from metallic alloys and ceramics to composites. In all these materials, the detection of open cracks easily accomplished because the void between the two crack surfaces provides sufficient acoustic impedance mismatch to reflect the incident energy. Closed or partially closed cracks, however, may often go undetected because contacting interfaces allow transmission of ultrasound. In the green (unsintered) state, powder metallurgy compacts typically contain high residual stresses that have the ability to close cracks formed during the compaction process, a result of oxide films, improper powder lubricant, mold design, etc. After sintering, the reduction of residual stresses may no longer be sufficient to close the crack. Although the crack may be more easily detected, it is obvious most desirable to discover defects prior to sintering. It has been shown that the displacements of an interface may be highly nonlinear if a stress wave of sufficient intensity propagates across it, a result of the stress wave either opening or closing the interface. Current efforts involve the application of nonlinear acoustic techniques, in particular acoustic harmonic generation measurements, for the detection and characterization of tightly closed cracks in powder metallurgy parts. A description of the equipment and the measurement technique will be discussed and initial experimental results on sintered and green compacts will be presented. - This work was performed at the Ames Laboratory, Iowa State University under USDOE Contract No. W-7405-ENG-82

  7. Characterization of aluminum/steel components from recycled swarf using the powder metallurgy as technique

    International Nuclear Information System (INIS)

    Souza, V.E.S.; Masieiro, F.R.S.; Lourenco, J.M.; Felipe, R.C.T.S.

    2009-01-01

    Full text: The powder metallurgy process consists to produce metallic or ceramic components through pressure in a powder mass. These components will be submitted to a sintering temperature in order to consolidate them and then improve their mechanical proprieties. The industry is responsible for the swarf generation from different manufacture process. This paper has main goal the reutilization of aluminum and steel swarf using the powder metallurgy as technique. The methodology used in this work consists to compact Al 6060 plus steel SAE 1045 as reinforce material at 250MPa, 400MPa and 600MPa. The composition about these compacted will be 30%, 40%, 50% of steel into aluminum matrix. In this way will be analyze the hardness as function of the compressibility and quantity of steel. The samples will be processed at 500°C during 45 minutes using a resistive furnace in a hydrogen atmosphere. Micrographs of the sintered samples will be obtained by using a Scanning Electron Microscope and Optic Microscope. X-rays diffraction will be also used to characterize the phases found to due diffusivity between the steel and aluminum. (author)

  8. Development of an extra-high strength powder metallurgy nickel-base superalloy

    Science.gov (United States)

    Kent, W. B.

    1977-01-01

    A program was conducted to optimize the composition of NASA IIb-11, an alloy originally developed as a wrought material, for thermal stability and to determine the feasibility for producing the alloy using powder metallurgy techniques. Seven compositions were melted and atomized, hot isostatically pressed, cross rolled to disks and heat treated. Tensile and stress rupture properties from room temperature to 870 C (1600 F) were determined in addition to thermal stability characteristics. Processing variables included hot isostatic pressing parameters and handling, cross rolling procedures and heat treatment cycles. NASA IIb-11E displayed the best combination of overall properties for service as a 760 C (1400 F) disk material. Its composition is 0.06 C, 8.5 Cr, 9.0 Co, 2.0 Mo, 7.1 W, 6.6 Ta, 4.5 Al, 0.75 Ti, 0.5 V, 0.7 Hf, 0.01 B, 0.05 Zr and balance Ni. While the alloy exhibits the highest 760 C (1400 F) rupture strength reported for any powder metallurgy disk alloy to date, additional studies to further evaluate the effects of heat treatment may be required. The alloy is not susceptible to topologically close-packed phase formation during thermal exposure at 870 C (1600 F) for 1,500 hours, but its mechanical property levels are lowered due to grain boundary carbide formation.

  9. Analysis of cancer mortality risk among workers of a research uranium metallurgy division in France

    International Nuclear Information System (INIS)

    Jejati, H.; Laurier, D.; Tirmarche, M.; Giraud, J.M.

    1997-01-01

    This cohort study has been undertaken in response to a suspected cluster of cancers mentioned by workers involved in research activities concerning the metallurgy of uranium. The studied population included all persons having worked between 1950 and 1968 at the Metallurgy Division of the French Atomic Energy Commission (CEA). Exposures were registered on an individual annual basis. For analysis, they were grouped in three categories: use of chemicals agents (Benzene, beryllium, alcohols, solvents ...), manipulation of radioactive materials (uranium, thorium, fission decay products), and exposure to external radiation. This relatively small cohort included 356 workers followed up to December 1990. Out of observed deaths, 21 were from cancer. Total mortality from cancer was less than expected from national rates (Standardised Mortality Ratio = 0.73). Cancer mortality did not increase with duration of exposure to external radiation or with duration of manipulation of radioactive materials. Risk of cancer was increasing with the number of years of exposure to chemicals. The small size of this cohort limits the conclusion of the observed results. The purpose, despite this lack of power, was to answer a worry of the workers, more than to estimate a clear dose-response relationship linked to a specific cancer site. The effect studied here is ''all cancers'', a distinction of the different sites being uninformative because of the very small number of cases observed. Nevertheless, this study suggests some routes for further research: it highlights the importance of considering concomitant exposures like chemical ones in studies of nuclear workers. (author)

  10. Metallurgy of high-silicon steel parts produced using Selective Laser Melting

    International Nuclear Information System (INIS)

    Garibaldi, Michele; Ashcroft, Ian; Simonelli, Marco; Hague, Richard

    2016-01-01

    The metallurgy of high-silicon steel (6.9%wt.Si) processed using Selective Laser Melting (SLM) is presented for the first time in this study. High-silicon steel has great potential as a soft magnetic alloy, but its employment has been limited due to its poor workability. The effect of SLM-processing on the metallurgy of the alloy is investigated in this work using microscopy, X-Ray Diffraction (XRD) and Electron Backscatter Diffraction (EBSD). XRD analysis suggests that the SLM high-silicon steel is a single ferritic phase (solid solution), with no sign of phase ordering. This is expected to have beneficial effects on the material properties, since ordering has been shown to make silicon steels more brittle and electrically conductive. For near-fully dense samples, columnar grains with a high aspect ratio and oriented along the build direction are found. Most importantly, a <001> fibre-texture along the build direction can be changed into a cube-texture when the qualitative shape of the melt-pool is altered (from shallow to deep) by increasing the energy input of the scanning laser. This feature could potentially open the path to the manufacture of three-dimensional grain-oriented high-silicon steels for electromechanical applications.

  11. Environmental legacy of copper metallurgy and Mongol silver smelting recorded in Yunnan Lake sediments.

    Science.gov (United States)

    Hillman, Aubrey L; Abbott, Mark B; Yu, JunQing; Bain, Daniel J; Chiou-Peng, TzeHuey

    2015-03-17

    Geochemical measurements on well-dated sediment cores from Lake Er (Erhai) are used to determine the timing of changes in metal concentrations over 4500 years in Yunnan, a borderland region in southwestern China noted for rich mineral deposits but with inadequately documented metallurgical history. Our findings add new insight into the impacts and environmental legacy of human exploitation of metal resources in Yunnan history. We observe an increase in copper at 1500 BC resulting from atmospheric emissions associated with metallurgy. These data clarify the chronological issues related to links between the onset of Yunnan metallurgy and the advent of bronze technology in adjacent Southeast Asia, subjects that have been debated for nearly half a century. We also observe an increase from 1100 to 1300 AD in a number of heavy metals including lead, silver, zinc, and cadmium from atmospheric emissions associated with silver smelting. Culminating during the rule of the Mongols, known as the Yuan Dynasty (1271-1368 AD), these metal concentrations approach levels three to four times higher than those from industrialized mining activity occurring within the catchment today. Notably, the concentrations of lead approach levels at which harmful effects may be observed in aquatic organisms. The persistence of this lead pollution over time created an environmental legacy that likely contributes to known issues in modern day sediment quality. We demonstrate that historic metallurgical production in Yunnan can cause substantial impacts on the sediment quality of lake systems, similar to other paleolimnological findings around the globe.

  12. Microstructural and mechanical characteristics of porous iron prepared by powder metallurgy.

    Science.gov (United States)

    Capek, Jaroslav; Vojtěch, Dalibor

    2014-10-01

    The demand for porous biodegradable load-bearing implants has been increasing recently. Based on investigations of biodegradable stents, porous iron may be a suitable material for such applications. In this study, we prepared porous iron samples with porosities of 34-51 vol.% by powder metallurgy using ammonium bicarbonate as a space-holder material. We studied sample microstructure (SEM-EDX and XRD), flexural and compressive behaviors (universal loading machine) and hardness HV5 (hardness tester) of the prepared samples. Sample porosity increased with the amount of spacer in the initial mixtures. Only the pore surfaces had insignificant oxidation and no other contamination was observed. Increasing porosity decreased the mechanical properties of the samples; although, the properties were still comparable with human bone and higher than those of porous non-metallic biomaterials and porous magnesium prepared in a similar way. Based on these results, powder metallurgy appears to be a suitable method for the preparation of porous iron for orthopedic applications. Copyright © 2014 Elsevier B.V. All rights reserved.

  13. Fractionation study in bioleached metallurgy wastes using six-step sequential extraction.

    Science.gov (United States)

    Krasnodebska-Ostrega, Beata; Pałdyna, Joanna; Kowalska, Joanna; Jedynak, Łukasz; Golimowski, Jerzy

    2009-08-15

    The stored metallurgy wastes contain residues from ore processing operations that are characterized by relatively high concentrations of heavy metals. The bioleaching process makes use of bacteria to recover elements from industrial wastes and to decrease potential risk of environmental contamination. Wastes were treated by solutions containing bacteria. In this work, the optimized six-stage sequential extraction procedure was applied for the fractionation of Ni, Cr, Fe, Mn, Cu and Zn in iron-nickel metallurgy wastes deposited in Southern Poland (Szklary). Fractionation and total concentrations of elements in wastes before and after various bioleaching treatments were studied. Analyses of the extracts were performed by ICP-MS and FAAS. To achieve the most effective bioleaching of Zn, Cr, Ni, Cu, Mn, Fe the usage of both autotrophic and heterotrophic bacteria in sequence, combined with flushing of the residue after bioleaching is required. 80-100% of total metal concentrations were mobilized after the proposed treatment. Wastes treated according to this procedure could be deposited without any risk of environmental contamination and additionally the metals could be recovered for industrial purposes.

  14. An Ethology of Urban Fabric(s)

    DEFF Research Database (Denmark)

    Fritsch, Jonas; Thomsen, Bodil Marie Stavning

    2014-01-01

    The article explores a non-metaphorical understanding of urban fabric(s), shifting the attention from a bird’s eye perspective to the actual, textural manifestations of a variety of urban fabric(s) to be studied in their real, processual, ecological and ethological complexity within urban life. We...... effectuate this move by bringing into resonance a range of intersecting fields that all deal with urban fabric(s) in complementary ways (interaction design and urban design activism, fashion, cultural theory, philosophy, urban computing)....

  15. Effect of Milling Time on the Microstructure, Physical and Mechanical Properties of Al-Al2O3 Nanocomposite Synthesized by Ball Milling and Powder Metallurgy

    Directory of Open Access Journals (Sweden)

    Meysam Toozandehjani

    2017-10-01

    Full Text Available The effect of milling time on the morphology, microstructure, physical and mechanical properties of pure Al-5 wt % Al2O3 (Al-5Al2O3 has been investigated. Al-5Al2O3 nanocomposites were fabricated using ball milling in a powder metallurgy route. The increase in the milling time resulted in the homogenous dispersion of 5 wt % Al2O3 nanoparticles, the reduction of particle clustering, and the reduction of distances between the composite particles. The significant grain refining during milling was revealed which showed as a reduction of particle size resulting from longer milling time. X-Ray diffraction (XRD analysis of the nanocomposite powders also showed that designated ball milling contributes to the crystalline refining and accumulation of internal stress due to induced severe plastic deformation of the particles. It can be argued that these morphological and microstructural variations of nanocomposite powders induced by designated ball milling time was found to contribute to an improvement in the density, densification, micro-hardness (HV, nano-hardness (HN, and Young’s modulus (E of Al-5Al2O3 nanocomposites. HV, HN, and E values of nanocomposites were increased by ~48%, 46%, and 40%, after 12 h of milling, respectively.

  16. Powder Metallurgy Processing of a WxTaTiVCr High-Entropy Alloy and Its Derivative Alloys for Fusion Material Applications.

    Science.gov (United States)

    Waseem, Owais Ahmed; Ryu, Ho Jin

    2017-05-16

    The W x TaTiVCr high-entropy alloy with 32at.% of tungsten (W) and its derivative alloys with 42 to 90at.% of W with in-situ TiC were prepared via the mixing of elemental W, Ta, Ti, V and Cr powders followed by spark plasma sintering for the development of reduced-activation alloys for fusion plasma-facing materials. Characterization of the sintered samples revealed a BCC lattice and a multi-phase structure. The selected-area diffraction patterns confirmed the formation of TiC in the high-entropy alloy and its derivative alloys. It revealed the development of C15 (cubic) Laves phases as well in alloys with 71 to 90at.% W. A mechanical examination of the samples revealed a more than twofold improvement in the hardness and strength due to solid-solution strengthening and dispersion strengthening. This study explored the potential of powder metallurgy processing for the fabrication of a high-entropy alloy and other derived compositions with enhanced hardness and strength.

  17. Effect of Milling Time on the Microstructure, Physical and Mechanical Properties of Al-Al₂O₃ Nanocomposite Synthesized by Ball Milling and Powder Metallurgy.

    Science.gov (United States)

    Toozandehjani, Meysam; Matori, Khamirul Amin; Ostovan, Farhad; Abdul Aziz, Sidek; Mamat, Md Shuhazlly

    2017-10-26

    The effect of milling time on the morphology, microstructure, physical and mechanical properties of pure Al-5 wt % Al₂O₃ (Al-5Al₂O₃) has been investigated. Al-5Al₂O₃ nanocomposites were fabricated using ball milling in a powder metallurgy route. The increase in the milling time resulted in the homogenous dispersion of 5 wt % Al₂O₃ nanoparticles, the reduction of particle clustering, and the reduction of distances between the composite particles. The significant grain refining during milling was revealed which showed as a reduction of particle size resulting from longer milling time. X-Ray diffraction (XRD) analysis of the nanocomposite powders also showed that designated ball milling contributes to the crystalline refining and accumulation of internal stress due to induced severe plastic deformation of the particles. It can be argued that these morphological and microstructural variations of nanocomposite powders induced by designated ball milling time was found to contribute to an improvement in the density, densification, micro-hardness ( HV ), nano-hardness ( HN ), and Young's modulus ( E ) of Al-5Al₂O₃ nanocomposites. HV , HN , and E values of nanocomposites were increased by ~48%, 46%, and 40%, after 12 h of milling, respectively.

  18. Effect of Milling Time on the Microstructure, Physical and Mechanical Properties of Al-Al2O3 Nanocomposite Synthesized by Ball Milling and Powder Metallurgy

    Science.gov (United States)

    Matori, Khamirul Amin; Ostovan, Farhad; Abdul Aziz, Sidek; Mamat, Md Shuhazlly

    2017-01-01

    The effect of milling time on the morphology, microstructure, physical and mechanical properties of pure Al-5 wt % Al2O3 (Al-5Al2O3) has been investigated. Al-5Al2O3 nanocomposites were fabricated using ball milling in a powder metallurgy route. The increase in the milling time resulted in the homogenous dispersion of 5 wt % Al2O3 nanoparticles, the reduction of particle clustering, and the reduction of distances between the composite particles. The significant grain refining during milling was revealed which showed as a reduction of particle size resulting from longer milling time. X-Ray diffraction (XRD) analysis of the nanocomposite powders also showed that designated ball milling contributes to the crystalline refining and accumulation of internal stress due to induced severe plastic deformation of the particles. It can be argued that these morphological and microstructural variations of nanocomposite powders induced by designated ball milling time was found to contribute to an improvement in the density, densification, micro-hardness (HV), nano-hardness (HN), and Young’s modulus (E) of Al-5Al2O3 nanocomposites. HV, HN, and E values of nanocomposites were increased by ~48%, 46%, and 40%, after 12 h of milling, respectively. PMID:29072632

  19. Influence of thermo-mechanical processing on the microstructure of Cu-based shape memory alloys produced by powder metallurgy

    International Nuclear Information System (INIS)

    Rodriguez, P.P.; Ibarra, A.; Iza-Mendia, A.; Recarte, V.; Perez-Landazabal, J.I.; San Juan, J.; No, M.L.

    2003-01-01

    Cu-Al-Ni shape memory alloys processed by powder metallurgy show very good thermo-mechanical properties, much better than those found in alloys produced by conventional casting. In this paper, we present the microstructural characterisation of these powder metallurgy alloys in order to find the microscopic mechanisms, linked to the powder metallurgy processing method, which are indeed responsible of such good thermo-mechanical behaviour. Electron microscopy studies [scanning electron microscopy (SEM), electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM)] show that powder metallurgy processing creates a sub-grain structure characterised by the presence of low angle sub-boundaries. These sub-boundaries are found to be lying on {1 1 0} and {1 1 2} lattice planes and are composed by an arrangement of superdislocations. These sub-boundaries may improve ductility in two ways: acting as a sink of dislocations which promotes plastic deformation and decreasing stress concentration at grain boundaries. Moreover, since sub-boundaries act as weak obstacles for the movement of martensite plates, the improvement on ductility is accomplished by an adequate thermo-mechanical behaviour

  20. Self-Paced Tutorial Courses for Mineral Science - Metallurgy Departments. Final Progress Report (July 1975-August 1980).

    Science.gov (United States)

    Twidwell, L. G.

    Four courses in extractive metallurgy (Pyrometallurgy, Hydrometallurgy, Electrometallurgy; and Physical Chemistry of Iron and Steel) were prepared in a modular, self-paced format. Development of the course materials included: (1) preparation of course outlines by unit coordinators and advisory committees; (2) approval of course outlines (included…

  1. Physical metallurgy

    International Nuclear Information System (INIS)

    Adda, Y.; Dupouy, J.M.; Philibert, J.; Quere, S.

    1979-01-01

    This manual deals with the following subjects: plastic deformation of pure metals, yield strength in pure metals, work hardening in pure metals, hardening of solid solutions, recovery, recrystallization, crystal growth, creep, rupture and fatigue properties, metal transformations [fr

  2. Physical metallurgy

    International Nuclear Information System (INIS)

    Adda, Y.; Dupouy, J.M.; Philibert, J.; Quere, Y.

    1976-01-01

    In this manual, the following topics are discussed: thermodynamics of solid solutions, phase diagrams, properties of dilute solid solutions, structure of solid solutions, thermodynamics of surfaces, perfect dislocations, partial dislocations and stacking faults, interfaces, point defects

  3. Physical metallurgy

    International Nuclear Information System (INIS)

    Adda, Y.; Dupouy, J.M.; Philibert, J.; Quere, Y.

    1976-01-01

    In this manual the following topics are reviewed: macroscopic thermodynamics, statistical mechanics, quantum mechanics, cristallography, elasticity and anelasticity, and plastic deformation of a homogeneous medium [fr

  4. Physical metallurgy

    International Nuclear Information System (INIS)

    Adda, Y.; Dupouy, J.M.; Philibert, J.; Quere, Y.

    1976-01-01

    In this manual, the following topics are discussed: atomic vibrations, lattice thermal properties, chemical bonds, free electron model, band theory, properties of actinides, rare earths and transition metals, transport phenomena, magnetic properties, properties of liquid metals and amorphous state alloys

  5. Practical Metallurgy

    DEFF Research Database (Denmark)

    Bissacco, Giuliano; Deganello, Davide

    2003-01-01

    This is the report regards the activities carried out during the practical metatllurgy course concerning material properties and structures and their testing & analysis methods. During the course several aspects of the materials have been considered and different techniques have been analyzed....

  6. Fabrication and Prototyping Lab

    Data.gov (United States)

    Federal Laboratory Consortium — Purpose: The Fabrication and Prototyping Lab for composite structures provides a wide variety of fabrication capabilities critical to enabling hands-on research and...

  7. Fabrication of recyclable superhydrophobic cotton fabrics

    Science.gov (United States)

    Han, Sang Wook; Park, Eun Ji; Jeong, Myung-Geun; Kim, Il Hee; Seo, Hyun Ook; Kim, Ju Hwan; Kim, Kwang-Dae; Kim, Young Dok

    2017-04-01

    Commercial cotton fabric was coated with SiO2 nanoparticles wrapped with a polydimethylsiloxane (PDMS) layer, and the resulting material surface showed a water contact angle greater than 160°. The superhydrophobic fabric showed resistance to water-soluble contaminants and maintained its original superhydrophobic properties with almost no alteration even after many times of absorption-washing cycles of oil. Moreover, superhydrophobic fabric can be used as a filter to separate oil from water. We demonstrated a simple method of fabrication of superhydrophobic fabric with potential interest for use in a variety of applications.

  8. Application of Microscopy and X-ray Diffraction in Optimization of the Production of NiTi Alloy by Powder Metallurgy

    Czech Academy of Sciences Publication Activity Database

    Novák, P.; Školáková, A.; Vojtěch, V.; Knaislová, A.; Pokorný, P.; Moravec, H.; Kopeček, Jaromír; Karlík, M.; Kubatík, Tomáš František

    2014-01-01

    Roč. 14, č. 3 (2014), s. 387-392 ISSN 1213-2489. [Mezinárodní konference „Mikroskopie a nedestruktivní zkoušení materiálů/3./. Litoměřice, 22.10.2014-24.10.2014] R&D Projects: GA ČR(CZ) GA14-03044S Institutional support: RVO:61389021 ; RVO:68378271 Keywords : powder metallurgy * NiTi, * mechanical alloying * reactive sintering Subject RIV: JG - Metallurgy; JG - Metallurgy (FZU-D) http://journal.strojirenskatechnologie.cz/templates/obalky_casopis/XIV_2014-3.pdf

  9. Some aspects of barreling in sintered plain carbon steel powder metallurgy preforms during cold upsetting

    Directory of Open Access Journals (Sweden)

    Sumesh Narayan

    2012-04-01

    Full Text Available The present research establishes a relationship of bulged diameter with densification and hydrostatic stress in forming of sintered iron (Fe powder metallurgy preforms cold upset under two different frictional conditions, namely, nil/no and graphite lubricant condition. Sintered plain carbon steel cylindrical preforms with carbon (C contents of 0, 0.35, 0.75 and 1.1% with constant initial theoretical density of 84% and aspect ratio of 0.4 and 0.6 were prepared using a suitable die-set assembly on a 1 MN capacity hydraulic press and sintered for 90 minutes at 1200 °C. Each sintered preform was cold upset under two different frictional constraints. It is seen that the degree of bulging reduces with reducing frictional constraints at the die contact surface. Further, it is found that the bulging ratio changed as a function of relative density and hydrostatic stress, respectively, according to the power law equations.

  10. Modeling of wear behavior of Al/B{sub 4}C composites produced by powder metallurgy

    Energy Technology Data Exchange (ETDEWEB)

    Sahin, Ismail; Bektas, Asli [Gazi Univ., Ankara (Turkey). Dept. of Industrial Design Engineering; Guel, Ferhat; Cinci, Hanifi [Gazi Univ., Ankara (Turkey). Dept. of Materials and Metallurgy Engineering

    2017-06-01

    Wear characteristics of composites, Al matrix reinforced with B{sub 4}C particles percentages of 5, 10,15 and 20 produced by the powder metallurgy method were studied in this study. For this purpose, a mixture of Al and B{sub 4}C powders were pressed under 650 MPa pressure and then sintered at 635 C. The analysis of hardness, density and microstructure was performed. The produced samples were worn using a pin-on-disk abrasion device under 10, 20 and 30 N load through 500, 800 and 1200 mesh SiC abrasive papers. The obtained wear values were implemented in an artificial neural network (ANN) model having three inputs and one output using feed forward backpropagation Levenberg-Marquardt algorithm. Thus, the optimum wear conditions and hardness values were determined.

  11. Modeling of wear behavior of Al/B4C composites produced by powder metallurgy

    International Nuclear Information System (INIS)

    Sahin, Ismail; Bektas, Asli; Guel, Ferhat; Cinci, Hanifi

    2017-01-01

    Wear characteristics of composites, Al matrix reinforced with B 4 C particles percentages of 5, 10,15 and 20 produced by the powder metallurgy method were studied in this study. For this purpose, a mixture of Al and B 4 C powders were pressed under 650 MPa pressure and then sintered at 635 C. The analysis of hardness, density and microstructure was performed. The produced samples were worn using a pin-on-disk abrasion device under 10, 20 and 30 N load through 500, 800 and 1200 mesh SiC abrasive papers. The obtained wear values were implemented in an artificial neural network (ANN) model having three inputs and one output using feed forward backpropagation Levenberg-Marquardt algorithm. Thus, the optimum wear conditions and hardness values were determined.

  12. Microstructure and microanalysis studies of copper-nickel-tin alloys obtained by conventional powder metallurgy processing

    Energy Technology Data Exchange (ETDEWEB)

    Monteiro, Waldemar A.; Carrio, Juan A.G.; Masson, T.J.; Vitor, E.; Abreu, C.D.; Marques, I.M., E-mail: fisica.cch@mackenzie.br [Universidade Presbiteriana Mackenzie (CCH), Sao Paulo, SP (Brazil). Centro de Ciencias e Humanidades; Silva, L.C.E. da, E-mail: jgcarrio@mackenzie.br [Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)

    2009-07-01

    The aim of this paper was to analyze the microstructural development in samples of Cu-Ni-Sn alloys (weight %) obtained by powder metallurgy (P/M). The powders were mixed for 1/2 hour. After this, they were pressed, in a cold uniaxial pressing (1000 kPa). In the next step the specimens were sintered at temperatures varying from 650 up to 780 deg C under vacuum. Secondly, the samples were homogenized at 500 deg C for several special times. The alloys were characterized by optical microscopy, electrical conductivity and Vickers hardness. X-rays powder diffraction data were collected for the sintered samples in order to a structural and microstructural analysis. The comparative analysis is based on the sintered density, densification parameter, hardness, macrostructures and microstructures of the samples. (author)

  13. New evidence for prehistoric copper metallurgy in the vicinity of Bor

    Directory of Open Access Journals (Sweden)

    Kapuran Aleksandar

    2016-01-01

    Full Text Available The last three years of archaeological investigations at the site Ru`ana in Banjsko Polje, in the immediate vicinity of Bor, have provided new evidence regarding the role of non-ferrous metallurgy in the economy of the prehistoric communities of north-eastern Serbia. The remains of metallurgical furnaces and a large amount of metallic slags at two neighbouring sites in the mentioned settlement reveal that locations with many installations for the thermal processing of copper ore existed in the Bronze Age. We believe, judging by the finds of material culture, that metallurgical activities in this area also continued into the Iron Age and, possibly, into the 4th century AD. [Projekat Ministarstva nauke Republike Srbije, br. 177020: Archaeology of Serbia: Cultural identity, integration factors, technological processes and the role of the central Balkans in the development of European prehistory

  14. Annual report of the Metallurgy Division [for the] period ending December 1976

    International Nuclear Information System (INIS)

    Elayaperumal, K.; Gupta, C.K.; Mukhopadhyay, P.; Rao, S.V.K.

    1977-01-01

    An account of the work done in the Metallurgy Division of the Bhabha Atomic Research Centre, Bombay, during the calendar year 1976 is given. Some of the major achievements are: (1) production of boron carbide and boral sheet for the Trombay R-5 reactor under construction, (2) production of niobium metal for the manufacture of Zr-Nb-Cu alloy garter springs, (3) development of a process for graphite coating on zircaloy, (4) studies on structural and metal physics aspects of zirconium alloys and steels, (5) studies on the corrosion behaviour of zircaloy-2 as affected by the replacement of helium and stress corrosion cracking of zircaloy fuel tubes in iodine atmosphere and (6) production of high density UO 2 pellets with stable microstructures and sinterable magnesium oxide for MHD application. (M.G.B.)

  15. Encyclopedic dictionary bilingual English-Spanish of sciences: mining, chemistry, geology, metallurgy and environment

    International Nuclear Information System (INIS)

    Munoz Maradona, M.; Bellini, M.; Busleiman, M.

    2007-01-01

    This dictionary has been designed to satisfy scientists, researchers, technicians, interpreters, translators and students' needs in the areas of chemistry, geology, mining, metallurgy and environment for they find it necessary to have an English- Spanish encyclopedia on their sciences. It is a reliable book when looking for words that are normally not included in everyday dictionaries. It is now reaching the final revision stage with more than 15,000 entries. It includes scientific terms, chemical formulas of minerals and other elements, noticeable scientists' biographies, tables, graphics, and images so as to help readers' understanding. It is divided into three columns: the first one presents the English term and its area of concern; the second, the corresponding Spanish equivalent, and in the third, a suitable explanation.(author)

  16. 9th Mining and metallurgy international congress, Leon, 24-28 May 1994

    International Nuclear Information System (INIS)

    1994-01-01

    The 9th Mining and Metallurgy International Congress had 201 communications. These was articulated into 4th areas: 1.- Geological resources management and profit: 1.1- Geological and mining research on geologic resources. 1.2.- Non energetic mineral resources exploitation. 1.3- Hydro-geologic and geothermia resources. 1.4- Geologic resources and planning. 2.- Energy: 2.1.- Energetic mining.- 2.2 Oil and gas. 2.3.- Electricity production and distribution. 2.4.- Coal clean technologies. 2.5.- Energetic management. 3.- Material engineering: 3.1.- Minerallurgia and metallurgic processes. 3.2- Industrial minerals and ornamental 10cks. 3.3 .- Building materials. 3.4 Advanced technology materials. 4.- Environmental and territorial engineering in basic industry. 4.1.-Valuation of environmental impacts. 4.2.- Restoration engineering in mining. 4.3.- Effluent and residue engineering. 4.4.- Environmental management and clean technologies 4.5.- Natural and technological risks

  17. [The organization of the comprehensive prevention of urolithiasis among ferrous metallurgy workers].

    Science.gov (United States)

    Egorova, A M

    2009-01-01

    The purpose of study is to evaluate the effectiveness of the set of preventive measures as applied to 321 workers of basic ferrous metallurgy specialties (steel makers, mill men, hot metal shearers). During the clinical examination all the workers were divided on three groups: the workers without any pathology (11.83%, the first group), the workers with metabolic disorders only without urolitiasis (64.81%, the second group) and the workers with urolitiasis diagnosis approved by ultrasonography (23.36%, the third group). The effectiveness of rehabilitation measures was evaluated during half a year (diet therapy, drinking regimen, medicinal plants treatment). After the course of preventive measures was applied the overall health condition of most workers ameliorated and the number of workers with urolitiasis development risk factors reliably decreased up to 6-12%.

  18. Separating and recycling metals from mixed metallic particles of crushed electronic wastes by vacuum metallurgy.

    Science.gov (United States)

    Zhan, Lu; Xu, Zhenming

    2009-09-15

    During the treatment of electronic wastes, a crushing process is usually used to strip metals from various base plates. Several methods have been applied to separate metals from nonmetals. However, mixed metallic particles obtained from these processes are still a mixture of various metals, including some toxic heavy metals such as lead and cadmium. With emphasis on recovering copper and other precious metals, there have hitherto been no satisfactory methods to recover these toxic metals. In this paper, the criterion of separating metals from mixed metallic particles by vacuum metallurgy is built. The results show that the metals with high vapor pressure have been almost recovered completely, leading to a considerable reduction of environmental pollution. In addition, the purity of copper in mixed particles has been improved from about 80 wt % to over 98 wt %.

  19. An Overview of Internal Fixation Implant Metallurgy and Galvanic Corrosion Effects.

    Science.gov (United States)

    Koh, Justin; Berger, Aaron; Benhaim, Prosper

    2015-08-01

    Orthopedic and hand surgery implants for internal fixation of fractures have evolved substantially over the past 50 years. Newer metal compositions have been used, and new standards have been applied to older alloys, resulting in modern implants with unique physical properties and better clinical performances. Conventional wisdom has long dictated that implanting different metals should be avoided, but few guidelines exist regarding the safety of using in proximity implant systems of dissimilar metals. To better characterize the landscape of internal fixation implant metallurgy, we have compiled the recommendations and conclusions of the currently available and pertinent literature. Copyright © 2015 American Society for Surgery of the Hand. Published by Elsevier Inc. All rights reserved.

  20. [Evaluation and prognosis of occupational risk in workers of nonferrous metallurgy enterprises].

    Science.gov (United States)

    Shliapnikov, D M; Kostarev, V G

    2014-01-01

    The article deals with results of a priori and a posteriori evaluation of occupational risk for workers' health. Categories of a priori occupational risk for workers are estimated as high to very high (intolerable) risk. Findings are that work conditions in nonferrous metallurgy workshop result in upper respiratory tract diseases (medium degree of occupational conditionality). Increased prevalence of such diseases among the workers is connected with length of service. The authors revealed priority factors for occupationally conditioned diseases. A promising approach in occupational medicine is creation of methods to evaluate and forecast occupational risk, that enable to specify goal parameters for prophylactic measures. For example, modelling the risk of occupationally conditioned diseases via changes in exposure to occupational factor and length of service proved that decrease of chemical concentrations in air of workplace to maximally allowable ones lowers risk of respiratory diseases from 14 to 6 cases per year, for length of service of 5 years and population risk.

  1. Characterization of Powder Metallurgy Processed Pure Magnesium Materials for Biomedical Applications

    Directory of Open Access Journals (Sweden)

    Matěj Březina

    2017-10-01

    Full Text Available Magnesium with its mechanical properties and nontoxicity is predetermined as a material for biomedical applications; however, its high reactivity is a limiting factor for its usage. Powder metallurgy is one of the promising methods for the enhancement of material mechanical properties and, due to the introduced plastic deformation, can also have a positive influence on corrosion resistance. Pure magnesium samples were prepared via powder metallurgy. Compacting pressures from 100 MPa to 500 MPa were used for samples’ preparation at room temperature and elevated temperatures. The microstructure of the obtained compacts was analyzed in terms of microscopy. The three-point bendisng test and microhardness testing were adopted to define the compacts’ mechanical properties, discussing the results with respect to fractographic analysis. Electrochemical corrosion properties analyzed with electrochemical impedance spectroscopy carried out in HBSS (Hank’s Balanced Salt Solution and enriched HBSS were correlated with the metallographic analysis of the corrosion process. Cold compacted materials were very brittle with low strength (up to 50 MPa and microhardness (up to 50 HV (load: 0.025 kg and degraded rapidly in both solutions. Hot pressed materials yielded much higher strength (up to 250 MPa and microhardness (up to 65 HV (load: 0.025 kg, and the electrochemical characteristics were significantly better when compared to the cold compacted samples. Temperatures of 300 °C and 400 °C and high compacting pressures from 300 MPa to 500 MPa had a positive influence on material bonding, mechanical and electrochemical properties. A compacting temperature of 500 °C had a detrimental effect on material compaction when using pressure above 200 MPa.

  2. Polymorphous computing fabric

    Science.gov (United States)

    Wolinski, Christophe Czeslaw [Los Alamos, NM; Gokhale, Maya B [Los Alamos, NM; McCabe, Kevin Peter [Los Alamos, NM

    2011-01-18

    Fabric-based computing systems and methods are disclosed. A fabric-based computing system can include a polymorphous computing fabric that can be customized on a per application basis and a host processor in communication with said polymorphous computing fabric. The polymorphous computing fabric includes a cellular architecture that can be highly parameterized to enable a customized synthesis of fabric instances for a variety of enhanced application performances thereof. A global memory concept can also be included that provides the host processor random access to all variables and instructions associated with the polymorphous computing fabric.

  3. Woven Apparel Fabrics

    OpenAIRE

    Redmore, Nicola

    2012-01-01

    This chapter considers the different woven manufacturing\\ud processes used in the production of apparel fabrics. It details the mainapparel fabric types and looks at the key performance requirements of those fabrics, in relation to both the weave structure and the fibre type. The chapter then goes on to briefly describe important considerations in the design process and the various end uses for woven fabric. Application examples detailed towards the end of the chapter include fabrics that are...

  4. FABRIC QUALITY CONTROL SYSTEMS

    Directory of Open Access Journals (Sweden)

    Özlem KISAOĞLU

    2006-02-01

    Full Text Available Woven fabric quality depends on yarn properties at first, then weaving preparation and weaving processes. Defect control of grey and finished fabric is done manually on the lighted tables or automatically. Fabrics can be controlled by the help of the image analysis method. In image system the image of fabrics can be digitized by video camera and after storing controlled by the various processing. Recently neural networks, fuzzy logic, best wavelet packet model on automatic fabric inspection are developed. In this study the advantages and disadvantages of manual and automatic, on-line fabric inspection systems are given comparatively.

  5. [Factors of working environment and process on non-ferrous metallurgy enterprises in Bashkortostan Republic and workers' occupational health].

    Science.gov (United States)

    Bakirov, A B; Takaev, R M; Kondrova, N S; Shaĭkhlislamova, E R

    2011-01-01

    The authors studied factors of working environment and process on nonferrous metallurgy enterprises in Bashkortostan Republic and evaluated their influence on the workers' occupational health over 1997-2009, with consideration of occupation, sex, age, length of service, work conditions and characters. The article demonstrates that sanitary and hygienic characteristics of occupations connected with machinery operation are prone to increased integral evaluation of work conditions due to underestimation of actual hardiness and intensity of work.

  6. Development of structural diagram of automated dispatch control system for power consumption at non-ferrous metallurgy enterprises

    Science.gov (United States)

    Klyuev, R. V.; Bosikov, I. I.; Madaeva, M. Z.; A-V Turluev, R.

    2018-03-01

    The structural scheme of the automated control system of power consumption at the industrial enterprise is developed in the article. At the non-ferrous metallurgy enterprise, an energy inspection and a rank analysis of the electrical energy consumption of the main processing equipment were carried out. It is established that the enterprises of non-ferrous metallurgy are a complex process system consisting of a set of thousands of jointly functioning technological facilities. For the most effective estimation of power consumption of enterprises, it is reasonable to use the automated system of dispatching control of power consumption (ASDCPC). The paper presents the results of the development of the ASDCPC structural diagram that allows one to perform on-line control and management of the energy and process parameters of the main production units and the enterprise as a whole. As a result of the introduction of ASDCPC at the non-ferrous metallurgy enterprise, the consumed active power was reduced during the peak hours of the load by 20%, the specific electricity consumption - by 14%, the cost of the energy component in the cost of production of hard alloys - by 3%.

  7. Application of vacuum metallurgy to separate pure metal from mixed metallic particles of crushed waste printed circuit board scraps.

    Science.gov (United States)

    Zhan, Lu; Xu, Zhenming

    2008-10-15

    The principle of separating pure metal from mixed metallic particles (MMPs) byvacuum metallurgy is that the vapor pressures of various metals at the same temperature are different As a result, the metal with high vapor pressure and low boiling point can be separated from the mixed metals through distillation or sublimation, and then it can be recycled through condensation under a certain condition. The vacuum metallurgy separation (VMS) of MMPs of crushed waste printed circuit boards (WPCBs) has been studied in this paper. Theoretical analyses show that the MMPs (copper, zinc, bismuth, lead, and indium, for example) can be separated by vacuum metallurgy. The copper particles (0.15-0.20 mm) and zinc particles (<0.30 mm) were chosen to simulate the MMPs of crushed WPCBs. Experimental results show that the separated efficiency of zinc in the copper-rich particles achieves 96.19 wt % when the vacuum pressure is 0.01-0.10 Pa, the heating temperature is 1123 K, and the heating time is 105 min. Under this operation condition, the separated efficiency of zinc in the copper-rich particles from crushed WPCBs achieves 97.00 wt % and the copper purity increases from 90.68 to 99.84 wt %.

  8. On Intensive Late Holocene Iron Mining and Production in the Northern Congo Basin and the Environmental Consequences Associated with Metallurgy in Central Africa.

    Directory of Open Access Journals (Sweden)

    Karen D Lupo

    Full Text Available An ongoing question in paleoenvironmental reconstructions of the central African rainforest concerns the role that prehistoric metallurgy played in shaping forest vegetation. Here we report evidence of intensive iron-ore mining and smelting in forested regions of the northern Congo Basin dating to the late Holocene. Volumetric estimates on extracted iron-ore and associated slag mounds from prehistoric sites in the southern Central African Republic suggest large-scale iron production on par with other archaeological and historically-known iron fabrication areas. These data document the first evidence of intensive iron mining and production spanning approximately 90 years prior to colonial occupation (circa AD 1889 and during an interval of time that is poorly represented in the archaeological record. Additional site areas pre-dating these remains by 3-4 centuries reflect an earlier period of iron production on a smaller scale. Microbotanical evidence from a sediment core collected from an adjacent riparian trap shows a reduction in shade-demanding trees in concert with an increase in light-demanding species spanning the time interval associated with iron intensification. This shift occurs during the same time interval when many portions of the Central African witnessed forest transgressions associated with a return to moister and more humid conditions beginning 500-100 years ago. Although data presented here do not demonstrate that iron smelting activities caused widespread vegetation change in Central Africa, we argue that intense mining and smelting can have localized and potentially regional impacts on vegetation communities. These data further demonstrate the high value of pairing archeological and paleoenvironmental analyses to reconstruct regional-scale forest histories.

  9. On Intensive Late Holocene Iron Mining and Production in the Northern Congo Basin and the Environmental Consequences Associated with Metallurgy in Central Africa.

    Science.gov (United States)

    Lupo, Karen D; Schmitt, Dave N; Kiahtipes, Christopher A; Ndanga, Jean-Paul; Young, D Craig; Simiti, Bernard

    2015-01-01

    An ongoing question in paleoenvironmental reconstructions of the central African rainforest concerns the role that prehistoric metallurgy played in shaping forest vegetation. Here we report evidence of intensive iron-ore mining and smelting in forested regions of the northern Congo Basin dating to the late Holocene. Volumetric estimates on extracted iron-ore and associated slag mounds from prehistoric sites in the southern Central African Republic suggest large-scale iron production on par with other archaeological and historically-known iron fabrication areas. These data document the first evidence of intensive iron mining and production spanning approximately 90 years prior to colonial occupation (circa AD 1889) and during an interval of time that is poorly represented in the archaeological record. Additional site areas pre-dating these remains by 3-4 centuries reflect an earlier period of iron production on a smaller scale. Microbotanical evidence from a sediment core collected from an adjacent riparian trap shows a reduction in shade-demanding trees in concert with an increase in light-demanding species spanning the time interval associated with iron intensification. This shift occurs during the same time interval when many portions of the Central African witnessed forest transgressions associated with a return to moister and more humid conditions beginning 500-100 years ago. Although data presented here do not demonstrate that iron smelting activities caused widespread vegetation change in Central Africa, we argue that intense mining and smelting can have localized and potentially regional impacts on vegetation communities. These data further demonstrate the high value of pairing archeological and paleoenvironmental analyses to reconstruct regional-scale forest histories.

  10. New radiation technologies and methods for control of technological processes in metallurgy

    International Nuclear Information System (INIS)

    Zaykin, Yu.

    1996-01-01

    Radiation Technology of Metal and Ceramic Production with Enhanced Service Properties. Based on application of radiation technique in powder metallurgy the new technology for obtaining metals, alloys and ceramic materials with high service properties is worked out. Radiation processing of powder materials at the certain stage of the process leads to profound structure alterations at all further stages and eventually effects the properties of the resulting product. Theoretical calculation and experimental studies of electron-positron annihilation in powder-pressed samples showed that irradiation caused powder particles surface state changes favorable for further sintering and crystallization processes development. It is shown that irradiation of metal powders and powder-pressed samples by high energy electrons is technologically most efficient. The right choice of the type-and the mode of the radiation processing makes it possible to obtain metals, alloys and ceramic materials (Mo,Fe, W, Al, Ni, Cu, stainless steels, ceramics, etc.) with homogeneous structure and stable enhanced service properties. The project on radiation technology application to powder metallurgy represented by a group of authors was awarded with the diploma and the gold medal at the 22 International Exhibition of Inventions (Geneva, 1994). New Technologic Opportunities of the Chromium-Nickel Alloys Processing To obtain the required phase-structure state special methods of the chromium-nickel alloy processing for sensitive elastic devices production were worked out combining plastic deformation, thermal and radiation processing. It is shown that h-gbb phase transfer not observed before is possible in extremely non-equilibrium conditions under electron irradiation. It is established that the complex reaction of recrystallization and gb-phase deposition proceeds under electron irradiation at the room temperature when the certain threshold plastic deformation degree is reached that leads to the same

  11. Innovative fabrication of fuels and targets for Pu recycling and minor actinide transmutation

    International Nuclear Information System (INIS)

    Haas, D.; Somers, J.; Charollais, F.

    1999-01-01

    At the Karlsruhe Transuranium Institute of the Joint Research Centre, a number of processes for the fabrication of MOX fuels and minor actinide targets for transmutation are being developed. For the highly radioactive materials, methods avoiding the use of powders are preferred. Therefore, the liquid routes, SOL GEL or INRAM (infiltration of radioactive materials) are used. A new laboratory for that purpose will be commissioned in 2001. For MOX fuels, laboratory scale fabrication is being undertaken following powder metallurgy (e.g. MIMAS) or SOL GEL routes. The present research programme concerns the development of MOX fuels with large grains, achieved by SOL GEL without any additives, and by the MIMAS process with the addition of 0.1 w/o mullite (3Al 2 O 3 , 2SiO 2 ). (orig.) [de

  12. Innovative fabrication of fuels and targets for Pu recycling and minor actinide transmutation

    International Nuclear Information System (INIS)

    Haas, D.; Somers, J.; Charollais, F.

    1999-01-01

    At the Karlsruhe Transuranium Institute of the Joint Research Centre, a number of processes for the fabrication of MOX fuels and minor actinide targets for transmutation are being developed. For the highly radioactive materials, methods avoiding the use of powders are preferred. Therefore, the liquid routes, SOL GEL or INRAM (infiltration of radioactive materials) are used. A new laboratory for that purpose will be commissioned in 2001. For MOX fuels, laboratory scale fabrication is being undertaken following powder metallurgy (e.g. MIMAS) or SOL GEL routes. The present research programme concerns the development of MOX fuels with large grains, achieved by SOL GEL without any additives and by the MIMAS process with the addition of 0.1 w/o mullite (3 Al 2 O 3 , 2SiO 2 ). (authors)

  13. An investigation of wear behaviors of different Monel alloys produced by powder metallurgy

    Energy Technology Data Exchange (ETDEWEB)

    Esgin, U.; Özyürek, D. [Karabük University, Technology Faculty, Department of Manufacturing Engineering / Karabuk (Turkey); Kaya, H., E-mail: hasan.kaya@kocaeli.edu.tr [Kocaeli University, Asim Kocabiyik Vocational School of Higher Education, Department of Machine / Kocaeli (Turkey)

    2016-04-21

    In the present study, wear behaviors of Monel 400, Monel 404, Monel R-405 and Monel K-500 alloys produced by Powder Metallurgy (P/M) method were investigated. These compounds prepared from elemental powders were cold-pressed (600 MPa) and then, sintered at 1150°C for 2 hours and cooled down to the room temperature in furnace environment. Monel alloys produced by the P/M method were characterized through scanning electron microscope (SEM+EDS), X-ray diffraction (XRD), hardness and density measurements. In wear tests, standard pin-on-disk type device was used. Specimens produced within four different Monel Alloys were tested under 1ms{sup −1} sliding speed, under three different loads (20N, 30N and 40N) and five different sliding distances (400-2000 m). The results show that Monel Alloys have γ matrix and that Al{sub 0,9}Ni{sub 4,22} intermetallic phase was formed in the structure. Also, the highest hardness value was measured with the Monel K-500 alloy. In wear tests, the maximum weight loss according to the sliding distance, was observed in Monel 400 and Monel 404 alloys while the minimum weight loss was achieved by the Monel K-500 alloy.

  14. Compressibility of 304 Stainless Steel Powder Metallurgy Materials Reinforced with 304 Short Stainless Steel Fibers

    Directory of Open Access Journals (Sweden)

    Bibo Yao

    2016-03-01

    Full Text Available Powder metallurgy (P/M technique is usually used for manufacturing porous metal materials. However, some P/M materials are limitedly used in engineering for their performance deficiency. A novel 304 stainless steel P/M material was produced by a solid-state sintering of 304 stainless steel powders and 304 short stainless steel fibers, which were alternately laid in layers according to mass ratio. In this paper, the compressive properties of the P/M materials were characterized by a series of uniaxial compression tests. The effects of fiber content, compaction pressure and high temperature nitriding on compressive properties were investigated. The results indicated that, without nitriding, the samples changed from cuboid to cydariform without damage in the process of compression. The compressive stress was enhanced with increasing fiber content ranging from 0 to 8 wt.%. For compaction pressure from 55 to 75 MPa, greater compaction pressure improved compressive stress. Moreover, high temperature nitriding was able to significantly improve the yield stress, but collapse failure eventually occurred.

  15. Production of titanium alloys for advanced aerospace systems by powder metallurgy

    Directory of Open Access Journals (Sweden)

    Vinicius André Rodrigues Henriques

    2005-12-01

    Full Text Available Titanium alloys parts are ideally suited for advanced aerospace systems because of their unique combination of high specific strength at both room temperature and moderately elevated temperature, in addition to excellent corrosion resistance. Despite these features, use of titanium alloys in engines and airframes is limited by cost. The alloys processing by powder metallurgy eases the obtainment of parts with complex geometry. In this work, results of the Ti-6Al-4V and Ti-13Nb-13Zr alloys production are presented. Samples were produced by mixing of initial metallic powders followed by uniaxial and cold isostatic pressing with subsequent densification by sintering between 900 up to 1500 °C, in vacuum. Sintered samples were characterized for phase composition, microstructure and microhardness by X-ray diffraction, scanning electron microscopy and Vickers indentation, respectively. It was shown that the samples were sintered to high densities and presented homogeneous microstructure from the elements dissolution with low interstitial pick-up.

  16. Hot alpha-emitting particles in residue of mining and metallurgy

    International Nuclear Information System (INIS)

    Freyer, K.; Treutler, H.C.; Weiss, H.; Ghose, R.; Selchau-Hansen, K.; Enge, W.

    1998-01-01

    Industrial residues of ore processing and metallurgy partly contain significant amounts of natural radionuclides. Such fine-grained, contaminated materials e.g. are scrubber dust slurry in the Mansfeld region, known as Theisenschlamm, and tailings of the uranium ore processing. The environmental significance of these materials in particular is related to the high mobility of its fine grain fractions by air and on the water path. By autoradiography using solid state nuclear track detectors the homogeneity of the distribution of alpha-emitting radionuclides in the above mentioned materials has been investigated. It has been found that beside a homogeneous background distribution of the alpha activity single spots with significant higher activity concentration exist in form of hot particles. Its concentration in different contaminated materials has been determined. A surfactant treatment process has been applied to separate uranium tailings material in different grain size fractions. The fractions have been characterized chemically, radiometrically and with respect to the amount of alpha-active hot particles. (orig.) [de

  17. Possibilities for saving energy in ferrous metallurgy: Integration of technological processes

    Directory of Open Access Journals (Sweden)

    Mihailov Emil

    2016-01-01

    Full Text Available One of the main factors having a significant effect on fuel and energy saving in the production of rolled ferrous metals is matching the operation of the continuous casting machines (CCM with that of the reheating furnaces so called “continuous technologies” in the form of “direct rolling” or “hot charging”. In order to investigate the heat exchange processes, the opportunities for enhancing the energy efficiency and determining the optimal parameters of the flat product production process in ferrous metallurgy, some mathematical models of metal solidification and cooling in a continuous steel casting machine were determined as well as a mathematical model of metal heating in the reheating furnaces. For efficient implementation of such technologies one common algorithm was built on the basis of the individual mathematical models, representing the continuous casting - rolling mill complex control technology, dynamically matching the operation of the individual units to the actual production conditions in on-line mode. The developed algorithm can be used as part of a system for analyzing the thermal condition of the blocks at any single moment for the purpose of optimization of the units’ operation within the whole technological process. As a conclusion, considering the original developed algorithm, a 21-51% energy saving was noticed.

  18. Air Emissions of Selected Substances from Particular Sectors Including Metallurgy in Poland

    Directory of Open Access Journals (Sweden)

    Kargulewicz I.

    2017-03-01

    Full Text Available This article presents data on the anthropogenic air emissions of selected substances (CO2, SO2, total suspended particles (TSP, dioxins and furans (PCDD/F, Pb and Cd subject to reporting under the Climate Convention (UNFCCC or the Convention on Long-range Transboundary Air Pollution (UNECE CLRTAP. It also presents the national emissions of these substances in 2014 by the major source categories and defines the share of metal production in these emissions. Analysis is based on national emission inventory reports. Most important source of air emission in case of CO2 and SO2 is 1.A.1 Energy industries category. TSP and PCDD/F are emitted mainly from fuel combustion in small sources (i.a. households. Emission of heavy metals (Pb and Cd is connected mostly with 1.A.2. Manufacturing industries and construction category. Metallurgy is significant source of emission only for lead and cadmium from among all considered substances. The shares of particular sectors in the national emissions of given pollutants are important, in view of the possible reduction measures and the determination in which industries they could bring about tangible results.

  19. Physical Protection Study of the Radio metallurgy Installation Using SAVIComputer Program

    International Nuclear Information System (INIS)

    Pinitoyo, Andreas

    2000-01-01

    Based on IAEA Recommendation on INFCIR/225/Rev.3 (The Physical Protectionof Nuclear Material), a nuclear installation shall have physical protectionsystem for protection or being secure on sabotage activities in theinstallation and thieve of nuclear materials. The recommendation states therequirements for physical protection of nuclear materials usage, transit andstorage. Radio metallurgy Installation of the Fuel Element and ReprocessingDevelopment Center (BATAN) at Serpong is a nuclear installation for researchon post irradiation of high radioactive spent fuel element, its processingand storage. The installation has risk on threat of a sabotage, which isdominant than thieve. The RMI building was designed and constructed ofphysical protection components and have been integrated with the BATAN Safetyand Security System and the Security Guards functions to be PhysicalProtection System for the RMI. By using the SAVI Computer Program with inputdata from the existing standards, assumptions for detection possibility,delay and response, that will result the probability of interruptions of theworst adversary paths PI = 0.1. These mean that the physical protectionsystems of the RMI shall be upgraded and improved in order to be reliable orbetter if the most of paths to the target PI = 1.0. (author)

  20. Bridging the gap between metallurgy and fatigue reliability of hydraulic turbine runners

    International Nuclear Information System (INIS)

    Thibault, D; Gagnon, M; Godin, S

    2014-01-01

    The failure of hydraulic turbine runners is a very rare event. Hence, in order to assess the reliability of these components, one cannot rely on statistical models based on the number of failures in a given population. However, as there is a limited number of degradation mechanisms involved, it is possible to use physically-based reliability models. Such models are more complicated but have the advantage of being able to account for physical parameters in the prediction of the evolution of runner degradation. They can therefore propose solutions to help improve reliability. With the use of such models, the effect of materials properties on runner reliability can easily be illustrated. This paper will present a brief review of the Kitagawa-Takahashi diagram that links the damage tolerance approach, based on fracture mechanics, to the stress or strain-life approaches. This diagram is at the centre of the reliability model used in this study. Using simplified response spectra obtained from on-site runner stress measurements, the paper will show how fatigue reliability is impacted by materials fatigue properties, namely fatigue crack propagation behaviour and fatigue limit obtained on S-N curves. It will also present a review of the most important microstructural features of 13%Cr- 4%Ni stainless steels used for runner manufacturing and will review how they influence fatigue properties in an effort to bridge the gap between metallurgy and turbine runners reliability

  1. Reuse of beneficiency residue from mining and metallurgy as source of zeolites

    International Nuclear Information System (INIS)

    Souza, J.A.S.; Rodrigues, E.C.; Souza, J.A.S.; Neves, R.F.; Macedo, E.N.; Moraes, C.G.

    2011-01-01

    The mining industry and metallurgy, located in Para State, brought the concern about the huge generation of solid waste (eg The Red Mud (LV) industry Alumina; waste alumina sand-kaolin industry, waste of cuba electrolytic aluminum industry and other metal) and with the gas emissions from the burning of fossil fuels these industries. In the case of solid waste, most of which require special care such as check dams and even storage areas protected. Since the waste gases are not always properly treated and are one of the most discussed environmental problem today, according to the emission of compounds such as SOx, NOx, Cox's treatment of these effluents should be given, necessarily involves techniques of adsorption followed by reaction neutralization. These techniques can be used in two ways: by wet and dry. In the specific case of gas emissions from fossil fuels is used to wash using aqueous suspensions of calcium oxide. In this context, studies conducted in the Laboratory of Ceramic Materials, UFPA [1, 2], showed that the Bayer process residue (red mud) has characteristics that indicate the possibility of its use in place of calcium oxide in the treatment of waste gases. Moreover, waste from kaolin industry can be used as adsorbents since they go through a process of synthesis, producing different types of synthetic zeolites can be extremely useful in the treatment of waste and various activities related to environmental issues. (author)

  2. Innovative technologies for powder metallurgy-based disk superalloys: Progress and proposal

    Science.gov (United States)

    Chong-Lin, Jia; Chang-Chun, Ge; Qing-Zhi, Yan

    2016-02-01

    Powder metallurgy (PM) superalloys are an important class of high temperature structural materials, key to the rotating components of aero engines. In the purview of the present challenges associated with PM superalloys, two novel approaches namely, powder preparation and the innovative spray-forming technique (for making turbine disk) are proposed and studied. Subsequently, advanced technologies like electrode-induction-melting gas atomization (EIGA), and spark-plasma discharge spheroidization (SPDS) are introduced, for ceramic-free superalloy powders. Presently, new processing routes are sought after for preparing finer and cleaner raw powders for disk superalloys. The progress of research in spray-formed PM superalloys is first summarized in detail. The spray-formed superalloy disks specifically exhibit excellent mechanical properties. This paper reviews the recent progress in innovative technologies for PM superalloys, with an emphasis on new ideas and approaches, central to the innovation driving techniques like powder processing and spray forming. Project supported by the National Natural Science Foundation of China (Grant Nos. 50974016 and 50071014).

  3. The Promotion of Liquid Phase Sintering of Boron-Containing Powder Metallurgy Steels by Adding Nickel

    Directory of Open Access Journals (Sweden)

    Wu Ming-Wei

    2015-01-01

    Full Text Available Boron is a feasible alloying element for liquid phase sintering (LPS of powder metallurgy (PM steels. This study investigated the effect of nickel (Ni, which is widely used in PM steels, on the liquid phase sintering of boron-containing PM steels. The results showed that the addition of 1.8wt% Ni does not apparently modify the LPS mechanism of boron-containing PM steels. However, adding 1.8wt% Ni slightly improves the LPS densification from 0.60 g/cm3 to 0.65 g/cm3, though the green density is reduced. Thermodynamic simulation demonstrated that the presence of Ni lowers the temperature region of liquid formation, resulting in enhanced LPS densification. Moreover, original graphite powders remains in the steels sintered at 1200 ºC. These graphite powders mostly dissolve into the base iron powder when the sintering temperature is increased from 1200 ºC to 1250 ºC.

  4. Production of a low young modulus titanium alloy by powder metallurgy

    Directory of Open Access Journals (Sweden)

    Dalcy Roberto dos Santos

    2005-12-01

    Full Text Available Titanium alloys have several advantages over ferrous and non-ferrous metallic materials, such as high strengthto-weight ratio and excellent corrosion resistance. A blended elemental titanium powder metallurgy process has been developed to offer low cost commercial products. The process employs hydride-dehydride (HDH powders as raw material. In this work, results of the Ti-35Nb alloy sintering are presented. This alloy due to its lower modulus of elasticity and high biocompatibility is a promising candidate for aerospace and medical use. Samples were produced by mixing of initial metallic powders followed by uniaxial and cold isostatic pressing with subsequent densification by isochronal sintering between 900 up to 1600 °C, in vacuum. Sintering behavior was studied by means of microscopy and density. Sintered samples were characterized for phase composition, microstructure and microhardness by X-ray diffraction, scanning electron microscopy and Vickers indentation, respectively. Samples sintered at high temperatures display a fine plate-like alpha structure and intergranular beta. A few remaining pores are still found and density above 90% for specimens sintered in temperatures over 1500 °C is reached.

  5. Emissions from Pre-Hispanic Metallurgy in the South American Atmosphere

    Science.gov (United States)

    De Vleeschouwer, François; Vanneste, Heleen; Mauquoy, Dmitri; Piotrowska, Natalia; Torrejón, Fernando; Roland, Thomas; Stein, Ariel; Le Roux, Gaël

    2014-01-01

    Metallurgical activities have been undertaken in northern South America (NSA) for millennia. However, it is still unknown how far atmospheric emissions from these activities have been transported. Since the timing of metallurgical activities is currently estimated from scarce archaeological discoveries, the availability of reliable and continuous records to refine the timing of past metal deposition in South America is essential, as it provides an alternative to discontinuous archives, as well as evidence for global trace metal transport. We show in a peat record from Tierra del Fuego that anthropogenic metals likely have been emitted into the atmosphere and transported from NSA to southern South America (SSA) over the last 4200 yrs. These findings are supported by modern time back-trajectories from NSA to SSA. We further show that apparent anthropogenic Cu and Sb emissions predate any archaeological evidence for metallurgical activities. Lead and Sn were also emitted into the atmosphere as by-products of Inca and Spanish metallurgy, whereas local coal-gold rushes and the industrial revolution contributed to local contamination. We suggest that the onset of pre-Hispanic metallurgical activities is earlier than previously reported from archaeological records and that atmospheric emissions of metals were transported from NSA to SSA. PMID:25353346

  6. Titanium nitride deposition in titanium implant alloys produced by powder metallurgy

    International Nuclear Information System (INIS)

    Henriques, V.A.R.; Cairo, C.A.A.; Faria, J.; Lemos, T.G.; Galvani, E.T.

    2009-01-01

    Titanium nitride (TiN) is an extremely hard material, often used as a coating on titanium alloy, steel, carbide, and aluminum components to improve wear resistance. Electron Beam Physical Vapor Deposition (EB-PVD) is a form of deposition in which a target anode is bombarded with an electron beam given off by a charged tungsten filament under high vacuum, producing a thin film in a substrate. In this work are presented results of TiN deposition in targets and substrates of Ti (C.P.) and Ti- 13 Nb- 13 Zr obtained by powder metallurgy. Samples were produced by mixing of hydride metallic powders followed by uniaxial and cold isostatic pressing with subsequent densification by sintering between 900°C up to 1400 °C, in vacuum. The deposition was carried out under nitrogen atmosphere. Sintered samples were characterized for phase composition, microstructure and microhardness by X-ray diffraction, scanning electron microscopy and Vickers indentation, respectively. It was shown that the samples were sintered to high densities and presented homogeneous microstructure, with ideal characteristics for an adequate deposition and adherence. The film layer presented a continuous structure with 15μm. (author)

  7. Emissions from pre-Hispanic metallurgy in the South American atmosphere.

    Directory of Open Access Journals (Sweden)

    François De Vleeschouwer

    Full Text Available Metallurgical activities have been undertaken in northern South America (NSA for millennia. However, it is still unknown how far atmospheric emissions from these activities have been transported. Since the timing of metallurgical activities is currently estimated from scarce archaeological discoveries, the availability of reliable and continuous records to refine the timing of past metal deposition in South America is essential, as it provides an alternative to discontinuous archives, as well as evidence for global trace metal transport. We show in a peat record from Tierra del Fuego that anthropogenic metals likely have been emitted into the atmosphere and transported from NSA to southern South America (SSA over the last 4200 yrs. These findings are supported by modern time back-trajectories from NSA to SSA. We further show that apparent anthropogenic Cu and Sb emissions predate any archaeological evidence for metallurgical activities. Lead and Sn were also emitted into the atmosphere as by-products of Inca and Spanish metallurgy, whereas local coal-gold rushes and the industrial revolution contributed to local contamination. We suggest that the onset of pre-Hispanic metallurgical activities is earlier than previously reported from archaeological records and that atmospheric emissions of metals were transported from NSA to SSA.

  8. Emissions from pre-Hispanic metallurgy in the South American atmosphere.

    Science.gov (United States)

    De Vleeschouwer, François; Vanneste, Heleen; Mauquoy, Dmitri; Piotrowska, Natalia; Torrejón, Fernando; Roland, Thomas; Stein, Ariel; Le Roux, Gaël

    2014-01-01

    Metallurgical activities have been undertaken in northern South America (NSA) for millennia. However, it is still unknown how far atmospheric emissions from these activities have been transported. Since the timing of metallurgical activities is currently estimated from scarce archaeological discoveries, the availability of reliable and continuous records to refine the timing of past metal deposition in South America is essential, as it provides an alternative to discontinuous archives, as well as evidence for global trace metal transport. We show in a peat record from Tierra del Fuego that anthropogenic metals likely have been emitted into the atmosphere and transported from NSA to southern South America (SSA) over the last 4200 yrs. These findings are supported by modern time back-trajectories from NSA to SSA. We further show that apparent anthropogenic Cu and Sb emissions predate any archaeological evidence for metallurgical activities. Lead and Sn were also emitted into the atmosphere as by-products of Inca and Spanish metallurgy, whereas local coal-gold rushes and the industrial revolution contributed to local contamination. We suggest that the onset of pre-Hispanic metallurgical activities is earlier than previously reported from archaeological records and that atmospheric emissions of metals were transported from NSA to SSA.

  9. Microstructurally sensitive crack nucleation around inclusions in powder metallurgy nickel-based superalloys

    International Nuclear Information System (INIS)

    Jiang, J.; Yang, J.; Zhang, T.; Zou, J.; Wang, Y.; Dunne, F.P.E.; Britton, T.B.

    2016-01-01

    Nickel-based superalloys are used in high strength, high-value applications, such as gas turbine discs in aero engines. In these applications the integrity of the disc is critical and therefore understanding crack initiation mechanisms is of high importance. With an increasing trend towards powder metallurgy routes for discs, sometimes unwanted non-metallic inclusions are introduced during manufacture. These inclusions vary in size from ∼10 μm to 200 μm which is comparable to the grain size of the nickel-based superalloys. Cracks often initiate near these inclusions, and the precise size, shape, location and path of these cracks are microstructurally sensitive. In this study, we focus on crack initiation at the microstructural length scale using a controlled three-point bend test, with the inclusion deliberately located within the tensile fibre of the beam. Electron backscatter diffraction (EBSD) is combined with high spatial resolution digital image correlation (HR-DIC) to explore full field plastic strain distributions, together with finite element modelling, to understand the micro-crack nucleation mechanisms. This full field information and controlled sample geometry enable us to systematically test crack nucleation criteria. We find that a combined stored energy and dislocation density provide promising results. These findings potentially facilitate more reliable and accurate lifing prediction tools to be developed and applied to engineering components. - Highlights: • High resolution digital image correlation. • High resolution electron backscatter diffraction. • Crack nucleation. • Non-metallic inclusion.

  10. Power-law creep of powder-metallurgy grade molybdenum sheet

    International Nuclear Information System (INIS)

    Ciulik, J.; Taleff, E.M.

    2007-01-01

    Creep behavior of commercial-purity, powder-metallurgy grade molybdenum (Mo) sheet has been investigated at temperatures between 1300 and 1600 deg. C (0.56-0.63 T m ) using tensile testing at controlled strain rates. Strain-rate-change tests were performed at constant-temperatures over true-strain rates from 1.0 x 10 -6 to 5.0 x 10 -4 s -1 . Results agree with previously published data indicating that Mo follows power-law creep with a stress exponent of about 5; however, the present results address a temperature range not previously documented. The activation energy for creep was determined to be 240 kJ/mol within this temperature range, which is lower than previously published values and approximately half the value reported for self-diffusion, indicating that diffusion mechanisms faster than lattice diffusion are active. It is shown that Mo creep data from a variety of investigations converge closely to a single line on a master plot of strain rate normalized using an activation energy of 240 kJ/mol when plotted against stress normalized by the temperature-dependent elastic modulus. This activation energy for creep is attributed to an effective diffusivity that fits the creep data obtained during this study as well as from previously published creep data from commercial-purity molybdenum

  11. The substitution of nickel for cobalt in hot isostatically pressed powder metallurgy UDIMET 700 alloys

    Science.gov (United States)

    Harf, F. H.

    1985-01-01

    Nickel was substituted in various proportions for cobalt in a series of five hot-isostatically-pressed powder metallurgy alloys based on the UDIMET 700 composition. These alloys were given 5-step heat treatments appropriate for use in turbine engine disks. The resultant microstructures displayed three distinct sizes of gamma-prime particles in a gamma matrix. The higher cobalt-content alloys contained larger amounts of the finest gamma-prime particles, and had the lowest gamma-gamma-prime lattice mismatch. While all alloys had approximately the same tensile properties at 25 and 650 gamma C, the rupture lives at 650 and 760 C peaked in the alloys with cobalt contents between 12.7 and 4.3 pct. Minimum creep rates increased as cobalt contents were lowered, suggesting their correlation with the gamma-prime particle size distribution and the gamma-gamma-prime mismatch. It was also found that, on overaging at temperatures higher than suitable for turbine disk use, the high cobalt-content alloys were prone to sigma phase formation.

  12. State-of-the-art of recycling e-wastes by vacuum metallurgy separation.

    Science.gov (United States)

    Zhan, Lu; Xu, Zhenming

    2014-12-16

    In recent era, more and more electric and electronic equipment wastes (e-wastes) are generated that contain both toxic and valuable materials in them. Most studies focus on the extraction of valuable metals like Au, Ag from e-wastes. However, the recycling of metals such as Pb, Cd, Zn, and organics has not attracted enough attentions. Vacuum metallurgy separation (VMS) processes can reduce pollution significantly using vacuum technique. It can effectively recycle heavy metals and organics from e-wastes in an environmentally friendly way, which is beneficial for both preventing the heavy metal contaminations and the sustainable development of resources. VMS can be classified into several methods, such as vacuum evaporation, vacuum carbon reduction and vacuum pyrolysis. This paper respectively reviews the state-of-art of these methods applied to recycling heavy metals and organics from several kinds of e-wastes. The method principle, equipment used, separating process, optimized operating parameters and recycling mechanism of each case are illustrated in details. The perspectives on the further development of e-wastes recycling by VMS are also presented.

  13. Anodization Mechanism on SiC Nanoparticle Reinforced Al Matrix Composites Produced by Power Metallurgy.

    Science.gov (United States)

    Ferreira, Sonia C; Conde, Ana; Arenas, María A; Rocha, Luis A; Velhinho, Alexandre

    2014-12-19

    Specimens of aluminum-based composites reinforced by silicon carbide nanoparticles (Al/SiC np ) produced by powder metallurgy (PM) were anodized under voltage control in tartaric-sulfuric acid (TSA). In this work, the influence of the amount of SiC np on the film growth during anodizing was investigated. The current density versus time response and the morphology of the porous alumina film formed at the composite surface are compared to those concerning a commercial aluminum alloy (AA1050) anodized under the same conditions. The processing method of the aluminum alloys influences the efficiency of the anodizing process, leading to a lower thicknesses for the unreinforced Al-PM alloy regarding the AA1050. The current density versus time response is strongly dependent on the amount of SiC np . The current peaks and the steady-state current density recorded at each voltage step increases with the SiC np volume fraction due to the oxidation of the SiC np . The formation mechanism of the anodic film on Al/SiC np composites is different from that occurring in AA1050, partly due the heterogeneous distribution of the reinforcement particles in the metallic matrix, but also to the entrapment of SiC np in the anodic film.

  14. Factors Influencing Dwell Fatigue Cracking in Notches of Powder Metallurgy Superalloys

    Science.gov (United States)

    Gabb, T. P.; Telesman, J.; Ghosn, L.; Garg, A.; Gayda, J.

    2011-01-01

    The influences of heat treatment and cyclic dwells on the notch fatigue resistance of powder metallurgy disk superalloys were investigated for low solvus high refractory (LSHR) and ME3 disk alloys. Disks were processed to produce material conditions with varied microstructures and associated mechanical properties. Notched specimens were first subjected to baseline dwell fatigue cycles having a dwell at maximum load, as well as tensile, stress relaxation, creep rupture, and dwell fatigue crack growth tests at 704 C. Several material heat treatments displayed a bimodal distribution of fatigue life with the lives varying by two orders-of-magnitude, while others had more consistent fatigue lives. This response was compared to other mechanical properties, in search of correlations. The wide scatter in baseline dwell fatigue life was observed only for material conditions resistant to stress relaxation. For selected materials and conditions, additional tests were then performed with the dwells shifted in part or in total to minimum tensile load. The tests performed with dwells at minimum load exhibited lower fatigue lives than max dwell tests, and also exhibited early crack initiation and a substantial increase in the number of initiation sites. These results could be explained in part by modeling evolution of peak stresses in the notch with continued dwell fatigue cycling. Fatigue-environment interactions were determined to limit life for the fatigue cycles with dwells.

  15. Compressibility of 304 Stainless Steel Powder Metallurgy Materials Reinforced with 304 Short Stainless Steel Fibers.

    Science.gov (United States)

    Yao, Bibo; Zhou, Zhaoyao; Duan, Liuyang; Xiao, Zhiyu

    2016-03-04

    Powder metallurgy (P/M) technique is usually used for manufacturing porous metal materials. However, some P/M materials are limitedly used in engineering for their performance deficiency. A novel 304 stainless steel P/M material was produced by a solid-state sintering of 304 stainless steel powders and 304 short stainless steel fibers, which were alternately laid in layers according to mass ratio. In this paper, the compressive properties of the P/M materials were characterized by a series of uniaxial compression tests. The effects of fiber content, compaction pressure and high temperature nitriding on compressive properties were investigated. The results indicated that, without nitriding, the samples changed from cuboid to cydariform without damage in the process of compression. The compressive stress was enhanced with increasing fiber content ranging from 0 to 8 wt.%. For compaction pressure from 55 to 75 MPa, greater compaction pressure improved compressive stress. Moreover, high temperature nitriding was able to significantly improve the yield stress, but collapse failure eventually occurred.

  16. Residual Stresses in a NiCrY-Coated Powder Metallurgy Disk Superalloy

    Science.gov (United States)

    Gabb, Timothy P.; Rogers, Richard B.; Nesbitt, James A.; Puleo, Bernadette J.; Miller, Robert A.; Telesman, Ignacy; Draper, Susan L.; Locci, Ivan E.

    2017-01-01

    Protective ductile coatings will be necessary to mitigate oxidation and corrosion attack on superalloy disks exposed to increasing operating temperatures in some turbine engine environments. However, such coatings must be resistant to harmful surface cracking during service. The objective of this study was to investigate how residual stresses evolve in such coatings. Cylindrical gage fatigue specimens of powder metallurgy-processed disk superalloy LSHR were coated with a NiCrY coating, shot peened, and then subjected to fatigue in air at room and high temperatures. The effects of shot peening and fatigue cycling on average residual stresses and other aspects of the coating were assessed. Shot peening did induce beneficial compressive residual stresses in the coating and substrate. However, these stresses became more tensile in the coating with subsequent heating and contributed to cracking of the coating in long intervals of cycling at 760 C. Substantial compressive residual stresses remained in the substrate adjacent to the coating, sufficient to suppress fatigue cracking. The coating continued to protect the substrate from hot corrosion pitting, even after fatigue cracks initiated in the coating.

  17. Dwell Notch Low Cycle Fatigue Behavior of a Powder Metallurgy Nickel Disk Alloy

    Science.gov (United States)

    Telesman, J.; Gabb, T. P.; Yamada, Y.; Ghosn, L. J.; Jayaraman, N.

    2012-01-01

    A study was conducted to determine the processes which govern dwell notch low cycle fatigue (NLCF) behavior of a powder metallurgy (P/M) ME3 disk superalloy. The emphasis was placed on the environmentally driven mechanisms which may embrittle the highly stressed notch surface regions and reduce NLCF life. In conjunction with the environmentally driven notch surface degradation processes, the visco-plastic driven mechanisms which can significantly change the notch root stresses were also considered. Dwell notch low cycle fatigue testing was performed in air and vacuum on a ME3 P/M disk alloy specimens heat treated using either a fast or a slow cooling rate from the solutioning treatment. It was shown that dwells at the minimum stress typically produced a greater life debit than the dwells applied at the maximum stress, especially for the slow cooled heat treatment. Two different environmentally driven failure mechanisms were identified as the root cause of early crack initiation in the min dwell tests. Both of these failure mechanisms produced mostly a transgranular crack initiation failure mode and yet still resulted in low NLCF fatigue lives. The lack of stress relaxation during the min dwell tests produced higher notch root stresses which caused early crack initiation and premature failure when combined with the environmentally driven surface degradation mechanisms. The importance of environmental degradation mechanisms was further highlighted by vacuum dwell NLCF tests which resulted in considerably longer NLCF lives, especially for the min dwell tests.

  18. Photochemical cutting of fabrics

    Science.gov (United States)

    Piltch, Martin S.

    1994-01-01

    Apparatus for the cutting of garment patterns from one or more layers of fabric. A laser capable of producing laser light at an ultraviolet wavelength is utilized to shine light through a pattern, such as a holographic phase filter, and through a lens onto the one or more layers of fabric. The ultraviolet laser light causes rapid photochemical decomposition of the one or more layers of fabric, but only along the pattern. The balance of the fabric of the one or more layers of fabric is undamaged.

  19. Obtainment, machining and wear of metal matrix composites processed by powder metallurgy

    International Nuclear Information System (INIS)

    Jesus, Edilson Rosa Barbosa de.

    1998-01-01

    The aim of this investigation was the obtainment of metal matrix composites (MMC) by the route of powder metallurgy, and the valuation of these materials with relation to their machining and wear characteristics. Firstly, were obtained pure commercial aluminium matrix composites materials, with 5, 10 and 15% volumetric fraction of silicon carbide particles. Was also obtained a material without reinforcement particles in order to verify by comparison, the influence of addition of reinforcement particles. The obtained materials were characterized physics (hydrostatic density), mechanics (hardness and tensile tests) and microstructurally (optical microscopy and scanning electron microscopy). The results showed a homogeneous distribution of reinforcement particles in the composite, and improvement in the mechanical properties, mainly tensile strength (UTS) in comparison to the unreinforced material. After, tests were made to verify the materials behavior during machining and to check the performance of several tool materials (cemented carbide, ceramics and polycrystalline diamond). In these tests, values of the cutting force were measured by instrumented tool-holders. Phenomena such as tool wear, built-up edge formation and mechanism of chip formation were also observed and evaluated. The results from the cemented carbide tool tests, were utilised for the machinability index determination of each material. These results were applied to the Taylor equation and the equation constants for each material and test conditions were determined. The results showed that the inclusion of silicon carbide particles made extremely difficult the machining of the composites, and only with diamond tool, satisfactory results were obtained. At last, wear tests were performed to verify the influence of the reinforcement particles in the characteristics of wear resistance of the materials. The results obtained were utilized in the wear coefficient determination for each material. The

  20. The utilization of mechanochemistry in the extractive metallurgy and at the nanocrystalline materials preparation

    Directory of Open Access Journals (Sweden)

    Boldižárová Eva

    2002-03-01

    Full Text Available The possibility of the application of mechanochemistry in the extractive metallurgy and the nanocrystalline materials preparation is studied. The aim of the experiments is the chloride leaching of a complex sulphidic CuPbZn concentrate (Hodruša-Hámre, the modification of properties of CaCO3 (Yauli, Peru for zinc sorption from model solutions and the mechanochemical reduction of copper sulphide by elemental iron.The chloride leaching of mechanically activated complex sulphidic CuPbZn concentrate is a selective process. While the recoveries of copper, lead and zinc are 65-85 %, the recoveries of silver and gold are less than 7 % and 2 %, respectively.The positive influence of CaCO3 mechanical activation for zinc sorption from ZnSO4 solution was observed. While only 58 % of zinc sorption was determined after 30 minutes for a non-activated sample, 98 % of zinc sorption was determined after 3 minutes sorption for the sample mechanically activated for 15 minutes.By the mechanochemical reduction of copper sulphide with iron, nanocrystalline copper and iron sulphide are formed. This reaction is an example of the new “solid state technology“, where chemical processes in the gaseous and liquid states are excluded.The results can serve as a contribution to the optimization of copper, lead and zinc extraction from complex sulphidic concentrates, the increase of non-ferrous metals sorption efficiency on mineral sorbents as well as to the nanocrystalline copper preparation.The application of mechanical activation has grown in the laboratory research. The Institute of Geotechnics of SAS has also achieved significant theoretical results in study of mechanical activation of sulphides and their reactivity in the different solid-phase reactions with the effect on industrial applications. The Institute has developed the technology of mechanochemical leaching (process MELT which was successfully tested in a pilot plant unit.

  1. The metallurgy, mechanics, modelling and assessment of dissimilar material brazed joints

    International Nuclear Information System (INIS)

    Hamilton, Niall Robert; Wood, James; Galloway, Alexander; Olsson Robbie, Mikael Brian; Zhang Yuxuan

    2013-01-01

    At the heart of any procedure for modelling and assessing the design or failure of dissimilar material brazed joints there must be a basic understanding of the metallurgy and mechanics of the joint. This paper is about developing this understanding and addressing the issues faced with modelling and predicting failure in real dissimilar material brazed joints and the challenges still to be overcome in many cases. An understanding of the key metallurgical features of such joints in relation to finite element modelling is presented in addition to a study of the mechanics and stress state at an abrupt interface between two materials. A discussion is also presented on why elastic singularities do not exist based on a consideration of the assumption of an abrupt change in material properties and plasticity in the vicinity of the joint. In terms of modelling real dissimilar material brazed joints; there are several barriers to accurately capturing the stress state in the region of the joint and across the brazed layer and these are discussed in relation to a metallurgical study of a real dissimilar material brazed joint. However, this does not preclude using a simplified modelling approach with a representative braze layer in design and failure assessment away from the interface. In addition modelling strategies and techniques for assessing the various failure mechanisms of dissimilar material brazed joints are discussed. The findings from this paper are applicable to dissimilar material brazed joints found in a range of applications; however the references listed are primarily focussed on work in fusion research and development.

  2. In vitro degradation and cytotoxicity of Mg/Ca composites produced by powder metallurgy.

    Science.gov (United States)

    Zheng, Y F; Gu, X N; Xi, Y L; Chai, D L

    2010-05-01

    Mg/Ca (1 wt.%, 5 wt.%, 10 wt.% Ca) composites were prepared from pure magnesium and calcium powders using the powder metallurgy method, aiming to enlarge the addition of Ca content without the formation of Mg(2)Ca. The microstructures, mechanical properties and cytotoxicities of Mg/Ca composite samples were investigated. The corrosion of Mg/Ca composites in Dulbecco's modified Eagle's medium (DMEM) for various immersion intervals was studied by electrochemical impedance spectroscopy measurements and environmental scanning electron microscope, with the concentrations of released Mg and Ca ions in DMEM for various immersion time intervals being measured. It was shown that the main constitutional phases were Mg and Ca, which were uniformly distributed in the Mg matrix. The ultimate tensile strength (UTS) and elongation of experimental composites decreased with increasing Ca content, and the UTS of Mg/1Ca composite was comparable with that of as-extruded Mg-1Ca alloy. The corrosion potential increased with increasing Ca content, whereas the current density and the impedance decreased. It was found that the protective surface film formed quickly at the initial immersion stage. With increasing immersion time, the surface film became compact, and the corrosion rate of Mg/Ca composites slowed down. The surface film consisted mainly of CaCO(3), MgCO(3)x3H(2)O, HA and Mg(OH)(2) after 72 h immersion in DMEM. Mg/1Ca and Mg/5Ca composite extracts had no significant toxicity (p>0.05) to L-929 cells, whereas Mg/10Ca composite extract induced approximately 40% reduced cell viability. Copyright (c) 2009 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

  3. Fabrics for aeronautic construction

    Science.gov (United States)

    Walen, E D

    1918-01-01

    The Bureau of Standards undertook the investigation of airplane fabrics with the view of finding suitable substitutes for the linen fabrics, and it was decided that the fibers to be considered were cotton, ramie, silk, and hemp. Of these, the cotton fiber was the logical one to be given primary consideration. Report presents the suitability, tensibility and stretching properties of cotton fabric obtained by laboratory tests.

  4. Fabricating architectural volume

    DEFF Research Database (Denmark)

    Feringa, Jelle; Søndergaard, Asbjørn

    2015-01-01

    The 2011 edition of Fabricate inspired a number of collaborations, this article seeks to highlight three of these. There is a common thread amongst the projects presented: sharing the ambition to close the rift between design and fabrication while incorporating structural design aspects early on....... The development of fabrication techniques in the work presented is considered an inherent part of architectural design and shares the aspiration of developing approaches to manufacturing architecture that are scalable to architectural proportions1 and of practical relevance....

  5. Study of alumina-trichite reinforcement of a nickel-based matric by means of powder metallurgy

    Science.gov (United States)

    Walder, A.; Hivert, A.

    1982-01-01

    Research was conducted on reinforcing nickel based matrices with alumina trichites by using powder metallurgy. Alumina trichites previously coated with nickel are magnetically aligned. The felt obtained is then sintered under a light pressure at a temperature just below the melting point of nickel. The halogenated atmosphere technique makes it possible to incorporate a large number of additive elements such as chromium, titanium, zirconium, tantalum, niobium, aluminum, etc. It does not appear that going from laboratory scale to a semi-industrial scale in production would create any major problems.

  6. Estimation of snow pollution in the region of non-ferrous metallurgy enterprises by the neutron activation method

    International Nuclear Information System (INIS)

    Khatamov, Sh.; Khamidova, R.; Kist, A.A.

    1980-01-01

    Possibility of determination of more than 25 chemical elements in snow water selected in the region of non-ferrous metallurgy enterprises has been shown using the methods of neutron activation and γ-spectrometry of high resolution. Elements were determined from one sample by three-fold irradiation in the nuclear reactor depending on the half-life period and other nuclear activation parameters of the formed radioisotopes. The analysis of snow cover has revealed the character of pollution of surrounding medium and air basin by toxical elements

  7. Effects of carbon and hafnium concentrations in wrought powder-metallurgy superalloys based on NASA 2B-11 alloy

    Science.gov (United States)

    Miner, R. V., Jr.

    1976-01-01

    A candidate alloy for advanced-temperature turbine engine disks, and four modifications of that alloy with various C and Hf concentrations were produced as cross-rolled disks from prealloyed powder that was hot isostatically compacted. The mechanical properties, microstructures, and phase relations of the alloys are discussed in terms of their C and Hf concentrations. A low-C and high-Hf modification of IIB-11 had the best balance of mechanical properties for service below about 750 C. Because of their finer grain sizes, none of the powder-metallurgy alloys produced had the high-temperature rupture strength of conventionally cast and wrought IIB-11.

  8. Early atmospheric metal pollution provides evidence for Chalcolithic/Bronze Age mining and metallurgy in Southwestern Europe

    Energy Technology Data Exchange (ETDEWEB)

    Martínez Cortizas, Antonio, E-mail: antonio.martinez.cortizas@usc.es [Departamento de Edafoloxía e Química Agrícola, Facultade de Bioloxía, Universidade de Santiago de Compostela, Campus Sur s/n, Santiago de Compostela (Spain); López-Merino, Lourdes, E-mail: lourdes.lopez-merino@brunel.ac.uk [Institute of Environment, Health and Societies, Brunel University London, UB8 3PH Uxbridge (United Kingdom); Bindler, Richard, E-mail: richard.bindler@umu.se [Department of Ecology and Environmental Science, Umeå University, Umeå (Sweden); Mighall, Tim, E-mail: t.mighall@abdn.ac.uk [Department of Geography & Environment, School of Geosciences, University of Aberdeen, Elphinstone Road, Aberdeen AB24 3UF (United Kingdom); Kylander, Malin E., E-mail: malin.kylander@geo.su.se [Department of Geological Sciences and the Bolin Centre for Climate Research, Stockholm University, SE-10691, Stockholm (Sweden)

    2016-03-01

    Although archaeological research suggests that mining/metallurgy already started in the Chalcolithic (3rd millennium BC), the earliest atmospheric metal pollution in SW Europe has thus far been dated to ~ 3500–3200 cal. yr. BP in paleo-environmental archives. A low intensity, non-extensive mining/metallurgy and the lack of appropriately located archives may be responsible for this mismatch. We have analysed the older section (> 2100 cal. yr. BP) of a peat record from La Molina (Asturias, Spain), a mire located in the proximity (35–100 km) of mines which were exploited in the Chalcolithic/Bronze Age, with the aim of assessing evidence of this early mining/metallurgy. Analyses included the determination of C as a proxy for organic matter content, lithogenic elements (Si, Al, Ti) as markers of mineral matter, and trace metals (Cr, Cu, Zn, Pb) and stable Pb isotopes as tracers of atmospheric metal pollution. From ~ 8000 to ~ 4980 cal. yr. BP the Pb composition is similar to that of the underlying sediments (Pb 15 ± 4 μg g{sup −1}; {sup 206}Pb/{sup 207}Pb 1.204 ± 0.002). A sustained period of low {sup 206}Pb/{sup 207}Pb ratios occurred from ~ 4980 to ~ 2470 cal. yr. BP, which can be divided into four phases: Chalcolithic (~ 4980–3700 cal. yr. BP), {sup 206}Pb/{sup 207}Pb ratios decline to 1.175 and Pb/Al ratios increase; Early Bronze Age (~ 3700–3500 cal. yr. BP), {sup 206}Pb/{sup 207}Pb increase to 1.192 and metal/Al ratios remain stable; Late Bronze Age (~ 3500–2800 cal. yr. BP), {sup 206}Pb/{sup 207}Pb decline to their lowest values (1.167) while Pb/Al and Zn/Al increase; and Early Iron Age (~ 2800–2470 cal. yr. BP), {sup 206}Pb/{sup 207}Pb increase to 1.186, most metal/Al ratios decrease but Zn/Al shows a peak. At the beginning of the Late Iron Age, {sup 206}Pb/{sup 207}Pb ratios and metal enrichments show a rapid return to pre-anthropogenic values. These results provide evidence of regional/local atmospheric metal pollution triggered by the

  9. Study of Proper Time Range for Current Flow to Resistance Spot Welding Inspected by Mechanical Property and Metallurgy Testing

    International Nuclear Information System (INIS)

    Pearsura, Prachya

    2007-08-01

    Full text: This research used the mechanical property and metallurgy testing to identify the proper time range for current flow. The specimen tested was 1 mm thick mild steel. The welded specimens were tested by Tensile Shear testing following JIS Z 3136: 1999 and Macro Structure testing follow by JIS Z 3139: 1978. Subsequently, the results from analyzing were compared with standard JIS Z 3140. The results show that the suitable current flow is 8 to 10 cycles. This technique can be applied to monitor the process and the quality of resistance spot welding

  10. Early atmospheric metal pollution provides evidence for Chalcolithic/Bronze Age mining and metallurgy in Southwestern Europe.

    Science.gov (United States)

    Martínez Cortizas, Antonio; López-Merino, Lourdes; Bindler, Richard; Mighall, Tim; Kylander, Malin E

    2016-03-01

    Although archaeological research suggests that mining/metallurgy already started in the Chalcolithic (3rd millennium BC), the earliest atmospheric metal pollution in SW Europe has thus far been dated to ~3500-3200 cal.yr. BP in paleo-environmental archives. A low intensity, non-extensive mining/metallurgy and the lack of appropriately located archives may be responsible for this mismatch. We have analysed the older section (>2100 cal.yr. BP) of a peat record from La Molina (Asturias, Spain), a mire located in the proximity (35-100 km) of mines which were exploited in the Chalcolithic/Bronze Age, with the aim of assessing evidence of this early mining/metallurgy. Analyses included the determination of C as a proxy for organic matter content, lithogenic elements (Si, Al, Ti) as markers of mineral matter, and trace metals (Cr, Cu, Zn, Pb) and stable Pb isotopes as tracers of atmospheric metal pollution. From ~8000 to ~4980 cal.yr. BP the Pb composition is similar to that of the underlying sediments (Pb 15 ± 4 μg g(-1); (206)Pb/(207)Pb 1.204 ± 0.002). A sustained period of low (206)Pb/(207)Pb ratios occurred from ~4980 to ~2470 cal.yr. BP, which can be divided into four phases: Chalcolithic (~4980-3700 cal.yr. BP), (206)Pb/(207)Pb ratios decline to 1.175 and Pb/Al ratios increase; Early Bronze Age (~3700-3500 cal.yr. BP), (206)Pb/(207)Pb increase to 1.192 and metal/Al ratios remain stable; Late Bronze Age (~3500-2800 cal.yr. BP), (206)Pb/(207)Pb decline to their lowest values (1.167) while Pb/Al and Zn/Al increase; and Early Iron Age (~2800-2470 cal.yr. BP), (206)Pb/(207)Pb increase to 1.186, most metal/Al ratios decrease but Zn/Al shows a peak. At the beginning of the Late Iron Age, (206)Pb/(207)Pb ratios and metal enrichments show a rapid return to pre-anthropogenic values. These results provide evidence of regional/local atmospheric metal pollution triggered by the earliest phases of mining/metallurgy in the area, and reconcile paleo-environmental and

  11. Annual Report on Scientific Activities in 1997 of Department of Physics and Nuclear Techniques, Academy of Mining and Metallurgy, Cracow

    International Nuclear Information System (INIS)

    Wolny, J.; Olszynska, E.

    1998-01-01

    The Annual Report 1997 is the review of scientific activities of the Department of Nuclear Physics and Techniques (DNPT) of the Academy of Mining and Metallurgy, Cracow. The studies connected with: radiometric analysis, nuclear electronics, solid state physics, elementary particle and detectors, medical physics, physics of environment, theoretical physics, nuclear geophysics, energetic problems, industrial radiometry and tracer techniques have been broadly presented. The fill list of works being published and presented at scientific conferences in 1997 by the staff of DNPT are also included

  12. Review of some past and present powder metallurgy programs at the Los Alamos Scientific Laboratory

    International Nuclear Information System (INIS)

    Sheinberg, H.

    1977-07-01

    A new process is described for molding and extruding complicated shapes of uranium-loaded graphite to close tolerances for use in nuclear propulsion engines. The process for hot-pressing copper-boron carbide and forming it into sheet for use as neutronic control material for these engines is also described. Fabrication procedure and deformation testing of carbide-graphite composites for fuel element supports are outlined, as is the procedure for fabricating tungsten-thoria heat shields for these reactors. Details are given for production of uranium carbide-zirconium carbide solid-solution powder and fabrication of this powder and molybdenum uranium oxide powder into fuel pins for thermionic reactors. Methods and details are given for spheroidization of lithium deuteride to be used as laser fusion targets and for quality upgrading and characterization of micron-size balloons for that use

  13. Fabricating architectural volume

    DEFF Research Database (Denmark)

    Feringa, Jelle; Søndergaard, Asbjørn

    2015-01-01

    The 2011 edition of Fabricate inspired a number of collaborations, this article seeks to highlight three of these. There is a common thread amongst the projects presented: sharing the ambition to close the rift between design and fabrication while incorporating structural design aspects early on...

  14. Smart Fabrics Technology Development

    Science.gov (United States)

    Simon, Cory; Potter, Elliott; Potter, Elliott; McCabe, Mary; Baggerman, Clint

    2010-01-01

    Advances in Smart Fabrics technology are enabling an exciting array of new applications for NASA exploration missions, the biomedical community, and consumer electronics. This report summarizes the findings of a brief investigation into the state of the art and potential applications of smart fabrics to address challenges in human spaceflight.

  15. Microstructure, Hardness, and Corrosion Behavior of TiC-Duplex Stainless Steel Composites Fabricated by Spark Plasma Sintering

    Science.gov (United States)

    Han, Ying; Zhang, Wei; Sun, Shicheng; Chen, Hua; Ran, Xu

    2017-08-01

    Duplex stainless steel composites with various weight fractions of TiC particles are prepared by spark plasma sintering. Ferritic 434L and austenitic 316L stainless steel powders are premixed in a 50:50 weight ratio and added with 3-9 wt.% TiC. The compacts are sintered in the solid state under vacuum conditions at 1223 K for 5 min. The effects of TiC content on the microstructure, hardness, and corrosion resistance of duplex stainless steel composites fabricated by powder metallurgy are evaluated. The results indicate that the TiC particulates as reinforcements can be distributed homogeneously in the steel matrix. Densification of sintered composites decreases with increasing TiC content. M23C6 carbide precipitates along grain boundary, and its neighboring Cr-Mo-depleted region is formed in the sintered microstructure, which can be eliminated subsequently with appropriate heat treatment. With the addition of TiC, the hardness of duplex stainless steel fabricated by powder metallurgy can be markedly enhanced despite increased porosity in the composites. However, TiC particles increase the corrosion rate and degrade the passivation capability, particularly for the composite with TiC content higher than 6 wt.%. Weakened metallurgical bonding in the composite with high TiC content provides the preferred sites for pitting nucleation and/or dissolution.

  16. Contribution to the study of copper and copper-arsenic archaeo-metallurgy using light element analysis and experimental fusion

    International Nuclear Information System (INIS)

    Papillon, F.

    1997-01-01

    The objective of this study is to try a direct reconstruction from ancient artefacts of the elaboration technology used in the dawning copper metallurgy. This word is based on both the light elements analysis and the carry out of the principles of physical metallurgy. However the study of an archaeological artefact necessitates the use of non destructive methods. A main aspect of this work consists in developing the most adequate metallographic technique and the methods for the determination of oxygen and carbon by ion beam analysis. Additionally experimental melting of copper and copper arsenic alloys were carried out in laboratory, under various temperature and atmosphere conditions, and 'on the field' in Archeodrome de Beaune, in order to reconstruct part of the prehistorical craftsmanship. The results of measurement are consistent with our general knowledge of oxido-reduction phenomena and the behaviour of copper and copper arsenic alloys s in agreement with the prediction of thermodynamics. The nuclear analysis of three ancient artefacts showed that the oxygen and carbon contents were closer to those of the Archeodrome than those of the laboratory. Further studies of the field should consider all parameters controlling the physical-chemistry of charcoal fire. (author)

  17. Effect of sintering conditions on the microstructural and mechanical characteristics of porous magnesium materials prepared by powder metallurgy.

    Science.gov (United States)

    Čapek, Jaroslav; Vojtěch, Dalibor

    2014-02-01

    There has recently been an increased demand for porous magnesium materials in many applications, especially in the medical field. Powder metallurgy appears to be a promising approach for the preparation of such materials. Many works have dealt with the preparation of porous magnesium; however, the effect of sintering conditions on material properties has rarely been investigated. In this work, we investigated porous magnesium samples that were prepared by powder metallurgy using ammonium bicarbonate spacer particles. The effects of the purity of the argon atmosphere and sintering time on the microstructure (SEM, EDX and XRD) and mechanical behaviour (universal loading machine and Vickers hardness tester) of porous magnesium were studied. The porosities of the prepared samples ranged from 24 to 29 vol.% depending on the sintering conditions. The purity of atmosphere played a significant role when the sintering time exceeded 6h. Under a gettered argon atmosphere, a prolonged sintering time enhanced diffusion connections between magnesium particles and improved the mechanical properties of the samples, whereas under a technical argon atmosphere, oxidation at the particle surfaces caused deterioration in the mechanical properties of the samples. These results suggest that a refined atmosphere is required to improve the mechanical properties of porous magnesium. © 2013.

  18. Comprehensive waste characterization and organic pollution co-occurrence in a Hg and As mining and metallurgy brownfield.

    Science.gov (United States)

    Gallego, J R; Esquinas, N; Rodríguez-Valdés, E; Menéndez-Aguado, J M; Sierra, C

    2015-12-30

    The abandonment of Hg-As mining and metallurgy sites, together with long-term weathering, can dramatically degrade the environment. In this work it is exemplified the complex legacy of contamination that afflicts Hg-As brownfields through the detailed study of a paradigmatic site. Firstly, an in-depth study of the former industrial process was performed to identify sources of different types of waste. Subsequently, the composition and reactivity of As- and Hg-rich wastes (calcines, As-rich soot, stupp, and flue dust) was analyzed by means of multielemental analysis, mineralogical characterization (X-ray diffraction, electronic, and optical microscopy, microbrobe), chemical speciation, and sequential extractions. As-rich soot in the form of arsenolite, a relatively mobile by-product of the pyrometallurgical process, and stupp, a residue originated in the former condensing system, were determined to be the main risk at the site. In addition, the screening of organic pollution was also aimed, as shown by the outcome of benzo(a) pyrene and other PAHs, and by the identification of unexpected Hg organo-compounds (phenylmercury propionate). The approach followed unravels evidence from waste from the mining and metallurgy industry that may be present in other similar sites, and identifies unexpected contaminants overlooked by conventional analyses. Copyright © 2015 Elsevier B.V. All rights reserved.

  19. Advanced methods for fabrication of PHWR and LMFBR fuels

    International Nuclear Information System (INIS)

    Ganguly, C.

    1988-01-01

    For self-reliance in nuclear power, the Department of Atomic Energy (DAE), India is pursuing two specific reactor systems, namely the pressurised heavy water reactors (PHWR) and the liquid metal cooled fast breeder reactors (LMFBR). The reference fuel for PHWR is zircaloy-4 clad high density (≤ 96 per cent T.D.) natural UO 2 pellet-pins. The advanced PHWR fuels are UO 2 -PuO 2 (≤ 2 per cent), ThO 2 -PuO 2 (≤ 4 per cent) and ThO 2 -U 233 O 2 (≤ 2 per cent). Similarly, low density (≤ 85 per cent T.D.) (UPu)O 2 pellets clad in SS 316 or D9 is the reference fuel for the first generation of prototype and commercial LMFBRs all over the world. However, (UPu)C and (UPu)N are considered as advanced fuels for LMFBRs mainly because of their shorter doubling time. The conventional method of fabrication of both high and low density oxide, carbide and nitride fuel pellets starting from UO 2 , PuO 2 and ThO 2 powders is 'powder metallurgy (P/M)'. The P/M route has, however, the disadvantage of generation and handling of fine powder particles of the fuel and the associated problem of 'radiotoxic dust hazard'. The present paper summarises the state-of-the-art of advanced methods of fabrication of oxide, carbide and nitride fuels and highlights the author's experience on sol-gel-microsphere-pelletisation (SGMP) route for preparation of these materials. The SGMP process uses sol gel derived, dust-free and free-flowing microspheres of oxides, carbide or nitride for direct pelletisation and sintering. Fuel pellets of both low and high density, excellent microhomogeneity and controlled 'open' or 'closed' porosity could be fabricated via the SGMP route. (author). 5 tables, 14 figs., 15 refs

  20. Fabrics in Function

    DEFF Research Database (Denmark)

    Bang, Anne Louise

    2007-01-01

    to the establishment of an initial framework for the project it has a focus on how to explore costumers and users emotional experiences with fabrics. The three year research project is based on experimental design research and the textile designer's competences and knowledge. During the research project exploring...... sensing of fabrics in function. It is proposed that tactile and visual sensing of fabrics is a way to investigate and express emotional utility values. The further purpose is to use experiments with repertory grid models as part of the mapping of the entire research project and also as a basis...

  1. The beginning of metallurgy in the southern Levant: a late 6th millennium CalBC copper awl from Tel Tsaf, Israel.

    Science.gov (United States)

    Garfinkel, Yosef; Klimscha, Florian; Shalev, Sariel; Rosenberg, Danny

    2014-01-01

    The beginning of metallurgy in the ancient Near East attracts much attention. The southern Levant, with the rich assemblage of copper artifacts from the Nahal Mishmar cave and the unique gold rings of the Nahal Qanah cave, is regarded as a main center of early metallurgy during the second half of the 5th millennium CalBC. However, a recently discovered copper awl from a Middle Chalcolithic burial at Tel Tsaf, Jordan Valley, Israel, suggests that cast metal technology was introduced to the region as early as the late 6th millennium CalBC. This paper examines the chemical composition of this item and reviews its context. The results indicate that it was exported from a distant source, probably in the Caucasus, and that the location where it was found is indicative of the social status of the buried individual. This rare finding indicates that metallurgy was first diffused [corrected] to the southern Levant through exchange networks and only centuries later involved local productionThis copper awl, the earliest metal artifact found in the southern Levant, indicates that the elaborate Late Chalcolithic metallurgy developed from a more ancient tradition.

  2. [CHEMICAL AIR POLLUTION OF THE OCCUPATIONAL ENVIRONMENT AS A FACTOR FOR PROFESSIONAL RISK FOR WORKERS OF MAIN OCCUPATIONS IN THE COPPER AND NICKEL METALLURGY].

    Science.gov (United States)

    Lipatov, G Ia; Adrianovskiĭ, V I; Gogoleva, O I

    2015-01-01

    There are presented the results of hygienic researches of the harmful substances content in the air of the working area ofthe copper and nickel metallurgy. Sulfur-containing gases (primarily sulfur dioxide), to the effects of which there are exposed workers of drying, smelting, converter conversion, are shown to play a leading role among professional factors.

  3. Construction, fabrication, and installation

    International Nuclear Information System (INIS)

    1992-05-01

    This standard specifies the construction, fabrication, and installation requirements that apply to concrete containment structures of a containment system designated as class containment components, parts and appurtenances for nuclear power plants

  4. Experimental Fabrication Facility

    Data.gov (United States)

    Federal Laboratory Consortium — Provides aviation fabrication support to special operations aircraft residing at Fort Eustis and other bases in the United States. Support is also provided to AATD...

  5. Alloy Fabrication Laboratory

    Data.gov (United States)

    Federal Laboratory Consortium — At NETL’s Alloy Fabrication Facility in Albany, OR, researchers conduct DOE research projects to produce new alloys suited to a variety of applications, from gas...

  6. Nuclear Fabrication Consortium

    Energy Technology Data Exchange (ETDEWEB)

    Levesque, Stephen [EWI, Columbus, OH (United States)

    2013-04-05

    This report summarizes the activities undertaken by EWI while under contract from the Department of Energy (DOE) Office of Nuclear Energy (NE) for the management and operation of the Nuclear Fabrication Consortium (NFC). The NFC was established by EWI to independently develop, evaluate, and deploy fabrication approaches and data that support the re-establishment of the U.S. nuclear industry: ensuring that the supply chain will be competitive on a global stage, enabling more cost-effective and reliable nuclear power in a carbon constrained environment. The NFC provided a forum for member original equipment manufactures (OEM), fabricators, manufacturers, and materials suppliers to effectively engage with each other and rebuild the capacity of this supply chain by : Identifying and removing impediments to the implementation of new construction and fabrication techniques and approaches for nuclear equipment, including system components and nuclear plants. Providing and facilitating detailed scientific-based studies on new approaches and technologies that will have positive impacts on the cost of building of nuclear plants. Analyzing and disseminating information about future nuclear fabrication technologies and how they could impact the North American and the International Nuclear Marketplace. Facilitating dialog and initiate alignment among fabricators, owners, trade associations, and government agencies. Supporting industry in helping to create a larger qualified nuclear supplier network. Acting as an unbiased technology resource to evaluate, develop, and demonstrate new manufacturing technologies. Creating welder and inspector training programs to help enable the necessary workforce for the upcoming construction work. Serving as a focal point for technology, policy, and politically interested parties to share ideas and concepts associated with fabrication across the nuclear industry. The report the objectives and summaries of the Nuclear Fabrication Consortium

  7. Fabricating nuclear components

    International Nuclear Information System (INIS)

    Anon.

    1977-01-01

    Activities of the Nuclear Engineering Division of Vickers Ltd., particularly fabrication of long slim tubular components for power reactors and the construction of irradiation loops and rigs, are outlined. The processes include hydraulic forming for fabrication of various types of tubes and outer cases of fuel transfer buckets, various specialised welding operations including some applications of the TIG process, and induction brazing of specialised assemblies. (U.K.)

  8. Steel, specially for the fabrication of welded structure working under pressure in nuclear installations

    International Nuclear Information System (INIS)

    Dolbenko, E.T.; Astafiev, A.A.; Kark, G.S.

    1981-01-01

    The present invention is in the field of metallurgy. Steels have found an increasing number of applications in mechanical constructions, and notably in the construction of materials for the production of energy and for the fabrication of welded structures operating under pressure at temperatures as high as 450 0 C. A possible application is the pressurized vessels of nuclear facilities. The steels of interest contain carbon, silicon, manganese, nickel, molybdenum, vanadium, aluminium, nitrogen, phosphorus and iron, but are characterized by the fact that they also contain arsenic, tin and calcium. The sum of the weighted percentages of nickel and manganese and the weighted percentage of phosphorous are related as follows: (Ni + Mn) . P [fr

  9. Assessment of heavy metals exposure, noise and thermal safety in the ambiance of a vacuum metallurgy separation system for recycling heavy metals from crushed e-wastes.

    Science.gov (United States)

    Zhan, Lu; Xu, Zhenming

    2014-12-01

    Vacuum metallurgy separation (VMS) is a technically feasible method to recover Pb, Cd and other heavy metals from crushed e-wastes. To further determine the environmental impacts and safety of this method, heavy metals exposure, noise and thermal safety in the ambiance of a vacuum metallurgy separation system are evaluated in this article. The mass concentrations of total suspended particulate (TSP) and PM10 are 0.1503 and 0.0973 mg m(-3) near the facilities. The concentrations of Pb, Cd and Sn in TSP samples are 0.0104, 0.1283 and 0.0961 μg m(-3), respectively. Health risk assessments show that the hazard index of Pb is 3.25 × 10(-1) and that of Cd is 1.09 × 10(-1). Carcinogenic risk of Cd through inhalation is 1.08 × 10(-5). The values of the hazard index and risk indicate that Pb and Cd will not cause non-cancerous effects or carcinogenic risk on workers. The noise sources are mainly the mechanical vacuum pump and the water cooling pump. Both of them have the noise levels below 80 dB (A). The thermal safety assessment shows that the temperatures of the vacuum metallurgy separation system surface are all below 303 K after adopting the circulated water cooling and heat insulation measures. This study provides the environmental information of the vacuum metallurgy separation system, which is of assistance to promote the industrialisation of vacuum metallurgy separation for recovering heavy metals from e-wastes. © The Author(s) 2014.

  10. The physical metallurgy of mechanically-alloyed, dispersion-strengthened Al-Li-Mg and Al-Li-Cu alloys

    Science.gov (United States)

    Gilman, P. S.

    1984-01-01

    Powder processing of Al-Li-Mg and Al-Li-Cu alloys by mechanical alloying (MA) is described, with a discussion of physical and mechanical properties of early experimental alloys of these compositions. The experimental samples were mechanically alloyed in a Szegvari attritor, extruded at 343 and 427 C, and some were solution-treated at 520 and 566 C and naturally, as well as artificially, aged at 170, 190, and 210 C for times of up to 1000 hours. All alloys exhibited maximum hardness after being aged at 170 C; lower hardness corresponds to the solution treatment at 566 C than to that at 520 C. A comparison with ingot metallurgy alloys of the same composition shows the MA material to be stronger and more ductile. It is also noted that properly aged MA alloys can develop a better combination of yield strength and notched toughness at lower alloying levels.

  11. Effects of Temperature and Pressure of Hot Isostatic Pressing on the Grain Structure of Powder Metallurgy Superalloy.

    Science.gov (United States)

    Tan, Liming; He, Guoai; Liu, Feng; Li, Yunping; Jiang, Liang

    2018-02-24

    The microstructure with homogeneously distributed grains and less prior particle boundary (PPB) precipitates is always desired for powder metallurgy superalloys after hot isostatic pressing (HIPping). In this work, we studied the effects of HIPping parameters, temperature and pressure on the grain structure in PM superalloy FGH96, by means of scanning electron microscope (SEM), electron backscatter diffraction (EBSD), transmission electron microscope (TEM) and Time-of-flight secondary ion spectrometry (ToF-SIMS). It was found that temperature and pressure played different roles in controlling PPB precipitation and grain structure during HIPping, the tendency of grain coarsening under high temperature could be inhibited by increasing HIPping pressure which facilitates the recrystallization. In general, relatively high temperature and pressure of HIPping were preferred to obtain an as-HIPped superalloy FGH96 with diminished PPB precipitation and homogeneously refined grains.

  12. Physical Metallurgy of Rene 65, a Next-Generation Cast and Wrought Nickel Superalloy for use in Aero Engine Components

    Science.gov (United States)

    Wessman, Andrew Ezekiel

    Advancements in the design of turbine engines are in large part made possible by advancements in the capability of nickel based superalloys. Greater temperature and stress capabilities in these materials allow for increased operating temperatures and speeds in the engines, which lead to increased fuel efficiency. Early jet engines were built using austenitic stainless steels, and moved to cast and wrought nickel alloys as higher temperatures were required. By the 1970s, the state of the art nickel superalloy was Inconel 718, which is strengthened by the Ni3Nb phase known as gamma double prime. This alloy performs well and is still in heavy use in turbine engines at temperatures up to approximately 650°C (1200°F), but at higher temperatures the main strengthening precipitate phase, gamma', is thermodynamically unstable, resulting in a loss of strength following exposure to high temperature. Further advancements in nickel superalloys generally involved alloys strengthened by the Ni3Al phase known as gamma'. This precipitate is stable at much higher temperatures, but due to compositional segregation in cast and wrought processing, these alloys were processed using powder metallurgy methods, at considerable economic cost. This study will examine the microstructure of a next generation cast and wrought nickel superalloy that can provide increased temperature capability relative to Inconel 718, at lower cost than powder metallurgy superalloys. The alloy chemistry is similar to that of the powder metallurgy superalloy Rene 88DT, with changes to make it better suited for cast and wrought processing and with a different processing route from billet processing through to final part heat treatment. It is a gamma prime strengthened superalloy. The alloy has been recently introduced into service in turbine engines by GE Aviation as the alloy Rene 65, the composition of which is shown below. In this work, the following has been shown: • Rene 65 gamma' precipitate structure

  13. Advanced Mechanical Properties of a Powder Metallurgy Ti-Al-N Alloy Doped with Ultrahigh Nitrogen Concentration

    Science.gov (United States)

    Shen, J.; Chen, B.; Umeda, J.; Kondoh, K.

    2018-03-01

    Titanium and its alloys are recognized for their attractive properties. However, high-performance Ti alloys are often alloyed with rare or noble-metal elements. In the present study, Ti alloys doped with only ubiquitous elements were produced via powder metallurgy. The experimental results showed that pure Ti with 1.5 wt.% AlN incorporated exhibited excellent tensile properties, superior to similarly extruded Ti-6Al-4V. Further analysis revealed that its remarkably advanced strength could primarily be attributed to nitrogen solid-solution strengthening, accounting for nearly 80% of the strength increase of the material. In addition, despite the ultrahigh nitrogen concentration up to 0.809 wt.%, the Ti-1.5AlN sample showed elongation to failure of 10%. This result exceeds the well-known limitation for nitrogen (over 0.45 wt.%) that causes embrittlement of Ti alloys.

  14. Comprehensive waste characterization and organic pollution co-occurrence in a Hg and As mining and metallurgy brownfield

    Energy Technology Data Exchange (ETDEWEB)

    Gallego, J.R., E-mail: jgallego@uniovi.es [Environmental Technology, Biotechnology and Geochemistry Group, C/Gonzalo Gutiérrez Quirós s/n, 33600 Mieres, Asturias (Spain); Esquinas, N.; Rodríguez-Valdés, E.; Menéndez-Aguado, J.M. [Environmental Technology, Biotechnology and Geochemistry Group, C/Gonzalo Gutiérrez Quirós s/n, 33600 Mieres, Asturias (Spain); Sierra, C. [Environmental Technology, Biotechnology and Geochemistry Group, C/Gonzalo Gutiérrez Quirós s/n, 33600 Mieres, Asturias (Spain); Escuela Superior Politécnica del Litoral, Guayaquil (Ecuador)

    2015-12-30

    Highlights: • Complex legacy of contamination afflicts As–Hg brownfields. • As- and Hg-rich waste analyzed in a paradigmatic study site. • Co-ocurrence of a complex speciation of As and Hg, and organic pollution (PAHs). • Arsenolite was determined to be the main source of risk at the site. • Unexpected Hg organo-compounds found. - Abstract: The abandonment of Hg–As mining and metallurgy sites, together with long-term weathering, can dramatically degrade the environment. In this work it is exemplified the complex legacy of contamination that afflicts Hg–As brownfields through the detailed study of a paradigmatic site. Firstly, an in-depth study of the former industrial process was performed to identify sources of different types of waste. Subsequently, the composition and reactivity of As- and Hg-rich wastes (calcines, As-rich soot, stupp, and flue dust) was analyzed by means of multielemental analysis, mineralogical characterization (X-ray diffraction, electronic, and optical microscopy, microbrobe), chemical speciation, and sequential extractions. As-rich soot in the form of arsenolite, a relatively mobile by-product of the pyrometallurgical process, and stupp, a residue originated in the former condensing system, were determined to be the main risk at the site. In addition, the screening of organic pollution was also aimed, as shown by the outcome of benzo(a) pyrene and other PAHs, and by the identification of unexpected Hg organo-compounds (phenylmercury propionate). The approach followed unravels evidence from waste from the mining and metallurgy industry that may be present in other similar sites, and identifies unexpected contaminants overlooked by conventional analyses.

  15. Quelccaya Ice Core Evidence of Widespread Atmospheric Pollution from Colonial Metallurgy after the Spanish Conquest of South America (1532 AD)

    Science.gov (United States)

    Gabrielli, P.; Uglietti, C.; Cooke, C. A.; Thompson, L. G.

    2014-12-01

    A few ice core records recovered from remote arctic regions suggest a widespread impact of toxic trace elements (Pb, Cu, Sb, As and Bi) to the North Hemisphere atmosphere prior to the onset of the Industrial Revolution (1780s-1830s). In the Southern Hemisphere, evidence for preindustrial trace element emissions are, to date, limited to sediment cores recovered from lakes located within the immediate airshed of major metallurgical centers of South America. Thus it remains unresolved whether they could have had a larger scale impact. Here, we present an annually resolved ice core record of anthropogenic trace element deposition from the remote drilling site of the Quelccaya Ice Cap (Peru) that spans 793-1989 AD. During the pre-Inca period (i.e., prior to ~1450 AD) the deposition of trace elements was dominated by the fallout of aeolian dust from the deglaciated margins of the ice cap and of ash from occasional volcanic eruptions. In contrast, the ice core record indicates a clear anthropogenic signal emerging after the onset of large scale colonial mining and metallurgy (1532-1820 AD), ~300 years prior to the Industrial Revolution during the last part of the Little Ice Age. This shift was coincidental with a major technological transition for silver extraction (1572 AD), from lead-based smelting to mercury amalgamation, that initiated a major increase in ore mining and milling that likely resulted in an increase of metallic dust emissions. While atmospheric trace element deposition resulting from colonial metallurgy was certainly much larger than during the pre-Colonial period, trace element fallout during the Colonial era was still several factors lower than during the 20th century, when the construction of the trans-Andean railway and highways promoted a widespread societal and industrial development of South America.

  16. Understanding core conductor fabrics

    International Nuclear Information System (INIS)

    Swenson, D E

    2011-01-01

    ESD Association standard test method ANSI/ESD STM2.1 - Garments (STM2.1), provides electrical resistance test procedures that are applicable for materials and garments that have surface conductive or surface dissipative properties. As has been reported in other papers over the past several years 1 fabrics are now used in many industries for electrostatic control purposes that do not have surface conductive properties and therefore cannot be evaluated using the procedures in STM2.1 2 . A study was conducted to compare surface conductive fabrics with samples of core conductor fibre based fabrics in order to determine differences and similarities with regards to various electrostatic properties. This work will be used to establish a new work item proposal within WG-2, Garments, in the ESD Association Standards Committee in the USA.

  17. MOX Fabrication Isolation Considerations

    Energy Technology Data Exchange (ETDEWEB)

    Eric L. Shaber; Bradley J Schrader

    2005-08-01

    This document provides a technical position on the preferred level of isolation to fabricate demonstration quantities of mixed oxide transmutation fuels. The Advanced Fuel Cycle Initiative should design and construct automated glovebox fabrication lines for this purpose. This level of isolation adequately protects the health and safety of workers and the general public for all mixed oxide (and other transmutation fuel) manufacturing efforts while retaining flexibility, allowing parallel development and setup, and minimizing capital expense. The basis regulations, issues, and advantages/disadvantages of five potential forms of isolation are summarized here as justification for selection of the preferred technical position.

  18. Metals for bone implants. Part 1. Powder metallurgy and implant rendering.

    Science.gov (United States)

    Andani, Mohsen Taheri; Shayesteh Moghaddam, Narges; Haberland, Christoph; Dean, David; Miller, Michael J; Elahinia, Mohammad

    2014-10-01

    New metal alloys and metal fabrication strategies are likely to benefit future skeletal implant strategies. These metals and fabrication strategies were looked at from the point of view of standard-of-care implants for the mandible. These implants are used as part of the treatment for segmental resection due to oropharyngeal cancer, injury or correction of deformity due to pathology or congenital defect. The focus of this two-part review is the issues associated with the failure of existing mandibular implants that are due to mismatched material properties. Potential directions for future research are also studied. To mitigate these issues, the use of low-stiffness metallic alloys has been highlighted. To this end, the development, processing and biocompatibility of superelastic NiTi as well as resorbable magnesium-based alloys are discussed. Additionally, engineered porosity is reviewed as it can be an effective way of matching the stiffness of an implant with the surrounding tissue. These porosities and the overall geometry of the implant can be optimized for strain transduction and with a tailored stiffness profile. Rendering patient-specific, site-specific, morphology-specific and function-specific implants can now be achieved using these and other metals with bone-like material properties by additive manufacturing. The biocompatibility of implants prepared from superelastic and resorbable alloys is also reviewed. Copyright © 2014 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

  19. Fabrication of Turbine Disk Materials by Additive Manufacturing

    Science.gov (United States)

    Sudbrack, Chantal; Bean, Quincy A.; Cooper, Ken; Carter, Robert; Semiatin, S. Lee; Gabb, Tim

    2014-01-01

    Precipitation-strengthened, nickel-based superalloys are widely used in the aerospace and energy industries due to their excellent environmental resistance and outstanding mechanical properties under extreme conditions. Powder-bed additive manufacturing (AM) technologies offer the potential to revolutionize the processing of superalloy turbine components by eliminating the need for extensive inventory or expensive legacy tooling. Like selective laser melting (SLM), electron beam melting (EBM) constructs three-dimensional dense components layer-by-layer by melting and solidification of atomized, pre-alloyed powder feedstock within 50-200 micron layers. While SLM has been more widely used for AM of nickel alloys like 718, EBM offers several distinct advantages, such as less retained residual stress, lower risk of contamination, and faster build rates with multiple-electron-beam configurations. These advantages are particularly attractive for turbine disks, for which excessive residual stress and contamination can shorten disk life during high-temperature operation. In this presentation, we will discuss the feasibility of fabricating disk superalloy components using EBM AM. Originally developed using powder metallurgy forging processing, disk superalloys contain a higher refractory content and precipitate volume fraction than alloy 718, thus making them more prone to thermal cracking during AM. This and other challenges to produce homogeneous builds with desired properties will be presented. In particular, the quality of lab-scale samples fabricated via a design of experiments, in which the beam current, build temperature, and beam velocity were varied, will be summarized. The relationship between processing parameters, microstructure, grain orientation, and mechanical response will be discussed.

  20. Fabrication experience of aluminium clad aluminium matrix dispersion fuels at BARC

    International Nuclear Information System (INIS)

    Ganguly, C.; Hedge, P.W.; Prasad, G.J.

    1995-01-01

    Aluminium clad, aluminium matrix plate type dispersion fuels have been fabricated in BARC in recent years as part of fuel development programme for small non-power research reactors. The present paper describes the flowsheet developed for fabrication of Al-UAl x , Al-U 3 Si 2 and Al-U 3 O 8 fuels at BARC. The Al-20% U alloy fuel for KAMINI neutron radiography reactor was prepared by 'melting and casting' route, followed by picture framing and roll-bonding. For higher 'U' density fuels namely, Al-UAl x , Al-U 3 O 8 and Al-U 3 Si 2 the 'powder metallurgy' route was followed for preparation of fuel meat. The novel features in fabrication route were: addition of Zr for stabilizing UAl 3 phase in Al-20% U alloy; x-ray radiography and microdensitometric scanning of radiographs for location of fuel outline inside fuel element and for confirming homogeneous distribution of fissile atoms; immersion ultrasonic testing for confirming good bonding between mating Al surface of the fuel plate. (author)

  1. Net shape fabrication of stainless-steel micro machine components from metallic powder

    International Nuclear Information System (INIS)

    Imbaby, M; Jiang, K; Chang, I

    2008-01-01

    A fabrication process of the net shape 316-L stainless-steel micro machine components is reported. The fabrication process combines softlithography and powder metallurgy to produce microcomponents of complex geometries of high quality. The process starts with softlithography by producing ultra thick SU-8 master moulds and their negative replicas of polydimethylsiloxane (PDMS). Then stainless-steel slurry is prepared by mixing super fine 316-L steel powder and binder to fill the PDMS moulds. The two binders used in the experiments were Duramax D-3005 and a mixture of B1000 and B1007. The PDMS micro moulds are filled with the metallic slurries and green parts are obtained from de-moulding, before going through de-binding and sintering in forming gas atmosphere. The fabrication steps were repeatedly tested. The resultant micro parts show high quality shape retention which is attributed to the quality of the SU-8 master moulds. The hardness property of the sintered microcomponents was tested with a micro indenter and a 200 g load was applied. The Vickers hardness of the sintered components was found to be about 255, which was higher than 225 of annealed 316L stainless steel and the two binders make little difference on the hardness of the sintered samples

  2. Pigmi mechanical fabrication

    International Nuclear Information System (INIS)

    Hart, V.E.

    1976-01-01

    A prime goal of the mechanical design effort associated with the PIGMI (Pion Generator for Medical Irradiations) program is to investigate new materials and fabrication techniques in an effort to obtain increased machine efficiency and reliability at a reasonable cost. A discussion is given dealing with the modeling program that LASL is pursuing for 450-MHz and 1350-MHz PIGMI development

  3. PIGMI mechanical fabrication

    International Nuclear Information System (INIS)

    Hart, V.E.

    1976-01-01

    A prime goal of the mechanical design effort associated with the PIGMI (Pion Generator for Medical Irradiations) program is to investigate new materials and fabrication techniques in an effort to obtain increased machine efficiency and reliability at a reasonable cost. The following discussion deals with the modeling program that LASL is pursuing for 450-MHz and 1350-MHz PIGMI development. (author)

  4. Fabrication activity for nanophotonics

    DEFF Research Database (Denmark)

    Malureanu, Radu; Chung, Il-Sug; Carletti, Luca

    We present the fabrication and characterization of new structures and materials to be used in nanophotonics. The first structure presented is a fractal metallic metasurface designed to be used as a high-sensitivity sensor for 810nm wavelength. A second structure is a high index contrast grating...

  5. Titanium dental copings prepared by a powder metallurgy method: a preliminary report.

    Science.gov (United States)

    Eriksson, Mikael; Andersson, Matts; Carlström, Elis

    2004-01-01

    The purpose of this study was to determine if the Procera pressed-powder method can be used to fabricate titanium copings. Commercially pure titanium powder was used to prepare the copings. The powder was pressed onto an enlarged tooth preparation die of aluminum using cold isostatic pressing. The outer shape of the coping was formed using a Procera milling machine, and the copings were vacuum sintered. Titanium copings could be prepared using this method. The density of the sintered copings reached 97% to 99%+ of theoretic density, and the copings showed ductile behavior after sintering. Enlarging the tooth preparation die to compensate for the sintering shrinkage could optimize the final size of the copings. Ductile and dense titanium dental copings can be produced with powder-metal processing using cold isostatic pressing, followed by milling and sintering to final shape. The forming technique has, if properly optimized, a potential of becoming a more cost-efficient production method than spark erosion.

  6. Preparation and properties of Cobalt-based soft magnetic material prepared by novel powder metallurgy

    Energy Technology Data Exchange (ETDEWEB)

    Srivastava, Yogesh, E-mail: 123209001_yogesh@manit.ac.in; Srivastava, Sanjay

    2017-02-01

    The present work deals with the development of nanocrystalline 60Co–26Fe–14Al (wt%) soft magnetic materials via mechanical milling of elemental powders. The evolution of solid solution during milling proceeded with continuous decrease in atomic order and the crystallite size, and an introduction of internal strain and dislocations. The milling-induced lattice defects, crystallite size reduction, and atomic disorder exhibited a decrease in saturation magnetization, remanence magnetization, squareness ratio, and blocking temperature with increasing milling time. It has been demonstrated that, at subzero temperatures, the magnetization decreases with increasing temperature due to the development of an effective anisotropy caused by an evolution of canted spin structure owing to the introduction of lattice defects during milling. - Highlights: • Co-based HA have been fabricated by mechanical alloying. • The effect of milling time was investigated. • The saturation magnetization can be reached up to 140.79 emu/g.

  7. Assessment Of Usability Of Molten Salt Mixtures In Metallurgy Of Aluminum Alloys And Recycling Of Composite Materials Based On The Matrix Of Al Alloys

    Directory of Open Access Journals (Sweden)

    Jackowski J.

    2015-09-01

    Full Text Available Effectiveness of the slags used in metallurgy of aluminum alloys and in recycling of composite materials containing these alloys depends on their surface properties at the phase boundaries they are in contact with. An index of surface properties of molten mixtures of slag-forming salts has been formulated. Its calculated values are compared with measured results of surface tension (liquid – atmosphere and interfacial tension (liquid – liquid in the considered systems. It was found that the index can be helpful for purposes of proper choice of the mixtures of slag-forming salts used both in Al alloys metallurgy and in recycling of composite materials based on the matrix of Al alloys.

  8. Recent applications of PIXE spectrometry in archaeology. Pt. 1; Observations on the early development of copper metallurgy in the Old World

    Energy Technology Data Exchange (ETDEWEB)

    Fleming, S.J. (MASCA, Univ. Museum, Univ. Pennsylvania, Philadelphia, PA (United States)); Swann, C.P. (Bartol Research Inst., Univ. Delaware, Newark, DE (United States))

    1993-04-01

    The early development of copper metallurgy can be characterized by three steps of innovation: (i) Exploitation of native copper resources for simple tool-making as early as the 7th millennium B.C. in the Near East; (ii) the recovery of copper metal from minerals such as malachite, by smelting, during the 5th millennium B.C., both in the Near East and in eastern Europe; and (iii) the deliberate alloying of copper and tin, to make bronze, circa 2800 B.C. in Mesopotamia (modern Iraq). This paper reviews the technological aspects associated the first two of these steps, comparing compositional patterns (as determined by PIXE spectrometry) for the copper metallurgy of various regions including the Middle Danube basin, the Tigris basin, and the Iranian Plateau. (orig.).

  9. Status report, canister fabrication

    Energy Technology Data Exchange (ETDEWEB)

    Andersson, Claes-Goeran; Eriksson, Peter; Westman, Marika [Swedish Nuclear Fuel and Waste Management Co., Stockholm (Sweden); Emilsson, Goeran [CSM Materialteknik AB, Linkoeping (Sweden)

    2004-06-01

    The report gives an account of the development of material and fabrication technology for copper canisters with cast inserts during the period from 2000 until the start of 2004. The engineering design of the canister and the choice of materials in the constituent components described in previous status reports have not been significantly changed. In the reference canister, the thickness of the copper shell is 50 mm. Fabrication of individual components with a thinner copper thickness is done for the purpose of gaining experience and evaluating fabrication and inspection methods for such canisters. As a part of the development of cast inserts, computer simulations of the casting processes and techniques used at the foundries have been performed for the purpose of optimizing the material properties. These properties have been evaluated by extensive tensile testing and metallographic inspection of test material taken from discs cut at different points along the length of the inserts. The testing results exhibit a relatively large spread. Low elongation values in certain tensile test specimens are due to the presence of poorly formed graphite, porosities, slag or other casting defects. It is concluded in the report that it will not be possible to avoid some presence of observed defects in castings of this size. In the deep repository, the inserts will be exposed to compressive loading and the observed defects are not critical for strength. An analysis of the strength of the inserts and formulation of relevant material requirements must be based on a statistical approach with probabilistic calculations. This work has been initiated and will be concluded during 2004. An initial verifying compression test of a canister in an isostatic press has indicated considerable overstrength in the structure. Seamless copper tubes are fabricated by means of three methods: extrusion, pierce and draw processing, and forging. It can be concluded that extrusion tests have revealed a

  10. The competitiveness of metallurgy and metal products industry in Spain; La competitividad de las industrias metalurgica y de productos metalicos en Espana

    Energy Technology Data Exchange (ETDEWEB)

    Mateos Torres, C.

    2012-07-01

    This article analyzes the competitiveness of metallurgy and manufacture of metal products sectors, in which the Industrial Observatory of the Metal Sector has studied the key factors of innovation for competitiveness. It includes a reference to the competitive situation of the Spanish iron and steel industry. Furthermore, the investments carried out by both sectors under the Competitiveness Promotion Programme for Strategic Industrial Sectors during the years 2009-2011 are analyzed. (Author)

  11. A Model for Converting Dilatometric Strain Measurements to the Fraction of Phase Formed during the Transformation of Austenite to Martensite in Powder Metallurgy Steels

    Science.gov (United States)

    Warke, Virendra S.; Sisson, Richard D.; Makhlouf, Makhlouf M.

    2009-03-01

    A model is developed to allow converting dilatometric strains that occur during the continuous cooling transformation (CCT) of austenite to martensite to volume fraction martensite formed in powder metallurgy steels. Unlike existing models, this model can accurately account for the observed decrease in the measured transformation strain with increased porosity. As a demonstration, the model is used to accurately calculate the volume fraction of martensite formed during the CCT of austenite to martensite in FL-4605 PM steel.

  12. Estimation and characterization of PCDD/Fs, dl-PCBs, PCNs, HxCBz and PeCBz emissions from magnesium metallurgy facilities in China.

    Science.gov (United States)

    Nie, Zhiqiang; Zheng, Minghui; Liu, Wenbin; Zhang, Bing; Liu, Guorui; Su, Guijin; Lv, Pu; Xiao, Ke

    2011-12-01

    Magnesium production is considered to be one potential source of unintentional persistent organic pollutants (unintentional POPs). However, studies on the emissions of unintentional POPs from magnesium metallurgy are still lacking. Emissions of unintentional POPs, such as polychlorinated dibenzo-p-dioxins/dibenzofurans (PCDD/Fs), dioxin-like polychlorinated biphenyls (dl-PCBs), polychlorinated naphthalenes (PCNs), hexachlorobenzene (HxCBz) and pentachlorobenzene (PeCBz) are covered under the Stockholm Convention. In this study, these emissions were investigated through a magnesium smelting process. Stack gas and fly ash samples from a typical magnesium plant in China were collected and analyzed to estimate the emissions of unintentional POPs from magnesium metallurgy. Emissions factors of 412 ng TEQ t(-1) for PCDD/Fs, 18.6 ng TEQ t(-1) for dl-PCBs, 3329 μg t(-1) for PCNs, 820 μg t(-1) for HxCBz, and 1326 μg t(-1) for PeCBz were obtained in 2009. Annual emissions from magnesium metallurgy in China were estimated to be 0.46 g WHO-TEQ for PCDD/Fs and dl-PCBs, 1651 g for PCNs, 403 g for HxCBz and 653 g for PeCBz, respectively. Copyright © 2011 Elsevier Ltd. All rights reserved.

  13. True and intentionally fabricated memories

    OpenAIRE

    Justice, L.V.; Morrison, C.M.; Conway, M. A.

    2012-01-01

    The aim of the experiment reported here was to investigate the processes underlying the construction of truthful and deliberately fabricated memories. Properties of memories created to be intentionally false - fabricated memories - were compared to properties of memories believed to be true - true memories. Participants recalled and then wrote or spoke true memories and fabricated memories of everyday events. It was found that true memories were reliably more vivid than fabricated memories an...

  14. Fabrication of Nanochannels

    Directory of Open Access Journals (Sweden)

    Yuqi Zhang

    2015-09-01

    Full Text Available Nature has inspired the fabrication of intelligent devices to meet the needs of the advanced community and better understand the imitation of biology. As a biomimetic nanodevice, nanochannels/nanopores aroused increasing interest because of their potential applications in nanofluidic fields. In this review, we have summarized some recent results mainly focused on the design and fabrication of one-dimensional nanochannels, which can be made of many materials, including polymers, inorganics, biotic materials, and composite materials. These nanochannels have some properties similar to biological channels, such as selectivity, voltage-dependent current fluctuations, ionic rectification current and ionic gating, etc. Therefore, they show great potential for the fields of biosensing, filtration, and energy conversions. These advances can not only help people to understand the living processes in nature, but also inspire scientists to develop novel nanodevices with better performance for mankind.

  15. Automated breeder fuel fabrication

    International Nuclear Information System (INIS)

    Goldmann, L.H.; Frederickson, J.R.

    1983-01-01

    The objective of the Secure Automated Fabrication (SAF) Project is to develop remotely operated equipment for the processing and manufacturing of breeder reactor fuel pins. The SAF line will be installed in the Fuels and Materials Examination Facility (FMEF). The FMEF is presently under construction at the Department of Energy's (DOE) Hanford site near Richland, Washington, and is operated by the Westinghouse Hanford Company (WHC). The fabrication and support systems of the SAF line are designed for computer-controlled operation from a centralized control room. Remote and automated fuel fabriction operations will result in: reduced radiation exposure to workers; enhanced safeguards; improved product quality; near real-time accountability, and increased productivity. The present schedule calls for installation of SAF line equipment in the FMEF beginning in 1984, with qualifying runs starting in 1986 and production commencing in 1987. 5 figures

  16. Metallurgical aspects of welding. Ferrous and nonferrous materials. 4. new rev. ed.; Die Metallurgie des Schweissens. Eisenwerkstoffe - nichteisenmetallische Werkstoffe

    Energy Technology Data Exchange (ETDEWEB)

    Schulze, Guenter

    2010-07-01

    This is the fourth edition of the standard work on welding metallurgy. The various problems of ferrous and nonferrous materials in the welding process are presented in great detail. In order to prevent corrosion of welded constructions, metallurgical properties and problems of all important technical materials are discussed, i.e. alloyed and unalloyed steels, cast iron materials, and the most relevant nonferrous materials. At the end of each chapter, the interested reader will find exercises for self-studies. Some of these can be solved using the material presented in the book while others are intended for deepening and further training. Easy examples (with solutions) are found all over the book; they are helpful because they provide information on underlying mechanisms and interdependences that are not obvious at first glance. The information was adapted to new EURO standards and international standards (up to March 2009) as far as these are relevant to Germany. New information is provided, e.g., on new steel standards (constructional steels according to DIN EN 10025), heat-treatable steels according to DIN EN 10025-6 and DIN EN 10083, high-alloy steels according to DIN EN 10088, and filler materials for steel welding according to DIN EN ISO 2560. The systematics of the ''law of cohabitation'' was applied to welding engineering for the first time here. (orig.) [German] Das in vierter Auflage erscheinende Buch widmet sich der Schweissmetallurgie mit ihren Besonderheiten. Die vielfaeltigen Probleme der Eisenwerkstoffe und der nichteisenmetallischen Werkstoffe bei ihrer schweisstechnischen Verarbeitung werden ausfuehrlich dargestellt. Um Korrosionsschaeden an geschweissten Konstruktionen vorzubeugen, wird die Metallurgie aller technisch bedeutsamen Werkstoffe, wie unlegierte und legierte Staehle, Eisen-Gusswerkstoffe, die wichtigsten NE-Metalle, ausfuehrlich besprochen. An den Kapitelenden findet der interessierte Leser Aufgaben, von denen ein

  17. Intentionally fabricated autobiographical memories

    OpenAIRE

    Justice, LV; Morrison, CM; Conway, MA

    2017-01-01

    Participants generated both autobiographical memories (AMs) that they believed to be true and intentionally fabricated autobiographical memories (IFAMs). Memories were constructed while a concurrent memory load (random 8-digit sequence) was held in mind or while there was no concurrent load. Amount and accuracy of recall of the concurrent memory load was reliably poorer following generation of IFAMs than following generation of AMs. There was no reliable effect of load on memory generation ti...

  18. Fabrication of nuclear fuel

    International Nuclear Information System (INIS)

    Ion, S.E.; Watson, R.H.; Loch, E.P.

    1989-01-01

    Commercial nuclear fuel fabrication is focused on providing quality products. Throughout manufacturing attention is placed on the precise control of processes, procedures and tooling to reduce product variability. This paper describes the processes used to manufacture fuel for the advanced gas cooled reactor, light water reactor, fast breeder reactor and Magnox reactor systems at the BNFL, Springfields, and Westinghouse Columbia, USA, facilities. It covers the chemical purification and conversion stages of fuel production before describing the fabrication of both oxide and metallic fuel and gives a general overview of the technology used. Although the principles of fuel fabrication in terms of providing a cladding designed to be the primary envelope to encase the fuel are similar for each system, there are detailed differences in manufacturing route and cladding type which arise from differing reactor requirements. These, together with developments made in response to customer needs, are reviewed and the need to maintain a high purity reliable product with low variability at all stages in manufacture is emphasized throughout. (author)

  19. Advanced fuel fabrication

    International Nuclear Information System (INIS)

    Bernard, H.

    1989-01-01

    This paper deals with the fabrication of advanced fuels, such as mixed oxides for Pressurized Water Reactors or mixed nitrides for Fast Breeder Reactors. Although an extensive production experience exists for the mixed oxides used in the FBR, important work is still needed to improve the theoretical and technical knowledge of the production route which will be introduced in the future European facility, named Melox, at Marcoule. Recently, the feasibility of nitride fuel fabrication in existing commercial oxide facilities was demonstrated in France. The process, based on carbothermic reduction of oxides with subsequent comminution of the reaction product, cold pressing and sintering provides (U, Pu)N pellets with characteristics suitable for irradiation testing. Two experiments named NIMPHE 1 and 2 fabricated in collaboration with ITU, Karlsruhe, involve 16 nitride and 2 carbide pins, operating at a linear power of 45 and 73 kW/m with a smear density of 75-80% TD and a high burn-up target of 15 at%. These experiments are currently being irradiated in Phenix, at Marcoule. (orig.)

  20. Ultrafine-grained porous titanium and porous titanium/magnesium composites fabricated by space holder-enabled severe plastic deformation

    Energy Technology Data Exchange (ETDEWEB)

    Qi, Yuanshen, E-mail: yuanshen.qi@monash.edu [Centre for Advanced Hybrid Materials, Department of Materials Engineering, Monash University, Clayton, Victoria 3800 (Australia); Contreras, Karla G. [Monash Institute of Medical Engineering, Faculty of Engineering, Monash University, Clayton, Victoria 3800 (Australia); Jung, Hyun-Do [Liquid Processing & Casting Technology R& D Group, Korea Institute of Industrial Technology, Incheon 406-840 (Korea, Republic of); Department of Materials Science and Engineering, Seoul National University, Seoul 151-742 (Korea, Republic of); Kim, Hyoun-Ee [Department of Materials Science and Engineering, Seoul National University, Seoul 151-742 (Korea, Republic of); Advanced Institutes of Convergence Technology, Seoul National University, Gwanggyo, Yeongtong-gu, Suwon-si, Gyeonggi-do 443-270 (Korea, Republic of); Lapovok, Rimma [Centre for Advanced Hybrid Materials, Department of Materials Engineering, Monash University, Clayton, Victoria 3800 (Australia); Estrin, Yuri, E-mail: yuri.estrin@monash.edu [Centre for Advanced Hybrid Materials, Department of Materials Engineering, Monash University, Clayton, Victoria 3800 (Australia); Laboratory of Hybrid Nanostructured Materials, NUST MISiS, Moscow 119490 (Russian Federation)

    2016-02-01

    Compaction of powders by equal channel angular pressing (ECAP) using a novel space holder method was employed to fabricate metallic scaffolds with tuneable porosity. Porous Ti and Ti/Mg composites with 60% and 50% percolating porosity were fabricated using powder blends with two kinds of sacrificial space holders. The high compressive strength and good ductility of porous Ti and porous Ti/Mg obtained in this way are believed to be associated with the ultrafine grain structure of the pore walls. To understand this, a detailed electron microscopy investigation was employed to analyse the interface between Ti/Ti and Ti/Mg particles, the grain structures in Ti particles and the topography of pore surfaces. It was found that using the proposed compaction method, high quality bonding between particles was obtained. Comparing with other powder metallurgy methods to fabricate Ti with an open porous structure, where thermal energy supplied by a laser beam or high temperature sintering is essential, the ECAP process conducted at a relatively low temperature of 400 °C was shown to produce unique properties. - Highlights: • Porous Ti and porous Ti/Mg composite scaffolds were fabricated successfully. • Space holder-enabled severe plastic deformation was first used in this application. • Silicon particles as sacrificial space holders were used for the first time. • Ultrafine-grained microstructure and good bonding between particles were obtained. • Good preosteoblast cell response to as-manufactured porous Ti was achieved.

  1. Ultrafine-grained porous titanium and porous titanium/magnesium composites fabricated by space holder-enabled severe plastic deformation

    International Nuclear Information System (INIS)

    Qi, Yuanshen; Contreras, Karla G.; Jung, Hyun-Do; Kim, Hyoun-Ee; Lapovok, Rimma; Estrin, Yuri

    2016-01-01

    Compaction of powders by equal channel angular pressing (ECAP) using a novel space holder method was employed to fabricate metallic scaffolds with tuneable porosity. Porous Ti and Ti/Mg composites with 60% and 50% percolating porosity were fabricated using powder blends with two kinds of sacrificial space holders. The high compressive strength and good ductility of porous Ti and porous Ti/Mg obtained in this way are believed to be associated with the ultrafine grain structure of the pore walls. To understand this, a detailed electron microscopy investigation was employed to analyse the interface between Ti/Ti and Ti/Mg particles, the grain structures in Ti particles and the topography of pore surfaces. It was found that using the proposed compaction method, high quality bonding between particles was obtained. Comparing with other powder metallurgy methods to fabricate Ti with an open porous structure, where thermal energy supplied by a laser beam or high temperature sintering is essential, the ECAP process conducted at a relatively low temperature of 400 °C was shown to produce unique properties. - Highlights: • Porous Ti and porous Ti/Mg composite scaffolds were fabricated successfully. • Space holder-enabled severe plastic deformation was first used in this application. • Silicon particles as sacrificial space holders were used for the first time. • Ultrafine-grained microstructure and good bonding between particles were obtained. • Good preosteoblast cell response to as-manufactured porous Ti was achieved.

  2. High Performance MG-System Alloys For Weight Saving Applications: First Year Results From The Green Metallurgy EU Project

    Science.gov (United States)

    D'Errico, Fabrizio; Plaza, Gerardo Garces; Hofer, Markus; Kim, Shae K.

    The GREEN METALLURGY Project, a LIFE+ project co-financed by the EU Commission, has just concluded its first year. The Project seeks to set manufacturing processes at a pre-industrial scale for nanostructured-based high-performance Mg-Zn(Y) magnesium alloys. The Project's goal is the reduction of specific energy consumed and the overall carbon-footprint produced in the cradle-to-exit gate phases. Preliminary results addressed potentialities of the upstream manufacturing process pathway. Two Mg-Zn(Y) system alloys with rapid solidifying powders have been produced and directly extruded for 100% densification. Examination of the mechanical properties showed that such materials exhibit strength and elongation comparable to several high performing aluminum alloys; 390 MPa and 440 MPa for the average UTS for two different system alloys, and 10% and 15% elongations for two system alloys. These results, together with the low-environmental impact targeted, make these novel Mg alloys competitive as lightweight high-performance materials for automotive components.

  3. Phase evolution, mechanical and corrosion behavior of Fe(100-x) Ni(x) alloys synthesized by powder metallurgy

    Science.gov (United States)

    Singh, Neera; Parkash, Om; Kumar, Devendra

    2018-03-01

    In the present investigation, Fe(100-x) Ni(x) alloys (x = 10, 20, 30, 40 and 50 wt%) were synthesized through the evolution of γ-taenite and α-kamacite phases by powder metallurgy route using commercially available Fe and Ni powders. Mechanically mixed powders of Fe and Ni were compacted at room temperature and sintered at three different temperatures 1000, 1200 and 1250 °C for 1 h. Both Ni concentration and sintering temperature have shown a strong impact on the phase formation, tribological and electrochemical behavior. Micro structural study has shown the formation of taenite (γ-Fe,Ni) and kamacite (α-Fe,Ni) phases in the sintered specimens. An increase in Ni fraction resulted in formation of more taenite which reduces hardness and wear resistance of specimens. Increasing the sintering temperature decreased the defect concentration with enhanced taenite formation, aiding to higher densification. Taenite formed completely in Fe50Ni50 after sintering at 1250 °C. Tribological test revealed the maximum wear resistance for Fe70Ni30 specimen due to the presence of both kamacite and taenite in significant proportions. The formation of taenite as well as the decrease in defect concentration improves the corrosion resistance of the specimens significantly in 1M HCl solution. A maximum corrosion protection efficiency of around ∼87% was achieved in acidic medium for Fe50Ni50, sintered at 1250 °C.

  4. Metallurgy and mechanical properties variation with heat input,during dissimilar metal welding between stainless and carbon steel

    Science.gov (United States)

    Ramdan, RD; Koswara, AL; Surasno; Wirawan, R.; Faturohman, F.; Widyanto, B.; Suratman, R.

    2018-02-01

    The present research focus on the metallurgy and mechanical aspect of dissimilar metal welding.One of the common parameters that significantly contribute to the metallurgical aspect on the metal during welding is heat input. Regarding this point, in the present research, voltage, current and the welding speed has been varied in order to observe the effect of heat input on the metallurgical and mechanical aspect of both welded metals. Welding was conducted by Gas Metal Arc Welding (GMAW) on stainless and carbon steel with filler metal of ER 309. After welding, hardness test (micro-Vickers), tensile test, macro and micro-structure characterization and Energy Dispersive Spectroscopy (EDS) characterization were performed. It was observed no brittle martensite observed at HAZ of carbon steel, whereas sensitization was observed at the HAZ of stainless steel for all heat input variation at the present research. Generally, both HAZ at carbon steel and stainless steel did not affect tensile test result, however the formation of chromium carbide at the grain boundary of HAZ structure (sensitization) of stainless steel, indicate that better process and control of welding is required for dissimilar metal welding, especially to overcome this issue.

  5. Microstructure and mechanical properties of a new group of nanocrystalline medical-grade stainless steels prepared by powder metallurgy

    International Nuclear Information System (INIS)

    Javanbakht, M.; Hadianfard, M.J.; Salahinejad, E.

    2015-01-01

    Highlights: • This paper focuses on the structure and mechanical properties of PM alloys. • A eutectic Mn–Si alloy sintering aid was successfully used. • Mechanical properties were improved by adding the sintering aid. - Abstract: This paper focuses on the structure and mechanical properties of powder metallurgy stainless steels (Fe–Cr–Mn–Mo–Si–N–C) developed for biomedical applications. The samples were prepared by mechanical alloying and subsequent liquid-phase sintering with a eutectic Mn–Si alloy additive. By changing the sintering aid content, the pore configuration, compressive strengths, and impact properties of the samples were assessed. The Rietveld X-ray diffraction analysis showed after sintering at 1050 °C for 60 min followed by water-quenching, a nanocrystalline austenitic structure was formed in the material. According to the mechanical experiments, by increasing the additive content from 0 wt% to 6 wt%, sintering densification, yield stress, compression strength, and absorbed impact energy were improved, where spoiling occurred when adding 8 wt% additive. Also, as realized from the impact fracture surface features, despite the presence of some unmelted additive particles, the role of the pore elimination in toughness prevailed over that of these particles

  6. Histomorphologic evaluation of Ti-13Nb-13Zr alloys processed via powder metallurgy. A study in rabbits

    International Nuclear Information System (INIS)

    Bottino, M.C.; Coelho, P.G.; Yoshimoto, M.; Koenig, B.; Henriques, V.A.R.; Bressiani, A.H.A.; Bressiani, J.C.

    2008-01-01

    This study presents the in-vivo evaluation of Ti-13Nb-13Zr alloy implants obtained by the hydride route via powder metallurgy. The cylindrical implants were processed at different sintering and holding times. The implants' were characterized for density, microstructure (SEM), crystalline phases (XRD), and bulk (EDS) and surface composition (XPS). The implants were then sterilized and surgically placed in the central region of the rabbit's tibiae. Two double fluorescent markers were applied at 2 and 3 weeks, and 6 and 7 weeks after implantation. After an 8-week healing period, the implants were retrieved, non-decalcified section processed, and evaluated by electron, UV light (fluorescent labeling), and light microscopy (toluidine blue). BSE-SEM showed close contact between bone and implants. Fluorescent labeling assessment showed high bone activity levels at regions close to the implant surface. Toluidine blue staining revealed regions comprising osteoblasts at regions of newly forming/formed bone close to the implant surface. The results obtained in this study support biocompatible and osseoconductive properties of Ti-13Nb-13Zr processed through the hydride powder route

  7. Histomorphologic evaluation of Ti-13Nb-13Zr alloys processed via powder metallurgy. A study in rabbits

    Energy Technology Data Exchange (ETDEWEB)

    Bottino, M.C. [Department of Materials Science and Engineering, University of Alabama at Birmingham, BEC 254 1530 3rd Avenue South, Birmingham, AL, 35294 (United States); Coelho, P.G. [Department of Biomaterials and Biomimetics, New York University, College of Dentistry, 345 East 24th Street, Room 804S, New York, NY, 10100 (United States)], E-mail: pgcoelho@nyu.edu; Yoshimoto, M. [Materials Science and Technology Center, Institute for Energy and Nuclear Research, Av. Prof. Lineu Prestes, 2242, Sao Paulo, SP, 05508-000 (Brazil); Koenig, B. [Department of Anatomy, Institute of Biomedical Sciences, University of Sao Paulo (ICB-USP) Av. Prof. Lineu Prestes, 2415, Sao Paulo, SP, 05508-900 (Brazil); Henriques, V.A.R. [Materials Division (AMR/IAE), CTA Brazilian Aerospace Technical Center, Sao Jose dos Campos, SP, 12228-904 (Brazil); Bressiani, A.H.A.; Bressiani, J.C. [Materials Science and Technology Center, Institute for Energy and Nuclear Research, Av. Prof. Lineu Prestes, 2242, Sao Paulo, SP, 05508-000 (Brazil)

    2008-03-10

    This study presents the in-vivo evaluation of Ti-13Nb-13Zr alloy implants obtained by the hydride route via powder metallurgy. The cylindrical implants were processed at different sintering and holding times. The implants' were characterized for density, microstructure (SEM), crystalline phases (XRD), and bulk (EDS) and surface composition (XPS). The implants were then sterilized and surgically placed in the central region of the rabbit's tibiae. Two double fluorescent markers were applied at 2 and 3 weeks, and 6 and 7 weeks after implantation. After an 8-week healing period, the implants were retrieved, non-decalcified section processed, and evaluated by electron, UV light (fluorescent labeling), and light microscopy (toluidine blue). BSE-SEM showed close contact between bone and implants. Fluorescent labeling assessment showed high bone activity levels at regions close to the implant surface. Toluidine blue staining revealed regions comprising osteoblasts at regions of newly forming/formed bone close to the implant surface. The results obtained in this study support biocompatible and osseoconductive properties of Ti-13Nb-13Zr processed through the hydride powder route.

  8. Effect of high energy milling time of the aluminum bronze alloy obtained by powder metallurgy with niobium carbide addition

    Energy Technology Data Exchange (ETDEWEB)

    Dias, Alexandre Nogueira Ottoboni; Silva, Aline da; Rodrigues, Carlos Alberto; Melo, Mirian de Lourdes Noronha Motta; Rodrigues, Geovani; Silva, Gilbert, E-mail: aottoboni@yahoo.com.br [Universidade Federal de Itajuba (UNIFEI), Itajuba, MG (Brazil)

    2017-05-15

    The aluminum bronze alloy is part of a class of highly reliable materials due to high mechanical strength and corrosion resistance being used in the aerospace and shipbuilding industry. It's machined to produce parts and after its use cycle, it's discarded, but third process is considered expensive and besides not being correct for environment reasons. Thus, reusing this material through the powder metallurgy (PM) route is considered advantageous. The aluminum bronze chips were submitted to high energy ball milling process with 3% of niobium carbide (NbC) addition. The NbC is a metal-ceramic composite with a ductile-brittle behaviour. It was analyzed the morphology of powders by scanning electron microscopy as well as particle size it was determined. X ray diffraction identified the phases and the influence of milling time in the diffractogram patterns. Results indicates that milling time and NbC addition improves the milling efficiency significantly and being possible to obtain nanoparticles. (author)

  9. Microstructural analyses of intermetallic TiAl(Nb)-compounds prepared by arc melting and by powder metallurgy

    International Nuclear Information System (INIS)

    Chen, S.

    1988-01-01

    Intermetallic compounds based on TiAl with Nb or V as alloying additions prepared by powder metallurgy (P/M) and arc melting (A/M) techniques have been investigated with respect to their potential as new high temperature materials. All the alloys with nominal Al-concentrations 34-36 wt% contain two phases, γ-TiAl and α 2 -Ti 3 Al, but significant differences in the distribution of γ and α 2 were found between the P/M and A/M materials. The role of impurities during processing and the microstructural stability in the planned service temperature range 700-1000 0 C are discussed. In the P/M TiAl alloys two carbide precipitates have been found, which are the cubic Perovskite-AlTi 3 C phase in the γ-matrix and the hexagonal H-AlTi 2 (C, N) phase at grain boundaries. At high temperatures the AlTi 3 C phase dissolves and is replaced by more stable H-phase, and therefore no longer contributes to the high temperature strength of the material. Mechanical properties of both the P/M and A/M alloys are compared in association with the processing methods and the resulting microstructures. (orig.) With 71 figs., 22 tabs [de

  10. Effect of intercritical annealing and quenching plus tempering heat treatments on microstructure of Ni added powder metallurgy steels

    International Nuclear Information System (INIS)

    Tekeli, S.; Gueral, A.

    2007-01-01

    In this study, intercritical annealing, which is usually practiced to low alloy ingot steels, and quenching + tempering heat treatments were applied to low alloy powder metallurgy steel. For these purposes, atomized iron powder (Ancorsteel 1000) was mixed with 0.3% graphite and Ni ranging 0-2% (wt.). The mixed powders were cold pressed at 700 MPa and sintered at 1200 deg. C for 30 min under pure Ar gas atmosphere. Some of the sintered specimens was quenched from 890 deg. C and tempered at 200 and 400 deg. C for 1 h. The other sintered specimens were annealed at intercritical heat treatment temperatures of 728 and 760 deg. C and quenched in water. The experimental results showed that a typical tempered martensite microstructure was obtained in the specimen without Ni addition after quenching + tempering, whereas the dispersion of Ni-rich areas in the microstructure of tempered martensite in Ni-added specimens was seen. With increasing tempering temperature, the volume fraction of Ni-rich areas slightly decreased. While ferrite + martensite microstructure was produced after intercritical annealing heat treatment, Ni-rich areas in the centre of martensite islands in ferrite matrix were seen in Ni-added specimens. Also, with increasing intercritical annealing temperature and Ni content, martensite volume fraction increased and ferrite ratio decreased

  11. In situ synthesis and strengthening of powder metallurgy high speed steel in addition of LaB6

    Science.gov (United States)

    Shen, Weijun; Yu, Linping; Li, Zhi; He, Yuehui; Zhang, Qiankun; Zhang, Huibin; Jiang, Yao; Lin, Nan

    2017-11-01

    A novel technology which was characterized by the vacuum solid state sintering was developed for powder metallurgy high speed steels production. During sintering, both the WC and Mo2C reacted with Fe and transformed to W and Mo rich M6C carbides which were the common hard phases in high speed steels. Also, a high number of W, Mo and Fe were dissolved in VC, forming the MC carbides. The densification of the material mainly relied on the solubility effect during the M6C and MC carbides formation. By alloying with a 0.1 wt% of LaB6 to the steel, the bending strength and the fracture toughness were improved from 3290 MPa and 25.6 MPam1/2 to 4018 MPa and 29.4 MPam1/2, respectively. The TEM analysis demonstrated three types of reaction products by the LaB6 addition: the amorphous phase, the core-shell structure and the La2O3 phase. The impurity elements such as the Mg, Al, Si, S, Ca, and O were absorbed following the LaB6 addition. Moreover, the deoxidization effect caused by the LaB6 addition promoted the sintering at a high-temperature period which contributed to the bending strength and fracture toughness improvement.

  12. The wear properties of in-situ 7075 Al-Ti composites produced by powder metallurgy route

    Energy Technology Data Exchange (ETDEWEB)

    Ay, H.; Özyurek, D.; Yıldırım, M., E-mail: musayildirim@karabuk.edu.tr [Karabük University, Technology Faculty, Department of Manufacturing Engineering / Karabuk (Turkey); Bostan, B. [Gazi University, Technology Faculty, Department of Metallurgy and Materials Engineering (Turkey)

    2016-04-21

    In this study, the wear properties of in-situ 7075 Al-Ti composites produced by powder metallurgy route were investigated. Different amount of Ti (2, 4, 6 %) added to gas atomized 7075 Al alloy powders and they were mixed in turbula with 47rpm for 45 minutes. Then the mixed powders were pre-shaped by press under 600 MPa pressure. The samples were cooled in the furnace after sintered at 580 °C for 4 hours in the atmosphere controlled furnace. Standard metallographic process such as grinding, polishing and etching were applied to sintered samples. The hardness values were measured. Scanning Electron Microscope (SEM), X-Ray Diffraction (XRD) examines were carried out. The wear tests were performed in a pin-on disc type wear apparatus with 1 ms{sup −1} sliding speed at six different sliding distance (500-3000 m) under 30 N loads. As a result of studies, hardness values were increased with increasing Ti content, in addition the weight losses were decreased with increasing Ti amount.

  13. Long-term ongoing impact of arsenic contamination on the environmental compartments of a former mining-metallurgy area.

    Science.gov (United States)

    González-Fernández, B; Rodríguez-Valdés, E; Boente, C; Menéndez-Casares, E; Fernández-Braña, A; Gallego, J R

    2018-01-01

    Arsenic and mercury are potentially toxic elements of concern for soil, surficial and ground waters, and sediments. In this work various geochemical and hydrogeological tools were used to study a paradigmatic case of the combined effects of the abandonment of Hg- and As-rich waste on these environmental compartments. Continuous weathering of over 40years has promoted As and Hg soil pollution (thousands of ppm) in the surroundings of a former Hg mining-metallurgy site and affected the water quality of a nearby river and shallow groundwater. In particular, the high availability of As both in soils and waste was identified as one of the main determinants of contaminant distribution, whereas the impact of Hg was found to be minor, which is explained by lower mobility. Furthermore, potential additional sources of pollution (coal mining, high natural backgrounds, etc.) discharging into the study river were revealed less significant than the contaminants generated in the Hg-mining area. The transport and deposition of pollutants within the water cycle has also affected several kilometres downstream of the release areas and the chemistry of stream sediments. Overall, the environmental compartments studies held considerable concentrations of Hg and As, as remarkably revealed by the average contaminant load released in the river (several tons of As per year) and the accumulation of toxic elements in sediments (enrichment factors of As and Hg above 35). Copyright © 2017 Elsevier B.V. All rights reserved.

  14. Mask fabrication process

    Science.gov (United States)

    Cardinale, Gregory F.

    2000-01-01

    A method for fabricating masks and reticles useful for projection lithography systems. An absorber layer is conventionally patterned using a pattern and etch process. Following the step of patterning, the entire surface of the remaining top patterning photoresist layer as well as that portion of an underlying protective photoresist layer where absorber material has been etched away is exposed to UV radiation. The UV-exposed regions of the protective photoresist layer and the top patterning photoresist layer are then removed by solution development, thereby eliminating the need for an oxygen plasma etch and strip and chances for damaging the surface of the substrate or coatings.

  15. Fabrication of zein nanostructure

    Science.gov (United States)

    Luecha, Jarupat

    The concerns on the increase of polluting plastic wastes as well as the U.S. dependence on imported petrochemical products have driven an attention towards alternative biodegradable polymers from renewable resources. Zein protein, a co-product from ethanol production from corn, is a good candidate. This research project aims to increase zein value by adopting nanotechnology for fabricating advanced zein packaging films and zein microfluidic devices. Two nanotechnology approaches were focused: the polymer nanoclay nanocomposite technique where the nanocomposite structures were created in the zein matrix, and the soft lithography and the microfluidic devices where the micro and nanopatterns were created on the zein film surfaces. The polymer nanoclay nanocomposite technique was adopted in the commonly used zein film fabrication processes which were solvent casting and extrusion blowing methods. The two methods resulted in partially exfoliated nanocomposite structures. The impact of nanoclays on the physical properties of zein films strongly depended on the film preparation techniques. The impact of nanoclay concentration was more pronounced in the films made by extrusion blowing technique than by the solvent casting technique. As the processability limitation for the extrusion blowing technique of the zein sample containing hight nanoclay content, the effect of the nanoclay content on the rheological properties of zein hybrid resins at linear and nonlinear viscoelastic regions were further investigated. A pristine zein resin exhibited soft solid like behavior. On the other hand, the zein hybrid with nanoclay content greater than 5 wt.% showed more liquid like behavior, suggesting that the nanoclays interrupted the entangled zein network. There was good correspondence between the experimental data and the predictions of the Wagner model for the pristine zein resins. However, the model failed to predict the steady shear properties of the zein nanoclay nanocomposite

  16. Fabrication process optimization for improved mechanical properties of Al 7075/SiCp metal matrix composites

    Directory of Open Access Journals (Sweden)

    Dipti Kanta Das

    2016-04-01

    Full Text Available Two sets of nine different silicon carbide particulate (SiCp reinforced Al 7075 Metal Matrix Composites (MMCs were fabricated using liquid metallurgy stir casting process. Mean particle size and weight percentage of the reinforcement were varied according to Taguchi L9 Design of Experiments (DOE. One set of the cast composites were then heat treated to T6 condition. Optical micrographs of the MMCs reveal consistent dispersion of reinforcements in the matrix phase. Mechanical properties were determined for both as-cast and heat treated MMCs for comparison of the experimental results. Linear regression models were developed for mechanical properties of the heat treated MMCs using list square method of regression analysis. The fabrication process parameters were then optimized using Taguchi based grey relational analysis for the multiple mechanical properties of the heat treated MMCs. The largest value of mean grey relational grade was obtained for the composite with mean particle size 6.18 µm and 25 weight % of reinforcement. The optimal combination of process parameters were then verified through confirmation experiments, which resulted 42% of improvement in the grey relational grade. Finally, the percentage of contribution of each process parameter on the multiple performance characteristics was calculated through Analysis of Variance (ANOVA.

  17. Design and fabrication of stainless steel components for long life of spent fuel reprocessing plants

    International Nuclear Information System (INIS)

    Natarajan, R.; Ramkumar, P.; Sundararaman, V.; Kamachi Mudali, U.; Baldev Raj; Shanmugam, K.

    2010-01-01

    Reprocessing of spent nuclear fuels based on the PUREX process is the proven process with many commercial plants operating satisfactorily worldwide. The process medium being nitric acid, austenitic stainless steel is the material of construction as it is the best commercially available material for meeting the conditions in the reprocessing plants. Because of the high radiation fields, contact maintenance of equipment and systems of these plants are very time consuming and costly unlike other chemical process plants. Though the plants constructed in the early years required extensive shut downs for replacement of equipment and systems within the first fifteen years of operation itself, development in the field of stainless steel metallurgy and fabrication techniques have made it possible to design the present day plants for an operating life period of forty years. A review of the operational experience of the PUREX process based aqueous reprocessing plants has been made in this paper and reveals that life limiting failures of equipment and systems are mainly due to corrosion while a few are due to stresses. Presently there are no standards for design specification of materials and fabrication of reprocessing plants like the nuclear power plants, where well laid down ASTM and ASME codes and standards are available which are based on the large scale operational feedbacks on pressure vessels for conventional and nuclear industries. (author)

  18. An Overview of Key Challenges in the Fabrication of Metal Matrix Nanocomposites Reinforced by Graphene Nanoplatelets

    Directory of Open Access Journals (Sweden)

    Abdollah Saboori

    2018-03-01

    Full Text Available This article provides an overview of research efforts with an emphasis on the fabrication of metal matrix nanocomposites (MMNCs reinforced by graphene nanoplatelets (GNPs. Particular attention is devoted to finding the challenges in the production of MMNCs through the powder metallurgy techniques. The main technical challenges can be listed as: (I reinforcement selection; (II dispersion of reinforcement within the matrix; (III reactivity between the reinforcement and matrix; (IV interfacial bonding; (V preferred orientation of reinforcement. It is found that some of these difficulties can be attributed to the nature of the materials involved, while the others are related to the preparation routes. It is reported that the challenges related to the process can often be addressed by changing the production process or by using post-processing techniques. More challenging issues instead are related to the composition of the matrix and reinforcement, their reactivity and the dispersion of reinforcement. These topics still bring significant challenges to the materials scientists, and it would be worth mentioning that the fabrication of MMNCs with a uniform dispersion of reinforcement, strong interfacial bonding, without detrimental reactions and improved isotropic properties is still a puzzling issue.

  19. Summary report on fuel development and miniplate fabrication for the RERTR Program, 1978 to 1990

    Energy Technology Data Exchange (ETDEWEB)

    Wiencek, T.C. [Argonne National Lab., IL (United States). Energy Technology Div.

    1995-08-01

    This report summarizes the efforts of the Fabrication Technology Section at Argonne National Laboratory in the program of Reduced Enrichment Research and Test Reactors (RERTR). The main objective of this program was to reduce the amount of high enriched ({approx}93% {sup 235}U) uranium (HEU) used in nonpower reactors. Conversion from low-density (0.8--1.6 g U/cm{sup 3}) HEU fuel elements to highly loaded (up to 7 g U/cm{sup 3}) low-enrichment (<20% {sup 235}U) uranium (LEU) fuel elements allows the same reactor power levels, core designs and sizes to be retained while greatly reducing the possibility of illicit diversion of HEU nuclear fuel. This document is intended as an overview of the period 1978--1990, during which the Section supported this project by fabricating mainly powder metallurgy uranium-silicide dispersion fuel plates. Most of the subjects covered in detail are fabrication-related studies of uranium silicide fuels and fuel plate properties. Some data are included for out-of-pile experiments such as corrosion and compatibility tests. Also briefly covered are most other aspects of the RERTR program such as irradiation tests, full-core demonstrations, and technology transfer. References included are for further information on most aspects of the entire program. A significant portion of the report is devoted to data that were never published in their entirety. The appendices contain a list of previous RERTR reports, ANL fabrication procedures, calculations for phases present in two-phase fuels, chemical analysis of fuels, miniplate characteristics, and a summary of bonding runs made by hot isostatic pressing.

  20. Summary report on fuel development and miniplate fabrication for the RERTR Program, 1978 to 1990

    International Nuclear Information System (INIS)

    Wiencek, T.C.

    1995-08-01

    This report summarizes the efforts of the Fabrication Technology Section at Argonne National Laboratory in the program of Reduced Enrichment Research and Test Reactors (RERTR). The main objective of this program was to reduce the amount of high enriched (∼93% 235 U) uranium (HEU) used in nonpower reactors. Conversion from low-density (0.8--1.6 g U/cm 3 ) HEU fuel elements to highly loaded (up to 7 g U/cm 3 ) low-enrichment ( 235 U) uranium (LEU) fuel elements allows the same reactor power levels, core designs and sizes to be retained while greatly reducing the possibility of illicit diversion of HEU nuclear fuel. This document is intended as an overview of the period 1978--1990, during which the Section supported this project by fabricating mainly powder metallurgy uranium-silicide dispersion fuel plates. Most of the subjects covered in detail are fabrication-related studies of uranium silicide fuels and fuel plate properties. Some data are included for out-of-pile experiments such as corrosion and compatibility tests. Also briefly covered are most other aspects of the RERTR program such as irradiation tests, full-core demonstrations, and technology transfer. References included are for further information on most aspects of the entire program. A significant portion of the report is devoted to data that were never published in their entirety. The appendices contain a list of previous RERTR reports, ANL fabrication procedures, calculations for phases present in two-phase fuels, chemical analysis of fuels, miniplate characteristics, and a summary of bonding runs made by hot isostatic pressing

  1. AFIP-6 Fabrication Summary Report

    Energy Technology Data Exchange (ETDEWEB)

    Glenn A. Moore; M. Craig Marshall

    2011-09-01

    The AFIP-6 (ATR Full-size plate In center flux trap Position) experiment was designed to evaluate the performance of monolithic fuels at a scale prototypic of research reactor fuel plates. Two qualified fueled plates were fabricated for the AFIP-6 experiment; to be irradiated in the INL Advanced Test Reactor (ATR). This report provides details of the fuel fabrication efforts, including material selection, fabrication processes, and fuel plate qualification.

  2. Filter Fabrics for Airport Drainage.

    Science.gov (United States)

    1979-09-01

    pneumatically filling a woven polypropylene stocking with sand and vibrating it into a prebored hole, while another method uses a polyester nonwoven fabric...Selected Nonwoven Filter Fabrics," Letter Report, June 1977, U. S. Army Engineer Waterways Experiment Station, CE, Vicksburg, Miss. 18. BalL, J. E...woven and nonwoven plastic filter fabric. It has been developed based on limited field performance observations and the laboratory test evaluation of

  3. Fabrication of carbon nanofiber-reinforced aluminum matrix composites assisted by aluminum coating formed on nanofiber surface by in situ chemical vapor deposition

    Science.gov (United States)

    Ogawa, Fumio; Masuda, Chitoshi

    2015-01-01

    The van der Waals agglomeration of carbon nanofibers (CNFs) and the weight difference and poor wettability between CNFs and aluminum hinder the fabrication of dense CNF-reinforced aluminum matrix composites with superior properties. In this study, to improve this situation, CNFs were coated with aluminum by a simple and low-cost in situ chemical vapor deposition (in situ CVD). Iodine was used to accelerate the transport of aluminum atoms. The coating layer formed by the in situ CVD was characterized using scanning electron microscopy, transmission electron microscopy, x-ray diffraction, Fourier transform-infrared spectroscopy, and x-ray photoelectron spectroscopy. The results confirmed that the CNFs were successfully coated with aluminum. The composites were fabricated to investigate the effect of the aluminum coating formed on the CNFs. The dispersion of CNFs, density, Vickers micro-hardness and thermal conductivity of the composites fabricated by powder metallurgy were improved. Pressure-less infiltration experiments were conducted to fabricate composites by casting. The results demonstrated that the wettability and infiltration were dramatically improved by the aluminum coating layer on CNFs. The aluminum coating formed by the in situ CVD technique was proved to be effective for the fabrication of CNF-reinforced aluminum matrix composites.

  4. Ultraviolet Protection by Fabric Engineering

    Directory of Open Access Journals (Sweden)

    Mukesh Kumar Singh

    2013-01-01

    Full Text Available Background. The increasing emission of greenhouse gases has evoked the human being to save the ozone layer and minimize the risk of ultraviolet radiation (UVR. Various fabric structures have been explored to achieve desired ultraviolet protection factor (UPF in various situations. Objective. In this study, the effect of various filament configurations like twisted, flat, intermingled, and textured in multifilament yarns on fabric in different combinations is assessed in order to engineer a fabric of better ultraviolet protection factor (UPF. Methods. In order to engineer a fabric having optimum UV protection with sufficient comfort level in multifilament woven fabrics, four different yarn configurations, intermingled, textured, twisted, and flat, were used to develop twelve different fabric samples. The most UV absorbing and most demanding fibre polyethylene terephthalate (PET was considered in different filament configuration. Results. The combinations of intermingled warp with flat, intermingled, and textured weft provided excellent UVR protection comparatively at about 22.5 mg/cm2 fabric areal density. The presence of twisted yarn reduced the UV protection due to enhanced openness in fabric structure. Conclusion. The appropriate combination of warp and weft threads of different configuration should be selected judiciously in order to extract maximum UV protection and wear comfort attributes in multifilament woven PET fabrics.

  5. Oxidation and the Effects of High Temperature Exposures on Notched Fatigue Life of an Advanced Powder Metallurgy Disk Superalloy

    Science.gov (United States)

    Sudbrack, Chantal K.; Draper, Susan L.; Gorman, Timothy T.; Telesman, Jack; Gab, Timothy P.; Hull, David R.

    2012-01-01

    Oxidation and the effects of high temperature exposures on notched fatigue life were considered for a powder metallurgy processed supersolvus heat-treated ME3 disk superalloy. The isothermal static oxidation response at 704 C, 760 C, and 815 C was consistent with other chromia forming nickel-based superalloys: a TiO2-Cr2O3 external oxide formed with a branched Al2O3 internal subscale that extended into a recrystallized - dissolution layer. These surface changes can potentially impact disk durability, making layer growth rates important. Growth of the external scales and dissolution layers followed a cubic rate law, while Al2O3 subscales followed a parabolic rate law. Cr- rich M23C6 carbides at the grain boundaries dissolved to help sustain Cr2O3 growth to depths about 12 times thicker than the scale. The effect of prior exposures was examined through notched low cycle fatigue tests performed to failure in air at 704 C. Prior exposures led to pronounced debits of up to 99 % in fatigue life, where fatigue life decreased inversely with exposure time. Exposures that produced roughly equivalent 1 m thick external scales at the various isotherms showed statistically equivalent fatigue lives, establishing that surface damage drives fatigue debit, not exposure temperature. Fractographic evaluation indicated the failure mode for the pre-exposed specimens involved surface crack initiations that shifted with exposure from predominately single intergranular initiations with transgranular propagation to multi-initiations from the cracked external oxide with intergranular propagation. Weakened grain boundaries at the surface resulting from the M23C6 carbide dissolution are partially responsible for the intergranular cracking. Removing the scale and subscale while leaving a layer where M23C6 carbides were dissolved did not lead to a significant fatigue life improvement, however, also removing the M23C6 carbide dissolution layer led to nearly full recovery of life, with a

  6. Precipitation in cold-rolled Al-Sc-Zr and Al-Mn-Sc-Zr alloys prepared by powder metallurgy

    KAUST Repository

    Vlach, Martin

    2013-12-01

    The effects of cold-rolling on thermal, mechanical and electrical properties, microstructure and recrystallization behaviour of the AlScZr and AlMnScZr alloys prepared by powder metallurgy were studied. The powder was produced by atomising in argon with 1% oxygen and then consolidated by hot extrusion at 350 C. The electrical resistometry and microhardness together with differential scanning calorimetry measurements were compared with microstructure development observed by transmission and scanning electron microscopy, X-ray diffraction and electron backscatter diffraction. Fine (sub)grain structure developed and fine coherent Al3Sc and/or Al3(Sc,Zr) particles precipitated during extrusion at 350 C in the alloys studied. Additional precipitation of the Al3Sc and/or Al3(Sc,Zr) particles and/or their coarsening was slightly facilitated by the previous cold rolling. The presence of Sc,Zr-containing particles has a significant antirecrystallization effect that prevents recrystallization at temperatures minimally up to 420 C. The precipitation of the Al6Mn- and/or Al 6(Mn,Fe) particles of a size ~ 1.0 μm at subgrain boundaries has also an essential antirecrystallization effect and totally suppresses recrystallization during 32 h long annealing at 550 C. The texture development of the alloys seems to be affected by high solid solution strengthening by Mn. The precipitation of the Mn-containing alloy is highly enhanced by a cold rolling. The apparent activation energy of the Al3Sc particles formation and/or coarsening and that of the Al6Mn and/or Al 6(Mn,Fe) particle precipitation in the powder and in the compacted alloys were determined. The cold deformation has no effect on the apparent activation energy values of the Al3Sc-phase and the Al 6Mn-phase precipitation. © 2013 Elsevier Inc.

  7. Intentionally fabricated autobiographical memories.

    Science.gov (United States)

    Justice, Lucy V; Morrison, Catriona M; Conway, Martin A

    2018-02-01

    Participants generated both autobiographical memories (AMs) that they believed to be true and intentionally fabricated autobiographical memories (IFAMs). Memories were constructed while a concurrent memory load (random 8-digit sequence) was held in mind or while there was no concurrent load. Amount and accuracy of recall of the concurrent memory load was reliably poorer following generation of IFAMs than following generation of AMs. There was no reliable effect of load on memory generation times; however, IFAMs always took longer to construct than AMs. Finally, replicating previous findings, fewer IFAMs had a field perspective than AMs, IFAMs were less vivid than AMs, and IFAMs contained more motion words (indicative of increased cognitive load). Taken together, these findings show a pattern of systematic differences that mark out IFAMs, and they also show that IFAMs can be identified indirectly by lowered performance on concurrent tasks that increase cognitive load.

  8. Fabrication of superhydrophobic cotton fabrics using crosslinking polymerization method

    Science.gov (United States)

    Jiang, Bin; Chen, Zhenxing; Sun, Yongli; Yang, Huawei; Zhang, Hongjie; Dou, Haozhen; Zhang, Luhong

    2018-05-01

    With the aim of removing and recycling oil and organic solvent from water, a facile and low-cost crosslinking polymerization method was first applied on surface modification of cotton fabrics for water/oil separation. Micro-nano hierarchical rough structure was constructed by triethylenetetramine (TETA) and trimesoyl chloride (TMC) that formed a polymeric layer on the surface of the fabric and anchored Al2O3 nanoparticles firmly between the fabric surface and the polymer layer. Superhydrophobic property was further obtained through self-assembly grafting of hydrophobic groups on the rough surface. The as-prepared cotton fabric exhibited superoleophilicity in atmosphere and superhydrophobicity both in atmosphere and under oil with the water contact angle of 153° and 152° respectively. Water/oil separation test showed that the as-prepared cotton fabric can handle with various oil-water mixtures with a high separation efficiency over 99%. More importantly, the separation efficiency remained above 98% over 20 cycles of reusing without losing its superhydrophobicity which demonstrated excellent reusability in oil/water separation process. Moreover, the as-prepared cotton fabric possessed good contamination resistance ability and self-cleaning property. Simulation washing process test showed the superhydrophobic cotton fabric maintained high value of water contact angle above 150° after 100 times washing, indicating great stability and durability. In summary, this work provides a brand-new way to surface modification of cotton fabric and makes it a promising candidate material for oil/water separation.

  9. From the TRIP effect and Quenching and Partitioning steels concepts to the development of new high-performance, lean powder metallurgy steels

    International Nuclear Information System (INIS)

    Torralba, José M.; Navarro, Alfonso; Campos, Mónica

    2013-01-01

    A new method of developing lean powder metallurgy steel is proposed. The microstructure of the steel is tailored by combining two different prealloyed steel grades. These materials open a new niche in steel grades for high-performance applications by using a low-cost method of production. Moreover, an alternative route to developing microstructures suitable for manufacturing TRIP and/or Q and P steels is proposed avoiding some of the complex steps that must otherwise be taken to obtain the proper starting microstructure

  10. Metallurgy of mercury in Almaden: from aludel furnaces until Pacific furnaces; La metalurgia del mercurio en Almaden: desde los hornos de aludeles a los hornos Pacific

    Energy Technology Data Exchange (ETDEWEB)

    Tejero-Manzanares, J.; Garrido Saenz, I.; Mata Cabrera, F.; Rubio Mesas, M. L.

    2014-07-01

    This paper shows the different types of furnaces for roasting cinnabar, used in the metallurgy of quicksilver over the centuries of exploitation of the Almaden Mines (Spain). Some of these techniques are part of our industrial heritage. They have contributed to name UNESCO World Heritage Site the vast technological legacy of these mines recently. This research contributes to close the long way of metallurgical activity from aludel furnaces until Pacif furnaces, first and lasted technology to produce on an industrial scale. It is delved into the most relevant aspects having to do with the type, evolution and number of furnaces existing on each of the periods. (Author)

  11. Initial Microstructure Evaluation of a U3Si2 + W Fuel Pin Fabricated Via Arc Melt Gravity Drop Casting

    Science.gov (United States)

    Hoggan, Rita E.; Harp, Jason M.

    2018-02-01

    Injection casting has historically been used to fabricate metallic nuclear fuel on a large scale. Casting of intermetallic fuel forms, such as U3Si2, may be an alternative pathway for fabrication of fuel pins to powder metallurgy. To investigate casting on a small scale, arc melt gravity drop casting was employed to cast a one-off pin of U3Si2 for evaluation as a fabrication method for U3Si2 as a light water reactor fuel. The pin was sectioned and examined via optical microscopy and scanning electron microscopy equipped with energy dispersive x-ray spectroscopy (EDS). Image analysis was used to estimate the volume fraction of phase impurities as well as porosity. The primary phase determined by EDS was U3Si2 with U-O and U-Si-W phase impurities. Unusually high levels of tungsten were observed because of accidental tungsten introduction during arc melting. No significant changes in microstructure were observed after annealing a section of the pin at 800°C for 72 h. The average density of the sectioned specimens was 12.4 g/cm3 measured via Archimedes principle immersion density and He gas displacement.

  12. Unidirectional Fabric Drape Testing Method.

    Science.gov (United States)

    Mei, Zaihuan; Shen, Wei; Wang, Yan; Yang, Jingzhi; Zhou, Ting; Zhou, Hua

    2015-01-01

    In most cases, fabrics such as curtains, skirts, suit pants and so on are draped under their own gravity parallel to fabric plane while the gravity is perpendicular to fabric plane in traditional drape testing method. As a result, it does not conform to actual situation and the test data is not convincing enough. To overcome this problem, this paper presents a novel method which simulates the real mechanical conditions and ensures the gravity is parallel to the fabric plane. This method applied a low-cost Kinect Sensor device to capture the 3-dimensional (3D) drape profile, thus we obtained the drape degree parameters and aesthetic parameters by 3D reconstruction and image processing and analysis techniques. The experiment was conducted on our self-devised drape-testing instrument by choosing different kinds of weave structure fabrics as our testing samples and the results were compared with those of traditional method and subjective evaluation. Through regression and correlation analysis we found that this novel testing method was significantly correlated with the traditional and subjective evaluation method. We achieved a new, non-contact 3D measurement method for drape testing, namely unidirectional fabric drape testing method. This method is more suitable for evaluating drape behavior because it is more in line with actual mechanical conditions of draped fabrics and has a well consistency with the requirements of visual and aesthetic style of fabrics.

  13. DRAPING SIMULATION OF WOVEN FABRICS

    Energy Technology Data Exchange (ETDEWEB)

    Rodgers, William [General Motors LLC; Jin, Xiaoshi [ESI Group NA; Zhu, Jiang [Optimal CAE; Wathen, Terrence [General Motors LLC; Doroudian2, Mark [ESI Group NA; Aitharaju, Venkat [General Motors LLC

    2016-09-07

    Woven fabric composites are extensively used in molding complex geometrical shapes due to their high conformability compared to other fabrics. Preforming is an important step in the overall process, where the two-dimensional fabric is draped to become the three-dimensional shape of the part prior to resin injection. During preforming, the orientation of the yarns may change significantly compared to the initial orientations. Accurate prediction of the yarn orientations after molding is important for evaluating the structural performance of the final part. This paper presents a systematic investigation of the angle changes during the preform operation for carbon fiber twill and satin weave fabrics. Preforming experiments were conducted using a truncated pyramid mold geometry designed and fabricated at the General Motors Research Laboratories. Predicted results for the yarn orientations were compared with experimental results and good agreement was observed

  14. Fabricating multifunctional silver nanoparticles-coated cotton fabric

    Directory of Open Access Journals (Sweden)

    Mohammad Shateri-Khalilabad

    2017-05-01

    Full Text Available Silver nanoparticles with high density coating were formed on the surface of cotton fabric through pre-activation by potassium hydroxide and in situ reduction of silver nitrate. The silver nanoparticles-coated fabric was then reacted with hexadecyltrimethoxysilane, which resulted in the formation of low surface energy layer around the fabric. The fabrics were characterized by reflectance spectrophotometry, scanning electron microscopy, energy dispersive X-ray spectroscopy and X-ray diffraction patterns. Wettability properties were measured by contact angle goniometry and shedding angle technique. Antibacterial activity was determined against Gram-positive Staphylococcus aureus and Gram-negative Escherichia coli. Ultraviolet-blocking was measured via transmittance data in the range of 280–400 nm. Microscopy images showed the formation of uniform and high density coating of silver on the surface of cotton fibers. The fabric showed hydrophobicity with CA of 158 ± 4.3° and SHA of 7°. Also, it demonstrated a high antibacterial activity against two bacterial challenges, as shown via formation of inhibition zone. Excellent ultraviolet protection of the fabric was demonstrated by ultraviolet protection factor value of 296. The fabric also showed good durability against repeated laundering.

  15. Superconducting circuit fabrication

    International Nuclear Information System (INIS)

    Stein, B.F.; Young, P.L.

    1984-01-01

    An improved method of anodization of thin films for the fabrication of superconducting devices. An electrically conducting contact layer is formed over a substrate between an electrically conducting object layer and the substrate. Also, an electrically insulating layer is formed between the object layer and the contact layer. The contact layer is connected to a power supply and at least a preselected portion of the object layer is anodized to a predetermined thickness. This may include anodizing all of some preselected portions through the complete thickness of the object layer. A pattern of hardened photoresist on the object layer provides portions not protected by the pattern. When anodization of the electrically conducting object layer takes place, the resulting anodized portion is thicker than the thickness of the portion of the object layer that it replaces. The present invention further includes reducing the preselected portion of the object layer to be anodized by a predetermined amount before anodizing so that when anodization is complete, the resulting partially anodized partially conducting object layer is substantially planar. Alternatively, the thickness of the anodized preselected portions can be reduced after anodizing by a predetermined amount to cause the layer to be substantially planar. The same pattern of hardened photoresist can be used when reducing the thickness of portions of the object layer or anodized preselected portions

  16. MOX fuel fabrication at AECL

    International Nuclear Information System (INIS)

    Dimayuga, F.C.; Jeffs, A.T.

    1995-01-01

    Atomic Energy of Canada Limited's mixed-oxide (MOX) fuel fabrication activities are conducted in the Recycle Fuel Fabrication Laboratories (RFFL) at the Chalk River Laboratories. The RFFL facility is designed to produce experimental quantities of CANDU MOX fuel for reactor physics tests or demonstration irradiations. From 1979 to 1987, several MOX fuel fabrication campaigns were run in the RFFL, producing various quantities of fuel with different compositions. About 150 bundles, containing over three tonnes of MOX, were fabricated in the RFFL before operations in the facility were suspended. In late 1987, the RFFL was placed in a state of active standby, a condition where no fuel fabrication activities are conducted, but the monitoring and ventilation systems in the facility are maintained. Currently, a project to rehabilitate the RFFL and resume MOX fuel fabrication is nearing completion. This project is funded by the CANDU Owners' Group (COG). The initial fabrication campaign will consist of the production of thirty-eight 37-element (U,Pu)O 2 bundles containing 0.2 wt% Pu in Heavy Element (H.E.) destined for physics tests in the zero-power ZED-2 reactor. An overview of the Rehabilitation Project will be given. (author)

  17. Precipitation in cold-rolled Al–Sc–Zr and Al–Mn–Sc–Zr alloys prepared by powder metallurgy

    International Nuclear Information System (INIS)

    Vlach, M.; Stulikova, I.; Smola, B.; Kekule, T.; Kudrnova, H.; Danis, S.; Gemma, R.; Ocenasek, V.; Malek, J.; Tanprayoon, D.; Neubert, V.

    2013-01-01

    The effects of cold-rolling on thermal, mechanical and electrical properties, microstructure and recrystallization behaviour of the AlScZr and AlMnScZr alloys prepared by powder metallurgy were studied. The powder was produced by atomising in argon with 1% oxygen and then consolidated by hot extrusion at 350 °C. The electrical resistometry and microhardness together with differential scanning calorimetry measurements were compared with microstructure development observed by transmission and scanning electron microscopy, X-ray diffraction and electron backscatter diffraction. Fine (sub)grain structure developed and fine coherent Al 3 Sc and/or Al 3 (Sc,Zr) particles precipitated during extrusion at 350 °C in the alloys studied. Additional precipitation of the Al 3 Sc and/or Al 3 (Sc,Zr) particles and/or their coarsening was slightly facilitated by the previous cold rolling. The presence of Sc,Zr-containing particles has a significant antirecrystallization effect that prevents recrystallization at temperatures minimally up to 420 °C. The precipitation of the Al 6 Mn- and/or Al 6 (Mn,Fe) particles of a size ∼ 1.0 μm at subgrain boundaries has also an essential antirecrystallization effect and totally suppresses recrystallization during 32 h long annealing at 550 °C. The texture development of the alloys seems to be affected by high solid solution strengthening by Mn. The precipitation of the Mn-containing alloy is highly enhanced by a cold rolling. The apparent activation energy of the Al 3 Sc particles formation and/or coarsening and that of the Al 6 Mn and/or Al 6 (Mn,Fe) particle precipitation in the powder and in the compacted alloys were determined. The cold deformation has no effect on the apparent activation energy values of the Al 3 Sc-phase and the Al 6 Mn-phase precipitation. - Highlights: • The Mn, Sc and Zr additions to Al totally suppresses recrystallization at 550 °C. • The Sc,Zr-containing particle precipitation is slightly facilitated by

  18. The potential for portable X-ray fluorescence determination of soil copper at ancient metallurgy sites, and considerations beyond measurements of total concentrations.

    Science.gov (United States)

    Tighe, M; Rogan, G; Wilson, S C; Grave, P; Kealhofer, L; Yukongdi, P

    2018-01-15

    Copper (Cu) at ancient metallurgy sites represents the earliest instance of anthropogenically generated metal pollution. Such sites are spread across a wide range of environments from Eurasia to South America, and provide a unique opportunity to investigate the past and present extent and impact of metalworking contamination. Establishing the concentration and extent of soil Cu at archaeometallurgy sites can enhance archaeological interpretations of site use but can also, more fundamentally, provide an initial indication of contamination risk from such sites. Systematic evaluations of total soil Cu concentrations at ancient metalworking sites have not been conducted, due in part to the limitations of conventional laboratory-based protocols. In this paper, we first review what is known about Cu soil concentrations at ancient metallurgy sites. We then assess the benefits and challenges of portable X-ray fluorescence spectrometry (pXRF) as an alternative, rapid technique for the assessment of background and contaminant levels of Cu in soils. We conclude that pXRF is an effective tool for identifying potential contamination. Finally, we provide an overview of some major considerations beyond total Cu concentrations, such as bioavailability assessments, that will need to be considered at such sites to move toward a complete assessment of environmental and human risk. Copyright © 2017 Elsevier Ltd. All rights reserved.

  19. Optimization of the Hot Forging Processing Parameters for Powder Metallurgy Fe-Cu-C Connecting Rods Based on Finite Element Simulation

    Science.gov (United States)

    Li, Fengxian; Yi, Jianhong; Eckert, Jürgen

    2017-12-01

    Powder forged connecting rods have the problem of non-uniform density distributions because of their complex geometric shape. The densification behaviors of powder metallurgy (PM) connecting rod preforms during hot forging processes play a significant role in optimizing the connecting rod quality. The deformation behaviors of a connecting rod preform, a Fe-3Cu-0.5C (wt pct) alloy compacted and sintered by the powder metallurgy route (PM Fe-Cu-C), were investigated using the finite element method, while damage and friction behaviors of the material were considered in the complicated forging process. The calculated results agree well with the experimental results. The relationship between the processing parameters of hot forging and the relative density of the connecting rod was revealed. The results showed that the relative density of the hot forged connecting rod at the central shank changed significantly compared with the relative density at the big end and at the small end. Moreover, the relative density of the connecting rod was sensitive to the processing parameters such as the forging velocity and the initial density of the preform. The optimum forging processing parameters were determined and presented by using an orthogonal design method. This work suggests that the processing parameters can be optimized to prepare a connecting rod with uniform density distribution and can help to better meet the requirements of the connecting rod industry.

  20. Fabric circuits and method of manufacturing fabric circuits

    Science.gov (United States)

    Chu, Andrew W. (Inventor); Dobbins, Justin A. (Inventor); Scully, Robert C. (Inventor); Trevino, Robert C. (Inventor); Lin, Greg Y. (Inventor); Fink, Patrick W. (Inventor)

    2011-01-01

    A flexible, fabric-based circuit comprises a non-conductive flexible layer of fabric and a conductive flexible layer of fabric adjacent thereto. A non-conductive thread, an adhesive, and/or other means may be used for attaching the conductive layer to the non-conductive layer. In some embodiments, the layers are attached by a computer-driven embroidery machine at pre-determined portions or locations in accordance with a pre-determined attachment layout before automated cutting. In some other embodiments, an automated milling machine or a computer-driven laser using a pre-designed circuit trace as a template cuts the conductive layer so as to separate an undesired portion of the conductive layer from a desired portion of the conductive layer. Additional layers of conductive fabric may be attached in some embodiments to form a multi-layer construct.

  1. Fabrication of cotton fabric with superhydrophobicity and flame retardancy.

    Science.gov (United States)

    Zhang, Ming; Wang, Chengyu

    2013-07-25

    A simple and facile method for fabricating the cotton fabric with superhydrophobicity and flame retardancy is described in the present work. The cotton fabric with the maximal WCA of 160° has been prepared by the covalent deposition of amino-silica nanospheres and the further graft with (heptadecafluoro-1,1,2,2-tetradecyl) trimethoxysilane. The geometric microstructure of silica spheres was measured by transmission electron microscopy (TEM). The cotton textiles before and after treatment were characterized by using scanning electron microscope (SEM) and X-ray photoelectron spectroscopy (XPS). The wetting behavior of cotton samples was investigated by water contact angle measurement. Moreover, diverse performances of superhydrophobic cotton textiles have been evaluated as well. The results exhibited the outstanding superhydrophobicity, excellent waterproofing durability and flame retardancy of the cotton fabric after treatment, offering a good opportunity to accelerate the large-scale production of superhydrophobic textiles materials for new industrial applications. Copyright © 2013 Elsevier Ltd. All rights reserved.

  2. Fabrication, characterization, and mechanical properties of spark plasma sintered Al–BN nanoparticle composites

    Energy Technology Data Exchange (ETDEWEB)

    Firestein, Konstantin L., E-mail: kosty@firestein.ru [National University of Science and Technology “MISIS”, Leninsky prospect 4, Moscow 119049 (Russian Federation); Steinman, Alexander E.; Golovin, Igor S. [National University of Science and Technology “MISIS”, Leninsky prospect 4, Moscow 119049 (Russian Federation); Cifre, Joan [Universitat de les Illes Balears, Ctra. de Valldemossa, km. 7.5, E-07122 Palma de Mallorca (Spain); Obraztsova, Ekaterina A.; Matveev, Andrei T.; Kovalskii, Andrey M. [National University of Science and Technology “MISIS”, Leninsky prospect 4, Moscow 119049 (Russian Federation); Lebedev, Oleg I. [CRISMAT, UMR 6508, CNRS-ENSICAEN, 6Bd Marechal Juin, 14050 Caen (France); Shtansky, Dmitry V., E-mail: shtansky@shs.misis.ru [National University of Science and Technology “MISIS”, Leninsky prospect 4, Moscow 119049 (Russian Federation); Golberg, Dmitri, E-mail: golberg.dmitri@nims.go.jp [World Premier International Center for Materials Nanoarchitectonics (WPI-MANA) National Institute for Materials Science (NIMS), Namiki 1, Tsukuba, Ibaraki 3050044 (Japan)

    2015-08-26

    Fabrication of high strength yet light and low cost composite materials with good mechanical properties at room and elevated temperatures is a challenge that metallurgy and materials science communities are facing for many years, and no “dream material” has been developed so far. The primary goal of this study was to fabricate, characterize, and to carry out tensile tests on Al-based composite materials strengthened with commercially-available BN nanoparticles (BNNPs). The composites were fabricated by spark plasma sintering (SPS) technique. The structures of powder mixtures and composite materials, as well as their fracture surfaces, were studied by scanning and transmission electron microscopy. The influence of BNNPs content (0.5, 1.5, 3, 4.5, 6, and 7.5 wt%) and holding times (5, 60, and 300 min) at 600 °C during SPS on the tensile strength was investigated. A maximum increase in strength was observed for Al-based composites with 4.5 wt% of BNNPs. The sample demonstrated a 50% increase in tensile strength compared with pristine Al. Although the tensile tests performed at 300 °C revealed that the tensile strength became 20% lower than the strength at room temperature, it was, however, still 75% higher compared with that of the pure Al at 300 °C. In addition, at 300 °C the Al–BNNPs composites demonstrated a much higher value of yield stress, about 115 MPa, which is 190% higher than that of pure Al at the same temperature. The damping properties of Al–BNNPs composites were evaluated by temperature dependent internal friction (TDIF) measurements. The obtained results are discussed based on structural analysis and the TDIF data.

  3. Fabrication of integrated metallic MEMS devices

    DEFF Research Database (Denmark)

    Yalcinkaya, Arda Deniz; Ravnkilde, Jan Tue; Hansen, Ole

    2002-01-01

    A simple and complementary metal oxide semiconductor (CMOS) compatible fabrication technique for microelectromechanical (MEMS) devices is presented. The fabrication technology makes use of electroplated metal layers. Among the fabricated devices, high quality factor microresonators...

  4. Fabrication of nanowires and nanostructures

    DEFF Research Database (Denmark)

    Mátéfi-Tempfli, Stefan; Mátéfi-Tempfli, M.; Piraux, L.

    2009-01-01

    We report on different approaches that we have adopted and developed for the fabrication of nanowires and nanostructures. Methods based on template synthesis and on self organization seem to be the most promising for the fabrication of nanomaterials and nanostructures due to their easiness and low...... cost. The development of a supported nanoporous alumina template and the possibility of using this template to combine electrochemical synthesis with lithographic methods open new ways for the fabrication of complex nanostructures. The numerous advantages of the supported template and its compatibility...

  5. Automated fabrication of reactor fuel

    International Nuclear Information System (INIS)

    Nyman, D.H.; McLemore, D.R.; Bennett, D.W.; Yatabe, J.M.

    1980-01-01

    The development of Secure Automated Fabrication (SAF) methods is the goal of the United States breeder reactor program and will form the technological basis for the future breeder reactor fuel supply. A major factor in achieving this goal is the development of remotely operated fuel fabrication equipment. The unit operations are being designed for microprocessor control connected to a central control center. The program schedule is to demonstrate the feasibility of automated pellet fuel fabrication and remote maintenance techniques by the mid-1980's. Development of major ceramic unit operations and the required computer control system is currently in the engineering testing stage

  6. Fabrication of integrated metallic MEMS devices

    DEFF Research Database (Denmark)

    Yalcinkaya, Arda Deniz; Ravnkilde, Jan Tue; Hansen, Ole

    2002-01-01

    A simple and complementary metal oxide semiconductor (CMOS) compatible fabrication technique for microelectromechanical (MEMS) devices is presented. The fabrication technology makes use of electroplated metal layers. Among the fabricated devices, high quality factor microresonators are characteri......A simple and complementary metal oxide semiconductor (CMOS) compatible fabrication technique for microelectromechanical (MEMS) devices is presented. The fabrication technology makes use of electroplated metal layers. Among the fabricated devices, high quality factor microresonators...

  7. Elevated temperature characterization of electron beam freeform fabricated Ti–6Al–4V and dispersion strengthened Ti–8Al–1Er

    International Nuclear Information System (INIS)

    Bush, R.W.; Brice, C.A.

    2012-01-01

    Highlights: ► Electron beam freeform fabrication process. ► Ti–6Al–4V and rare-earth dispersion Ti alloy. ► Tensile, creep, and oxidation properties comparable to alloys made with conventional fabrication methods. ► Fabrication process allows use of rare-earth dispersion Ti alloy. - Abstract: Electron beam freeform fabrication is an additive manufacturing process that can be used to build fully dense, structural metallic parts directly from a three-dimensional computer model. This technique can replace conventional fabrication methods, such as forging or machining from plate, and enable significant cost, time, and tool savings. Additionally, this method enables the fabrication of alloys with novel compositions that are not well suited to production via ingot metallurgy processes. Ti–8Al–1Er is an experimental dispersion strengthened titanium alloy composition that requires rapid cooling to achieve optimal properties and thus is not amenable to ingot metallurgy production methods. Oxide dispersion strengthened alloys, such as Ti–8Al–1Er are known to have excellent thermal stability and improved high temperature properties. In this work, the room temperature tensile, elevated temperature tensile, creep properties and oxidation resistance of electron beam additive manufactured Ti–6Al–4V and Ti–8Al–1Er were measured and compared to those of laser beam additive manufactured Ti–8Al–1Er and wrought Ti–6Al–4V. Elevated temperature tensile properties were measured between 93° and 538 °C. Creep tests were performed between 425° and 455 °C at stresses between 345 and 483 MPa. It was found that the elevated temperature properties of the electron beam additive manufactured products are comparable to those of wrought forms. The elevated temperature strengths of Ti–8Al–1Er are comparable to those of Ti–6Al–4V in percentage of room temperature strength retained at temperature. Based on a Larson–Miller analysis of the creep test

  8. Pilling Resistance of Knitted Fabrics

    Directory of Open Access Journals (Sweden)

    Gita BUSILIENĖ

    2011-09-01

    Full Text Available Knitted fabrics with different quantity of elastane, conspicuous by high viscosity and elasticity, having one of the most important performance properties - resistance to pilling are often used in the production of high quality sportswear. During technological process imitating operating conditions, the behaviour of knitted fabrics may be changed by different industrial softeners from 12 % to 20 % of active substance, for example fatty acid condensate (Tubingal 5051 or silicone micro emulsion (Tubingal SMF. The aim of this investigation is to define the influence of fibrous composition and chemical softeners to the propensity of fuzzing and pilling of plain and plated jersey pattern knitted fabrics. The results of investigations showed that fibrous composition and thickness of materials (up to 6 % and washing as well as softening (from 33 % to 67 % change the resistance of knitted fabrics to pilling.http://dx.doi.org/10.5755/j01.ms.17.3.597

  9. Geoacoustic Physical Model Fabrication Laboratory

    Data.gov (United States)

    Federal Laboratory Consortium — FUNCTION: Fabricates three-dimensional rough surfaces (e.g., fractals, ripples) out of materials such as PVC or wax to simulate the roughness properties associated...

  10. Plasmonic components fabrication via nanoimprint

    DEFF Research Database (Denmark)

    Boltasseva, Alexandra

    2009-01-01

    A review report on nanoimprinted plasmonic components is given. The fabrication of different metal–dielectric geometries and nanostructured surfaces that support either propagating or localized surface plasmon modes is discussed. The main characteristics and advantages of the nanoimprint technology...... for the fabrication of various plasmonic structures are outlined. The discussion of plasmonic waveguiding structures focuses on planar waveguides based on metal strips embedded into a dielectric and on profiled metal surfaces. Nanoimprint-based fabrication of two-dimensional nanostructured plasmonic surfaces...... for enhanced transmission studies and sensor applications is also discussed. Throughout the report, the main fabrication schemes are described, as well as the challenges facing future manufacturing of plasmonic components for device applications....

  11. The Mechanical Properties and In Vitro Biocompatibility of PM-Fabricated Ti-28Nb-35.4Zr Alloy for Orthopedic Implant Applications.

    Science.gov (United States)

    Xu, Wei; Li, Ming; Wen, Cuie; Lv, Shaomin; Liu, Chengcheng; Lu, Xin; Qu, Xuanhui

    2018-03-30

    A biocompatible Ti-28Nb-35.4Zr alloy used as bone implant was fabricated through the powder metallurgy process. The effects of mechanical milling and sintering temperatures on the microstructure and mechanical properties were investigated systematically, before in vitro biocompatibility of full dense Ti-28Nb-35.4Zr alloy was evaluated by cytotoxicity tests. The results show that the mechanical milling and sintering temperatures have significantly effects on the density and mechanical properties of the alloys. The relative density of the alloy fabricated by the atomized powders at 1500 °C is only 83 ± 1.8%, while the relative density of the alloy fabricated by the ball-milled powders can rapidly reach at 96.4 ± 1.3% at 1500 °C. When the temperature was increased to 1550 °C, the alloy fabricated by ball-milled powders achieve full density (relative density is 98.1 ± 1.2%). The PM-fabricated Ti-28Nb-35.4Zr alloy by ball-milled powders at 1550 °C can achieve a wide range of mechanical properties, with a compressive yield strength of 1058 ± 35.1 MPa, elastic modulus of 50.8 ± 3.9 GPa, and hardness of 65.8 ± 1.5 HRA. The in vitro cytotoxicity test suggests that the PM-fabricated Ti-28Nb-35.4Zr alloy by ball-milled powders at 1550 °C has no adverse effects on MC3T3-E1 cells with cytotoxicity ranking of 0 grade, which is nearly close to ELI Ti-6Al-4V or CP Ti. These properties and the net-shape manufacturability makes PM-fabricated Ti-28Nb-35.4Zr alloy a low-cost, highly-biocompatible, Ti-based biomedical alloy.

  12. Silicone nanocomposite coatings for fabrics

    Science.gov (United States)

    Eberts, Kenneth (Inventor); Lee, Stein S. (Inventor); Singhal, Amit (Inventor); Ou, Runqing (Inventor)

    2011-01-01

    A silicone based coating for fabrics utilizing dual nanocomposite fillers providing enhanced mechanical and thermal properties to the silicone base. The first filler includes nanoclusters of polydimethylsiloxane (PDMS) and a metal oxide and a second filler of exfoliated clay nanoparticles. The coating is particularly suitable for inflatable fabrics used in several space, military, and consumer applications, including airbags, parachutes, rafts, boat sails, and inflatable shelters.

  13. Fabricating plasmonic components for nanophotonics

    DEFF Research Database (Denmark)

    Boltasseva, Alexandra; Nielsen, Rasmus Bundgaard; Jeppesen, Claus

    2009-01-01

    We report on experimental realization of different metal-dielectric structures that are used as surface plasmon polariton waveguides and as plasmonic metamaterials. Fabrication approaches based on different lithographic and deposition techniques are discussed.......We report on experimental realization of different metal-dielectric structures that are used as surface plasmon polariton waveguides and as plasmonic metamaterials. Fabrication approaches based on different lithographic and deposition techniques are discussed....

  14. Fabrication of mercury target vessel

    International Nuclear Information System (INIS)

    Wakui, Takashi; Kogawa, Hiroyuki; Haga, Katsuhiro; Futakawa, Masatoshi; Hayashi, Ryoichi; Uchiyama, Naoyoshi; Okamoto, Yoshinao; Nakamura, Koji

    2010-03-01

    The construction of materials and life science experimental facility in J-PARC (Japan Proton Accelerator Complex) project had been completed and accepted pulsed proton beams with low power. Since 2003, the detailed design, fabrication and examination for the mercury target vessel as a pulsed neutron source were carried out by the vender. The mercury target vessel consists of triple-walled structure in order to prevent the leak of mercury to outside at the failure of the mercury vessel and to remove the heat of the safety hull, which covers the mercury vessel, due to the injection of the pulsed proton beams. The high fabrication accuracy is required for the mercury target vessel assembled by the welding, because there are the relationships between the mercury target vessel and other components (target trolley, target storage container, flange of helium vessel, reflector and water-cooled shield). At each fabrication step, the examinations for the mercury target vessel with multi-walled structure were required. In this report, the required specification and basic structure of parts in the mercury target vessel are described and the fabrication procedure of the mercury target vessel by the vender is reported. In the fabrication of the mercury target vessel, there were many troubles such as large deformation due to the welding and then the vender repaired and brought the mercury target vessel to completion. Furthermore, improvements for the design and fabrication of the mercury target are reported. (author)

  15. Progress report on nuclear science and technology in China (Vol.3). Proceedings of academic annual meeting of China Nuclear Society in 2013, No.2--uranium mining and metallurgy sub-volume

    International Nuclear Information System (INIS)

    2014-05-01

    Progress report on nuclear science and technology in China (Vol. 3) includes 48 articles which are communicated on the third national academic annual meeting of China Nuclear Society. There are 10 books totally. This is the second one, the content is about uranium mining and metallurgy sub-volume

  16. Progress report on nuclear science and technology in China (Vol.1). Proceedings of academic annual meeting of China Nuclear Society in 2009, No.2--uranium mining and metallurgy sub-volume

    International Nuclear Information System (INIS)

    2010-11-01

    Progress report on nuclear science and technology in China (Vol. 1) includes 889 articles which are communicated on the first national academic annual meeting of China Nuclear Society. There are 10 books totally. This is the second one, the content is about uranium mining, uranium metallurgy and nuclear power.

  17. Applications of Phase Diagrams in Metallurgy and Ceramics: Proceedings of a Workshop Held at the National Bureau of Standards, Gaithersburg, Maryland, January 10-12, 1977. Volumes 1 [and] 2.

    Science.gov (United States)

    Carter, G. C., Ed.

    This document is a special National Bureau of Standards publication on a Workshop on Applications of Phase Diagrams in Metallurgy and Ceramics. The purposes of the Workshop were: (1) to assess the current national and international status of phase diagram determinations and evaluations for alloys, ceramics and semiconductors; (2) to determine the…

  18. Powder Metallurgy Facility

    Data.gov (United States)

    Federal Laboratory Consortium — The facility is uniquely equipped as the only laboratory within DA to conduct PM processing of refractory metals and alloys as well as the processing of a wide range...

  19. Fundamentals in physical metallurgy

    International Nuclear Information System (INIS)

    Adda, Y.; Dupouy, J.M.; Philibert, J.; Quere, Y.

    1978-01-01

    In this manual, the following topics are discussed: diffusion (principles and applications to metals); climb of dislocations, phase transformations; nucleation, growth, coalescence and kinetics of transformations; diffusion transformations; shear transformations; solidification [fr

  20. Fundamental Metallurgy of Solidification

    DEFF Research Database (Denmark)

    Tiedje, Niels

    2004-01-01

    The text takes the reader through some fundamental aspects of solidification, with focus on understanding the basic physics that govern solidification in casting and welding. It is described how the first solid is formed and which factors affect nucleation. It is described how crystals grow from ...

  1. Metallurgy: A compilation

    Science.gov (United States)

    1973-01-01

    A technology utilization program is presented for the dissemination of information on technological developments which have potential utility outside the aerospace and nuclear communities. Discussion is restricted to the effects of hydrogen on a variety of metal alloys, and the mechanical properties of some recently developed alloys. Hydrogen at both low and high pressure is shown to have adverse effects on alloys such as ultrahigh-strength steels, irradiated steels, columbium, inconel alloys, titanium alloys, and certain stainless steels. The mechanical and physical properties of a wide range of alloys, their performance at elevated temperatures, and some of the processes involved in their development are also considered.

  2. Use of Amino‐Functionalized CNTs and CVD Grown CNTs for Better Dispersion in Al Powder in the Fabrication of Composites

    Energy Technology Data Exchange (ETDEWEB)

    Singhal, S. K.; Mathur, R. B. [National Physical Laboratory (CSIR), New Delhi‐1100 12 (India); Mamta,; Teotia, Satish [Guru Jambheshwar University of Science and Technology, Hisar (India); Chahal, Rajiv [Nanoscience and Nanotechnology, Panjab University, Chandigarh (India)

    2011-12-12

    We report an improved process for the better dispersion of multiwalled carbon nanotubes (MWCNTs) in Al powder used for the fabrication of Al‐matrix composites employing powder metallurgy process. For obtaining a better dispersion of MWCNTs in Al, we used two types of MWCNTs. In the first type, the MWCNTs were firstly functionalized by using ammonium bi‐carbonate and mix with Al powder using a high energy ball mill in the presence of a process control agent. In the second type we grew MWCNTs directly on Al powder using CVD. Various mechanical properties of the composites including micro hardness, compressive strength etc. were determined. It has been observed that using functionalized MWCNTs (fCNTs) and CVD grown MWCNTs, these properties were found to enhance significantly. The dispersion of functionalized CNTs was studied by SEM and the interfacial bonding between functionalized CNTs and Al matrix using high resolution transmission electron microscopy (HRTEM).

  3. ITER Central Solenoid Module Fabrication

    Energy Technology Data Exchange (ETDEWEB)

    Smith, John [General Atomics, San Diego, CA (United States)

    2016-09-23

    The fabrication of the modules for the ITER Central Solenoid (CS) has started in a dedicated production facility located in Poway, California, USA. The necessary tools have been designed, built, installed, and tested in the facility to enable the start of production. The current schedule has first module fabrication completed in 2017, followed by testing and subsequent shipment to ITER. The Central Solenoid is a key component of the ITER tokamak providing the inductive voltage to initiate and sustain the plasma current and to position and shape the plasma. The design of the CS has been a collaborative effort between the US ITER Project Office (US ITER), the international ITER Organization (IO) and General Atomics (GA). GA’s responsibility includes: completing the fabrication design, developing and qualifying the fabrication processes and tools, and then completing the fabrication of the seven 110 tonne CS modules. The modules will be shipped separately to the ITER site, and then stacked and aligned in the Assembly Hall prior to insertion in the core of the ITER tokamak. A dedicated facility in Poway, California, USA has been established by GA to complete the fabrication of the seven modules. Infrastructure improvements included thick reinforced concrete floors, a diesel generator for backup power, along with, cranes for moving the tooling within the facility. The fabrication process for a single module requires approximately 22 months followed by five months of testing, which includes preliminary electrical testing followed by high current (48.5 kA) tests at 4.7K. The production of the seven modules is completed in a parallel fashion through ten process stations. The process stations have been designed and built with most stations having completed testing and qualification for carrying out the required fabrication processes. The final qualification step for each process station is achieved by the successful production of a prototype coil. Fabrication of the first

  4. A facile method to fabricate superhydrophobic cotton fabrics

    Science.gov (United States)

    Zhang, Ming; Wang, Shuliang; Wang, Chengyu; Li, Jian

    2012-11-01

    A facile and novel method for fabricating superhydrophobic cotton fabrics is described in the present work. The superhydrophobic surface has been prepared by utilizing cationic poly (dimethyldiallylammonium chloride) and silica particles together with subsequent modification of (heptadecafluoro-1,1,2,2-tetradecyl) trimethoxysilane. The size distribution of silica particles was measured by Particle Size Analyzer. The cotton textiles before and after treatment were characterized by using scanning electron microscope (SEM) and X-ray photoelectron spectroscopy (XPS). The wetting behavior of cotton samples was investigated by water contact angle measurement. Moreover, the superhydrophobic durability of coated cotton textiles has been evaluated by exposure, immersion and washing tests. The results show that the treated cotton fabrics exhibited excellent chemical stability and outstanding non-wettability with the WCA of 155 ± 2°, which offers an opportunity to accelerate the large-scale production of superhydrophobic textiles materials for new industrial applications.

  5. Fabrication of Nanoimprint stamps for photonic crystals

    International Nuclear Information System (INIS)

    Kouba, J; Kubenz, M; Mai, A; Ropers, G; Eberhardt, W; Loechel, B

    2006-01-01

    We report on fabrication of nanoimprint stamps for fabrication of two dimensional photonic crystals in visible range of spectra. Nanoimprint stamps made of silicon and/or nickel were successfully fabricated using electron beam lithography and advanced dry etching techniques. The quality of the stamps was evaluated using scanning electron microscopy. The fabricated stamps were also evaluated by imprinting them into suitable polymer materials

  6. Fabrication and characterization of Y{sub 2}O{sub 3} dispersion strengthened copper alloys

    Energy Technology Data Exchange (ETDEWEB)

    Carro, G.; Muñoz, A. [Departamento de Física, Universidad Carlos III de Madrid, 28911 Leganés (Spain); Monge, M.A., E-mail: mmonge@fis.uc3m.es [Departamento de Física, Universidad Carlos III de Madrid, 28911 Leganés (Spain); Savoini, B.; Pareja, R.; Ballesteros, C. [Departamento de Física, Universidad Carlos III de Madrid, 28911 Leganés (Spain); Adeva, P. [Centro Nacional de Investigaciones Metalúrgicas, CSIC, Av. Gregorio del Amo, 8, 28040 Madrid (Spain)

    2014-12-15

    Three copper base materials were fabricated following different routes: cast Cu–1 wt.%Y (C-Cu1Y) produced by vacuum induction melting, and Cu–1 wt.%Y (PM-Cu1Y) and Cu–1 wt.%Y{sub 2}O{sub 3} (PM-Cu1Y{sub 2}O{sub 3}) both processed by a powder metallurgy route and sintering by hot isostatic pressing. PM-Cu1Y alloy was prepared by cryomilling and PM-Cu1Y{sub 2}O{sub 3} by conventional milling at room temperature. The materials were characterized by X-ray diffraction, optical and electron microscopy and microhardness measurements. C-Cu1Y presents a characteristic eutectic microstructure while PM-Cu1Y{sub 2}O{sub 3} exhibits a composite like microstructure. Electron microscopy analyses of as-HIP PM-Cu1Y revealed irregular decoration of yttrium-rich oxides at the grain boundaries and an inhomogeneous dispersion of polygonal shaped yttrium-rich oxides dispersed in the Cu matrix. Tensile tests performed on PM-Cu–1Y on the temperature range of 293–773 K have showed a decrease of the yield strength at temperatures higher than 473 K, and monotonically decrease of the ultimate tensile strength and maximum plastic strain on increasing temperature.

  7. Metallic Reactor Fuel Fabrication for SFR

    Energy Technology Data Exchange (ETDEWEB)

    Song, Hoon; Kim, Jong-Hwan; Ko, Young-Mo; Woo, Yoon-Myung; Kim, Ki-Hwan; Lee, Chan-Bock [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of)

    2015-05-15

    The metal fuel for an SFR has such advantages such as simple fabrication procedures, good neutron economy, high thermal conductivity, excellent compatibility with a Na coolant, and inherent passive safety 1. U-Zr metal fuel for SFR is now being developed by KAERI as a national R and D program of Korea. The fabrication technology of metal fuel for SFR has been under development in Korea as a national nuclear R and D program since 2007. The fabrication process for SFR fuel is composed of (1) fuel slug casting, (2) loading and fabrication of the fuel rods, and (3) fabrication of the final fuel assemblies. Fuel slug casting is the dominant source of fuel losses and recycled streams in this fabrication process. Fabrication on the rod type metallic fuel was carried out for the purpose of establishing a practical fabrication method. Rod-type fuel slugs were fabricated by injection casting. Metallic fuel slugs fabricated showed a general appearance was smooth.

  8. Application of Box-Behnken Design and Response Surface Methodology for Surface Roughness Prediction Model of CP-Ti Powder Metallurgy Components Through WEDM

    Science.gov (United States)

    Das, Arunangsu; Sarkar, Susenjit; Karanjai, Malobika; Sutradhar, Goutam

    2018-04-01

    The present work was undertaken to investigate and characterize the machining parameters (such as surface roughness, etc.) of uni-axially pressed commercially pure titanium sintered powder metallurgy components. Powder was uni-axially pressed at designated pressure of 840 MPa to form cylindrical samples and the green compacts were sintered at 0.001 mbar for about 4 h with sintering temperature varying from 1350 to 1450 °C. The influence of the sintering temperature, pulse-on and pulse-off time at wire-EDM on the surface roughness of the preforms has been investigated thoroughly. Experiments were conducted under different machining parameters in a CNC operated wire-cut EDM. The surface roughness of the machined surface was measured and critically analysed. The optimum surface roughness was achieved under the conditions of 6 μs pulse-on time, 9 μs pulse-off time and at sintering temperature of 1450 °C.

  9. Effect the addition of 10% (volume fraction) chromium on the mechanical properties of NiAlCr processed by powder metallurgy

    International Nuclear Information System (INIS)

    Garcia-Barriocanal, J.; Garces, G.; Perez, P.; Adeva, P.

    2005-01-01

    The mechanical properties of Ni 3 Al-Cr reinforced with 10% in volume fraction of chromium particles produced by powder metallurgy have been studied. For this purpose, milled powders with composition of Ni-20.9Al-8Cr-0.49B (% st.) with and without the addition of 10% in volume fraction of chromium particles have been produced. Both alloys were consolidated by hot isostatic pressing (HIP). After HIP, heat treatment was applied to homogenize the microstructure. The chromium reinforcement has an important effect in the yield strength and ultimate strength increase. The reinforced alloy presents a yield strength of 1300 MPa at room temperature with respect to 800 MPa for the un-reinforced material. After heat treatment, the yield strength of both alloys does not change significantly. However, a decrease in ductility and ultimate tensile strength have been observed. (Author) 4 refs

  10. Application of Box-Behnken Design and Response Surface Methodology for Surface Roughness Prediction Model of CP-Ti Powder Metallurgy Components Through WEDM

    Science.gov (United States)

    Das, Arunangsu; Sarkar, Susenjit; Karanjai, Malobika; Sutradhar, Goutam

    2017-06-01

    The present work was undertaken to investigate and characterize the machining parameters (such as surface roughness, etc.) of uni-axially pressed commercially pure titanium sintered powder metallurgy components. Powder was uni-axially pressed at designated pressure of 840 MPa to form cylindrical samples and the green compacts were sintered at 0.001 mbar for about 4 h with sintering temperature varying from 1350 to 1450 °C. The influence of the sintering temperature, pulse-on and pulse-off time at wire-EDM on the surface roughness of the preforms has been investigated thoroughly. Experiments were conducted under different machining parameters in a CNC operated wire-cut EDM. The surface roughness of the machined surface was measured and critically analysed. The optimum surface roughness was achieved under the conditions of 6 μs pulse-on time, 9 μs pulse-off time and at sintering temperature of 1450 °C.

  11. SRF Cavity Fabrication and Materials

    CERN Document Server

    Singer, W

    2014-07-17

    The technological and metallurgical requirements of material for highgradient superconducting cavities are described. High-purity niobium, as the preferred metal for the fabrication of superconducting accelerating cavities, should meet exact specifications. The content of interstitial impurities such as oxygen, nitrogen, and carbon must be below 10μg/g. The hydrogen content should be kept below 2μg/g to prevent degradation of the Q-value under certain cool-down conditions. The material should be free of flaws (foreign material inclusions or cracks and laminations) that can initiate a thermal breakdown. Defects may be detected by quality control methods such as eddy current scanning and identified by a number of special methods. Conventional and alternative cavity fabrication methods are reviewed. Conventionally, niobium cavities are fabricated from sheet niobium by the formation of half-cells by deep drawing, followed by trim machining and Electron-Beam Welding (EBW). The welding of half-cells is a delicate...

  12. Study of the microstructural and mechanical properties of titanium-niobium-zirconium based alloys processed with hydrogen and powder metallurgy for use in dental implants

    International Nuclear Information System (INIS)

    Duvaizem, Jose Helio

    2009-01-01

    Hydrogen has been used as pulverization agent in alloys based on rare earth and transition metals due to its extremely high diffusion rate even on low temperatures. Such materials are used on hydrogen storage dispositives, generation of electricity or magnetic fields, and are produced by a process which the first step is the transformation of the alloy in fine powder by miling. Besides those, hydrogenium is also being used to obtain alloys based on titanium - niobium - zirconium in the pulverization. Powder metallurgy is utilized on the production of these alloys, making it possible to obtain structures with porous surface as result, requirement for its application as biomaterials. Other advantages of powder metallurgy usage include better surface finish and better microstructural homogeneity. In this work samples were prepared in the Ti-13Nb-13Zr composition. The hydrogenation was performed at 700 degree C, 600 degree C, and 500 degree C for titanium, niobium and zirconium respectively. After hydrogenation, the milling stage was carried out on high energy planetary ball milling with 200rpm during 90 minutes, and also in conventional ball milling for 30 hours. Samples were pressed in uniaxial press, followed by isostatic cold press, and then sintered at 1150 degree C for 7-13 hours. Microstructural properties of the samples were characterized by scanning electron microscope (SEM), energy dispersive spectroscopy (EDS) and x-ray diffraction. Mechanical and structural properties determined were density, microhardness and moduli of elasticity. The sample sintered at 1150 degree C for 7h, hydrogenated using 10.000 mbar and produced by milling on high energy planetary ball milling presented the best mechanical properties and microstructural homogeneity. (author)

  13. The shielding against radiation produced by powder metallurgy with tungsten copper alloy applied on transport equipment for radio-pharmaceutical products

    International Nuclear Information System (INIS)

    Cione, Francisco C.; Sene, Frank F.; Souza, Armando C. de; Betini, Evandro G.; Rossi, Jesualdo L.; Rizzuto, Marcia A.

    2015-01-01

    Safety is mandatory on medicine radiopharmaceutical transportation and dependent on radiation shielding material. The focus of the present work is to minimize the use of harmful materials as lead and depleted uranium usually used in packages transportation. The tungsten-copper composite obtained by powder metallurgy (PM) is non-toxic. In powder metallurgy the density and the porosity of the compacted parts depends basically upon particle size distribution of each component, mixture, compacting pressure and sintering temperature cycle. The tungsten-copper composite, when used for shielding charged particles, X-rays, gamma photons or other photons of lower energy require proper interpretation of the radiation transport phenomena. The radioactive energy reduction varies according to the porosity and density of the materials used as shielding. The main factor for radiation attenuation is the cross section value for tungsten. The motivation research factor is an optimization of the tungsten and cooper composition in order to achieve the best linear absorption coefficient given by equation I (x) = I 0 e (-ux) . Experiments were conducted to quantify the effective radiation shielding properties of tungsten-copper composite produced by PM, varying the cooper amount in the composite. The studied compositions were 15%, 20% and 25% copper in mass. The Compaction pressure was 270 MPa and the sintering atmosphere was in 1.1 atm in N 2 +H 2 . The sintering temperature was 980 deg C for 2 h. The linear absorption coefficient factor was similar either for the green and the sintered compacts, due the amount of porosity did not affect the radiation attenuation. Thus the sintered was meant for size reduction and mechanical properties enhancement. (author)

  14. Emission profiles of polychlorinated dibenzodioxins, polychlorinated dibenzofurans (PCDD/Fs), dioxin-like PCBs and hexachlorobenzene (HCB) from secondary metallurgy industries in Portugal.

    Science.gov (United States)

    Antunes, Pedro; Viana, Paula; Vinhas, Tereza; Rivera, J; Gaspar, Elvira M S M

    2012-09-01

    This paper reports, for the first time, a study of dioxin emissions from 10 siderurgies and metallurgies, secondary copper, aluminum and lead metallurgies, in Portugal. The study reports the emission factors and total emission amounts of PCDD/Fs, dioxin-like PCBs and hexachlorobenzene (HCB). The congener patterns were characterized and are discussed. The results showed that the total amount of PCDFs is higher than PCDDs in flue gas of each industrial unit. The toxic equivalent emission factors of pollutants emitted are 3098-3338 ngI-TEQt(-1) for PCDD/Fs and 597-659 ng I-TEQt(-1) for dioxin-like PCBs in siderurgies production (total estimated emission amounts released to atmosphere of 3.9-4.5 g I-TEQyr(-1)), 50-152 ng I-TEQt(-1) for PCDD/Fs and 24-121 ng I-TEQt(-1) for dioxin-like PCBs in ferrous foundries production (total estimated emission amounts released to atmosphere of 0.0010-0.0016 g I-TEQyr(-1)) and 5.8-5715 ng I-TEQt(-1) for PCDD/Fs and 0.49-259 ng I-TEQt(-1) for dioxin-like PCBs in non-ferrous foundries production (total estimated emission amounts released to atmosphere of 0.00014-0.12 g I-TEQyr(-1)). The HCB emission from siderurgies production is 0.94-3.2 mg t(-1) (total estimated emission amounts released 0.94-3.8 g yr(-1)), being much smaller, residual, in the emissions of the other types of plants (0.0012-0.026 mg t(-1) production and total estimated emission amounts released to atmosphere of 0.013-1.7 mg yr(-1)). Copyright © 2012 Elsevier Ltd. All rights reserved.

  15. Relevance of urinary 3-hydroxybenzo(a)pyrene and 1-hydroxypyrene to assess exposure to carcinogenic polycyclic aromatic hydrocarbon mixtures in metallurgy workers.

    Science.gov (United States)

    Barbeau, Damien; Persoons, Renaud; Marques, Marie; Hervé, Claire; Laffitte-Rigaud, Gilbert; Maitre, Anne

    2014-06-01

    In metallurgy, workers are exposed to mixtures of polycyclic aromatic hydrocarbons (PAHs) in which some compounds are carcinogenic. Biomonitoring of PAH exposure has been performed by measuring urinary 1-hydroxypyrene (1-OHP), a metabolite of pyrene which is not carcinogenic. This study investigated the use of 3-hydroxybenzo(a)pyrene (3-OHBaP), a metabolite of benzo(a)pyrene (BaP) which is the main carcinogenic component in PAHs, to improve carcinogen exposure assessment. We included 129 metallurgy workers routinely exposed to PAHs during working hours. Urinary samples were collected at three sampling times at the beginning and at the end of the working week for 1-OHP and 3-OHBaP analyses. Workers in anode production showed greater exposure to both biomarkers than those in cathode or silicon production, with respectively, 71, 40, and 30% of 3-OHBaP concentrations exceeding the value of 0.4 nmol mol(-1) creatinine. No difference was observed between the 3-OHBaP levels found at the end of the penultimate workday shift and those at the beginning of the last workday shift. Within these plants, the 1-OHP/3-OHBaP ratios varied greatly according to the workers' activity and emission sources. Using linear regression between these two metabolites, the 1-OHP level corresponding to the guidance value for 3-OHBaP ranged from 0.7 to 2.4 µmol mol(-1) creatinine, depending on the industrial sector. This study emphasizes the interest of monitoring urinary 3-OHBaP at the end of the last workday shift when working week exposure is relatively steady, and the irrelevance of a single guideline value for 1-OHP when assessing occupational health risk. © The Author 2014. Published by Oxford University Press on behalf of the British Occupational Hygiene Society.

  16. MQXFS1 Quadrupole Fabrication Report

    Energy Technology Data Exchange (ETDEWEB)

    Ambrosio, G. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Anerella, M. [Brookhaven National Lab. (BNL), Upton, NY (United States); Bossert, R. [European Organization for Nuclear Research (CERN), Geneva (Switzerland); Cavanna, E. [European Organization for Nuclear Research (CERN), Geneva (Switzerland); Cheng, D. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Chlachidize, G. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Cooley, L. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Dietderich, D. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Felice, H. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Ferracin, P. [European Organization for Nuclear Research (CERN), Geneva (Switzerland); Ghosh, A. [Brookhaven National Lab. (BNL), Upton, NY (United States); Hafalia, R. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Holik, E. F. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Bermudez, S. Izquierdo [European Organization for Nuclear Research (CERN), Geneva (Switzerland); Juchno, M. [European Organization for Nuclear Research (CERN), Geneva (Switzerland); Krave, S. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Marchevsky, M. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Muratore, J. [Brookhaven National Lab. (BNL), Upton, NY (United States); Nobrega, F. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Pan, H. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Perez, J. C. [European Organization for Nuclear Research (CERN), Geneva (Switzerland); Pong, I. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Prestemon, S. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Ravaioli, E. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Sabbi, G. L. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Santini, C. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Schmalzle, J. [Brookhaven National Lab. (BNL), Upton, NY (United States); Stoynev, S. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Strauss, T. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Vallone, G. [European Organization for Nuclear Research (CERN), Geneva (Switzerland); Wanderer, P. [Brookhaven National Lab. (BNL), Upton, NY (United States); Wang, X. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Yu, M. [Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States)

    2017-07-16

    This report presents the fabrication and QC data of MQXFS1, the first short model of the low-beta quadrupoles (MQXF) for the LHC High Luminosity Upgrade. It describes the conductor, the coils, and the structure that make the MQXFS1 magnet. Qualification tests and non-conformities are also presented and discussed. The fabrication of MQXFS1 was started before the finalization of conductor and coil design for MQXF magnets. Two strand design were used (RRP 108/127 and RRP 132/169). Cable and coil cross-sections were “first generation”.

  17. MQXFS1 Quadrupole Fabrication Report

    International Nuclear Information System (INIS)

    Ambrosio, G.; Anerella, M.; Bossert, R.; Cavanna, E.; Cheng, D.; Chlachidize, G.; Cooley, L.; Dietderich, D.; Felice, H.; Ferracin, P.; Ghosh, A.; Hafalia, R.; Holik, E. F.; Bermudez, S. Izquierdo; Juchno, M.; Krave, S.; Marchevsky, M.; Muratore, J.; Nobrega, F.; Pan, H.; Perez, J. C.; Pong, I.; Prestemon, S.; Ravaioli, E.; Sabbi, G. L.; Santini, C.; Schmalzle, J.; Stoynev, S.; Strauss, T.; Vallone, G.; Wanderer, P.; Wang, X.; Yu, M.

    2017-01-01

    This report presents the fabrication and QC data of MQXFS1, the first short model of the low-beta quadrupoles (MQXF) for the LHC High Luminosity Upgrade. It describes the conductor, the coils, and the structure that make the MQXFS1 magnet. Qualification tests and non-conformities are also presented and discussed. The fabrication of MQXFS1 was started before the finalization of conductor and coil design for MQXF magnets. Two strand design were used (RRP 108/127 and RRP 132/169). Cable and coil cross-sections were “first generation”.

  18. Fabrication Aware Form-finding

    DEFF Research Database (Denmark)

    Egholm Pedersen, Ole; Larsen, Niels Martin; Pigram, Dave

    2014-01-01

    parts. The first material system employs a novel rotated joint design to allow the structural tuning of quasi-reciprocal timber frame elements fabricated from multi-axis machined plywood sheet stock. The second em-loys discontinuous post-tensioning to assemble unique precast concrete components......This paper describes a design and construction method that combines two distinct material systems with fabrication aware form-finding and file-to-factory workflows. The method enables the fluent creation of complex materially efficient structures comprising high populations of geometrically unique...

  19. Advanced fabrication of hyperbolic metamaterials

    DEFF Research Database (Denmark)

    Shkondin, Evgeniy; Sukham, Johneph; Panah, Mohammad Esmail Aryaee

    2017-01-01

    Hyperbolic metamaterials can provide unprecedented properties in accommodation of high-k (high wave vector) waves and enhancement of the optical density of states. To reach such performance the metamaterials have to be fabricated with as small imperfections as possible. Here we report on our...... advances in two approaches in fabrication of optical metamaterials. We deposit ultrathin ultrasmooth gold layers with the assistance of organic material (APTMS) adhesion layer. The technology supports the stacking of such layers in a multiperiod construction with alumina spacers between gold films, which...

  20. List of unclassified documents by the staff of Metallurgy Division AERE Harwell from August 1980 to July 1982

    International Nuclear Information System (INIS)

    Winkless, M.S.

    1983-01-01

    The contents of the report have been provided by the following groups at AERE Harwell: Fast Reactor Fuels Group, Advanced Systems Group, Fracture Studies Group, Core Components and Structural Materials Group, radiation Effects Group, Composite Materials Group, High Voltage Microscope Group, Fabrication Technology Group and Management and Administration. AERE reports and memoranda are listed first followed by other literature; papers in periodicals, conference and symposia papers and lectures, books, articles and patent specifications. The information given is document type, title, author and date of publication (for papers). A total of 189 documents are listed. (U.K.)

  1. Fabrication of metallic glass structures

    Science.gov (United States)

    Cline, C.F.

    1983-10-20

    Amorphous metal powders or ribbons are fabricated into solid shapes of appreciable thickness by the application of compaction energy. The temperature regime wherein the amorphous metal deforms by viscous flow is measured. The metal powders or ribbons are compacted within the temperature regime.

  2. The Danish fabricated metal industry:

    DEFF Research Database (Denmark)

    Hansen, Teis

    2010-01-01

    . This is less the case for low-tech industries, but their economic importance continues to be large, however. It is thus interesting to analyse how they manage to remain competitive. The analysis focuses on a case study of the fabricated metal industry by identifying the innovation strategies followed by firms...

  3. Fabrication of green polymeric membranes

    KAUST Repository

    Kim, Dooli

    2017-06-16

    Provided herein are methods of fabricating membranes using polymers with functionalized groups such as sulfone (e.g., PSf and PES), ether (e.g., PES), acrylonitrile (e.g., PAN), fluoride(e.g., pvdf and other fluoropolymers), and imide (e.g., extem) and ionic liquids. Also provided are membranes made by the provided methods.

  4. Transverse permeability of woven fabrics

    NARCIS (Netherlands)

    Grouve, Wouter Johannes Bernardus; Akkerman, Remko; Loendersloot, Richard; van den Berg, S.

    2008-01-01

    The transverse permeability is an essential input in describing the consolidation process of CETEX® laminates. A two-dimensional, finite difference based, Stokes flow solver has been developed to determine the mesoscopic permeability of arbitrary fabric structures. The use of a multigrid solver

  5. Microfluidic fabrication of plasmonic microcapsules

    NARCIS (Netherlands)

    Wang, J.; Jin, Mingliang; Eijkel, Jan C.T.; van den Berg, Albert; Zhou, G.F.; Shui, L.L.

    2016-01-01

    This paper presents the plasmonic microcapsules with well-ordered nanoparticles embedded in polymer network fabricated by using a microfluidic device. The well-ordered nanoparticle arrays on the microcapsule form high-density uniform “hot-spots‿ with a deposited metal film, on which the localized

  6. Fabrication Aware Form-finding

    DEFF Research Database (Denmark)

    Egholm Pedersen, Ole; Larsen, Niels Martin; Pigram, Dave

    2014-01-01

    This paper describes a design and construction method that combines two distinct material systems with fabrication aware form-finding and file-to-factory workflows. The method enables the fluent creation of complex materially efficient structures comprising high populations of geometrically uniqu...

  7. Fabrication of CANDU dupic fuel

    International Nuclear Information System (INIS)

    Sullivan, J.D.; Ryz, M.A.; Lee, J.W.

    1999-01-01

    An important new fuel cycle that exploits the synergism between CANDU and pressurized-water reactors (PWRs) is the Direct Use of spent PWR Fuel in CANDU (DUPIC). In this fuel cycle, spent PWR fuel is reconfigured, using only dry processing techniques, to make it compatible with a CANDU reactor. The dry processing technique is inherently simpler than wet chemical processing techniques used for recycling spent fuel. Actinides and fission products are retained in the fuel, so that DUPIC fuel is highly radioactive, affording the fuel cycle a high degree of proliferation resistance. AECL's project to develop the fuel cycle has now progressed to the stage of fabricating DUPIC fuel elements for irradiation testing in a research reactor. The goal of this phase of the project is to demonstrate that the DUPIC fuel cycle is technically feasible. A major part of the technical feasibility study is demonstration of the irradiation performance of DUPIC fuel under CANDU conditions. Spent PWR fuel has been subjected to the oxidation and reduction of oxide fuels (OREOX) process, and the resulting powder has been fabricated into CANDU-quality pellets. The DUPIC pellets have been loaded into fuel elements for irradiation testing in the NRU research reactor at the Chalk River Laboratories. The fabrication stages included spent fuel decladding, powder production using the OREOX process, powder milling (to improve sinterability), pellet pressing, sintering, centreless grinding, element loading and element welding. This paper details the fabrication of the DUPIC pellets and elements and initial results of their characterization. The equipment used for fabrication of the DUPIC fuel elements is described, and the irradiation plan for these elements is also outlined. (author)

  8. Laser target fabrication, structure and method for its fabrication

    Science.gov (United States)

    Farnum, Eugene H.; Fries, R. Jay

    1985-01-01

    The disclosure is directed to a laser target structure and its method of fabrication. The target structure comprises a target plate containing an orifice across which a pair of crosshairs are affixed. A microsphere is affixed to the crosshairs and enclosed by at least one hollow shell comprising two hemispheres attached together and to the crosshairs so that the microsphere is juxtapositioned at the center of the shell.

  9. Preparation of activated carbon fabrics from cotton fabric precursor

    Science.gov (United States)

    Salehi, R.; Dadashian, F.; Abedi, M.

    2017-10-01

    The preparation of activated carbon fabrics (ACFs) from cotton fabric was performed by chemical activation with phosphoric acid (H3PO4). The operation conditions for obtaining the ACFs with the highest the adsorption capacity and process yield, proposed. Optimized conditions were: impregnation ratio of 2, the rate of temperature rising of 7.5 °C min-1, the activation temperature of 500 °C and the activation time of 30 min. The ACFs produced under optimized conditions was characterized by scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX). The surface area and pore volume of carbon nanostructures was characterized by BET nitrogen adsorption isotherm at 77 °K. The pore size distribution calculated from the desorption branch according to BJH method. The iodine number of the prepared ACFs was determined by titration at 30 °C based on the ASTM D4607-94. The results showed the improvement of porous structure, fabric shape, surface area (690 m2/g), total pore volume (0.3216 cm3/g), and well-preserved fibers integrity.

  10. Qualitative Investigation of Some Locally Produced Printed Fabrics ...

    African Journals Online (AJOL)

    The results obtained showed that the locally produced fabrics exhibited comparably better end – use performance characteristics in terms of fabric weight per square meter, fabric flammability, and linear density. While the foreign fabrics are better in terms of Crease recovery, fabric handle, fabric sett, fabric shrinkage, and ...

  11. Nylon fabric reinforced natural rubber compound

    Science.gov (United States)

    Kamal, Mazlina Mustafa; Ismail, Ismaliza

    2017-12-01

    Rubber fabric coated is a unique rubber-textile composite, in which technical textile acts as reinforcing material and strength providing material. In rubber textile composite, rubber to fabric adhesion plays the most critical role for determining assembly process and ultimate strength of product. A vulcanisable adhesive for rubber to fabric fabrication of composite material was developed which compatible with rubber as well as fabric. Evaluation of bonding system with respect to peel strength, shear adhesion strength and weave pattern of fabrics were the major determining criteria for selection and optimization of fabric for rubber hose application. Thus adhesive Cohedure with characteristics of high adhesive strength in Natural Rubber Polyester Fabric compound has been developed.

  12. Nanosensor Fabrication with 3D Manufacturing Techniques

    Data.gov (United States)

    National Aeronautics and Space Administration — We use 3D manufacturing techniques to fabricate sensors based on nanomaterials. We use 3D manufacturing techniques to fabricate sensors based on nanomaterials. This...

  13. Paving fabrics for reducing reflective cracking

    Science.gov (United States)

    1991-11-01

    This research effort was part of ADOT's New Product Evaluation Program. The objective was to evaluate the construction and field performances of three commercially available paving fabrics; Paveprep, Glassgrid, and Tapecoat. The fabrics were designed...

  14. Fabric quality issues related to apparel merchandising

    CSIR Research Space (South Africa)

    Das, Sonali

    2015-02-01

    Full Text Available The objectives of this study are to develop an understanding of fabric quality related issues and research gaps relevant to apparel manufacturing and merchandising within the South African context. The specific focus is on fabric objective...

  15. On the effect of TiC particles on the tensile properties and on the intrinsic two way effect of NiTi shape memory alloys produced by powder metallurgy

    International Nuclear Information System (INIS)

    Johansen, K.; Voggenreiter, H.; Eggeler, G.

    1999-01-01

    The present study investigates the tensile properties of a nickel titanium (NiTi) shape memory alloy (SMA) produced by powder metallurgy (PM) with and without TiC-particles. It discusses the effect of the addition of particles on the mechanical behavior in tension and studies the intrinsic two way effect (ε 2W ) after thermomechanical training. Special emphasis is placed on the stability of ε 2W after subsequent thermal cycling. The results are discussed on the basis of an analysis of the thermomechanical data and microstructural results. The present study shows that the PM route can produce NiTi SMAs with tensile properties which match those of materials produced by classical ingot metallurgy. Adding TiC particles to NiTi SMAs alters the phase transition temperatures (PTTs) and affects the SMA performance. Adding more than ten volume percent TiC particles results in early and brittle rupture during tensile loading. (orig.)

  16. The fabrication of nuclear fuel

    International Nuclear Information System (INIS)

    D'Amore, Mead

    1987-01-01

    The chronology of fuel product and core management development over the past 25 years in the USA is explained. Nuclear fuel for Westinghouse reactors is made by converting enriched uranium hexafluoride (UF 6 ) into uranium dioxide (UO 2 ) powder. The powder is pressed into pellets which are loaded into zircalloy fuel tubes (typically over 14 million pellets in 50,952 rods). The fuel rods are arranged in fuel assemblies which are shipped to the reactor site (typically 193 fuel assemblies are needed for one 1000MWe reactor). Each stage of the fuel fabrication cycle (cladding manufacture, chemical conversion UF 6 - UO 2 , pellet production, fuel rod fabrication, grid assembly, skeleton assembly, fuel assembly) is described, with particular reference to the Westinghouse process and plant. (UK)

  17. Quality in the fabrication process

    International Nuclear Information System (INIS)

    Romano, A.; Aguirre, F.

    2010-01-01

    Enusa commitment to quality in the manufacture process materializes in the application of the most advanced product quality control technologies such as not-destructive inspection techniques, like artificial vision, X-ray or UT inspection, or process parameter statistical control systems. Quality inspectors are trained and certified by the main National Quality Organizations and receive periodic training under a formal company training program that constantly updates their qualification. Fabrication quality control reliability is based on a strategy that prioritizes redundancy of critical inspection equipment's and inspection personnel knowledge polyvalence. Furthermore, improvement in fabrication quality is obtained by a systematic application of the six sigma methodology where added value is created in projects integrating crosscutting company knowledge, reinforcing the global company vision that the fuel business is based on quality. (Author)

  18. Solid Freeform Fabrication Proceedings -1999

    Science.gov (United States)

    1999-08-11

    noded bilinear thermal elements are used as part of the ABAQUS finite element software package. The laser beam focused on the top surface of substrate...with the PDM technology. The advantage of SDM is that refractory metals can be melted with the plasma-welding torch. In 3-D Printing, a green part is...Freeform Growth. I. Introduction Previous efforts in vapor-phase solid freeform fabrication have concentrated on the growth of transition and refractory

  19. Nanocarbon materials fabricated using plasmas

    Science.gov (United States)

    Hatakeyama, Rikizo

    2017-12-01

    Since the discovery of fullerenes more than three decades ago, new kinds of nanoscale materials of carbon allotropes called "nanocarbons" have so far been discovered or synthesized at successive intervals as cases such as carbon nanotubes, carbon nanohorns, graphene, carbon nanowalls, and a carbon nanobelt, while nanodiamonds were actually discovered before then. Their attractively excellent mechanical, physical, and chemical properties have driven researchers to continuously create one of the hottest frontiers in materials science and technology. While plasma states have often been involved in their discovery, on the other hand, plasma-based approaches to this exciting field originally hold promising and enormous potentials for advancing and expanding industrial/biomedical applications of nanocarbons of great diversity. This article provides an extensive overview on plasma-fabricated nanocarbon materials, where the term "fabrication" is defined as synthesis, functionalization, and assembly of devices to cover a wide range of issues associated with the step-by-step plasma processes. Specific attention has been paid to the comparative examination between plasma-based and non-plasma methods for fabricating the nanocarobons with an emphasis on the advantages of plasma processing, such as low-temperature/large-scale fabrication and diversity-carrying structure controllability. The review ends with current challenges and prospects including a ripple effect of the nanocarbon studies on the development of related novel nanomaterials such as transition metal dichalcogenides. It contains not only the latest progress in the field for cutting-edge scientists and engineers, but also the introductory guidance to non-specialists such as lower-class graduate students.

  20. Zircaloy 4 ingots' industrial fabrication

    International Nuclear Information System (INIS)

    Leyt, A.

    1987-01-01

    The technology developed for the industrial fabrication of Zircaloy-4 ingots is presented. According to the results obtained: a) the homogeneity of the ingots is analyzed, regarding the distribution of components (tin, iron, chromium, oxygen) and Brinell hardness as a function of different types of charge: zirconium sponge-recycling alloy material, sponge of zirconium-alloy; b) the distribution of the same parameters as a function of production is also analyzed. (Author)

  1. Possibilities for increasing the purity of steel in production using secondary-metallurgy equipment: Možnosti povečanja čistosti jekla pri proizvodnji z uporabo opreme za sekundarno metalurgijo:

    OpenAIRE

    Čamek, Libor; Korbáš, Martin; Raclavský, Milan

    2014-01-01

    The possibilities for increasing the purity of steel during the production of the liquid phase using secondary metallurgy mainly relate to affecting the number of emerging occlusions, their size, morphology and chemical composition. The metallographic purity of steel during production in an electric-arc furnace (EAF), in a ladle furnace (LF) and during processing with VD caisson technology was assessed. The steel samples were processed by means of an electron microscope and were simultaneousl...

  2. Obtenção de titânio metálico com porosidade controlada por metalurgia do pó Porous titanium production and porosity control by powder metallurgy (P/M)

    OpenAIRE

    Neila de Almeida Braga; Neidenêi Gomes Ferreira; Carlos Alberto Alves Cairo

    2007-01-01

    Titanium is an attractive material for structural and biomedical applications because of its excellent corrosion resistance, biocompatibility and high strength-to-weight ratio. The high reactivity of titanium in the liquid phase makes it difficult to produce it by fusion. Powder metallurgy has been shown to be an adequate technique to obtain titanium samples at low temperatures and solid-phase consolidation. The production of compacts with different porosities obtained by uniaxial pressing an...

  3. Fabrication technology for ODS Alloy MA957

    International Nuclear Information System (INIS)

    ML Hamilton; DS Gelles; RJ Lobsinger; MM Paxton; WF Brown

    2000-01-01

    A successful fabrication schedule has been developed at Carpenter Technology Corporation for the production of MA957 fuel and blanket cladding. Difficulties with gun drilling, plug drawing and recrystallization were overcome to produce a pilot lot of tubing. This report documents the fabrication efforts of two qualified vendors and the support studies performed at WHC to develop the fabrication-schedule

  4. Natural fabric sandwich laminate composites: development and ...

    Indian Academy of Sciences (India)

    Home; Journals; Bulletin of Materials Science; Volume 40; Issue 1 ... Natural fabrics; jute; linen; sandwich laminate; mechanical properties; fractographic analysis. ... In this work, eco-friendly natural fabric sandwich laminate (NFSL) composites are formulated using jute and linen-fabric-reinforced epoxy with different layer ...

  5. Method for fabricating semiconductor devices

    Science.gov (United States)

    Kaiser, William J. (Inventor); Grunthaner, Frank J. (Inventor); Hecht, Michael H. (Inventor); Bell, Lloyd D. (Inventor)

    1995-01-01

    A process for fabricating gold/gallium arsenide structures, in situ, on molecular beam epitaxially grown gallium arsenide. The resulting interface proves to be Ohmic, an unexpected result which is interpreted in terms of increased electrode interdiffusion. More importantly, the present invention surprisingly permits the fabrication of Ohmic contacts in a III-V semiconductor material at room temperature. Although it may be desireable to heat the Ohmic contact to a temperature of, for example, 200 degrees Centigrade if one wishes to further decrease the resistance of the contact, such low temperature annealing is much less likely to have any deleterious affect on the underlying substrate. The use of the term in situ herein, contemplates continuously maintaining an ultra-high vacuum, that is a vacuum which is at least 10.sup.-8 Torr, until after the metallization has been completed. An alternative embodiment of the present invention comprising an additional step, namely the termination of the gallium arsenide by a two monolayer thickness of epitaxial aluminum arsenide as a diffusion barrier, enables the recovery of Schottky barrier behavior, namely a rectified I-V characteristic. The present invention provides a significant breakthrough in the fabrication of III-V semiconductor devices wherein excellent Ohmic contact and Schottky barrier interfaces to such devices can be achieved simply and inexpensively and without requiring the high temperature processing of the prior art and also without requiring the use of exotic high temperature refractory materials as substitutes for those preferred contact metals such as gold, aluminum and the like.

  6. Phosphorene: Fabrication, Properties, and Applications.

    Science.gov (United States)

    Kou, Liangzhi; Chen, Changfeng; Smith, Sean C

    2015-07-16

    Phosphorene, the single- or few-layer form of black phosphorus, was recently rediscovered as a two-dimensional layered material holding great promise for applications in electronics and optoelectronics. Research into its fundamental properties and device applications has since seen exponential growth. In this Perspective, we review recent progress in phosphorene research, touching upon topics on fabrication, properties, and applications; we also discuss challenges and future research directions. We highlight the intrinsically anisotropic electronic, transport, optoelectronic, thermoelectric, and mechanical properties of phosphorene resulting from its puckered structure in contrast to those of graphene and transition-metal dichalcogenides. The facile fabrication and novel properties of phosphorene have inspired design and demonstration of new nanodevices; however, further progress hinges on resolutions to technical obstructions like surface degradation effects and nonscalable fabrication techniques. We also briefly describe the latest developments of more sophisticated design concepts and implementation schemes that address some of the challenges in phosphorene research. It is expected that this fascinating material will continue to offer tremendous opportunities for research and development for the foreseeable future.

  7. Micro Machining Enhances Precision Fabrication

    Science.gov (United States)

    2007-01-01

    Advanced thermal systems developed for the Space Station Freedom project are now in use on the International Space Station. These thermal systems employ evaporative ammonia as their coolant, and though they employ the same series of chemical reactions as terrestrial refrigerators, the space-bound coolers are significantly smaller. Two Small Business Innovation Research (SBIR) contracts between Creare Inc. of Hanover, NH and Johnson Space Center developed an ammonia evaporator for thermal management systems aboard Freedom. The principal investigator for Creare Inc., formed Mikros Technologies Inc. to commercialize the work. Mikros Technologies then developed an advanced form of micro-electrical discharge machining (micro-EDM) to make tiny holes in the ammonia evaporator. Mikros Technologies has had great success applying this method to the fabrication of micro-nozzle array systems for industrial ink jet printing systems. The company is currently the world leader in fabrication of stainless steel micro-nozzles for this market, and in 2001 the company was awarded two SBIR research contracts from Goddard Space Flight Center to advance micro-fabrication and high-performance thermal management technologies.

  8. Fabrication of plastic microfluidic components

    Science.gov (United States)

    Martin, Peter M.; Matson, Dean W.; Bennett, Wendy D.; Hammerstrom, D. J.

    1998-09-01

    Plastic components have many advantages, including ease of fabrication, low cost, chemical inertness, lightweight, and disposability. We report on the fabrication of three plastics-based microfluidic components: a motherboard, a dialysis unit, and a metal sensor. Microchannels, headers, and interconnects were produced in thin sheets (>=50 microns) of polyimide, PMMA, polyethylene, and polycarbonate using a direct-write excimer laser micromachining system. Machined sheets were laminated by thermal and adhesive bonding to form leak-tight microfluidic components. The microfluidic motherboard borrowed the `functionality on a chip' concept from the electronics industry and was the heart of a complex microfluidic analytical device. The motherboard platform was designed to be tightly integrated and self-contained (i.e., liquid flows are all confined within machined microchannels), reducing the need for tubing with fluid distribution and connectivity. This concept greatly facilitated system integration and miniaturization. As fabricated, the motherboard consisted of three fluid reservoirs connected to micropumps by microchannels. The fluids could either be pumped independently or mixed in microchannels prior to being directed to exterior analytical components via outlet ports. The microdialysis device was intended to separate electrolytic solutes from low volume samples prior to mass spectrometric analysis. The device consisted of a dialysis membrane laminated between opposed serpentine microchannels containing the sample fluid and a buffer solution. The laminated metal sensor consisted of fluid reservoirs, micro-flow channels, micropumps, mixing channels, reaction channels, and detector circuitry.

  9. Characterization of Ni{sub 5}3.5-Fe{sub 1}9.5-Ga{sub 2}7 Ni{sub 5}3.5 ferromagnetic shape memory alloy produced by powder metallurgy; Caracterizacion de la aleacion Ni{sub 5}3.5-Fe{sub 1}9.5-Ga{sub 2}7 con memoria de forma ferromagnetica producida por metalurgia de polvos

    Energy Technology Data Exchange (ETDEWEB)

    Olmos, L.; Alvarado-Hernandez, F.; Omar Jimenez, H.; Vergara-Hernandez, J.; Arroyo Albiter, M.; Ochoa-Gamboa, R. A.

    2015-07-01

    The main drawback of ferromagnetic shape memory alloys fabricated through casting methods are its brittleness. In order to overcome this disadvantage, powder metallurgy is an ideal technique for the consolidation of many engineering parts. This paper is focused on the study of the milling and sintering effects of metallic powders over the evolution of the crystalline phases responsibly for the shape memory effect of these materials. To achieve this objective, ferromagnetic shape memory alloy powders (Ni{sub 5}3.5-Fe{sub 1}9.5-Ga{sub 2}7) were prepared from a cast ingot by mechanical milling at two different times of 30 and 60 minutes. The evolution of the phases was investigated through high temperature X-ray diffraction (HTXRD), whereas sintering was analyzed with dilatometry tests. X-ray studies showed that four different phases can be present depending on the particle size and temperature at which the heat treatment was performed. Coarser powders showed a B2 structure along with a γ phase while the finer showed a L21 structure when treated below 1173 K. Furthermore, finer powders had a modulated M14 martensitic structure after sintering at temperatures above 1273 K. The sintering of powders was slow and a mass diffusion mechanism was not clearly observed. (Author)

  10. High-Thermal-Conductivity Fabrics

    Science.gov (United States)

    Chibante, L. P. Felipe

    2012-01-01

    Heat management with common textiles such as nylon and spandex is hindered by the poor thermal conductivity from the skin surface to cooling surfaces. This innovation showed marked improvement in thermal conductivity of the individual fibers and tubing, as well as components assembled from them. The problem is centered on improving the heat removal of the liquid-cooled ventilation garments (LCVGs) used by astronauts. The current design uses an extensive network of water-cooling tubes that introduces bulkiness and discomfort, and increases fatigue. Range of motion and ease of movement are affected as well. The current technology is the same as developed during the Apollo program of the 1960s. Tubing material is hand-threaded through a spandex/nylon mesh layer, in a series of loops throughout the torso and limbs such that there is close, form-fitting contact with the user. Usually, there is a nylon liner layer to improve comfort. Circulating water is chilled by an external heat exchanger (sublimator). The purpose of this innovation is to produce new LCVG components with improved thermal conductivity. This was addressed using nanocomposite engineering incorporating high-thermalconductivity nanoscale fillers in the fabric and tubing components. Specifically, carbon nanotubes were added using normal processing methods such as thermoplastic melt mixing (compounding twin screw extruder) and downstream processing (fiber spinning, tubing extrusion). Fibers were produced as yarns and woven into fabric cloths. The application of isotropic nanofillers can be modeled using a modified Nielsen Model for conductive fillers in a matrix based on Einstein s viscosity model. This is a drop-in technology with no additional equipment needed. The loading is limited by the ability to maintain adequate dispersion. Undispersed materials will plug filtering screens in processing equipment. Generally, the viscosity increases were acceptable, and allowed the filled polymers to still be

  11. Facile fabrication of a superhydrophobic fabric with mechanical stability and easy-repairability.

    Science.gov (United States)

    Zhu, Xiaotao; Zhang, Zhaozhu; Yang, Jin; Xu, Xianghui; Men, Xuehu; Zhou, Xiaoyan

    2012-08-15

    The poor mechanical stability of superhydrophobic fabrics severely hindered their use in practical applications. Herein, to address this problem, we fabricated a superhydrophobic fabric with both mechanical stability and easy-repairability by a simple method. The mechanical durability of the obtained superhydrophobic fabric was evaluated by finger touching and abrasion with sandpaper. The results show that rough surface textures of the fabric were retained, and the fabric surface still exhibited superhydrophobicity after tests. More importantly, when the fabric lost its superhydrophobicity after a long-time abrasion, it can be easily rendered with superhydrophobicity once more by a regeneration process. Copyright © 2012 Elsevier Inc. All rights reserved.

  12. Innovative Application of Fabric Recycling in Fashion

    Directory of Open Access Journals (Sweden)

    Chenyang Lee

    2017-10-01

    Full Text Available With the continuous development of the socialist market economy, human aesthetic standards are constantly changing, the occurrence of this situation to the development of the garment industry challenges, that is a single fabric has long been unable to meet people's aesthetic needs, And then the art of fabric reengineering will be born. This paper elaborates the meaning of fabric reworking art. This paper systematically describes the meaning of fabric reengineering to garment designer and garment itself, and comprehensively summarizes the fabric recycling technique and its characteristics.

  13. Micro-fabricated all optical pressure sensors

    DEFF Research Database (Denmark)

    Havreland, Andreas Spandet; Petersen, Søren Dahl; Østergaard, Christian

    2017-01-01

    Optical pressure sensors can operate in certain harsh application areas where the electrical pressure sensors cannot. However, the sensitivity is often not as good for the optical sensors. This work presents an all optical pressure sensor, which is fabricated by micro fabrication techniques, where...... the sensitivity can be tuned in the fabrication process. The developed sensor design, simplifies the fabrication process leading to a lower fabrication cost, which can make the all optical pressure sensors more competitive towards their electrical counterpart. The sensor has shown promising results and a linear...

  14. Remote fabrication of nuclear fuel: a secure automated fabrication overview

    International Nuclear Information System (INIS)

    Nyman, D.H.; Benson, E.M.; Yatabe, J.M.; Nagamoto, T.T.

    1981-01-01

    An automated line for the fabrication of breeder reactor fuel pins is being developed. The line will be installed in the Fuels and Materials Examination Facility (FMEF) presently under construction at the Hanford site near Richland, Washington. The application of automation and remote operations to fuel processing technology is needed to meet program requirements of reduced personnel exposure, enhanced safeguards, improved product quality, and increased productivity. Commercially available robots are being integrated into operations such as handling of radioactive material within a process operation. These and other automated equipment and chemistry analyses systems under development are described

  15. Properties of honeycomb polyester knitted fabrics

    Science.gov (United States)

    Feng, A. F.

    2016-07-01

    The properties of honeycomb polyester weft-knitted fabrics were studied to understand their advantages. Seven honeycomb polyester weft-knitted fabrics and one common polyester weft-knitted fabric were selected for testing. Their bursting strengths, fuzzing and pilling, air permeability, abrasion resistance and moisture absorption and perspiration were studied. The results show that the honeycomb polyester weft-knitted fabrics have excellent moisture absorption and liberation. The smaller their thicknesses and area densities are, the better their moisture absorption and liberation will be. Their anti-fuzzing and anti-pilling is good, whereas their bursting strengths and abrasion resistance are poorer compared with common polyester fabric's. In order to improve the hygroscopic properties of the fabrics, the proportion of the honeycomb microporous structure modified polyester in the fabrics should not be less than 40%.

  16. Design Thinking for Digital Fabrication in Education

    DEFF Research Database (Denmark)

    Smith, Rachel Charlotte; Iversen, Ole Sejer; Hjorth, Mikkel

    2015-01-01

    In this paper, we argue that digital fabrication in education may benefit from design thinking, to foster a more profound understanding of digital fabrication processes among students. Two related studies of digital fabrication in education are presented in the paper. In an observational study we...... found that students (eleven to fifteen) lacked an understanding of the complexity of the digital fabrication process impeding on the potentials of digital fabrication in education. In a second explorative research through design study, we investigated how a focus on design thinking affected the students......’ performance in digital fabrication processes. Our findings indicate that design thinking can provide students with a general understanding of the creative and complex process through which artifacts and futures emerge in processes of digital fabrication....

  17. DESIGN AND FABRICATION OF MICRONOZZLES

    Directory of Open Access Journals (Sweden)

    Kean How Cheah

    2011-05-01

    Full Text Available Normal 0 false false false EN-US ZH-CN X-NONE MicrosoftInternetExplorer4 /* Style Definitions */ table.MsoNormalTable {mso-style-name:"Table Normal"; mso-tstyle-rowband-size:0; mso-tstyle-colband-size:0; mso-style-noshow:yes; mso-style-priority:99; mso-style-qformat:yes; mso-style-parent:""; mso-padding-alt:0in 5.4pt 0in 5.4pt; mso-para-margin:0in; mso-para-margin-bottom:.0001pt; mso-pagination:widow-orphan; font-size:11.0pt; font-family:"Calibri","sans-serif"; mso-ascii-font-family:Calibri; mso-ascii-theme-font:minor-latin; mso-fareast-font-family:SimSun; mso-fareast-theme-font:minor-fareast; mso-hansi-font-family:Calibri; mso-hansi-theme-font:minor-latin; mso-bidi-font-family:"Times New Roman"; mso-bidi-theme-font:minor-bidi;} Micronozzle, a key component in micropropulsion system, has been designed and fabricated. Quasi 1D inviscid theory was used in designing a series of conical micronozzles of different expander half-angles (10°-50°. Aerospike micronozzle, a promising candidate to achieve high performance propulsion system, was designed with Angelino method (or Approximate method. Both micronozzles were fabricated using soft lithography, an inexpensive and relatively simple technique comparing to well-established deep reactive ion etching (DRIE technique, with polydimethylsiloxane (PDMS as structural material. Micronozzles with two different nozzle throat width, 53.5µm and 107µm, were fabricated for comparison. Microscopic inspections reveal 107µm is the more producible nozzle throat width with current equipments. The PDMS-based micronozzle can be used as cold gas microthruster system for micro- and nanosatellites.

  18. Application of the ecologically clean technology of mining metallurgy and power industry wastes recycling based on the use of electron beams

    International Nuclear Information System (INIS)

    Mazhrenova, N.R.; Askarova, G.Sh.

    1997-01-01

    Advantage of electron beam technologies application for industrial wastes recycling is illustrated for following trends: 1).Off gases of mining metallurgy and the thermal power plant can be refined from SO 2 and NO x toxic combination by means of their further chemical and radiation oxidation with following obtaining of acids on the base industrial accelerator ELV-8. In this method a radiation-chemical process in irradiated gas results in excited complexes, radicals and ion formation. Ion cause the activation of reaction chain which convert SO 2 and NO x toxic gases into the combination with high number of oxidation. In presence of water, coming from drip cooler, the combination of sulphuric and nitric acids neutralization results in the obtaining of ammonium solid combination which are mainly sulphates and nitrates; 2). For waste water refinement from organic pollution, for instance butyl xanthate, ions of heavy metals and etc.; 3). For non-ferrous, sparse and and dispersed metal extraction from the cinder and slag wastes. Different technological schemes for mineral extraction are elaborated

  19. Study of tribological properties on Al/Al2O3/MoS2 hybrid composite processed by powder metallurgy

    Directory of Open Access Journals (Sweden)

    K. Kanthavel

    2016-03-01

    Full Text Available Aluminium ceramic composites with improved mechanical and chemical properties are essential and needed in aerospace and automotive application. The aluminium matrix composite reinforced with ceramic material of alumina (Al2O3 has good tribological properties. However, aluminium based ceramic composites require improvements in their lubrication properties. In this study an attempt is made in the development of a new material through powder metallurgy technique by the addition of molybdenum disulphide (MoS2, which acts as a solid lubricant. This molybdenum disulphide (MoS2 based solid lubricant has unique advantage that it can be used in vacuum space, but the same is not applicable in case of graphite. The microstructures, material combination, wear and friction properties were analysed by scanning electron microscopy, EDX, and pin-on-disc wear tester. The newly developed aluminium composite has significant improvements in tribological properties with a combination of 5% alumina (Al2O3 and 5% molybdenum disulphide (MoS2. The test reveals that sliding distance of 1000 m and sliding speed of 1.5 m/s with applied load of 5 N result in minimum wear loss of 0.0102 g and coefficient of friction as 0.117.

  20. Risk Assessment of Potentially Toxic Elements (PTEs Pollution at a Rural Industrial Wasteland in an Abandoned Metallurgy Factory in North China

    Directory of Open Access Journals (Sweden)

    Zheng Sun

    2018-01-01

    Full Text Available The potential toxic elements (PTEs pollution problems in many rural industrial wastelands have been observed to be conspicuous. Therefore, 40 top soil samples were collected from the wasteland of a typical rural metallurgy factory in Baoding, China. The total concentrations of six key PTEs were measured. The soil properties and speciation of the PTEs were also identified. Extremely high concentrations of As, Cd, Pb, and Zn were observed in the surface soils. Using the PTEs concentration in the top soils of the rural industrial wasteland, the following indices of pollution were calculated: the pollution load index (PLI, the geo-accumulation Index (Igeo, the risk assessment code (RAC, and the health risk assessment (HRA. The analysis of the PLI and Igeo indicated that site #1 was relatively clean, while sites #2 and #3 were heavily polluted. The results of the RAC showed that PTEs in top soils at sites #2 and #3 were significantly increased (p <  0.05 for Cd and Zn. The HRA indicated that both As and Pb presented non-carcinogenic risks to children and adults at sites #2 and #3. Our findings can be a reference for risk prevention of industrially abandoned land in rural China.

  1. Effects of long-time elevated temperature exposures on hot-isostatically-pressed power-metallurgy Udimet 700 alloys with reduced cobalt contents

    Science.gov (United States)

    Hart, F. H.

    1984-01-01

    Because almost the entire U.S. consumption of cobalt depends on imports, this metal has been designated "strategic'. The role and effectiveness of cobalt is being evaluated in commercial nickel-base superalloys. Udiment 700 type alloys in which the cobalt content was reduced from the normal 17% down to 12.7%, 8.5%, 4.3%, and 0% were prepared by standard powder metallurgy techniques and hot isostatically pressed into billets. Mechanical testing and microstructural investigations were performed. The mechanical properties of alloys with reduced cobalt contents which were heat-treated identically were equal or better than those of the standard alloy, except that creep rates tended to increase as cobalt was reduced. The effects of long time exposures at 760 C on mechanical properties and at 760 C and 845 C on microstructures were determined. Decreased tensile properties and shorter rupture lives with increased creep rates were observed in alloy modifications. The exposures caused gamma prime particle coarsening and formation of sigma phase in the alloys with higher cobalt contents. Exposure at 845 C also reduced the amount of MC carbides.

  2. The effect of annealing temperature on the properties of powder metallurgy processed Ti-35Nb-2Zr-0.5O alloy.

    Science.gov (United States)

    Málek, Jaroslav; Hnilica, František; Veselý, Jaroslav; Smola, Bohumil; Medlín, Rostislav

    2017-11-01

    Ti-35Nb-2Zr-0.5O (wt%) alloy was prepared via a powder metallurgy process (cold isostatic pressing of blended elemental powders and subsequent sintering) with the primary aim of using it as a material for bio-applications. Sintered specimens were swaged and subsequently the influence of annealing temperature on the mechanical and structural properties was studied. Specimens were annealed at 800, 850, 900, 950, and 1000°C for 0.5h and water quenched. Significant changes in microstructure (i.e. precipitate dissolution or grain coarsening) were observed in relation to increasing annealing temperature. In correlation with those changes, the mechanical properties were also studied. The ultimate tensile strength increased from 925MPa (specimen annealed at 800°C) to 990MPa (900°C). Also the elongation increased from ~ 13% (800°C) to more than 20% (900, 950, and 1000°C). Copyright © 2017 Elsevier Ltd. All rights reserved.

  3. The influence of the intensity of smoking and years of work in the metallurgy on pro-oxidant/antioxidant balance in the blood of smelters.

    Science.gov (United States)

    Bizon, Anna; Antonowicz-Juchniewicz, Jolanta; Andrzejak, Ryszard; Milnerowicz, Halina

    2013-03-01

    The aim of this study was to investigate the effect of cigarette smoking and occupational exposure to heavy metals on the degree of pro-oxidant/antioxidant imbalance in smelters. The investigations were performed on the blood and urine of 400 subjects: 300 male copper smelters and 100 nonexposed male subjects. Biological material was divided into three groups: nonsmokers, those who smoked less than 20 cigarettes a day and those who smoked more than 20 cigarettes a day. The results showed a significant increase in the concentration of lead, cadmium and arsenic in the blood and urine of smelters, while smoking more than 20 cigarettes a day caused a further increase in the concentration of these metals. The level of malondialdehyde was approximately twofold higher in the plasma of the smelters compared to the control group. We have observed a disturbance in the level of antioxidants in erythrocyte lysate manifested by an increase in metallothionein and glutathione concentrations as well as superoxide dismutase and glutathione peroxidase activities and the decrease in glutathione S-transferase activity. Cigarette smoking, years of work in metallurgy and age of smelters were additional factors significantly affecting the pro-oxidant/antioxidant balance.

  4. Risk Assessment of Potentially Toxic Elements (PTEs) Pollution at a Rural Industrial Wasteland in an Abandoned Metallurgy Factory in North China.

    Science.gov (United States)

    Sun, Zheng; Chen, Jiajun

    2018-01-06

    The potential toxic elements (PTEs) pollution problems in many rural industrial wastelands have been observed to be conspicuous. Therefore, 40 top soil samples were collected from the wasteland of a typical rural metallurgy factory in Baoding, China. The total concentrations of six key PTEs were measured. The soil properties and speciation of the PTEs were also identified. Extremely high concentrations of As, Cd, Pb, and Zn were observed in the surface soils. Using the PTEs concentration in the top soils of the rural industrial wasteland, the following indices of pollution were calculated: the pollution load index (PLI), the geo-accumulation Index (I geo ), the risk assessment code (RAC), and the health risk assessment (HRA). The analysis of the PLI and I geo indicated that site #1 was relatively clean, while sites #2 and #3 were heavily polluted. The results of the RAC showed that PTEs in top soils at sites #2 and #3 were significantly increased ( p <  0.05) for Cd and Zn. The HRA indicated that both As and Pb presented non-carcinogenic risks to children and adults at sites #2 and #3. Our findings can be a reference for risk prevention of industrially abandoned land in rural China.

  5. Phase composition, microstructure, and mechanical properties of porous Ti-Nb-Zr alloys prepared by a two-step foaming powder metallurgy method.

    Science.gov (United States)

    Rao, X; Chu, C L; Zheng, Y Y

    2014-06-01

    Porous Ti-Nb-Zr alloys with different porosities from 6.06 to 62.8% are prepared by a two-step foaming powder metallurgy method using TiH2, Nb, and Zr powders together with 0 to 50wt% of NH4HCO3. The effects of the amounts of Nb and Zr as well as the sintering temperature (1473 to 1673K) on their phase composition, porosity, morphology, and mechanical characteristics are investigated. By controlling the porosity, Nb and Zr concentrations as well as the sintering temperature, porous Ti-Nb-Zr alloys with different mechanical properties can be obtained, for example, the hardness between 290 and 63HV, the compressive strength between 1530.5 and 73.4MPa, and the elastic modulus between 10.8 and 1.2GPa. The mechanical properties of the sintered porous Ti-Nb-Zr alloys can be tailored to match different requirements for the human bones and are thus potentially useful in the hard tissue implants. Copyright © 2014 Elsevier Ltd. All rights reserved.

  6. Radioactive Mapping Contaminant of Alpha on The Air in Space of Repair of Hot Cell and Medium Radioactivity Laboratory in Radio metallurgy Installation

    International Nuclear Information System (INIS)

    Yusuf-Nampira; Endang-Sukesi; S-Wahyuningsih; R-Budi-Santoso

    2007-01-01

    Hot cell and space of acid laboratory medium activity in Radio metallurgy Installation are used for the examination preparation of fuel nuclear post irradiation. The sample examined is dangerous radioactive material representing which can disseminate passing air stream. The dangerous material spreading can be pursued by arranging air stream from laboratory space to examination space. To know the performance the air stream arrangement is hence conducted by radioactive mapping contaminant of alpha in laboratory / space of activity place, for example, medium activity laboratory and repair space. This mapping radioactivity contaminant is executed with the measurement level of the radioactivity from sample air taken at various height with the distance of 1 m, various distance and from potential source as contaminant spreading access. The mapping result indicate that a little spreading of radioactive material happened from acid cupboard locker to laboratory activity up to distance of 3 m from acid cupboard locker and spreading of radioactive contaminant from goods access door of the hot cell 104 to repair space reach the distance of 2 m from goods door access. Level of the radioactive contamination in the space was far under maximum limitation allowed (20 Bq / m 3 ). (author)

  7. Fabrication of metal matrix composite by semi-solid powder processing

    Energy Technology Data Exchange (ETDEWEB)

    Wu, Yufeng [Iowa State Univ., Ames, IA (United States)

    2011-01-01

    Various metal matrix composites (MMCs) are widely used in the automotive, aerospace and electrical industries due to their capability and flexibility in improving the mechanical, thermal and electrical properties of a component. However, current manufacturing technologies may suffer from insufficient process stability and reliability and inadequate economic efficiency and may not be able to satisfy the increasing demands placed on MMCs. Semi-solid powder processing (SPP), a technology that combines traditional powder metallurgy and semi-solid forming methods, has potential to produce MMCs with low cost and high efficiency. In this work, the analytical study and experimental investigation of SPP on the fabrication of MMCs were explored. An analytical model was developed to understand the deformation mechanism of the powder compact in the semi-solid state. The densification behavior of the Al6061 and SiC powder mixtures was investigated with different liquid fractions and SiC volume fractions. The limits of SPP were analyzed in terms of reinforcement phase loading and its impact on the composite microstructure. To explore adoption of new materials, carbon nanotube (CNT) was investigated as a reinforcing material in aluminum matrix using SPP. The process was successfully modeled for the mono-phase powder (Al6061) compaction and the density and density distribution were predicted. The deformation mechanism at low and high liquid fractions was discussed. In addition, the compaction behavior of the ceramic-metal powder mixture was understood, and the SiC loading limit was identified by parametric study. For the fabrication of CNT reinforced Al6061 composite, the mechanical alloying of Al6061-CNT powders was first investigated. A mathematical model was developed to predict the CNT length change during the mechanical alloying process. The effects of mechanical alloying time and processing temperature during SPP were studied on the mechanical, microstructural and

  8. Near-Net Shape Fabrication Using Low-Cost Titanium Alloy Powders

    Energy Technology Data Exchange (ETDEWEB)

    Dr. David M. Bowden; Dr. William H. Peter

    2012-03-31

    feasibility studies were performed to identify the most viable approaches to NNS preform fabrication using basic powder metallurgy mill product forms as the building blocks and advanced joining techniques including fusion and solid state joining to assemble these building blocks into efficient machining performs.

  9. FFTF metal fuel pin fabrication

    International Nuclear Information System (INIS)

    Dittmer, J.O.; Benecke, M.W.; Feigenbutz, L.V.

    1989-01-01

    A major new initiative to develop, irradiate, and qualify a binary uranium/zirconium metal-fuel system in the Fast Flux Test Facility (FFTF) has been implemented by the Westinghouse Hanford Company for the US Department of Energy. Metal-fuel test assemblies have been designed and fabricated, and are now being irradiated in FFTF to provide the data needed to support the potential use of binary metal fuels in FFTF and other liquid-metal reactors. These development efforts support licensing activities for metal-fuel use in near-term advanced liquid-metal reactors

  10. The Fabrication of Qualified Citizens

    DEFF Research Database (Denmark)

    Andrade-Molina, Melissa

    2017-01-01

    Within the practices of school mathematics there exists many naturalized truths that have been (re)produced in different times and in different places. The belief of mathematics education becoming the key to economical progress assuring the future growth of nations is problematized. By following...... a rhizomatic analytical move, a historization of the present is deployed to map the fabrication of the desired qualified citizen in Chile. The analysis evidences the (re)production of dominant narratives about the “qualified citizen” are and have been entangled with the functioning of school geometry...

  11. Corning lightweight core fabrication technologies

    Science.gov (United States)

    VanBrocklin, Randy R.; Edwards, Mary J.; Hobbs, Thomas W.

    2003-12-01

    Fabrication of lightweight mirrors from low expansion glasses can be achieved using various core and faceplate lightweighting techniques. Lightweighting can be achieved using abrasive waterjet cutting, CNC milling and a new approach that Corning is developing to produce lightweight cores based on Corning's patented ceramic extrusion process. The selection of which lightweighting technology to use is dependent on customer design considerations of the lightweight mirror. These lightweighting techniques are reviewed and discussed, along with advantages and disadvantages of each technique. Corning will also introduce and discuss their new core lightweighting process.

  12. Porosity Prediction of Plain Weft Knitted Fabrics

    Directory of Open Access Journals (Sweden)

    Muhammad Owais Raza Siddiqui

    2014-12-01

    Full Text Available Wearing comfort of clothing is dependent on air permeability, moisture absorbency and wicking properties of fabric, which are related to the porosity of fabric. In this work, a plug-in is developed using Python script and incorporated in Abaqus/CAE for the prediction of porosity of plain weft knitted fabrics. The Plug-in is able to automatically generate 3D solid and multifilament weft knitted fabric models and accurately determine the porosity of fabrics in two steps. In this work, plain weft knitted fabrics made of monofilament, multifilament and spun yarn made of staple fibers were used to evaluate the effectiveness of the developed plug-in. In the case of staple fiber yarn, intra yarn porosity was considered in the calculation of porosity. The first step is to develop a 3D geometrical model of plain weft knitted fabric and the second step is to calculate the porosity of the fabric by using the geometrical parameter of 3D weft knitted fabric model generated in step one. The predicted porosity of plain weft knitted fabric is extracted in the second step and is displayed in the message area. The predicted results obtained from the plug-in have been compared with the experimental results obtained from previously developed models; they agreed well.

  13. Versatile superamphiphobic cotton fabrics fabricated by coating with SiO2/FOTS

    Science.gov (United States)

    Li, Deke; Guo, Zhiguang

    2017-12-01

    A multifunctional superamphiphobic cotton fabric was fabricated by coating silica nanoparticles on the cotton fabric surface and further modification by 1H,1H,2H,2H-perfluorooctyltrichlorosilane (FOTS). The fluctuant woven fabric and the fluffy spherical SiO2 nanoparticles constructed a dual micro/nano-structures. The surface free energy of the fabric composite was reduced by FOTS modifier. The interplay of the structured and perfluorinated SiO2 nanoparticles could not only endow the fabric highly liquid repellent ability, but could also to enhance the coating stability. The prepared cotton fabrics exhibited high liquid repellency to water, colza oil and n-hexadecane with lower surface tension, showing a contact angle of 158°, 152°, and 153°, respectively. The results demonstrated that superamphiphobic cotton fabric possessed desirable chemical and mechanical durability, self-cleaning and self-healing property, the robust and multifunctional fabric would find innovative opportunities for practical applications.

  14. Optimization of Ultrasonic Fabric Cleaning

    Energy Technology Data Exchange (ETDEWEB)

    Hand, T.E.

    1998-05-13

    The fundamental purpose of this project was to research and develop a process that would reduce the cost and improve the environmental efficiency of the present dry-cleaning industry. This second phase of research (see report KCP-94-1006 for information gathered during the first phase) was intended to allow the optimal integration of all factors of ultrasonic fabric cleaning. For this phase, Garment Care performed an extensive literature search and gathered data from other researchers worldwide. The Garment Care-AlliedSignal team developed the requirements for a prototype cleaning tank for studies and acquired that tank and the additional equipment required to use it properly. Garment Care and AlliedSignal acquired the transducers and generators from Surftran Martin-Walter in Sterling Heights, Michigan. Amway's Kelly Haley developed the test protocol, supplied hundreds of test swatches, gathered the data on the swatches before and after the tests, assisted with the cleaning tests, and prepared the final analysis of the results. AlliedSignal personnel, in conjunction with Amway and Garment Care staff, performed all the tests. Additional planning is under way for future testing by outside research facilities. The final results indicated repeatable performance and good results for single layered fabric swatches. Swatches that were cleaned as a ''sandwich,'' that is, three or more layers.

  15. Polymer micromold and fabrication process

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Abraham P. (1428 Whitecliff Way, Walnut Creek, CA 94596); Northrup, M. Allen (923 Creston Rd., Berkeley, CA 94708); Ahre, Paul E. (1299 Gonzaga Ct., Livermore, CA 94550); Dupuy, Peter C. (1736 Waldo Ct., Modesto, CA 95358)

    1997-01-01

    A mold assembly with micro-sized features in which the hollow portion thereof is fabricated from a sacrificial mandrel which is surface treated and then coated to form an outer shell. The sacrificial mandrel is then selectively etched away leaving the outer shell as the final product. The sacrificial mandrel is fabricated by a precision lathe, for example, so that when removed by etching the inner or hollow area has diameters as small as 10's of micros (.mu.m). Varying the inside diameter contours of the mold can be accomplished with specified ramping slopes formed on the outer surface of the sacrificial mandrel, with the inside or hollow section being, for example, 275 .mu.m in length up to 150 .mu.m in diameter within a 6 mm outside diameter (o.d.) mold assembly. The mold assembly itself can serve as a micronozzle or microneedle, and plastic parts, such as microballoons for angioplasty, polymer microparts, and microactuators, etc., may be formed within the mold assembly.

  16. Polymer micromold and fabrication process

    Energy Technology Data Exchange (ETDEWEB)

    Lee, A.P.; Northrup, M.A.; Ahre, P.E.; Dupuy, P.C.

    1997-08-19

    A mold assembly is disclosed with micro-sized features in which the hollow portion thereof is fabricated from a sacrificial mandrel which is surface treated and then coated to form an outer shell. The sacrificial mandrel is then selectively etched away leaving the outer shell as the final product. The sacrificial mandrel is fabricated by a precision lathe, for example, so that when removed by etching the inner or hollow area has diameters as small as 10`s of micros ({micro}m). Varying the inside diameter contours of the mold can be accomplished with specified ramping slopes formed on the outer surface of the sacrificial mandrel, with the inside or hollow section being, for example, 275 {micro}m in length up to 150 {micro}m in diameter within a 6 mm outside diameter (o.d.) mold assembly. The mold assembly itself can serve as a micronozzle or microneedle, and plastic parts, such as microballoons for angioplasty, polymer microparts, and microactuators, etc., may be formed within the mold assembly. 6 figs.

  17. LEU fuel fabrication in Argentina

    International Nuclear Information System (INIS)

    Giorsetti, D.R.; Gomez, J.O.; Marajofsky, A.; Kohut, C.

    1985-01-01

    As an Institution, aiming to meet with its own needs, CNEA has been intensively developing reduced enriched fuel to use in its own research and test reactors. Development of the fabrication technology as well as the design, installation and operation of the manufacturing plant, have been carried out with its own funds. Irradiation and post-irradiation of test miniplates have been taking place within the framework of the RERTR program. During the last years, CNEA has developed three LEU fuel types. In the previous RERTR meetings, we presented the technological results obtained with these fuel types. This paper focuses on CNEA LEU fuel element manufacturing status and the trained personnel we can offer in design and manufacture fuel capability. CNEA has its own fuel manufacturing technology; the necessary facilities to start the fuel fabrication; qualified technicians and professionals for: fuel design and behaviour analysis; fuel manufacturing and QA; international recognition of its fuel development and manufacturing capability through its ORR miniplate irradiation; its own natural uranium and the future possibility to enrich up to 20% U 235 ; the probability to offer a competitive fuel manufacturing cost in the international market; the disposition to cooperate with all countries that wish to take part and aim to reach an self-sufficiency in their own fuel supply needs

  18. QUIJOTE telescope design and fabrication

    Science.gov (United States)

    Gomez, Alberto; Murga, Gaizka; Etxeita, Borja; Sanquirce, Rubén; Rebolo, Rafael; Rubiño-Martin, Jose Alberto; Herreros, José-Miguel; Hoyland, Roger; Gomez, Francisca; Génova-Santos, Ricardo T.; Piccirillo, Lucio; Maffei, Bruno; Watson, Robert

    2010-07-01

    The QUIJOTE CMB experiment aims to characterize the polarization of the CMB in the frequency range 10-30 GHz and large angular scales. It will be installed in the Teide Observatory, following the projects that the Anisotropy of the Cosmic Microwave Background group has developed in the past (Tenerife experiment, IAC-Bartol experiment...) and is running at the present time (VSA, Cosmosomas). The QUIJOTE CMB experiment will consist of two telescopes which will be installed inside a unique enclosure, which is already constructed. The layout of both telescopes is based on an altazimuth mount supporting a primary and a secondary mirror disposed in a offset Gregorian Dragon scheme. The use of industrial-like fabrication techniques, such as sand-mould casting, CNC machining, and laser tracker measuring for alignment, provided the required performances for microwave observation. A fast-track construction scheme, altogether with the use of these fabrication techniques allowed designing and manufacturing the opto-mechanics of the telescope in 14 months prior to delivery for final start-up in December 2008.

  19. Fabrication, characterization and in vitro biocompatibility evaluation of porous Ta–Nb alloy for bone tissue engineering

    Energy Technology Data Exchange (ETDEWEB)

    Wang, Huifeng; Li, Jing; Yang, Hailin; Liu, Chao; Ruan, Jianming, E-mail: jianming@csu.edu.cn

    2014-07-01

    Porous Ta–Nb alloys were fabricated using the sponge impregnation technique and the powder metallurgy technique (P/M) in combination. All porous Ta–Nb alloys displayed interconnected open cell structures with porosities around 64% and pore sizes in the range of 300–500 μm. No carbide, oxide, or intermetallic-related phases were detected by the X-ray diffraction (XRD). Porous Ta–Nb alloys displayed sintering neck growth, smoother surface of the particles and more shrinkage of the micropores, with Nb contents increasing from 5% to 15%. The compressive strength and Young's modulus of the Ta–Nb alloys agreed well with the requirements of trabecular bone. The normalized compressive plateau stress and Young's modulus increased from 52.27 MPa to 85.43 MPa and from 1.850 GPa to 2.540 GPa, respectively, with Nb contents increasing from 5% to 15%. Porous Ta–Nb alloys had no cytotoxicity and possessed the excellent biocompatibility similar to porous Ta scaffolds. - Highlights: • Porous Ta–Nb alloys were prepared as a novel biomaterial for the first time. • Excellent mechanical properties of the porous Ta–Nb alloy were obtained. • The mechanical properties can be tailored by adjusting the Nb content. • The excellent in vitro biocompatibility of porous Ta–Nb alloys was shown.

  20. Effect of sintering temperature on physical properties & hardness of CoCrMo alloys fabricated by metal injection moulding process

    Science.gov (United States)

    Ridhwan Abdullah, Ahmad; Aidah Nabihah Dandang, Nur; Zalikha Khalil, Nur; Harun, Wan Sharuzi Wan

    2017-10-01

    Metal Injection Moulding (MIM) process is one of the Powder Metallurgy manufacturing techniques utilised to produce Cobalt Chromium Molybdenum (CoCrMo) compacts. The objective of this study is to determine physical properties and hardness of CoCrMo alloy compact sintered at three different sintering temperature at the similar soaking time. At the beginning, sample were fabricated by using Injection Moulding machine. Cobalt Chrome Molybdenum (CoCrMo) metal powder was selected for this study. A morphological study was conducted using optical microscope (OM) and micro-Vickers hardness testing. From the result obtained, it shows upward trend either on the hardness or physical properties of the samples. CoCrMo sintered compact become harder and volume of pores on surface become less due to the increase on sintering temperature. However, effect of increasing sintering temperature shows significant shrinkage of the sample, beginning losses in dimensional accuracy. It is discovered that a little change in sintering temperature gives significant impact on the microstructure, physical, mechanical of the alloy.

  1. The Usability of Boric Acid as an Alternative Foaming Agent on the Fabrication of Al/Al2O3 Composite Foams

    Science.gov (United States)

    Yaman, Bilge; Onuklu, Eren; Korpe, Nese O.

    2017-09-01

    Pure Al and alumina (2, 5, 10 wt.% Al2O3)-added Al composite foams were fabricated through powder metallurgy technique, where boric acid (H3BO3) is employed as a new alternative foaming agent. It is aimed to determine the effects of boric acid on the foaming behavior and cellular structure and also purposed to develop the mechanical properties of Al foams by addition of Al2O3. Al and Al composite foams with porosity fraction in the range of 46-53% were achieved by sintering at 620 °C for 2 h. Cell morphology was characterized using a combination of stereomicroscope equipped with image analyzer and scanning electron microscopy. Microhardness values were measured via using Vickers indentation technique. Quasi-static compression tests were performed at strain rate of 10-3 s-1. Compressive strength and energy absorption of the composite foams enhanced not only by the increasing weight fraction of alumina, but also by the usage of boric acid which leads to formation of boron oxide (B2O3) acting as a binder in obtaining dense cell walls. The results revealed that the boric acid has outstanding potential as foaming agent in the fabrication of Al and Al composite foams by providing improved mechanical properties.

  2. Fabrication of nuclear fuel by powder injection moulding: Study of the binders systems and the de-binding of feedstock containing actinide powder

    International Nuclear Information System (INIS)

    Bricout, J.

    2012-01-01

    Powder Injection Moulding (PIM) is identified as an innovative process for the nuclear fuel fabrication. Technological breakthrough compared to the current process of powder metallurgy, the impact of actinide powder's specificities on the different steps of PIM is performed. Alumina powders simulating actinide powder have been implemented with a reference binders system. Thermal and rheological studies show the injectability and the de-binding of feedstocks with adequate solid loading (≥50 %vol), thanks to the de-agglomeration during the mixing step, which allow to obtain net shape fuel pellet. Specific surface area of powders, acting as a key role in behaviour's feedstocks, has been integrated in analysis models of viscosity prediction according to the shear rate. Also conducted studies on uranium oxide powder show that the selected binders systems, which have a compatible rheological behaviour with PIM process, impact the de-agglomeration of powder and final microstructure of the fuel pellet, consistent with the results obtained on alumina powders. Independent behaviour of binders and uranium oxide powder, showing no adverse chemical reaction against the PIM process, show a residual mass of carbon of about 150 ppm after sintering. Binders system using polystyrene, resistant to radiolysis phenomena and loadable more than 50 %(vol) of actinide powder, shows the promising potential of PIM process for the fuel fabrication. (author) [fr

  3. Fabrication of Flexible Piezoelectric PZT/Fabric Composite

    Directory of Open Access Journals (Sweden)

    Caifeng Chen

    2013-01-01

    Full Text Available Flexible piezoelectric PZT/fabric composite material is pliable and tough in nature which is in a lack of traditional PZT patches. It has great application prospect in improving the sensitivity of sensor/actuator made by piezoelectric materials especially when they are used for curved surfaces or complicated conditions. In this paper, glass fiber cloth was adopted as carrier to grow PZT piezoelectric crystal particles by hydrothermal method, and the optimum conditions were studied. The results showed that the soft glass fiber cloth was an ideal kind of carrier. A large number of cubic-shaped PZT nanocrystallines grew firmly in the carrier with a dense and uniform distribution. The best hydrothermal condition was found to be pH 13, reaction time 24 h, and reaction temperature 200°C.

  4. Fabrication of superhydrophobic cotton fabrics by silica hydrosol and hydrophobization

    Science.gov (United States)

    Xu, Lihui; Zhuang, Wei; Xu, Bi; Cai, Zaisheng

    2011-04-01

    Superhydrophobic cotton fabrics were prepared by the incorporation of silica nanoparticles and subsequent hydrophobization with hexadecyltrimethoxysilane (HDTMS). The silica nanoparticles were synthesized via sol-gel reaction with methyl trimethoxy silane (MTMS) as the precursor in the presence of the base catalyst and surfactant in aqueous solution. As for the resulting products, characterization by particle size analyzer, scanning electron microscopy (SEM), scanning probe microscopy (SPM), X-ray photoelectron spectroscopy (XPS), and thermal gravimetric analysis (TGA) were performed respectively. The size of SiO2 nanoparticles can be controlled by adjusting the catalyst and surfactant concentrations. The wettability of cotton textiles was evaluated by the water contact angle (WCA) and water shedding angle (WSA) measurements. The results showed that the treated cotton sample displayed remarkable water repellency with a WCA of 151.9° for a 5 μL water droplet and a WSA of 13° for a 15 μL water droplet.

  5. Fabrication and characterization of laminated Ti-(TiB+La2O3/Ti composite

    Directory of Open Access Journals (Sweden)

    Yuanfei Han

    2015-10-01

    Full Text Available The incorporation of ceramic particulate reinforcements into titanium alloys can improve the specific strength and specific stiffness, while inevitably reduce the plasticity and ductility. In this study, in situ synthesized multilayer Ti-(TiB+La2O3/Ti composite was designed by learning from the microstructure of nature biological materials with excellent mechanical properties. The Ti-(TiB+La2O3/Ti composite with unique characteristic of laminated structure was prepared by combined powder metallurgy and hot rolling. The method has the synthesize advantages with in-situ reaction of Ti and LaB6 at high temperature and controllability of reinforcements size and constituent phases in composites. The result shows that the pores in the as sintered laminated structure composite completely disappeared after hot rolling at 1050 °C. The agglomerated reinforcement particles were well dispersed and distributed uniformly along the rolling direction. The thickness of pure Ti layer and (TiB+La2O3/Ti composite layer decreased from 1 mm to about 200 μm. Meanwhile, the grains size was refined obviously after rolling deformation. The room temperature tensile test indicates that the elongation of the laminated Ti-(TiB+La2O3/Ti composite improved from 13% to 17% in comparison with the uniform (TiB+La2O3/Ti composite, while the tensile strength had little change. It provides theoretical and experimental basis for fabricating the novel high performance laminated Ti-(TiB+La2O3/Ti composites.

  6. Update On Monolithic Fuel Fabrication Development

    Energy Technology Data Exchange (ETDEWEB)

    C. R Clark; J. M. Wight; G. C. Knighton; G. A. Moore; J. F. Jue

    2005-11-01

    Efforts to develop a viable monolithic research reactor fuel plate have continued at Idaho National Laboratory. These efforts have concentrated on both fabrication process refinement and scale-up to produce full sized fuel plates. Advancements have been made in the production of U-Mo foil including full sized foils. Progress has also been made in the friction stir welding and transient liquid phase bonding fabrication processes resulting in better bonding, more stable processes and the ability to fabricate larger fuel plates.

  7. Plasmonic nanoparticles: Towards the fabrication of biosensors

    Science.gov (United States)

    Shen, Hui

    2015-07-01

    Au and Ag nanoparticles are mainly employed in the fabrication of biosensors owing to their unique optical properties compared to other noble metal nanoparticles. Many biosensors are fabricated for the rapid detection of different analytes such as organic and inorganic molecules, biomolecules like DNA, proteins, biotoxins and pathogens. In this mini review we mainly discuss on the usage of Au and Ag nanoparticles for the fabrication of colorimetric, SERS and two photon based photoluminescence biosensors.

  8. Nanocrystal thin film fabrication methods and apparatus

    Energy Technology Data Exchange (ETDEWEB)

    Kagan, Cherie R.; Kim, David K.; Choi, Ji-Hyuk; Lai, Yuming

    2018-01-09

    Nanocrystal thin film devices and methods for fabricating nanocrystal thin film devices are disclosed. The nanocrystal thin films are diffused with a dopant such as Indium, Potassium, Tin, etc. to reduce surface states. The thin film devices may be exposed to air during a portion of the fabrication. This enables fabrication of nanocrystal-based devices using a wider range of techniques such as photolithography and photolithographic patterning in an air environment.

  9. Plutonium fuel fabrication residues and wastes

    International Nuclear Information System (INIS)

    Arnal, T.; Cousinou, G.; Desille, H.

    1982-04-01

    This paper discusses the current situation in the fabrication plant at Cadarache with an annual plutonium throughput of several tons. Three major fabrication byproduct categories are defined in this plant: 1) scraps, directly recycled at the fabrication input station; 2) residues, byproducts recycled by chemical processes, or processed in washing and incineration stations; 3) wastes, placed in drums and evacuated directly to a waste conditioning station. The borderline between residues and wastes has yet to be precisely determined

  10. FABRIC TENSOR FOR DISCONTINUOUS GEOLOGICAL MATERIALS

    OpenAIRE

    小田, 匡寛

    1982-01-01

    Geometrical property (fabric) of discontinuity in geological materials is discussed in terms of (1) position and density, (2) shape and dimension and (3) orientation of related discontinuities such as joint, fault and discrete particle. By taking into account these geometrical elements, a unique measure called fabric tensor F_ is definitely introduced to embody the fabric concept without loss of generality.The first invariant of F_ is important as an index measure to evaluate the crack intens...

  11. Hemp nanocellulose: fabrication, characterisation and application

    OpenAIRE

    Dasong, Dai

    2015-01-01

    This thesis was submitted for the award of Doctor of Philosophy and was awarded by Brunel University London Nanocellulose has gained lots of attentions in recent years due to the development of nanotechnology. Thousands of publications have been reported about the fabrication, characterization and application of nanocellulose, among which most of the nanocelluloses were fabricated from the microcrystalline cellulose (MCC) or pulp, and only two methods about the nanocellulose fabrication ha...

  12. Development of Self-Cleaning Denim Fabrics

    Science.gov (United States)

    Uğur, Ş. S.; Sarıışık, A. M.; Çavuşlar, E.; Ertek, M.

    2017-10-01

    Denim fabrics coated with TiO2 nanolayers for self-cleaning properties by using a continuous layer-by-layer method. Nanolayer coated denim fabrics washed with an enzyme process for aging affect. Fabrics were analyzed with SEM-EDX and XPS measurements. Self-cleaning properties of the nanolayer deposited denim fabrics were tested according to red wine stain against to Suntest visible light irradiation after 72 h. And also, some physical (air permeability, tensile strength) and color (color difference and rubbing fastness) properties were evaluated.

  13. Photolithography and Micro-Fabrication/ Packaging Laboratories

    Data.gov (United States)

    Federal Laboratory Consortium — The Photolithography and Micro-Fabrication/Packaging laboratories provide research level semiconductor processing equipment and facilities that do not require a full...

  14. Advances in superconducting quantum electronic microcircuit fabrication

    International Nuclear Information System (INIS)

    Kirschman, R.K.; Notarys, H.A.; Mercereau, J.E.

    1975-01-01

    Standard microelectronic fabrication techniques were utilized to produce batch quantities of superconducting quantum electronic devices and circuits. The over-all goal is a fabrication technology yielding circuits that are rugged, stable, and capable of being fabricated controllably and reproducibly in sizeable quantities. Progress toward this goal is presented, with primary emphasis on the most recent work, which includes the use of electron-beam lithography and techniques of hybrid microelectronics. Several prototype microcircuits were successfully fabricated. These microcircuits are formed in a thin-film parent material consisting of layers of superconducting and normal metals, and use proximity effect structures as the active circuit elements

  15. Development of blanket box structure fabrication technology

    International Nuclear Information System (INIS)

    Mohri, K.; Sato, S.; Kawaguchi, I.; Sato, K.; Kuroda, T.; Hashimoto, T.; Sato, S.; Takatsu, H.

    1995-01-01

    Fabrication studies have been performed for the first wall and blanket box structure in the fusion experimental reactor designed in Japan. The hot isostatic pressing technique has been proposed as one of the most promising candidate methods for fabricating the first wall. This paper describes the trial fabrication of a half-scale mock-up for part of an outboard module near the midplane, without the internal structure of a breeding region, to investigate its feasibility and to clarify technological issues associated with the proposed fabrication technologies. (orig.)

  16. Propulsion Design with Freeform Fabrication, Phase I

    Data.gov (United States)

    National Aeronautics and Space Administration — Propulsion Design with Freeform Fabrication (PDFF) will develop and implement a novel design methodology that leverages the rapidly evolving Solid Freeform...

  17. Woven Fabrics Made of Auxetic Plied Yarns

    Directory of Open Access Journals (Sweden)

    Wing Sum Ng

    2018-02-01

    Full Text Available Auxetic plied yarns are specially constructed with two types of single yarns of different sizes and moduli. This paper investigates how to use these types of yarns to produce woven fabrics with auxetic effects. Four-ply auxetic yarns were first incorporated into a series of woven fabrics with different design parameters to study their auxetic behavior and percent open area during extension. Effects of auxetic plied yarn arrangement, single component yarn properties, weft yarn type, and weave structure were then evaluated. Additional double helical yarn (DHY and 6-ply auxetic yarn woven fabrics were also made for comparison. The results show that the alternative arrangement of S- and Z-twisted 4-ply auxetic yarns in a woven fabric can generate a higher negative Poisson’s ratio (NPR of the fabric. While the higher single stiff yarn modulus of auxetic yarn can result in greater NPR behavior, finer soft auxetic yarn does not necessarily generate such an effect. Weft yarns with low modulus and short float over the 4-ply auxetic yarns in fabric structure are favorable for producing high NPR behavior. The weft cover factor greatly affects the variation of the percent open area of the 4-ply auxetic yarn fabrics during extension. When different kinds of helical auxetic yarns (HAYs are made into fabrics, the fabric made of DHY does not have the highest NPR effect but it has the highest percent open area, which increases with increasing tensile strain.

  18. Fabrication of Games and Learning

    DEFF Research Database (Denmark)

    Schoenau-Fog, Henrik; Reng, Lars; Kofoed, Lise

    2015-01-01

    The concept of Game based learning has proven to have many possibilities for supporting better learning outcomes, when using educational or commercial games in the classroom. However, there is also a great potential in using game development as a motivator in several other kinds of learning...... scenarios. Using game development as an approach for including game based learning in various educations has become more accessible due to more user friendly game development tools and systems. This study will thus focus on an exploration on how game development motivates students and what they learn when...... creating games. We exemplify the potential of using game fabrication as a learning environment with the investigation of a game production, which involved over 25 students across semesters. In order to investigate students’ experiences during this purposive game production, we set up an experiment where...

  19. Remote Microelectronics Fabrication Laboratory MEFLab

    Directory of Open Access Journals (Sweden)

    Jan Machotka

    2008-07-01

    Full Text Available Over the last decade, there has been a move towards using remote laboratories in engineering education. The majority of these laboratories are static, involving limited user-controlled mechanical movements. The University of South Australia has developed such a laboratory, called NetLab that has been successfully utilized for teaching both on-campus and transnational programs in electrical and electronics engineering. Following this success, we are now developing a remote laboratory for microelectronic fabrication, MEFLab. The first stage of the development is a remote laboratory for visual inspection and testing of electronic circuits directly on the silicon wafer under a microscope which is normally conducted in a cleanroom. The major challenge of this project is the accurate positioning of micro-probes remotely over the internet. This paper presents the details of the setup of this new remote laboratory, with a particular emphasis on the development of the hardware, software and graphical user interface.

  20. Fabrication of Metallic Hollow Nanoparticles

    Science.gov (United States)

    Kim, Jae-Woo (Inventor); Choi, Sr., Sang H. (Inventor); Lillehei, Peter T. (Inventor); Chu, Sang-Hyon (Inventor); Park, Yeonjoon (Inventor); King, Glen C. (Inventor); Elliott, James R. (Inventor)

    2016-01-01

    Metal and semiconductor nanoshells, particularly transition metal nanoshells, are fabricated using dendrimer molecules. Metallic colloids, metallic ions or semiconductors are attached to amine groups on the dendrimer surface in stabilized solution for the surface seeding method and the surface seedless method, respectively. Subsequently, the process is repeated with additional metallic ions or semiconductor, a stabilizer, and NaBH.sub.4 to increase the wall thickness of the metallic or semiconductor lining on the dendrimer surface. Metallic or semiconductor ions are automatically reduced on the metallic or semiconductor nanoparticles causing the formation of hollow metallic or semiconductor nanoparticles. The void size of the formed hollow nanoparticles depends on the dendrimer generation. The thickness of the metallic or semiconductor thin film around the dendrimer depends on the repetition times and the size of initial metallic or semiconductor seeds.