Estimation of identification limit for a small-type OSL dosimeter on the medical images by measurement of X-ray spectra.

Science.gov (United States)

Takegami, Kazuki; Hayashi, Hiroaki; Okino, Hiroki; Kimoto, Natsumi; Maehata, Itsumi; Kanazawa, Yuki; Okazaki, Tohru; Hashizume, Takuya; Kobayashi, Ikuo

2016-07-01

Our aim in this study is to derive an identification limit on a dosimeter for not disturbing a medical image when patients wear a small-type optically stimulated luminescence (OSL) dosimeter on their bodies during X-ray diagnostic imaging. For evaluation of the detection limit based on an analysis of X-ray spectra, we propose a new quantitative identification method. We performed experiments for which we used diagnostic X-ray equipment, a soft-tissue-equivalent phantom (1-20 cm), and a CdTe X-ray spectrometer assuming one pixel of the X-ray imaging detector. Then, with the following two experimental settings, corresponding X-ray spectra were measured with 40-120 kVp and 0.5-1000 mAs at a source-to-detector distance of 100 cm: (1) X-rays penetrating a soft-tissue-equivalent phantom with the OSL dosimeter attached directly on the phantom, and (2) X-rays penetrating only the soft-tissue-equivalent phantom. Next, the energy fluence and errors in the fluence were calculated from the spectra. When the energy fluence with errors concerning these two experimental conditions was estimated to be indistinctive, we defined the condition as the OSL dosimeter not being identified on the X-ray image. Based on our analysis, we determined the identification limit of the dosimeter. We then compared our results with those for the general irradiation conditions used in clinics. We found that the OSL dosimeter could not be identified under the irradiation conditions of abdominal and chest radiography, namely, one can apply the OSL dosimeter to measurement of the exposure dose in the irradiation field of X-rays without disturbing medical images.

Time-resolved x-ray spectra of laser irradiated high-Z targets

International Nuclear Information System (INIS)

Lee, P.H.Y.; Attwood, D.T.; Boyle, M.J.; Campbell, E.M.; Coleman, L.C.; Kornblum, H.N.

1977-01-01

Recent results obtained by using the Livermore 15 psec x-ray streak camera to record x-ray emission from laser-irradiated high-z targets in the 1-20 keV range are reported. Nine to eleven K-edge filter channels were used for the measurements. In the lower energy channels, a dynamic range of x-ray emission intensity of better than three orders of magnitude have been recorded. Data will be presented which describe temporally and spectrally resolved x-ray spectra of gold disk targets irradiated by laser pulses from the Argus facility, including the temporal evolution of the superthermal x-ray tail

Compton spectra of atoms at high x-ray intensity

Science.gov (United States)

Son, Sang-Kil; Geffert, Otfried; Santra, Robin

2017-03-01

Compton scattering is the nonresonant inelastic scattering of an x-ray photon by an electron and has been used to probe the electron momentum distribution in gas-phase and condensed-matter samples. In the low x-ray intensity regime, Compton scattering from atoms dominantly comes from bound electrons in neutral atoms, neglecting contributions from bound electrons in ions and free (ionized) electrons. In contrast, in the high x-ray intensity regime, the sample experiences severe ionization via x-ray multiphoton multiple ionization dynamics. Thus, it becomes necessary to take into account all the contributions to the Compton scattering signal when atoms are exposed to high-intensity x-ray pulses provided by x-ray free-electron lasers (XFELs). In this paper, we investigate the Compton spectra of atoms at high x-ray intensity, using an extension of the integrated x-ray atomic physics toolkit, xatom. As the x-ray fluence increases, there is a significant contribution from ionized electrons to the Compton spectra, which gives rise to strong deviations from the Compton spectra of neutral atoms. The present study provides not only understanding of the fundamental XFEL-matter interaction but also crucial information for single-particle imaging experiments, where Compton scattering is no longer negligible. , which features invited work from the best early-career researchers working within the scope of J. Phys. B. This project is part of the Journal of Physics series’ 50th anniversary celebrations in 2017. Sang-Kil Son was selected by the Editorial Board of J. Phys. B as an Emerging Leader.

Monte Carlo simulation of x-ray spectra in diagnostic radiology and mammography using MCNP4C

Energy Technology Data Exchange (ETDEWEB)

Ay, M R [Department of Physics and Nuclear Sciences, AmirKabir University of Technology, Tehran (Iran, Islamic Republic of); Shahriari, M [Department of Nuclear Engineering, Shahid Beheshti University, Tehran (Iran, Islamic Republic of); Sarkar, S [Department of Medical Physics, Tehran University of Medical Science, Tehran (Iran, Islamic Republic of); Adib, M [TPP Co., GE Medical Systems, Iran Authorized Distributor, Tehran (Iran, Islamic Republic of); Zaidi, H [Division of Nuclear Medicine, Geneva University Hospital, 1211 Geneva (Switzerland)

2004-11-07

The general purpose Monte Carlo N-particle radiation transport computer code (MCNP4C) was used for the simulation of x-ray spectra in diagnostic radiology and mammography. The electrons were transported until they slow down and stop in the target. Both bremsstrahlung and characteristic x-ray production were considered in this work. We focus on the simulation of various target/filter combinations to investigate the effect of tube voltage, target material and filter thickness on x-ray spectra in the diagnostic radiology and mammography energy ranges. The simulated x-ray spectra were compared with experimental measurements and spectra calculated by IPEM report number 78. In addition, the anode heel effect and off-axis x-ray spectra were assessed for different anode angles and target materials and the results were compared with EGS4-based Monte Carlo simulations and measured data. Quantitative evaluation of the differences between our Monte Carlo simulated and comparison spectra was performed using student's t-test statistical analysis. Generally, there is a good agreement between the simulated x-ray and comparison spectra, although there are systematic differences between the simulated and reference spectra especially in the K-characteristic x-rays intensity. Nevertheless, no statistically significant differences have been observed between IPEM spectra and the simulated spectra. It has been shown that the difference between MCNP simulated spectra and IPEM spectra in the low energy range is the result of the overestimation of characteristic photons following the normalization procedure. The transmission curves produced by MCNP4C have good agreement with the IPEM report especially for tube voltages of 50 kV and 80 kV. The systematic discrepancy for higher tube voltages is the result of systematic differences between the corresponding spectra.

Monte Carlo simulation of x-ray spectra in diagnostic radiology and mammography using MCNP4C

Science.gov (United States)

Ay, M. R.; Shahriari, M.; Sarkar, S.; Adib, M.; Zaidi, H.

2004-11-01

The general purpose Monte Carlo N-particle radiation transport computer code (MCNP4C) was used for the simulation of x-ray spectra in diagnostic radiology and mammography. The electrons were transported until they slow down and stop in the target. Both bremsstrahlung and characteristic x-ray production were considered in this work. We focus on the simulation of various target/filter combinations to investigate the effect of tube voltage, target material and filter thickness on x-ray spectra in the diagnostic radiology and mammography energy ranges. The simulated x-ray spectra were compared with experimental measurements and spectra calculated by IPEM report number 78. In addition, the anode heel effect and off-axis x-ray spectra were assessed for different anode angles and target materials and the results were compared with EGS4-based Monte Carlo simulations and measured data. Quantitative evaluation of the differences between our Monte Carlo simulated and comparison spectra was performed using student's t-test statistical analysis. Generally, there is a good agreement between the simulated x-ray and comparison spectra, although there are systematic differences between the simulated and reference spectra especially in the K-characteristic x-rays intensity. Nevertheless, no statistically significant differences have been observed between IPEM spectra and the simulated spectra. It has been shown that the difference between MCNP simulated spectra and IPEM spectra in the low energy range is the result of the overestimation of characteristic photons following the normalization procedure. The transmission curves produced by MCNP4C have good agreement with the IPEM report especially for tube voltages of 50 kV and 80 kV. The systematic discrepancy for higher tube voltages is the result of systematic differences between the corresponding spectra.

Determination of half value layer and applied voltage from emitted spectra by an X-ray tube

International Nuclear Information System (INIS)

Santos, Josilene C.; Gonzales, Alejandro H.L.; Terini, Ricardo A.; Costa, Paulo R.

2016-01-01

This work describes a method for assessment of half value layer (HVL) and peak tube voltage (kVp) applied in an X-ray tube by means of experimental X-ray spectra measured using a CdTe detector. It was assessed some parameters that can affect the evaluation of these quantities such as dead time, count rate and tube current (mA). For this study, two sets of X-ray spectra were measured: Set A), spectra measurements using Cu filters with different thicknesses (1.8 - 5.4 mm) and fixed tube current; Set B), spectra measurements keeping a fixed Cu filtration and varying tube current (0.5 - 3.0 mA). The experimental setup for the Set A spectra measurements allowed the assessment of the HVL and kVp for different count rates and dead time in the detection system, while the Set B setup allowed to assess the dependence of these quantities with the tube current. The spectrometer was energy calibrated using standard X/γ rays radioactive sources. The tube voltage values were estimated by means of experimental measured X-ray spectra, using linear regression in order to search the end point of each spectrum. The spectra correction was performed using the stripping procedure developed for the Matlab® software and the HVL values were derived from these corrected spectra. For comparison, HVL was also determined using a 30 cm"3 ion chamber and high purity Al filters. The results show that it is possible to determine the kVp with accuracy and reproducibility using spectra with dead time of up to 10%. In spite of this, the values obtained showed a deviation of up to 7 kV, for spectra measured using the same nominal tube voltage different tube current values, indicating dependence between these two parameters. (author)

Determination of semi-reducing layer and applied stress through spectra emitted by an X-ray tube

International Nuclear Information System (INIS)

Santos, Josilene C.; Gonzalez, Alejandro H.L.; Terini, Ricardo A.; Costa, Paulo R.

2016-01-01

This work describes a method for assessment of half value layer (HVL) and peak tube voltage (kVp) by means of experimental x-ray spectra measured using a CdTe detector. The work also evaluated spectrometry parameters such as dead time and count rate, and x-ray tube characteristics that can affect the assessment of these quantities. Two sets of x-ray spectra were measured: A) using Cu filters with different thicknesses and fixed tube current, and B) keeping a fixed Cu filtration and different tube current and, so, ranging the count rates. The spectrometer was energy calibrated using standard radioactive sources. kVp value was estimated by means of experimental measured x-ray spectra, using linear regression in order to search the end point of each spectrum. HVL was estimated after the correction of the measured spectra, using an analytical method implemented using Matlab® software. For comparison, HVL was also determined using a 30 cm"3 ion chamber and high purity Al filters. (author)

Theory of X-ray absorption and emission spectra

International Nuclear Information System (INIS)

Mukoyama, Takeshi

2004-01-01

Theoretical studies on X-ray absorption and emission spectroscopy are discussed. Simple expressions for X-ray emission rate and X-ray absorption cross section are presented in the dipole approximation. Various atomic models to obtain realistic wave functions and theoretical calculations for X-ray absorption cross sections and X-ray emission rates are described. In the case of molecules and solids, molecular orbital methods for electronic structures and molecular wave functions are discussed. The emphasis is on the procedures to obtain the excited-state and continuum wave functions for molecules and to calculate the multi-center dipole matrix elements. The examples of the calculated X-ray absorption and emission spectra are shown and compared with the experimental results

LINE FORMATION IN SPECTRA OF X-RAY NOVAE

OpenAIRE

Suleimanov, V. F.; Shimansky, V. V.

2017-01-01

Results of X-ray Novae (XN) optical spectra computation are presented. The continuum and Balmer line are calculated. The model of XN as a self-irradiated accretion disk is used. Local (for given radius) disk atmospheres as model stellar atmospheres, heated due to external X-ray radiation are treated. Changes of spectra shape and equivalent widths of the Balmer lines depending from the luminosity and some others accretion disk parameters are investigated. The comparison of GRO JO422+32 observe...

Soft x-ray absorption spectra of ilmenite family.

Science.gov (United States)

Agui, A; Mizumaki, M; Saitoh, Y; Matsushita, T; Nakatani, T; Fukaya, A; Torikai, E

2001-03-01

We have carried out soft x-ray absorption spectroscopy to study the electronic structure of ilmenite family, such as MnTiO3, FeTiO3, and CoTiO3 at the soft x-ray beamline, BL23SU, at the SPring-8. The Ti and M L2,3 absorption spectra of MTiO3 (M=Mn, Fe, and Co) show spectra of Ti4+ and M2+ electron configurations, respectively. Except the Fe L2,3 spectrum, those spectra were understood within the O(h) symmetry around the transition metal ions. The Fe L3-edge spectrum clearly shows a doublet peak at the L3 edge, which is attributed to Fe2+ state, moreover the very high-resolution the L-edge spectra of transition metals show fine structures. The spectra of those ilmenites are compared.

Indirect measure of X-rays spectra using TLDs; Medicion indirecta de espectros de rayos X utilizando TLDs

Energy Technology Data Exchange (ETDEWEB)

Bonzi, E. V.; Mainardi, R. T. [Universidad Nacional de Cordoba, Facultad de Matematica, Astronomia y Fisica, Av. Haya de la Torre y Av. Medina Allende s/n, Ciudad Universitaria, X5016LEA Cordoba (Argentina)

2011-10-15

A methodology of indirect measure of X-rays spectra, emitted by conventional tubes, was developed recently and its feasibility verified in the first place by Monte Carlo simulations. For that case is intended to measure, by means of plastic scintillators, attenuation curves of dispersed beams previously. In this work were carried out measurements of attenuation curves with thermoluminescent dosimeters (TLD) to verify the kindness of the indirect measure method. The attenuation curve was also measured using an ionization chamber brand Capintec (model 192) with the purpose of making a comparison. The results of the attenuation curve measured with both dosimeters present a good resolution inside the statistical fluctuations and the spectral reconstruction using diverse parametric functions is carried out in a quick and simple way with excellent resolutions in the functional form. For this reconstruction method are of fundamental importance the following properties of the used dosimeter: in the first place the repetition of the measures, property that could check; in second place the precision of the measured data and lastly the dosimeter response, this is, the increase of the thermoluminescent signal before an increase of the photons flow of X-rays. This parameter is the gradient of the curve thermoluminescent signal versus the dose imparted to the dosimeter. The measures were realized with a generator of X-rays brand Kevex provided of a conventional tube with tungsten anti cathode that polarizes with high tension to a maximum value of 50 kV and current of 0.5 ma. (Author)

Tetrahedral hydrocarbon nanoparticles in space: X-ray spectra

Science.gov (United States)

Bilalbegović, G.; Maksimović, A.; Valencic, L. A.

2018-06-01

It has been proposed, or confirmed, that diamond nanoparticles exist in various environments in space: close to active galactic nuclei, in the vicinity of supernovae and pulsars, in the interior of several planets in the Solar system, in carbon planets, and other exoplanets, carbon-rich stars, meteorites, in X-ray active Herbig Ae/Be stars, and in the interstellar medium. Using density functional theory methods, we calculate the carbon K-edge X-ray absorption spectrum of two large tetrahedral nanodiamonds: C26H32 and C51H52. We also study and test our methods on the astrophysical molecule CH4, the smallest C-H tetrahedral structure. A possible detection of nanodiamonds from X-ray spectra by future telescopes, such as the project Arcus, is proposed. Simulated spectra of the diffuse interstellar medium using Cyg X-2 as a source show that nanodiamonds studied in this work can be detected by Arcus, a high-resolution X-ray spectrometer mission selected by NASA for a Phase A concept study.

Experimental and Monte Carlo simulated spectra of a liquid-metal-jet x-ray source

International Nuclear Information System (INIS)

Marziani, M.; Gambaccini, M.; Di Domenico, G.; Taibi, A.; Cardarelli, P.

2014-01-01

A prototype x-ray system based on a liquid-metal-jet anode was evaluated within the framework of the LABSYNC project. The generated spectrum was measured using a CZT-based spectrometer and was compared with spectra simulated by three Monte Carlo codes: MCNPX, PENELOPE and EGS5. Notable differences in the simulated spectra were found. These are mainly attributable to differences in the models adopted for the electron-impact ionization cross section. The simulation that more closely reproduces the experimentally measured spectrum was provided by PENELOPE. - Highlights: • The x-ray spectrum of a liquid-jet x-ray anode was measured with a CZT spectrometer. • Results were compared with Monte Carlo simulations using MCNPX, PENELOPE, EGS5. • Notable differences were found among the Monte Carlo simulated spectra. • The key role was played by the electron-impact ionization cross-section model used. • The experimentally measured spectrum was closely reproduced by the PENELOPE code

X-ray spectra of PG quasars. I. The continuum from X-rays to infrared

International Nuclear Information System (INIS)

Elvis, M.; Green, R.F.; Bechtold, J.; Schmidt, M.; Neugebauer, G.; Kitt Peak National Observatory, Tucson, AZ; Steward Observatory, Tucson, AZ; Palomar Observatory, Pasadena, CA)

1986-01-01

Einstein IPC X-ray spectra for a sample of eight optically selected quasars from the Palomar Bright Quasar survey are presented. The quasars have a mean power law energy slope which in five individual cases is inconsistent with the value found in hard X-ray selection criterion rather than luminosity, redshift, or U-B color. New IUE and optical continuum spectra and infrared photometry are presented for these quasars. The data are combined into log vf(v) and log v distributions which support the decomposition of the overall quasar spectrum into a power law plus a superposed optical-UV big bump which may be due to an accretion disk. At least six of the quasars have vf(v)s which are roughly constant between their infrared and X-ray power laws, suggesting a strong link between the two regions. 104 references

Time-resolved soft x-ray spectra from laser-produced Cu plasma

International Nuclear Information System (INIS)

Cone, K.V.; Dunn, J.; Baldis, H.A.; May, M.J.; Purvis, M.A.; Scott, H.A.; Schneider, M.B.

2012-01-01

The volumetric heating of a thin copper target has been studied with time resolved x-ray spectroscopy. The copper target was heated from a plasma produced using the Lawrence Livermore National Laboratory's Compact Multipulse Terrawatt (COMET) laser. A variable spaced grating spectrometer coupled to an x-ray streak camera measured soft x-ray emission (800-1550 eV) from the back of the copper target to characterize the bulk heating of the target. Radiation hydrodynamic simulations were modeled in 2-dimensions using the HYDRA code. The target conditions calculated by HYDRA were post-processed with the atomic kinetics code CRETIN to generate synthetic emission spectra. A comparison between the experimental and simulated spectra indicates the presence of specific ionization states of copper and the corresponding electron temperatures and ion densities throughout the laser-heated copper target.

Lα1 satellites in X-ray emission spectra of higher - Z elements

International Nuclear Information System (INIS)

Poonia, S.

2004-01-01

Full text: The X-ray satellite spectra arising due to 2p 3/2 -1 3x -1 - 3x -1 3d -1 (x ≡ s, p, d) transition array, in elements with Z 74 to 92, have been calculated. While the energies of various transitions of the array have been determined by using available Hartree-Fock-Slater data on 1s -1 - 2p -1 3x -1 and 2p 3/2 -1 - 3x -1 , 3x' -1 Auger transition energies and their relative intensities have been estimated by considering cross - sections of singly ionized 2x -1 (x ≡ s, p) states and then of subsequent Coster-Kronig and shake off processes. The calculated spectra have been compared with the measured satellite energies in Lα1 spectra. Their intense peaks have been identified as the observed satellite lines. The one to one correspondence between the peaks in calculated spectra and the satellites in measured spectra has been established on the basis of the agreement between the separations in the peak energies and those in the measured satellite energies. It has been established that three satellites observed in the Lα 1 region of the X-ray spectra of various elements and named α', α ix and α x in order of increasing energy are mainly emitted by 2p 3/2 -1 3d -1 - 3d -2 transitions. It is observed that the satellite α' in all these spectra can be assigned to the superposition of 3 F 4 - 3 F 4 transition and that this must be most intense one out of all these satellites, contributing in order of decreasing intensity. The line α ix , has been assigned to mainly the 1 F 3 - 1 G 4 , 1 P 1 - 1 D 2 and 1 F 3 - 1 D 2 transitions. Finally, the satellite α x , reported in the spectra of elements with Z = 74-92, has been associated with the transition 3 D 3 - 3 F 4 . The possible contributions of other transitions of the 2p 3/2 -1 3x -1 - 3x -1 3d -1 (x ≡ s, p, d) array having appreciable intensities, have also been discussed

High-energy X-ray spectra of Cygnus XR-1 observed from OSO 8

Science.gov (United States)

Dolan, J. F.; Crannell, C. J.; Dennis, B. R.; Frost, K. J.; Orwig, L. E.

1979-01-01

X-ray spectra of Cygnus XR-1 were measured with the scintillation spectrometer aboard the OSO 8 satellite during a period of one-and-one-half to three weeks in each of the years from 1975 to 1977. Typical spectra of the source between 15 and 250 keV are presented and the spectra are found to be well represented by a single power-law expression whose photon number spectral index is different for the two intensity states that were considered. The observed pivoting effect is consistent with two-temperature accretion disk models of the X-ray emitting region.

Modeling X-ray Spectra of Astrophysical Plasmas: Current Status and Future Needs

Science.gov (United States)

Smith, Randall

Existing high-resolution astrophysical X-ray spectra has exposed the need for high-quality atomic data of all stripes: wavelengths, collisional and absorption cross sections, and radiative rates. The Astro-H soft X-ray spectrometer (2015 launch) will vastly increase the number and type of high-resolution X-ray spectra available and likely expose a number of shortcomings in our models. I will describe recent advances in theoretical calculations and laboratory measurements, as well as a number of existing needs in the field. These include accurate soft X-ray wavelengths for L-shell ions, diagnostic emission line ratios with estimated error bars, and high-resolution absorption cross sections for abundant ions and molecules. Finally, new models of emission from non-equilibrium ionization plasmas and astrophysical charge exchange will be discussed. This latter emission arises due to the interaction of highly charged ions with neutral atoms, forming a diffuse background in the case of solar wind ions and possibly also arising in more distant environments.

An accurate method for computer-generating tungsten anode x-ray spectra from 30 to 140 kV.

Science.gov (United States)

Boone, J M; Seibert, J A

1997-11-01

A tungsten anode spectral model using interpolating polynomials (TASMIP) was used to compute x-ray spectra at 1 keV intervals over the range from 30 kV to 140 kV. The TASMIP is not semi-empirical and uses no physical assumptions regarding x-ray production, but rather interpolates measured constant potential x-ray spectra published by Fewell et al. [Handbook of Computed Tomography X-ray Spectra (U.S. Government Printing Office, Washington, D.C., 1981)]. X-ray output measurements (mR/mAs measured at 1 m) were made on a calibrated constant potential generator in our laboratory from 50 kV to 124 kV, and with 0-5 mm added aluminum filtration. The Fewell spectra were slightly modified (numerically hardened) and normalized based on the attenuation and output characteristics of a constant potential generator and metal-insert x-ray tube in our laboratory. Then, using the modified Fewell spectra of different kVs, the photon fluence phi at each 1 keV energy bin (E) over energies from 10 keV to 140 keV was characterized using polynomial functions of the form phi (E) = a0[E] + a1[E] kV + a2[E] kV2 + ... + a(n)[E] kVn. A total of 131 polynomial functions were used to calculate accurate x-ray spectra, each function requiring between two and four terms. The resulting TASMIP algorithm produced x-ray spectra that match both the quality and quantity characteristics of the x-ray system in our laboratory. For photon fluences above 10% of the peak fluence in the spectrum, the average percent difference (and standard deviation) between the modified Fewell spectra and the TASMIP photon fluence was -1.43% (3.8%) for the 50 kV spectrum, -0.89% (1.37%) for the 70 kV spectrum, and for the 80, 90, 100, 110, 120, 130 and 140 kV spectra, the mean differences between spectra were all less than 0.20% and the standard deviations were less than approximately 1.1%. The model was also extended to include the effects of generator-induced kV ripple. Finally, the x-ray photon fluence in the units of

Automated generation and ensemble-learned matching of X-ray absorption spectra

Science.gov (United States)

Zheng, Chen; Mathew, Kiran; Chen, Chi; Chen, Yiming; Tang, Hanmei; Dozier, Alan; Kas, Joshua J.; Vila, Fernando D.; Rehr, John J.; Piper, Louis F. J.; Persson, Kristin A.; Ong, Shyue Ping

2018-03-01

X-ray absorption spectroscopy (XAS) is a widely used materials characterization technique to determine oxidation states, coordination environment, and other local atomic structure information. Analysis of XAS relies on comparison of measured spectra to reliable reference spectra. However, existing databases of XAS spectra are highly limited both in terms of the number of reference spectra available as well as the breadth of chemistry coverage. In this work, we report the development of XASdb, a large database of computed reference XAS, and an Ensemble-Learned Spectra IdEntification (ELSIE) algorithm for the matching of spectra. XASdb currently hosts more than 800,000 K-edge X-ray absorption near-edge spectra (XANES) for over 40,000 materials from the open-science Materials Project database. We discuss a high-throughput automation framework for FEFF calculations, built on robust, rigorously benchmarked parameters. FEFF is a computer program uses a real-space Green's function approach to calculate X-ray absorption spectra. We will demonstrate that the ELSIE algorithm, which combines 33 weak "learners" comprising a set of preprocessing steps and a similarity metric, can achieve up to 84.2% accuracy in identifying the correct oxidation state and coordination environment of a test set of 19 K-edge XANES spectra encompassing a diverse range of chemistries and crystal structures. The XASdb with the ELSIE algorithm has been integrated into a web application in the Materials Project, providing an important new public resource for the analysis of XAS to all materials researchers. Finally, the ELSIE algorithm itself has been made available as part of veidt, an open source machine-learning library for materials science.

Many-body effects on the x-ray spectra of metals

International Nuclear Information System (INIS)

Satpathy, S.S.

1982-01-01

The effects of band structure, of a solid surface, of temperature, and of disorder on the many-electron x-ray spectra of metals are evaluated in a change-of-mean-field approximation using a one-dimensional nearest-neighbor tight-binding model of a metal. The x-ray spectral shapes are determined by both the band structure and the final-state interactions. The effect of the band being non-free-electron-like is not felt at the x-ray threshold, but away from it such effects are noticeable. When the core hole is created at the surface, the spectra at the edge exhibit a Nozieres-de Dominicis-type singularity with the appropriate surface phase-shifts. At energies away from the edge, the one-particle effects are prominent with the x-ray emission and absorption spectra closely reflecting the local one-electron density of states. The recoil spectrum of a Fermi sea at a non-zero temperature has less asymmetry than the zero-temperature case. It was found that at ordinary temperatures the reduction of the asymmetry due to the thermal distribution of one-electron states is not very significant. Finally, using a one-dimensional Anderson model, the effect of lattice disorder on the x-ray absorption spectra is studied for the first time. There are two effects: (1) the strong infrared divergence peak is gradually quenched as disorder is increased, and (2) the threshold is broadened because the threshold energies for absorption at different sites in the crystal depend on the varying local lattice environment. It is proposed that the x-ray spectra may be useful as a tool for studying the degree of electron localization in disordered many-electron systems

THE XMM-NEWTON X-RAY SPECTRA OF THE MOST X-RAY LUMINOUS RADIO-QUIET ROSAT BRIGHT SURVEY-QSOs: A REFERENCE SAMPLE FOR THE INTERPRETATION OF HIGH-REDSHIFT QSO SPECTRA

International Nuclear Information System (INIS)

Krumpe, M.; Markowitz, A.; Lamer, G.; Corral, A.

2010-01-01

We present the broadband X-ray properties of four of the most X-ray luminous (L X ≥ 10 45 erg s -1 in the 0.5-2 keV band) radio-quiet QSOs found in the ROSAT Bright Survey. This uniform sample class, which explores the extreme end of the QSO luminosity function, exhibits surprisingly homogenous X-ray spectral properties: a soft excess with an extremely smooth shape containing no obvious discrete features, a hard power law above 2 keV, and a weak narrow/barely resolved Fe Kα fluorescence line for the three high signal-to-noise ratio (S/N) spectra. The soft excess can be well fitted with only a soft power law. No signatures of warm or cold intrinsic absorbers are found. The Fe Kα centroids and the line widths indicate emission from neutral Fe (E = 6.4 keV) originating from cold material from distances of only a few light days or further out. The well-constrained equivalent widths (EW) of the neutral Fe lines are higher than expected from the X-ray Baldwin effect which has been only poorly constrained at very high luminosities. Taking into account our individual EW measurements, we show that the X-ray Baldwin effect flattens above L X ∼ 10 44 erg s -1 (2-10 keV band) where an almost constant (EW) of ∼100 eV is found. We confirm the assumption of having very similar X-ray active galactic nucleus properties when interpreting stacked X-ray spectra. Our stacked spectrum serves as a superb reference for the interpretation of low S/N spectra of radio-quiet QSOs with similar luminosities at higher redshifts routinely detected by XMM-Newton and Chandra surveys.

Analysis of X-Ray (L) spectra of heavy elements

International Nuclear Information System (INIS)

Souza Coelho, L.F. de.

1976-08-01

The general problem of obtaining and analysing spectra is presented, with emphasis in the comparison of methods for the analysis of gamma rays and X rays. The method proposed to obtain a standard and later the intensities of lines of an X-ray (L) spectrum is discussed. The good eesults obtained by the program RAIOXL, when simulated spectra are used, and by the program RAIXL1, when doublets are decomposed, are shown. In annex A, the listings of the programs used are presented, and in annex B a review is made of the analytical formulae used for adjustment of the pulses. (I.C.R.) [pt

Indirect measurements of X-ray spectra; Mediciones indirectas de espectros de rayos X

Energy Technology Data Exchange (ETDEWEB)

Mainardi, R.T. [Facultad de Matematica, Astronomia y Fisica, Universidad Nacional de Cordoba, X5000HUA Cordoba (Argentina)

2006-07-01

To the effects of measuring the spectral distribution of the radiation emitted by the x-ray tubes and electron accelerators, numerous procedures that are grouped in two big categories exist at the present time: direct and indirect methods. The first ones use high resolution detectors that should be positioned, together with the appropriate collimator, in the direction of the x ray beam. The user should be an expert in the use and correction of the obtained data by the different effects that affect the detector operation such as efficiency and resolution in terms of the energy of the detected radiation. The indirect procedures, although its are more simple to use, its also require a considerable space along the beam to position the ionization chamber and the necessary absorbents to construct by this way the denominated attenuation curve. We will analyze the operation principle of the indirect methods and a new proposal in which such important novelties are introduced as the beam dispersion to avoid to measure along the main beam and that of determination of the attenuation curve in simultaneous form. By this way, with a single shot of the tube, the attenuation curve is measured, being necessary at most a shot of additional calibration to know the relative response of the detectors used in the experimental array. The physical processes involved in the obtaining of an attenuation curve are very well well-known and this it finishes it can be theoretically calculated if the analytic form of the spectrum is supposed well-known. Finally, we will see a spectra reconstruction example with the Kramers parametric form and comparisons with numeric simulations carried out with broadly validated programs as well as the possibility of the use of solid state dosemeters in the obtention of the attenuation curve. (Author)

Laboratory Studies of X-ray Spectra Formed by Charge Exchange

Science.gov (United States)

Beiersdorfer, Peter; Ali, R.; Brown, G. V.; Koutroumpa, D.; Kelley, R. L.; Kilbourne, C.; Leutenegger, M. A.; Porter, F.

2013-04-01

Charge exchange between ions and neutral atoms or molecules has been accepted at an important soft producing process in our solar system. By extension, charge exchange may contribute to the X-ray emission of circumstellar material. It may also produce X-ray emission at the boundaries of supernova ejecta and star burst galaxies, or whenever hot plasma collides with neutral matter. X-ray spectra of K-shell and L-shell ions formed by charge exchange have now been studied in a variety of laboratory settings. These experiments have shown several characteristic features of line formation by charge exchange when compared to the X-ray emission produced by electron-impact excitation, e.g., enhancement emission of forbidden lines and of lines from levels with high principal quantum number. They have also shown a dependence on the interaction gas and on the energy of the ion-neutral collision. Moreover, the transfer of multiple electrons is typically preferred, provided the donor molecules or atoms have multiple valence-shell electrons. The laboratory measurements are in qualitative agreement with theory. However, the details of the observed X-ray spectra, especially those recorded with high spectral resolution, can differ substantially from predictions, especially for spectra produced at collision velocities equal to or lower than those found in thermal plasmas or produced with neutral gases other than atomic hydrogen. Puzzling discrepancies can be noted, such as enhanced emission from an upper level with the 'wrong' principal quantum number. Even more puzzling is a recent experiment in which two, co-mixed bare ion species of similar atomic number produce very different Lyman series emission upon charge exchange with a given neutral gas, defying both theoretical predictions and empirical scaling. Laboratory measurements have also shown that some of the characteristic features of charge exchange can be reproduced by radiative electron capture, i.e., by capture of a continuum

Envelope method for background elimination from X-ray fluorescence spectra

International Nuclear Information System (INIS)

Monakhov, V.V.; Naumenko, P.A.; Chashinskaya, O.A.

2006-01-01

The influence of the background noise caused by Bremsstrahlung on the accuracy of the envelope method at x-ray fluorescence spectra processing is studied. This is carried out by the example of model spectra at different forms of Bremsstrahlung noise as well as at the presence of background noise in spectra. The interpolation by parabolic splines is used for the estimation of the error of the envelope method for the elimination of continuos background noise. It is found out that the error of the proposed method constitutes decimal parts of percent. It is shown that the envelope method is the effective technique for the elimination of the continuous Bremsstrahlung from x-ray fluorescence spectra of the first order [ru

An optimal ross filter system for soft X-ray spectra measurement

International Nuclear Information System (INIS)

Huang Tianxuan; Zheng Zhijian; Sun Kexu; Jiang Shaoen

2000-01-01

A broadband Ross filter spectrometer is described for measuring soft X-ray radiation (0.1∼1.5 keV) emitted from laser plasma. It consists of a number of channels, each representing a Ross filter pair in conjunction with Al cathode X-ray diodes. An optimal channel has flat response within the sensitivity band, and minimal response outside it. The effect of some uncertainties on the accuracy of measurements is calculated

An examination of mass thickness measurements with X-ray sources

International Nuclear Information System (INIS)

Chen Mincong; Li Hongmei; Chen Ziyu; Shen Ji

2008-01-01

A method using X-rays to measure mass thickness is discussed. The method utilizes a filter to absorb low energy and characteristic photons so that the hardened X-ray spectra have a peaked energy distribution. An equivalent X-ray energy, which defines the attenuation in a material of interest can be used. The effect on the X-ray spectra of different filters is examined with Monte Carlo simulation using the EGSnrc package. A theoretical model for X-ray absorption that shows that the method can achieve good precision for a certain range of mass thicknesses is advanced. Experimental results agree well with the theoretical analysis. It is found that for a certain range of mass thicknesses, the relative error can be less than 1% for the aluminum alloy sample at the tube voltage of 30 or 45 kV

An examination of mass thickness measurements with X-ray sources

Energy Technology Data Exchange (ETDEWEB)

Chen Mincong; Li Hongmei; Chen Ziyu [Department of Modern Physics, University of Science and Technology of China, Jin Zhai Road, Hefei 230026 (China); Shen Ji [Department of Modern Physics, University of Science and Technology of China, Jin Zhai Road, Hefei 230026 (China)], E-mail: shenji@ustc.edu.cn

2008-10-15

A method using X-rays to measure mass thickness is discussed. The method utilizes a filter to absorb low energy and characteristic photons so that the hardened X-ray spectra have a peaked energy distribution. An equivalent X-ray energy, which defines the attenuation in a material of interest can be used. The effect on the X-ray spectra of different filters is examined with Monte Carlo simulation using the EGSnrc package. A theoretical model for X-ray absorption that shows that the method can achieve good precision for a certain range of mass thicknesses is advanced. Experimental results agree well with the theoretical analysis. It is found that for a certain range of mass thicknesses, the relative error can be less than 1% for the aluminum alloy sample at the tube voltage of 30 or 45 kV.

Quantum chemistry interpretation of x-ray spectra

International Nuclear Information System (INIS)

Bocharov, D.; Kuzmin, A.

2005-01-01

Full text: In this study, we present the results of ab initio computer simulations on X-ray absorption spectra of some perovskite-type tungsten oxides. For our calculations, we combine a periodic bulk model with Hartree-Fock method including a posteriori electron correlation corrections, as implemented in CRYSTAL98 computer code [1]. First, we describe the results of calculations performed on some bulk properties of the tungsten oxides (lattice constant and bulk modulus), in order to achieve the necessary level of agreement with available experimental and theoretical data. Our calculations on the densities of oneelectron energy states (DOS) for models of tungsten oxides are verified by experimental X-ray absorption spectra, which allow us to make correct qualitative interpretation of the latter. The main difficulties appearing during our first principles simulations will be discussed. [1] V.R. Saunders, R. Dovesi, C. Roetti, M. Causi, N.M. Harrison, R. Orlando, and C.M. Zicovich-Wilson, CRYSTAL-98 User Manual, University of Turin, 1999

Measurement of high-dynamic range x-ray Thomson scattering spectra for the characterization of nano-plasmas at LCLS

Energy Technology Data Exchange (ETDEWEB)

MacDonald, M. J., E-mail: macdonm@umich.edu [University of Michigan, Ann Arbor, Michigan 48109 (United States); SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Gorkhover, T. [SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Technische Universität, 10623 Berlin (Germany); Bachmann, B.; Hau-Riege, S. P.; Pardini, T.; Döppner, T. [Lawrence Livermore National Laboratory, Livermore, California 94551 (United States); Bucher, M. [SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Argonne National Lab, Lemont, Illinois 60439 (United States); Carron, S. [California Lutheran University, Thousand Oaks, California 91360 (United States); Coffee, R. N.; Fletcher, L. B.; Gamboa, E. J.; Glenzer, S. H.; Göde, S.; Krzywinski, J.; O’Grady, C. P.; Osipov, T.; Swiggers, M. [SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Drake, R. P. [University of Michigan, Ann Arbor, Michigan 48109 (United States); Ferguson, K. R. [SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Stanford University, Stanford, California 94305 (United States); Kraus, D. [University of California, Berkeley, California 94720 (United States); and others

2016-11-15

Atomic clusters can serve as ideal model systems for exploring ultrafast (∼100 fs) laser-driven ionization dynamics of dense matter on the nanometer scale. Resonant absorption of optical laser pulses enables heating to temperatures on the order of 1 keV at near solid density conditions. To date, direct probing of transient states of such nano-plasmas was limited to coherent x-ray imaging. Here we present the first measurement of spectrally resolved incoherent x-ray scattering from clusters, enabling measurements of transient temperature, densities, and ionization. Single shot x-ray Thomson scattering signals were recorded at 120 Hz using a crystal spectrometer in combination with a single-photon counting and energy-dispersive pnCCD. A precise pump laser collimation scheme enabled recording near background-free scattering spectra from Ar clusters with an unprecedented dynamic range of more than 3 orders of magnitude. Such measurements are important for understanding collective effects in laser-matter interactions on femtosecond time scales, opening new routes for the development of schemes for their ultrafast control.

Soft x-ray measurements from the PDX tokamak

International Nuclear Information System (INIS)

Silver, E.H.; Bitter, M.; Brau, K.; Eames, D.; Greenberger, A.; Hill, K.W.; Meade, D.M.; Roney, W.; Sauthoff, N.R.; von Goeler, S.

1982-05-01

Temporally and spatially-resolved profiles of the PDX soft x-ray spectra have been measured during single tokamak pulses of circular and divertor plasmas with a recently developed pulse height analyzer. This detection system incorporates an array of five vertically displaced sets of lithium-drifted silicon detectors, each consisting of three independent channels optimized for rapid data collection in adjacent energy regions. Simultaneous measurement of x-ray emission integrated along five chords of the plasma cross section can thereby be achieved. Abel inversion of these data yields temporally-resolved radial profiles of the local electron temperature from the slope of the continuum, concentrations of high-Z impurities from the characteristic line intensities, and a measure of Z/sub eff/ from the continuum intensity. The techniques of x-ray pulse height analysis, with illustrations featuring the results from the initial PDX circular plasma experiments are discussed in detail. In addition, comparisons between circular and divertor plasmas on PDX, derived from the x-ray measurements, are also presented

Modeling of X-ray Images and Energy Spectra Produced by Stepping Lightning Leaders

Science.gov (United States)

Xu, Wei; Marshall, Robert A.; Celestin, Sebastien; Pasko, Victor P.

2017-11-01

Recent ground-based measurements at the International Center for Lightning Research and Testing (ICLRT) have greatly improved our knowledge of the energetics, fluence, and evolution of X-ray emissions during natural cloud-to-ground (CG) and rocket-triggered lightning flashes. In this paper, using Monte Carlo simulations and the response matrix of unshielded detectors in the Thunderstorm Energetic Radiation Array (TERA), we calculate the energy spectra of X-rays as would be detected by TERA and directly compare with the observational data during event MSE 10-01. The good agreement obtained between TERA measurements and theoretical calculations supports the mechanism of X-ray production by thermal runaway electrons during the negative corona flash stage of stepping lightning leaders. Modeling results also suggest that measurements of X-ray bursts can be used to estimate the approximate range of potential drop of lightning leaders. Moreover, the X-ray images produced during the leader stepping process in natural negative CG discharges, including both the evolution and morphological features, are theoretically quantified. We show that the compact emission pattern as recently observed in X-ray images is likely produced by X-rays originating from the source region, and the diffuse emission pattern can be explained by the Compton scattering effects.

X ray spectra and qualities for use in diagnostic radiology and equipment calibration

International Nuclear Information System (INIS)

Souza, Karla Cristina de

1996-12-01

The goal of this work was the standardization of radiation qualities of diagnostic X ray equipment of the Assay Laboratory of the Institute for Radiation Protection and Dosimetry (IRD) of the National Commission of Nuclear Energy, Brazil. X ray spectra were determined from pulse height distribution measured directly on the primary beam using a high pure planar Ge detector. A program was developed to convert pulse height distribution into radiation spectra in the range from 20 to 150 keV. X ray qualities based on those used by the 'Physikalish-Technish Bundesantalt' (PTB) primary laboratory were implanted in three radiological equipment of the Assay Laboratory. These qualities simulate radiation beams on patients submitted to typical radiological examinations. Besides the spectrometric system, a reference measurement system based on an ionization chamber calibrated in air kerma was used to establish parameters such as kilovoltage, first and second half-value layer, mean energy, effective energy and inherent filtration. Our data have shown that the implantation of these radiation qualities in the Assay Laboratory results on a metrological basis for calibration of dose measurement assemblies and kV-meters, like those used by IRD to evaluate the parameters of X ray equipment around the country. A catalogue of spectral data resulting from this work is a data bank that allows various applications like dose calculation using Monte Carlo simulation techniques. (author)

Broadband X-ray spectra of the ultraluminous x-ray source Holmberg IX X-1 observed with NuSTAR, XMM-Newton, and Suzaku

DEFF Research Database (Denmark)

Walton, D. J.; Harrison, F. A.; Grefenstette, B. W.

2014-01-01

We present results from the coordinated broadband X-ray observations of the extreme ultraluminous X-ray source Holmberg IX X-1 performed by NuSTAR, XMM-Newton, and Suzaku in late 2012. These observations provide the first high-quality spectra of Holmberg IX X-1 above 10 keV to date, extending the...

Spatial power-spectra from Yohkoh soft X-ray images

Science.gov (United States)

Martens, Petrus C. H.; Gomez, Daniel O.

1992-01-01

We analyze three sequences of images from active regions, and a full disk image obtained by Yohkoh's Soft X-ray Telescope. Two sequences are from a region at center disk observed through different filters, and one sequence is from the limb. After Fourier-transforming the X-ray intensity of the images we find nearly isotropic power-spectra with an azimuthally integrated slope of -2.1 for the center disk, and -2.8 for the limb images. The full-disk picture yields a spectrum of -2.4. These results are different from the active region spectra obtained with the Normal Incidence X-ray Telescope which have a slope of the order of -3.0, and we ascribe this to the difference in temperature response between the instruments. However, both the SXT and NIXT results are consistent with coronal heating as the end result of a downward quasistatic cascade (in lengthscales) of free magnetic energy in the corona, driven by footpoint motions in the photosphere.

Quasar energy distributions. I. Soft X-ray spectra of quasars

International Nuclear Information System (INIS)

Wilkes, B.J.; Elvis, M.

1987-01-01

As the initial stage of a study of quasar energy distributions (QEDs), Einstein IPC spectra of 24 quasars are presented. These are combined with previously reported IPC spectra to form a sample of 33 quasars with well-determined soft X-ray slopes. A correlation analysis shows that radio loudness, rather than redshift or luminosity, is fundamentally related to the X-ray slope. This correlation is not followed by higher energy spectra of active galaxies. Two components are required to explain both sets of results. The best-fit column densities are systematically smaller than the Galactic values. The same effect is not present in a sample of BL Lac objects, implying that the effect is intrinsic to the quasars and is caused by a low-energy turnup in the quasar spectra. 74 references

On the origin of X-ray spectra in luminous blazars

International Nuclear Information System (INIS)

Sikora, Marek; Janiak, Mateusz; Moderski, Rafał; Nalewajko, Krzysztof; Madejski, Greg M.

2013-01-01

Gamma-ray luminosities of some quasar-associated blazars imply jet powers reaching values comparable to the accretion power even if assuming very strong Doppler boosting and very high efficiency of gamma-ray production. With much lower radiative efficiencies of protons than of electrons, and the recent reports of very strong coupling of electrons with shock-heated protons indicated by particle-in-cell simulations, the leptonic models seem to be strongly favored over the hadronic ones. However, the electron-proton coupling combined with the external-radiation-Compton (ERC) models of gamma-ray production in leptonic models predict extremely hard X-ray spectra, with energy indices α x ∼ 0. This is inconsistent with the observed 2-10 keV slopes of blazars, which cluster around α x ∼ 0.6. This problem can be resolved by assuming that electrons can be efficiently cooled down radiatively to non-relativistic energies, or that blazar spectra are entirely dominated by the synchrotron self-Compton (SSC) component up to at least 10 keV. Here, we show that the required cooling can be sufficiently efficient only at distances r < 0.03 pc. SSC spectra, on the other hand, can be produced roughly co-spatially with the observed synchrotron and ERC components, which are most likely located roughly at a parsec scale. We show that the dominant SSC component can also be produced much further than the dominant synchrotron and ERC components, at distances of ≳ 10 pc. Hence, depending on the spatial distribution of the energy dissipation along the jet, one may expect to see γ-ray/optical events with either correlated or uncorrelated X-rays. In all cases the number of e + e – pairs per proton is predicted to be very low. The direct verification of the proposed SSC scenario, and particularly the question of the co-spatiality of the SSC component with other spectral components, requires sensitive observations in the hard X-ray band. This is now possible with the deployment of the Nu

Determination of x-ray spectra incident on and transmitted through whole excised breast for improved mammographic exposing technique

International Nuclear Information System (INIS)

Haus, A.G.; Metz, C.E.; Doi, K.; Bernstein, J.

1976-01-01

Measurements were made of x-ray spectra incident on and transmitted through whole excised fresh breast tissue. The spectra and corresponding radiographs show that hardening of the x-ray beam from a molybdenum anode x-ray tube by a 0.5 mm Al filter instead of the conventional 0.03 mm Mo filter allows shorter exposure times and reduces patient radiation exposure. With the Al filter, acceptable image contrast is preserved in mammography of thick or dense breasts

High resolution krypton M/sub 4,5/ x-ray emission spectra

International Nuclear Information System (INIS)

Perera, R.C.C.; Hettrick, M.C.; Lindle, D.W.

1987-10-01

High resolution M/sub 4,5/ (3d → 4p) x-ray emission spectra from a krypton plasma were measured using a recently developed grazing-incidence reflection-grating monochromator/spectrometer with very high flux rates at extreme ultraviolet and soft x-ray wave lengths. The nominal resolving power of the instrument, E/ΔE, is about 300 in this energy range (∼80 eV). Three dipole-allowed 3d → 4p emission lines were observed at 80.98 eV, 80.35 eV and 79.73 eV. A broad peak at about 82.3 eV is tentatively assigned to transitions resulting from Kr 2+ , and effects of excitation energy on M/sub 4,5/ x-ray emission were observed. 9 refs., 3 figs., 1 tab

INTEGRAL hard X-ray spectra of the cosmic X-ray background and Galactic ridge emission

Science.gov (United States)

Türler, M.; Chernyakova, M.; Courvoisier, T. J.-L.; Lubiński, P.; Neronov, A.; Produit, N.; Walter, R.

2010-03-01

Aims: We derive the spectra of the cosmic X-ray background (CXB) and of the Galactic ridge X-ray emission (GRXE) in the ~20-200 keV range from the data of the IBIS instrument aboard the INTEGRAL satellite obtained during the four dedicated Earth-occultation observations in early 2006. Methods: We analyze the modulation of the IBIS/ISGRI detector counts induced by the passage of the Earth through the field of view of the instrument. Unlike previous studies, we do not fix the spectral shape of the various contributions, but model instead their spatial distribution and derive for each of them the expected modulation of the detector counts. The spectra of the diffuse emission components are obtained by fitting the normalizations of the model lightcurves to the observed modulation in different energy bins. Because of degeneracy, we guide the fits with a realistic choice of the input parameters and a constraint for spectral smoothness. Results: The obtained CXB spectrum is consistent with the historic HEAO-1 results and falls slightly below the spectrum derived with Swift/BAT. A 10% higher normalization of the CXB cannot be completely excluded, but it would imply an unrealistically high albedo of the Earth. The derived spectrum of the GRXE confirms the presence of a minimum around 80 keV with improved statistics and yields an estimate of ~0.6 M⊙ for the average mass of white dwarfs in the Galaxy. The analysis also provides updated normalizations for the spectra of the Earth's albedo and the cosmic-ray induced atmospheric emission. Conclusions: This study demonstrates the potential of INTEGRAL Earth-occultation observations to derive the hard X-ray spectra of three fundamental components: the CXB, the GRXE and the Earth emission. Further observations would be extremely valuable to confirm our results with improved statistics.

Modeling of X-ray images and energy spectra produced by stepping lightning leaders

OpenAIRE

Xu , Wei; Marshall , Robert A.; Celestin , Sébastien; Pasko , Victor P.

2017-01-01

International audience; Recent ground-based measurements at the International Center for Lightning Research and Testing (ICLRT) have greatly improved our knowledge of the energetics, fluence, and evolution of X-ray emissions during natural cloud-to-ground (CG) and rocket-triggered lightning flashes. In this paper, using Monte Carlo simulations and the response matrix of unshielded detectors in the Thunderstorm Energetic Radiation Array (TERA), we calculate the energy spectra of X-rays as woul...

Theoretical modeling of Comptonized X-ray spectra of super-Eddington accretion flow: Origin of hard excess in ultraluminous X-ray sources

Science.gov (United States)

Kitaki, Takaaki; Mineshige, Shin; Ohsuga, Ken; Kawashima, Tomohisa

2017-12-01

X-ray continuum spectra of super-Eddington accretion flow are studied by means of Monte Carlo radiative transfer simulations based on the radiation hydrodynamic simulation data, in which both thermal- and bulk-Compton scatterings are taken into account. We compare the calculated spectra of accretion flow around black holes with masses of MBH = 10, 102, 103, and 104 M⊙ for a fixed mass injection rate (from the computational boundary at 103 rs) of 103 LEdd/c2 (with rs, LEdd, and c being the Schwarzschild radius, the Eddington luminosity, and the speed of light, respectively). The soft X-ray spectra exhibit mass dependence in accordance with the standard-disk relation; the maximum surface temperature is scaled as T ∝ M_{ BH}^{ -1/4}. The spectra in the hard X-ray band, by contrast with soft X-ray, look to be quite similar among different models, if we normalize the radiation luminosity by MBH. This reflects that the hard component is created by thermal- and bulk-Compton scatterings of soft photons originating from an accretion flow in the overheated and/or funnel regions, the temperatures of which have no dependence on mass. The hard X-ray spectra can be reproduced by a Wien spectrum with the temperature of T ˜ 3 keV accompanied by a hard excess at photon energy above several keV. The excess spectrum can be fitted well with a power law with a photon index of Γ ˜ 3. This feature is in good agreement with that of the recent NuSTAR observations of ULXs (ultra-luminous X-ray sources).

High-resolution x-ray photoemission spectra of silver

DEFF Research Database (Denmark)

Barrie, A.; Christensen, N. E.

1976-01-01

An electron spectrometer fitted with an x-ray monochromator for Al Kα1,2 radiation (1486.6 eV) has been used to record high-resolution x-ray photoelectron spectra for the 4d valence band as well as the 3d spin doublet in silver. The core-level spectrum has a line shape that can be described...... successfully in terms of the many-body theory of Mahan, Nozières, and De Dominicis. The 4d spectrum agrees well with predictions based on a relativistic-augmented-plane-wave band-structure calculation....

Model independent method to deconvolve hard X-ray spectra

Energy Technology Data Exchange (ETDEWEB)

Polcaro, V.F.; Bazzano, A.; Ubertini, P.; La Padula, C. (Consiglio Nazionale delle Ricerche, Frascati (Italy). Lab. di Astrofisica Spaziale); Manchanda, R.K. (Tata Inst. of Fundamental Research, Bombay (India))

1984-07-01

A general purpose method to deconvolve the energy spectra detected by means of the use of a hard X-ray telescope is described. The procedure does not assume any form of input spectrum and the observed energy loss spectrum is directly deconvolved into the incident photon spectrum, the form of which can be determined independently of physical interpretation of the data. Deconvolution of the hard X-ray spectrum of Her X-1, detected during the HXR 81M experiment, by the method independent method is presented.

OSO 8 X-ray spectra of clusters of galaxies. II - Discussion

Science.gov (United States)

Smith, B. W.; Mushotzky, R. F.; Serlemitsos, P. J.

1979-01-01

An observational description of X-ray clusters of galaxies is given based on OSO 8 X-ray results for spatially integrated spectra of 20 such clusters and various correlations obtained from these results. It is found from a correlation between temperature and velocity dispersion that the X-ray core radius should be less than the galaxy core radius or, alternatively, that the polytropic index is about 1.1 for most of the 20 clusters. Analysis of a correlation between temperature and emission integral yields evidence that more massive clusters accumulate a larger fraction of their mass as intracluster gas. Galaxy densities and optical morphology, as they correlate with X-ray properties, are reexamined for indications as to how mass injection by galaxies affects the density structure of the gas. The physical arguments used to derive iron abundances from observed equivalent widths of iron line features in X-ray spectra are critically evaluated, and the associated uncertainties in abundances derived in this manner are estimated to be quite large.

Optimization of tungsten x-ray spectra for digital mammography: a comparison of model to experiment

Science.gov (United States)

Andre, Michael P.; Spivey, Brett A.

1997-05-01

Tungsten (W) target x-rays tubes are being studied for use in digital mammography to improve x-ray flux, reduce noise and increase tube heat capacity. A parametric model was developed for digital mammography to evaluate optimization of x-ray spectra for a particular sensor. The model computes spectra and mean glandular doses (MGD) for combinations of W target, beam filters, kVp, breast type and thickness. Two figures of merit were defined: (signal/noise)2/MGD and spectral quantum efficiency; these were computed as a means to approach optimization of object contrast. The model is derived from a combination of classic equations, XCOM from NBS, and published data. X-ray spectra were calculated and measured for filters of Al, Sn, Rh, Mo and Ag on a Eureka tube. (Signal/noise)2/MGD was measured for a filtered W target tube and a digital camera employing CsI scintillator optically coupled to a CCD for which the detective quantum efficiency (DQE) was known. A 3-mm thick acrylic disk was imaged on thickness of 3-8 cm of acrylic and the results were compared to the predictions of the model. The relative error between predicted and measured spectra was +/- 2 percent from 24 to 34 kVp. Calculated MGD as a function of breast thickness, half-value layer and beam filter compares very well to published data. Best performance was found for the following combinations: Mo filter with 30 mm breast, Ag filter with 45 mm, Sn filter for 60 mm, and Al filter for 75 mm thick breast. The parametric model agrees well with measurement and provides a means to explore optimum combinations of kVp and beam filter. For a particular detector, this data may be used with the DQE to estimate total system signal-to-noise ratio for a particular imaging task.

The X-ray electronic spectra of TiC-NbC solid solution

International Nuclear Information System (INIS)

Cherkashenko, V.M.; Ezhov, A.V.; Nazarova, S.Z.; Kurmaev, Eh.Z.; Nojmann, M.

2001-01-01

X-ray photoelectronic spectra of inner levels and valency lands in TiC-NbC solid solutions were studied. Results of combining TiL α -, NbL β2.15 -, CK α - X-ray emission spectra and photoelectronic spectra of valency bands in one energy scale in reference to the Fermi level were analyzed. It is shown that a change in crystal lattice parameters, as well as charge redistribution between titanium and niobium atoms, produce a strong effect on electronic structure formation in the mixed carbides mentioned [ru

Characteristics of an intrinsic germanium detector for measurement of soft x-rays from high-temperature plasmas

International Nuclear Information System (INIS)

Kumagai, Katsuaki; Matoba, Tohru; Funahashi, Akimasa; Kawakami, Tomohide

1976-09-01

An intrinsic germanium (Ge(I)) detector has been prepared for measurement of soft X-ray spectra from high-temperature tokamak plasmas. Its characteristics of photo-peak efficiency, escape-peak and Compton scattering were calibrated with standard radioisotopes and soft X-rays from the JFT-2a plasma, and compared with those of a lithium-drifted silicon (Si(Li)) detector. Features of the Ge(I) detector are as follows: (i) high detection efficiency in the high energy range, (ii) wide energy range for measurement of soft X-ray spectra, and (iii) low Compton scattering effect in measurement of continuous spectra. Its dead-layer depth is about 0.06μm, and the minimum detectable energies in the Ge(I) detector are similar to those in the Si(Li) detector. The Ge(I) detector is effective for measuring soft X-ray spectra from high-temperature tokamak plasmas. (auth.)

X-ray spectra of clusters of galaxies

Science.gov (United States)

Sarazin, Craig L.

1990-01-01

X-ray line observations of clusters of galaxies have shown that the X-ray emission in clusters is mainly thermal emission from hot diffuse gas, and that much of this gas has come out of stars, probably having been ejected from galaxies in the cluster. Future high resolution observations should allow us to determine the physical state of the gas. X-ray line measurements and abundance determinations can lead to strong constraints on the origin of the intracluster gas, and on the chemical evolution and history of galaxies. Some of the stronger resonant X-ray lines may be observable as absorption lines against a background quasar. Such X-ray absorption line measurement can be used to directly derive distances to clusters, using a technique similar to (and possibly complementary to) that the well-known method using the Zel'dovich-Syunyaev effect.

SU-F-I-76: Fluoroscopic X-Ray Beam Profiles for Spectra Incorporating Copper Filtration

Energy Technology Data Exchange (ETDEWEB)

Wunderle, K [Cleveland Clinic Foundation, Cleveland, OH (United States); Wayne State University School of Medicine, Detroit, MI (United States); Godley, A; Shen, Z; Dong, F [Cleveland Clinic Foundation, Cleveland, OH (United States); Rakowski, J [Wayne State University School of Medicine, Detroit, MI (United States)

2016-06-15

Purpose: The purpose of this investigation is to characterize and quantify X-ray beam profiles for fluoroscopic x-ray beam spectra incorporating spectral (copper) filtration. Methods: A PTW (Freiburg, Germany) type 60016 silicon diode detector and PTW MP3 water tank were used to measure X-ray beam profiles for 60, 80, 100 and 120 kVp x-ray beams at five different copper filtration thicknesses ranging from 0–0.9 mm at 22 and 42 cm fields of view and depths of 1, 5, and 10 cm in both the anode-cathode axis (inplane) and cross-plane directions. All measurements were acquired on a Siemens (Erlangen, Germany) Artis ZeeGo fluoroscope inverted from the typical orientation providing an x-ray beam originating from above the water surface with the water level set at 60 cm from the focal spot. Results: X-ray beam profiles for beam spectra without copper filtration compared well to previously published data by Fetterly et al. [Med Phys, 28, 205 (2001)]. Our data collection benefited from the geometric orientation of the fluoroscope, providing a beam perpendicular to the tank water surface, rather than through a thin side wall as did the previously mentioned study. Profiles for beams with copper filtration were obtained which have not been previously investigated and published. Beam profiles in the anode-cathode axis near the surface and at lower x-ray energy exhibited substantial heel effect, which became less pronounced at greater depth. At higher energy with copper filtration in the beam, the dose falloff out-of-field became less pronounced, as would be anticipated given higher scatter photon energy. Conclusion: The x-ray beam profile data for the fluoroscopic x-ray beams incorporating copper filtration are intended for use as reference data for estimating doses to organs or soft tissue, including fetal dose, involving similar beam qualities or for comparison with mathematical models.

Invisible structures in the X-ray absorption spectra of actinides

NARCIS (Netherlands)

Kvashnina, Kristina O.; De Groot, Frank M F

The X-ray absorption spectra of actinides are discussed with an emphasis on the fundamental effects that influence their spectral shape, including atomic multiplet theory, charge transfer theory and crystal field theory. Many actinide spectra consist of a single peak and it is shown that the use of

X-ray spectra and time variability of active galactic nuclei

International Nuclear Information System (INIS)

Mushotzky, R.F.

1984-02-01

The X-ray spectra of broad line active galactic nuclei (AGN) of all types (Seyfert I's, NELG's, broadline radio galaxies) are well fit by a power law in the .5 to 100 keV band of man energy slope alpha .68 + or - .15. There is, as yet, no strong evidence for time variability of this slope in a given object. The constraints that this places on simple models of the central energy source are discussed. BL Lac objects have quite different X-ray spectral properties and show pronounced X-ray spectral variability. On time scales longer than 12 hours most radio quiet AGN do not show strong, delta I/I .5, variability. The probability of variability of these AGN seems to be inversely related to their luminosity. However characteristics timescales for variability have not been measured for many objects. This general lack of variability may imply that most AGN are well below the Eddington limit. Radio bright AGN tend to be more variable than radio quiet AGN on long, tau approx 6 month, timescales

Laser plasma x-ray source for ultrafast time-resolved x-ray absorption spectroscopy

Directory of Open Access Journals (Sweden)

L. Miaja-Avila

2015-03-01

Full Text Available We describe a laser-driven x-ray plasma source designed for ultrafast x-ray absorption spectroscopy. The source is comprised of a 1 kHz, 20 W, femtosecond pulsed infrared laser and a water target. We present the x-ray spectra as a function of laser energy and pulse duration. Additionally, we investigate the plasma temperature and photon flux as we vary the laser energy. We obtain a 75 μm FWHM x-ray spot size, containing ∼106 photons/s, by focusing the produced x-rays with a polycapillary optic. Since the acquisition of x-ray absorption spectra requires the averaging of measurements from >107 laser pulses, we also present data on the source stability, including single pulse measurements of the x-ray yield and the x-ray spectral shape. In single pulse measurements, the x-ray flux has a measured standard deviation of 8%, where the laser pointing is the main cause of variability. Further, we show that the variability in x-ray spectral shape from single pulses is low, thus justifying the combining of x-rays obtained from different laser pulses into a single spectrum. Finally, we show a static x-ray absorption spectrum of a ferrioxalate solution as detected by a microcalorimeter array. Altogether, our results demonstrate that this water-jet based plasma source is a suitable candidate for laboratory-based time-resolved x-ray absorption spectroscopy experiments.

A method to unfold the efficiency of gaseous detectors exposed to broad X-ray spectra

International Nuclear Information System (INIS)

Almeida, Gevaldo L. de; Souza, Maria Ines S. de; Lopes, Ricardo T.

2000-01-01

A method to obtain the efficiency of a gaseous detector exposed to broad energy X-ray spectra was developed. It consists in the de-convolution of the integrated detector response using the shapes of those spectra as a tool to unfold the aimed detector efficiency curve. For this purpose, the spectra emitted by a X-ray tube under several anode voltages, were properly characterized through measurements with a NaI(Tl) spectrometer. A Lorentz function was then fitted to each of the spectra, and their parameters expressed as a function of the anode voltage, by using polynomial and gaussian fittings. The integral of the product of each Lorentz function, by another unknown Lorentz function, expressing the detector efficiency curve, represents the response of the detector for each anode tension, e.g., each X-ray spectrum. The symbolical integration of that product, produces a general function containing the unknown parameters of the unknown efficiency curve. A non-linear fitting of this general function, to the detector response points, as experimentally obtained, generates the aimed parameters for the efficiency curve. The final detector efficiency curve is obtained after normalization procedures. (author)

Wavelength dispersive X-ray absorption fine structure imaging by parametric X-ray radiation

International Nuclear Information System (INIS)

Inagaki, Manabu; Sakai, Takeshi; Sato, Isamu; Hayakawa, Yasushi; Nogami, Kyoko; Tanaka, Toshinari; Hayakawa, Ken; Nakao, Keisuke

2008-01-01

The parametric X-ray radiation (PXR) generator system at Laboratory for Electron Beam Research and Application (LEBRA) in Nihon University is a monochromatic and coherent X-ray source with horizontal wavelength dispersion. The energy definition of the X-rays, which depends on the horizontal size of the incident electron beam on the generator target crystal, has been investigated experimentally by measuring the X-ray absorption near edge structure (XANES) spectra on Cu and CuO associated with conventional X-ray absorption imaging technique. The result demonstrated the controllability of the spectrum resolution of XANES by adjusting of the horizontal electron beam size on the target crystal. The XANES spectra were obtained with energy resolution of several eV at the narrowest case, which is in qualitative agreement with the energy definition of the PXR X-rays evaluated from geometrical consideration. The result also suggested that the wavelength dispersive X-ray absorption fine structure measurement associated with imaging technique is one of the promising applications of PXR. (author)

A study on the measurement of effective energy of leakage X-rays

International Nuclear Information System (INIS)

Fijimoto, Nobuhisa; Oogama, Noboru; Nishitani, Motohiro; Yamada, Katsuhiko

1997-01-01

It is important to correct for the energy response of the X-ray detector in measuring X-ray leakage from the protective barrier of the examination room. However, measurement of effective energy of leakage X-rays is very difficult in the clinical setting. In this paper, we discuss a method for estimating the effective energy of both primary and scattered X-rays. This method is based on the measurement of leakage X-ray spectra using a semiconductor-fitted X-ray detector and analyzing the relationship between X-ray tube voltage and effective energy. In this study. we found that the effective energy of leakage X-rays was not dependent on the thickness of shielding materials like concrete and lead. With the concrete barrier, it was possible to express the relation-ship between X-ray tube voltage and the effective energy of leakage X-rays with a simple approximate equation. With the lead-lined barrier, the absorption of the K-edge of lead needs to be considered in estimating the effective energy of leakage X-rays at relatively high tube voltages. (author)

Changes of soft X-ray emission spectra of oxygen and copper in high Tc superconductors

International Nuclear Information System (INIS)

Fukushima, Sei; Gohshi, Yohichi; Kohiki, Shigemi; Saitoh, Naoki

1989-01-01

X-ray induced soft X-ray emission spectroscopy is one of the bulk analysis methods used to characterize high-Tc superconductor. In this report, some observations on the changes in O Kα and Cu L spectra of thin layer LnBa 2 Cu 3 O 7-δ (Ln=Er,Gd) samples are presented. From the measurement of O Kα, no discernible difference was found between those of Gd compounds which were composed single phase or not. It may be said that the electronic structure of p state localized on the O is not sensitive to the change of Tc or zero-resistance temperature. From the measurement of Cu L spectra, it was found that Cu Lα of only Gd containing compounds has a low energy shoulder

OSO 8 X-ray spectra of clusters of galaxies. I - Observations of twenty clusters: Physical correlations

Science.gov (United States)

Mushotzky, R. F.; Serlemitsos, P. J.; Boldt, E. A.; Holt, S. S.; Smith, B. W.

1978-01-01

OSO 8 X-ray spectra from 2 to 20 keV have been analyzed for 26 clusters of galaxies. For 20 clusters temperatures, emission integrals, iron abundances, and low-energy absorption measurements are presented. The data give, in general, better fits to thermal bremsstrahlung than to power-law models. Eight clusters have positive iron emission-line detections at the 90% confidence level, and all 20 cluster spectra are consistent with Fe/H = 0.000014 by number with the possible exception of Virgo. Thus it is confirmed that X-ray emission in this energy band is predominantly thermal radiation from hot intracluster gas rather than inverse Compton radiation. Physical correlations between X-ray spectral parameters and other cluster properties are examined. It is found that (1) the X-ray temperature is approximately proportional to the square of the velocity dispersion of the galaxies; (2) the emission integral is a strong function of the X-ray temperature; (3) the X-ray temperature and emission integral are better correlated with cluster central-galaxy density than with richness; and (4) the fraction of galaxies which are spirals is correlated with the observed ram pressure in the cluster core.

Galactic and extragalactic hydrogen in the X-ray spectra of Gamma Ray Bursts

Science.gov (United States)

Rácz, I. I.; Bagoly, Z.; Tóth, L. V.; Balázs, L. G.; Horváth, I.; Pintér, S.

2017-07-01

Two types of emission can be observed from gamma-ray bursts (GRBs): the prompt emission from the central engine which can be observed in gamma or X-ray (as a low energy tail) and the afterglow from the environment in X-ray and at shorter frequencies. We examined the Swift XRT spectra with the XSPEC software. The correct estimation of the galactic interstellar medium is very important because we observe the host emission together with the galactic hydrogen absorption. We found that the estimated intrinsic hydrogen column density and the X-ray flux depend heavily on the redshift and the galactic foreground hydrogen. We also found that the initial parameters of the iteration and the cosmological parameters did not have much effect on the fitting result.

Experimental device for the X-ray energetic distribution measurement in a tokamak plasma

International Nuclear Information System (INIS)

Perez-Navarro, A.

1977-01-01

An experimental system to measure the X-ray spectrum in a tokamak plasma is described, emphasizing its characteristics: resolution, dead time and the pulse pile-up distortion effects on the X-ray spectra. (author) [es

Lifetime-vibrational interference effects in resonantly excited x-ray emission spectra of CO

Energy Technology Data Exchange (ETDEWEB)

Skytt, P.; Glans, P.; Gunnelin, K. [Uppsala Univ. (Sweden)] [and others

1997-04-01

The parity selection rule for resonant X-ray emission as demonstrated for O{sub 2} and N{sub 2} can be seen as an effect of interference between coherently excited degenerate localized core states. One system where the core state degeneracy is not exact but somewhat lifted was previously studied at ALS, namely the resonant X-ray emission of amino-substituted benzene (aniline). It was shown that the X-ray fluorescence spectrum resulting from excitation of the C1s at the site of the {open_quotes}aminocarbon{close_quotes} could be described in a picture separating the excitation and the emission processes, whereas the spectrum corresponding to the quasi-degenerate carbons could not. Thus, in this case it was necessary to take interference effects between the quasi-degenerate intermediate core excited states into account in order to obtain agreement between calculations and experiment. The different vibrational levels of core excited states in molecules have energy splittings which are of the same order of magnitude as the natural lifetime broadening of core excitations in the soft X-ray range. Therefore, lifetime-vibrational interference effects are likely to appear and influence the band shapes in resonant X-ray emission spectra. Lifetime-vibrational interference has been studied in non-resonant X-ray emission, and in Auger spectra. In this report the authors discuss results of selectively excited soft X-ray fluorescence spectra of molecules, where they focus on lifetime-interference effects appearing in the band shapes.

Electron-electron correlation, resonant photoemission and X-ray emission spectra

International Nuclear Information System (INIS)

Parlebas, J.C.; Kotani, Akio; Tanaka, Satoshi.

1991-01-01

In this short review paper we essentially focus on the high energy spectroscopies which involve second order quantum processes, i.e., resonance photoemission, Auger and X-ray emission spectroscopies, denoted respectively by RXPS, AES and XES. First, we summarize the main 3p-RXPS and AES results obtained in Cu and Ni metals; especially we recall that the satellite near the 3p-threshold in the spectra, which arises from a d-hole pair bound state, needs a careful treatment of the electron-electron correlation. Then we analyze the RXPS spectra in a few Ce compounds (CeO 2 , Ce 2 O 3 and CeF 3 ) involving 3d or 4d core levels and we interpret the spectra consistently with the other spectroscopies, such as core XPS and XAS which are first order quantum processes. Finally within the same one-impurity model and basically with the same sets of parameters, we review a theory for the Ce 5p→3d XES, as well as for the corresponding RXES, where (1) the incident X-ray is tuned to resonate with the 3d→4f transition and (2) the X-ray emission due to the 5p→3d transition is actually observed. The paper ends with a general discussion. (author) 77 refs

A model independent method to deconvolve hard X-ray spectra

International Nuclear Information System (INIS)

Polcaro, V.F.; Bazzano, A.; Ubertini, P.; La Padula, C.

1984-01-01

A general purpose method to deconvolve the energy spectra detected by means of the use of a hard X-ray telescope is described. The procedure does not assume any form of input spectrum and the observed energy loss spectrum is directly deconvolved into the incident photon spectrum, the form of which can be determined independently of physical interpretation of the data. Deconvolution of the hard X-ray spectrum of Her X-1, detected during the HXR 81M experiment, by the method independent method is presented. (orig.)

Vibrational spectra, powder X-ray diffractions and physical properties of cyanide complexes with 1-ethylimidazole

Science.gov (United States)

Kürkçüoğlu, Güneş Süheyla; Kiraz, Fulya Çetinkaya; Sayın, Elvan

2015-10-01

The heteronuclear tetracyanonickelate(II) complexes of the type [M(etim)Ni(CN)4]n (hereafter, abbreviated as M-Ni-etim, M = Mn(II), Fe(II) or Co(II); etim = 1-ethylimidazole, C5H8N2) were prepared in powder form and characterized by FT-IR and Raman spectroscopy, powder X-ray diffraction (PXRD), thermal (TG; DTG and DTA), and elemental analysis techniques. The structures of these complexes were elucidated using vibrational spectra and powder X-ray diffraction patterns with the peak assignment to provide a better understanding of the structures. It is shown that the spectra are consistent with a proposed crystal structure for these compounds derived from powder X-ray diffraction measurements. Vibrational spectra of the complexes were presented and discussed with respect to the internal modes of both the etim and the cyanide ligands. The C, H and N analyses were carried out for all the complexes. Thermal behaviors of these complexes were followed using TG, DTG and DTA curves in the temperature range 30-700 °C in the static air atmosphere. The FT-IR, Raman spectra, thermal and powder X-ray analyses revealed no significant differences between the single crystal and powder forms. Additionally, electrical and magnetic properties of the complexes were investigated. The FT-IR and Raman spectroscopy, PXRD, thermal and elemental analyses results propose that these complexes are similar in structure to the Hofmann-type complexes.

Sub-keV, subnanosecond measurements of x-ray spectra from laser-produced plasmas

International Nuclear Information System (INIS)

Kornblum, H.N.; Koppel, L.N.; Slivinsky, V.W.; Glaros, S.S.; Ahlstrom, H.G.; Larsen, J.T.

1977-01-01

As part of the effort to extend our x-ray diagnostic capabilities, we have made x-ray spectral measurements of laser-produced plasmas for photon energies down to 100 eV with a time response of 0.5 nsec. Fast, windowless x-ray diodes were used in conjunction with critical angle reflecting mirrors and thin filters for energy definition for two channels, 300 to 600 eV and 800 to 1300 eV. A third channel, using only an x-ray diode and filter, provided spectral information in the 100 to 300 eV region. Results from exploding pusher targets will be presented and compared with those of other diagnostic techniques and Lasnex calculations. Future expansion and modifications of the present system will be discussed

Atomic Physics Measurements in Support of X-ray Astronomy

Science.gov (United States)

Beiersdorfer, Peter; Brown, G. V.; Kelley, R. E.; Kilbourne, C. A.; Leutenegger, M.; Porter, F. S.; Obst, M.; Lepson, J. K.; Desai, P.; Gu, M. F.

2010-10-01

X-ray astronomy has been a voracious consumer of atomic data, especially after the launch of the Chandra and XMM-Newton X-ray Observatories, which have produced very high-resolution grating spectra of point sources. One of the important issues has been to understand the physics underlying the Fe L-shell spectra, and the Fe XVII spectrum in particular. A lot of progress has been made, including measurements of the electron-impact and resonance excitation cross sections, which now provides a rather clear picture of the production mechanism of the Fe XVII spectrum. Recent measurements of the radiative rates provide additional information on the deexcitation channels, while investigations of dielectronic satellite transitions provide a measure of the electron temperature. Many questions, however, still remain. Work at LLNL was performed under the auspices of DOE under contract DE-AC53-07NA27344 and supported by NASA's APRA program under contracts NNH07AF81I and NNG06WF08I. Part of this work was supported by Chandra Cycle 10 Award AR9-0002X.

Steep Hard-X-ray Spectra Indicate Extremely High Accretion Rates in Weak Emission-Line Quasars

Science.gov (United States)

Marlar, Andrea; Shemmer, Ohad; Anderson, Scott F.; Brandt, W. Niel; Diamond-Stanic, Aleksandar M.; Fan, Xiaohui; Luo, Bin; Plotkin, Richard; Richards, Gordon T.; Schneider, Donald P.; Wu, Jianfeng

2018-06-01

We present XMM-Newton imaging spectroscopy of ten weak emission-line quasars (WLQs) at 0.928 ≤ z ≤ 3.767, six of which are radio quiet and four which are radio intermediate. The new X-ray data enabled us to measure the hard-X-ray power-law photon index (Γ) in each source with relatively high accuracy. These measurements allowed us to confirm previous reports that WLQs have steeper X-ray spectra, therefore indicating higher accretion rates with respect to "typical" quasars. A comparison between the Γ values of our radio-quiet WLQs and those of a carefully-selected, uniform sample of 84 quasars shows that the first are significantly higher, at the ≥ 3σ level. Collectively, the four radio-intermediate WLQs have lower Γ values with respect to the six radio-quiet WLQs, as may be expected if the spectra of the first group are contaminated by X-ray emission from a jet. These results suggest that, in the absence of significant jet emission along our line of sight, WLQs constitute the extreme high end of the accretion rate distribution in quasars. We detect soft excess emission in our lowest-redshift radio-quiet WLQ, in agreement with previous findings suggesting that the prominence of this feature is associated with a high accretion rate. We have not detected signatures of Compton reflection, Fe Kα lines, or strong variability between two X-ray epochs in any of our WLQs.

Spatially resolved density and ionization measurements of shocked foams using x-ray fluorescence

Energy Technology Data Exchange (ETDEWEB)

MacDonald, M. J.; Keiter, P. A.; Montgomery, D. S.; Scott, H. A.; Biener, M. M.; Fein, J. R.; Fournier, K. B.; Gamboa, E. J.; Kemp, G. E.; Klein, S. R.; Kuranz, C. C.; LeFevre, H. J.; Manuel, M. J. -E.; Wan, W. C.; Drake, R. P.

2016-09-28

We present experiments at the Trident laser facility demonstrating the use of x-ray fluorescence (XRF) to simultaneously measure density, ionization state populations, and electron temperature in shocked foams. An imaging x-ray spectrometer obtained spatially resolved measurements of Ti K-α emission. Density profiles were measured from K-α intensity. Ti ionization state distributions and electron temperatures were inferred by fitting K-α spectra to spectra from CRETIN simulations. This work shows that XRF provides a powerful tool to complement other diagnostics to make equation of state measurements of shocked materials containing a suitable tracer element.

Reconstruction of energetic electron spectra in the upper atmosphere: balloon observations of auroral X-rays coordinated with measurements from the Eiscat radar

International Nuclear Information System (INIS)

Olafsson, K.J.

1990-01-01

Energetic electron precipitation in the auroral zone has been studied using coordinated auroral X-ray measurements from balloons, altitude profiles of the ionospheric electron density measured by the EISCAT radar above the balloons, and cosmic noise absorption data from the Scandinavian riometer network. The data were obtained during the coordinated EISCAT and balloon observation campaign in August 1984. A method by which an estimate of the energy spectrum of precipitating energetic electrons can be obtained from balloon measurements of bremsstrahlung X-rays is described. The energy spectral variation of both the X-ray fluxes and the primary precipitating electrons were examined for two precipitation events in the morning sector. As far as reasonably can be concluded from observations of magnetic activity in the auroral zone, and from the temporal development of the energy spectra, the two precipitation events can be interpreted in the frame of present models of energetic electron precipitation on the morning side of the auroral zone. 96 refs

Krypton K-shell X-ray spectra recorded by the HENEX spectrometer

Energy Technology Data Exchange (ETDEWEB)

Seely, J.F. [Naval Research Laboratory, Space Science Division, Washington DC 20375 (United States)]. E-mail: john.seely@nrl.navy.mil; Back, C.A. [Lawrence Livermore National Laboratory, Livermore CA 94550 (United States); Constantin, C. [Lawrence Livermore National Laboratory, Livermore CA 94550 (United States); Lee, R.W. [Lawrence Livermore National Laboratory, Livermore CA 94550 (United States); Chung, H.-K. [Lawrence Livermore National Laboratory, Livermore CA 94550 (United States); Hudson, L.T. [National Institute of Standards and Technology, Gaithersburg MD 20899 (United States); Szabo, C.I. [National Institute of Standards and Technology, Gaithersburg MD 20899 (United States); Henins, A. [National Institute of Standards and Technology, Gaithersburg MD 20899 (United States); Holland, G.E. [SFA Inc., 9315 Largo Drive West Suite 200, Largo MD 20774 (United States); Atkin, R. [Tiger Innovations, L.L.C., 3610 Vacation Lane, Arlington VA 22207 (United States); Marlin, L. [Naval Research Laboratory, Space Science Division, Washington DC 20375 (United States)

2006-05-15

High-resolution X-ray spectra were recorded by the High-Energy Electronic X-ray (HENEX) spectrometer from a variety of targets irradiated by the Omega laser at the Laboratory for Laser Energetics. The HENEX spectrometer utilizes four reflection crystals covering the 1-20keV energy range and one quartz(10-11) transmission crystal (Laue geometry) covering the 11-40keV range. The time-integrated spectral images were recorded on five CMOS X-ray detectors. In the spectra recorded from krypton-filled gasbag and hohlraum targets, the helium-like K-shell transitions n=1-2, 1-3, and 1-4 appeared in the 13-17keV energy range. A number of additional spectral features were observed at energies lower than the helium-like n=1-3 and n=1-4 transitions. Based on computational simulations of the spectra using the FLYCHK/FLYSPEC codes, which included opacity effects, these additional features are identified to be inner-shell transitions from the Li-like through N-like krypton charge states. The comparisons of the calculated and observed spectra indicate that these transitions are characteristic of the plasma conditions immediately after the laser pulse when the krypton density is 2x10{sup 18}cm{sup -3} and the electron temperature is in the range 2.8-3.2keV. These spectral features represent a new diagnostic for the charge state distribution, the density and electron temperature, and the plasma opacity. Laboratory experiments indicate that it is feasible to record K-shell spectra from gold and higher Z targets in the >60keV energy range using a Ge(220) transmission crystal.

Measuring Quasar Spin via X-ray Continuum Fitting

Science.gov (United States)

Jenkins, Matthew; Pooley, David; Rappaport, Saul; Steiner, Jack

2018-01-01

We have identified several quasars whose X-ray spectra appear very soft. When fit with power-law models, the best-fit indices are greater than 3. This is very suggestive of thermal disk emission, indicating that the X-ray spectrum is dominated by the disk component. Galactic black hole binaries in such states have been successfully fit with disk-blackbody models to constrain the inner radius, which also constrains the spin of the black hole. We have fit those models to XMM-Newton spectra of several of our identified soft X-ray quasars to place constraints on the spins of the supermassive black holes.

Estimation of identification limit for a small-type OSL dosimeter on the medical images by measurement of X-ray spectra

OpenAIRE

Takegami, Kazuki ; Hayashi, Hiroaki; Okino, Hiroki; Kimoto, Natsumi ; Maehata, Itsumi ; Kanazawa, Yuki ; Okazaki, Tohru ; Hashizume, Takuya ; Kobayashi, Ikuo 

2016-01-01

Our aim in this study is to derive an identification limit on a dosimeter for not disturbing a medical image when patients wear a small-type optically stimulated luminescence (OSL) dosimeter on their bodies during X-ray diagnostic imaging. For evaluation of the detection limit based on an analysis of X-ray spectra, we propose a new quantitative identification method. We performed experiments for which we used diagnostic X-ray equipment, a soft-tissue-equivalent phantom (1–20 cm), and a CdTe X...

Extracting ion emission lines from femtosecond-laser plasma x-ray spectra heavily contaminated by spikes

International Nuclear Information System (INIS)

Gasilov, S. V.; Faenov, A. Ya.; Pikuz, T. A.; Villoresi, P.; Poletto, L.; Stagira, S.; Calegari, F.; Vozzi, C.; Nisoli, M.

2007-01-01

Nowadays charged-coupled device (CCD) detectors are widely used for the registration of multicharged ions x-ray spectra. These spectra are generated in a plasma during interaction of ultrashort, ultraintense laser pulses with solid targets. Strong parasitic radiation from the plasma affects CCD detectors and contaminates resulting spectra, so that spectral features can be completely covered by noise even during measurements with a very short accumulation time. In this work we propose a ''mean to median'' (M2M) algorithm for noise suppression in femtosecond laser plasma x-ray spectra. Series of spectra is necessary for the identification of corrupted data points by the developed method. The algorithm was tested with model spectra which reflect main features of experimental data. In practice we used it for extracting information about spectral lines of Ne-like Fe ions and He-like Al ions which allowed us to calculate plasma parameters. It is demonstrated that M2M method is able to clean spectra with more than 10% of corrupted pixels. Fluctuations in intensity of spectral lines induced by laser instability do not affect validity of the proposed method

Dynamical and Radiative Properties of X-Ray Pulsar Accretion Columns: Phase-averaged Spectra

Energy Technology Data Exchange (ETDEWEB)

West, Brent F. [Department of Electrical and Computer Engineering, United States Naval Academy, Annapolis, MD (United States); Wolfram, Kenneth D. [Naval Research Laboratory (retired), Washington, DC (United States); Becker, Peter A., E-mail: bwest@usna.edu, E-mail: kswolfram@gmail.com, E-mail: pbecker@gmu.edu [Department of Physics and Astronomy, George Mason University, Fairfax, VA (United States)

2017-02-01

The availability of the unprecedented spectral resolution provided by modern X-ray observatories is opening up new areas for study involving the coupled formation of the continuum emission and the cyclotron absorption features in accretion-powered X-ray pulsar spectra. Previous research focusing on the dynamics and the associated formation of the observed spectra has largely been confined to the single-fluid model, in which the super-Eddington luminosity inside the column decelerates the flow to rest at the stellar surface, while the dynamical effect of gas pressure is ignored. In a companion paper, we have presented a detailed analysis of the hydrodynamic and thermodynamic structure of the accretion column obtained using a new self-consistent model that includes the effects of both gas and radiation pressures. In this paper, we explore the formation of the associated X-ray spectra using a rigorous photon transport equation that is consistent with the hydrodynamic and thermodynamic structure of the column. We use the new model to obtain phase-averaged spectra and partially occulted spectra for Her X-1, Cen X-3, and LMC X-4. We also use the new model to constrain the emission geometry, and compare the resulting parameters with those obtained using previously published models. Our model sheds new light on the structure of the column, the relationship between the ionized gas and the photons, the competition between diffusive and advective transport, and the magnitude of the energy-averaged cyclotron scattering cross-section.

Dynamics of hot spots in the DPF-78 plasma focus from x-ray spectra and REB emission

International Nuclear Information System (INIS)

Schmidt, H.; Wang, X.X.

1995-01-01

The X-ray emission from hot spots in the plasma focus DPF-78 was investigated with the help of two X-ray quartz crystal spectrometers of the Johann type and a 4 fold magnifying X-ray pinhole camera. In the experiments the working gas was chosen to be 300 Pa deuterium with 20 Pa argon admixture. X-ray spectra in the wavelength range from 3.55 angstrom to 4.0 angstrom, including H-like and He-like Argon lines, were recorded on Kodak DEF-2 film. From the spatially resolved spectra recorded side-on, a relative spectral shift between different hot spots of the same shot was often observed. The shift could be attributed to the Doppler shift. From spectral characteristics such as intensities and FWHM of Ar resonant and intercombination lines electron densities of up to 3 x 10 27 m -3 were determined. Radial dimensions of the hot spots ranging from about 140 microm to 300 microm were found from pinhole pictures applying the penumbra method. Usually two pulses of relativistic electron beams were observed using Cherenkov detectors in a magnetic spectrometer. The energy of the first pulse, which was emitted at the time of maximum compression, was higher than that of the second pulse. The measured FWHM of the REB pulses ranges from 3 ns to about 10 ns. The characteristics of the time-integrated X-ray spectra and the time resolved REB spectra and their dependence on the composition of the filling gas are discussed

A study on the measurement of effective energy of scattering X-rays

International Nuclear Information System (INIS)

Oogama, Noboru; Fujimoto, Nobuhisa; Nishitani, Motohiro; Yamada, Katsuhiko

1995-01-01

Only a few studies have been reported on the measurement and evaluation of the effective energy of scattering X-rays using an ionization chamber. The reason for this is due to the difficulty in accurately measuring attenuation curve in scattering X-rays lacking any directional properties. We could come up with a new method for calculating the effective energy of scattering X-rays by utilizing their spectra data. First, for analysing the accuracy of our calculation method with using primary X-rays, a comparison was made of calculated values of the effective energy obtained by our calculation method with the measurement values obtained using an ionization chamber. The results gave the calculated values agreeing with the measurement values within a maximum error of 2%, and this method was very helpful in measuring the effective energy of the scattering X-rays. Consequently, this method was capable of measuring the effective energy of scattering X-rays in the following parameters: X-ray tube voltage, scattering angle and size of scatterer. In conclusion, it is considered that our method could solve the present difficulty regarding the measurement of effective energy of the scattering X-rays, and provided a useful procedure concerning the study of radiation protection. (author)

Absorption spectra response of XRQA radiochromic film to x-ray radiation

International Nuclear Information System (INIS)

Alnawaf, Hani; Cheung, Tsang; Butson, Martin J.; Yu, Peter K.N.

2010-01-01

Gafchromic XRQA, radiochromic film is a high sensitivity auto developing x-ray analysis films designed and available for kilovoltage x-ray, dose and QA assessment applications. The film is designed for reflective analysis with a yellow transparent top filter and white opaque backing materials. This allows the film to be visually inspected for colour changes with a higher level of contrast than clear coated radiochromic films such as Gafchromic EBT version 1. The spectral absorption properties in the visible wavelengths have been investigated and results show two main peaks in absorption located at 636 nm and 585 nm. These peaks are located in the same position as EBT Gafchromic film highlighting a similar chemical monomer/polymer for radiation sensitivity. A much higher sensitivity however is found at kilovoltage energies with an average 1.55 OD units per 20 cGy irradiation variation measured at 636 nm using 150 kVp x-rays. This is compared to approximately 0.12 OD units per 20 cGy measured at 636 nm for EBT film at 6 MV x-ray energy. That is, the XRQA film is more than 10 times more sensitive than EBT1 film. The visual colour change is enhanced by the yellow polyester coating. However this does not affect the absorption spectra properties in the red region of analysis which is the main area for use using desktop scanners in reflection mode.

First Principles Calculations for X-ray Resonant Spectra and Elastic Properties

International Nuclear Information System (INIS)

Yongbin Lee

2006-01-01

In this thesis, we discuss applications of first principles methods to x-ray resonant spectra and elastic properties calculation. We start with brief reviews about theoretical background of first principles methods, such as density functional theory, local density approximation (LDA), LDA+U, and the linear augmented plane wave (LAPW) method to solve Kohn-Sham equations. After that we discuss x-ray resonant scattering (XRMS), x-ray magnetic circular dichroism (XMCD) and the branching problem in the heavy rare earths Ledges. In the last chapter we discuss the elastic properties of the second hardest material AlMgB 14

New Observations of Soft X-ray (0.5-5 keV) Solar Spectra

Science.gov (United States)

Caspi, A.; Woods, T. N.; Mason, J. P.; Jones, A. R.; Warren, H. P.

2013-12-01

The solar corona is the brightest source of X-rays in the solar system, and the X-ray emission is highly variable on many time scales. However, the actual solar soft X-ray (SXR) (0.5-5 keV) spectrum is not well known, particularly during solar quiet periods, as, with few exceptions, this energy range has not been systematically studied in many years. Previous observations include high-resolution but very narrow-band spectra from crystal spectrometers (e.g., Yohkoh/BCS), or integrated broadband irradiances from photometers (e.g., GOES/XRS, TIMED/XPS, etc.) that lack detailed spectral information. In recent years, broadband measurements with moderate energy resolution (~0.5-0.7 keV FWHM) were made by SphinX on CORONAS-Photon and SAX on MESSENGER, although they did not extend to energies below ~1 keV. We present observations of solar SXR emission obtained using new instrumentation flown on recent SDO/EVE calibration rocket underflights. The photon-counting spectrometer, a commercial Amptek X123 with a silicon drift detector and an 8 μm Be window, measures the solar disk-integrated SXR emission from ~0.5 to >10 keV with ~0.15 keV FWHM resolution and 1 s cadence. A novel imager, a pinhole X-ray camera using a cooled frame-transfer CCD (15 μm pixel pitch), Ti/Al/C filter, and 5000 line/mm Au transmission grating, images the full Sun in multiple spectral orders from ~0.1 to ~5 nm with ~10 arcsec/pixel and ~0.01 nm/pixel spatial and spectral detector scales, respectively, and 10 s cadence. These instruments are prototypes for future CubeSat missions currently being developed. We present new results of solar observations on 04 October 2013 (NASA sounding rocket 36.290). We compare with previous results from 23 June 2012 (NASA sounding rocket 36.286), during which solar activity was low and no signal was observed above ~4 keV. We compare our spectral and imaging measurements with spectra and broadband irradiances from other instruments, including SDO/EVE, GOES/XRS, TIMED

Charge exchange recombination in X-ray spectra of He-like argon measured at the tokamak TEXTOR

Energy Technology Data Exchange (ETDEWEB)

Schlummer, Tobias

2014-06-16

Charge exchange recombination between ions and atomic hydrogen is an important atomic process in magnetically confined fusion plasmas. Besides radiative cooling of the plasma edge, charge exchange causes modifications of the ionization balance and the population densities of excited ion states. The central goal of this work is to investigate the influence of charge exchange on X-ray spectra measured at the tokamak TEXTOR. A new 2D X-ray spectrometer developed for future use at the stellarator W7-X was recently installed at TEXTOR. The spectrometer is optimized for measuring the K{sub α}-spectrum of He-like argon (1s2l - 1s{sup 2}) at wavelengths close to 4 Aa. K{sub α}-spectroscopy on He-like impurity ions is an established diagnostic for electron and ion temperature measurements in fusion plasmas. Still, up to now the observed intensity ratios of the K{sub α}-lines and their associated satellites are not fully understood. They show significant deviations from the predictions made by basic corona models. In the past charge exchange with the neutral particle background and radial impurity transport have been discussed as likely explanations. Yet a detailed description of the experimental spectra still has not been achieved. To reconstruct the 2D K{sub α}-spectra measured at TEXTOR the radial argon ion distribution is modeled using an impurity transport code. The model accounts for charge exchange and transport on basis of given radial profiles of the neutral particle density n{sub 0}(r) and the diffusion coefficient D {sub perpendicular} {sub to} (r). The theoretical spectrum is then constructed based on the processes relevant for line emission. Within an iterative procedure n{sub 0}(r) and D {sub perpendicular} {sub to} (r) are varied until consistency between the theoretical and the experimental spectra is achieved. It is shown that the 2D K{sub α}-spectra allow a clear distinction of charge exchange and transport effects, ensuring unique solutions for n

Analysis of neon soft x-ray spectra from short-pulse laser-produced plasmas

International Nuclear Information System (INIS)

Abare, A.C.; Keane, C.J.; Crane, J.K.; DaSilva, L.B.; Lee, R.W.; Perry, M.D.; Falcone, R.W.

1993-04-01

We report preliminary results from the analysis of streaked soft x-ray neon spectra a gas jet target. In obtained from the interaction of a picosecond Nd:glass laser with these experiments streaked spectra show prompt harmonic emission followed by longer time duration soft x-ray line emission. The majority of the line emission observed was found to originate from Li- and Be-like Ne and the major transitions in the observed spectra have been identified. Li-like emission lines were observed to decay faster in time than Be-like transitions, suggesting that recombination is taking place. Line ratios of n=4-2 and n=3-2 transitions supported the view that these lines were optically thin and thick, respectively. The time history of Li-like Ne 2p-4d and 2p-3d lines is in good agreement with a simple adiabatic expansion model coupled to a time dependent collisional-radiative code. Further x-ray spectroscopic analysis is underway which is aimed at diagnosing plasma conditions and assessing the potential of this recombining neon plasma as a quasi-steady-state recombination x-ray laser medium

Quantifying the effect of anode surface roughness on diagnostic x-ray spectra using Monte Carlo simulation

Energy Technology Data Exchange (ETDEWEB)

Mehranian, A.; Ay, M. R.; Alam, N. Riyahi; Zaidi, H. [Department of Medical Physics and Biomedical Engineering, Tehran University of Medical Sciences, P.O. Box 14155-6447, Tehran (Iran, Islamic Republic of) and Research Center for Science and Technology in Medicine, Tehran University of Medical Sciences, P.O. Box 14185-615, Tehran (Iran, Islamic Republic of); Department of Medical Physics and Biomedical Engineering, Tehran University of Medical Sciences, P.O. Box 14155-6447, Tehran (Iran, Islamic Republic of); Research Center for Science and Technology in Medicine, Tehran University of Medical Sciences, P.O. Box 14185-615, Tehran (Iran, Islamic Republic of) and Research Institute for Nuclear Medicine, Tehran University of Medical Sciences, P.O. Box 14155-6447, Tehran (Iran, Islamic Republic of); Department of Medical Physics and Biomedical Engineering, Tehran University of Medical Sciences, P.O. Box 14155-6447, Tehran (Iran, Islamic Republic of); Division of Nuclear Medicine, Geneva University Hospital, CH-1211 Geneva (Switzerland) and Geneva Neuroscience Center, Geneva University, CH-1205 Geneva (Switzerland)

2010-02-15

Purpose: The accurate prediction of x-ray spectra under typical conditions encountered in clinical x-ray examination procedures and the assessment of factors influencing them has been a long-standing goal of the diagnostic radiology and medical physics communities. In this work, the influence of anode surface roughness on diagnostic x-ray spectra is evaluated using MCNP4C-based Monte Carlo simulations. Methods: An image-based modeling method was used to create realistic models from surface-cracked anodes. An in-house computer program was written to model the geometric pattern of cracks and irregularities from digital images of focal track surface in order to define the modeled anodes into MCNP input file. To consider average roughness and mean crack depth into the models, the surface of anodes was characterized by scanning electron microscopy and surface profilometry. It was found that the average roughness (R{sub a}) in the most aged tube studied is about 50 {mu}m. The correctness of MCNP4C in simulating diagnostic x-ray spectra was thoroughly verified by calling its Gaussian energy broadening card and comparing the simulated spectra with experimentally measured ones. The assessment of anode roughness involved the comparison of simulated spectra in deteriorated anodes with those simulated in perfectly plain anodes considered as reference. From these comparisons, the variations in output intensity, half value layer (HVL), heel effect, and patient dose were studied. Results: An intensity loss of 4.5% and 16.8% was predicted for anodes aged by 5 and 50 {mu}m deep cracks (50 kVp, 6 deg. target angle, and 2.5 mm Al total filtration). The variations in HVL were not significant as the spectra were not hardened by more than 2.5%; however, the trend for this variation was to increase with roughness. By deploying several point detector tallies along the anode-cathode direction and averaging exposure over them, it was found that for a 6 deg. anode, roughened by 50 {mu}m deep

Probing symmetry and symmetry breaking in resonant soft-x-ray fluorescence spectra of molecules

Energy Technology Data Exchange (ETDEWEB)

Glans, P.; Gunnelin, K.; Guo, J. [Uppsala Univ. (Sweden)] [and others

1997-04-01

Conventional non-resonant soft X-ray emission brings about information about electronic structure through its symmetry and polarization selectivity, the character of which is governed by simple dipole rules. For centro-symmetric molecules with the emitting atom at the inversion center these rules lead to selective emission through the required parity change. For the more common classes of molecules which have lower symmetry or for systems with degenerate core orbitals (delocalized over identical sites), it is merely the local symmetry selectivity that provides a probe of the local atomic orbital contribution to the molecular orbital. For instance, in X-ray spectra of first row species the intensities essentially map the p-density at each particular atomic site, and, in a molecular orbital picture, the contribution of the local p-type atomic orbitals in the LCAO description of the molecular orbitals. The situation is different for resonant X-ray fluorescence spectra. Here strict parity and symmetry selectivity gives rise to a strong frequency dependence for all molecules with an element of symmetry. In addition to symmetry selectivity the strong frequency dependence of resonant X-ray emission is caused by the interplay between the shape of a narrow X-ray excitation energy function and the lifetime and vibrational broadenings of the resonantly excited core states. This interplay leads to various observable effects, such as linear dispersion, resonance narrowing and emission line (Stokes) doubling. Also from the point of view of polarization selectivity, the resonantly excited X-ray spectra are much more informative than the corresponding non-resonant spectra. Examples are presented for nitrogen, oxygen, and carbon dioxide molecules.

Kα X-ray satellite spectra of Ti, V, Cr and Mn induced by photons

Indian Academy of Sciences (India)

K X-ray emission spectra of Ti, V, Cr and Mn generated by photon excitation have been studied with a crystal spectrometer. The measured energy shifts of K satellite relative to the diagram line are compared with values obtained by electron excitation and with different theoretical estimates. The present experimental ...

Correction of diagnostic x-ray spectra measured with CdTe and CdZnTe detectors

Energy Technology Data Exchange (ETDEWEB)

Matsumoto, M [Osaka Univ., Suita (Japan). Medical School; Kanamori, H; Toragaito, T; Taniguchi, A

1996-07-01

We modified the formula of stripping procedure presented by E. Di. Castor et al. We added the Compton scattering and separated K{sub {alpha}} radiation of Cd and Te (23 and 27keV, respectively). Using the new stripping procedure diagnostic x-ray spectra (object 4mm-Al) of tube voltage 50kV to 100kV for CdTe and CdZnTe detectors are corrected with comparison of those spectra for the Ge detector. The corrected spectra for CdTe and CdZnTe detectors coincide with those for Ge detector at lower tube voltage than 70kV. But the corrected spectra at higher tube voltage than 70kV do not coincide with those for Ge detector. The reason is incomplete correction for full energy peak efficiencies of real CdTe and CdZnTe detectors. (J.P.N.)

The high energy X-ray spectra of supernova remnants

Science.gov (United States)

Pravdo, S. H.; Nugent, J. J.

The results of fitting an ionization-nonequilibrium (INE) model to the high-energy (above 5-keV) X-ray spectra of the young supernova remnants Cas A and Tycho are presented. As an additional constraint, the models must simultaneously fit lower-energy, higher-resolution data. For Cas A, a single INE component cannot adequately reproduce the features for the entire X-ray spectrum because the ionization structure of iron ions responsible for the K emission is inconsistent with that of the ions responsible for the lower-energy lines, and the flux of the highest-energy X-rays is underestimated. The iron K line and the high-energy continuum could arise from the same INE component, but the identification of this component with either the blast wave or the ejecta in the standard model is difficult. In Tycho, the high-energy data rule out a class of models for the lower-energy data which have too large a continuum contribution.

Measurement of position dependence of spectral distribution in primary X-ray beam of CT system using compton spectroscopy

International Nuclear Information System (INIS)

Matsumoto, Masao; Maeda, Koji; Maeda, Koji

2005-01-01

Our purpose is to acquire the diagnostic x-ray spectra of the CT system easily under clinical conditions by Compton scatter spectroscopy using a high resolution Schottky CdTe detector recently developed and to estimate the quality and quantity of these spectra compared the relative exposure measured using an ionization chamber with curves measured by the reconstructed spectra. Although the spectral broadening and the fluctuation were slightly shown, the errors of the relative exposure were under 10%. Though the experimental arrangement of this method is so easy and reconstructed algorithm is simple, these results suggested that this method is little influenced by the variation of dose rates or property of the incident x rays. We therefore propose that the Compton scatter spectroscopy with the newly developed Schottky CdTe detector is suitable for measuring the diagnostic x-ray spectra of the CT system under the clinical conditions and useful for quality assurance and quality control of the clinical x-ray CT system. (author)

X-ray spectroscopy for high energy-density X pinch density and temperature measurements (invited)

International Nuclear Information System (INIS)

Pikuz, S.A.; Shelkovenko, T.A.; Chandler, K.M.; Mitchell, M.D.; Hammer, D.A.; Skobelev, I.Y.; Shlyaptseva, A.S.; Hansen, S.B.

2004-01-01

X pinch plasmas produced from fine metal wires can reach near solid densities and temperatures of 1 keV or even more. Plasma conditions change on time scales as short as 5-10 ps as determined using an x-ray streak camera viewing a focusing crystal spectrograph or directly viewing the plasma through multiple filters on a single test. As a result, it is possible to determine plasma conditions from spectra with ∼10 ps time resolution. Experiments and theory are now coming together to give a consistent picture of the dynamics and kinetics of these high energy density plasmas with very high temporal and spatial precision. A set of diagnostic techniques used in experiments for spectrally, temporally, and spatially resolved measurements of X pinch plasmas is described. Results of plasma parameter determination from these measurements are presented. X ray backlighting of one x-pinch by another with ∼30 ps x-ray pulses enables the dynamics and kinetics to be correlated in time

A Comparison Of GADRAS Simulated And Measured Gamma Ray Spectra

International Nuclear Information System (INIS)

Jeffcoat, R.; Salaymeh, S.

2010-01-01

Gamma-ray radiation detection systems are continuously being developed and improved for detecting the presence of radioactive material and for identifying isotopes present. Gamma-ray spectra, from many different isotopes and in different types and thicknesses of attenuation material and matrixes, are needed to evaluate the performance of these devices. Recently, a test and evaluation exercise was performed by the Savannah River National Laboratory that required a large number of gamma-ray spectra. Simulated spectra were used for a major portion of the testing in order to provide a pool of data large enough for the results to be statistically significant. The test data set was comprised of two types of data, measured and simulated. The measured data were acquired with a hand-held Radioisotope Identification Device (RIID) and simulated spectra were created using Gamma Detector Response and Analysis Software (GADRAS, Mitchell and Mattingly, Sandia National Laboratory). GADRAS uses a one-dimensional discrete ordinate calculation to simulate gamma-ray spectra. The measured and simulated spectra have been analyzed and compared. This paper will discuss the results of the comparison and offer explanations for spectral differences.

Electron temperature from x-ray continuum measurements on the NIF

Science.gov (United States)

Jarrott, Leonard; Bachmann, Benjamin; Benedetti, Robin; Izumi, Nobuhiko; Khan, Shahab; Landen, Otto; Ma, Tammy; Nagel, Sabrina; Pak, Arthur; Patel, Prav; Schneider, Marilyn; Springer, Paul; LLNL Collaboration

2017-10-01

We report on measurements of the electron temperature within the hot spot of inertially confined, layered implosions on the NIF using a titanium differential filtering x-ray diagnostic. The electron temperature from x-ray emission is insensitive to non-thermal velocity flows as is the case with ion temperature measurements and is thus a critical parameter in interpreting stagnated hot spot conditions. Here we discuss measurements using titanium filters ranging from 10 μm to 1mm in thickness with a sensitivity band of 10-30keV coupled with penumbral pinholes. The use of larger pinhole diameters increases x-ray fluence improving sensitivity of photon energies with minimal attenuation from the compressed fuel/shell. This diagnostic has been fielded on a series of cryogenic shots with DT ion temperatures ranging from 2-5keV. Analysis of the measurement will be presented along with a comparison against simulated electron temperatures and x-ray spectra as well as a comparison to DT ion temperature measurements. This work was performed under the auspices of U.S. DoE by LLNL under Contract No. DE-AC52-07NA27344.

On the Weak-Wind Problem in Massive Stars: X-Ray Spectra Reveal a Massive Hot Wind in mu Columbae

Science.gov (United States)

Huenemoerder, David P.; Oskinova, Lidia M.; Ignace, Richard; Waldron, Wayne L.; Todt, Helge; Hamaguchi, Kenji; Kitamoto, Shunji

2012-01-01

Mu Columbae is a prototypical weak-wind O star for which we have obtained a high-resolution X-ray spectrum with the Chandra LETG/ACIS instrument and a low-resolution spectrum with Suzaku. This allows us, for the first time, to investigate the role of X-rays on the wind structure in a bona fide weak-wind system and to determine whether there actually is a massive hot wind. The X-ray emission measure indicates that the outflow is an order of magnitude greater than that derived from UV lines and is commensurate with the nominal wind-luminosity relationship for O stars. Therefore, the "weak-wind problem"--identified from cool wind UV/optical spectra--is largely resolved by accounting for the hot wind seen in X-rays. From X-ray line profiles, Doppler shifts, and relative strengths, we find that this weak-wind star is typical of other late O dwarfs. The X-ray spectra do not suggest a magnetically confined plasma-the spectrum is soft and lines are broadened; Suzaku spectra confirm the lack of emission above 2 keV. Nor do the relative line shifts and widths suggest any wind decoupling by ions. The He-like triplets indicate that the bulk of the X-ray emission is formed rather close to the star, within five stellar radii. Our results challenge the idea that some OB stars are "weak-wind" stars that deviate from the standard wind-luminosity relationship. The wind is not weak, but it is hot and its bulk is only detectable in X-rays.

Radiation detectors of PIN type for X-rays

International Nuclear Information System (INIS)

Ramirez-Jimenez, F.J.

2003-01-01

In this laboratory session, tree experiments are proposed: the measurement of X-ray energy spectra from radioactive sources with a high resolution cooled Si-Li detector, with a room temperature PIN diode and the measurement of the response of a PIN diode to the intensity of X-rays of radio-diagnostic units. The spectra obtained with the Si-Li detector help to understand the energy distribution of X-rays and are used as a reference to compare the results obtained with the PIN diode. Measurements in medical X-ray machines are proposed. Low cost, simple electronic instruments and systems are used as tools to make measurements in X-ray units used in radio-diagnostic

X-ray diagnostic in gas discharge

International Nuclear Information System (INIS)

Chen Suhe; Wang Dalun; Cui Gaoxian; Wang Mei; Fu Yibei; Zhang Xinwei; Zhang Wushou

1995-01-01

X rays were observed when the anomalous phenomenon in the metal loaded with deuterium studied by the gas-discharge method. Therefore the X-ray energy spectra were measured by the absorption method, the specific X-ray approach and the NaI scintillation counter, while X-ray intensity was estimated by using 7 Li thermoluminescent foils. The X-ray average energy measured by the absorption method is 27.6 +- 2.1 keV, which is fitted within the error extent to 26.0 +-2.4 keV monoenergetic X rays measured by the NaI scintillation counter

X-ray spectroscopy and dosimetry with a portable CdTe device

International Nuclear Information System (INIS)

Abbene, Leonardo; La Manna, Angelo; Fauci, Francesco; Gerardi, Gaetano; Stumbo, Simone; Raso, Giuseppe

2007-01-01

X-ray spectra and dosimetry information are very important for quality assurance (QA) and quality control (QC) in medical diagnostic X-ray systems. An accurate knowledge of the diagnostic X-ray spectra would improve the patient dose optimization, without compromising image information. In this work, we performed direct diagnostic X-ray spectra measurements with a portable device, based on a CdTe solid-state detector. The portable device is able to directly measure X-ray spectra at high photon fluence rates, as typical of clinical radiography. We investigated on the spectral performances of the system in the mammographic energy range (up to ∼40 keV). Good system response to monoenergetic photons was measured (energy resolution of 5% FWHM at 22.1 keV). We measured the molybdenum X-ray spectra produced by a mammographic X-ray unit (GE Senographe DMR) at 28 kV and 30 kV under clinical conditions. The results showed the good reproducibility of the system and low pile-up distortions. Preliminary dosimetric measurements have been regarded as exposure and half value layer (HVL) values obtained from direct measurements and from measured X-ray spectral data, and a good agreement between exposure attenuation curves and the HVL values was obtained. The results indicated that the portable device is suitable for mammographic X-ray spectroscopy under clinical conditions

On hard X-ray spectra of accreting neutron stars

International Nuclear Information System (INIS)

Zheleznyakov, V.V.

1982-01-01

Formation of the spectra of X-ray pulsars and gamma bursters is investigated. Interpretation of a hard X-ray spectrum of pulsars containing cyclotron lines is feasible on the basis of an isothermal model of a polar spot heated due to acccretion to a neutron star. It has been ascertained that in the regions responsible for the formation of continuum radiation and lines the mode polarization is determined by a magnetized vacuum rather than by a plasma. Bearing this in mind, the influence of the magnetic field of a star on the wide wings of the cyclotron line and on its depth is discussed. The part played by the accreting column in the case of strong accretion (approx. equal to 10 19 el cm -3 ) needed for long sustaining of the high level of X-rays from a neutron star-pulsar is studied. There occur the gaps in spectrum at frequencies close to the electron gyro-frequency and its harmonics due to the screening of the hot spot by the opaque gyro-resonant layer located within the accreting column. These gaps ensure the formation of cyclotron lines in absorption irrespective of the presence of such lines in the X-ray spectrum of a polar hot spot. (orig./WL)

X-ray stars observed in LAMOST spectral survey

Science.gov (United States)

Lu, Hong-peng; Zhang, Li-yun; Han, Xianming L.; Shi, Jianrong

2018-05-01

X-ray stars have been studied since the beginning of X-ray astronomy. Investigating and studying the chromospheric activity from X-ray stellar optical spectra is highly significant in providing insights into stellar magnetic activity. The big data of LAMOST survey provides an opportunity for researching stellar optical spectroscopic properties of X-ray stars. We inferred the physical properties of X-ray stellar sources from the analysis of LAMOST spectra. First, we cross-matched the X-ray stellar catalogue (12254 X-ray stars) from ARXA with LAMOST data release 3 (DR3), and obtained 984 good spectra from 713 X-ray sources. We then visually inspected and assigned spectral type to each spectrum and calculated the equivalent width (EW) of Hα line using the Hammer spectral typing facility. Based on the EW of Hα line, we found 203 spectra of 145 X-ray sources with Hα emission above the continuum. For these spectra we also measured the EWs of Hβ, Hγ, Hδ and Ca ii IRT lines of these spectra. After removing novae, planetary nebulae and OB-type stars, we found there are 127 X-ray late-type stars with Hα line emission. By using our spectra and results from the literature, we found 53 X-ray stars showing Hα variability; these objects are Classical T Tauri stars (CTTs), cataclysmic variables (CVs) or chromospheric activity stars. We also found 18 X-ray stars showing obvious emissions in the Ca ii IRT lines. Of the 18 X-ray stars, 16 are CTTs and 2 are CVs. Finally, we discussed the relationships between the EW of Hα line and X-ray flux.

Measuring spectroscopy and magnetism of extracted and intracellular magnetosomes using soft X-ray ptychography.

Science.gov (United States)

Zhu, Xiaohui; Hitchcock, Adam P; Bazylinski, Dennis A; Denes, Peter; Joseph, John; Lins, Ulysses; Marchesini, Stefano; Shiu, Hung-Wei; Tyliszczak, Tolek; Shapiro, David A

2016-12-20

Characterizing the chemistry and magnetism of magnetotactic bacteria (MTB) is an important aspect of understanding the biomineralization mechanism and function of the chains of magnetosomes (Fe 3 O 4 nanoparticles) found in such species. Images and X-ray absorption spectra (XAS) of magnetosomes extracted from, and magnetosomes in, whole Magnetovibrio blakemorei strain MV-1 cells have been recorded using soft X-ray ptychography at the Fe 2p edge. A spatial resolution of 7 nm is demonstrated. Precursor-like and immature magnetosome phases in a whole MV-1 cell were visualized, and their Fe 2p spectra were measured. Based on these results, a model for the pathway of magnetosome biomineralization for MV-1 is proposed. Fe 2p X-ray magnetic circular dichroism (XMCD) spectra have been derived from ptychography image sequences recorded using left and right circular polarization. The shape of the XAS and XMCD signals in the ptychographic absorption spectra of both sample types is identical to the shape and signals measured with conventional bright-field scanning transmission X-ray microscope. A weaker and inverted XMCD signal was observed in the ptychographic phase spectra of the extracted magnetosomes. The XMCD ptychographic phase spectrum of the intracellular magnetosomes differed from the ptychographic phase spectrum of the extracted magnetosomes. These results demonstrate that spectro-ptychography offers a superior means of characterizing the chemical and magnetic properties of MTB at the individual magnetosome level.

Theory of pump–probe ultrafast photoemission and X-ray absorption spectra

Energy Technology Data Exchange (ETDEWEB)

Fujikawa, Takashi, E-mail: tfujikawa@faculty.chiba-u.jp; Niki, Kaori

2016-01-15

Highlights: • Pump–probe ultrafast XAFS and XPS spectra are theoretically studied. • Keldysh Green's function theory is applied. • Important many-body effects are explicitly included. - Abstract: Keldysh Green's function approach is extensively used in order to derive practical formulas to analyze pump–probe ultrafast photoemission and X-ray absorption spectra. Here the pump pulse is strong enough whereas the probe X-ray pulse can be treated by use of a perturbation theory. We expand full Green's function in terms of renormalized Green's function without the interaction between electrons and probe pulse. The present theoretical formulas allow us to handle the intrinsic and extrinsic losses, and furthermore resonant effects in X-ray Absorption Fine Structures (XAFS). To understand the radiation field screening in XPS spectra, we have to use more sophisticated theoretical approach. In the ultrafast XPS and XAFS analyses the intrinsic and extrinsic loss effects can interfere as well. In the XAFS studies careful analyses are necessary to handle extrinsic losses in terms of damped photoelectron propagation. The nonequilibrium dynamics after the pump pulse irradiation is well described by use of the time-dependent Dyson orbitals. Well above the edge threshold, ultrafast photoelectron diffraction and extended X-ray absorption fine structure (EXAFS) provide us with transient structural change after the laser pump excitations. In addition to these slow processes, the rapid oscillation in time plays an important role related to pump electronic excitations. Near threshold detailed information could be obtained for the combined electronic and structural dynamics. In particular high-energy photoemission and EXAFS are not so influenced by the details of excited states by pump pulse. Random-Phase Approximation (RPA)-boson approach is introduced to derive some practical formulas for time-dependent intrinsic amplitudes.

Effects of phonon broadening on x-ray near-edge spectra in molecular crystals

Science.gov (United States)

Vinson, John; Jach, Terrence; Elam, Tim; Denlinger, Jonathon

2014-03-01

Calculations of near-edge x-ray spectra are often carried out using the average atomic coordinates from x-ray or neutron scattering experiments or from density functional theory (DFT) energy minimization. This neglects disorder from thermal and zero-point vibrations. Here we look at the nitrogen K-edge of ammonium chloride and ammonium nitrate, comparing Bethe-Salpeter calculations of absorption and fluorescence to experiment. We find that intra-molecular vibrational effects lead to significant, non-uniform broadening of the spectra, and that for some features zero-point motion is the primary source of the observed shape.

Spatially resolved X-ray spectra of coronal active regions

International Nuclear Information System (INIS)

Catura, R.C.; Acton, L.W.; Joki, E.G.; Rapley, C.G.; Culhane, J.L.

1975-01-01

X-ray spectra from a number of coronal active regions were obtained during ATM support rocket flights carried out by the Lockheed group on June 11 and December 19, 1973. Multi-grid collimators were used to provide fields of view of 40ins. diameter and 90ins. diameter for a number of scanning crystal spectrometers and a bent crystal spectrometer which employed a position sensitive proportional counter to register the diffracted spectrum. A solar image was produced on film and on a TV camera on board the rocket with the aid of a 1 A Hα filter. A small part of the X-ray collimator was used to generate a multiple spot diffraction pattern which was superimposed on the Hα image and the composite picture was transmitted to the ground. Pre-launch calibrations allowed the spot corresponding to the X-ray collimator axis to be identified and so the collimator pointing direction on the solar disc was controlled from the ground by means of commands sent to the rocket. (Auth.)

The X-ray spectra of clusters of galaxies and their relationship to other cluster properties

International Nuclear Information System (INIS)

Mitchell, R.J.; Dickens, R.J.; Burnell, S.J.B.; Culhane, J.L.

1979-01-01

New observations with the MSSL proportional counter spectrometer on the Ariel V satellite of the X-ray spectra of 20 candidate clusters of galaxies are reported. The data are compared with the results from the OSO-8 satellite and the combined sample of some 30 cluster X-ray spectra are analysed. The present study finds generally larger values of Lsub(X) than do Uhuru or the SSI, which, because of the larger field of view, may indicate significant amounts of hot gas away from the cluster centres. The validity of all X-ray cluster identifications has been examined, and sources have been classified according to certainty of identification. The incidence of X-ray line emission from the clusters has been investigated and temperatures, kTsub(X), have been derived on the basis of an isothermal model. Relationships between X-ray, optical and radio properties of the clusters have been studied. The more massive, centrally condensed clusters generally contain higher temperature gas and have a greater luminosity than the less massive, more irregular clusters. (author)

gamma-ray spectra measurements for long cooled MOX spent fuels

International Nuclear Information System (INIS)

Murakami, Kiyonobu; Kobayashi, Iwao

1993-09-01

Gamma-ray spectra of spent fuels have important informations in the estimation of burnup rate, concentration of fission products, cooling time and etc. which are required in the fuel loading control of reactors and special nuclear materials accountancy from the view point of safe guard. Although, some available data are given about uranium dioxide fuels, few data are given about uranium and plutonium dioxide mixtures (MOX fuels). Especially, there is few data about MOX fuels which are irradiated in thermal reactors and cooled more than ten years. Gamma-ray spectra are measured for PuO 2 -UO 2 fuel rods (IFA-159, IFA-160) which are irradiated at HBWR in Norway up to 9,420 and 5,340MWd/t respectively. Gamma-ray spectra had been measured about the two fuels ten years ago at the spent fuel pond of Japan Demonstration Reactor (JPDR). The objectives of this measurement is to know how decayed the gamma-ray spectra in these ten years and some fission products are there which are effective to estimate burnup rate of spent MOX fuels. (author)

New Spectral Model for Constraining Torus Covering Factors from Broadband X-Ray Spectra of Active Galactic Nuclei

Science.gov (United States)

Baloković, M.; Brightman, M.; Harrison, F. A.; Comastri, A.; Ricci, C.; Buchner, J.; Gandhi, P.; Farrah, D.; Stern, D.

2018-02-01

The basic unified model of active galactic nuclei (AGNs) invokes an anisotropic obscuring structure, usually referred to as a torus, to explain AGN obscuration as an angle-dependent effect. We present a new grid of X-ray spectral templates based on radiative transfer calculations in neutral gas in an approximately toroidal geometry, appropriate for CCD-resolution X-ray spectra (FWHM ≥ 130 eV). Fitting the templates to broadband X-ray spectra of AGNs provides constraints on two important geometrical parameters of the gas distribution around the supermassive black hole: the average column density and the covering factor. Compared to the currently available spectral templates, our model is more flexible, and capable of providing constraints on the main torus parameters in a wider range of AGNs. We demonstrate the application of this model using hard X-ray spectra from NuSTAR (3–79 keV) for four AGNs covering a variety of classifications: 3C 390.3, NGC 2110, IC 5063, and NGC 7582. This small set of examples was chosen to illustrate the range of possible torus configurations, from disk-like to sphere-like geometries with column densities below, as well as above, the Compton-thick threshold. This diversity of torus properties challenges the simple assumption of a standard geometrically and optically thick toroidal structure commonly invoked in the basic form of the unified model of AGNs. Finding broad consistency between our constraints and those from infrared modeling, we discuss how the approach from the X-ray band complements similar measurements of AGN structures at other wavelengths.

Coronal temperature diagnostics from high-resolution soft X-ray spectra

Science.gov (United States)

Strong, K. T.; Claflin, E. S.; Lemen, J. R.; Linford, G. A.

1988-01-01

The problem of deriving the temperature of the coronal plasma from soft X-ray spectra is discussed. Spectral atlas scans of the soft X-ray spectrum from the Flat Crystal Spectrometer on the Solar Maximum Mission are compared with theoretical predictions of the relative intensities of some of the brighter lines to determine which line intensity ratios give the most reliable temperature diagnostics. The techniques considered include line widths, He-like G ratios, intensity ratios, and ratios of lines formed by different elements. It is found that the best temperature diagnostics come from the ratios of lines formed by successive ionization stages of the same element.

Theoretically predicted soft x-ray emission and absorption spectra of graphitic-structured BC2N

Science.gov (United States)

Muramatsu, Yasuji

Theoretical B K, C K and N K x-ray emission/absorption spectra of three possible graphitic-structured BC2N clusters are predicted based on the B2p-, C2p-, and N2p- density-of-states (DOS) calculated by discrete variational (DV)-X[alpha] molecular orbital calculations. Several prominent differences in DOS spectral features among BC2Ns, h-BN, and graphite are confirmed from comparison of calculated B2p-, C2p-, and N2p-DOS spectra. These variations in the spectra allow BC2N structures to be positively identified by high-resolution x-ray emission/absorption spectroscopy in the B K, C K, and N K regions.

Monte Carlo derivation of filtered tungsten anode X-ray spectra for dose computation in digital mammography

Energy Technology Data Exchange (ETDEWEB)

Paixao, L.; Oliveira, B. B.; Nogueira, M. do S. [Centro de Desenvolvimento da Tecnologia Nuclear, Post-graduation in Science and Technology of Radiations, Minerals and Materials, Pte. Antonio Carlos 6.627, Pampulha, 31270-901 Belo Horizonte (Brazil); Viloria, C. [UFMG, Departamento de Engenharia Nuclear, Post-graduation in Nuclear Sciences and Techniques, Pte. Antonio Carlos 6.627, Pampulha, 31270-901 Belo Horizonte (Brazil); Alves de O, M. [UFMG, Department of Anatomy and Imaging, Prof. Alfredo Balena 190, 30130-100 Belo Horizonte (Brazil); Araujo T, M. H., E-mail: lpr@cdtn.br [Dr Maria Helena Araujo Teixeira Clinic, Guajajaras 40, 30180-100 Belo Horizonte (Brazil)

2014-08-15

It is widely accepted that the mean glandular dose (D{sub G}) for the glandular tissue is the more useful magnitude for characterizing the breast cancer risk. The procedure to estimate the D{sub G}, for being difficult to measure it directly in the breast, it is to make the use of conversion factors that relate incident air kerma (K{sub i}) at this dose. Generally, the conversion factors vary with the x-ray spectrum half-value layer and the breast composition and thickness. Several authors through computer simulations have calculated such factors by the Monte Carlo (Mc) method. Many spectral models for D{sub G} computer simulations purposes are available in the diagnostic range. One of the models available generates unfiltered spectra. In this work, the Monte Carlo EGSnrc code package with the C++ class library (eg spp) was employed to derive filtered tungsten x-ray spectra used in digital mammography systems. Filtered spectra for rhodium and aluminium filters were obtained for tube potentials between 26 and 32 kV. The half-value layer of simulated filtered spectra were compared with those obtained experimentally with a solid state detector Unfors model 8202031-H Xi R/F and Mam Detector Platinum and 8201023-C Xi Base unit Platinum Plus w m As in a Hologic Selenia Dimensions system using a Direct Radiography mode. Calculated half-value layer values showed good agreement compared to those obtained experimentally. These results show that the filtered tungsten anode x-ray spectra and the EGSnrc Mc code can be used for D{sub G} determination in mammography. (Author)

Monte Carlo derivation of filtered tungsten anode X-ray spectra for dose computation in digital mammography

International Nuclear Information System (INIS)

Paixao, L.; Oliveira, B. B.; Nogueira, M. do S.; Viloria, C.; Alves de O, M.; Araujo T, M. H.

2014-08-01

It is widely accepted that the mean glandular dose (D G ) for the glandular tissue is the more useful magnitude for characterizing the breast cancer risk. The procedure to estimate the D G , for being difficult to measure it directly in the breast, it is to make the use of conversion factors that relate incident air kerma (K i ) at this dose. Generally, the conversion factors vary with the x-ray spectrum half-value layer and the breast composition and thickness. Several authors through computer simulations have calculated such factors by the Monte Carlo (Mc) method. Many spectral models for D G computer simulations purposes are available in the diagnostic range. One of the models available generates unfiltered spectra. In this work, the Monte Carlo EGSnrc code package with the C++ class library (eg spp) was employed to derive filtered tungsten x-ray spectra used in digital mammography systems. Filtered spectra for rhodium and aluminium filters were obtained for tube potentials between 26 and 32 kV. The half-value layer of simulated filtered spectra were compared with those obtained experimentally with a solid state detector Unfors model 8202031-H Xi R/F and Mam Detector Platinum and 8201023-C Xi Base unit Platinum Plus w m As in a Hologic Selenia Dimensions system using a Direct Radiography mode. Calculated half-value layer values showed good agreement compared to those obtained experimentally. These results show that the filtered tungsten anode x-ray spectra and the EGSnrc Mc code can be used for D G determination in mammography. (Author)

Comparison of hard X-ray spectra obtained by spectrometers on Hinotori and SMM and detection of 'superhot' component

Science.gov (United States)

Nitta, Nariaki

1988-01-01

Hard X-ray spectra in solar flares obtained by the broadband spectrometers aboard Hinotori and SMM are compared. Within the uncertainty brought about by assuming the typical energy of the background X-rays, spectra by the Hinotori spectrometer are usually consistent with those by the SMM spectrometer for flares in 1981. On the contrary, flares in 1982 persistently show 20-50-percent higher flux by Hinotori than by SMM. If this discrepancy is entirely attributable to errors in the calibration of energy ranges, the errors would be about 10 percent. Despite such a discrepancy in absolute flux, in the the decay phase of one flare, spectra revealed a hard X-ray component (probably a 'superhot' component) that could be explained neither by emission from a plasma at about 2 x 10 to the 7th K nor by a nonthermal power-law component. Imaging observations during this period show hard X-ray emission nearly cospatial with soft X-ray emission, in contrast with earlier times at which hard and soft X-rays come from different places.

Effects of X-ray tube parameters on thickness measure precision in X-ray profile gauge

International Nuclear Information System (INIS)

Miao Jichen; Wu Zhifang; Xing Guilai

2011-01-01

Instantaneous profile gauge technology has been widely used in metallurgy industry because it can on-line get the profile of steel strip. It has characters of high measure precision and wide measure range, but the X-ray tube parameters only can be set few different values during measurement. The relations of thickness measure precision and X-ray tube current, X-ray tube voltage were analyzed. The results show that the X-ray tube current affects the thickness measure precision and the X-ray tube voltage determines the thickness measure range. The method of estimating the X-ray current by thickness measure precision was provided in the end. This method is the base of X-ray source selection and X-ray source parameter's setting in the instantaneous profile gauge. (authors)

Reconstruction of energetic electron spectra in the upper atmosphere: balloon observations of auroral X-rays coordinated with measurements from the EISCAT radar

International Nuclear Information System (INIS)

Olafsson, K.J.

1990-08-01

Energetic electron precipitation in the auroral zone has been studied using coordinated auroral X-ray measurements from balloons, altitude profiles of the ionospheric electron density measured by the EISCAT radar above the balloons, and cosmic noise absorption data from the Scandinavian riometer network. The data were obtained during the Coordinated EISCAT and Balloon Observations (CEBO) campaign in August 1984. The energy spectral variations of both the X-ray fluxes and the primary precipitating electrons were examined for two precipitation events in the morning sector. As far as reasonably can be concluded from observations of magnetic activity in the auroral zone, and from the temporal development of the energy spectra, the two precipitation events can be interpreted in the frame of present models of energetic electron precipitation on the mordning side of the auroral zone. 96 refs., 70 figs., 11 tabs

Modification of the TASMIP x-ray spectral model for the simulation of microfocus x-ray sources

Energy Technology Data Exchange (ETDEWEB)

Sisniega, A.; Vaquero, J. J., E-mail: juanjose.vaquero@uc3m.es [Departamento de Bioingeniería e Ingeniería Aeroespacial, Universidad Carlos III de Madrid, Madrid ES28911 (Spain); Instituto de Investigación Sanitaria Gregorio Marañón, Madrid ES28007 (Spain); Desco, M. [Departamento de Bioingeniería e Ingeniería Aeroespacial, Universidad Carlos III de Madrid, Madrid ES28911 (Spain); Instituto de Investigación Sanitaria Gregorio Marañón, Madrid ES28007 (Spain); Centro de Investigación Biomédica en Red de Salud Mental (CIBERSAM), Madrid ES28029 (Spain)

2014-01-15

Purpose: The availability of accurate and simple models for the estimation of x-ray spectra is of great importance for system simulation, optimization, or inclusion of photon energy information into data processing. There is a variety of publicly available tools for estimation of x-ray spectra in radiology and mammography. However, most of these models cannot be used directly for modeling microfocus x-ray sources due to differences in inherent filtration, energy range and/or anode material. For this reason the authors propose in this work a new model for the simulation of microfocus spectra based on existing models for mammography and radiology, modified to compensate for the effects of inherent filtration and energy range. Methods: The authors used the radiology and mammography versions of an existing empirical model [tungsten anode spectral model interpolating polynomials (TASMIP)] as the basis of the microfocus model. First, the authors estimated the inherent filtration included in the radiology model by comparing the shape of the spectra with spectra from the mammography model. Afterwards, the authors built a unified spectra dataset by combining both models and, finally, they estimated the parameters of the new version of TASMIP for microfocus sources by calibrating against experimental exposure data from a microfocus x-ray source. The model was validated by comparing estimated and experimental exposure and attenuation data for different attenuating materials and x-ray beam peak energy values, using two different x-ray tubes. Results: Inherent filtration for the radiology spectra from TASMIP was found to be equivalent to 1.68 mm Al, as compared to spectra obtained from the mammography model. To match the experimentally measured exposure data the combined dataset required to apply a negative filtration of about 0.21 mm Al and an anode roughness of 0.003 mm W. The validation of the model against real acquired data showed errors in exposure and attenuation in

Modification of the TASMIP x-ray spectral model for the simulation of microfocus x-ray sources

International Nuclear Information System (INIS)

Sisniega, A.; Vaquero, J. J.; Desco, M.

2014-01-01

Purpose: The availability of accurate and simple models for the estimation of x-ray spectra is of great importance for system simulation, optimization, or inclusion of photon energy information into data processing. There is a variety of publicly available tools for estimation of x-ray spectra in radiology and mammography. However, most of these models cannot be used directly for modeling microfocus x-ray sources due to differences in inherent filtration, energy range and/or anode material. For this reason the authors propose in this work a new model for the simulation of microfocus spectra based on existing models for mammography and radiology, modified to compensate for the effects of inherent filtration and energy range. Methods: The authors used the radiology and mammography versions of an existing empirical model [tungsten anode spectral model interpolating polynomials (TASMIP)] as the basis of the microfocus model. First, the authors estimated the inherent filtration included in the radiology model by comparing the shape of the spectra with spectra from the mammography model. Afterwards, the authors built a unified spectra dataset by combining both models and, finally, they estimated the parameters of the new version of TASMIP for microfocus sources by calibrating against experimental exposure data from a microfocus x-ray source. The model was validated by comparing estimated and experimental exposure and attenuation data for different attenuating materials and x-ray beam peak energy values, using two different x-ray tubes. Results: Inherent filtration for the radiology spectra from TASMIP was found to be equivalent to 1.68 mm Al, as compared to spectra obtained from the mammography model. To match the experimentally measured exposure data the combined dataset required to apply a negative filtration of about 0.21 mm Al and an anode roughness of 0.003 mm W. The validation of the model against real acquired data showed errors in exposure and attenuation in

Study of X-Ray and $\\gamma$-Ray Spectra from Antiprotonic Atoms at the Slowly Extracted Antiproton Beam of LEAR

CERN Multimedia

2002-01-01

This experiment will study the X-ray spectra of antiprotonic atoms and the $\\gamma$ spectra of residual nuclei after the antiproton absorption. We intend to begin with measurements on selected isotopically pure targets. Strong interaction effects, the antiproton absorption and the atomic cascade are analysed through the measurement of energies, lineshapes, relative and absolute intensities of all observable lines. The experiments are continued to determine st in resolved fine structure levels and in different isotopes of the same element. Coincidence techniques may be applied. All components of the experimental set-up are already existing from previous experiments and we could begin the measurements with any slowly extracted beam of low energy at LEAR.

X-ray scattering measurements from thin-foil x-ray mirrors

DEFF Research Database (Denmark)

Christensen, Finn Erland; BYRNAK, BP; Hornstrup, Allan

1992-01-01

Thin foil X-ray mirrors are to be used as the reflecting elements in the telescopes of the X-ray satellites Spectrum-X-Gamma (SRG) and ASTRO-D. High resolution X-ray scattering measurements from the Au coated and dip-lacquered Al foils are presented. These were obtained from SRG mirrors positioned...... in a test quadrant of the telescope structure and from ASTRO-D foils held in a simple fixture. The X-ray data is compared with laser data and other surface structure data such as STM, atomic force microscopy (AFM), TEM, and electron micrography. The data obtained at Cu K-alpha(1), (8.05 keV) from all...

High-Resolution X-Ray Spectra of the Symbiotic Star SS73 17

Science.gov (United States)

Eze, R. N. C.; Luna, G. J. M.; Smith, R. K.

2010-01-01

SS73 17 was an innocuous Mira-type symbiotic star until the International Gamma-Ray Astrophysics Laboratory and Swift discovered its bright hard X-ray emission, adding it to the small class of "hard X-ray emitting symbiotics." Suzaku observations in 2006 then showed it emits three bright iron lines as well, with little to no emission in the 0.3-2.0 keV bandpass. We present here follow-up observations with the Chandra High Energy Transmission Grating and Suzaku that confirm the earlier detection of strong emission lines of Fe K(alpha) fluorescence, Fe XXV and Fe XXVI but also show significantly more soft X-ray emission. The high-resolution spectrum also shows emission lines of other highly ionized ions as Si xiv and possibly S XVI. In addition, a re-analysis of the 2006 Suzaku data using the latest calibration shows that the hard (15-50 keV) X-ray emission is brighter than previously thought and remains constant in both the 2006 and 2008 data. The G ratio calculated from the Fe xxv lines shows that these lines are thermal, not photoionized, in origin.With the exception of the hard X-ray emission, the spectra from both epochs can be fit using thermal radiation assuming a differential emission measure based on a cooling-flow model combined with a full and partial absorber. We show that acceptable fits can be obtained for all the data in the 1-10 keV band varying only the partial absorber. Based on the temperature and accretion rate, the thermal emission appears to be arising from the boundary layer between the accreting white dwarf and the accretion disk.

HIGH-RESOLUTION X-RAY SPECTRA OF THE SYMBIOTIC STAR SS73 17

International Nuclear Information System (INIS)

Eze, R. N. C.; Luna, G. J. M.; Smith, R. K.

2010-01-01

SS73 17 was an innocuous Mira-type symbiotic star until the International Gamma-Ray Astrophysics Laboratory and Swift discovered its bright hard X-ray emission, adding it to the small class of 'hard X-ray emitting symbiotics'. Suzaku observations in 2006 then showed it emits three bright iron lines as well, with little to no emission in the 0.3-2.0 keV bandpass. We present here follow-up observations with the Chandra High Energy Transmission Grating and Suzaku that confirm the earlier detection of strong emission lines of Fe Kα fluorescence, Fe XXV and Fe XXVI but also show significantly more soft X-ray emission. The high-resolution spectrum also shows emission lines of other highly ionized ions as Si XIV and possibly S XVI. In addition, a re-analysis of the 2006 Suzaku data using the latest calibration shows that the hard (15-50 keV) X-ray emission is brighter than previously thought and remains constant in both the 2006 and 2008 data. The G ratio calculated from the Fe XXV lines shows that these lines are thermal, not photoionized, in origin. With the exception of the hard X-ray emission, the spectra from both epochs can be fit using thermal radiation assuming a differential emission measure based on a cooling-flow model combined with a full and partial absorber. We show that acceptable fits can be obtained for all the data in the 1-10 keV band varying only the partial absorber. Based on the temperature and accretion rate, the thermal emission appears to be arising from the boundary layer between the accreting white dwarf and the accretion disk.

NEWFIT, a computer program for the analysis of alpha, X-ray and gamma-ray spectra

International Nuclear Information System (INIS)

Welch, R.B.; Gyger, F.; Jost, D.T.; Gunten, H.R. von; Kraehenbuehl, U.

1988-01-01

The computer program NEWFIT has been developed for analysis of gamma-ray, X-ray and alpha spectra. The general shape used for the analysis of activity peaks is a Gaussian function. An exponential tail can be added for use in alpha spectra analysis. The algorithms to analyze the peak shapes and the program operation are presented. Special features include the ability to create realistic peak shapes based on the systematic deviations of the real peaks from the theoretical Gaussian shape, as well as the option to constrain the calculated areas of peaks from a given emitting nuclide to their relative branching ratios. The program is available from the authors. (orig.)

Improving x-ray fluorescence signal for benchtop polychromatic cone-beam x-ray fluorescence computed tomography by incident x-ray spectrum optimization: a Monte Carlo study.

Science.gov (United States)

Manohar, Nivedh; Jones, Bernard L; Cho, Sang Hyun

2014-10-01

To develop an accurate and comprehensive Monte Carlo (MC) model of an experimental benchtop polychromatic cone-beam x-ray fluorescence computed tomography (XFCT) setup and apply this MC model to optimize incident x-ray spectrum for improving production/detection of x-ray fluorescence photons from gold nanoparticles (GNPs). A detailed MC model, based on an experimental XFCT system, was created using the Monte Carlo N-Particle (MCNP) transport code. The model was validated by comparing MC results including x-ray fluorescence (XRF) and scatter photon spectra with measured data obtained under identical conditions using 105 kVp cone-beam x-rays filtered by either 1 mm of lead (Pb) or 0.9 mm of tin (Sn). After validation, the model was used to investigate the effects of additional filtration of the incident beam with Pb and Sn. Supplementary incident x-ray spectra, representing heavier filtration (Pb: 2 and 3 mm; Sn: 1, 2, and 3 mm) were computationally generated and used with the model to obtain XRF/scatter spectra. Quasimonochromatic incident x-ray spectra (81, 85, 90, 95, and 100 keV with 10 keV full width at half maximum) were also investigated to determine the ideal energy for distinguishing gold XRF signal from the scatter background. Fluorescence signal-to-dose ratio (FSDR) and fluorescence-normalized scan time (FNST) were used as metrics to assess results. Calculated XRF/scatter spectra for 1-mm Pb and 0.9-mm Sn filters matched (r ≥ 0.996) experimental measurements. Calculated spectra representing additional filtration for both filter materials showed that the spectral hardening improved the FSDR at the expense of requiring a much longer FNST. In general, using Sn instead of Pb, at a given filter thickness, allowed an increase of up to 20% in FSDR, more prominent gold XRF peaks, and up to an order of magnitude decrease in FNST. Simulations using quasimonochromatic spectra suggested that increasing source x-ray energy, in the investigated range of 81-100 ke

Monte Carlo simulations of plutonium gamma-ray spectra

International Nuclear Information System (INIS)

Koenig, Z.M.; Carlson, J.B.; Wang, Tzu-Fang; Ruhter, W.D.

1993-01-01

Monte Carlo calculations were investigated as a means of simulating the gamma-ray spectra of Pu. These simulated spectra will be used to develop and evaluate gamma-ray analysis techniques for various nondestructive measurements. Simulated spectra of calculational standards can be used for code intercomparisons, to understand systematic biases and to estimate minimum detection levels of existing and proposed nondestructive analysis instruments. The capability to simulate gamma-ray spectra from HPGe detectors could significantly reduce the costs of preparing large numbers of real reference materials. MCNP was used for the Monte Carlo transport of the photons. Results from the MCNP calculations were folded in with a detector response function for a realistic spectrum. Plutonium spectrum peaks were produced with Lorentzian shapes, for the x-rays, and Gaussian distributions. The MGA code determined the Pu isotopes and specific power of this calculated spectrum and compared it to a similar analysis on a measured spectrum

Influence of smoothing of X-ray spectra on parameters of calibration model

International Nuclear Information System (INIS)

Antoniak, W.; Urbanski, P.; Kowalska, E.

1998-01-01

Parameters of the calibration model before and after smoothing of X-ray spectra have been investigated. The calibration model was calculated using multivariate procedure - namely the partial least square regression (PLS). Investigations have been performed on an example of six sets of various standards used for calibration of some instruments based on X-ray fluorescence principle. The smoothing methods were compared: regression splines, Savitzky-Golay and Discrete Fourier Transform. The calculations were performed using a software package MATLAB and some home-made programs. (author)

The influence of magnetic field geometry on magnetars X-ray spectra

International Nuclear Information System (INIS)

Viganò, D; Pons, J A; Miralles, J A; Parkins, N; Zane, S; Turolla, R

2012-01-01

Nowadays, the analysis of the X-ray spectra of magnetically powered neutron stars or magnetars is one of the most valuable tools to gain insight into the physical processes occurring in their interiors and magnetospheres. In particular, the magnetospheric plasma leaves a strong imprint on the observed X-ray spectrum by means of Compton up-scattering of the thermal radiation coming from the star surface. Motivated by the increased quality of the observational data, much theoretical work has been devoted to develop Monte Carlo (MC) codes that incorporate the effects of resonant Compton scattering (RCS) in the modeling of radiative transfer of photons through the magnetosphere. The two key ingredients in this simulations are the kinetic plasma properties and the magnetic field (MF) configuration. The MF geometry is expected to be complex, but up to now only mathematically simple solutions (self-similar solutions) have been employed. In this work, we discuss the effects of new, more realistic, MF geometries on synthetic spectra. We use new force-free solutions [14] in a previously developed MC code [9] to assess the influence of MF geometry on the emerging spectra. Our main result is that the shape of the final spectrum is mostly sensitive to uncertain parameters of the magnetospheric plasma, but the MF geometry plays an important role on the angle-dependence of the spectra.

SU-F-I-75: Half-Value Layer Thicknesses and Homogeneity Coefficients for Fluoroscopic X-Ray Beam Spectra Incorporating Spectral Filtration

Energy Technology Data Exchange (ETDEWEB)

Wunderle, K [Cleveland Clinic Foundation, Cleveland, OH (United States); Wayne State University School of Medicine, Detroit, MI (United States); Godley, A; Shen, Z; Dong, F [Cleveland Clinic Foundation, Cleveland, OH (United States); Rakowski, J [Wayne State University School of Medicine, Detroit, MI (United States)

2016-06-15

Purpose: The purpose of this investigation is to quantify various first half-value-layers (HVLs), second HVLs and homogeneity coefficients (HCs) for a state-of-the-art fluoroscope utilizing spectral (copper) filtration. Methods: A Radcal (Monrovia, Ca) AccuPro dosimeter with a 10×6-6 calibrated ionization chamber was used to measure air kerma for radiographic x-ray exposures made on a Siemens (Erlangen, Germany) Artis ZeeGo fluoroscope operated in the service mode. The ionization chamber was centered in the x-ray beam at 72 cm from the focal spot with a source-to-image-distance of 120 cm. The collimators were introduced to limit the x-ray field to approximately 5 cm × 5 cm at the ionization chamber plane. Type-1100 aluminum filters, in 0.5 mm increments, were used to determine the HVL. Two HVL calculation methods were used, log-linear interpolation and Lambert-W interpolation as described by Mathieu [Med Phys, 38(8), 4546 (2011)]. Multiple measurements were made at 60, 80, 100, 120 kVp at spectral filtration thicknesses of 0, 0.1, 0.3, 0.6 and 0.9 mm. Results: First HVL, second HVL, and HCs are presented for the fluoroscopic x-ray beam spectra indicated above, with nearly identical results from the two interpolation methods. Accuracy of the set kVp was also determined and deviated less than 2%. First HVLs for fluoroscopic x-ray beam spectra without spectral filtration determined in our study were 7%–16% greater than previously published data by Fetterly et al. [Med Phys, 28, 205 (2001)]. However, the FDA minimum HVL requirements changed since that publication, requiring larger HVLs as of 2006. Additionally, x-ray tube and generator architecture have substantially changed over the last 15 years providing different beam spectra. Conclusion: X-ray beam quality characteristics for state-of-the-art fluoroscopes with spectral filtration have not been published. This study provides reference data which will be useful for defining beam qualities encountered on

An iterative method for unfolding time-resolved soft x-ray spectra of laser plasmas

International Nuclear Information System (INIS)

Tang Yongjian; Shen Kexi; Xu Hepin

1991-01-01

Dante-recorded temporal waveforms have been unfolded by using Fast Fourier transformation (FFT) and the inverted convolution theorem of Fourier analysis. The conversion of the signals to time-dependent soft x-ray spectra is accomplished on the IBM-PC/XT-286 microcomputer system with the code DTSP including SAND II reported by W.N.Mcelory et al.. An amplitude-limited iterative and periodic smoothing technique has been developed in the code DTSP. Time-resolved soft x-ray spectra with sixteen time-cell, and time-dependent radiation, [T R (t)], have been obtained for hohlraum targets irradiated with laser beams (λ = 1.06 μm) on LF-12 in 1989

Simulation of pulse height analysis soft X-ray spectra expected from W7-X

Science.gov (United States)

Jabłoński, S.; Czarnecka, A.; Kubkowska, M.; Ryć, L.; Weller, A.; Biedermann, C.; König, R.; W7-X Team

2015-10-01

A computer code named RayX has been developed for checking the performance of a spectroscopy system and optimizing individual parts, like detectors and filters for the pulse height analysis (PHA) diagnostic system designed for the stellarator W7-X. Using the code, the intensity and shape of the X-ray spectra are simulated for different plasma scenarios characterized by varying the temperature and density profiles as well as the electron cyclotron resonance heating (ECRH) power over a wide range. In the simulations of the recorded spectra, the influence of geometrical configuration changes of the diagnostic system (pinhole size, detector size, location of each diagnostic component), of the timing of data collection, as well as of the type and thickness of filters are being investigated. The atomic processes of free-free (bremsstrahlung), free-bound (recombination radiation), and bound-bound emission (line radiation) are considered. For the impurities fractional abundancies of 3% carbon (C), 0.5% oxygen (O) and 0.002% iron (Fe) are taken into account. Information about the number of photons which reach the detector and the current generated inside the detector is given. It is shown that the distance between pinhole and detector has a larger impact on the registered spectra (intensity and total number of photons) than the distance between plasma and pinhole. Based on the results of the simulations, the expected optimal positions of the individual components (pinholes, detectors) were defined for the PHA W7-X diagnostic system. A shorter version of this contribution is due to be published in PoS at: 1st EPS conference on Plasma Diagnostics

Changes in X-ray photoelectron spectra of yttria-tetragonal zirconia polycrystal by ion sputtering

Energy Technology Data Exchange (ETDEWEB)

Watanabe, Eiko; Yoshinari, Masao [Tokyo Dental College, Oral Health Science Center, Tokyo, Chiyoda-ku (Japan)

2016-04-15

This paper reports changes in X-ray photoelectron spectroscopy spectra of yttria-tetragonal zirconia polycrystal (Y-TZP) brought about by Ar ion sputtering. The changes in the core-level spectra of Y-TZP suggest that preferential sputtering of oxygen occurred. A new peak was observed near 0 eV binding energy accompanied with changes in the core-level spectra by the sputtering. After 18 h in a high vacuum following the sputtering, the spectra changed by the sputtering were returned to their original shapes. In contrast, the color of Y-TZP was changed from white to pale brown by X-ray irradiation and was changed from pale brown to dark gray by ion sputtering. However, when the new peak near 0 eV decreased after 18 h, no color change was observed. Therefore, it is thought that the new peak was mainly derived from electrons trapped in various kinds of oxygen vacancies created by the sputtering in other than color centers. (orig.)

Studies of the X-ray absorption spectra of some methylcyano esters

International Nuclear Information System (INIS)

Takahashi, Osamu; Saito, Ko; Mitani, Masaki; Yoshida, Hiroaki; Tahara, Fumitaka; Sunami, Tetsuji; Waki, Keiichiro; Senba, Yasunori; Hiraya, Atsunari; Pettersson, Lars G.M.

2005-01-01

Density functional theory (DFT) has been applied to simulate core-excited photoabsorption spectra for some methylcyano esters within a transition potential (TP) framework. Our calculations for methylcyano formate at the N and O K-edges are consistent with previous experimental spectra. For methylcyano acetate the photoabsorption spectra at the N and O K-edges were reinvestigated experimentally. Contrary to the previous experiment, only one main peak was observed at the N K-edge and this peak was assigned to N(1s) ->π* excitation. This result was supported by our theoretical calculations. The general trends in the X-ray absorption spectra and the site-specific bond scission of methylcyano esters at the N and O K-edges are also discussed

X-ray streak crystal spectography

International Nuclear Information System (INIS)

Kauffman, R.L.; Brown, T.; Medecki, H.

1983-01-01

We have built an x-ray streaked crystal spectrograph for making time-resolved x-ray spectral measurements. This instrument can access Bragg angles from 11 0 to 38 0 and x-ray spectra from 200 eV to greater than 10 keV. We have demonstrated resolving powers, E/δE > 200 at 1 keV and time resolution less than 20 psec. A description of the instrument and an example of the data is given

F K-edge soft X-ray absorption spectroscopy

International Nuclear Information System (INIS)

Sugimura, Tetsuro; Kawai, Jun; Maeda, Kuniko; Fukushima, Akiko; Shin, S.; Motoyama, Muneyuki; Nakajima Tsuyoshi

2001-01-01

We measured F X-ray absorption spectra of various fluorine compounds using a synchrotron radiation at KEK-PF. The absorption spectra were measured using X-ray fluorescence yield (XFY) and total electron yield (TEY) methods. Change of the spectral shape has a relation to the metal-fluorine bond distance. By comparing with the experimental spectrum and calculated spectrum, F 2p state density is divined into up and down states. (author)

The Zone of Avoidance as an X-ray absorber - the role of the galactic foreground modelling Swift XRT spectra

Science.gov (United States)

Racz, I. I.; Bagoly, Z.; Tóth, L. V.; Balázs, L. G.; Horvath, I.; Zahorecz, S.

2018-05-01

Gamma-ray bursts (GRBs) are the most powerful explosive events in the Universe. The prompt gamma emission is followed by an X-ray afterglow that is also detected for over nine hundred GRBs by the Swift BAT and XRT detectors. The X-ray afterglow spectrum bears essential information about the burst, and the surrounding interstellar medium (ISM). Since the radiation travels through the line of sight intergalactic medium and the ISM in the Milky Way, the observed emission is influenced by extragalactic and galactic components. The column density of the Galactic foreground ranges several orders of magnitudes, due to both the large scale distribution of ISM and its small scale structures. We examined the effect of local HI column density on the penetrating X-ray emission, as the first step towards a precise modeling of the measured X-ray spectra. We fitted the X-ray spectra using the Xspec software, and checked how the shape of the initially power low spectrum changes with varying input Galactic HI column density. The total absorbing HI column is a sum of the intrinsic and Galactic component. We also investigated the model results for the intrinsic component varying the Galactic foreground. We found that such variations may alter the intrinsic hydrogen column density up to twenty-five percent. We will briefly discuss its consequences.

X-ray binaries, part 1

International Nuclear Information System (INIS)

Hammerschlag-Hensberge, G.C.M.J.

1977-01-01

Optical observations of X-ray binaries and their interpretation are described. A number of early-type stars which are identified as companions of X-ray sources are photometrically and spectroscopically observed. The spectra were obtained with the coude spectrograph attached to the 1.5 m telescope of the European Southern Observatory, La Silla, Chile. Registrations of the spectra were made with the Faul-Coradi microphotometer of the Observatory at Utrecht. To study radial velocity variations, the positions of the spectral lines were measured with the Grant comparator of the University of Groningen

The Soft X-Ray Spectra of Sulfur Compounds.

Science.gov (United States)

Zhou, Ling

1995-01-01

The sulfur compounds including CdS, ZnS, rm MoS_2, WS_2, NiS, FeS, GaS, SnS, MgS and Alloy rm ZnS_{x }Se_{1-x} were investigated by using photon/e-beam excited soft x-ray spectroscopy through SXA, SXE, SXF and inelastic Resonant Raman scattering and resonant elastic scattering processes. For valence bands, the PDOS of S L_{2,3}, Zn M_{2,3}, Se M _{4,5}, bands locations, band gaps Eg, core level spin splitting, the lifetime broadening of valence band t_{1/2}, branching ratio of rm L_2/L_3 and shallow d level and exciton state were measured in some of these materials respectively. The excitation mechanism or threshold effects were studied for CdS, ZnS, MoS_2, WS_2, FeS, NiS, and alloy. In photon excited S L_ {2,3}^ectra, local core levels with spin splitting were found to charge threshold effects. The threshold effects are also found to be influenced by resonant elastic and inelastic scattering process. A simple model and the second order perturbation theory are used to explain the observed inelastic Raman scattering of Zn M _{2,3} spectra near d threshold. The d participation in the chemical bonding and interactions was studied. Atomiclike d bands were found in FeS and NiS from strong d-d and d-p couplings. Two groups of d bands were observed in Transitional Metal Sulfides (TMS) and the no-bonding group with a few d bands was found to across whole valence bands in TMS. The direct connection between valence bands and conduction bands is built and some conduction bands were studied. A study of alloy was included briefly. These experiments provide a rich information about TMS, and prove that Soft X-ray Spectroscopy is a powerful, precise and reliable tool in the study of fine electronic band structure in solids.

Soft X-ray absorption spectra of aqueous salt solutions with highly charged cations in liquid microjets

Energy Technology Data Exchange (ETDEWEB)

Schwartz, Craig P.; Uejio, Janel S.; Duffin, Andrew M.; Drisdell, Walter S.; Smith, Jared D.; Saykally, Richard J.

2010-03-11

X-ray absorption spectra of 1M aqueous solutions of indium (III) chloride, yttrium (III) bromide, lanthanum (III) chloride, tin (IV) chloride and chromium (III) chloride have been measured at the oxygen K-edge. Relatively minor changes are observed in the spectra compared to that of pure water. SnCl{sub 4} and CrCl{sub 3} exhibit a new onset feature which is attributed to formation of hydroxide or other complex molecules in the solution. At higher energy, only relatively minor, but salt-specific changes in the spectra occur. The small magnitude of the observed spectral changes is ascribed to offsetting perturbations by the cations and anions.

Measurement and calculation of characteristic prompt gamma ray spectra emitted during proton irradiation

Energy Technology Data Exchange (ETDEWEB)

Polf, J C; Peterson, S; Beddar, S [M D Anderson Cancer Center, Univeristy of Texas, Houston, TX 77030 (United States); McCleskey, M; Roeder, B T; Spiridon, A; Trache, L [Cyclotron Institute, Texas A and M University, College Station, TX 77843 (United States)], E-mail: jcpolf@mdanderson.org

2009-11-21

In this paper, we present results of initial measurements and calculations of prompt gamma ray spectra (produced by proton-nucleus interactions) emitted from tissue equivalent phantoms during irradiations with proton beams. Measurements of prompt gamma ray spectra were made using a high-purity germanium detector shielded either with lead (passive shielding), or a Compton suppression system (active shielding). Calculations of the spectra were performed using a model of both the passive and active shielding experimental setups developed using the Geant4 Monte Carlo toolkit. From the measured spectra it was shown that it is possible to distinguish the characteristic emission lines from the major elemental constituent atoms (C, O, Ca) in the irradiated phantoms during delivery of proton doses similar to those delivered during patient treatment. Also, the Monte Carlo spectra were found to be in very good agreement with the measured spectra providing an initial validation of our model for use in further studies of prompt gamma ray emission during proton therapy. (note)

Reconstruction of X-rays spectra of clinical linear accelerators using the generalized simulated annealing method

International Nuclear Information System (INIS)

Manrique, John Peter O.; Costa, Alessandro M.

2016-01-01

The spectral distribution of megavoltage X-rays used in radiotherapy departments is a fundamental quantity from which, in principle, all relevant information required for radiotherapy treatments can be determined. To calculate the dose delivered to the patient who make radiation therapy, are used treatment planning systems (TPS), which make use of convolution and superposition algorithms and which requires prior knowledge of the photon fluence spectrum to perform the calculation of three-dimensional doses and thus ensure better accuracy in the tumor control probabilities preserving the normal tissue complication probabilities low. In this work we have obtained the photon fluence spectrum of X-ray of the SIEMENS ONCOR linear accelerator of 6 MV, using an character-inverse method to the reconstruction of the spectra of photons from transmission curves measured for different thicknesses of aluminum; the method used for reconstruction of the spectra is a stochastic technique known as generalized simulated annealing (GSA), based on the work of quasi-equilibrium statistic of Tsallis. For the validation of the reconstructed spectra we calculated the curve of percentage depth dose (PDD) for energy of 6 MV, using Monte Carlo simulation with Penelope code, and from the PDD then calculate the beam quality index TPR_2_0_/_1_0. (author)

Laboratory characterization of Woelter x-ray optics

International Nuclear Information System (INIS)

Remington, B.A.; Morales, R.I.

1994-04-01

We have conducted an extensive series of characterization measurements of a Woe1ter incidence x-ray microscope. The measurements were carried out on 5% sectors of the Woe1ter x-ray optic in a laboratory utilizing a high brightness, ''point'' x-ray source and fall into two categories. (1) Absolute reflectance measurements as a function of x-ray energy were made with Si(Li) detectors to acquire continuum spectra prior to and after reflecting off the Woe1ter optic. (2) Spatial resolution measurements were made using back-illuminated pinholes or grids imaged onto film or an x-ray CCD camera. The depth of field was mapped out by varying the distance between the Woe1ter optic and the backlit grid

Calculations of magnetic x-ray dichroism in the 3d absorption spectra of rare-earth compounds

NARCIS (Netherlands)

GOEDKOOP, JB; THOLE, BT; VANDERLAAN, G; SAWATZKY, GA; DEGROOT, FMF; FUGGLE, JC; de Groot, Frank|info:eu-repo/dai/nl/08747610X

1988-01-01

We present atomic calculations for the recently discovered magnetic x-ray dichroism (MXD) displayed by the 3d x-ray-absorption spectra of rare-earth compounds. The spectral shapes expected at T=0 K for linear polarization parallel and normal to the local magnetic field is given, together with the

Finite temperature effects on the X-ray absorption spectra of energy related materials

Science.gov (United States)

Pascal, Tod; Prendergast, David

2014-03-01

We elucidate the role of room-temperature-induced instantaneous structural distortions in the Li K-edge X-ray absorption spectra (XAS) of crystalline LiF, Li2SO4, Li2O, Li3N and Li2CO3 using high resolution X-ray Raman spectroscopy (XRS) measurements and first-principles density functional theory calculations within the eXcited electron and Core Hole (XCH) approach. Based on thermodynamic sampling via ab-initio molecular dynamics (MD) simulations, we find calculated XAS in much better agreement with experiment than those computed using the rigid crystal structure alone. We show that local instantaneous distortion of the atomic lattice perturbs the symmetry of the Li 1 s core-excited-state electronic structure, broadening spectral line-shapes and, in some cases, producing additional spectral features. This work was conducted within the Batteries for Advanced Transportation Technologies (BATT) Program, supported by the U.S. Department of Energy Vehicle Technologies Program under Contract No. DE-AC02-05CH11231.

Determining misorientation of graphite grains from the angular dependence of X-ray emission spectra

International Nuclear Information System (INIS)

Belavin, V. V.; Okotrub, A. V.; Bulusheva, L. G.; Kotosonov, A. S.; Vyalykh, D. V.; Molodtsov, S. L.

2006-01-01

Angular-resolved X-ray absorption spectra were measured for pyrolytic graphite samples of various quality. A new approach to determining the misorientation of graphite grains in polycrystalline samples is proposed, which is based on calculations of the angular dependence of the relative intensity of a peak corresponding to the π* state for a normal distribution of grains. The experimental values are used to construct theoretical angular dependences using partial densities of the π* and σ* states determined from the nonempirical calculations for graphite

An analysis of the MO X-ray spectra in U92+-Pb collisions

International Nuclear Information System (INIS)

Schulze, K.; Anton, J.; Sepp, W.-D.; Fricke, B.

1999-01-01

The investigation of quasimolecular X-rays from superheavy collision systems with bare or H-like projectiles seems to be a promising approach to get information about the behaviour of inner shell electrons with energy eigenvalues in the vicinity of the negative continuum. We present calculations of the MO X-ray spectra for the system U 92+ -Pb for varying impact energies. Furthermore we analyse the contributions due to electrons in higher lying states. The results are discussed with respect to the experimental determination of the transition energies in the superheavy quasimolecule. (orig.)

Resonant X-ray Raman scattering for Al, Si and their oxides

International Nuclear Information System (INIS)

Szlachetko, J.; Berset, M.; Dousse, J.-Cl.; Fennane, K.; Szlachetko, M.; Barrett, R.; Hoszowska, J.; Kubala-Kukus, A.; Pajek, M.

2005-01-01

High-resolution measurements of the resonant X-ray Raman scattering (RRS) of Al and Si and their oxides were performed at the European Synchrotron Radiation Facility (ESRF) in Grenoble, France, using a von Hamos Bragg-type curved crystal spectrometer. To probe the influence of chemical effects on the RRS X-ray spectra, Al 2 O 3 and SiO 2 samples were also investigated. The X-ray RRS spectra were measured at different photon beam energies tuned below the K-absorption edge. The measured spectra are compared to results of RRS calculations based on the second-order perturbation theory within the Kramers-Heisenberg approach

Measurement of X-ray emission efficiency for K-lines.

Science.gov (United States)

Procop, M

2004-08-01

Results for the X-ray emission efficiency (counts per C per sr) of K-lines for selected elements (C, Al, Si, Ti, Cu, Ge) and for the first time also for compounds and alloys (SiC, GaP, AlCu, TiAlC) are presented. An energy dispersive X-ray spectrometer (EDS) of known detection efficiency (counts per photon) has been used to record the spectra at a takeoff angle of 25 degrees determined by the geometry of the secondary electron microscope's specimen chamber. Overall uncertainty in measurement could be reduced to 5 to 10% in dependence on the line intensity and energy. Measured emission efficiencies have been compared with calculated efficiencies based on models applied in standardless analysis. The widespread XPP and PROZA models give somewhat too low emission efficiencies. The best agreement between measured and calculated efficiencies could be achieved by replacing in the modular PROZA96 model the original expression for the ionization cross section by the formula given by Casnati et al. (1982) A discrepancy remains for carbon, probably due to the high overvoltage ratio.

An energy-dispersive X-ray monochromator for measurements in the soft X-ray spectra: design, construction and first measurements. Ein energiedispersiver Roentgenmonochromator mit der Moeglichkeit von Messungen im weichen Roentgenbereich: Entwurf, Aufbau und erste Messungen

Energy Technology Data Exchange (ETDEWEB)

Steil, S.

1993-12-01

An Energy-Dispersive X-ray Monochromator (EDM) for time-resolved X-ray absorption spectroscopy was built in the Synchrotron radiation laboratory at the 3.5 GeV ELectron Stretcher and Accelerator (ELSA). Bragg angles up to 70 and a specially designed vacuum system allow measurements down to an energy of 2.149 keV (P K-edge) with a Si(111)-crystal. Compared to a standard double crystal monochromator and for an EXAFS spectrum at the Cu K-edge at 8.979 keV for concentrated samples, the EDM boosts time resolution by 3 orders of magnitude. The time resolution increases by a factor of 50 for a XANES spectrum at the S K-edge at 2.472 keV for a rubber sample with 4% sulfur. The energy resolution of the EDM is limited by the Darwin width [Omega] of the Bragg crystal. The harmonics in the 'monochromatized' beam, which increase to lower energies, could be nearly eliminated by using a quartz mirror. The spherical aberration of the focus was described theoretically for a cylindrically bent crystal and compared with measurements. In a first time-resolved measurement at the S K-edge, which comprehended about 120 spectra taken in 40 minutes, the thermal ageing of a rubber sample was investigated to demonstrate the performance of the monochromator. (orig.)

Measurement of the energy distribution of parametric X-ray radiation from a double-crystal system

International Nuclear Information System (INIS)

Mori, Akira; Hayakawa, Yasushi; Kidokoro, Akio; Sato, Isamu; Tanaka, Toshinari; Hayakawa, Ken; Kobayashi, Kouji; Ohshima, Hisashi

2006-01-01

A parametric X-ray radiation (PXR) generator system was developed at the Laboratory for Electron Beam Research and Applications (LEBRA) at Nihon University; this PXR generator system is a tunable wavelength and quasi-monochromatic X-ray source constructed as one of the advanced applications of the LEBRA 125-MeV electron linear accelerator. The PXR beam which has characteristic of energy distribution. The theoretical values of energy distribution obtained at the output port were calculated to be approximately 300 eV and 2 keV at the central X-ray energies of 7 keV and 20 keV, respectively. In order to investigate the energy distribution, several measurements of the X-ray energy were carried out. The X-ray absorption of known materials and that of thin aluminum has been evaluated based on analyses of images taken using an imaging plate. The X-ray energy was deduced base on the identification of the absorption edges, and the energy distribution was estimated based on measurements using aluminum step method. In addition, an X-ray diffraction method using a perfect silicon crystal was employed, and spectra were measured using a solid state detector (SSD). The results of these experiments agreed with the calculated results. In particular, the well-defined absorption edges in the X-ray images and the typical rocking curves obtained by the measurement of the X-ray diffraction indicated that the distribution has a high-energy resolution

Measurements of ionic structure in shock compressed lithium hydride from ultrafast x-ray Thomson scattering.

Science.gov (United States)

Kritcher, A L; Neumayer, P; Brown, C R D; Davis, P; Döppner, T; Falcone, R W; Gericke, D O; Gregori, G; Holst, B; Landen, O L; Lee, H J; Morse, E C; Pelka, A; Redmer, R; Roth, M; Vorberger, J; Wünsch, K; Glenzer, S H

2009-12-11

We present the first ultrafast temporally, spectrally, and angularly resolved x-ray scattering measurements from shock-compressed matter. The experimental spectra yield the absolute elastic and inelastic scattering intensities from the measured density of free electrons. Laser-compressed lithium-hydride samples are well characterized by inelastic Compton and plasmon scattering of a K-alpha x-ray probe providing independent measurements of temperature and density. The data show excellent agreement with the total intensity and structure when using the two-species form factor and accounting for the screening of ion-ion interactions.

X-ray spectra from the Cornell Electron-Beam Ion Source (CEBIS I)

International Nuclear Information System (INIS)

Johnson, B.M.; Jones, K.W.; Kostroun, V.O.; Ghanbari, E.; Janson, S.W.

1985-01-01

Radiation emitted from the Cornell electron beam ion source (CEBIS I) has been surveyed with a Si(Li) x-ray detector. These spectra can be used to estimate backgrounds from electron bremsstrahlung and to evaluate the feasibility of atomic physics experiments using the CEBIS I source in this configuration. 1 ref., 2 figs

A model of tungsten anode x-ray spectra

Energy Technology Data Exchange (ETDEWEB)

Hernández, G.; Fernández, F., E-mail: fdz@usal.es [Física Fundamental, Universidad de Salamanca, Salamanca 37008 (Spain)

2016-08-15

Purpose: A semiempirical model for x-ray production in tungsten thick-targets was evaluated using a new characterization of electron fluence. Methods: Electron fluence is modeled taking into account both the energy and angular distributions, each of them adjusted to Monte Carlo simulated data. Distances were scaled by the CSDA range to reduce the energy dependence. Bremsstrahlung production was found by integrating the cross section with the fluence in a 1D penetration model. Characteristic radiation was added using a semiempirical law whose validity was checked. The results were compared the experimental results of Bhat et al., with the SpekCalc numerical tool, and with MCNPX simulation results from the work of Hernandez and Boone. Results: The model described shows better agreement with the experimental results than the SpekCalc predictions in the sense of area between the spectra. A general improvement of the predictions of half-value layers is also found. The results are also in good agreement with the simulation results in the 50–640 keV energy range. Conclusions: A complete model for x-ray production in thick bremsstrahlung targets has been developed, improving the results of previous works and extending the energy range covered to the 50–640 keV interval.

Interpretation of magnetic circular dichroism of X-ray emission spectra

International Nuclear Information System (INIS)

Takayama, Yasuhiro; Yoshida, Tetsuo; Nakamura, Satoshi; Sasaki, Naoya; Ishii, Hiroyoshi; Miyahara, Tsuneaki

2006-01-01

We have measured the dependence of the magnetic circular dichroism (MCD) of the X-ray emission spectra (XES) on the temperature and incident angle for a Gd thin film. The energy of the incident photon for the XES was 138.25eV, which corresponded to the resonant excitation to the 8 D 9/2 intermediate state. The dependence of the observed MCD on the temperature and incident angle was quite different from that of the magnetic moment estimated with a SQUID magnetometer. By considering the reflection, saturation effect, self-absorption effect and magnetic anisotropy of the thin film, the agreement of the two behaviors was considerably improved. This result shows that the revisions of the MCD of the XES are extremely important for the quantitative estimation of the magnetic moment from the MCD of the XES. (author)

X-Ray Spectra from MHD Simulations of Accreting Black Holes

Science.gov (United States)

Schnittman, Jeremy D.; Krolik, Julian H.; Noble, Scott C.

2012-01-01

We present the results of a new global radiation transport code coupled to a general relativistic magneto-hydrodynamic simulation of an accreting, nonrotating black hole. For the first time, we are able to explain from first principles in a self-consistent way the X-ray spectra observed from stellar-mass black holes, including a thermal peak, Compton reflection hump, power-law tail, and broad iron line. Varying only the mass accretion rate, we are able to reproduce the low/hard, steep power-law, and thermal-dominant states seen in most galactic black hole sources. The temperature in the corona is T(sub e) 10 keV in a boundary layer near the disk and rises smoothly to T(sub e) greater than or approximately 100 keV in low-density regions far above the disk. Even as the disk's reflection edge varies from the horizon out to approximately equal to 6M as the accretion rate decreases, we find that the shape of the Fe Ka line is remarkably constant. This is because photons emitted from the plunging region are strongly beamed into the horizon and never reach the observer. We have also carried out a basic timing analysis of the spectra and find that the fractional variability increases with photon energy and viewer inclination angle, consistent with the coronal hot spot model for X-ray fluctuations.

Determination of Al concentration in Al doped ZnO using Auger spectra excited by Mo X-rays

International Nuclear Information System (INIS)

Toth, J.; Koever, L.; Cserny, I.; Varga, D.

2006-01-01

Complete text of publication follows. A good conductor with excellent transparency is of crucial importance for the window layer of CIGS solar cells. Al doped ZnO is a good candidate for this purpose, its conductivity depends on the concentration and chemical state of the Al dopant atoms. It was demonstrated that the non-conventional XPS using Mo X-rays for excitation is a very sensitive tool for the detection of Al, P, Si [1, 2, 3]. The present paper compares the experimental ratios for Zn/Al photoinduced peak intensity ratios obtained using both Al and Mo X-ray excitations. The Mo excited Zn/Al intensity ratios can be determined with higher selectivity and sensitivity than the Zn/Al intensity ratios excited by Al X-rays. The experiments were performed with a hemispherical deflector electron spectrometer [4]. The chemical state of the Al was identified to be close to that in Al 2 O 3 . The atomic concentrations were determined using a calibration curve based on ZnO/Al samples with known composition of Al. The energy dependent efficiency of the electron spectrometer was determined comparing REELS spectra of Cu specimen to standard spectra measured by K. Goto (Nagoya Institute of Technology, Japan). For evaluation of the Al atomic concentrations from the measured photoelectron intensities the photoionisation cross-sections of Band et al [5] and the IMFP data of S. Tanuma et al [6] and C.J. Powell and A. Jablonski [7] were used. (author)

Monte Carlo derivation of filtered tungsten anode X-ray spectra for dose computation in digital mammography*

Science.gov (United States)

Paixão, Lucas; Oliveira, Bruno Beraldo; Viloria, Carolina; de Oliveira, Marcio Alves; Teixeira, Maria Helena Araújo; Nogueira, Maria do Socorro

2015-01-01

Objective Derive filtered tungsten X-ray spectra used in digital mammography systems by means of Monte Carlo simulations. Materials and Methods Filtered spectra for rhodium filter were obtained for tube potentials between 26 and 32 kV. The half-value layer (HVL) of simulated filtered spectra were compared with those obtained experimentally with a solid state detector Unfors model 8202031-H Xi R/F & MAM Detector Platinum and 8201023-C Xi Base unit Platinum Plus w mAs in a Hologic Selenia Dimensions system using a direct radiography mode. Results Calculated HVL values showed good agreement as compared with those obtained experimentally. The greatest relative difference between the Monte Carlo calculated HVL values and experimental HVL values was 4%. Conclusion The results show that the filtered tungsten anode X-ray spectra and the EGSnrc Monte Carlo code can be used for mean glandular dose determination in mammography. PMID:26811553

Monte Carlo derivation of filtered tungsten anode X-ray spectra for dose computation in digital mammography

Directory of Open Access Journals (Sweden)

Lucas Paixão

2015-12-01

Full Text Available Abstract Objective: Derive filtered tungsten X-ray spectra used in digital mammography systems by means of Monte Carlo simulations. Materials and Methods: Filtered spectra for rhodium filter were obtained for tube potentials between 26 and 32 kV. The half-value layer (HVL of simulated filtered spectra were compared with those obtained experimentally with a solid state detector Unfors model 8202031-H Xi R/F & MAM Detector Platinum and 8201023-C Xi Base unit Platinum Plus w mAs in a Hologic Selenia Dimensions system using a direct radiography mode. Results: Calculated HVL values showed good agreement as compared with those obtained experimentally. The greatest relative difference between the Monte Carlo calculated HVL values and experimental HVL values was 4%. Conclusion: The results show that the filtered tungsten anode X-ray spectra and the EGSnrc Monte Carlo code can be used for mean glandular dose determination in mammography.

Optically detected X-ray absorption spectroscopy measurements as a means of monitoring corrosion layers on copper.

Science.gov (United States)

Dowsett, Mark G; Adriaens, Annemie; Jones, Gareth K C; Poolton, Nigel; Fiddy, Steven; Nikitenko, Sergé

2008-11-15

XANES and EXAFS information is conventionally measured in transmission through the energy-dependent absorption of X-rays or by observing X-ray fluorescence, but secondary fluorescence processes, such as the emission of electrons and optical photons (e.g., 200-1000 nm), can also be used as a carrier of the XAS signatures, providing complementary information such as improved surface specificity. Where the near-visible photons have a shorter range in a material, the data will be more surface specific. Moreover, optical radiation may escape more readily than X-rays through liquid in an environmental cell. Here, we describe a first test of optically detected X-ray absorption spectroscopy (ODXAS) for monitoring electrochemical treatments on copper-based alloys, for example, heritage metals. Artificially made corrosion products deposited on a copper substrate were analyzed in air and in a 1% (w/v) sodium sesquicarbonate solution to simulate typical conservation methods for copper-based objects recovered from marine environments. The measurements were made on stations 7.1 and 9.2 MF (SRS Daresbury, UK) using the mobile luminescence end station (MoLES), supplemented by XAS measurements taken on DUBBLE (BM26 A) at the ESRF. The ODXAS spectra usually contain fine structure similar to that of XAS spectra measured in X-ray fluorescence. Importantly, for the compounds examined, the ODXAS is significantly more surface specific, and >98% characteristic of thin surface layers of 0.5-1.5-microm thickness in cases where X-ray measurements are dominated by the substrate. However, EXAFS and XANES from broadband optical measurements are superimposed on a high background due to other optical emission modes. This produces statistical fluctuations up to double what would be expected from normal counting statistics because the data retain the absolute statistical fluctuation in the original raw count, while losing up to 70% of their magnitude when background is removed. The problem may be

A method of measuring gold nanoparticle concentrations by x-ray fluorescence for biomedical applications

Energy Technology Data Exchange (ETDEWEB)

Wu Di; Li Yuhua; Wong, Molly D.; Liu Hong [Center for Bioengineering and School of Electrical and Computer Engineering, University of Oklahoma, Norman, Oklahoma 73019 (United States)

2013-05-15

Purpose: This paper reports a technique that enables the quantitative determination of the concentration of gold nanoparticles (GNPs) through the accurate detection of their fluorescence radiation in the diagnostic x-ray spectrum. Methods: Experimentally, x-ray fluorescence spectra of 1.9 and 15 nm GNP solutions are measured using an x-ray spectrometer, individually and within chicken breast tissue samples. An optimal combination of excitation and emission filters is determined to segregate the fluorescence spectra at 66.99 and 68.80 keV from the background scattering. A roadmap method is developed that subtracts the scattered radiation (acquired before the insertion of GNP solutions) from the signal radiation acquired after the GNP solutions are inserted. Results: The methods effectively minimize the background scattering in the spectrum measurements, showing linear relationships between GNP solutions from 0.1% to 10% weight concentration and from 0.1% to 1.0% weight concentration inside a chicken breast tissue sample. Conclusions: The investigation demonstrated the potential of imaging gold nanoparticles quantitatively in vivo for in-tissue studies, but future studies will be needed to investigate the ability to apply this method to clinical applications.

Broadband X-ray spectra of the ultraluminous X-ray source Holmberg IX X-1 observed with NuSTAR, XMM-Newton, and Suzaku

Energy Technology Data Exchange (ETDEWEB)

Walton, D. J.; Harrison, F. A.; Grefenstette, B. W.; Fuerst, F.; Madsen, K. K.; Rana, V.; Stern, D. [Space Radiation Laboratory, California Institute of Technology, Pasadena, CA 91125 (United States); Miller, J. M. [Department of Astronomy, University of Michigan, 500 Church Street, Ann Arbor, MI 48109-1042 (United States); Bachetti, M.; Barret, D.; Webb, N. [Universite de Toulouse, UPS-OMP, IRAP, Toulouse (France); Boggs, S. E.; Craig, W. W. [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Christensen, F. E. [DTU Space, National Space Institute, Technical University of Denmark, Elektrovej 327, DK-2800 Lyngby (Denmark); Fabian, A. C.; Parker, M. L. [Institute of Astronomy, University of Cambridge, Madingley Road, Cambridge CB3 0HA (United Kingdom); Hailey, C. J. [Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Ptak, A.; Zhang, W. W., E-mail: dwalton@srl.caltech.edu [NASA Goddard Space Flight Center, Greenbelt, MD 20771 (United States)

2014-09-20

We present results from the coordinated broadband X-ray observations of the extreme ultraluminous X-ray source Holmberg IX X-1 performed by NuSTAR, XMM-Newton, and Suzaku in late 2012. These observations provide the first high-quality spectra of Holmberg IX X-1 above 10 keV to date, extending the X-ray coverage of this remarkable source up to ∼30 keV. Broadband observations were undertaken at two epochs, between which Holmberg IX X-1 exhibited both flux and strong spectral variability, increasing in luminosity from L {sub X} = (1.90 ± 0.03) × 10{sup 40} erg s{sup –1} to L {sub X} = (3.35 ± 0.03) × 10{sup 40} erg s{sup –1}. Neither epoch exhibits a spectrum consistent with emission from the standard low/hard accretion state seen in Galactic black hole binaries, which would have been expected if Holmberg IX X-1 harbors a truly massive black hole accreting at substantially sub-Eddington accretion rates. The NuSTAR data confirm that the curvature observed previously in the 3-10 keV bandpass does represent a true spectral cutoff. During each epoch, the spectrum appears to be dominated by two optically thick thermal components, likely associated with an accretion disk. The spectrum also shows some evidence for a nonthermal tail at the highest energies, which may further support this scenario. The available data allow for either of the two thermal components to dominate the spectral evolution, although both scenarios require highly nonstandard behavior for thermal accretion disk emission.

Time-resolved suprathermal x-rays

International Nuclear Information System (INIS)

Lee, P.H.Y.; Rosen, M.D.

1978-01-01

Temporally resolved x-ray spectra in the range of 1 to 20 keV have been obtained from gold disk targets irradiated by 1.06 μm laser pulses from the Argus facility. The x-ray streak camera used for the measurement has been calibrated for streak speed and dynamic range by using an air-gap Fabry-Perot etalon, and the instrument response has been calibrated using a multi-range monoenergetic x-ray source. The experimental results indicate that we are able to observe the ''hot'' x-ray temperature evolve in time and that the experimentally observed values can be qualitatively predicted by LASNEX code computations when the inhibited transport model is used

Precise material identification method based on a photon counting technique with correction of the beam hardening effect in X-ray spectra

International Nuclear Information System (INIS)

Kimoto, Natsumi; Hayashi, Hiroaki; Asahara, Takashi; Mihara, Yoshiki; Kanazawa, Yuki; Yamakawa, Tsutomu; Yamamoto, Shuichiro; Yamasaki, Masashi; Okada, Masahiro

2017-01-01

The aim of our study is to develop a novel material identification method based on a photon counting technique, in which the incident and penetrating X-ray spectra are analyzed. Dividing a 40 kV X-ray spectra into two energy regions, the corresponding linear attenuation coefficients are derived. We can identify the materials precisely using the relationship between atomic number and linear attenuation coefficient through the correction of the beam hardening effect of the X-ray spectra. - Highlights: • We propose a precise material identification method to be used as a photon counting system. • Beam hardening correction is important, even when the analysis is applied to the short energy regions in the X-ray spectrum. • Experiments using a single probe-type CdTe detector were performed, and Monte Carlo simulation was also carried out. • We described the applicability of our method for clinical diagnostic X-ray imaging in the near future.

Local moments and electronic correlations in Fe-based Heusler alloys: Kα x-ray emission spectra measurements

International Nuclear Information System (INIS)

Svyazhin, Artem; Kurmaev, Ernst; Shreder, Elena; Shamin, Sergey; Sahle, Christoph J.

2016-01-01

Heusler alloys are a property-rich class of materials, intensively investigated today from both theoretical and real-world application points of view. In this paper, we attempt to shed light on the role of electronic correlations in the Fe_2MeAl group (where Me represents all 3d elements from Ti to Ni) of Heusler alloys. For this purpose, we have investigated the local moments of iron by means of the x-ray emission spectroscopy technique. To obtain numerical values of local moments, the Kα-FWHM method has been employed for the first time. In every compound of the group, the presence of a local moment on the Fe atom was detected. As has been revealed, the values of these moments are temperature-independent, pointing to an insufficiency of a pure itinerant approach to magnetism in these alloys. We also comprehensively compare the usage of Kβ main lines and Kα spectra as tools for the probing of local moments and point out the significant advantages of the latter. - Highlights: • Local spin moments of iron in Fe_2MeAl (Me = Ti … Ni) Heusler alloys were investigated by means of x-ray emission spectroscopy. • Independence of the local moments from temperature confirms their localized nature. • A local moment value of iron in Fe_2MeAl raises with the atomic number of element Me. • The applicability of the Kα x-ray emission line for extracting local moment values of 3d elements was established.

Parallel of semi-empirical results simulated by MCNP of X-ray spectra with a semiconductor

International Nuclear Information System (INIS)

Santos, L.R.; Vivolo, V.; Potiens, M.P.A.; Navarro, M.V.T.; Santos, W.S.

2016-01-01

The aim of this study was to use the MCNPX radiation transport code to simulate X-ray spectra generated by a constant voltage system in a CdTe semiconductor detector. As part of the validation process, we obtained a series of experimental spectra. Comparatively, in all cases there is a good correlation between the two spectra. There were no statistically significant differences between the experimental results with the simulated. (author)

Observation of soft X-ray spectra from a Seyfert 1 and a narrow emission-line galaxy

International Nuclear Information System (INIS)

Singh, K.P.; Garmire, G.P.; Nousek, J.

1985-01-01

The 0.2-40 keV X-ray spectra of the Seyfert 1 galaxy Mrk 509 and the narrow emission-line galaxy NGC 2992 are analyzed. The results suggest the presence of a steep soft X-ray component in Mrk 509 in addition to the well-known Gamma = 1.7 component found in other active galactic nuclei in the 2-40 keV energy range. The soft X-ray component is interpreted as due to thermal emission from a hot gas, probably associated with the highly ionized gas observed to be outflowing from the galaxy. The X-ray spectrum of NGC 2992 does not show any steepening in the soft X-ray band and is consistent with a single power law (Gamma = 1.78) with very low absorbing column density of 4 x 10 to the 21st/sq cm. A model with partial covering of the nuclear X-ray source is preferred, however, to a simple model with a single power law and absorption. 34 references

A New High-sensitivity solar X-ray Spectrophotometer SphinX:early operations and databases

Science.gov (United States)

Gburek, Szymon; Sylwester, Janusz; Kowalinski, Miroslaw; Siarkowski, Marek; Bakala, Jaroslaw; Podgorski, Piotr; Trzebinski, Witold; Plocieniak, Stefan; Kordylewski, Zbigniew; Kuzin, Sergey; Farnik, Frantisek; Reale, Fabio

The Solar Photometer in X-rays (SphinX) is an instrument operating aboard Russian CORONAS-Photon satellite. A short description of this unique instrument will be presented and its unique capabilities discussed. SphinX is presently the most sensitive solar X-ray spectrophotometer measuring solar spectra in the energy range above 1 keV. A large archive of SphinX mea-surements has already been collected. General access to these measurements is possible. The SphinX data repositories contain lightcurves, spectra, and photon arrival time measurements. The SphinX data cover nearly continuously the period since the satellite launch on January 30, 2009 up to the end-of November 2009. Present instrument status, data formats and data access methods will be shown. An overview of possible new science coming from SphinX data analysis will be discussed.

Diagnostic X-ray spectrometry using a commercial CdZnTe detector

International Nuclear Information System (INIS)

Becker, P.H.B.

1998-01-01

X ray spectrometry using Ge or Si detectors is an established tool to measure characterization parameters of X-ray beams. This work describes how a commercial CdZnTe was used to perform diagnostic X-ray spectrometry. Spectra were measured for two X-ray machines and compared with similar data found in the literature with an agreement of 2% rms

SphinX MEASUREMENTS OF THE 2009 SOLAR MINIMUM X-RAY EMISSION

OpenAIRE

Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Kuzin, S.; Farnik, F.; Reale, F.; Phillips, K. J. H.; Bakala, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B.

2012-01-01

The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 x 10^47 cm^-3 and 1.1 x 10^48 cm^-3. Comparing Sph...

Measurement of central nickel density in Doublet III plasmas with a soft x-ray diode array

International Nuclear Information System (INIS)

Groebner, R.J.; Jahns, G.L.; Ejima, S.; Hsieh, C.L.

1985-01-01

An array of soft x-ray diodes has been used to obtain central nickel densities for discharges in the Doublet III tokamak, during operation with an inconel primary limiter, in which nickel L-line radiation dominated the diode signals. The nature of the diode signals is determined primarily by comparison with soft x-ray spectra. The contribution of the continuum portion of the spectra to the central diode signal can be calculated and compared to the observed signal. When the diode signal is dominated by nickel L-line emission, the observed signal is considerably larger than the calculated continuum contribution. Chordal data from the array of diodes are inverted to provide the spatial profile of soft x-ray emission. Because the diodes are absolute detectors of radiation, the soft x-ray emission profile is used to obtain the absolute nickel concentration and density profile in the center of the plasma. A computer code, including over 100 nickel L-line transitions, has been developed to obtain the nickel density. The nickel L-line cooling rate, calculated with the code, is presented. The nickel density obtained by this technique agrees well with that obtained from the K/sub α/ line intensity measured with a soft x-ray spectrometer and that obtained from a bolometric measurement of central radiated power coupled with a coronal equilibrium model of the radiation

X-ray photoelectron and x-ray-induced Auger electron spectroscopic data, 1

International Nuclear Information System (INIS)

Baba, Yuji; Sasaki, T.A.

1984-02-01

The intrinsic data of the X-ray photoelectron spectra (XPS) and X-ray-induced Auger electron spectra (XAES) for 3d transition-metals and related oxides were presented. The clean surfaces of the metals were obtained by two different methods ; mechanical filings and Ar + ion etchings. The oxides examined are typical compounds such as Sc 2 O 3 , TiO 2 , V 2 O 5 and NiO. The report consists of 4 wide scans, 26 core-line spectra, 10 valence-band spectra and 20 XAES spectra. The peak positions of the core-lines and the Auger lines were summarized in 8 tables together with their chemical shifts. (author)

X-ray imaging and spectroscopic measurements of implosions

International Nuclear Information System (INIS)

Hammel, B.A.; Ress, D.R.; Keane, C.J.; Kilkenny, J.D.; Landen, O.L.; Bell, P.; Pasha, R.; Wallace, R.J.; Bradley, D.K.

1992-01-01

Time-resolved x-ray measurements are essential in the investigation of laser-driven inertial confinement fusion, where neutron and x-ray emission are the only observable signatures of the compressed core conditions. High-speed detectors, available for x-ray measurement, provide a means of measuring the rapidly evolving conditions in imploding capsules on picosecond time scales. We address a wide range of issues in our indirectly driven implosion experiments on Nova, with a large variety of x-ray measurement techniques. Critical issues include symmetry of the compressed core, fuel density and temperature and hydrodynamic mix at the pusher/fuel interface

Effective Energy Determination Of Radiodiagnostic X-Rays

International Nuclear Information System (INIS)

Sumarni; Mart, Terry

2000-01-01

X-rays have been used for diagnostic radiology to produce image on film that give anatomy information. Effective energy should be known to get benefit exposure. Half value layer (HVL) as shown as monoenergetic x-rays has similar spectra of energy x-rays. It has been done measurement with x-ray machine Tanka at P3KRBIN-Batan for 40 kVp to 119 kVp of potential found of Aluminium HVL are 0.115 cm to 0.385 cm and energy effective between 23.24 keV to 37.5 keV

A new X-ray pinhole camera for energy dispersive X-ray fluorescence imaging with high-energy and high-spatial resolution

Energy Technology Data Exchange (ETDEWEB)

Romano, F.P., E-mail: romanop@lns.infn.it [IBAM, CNR, Via Biblioteca 4, 95124 Catania (Italy); INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy); Altana, C. [INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy); Dipartimento di Fisica e Astronomia, Università di Catania, Via S. Sofia 64, 95123 Catania (Italy); Cosentino, L.; Celona, L.; Gammino, S.; Mascali, D. [INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy); Pappalardo, L. [IBAM, CNR, Via Biblioteca 4, 95124 Catania (Italy); INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy); Rizzo, F. [INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy); Dipartimento di Fisica e Astronomia, Università di Catania, Via S. Sofia 64, 95123 Catania (Italy)

2013-08-01

A new X-ray pinhole camera for the Energy Dispersive X-ray Fluorescence (ED-XRF) imaging of materials with high-energy and high-spatial resolution, was designed and developed. It consists of a back-illuminated and deep depleted CCD detector (composed of 1024 × 1024 pixels with a lateral size of 13 μm) coupled to a 70 μm laser-drilled pinhole-collimator, positioned between the sample under analysis and the CCD. The X-ray pinhole camera works in a coaxial geometry allowing a wide range of magnification values. The characteristic X-ray fluorescence is induced on the samples by irradiation with an external X-ray tube working at a maximum power of 100 W (50 kV and 2 mA operating conditions). The spectroscopic capabilities of the X-ray pinhole camera were accurately investigated. Energy response and energy calibration of the CCD detector were determined by irradiating pure target-materials emitting characteristic X-rays in the energy working-domain of the system (between 3 keV and 30 keV). Measurements were performed by using a multi-frame acquisition in single-photon counting. The characteristic X-ray spectra were obtained by an automated processing of the acquired images. The energy resolution measured at the Fe–Kα line is 157 eV. The use of the X-ray pinhole camera for the 2D resolved elemental analysis was investigated by using reference-patterns of different materials and geometries. The possibility of the elemental mapping of samples up to an area of 3 × 3 cm{sup 2} was demonstrated. Finally, the spatial resolution of the pinhole camera was measured by analyzing the profile function of a sharp-edge. The spatial resolution determined at the magnification values of 3.2 × and 0.8 × (used as testing values) is about 90 μm and 190 μm respectively. - Highlights: • We developed an X-ray pinhole camera for the 2D X-ray fluorescence imaging. • X-ray spectra are obtained by a multi-frame acquisition in single photon mode. • The energy resolution in the X-ray

A color display device recording X ray spectra, especially intended for medical radiography

International Nuclear Information System (INIS)

Boulch, J.-M.

1975-01-01

Said invention relates to a color display recording device for X ray spectra intended for medical radiography. The video signal of the X ray camera receiving the radiation having passed through the patient is amplified and transformed into a color coding according to the energy spectrum received by the camera. In a first version, the energy spectrum from the camera gives directly an image on the color tube. In a second version the energy spectrum, after having been transformed into digital signals, is first sent into a memory, then into a computer used as a spectrum analyzer, and finally into the color display device [fr

Core-hole effects in the x-ray-absorption spectra of transition-metal silicides

NARCIS (Netherlands)

WEIJS, PJW; CZYZYK, MT; VANACKER, JF; SPEIER, W; GOEDKOOP, JB; VANLEUKEN, H; HENDRIX, HJM; DEGROOT, RA; VANDERLAAN, G; BUSCHOW, KHJ; WIECH, G; FUGGLE, JC

1990-01-01

We report systematic differences between the shape of the Si K x-ray-absorption spectra of transition-metal silicides and broadened partial densities of Si p states. We use a variety of calculations to show that the origin of these discrepancies is the core-hole potential appropriate to the final

Soft X-ray scanning transmission X-ray microscopy (STXM) of actinide particles.

Science.gov (United States)

Nilsson, Hans J; Tyliszczak, Tolek; Wilson, Richard E; Werme, Lars; Shuh, David K

2005-09-01

A descriptive account is given of our most recent research on the actinide dioxides with the Advanced Light Source Molecular Environmental Science (ALS-MES) Beamline 11.0.2 soft X-ray scanning transmission X-ray microscope (STXM) at the Lawrence Berkeley National Laboratory (LBNL). The ALS-MES STXM permits near-edge X-ray absorption fine structure (NEXAFS) and imaging with 30-nm spatial resolution. The first STXM spectromicroscopy NEXAFS spectra at the actinide 4d5/2 edges of the imaged transuranic particles, NpO2 and PuO2, have been obtained. Radiation damage induced by the STXM was observed in the investigation of a mixed oxidation state particle (Np(V,VI)) and was minimized during collection of the actual spectra at the 4d5/2 edge of the Np(V,VI) solid. A plutonium elemental map was obtained from an irregular PuO2 particle with the dimensions of 650 x 650 nm. The Pu 4d5/2 NEXAFS spectra were collected at several different locations from the PuO2 particle and were identical. A representative oxygen K-edge spectrum from UO2 was collected and resembles the oxygen K-edge from the bulk material. The unique and current performance of the ALS-MES STXM at extremely low energies (ca. 100 eV) that may permit the successful measurement of the actinide 5d edge is documented. Finally, the potential of STXM as a tool for actinide investigations is briefly discussed.

Analysis of the X-ray emission spectra of copper, germanium and rubidium plasmas produced at the Phelix laser facility

Science.gov (United States)

Comet, M.; Pain, J.-C.; Gilleron, F.; Piron, R.; Denis-Petit, D.; Méot, V.; Gosselin, G.; Morel, P.; Hannachi, F.; Gobet, F.; Tarisien, M.; Versteegen, M.

2017-03-01

We present the analysis of X-ray emission spectra of copper, germanium and rubidium plasmas measured at the Phelix laser facility. The laser intensity was around 6×1014 W.cm-2. The analysis is based on the hypothesis of an homogeneous plasma in local thermodynamic equilibrium using an effective temperature. This temperature is deduced from hydrodynamic simulations and collisional-radiative computations. Spectra are then calculated using the LTE opacity codes OPAMCDF and SCO-RCG and compared to experimental data.

X-ray Spectra of Distant Clusters

Science.gov (United States)

Ellingson, E.

1998-01-01

The masses of galaxy clusters are dominated by dark matter, and a robust determination of their temperatures and masses has the potential of indicating how much dark matter exists on large scales in the universe, and the cosmological parameter Omega. X-ray observations of galaxy clusters provide a direct measure of both the gas mass in the intra-cluster medium, and also the total gravitating mass of the cluster. We used new and archival ASCA and ROSAT observations to measure these quantities for a sample of intermediate redshift clusters which have also been subject to intensive dynamical studies, in order to compare the mass estimates from different methods. We used data from 12 of the CNOC cluster sample at 0.18 less than z less than 0.55 for this study. A direct comparison of dynamical mass estimates from Carlberg, Yee & Ellingson (1997) yielded surprisingly good results. The X-ray/dynamical mass ratios have a mean of 0.96+/- 0.10, indicating that for this sample, both methods are probably yielding very robust mass estimates. Comparison with mass estimates from gravitational lensing studies from the literature showed a small systematic with weak lensing estimates, and large discrepancies with strong lensing estimates. This latter is not surprising, given that these measurements are made close to the central core, where optical and Xray estimates are less certain, and where substructure and the effects of individual galaxies will be more pronounced. These results are presented in Lewis, Ellingson, Morris \\& Carlberg, 1998, submitted to the Astrophysical Journal.

Energy spectrum measurement of high power and high energy(6 and 9 MeV) pulsed x-ray source for industrial use

Energy Technology Data Exchange (ETDEWEB)

Takagi, Hiroyuki [Hitachi, Ltd. Power Systems Company, Ibaraki (Japan); Murata, Isao [Graduate School of Engineering, Osaka University, Osaka (Japan)

2016-06-15

Industrial X-ray CT system is normally applied to non-destructive testing (NDT) for industrial product made from metal. Furthermore there are some special CT systems, which have an ability to inspect nuclear fuel assemblies or rocket motors, using high power and high energy (more than 6 MeV) pulsed X-ray source. In these case, pulsed X-ray are produced by the electron linear accelerator, and a huge number of photons with a wide energy spectrum are produced within a very short period. Consequently, it is difficult to measure the X-ray energy spectrum for such accelerator-based X-ray sources using simple spectrometry. Due to this difficulty, unexpected images and artifacts which lead to incorrect density information and dimensions of specimens cannot be avoided in CT images. For getting highly precise CT images, it is important to know the precise energy spectrum of emitted X-rays. In order to realize it we investigated a new approach utilizing the Bayesian estimation method combined with an attenuation curve measurement using step shaped attenuation material. This method was validated by precise measurement of energy spectrum from a 1 MeV electron accelerator. In this study, to extend the applicable X-ray energy range we tried to measure energy spectra of X-ray sources from 6 and 9 MeV linear accelerators by using the recently developed method. In this study, an attenuation curves are measured by using a step-shaped attenuation materials of aluminum and steel individually, and the each X-ray spectrum is reconstructed from the measured attenuation curve by the spectrum type Bayesian estimation method. The obtained result shows good agreement with simulated spectra, and the presently developed technique is adaptable for high energy X-ray source more than 6 MeV.

A sample cell to study hydrate formation with x-ray scattering

International Nuclear Information System (INIS)

Conrad, Heiko; Lehmkuehler, Felix; Sternemann, Christian; Feroughi, Omid; Tolan, Metin; Simonelli, Laura; Huotari, Simo

2009-01-01

We present a new sample cell for measuring nonresonant inelastic x-ray scattering spectra of a tetrahydrofuran (THF)-water liquid mixture and THF hydrate. The hydrate is formed inside the cell after nucleation seeds have been offered by a special magnetic stirring mechanism. Hydrate formation was verified by wide angle x-ray scattering and nonresonant x-ray Raman scattering spectra at the oxygen K-edge. A broad range of scattering angles can be studied with this cell which is necessary for momentum transfer dependent inelastic x-ray scattering. This cell is ideal to examine other liquid hydrate formers or other liquid samples, which have to be mixed in situ during the measurements.

Study of soft X-ray energy spectra from gas-puff Z-pinch plasma

International Nuclear Information System (INIS)

Zou Xiaobing; Wang Xinxin; Zhang Guixin; Han Min; Luo Chengmu

2006-01-01

A ROSS-FILTER-PIN spectrometer in the spectral range of 0.28 keV-1.56 keV was developed to study the soft X-ray radiation emitted from gas-puff Z-pinch plasma. It is composed of five channels covering the energy interval of interest without gaps. Soft X-ray spectral energy cuts were determined by the L absorption edges of selected filter elements (K absorption edges being used for light filter elements), and the optimum thickness of filter material was designed using computer code. To minimize the residual sensitivity outside the sensitivity range of each channel, element of the first filter was added into the second filter of all the Ross pair. To diminish the area of each filter, PIN detector with small sensitive area of 1 mm 2 was adopted for the spectrometer. A filter with small area is easy to fabricate and would be helpful to withstand the Z-pinch discharge shock wave. With this ROSS-FILTER-PIN spectrometer, the energy spectra of soft X-ray from a small gas-puff Z-pinch were investigated, and the correlation between the soft X-ray yield and the plasma implosion state was also studied. (authors)

LABORATORY MEASUREMENTS COMPELLINGLY SUPPORT A CHARGE-EXCHANGE MECHANISM FOR THE “DARK MATTER” ∼3.5 keV X-Ray LINE

Energy Technology Data Exchange (ETDEWEB)

Shah, Chintan; Dobrodey, Stepan; Bernitt, Sven; Steinbrügge, René; López-Urrutia, José R. Crespo [Max-Planck-Institut für Kernphysik, Heidelberg, D-69117 Heidelberg (Germany); Gu, Liyi; Kaastra, Jelle [SRON Netherlands Institute for Space Research, Sorbonnelaan 2, 3584 CA, Utrecht (Netherlands)

2016-12-10

The reported observations of an unidentified X-ray line feature at ∼3.5 keV have driven a lively discussion about its possible dark matter origin. Motivated by this, we have measured the K-shell X-ray spectra of highly ionized bare sulfur ions following charge exchange with gaseous molecules in an electron beam ion trap, as a source of or a contributor to this X-ray line. We produced S{sup 16+} and S{sup 15+} ions and let them capture electrons in collision with those molecules with the electron beam turned off while recording X-ray spectra. We observed a charge-exchange-induced X-ray feature at the Lyman series limit (3.47 ± 0.06 keV). The inferred X-ray energy is in full agreement with the reported astrophysical observations and supports the novel scenario proposed by Gu et al.

Some complementary results to the granularity of industrial X-ray films

International Nuclear Information System (INIS)

Stade, J.

1987-01-01

The granularity of industrial x-ray films was examined by measurements of the Wiener spectra. The dependence of the Weiner spectra on film density, type of film, type of developer, energy of the exposing x-radiation, and light exposure, was also investigated. The results revealed that the Weiner spectrum or related quantities were suitable as a tool for measuring the influence of different radiographic parameters on the x-ray film, as well as to characterize its properties. (UK)

Flash X-Ray (FXR) Accelerator Optimization Electronic Time-Resolved Measurement of X-Ray Source Size

International Nuclear Information System (INIS)

Jacob, J; Ong, M; Wargo, P

2005-01-01

Lawrence Livermore National Laboratory (LLNL) is currently investigating various approaches to minimize the x-ray source size on the Flash X-Ray (FXR) linear induction accelerator in order to improve x-ray flux and increase resolution for hydrodynamic radiography experiments. In order to effectively gauge improvements to final x-ray source size, a fast, robust, and accurate system for measuring the spot size is required. Timely feedback on x-ray source size allows new and improved accelerator tunes to be deployed and optimized within the limited run-time constraints of a production facility with a busy experimental schedule; in addition, time-resolved measurement capability allows the investigation of not only the time-averaged source size, but also the evolution of the source size, centroid position, and x-ray dose throughout the 70 ns beam pulse. Combined with time-resolved measurements of electron beam parameters such as emittance, energy, and current, key limiting factors can be identified, modeled, and optimized for the best possible spot size. Roll-bar techniques are a widely used method for x-ray source size measurement, and have been the method of choice at FXR for many years. A thick bar of tungsten or other dense metal with a sharp edge is inserted into the path of the x-ray beam so as to heavily attenuate the lower half of the beam, resulting in a half-light, half-dark image as seen downstream of the roll-bar; by measuring the width of the transition from light to dark across the edge of the roll-bar, the source size can be deduced. For many years, film has been the imaging medium of choice for roll-bar measurements thanks to its high resolution, linear response, and excellent contrast ratio. Film measurements, however, are fairly cumbersome and require considerable setup and analysis time; moreover, with the continuing trend towards all-electronic measurement systems, film is becoming increasingly difficult and expensive to procure. Here, we shall

A measurement-based X-ray source model characterization for CT dosimetry computations.

Science.gov (United States)

Sommerville, Mitchell; Poirier, Yannick; Tambasco, Mauro

2015-11-08

The purpose of this study was to show that the nominal peak tube voltage potential (kVp) and measured half-value layer (HVL) can be used to generate energy spectra and fluence profiles for characterizing a computed tomography (CT) X-ray source, and to validate the source model and an in-house kV X-ray dose computation algorithm (kVDoseCalc) for computing machine- and patient-specific CT dose. Spatial variation of the X-ray source spectra of a Philips Brilliance and a GE Optima Big Bore CT scanner were found by measuring the HVL along the direction of the internal bow-tie filter axes. Third-party software, Spektr, and the nominal kVp settings were used to generate the energy spectra. Beam fluence was calculated by dividing the integral product of the spectra and the in-air NIST mass-energy attenuation coefficients by in-air dose measurements along the filter axis. The authors found the optimal number of photons to seed in kVDoseCalc to achieve dose convergence. The Philips Brilliance beams were modeled for 90, 120, and 140 kVp tube settings. The GE Optima beams were modeled for 80, 100, 120, and 140 kVp tube settings. Relative doses measured using a Capintec Farmer-type ionization chamber (0.65 cc) placed in a cylindrical polymethyl methacrylate (PMMA) phantom and irradiated by the Philips Brilliance, were compared to those computed with kVDoseCalc. Relative doses in an anthropomorphic thorax phantom (E2E SBRT Phantom) irradiated by the GE Optima were measured using a (0.015 cc) PTW Freiburg ionization chamber and compared to computations from kVDoseCalc. The number of photons required to reduce the average statistical uncertainty in dose to measurement over all 12 PMMA phantom positions was found to be 1.44%, 1.47%, and 1.41% for 90, 120, and 140 kVp, respectively. The maximum percent difference between calculation and measurement for all energies, measurement positions, and phantoms was less than 3.50%. Thirty-five out of a total of 36 simulation conditions were

Measurement of anisotropic soft X-ray emission during radio-frequency current drive in the JFT-2M tokamak

International Nuclear Information System (INIS)

Kawashima, Hisato; Matoba, Tohru; Hoshino, Katsumichi; Kawakami, Tomohide; Yamamoto, Takumi; Hasegawa, Mitsuru; Fuchs, Gerhard; Uesugi, Yoshihiko.

1994-01-01

A new vertical soft X-ray pulse height analyzer (PHA) system and a tangential PHA system were used to measure the anisotropy of soft X-ray emission during lower-hybrid current drive (LHCD) and also during current drive by the combination of LHCD and electron cyclotron resonance heating (ECRH) in the JFT-2M tokamak. The strong soft X-ray emission was measured in the parallel forward direction during LHCD. When ECRH was applied during LHCD, the perpendicular emission was enhanced. The high-energy electron velocity distribution was evaluated by comparing the measured and calculated X-ray spectra. The distribution form was consistent with the theoretical prediction based on the electron Landau damping of lower-hybrid waves and the electron cyclotron damping of electron cyclotron waves for reasonable energy ranges. (author)

Spectra transmitted by mortar barite in X-Ray qualities applied in diagnostic radiology as shielding

Energy Technology Data Exchange (ETDEWEB)

Almeida Junior, Airton T., E-mail: airton.almeida@fundacentro.gov.br [Fundacaoo Jorge Duprat Figueiredo de Seguranca e Medicina do Trabalho (FUNDACENTRO), Belo Horizonte, MG (Brazil); Araujo, F.G.S. [Universidade Federal de Ouro Preto (REDEMAT/UFOP), MG (Brazil); Nogueira, M.S., E-mail: mnogue@cdtn.br [Centro de Desenvolvimento da Tecnologia Nuclear (CDTN/CNEN-MG), Belo Horizonte, MG (Brazil); Santos, M.A.P. [Centro Regional de Ciencias Nucleares do Nordeste (CRCN-NE/CNEN-PE), Recife, PE (Brazil)

2015-07-01

Concrete which contains water, cement and aggregate, is widely used in building construction such as medical hospitals. The CdZnTe spectrometry system was used to acquire the transmitted spectra in the RQR qualities and the stripping procedure was performed by taking into account both the contributions of efficiency and x-ray escape fraction, experimentally determined. The samples were prepared in rectangular plate format with dimensions of (5 x 5) cm with thicknesses varying from 0.2cm to 2cm and exposed to x-ray beams generated. The HVL and the mean energy in this energy range was determined. (author)

SphinX MEASUREMENTS OF THE 2009 SOLAR MINIMUM X-RAY EMISSION

International Nuclear Information System (INIS)

Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Bakała, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B.; Kuzin, S.; Farnik, F.; Reale, F.; Phillips, K. J. H.

2012-01-01

The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 × 10 47 cm –3 and 1.1 × 10 48 cm –3 . Comparing SphinX emission with that from the Hinode X-ray Telescope, we deduce that most of the emission is from general coronal structures rather than confined features like bright points. For one of 27 intervals of exceptionally low activity identified in the SphinX data, the Sun's X-ray luminosity in an energy range roughly extrapolated to that of ROSAT (0.1-2.4 keV) was less than most nearby K and M dwarfs.

SphinX Measurements of the 2009 Solar Minimum X-Ray Emission

Science.gov (United States)

Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Kuzin, S.; Farnik, F.; Reale, F.; Phillips, K. J. H.; Bakała, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B.

2012-06-01

The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 × 1047 cm-3 and 1.1 × 1048 cm-3. Comparing SphinX emission with that from the Hinode X-ray Telescope, we deduce that most of the emission is from general coronal structures rather than confined features like bright points. For one of 27 intervals of exceptionally low activity identified in the SphinX data, the Sun's X-ray luminosity in an energy range roughly extrapolated to that of ROSAT (0.1-2.4 keV) was less than most nearby K and M dwarfs.

SphinX MEASUREMENTS OF THE 2009 SOLAR MINIMUM X-RAY EMISSION

Energy Technology Data Exchange (ETDEWEB)

Sylwester, J.; Kowalinski, M.; Gburek, S.; Siarkowski, M.; Bakala, J.; Gryciuk, M.; Podgorski, P.; Sylwester, B. [Space Research Centre, Polish Academy of Sciences, 51-622, Kopernika 11, Wroclaw (Poland); Kuzin, S. [P. N. Lebedev Physical Institute (FIAN), Russian Academy of Sciences, Leninsky Prospect 53, Moscow 119991 (Russian Federation); Farnik, F. [Astronomical Institute, Ondrejov Observatory (Czech Republic); Reale, F. [Dipartimento di Fisica, Universita di Palermo, Palermo, Italy, and INAF, Osservatorio Astronomico di Palermo, Palermo (Italy); Phillips, K. J. H., E-mail: js@cbk.pan.wroc.pl [Mullard Space Science Laboratory, University College London, Holmbury St. Mary, Dorking, Surrey RH5 6NT (United Kingdom)

2012-06-01

The SphinX X-ray spectrophotometer on the CORONAS-PHOTON spacecraft measured soft X-ray emission in the 1-15 keV energy range during the deep solar minimum of 2009 with a sensitivity much greater than GOES. Several intervals are identified when the X-ray flux was exceptionally low, and the flux and solar X-ray luminosity are estimated. Spectral fits to the emission at these times give temperatures of 1.7-1.9 MK and emission measures between 4 Multiplication-Sign 10{sup 47} cm{sup -3} and 1.1 Multiplication-Sign 10{sup 48} cm{sup -3}. Comparing SphinX emission with that from the Hinode X-ray Telescope, we deduce that most of the emission is from general coronal structures rather than confined features like bright points. For one of 27 intervals of exceptionally low activity identified in the SphinX data, the Sun's X-ray luminosity in an energy range roughly extrapolated to that of ROSAT (0.1-2.4 keV) was less than most nearby K and M dwarfs.

Measurement of keV-neutron capture cross sections and capture gamma-ray spectra of Er isotopes

International Nuclear Information System (INIS)

Harun-Ar-Rashid, A.K.M.; Igashira, Masayuki; Ohsaki, Toshiro

2000-01-01

Neutron capture cross sections and capture γ-ray spectra of 166,167, 168 Er were measured in the energy region of 10 to 550 keV. The measurements were performed with a pulsed 7 Li(p,n) 7 Be neutron source and a large anti-Compton NaI(Tl) γ-ray spectrometer. A pulse-height weighting technique and the standard capture cross sections of gold were used to derive the capture cross sections. The errors of the derived cross sections were about 5%. The present results were compared with other measurements and evaluations. The observed capture γ-ray pulse-height spectra were unfolded to obtain the corresponding γ-ray spectra. An anomalous shoulder was observed around 3 MeV in each of the capture γ-ray spectra. (author)

Correcting X-ray spectra obtained from the AXAF VETA-I mirror calibration for pileup, continuum, background and deadtime

Science.gov (United States)

Chartas, G.; Flanagan, K.; Hughes, J. P.; Kellogg, E. M.; Nguyen, D.; Zombek, M.; Joy, M.; Kolodziejezak, J.

1993-01-01

The VETA-I mirror was calibrated with the use of a collimated soft X-ray source produced by electron bombardment of various anode materials. The FWHM, effective area and encircled energy were measured with the use of proportional counters that were scanned with a set of circular apertures. The pulsers from the proportional counters were sent through a multichannel analyzer that produced a pulse height spectrum. In order to characterize the properties of the mirror at different discrete photon energies one desires to extract from the pulse height distribution only those photons that originated from the characteristic line emission of the X-ray target source. We have developed a code that fits a modeled spectrum to the observed X-ray data, extracts the counts that originated from the line emission, and estimates the error in these counts. The function that is fitted to the X-ray spectra includes a Prescott function for the resolution of the detector a second Prescott function for a pileup peak and a X-ray continuum function. The continuum component is determined by calculating the absorption of the target Bremsstrahlung through various filters, correcting for the reflectivity of the mirror and convolving with the detector response.

SpekCalc: a program to calculate photon spectra from tungsten anode x-ray tubes

International Nuclear Information System (INIS)

Poludniowski, G; Evans, P M; Landry, G; DeBlois, F; Verhaegen, F

2009-01-01

A software program, SpekCalc, is presented for the calculation of x-ray spectra from tungsten anode x-ray tubes. SpekCalc was designed primarily for use in a medical physics context, for both research and education purposes, but may also be of interest to those working with x-ray tubes in industry. Noteworthy is the particularly wide range of tube potentials (40-300 kVp) and anode angles (recommended: 6-30 deg.) that can be modelled: the program is therefore potentially of use to those working in superficial/orthovoltage radiotherapy, as well as diagnostic radiology. The utility is free to download and is based on a deterministic model of x-ray spectrum generation (Poludniowski 2007 Med. Phys. 34 2175). Filtration can be applied for seven materials (air, water, Be, Al, Cu, Sn and W). In this note SpekCalc is described and illustrative examples are shown. Predictions are compared to those of a state-of-the-art Monte Carlo code (BEAMnrc) and, where possible, to an alternative, widely-used, spectrum calculation program (IPEM78). (note)

Hard X-ray studies on the Castor tokamak

International Nuclear Information System (INIS)

Mlynar, J.

1990-04-01

The electron runaway processes in tokamaks are discussed with regard to hard X radiation measurements. The origin and confinement of runaway electrons, their bremsstrahlung spectra and the influence of lower hybrid current drive on the distribution of high-energy electrons are analyzed for the case of the Castor tokamak. The hard X-ray spectrometer designed for the Castor tokamak is also described and preliminary qualitative results of hard X-ray measurements are presented. The first series of integral measurements made it possible to map the azimuthal dependence of the hard X radiation

Restricted active space calculations of L-edge X-ray absorption spectra: from molecular orbitals to multiplet states.

Science.gov (United States)

Pinjari, Rahul V; Delcey, Mickaël G; Guo, Meiyuan; Odelius, Michael; Lundberg, Marcus

2014-09-28

The metal L-edge (2p → 3d) X-ray absorption spectra are affected by a number of different interactions: electron-electron repulsion, spin-orbit coupling, and charge transfer between metal and ligands, which makes the simulation of spectra challenging. The core restricted active space (RAS) method is an accurate and flexible approach that can be used to calculate X-ray spectra of a wide range of medium-sized systems without any symmetry constraints. Here, the applicability of the method is tested in detail by simulating three ferric (3d(5)) model systems with well-known electronic structure, viz., atomic Fe(3+), high-spin [FeCl6](3-) with ligand donor bonding, and low-spin [Fe(CN)6](3-) that also has metal backbonding. For these systems, the performance of the core RAS method, which does not require any system-dependent parameters, is comparable to that of the commonly used semi-empirical charge-transfer multiplet model. It handles orbitally degenerate ground states, accurately describes metal-ligand interactions, and includes both single and multiple excitations. The results are sensitive to the choice of orbitals in the active space and this sensitivity can be used to assign spectral features. A method has also been developed to analyze the calculated X-ray spectra using a chemically intuitive molecular orbital picture.

Time-resolved x-ray line diagnostics of laser-produced plasmas

International Nuclear Information System (INIS)

Kauffman, R.L.; Matthews, D.L.; Kilkenny, J.D.; Lee, R.W.

1982-11-01

We have examined the underdense plasma conditions of laser irradiated disks using K x-rays from highly ionized ions. A 900 ps laser pulse of 0.532 μm light is used to irradiate various Z disks which have been doped with low concentrations of tracer materials. The tracers, whose Z's range from 13 to 22, are chosen so that their K x-ray spectrum is sensitive to typical underdense plasma temperatures and densities. Spectra are measured using a time-resolved crystal spectrograph recording the time history of the x-ray spectrum. A spatially-resolved, time-integrated crystal spectrograph also monitors the x-ray lines. Large differences in Al spectra are observed when the host plasms is changed from SiO 2 to PbO or In. Spectra will be presented along with preliminary analysis of the data

Time-resolved x-ray line diagnostics of laser-produced plasmas

International Nuclear Information System (INIS)

Kauffman, R.L.; Matthews, D.L.; Kilkenny, J.D.; Lee, R.W.

1982-01-01

We have examined the underdense plasma conditions of laser irradiated disks using K x-rays from highly ionized ions. A 900 ps laser pulse of 0.532 μm light is used to irradiate various Z disks which have been doped with low concentrations of tracer materials. The tracers whose Z's range from 13 to 22 are chosen so that their K x-ray spectrum is sensitive to typical underdense plasma temperatures and densities. Spectra are measured using a time-resolved crystal spectrograph recording the time history of the x-ray spectrum. A spatially-resolved, time-integrated crystal spectrograph also monitors the x-ray lines. Large differences in Al spectra are observed when the host plasma is changed from SiO 2 to PbO or In. Spectra will be presented along with preliminary analysis of the data

On The Utilization of (1-X)Cu-X Pb) Alloys for Gamma-Rays Shielding

International Nuclear Information System (INIS)

Abd El-Latif, A.A.; Saeid, Kh.S.; Abd El-Latif, A.A.

2011-01-01

The present work deals with the study of the attenuation properties of gamma rays for [(1-X) Cu -X Pb] alloys where, x=10%, 20%, 30%, and 40% Pb waste by weight. Investigation has been performed by measuring the transmitted gamma ray spectra behind cylindrical samples of [(1-X) Cu - X Pb] alloys of different thicknesses. A collimated beam of gamma ray measured by using γ - ray spectrometer NaI(Tl) Scintillation detector with multichannel analyzer (MCA) cassy. Total mass attenuation coefficients (μ/ρ) of γ-ray have been evaluated and calculated using measured results and XCOM code respectively . Comparison between measured and calculated results shows a reasonable divergence at 0.511 MeV ,and 0.662 MeV γ-ray energies, in addition there is a convergence at 1.17 MeV, 1.274 MeV, and 1.3 MeV γ-ray energies

The Soft X-ray Spectrophotometer SphinX for the CORONAS-Photon Mission

Science.gov (United States)

Sylwester, Janusz; Kowalinski, Miroslaw; Szymon, Gburek; Bakala, Jaroslaw; Kuzin, Sergey; Kotov, Yury; Farnik, Frantisek; Reale, Fabio

The purpose, construction details and calibration results of the new design, Polish-led solar X-ray spectrophotometer SphinX will be presented. The instrument constitutes a part of the Russian TESIS X-ray and EUV complex aboard the forthcoming CORONAS-Photon solar mission to be launched later in 2008. SphinX uses Si-PIN detectors for high time resolution (down to 0.01 s) measurements of solar spectra in the energy range between 0.5 keV and 15 keV. The spectral resolution allows separating 256 individual energy channels in this range with particular groups of lines clearly distinguishable. Unprecedented accuracy of the instrument calibration at the XACT (Palermo) and BESSY (Berlin) synchrotron will allow for establishing the solar soft X-ray photometric reference system. The cross-comparison between SphinX and the other instruments presently in orbit like XRT on Hinode, RHESSI and GOES X-ray monitor, will allow for a precise determination of the coronal emission measure and temperature during both very low and very high activity periods. Examples of the detectors' ground calibration results as well as the calculated synthetic spectra will be presented. The operation of the instrument while in orbit will be discussed allowing for suggestions from other groups to be still included in mission planning.

Measurement of conversion coefficients between air Kerma and personal dose equivalent and backscatter factors for diagnostic X-ray beams

International Nuclear Information System (INIS)

Rosado, Paulo Henrique Goncalves

2008-01-01

Two sets of quantities are import in radiological protection: the protection and operational quantities. Both sets can be related to basic physical quantities such as kerma through conversion coefficients. For diagnostic x-ray beams the conversion coefficients and backscatter factors have not been determined yet, those parameters are need for calibrating dosimeters that will be used to determine the personal dose equivalent or the entrance skin dose. Conversion coefficients between air kerma and personal dose equivalent and backscatter factors were experimentally determined for the diagnostic x-ray qualities RQR and RQA recommended by the International Electrotechnical Commission (IEC). The air kerma in the phantom and the mean energy of the spectrum were measured for such purpose. Harshaw LiF-100H thermoluminescent dosemeters (TLD) were used for measurements after being calibrated against an 180 cm 3 Radcal Corporation ionization chamber traceable to a reference laboratory. A 300 mm x 300 mm x 150 mm polymethylmethacrylate (PMMA) slab phantom was used for deep-dose measurements. Tl dosemeters were placed in the central axis of the x-ray beam at 5, 10, 15, 25 and 35 mm depth in the phantom upstream the beam direction Another required parameter for determining the conversion coefficients from was the mean energy of the x-ray spectrum. The spectroscopy of x-ray beams was done with a CdTe semiconductor detector that was calibrated with 133 Ba, 241 Am and 57 Co radiation sources. Measurements of the x-ray spectra were carried out for all RQR and RQA IEC qualities. Corrections due to the detector intrinsic efficiency, total energy absorption, escape fraction of the characteristic x-rays, Compton effect and attenuation in the detector were done aiming an the accurate determination of the mean energy. Measured x-ray spectra were corrected with the stripping method by using these response functions. The typical combined standard uncertainties of conversion coefficients and

Simultaneous acquisition of X-ray spectra using a multi-wire, position-sensitive gas flow detector

International Nuclear Information System (INIS)

Beaven, Peter A.; Marmotti, Mauro; Kampmann, Reinhard; Knoth, Joachim; Schwenke, Heinrich

2003-01-01

A multi-wire, gas-filled position-sensitive detector has been developed for the simultaneous recording of wavelength-dispersed X-ray signals that enables X-ray fluorescence spectrometry with a limited multi-element capability in the low Z element range. Details of the modular construction of the detector are given. The detector performance was characterized using Al-Kα radiation and a variable slit system. The detector has been applied in a laboratory spectrometer equipped with an electron source and a double multilayer mirror device as the wavelength-dispersing element. Spectra from Al and Si obtained in the simultaneous acquisition mode show good agreement with calculations performed using a ray-tracing model

Pulsator-like Spectra from Ultraluminous X-Ray Sources and the Search for More Ultraluminous Pulsars

International Nuclear Information System (INIS)

Pintore, F.; Mereghetti, S.; Zampieri, L.; Stella, L.; Israel, G. L.; Wolter, A.

2017-01-01

Ultraluminous X-ray sources (ULXs) are a population of extragalactic objects whose luminosity exceeds the Eddington limit for a 10 M ⊙ black hole (BH). Their properties have been widely interpreted in terms of accreting stellar-mass or intermediate-mass BHs. However at least three neutron stars (NSs) have been recently identified in ULXs through the discovery of periodic pulsations. Motivated by these findings we studied the spectral properties of a sample of bright ULXs using a simple continuum model which was extensively used to fit the X-ray spectra of accreting magnetic NSs in the Galaxy. We found that such a model, consisting of a power-law with a high-energy exponential cut-off, fits most of the ULX spectra analyzed here very well, at a level comparable to that of models involving an accreting BH. On these grounds alone we suggest that other non-pulsating ULXs may host NSs. We also found that above 2 keV the spectrum of known pulsating ULXs is harder than that of the majority of the other ULXs of the sample, with only IC 342 X-1 and Ho IX X-1 displaying spectra of comparable hardness. We thus suggest that these two ULXs may host an accreting NS and encourage searches for periodic pulsations in the flux.

Pulsator-like Spectra from Ultraluminous X-Ray Sources and the Search for More Ultraluminous Pulsars

Energy Technology Data Exchange (ETDEWEB)

Pintore, F.; Mereghetti, S. [INAF-IASF Milano, via E. Bassini 15, I-20133 Milano (Italy); Zampieri, L. [INAF-Osservatorio Astronomico di Padova, Vicolo dell’Osservatorio 5, I-35122 Padova (Italy); Stella, L.; Israel, G. L. [INAF—Osservatorio astronomico di Roma, Via Frascati 44, I-00078, Monteporzio Catone (Italy); Wolter, A. [INAF, Osservatorio Astronomico di Brera, via Brera 28, I-20121 Milano (Italy)

2017-02-10

Ultraluminous X-ray sources (ULXs) are a population of extragalactic objects whose luminosity exceeds the Eddington limit for a 10 M {sub ⊙} black hole (BH). Their properties have been widely interpreted in terms of accreting stellar-mass or intermediate-mass BHs. However at least three neutron stars (NSs) have been recently identified in ULXs through the discovery of periodic pulsations. Motivated by these findings we studied the spectral properties of a sample of bright ULXs using a simple continuum model which was extensively used to fit the X-ray spectra of accreting magnetic NSs in the Galaxy. We found that such a model, consisting of a power-law with a high-energy exponential cut-off, fits most of the ULX spectra analyzed here very well, at a level comparable to that of models involving an accreting BH. On these grounds alone we suggest that other non-pulsating ULXs may host NSs. We also found that above 2 keV the spectrum of known pulsating ULXs is harder than that of the majority of the other ULXs of the sample, with only IC 342 X-1 and Ho IX X-1 displaying spectra of comparable hardness. We thus suggest that these two ULXs may host an accreting NS and encourage searches for periodic pulsations in the flux.

Spectrometry of X-ray beams using Cadmium and Zinc Teluride detector

International Nuclear Information System (INIS)

Becker, Paulo Henriques Bastos

1997-06-01

Determination of X-ray spectra to be utilized for medical diagnostics is a complementary process to the development of procedures to be applied to the quality control of radiodiagnostics X-ray equipment. Until some years ago, that was only possible using Germanium or Silicon detectors. Both have an excellent resolution in this energy range, but present also some restrictions as there are high costs and the necessity of operating them at temperature of liquid Nitrogen, which is not always available at the measurement's place. Room temperature detectors like Cadmium Telluride and Mercury Iodine don't have these restrictions. They, however, have a lower resolution and incomplete collection of the charges produced by their interaction with radiation. With technological advance of crystal growth in general and new techniques like cooling the crystal with a Peltier cell and rise time discrimination circuits, today Cadmium Telluride detectors show a resolution very close to that from Germanium detectors. This work relates to the routine use of Cadmium and Zinc Telluride detectors for measuring X-ray spectra in loco of diagnostic X-ray units. It characterizes the properties of a commercially available detector and offers a model for stripping the measured pulse height distribution. It was also developed a collimator to allow the direct measurement of the beam. The model developed and the constructed set-up were applied to two X-ray tubes and the achieved spectra compared with some spectra available from the literature. (author)

Reflectivity around the gold L-edges of X-ray reector of the soft X-ray telescope onboard ASTRO-H

DEFF Research Database (Denmark)

Maeda, Yoshitomo; Kikuchi, Naomichi; Kurashima, Sho

2017-01-01

We report the atomic scattering factor in the 11.2-15.4 keV for the ASTRO-H Soft X-ray Telescope (SXT)9 obtained in the ground based measurements. The large effective area of the SXT covers above 10 keV. In fact, the flight data show the spectra of the celestical objects in the hard X-ray band. I...

ROSAT Energy Spectra of Low-Mass X-Ray Binaries

Science.gov (United States)

Schulz, N. S.

1999-01-01

The 0.1-2.4 keV bandpass of the ROSAT Position Sensitive Proportional Counter (PSPC) offers an opportunity to study the very soft X-ray continuum of bright low-mass X-ray binaries (LMXBs). In 46 pointed observations, 23 LMXBs were observed with count rates between 0.4 and 165.4 counts s-1. The survey identified a total of 29 different luminosity levels, which are compared with observations and identified spectral states from other missions. The atoll source 4U 1705-44 was observed near Eddington luminosities in an unusually high intensity state. Spectral analysis provided a measure of the interstellar column density for all 49 observations. The sensitivity of spectral fits depends strongly on column density. Fits to highly absorbed spectra are merely insensitive toward any particular spectral model. Sources with column densities well below 1022 cm-2 are best fitted by power laws, while the blackbody model gives clearly worse fits to the data. Most single-component fits from sources with low column densities, however, are not acceptable at all. The inclusion of a blackbody component in eight sources can improve the fits significantly. The obtained emission radii of less than 5 km suggest emission from the neutron star surface. In 10 sources acceptable fits can only be achieved by including soft-line components. With a spectral resolution of the PSPC of 320-450 eV, between 0.6 and 1.2 keV unresolved broad-line features were detected around 0.65, 0.85, and 1.0 keV. The line fluxes range within 10-11 and 10-12 ergs cm-2 s-1, with equivalent widths between 24 and 210 eV. In LMC X-2, 2S 0918-549, and 4U 1254-690, line emission is indicated for the first time. The soft emission observed in 4U 0614+091 compares with recent ASCA results, with a new feature indicated at 1.31 keV. The deduced line fluxes in 4U 1820-30 and Cyg X-2 showed variability of a factor of 2 within timescales of 1-2 days. Average fluxes of line components in 4U 1820-30 varied by the same factor over a

A mirror for lab-based quasi-monochromatic parallel x-rays.

Science.gov (United States)

Nguyen, Thanhhai; Lu, Xun; Lee, Chang Jun; Jung, Jin-Ho; Jin, Gye-Hwan; Kim, Sung Youb; Jeon, Insu

2014-09-01

A multilayered parabolic mirror with six W/Al bilayers was designed and fabricated to generate monochromatic parallel x-rays using a lab-based x-ray source. Using this mirror, curved bright bands were obtained in x-ray images as reflected x-rays. The parallelism of the reflected x-rays was investigated using the shape of the bands. The intensity and monochromatic characteristics of the reflected x-rays were evaluated through measurements of the x-ray spectra in the band. High intensity, nearly monochromatic, and parallel x-rays, which can be used for high resolution x-ray microscopes and local radiation therapy systems, were obtained.

Experimental setup for x-ray absorption spectroscopy at the DESY

International Nuclear Information System (INIS)

Rabe, P.; Tolkiehn, G.; Werner, A.

1979-10-01

In this paper we describe an apparatus used at the Deutsches Elektronen-Synchrotron (DESY) for the measurement of x-ray absorption spectra, specially designed for the investigation of the extended x-ray absorption fine structure (EXAFS). Performance of the setup is discussed and compared with an apparatus using the bremsstrahlung of a conventional x-ray source. (orig.)

Solar X-rays from Axions: Rest-Mass Dependent Signatures

CERN Document Server

Zioutas, Konstantin; Semertzidis, Yannis; Papaevangelou, Thomas; Gardikiotis, Antonios; Dafni, Theopisti; Anastassopoulos, Vassilis

2010-01-01

The spectral shape of solar X-rays is a power law. The more active the Sun is, the less steep the distribution. This behaviour can be explained by axion regeneration to X-rays occurring ~400km deep into the photosphere. Their down-comptonization reproduces the measured spectral shape, pointing at axions with rest mass m_a~17 meV/c2, without contradicting astrophysical-laboratory limits. Directly measured soft X-ray spectra from the extremely quiet Sun during 2009 (SphinX mission), though hitherto overlooked, fitt the axion scenario.

CHARGE-TRANSFER SATELLITES AND MULTIPLET SPLITTING IN X-RAY PHOTOEMISSION SPECTRA OF LATE TRANSITION-METAL HALIDES

NARCIS (Netherlands)

OKADA, K; KOTANI, A; THOLE, BT

1992-01-01

Core-level X-ray photoemission spectra (XPS) are calculated for Ni and Co dihalides with an MX6 cluster model (M = Ni, Co; X = F, Cl, Br), where intra-atomic multiplet coupling as well as covalency mixing is taken into account. The effects of the intra-atomic configuration interaction between

Spectra of γ-rays from capture of 2 eV to 9 x 104 eV neutrons by 181Ta

International Nuclear Information System (INIS)

Stelts, M.L.

Using new experimental techniques, the spectra of γ-rays from the capture of neutrons by 181 Ta were measured at the Livermore 100-MeV linac for neutrons from 2 eV to 9 x 10 4 eV with a (Ge(Li)-NaI) three-crystal spectrometer. Individual primary γ-ray lines were resolved to 1778-keV excitation in 182 Ta. Neutron resonances were resolved to 200-eV neutron energy. Data analysis techniques and codes were developed to extract positions and intensities of resolved transitions from the large data matrices accumulated in this experiment. Techniques were developed to unfold the unresolved γ-ray spectra using the simple response of the three-crystal spectrometer. The resolved transition data were used to place 110 states with spin and parity assignments in the 182 Ta level diagram below 1780-keV excitation. A set of 1240 E1 transition strengths were analyzed to extract 1.38 +- 0.11 degrees of freedom for the most likely chisquared fit to the distribution of widths. The E1 strength function was extracted for E/sub gamma/ = 4 to 6 MeV and compared with previous results. The γ-ray spectra for E/sub gamma/ = 1.5 to 6.1 MeV were unfolded for neutron energy groups between 20 and 9 x 10 4 eV. Below 5-MeV γ-ray energy no dependence of the spectral shape on neu []ron energy was observed. (30 figures, 4 tables) (auth)

Photoemission measurements for low energy x-ray detector applications

International Nuclear Information System (INIS)

Day, R.H.

1981-01-01

Photoemission has been studied for nearly 100 years as both a means of investigating quantum physics, and as a practical technique for transducing optical/x-ray photons into electrical currents. Numerous x-ray detection schemes, such as streak cameras and x-ray sensitive diodes, exploit this process because of its simplicity, adaptability, and speed. Recent emphasis on diagnostics for low temperature, high density, and short-lived, plasmas for inertial confinement fusion has stimulated interest in x-ray photoemission in the sub-kilovolt regime. In this paper, a review of x-ray photoemission measurements in the 50 eV to 10 keV x-ray region is given and the experimental techniques are reviewed. A semiempirical model of x-ray photoemission is discussed and compared to experimental measurements. Finally, examples of absolutely calibrated instruments are shown

X-ray measurements of water fog density

International Nuclear Information System (INIS)

Camp, A.L.

1982-11-01

Water-fog densities were measured in a laboratory experiment using x-ray diagnostics. Fog densities were measured, varying the flow rate, nozzle type, nozzle configuration, nozzle height above the x-ray beam, and water surface tension. Suspended water volume fractions between 0.0008 and 0.0074 percent were measured. The fog density increases approximately as the square root of the flow rate; the other parameters had little effect on the density

Measurement of characteristic X-rays by positron impact

International Nuclear Information System (INIS)

Nagashima, Y.; Saito, F.; Itoh, Y.; Goto, A.; Hyodo, T.

2004-01-01

An X-ray detector with thin Si(Li) crystals has been fabricated and employed to detect the characteristic X-rays by positron impact. Use of thin detector crystals is essential for the measurements of the characteristic X-rays induced by positron impact. Otherwise the background produced in the crystals by the annihilation γ-rays is too large to isolate the X-ray peaks. The data has been analyzed to obtain the inner-shell ionization cross sections by positron impact. (orig.)

The MeV spectra of gamma-ray bursts measured with COMPTEL

International Nuclear Information System (INIS)

Hoover, A.S.; Kippen, R.M.; McConnell, M.L.

2005-01-01

The past decade has produced a wealth of observational data on the energy spectra of prompt emission from gamma-ray bursts. Most of the data cover the energy range from a few to several hundred KeV. One set of higher energy observations comes from the Imaging Compton Telescope COMPTEL on the Compton Observatory, which measured in the energy range from 0.75 to 30 MeV. We analyzed the full 9.2 years COMPTEL data to reveal the significant detection of 44 gamma-ray bursts. We present preliminary results obtained in the process of preparing a final catalog of the spectral analysis of these events. In addiction, we compare the COMPTEL spectra to simultaneous BATSE measurements for purposes of cross-calibration

X-ray imaging with amorphous selenium: Pulse height measurements of avalanche gain fluctuations

International Nuclear Information System (INIS)

Lui, Brian J. M.; Hunt, D. C.; Reznik, A.; Tanioka, K.; Rowlands, J. A.

2006-01-01

Avalanche multiplication in amorphous selenium (a-Se) can provide a large, adjustable gain for active matrix flat panel imagers (AMFPI), enabling quantum noise limited x-ray imaging during both radiography and fluoroscopy. In the case of direct conversion AMFPI, the multiplication factor for each x ray is a function of its depth of interaction, and the resulting variations in gain can reduce the detective quantum efficiency (DQE) of the system. An experimental method was developed to measure gain fluctuations by analyzing images of individual x rays that were obtained using a video camera with an a-Se target operated in avalanche mode. Pulse height spectra (PHS) of the charge produced per x ray were recorded for monoenergetic 30.9, 49.4, and 73.8 keV x-ray sources. The rapid initial decay and long tail of each PHS can be explained by a model in which positive charge dominates the initiation of avalanche. The Swank information factor quantifies the effect of gain fluctuation on DQE and was calculated from the PHS. The information factor was found to be 0.5 for a 25 μm a-Se layer with a maximum gain of ∼300. Changing the energy of the incident x ray influenced the range of the primary photoelectron and noticeably affected the tail of the experimental PHS, but did not significantly change the avalanche Swank factor

Automation of an X-ray photoelectron spectrometer

International Nuclear Information System (INIS)

Ashury, M.R.

2003-02-01

The Institute of Solid State Physics of the Vienna University of Technology is established with an X-ray Photoelectron Spectrometer Kratos XSAM 800. In its original state the instrument enables measurements of photoelectron spectra in a semiautomatical mode. After mounting of the specimen an eventual surface cleaning by argon ion sputtering is possible. Next steps are setting of x-ray tube high voltage and current, start energy and energy range of spectrum and time of measurement. Data are obtained by an x-t plotter and evaluations are performed from the registration charts. If necessary, measured spectra have to be digitized by means of a scanner. In the Introduction of this thesis the principle of X-ray photoelectron spectrometry is treated including a number of practical examples. It shows that an automation allows an extension of the performance of the instrument. Details are remote controlled experiments, wider energy ranges with improved energy resolution. Furthermore, the digitized data treatment enables background subtration, determination of line positions and integrated signal strengths, and is the detection of lowlevel of lines (the peak with lowamplitude) possible. A further advantage is the computer assisted documentation and comparison of results from different specimens. After this description of the essential requirements different possible solutions of an automation are discussed. Thus, it is decided to develop a completely new hardware for a perfect control of the spectrometer. A further decision is to be made on the most efficient kind of micro processor. From the considerations follows a completely new control board with a transputer as multi tasking processor. The complete control unit consists of a digital system, an analog system and a power unit. The digital system controls settings and spectra accumulation and includes the transputer board, the pc-link card, the i/o-card and the step scanning control board. The analog system controls the

Mass attenuation coefficient (μ/ρ), effective atomic number (Zeff) and measurement of x-ray energy spectra using based calcium phosphate biomaterials: a comparative study

International Nuclear Information System (INIS)

Fernandes Z, M. A.; Da Silva, T. A.; Nogueira, M. S.; Goncalves Z, E.

2015-10-01

In dentistry, alveolar bone regeneration procedures using based calcium phosphate biomaterials have been shown effective. However,there are not reports in the literature of studies the interaction of low energy radiation in these biomaterials used as attenuator and not being then allowed a comparison between the theoretical values and experimental.The objective of this study was to determine the interaction of radiation parameters of four dental biomaterials - BioOss, Cerasorb M Dental, Straumann Boneceramic and Osteogen for diagnostic radiology qualities. As a material and methods, the composition of the biomaterials was determined by the analytical techniques. The samples with 0.181 cm to 0,297 cm thickness were experimentally used as attenuators for the measurement of the transmitted X-rays spectra in X-ray equipment with 50 to 90 kV range by spectrometric system comprising the Cd Te detector. After this procedure, the mass attenuation coefficient, the effective atomic number were determined and compared between all the specimens analyzed, using the program WinXCOM in the range of 10 to 200 keV. In all strains examined observed that the energy spectrum of x-rays transmitted through the BioOss has the mean energy slightly smaller than the others biomaterials for close thickness. The μ/ρ and Z eff of the biomaterials showed its dependence on photon energy and atomic number of the elements of the material analyzed. It is concluded according to the methodology employed in this study that the measurements of x-ray spectrum, μ/ρ and Z eff using biomaterials as attenuators confirmed that the thickness, density, composition of the samples, the incident photon energy are factors that determine the characteristics of radiation in a tissue or equivalent material. (Author)

Influence of changes in the valence electronic configuration on the structure of L-X-ray spectra of molybdenum

International Nuclear Information System (INIS)

Polasik, M; Koziol, K; Slabkowska, K; Czarnota, M; Pajek, M

2009-01-01

Extensive multiconfiguration Dirac-Fock (MCDF) calculations with the inclusion of the transverse (Breit) interaction and QED corrections have been carried out on molybdenum to explain the dependence of the structure of Lα 1,2 and Lβ 1 lines on the changes in configurations of the valence electrons belonging to two different configuration types: three open-shell 4d 6-r 5s r (r = 2,1,0) configurations and one closed-shell 4d 4 3/2 5s 2 configuration. It has been found that the MCDF predictions for open-shell valence configurations (4d 4 5s 2 , 4d 5 5s 1 , 4d 6 5s 0 ) much better reproduce observed structure of Lα 1,2 lines in X-ray spectra of molybdenum than closed-shell 4d 4 3/2 5s 2 valence configuration. The influence of changes in the valence electronic configuration on the structure of L-X-ray spectra of molybdenum is noticeable. Moreover, the observation of the shapes of L-X-ray spectra seems to be very good method to investigate the changes of the valence electronic configuration caused by the chemical environment.

Thermoluminescent dosimeters for low dose X-ray measurements

International Nuclear Information System (INIS)

Del Sol Fernández, S.; García-Salcedo, R.; Sánchez-Guzmán, D.; Ramírez-Rodríguez, G.; Gaona, E.; León-Alfaro, M.A. de; Rivera-Montalvo, T.

2016-01-01

The response of TLD-100, CaSO_4:Dy and LiF:Mg,Cu,P for a range of X-ray low dose was measured. For calibration, the TLDs were arranged at the center of the X-ray field. The dose output of the X-ray machine was determined using an ACCU-Gold. All dosimeters were exposed at the available air kerma values of 14.69 mGy within a field 10×10 cm"2 at 80 cm of SSD. Results of LiF:Mg,Cu,P X-ray irradiated showed 4.8 times higher sensitivity than TLD-100. Meanwhile, TL response of CaSO_4:Dy exposed at the same dose was 5.6 time higher than TLD-100. Experimental results show for low dose X-ray measurements a better linearity for LiF:Mg,Cu,P compared with that of TLD-100. CaSO_4:Dy showed a linearity from 0.1 to 60 mGy - Highlights: • Low dose X-ray doses for personal dosimetry were measured. • Radiation dose (µGy ) for environmental dosimetry were determined. • Scattering radiation dose were measured by TLDs. • Linearity of pair TLD system was successful in the range of microgray. • Pair TLDs composed by CaSO_4:Dy and by LiF:Mg,Cu,P. is suggested for clinical dosimetry.

Remote planetary geochemical exploration with the NEAR X-ray/gamma-ray spectrometer

International Nuclear Information System (INIS)

Trombka, J.I.; Boynton, W.V.; Brueckner, J.; Squyres, S.; Clark, P.E.; Starr, R.; Evans, L.G.; Floyd, S.R.; McClanahan, T.P.; Goldsten, J.; Mcnutt, R.; Schweitzer, J.S.

1999-01-01

The X-ray/gamma-ray spectrometer (XGRS) instrument onboard the Near Earth Asteroid Rendezvous (NEAR) spacecraft will map asteroid 433 Eros in the 0.2 keV to 10 MeV energy region. Measurements of the discrete line X-ray and gamma-ray emissions in this energy domain can be used to obtain both qualitative and quantitative elemental composition maps of the asteroid surface. The NEAR X-ray/gamma-ray spectrometer (XGRS) was turned on for the first time during the week of 7 April 1996. Rendezvous with Eros 433 is expected during December 1998. Observations of solar X-ray spectra during both quiescent and active periods have been made. A gamma-ray transient detection system has been implemented and about three gamma-ray transient events a week have been observed which are associated with either gamma-ray bursts or solar flares

Hard X ray lines from neutron stars

Energy Technology Data Exchange (ETDEWEB)

Polcaro, V.F.; Bazzano, A.; La Padula, C.; Ubertini, P.

1982-01-01

Experimental evidence is presented and evaluated concerning the features of the hard X-ray spectra detected in a number of cosmic X-ray sources which contain a neutron star. The strong emission line at cyclotron resonance detected in the spectrum of Her XI at an energy of 58 keV is evaluated and the implications of this finding are discussed. Also examined is the presence of spectral features in the energy range 20-80 keV found in the spectra of gamma-ray bursts, which have been interpreted as cyclotron resonance from interstellar-gas-accreting neutron stars. The less understood finding of a variable emission line at approximately 70 keV in the spectrum of the Crab Pulsar is considered. It is determined that several features varying with time are present in the spectra of cosmic X-ray sources associated with neutron stars. If these features are due to cyclotron resonance, it is suggested that they provide a direct measurement of neutron star magnetic fields on the order of 10 to the 11th-10 to the 13th Gauss. However, the physical condition of the emitting region and its geometry are still quite obscure.

The measurement of X-rays radiation temperature with a new developed filter-fluorescence spectroscopy

International Nuclear Information System (INIS)

Zhang Chuanfei; Lin Libin; Lou Fuhong; Peng Taiping

2001-01-01

The author introduces how to measure the energy spectra of X-rays by filter-fluorescence spectroscopy. The design principle and structure of new-developed double diaphragms and filter-fluorescence spectroscopy with 5 channels are depicted. The parameters of optimized spectroscopy by numerical method are given. The filter-fluorescence spectroscopy designed according as Rousseau balance principle improves signal-noises ratio

New Solar Irradiance Measurements from the Miniature X-Ray Solar Spectrometer Cubesat

Energy Technology Data Exchange (ETDEWEB)

Woods, Thomas N.; Jones, Andrew; Kohnert, Richard; Mason, James Paul; Moore, Christopher S.; Palo, Scott; Rouleau, Colden [University of Colorado, Boulder, CO (United States); Caspi, Amir [Southwest Research Institute, Boulder, CO (United States); Chamberlin, Phillip C. [NASA Goddard Space Flight Center, Greenbelt, MD (United States); Solomon, Stanley C. [National Center for Atmospheric Research, Boulder, CO (United States); Machol, Janet; Viereck, Rodney [NOAA Space Weather Prediction Center, Boulder, CO (United States)

2017-02-01

The goal of the Miniature X-ray Solar Spectrometer ( MinXSS ) CubeSat is to explore the energy distribution of soft X-ray (SXR) emissions from the quiescent Sun, active regions, and during solar flares and to model the impact on Earth's ionosphere and thermosphere. The energy emitted in the SXR range (0.1–10 keV) can vary by more than a factor of 100, yet we have limited spectral measurements in the SXRs to accurately quantify the spectral dependence of this variability. The MinXSS primary science instrument is an Amptek, Inc. X123 X-ray spectrometer that has an energy range of 0.5–30 keV with a nominal 0.15 keV energy resolution. Two flight models have been built. The first, MinXSS -1, has been making science observations since 2016 June 9 and has observed numerous flares, including more than 40 C-class and 7 M-class flares. These SXR spectral measurements have advantages over broadband SXR observations, such as providing the capability to derive multiple-temperature components and elemental abundances of coronal plasma, improved irradiance accuracy, and higher resolution spectral irradiance as input to planetary ionosphere simulations. MinXSS spectra obtained during the M5.0 flare on 2016 July 23 highlight these advantages and indicate how the elemental abundance appears to change from primarily coronal to more photospheric during the flare. MinXSS -1 observations are compared to the Geostationary Operational Environmental Satellite ( GOES ) X-ray Sensor (XRS) measurements of SXR irradiance and estimated corona temperature. Additionally, a suggested improvement to the calibration of the GOES XRS data is presented.

X-ray calorimeters used for measurement in laser-fusion experiments

International Nuclear Information System (INIS)

Tang Daorun; China Academy of Engineering Physics, Mianyang; Wu Dengxue; Lin Libin; Sun Kexu; Jiang Shaoen

2005-01-01

X-ray calorimeters are ready to measure the total soft X-ray energy emitted from the plasma produced by laser because of their bodily absorption, linear response, insensitivity to the electromagnetic disturbance, and so on. The calorimeters mainly include absorbers, thermocouples, bases and shrouds. When X-rays are deposited in the absorbers, photon energy absorbed is quickly converted into intrinsic energy which simultaneously dissipates by thermal conduction and radiation. The X-ray calorimeters were absolutely on-line calibrated in Shenguang-II laser facility with the X-ray diode array spectrometer which has been absolutely calibrated on Beijing Synchrotron Radiation Facility. 20 shots' experimental results show that the X-ray calorimeters are stable, the sensitivity of calorimeter is (84.1 ± 3.4) μv/mJ and the related combined standard uncertainty in the X-ray energy measure is about 31%. The calorimeters can be applied to measure the X-ray energy. (authors)

Measuring the Dust Grains and Distance to X Persei Via Its X-ray Halo

Science.gov (United States)

Smith, Randall

2006-09-01

We propose to observe the X-ray halo of the high mass X-ray binary pulsar X Per to measure interstellar dust grains along the line of sight (LOS) and to determine the distance to X Per. The X-ray halo is formed by scattering from grains along the LOS, which for X Per appear to be concentrated in one molecular cloud. Unlike many other X-ray halo observations, this low-absorption high-latitude sightline is well-characterized from absorption spectroscopy done with HST, Copernicus, and FUSE. This halo observation will measure the distance to the cloud and the dust size distribution in it. We will also be able to determine the distance to X Per by measuring the time delayed pulses in the X-ray halo.

Construction of a catalog of X-ray spectra for mammography simulations

International Nuclear Information System (INIS)

Santos, L.C.S.; Vieira, J.W.

2017-01-01

Computational Exposure Models (MCEs) allow the simulation of the interaction of radiation with matter by means of Monte Carlo (MC) techniques. Generally, MCEs are composed of phantom, simulator algorithms of radioactive sources and an MC code to simulate the transport, interaction of the radiation with matter and to evaluate the energy deposited in regions of interest. To compose an MCE for simulations in mammography, the construction of a catalog of X-ray spectra was started, based on the catalog model constructed and using until then in MCEs by the Group of Research in Numerical Dosimetry and by the Group of Research in Computational Dosimetry & Embedded Systems (both referenced in this work as GDN). Potential of 25 kV and 35 kV and used target / filter were applied to the tube: Mo / Mo. The file containing the spectra was read correctly by EGSnrc

Measurement of high energy x-ray beam penumbra with Gafchromic trade mark sign EBT radiochromic film

International Nuclear Information System (INIS)

Cheung Tsang; Butson, Martin J.; Yu, Peter K. N.

2006-01-01

High energy x-ray beam penumbra are measured using Gafchromic trade mark sign EBT film. Gafchromic trade mark sign EBT, due to its limited energy dependence and high spatial resolution provide a high level of accuracy for dose assessment in penumbral regions. The spatial resolution of film detector systems is normally limited by the scanning resolution of the densitometer. Penumbral widths (80%/20%) measured at D max were found to be 2.8, 3.0, 3.2, and 3.4 mm (±0.2 mm) using 5, 10, 20, and 30 cm square field sizes, respectively, for a 6 MV linear accelerator produced x-ray beam. This is compared to 3.2 mm±0.2 mm (Kodak EDR2) and 3.6 mm±0.2 mm (Kodak X-Omat V) at 10 cmx10 cm measured using radiographic film. Using a zero volume extrapolation technique for ionization chamber measurements, the 10 cmx10 cm field penumbra at D max was measured to be 3.1 mm, a close match to Gafchromic trade mark sign EBT results. Penumbral measurements can also be made at other depths, including the surface, as the film does not suffer significantly from dosimetric variations caused by changing x-ray energy spectra. Gafchromic trade mark sign EBT film provides an adequate measure of penumbral dose for high energy x-ray beams

THE BROADBAND XMM-NEWTON AND NuSTAR X-RAY SPECTRA OF TWO ULTRALUMINOUS X-RAY SOURCES IN THE GALAXY IC 342

Energy Technology Data Exchange (ETDEWEB)

Rana, Vikram; Harrison, Fiona A.; Walton, Dominic J.; Furst, Felix; Grefenstette, Brian W.; Madsen, Kristin K. [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, Pasadena, CA 91125 (United States); Bachetti, Matteo; Barret, Didier; Webb, Natalie A. [Université de Toulouse, UPS-OMP, IRAP, Toulouse (France); Miller, Jon M. [Department of Astronomy, University of Michigan, 500 Church Street, Ann Arbor, MI 48109-1042 (United States); Fabian, Andrew C. [Institute of Astronomy, University of Cambridge, Madingley Road, Cambridge CB3 0HA (United Kingdom); Boggs, Steven E.; Craig, William W. [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Christensen, Finn C. [DTU Space, National Space Institute, Technical University of Denmark, Elektrovej 327, DK-2800 Lyngby (Denmark); Hailey, Charles J. [Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Ptak, Andrew F.; Zhang, William W. [NASA Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Stern, Daniel [Jet Propulsion Laboratory, California Institute of Technology, Pasadena, CA 91109 (United States)

2015-02-01

We present results for two ultraluminous X-ray sources (ULXs), IC 342 X-1 and IC 342 X-2, using two epochs of XMM-Newton and NuSTAR observations separated by ∼7 days. We observe little spectral or flux variability above 1 keV between epochs, with unabsorbed 0.3-30 keV luminosities being 1.04{sub −0.06}{sup +0.08}×10{sup 40} erg s{sup –1} for IC 342 X-1 and 7.40 ± 0.20 × 10{sup 39} erg s{sup –1} for IC 342 X-2, so that both were observed in a similar, luminous state. Both sources have a high absorbing column in excess of the Galactic value. Neither source has a spectrum consistent with a black hole binary in low/hard state, and both ULXs exhibit strong curvature in their broadband X-ray spectra. This curvature rules out models that invoke a simple reflection-dominated spectrum with a broadened iron line and no cutoff in the illuminating power-law continuum. X-ray spectrum of IC 342 X-1 can be characterized by a soft disk-like blackbody component at low energies and a cool, optically thick Comptonization continuum at high energies, but unique physical interpretation of the spectral components remains challenging. The broadband spectrum of IC 342 X-2 can be fit by either a hot (3.8 keV) accretion disk or a Comptonized continuum with no indication of a seed photon population. Although the seed photon component may be masked by soft excess emission unlikely to be associated with the binary system, combined with the high absorption column, it is more plausible that the broadband X-ray emission arises from a simple thin blackbody disk component. Secure identification of the origin of the spectral components in these sources will likely require broadband spectral variability studies.

Stress measurement by x-ray diffractometry

Energy Technology Data Exchange (ETDEWEB)

Mitchell, C M

1985-10-22

This invention relates to x-ray diffractometry and more particularly to apparatus and methods for the measurement of residual stress in polycrystalline, e.g. metallic, specimens. The procedure is based on measurement of the lattice strain of crystals by x-ray diffraction, in which change in the interplanar spacing of a set of crystal lattice planes due to strain causes a change in the diffraction angle of the scattered x-ray beam, from which latter change the magnitude of the strain can be determined. In a polycrystalline specimen, from well know relations for elastic behaviour in isotropic materials, the stress on a plane normal to a given direction in the surface has a component in the given direction which can be calculated from measurement of lattice strain in two directions in a plane containing the given direction and the normal to the specimen surface. In general three such stress components in three directions in the surface are required to determine the principal stresses and thus express the state of stress in the surface. (author). 2 tabs., 9 figs.

Current status of the Scanning X-ray Microscope at the ESRF

International Nuclear Information System (INIS)

Barrett, Ray; Kaulich, Burkhard; Salome, Murielle; Susini, Jean

2000-01-01

A short description of the Scanning X-ray Microscope of the ESRF ID21 X-ray microscopy beamline is given and the consequences of the relatively wide operating energy range discussed. The current capabilities of the instrument are demonstrated through images and spectra recorded from a variety of pilot experiments, including X-ray fluorescence imaging, microdiffraction and XANES measurements

X-ray photoelectron spectra structure of actinide compounds stipulated by electrons of the inner valence molecular orbitals (IVMO)

International Nuclear Information System (INIS)

Teterin, Yu. A.; Ivanov, K. E.

1997-01-01

Development of precise X-ray photoelectron spectroscopy using X-ray radiation hν< 1.5 KeV allowed to carry out immediate investigations of fine spectra structure of both weakly bond and deep electrons. Based on the experiments and the obtained results it may be concluded: 1. Under favourable conditions the inner valence molecular orbitals (IVMO) may form in all actinide compounds. 2. The XPS spectra fine structure stipulated by IVMO electrons allows to judge upon the degree of participation of the filled AO electrons in the chemical bond, on the structure o considered atom close environment and the bond lengths in compounds. For amorphous compounds the obtaining of such data based on X-ray structure analysis is restricted. 3. The summary contribution of IVMO electrons to the absolute value of the chemical bonding is comparable with the corresponding value of OMO electrons contribution to the atomic bonding. This fact is very important and new in chemistry. (author)

Applying a physical continuum model to describe the broadband X-ray spectra of accreting pulsars at high luminosity

Science.gov (United States)

Pottschmidt, Katja; Hemphill, Paul B.; Wolff, Michael T.; Cheatham, Diana M.; Iwakiri, Wataru; Gottlieb, Amy M.; Falkner, Sebastian; Ballhausen, Ralf; Fuerst, Felix; Kuehnel, Matthias; Ferrigno, Carlo; Becker, Peter A.; Wood, Kent S.; Wilms, Joern

2018-01-01

A new window for better understanding the accretion onto strongly magnetized neutron stars in X-ray binaries is opening. In these systems the accreted material follows the magnetic field lines as it approaches the neutron star, forming accretion columns above the magnetic poles. The plasma falls toward the neutron star surface at near-relativistic speeds, losing energy by emitting X-rays. The X-ray spectral continua are commonly described using phenomenological models, i.e., power laws with different types of curved cut-offs at higher energies. Here we consider high luminosity pulsars. In these systems the mass transfer rate is high enough that the accreting plasma is thought to be decelerated in a radiation-dominated radiative shock in the accretion columns. While the theory of the emission from such shocks had already been developed by 2007, a model for direct comparison with X-ray continuum spectra in xspec or isis has only recently become available. Characteristic parameters of this model are the accretion column radius and the plasma temperature, among others. Here we analyze the broadband X-ray spectra of the accreting pulsars Centaurus X-3 and 4U 1626-67 obtained with NuSTAR. We present results from traditional empirical modeling as well as successfully apply the radiation-dominated radiative shock model. We also take the opportunity to compare to similar recent analyses of both sources using these and other observations.

X-ray Absorption Spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Yano, Junko; Yachandra, Vittal K.

2009-07-09

This review gives a brief description of the theory and application of X-ray absorption spectroscopy, both X-ray absorption near edge structure (XANES) and extended X-ray absorption fine structure (EXAFS), especially, pertaining to photosynthesis. The advantages and limitations of the methods are discussed. Recent advances in extended EXAFS and polarized EXAFS using oriented membranes and single crystals are explained. Developments in theory in understanding the XANES spectra are described. The application of X-ray absorption spectroscopy to the study of the Mn4Ca cluster in Photosystem II is presented.

Characteristics and quality test of X-ray with CZT detector

International Nuclear Information System (INIS)

Rianto, Sugeng

2000-01-01

The study examines the use of direct measurements of x-ray spectra for testing the quality of x-ray beam by using a peltier-cooled CZT detector under different conditions. The typical calibration of the spectrometry system shows that the energy resolution of the system is 1,2 keV at 122 keV of 57 Co. The utilization CZT based spectrometer for assessing the quality of x-ray machine on its spectra show that the CZT could accurately measure the spectra at various kVp, m As and filtration, except at the kVp greater than 140 and m As higher than 2 without added filtration. A comparison of CZT with the field instruments showed that there is a reasonable agreement between the Keithley and CZT at lower energies regardless of filtration however at high energies there is a large difference.In contrast the discrepancy between the CZT and Nero increased at lower photon energies particularly for high filtration

The Mapping X-ray Fluorescence Spectrometer (MapX)

Science.gov (United States)

Sarrazin, P.; Blake, D. F.; Marchis, F.; Bristow, T.; Thompson, K.

2017-12-01

Many planetary surface processes leave traces of their actions as features in the size range 10s to 100s of microns. The Mapping X-ray Fluorescence Spectrometer (MapX) will provide elemental imaging at 100 micron spatial resolution, yielding elemental chemistry at a scale where many relict physical, chemical, or biological features can be imaged and interpreted in ancient rocks on planetary bodies and planetesimals. MapX is an arm-based instrument positioned on a rock or regolith with touch sensors. During an analysis, an X-ray source (tube or radioisotope) bombards the sample with X-rays or alpha-particles / gamma-rays, resulting in sample X-ray Fluorescence (XRF). X-rays emitted in the direction of an X-ray sensitive CCD imager pass through a 1:1 focusing lens (X-ray micro-pore Optic (MPO)) that projects a spatially resolved image of the X-rays onto the CCD. The CCD is operated in single photon counting mode so that the energies and positions of individual X-ray photons are recorded. In a single analysis, several thousand frames are both stored and processed in real-time. Higher level data products include single-element maps with a lateral spatial resolution of 100 microns and quantitative XRF spectra from ground- or instrument- selected Regions of Interest (ROI). XRF spectra from ROI are compared with known rock and mineral compositions to extrapolate the data to rock types and putative mineralogies. When applied to airless bodies and implemented with an appropriate radioisotope source for alpha-particle excitation, MapX will be able to analyze biogenic elements C, N, O, P, S, in addition to the cations of the rock-forming elements >Na, accessible with either X-ray or gamma-ray excitation. The MapX concept has been demonstrated with a series of lab-based prototypes and is currently under refinement and TRL maturation.

DCARR: a spectrograph for measuring low-energy x rays

International Nuclear Information System (INIS)

Anon.

1978-01-01

DCARR, the Differential Critical Angle Reflection Refraction detector system, is described. This detector was designed to measure low-energy x rays, 500 to 5000 eV, with a high degree of resolution, 250 eV. DCARR was developed because these low-energy measurements are of interest in the diagnostics of x-radiation in nuclear tests and available equipment could not make measurements at this low an energy in field tests. DCARR is a versatile piece of equipment that can also be used as a laboratory tool, such as in measuring the low-energy x rays emitted by lasers and various x-ray machines

X-ray Reflected Spectra from Accretion Disk Models. III. A Complete Grid of Ionized Reflection Calculations

Science.gov (United States)

Garcia, J.; Dauser, T.; Reynolds, C. S.; Kallman, T. R.; McClintock, J. E.; Wilms, J.; Ekmann, W.

2013-01-01

We present a new and complete library of synthetic spectra for modeling the component of emission that is reflected from an illuminated accretion disk. The spectra were computed using an updated version of our code xillver that incorporates new routines and a richer atomic data base. We offer in the form of a table model an extensive grid of reflection models that cover a wide range of parameters. Each individual model is characterized by the photon index Gamma of the illuminating radiation, the ionization parameter zeta at the surface of the disk (i.e., the ratio of the X-ray flux to the gas density), and the iron abundance A(sub Fe) relative to the solar value. The ranges of the parameters covered are: 1.2 <= Gamma <= 3.4, 1 <= zeta <= 104, and 0.5 <= A(sub Fe) <= 10. These ranges capture the physical conditions typically inferred from observations of active galactic nuclei, and also stellar-mass black holes in the hard state. This library is intended for use when the thermal disk flux is faint compared to the incident power-law flux. The models are expected to provide an accurate description of the Fe K emission line, which is the crucial spectral feature used to measure black hole spin. A total of 720 reflection spectra are provided in a single FITS file suitable for the analysis of X-ray observations via the atable model in xspec. Detailed comparisons with previous reflection models illustrate the improvements incorporated in this version of xillver.

Probing the Cosmic X-Ray and MeV Gamma-Ray Background Radiation through the Anisotropy

Energy Technology Data Exchange (ETDEWEB)

Inoue, Yoshiyuki [Stanford Univ., CA (United States). Kavli Inst. for Particle Astrophysics and Cosmology; SLAC National Accelerator Lab., Menlo Park, CA (United States); Murase, Kohta [Inst. for Advanced Study, Princeton, NJ (United States). School of Natural Sciences; Madejski, Grzegorz M. [Stanford Univ., CA (United States). Kavli Inst. for Particle Astrophysics and Cosmology; SLAC National Accelerator Lab., Menlo Park, CA (United States); Uchiyama, Yasunobu [Stanford Univ., CA (United States). Kavli Inst. for Particle Astrophysics and Cosmology; SLAC National Accelerator Lab., Menlo Park, CA (United States); Rikkyo Univ., Tokyo (Japan). Dept. of Physics

2013-09-24

While the cosmic soft X-ray background is very likely to originate from individual Seyfert galaxies, the origin of the cosmic hard X-ray and MeV gamma-ray background is not fully understood. It is expected that Seyferts including Compton thick population may explain the cosmic hard X-ray background. At MeV energy range, Seyferts having non-thermal electrons in coronae above accretion disks or MeV blazars may explain the background radiation. We propose that future measurements of the angular power spectra of anisotropy of the cosmic X-ray and MeV gamma-ray backgrounds will be key to deciphering these backgrounds and the evolution of active galactic nuclei (AGNs). As AGNs trace the cosmic large-scale structure, spatial clustering of AGNs exists. We show that e-ROSITA will clearly detect the correlation signal of unresolved Seyferts at 0.5-2 keV and 2-10 keV bands and will be able to measure the bias parameter of AGNs at both bands. Once the future hard X-ray all sky satellites achieve the sensitivity better than 10^-12 erg/cm²/s^-1 at 10-30 keV or 30-50 keV - although this is beyond the sensitivities of current hard X-ray all sky monitors - angular power spectra will allow us to independently investigate the fraction of Compton-thick AGNs in all Seyferts. We also find that the expected angular power spectra of Seyferts and blazars in the MeV range are different by about an order of magnitude, where the Poisson term, so-called shot noise, is dominant. Current and future MeV instruments will clearly disentangle the origin of the MeV gamma-ray background through the angular power spectrum.

Probing the cosmic x-ray and MeV gamma ray background radiation through the anisotropy

Energy Technology Data Exchange (ETDEWEB)

Inoue, Yoshiyuki [Stanford Univ., CA (United States); Murase, Kohta [Inst. for Advanced Study, Princeton, NJ (United States); Madejski, Grzegorz M. [Stanford Univ., CA (United States); Uchiyama, Yasunobu [Stanford Univ., CA (United States); Rikkyo Univ., Tokyo (Japan)

2013-09-24

While the cosmic soft X-ray background is very likely to originate from individual Seyfert galaxies, the origin of the cosmic hard X-ray and MeV gamma-ray background is not fully understood. It is expected that Seyferts including Compton thick population may explain the cosmic hard X-ray background. At MeV energy range, Seyferts having non-thermal electrons in coronae above accretion disks or MeV blazars may explain the background radiation. We propose that future measurements of the angular power spectra of anisotropy of the cosmic X-ray and MeV gamma-ray backgrounds will be key to deciphering these backgrounds and the evolution of active galactic nuclei (AGNs). As AGNs trace the cosmic large-scale structure, spatial clustering of AGNs exists. We show that e-ROSITA will clearly detect the correlation signal of unresolved Seyferts at 0.5-2 keV and 2-10 keV bands and will be able to measure the bias parameter of AGNs at both bands. Once future hard X-ray all sky satellites achieve a sensitivity better than 10–12 erg cm–2 s–1 at 10-30 keV or 30-50 keV—although this is beyond the sensitivities of current hard X-ray all sky monitors—angular power spectra will allow us to independently investigate the fraction of Compton-thick AGNs in all Seyferts. We also find that the expected angular power spectra of Seyferts and blazars in the MeV range are different by about an order of magnitude, where the Poisson term, so-called shot noise, is dominant. Current and future MeV instruments will clearly disentangle the origin of the MeV gamma-ray background through the angular power spectrum.

Nitrogen K-edge X-ray absorption near edge structure (XANES) spectra of purine-containing nucleotides in aqueous solution

Energy Technology Data Exchange (ETDEWEB)

Shimada, Hiroyuki; Fukao, Taishi; Minami, Hirotake; Ukai, Masatoshi [Department of Applied Physics, Tokyo University of Agriculture and Technology, Koganei-shi, Tokyo 184-8588 (Japan); Fujii, Kentaro; Yokoya, Akinari [Advanced Science Research Center, Japan Atomic Energy Agency, Tokai-mura, Naka-gun, Ibaraki 319-1195 (Japan); Fukuda, Yoshihiro; Saitoh, Yuji [Synchrotron Radiation Research Center, Japan Atomic Energy Agency, Sayo-gun, Hyougo 679-5148 (Japan)

2014-08-07

The N K-edge X-ray absorption near edge structure (XANES) spectra of the purine-containing nucleotide, guanosine 5{sup ′}-monophosphate (GMP), in aqueous solution are measured under various pH conditions. The spectra show characteristic peaks, which originate from resonant excitations of N 1s electrons to π* orbitals inside the guanine moiety of GMP. The relative intensities of these peaks depend on the pH values of the solution. The pH dependence is explained by the core-level shift of N atoms at specific sites caused by protonation and deprotonation. The experimental spectra are compared with theoretical spectra calculated by using density functional theory for GMP and the other purine-containing nucleotides, adenosine 5{sup ′}-monophosphate, and adenosine 5{sup ′}-triphosphate. The N K-edge XANES spectra for all of these nucleotides are classified by the numbers of N atoms with particular chemical bonding characteristics in the purine moiety.

Comparison of theoretically predicted and observed Solar Maximum Mission X-ray spectra for the 1980 April 13 and May 9 flares

International Nuclear Information System (INIS)

Smith, D.F.; Orwig, L.E.

1982-01-01

A method for predicting the hard X-ray spectrum in the 10--100 keV range for compact flares during their initial rise is developed on the basis of a thermal model. Observations of the flares of 1980 April 13, 4:05 U.T., and 1980 May 9, 7:12 U.T. are given and their combined spectra from the Hard X-ray Burst Spectrometer and Hard X-ray Imaging Spectrometer on the Solar Maximum Mission are deduced. Constraints on the cross sectional area of the supposed emitting arch are obtained from data from the Hard X-ray Imaging Spectrometer. A power-law spectrum is predicted for the rise of the flare of April 13 for initial arch densities less than 10 10 cm -3 and also for the flare of May 9 for initial arch densities less than 5.4 x 10 10 cm -3 . In both cases power-law spectra are observed. Limitations and implications of these results are discussed

Note: Application of a pixel-array area detector to simultaneous single crystal x-ray diffraction and x-ray absorption spectroscopy measurements

International Nuclear Information System (INIS)

Sun, Cheng-Jun; Brewe, Dale L.; Heald, Steve M.; Zhang, Bangmin; Chen, Jing-Sheng; Chow, G. M.; Venkatesan, T.

2014-01-01

X-ray diffraction (XRD) and X-ray absorption spectroscopy (XAS) are two main x-ray techniques in synchrotron radiation facilities. In this Note, we present an experimental setup capable of performing simultaneous XRD and XAS measurements by the application of a pixel-array area detector. For XRD, the momentum transfer in specular diffraction was measured by scanning the X-ray energy with fixed incoming and outgoing x-ray angles. By selecting a small fixed region of the detector to collect the XRD signal, the rest of the area was available for collecting the x-ray fluorescence for XAS measurements. The simultaneous measurement of XRD and X-ray absorption near edge structure for Pr 0.67 Sr 0.33 MnO 3 film was demonstrated as a proof of principle for future time-resolved pump-probe measurements. A static sample makes it easy to maintain an accurate overlap of the X-ray spot and laser pump beam

Measurement of X-ray beam emittance using crystal optics at an X-ray undulator beamline

CERN Document Server

Kohmura, Y; Awaji, M; Tanaka, T; Hara, T; Goto, S; Ishikawa, T

2000-01-01

We present a method of using crystal optics to measure the emittance of the X-ray source. Two perfect crystals set in (++) configuration work as a high-resolution collimator. The phase-space diagram (i.e. beam cross-section and angular distribution) could be determined without any assumptions on the light source. When the measurement is done at short wavelength radiation from undulator, the electron beam emittance is larger than the diffraction limit of the X-rays. Therefore, the electron beam emittance could be estimated. The measurement was done with the hard X-rays of 18.5 and 55 keV from an undulator beamline, BL 47XU, of SPring-8. The horizontal emittance of the X-ray beam was estimated to be about 7.6 nmrad, close to the designed electron beam emittance of the storage ring (7 nmrad). Some portions of the instrumental functions, such as the scattering by filters and windows along the beamline and the slight bent of the crystal planes of the monochromator, could not be precisely evaluated, but an upper li...

Soft x-ray circular dichroism of biomolecules

International Nuclear Information System (INIS)

Nakagawa, Kazumichi; Tanaka, Makoto; Agui, Akane

2005-01-01

We succeeded to observe natural circular dichroism NCD for biomolecules in soft X-ray region for the first time. Evaporated films of amino acids, phenylalanine (phe) and serine (ser) were prepared in vacuum with the thickness of about 300 nm. Measurement was carried out at the soft X-ray undulator beamline BL23SU of the Spring-8, where left- and right-circularly polarized light (LCPL and RCPL) was available from an APPLE-2 undulator. Difference spectra DA(hν) was plotted as a function of photon energy hν of soft X-ray to be the difference between absorption coefficient A L for LCPL and absorption coefficient A R for RCPL, namely, DA(hν) ≡ A L (hν) - A R (hν). Values of A L and A R were determined by means of the photoelectric drain current measurement. In the DA(hν) spectra for L-phe films, negative peak was observed at 407 eV. On the contrary, for D-phe films, positive peak was observed at 407 eV with the same magnitude but opposite sign. Moreover, no signal was observed for racemic phenylalanine (DL-phe). In the wavelength region of visible to ultraviolet, there is well-known general law in which NCD signals for D- and L-enantiomers are the same magnitude but opposite sign and racemic compound does not show NCD spectra. Characteristic features in DA(hν) spectra of the L-phe, D-phe and DL-phe were of good agreement with this well-known general law. Based on this good agreement, we concluded that peaks at 407 eV in the DA(hν) spectra are true NCD peaks. For ser films, we assigned peaks at 540 eV and 548 eV to be NCD peaks in the same manner. We hope that our first observation of NCD for biomolecules at soft X-ray region will open new science and technologies such as basic science including elucidation of fundamental mechanism of NCD and application to manipulate biomolecules using circularly polarized soft X-ray beams. (author)

JEM-X: The X-ray monitor aboard INTEGRAL

DEFF Research Database (Denmark)

Lund, Niels; Budtz-Jørgensen, Carl; Westergaard, Niels Jørgen Stenfeldt

2003-01-01

The JEM-X monitor provides X-ray spectra and imaging with arcminute angular resolution in the 3 to 35 keV band. The good angular resolution and the low energy response of JEM-X plays an important role in the identification of gamma ray sources and in the analysis and scientific interpretation...

X-Ray and Near-Infrared Spectroscopy of Dim X-Ray Point Sources Constituting the Galactic Ridge X-Ray Emission

Directory of Open Access Journals (Sweden)

Kumiko Morihana

2014-12-01

Full Text Available We present the results of X-ray and Near-Infrared observations of the Galactic Ridge X-ray Emission (GRXE. We extracted 2,002 X-ray point sources in the Chandra Bulge Field (l =0°.113, b = 1°.424 down to ~10-14.8 ergscm-2s-1 in 2-8 keV band with the longest observation (900 ks of the GRXE. Based on X-ray brightness and hardness, we classied the X-ray point sources into three groups: A (hard, B (soft and broad spectrum, and C (soft and peaked spectrum. In order to know populations of the X-ray point sources, we carried out NIR imaging and spectroscopy observation. We identied 11% of X-ray point sources with NIR and extracted NIR spectra for some of them. Based on X-ray and NIR properties, we concluded that non-thermal sources in the group A are mostly active galactic nuclei and the thermal sources are mostly white dwarf binaries such as cataclysmic variables (CVs and Pre-CVs. We concluded that the group B and C sources are X-ray active stars in flare and quiescence, respectively.

X-ray and UV spectroscopy of Cygnus X-1 = HDE226868

Science.gov (United States)

Pravdo, S. H.; White, N. E.; Kondo, Y.; Becker, R. H.; Boldt, E. A.; Holt, S. S.; Serlemitsos, P. J.; Mccluskey, B. G.

1980-01-01

Observations are presented of Cygnus X-1 with the solid-state spectrometer on the Einstein Observatory. The X-ray spectra of two intensity dips viewed near superior conjunction did not exhibit increased photoelectric absorption. Rather the data support a model in which an increase in the electron scattering optical depth modifies both the observed spectrum and the intensity. The characteristic temperature of the intervening material is greater than 5 x 10 to the 7th power K. These measurements were in part simultaneous with observations by IUE. The ultra violet spectrum and intensity remained relatively constant during an X-ray intensity dip.

The advantages of soft X-rays and cryogenic spectrometers for measuring chemical speciation by X-ray spectroscopy

Energy Technology Data Exchange (ETDEWEB)

Drury, Owen B. [Lawrence Livermore National Laboratory, Advanced Detector Group, 7000 East Ave., L-270, Livermore, CA 94550 (United States); UC Davis, Biophysics Graduate Group, 1 Shields Ave, CA 95616 (United States); LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States); Friedrich, Stephan [Lawrence Livermore National Laboratory, Advanced Detector Group, 7000 East Ave., L-270, Livermore, CA 94550 (United States) and LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States)]. E-mail: friedrich1@llnl.gov; George, Simon J. [LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States); Cramer, Stephen P. [UC Davis, Biophysics Graduate Group, 1 Shields Ave, CA 95616 (United States); LBNL, Advanced Biological and Environmental X-ray Facility, 1 Cyclotron Road, MS 6-2100, Berkeley, CA 92720 (United States)

2006-04-15

We have built a 36-pixel high-resolution superconducting tunnel junction (STJ) soft X-ray spectrometer for chemical analysis of dilute metals by fluorescence-detected X-ray absorption spectroscopy (XAS) at the Advanced Light Source synchrotron. Soft X-ray absorption edges are preferred over traditional hard X-ray spectroscopy at the K-edges, since they have narrower natural linewidths and exhibit stronger chemical shifts. STJ detectors are preferred in the soft X-ray band over traditional Ge or grating spectrometers, since they have sufficient energy resolution to resolve transition metal L and M lines from light element K emission, and sufficient detection efficiency to measure the weak lines of dilute specimens within an acceptable time. We demonstrate the capabilities of our STJ spectrometer for chemical analysis with soft XAS measurements of molybdenum speciation on the Mo M{sub 4,5}-edges.

Dynamical correlation effects in a weakly correlated material: Inelastic x-ray scattering and photoemission spectra of beryllium

Science.gov (United States)

Seidu, Azimatu; Marini, Andrea; Gatti, Matteo

2018-03-01

Beryllium is a weakly correlated simple metal. Still we find that dynamical correlation effects, beyond the independent-particle picture, are necessary to successfully interpret the electronic spectra measured by inelastic x-ray scattering (IXS) and photoemission spectroscopies (PES). By combining ab initio time-dependent density-functional theory (TDDFT) and many-body Green's function theory in the G W approximation (G W A ), we calculate the dynamic structure factor, the quasiparticle (QP) properties and PES spectra of bulk Be. We show that band-structure effects (i.e., due to interaction with the crystal potential) and QP lifetimes (LT) are both needed in order to explain the origin of the measured double-peak features in the IXS spectra. A quantitative agreement with experiment is obtained only when LT are supplemented to the adiabatic local-density approximation (ALDA) of TDDFT. Besides the valence band, PES spectra display a satellite, a signature of dynamical correlation due to the coupling of QPs and plasmons, which we are able to reproduce thanks to the combination of the G W A for the self-energy with the cumulant expansion of the Green's function.

DXRaySMCS. First user friendly interface developed for prediction of diagnostic radiology X-ray spectra produced by Monte Carlo (MCNP-4C) simulation in Iran

International Nuclear Information System (INIS)

Bahreyni Toossi, M.T.; Zare, H.; Moradi Faradanbe, H.

2008-01-01

An accurate knowledge of the output energy spectra of an x-ray tube is essential in many areas of radiological studies. It forms the basis of almost all image quality simulations and enable system designers to predict patient dose more accurately. Many radiological physics problems that can be solved by Monte Carlo simulation methods require an x-ray spectra as input data. Computer simulation of x-ray spectra is one of the most important tools for investigation of patient dose and image quality in diagnostic radiology systems. In this work the general purpose Monte Carlo N-particle radiation transport computer code (MCNP-4C) was used for the simulation of x-ray spectra in diagnostic radiology, Electron's path in the target was followed until it's energy was reduced to 10 keV. A user friendly interface named 'Diagnostic X-ray Spectra by Monte Carlo Simulation (DXRaySMCS)' was developed to facilitate the application of MCNP-4C code for diagnostic radiology spectrum prediction. The program provides a user friendly interface for modifying the MCNP input file, launching the MCNP program to simulate electron and photon transport and processing the MCNP output file to yield a summary of the results (Relative Photon Number per Energy Bin). In this article the development and characteristics of DXRaySMCS are outlined. As part of the validation process, out put spectra for 46 diagnostic radiology system settings produced by DXRaySMCS were compared with the corresponding IPEM78. Generally, there is a good agreement between the two sets of spectra. No statistically significant differences have been observed between IPEM78 reported spectra and the simulated spectra generated in this study. (author)

Measurement of non-invasive X-ray measuring instruments

International Nuclear Information System (INIS)

Abe, Shinji

2013-01-01

Described are the history, measuring system, characteristics and present state of the instruments in the title (NXMI). NXMI, non-invasive to the inner circuit of X-ray generator, is now essential for the quality control of generator with reference to definitions by International Electrotechnical Commission (IEC) and Japan Industrial Standards (JIS). Non-invasive measurement of the generator's tube voltage in 1944 is the first report where the absorption difference of Cu plates with different thickness is used. At present, NXMI, being compact, can measure multiple properties of X-ray generated, such as the tube voltage (TV), current (TC), imaging time, dose/dose rate, total filtration, half value layer, and TV/output waveform. TV is measurable by the penetration difference of X-rays through Cu filters of different thickness, which is a linear function of TV; TC, with the clamp-type ammeter placed at the generator high voltage cable; and the dose, with the semiconductor detector. Characteristics can be evaluable within the upper trigger level of the detector (radiation time, dose measured here), in which measured are the irradiation (imaging) time, delay time, and TV (within the window width). Authors' practical quality control of the generator is conducted through calibration for which data are obtained by invasive (direct) precise measurement of TV, TC, imaging time and dose with reference to JIS. Periodical calibration and consequent quality control of NXMI are essential for the maintenance of precision of the generator. (T.T.)

Traditional x-ray imaging

International Nuclear Information System (INIS)

Hay, G.A.

1982-01-01

Methods of imaging x-rays, with particular reference to medicine, are reviewed. The history and nature of x-rays, their production and spectra, contrast, shapes and fine structure, image transducers, including fluorescent screens, radiography, fluoroscopy, and image intensifiers, image detection, perception and enhancement and clinical applications are considered. (U.K.)

X-ray fluorescence in Member States (Italy): Full field X-ray fluorescence imaging with high-energy and high-spatial resolution

Energy Technology Data Exchange (ETDEWEB)

Romano, F. P.; Masini, N.; Pappalardo, L., E-mail: romanop@lns.infn.it [IBAM, CNR, Via Biblioteca 4, 95124 Catania (Italy); Cosentino, L.; Gammino, S.; Mascali, D.; Rizzo, F. [INFN-LNS, Via S. Sofia 62, 95123 Catania (Italy)

2014-02-15

A full field X-ray camera for the X-Ray Fluorescence imaging of materials with high-energy and high-spatial resolution was designed and developed. The system was realized by coupling a pinhole collimator with a positionsensitive CCD detector. X-Ray fluorescence is induced on the samples by irradiation with an external X-ray tube. The characteristic X-ray spectra of the investigated materials are obtained by using a multi-frames acquisition in single-photon counting. The energy resolution measured at the Fe-Kα line was 157 eV. The spatial resolution of the system was determined by the analysis of a sharp-edge at different magnification values; it was estimated to be 90 μm at a magnification value of 3.2x and 190 μm at 0.8x. The present set-up of the system is suited to analyze samples with dimensions up to 5x4 cm{sup 2}. Typical measurement time is in the range between 1h to 4 h. (author)

Femtosecond X-ray magnetic circular dichroism absorption spectroscopy at an X-ray free electron laser

Energy Technology Data Exchange (ETDEWEB)

Higley, Daniel J., E-mail: dhigley@stanford.edu; Yuan, Edwin [SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, California 94025 (United States); Department of Applied Physics, Stanford University, Stanford, California 94305 (United States); Hirsch, Konstantin; Dakovski, Georgi L.; Jal, Emmanuelle; Lutman, Alberto A.; Coslovich, Giacomo; Hart, Philip; Hoffmann, Matthias C.; Mitra, Ankush; Moeller, Stefan; Ohldag, Hendrik; Seaberg, Matthew; Stöhr, Joachim; Nuhn, Heinz-Dieter; Reid, Alex H.; Dürr, Hermann A.; Schlotter, William F. [SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, California 94025 (United States); Liu, Tianmin; MacArthur, James P. [SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, California 94025 (United States); Department of Physics, Stanford University, Stanford, California 94305 (United States); and others

2016-03-15

X-ray magnetic circular dichroism spectroscopy using an X-ray free electron laser is demonstrated with spectra over the Fe L{sub 3,2}-edges. The high brightness of the X-ray free electron laser combined with high accuracy detection of incident and transmitted X-rays enables ultrafast X-ray magnetic circular dichroism studies of unprecedented sensitivity. This new capability is applied to a study of all-optical magnetic switching dynamics of Fe and Gd magnetic sublattices in a GdFeCo thin film above its magnetization compensation temperature.

The X-ray Variability of Eta Car, 1996-2010

Science.gov (United States)

Corcoran, Michael F.; Hamaguchi, K.; Gull, T.; Owocki, S.; Pittard, J.

2010-01-01

X-ray photometry in the 2-10 keY band of the the supermassive binary star Eta Car has been measured with the Rossi X-ray Timing Explorer from 1996-2010. The ingress to X-ray minimum is consistent with a period of 2024 days. The 2009 X-ray minimum began on January 162009 and showed an unexpectedly abrupt recovery starting after 12 Feb 2009. The X-ray colors become harder about half-way through all three minima and continue until flux recovery. The behavior of the fluxes and X-ray colors for the most recent X-ray minimum, along with Chandra high resolution grating spectra at key phases suggests a significant change in the inner wind of Eta Car, a possible indicator that the star is entering a new unstable phase of mass loss.

HIGHER ORDER SPECIATION EFFECTS ON PLUTONIUM L3 X-RAY ABSORPTION NEAR EDGE SPECTRA.

Energy Technology Data Exchange (ETDEWEB)

Conradson, Steven D.; Abney, Kent D.; Begg, Bruce D.; Brady, Erik D.; Clark, David L.; den Auwer, Christophe; Ding, Mei; Dorhout, Peter K.; Espinosa-Faller, Francisco J.; Gordon, Pamela L.; Hess, Nancy J.; Hess, Ryan F.; Keogh, D. Webster; Lander, Gerard H.; Lupinetti, Anthony J.; Neu, Mary P.; Palmer, Phillip D.; Paviet-Hartmann, Patricia; Reilly, Sean D.; Runde, Wolfgang H.; Tait, C. Drew; Veirs, D. Kirk

2003-06-09

Pu L{sub 3} X-ray Near Edge Absorption Spectra for Pu(0-VII) are reported for more than 50 chalcogenides, chlorides, hydrates, hydroxides, nitrates, carbonates, oxy-hydroxides, and other compounds both as solids and in solution, and substituted in zirconlite, perovksite, and borosilicate glass. This large data base extends the known correlations between the energy and shape of these spectra from the usual association of the XANES with valence and site symmetry to higher order chemical effects. Because of the large number of compounds of these different types a number of novel and unexpected behaviors are observed.

A study of radiative Auger emission, satellites and hypersatellites in photon-induced K x-ray spectra of some elements in the range 20≤Z≤32

International Nuclear Information System (INIS)

Verma, H.R.

2000-01-01

Photon-induced K x-ray spectra of Ca, Ti, Fe, Zn and Ge have been investigated. The measurements have been made using a crystal spectrometer combined with a thin scintillation detector. Excited by the collimated photon beam from an Rh-anode x-ray tube, the spectra of all these elements reveal the existence of radiative Auger emission (RAE) structure and the satellite and hypersatellite lines along with the diagram lines. The energies and intensities of the Kα 2 , Kα 1 , Kβ 1,3 and Kβ 5 diagram lines and the Kα satellites and hypersatellite transitions are presented. The intensity of the RAE structure corresponding to the Kβ 1,3 x-ray transition and the energy of the RAE edge for each element is also reported. The measured results have been compared with the values from other sources such as electron/heavy-ion excitation and theoretical values. From the intensities of the satellite lines of these elements, the average L-vacancy fraction P L has been deduced in each case. (author)

Experimental time resolved measurement of fluence and energy spectra of photons emitted by a pulsed X-ray generator in the range 5-300 keV

International Nuclear Information System (INIS)

Vie, M.; Baboulet, J.P.

1989-01-01

We have developed: - A sensor to measure locally X ray fluence rate amplitude and variation versus time during X ray pulses, - A spectrometer based on ROSS method to measure absolute X ray spectrum versus time during X ray pulses. This metrology is used to characterise single shot X ray pulsed sources emitting photons in the range of 5 to 300 keV. Fluence domain is between 10 -9 and 5 10 -4 J. cm -2 with a few nanoseconds time resolution [fr

Flat Field Anomalies in an X-Ray CCD Camera Measured Using a Manson X-Ray Source

International Nuclear Information System (INIS)

Michael Haugh

2008-01-01

The Static X-ray Imager (SXI) is a diagnostic used at the National Ignition Facility (NIF) to measure the position of the X-rays produced by lasers hitting a gold foil target. It determines how accurately NIF can point the laser beams and is critical to proper NIF operation. Imagers are located at the top and the bottom of the NIF target chamber. The CCD chip is an X-ray sensitive silicon sensor, with a large format array (2k x 2k), 24 (micro)m square pixels, and 15 (micro)m thick. A multi-anode Manson X-ray source, operating up to 10kV and 2mA, was used to characterize and calibrate the imagers. The output beam is heavily filtered to narrow the spectral beam width, giving a typical resolution E/ΔE ∼ 12. The X-ray beam intensity was measured using an absolute photodiode that has accuracy better than 1% up to the Si K edge and better than 5% at higher energies. The X-ray beam provides full CCD illumination and is flat, within ±1.5% maximum to minimum. The spectral efficiency was measured at 10 energy bands ranging from 930 eV to 8470 eV. The efficiency pattern follows the properties of Si. The maximum quantum efficiency is 0.71. We observed an energy dependent pixel sensitivity variation that showed continuous change over a large portion of the CCD. The maximum sensitivity variation was >8% at 8470 eV. The geometric pattern did not change at lower energies, but the maximum contrast decreased and was less than the measurement uncertainty below 4 keV. We were also able to observe debris on the CCD chip. The debris showed maximum contrast at the lowest energy used, 930 eV, and disappeared by 4 keV. The Manson source is a powerful tool for characterizing the imaging errors of an X-ray CCD imager. These errors are quite different from those found in a visible CCD imager

Quasar X-Ray Spectra At z=1.5

Science.gov (United States)

Siemiginowska, Aneta

2001-01-01

The predicted counts for ASCA observation was much higher than actually observed counts in the quasar. However, there are three weak hard x-ray sources in the GIS field. We are adding them to the source counts in modeling of hard x-ray background. The work is in progress. We have published a paper in Ap.J. on the luminosity function and the quasar evolution. Based on the theory described in this paper we are predicting a number of sources and their contribution to the x-ray background at different redshifts. These model predictions will be compared to the observed data in the final paper.

Measurement of X-ray beam emittance using crystal optics at an X-ray undulator beamline

International Nuclear Information System (INIS)

Kohmura, Yoshiki; Suzuki, Yoshio; Awaji, Mitsuhiro; Tanaka, Takashi; Hara, Toru; Goto, Shunji; Ishikawa, Tetsuya

2000-01-01

We present a method of using crystal optics to measure the emittance of the X-ray source. Two perfect crystals set in (++) configuration work as a high-resolution collimator. The phase-space diagram (i.e. beam cross-section and angular distribution) could be determined without any assumptions on the light source. When the measurement is done at short wavelength radiation from undulator, the electron beam emittance is larger than the diffraction limit of the X-rays. Therefore, the electron beam emittance could be estimated. The measurement was done with the hard X-rays of 18.5 and 55 keV from an undulator beamline, BL 47XU, of SPring-8. The horizontal emittance of the X-ray beam was estimated to be about 7.6 nmrad, close to the designed electron beam emittance of the storage ring (7 nmrad). Some portions of the instrumental functions, such as the scattering by filters and windows along the beamline and the slight bent of the crystal planes of the monochromator, could not be precisely evaluated, but an upper limit for the vertical emittance of the electron beam could be obtained as 0.14 nmrad

X-ray spectroscopy and X-ray crystallography of metalloenzymes at XFELs

International Nuclear Information System (INIS)

Yano, Junko

2016-01-01

The ultra-bright femtosecond X-ray pulses provided by X-ray Free Electron Lasers (XFELs) open capabilities for studying the structure and dynamics of a wide variety of biological and inorganic systems beyond what is possible at synchrotron sources. Although the structure and chemistry at the catalytic sites have been studied intensively in both biological and inorganic systems, a full understanding of the atomic-scale chemistry requires new approaches beyond the steady state X-ray crystallography and X-ray spectroscopy at cryogenic temperatures. Following the dynamic changes in the geometric and electronic structure at ambient conditions, while overcoming X-ray damage to the redox active catalytic center, is key for deriving reaction mechanisms. Such studies become possible by using the intense and ultra-short femtosecond X-ray pulses from an XFEL, where sample is probed before it is damaged. We have developed methodology for simultaneously collecting crystallography data and X-ray emission spectra, using an energy dispersive spectrometer at ambient conditions. In addition, we have developed a way to collect metal L-edge data of dilute samples using soft X-rays at XFELs. The advantages and challenges of these methods will be described in this review. (author)

Evolution of Cygnus X-3 through its Radio and X-ray States

International Nuclear Information System (INIS)

Szostek, A.; Zdziarski, A. A.; McCollough, M. L.

2009-01-01

Based on X-ray spectra and studies of the long-term correlated behavior between radio and soft X-ray, we present a detailed evolution of Cyg X-3 through its radio and X-ray states. We comment on the nature of the hard X-ray tail and possible Simbol X contribution in constraining the models.

Evolution of Cygnus X-3 through its Radio and X-ray States

Science.gov (United States)

Szostek, A.; Zdziarski, A. A.; McCollough, M. L.

2009-05-01

Based on X-ray spectra and studies of the long-term correlated behavior between radio and soft X-ray, we present a detailed evolution of Cyg X-3 through its radio and X-ray states. We comment on the nature of the hard X-ray tail and possible Simbol X contribution in constraining the models.

A multichannel magnetic β-ray spectrometer for rapid measurements of electron spectra

International Nuclear Information System (INIS)

Kariya, Komyo; Morikawa, Kaoru.

1989-01-01

In order to make the magnetic β-ray spectrometer suitable for rapid measurements of electron spectra with short-lived nuclides, twelve small GM counters have been arrayed along the focal plane of a 180deg focusing flat type design. All the signal pulses from each one of these detectors are mixed together onto a single cable. By means of multichannel PHA, each pulse can be traced back to the specific detector which sent it out. In order to avoid time consuming evacuation procedures, the sample source is placed outside a thin window of the preevacuated analyzer chamber. By the use of this multichannel spectrometer a β-ray spectrum with maximum energy up to about 10 MeV can be measured within 1 min or so. Electron spectra measured with 113m In, 119m In and 144 Pr source are shown. (author)

An angle-dependent estimation of CT x-ray spectrum from rotational transmission measurements

International Nuclear Information System (INIS)

Lin, Yuan; Samei, Ehsan; Ramirez-Giraldo, Juan Carlos; Gauthier, Daniel J.; Stierstorfer, Karl

2014-01-01

Purpose: Computed tomography (CT) performance as well as dose and image quality is directly affected by the x-ray spectrum. However, the current assessment approaches of the CT x-ray spectrum require costly measurement equipment and complicated operational procedures, and are often limited to the spectrum corresponding to the center of rotation. In order to address these limitations, the authors propose an angle-dependent estimation technique, where the incident spectra across a wide range of angular trajectories can be estimated accurately with only a single phantom and a single axial scan in the absence of the knowledge of the bowtie filter. Methods: The proposed technique uses a uniform cylindrical phantom, made of ultra-high-molecular-weight polyethylene and positioned in an off-centered geometry. The projection data acquired with an axial scan have a twofold purpose. First, they serve as a reflection of the transmission measurements across different angular trajectories. Second, they are used to reconstruct the cross sectional image of the phantom, which is then utilized to compute the intersection length of each transmission measurement. With each CT detector element recording a range of transmission measurements for a single angular trajectory, the spectrum is estimated for that trajectory. A data conditioning procedure is used to combine information from hundreds of collected transmission measurements to accelerate the estimation speed, to reduce noise, and to improve estimation stability. The proposed spectral estimation technique was validated experimentally using a clinical scanner (Somatom Definition Flash, Siemens Healthcare, Germany) with spectra provided by the manufacturer serving as the comparison standard. Results obtained with the proposed technique were compared against those obtained from a second conventional transmission measurement technique with two materials (i.e., Cu and Al). After validation, the proposed technique was applied to measure

Analysis of X-ray Spectra of High-Z Elements obtained on Nike with high spectral and spatial resolution

Science.gov (United States)

Aglitskiy, Yefim; Weaver, J. L.; Karasik, M.; Serlin, V.; Obenschain, S. P.; Ralchenko, Yu.

2014-10-01

The spectra of multi-charged ions of Hf, Ta, W, Pt, Au and Bi have been studied on Nike krypton-fluoride laser facility with the help of two kinds of X-ray spectrometers. First, survey instrument covering a spectral range from 0.5 to 19.5 angstroms which allows simultaneous observation of both M- and N- spectra of above mentioned elements with high spectral resolution. Second, an imaging spectrometer with interchangeable spherically bent Quartz crystals that added higher efficiency, higher spectral resolution and high spatial resolution to the qualities of the former one. Multiple spectral lines with X-ray energies as high as 4 keV that belong to the isoelectronic sequences of Fe, Co, Ni, Cu and Zn were identified with the help of NOMAD package developed by Dr. Yu. Ralchenko and colleagues. In our continuous effort to support DOE-NNSA's inertial fusion program, this campaign covered a wide range of plasma conditions that result in production of relatively energetic X-rays. Work supported by the US DOE/NNSA.

Quantum many-body effects in x-ray spectra efficiently computed using a basic graph algorithm

Science.gov (United States)

Liang, Yufeng; Prendergast, David

2018-05-01

The growing interest in using x-ray spectroscopy for refined materials characterization calls for an accurate electronic-structure theory to interpret the x-ray near-edge fine structure. In this work, we propose an efficient and unified framework to describe all the many-electron processes in a Fermi liquid after a sudden perturbation (such as a core hole). This problem has been visited by the Mahan-Noziéres-De Dominicis (MND) theory, but it is intractable to implement various Feynman diagrams within first-principles calculations. Here, we adopt a nondiagrammatic approach and treat all the many-electron processes in the MND theory on an equal footing. Starting from a recently introduced determinant formalism [Phys. Rev. Lett. 118, 096402 (2017), 10.1103/PhysRevLett.118.096402], we exploit the linear dependence of determinants describing different final states involved in the spectral calculations. An elementary graph algorithm, breadth-first search, can be used to quickly identify the important determinants for shaping the spectrum, which avoids the need to evaluate a great number of vanishingly small terms. This search algorithm is performed over the tree-structure of the many-body expansion, which mimics a path-finding process. We demonstrate that the determinantal approach is computationally inexpensive even for obtaining x-ray spectra of extended systems. Using Kohn-Sham orbitals from two self-consistent fields (ground and core-excited state) as input for constructing the determinants, the calculated x-ray spectra for a number of transition metal oxides are in good agreement with experiments. Many-electron aspects beyond the Bethe-Salpeter equation, as captured by this approach, are also discussed, such as shakeup excitations and many-body wave function overlap considered in Anderson's orthogonality catastrophe.

Fundamental quantification procedure for total reflection X-ray fluorescence spectra analysis and elements determination

International Nuclear Information System (INIS)

Wegrzynek, D.; Holynska, B.

1997-01-01

A method for the determination of the concentrations of elements in particulate-like samples measured in total reflection geometry is proposed. In the proposed method the fundamental parameters are utilized for calculating the sensitivities of elements and an internal standard is used to account for the unknown mass per unit area of a sample and geometrical constant of the spectrometer. The modification of the primary excitation spectrum on its way to a sample has been taken into consideration. The concentrations of the elements to be determined are calculated simultaneously with the spectra deconvolution procedure. In the process of quantitative analysis the intensities of all X-ray peaks corresponding to K and L-series lines present in the analyzed spectrum are taken into account. (Author)

Soft x-ray measurements on the PLT Tokamak

International Nuclear Information System (INIS)

Von Goeler, S.; Sauthoff, N.; Bitter, M.

1977-10-01

Four experiments are described that currently run on the PLT tokamak and which utilize the soft x-ray emission of the plasma as a diagnostic: the pulse height analysis system for temperature and impurity measurements; the curved crystal Bragg spectrometer for the determination of ionization states of impurities; ''windowless'' surface barrier detectors for the investigation of the ultra soft x-ray radiation in the energy range 0.1 keV < hν < 1 keV and a silicon diode array for x-ray fluctuation measurements. For each diagnostic a short technical description and some recent results obtained with it on PLT are given in order to demonstrate its use

X-Ray Absorption Spectra of Amorphous Ices from GW Quasiparticle Calculation

Science.gov (United States)

Kong, Lingzhu; Car, Roberto

2013-03-01

We use a GW approach[2] to compute the x-ray absorption spectra of model low- and high-density amorphous ice structures(LDA and HDA)[3]. We include the structural effects of quantum zero point motion using colored-noise Langevin molecular dynamics[4]. The calculated spectra differences in the main and post edge region between LDA and HDA agree well with experimental observations. We attribute these differences to the presence of interstitial molecules within the first coordination shell range in HDA. This assignment is further supported by a calculation of the spectrum of ice VIII, a high-pressure structure that maximizes the number of interstitial molecules and, accordingly, shows a much weaker post-edge feature. We further rationalize the spectral similarity between HDA and liquid water, and between LDA and ice Ih in terms of the respective similarities in the H-bond network topology and bond angle distributions. Supported by grants DOE-DE-SC0005180, DOE DE-SC0008626 and NSF-CHE-0956500.

Automated IBM PC/XT/AT based measurement and control system for the DRON-3M X-ray diffractometer

International Nuclear Information System (INIS)

Tulaev, A.B.

1989-01-01

An automated IBM PC/XT/AT based measurement and control system for the DRON-3M X-ray diffractometer is decribed. The system permits carrying out of real time diffractometer control automatic X-spectra measurement and data acquisition, as well as experimental information computing and representation. The electronic of the system consists of a CAMAC crate with analog and power modules, and a control and measurement organization module, performed as a single bord in the standard of PC electronics. The system provides X-spectra acquisition with volume up to 4K in the angle range from 100 to 160 degrees with a resolution of 0.01 degree, a dead time less than 1mks and an exposition time from tenths of a second to dozens of minutes. 3 refs.; 5 figs

X-Ray Study of Variable Gamma-Ray Pulsar PSR J2021+4026

Science.gov (United States)

Wang, H. H.; Takata, J.; Hu, C.-P.; Lin, L. C. C.; Zhao, J.

2018-04-01

PSR J2021+4026 showed a sudden decrease in the gamma-ray emission at the glitch that occurred around 2011 October 16, and a relaxation of the flux to the pre-glitch state at around 2014 December. We report X-ray analysis results of the data observed by XMM-Newton on 2015 December 20 in the post-relaxation state. To examine any change in the X-ray emission, we compare the properties of the pulse profiles and spectra at the low gamma-ray flux state and at the post-relaxation state. The phase-averaged spectra for both states can be well described by a power-law component plus a blackbody component. The former is dominated by unpulsed emission and probably originated from the pulsar wind nebula as reported by Hui et al. The emission property of the blackbody component is consistent with the emission from the polar cap heated by the back-flow bombardment of the high-energy electrons or positrons that were accelerated in the magnetosphere. We found no significant change in the X-ray emission properties between two states. We suggest that the change of the X-ray luminosity is at an order of ∼4%, which is difficult to measure with the current observations. We model the observed X-ray light curve with the heated polar cap emission, and we speculate that the observed large pulsed fraction is owing to asymmetric magnetospheric structure.

Gamma-ray Output Spectra from 239 Pu Fission

International Nuclear Information System (INIS)

Ullmann, John

2015-01-01

Gamma-ray multiplicities, individual gamma-ray energy spectra, and total gamma energy spectra following neutron-induced fission of 239 Pu were measured using the DANCE detector at Los Alamos. Corrections for detector response were made using a forward-modeling technique based on propagating sets of gamma rays generated from a paramaterized model through a GEANT model of the DANCE array and adjusting the parameters for best fit to the measured spectra. The results for the gamma-ray spectrum and multiplicity are in general agreement with previous results, but the measured total gamma-ray energy is about 10% higher. A dependence of the gamma-ray spectrum on the gamma-ray multplicity was also observed. Global model calculations of the multiplicity and gamma energy distributions are in good agreement with the data, but predict a slightly softer total-energy distribution

System for calibration of instruments of x-ray measurement (CIR-X) applying the PGCS

International Nuclear Information System (INIS)

Gaytan G, E.; Rivero G, T.; Cruz E, P.; Tovar M, V.M.; Vergara M, F.J.

2007-01-01

The Department of Metrology of Ionizing Radiations of the ININ carries out calibration of instruments for X-ray measurement that determine the operation parameters in X-ray diagnostic machines of the health and private sectors. To facilitate this task, the Department of Automation and Instrumentation developed a system for acquisition and signals processing coming from a reference voltage divider with traceability at NIST that is connected directly to the X-rays tube. The system is integrated by the X-ray unit, the X-ray measurement equipment Dynalizer IIIU of RADCAL, a data acquisition card, a personal computer and the acquisition software and signals processing. (Author)

Bright circularly polarized soft X-ray high harmonics for X-ray magnetic circular dichroism.

Science.gov (United States)

Fan, Tingting; Grychtol, Patrik; Knut, Ronny; Hernández-García, Carlos; Hickstein, Daniel D; Zusin, Dmitriy; Gentry, Christian; Dollar, Franklin J; Mancuso, Christopher A; Hogle, Craig W; Kfir, Ofer; Legut, Dominik; Carva, Karel; Ellis, Jennifer L; Dorney, Kevin M; Chen, Cong; Shpyrko, Oleg G; Fullerton, Eric E; Cohen, Oren; Oppeneer, Peter M; Milošević, Dejan B; Becker, Andreas; Jaroń-Becker, Agnieszka A; Popmintchev, Tenio; Murnane, Margaret M; Kapteyn, Henry C

2015-11-17

We demonstrate, to our knowledge, the first bright circularly polarized high-harmonic beams in the soft X-ray region of the electromagnetic spectrum, and use them to implement X-ray magnetic circular dichroism measurements in a tabletop-scale setup. Using counterrotating circularly polarized laser fields at 1.3 and 0.79 µm, we generate circularly polarized harmonics with photon energies exceeding 160 eV. The harmonic spectra emerge as a sequence of closely spaced pairs of left and right circularly polarized peaks, with energies determined by conservation of energy and spin angular momentum. We explain the single-atom and macroscopic physics by identifying the dominant electron quantum trajectories and optimal phase-matching conditions. The first advanced phase-matched propagation simulations for circularly polarized harmonics reveal the influence of the finite phase-matching temporal window on the spectrum, as well as the unique polarization-shaped attosecond pulse train. Finally, we use, to our knowledge, the first tabletop X-ray magnetic circular dichroism measurements at the N4,5 absorption edges of Gd to validate the high degree of circularity, brightness, and stability of this light source. These results demonstrate the feasibility of manipulating the polarization, spectrum, and temporal shape of high harmonics in the soft X-ray region by manipulating the driving laser waveform.

Feasibility of kilovoltage x-ray energy modulation by gaseous media and its application in contrast-enhanced radiotherapy

Energy Technology Data Exchange (ETDEWEB)

Facundo-Flores, E. L.; Garnica-Garza, H. M. [Centro de Investigación y de Estudios Avanzados del Instituto Politécnico Nacional, Unidad Monterrey, Vía del Conocimiento 201 Parque PIIT, Apodaca, Nuevo León 66600 (Mexico)

2013-09-15

Purpose: To present a method to modulate the energy contents of a kilovoltage x-ray beam that makes use of a gas as the modulating medium. The method is capable of producing arbitrary x-ray spectra by varying the pressure of the modulating gas and the peak kilovoltage (kVp) of the x-ray beams whose energy is being modulated.Methods: An aluminum chamber was machined with a 0.5 cm wall thickness, designed to withstand pressures of more than 80 atm. A pressure sensor and electrovalves were used to monitor and regulate the gas pressure. Argon was used as the modulating gas. A CdTe spectrometer was used to measure x-ray spectra for different combinations of kVp and gas pressure, thus obtaining a set of basis x-ray functions. An arbitrary x-ray spectrum can then be formed by the linear combination of such basis functions. In order to show one possible application of the modulation method, a contrast-enhanced radiotherapy prostate treatment was optimized with respect to the x-ray beam energy, without restrictions on the possible shape of the resultant x-ray spectra.Results: The x-ray spectra basis functions obtained display a smooth and gradual variation of their average energy as a function of the gas pressure for a given kVp, sometimes in the order of 1 or 2 keV. This gradual variation would be difficult to obtain with a conventional aluminum or copper filters, as the change in thickness necessary to reproduce the data presented would be in the order of micrometers, making necessary the use of a large number of such filters. Using the modulation method presented here, the authors were able to reconstruct the optimized x-ray spectra from the measured basis functions, for different optimization objectives.Conclusions: A method has been developed that allows for the controlled modulation of the energy contents of kilovoltage x-ray spectra. The method has been shown to be able to reproduce spectra of arbitrary shape, such as those obtained from the optimization of contrast

DMSO-Water Clustering in Solution Observed in Soft X-ray Spectra.

Science.gov (United States)

Engel, Nicholas; Atak, Kaan; Lange, Kathrin M; Gotz, Malte; Soldatov, Mikhail; Golnak, Ronny; Suljoti, Edlira; Rubensson, Jan-Erik; Aziz, Emad F

2012-12-20

The significant deviation from the ideality of dimethyl sulfoxide (DMSO)/water mixtures can be addressed based on the change of the local molecular orbitals of each solvent upon mixing. Oxygen K-edge absorption and emission spectra of DMSO/water solutions were measured using the liquid microjet technique. The spectra demonstrate that the hydrogen bond network in liquid water is already influenced at small DMSO concentrations, and at the molar fraction xDMSO = 0.43 we find strong evidence of DMSO-water clustering reflected by the influence on the occupied molecular orbitals.

The X-ray Telescope for the SWIFT Gamma-Ray Burst Mission

International Nuclear Information System (INIS)

Wells, A.; Abbey, A.F.; Beardmore, A.; Mukerjee, K.; Osborne, J.P.; Watson, D.J.; Willingale, R.; Burrows, D. N.; Hill, J. E.; Nousek, J.A.; Miles, B.J.; Mori, K.; Morris, D.C.; Zugger, M.; Chincarini, G.; Campana, S.; Citterio, O.; Moretti, A.; Tagliaferri, G.; Bosworth, J.

2004-01-01

The X-ray Telescope (XRT) for the SWIFT mission, built by the international consortium from Pennsylvania State University (United States), University of Leicester (UK) and Osservatorio Astronomico di Brera (Italy), is already installed on the SWIFT spacecraft. The XRT has two key functions on SWIFT; to determine locations of GRBs to better than 5 arc seconds within 100 seconds of initial detection of a burst and to measure spectra and light curves of the X-ray afterglow over around four orders of magnitude of decay in the afterglow intensity. This paper summarises the XRT performance, operating modes and sensitivity for the detection of prompt and extended X-ray afterglows from gamma-ray bursts. The performance characteristics have been determined from data taken during the ground calibration campaign at MPE's Panter facility in September 2002

Self-consistent method for quantifying indium content from X-ray spectra of thick compound semiconductor specimens in a transmission electron microscope.

Science.gov (United States)

Walther, T; Wang, X

2016-05-01

Based on Monte Carlo simulations of X-ray generation by fast electrons we calculate curves of effective sensitivity factors for analytical transmission electron microscopy based energy-dispersive X-ray spectroscopy including absorption and fluorescence effects, as a function of Ga K/L ratio for different indium and gallium containing compound semiconductors. For the case of InGaN alloy thin films we show that experimental spectra can thus be quantified without the need to measure specimen thickness or density, yielding self-consistent values for quantification with Ga K and Ga L lines. The effect of uncertainties in the detector efficiency are also shown to be reduced. © 2015 The Authors Journal of Microscopy © 2015 Royal Microscopical Society.

Electron-ion-x-ray spectrometer system

International Nuclear Information System (INIS)

Southworth, S.H.; Deslattes, R.D.; MacDonald, M.A.

1993-01-01

The authors describe a spectrometer system developed for electron, ion, and x-ray spectroscopy of gas-phase atoms and molecules following inner-shell excitation by tunable synchrotron radiation. The spectrometer has been used on beamline X-24A at the National Synchrotron Light Source for excitation-dependent studies of Ar L-shell and K-shell photoexcitation and vacancy decay processes. The instrumentation and experimental methods are discussed, and examples are given of electron spectra and coincidence spectra between electrons and fluorescent x-rays

X-Ray-Scattering Measurements Of Strain In PEEK

Science.gov (United States)

Cebe, Peggy; Lowry, Lynn E.; Chung, Shirley Y.; Yavrouian, Andre H.; Gupta, Amitava

1988-01-01

Internal stress relieved by heating above glass-transition temperature. Report describes wide-angle x-ray scattering and differential scanning calorimetry of specimens of poly(etheretherketone) having undergone various thermal treatments. Wide-angle x-ray scattering particularly useful in determining distances between atoms, crystallinity, and related microstructurally generated phenomena, as thermal expansion and strain. Calorimetric measurements aid interpretation of scattering measurements by enabling correlation with thermal effects.

X-ray excited optical luminescence, photoluminescence, photostimulated luminescence and x-ray photoemission spectroscopy studies on BaFBr:Eu

CERN Document Server

Subramanian, N; Govinda-Rajan, K; Mohammad-Yousuf; Santanu-Bera; Narasimhan, S V

1997-01-01

The results of x-ray excited optical luminescence (XEOL), photoluminescence (PL), photostimulated luminescence (PSL) and x-ray photoemission spectroscopy (XPS) studies on the x-ray storage phosphor BaFBr:Eu are presented in this paper. Analyses of XEOL, PL and PSL spectra reveal features corresponding to the transitions from 4f sup 6 td sup 1 to 4f sup 7 configurations in different site symmetries of Eu sup 2 sup +. Increasing x-ray dose is seen to lead to a red shift in the maximum of the PL excitation spectrum for the 391 nm emission. The XEOL and XPS spectra do not show any signature of Eu sup 3 sup + in the samples studied by us, directly raising doubts about the model of Takahashi et al in which Eu sup 2 sup + is expected to ionize to Eu sup 3 sup + upon x-ray irradiation and remain stable until photostimulation. XEOL and PSL experiments with simultaneous x-ray irradiation and He - Ne laser excitation as well as those with sequential x-ray irradiation and laser stimulation bring out the competition betwe...

Mass attenuation coefficient (μ/ρ), effective atomic number (Z{sub eff}) and measurement of x-ray energy spectra using based calcium phosphate biomaterials: a comparative study

Energy Technology Data Exchange (ETDEWEB)

Fernandes Z, M. A.; Da Silva, T. A.; Nogueira, M. S. [Centro de Desenvolvimento da Tecnologia Nuclear / CNEN, Pte. Antonio Carlos 6627, Belo Horizonte 31270-901, Minas Gerais (Brazil); Goncalves Z, E., E-mail: madelon@cdtn.br [Pontifice Catholic University of Minas Gerais, Av. Dom Jose Gaspar 500, Belo Horizonte 30535-901, Minas Gerais (Brazil)

2015-10-15

In dentistry, alveolar bone regeneration procedures using based calcium phosphate biomaterials have been shown effective. However,there are not reports in the literature of studies the interaction of low energy radiation in these biomaterials used as attenuator and not being then allowed a comparison between the theoretical values and experimental.The objective of this study was to determine the interaction of radiation parameters of four dental biomaterials - BioOss, Cerasorb M Dental, Straumann Boneceramic and Osteogen for diagnostic radiology qualities. As a material and methods, the composition of the biomaterials was determined by the analytical techniques. The samples with 0.181 cm to 0,297 cm thickness were experimentally used as attenuators for the measurement of the transmitted X-rays spectra in X-ray equipment with 50 to 90 kV range by spectrometric system comprising the Cd Te detector. After this procedure, the mass attenuation coefficient, the effective atomic number were determined and compared between all the specimens analyzed, using the program WinXCOM in the range of 10 to 200 keV. In all strains examined observed that the energy spectrum of x-rays transmitted through the BioOss has the mean energy slightly smaller than the others biomaterials for close thickness. The μ/ρ and Z{sub eff} of the biomaterials showed its dependence on photon energy and atomic number of the elements of the material analyzed. It is concluded according to the methodology employed in this study that the measurements of x-ray spectrum, μ/ρ and Z{sub eff} using biomaterials as attenuators confirmed that the thickness, density, composition of the samples, the incident photon energy are factors that determine the characteristics of radiation in a tissue or equivalent material. (Author)

Soft X-rays from the sunlit earth's atmosphere

International Nuclear Information System (INIS)

McKenzie, D.L.; Rugge, H.R.; Charles, P.A.

1982-01-01

The HEAO-1 A-2 experiment low energy proportional counters have been used to measure the X-ray spectrum of the sunlit earth in the energy range 0.2 to 0.8 keV. The X-rays arise by coherent scattering of, or fluorescence of atmospheric constituents by, solar coronal X-rays incident on the atmosphere. Although the relative spectral contributions of the two processes depend upon the sun-earth-satellite geometry, fluorescent oxygen and nitrogen K X-ray emission is always important. The observed spectra were compared with calculations in order to derive the coronal temperature and emission measure, parameters that characterize the incident solar spectrum. These derived parameters agree well with the expected values for the nonflaring sun, and good agreement was obtained between measurements closely spaced in time but having a wide range of geometries and counting rates. Thus X-ray observations of the sunlit earth's atmosphere can be a useful monitor of solar activity for satellite-borne instrumentation unable to view the sun directly. The total measured fluorescent line flux agreed well with calculations, but the N:O line ratio did not. This disagreement is attributed to several causes which are discussed. (author)

Quality assurance challenges in x-ray emission based analyses

International Nuclear Information System (INIS)

Papp, T.

2005-01-01

Complete text of publication follows. There is a large scatter in the results of X-ray analysis with solid-state detectors suggesting methodological origin. Although the PIXE (proton induced X-ray emission) analytical technique can work without relation to any physics, as was commented at the recent PIXE conference, one could argue that if the same technique is used for measuring physical quantities reveals problems, then perhaps potential methodological issues can not apriory be excluded. We present a simple example which could be interpreted as indications for methodological considerations. Recently an inter-comparison was made of analysis of the spectra measured at the laboratory of the International Atomic Energy Agency (IAEA). Four participating analytical software packages were used to evaluate the X-ray spectra. There are several thin metal samples spectra, for which common energy scale could not be established. The quality of the spectrum can be judged from the line shape. The line shape is parametrized by the full widths at half maximum (FWHM) of a peak and the so-called low energy tailing. Fitting the spectra individually we obtained FWHM squared values at different energies and determined the linear regression parameters. The parameters suggest a rather poor detector performance. It is generally assumed that the (FWHM) 2 values have a first order polynomial form as a function of X-ray energy. Having done a linear regression analysis, we can plot the standard residual, presented in Fig. 1, which clearly shows a three-sigma deviation. The probability to having a three-sigma deviation is 1%. In other words, the probability that these spectra are in accordance with the expected FWHM functional form is less than 1%. The main problem is that, although the composite spectra were analyzed using four different programs, the difficulty in interpreting the spectra was not commented upon by any of the participants in the inter-comparison. (author)

X-ray photoelectron and x-ray-induced auger electron spectroscopic data, 2

International Nuclear Information System (INIS)

Baba, Yuji; Sasaki, Teikichi

1984-04-01

The intrinsic data of the X-ray photoelectron spectra (XPS) and X-ray-induced Auger electron spectra (XAES) for 4d transition-metals and related oxides were obtained by means of a spherical electron spectrometer. The metallic surfaces were cleaned by two different metheds : mechanical filing and Ar + ion etching. In the case of the Ar + io n bombarded Y, Zr, and Nb metals, the binding energies of the core-lines and the kinetic energies of the Auger lines shift from those for the mechanically filed surfaces. The energy shifts were interpreted in terms of the ion-induced lattice distortion of the metal surfaces. The oxides examined are typical compounds such as Y 2 O 3 , ZrO 2 , Nb 2 O 5 , MoO 3 and RuO 2 . The data consists of 4 wide scans, 33 core-line spectra, 10 valence-band spectra and 12 XAES spectra. The peak positions of the core-lines and the Auger lines were summarized in 6 tables together with their chemical shifts. (author)

Equivalent half-value thickness and mean energies of filtered X-ray bremsstrahlung spectra

International Nuclear Information System (INIS)

Seelentag, W.W.; Panzer, W.

1980-01-01

X-ray beam qualities are often conveniently described by half-value thicknesses (in connection with tube voltage and filtration). Aluminium and copper are commonly used as half-value thickness materials, and either material may be used in a large intermediate energy range. Data comparisons frequently require conversions from values in Al to values in Cu. Equivalent half-value thicknesses for polychromatic radiations depend on the shapes of the spectra, but spectrometry is too expensive for routine application. Half-value thicknesses in both Al and Cu have been determined for some 250 spectra (tube potentials 10 to 300 kV). The results are tabulated, and these results together with a nomogram enable conversion with an accuracy of better than +- 5% in most cases. (UK)

Quantitative measurements of oxidative stress in mouse skin induced by X-ray irradiation

International Nuclear Information System (INIS)

Chi, Cuiping; Tanaka, Ryoko; Okuda, Yohei; Ikota, Nobuo; Ozawa, Toshihiko; Anzai, Kazunori; Yamamoto, Haruhiko; Urano, Shiro

2005-01-01

To find efficient methods to evaluate oxidative stress in mouse skin caused by X-ray irradiation, several markers and methodologies were examined. Hairless mice were irradiated with 50 Gy X-rays and skin homogenates or skin strips were prepared. Lipid peroxidation was measured using the skin homogenate as the level of thiobarbituric acid reactive substances. The level of lipid peroxidation increased with time after irradiation and was twice that of the control at 78 h. Electron spin resonance (ESR) spectra of skin strips showed a clear signal for the ascorbyl radical, which increased with time after irradiation in a manner similar to that of lipid peroxidation. To measure levels of glutathione (GSH) and its oxidized forms (GSSG) simultaneously, two high performance liquid chromatography (HPLC) methods, sample derivatization with 1-fluoro-2,4-dinitrobenzene and detection with a UV detector (method A) and no derivatization and detection with an electrochemical detector (method B), were compared and the latter was found to be better. No significant change was observed within 24 h after irradiation in the levels of GSH and GSSG measured by method B. The GSH/GSSG ratio may be a less sensitive parameter for the evaluation of acute oxidative stress caused by X-ray irradiation in the skin. Monitoring the ascorbyl radical seems to be a good way to evaluate oxidative stress in skin in vivo. (author)

Measurement of X-ray attenuation coefficients around K-absorption edges using Fe Kα X-rays

International Nuclear Information System (INIS)

Kerur, B.R.; Thontadarya, S.R.; Hanumaiah, B.

1993-01-01

The x-ray mass attenuation coefficients were measured around the K-absorption edges of elements in the range 16 ≤ Z ≤ 30 using Fe Kα x-rays of energy 6.400 keV, which is the weighted average energy of Kα 1 and Kα 2 x-ray components from the 57 Co radioactive source. Kβ x-rays were almost eliminated by the differential absorption technique. The small difference in energy between Kα 1 and Kα 2 , 13 eV, was shown to be inconsequential by comparing the measured and theoretical values of μ/ρ for standard materials such as Al, Cu, Mo and Ta. The effect of fine structure of the K-absorption edge on μ/ρ was elucidated by using the compounds of elements in the range 16 ≤ X ≤ 30, containing one element with its K-absorption edge energy (E k ) close to the incident photon energy (E x ). The results clearly indicate the validity of the theoretical mixture rule for all those compounds whose K edge is far away from the incident energy but show deviations of as much as 10% for the manganese compound whose K edge is 140 eV above E x and about 12% for the chromium compound whose K edge is 410 eV below E x . These deviations are attributed to the possible influence of resonance Raman scattering when the incident photon energy E x is less than the edge and to the influence of EXAFS when E x is more than the edge energy. (Author)

Breast tissue classification using x-ray scattering measurements and multivariate data analysis

Science.gov (United States)

Ryan, Elaine A.; Farquharson, Michael J.

2007-11-01

This study utilized two radiation scatter interactions in order to differentiate malignant from non-malignant breast tissue. These two interactions were Compton scatter, used to measure the electron density of the tissues, and coherent scatter to obtain a measure of structure. Measurements of these parameters were made using a laboratory experimental set-up comprising an x-ray tube and HPGe detector. The breast tissue samples investigated comprise five different tissue classifications: adipose, malignancy, fibroadenoma, normal fibrous tissue and tissue that had undergone fibrocystic change. The coherent scatter spectra were analysed using a peak fitting routine, and a technique involving multivariate analysis was used to combine the peak fitted scatter profile spectra and the electron density values into a tissue classification model. The number of variables used in the model was refined by finding the sensitivity and specificity of each model and concentrating on differentiating between two tissues at a time. The best model that was formulated had a sensitivity of 54% and a specificity of 100%.

Breast tissue classification using x-ray scattering measurements and multivariate data analysis

Energy Technology Data Exchange (ETDEWEB)

Ryan, Elaine A; Farquharson, Michael J [School of Allied Health Sciences, City University, Charterhouse Square, London EC1M 6PA (United Kingdom)

2007-11-21

This study utilized two radiation scatter interactions in order to differentiate malignant from non-malignant breast tissue. These two interactions were Compton scatter, used to measure the electron density of the tissues, and coherent scatter to obtain a measure of structure. Measurements of these parameters were made using a laboratory experimental set-up comprising an x-ray tube and HPGe detector. The breast tissue samples investigated comprise five different tissue classifications: adipose, malignancy, fibroadenoma, normal fibrous tissue and tissue that had undergone fibrocystic change. The coherent scatter spectra were analysed using a peak fitting routine, and a technique involving multivariate analysis was used to combine the peak fitted scatter profile spectra and the electron density values into a tissue classification model. The number of variables used in the model was refined by finding the sensitivity and specificity of each model and concentrating on differentiating between two tissues at a time. The best model that was formulated had a sensitivity of 54% and a specificity of 100%.

Catalogue of response spectra for unfolding in situ gamma-ray pulse-height distributions

International Nuclear Information System (INIS)

Dymke, N.

1982-01-01

To unfold in situ gamma-ray pulse-height distributions by means of a response matrix technique, the matrix must be in keeping with the measurement geometry, detector size, and energy range to be covered by the measurements. A methodology has been described for determination of standard gamma-ray spectra needed in deriving response matrices and a spectrum catalogue compiled containing graphs and data for the 0-3 MeV (4 x 4 in. NaI(Tl)) and 0-8 MeV (1.5 x 1.5 in. NaI(Tl)) ranges. (author)

Profile correction to electron temperature and enhancement factor in soft-x-ray pulse-height-analysis measurements in tokamaks

International Nuclear Information System (INIS)

Sesnic, S.; Diesso, M.; Hill, K.; Holland, A.; Pohl, F.

1988-01-01

Because soft-x-ray pulse-height-analysis spectra contain chordal information, the electron temperature and the radiation intensity (enhancement factor) measurements do not represent the local values. The correction factors for the electron temperature and the enhancement factor as a function of the temperature and density profile parameters and the energy are obtained. The spectrum distortion due to pulse pileup effects is also evaluated. A set of curves is given from which the distortion of the spectrum can be obtained if the electron temperature, the Be filter thickness, and the electronic parameters of the acquisition system are known. PG 1810,1812 ID 131801CON N X-ray diagnostics TT Profile correction to electron temperature and enhancement factor in soft-x-ray pulse-height-analysis measurements in tokamaks AU S. Sesnic, M. Diesso, K. Hill, and A. Holland LO Princeton University, Plasma Physics Laboratory, P.O. Box 451, Princeton, New Jersey 08543 AU F. Pohl LO Max-Planck Institut fuer Plasmaphysik, 8046-Garching, Federal Republic of Germany SD (Presented on 16 March 1988) AB Because soft-x-ray pulse-height-analysis spectra contain chordal information, the electron temperature and the radiation intensity (enhancement factor) measurements do not represent the local values. The correction factors for the electron temperature and the enhancement factor as a function of the temperature and density profile parameters and the energy are obtained. The spectrum distortion due to pulse pileup effects is also evaluated. A set of curves is given from which the distortion of the spectrum can be obtained if the electron tempe

Spatially resolved single crystal x-ray spectropolarimetry of wire array z-pinch plasmas.

Science.gov (United States)

Wallace, M S; Haque, S; Neill, P; Pereira, N R; Presura, R

2018-01-01

A recently developed single-crystal x-ray spectropolarimeter has been used to record paired sets of polarization-dependent and axially resolved x-ray spectra emitted by wire array z-pinches. In this measurement, two internal planes inside a suitable crystal diffract the x-rays into two perpendicular directions that are normal to each other, thereby separating incident x-rays into their linearly polarized components. This paper gives considerations for fielding the instrument on extended sources. Results from extended sources are difficult to interpret because generally the incident x-rays are not separated properly by the crystal. This difficulty is mitigated by using a series of collimating slits to select incident x-rays that propagate in a plane of symmetry between the polarization-splitting planes. The resulting instrument and some of the spatially resolved polarized x-ray spectra recorded for a 1-MA aluminum wire array z-pinch at the Nevada Terawatt Facility at the University of Nevada, Reno will be presented.

ERX: a software for editing files containing X-ray spectra to be used in exposure computational models

International Nuclear Information System (INIS)

Cabral, Manuela O.M.; Vieira, Jose W.; Silva, Alysson G.; Leal Neto, Viriato; Oliveira, Alex C.H.; Lima, Fernando R.A.

2011-01-01

Exposure Computational Models (ECMs) are utilities that simulate situations in which occurs irradiation in a given environment. An ECM is composed primarily by an anthropomorphic model (phantom), and a Monte Carlo code (MC). This paper presents a tutorial of the software Espectro de Raios-X (ERX). This software performs reading and numerical and graphical analysis of text files containing diagnostic X-ray spectra for use in algorithms of radioactive sources in the ECMs of a Grupo de Dosimetria Numerica. The ERX allows the user to select one among several X-ray spectrums in the energy range Diagnostic radiology X-Ray most commonly used in radiology clinics. In the current version of the ERX there are two types of input files: the contained in mspectra.dat file and the resulting of MC simulations in Geant4. The software allows the construction of charts of the Probability Density Function (PDF) and Cumulative Distribution Function (CDF) of a selected spectrum as well as the table with the values of these functions and the spectrum. In addition, the ERX allows the user to make comparative analysis between the PDF graphics of the two catalogs of spectra available, besides being can perform dosimetric evaluations with the selected spectrum. A software of this kind is an important computational tool for researchers in numerical dosimetry because of the diversity of Diagnostic radiology X-Ray machines, which implies in a mass of input data highly diverse. And because of this, the ERX provides independence to the group related to the data origin that is contained in the catalogs created, not being necessary to resort to others. (author)

Analytical Energy Dispersive X-Ray Fluorescence Measurements with a Scanty Amounts of Plant and Soil Materials

Science.gov (United States)

Mittal, R.; Rao, P.; Kaur, P.

2018-01-01

Elemental evaluations in scanty powdered material have been made using energy dispersive X-ray fluorescence (EDXRF) measurements, for which formulations along with specific procedure for sample target preparation have been developed. Fractional amount evaluation involves an itinerary of steps; (i) collection of elemental characteristic X-ray counts in EDXRF spectra recorded with different weights of material, (ii) search for linearity between X-ray counts and material weights, (iii) calculation of elemental fractions from the linear fit, and (iv) again linear fitting of calculated fractions with sample weights and its extrapolation to zero weight. Thus, elemental fractions at zero weight are free from material self absorption effects for incident and emitted photons. The analytical procedure after its verification with known synthetic samples of macro-nutrients, potassium and calcium, was used for wheat plant/ soil samples obtained from a pot experiment.

Modeling of X-ray emissions produced by stepping lightning leaders

OpenAIRE

Xu , Wei; Celestin , Sebastien; Pasko , Victor P.

2014-01-01

International audience; Intense and brief bursts of X-ray emissions have been measured during the stepping processof both natural cloud-to-ground (CG) and rocket-triggered lightning flashes. In this paper, we investigatetheoretically the energy spectra of X-rays produced by the bremsstrahlung emission of thermal runawayelectrons accelerated in the inhomogeneous electric field produced around lightning leader tips. The X-rayenergy spectrum depends on the physical properties of the associated l...

Structure and dynamics in liquid water from x-ray absorption spectroscopy

International Nuclear Information System (INIS)

Wernet, Philippe

2009-01-01

Oxygen K-edge x-ray absorption spectra of water are discussed. The spectra of gas-phase water, liquid water and ice illustrate the sensitivity of oxygen K-edge x-ray absorption spectroscopy to hydrogen bonding in water. Transmission mode spectra of amorphous and crystalline ice are compared to x-ray Raman spectra of ice. The good agreement consolidates the experimental spectrum of crystalline ice and represents an incentive for theoretical calculations of the oxygen K-edge absorption spectrum of crystalline ice. Time-resolved infrared-pump and x-ray absorption probe results are finally discussed in the light of this structural interpretation.

X-ray fluorescence in some medium-Z elements excited by 59.5 keV photons

International Nuclear Information System (INIS)

Han, I.; Shahin, M.; Demir, L.; Narmanli, E.

2010-01-01

K X-ray fluorescence parameters cross sections and average shell fluorescence yields) for selected ten elements in the atomic range 42 ≤ Z ≤ 66 have been experimentally determined at photon excitation energy of 59.5 keV. K X-rays emitted from the samples have been counted by a Si (Li) detector. The K spectra for investigated elements have been derived from the measured K shell X-ray spectra by peak fitting process. Experimental results of K X-ray fluorescence parameters have been compared with theory. In general there is an agreement within the standard uncertainties of the experimental and theoretical values

NuSTAR Hard X-Ray Survey of the Galactic Center Region. II. X-Ray Point Sources

DEFF Research Database (Denmark)

Hong, JaeSub; Mori, Kaya; Hailey, Charles J.

2016-01-01

persistent luminous X-ray binaries (XBs) and the likely run-away pulsar called the Cannonball. New source-detection significance maps reveal a cluster of hard (>10 keV) X-ray sources near the Sgr. A diffuse complex with no clear soft X-ray counterparts. The severe extinction observed in the Chandra spectra...

X-ray measurements and protection, 1913-1964

International Nuclear Information System (INIS)

Taylor, L.S.

1981-12-01

This report reviews the development of measurement standards and protection against x rays. The story of x rays can be divided into three periods up to 1925, a period of discovery, application, and a recognized new danger; up to 1955, a period of exploitation, measurement, control, and protection, and from then, a time of consolidation, public awareness, and political activism. This book is an account of how government and non-government organizations have worked together. Attention is directed to some of the changes and differences between government laboratory operations today and those in the first half of the 20th century

X-rays as a probe of the Universe

Indian Academy of Sciences (India)

Table of contents. X-rays as a probe of the Universe · Probing the Universe ….. Flux = sT4 umax = 1011 T (in Kelvin) · History of x-ray astronomy · X-ray Production · X-ray spectra · Celestial sphere as seen by UHURU (1970) · Slide 8 · X-rays from accreting binary systems · Slide 10 · Neutron stars: Black Hole: · Primary X-ray ...

The spectra of the standard x-ray qualities used in STUK's Radiation Metrology Laboratory

International Nuclear Information System (INIS)

Tapiovaara, T.; Tapiovaara, M.; Siiskonen, T.; Hakanen, A.

2008-02-01

This report presents the fluence spectra of the standard x-radiation qualities used in the Radiation Dosimetry Laboratory of Radiation and Nuclear Safety Authority (STUK). The spectra were measured in August 2007. The radiation qualities characterised in the report are the ISO Narrow spectrum series (ISO N10-N200, ISO 4037-1:1996) and both of the RQR-spectrum series specified by the IEC (IEC 1267:1994 and IEC 61267:2005). The measurements were made using a high purity Ge-detector and the measured pulse height spectra were corrected to fluence spectra. Spectral characteristics were computed from the spectral data and compared to the requirements in the standards and to the values given in the quality manual of the laboratory. (orig.)

Jupiter's X-ray Auroral Pulsations and Spectra During Juno Perijove 7

Science.gov (United States)

Dunn, W.; Branduardi-Raymont, G.; Ray, L. C.; Jackman, C. M.; Kraft, R.; Gladstone, R.; Yao, Z.; Rae, J.; Gray, R.; Elsner, R.; Grodent, D. C.; Nichols, J. D.; Ford, P. G.; Ness, J. U.; Kammer, J.; Rodriguez, P.

2017-12-01

Jupiter's X-ray aurora is concentrated into a bright and dynamic hot spot that is produced by precipitating 10 MeV ions [Gladstone et al. 2002; Elsner et al. 2005; Branduardi-Raymont et al. 2007]. These highly energetic emissions exhibit pulsations over timescales of 10s of minutes and change morphology, intensity and precipitating particle populations from observation to observation and pole to pole [e.g. Dunn et al. 2016; in-press]. The acceleration process/es that allow Jupiter to produce these high-energy ion charge exchange emissions are not well understood, but are concentrated in the most poleward regions of the aurora, where field lines map to the outer magnetosphere and possibly beyond [Vogt et al. 2015; Kimura et al. 2016]. On July 11th 2017, NASA's Juno spacecraft conducted its 7th perijove flyby of Jupiter and is predicted to have flown directly through field lines that map to the Northern and Southern X-ray hot spots. During this unique flight, the XMM-Newton observatory conducted 40 hours of continuous time-tagged X-ray observations. We present the results from these X-ray observations, showing that Jupiter's X-ray aurora varies significantly from one planetary rotation to the next and that the spectral signatures, indicative of the precipitating ion and electron populations producing the emission, also vary. We measure the Doppler broadening of the spectral lines to calculate the ion energies at the point when they impact the ionosphere, in order that these might be compared with in-situ data to constrain Jovian auroral acceleration processes. Finally, we compare X-ray signatures from the last decade of observations with UV polar emissions at similar times to further enrich multi-wavelength connections and deepen our understanding of how Jupiter is able to generate its highly energetic polar auroral precipitations.

SphinX: A Fast Solar Photometer in X-rays J. Sylwester , S. Kuzin ...

Indian Academy of Sciences (India)

NAS solar mission. SphinX (Solar Photometer in X-rays) will use PIN silicon detectors for high time resolution (0.01 s) measurements of the solar spectra of .... right panel of Fig. 2. In this NBF concept, three fluorescing targets illuminate a single. PIN detector. The fluorescence radiation is coming from three different pure ...

Anatomy of the AGN in NGC 5548. IX. Photoionized emission features in the soft X-ray spectra

Science.gov (United States)

Mao, Junjie; Kaastra, J. S.; Mehdipour, M.; Gu, Liyi; Costantini, E.; Kriss, G. A.; Bianchi, S.; Branduardi-Raymont, G.; Behar, E.; Di Gesu, L.; Ponti, G.; Petrucci, P.-O.; Ebrero, J.

2018-04-01

The X-ray narrow emission line region (NELR) of the archetypal Seyfert 1 galaxy NGC 5548 has been interpreted as a single-phase photoionized plasma that is absorbed by some of the warm absorber components. This scenario requires those overlaying warm absorber components to have larger distance (to the central engine) than the X-ray NELR, which is not fully consistent with the distance estimates found in the literature. Therefore, we reanalyze the high-resolution spectra obtained in 2013-2014 with the Reflection Grating Spectrometer (RGS) aboard XMM-Newton to provide an alternative interpretation of the X-ray narrow emission features. We find that the X-ray narrow emission features in NGC 5548 can be described by a two-phase photoionized plasma with different ionization parameters (logξ = 1.3 and 0.1) and kinematics (vout = -50 and -400 km s-1), and no further absorption by the warm absorber components. The X-ray and optical NELR might be the same multi-phase photoionized plasma. Both X-ray and optical NELR have comparable distances, asymmetric line profiles, and the underlying photoionized plasma is turbulent and compact in size. The X-ray NELR is not the counterpart of the UV/X-ray absorber outside the line of sight because their distances and kinematics are not consistent. In addition, X-ray broad emission features that we find in the spectrum can be accounted for by a third photoionized emission component. The RGS spectrum obtained in 2016 is analyzed as well, where the luminosity of most prominent emission lines (the O VII forbidden line and O VIII Lyα line) are the same (at a 1σ confidence level) as in 2013-2014.

Relative probabilities of the uranium isotopes for thorium x-ray emission and fluorescence of uranium x-rays

International Nuclear Information System (INIS)

Parker, J.L.

1991-01-01

Both thorium x-rays from decaying uranium isotopes and self-fluoresced uranium x-rays are prominent in high-resolution gamma-ray spectra of uranium-bearing materials. Useful application of the information carried by those x-rays has been curtailed because the probabilities of the uranium isotopes for thorium x-ray emission and for uranium x-ray fluorescence have not been known. By analyzing enrichment-meter geometry spectra from uranium oxide standards whose enrichments ranged from 0.7% to 91%, relative values, primarily, have been obtained for the probabilities of both processes. Thorium x-ray emission is very heavily dominated by 235 U. In all ordinarily occurring uranium isotopic distributions, thorium x-rays may be used as a valid 235 U signature. The probability for a thorium K α1 x-ray to be emitted in the decay of a 235 U atom is 0.048 ±0.002. In infinitely thick uranium oxide materials, the relative ratios of effectiveness for self-fluorescence, on a per unit mass basis, are approximately 234 U : 235 U : 236 U : 238 U = 1.13 : 1.00 : 0.52 : 0.028. on a per decay basis, the approximate ratios are 0.00039 : 1.00 : 0.017 : 0.18. These results imply that, contrary to what has often been stated, gamma rays are far more important than alpha particles in the self-fluorescence of uranium. Because of the importance of gamma-ray self-fluorescence, the uranium x-ray yield will be somewhat influenced by the size, shape, and composition of the materials. 4 refs., 1 fig

X-ray observations of the starburst galaxy M82

International Nuclear Information System (INIS)

Schaaf, R.; Pietsch, W.; Biermann, P.L.; Kronberg, P.P.; Schmutzler, T.

1989-01-01

Long X-ray observations of the starburst galaxy M82 with the European X-ray satellite EXOSAT are reported. The observations with the low-energy imaging instrument confirm that there is extended X-ray emission from above and below the disk, with an overall extent perpendicular to the disk of almost 6 arcmin corresponding to 6 kpc. One of the best defined X-ray spectra yet of a starburst galaxy is presented. The medium energy instrument measurements can be fitted with a power-law spectrum, consistent with inverse Compton emission, or with thermal emission from optically thin hot gas of a temperature of 9 + 9 or -4 keV. Using, in addition, the earlier Einstein HRI and MPC observations, the possible origin of the X-ray emission is discussed. 31 references

Application of X-ray spectroscopy in nondestructive photon activation analysis

International Nuclear Information System (INIS)

Weise, H.-P.; Segebade, Chr.

1977-01-01

The use of X-ray spectroscopy for the qualitative and quantitative analysis of samples activated by 30 MeV bremsstrahlung from an electron linear accelerator. Detection limits are calculated from the measured X-ray spectra and compared with those for γ-ray spectroscopy. In general, the detection limits for γ-ray and X-ray spectroscopy are comparable. Higher sensitivities for X-ray spectroscopy are observed when only low intensity γ-rays are emitted by the activation products. X-ray spectroscopy should be applied in three cases: (a) low γ-ray emission probability, (b) extremely complicated γ-ray spectrum, (c) overlapping of γ-ray lines from different elements. γ-ray spectroscopy should be preferred for the analysis of light elements for two reasons: very strong absorption of low energy X-rays (low Z) within the sample, low X-ray emission probability for the activation products of light elements. Therefore no attempt was made to use X-ray spectroscopy for the analysis of elements below Ti. Some practical applications of X-ray spectroscopy in nondestructive multielement analysis are quoted. (T.G.)

Measurements of radio frequent cavity volt ages by X-ray spectrum measurements

Directory of Open Access Journals (Sweden)

Toprek Dragan

2005-01-01

Full Text Available This paper deals with X-ray spectrum measurement as a method for the measurement of radio frequent cavity voltage and the theory of X-ray spectrum calculation. Experimental results at 72 MHz for three different values of the radio frequent power of ACCEL K250 super conducting cyclotron are being presented.

Einstein Observatory SSS and MPC observations of the complex X-ray spectra of Seyfert galaxies. [Solid State Spectrometer and Monitor Proportional Counter

Science.gov (United States)

Turner, T. J.; Weaver, K. A.; Mushotzky, R. F.; Holt, S. S.; Madejski, G. M.

1991-01-01

The X-ray spectra of 25 Seyfert galaxies measured with the Solid State Spectrometer on the Einstein Observatory have been investigated. This new investigation utilizes simultaneous data from the Monitor Proportional Counter, and automatic correction for systematic effects in the Solid State Spectrometer which were previously handled subjectively. It is found that the best-fit single-power-law indices generally agree with those previously reported, but that soft excesses of some form are inferred for about 48 percent of the sources. One possible explanation of the soft excess emission is a blend of soft X-ray lines, centered around 0.8 keV. The implications of these results for accretion disk models are discussed.

A quality measurement study of a diagnostic x-ray

International Nuclear Information System (INIS)

Nishitani, Motohiro; Fujimoto, Nobuhisa; Yamada, Katsuhiko

1982-01-01

It is important to check periodically the quality and quantity of the X-rays emitted, in order to obtain the best possible performance from your diagnostic X-ray apparatus. The best way of checking the exact quality of the X-ray is to measure the spectrum of the X-ray, but it is not an easy task to carry out. The second way is to plot the attenuation curve of the X-rays. We have developed a method to plot the attenuation curve by a single exposure, utilizing J.r. Greening's empirical formula. The output of the three cavity ionization chambers, one with 7 mmAl filter, another with a 3 mmAl and the third without any filter, exposed to the same X-ray, were put into a microcomputer. The programming was arranged to display the attenuation curve of the X-rays, effective energy of the X-rays, the 1st HVL and the 2nd HVL on the CRT. The attenuation curves of the X-rays, emitted at a tube voltage at between 60 and 140 kV obtained by this method, agreed with the experimental results with an error of +-4 %. The effective energy obtained by this method agreed with the experimental data with an error of +-1 %. (author)

Elemental analysis of bronze artifacts by muonic X-ray spectroscopy

International Nuclear Information System (INIS)

Ninomiya, Kazuhiko; Shinohara, Atsushi; Kubo, Michael K.; Strasser, Patrick; Nagatomo, Takashi; Kawamura, Naritoshi; Shimomura, Koichiro; Miyake, Yasuhiro; Kobayashi, Yoshio; Ishida, Katsuhiko; Higemoto, Wataru; Suzuki, Takao; Saito, Tsutomu

2015-01-01

A quantitative and multi-elemental analysis method for bulk samples based on muonic X-ray spectroscopy was applied to bronze artifacts (Tempo-Tsuho coins and a Seiun-kyo mirror). This method is based on the measurement of the characteristic high-energy muonic X-rays emitted in a sample after muon irradiation. The elemental compositions of these bronze artifacts were determined from muonic X-ray intensities in a non-destructive manner, using the relation between the muonic X-ray intensity and the elemental composition of the Cu–Sn–Pb alloy system. The analyzed values agreed well with those determined by X-ray fluorescence spectroscopy. We also estimated the detection limit of this method in the present experimental setup as 0.81 wt% of the background signal of the muonic X-ray spectra. (author)

The supersoft X-ray source in V5116 Sagittarii. I. The high resolution spectra

Science.gov (United States)

Sala, G.; Ness, J. U.; Hernanz, M.; Greiner, J.

2017-05-01

Context. Classical nova explosions occur on the surface of an accreting white dwarf in a binary system. After ejection of a fraction of the envelope and when the expanding shell becomes optically thin to X-rays, a bright source of supersoft X-rays arises, powered by residual H burning on the surface of the white dwarf. While the general picture of the nova event is well established, the details and balance of accretion and ejection processes in classical novae are still full of unknowns. The long-term balance of accreted matter is of special interest for massive accreting white dwarfs, which may be promising supernova Ia progenitor candidates. Nova V5116 Sgr 2005b was observed as a bright and variable supersoft X-ray source by XMM-Newton in March 2007, 610 days after outburst. The light curve showed a periodicity consistent with the orbital period. During one third of the orbit the luminosity was a factor of seven brighter than during the other two thirds of the orbital period. Aims: In the present work we aim to disentangle the X-ray spectral components of V5116 Sgr and their variability. Methods: We present the high resolution spectra obtained with XMM-Newton RGS and Chandra LETGS/HRC-S in March and August 2007. Results: The grating spectrum during the periods of high-flux shows a typical hot white dwarf atmosphere dominated by absorption lines of N VI and N VII. During the low-flux periods, the spectrum is dominated by an atmosphere with the same temperature as during the high-flux period, but with several emission features superimposed. Some of the emission lines are well modeled with an optically thin plasma in collisional equilibrium, rich in C and N, which also explains some excess in the spectra of the high-flux period. No velocity shifts are observed in the absorption lines, with an upper limit set by the spectral resolution of 500 km s-1, consistent with the expectation of a non-expanding atmosphere so late in the evolution of the post-nova. Based on

EMISSION LINES BETWEEN 1 AND 2 keV IN COMETARY X-RAY SPECTRA

Energy Technology Data Exchange (ETDEWEB)

Ewing, Ian; Christian, Damian J. [Department of Physics and Astronomy, California State University, 18111 Nordhoff Street, Northridge, CA 91330 (United States); Bodewits, Dennis [Department of Astronomy, University of Maryland, College Park, MD 20742 (United States); Dennerl, Konrad [Max-Planck-Institut fuer extraterrestrische Physik, Postfach 1312, D-85741 Garching Germany (Germany); Lisse, Carey M. [Planetary Exploration Group, Space Department, Johns Hopkins University Applied Physics Laboratory, 11100 Johns Hopkins Rd, Laurel, MD 20723 (United States); Wolk, Scott J., E-mail: ian.ewing.794@my.csun.edu, E-mail: daman.christian@csun.edu [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States)

2013-01-20

We present the detection of new cometary X-ray emission lines in the 1.0-2.0 keV range using a sample of comets observed with the Chandra X-Ray Observatory and ACIS spectrometer. We have selected five comets from the Chandra sample with good signal-to-noise spectra. The surveyed comets are C/1999 S4 (LINEAR), C/1999 T1 (McNaught-Hartley), 153P/2002 (Ikeya-Zhang), 2P/2003 (Encke), and C/2008 8P (Tuttle). We modeled the spectra with an extended version of our solar wind charge exchange (SWCX) emission model. Above 1 keV, we find Ikeya-Zhang to have strong emission lines at 1340 and 1850 eV which we identify as being created by SWCX lines of Mg XI and Si XIII, respectively, and weaker emission lines at 1470, 1600, and 1950 eV formed by SWCX of Mg XII, Mg XI, and Si XIV, respectively. The Mg XI and XII and Si XIII and XIV lines are detected at a significant level for the other comets in our sample (LS4, MH, Encke, 8P), and these lines promise additional diagnostics to be included in SWCX models. The silicon lines in the 1700-2000 eV range are detected for all comets, but with the rising background and decreasing cometary emission, we caution that these detections need further confirmation with higher resolution instruments.

Measurement of soft X-ray power from high-power Z-pinch plasma

International Nuclear Information System (INIS)

Wang Wensheng; Qiu Aici; Sun Fengrong; Luo Jianhui; Zhou Haisheng; He Duohui

2003-01-01

A Ni-film bolometer driven by the pulsed constant-voltage supply was developed for measuring soft X-ray energy under 1 keV generated from the Qiang-Guang-I, while the measuring system of the soft X-ray power was established with an X-ray diode detector. Results of the soft X-ray energy and power measurements were obtained at the experiment of Kr gas-puff high-power Z-pinch plasma

Measurements of Cosmic-Ray Proton and Helium Spectra from the BESS-Polar Long-Duration Balloon Flights Over Antarctica

Science.gov (United States)

Abe, K.; Fuke, H.; Haino, S.; Hams, T.; Hasegawa, M.; Horikoshi, A.; Itazaki, A.; Kim, K. C.; Kumazawa, T.; Kusumoto, A.;

Symbiotic Stars in X-rays

Science.gov (United States)

Luna, G. J. M.; Sokoloski, J. L.; Mukai, K.; Nelson, T.

2014-01-01

Until recently, symbiotic binary systems in which a white dwarf accretes from a red giant were thought to be mainly a soft X-ray population. Here we describe the detection with the X-ray Telescope (XRT) on the Swift satellite of 9 white dwarf symbiotics that were not previously known to be X-ray sources and one that was previously detected as a supersoft X-ray source. The 9 new X-ray detections were the result of a survey of 41 symbiotic stars, and they increase the number of symbiotic stars known to be X-ray sources by approximately 30%. Swift/XRT detected all of the new X-ray sources at energies greater than 2 keV. Their X-ray spectra are consistent with thermal emission and fall naturally into three distinct groups. The first group contains those sources with a single, highly absorbed hard component, which we identify as probably coming from an accretion-disk boundary layer. The second group is composed of those sources with a single, soft X-ray spectral component, which likely arises in a region where low-velocity shocks produce X-ray emission, i.e. a colliding-wind region. The third group consists of those sources with both hard and soft X-ray spectral components. We also find that unlike in the optical, where rapid, stochastic brightness variations from the accretion disk typically are not seen, detectable UV flickering is a common property of symbiotic stars. Supporting our physical interpretation of the two X-ray spectral components, simultaneous Swift UV photometry shows that symbiotic stars with harder X-ray emission tend to have stronger UV flickering, which is usually associated with accretion through a disk. To place these new observations in the context of previous work on X-ray emission from symbiotic stars, we modified and extended the alpha/beta/gamma classification scheme for symbiotic-star X-ray spectra that was introduced by Muerset et al. based upon observations with the ROSAT satellite, to include a new sigma classification for sources with

X-ray PIV measurements of blood flows without tracer particles

International Nuclear Information System (INIS)

Kim, Guk Bae; Lee, Sang Joon

2006-01-01

We analyzed the non-Newtonian flow characteristics of blood moving in a circular tube flow using an X-ray PIV method and compared the experimental results with hemodynamic models. The X-ray PIV method was improved for measuring quantitative velocity fields of blood flows using a coherent synchrotron X-ray. Without using any contrast media, this method can visualize flow pattern of blood by enhancing the phase-contrast and interference characteristics of blood cells. The enhanced X-ray images were achieved by optimizing the sample-to-scintillator distance, the sample thickness, and hematocrit in detail. The quantitative velocity fields of blood flows inside opaque conduits were obtained by applying a two-frame PIV algorithm to the X-ray images of the blood flows. The measured velocity data show typical features of blood flow such as the yield stress and shear-thinning effects. (orig.)

X-ray spectral determination by detection of radiation scattered at different angles

International Nuclear Information System (INIS)

Barrea, Raul; Mainardi, R.T.

1987-01-01

A precise knowledge of the spectral content of an X-ray beam is of fundamental importance in areas such as X-ray fluorescence analysis by absolute methods, radiodiagnosis, radiotherapy, computed tomography, etc. A simple practical method was developed to determine X-ray spectra emitted by X-ray tubes. It is based on the scattering of the beam on a solid target and detection of this radiation at different angles. This methodology can easily be adapted to the successive attenuation of the beam procedure. Numerical parameter values of a proposed analytical function for the energy spectrum are found measuring the radiation intensity with a suitable detector (ionization chamber or plastic scintillation detector) and equating it with the convolution integral of the proposed spectrum with the incoherent scattering function. This procedure of spectra determination is enclosed in the same group of those generically referred as successive modifications of the irradiation set up used in absolute methods of X-ray fluorescence analysis. (Author) [es

What Can Simbol-X Do for Gamma-ray Binaries?

Science.gov (United States)

Cerutti, B.; Dubus, G.; Henri, G.; Hill, A. B.; Szostek, A.

2009-05-01

Gamma-ray binaries have been uncovered as a new class of Galactic objects in the very high energy sky (>100 GeV). The three systems known today have hard X-ray spectra (photon index ~1.5), extended radio emission and a high luminosity in gamma-rays. Recent monitoring campaigns of LSI +61°303 in X-rays have confirmed variability in these systems and revealed a spectral hardening with increasing flux. In a generic one-zone leptonic model, the cooling of relativistic electrons accounts for the main spectral and temporal features observed at high energy. Persistent hard X-ray emission is expected to extend well beyond 10 keV. We explain how Simbol-X will constrain the existing models in connection with Fermi Space Telescope measurements. Because of its unprecedented sensitivity in hard X-rays, Simbol-X will also play a role in the discovery of new gamma-ray binaries, giving new insights into the evolution of compact binaries.

What Can Simbol-X Do for Gamma-ray Binaries?

International Nuclear Information System (INIS)

Cerutti, B.; Dubus, G.; Henri, G.; Hill, A. B.; Szostek, A.

2009-01-01

Gamma-ray binaries have been uncovered as a new class of Galactic objects in the very high energy sky (>100 GeV). The three systems known today have hard X-ray spectra (photon index ∼1.5), extended radio emission and a high luminosity in gamma-rays. Recent monitoring campaigns of LSI +61 deg. 303 in X-rays have confirmed variability in these systems and revealed a spectral hardening with increasing flux. In a generic one-zone leptonic model, the cooling of relativistic electrons accounts for the main spectral and temporal features observed at high energy. Persistent hard X-ray emission is expected to extend well beyond 10 keV. We explain how Simbol-X will constrain the existing models in connection with Fermi Space Telescope measurements. Because of its unprecedented sensitivity in hard X-rays, Simbol-X will also play a role in the discovery of new gamma-ray binaries, giving new insights into the evolution of compact binaries.

Measurements of x-rays and γ-rays from stopped kaons

International Nuclear Information System (INIS)

Godfrey, G.L.

1975-01-01

Intensities of x rays and γ rays from negative kaons stopped in elements, pure isotopes, and some compounds ranging from Z = 2 through Z = 92 have been measured. Included were x rays from K - atoms, Σ - atoms, and π - atoms. Also some nuclear γ rays associated with the stopped kaons were observed. The kaonic x-ray intensities for low n, Δn = 1 transitions, varied from .1 to .5 x rays/K/sub stop/ and showed a remarkable oscillation as Z changed. Peaks occurred near elements with closed electron shells. Within experimental accuracy, isotopes of the same elements yielded equal intensities. By searching for μ - from K - → μ - anti ν it was concluded that less than or equal to 5 percent of the stopped kaons decayed before nuclear capture in those elements studied. A cascade calculation was performed that reasonably reproduced the Δn = 1 intensities but gave Δn = 2 intensities high by a factor of 2. Initial kaon distributions in n = 30 proportional to (2l + 1) out to some l/sub max/ were used to begin the cascade. The value of l/sub max/ changed with Z. It is suggested that l/sub max/ might be related to an impact parameter picture with the lever arm equal to one-half the distance between the atoms in their lattice. (U.S.)

Research on temperature measurement by X-ray transmission intensity

International Nuclear Information System (INIS)

Chen, Shuyue; Cheng, Rong

2013-01-01

The relationship between temperature and X-ray transmission intensity was researched and analyzed by inspecting material density change, which is caused by thermal expansion. A digital radiographic system was employed to obtain the images. On this basis, we deduced the temperature formula based on the average gray level of the captured images. The measured temperatures were obtained from the experiments and the errors were analyzed. We concluded that when X-rays pass through an object, the X-ray strength and the gray level of the image under high temperatures are greater than those under lower temperatures and the image gray level error has great impact on the accuracy of the measured temperature. The presented approach allowed the non-contact temperature measurement of material

Measurement of the electron and ion temperatures by the x-ray imaging crystal spectrometer on joint Texas experimental tokamak

Energy Technology Data Exchange (ETDEWEB)

Yan, W.; Chen, Z. Y., E-mail: zychen@hust.edu.cn; Huang, D. W.; Tong, R. H.; Wang, S. Y.; Wei, Y. N.; Ma, T. K.; Zhuang, G. [State Key Laboratory of Advanced Electromagnetic Engineering and Technology, School of Electrical and Electronic Engineering, Huazhong University of Science and Technology, Wuhan (China); Jin, W. [Center of Interface Dynamics for Sustainability, China Academy of Engineering Physics, Chengdu, Sichuan 610200 (China); Lee, S. G. [National Fusion Research Institute, Daejeon 305-333 (Korea, Republic of); Shi, Y. J. [Department of Nuclear Engineering, Seoul National University, Seoul 08826 (Korea, Republic of)

2016-11-15

An x-ray imaging crystal spectrometer has been developed on joint Texas experimental tokamak for the measurement of electron and ion temperatures from the K{sub α} spectra of helium-like argon and its satellite lines. A two-dimensional multi-wire proportional counter has been applied to detect the spectra. The electron and ion temperatures have been obtained from the Voigt fitting with the spectra of helium-like argon ions. The profiles of electron and ion temperatures show the dependence on electron density in ohmic plasmas.

A reaction cell for ambient pressure soft x-ray absorption spectroscopy

Science.gov (United States)

Castán-Guerrero, C.; Krizmancic, D.; Bonanni, V.; Edla, R.; Deluisa, A.; Salvador, F.; Rossi, G.; Panaccione, G.; Torelli, P.

2018-05-01

We present a new experimental setup for performing X-ray Absorption Spectroscopy (XAS) in the soft X-ray range at ambient pressure. The ambient pressure XAS setup is fully compatible with the ultra high vacuum environment of a synchrotron radiation spectroscopy beamline end station by means of ultrathin Si3N4 membranes acting as windows for the X-ray beam and seal of the atmospheric sample environment. The XAS detection is performed in total electron yield (TEY) mode by probing the drain current from the sample with a picoammeter. The high signal/noise ratio achievable in the TEY mode, combined with a continuous scanning of the X-ray energies, makes it possible recording XAS spectra in a few seconds. The first results show the performance of this setup to record fast XAS spectra from sample surfaces exposed at atmospheric pressure, even in the case of highly insulating samples. The use of a permanent magnet inside the reaction cell enables the measurement of X-ray magnetic circular dichroism at ambient pressure.

Application of direct peak analysis to energy dispersive x-ray fluorescence spectra

International Nuclear Information System (INIS)

Nielson, K.K.

1977-07-01

A modified Covell method for direct peak analysis has been applied to energy dispersive x-ray fluorescence spectra. The method is background independent and is well-suited to computerized data reduction. It provides acceptable precision, minimizes errors from instrumental gain shift, and permits peak overlap correction. Peak overlap errors exhibit both positive and negative nodes as a function of peak separation distance, and are corrected using concentration ratios determined from thin, single-element standards. Peak precisions and overlaps are evaluated as a function of window width to aid in width selection. Least-square polynomial smoothing prior to peak analysis significantly improves peak area precisions without significantly affecting their accuracies

X-ray emission in heavy-ion collisions. Progress report, April 1, 1980-February 28, 1981

International Nuclear Information System (INIS)

Watson, R.L.

1981-03-01

During the past year, work on x-ray emission in heavy-ion collisions has concentrated on the following topics: environmental influences on the Kα x-ray spectra of 65-MeV sulfur ions traveling in solids; multiplet structure of few-electron sulfur ions; multiplet structure of Mg Kα x-ray satellites; polarization of 1s2p→1s 2 transitions in He-like sulfur ions; and interatomic electron transfer in ionic fluorine compounds following 1s2p vacancy production. Among the most significant accomplishments of the program was a study of the dependence of dynamic screening energy shifts on electron density. It was found that the shifts measured for the 2 1 P→1 1 S and 2 2 P→1 2 S x-ray transitions of He- and H-like sulfur ions (respectively) were in remarkably good agreement with theoretical expectations. Another interesting discovery evolved from measurements of fluorine Kα x-ray spectra for the alkali metal and alkaline earth fluorides using 5.5-MeV He + ions. The systematics of these spectra provide the first evidence for direct electron transfer between inner levels of neighboring atoms in a solid. 10 figures, 3 tables

Comparative Analysis and Variability of the Jovian X-Ray Spectra Detected by the Chandra and XMM-Newton Observatories

Energy Technology Data Exchange (ETDEWEB)

Hui, Yawei [ORNL; Schultz, David Robert [ORNL; Kharchenko, Vasili A [ORNL; Bhardwaj, Anil [Vikram Sarabhai Space Center, Trivandrum, India; Branduardi-Raymont, Graziella [University College, London; Stancil, Phillip C. [University of Georgia, Athens, GA; Cravens, Thomas E. E. [University of Kansas; Lisse, Carey M. [Johns Hopkins University; Dalgarno, A. [Harvard-Smithsonian Center for Astrophysics

2010-01-01

Expanding upon recent work, a more comprehensive spectral model based on charge exchange induced X-ray emission by ions precipitating into the Jovian atmosphere is used to provide new understanding of the polar auroras. In conjunction with the Xspec spectral fitting software, the model is applied to analyze observations from both Chandra and XMM-Newton by systematically varying the initial precipitating ion parameters to obtain the best fit model for the observed spectra. In addition to the oxygen and sulfur ions considered previously, carbon is included to discriminate between solar wind and Jovian magnetospheric ion origins, enabled by the use of extensive databases of both atomic collision cross sections and radiative transitions. On the basis of fits to all the Chandra observations, we find that carbon contributes negligibly to the observed polar X-ray emission suggesting that the highly accelerated precipitating ions are of magnetospheric origin. Most of the XMM-Newton fits also favor this conclusion with one exception that implies a possible carbon contribution. Comparison among all the spectra from these two observatories in light of the inferred initial energies and relative abundances of precipitating ions from the modeling show that they are significantly variable in time (observation date) and space (north and south polar X-ray auroras).

X-ray scatter signatures for enhanced breast imaging

Energy Technology Data Exchange (ETDEWEB)

Kidane, Ghirmay; Speller, Robert; Royle, Gary [Medical Physics and Bioengineering Department, University College Landon, 11-20 Capper Street, London WC1E 6JA (United Kingdom)

1999-12-31

Conventional mammographic imaging suffers from a low specificity. The main cause is the small difference in the x-ray attenuation properties of healthy and diseased tissue leading to poor contrast in the image. It has been observed that additional information on breast tissue type can be obtained from x-ray diffraction effects. A study of excised normal and neoplastic breast tissue samples using x-ray diffraction apparatus has been observed that significant differences exist in the measured spectra between carcinoma and healthy tissue adjacent to the carcinoma. Such a difference allows tissue type to be characterised according to is diseased state. Furthermore the information can be applied to improve diagnosis. It is proposed that collection and analysis of the scattered x-rays present during a mammographic procedure can supply the additional information and be used to improve the image contrast. The ultimate aim of the project is to improve the specificity of x-ray mammography. (authors) 10 refs., 3 figs.

Fat to muscle ratio measurements with dual energy x-ray absorbtiometry

Energy Technology Data Exchange (ETDEWEB)

Chen, A. [Shenzhen College of International Education, 1st HuangGang Park St., Shenzhen, GuangDong (China); Luo, J. [Department of Biomedical Engineering, University at Buffalo, 332 Bonner Hall, Buffalo, NY 14260-1920 (United States); Wang, A. [Department of Computer Science, Carnegie Mellon University, Pittsburgh, PA 15213 (United States); Broadbent, C. [School of Engineering, Columbia University, 1130 Amsterdam Av., New York, NY 10027 (United States); Zhong, J. [Department of English, Dartmouth College, 6032 Sanborn House, Hanover, NH 03755 (United States); Dilmanian, F.A. [Departments of Radiation Oncology, Neurology, and Radiology, Stony Brook University, Stony Brook, NY 11794 (United States); Zafonte, F.; Zhong, Z. [National Synchrotron Light Source II, Brookhaven National Laboratory, Bldg. 743, Upton, NY 11973 (United States)

2015-07-11

Accurate measurement of the fat-to-muscle ratio in animal model is important for obesity research. An efficient way to measure the fat to muscle ratio in animal model using dual-energy absorptiometry is presented in this paper. A radioactive source exciting x-ray fluorescence from a target material is used to provide the two x-ray energies needed. The x-rays, after transmitting through the sample, are measured with an energy-sensitive Ge detector. Phantoms and specimens were measured. The results showed that the method was sensitive to the fat to muscle ratios with good linearity. A standard deviation of a few percent in the fat to muscle ratio could be observed with the x-ray dose of 0.001 mGy.

X-ray beam qualities for dental radiology purposes

International Nuclear Information System (INIS)

Santos, Marcus Aurelio P. dos; Fragoso, Maria da Conceicao de F.; Lima, Ricardo de A.; Hazim, Clovis A.

2009-01-01

In order to establish characteristics or properties of equipment for diagnostic radiology, e.g. ion chambers and semiconductor detectors, calibration laboratories offer a set of well-defined radiation conditions, called X-ray qualities, which can be used for many Physics studies and medical purposes. The standardization of radiation qualities has been carried out in several fields of study, but little attention has been given to the area of dental radiology, mainly for medical and physical applications using single-phase units with half-wave rectification. For this reason, a single-phase dental unit with adjustable peak voltage and tube current, called 'variable potential X-ray equipment', was developed aiming to define X-ray beam qualities for test and calibrations purposes. X-ray spectra at 50, 60 and 70 kVp were determined by using a CdTe detector and compared with those obtained for ten commercial X-ray dental units. As a result of this study, a set of X-ray qualities for the variable potential X-ray equipment was determined. The X-ray qualities spectra were utilized as reference for determination of a new set of X-ray qualities characterized for a constant potential X-ray equipment. Thus, sets of X-ray qualities were standardized and implemented in two X-ray laboratories: one with the variable potential X-ray equipment and other with constant potential X-ray equipment. These reference X-ray beam qualities should be used for test and calibration purposes involving scientific studies and services. (author)

Conceptual design of a novel instrument for producing intense pulses of 10 ps X-rays for ultra-fast fluorescence measurements

Energy Technology Data Exchange (ETDEWEB)

Gruber, G.J.

1996-05-01

A novel bench-top device for producing intense, fast pulses of x-rays has been designed with 10 ps fwhm (full-width at half-maximum) x-ray pulse width, 120 keV maximum energy, 100 kHz repetition rate, and 1 A peak current onto the x-ray anode. The device includes three sections: (1) an electron gun that generates 5 ns wide pulses of 120 keV electrons at 100 kHz; (2) solenoidal magnetic lenses and deflection plates that focus the electrons onto an aperture plate and sweep the pulsed beam past the aperture, respectively; and (3) a tungsten anode onto which the post-aperture electrons are focused, producing pulses of x-rays. At a sweeping rate of 10{sup 13} V/s, the electron pulses and resulting x-ray pulses are reduced to about 10 ps. The design process used EGUN (an electron optics and gun design program) electron trajectory simulations, including calculation of important space charge effects. When built, this instrument will be used to excite new, fast, bright scintillator samples in crystal or powdered form, allowing fluorescent lifetimes and spectra to be measured with a microchannel PMT. The very narrow 10 ps x-ray pulse width is necessary for accurate measurements of the risetimes of very fast scintillators (e.g., BaF{sub 2}). In addition, the large x-ray flux (1 A peak current) is advantageous when using a reflection grating monochromator to measure decay times at different wavelengths.

Conceptual design of a novel instrument for producing intense pulses of 10 ps X-rays for ultra-fast fluorescence measurements

International Nuclear Information System (INIS)

Gruber, G.J.

1996-05-01

A novel bench-top device for producing intense, fast pulses of x-rays has been designed with 10 ps fwhm (full-width at half-maximum) x-ray pulse width, 120 keV maximum energy, 100 kHz repetition rate, and 1 A peak current onto the x-ray anode. The device includes three sections: (1) an electron gun that generates 5 ns wide pulses of 120 keV electrons at 100 kHz; (2) solenoidal magnetic lenses and deflection plates that focus the electrons onto an aperture plate and sweep the pulsed beam past the aperture, respectively; and (3) a tungsten anode onto which the post-aperture electrons are focused, producing pulses of x-rays. At a sweeping rate of 10 13 V/s, the electron pulses and resulting x-ray pulses are reduced to about 10 ps. The design process used EGUN (an electron optics and gun design program) electron trajectory simulations, including calculation of important space charge effects. When built, this instrument will be used to excite new, fast, bright scintillator samples in crystal or powdered form, allowing fluorescent lifetimes and spectra to be measured with a microchannel PMT. The very narrow 10 ps x-ray pulse width is necessary for accurate measurements of the risetimes of very fast scintillators (e.g., BaF 2 ). In addition, the large x-ray flux (1 A peak current) is advantageous when using a reflection grating monochromator to measure decay times at different wavelengths

Active silicon x-ray for measuring electron temperature

International Nuclear Information System (INIS)

Snider, R.T.

1994-07-01

Silicon diodes are commonly used for x-ray measurements in the soft x-ray region between a few hundred ev and 20 keV. Recent work by Cho has shown that the charge collecting region in an underbiased silicon detector is the depletion depth plus some contribution from a region near the depleted region due to charge-diffusion. The depletion depth can be fully characterized as a function of the applied bias voltage and is roughly proportional to the squart root of the bias voltage. We propose a technique to exploit this effect to use the silicon within the detector as an actively controlled x-ray filter. With reasonable silicon manufacturing methods, a silicon diode detector can be constructed in which the sensitivity of the collected charge to the impinging photon energy spectrum can be changed dynamically in the visible to above the 20 keV range. This type of detector could be used to measure the electron temperature in, for example, a tokamak plasma by sweeping the applied bias voltage during a plasma discharge. The detector samples different parts of the energy spectrum during the bias sweep, and the data collected contains enough information to determine the electron temperature. Benefits and limitations of this technique will be discussed along with comparisons to similar methods for measuring electron temperature and other applications of an active silicon x-ray filter

Alpha Particle Induced X-ray Emission in the Classroom

International Nuclear Information System (INIS)

Lopez, Jorge A.; Borunda, Mario F.; Morales, Jaime

2003-01-01

We report on an experimental demonstration in an introductory modern physics course to elucidate the X-ray line spectra, and how they arise from transitions of electrons to inner shells. We seek to determine the effect of limited use of an interactive component as a supplement to a traditional lecture, and how it would improve the student achievement. In this preliminary study the students were exposed to traditional lectures on X-ray production and Bohr's model, they then were given a homework on the abc of X-ray spectra, after which they were given a pre-test on the materials, followed by an in-class demonstration, and a final post-exam. The gain, as measured from pre- to post-exams appears to remark the differences in how students approached the subject before and after the use of the demonstration. This initial study shows the validity of in-class demonstrations as teaching tools and opens a wide new area of research in modern physics teaching

Software System for the Calibration of X-Ray Measuring Instruments

International Nuclear Information System (INIS)

Gaytan-Gallardo, E.; Tovar-Munoz, V. M.; Cruz-Estrada, P.; Vergara-Martinez, F. J.; Rivero-Gutierrez, T.

2006-01-01

A software system that facilities the calibration of X-ray measuring instruments used in medical applications is presented. The Secondary Standard Dosimetry Laboratory (SSDL) of the Nuclear Research National Institute in Mexico (ININ in Spanish), supports activities concerning with ionizing radiations in medical area. One of these activities is the calibration of X-ray measuring instruments, in terms of air kerma or exposure by substitution method in an X-ray beam at a point where the rate has been determined by means of a standard ionization chamber. To automatize this process, a software system has been developed, the calibration system is composed by an X-ray unit, a Dynalizer IIIU X-ray meter by RADCAL, a commercial data acquisition card, the software system and the units to be tested and calibrated. A quality control plan has been applied in the development of the software system, ensuring that quality assurance procedures and standards are being followed

Correction of build-up factor one x-ray hvl measurement

International Nuclear Information System (INIS)

Yuliati, Helfi; Akhadi, Mukhlis

2000-01-01

Research to obtain the value build-up factor (b) on half value layers (HVL) measurement of diagnostic X-Rays using pocket dosimeter behind aluminium (AI) filter with its thickness vary from 1 to 4 mm. From the measurement it was obtained HVL value of 1.997, 2.596 and 2.718 mmAI for X-Rays of kVp : 80 Kv with 1, 2, 3 and 4 mm filter thickness respectively. HVL value significantly increase with increasing AI filter thickness. Increasing of HVL means increasing filter thickness. From the calculation it was obtained increasing b value relative to 1 mm AI filter of 18.26 and 46% for filter thickness of 2, 3 and 4 mm respectively. Experiment result shows the need of involving b value in HVL calculation of X-Rays if the filter is relatively thick. Calculation of HVL of X-Rays can be carried out with thin layers filter. Key words : x-rays, half value layer, build up factor

MEASUREMENTS OF COSMIC-RAY PROTON AND HELIUM SPECTRA FROM THE BESS-POLAR LONG-DURATION BALLOON FLIGHTS OVER ANTARCTICA

Energy Technology Data Exchange (ETDEWEB)

Abe, K.; Itazaki, A.; Kusumoto, A.; Matsukawa, Y.; Orito, R. [Kobe University, Kobe, Hyogo 657-8501 (Japan); Fuke, H. [Institute of Space and Astronautical Science, Japan Aerospace Exploration Agency (ISAS/JAXA), Sagamihara, Kanagawa 252-5210 (Japan); Haino, S.; Hasegawa, M.; Horikoshi, A.; Kumazawa, T.; Makida, Y.; Matsuda, S.; Matsumoto, K.; Nozaki, M. [High Energy Accelerator Research Organization (KEK), Tsukuba, Ibaraki 305-0801 (Japan); Hams, T.; Mitchell, J. W. [NASA-Goddard Space Flight Center (NASA-GSFC), Greenbelt, MD 20771 (United States); Kim, K. C.; Lee, M. H.; Myers, Z. [IPST, University of Maryland, College Park, MD 20742 (United States); Nishimura, J., E-mail: Kenichi.Sakai@nasa.gov [The University of Tokyo, Bunkyo, Tokyo 113-0033 (Japan); and others

2016-05-10

The BESS-Polar Collaboration measured the energy spectra of cosmic-ray protons and helium during two long-duration balloon flights over Antarctica in 2004 December and 2007 December at substantially different levels of solar modulation. Proton and helium spectra probe the origin and propagation history of cosmic rays in the galaxy, and are essential to calculations of the expected spectra of cosmic-ray antiprotons, positrons, and electrons from interactions of primary cosmic-ray nuclei with the interstellar gas, and to calculations of atmospheric muons and neutrinos. We report absolute spectra at the top of the atmosphere for cosmic-ray protons in the kinetic energy range 0.2–160 GeV and helium nuclei in the range 0.15–80 GeV/nucleon. The corresponding magnetic-rigidity ranges are 0.6–160 GV for protons and 1.1–160 GV for helium. These spectra are compared to measurements from previous BESS flights and from ATIC-2, PAMELA, and AMS-02. We also report the ratio of the proton and helium fluxes from 1.1 to 160 GV and compare this to the ratios from PAMELA and AMS-02.

A Comparison Between Spectral Properties of ULXs and Luminous X-ray Binaries

Science.gov (United States)

Berghea, C. T.; Colbert, E. J. M.; Roberts, T. P.

2004-05-01

What is special about the 1039 erg s-1 limit that is used to define the ULX class? We investigate this question by analyzing Chandra X-ray spectra of 71 X-ray bright point sources from nearby galaxies. Fifty-one of these sources are ULXs (LX(0.3-8.0 keV) ≥ 1039 erg s-1), and 20 sources (our comparison sample) are less-luminous X-ray binaries with LX(0.3-8.0 keV) = 1038-39 erg s-1. Our sample objects were selected from the Chandra archive to have ≥1000 counts and thus represent the highest quality spectra in the Chandra archives for extragalactic X-ray binaries and ULXs. We fit the spectra with one-component models (e.g., cold absorption with power-law, or cold absorption with multi-colored disk blackbody) and two-component models (e.g. absorption with both a power-law and a multi colored disk blackbody). A crude measure of the spectral states of the sources are determined observationally by calibrating the strength of the disk (blackbody) and coronal (power-law) components. These results are then use to determine if spectral properties of the ULXs are statistically distinct from those of the comparison objects, which are assumed to be ``normal'' black-hole X-ray binaries.

Valence-to-core-detected X-ray absorption spectroscopy

DEFF Research Database (Denmark)

Hall, Eleanor R.; Pollock, Christopher J.; Bendix, Jesper

2014-01-01

X-ray absorption spectroscopy (XAS) can provide detailed insight into the electronic and geometric structures of transition-metal active sites in metalloproteins and chemical catalysts. However, standard XAS spectra inherently represent an average contribution from the entire coordination...... environment with limited ligand selectivity. To address this limitation, we have investigated the enhancement of XAS features using valence-to-core (VtC)-detected XAS, whereby XAS spectra are measured by monitoring fluorescence from valence-to-core X-ray emission (VtC XES) events. VtC emission corresponds...... to transitions from filled ligand orbitals to the metal 1s core hole, with distinct energetic shifts for ligands of differing ionization potentials. VtC-detected XAS data were obtained from multiple valence emission features for a series of well-characterized Mn model compounds; taken together, these data...

X-Ray Measurements Of A Thermo Scientific P385 DD Neutron Generator

International Nuclear Information System (INIS)

Wharton, C. J.; Seabury, E. H.; Chichester, D. L.; Caffrey, A. J.; Simpson, J.; Lemchak, M.

2011-01-01

Idaho National Laboratory is experimenting with electrical neutron generators, as potential replacements for californium-252 radioisotopic neutron sources in its PINS prompt gamma-ray neutron activation analysis (PGNAA) system for the identification of military chemical warfare agents and explosives. In addition to neutron output, we have recently measured the x-ray output of the Thermo Scientific P385 deuterium-deuterium neutron generator. X rays are a normal byproduct from neutron generators, but depending on their intensity and energy, x rays can interfere with gamma rays from the object under test, increase gamma-spectrometer dead time, and reduce PGNAA system throughput. The P385 x-ray energy spectrum was measured with a high-purity germanium (HPGe) detector, and a broad peak is evident at about 70 keV. To identify the source of the x rays within the neutron generator assembly, it was scanned by collimated scintillation detectors along its long axis. At the strongest x-ray emission points, the generator also was rotated 60 deg. between measurements. The scans show the primary source of x-ray emission from the P385 neutron generator is an area 60 mm from the neutron production target, in the vicinity of the ion source. Rotation of the neutron generator did not significantly alter the x-ray count rate, and its x-ray emission appears to be axially symmetric. A thin lead shield, 3.2 mm (1/8 inch) thick, reduced the 70-keV generator x rays to negligible levels.

X-ray beam size measurements on the Advanced Test Accelerator

International Nuclear Information System (INIS)

Struve, K.W.; Chambers, F.W.; Lauer, E.J.; Slaughter, D.R.

1986-01-01

The electron beam size has been determined on the Advanced Test Accelerator (ATA) by intercepting the beam with a target and measuring the resulting x-ray intensity as a function of time as the target is moved through the beam. Several types of targets have been used. One is a tantalum rod which extends completely across the drift chamber. Another is a tungsten powder filled carbon crucible. Both of these probes are moved from shot to shot so that the x-ray signal intensity varies with probe position. A third is a larger tantalum disk which is inserted on beam axis to allow determining beam size on a one shot basis. The x-ray signals are detected with an MCP photomultiplier tube located at 90 0 to the beamline. It is sufficiently shielded to reject background x-rays and neutrons. The signals were digitized, recorded and later unfolded to produce plots of x-ray intensity versus probe position for several times during the pulse. The presumption that the x-ray intensity is proportional to beam current density is checked computationally. Details of the probe construction and PMT shielding, as well as sample measurements are given

Quantitative schemes in energy dispersive X-ray fluorescence implemented in AXIL

International Nuclear Information System (INIS)

Tchantchane, A.; Benamar, M.A.; Tobbeche, S.

1995-01-01

E.D.X.R.F (Energy Dispersive X-ray Fluorescence) has long been used for quantitative analysis of many types of samples including environment samples. the software package AXIL (Analysis of x-ray spectra by iterative least quares) is extensively used for the spectra analysis and the quantification of x-ray spectra. It includes several methods of quantitative schemes for evaluating element concentrations. We present the general theory behind each scheme implemented into the software package. The spectra of the performance of each of these quantitative schemes. We have also investigated their performance relative to the uncertainties in the experimental parameters and sample description

X-ray determination of charge states of ions moving in solids

International Nuclear Information System (INIS)

Fortner, R.J.; Matthews, D.L.

1974-02-01

The first part of this work discusses previous measurements of x-ray spectra and thick-target yields for Ar ions moving in solid graphite targets. These data are strongly affected by ''solid target effects.'' There are some rather serious limitations in the above measurements. This proposal solicits funds to expand the program to eliminate the limitations. The second part of the proposal contains a more detailed presentation of three types of measurements. These involve the extension of work to other collision systems, the development of an Auger electron spectrometer, and the use of a 7-m grazing-incidence spectrograph for x-ray spectroscopy. These measurements will enable testing of current pictures describing ions moving in solids and shed light on the feasibility of producing a beam of ions which could give rise to amplified stimulated x-ray emission (x-ray laser). (11 figures) (U.S.)

X-ray stress measurement by use of synchrotron radiation source

International Nuclear Information System (INIS)

Yoshioka, Yasuo; Matsui, Hisaaki; Moro-oka, Toshimasa; Hasegawa, Ken-ichi; Nakajima, Tetsuo.

1986-01-01

In the field of X-ray stress measurement of polycrystalline materials, a diffraction plane at higher Bragg angle has to be selected in order to obtain the precise value of stress. However, the stress measurement on an optional (hkl) plane desired is not always possible because the X-ray beam exited from a metal target has a dispersive wave length. Recently, we have been able to use the synchrotron radiation source (SR) as an excellent X-ray source. In Japan, the facility of synchrotron radiation (Photon Factory, PF) was constructed in the National Laboratory for High Energy Physics (KEK) at Tsukuba academic city. The use of this SR enables the stress measurements on many (hkl) planes with high accuracy in the higher Bragg angle region by providing an X-ray beam having an optional wave length. We have started the X-ray stress analysis by use of the synchrotron radiation source. This paper reports the system of measurement and some results of preliminaly experiments. Since a monochromatic X-ray beam is required for the stress measurement, we used a beam line which consists of a double crystal monochrometer and a focusing mirror. X-rays between 4 KeV (λ = 0.31 nm) and 10 KeV (λ = 0.12 nm) are available with this optical system. We adopted a constant Bragg angle of 2θ = 154 deg for all the diffraction planes. A PSPC having a carbon fiber anode is made and used as a detector with the use of a fast digital signal processor. We could observe the diffraction profiles from (200), (211), (220), (310) and (321) crystal plane of alpha iron, respectively, and the residual stresses in these planes except the (200) plane were measured with high accuracy in a short time. Such feature especially suits the stress analysis of the material which has preferred orientation or stress gradient. (author)

Measurement of x-ray scattering cross sections of hydrogen and helium with synchrotron radiation

International Nuclear Information System (INIS)

Ice, G.E.

1977-01-01

Total x-ray scattering is a two-electron expectation value. The prominence of the electron correlation effect was demonstrated in recent theoretical work. Only one measurement of x-ray scattering from H 2 has been reported heretofore, nearly fifty years ago. New measurements were carried out using the virtually monochromatic, intense flux of synchrotron radiation in the SSRP EXAFS line. The targets, at 1 atm pressure, were UHP He and ultrapure H 2 that had been passed through a hot Pd--Ag alloy diffusion purifier. The scattered-photon spectra were measured with a Xe-filled proportional counter and fast multichannel analyzer. The incident flux was monitored with a parallel-plate ion chamber, calibrated by direct counting of the absorber-attenuated beam. Measurements were performed at 5, 6, and 7 keV photon energy, as a function of scattering angle (60, 90, and 135 deg) and azimuthal angle (i.e., polarization). The relative total differential photon scattering cross sections for H 2 over the range 3.0 less than or equal to x = 4πsin (theta/2)lambda less than or equal to 5.6 A -1 agree to within approx. 1% with the correlated calculations of Bentley and Stewart. The ratios of measured cross sections for H 2 to those for He at x = 3.0 and 5.6 A -1 agree to within 1% with the ratios of the Bentley--Stewart H 2 cross sections to the correlated wave-function calculations of Brown for He

X-ray photoelectron spectra structure and chemical bonding in AmO2

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Teterin Yury A.

2015-01-01

Full Text Available Quantitative analysis was done of the X-ray photoelectron spectra structure in the binding energy range of 0 eV to ~35 eV for americium dioxide (AmO2 valence electrons. The binding energies and structure of the core electronic shells (~35 eV-1250 eV, as well as the relativistic discrete variation calculation results for the Am63O216 and AmO8 (D4h cluster reflecting Am close environment in AmO2 were taken into account. The experimental data show that the many-body effects and the multiplet splitting contribute to the spectral structure much less than the effects of formation of the outer (0-~15 eV binding energy and the inner (~15 eV-~35 eV binding energy valence molecular orbitals. The filled Am 5f electronic states were shown to form in the AmO2 valence band. The Am 6p electrons participate in formation of both the inner and the outer valence molecular orbitals (bands. The filled Am 6p3/2 and the O 2s electronic shells were found to make the largest contributions to the formation of the inner valence molecular orbitals. Contributions of electrons from different molecular orbitals to the chemical bond in the AmO8 cluster were evaluated. Composition and sequence order of molecular orbitals in the binding energy range 0-~35 eV in AmO2 were established. The experimental and theoretical data allowed a quantitative scheme of molecular orbitals for AmO2, which is fundamental for both understanding the chemical bond nature in americium dioxide and the interpretation of other X-ray spectra of AmO2.

Recent X-ray hybrid CMOS detector developments and measurements

Science.gov (United States)

Hull, Samuel V.; Falcone, Abraham D.; Burrows, David N.; Wages, Mitchell; Chattopadhyay, Tanmoy; McQuaide, Maria; Bray, Evan; Kern, Matthew

2017-08-01

The Penn State X-ray detector lab, in collaboration with Teledyne Imaging Sensors (TIS), have progressed their efforts to improve soft X-ray Hybrid CMOS detector (HCD) technology on multiple fronts. Having newly acquired a Teledyne cryogenic SIDECARTM ASIC for use with HxRG devices, measurements were performed with an H2RG HCD and the cooled SIDECARTM. We report new energy resolution and read noise measurements, which show a significant improvement over room temperature SIDECARTM operation. Further, in order to meet the demands of future high-throughput and high spatial resolution X-ray observatories, detectors with fast readout and small pixel sizes are being developed. We report on characteristics of new X-ray HCDs with 12.5 micron pitch that include in-pixel CDS circuitry and crosstalk-eliminating CTIA amplifiers. In addition, PSU and TIS are developing a new large-scale array Speedster-EXD device. The original 64 × 64 pixel Speedster-EXD prototype used comparators in each pixel to enable event driven readout with order of magnitude higher effective readout rates, which will now be implemented in a 550 × 550 pixel device. Finally, the detector lab is involved in a sounding rocket mission that is slated to fly in 2018 with an off-plane reflection grating array and an H2RG X-ray HCD. We report on the planned detector configuration for this mission, which will increase the NASA technology readiness level of X-ray HCDs to TRL 9.

X-ray fluorescence/Auger-electron coincidence spectroscopy of vacancy cascades in atomic argon

International Nuclear Information System (INIS)

Arp, U.

1996-01-01

Argon L 2.3 -M 2.3 M 2.3 Auger-electron spectra were measured in coincidence with Kα fluorescent x-rays in studies of Ar K-shell vacancy decays at several photon energies above the K-threshold and on the 1s-4p resonance in atomic argon. The complex spectra recorded by conventional electron spectroscopy are greatly simplified when recorded in coincidence with fluorescent x-rays, allowing a more detailed analysis of the vacancy cascade process. The resulting coincidence spectra are compared with Hartree-Fock calculations which include shake-up transitions in the resonant case. Small energy shifts of the coincidence electron spectra are attributed to post-collision interaction with 1s photoelectrons

Resonant inelastic X-ray scattering spectra at the Ir L-edge in Na{sub 2}IrO{sub 3}

Energy Technology Data Exchange (ETDEWEB)

Igarashi, Jun-ichi, E-mail: junichi.igarashi.kiryu@vc.ibaraki.ac.jp [Faculty of Science, Ibaraki University, Mito, Ibaraki 310-8512 (Japan); Nagao, Tatsuya, E-mail: nagao@gunma-u.ac.jp [Faculty of Engineering, Gunma University, Kiryu, Gunma 376-8515 (Japan)

2016-10-15

Highlights: • A theoretical framework of resonant inelastic X-ray scattering (RIXS) on the basis of the itinerant electron scheme has been developed. • The RIXS theory is applied to iridate Na{sub 2}IrO{sub 3}. • The origins of the multi-peak structure of the excitation spectra found in the RIXS experiment have been assigned to the magnetic and excitonic excitations. - Abstract: We analyze resonant X-ray scattering (RIXS) spectra in Na{sub 2}IrO{sub 3} on the basis of the itinerant electron picture. Employing a multi-orbital tight-binding model on a honeycomb lattice, we find that the zigzag magnetic order is the most stable with sizable energy gap in the one-electron band within the Hartree–Fock approximation. We derive the RIXS spectra, which are connected to the generalized density–density correlation function. We calculate the spectra as a function of excitation energy ω, within the random phase approximation. The spectra consist of the peaks with ω < 20 meV, and of the peaks with 0.4 < ω < 0.8 eV. The former peaks are composed of four bound states in the density–density correlation function, and may be identified as the magnetic excitations, while the latter peaks are composed of 16 bound states below the energy continuum of individual electron–hole pair excitations, and may be identified as the excitonic excitations. The calculated spectra agree qualitatively with the recent RIXS experiment.

Energy dependence measurement of small-type optically stimulated luminescence (OSL) dosimeter by means of characteristic X-rays induced with general diagnostic X-ray equipment.

Science.gov (United States)

Takegami, Kazuki; Hayashi, Hiroaki; Okino, Hiroki; Kimoto, Natsumi; Maehata, Itsumi; Kanazawa, Yuki; Okazaki, Tohru; Hashizume, Takuya; Kobayashi, Ikuo

2016-01-01

For X-ray inspections by way of general X-ray equipment, it is important to measure an entrance-skin dose. Recently, a small optically stimulated luminescence (OSL) dosimeter was made commercially available by Landauer, Inc. The dosimeter does not interfere with the medical images; therefore, it is expected to be a convenient detector for measuring personal exposure doses. In an actual clinical situation, it is assumed that X-rays of different energies will be detected by a dosimeter. For evaluation of the exposure dose measured by a dosimeter, it is necessary to know the energy dependence of the dosimeter. Our aim in this study was to measure the energy dependence of the OSL dosimeter experimentally in the diagnostic X-ray region. Metal samples weighing several grams were irradiated and, in this way, characteristic X-rays having energies ranging from 8 to 85 keV were generated. Using these mono-energetic X-rays, the dosimeter was irradiated. Simultaneously, the fluence of the X-rays was determined with a CdTe detector. The energy-dependent efficiency of the dosimeter was derived from the measured value of the dosimeter and the fluence. Moreover, the energy-dependent efficiency was calculated by Monte-Carlo simulation. The efficiency obtained in the experiment was in good agreement with that of the simulation. In conclusion, our proposed method, in which characteristic X-rays are used, is valuable for measurement of the energy dependence of a small OSL dosimeter in the diagnostic X-ray region.

Investigation of the antiprotonic X-ray spectra of the isotopes 6Li, 7Li and 40Ca

International Nuclear Information System (INIS)

Barth, H.

1987-04-01

With the commissioning of the Low-Energy Antiproton Ring (LEAR) at CERN in Geneva a high intensity, high purity antiproton beam became available, enabling precision measurements of antiprotonic X-ray spectra to be carried out. Besides informations about properties of the elementary particle antiproton itself, as for example its mass and its magnetic moment, such measurements provide informations about the strong-interaction potential between antiproton and nucleus at very low energies, which, in turn, can be derived from the elementary antinucleon-nucleon interaction by using microscopic models. This work investigates the antiprotonic X-ray spectra of the isotopes 6 Li, 7 Li and 40 Ca. The data were taken during the experiment PS176 at LEAR. The strong interaction between antiproton and nucleus leads to an energy shift ε and an absorption width Γ of the lower level of the last observable transition and also to intensity reductions, which can be converted to an absorption width for the upper level. For the isotopes 6 Li, 7 Li and 40 Ca the following results were obtained: 6 Li: ε(2p)=(-215±25) eV, Γ(2p)=(660±170) eV and Γ(3d)=(135±16) meV, 7 Li ε(2p)=(-265±20) eV, Γ(2p)=(690±170) eV and Γ(3d)=(129±13) meV, 40 Ca: ε(4f)=(-1060±130) eV, Γ(4f)=(3670±600) eV and Γ(5g)=(34.9±3.3) eV. The results are in fair agreement with theoretical calculations, at the same time showing up the limits of present understanding of antiproton-nucleus interaction. Particularly the spin-orbit part of the strong interaction seems to play a nonnegligible role. (orig.) [de

Measuring Cavitation with Synchrotron X-Rays

Science.gov (United States)

Duke, Daniel; Kastengren, Alan; Powell, Chris; X-Ray Fuel Spray Group, Energy Systems Division Team

2012-11-01

Cavitation plays an important role in the formation of sprays from small nozzles such as those found in fuel injection systems. A sharp-edged inlet from the sac into the nozzle of a diesel fuel injector is shown to inititate a strong sheet-like cavitation along the boundary layer of the nozzle throat, which is difficult to measure and can lead to acoustic damage. To investigate this phenomenon, a diagnostic technique capable of mapping the density field of the nozzle through regions of intense cavitation is required. Available visible-light techniques are limited to qualitative observations of the outer extent of cavitation zones. However, brilliant X-rays from a synchrotron source have negligible refraction and are capable of penetrating the full extent of cavitation zones. We present the early results of a novel application of line-of-sight, time-resolved X-ray radiography on a cavitating model nozzle. Experiments were conducted at Sector 7-BM of the Advanced Photon Source. Density and vapor distribution are measured from the quantitative absorption of monochromatic X-rays. The density field can then be tomographically reconstructed from the projections. The density is then validated against a range of compressible and incompressible numerical simulations. This research was performed at the 7-BM beamline of the Advanced Photon Source. We acknowledge the support of the U.S. Department of Energy under Contract No. DE-AC02-06CH11357 and the DOE Vehicle Technologies Program (DOE-EERE).