WorldWideScience

Sample records for material heat treatment

  1. Plasma treatment of heat-resistant materials

    International Nuclear Information System (INIS)

    Vlasov, V A; Kosmachev, P V; Skripnikova, N K; Bezukhov, K A

    2015-01-01

    Refractory lining of thermal generating units is exposed to chemical, thermal, and mechanical attacks. The degree of fracture of heat-resistant materials depends on the chemical medium composition, the process temperature and the material porosity. As is known, a shortterm exposure of the surface to low-temperature plasma (LTP) makes possible to create specific coatings that can improve the properties of workpieces. The aim of this work is to produce the protective coating on heat-resistant chamotte products using the LTP technique. Experiments have shown that plasma treatment of chamotte products modifies the surface, and a glass-ceramic coating enriched in mullite is formed providing the improvement of heat resistance. For increasing heat resistance of chamotte refractories, pastes comprising mixtures of Bacor, alumina oxide, and chamot were applied to their surfaces in different ratios. It is proved that the appropriate coating cannot be created if only one of heat-resistant components is used. The required coatings that can be used and recommended for practical applications are obtained only with the introduction of powder chamot. The paste composition of 50% chamot, 25% Bacor, and 25% alumina oxide exposed to plasma treatment, has demonstrated the most uniform surface fusion. (paper)

  2. Uninterrupted heat-treatment of starch raw materials

    Energy Technology Data Exchange (ETDEWEB)

    Bronshtein, D Z

    1958-01-01

    A setup is presented, with a Rekord grinder, a Khronos scale, and other equipment of Soviet manufacture, in which oats, rye, wheat, and other grains are treated at 42 to 45 degrees prior to their use as raw materials in the ethanol industry. These materials are analyzed with respect to H/sub 2/O, starch, bulk, weight, screen analysis, and the final ethanol yields/ton of such raw materials. In a three year run in plant, this heat-treatment was advantageous, as compared to the former treatment of the starch materials.

  3. Uninterrupted heat-treatment of starch raw materials

    Energy Technology Data Exchange (ETDEWEB)

    Bronshtein, D Z

    1958-01-01

    A setup is presented, with a Rekord grinder, a Khronos scale, and other equipment of Soviet manufacture, in which oats, rye, wheat, and other grains are treated at 42 to 45/sup 0/ prior to their use as raw materials in the ethanol industry. These materials are analyzed with respect to H/sub 2/O, starch, bulk weight, screen analysis, and the final ethanol yields/ton of such raw materials. In a three year run in a plant, this heat-treatment was advantageous, as compared to the former treatment of the starch materials.

  4. Improved process for the treatment of bituminous materials. [two heat treatments

    Energy Technology Data Exchange (ETDEWEB)

    1947-04-30

    A continuous process for recovering valuable hydrocarbon oils from solid minerals adapted to produce such oils upon application of heat, consists of reducing the raw minerals to a powder, suspending the powdered minerals in a gaseous medium and subjecting the suspension thus formed to heat treatment in a primary reaction zone, followed by heat treatment in a secondary reaction zone separate from the primary reaction zone. The temperature during the second of said treatments being substantially higher than that of the first.

  5. Evaluation of the Characteristics of the Aluminum Alloy Casting Material by Heat Treatment

    International Nuclear Information System (INIS)

    Lee, Syung Yul; Park, Dong Hyun; Won, Jong Pil; Kim, Yun Hae; Lee, Myung Hoon; Moon, Kyung Man; Jeong, Jae Hyun

    2012-01-01

    Aluminum is on active metal, but it is well known that its oxide film plays a role as protective barrier which is comparatively stable in air and neutral aqueous solution. Thus, aluminum alloys have been widely applied in architectural trim, cold and hot-water storage vessels and piping etc., furthermore, the aluminum alloy of AC8A have been widely used in mold casting material of engine piston because of its properties of temperature and wear resistance. In recent years, the oil price is getting higher and higher, thus the using of low quality oil has been significantly increased in engines of ship and vehicle. Therefore it is considered that evaluation of corrosion resistance as well as wear resistance of AC8A material is also important to improve its property and prolong its lifetime. In this study, the effect of solution and tempering heat treatment to corrosion and wear resistance is investigated with electrochemical method and measurement of hardness. The hardness decreased with solution heat treatment compared to mold casting condition, but its value increased with tempering heat treatment and exhibited the highest value of hardness with tempering heat treatment temperature at 190 .deg. C for 24hrs. Furthermore, corrosion resistance increased with decreasing of the hardness, and decreased with increasing of the hardness reversely. As a result, it is suggested that the optimum heat treatment to improve both corrosion and wear resistance is tempering heat treatment temperature at 190 .deg. C for 16hrs

  6. Study on mechanical properties of the laminated composite materials with compatible heat treatments

    International Nuclear Information System (INIS)

    Pashkov, P.O.; Pektemirov, B.G.; Yaroshenko, A.P.

    1980-01-01

    Considered is the behaviour during axial extension of trilament composite materials, the mechanical properties of which are formed mainly by heat treatment. Application in the composite of the materials with compatible heat treatment is most rational. It is shown that for (ATsMg+N18K8M5T+ATsMg), (KhN78+VKS+KhH78) composites, the constituents of which are relatively plastic and tightly bound with each other, the tensile strength and uniform strain are changed additively

  7. Preliminary study on the forgeability and heat treatment response of niobium - containing tool steels materials

    International Nuclear Information System (INIS)

    Cescon, T.; Papaleo, R.

    1981-01-01

    The forgeability and microstructure of tool steels materials based on the M-2 composition, where W and V were partially replaced by Nb, were examined. The optimum heat-treating conditions were established. The poor response to heat treatment of some of the alloys studied indicated the need of increasing the C content of the steels when Nb is used as a substitute for W and V. (Author) [pt

  8. Investigation of heat treatment conditions of structural material for blanket fabrication process

    International Nuclear Information System (INIS)

    Hirose, Takanori; Suzuki, Satoshi; Akiba, Masato; Shiba, Kiyoyuki; Sawai, Tomotsugu; Jitsukawa, Shiro

    2004-01-01

    This paper presents recent results of thermal hysteresis effects on ceramic breeder blanket structural material. Reduced activation ferritic/martensitic (RAF) steel is the leading candidates for the first wall structural materials of breeding blankets. RAF steel demonstrates superior resistance to high dose neutron irradiation, because the steel has tempered martensite structure which contains the number of sink site for radiation defects. This microstructure obtained by two-step heat treatment, first is normalizing at temperature above 1200 K and the second is tempering at temperature below 1100 K. Recent study revealed the thermal hysteresis has significant impacts on the post-irradiation mechanical properties. The breeding blanket has complicated structure, which consists of tungsten armor and thin first wall with cooling pipe. The blanket fabrication requires some high temperature joining processes. Especially hot isostatic pressing (HIP) is examined as a near-net-shape fabrication process for this structure. The process consists of heating above 1300 K and isostatic pressing at the pressure above 150 MPa followed by tempering. Moreover ceramics pebbles are packed into blanket module and the module is to be seamed by welding followed by post weld heat treatment in the final assemble process. Therefore the final microstructural features of RAFs strongly depend on the blanket fabrication process. The objective of this work is to evaluate the effects of thermal hysteresis corresponding to blanket fabrication process on RAFs microstructure in order to establish appropriate blanket fabrication process. Japanese RAFs F82H (Fe-0.1C-8Cr-2W-0.2V-0.05Ta) was investigated by metallurgical method after isochronal heat treatment up to 1473 K simulating high temperature bonding process. Although F82H showed significant grain growth after conventional solid HIP conditions (1313 K x 2 hr.), this coarse grained microstructure was refined by the post HIP normalizing at

  9. Microbial safety control of compost material with cow dung by heat treatment.

    Science.gov (United States)

    Gong, Chun-ming

    2007-01-01

    Various kinds of pathogenic bacteria derived from the intestinal tract of animals exist in compost material like cow dung. In order to sterilize the pathogenic bacteria completely in compost material, the cow dung was put into a heat treatment machine in pilot plan, and harmless condition in short time was examined. The results indicated, pathogenic indicator bacteria such as coliform bacteria, fecal coliform, Escherichia coli and salmonella were all 106 cfu/g dw at the beginning, died rapidly when cow dung temperature rose to above 50 degrees C, and not detected at 54-68 degrees C for 6-24 h heat treatment. Coliform bacteria and salmonella in heated cow dung were not detected by re-growth culture and enrichment culture examination. Moreover, it was hardly influenced on the fermentation ability of composting microbe, organic decomposition bacteria. During heat treatment, the mesophile decreased rapidly and the thermophile stabilized or increased, and the most of composting microbe were bacillus in cow dung by fluorescence microscope, this indicated that bacillus was dominator and composting microbe in composting process.

  10. Increase of efficiency of plant materials heat treatment in tubular reactors

    Directory of Open Access Journals (Sweden)

    A. V. Golubkovich

    2016-01-01

    Full Text Available In agriculture products of pyrolysis of plant materials in the form of waste of the main production can be applied as a source of heat and electric power. Besides, their use prevents ecological pollution of the soil and the atmosphere. Pyrolysis plants can be used for work with tubular reactors anywhere. Due to them farmers can dry grain, using waste heat of diesel generators, heatgenerators, boiler plants and receiving thus gaseous products, liquid and firm fractions. A technology based on cyclic and continuous plant mass movement by a piston in a pipe from a loading site to a place of unloading of a firm phase consistently through cameras of drying, pyrolysis, condensation of gaseous products. Exhaust furnace gases with a temperature up to 600 degrees Celsius are given countercurrent material movement from a power equipment. The gaseous, liquid and firm products from the pyrolysis camera are used for heat and electric power generation. Calculation of parameters of subdrying and pyrolysis cameras is necessary for effective and steady operation of the tubular reactor. The authors determined the speed of raw materials movement, and also duration of drying and pyrolysis in working chambers. An analysis of a simplified mathematical model of process was confirmed with results of experiments. Models of heat treatment of wet plant materials in tubular reactors are worked out on a basis of equality of speeds of material movement in the reactor and distribution of a temperature front in material on radius. The authors defined estimated characteristic for determination of tubular reactor productivity and size of heat, required for drying and pyrolysis.

  11. Corrosion resistance of structural material AlMg-2 in water following heat treatment and cooling

    International Nuclear Information System (INIS)

    Maman Kartaman A; Djoko Kisworo; Dedi Hariyadi; Sigit

    2005-01-01

    Corrosion tests of structural material AlMg-2 in water were carried out using autoclave in order to study the effects of heat treatment on the corrosion resistance of the material. Prior to the tests, the samples were heat-treated at temperatures of 90, 200, 300 and 500 °C and cooled in air, sand and water. The corrosion tests were conducted in water at temperature of 150 °C for 250 hours. The results showed that AlMg-2 samples were corroded although the increase of mass gain was relatively small. Heat treatment from 90 to 500 °C in sand cooling media resulted in an increase of mass gain despite that at 300 °C the increase was less than those at 200 °C and 500 °C. For water cooling media in the temperature range of 90 to 200 °C, the mass gain increased from 0.1854 g/cm 2 to 2.1204 g/cm 2 although after 200 °C it decreased to 1.8207 g/cm 2 and 1.6779 g/cm 2 respectively. For air cooling media, the mass gain was relatively constant. Based on the experiment results, it can be concluded that heat treatment and cooling did not significantly influence the corrosion resistance of material AlMg-2. The passive film Al 2 O 3 on the surface was able to protect the inner surface from further corrosion. Water media with pH range from 4 – 9 did not cause damage to passive layer formed. (author)

  12. Apparatus with moderating material for microwave heat treatment of manufactured components

    Science.gov (United States)

    Ripley, Edward B [Knoxville, TN

    2011-05-10

    An apparatus for heat treating manufactured components using microwave energy and microwave susceptor material. Heat treating medium such as eutectic salts may be employed. A fluidized bed introduces process gases which may include carburizing or nitriding gases The process may be operated in a batch mode or continuous process mode. A microwave heating probe may be used to restart a frozen eutectic salt bath.

  13. Effect of heat treatment and composition on stress corrosion cracking of steam generation tubing materials

    International Nuclear Information System (INIS)

    Kim, H. P.; Hwang, S. S.; Kuk, I. H.; Kim, J. S.; Oh, C. Y.

    1998-01-01

    Effects of heat treatment and alloy composition on stress corrosion cracking (SCC) of steam generator tubing materials have been studied in 40% NaOH at 315.deg.C at potential of +200mV above corrosion potential using C-ring specimen and reverse U bend specimen. The tubing materials used were commercial Alloy 600, Alloy 690 and laboratory alloys, Ni-χCr-10Fe. Commercial Alloy 600, Alloy 690 were mill annealed or thermally treated.Laboratory alloy Ni-χCr-10Fe, and some of Alloy 600 and Alloy 690 were solution annealed. Polarization curves were measured to find out any relationship between SCC susceptibility and electrochemical behaviour. The variation in thermal treatment of Alloy 600 and Alloy 690 had no effect on polarization behaviour probably due to small area fraction of carbide and Cr depletion zone near grain boundary. In anodic polarization curves, the first and second anodic peaks at about 170mV and about at 260mV, respectively, above corrosion potential were independent of Cr content, whereas the third peak at 750mV above corrosion potential and passive current density in-creased with Cr content. SCC susceptibility decreased with Cr content and thermal treatment producing semicontinuous grain boundary decoration. Examination of cross sectional area of C-ring specimen showed deep SCC cracks for the alloys with less than 17%Cr and many shallow attacks for alloy 690. The role of Cr content in steam generator tubing materials and grain boundary carbide on SCC were discussed

  14. Surface Observation and Pore Size Analyses of Polypropylene/Low-Melting Point Polyester Filter Materials: Influences of Heat Treatment

    Directory of Open Access Journals (Sweden)

    Lin Jia-Horng

    2016-01-01

    Full Text Available This study proposes making filter materials with polypropylene (PP and low-melting point (LPET fibers. The influences of temperatures and times of heat treatment on the morphology of thermal bonding points and average pore size of the PP/LPET filter materials. The test results indicate that the morphology of thermal bonding points is highly correlated with the average pore size. When the temperature of heat treatment is increased, the fibers are joined first with the thermal bonding points, and then with the large thermal bonding areas, thereby decreasing the average pore size of the PP/LPET filter materials. A heat treatment of 110 °C for 60 seconds can decrease the pore size from 39.6 μm to 12.0 μm.

  15. Curie Temperature and Microstructural Changes Due to the Heating Treatment of Magnetic Amorphous Materials

    Directory of Open Access Journals (Sweden)

    Gondro J.

    2016-03-01

    Full Text Available Three distinct alloys: Fe86Zr7Nb1Cu1B5, Fe82Zr7Nb2Cu1B8, and Fe81Pt5Zr7Nb1Cu1B5 were characterized both magnetically and structurally. The samples, obtained with spinning roller method as a ribbons 3 mm in width and 20 μm thick, were investigated as-quenched and after each step of a multi steps heating treatment procedure. Each sample was annealed at four steps, fifteen minutes at every temperature, starting from 573K+600K up to +700K depending on type of alloy. Mössbauer spectroscopy data and transmission electron microscope (HRE M pictures confirmed that the as-quenched samples are fully amorphous. This is not changed after the first stages of treatment heating leads to a reduction of free volumes. The heating treatment has a great influence on the magnetic susceptibilities. The treatment up to 600K improves soft magnetic properties: an χ increase was observed, from about 400 to almost 1000 for the samples of alloys without Pt, and from about 200 to 450 at maximum, for the Fe81Pt5Zr7Nb1Cu1B5. Further heating, at more elevated temperatures, leads to magnetic hardening of the samples. Curie temperatures, established from the location of Hopkinson’s maxima on the χ(T curve are in very good agreement with those obtained from the data of specific magnetization, σ(T, measured in a field of 0.75T. As a critical parameter β was chosen to be equal 0.36 for these calculations, it confirmed that the alloys may be considered as ferromagnetic of Heisenberg type. Heating treatment resulted in decreasing of TC. These changes are within a range of several K.

  16. The Effect of Heat Treatment on the Pull-off Strength of Optionally Varnished Surfaces of Five Wood Materials

    Directory of Open Access Journals (Sweden)

    Musa Atar

    2015-09-01

    Full Text Available This study investigated the effects of heat treatment, following optional treatment with synthetic, water-based, and alkyd varnishes, on the pull-off strength of wooden materials sampled from oriental beech (Fagus orientalis L., oak (Quercus petraea Liebl., black poplar (Populus nigra L., pine (Pinus sylvestris L., and fir (Abies bornmulleriana M.. The test samples were subjected to heat treatment at temperatures of 165 °C and 175 °C for periods of 2 and 4 h with a total of 4 variations. With respect to the wood type, the samples of beech wood yielded the highest results for pull-off strength, while fir wood yielded the lowest. With respect to the varnish types, the highest pull-off strength was found in the samples of synthetic varnished beech (5,452 with a 37.2% improvement at 175 °C heat treatment for 4 h, while the lowest results were obtained in the samples of fir (0.991 with a 48.5% decrease at 175 °C heat treatment for 4 h. In conclusion, heat treatment significantly decreased the pull-off strength of the woods.

  17. Simple approach to carboxyl-rich materials through low-temperature heat treatment of hydrothermal carbon in air

    Energy Technology Data Exchange (ETDEWEB)

    Chen Zhen; Ma Lijian; Li Shuqiong; Geng Junxia; Song Qiang; Liu Jun; Wang Chunli; Wang Hang; Li Juan [College of Chemistry, Sichuan University, Key Laboratory of Radiation Physics and Technology (Sichuan University), Ministry of Education, Chengdu 610064 (China); Qin Zhi [Institute of Modern Physics, Chinese Academy of Sciences, Lanzhou 730000 (China); Li Shoujian, E-mail: sjli000616@scu.edu.cn [College of Chemistry, Sichuan University, Key Laboratory of Radiation Physics and Technology (Sichuan University), Ministry of Education, Chengdu 610064 (China)

    2011-08-01

    It was found that a large number of oxygen-containing functional groups (OFGs) could be created on the surface of hydrothermal carbon (HTC) by simply heating at lower temperature in air during the course of our preliminary experiments which focused on oxidation pre-treatment of pristine HTC for the purpose of grafting functionalization. Especially carboxyl groups on HTC would increase significantly, from 0.53 to 3.70 mmol/g after heat treatment at 300 deg. C. So, effects of heat-treatment on the OFGs on the carbon microsphere were deeply studied to confirm and explain the findings. Experiments involving different materials (HTC, activated carbon and glucose) were performed under varying conditions (heating temperature and time, in air or in Ar atmosphere). A reaction mechanism for newly generating carboxyl groups on HTC surface during heat-treatment process was supposed based on the results from the sample characterization using Boehm titrations, infrared spectra, X-ray photoelectron spectroscopy, energy dispersive spectrometry and elemental analysis. In addition, the as heat-treated product has excellent sorption capability for Pb{sup 2+} and Cd{sup 2+} ions.

  18. Influence of heat treatment on hardness and kinetics of growth of intermetallic compound interlayer in titanium-steel composite material

    International Nuclear Information System (INIS)

    Shmorgun, V.G.; Slaustin, O.V.; Trykov, Yu.P.

    2005-01-01

    The effect of heat treatment conditions on microhardness and diffusion interlayer thickness is studied for composite material of titanium VT1-O + steel 08kp + titanium VT1-O. Heat treatments are carried out at temperatures of 800-1000 deg C and holding at heat for 3 h in a vacuum furnace (1 x 10 -4 mmHg) as well as in an electric furnace with coating a dual protective layer. It is stated that the hardness and the thickness of the interlayer are higher after heat treatment in an ordinary electric furnaces as compared to vacuum heating. all other things being equal. Annealed in electric furnace specimens are water quenched from temperatures of 600-950 deg C. It is shown that the hardness of the interlayer increases sharply when hardening from 650 deg C comparing with annealed specimens (from 4.5-5.2 to 7-9 GPa). The quenching from 700 and 800 deg C results in an interlayer hardness decrease down to 4.8-5.4 and 3.1-3 GPa respectively. A quenching temperature increase up to 800-900 deg C is accompanied by a monotonic enhancement of hardness from 3.5-4.8 up to 5.1-6.8 GPa [ru

  19. Heat-resistant materials

    CERN Document Server

    1997-01-01

    This handbook covers the complete spectrum of technology dealing with heat-resistant materials, including high-temperature characteristics, effects of processing and microstructure on high-temperature properties, materials selection guidelines for industrial applications, and life-assessment methods. Also included is information on comparative properties that allows the ranking of alloy performance, effects of processing and microstructure on high-temperature properties, high-temperature oxidation and corrosion-resistant coatings for superalloys, and design guidelines for applications involving creep and/or oxidation. Contents: General introduction (high-temperature materials characteristics, and mechanical and corrosion properties, and industrial applications); Properties of Ferrous Heat-Resistant Alloys (carbon, alloy, and stainless steels; alloy cast irons; and high alloy cast steels); Properties of superalloys (metallurgy and processing, mechanical and corrosion properties, degradation, and protective coa...

  20. Improve the material absorption of light and enhance the laser tube bending process utilizing laser softening heat treatment

    Science.gov (United States)

    Imhan, Khalil Ibraheem; Baharudin, B. T. H. T.; Zakaria, Azmi; Ismail, Mohd Idris Shah B.; Alsabti, Naseer Mahdi Hadi; Ahmad, Ahmad Kamal

    2018-02-01

    Laser forming is a flexible control process that has a wide spectrum of applications; particularly, laser tube bending. It offers the perfect solution for many industrial fields, such as aerospace, engines, heat exchangers, and air conditioners. A high power pulsed Nd-YAG laser with a maximum average power of 300 W emitting at 1064 nm and fiber-coupled is used to irradiate stainless steel 304 (SS304) tubes of 12.7 mm diameter, 0.6 mm thickness and 70 mm length. Moreover, a motorized rotation stage with a computer controller is employed to hold and rotate the tube. In this paper, an experimental investigation is carried out to improve the laser tube bending process by enhancing the absorption coefficient of the material and the mechanical formability using laser softening heat treatment. The material surface is coated with an oxidization layer; hence, the material absorption of laser light is increased and the temperature rapidly rises. The processing speed is enhanced and the output bending angle is increased to 1.9° with an increment of 70% after the laser softening heat treatment.

  1. The Influence of T6 Heat Treatment to Hardness and Microstructure of Al-Si-Mg Alloys Materials

    International Nuclear Information System (INIS)

    Eddy Djatmiko; Budiarto

    2008-01-01

    Al-Si-Mg alloy is one of aluminium alloys that is suitable to be used as a car piston material. This is because it has some benefits such as light weight, corrosion resistance and interesting color but its mechanical properties do not meet criteria of JIS H5201. For that reason, to meet the standard, its mechanical properties need to be improved. Mechanical properties of this alloy can be improved using many ways. In this research the alloy was T6 heat treated (holding times 4 hour with treatment temperature variation of 30, 150, 180, 210, and 240 o C). Some tests were conducted to these new alloys including hardness test, impact test, phase identification and micro structural analysis. Test results showed that the change mechanical properties occurs due to increasing temperature during T6 heat treatment to these alloys. The optimum mechanical properties were obtained at treatment temperature of 210 o C. In this condition, the alloy has hardness of 93.30 HVN and impact strength of 5.13 J/cm 2 and these results fulfil JIS H5201 standard. The alloy microstructure showed hypoeutectic structure comprising primary aluminium dendrite and Al-Si-Mg eutectic mixture. The result of phase identification after T6 heat treatment showed that Al-Si-Mg alloys have α-Al phase, Si phase and MnAl 6 phase. (author)

  2. Properties variation according to heat treatment for gas turbine blade(bucket) material of GTD-111DS

    International Nuclear Information System (INIS)

    Kim, Moon Young; Park, Sang Yeal; Yang, Sung Ho

    2006-01-01

    The gas turbine components is used on high temperature conditions which under severely circumstance with start-up and stop several times. Therefore, it is used nickel-base superalloys like and GTD-111DS. Damaged buckets on the blade tip during operating are repaired per 24,000 hr to three times according to repair specification of manufacture. It is applied pre-heat, HIP(Hot Isostatic Pressing) and post-heat treatment to support welding repair on blade tip effectively. On this study, it is utilize of WRAP TM (Welding Repair Advanced Process) method to make tension test specimens for this study. And then, material strength and characteristic for GTD-111DS was analyzed

  3. Microstructure and mechanical properties of reactor pressure vessel mock-up material treated by intercritical heat treatment

    International Nuclear Information System (INIS)

    Kim, M. C.; Lee, B. S.; Hong, J. H.; Lee, H. J.; Park, S. D.; Kim, K. B.; Yoon, J. H.; Kim, J. S.; Oh, J. M.

    2003-12-01

    The mechanical properties and microstructures of base metal and weld HAZ (Heat-Affected Zone) of a Mn-Mo-Ni low alloy steels treated by intercritical heat treatment were investigated to evaluate effects of intercritical heat treatment on mechanical properties. In order to clarify the effects of intercritical heat treatment, two types of specimen were prepared by CHT(Conventional Heat Treatment) and IHT(CHT+Intercritical Heat Treatment). Tensile test, charpy impact test and vickers hardness test were carried out to evaluate the mechanical properties. It is found that impact toughness and hardness were improved by intercritical heat treatment. Mean size of precipitates and effective grain were quantitatively analysed as microstructural factors. It is found that precipitate size was decreased and shape of precipitate was spherodized by intercritical heat treatment and grain size was also decreased. So, it is thought that these microstructural changes cause the improvement of mechanical properties by intercritical heat treatment. The simulated specimen using a Gleeble thermal simulator system was used to evaluate the mechanical properties of HAZ. It is well known that IRHAZ and SRHAZ have lower toughness than base metal. However, in the case of IHT, impact toughness of IRHAZ and SRHAZ were slightly higher than that of base metal. It is obvious that this improvement of fracture toughness in IRHAZ and SRHAZ region was closely related to the microstructural changes, such as spheroidization of precipitate and decreases of precipitate size and grain size

  4. 29 CFR 1919.80 - Heat treatment.

    Science.gov (United States)

    2010-07-01

    ... 29 Labor 7 2010-07-01 2010-07-01 false Heat treatment. 1919.80 Section 1919.80 Labor Regulations...) GEAR CERTIFICATION Certification of Shore-Based Material Handling Devices § 1919.80 Heat treatment. (a) Wherever heat treatment of any loose gear is recommended by the manufacturer, it shall be carried out in...

  5. Thermal stresses in hexagonal materials - heat treatment influence on their mechanical behaviour

    International Nuclear Information System (INIS)

    Gloaguen, D.; Freour, S.; Guillen, R.; Royer, J.; Francois, M.

    2004-01-01

    Internal stresses due to anisotropic thermal and plastic properties were investigated in rolled zirconium and titanium. The thermal stresses induced by a cooling process were predicted using a self-consistent model and compared with experimental results obtained by X-ray diffraction. The study of the elastoplastic response during uniaxial loading was performed along the rolling and the transverse direction of the sheet, considering the influence of the texture and the thermal stresses on the mechanical behaviour. An approach in order to determine the thermal behaviour of phases embedded in two-phase materials is also presented. For zirconium, the residual stresses due to thermal anisotropy are rather important (equivalent to 35% of the yield stress) and consequently they play an important role on the elastoplastic transition contrary to titanium. The study of two-phase material shows the influence and the interaction of the second phase on the thermal behaviour in the studied phase

  6. Heat treatment furnace

    Science.gov (United States)

    Seals, Roland D; Parrott, Jeffrey G; DeMint, Paul D; Finney, Kevin R; Blue, Charles T

    2014-10-21

    A furnace heats through both infrared radiation and convective air utilizing an infrared/purge gas design that enables improved temperature control to enable more uniform treatment of workpieces. The furnace utilizes lamps, the electrical end connections of which are located in an enclosure outside the furnace chamber, with the lamps extending into the furnace chamber through openings in the wall of the chamber. The enclosure is purged with gas, which gas flows from the enclosure into the furnace chamber via the openings in the wall of the chamber so that the gas flows above and around the lamps and is heated to form a convective mechanism in heating parts.

  7. Influence of heat treatment and indenter tip material on depth sensing hardness tests at high temperatures of fusion relevant materials

    International Nuclear Information System (INIS)

    Bredl, Julian; Dany, Manuel; Albinski, Bartlomiej; Schneider, Hans-Christian; Kraft, Oliver

    2015-01-01

    Highlights: • Operation of a custom-made indentation device designed for test temperatures up to 650 °C and a remote handled operation in a Hot Cell. • Instrumented indentation and conventional hardness testing of unirradiated MANET II and EUROFER. • Comparison of diamond and sapphire as indenter tip materials. - Abstract: The instrumented indentation is a suitable method for testing of even small neutron-irradiated specimens. From the continuously recorded indentation depth and the indentation force, it is possible to deduce mechanical parameters of the tested material. In this paper, a brief description of the high temperature device is given and representative results are presented. In the study, unirradiated steels are investigated by instrumented indentation at temperatures up to 500 °C. It is shown that the hardness is highly depending on the testing-temperature and can be correlated to the results of conventional tensile testing experiments. A not negligible influence of the indenter tip material is observed. The results show the functionality of the high-temperature indentation device.

  8. Influence of heat treatment and indenter tip material on depth sensing hardness tests at high temperatures of fusion relevant materials

    Energy Technology Data Exchange (ETDEWEB)

    Bredl, Julian, E-mail: julian.bredl@kit.edu; Dany, Manuel; Albinski, Bartlomiej; Schneider, Hans-Christian; Kraft, Oliver

    2015-10-15

    Highlights: • Operation of a custom-made indentation device designed for test temperatures up to 650 °C and a remote handled operation in a Hot Cell. • Instrumented indentation and conventional hardness testing of unirradiated MANET II and EUROFER. • Comparison of diamond and sapphire as indenter tip materials. - Abstract: The instrumented indentation is a suitable method for testing of even small neutron-irradiated specimens. From the continuously recorded indentation depth and the indentation force, it is possible to deduce mechanical parameters of the tested material. In this paper, a brief description of the high temperature device is given and representative results are presented. In the study, unirradiated steels are investigated by instrumented indentation at temperatures up to 500 °C. It is shown that the hardness is highly depending on the testing-temperature and can be correlated to the results of conventional tensile testing experiments. A not negligible influence of the indenter tip material is observed. The results show the functionality of the high-temperature indentation device.

  9. PENGARUH VARIASI SUHU POST WELD HEAT TREATMENT ANNEALING TERHADAP SIFAT MEKANIS MATERIAL BAJA EMS-45 DENGAN METODE PENGELASAN SHIELDED METAL ARC WELDING (SMAW

    Directory of Open Access Journals (Sweden)

    Rusiyanto Rusiyanto

    2012-02-01

    Full Text Available Penelitian ini bertujuan Untuk mengetahui nilai kekerasan Vickers material Baja EMS-45 sebelum proses pengelasan dan setelah dilakukan proses pengelasan tanpa post weld heat treatment annealing, Untuk mengetahui berapakah suhu optimal post weld heat treatment annealing untuk material baja EMS-45 dengan variasi suhu yang digunakan 350 o C, 550 o C, dan 750 C. Untuk mengetahui struktur mikro dari material baja EMS-45 akibat variasi suhu post weld heat treatment annealing pada proses pengelasan dengan menggunakan metode pengelasan shielded metal arc welding. Bahan atau material dasar yang digunakan pada penelitian ini adalah Baja EMS-45 dengan ketebalan pelat 10 mm, lebar pelat 20 mm dan panjang 100 mm. Berdasarkan hasil pengujian nilai kekerasan tertinggi setelah proses pengelasan terletak pada daerah Logam Las. Pengelasan non PWHT memiliki nilai kekerasan paling tinggi setelah proses pengelasan yaitu sebesar 183,2 VHN. Suhu optimal Post Weld Heat Treatment Annealing untuk material baja EMS-45 adalah pada suhu 750 C. Karena pada PWHT pada suhu tersebut mengalami penurunan kekerasan yang besar yaitu sebesar 127,2 VHN, sehingga material baja EMS-45 dapat memperbaiki sifat mampu mesinnya. Struktur mikro dari material baja EMS-45 sebelum proses pengelasan berupa grafit serpih, perlit dan ferit, setelah dilakukan proses pengelasan mempunyai struktur mikro berupa matrik ferit dan grafit pada daerah logam las, matrik perlit kasar dan grafit serpih pada daerah HAZ dan struktur perlit, grafit serpih dan ferit pada daerah logam induk o o

  10. Plasma assisted heat treatment: annealing

    International Nuclear Information System (INIS)

    Brunatto, S F; Guimaraes, N V

    2009-01-01

    This work comprises a new dc plasma application in the metallurgical-mechanical field, called plasma assisted heat treatment, and it presents the first results for annealing. Annealing treatments were performed in 90% reduction cold-rolled niobium samples at 900 deg. C and 60 min, in two different heating ways: (a) in a hollow cathode discharge (HCD) configuration and (b) in a plasma oven configuration. The evolution of the samples' recrystallization was determined by means of the microstructure, microhardness and softening rate characterization. The results indicate that plasma species (ions and neutrals) bombardment in HCD plays an important role in the recrystallization process activation and could lead to technological and economical advantages considering the metallic materials' heat treatment application. (fast track communication)

  11. Effect of microwave heat-treatment time on the properties of activated carbons as electrode materials for supercapacitors

    Energy Technology Data Exchange (ETDEWEB)

    He, X.; Wang, T.; Long, S.; Zhang, X.; Zheng, M. [Anhui Univ. of Technology, Ma' aushan (China). School of Chemistry and Chemical Engineering, Anhui Key Lab of Coal Clean Conversion and Utilization

    2010-07-01

    A microwave-assisted heating technique was used to prepare activated carbons (ACs) from petroleum coke with potassium hydroxide (KOH) as an activating agent. The aim of the study was to investigate the effect of heat treatment time on AC properties at 3, 5, and 7 minutes with a microwave power rate of 700 W. The structure and electrochemical performance of the microwave ACs were then compared with commercially prepared ACs. The study showed that the specific capacitance, equivalent series resistance and energy density of the AC electrodes decreased, while the cycle performance of the AC electrodes was improved. The specific capacitance and energy density of the ACs treated with microwave heat at 3 and 7 minutes was higher than rates observed in commercially-prepared ACs. Results showed that the microwave heat treatment method is an efficient means of obtaining stable ACs for use in supercapacitors. 3 refs., 1 tab., 1 fig.

  12. Microwave heating processes involving carbon materials

    Energy Technology Data Exchange (ETDEWEB)

    Menendez, J.A.; Arenillas, A.; Fidalgo, B.; Fernandez, Y.; Zubizarreta, L.; Calvo, E.G.; Bermudez, J.M. [Instituto Nacional del Carbon, CSIC, Apartado 73, 33080 Oviedo (Spain)

    2010-01-15

    Carbon materials are, in general, very good absorbents of microwaves, i.e., they are easily heated by microwave radiation. This characteristic allows them to be transformed by microwave heating, giving rise to new carbons with tailored properties, to be used as microwave receptors, in order to heat other materials indirectly, or to act as a catalyst and microwave receptor in different heterogeneous reactions. In recent years, the number of processes that combine the use of carbons and microwave heating instead of other methods based on conventional heating has increased. In this paper some of the microwave-assisted processes in which carbon materials are produced, transformed or used in thermal treatments (generally, as microwave absorbers and catalysts) are reviewed and the main achievements of this technique are compared with those obtained by means of conventional (non microwave-assisted) methods in similar conditions. (author)

  13. Investigations on the behaviour of reactor pressure vessel material 20 MnMoNi 55 during heat and stress relieving treatments. Vol. 1 and 2

    International Nuclear Information System (INIS)

    Blind, D.; Schroeder-Obst, D.; Herz, K.; Maidorn, C.

    1984-01-01

    Variation of various heat treatment parameters with regard to forging, hardening, tempering and stress-relieving has been applied to several heats of pressure vessel steels with the aim of testing the possibility to obtain higher notch impact energy values. On one hand the variation of heat treatment parameters within the limits of the current VdTUeV material sheet 401/4 5.80 did not result in outstanding improvements of toughness. On the other hand, when employing procedures which did not correspond to the specifications, e.g. tempering up to 100 h, an evident decrease of the upper shelf and an increase of the transition temperature could be observed. Nevertheless, the specified values were generally reached. Essentially, the observations on the test materials confirm, apart from a few exceptions, the positive practical experience with the material 20 MnMoNi 5 5. Based on these relations between thoughness and forging as well as heat treatment the manufacturer obtained, in accordance with the current research program, an outstanding improvement of toughness by means of various optimization measures which had the effect of optimal, evidently increased upper shelfs and which excluded difficulties concerning acceptance criteria, e.g. too high notch impact energy transition temperatures. (orig./IHOE) [de

  14. Heat-treatment and heat-to-heat variations in the fracture toughness of Alloy 718

    International Nuclear Information System (INIS)

    Mills, W.J.

    1981-07-01

    The effect of heat-treatment and heat-to-heat variations on the J Ic fracture toughness response of Alloy 718 was examined at room and elevated temperatures using the multiple-specimen R-curve technique. Six heats of alloy 718 were tested in the conventional and modified heat-treated conditions. The fracture toughness response for the modified superalloy was found to be superior to that exhibited by the conventional material. Heat-to-heat variations in the J Ic response of Alloy 718 were observed in both heat-treated conditions; the modified treatment exhibited much larger variability. The J Ic and corresponding K Ic fracture toughness values were analyzed statistically to establish minimum expected toughness, values for use in design and safety analyses. 26 refs., 10 figs., 9 tabs

  15. Surface engineering and heat treatment

    International Nuclear Information System (INIS)

    Morton, P.H.

    1991-01-01

    This book is the proceedings of a Conference organised jointly by The Institute of Metals and The Centre for Exploitation of Science and Technology (CEST). It sets out to review this role and point the way to the future by collecting together a series of invited papers written by noted authorities in their fields. The opening review by CEST highlights the economic and industrial importance of Surface Engineering and is followed by a group of four articles devoted to specific branches of industry. Several technical papers then describe various aspects of the development of heat treatment over the last twenty-five years. These are followed by papers describing advances made possible by new technologies such as plasma, laser and ion beam. A separate abstract has been prepared for a paper on materials aspects of ion beam technology. (author)

  16. 49 CFR 179.200-11 - Postweld heat treatment.

    Science.gov (United States)

    2010-10-01

    ... 49 Transportation 2 2010-10-01 2010-10-01 false Postweld heat treatment. 179.200-11 Section 179.200-11 Transportation Other Regulations Relating to Transportation PIPELINE AND HAZARDOUS MATERIALS... Postweld heat treatment. When specified in § 179.201-1, after welding is complete, postweld heat treatment...

  17. Latent Heat Storage Through Phase Change Materials

    Indian Academy of Sciences (India)

    IAS Admin

    reducing storage volume for different materials. The examples are numerous: ... Latent heat is an attractive way to store solar heat as it provides high energy storage density, .... Maintenance of the PCM treated fabric is easy. The melted PCM.

  18. Effect of heat treatment upon the mechanical and poro-mechanical behaviour of cement-based materials: hydraulic properties and morphological changes

    International Nuclear Information System (INIS)

    Chen, Xiao-Ting

    2009-01-01

    This work investigates the effects of morphological changes of a cement-based material subjected to heat treatment (up to 400 C). For a model W/C=0.5 mortar, we have characterized experimentally hydraulic behaviour (gas permeability), mechanical behaviour (in uniaxial compression, hydrostatic compression with or without deviatoric stress) and poro-mechanical behaviour (incompressibility moduli Kb, Ks and Biot's coefficient b) after a heating/cooling cycle. We have also developed an original experiment aimed at quantifying the accessible pore space volume under hydrostatic compression. The creation of occluded porosity under high confinement is confirmed, which justifies the observed decrease of solid matrix rigidity Ks under high confinement. A gas retention phenomenon was identified under simultaneous thermal and hydrostatic loadings for mortar, and industrial concretes (provided by CERIB and ANDRA). A predictive thermo-elasto-plastic model with isotropic damage and a micro-mechanical approach, which represents micro-cracking, are coupled in order to analyze or predict the evolution of mechanical and poro-elastic properties after heat cycling. (author)

  19. Assembly for melting and heat treatment

    International Nuclear Information System (INIS)

    Blumenfeld, M.

    1976-11-01

    Laboratory scale production of alloys having a precise alloying materials content and the exact heat treatment of metallurgical specimens are discussed. The design and assembly of two relevant instruments are described. These instruments include a laboratory vacuum induction furnace and a specially designed glass lathe, that enables even an unskilled operator to encapsulate and seal metallurgical specimens in glass capsules. (author)

  20. Effect of heat treatment temperature on microstructure

    Indian Academy of Sciences (India)

    The results of electrochemical performance measurements for the HCSs as anode material for lithium ion batteries indicate that the discharge capacity of the HCSs is improved after heat treatment at 800°C compared with the as-prepared HCSs and have a maximum value of 357 mAh/g and still retains 303 mAh/g after 40 ...

  1. Study of parameters of heat treatment in obtaining glass ceramic materials with addition of the industrial waste

    International Nuclear Information System (INIS)

    Kniess, C.T.; Prates, P.B.; Martins, G.J.M.; Riella, H.G.; Matsinhe, Jonas; Kuhnen, N.C.

    2012-01-01

    The production of materials from crystallization of glass, called glass ceramic, have proved interesting by the possibility of development of different microstructures, with reduced grain size and the presence of residual amorphous phase in different quantities. The method that uses the differential thermal analysis (DTA) provides research on the material properties over a wide temperature range, it's widely applied to crystallization processes of glass ceramic materials. Within this context, this paper aims to study the kinetics of nucleation and crystal growth in glass ceramic materials in the system SiO 2 - Al 2 O 3 -Li 2 O, obtained with the addition of mineral coal bottom ash as source of aluminosilicates, through the technique of differential thermal analysis. (author)

  2. Highly heat removing radiation shielding material

    International Nuclear Information System (INIS)

    Asano, Norio; Hozumi, Masahiro.

    1990-01-01

    Organic materials, inorganic materials or metals having excellent radiation shielding performance are impregnated into expanded metal materials, such as Al, Cu or Mg, having high heat conductivity. Further, the porosity of the expanded metals and combination of the expanded metals and the materials to be impregnated are changed depending on the purpose. Further, a plurality of shielding materials are impregnated into the expanded metal of the same kind, to constitute shielding materials. In such shielding materials, impregnated materials provide shielding performance against radiation rays such as neutrons and gamma rays, the expanded metals provide heat removing performance respectively and they act as shielding materials having heat removing performance as a whole. Accordingly, problems of non-informity and discontinuity in the prior art can be dissolved be provide materials having flexibility in view of fabrication work. (T.M.)

  3. The influence of storage and heat treatment on a magnesium-based implant material: an in vitro and in vivo study.

    Science.gov (United States)

    Bracht, Katja; Angrisani, Nina; Seitz, Jan-Marten; Eifler, Rainer; Weizbauer, Andreas; Reifenrath, Janin

    2015-10-19

    Magnesium alloys are recommended as a potential material for osteosynthesis. It is known that storage-induced property modifications can occur in materials like aluminum. Thus the aim of this study was to analyze the influence of storage durations of up to 48 weeks on the biomechanical, structural, and degradation properties of the degradable magnesium alloy LAE442. Extruded implants (n = 104; Ø 2.5 mm × 25 mm) were investigated after storage periods of 0, 12, 24, and 48 weeks in three different sub-studies: (I) immediately after the respective storage duration and after an additional (II) 56 days of in vitro corrosion in simulated body fluid (SFB), and (III) 48 weeks in vivo corrosion in a rabbit model, respectively. In addition, the influence of a T5-heat treatment (206 °C for 15 h in an argon atmosphere) was tested (n = 26; 0 week of storage). Evaluation was performed by three-point bending, scanning electron microscopy, radiography, µ-computed tomography, evaluation of the mean grain size, and contrast analysis of precipitations (such as aluminum or lithium). The heat treatment induced a significant reduction in initial stability, and enhanced the corrosion resistance. In vivo experiments showed a good biocompatibility for all implants. During the storage of up to 48 weeks, no significant changes occurred in the implant properties. LAE442 implants can be safely used after up to 48 weeks of storage.

  4. Failures of tool steels after heat treatments

    International Nuclear Information System (INIS)

    Nunez-Gonzalez, G.

    1990-01-01

    The main objective of the work was to determine the most common defects occuring in tool steels of the AISI D-2, S-1, 0-1 and W-2 series during thermal treatment. Defects were evaluated by metallographic analyses, a method used to determine and recognize micro structural defects and their origin in order to be able to eliminate and correct some of the stages that are caused by heat treatment. Results show a large number of defects due to irregularities during thermal heating such as excess or lack of temperature, heating time, and atmosphere, rectifying and handling in service and, to a lesser extent, poor design. In conclusion, with the results obtained for each of the thermal treatments it is necessary to define, particularly the values each of these variables should have since they affect the material properties. (Author)

  5. Development of high J c Bi2223/Ag thick film materials prepared by heat treatment under low P O2

    Science.gov (United States)

    Takeda, Y.; Shimoyama, J.; Motoki, T.; Nakamura, S.; Nakashima, T.; Kobayashi, S.; Kato, T.

    2018-07-01

    In general, a dense and c-axis grain-oriented microstructure is desirable in order to achieve the high critical current properties of Bi2223 polycrystalline materials. On the other hand, our recent studies have shown that precise control of the chemical compositions of Bi2223 is also effective for the enhancement of intergrain J c. In this study, the development of Bi2223 thick film materials with high critical current properties was attempted by controlling both the microstructure and the chemical compositions. A high intergrain J c of ∼8 kA cm‑2 at 77 K of a film with ∼40 μm t was achieved by increasing the Pb substitution level for the Bi site and controlling the nonstoichiometric chemical compositions. Furthermore, it was revealed that an increase in the thickness enabled us to obtain high I c films suitable for practical applications. In contrast, there are still issues, especially in controlling the grain alignment at the inner part of the film, which suggests that the J c properties of thick film materials could be further improved by forming a more ideal microstructure, as realized in the Bi2223 filaments of multi-filamentary Ag-sheathed tapes.

  6. Energy saving by enhanced temperature measurement of stock materials of heat- and heat treatment process. Final report; Energieeinsparung durch verbesserte Nutzguttemperaturbestimmung bei Waerm- und Waermebehandlungsprozessen. Schlussbericht

    Energy Technology Data Exchange (ETDEWEB)

    Ley, I.; Klima, R.

    1999-06-01

    The essential source of errors for stock temperature measurement in industrial furnaces is the not well enough known emissivity and the reflected radiation. The examined pyrometers turned out to be not precise enough especially in case of reflected radiation. Measures trying to compensate the reflected radiation by measuring it separately or shielding the pyrometer from reflected radiation did not show satisfactory results. The most important result of the project was the development and operational test of a thermoelectric measurement by a so-called thermocouple probe. This probe measures by a thermocouple which is positioned to have a very intensive radiation exchange with the surface of the stock. Thus it can measure the surface temperature almost independently from emissivity. The advantages of the thermocouple probe where shown by installations at a heat treating and a reheating furnace. Because of the continuous measurement the furnaces could be optimised for energy saving or better product quality. The thermocouple probe enables strict optimisation of model aided furnace control and leads to improved quality and energy savings. (orig.) [German] Die wesentlichen Fehlerquellen bei der Messung der Nutzgutoberflaechentemperatur sind der haeufig nicht genau genug bekannte Nutzgut-Emissionsgrad und die an der Nutzgutoberflaeche reflektierte Fremdstrahlung. Die untersuchten auf dem Markt befindlichen Pyrometer erwiesen sich bei vorhandener Fremdstrahlung in Oefen als nicht genau und verlaesslich genug. Sowohl Versuche zur Abschirmung der Fremdstrahlung wie auch zur separaten Messung und Beruecksichtigung der Fremdstrahlung liefern bei wechselnden Prozesszustaenden jedoch keine befriedigenden Ergebnisse. In dieser Arbeit wurde als wichtigstes Ergebnis ein thermoelektrisches Temperaturmessverfahren mittels einer sogenannten Thermoelementsonde entwickelt und betrieblich erprobt. Mit der Thermoelementsonde wird die Nutzgutoberflaechentemperatur mittels eines

  7. Fabrication techniques to eliminate postweld heat treatment

    International Nuclear Information System (INIS)

    Lochhead, J.C.

    1978-01-01

    Postweld heat treatments to reduce residual stresses (stress relief operations) have been a common practice in the pressure vessel industry for a large number of years. A suitable heat treatment operation can, in particular for low alloy steels, have additional beneficial effects, i.e. a reduction in peak hardness values in the heat-affected zone, an improvement in weld metal properties, and a lowering of the adverse effects of the welding process on the mechanical properties of the parent material adjacent to the weld metal. However, continuing studies in the field of brittle fracture, improved parent materials, and more sophisticated nondestructive testing techniques have led to the elimination of such a practice in ever-increasing thickness ranges and types of material. For instance, the recently issued BS 5500 compared with BS 1113 (1969) lifts the thickness limit requiring stress relief in certain circumstances from 19 to 35mm for C steels. With respect to materials the CEGB has stated that as a result of successful operational experience it will no longer be necessary to postweld heat treat butt welds in 2 1/4 Cr-1Mo tubes of certain dimensions. Despite this trend, over a period of years a number of instances have arisen where, because of some factor, postweld heat treatment, although perhaps desirable, is not possible. This Paper describes several such examples. It must be noted that the examples quoted consist of relatively important and major items. It has been necessary within the confines of this Paper to condense the reports. It is hoped that no significant factors have been omitted. (author)

  8. Heat conductivity of buffer materials

    International Nuclear Information System (INIS)

    Boergesson, L.; Fredrikson, Anders; Johannesson, L.E.

    1994-11-01

    The report deals with the thermal conductivity of bentonite based buffer materials. An improved technique for measuring the thermal conductivity of buffer materials is described. Measurements of FLAC calculations applying this technique have led to a proposal of how standardized tests should be conducted and evaluated. The thermal conductivity of bentonite with different void ratio and degree of water saturation has been determined in the following different ways: * Theoretically according to three different investigations by other researchers. * Laboratory measurements with the proposed method. * Results from back-calculated field tests. Comparison and evaluation showed that these results agreed very well, when the buffer material was almost water saturated. However, the influence of the degree of saturation was not very well predicted with the theoretical methods. Furthermore, the field tests showed that the average thermal conductivity in situ of buffer material (compacted to blocks) with low degree of water saturation was lower than expected from laboratory tests. 12 refs, 29 figs, 11 tabs

  9. Heat transfer in multi-phase materials

    CERN Document Server

    Öchsner, Andreas

    2011-01-01

    This book provides a profound understanding, which physical processes and mechanisms cause the heat transfer in composite and cellular materials. It shows models for all important classes of composite materials and introduces into the latest advances. In three parts, the book covers Composite Materials (Part A), Porous and Cellular Materials (Part B) and the appearance of a conjoint solid phase and fluid aggregate (Part C).

  10. 49 CFR 179.300-10 - Postweld heat treatment.

    Science.gov (United States)

    2010-10-01

    ... 49 Transportation 2 2010-10-01 2010-10-01 false Postweld heat treatment. 179.300-10 Section 179.300-10 Transportation Other Regulations Relating to Transportation PIPELINE AND HAZARDOUS MATERIALS... Postweld heat treatment. After welding is complete, steel tanks and all attachments welded thereto, must be...

  11. 29 CFR 1919.36 - Heat treatment.

    Science.gov (United States)

    2010-07-01

    ... 29 Labor 7 2010-07-01 2010-07-01 false Heat treatment. 1919.36 Section 1919.36 Labor Regulations...) GEAR CERTIFICATION Certification of Vessels: Tests and Proof Loads; Heat Treatment; Competent Persons § 1919.36 Heat treatment. (a) The annealing of wrought iron gear required by this part shall be...

  12. Paving materials for heat island mitigation

    Energy Technology Data Exchange (ETDEWEB)

    Pomerantz, M.; Akbari, H.; Chen, A.; Taha, H. [Lawrence Berkeley National Lab., CA (United States); Rosenfeld, A.H. [Dept. of Energy, Washington, DC (United States)

    1997-11-01

    This report summarizes paving materials suitable for urban streets, driveways, parking lots and walkways. The authors evaluate materials for their abilities to reflect sunlight, which will reduce their temperatures. This in turn reduces the excess air temperature of cities (the heat island effect). The report presents the compositions of the materials, their suitability for particular applications, and their approximate costs (in 1996). Both new and resurfacing are described. They conclude that, although light-colored materials may be more expensive than conventional black materials, a thin layer of light-colored pavement may produce energy savings and smog reductions whose long-term worth is greater than the extra cost.

  13. Heat resistance study of basalt fiber material via mechanical tests

    Science.gov (United States)

    Gao, Y. Q.; Jia, C.; Meng, L.; Li, X. H.

    2017-12-01

    This paper focuses on the study of the relationship between the fracture strength of basalt rovings and temperature. Strong stretching performance of the rovings has been tested after the treatment at fixed temperatures but different heating time and then the fracture strength of the rovings exposed to the heating at different temperatures and cooled in different modes investigated. Finally, the fracture strength of the basalt material after the heat treatment was studied. The results showed that the room-temperature strength tends to decrease with an increase of the heat treatment time at 250 °C, but it has the local maximum after 2h heating. And the basalt rovings strength increased after the heat treatment up to 200 °C. It was 16.7 percent higher than the original strength. The strength depends not only on the temperature and duration of the heating, but also on the cooling mode. The value of the strength measured after cold water cooling was less by 6.3% compared with an ambient air cooling mode. The room-temperature breaking strength of the rovings heated at 200 °C and 100 °C for 2 hours each increased by about 14.6% with respect to unpretreated basalt rovings.

  14. Thermophysical Properties of Heat Resistant Shielding Material

    International Nuclear Information System (INIS)

    Porter, W.D.

    2004-01-01

    This project was aimed at determining thermal conductivity, specific heat and thermal expansion of a heat resistant shielding material for neutron absorption applications. These data are critical in predicting the structural integrity of the shielding under thermal cycling and mechanical load. The measurements of thermal conductivity and specific heat were conducted in air at five different temperatures (-31 F, 73.4 F, 140 F, 212 F and 302 F). The transient plane source (TPS) method was used in the tests. Thermal expansion tests were conducted using push rod dilatometry over the continuous range from -40 F (-40 C) to 302 F (150 C)

  15. Polymer Materials for the Heat Recovery

    International Nuclear Information System (INIS)

    Kolasińska, E; Mazurek, B; Kolasiński, P

    2016-01-01

    Many of the processes in the industry, agriculture and microscale systems are associated with the waste heat generation, which often may be a menace or lower the efficiency of the processes. The thermoelectric cooling is becoming increasingly popular and gives the possibility to convert waste heat into electricity. The current thermoelectric cooling solutions are based on alloy materials. However, the new technologies pay attention to the environment burden, moreover the regulations of the production and recycling are becoming more and more restrictive. Conducting polymers are thermoelectrically active at low temperatures, cheap and environmentally safe. In this paper authors discuss the possibility of the application of conducting polymers for the heat recovery. Due to the operating temperature range and different nature of the waste heat sources, polymers might be an interesting solution and a complement for alloy-based thermoelectric materials. The character and nature of the formation of waste heat sources and conventional technologies of its recovery are also described in this paper. Moreover the advantages of thermoelectric cooling with the use of polymers are presented and two materials based on polyaniline are proposed. (paper)

  16. Phase Change Material Heat Exchanger Life Test

    Science.gov (United States)

    Lillibridge, Sean; Stephan, Ryan

    2009-01-01

    Low Lunar Orbit (LLO) poses unique thermal challenges for the orbiting space craft, particularly regarding the performance of the radiators. The IR environment of the space craft varies drastically from the light side to the dark side of the moon. The result is a situation where a radiator sized for the maximal heat load in the most adverse situation is subject to freezing on the dark side of the orbit. One solution to this problem is to implement Phase Change Material (PCM) Heat Exchangers. PCM Heat Exchangers act as a "thermal capacitor," storing thermal energy when there is too much being produced by the space craft to reject to space, and then feeding that energy back into the thermal loop when conditions are more favorable. Because they do not use an expendable resource, such as the feed water used by sublimators and evaporators, PCM Heat Exchangers are ideal for long duration LLO missions. In order to validate the performance of PCM Heat Exchangers, a life test is being conducted on four n-Pentadecane, carbon filament heat exchangers. Fluid loop performance, repeatability, and measurement of performance degradation over 2500 melt-freeze cycles will be performed.

  17. Thermoluminescent determination of prehistoric heat treatment of chert artifacts

    International Nuclear Information System (INIS)

    Melcher, C.L.; Zimmerman, D.W.

    1977-01-01

    In recent years archeologists have become interested in the extent to which prehistoric peoples heat-treated chert prior to shaping it into tools. Thermoluminescent determination of the radiation dose accumulated by an artifact since it was formed or last heated provides a simple, reliable test for such heat treatment. This test can be applied to single artifacts without the need for raw source material for comparison. Results on 25 artifacts from four sites indicate that, for many chert sources, color and luster are not useful indicators of heat treatment by prehistoric peoples

  18. Effect of heat-treatment on elevated temperature fatigue-crack growth behavior of two heats of Alloy 718

    International Nuclear Information System (INIS)

    Mills, W.J.; James, L.A.

    1978-05-01

    The room temperature and elevated temperature fatigue-crack growth behavior of two heats of Alloy 718 was characterized within a linear-elastic fracture mechanics framework. Two different heat-treatments were used: the ''conventional'' (ASTM A637) treatment, and a ''modified'' heat-treatment designed to improve the toughness of Alloy 718 base metal and weldments. Heat-to-heat variations in the fatigue-crack propagation behavior were observed in the conventionally-treated material. On the other hand, no heat-to-heat variations were observed in the modified condition. Furthermore, both heats of Alloy 718 exhibited superior fatigue-crack growth resistance when given the modified heat-treatment. Electron fractographic examination of Alloy 718 fatigue fracture surfaces revealed that the operative crack growth mechanisms were dependent on heat-treatment, temperature, and ΔK level

  19. Computational simulation of heat transfer in laser melted material flow

    International Nuclear Information System (INIS)

    Shankar, V.; Gnanamuthu, D.

    1986-01-01

    A computational procedure has been developed to study the heat transfer process in laser-melted material flow associated with surface heat treatment of metallic alloys to improve wear-and-tear and corrosion resistance. The time-dependent incompressible Navier-Stokes equations are solved, accounting for both convective and conductive heat transfer processes. The convection, induced by surface tension and high surface temperature gradients, sets up a counterrotating vortex flow within the molten pool. This recirculating material flow is responsible for determining the molten pool shape and the associated cooling rates which affect the solidifying material composition. The numerical method involves an implicit triple-approximate factorization scheme for the energy equation, and an explicit treatment for the momentum and the continuity equations. An experimental setup, using a continuous wave CO 2 laser beam as a heat source, has been carried out to generate data for validation of the computational model. Results in terms of the depth, width, and shape of the molten pool and the heat-affected zone for various power settings and shapes of the laser, and for various travel speeds of the workpiece, compare very well with experimental data. The presence of the surface tension-induced vortex flow is demonstrated

  20. Heat treatment of nickel alloys

    International Nuclear Information System (INIS)

    Smith, D.F. Jr.; Clatworthy, E.F.

    1975-01-01

    A heat treating process is described that can be used to produce desired combinations of strength, ductility, and fabricability characteristics in heat resistant age-hardenable alloys having precipitation-hardening amounts of niobium, titanium, and/or tantalum in a nickel-containing matrix. (U.S.)

  1. 29 CFR 1919.16 - Heat treatment.

    Science.gov (United States)

    2010-07-01

    ... 29 Labor 7 2010-07-01 2010-07-01 false Heat treatment. 1919.16 Section 1919.16 Labor Regulations Relating to Labor (Continued) OCCUPATIONAL SAFETY AND HEALTH ADMINISTRATION, DEPARTMENT OF LABOR (CONTINUED) GEAR CERTIFICATION Certification of Vessels' Cargo Gear § 1919.16 Heat treatment. (a) All chains (other...

  2. Ultrasonic evaluation of heat treatment for stress relief in steel

    International Nuclear Information System (INIS)

    Bittencourt, Marcelo de S.Q.; Lamy, Carlos A.; Goncalves Filho, Orlando J.A.; Payao Filho, Joao da C.

    2000-01-01

    Residual stresses in materials arise due to the manufacturing processes. As a consequence, in the nuclear area some components must suffer a stress relief treatment according to strict criteria. Although these treatments are carefully carried on, concern with nuclear safety is constantly growing. This work proposes a nondestructive ultrasonic method to guarantee the efficiency of the heat treatment. It was used a short peened steel plate with tensile and compressive stresses which was submitted to a stress relief treatment. The results show that the proposed ultrasonic method could be used to confirm the efficiency of the stress relief heat treatment. (author)

  3. Advances in the heat treatment of steels

    International Nuclear Information System (INIS)

    Morris, J.W. Jr.; Kim, J.I.; Syn, C.K.

    1978-06-01

    A number of important recent advances in the processing of steels have resulted from the sophisticated uses of heat treatment to tailor the microstructure of the steels so that desirable properties are established. These new heat treatments often involve the tempering or annealing of the steel to accompish a partial or complete reversion from martensite to austenite. The influence of these reversion heat treatments on the product microstructure and its properties may be systematically discussed in terms of the heat treating temperature in relation to the phase diagram. From this perspective, four characteristic heat treatments are defined: (1) normal tempering, (2) inter-critical tempering, (3) intercritical annealing, and (4) austenite reversion. The reactions occurring during each of these treatments are described and the nature and properties of typical product microstructures discussed, with specific reference to new commercial or laboratory steels having useful and exceptional properties

  4. FY 2000 report on the survey of the freon recovery/treatment technology for construction use heat insulating materials; 2000 nendo chosa hokokusho. Kenchiku yo dannetsuzai furon kaishu shori gijutsu chosa

    Energy Technology Data Exchange (ETDEWEB)

    NONE

    2002-03-01

    An investigational study was made of the quantity of the specified freon remaining in the construction use heat insulating material, the rational method for the recovery/treatment, etc. As to the standardization of the method to analyze the remaining freon quantity, the tube furnace - GC method and the MS method were proposed, and the basic items that can be developed to JIS (Japanese Industrial Standard) were standardized. In the estimation of the remaining freon quantity, the actual state of the use of heat insulating materials was surveyed from the statistics on the start of construction work, survey of the heat insulating area in actual buildings and listening to heat insulation workers/cold store construction companies, etc. Further, the remaining quantity was analyzed of samples collected from various buildings nationwide and by years of completion. As a result, it was found out that, even in samples before 1995, HCFC is used in about 10% and that, in case of limiting to the specified freon (CFC), the freon remaining quantity was more than 1-4 wt% even after a lapse of 30 years. The paper arranged subjects on the freon recovery/treatment in each stage of the life cycle and the required conditions for technology/equipment. (NEDO)

  5. CarbAl Heat Transfer Material

    Science.gov (United States)

    Fink, Richard

    2015-01-01

    The increasing use of power electronics, such as high-current semiconductor devices and modules, within space vehicles is driving the need to develop specialty thermal management materials in both the packaging of these discrete devices and the packaging of modules consisting of these device arrays. Developed by Applied Nanotech, Inc. (ANI), CarbAl heat transfer material is uniquely characterized by its low density, high thermal diffusivity, and high thermal conductivity. Its coefficient of thermal expansion (CTE) is similar to most power electronic materials, making it an effective base plate substrate for state-of-the-art silicon carbide (SiC) super junction transistors. The material currently is being used to optimize hybrid vehicle inverter packaging. Adapting CarbAl-based substrates to space applications was a major focus of the SBIR project work. In Phase I, ANI completed modeling and experimentation to validate its deployment in a space environment. Key parameters related to cryogenic temperature scaling of CTE, thermal conductivity, and mechanical strength. In Phase II, the company concentrated on improving heat sinks and thermally conductive circuit boards for power electronic applications.

  6. Carbonaceous material treatment

    Energy Technology Data Exchange (ETDEWEB)

    Trevor, S R

    1939-05-04

    To separate and collect for use the component parts of carbonaceous materials, they are fed to superimposed connected vertical or substantially vertical chambers, located over a furnace, the flue gases from which pass to space or spaces of a casing surrounding the superimposed chambers. Pipes are provided so that part or whole of the gases may be passed through the chambers. Take-off pipes are connected to expansion chambers, through which the gases pass to condenser coils and separating tanks.

  7. Examination of heat treatments at preservation of grape must

    Directory of Open Access Journals (Sweden)

    Péter Korzenszky

    2014-02-01

    Full Text Available Heat treatment is a well-known process in food preservation. It is made to avoid and to slow down food deterioration. The process was developed by Louise Pasteur French scientist to avoid late among others wine further fermentation. The different heat treatments influence the shelf life in food production. In our article we present the process of grape must fermentation, as grape must is the base material of wine production. The treatment of harvested fresh grape juice has a big influence on end product quality. It is our experiments we examined the same grape must with four different methods in closed and in open spaces to determine CO2 concentration change. There are four different methods for treatment of grape juice: boiling, microwave treatment, treatment by water bath thermostat and a control without treatment. As a result of the comparison it can be stated that the heat treatment delays the start of fermentation, thereby increasing shelf life of grape must. However, no significant differences were found between two fermentation of heat-treated grape must by the microwave and water-bath thermostat. The different heat treatment of grape must base materials was done at the laboratory in Faculty of Mechanical Engineering of Szent István University. The origin of the table grapes used for the examination was Gödöllő-hillside. Normal 0 21 false false false HU X-NONE X-NONE

  8. Mechanical Treatment: Material Recovery Facilities

    DEFF Research Database (Denmark)

    Christensen, Thomas Højlund; Bilitewski, B.

    2011-01-01

    A wide variety of mechanical treatment unit processes, including manual sorting, is described in Chapter 7.1. These unit processes may be used as a single separate operation (e.g. baling of recyclable cardboard) or as a single operation before or after biological and thermal treatment processes (e.......g. shredding prior to incineration or screening after composting). The mechanical treatment unit process is in the latter case an integrated part of the overall treatment usually with the purpose of improving the quality of the input material, or the efficiency or stability of the biological or thermal process......, or improving the quality of the output material. Examples hereof appear in the chapters on biological and thermal treatment. Mechanical treatment unit processes may also appear at industries using recycled material as part of their feedstock, for example, for removing impurities and homogenizing the material...

  9. MATHEMATICAL MODELING OF HEATING RATE PRODUCT AT HIGH HEAT TREATMENT

    Directory of Open Access Journals (Sweden)

    M. M. Akhmedova

    2014-01-01

    Full Text Available Methods of computing and mathematical modeling are all widely used in the study of various heat exchange processes that provide the ability to study the dynamics of the processes, as well as to conduct a reasonable search for the optimal technological parameters of heat treatment.This work is devoted to the identification of correlations among the factors that have the greatest effect on the rate of heating of the product at hightemperature heat sterilization in a stream of hot air, which are chosen as the temperature difference (between the most and least warming up points and speed cans during heat sterilization.As a result of the experimental data warming of the central and peripheral layers compote of apples in a 3 liter pot at high-temperature heat treatment in a stream of hot air obtained by the regression equation in the form of a seconddegree polynomial, taking into account the effects of pair interaction of these parameters. 

  10. Heat Treatment of Tools in Light Industry

    Science.gov (United States)

    Petukhov, V. A.

    2005-09-01

    Heat treatment processes for some tools (knitting needles, travelers for thimbles of spinning and doubling frames, thread-forming spinnerets) used for the production of cloths, hosiery, and other articles) in the knitting and textile industries are considered. Problems of the choice of steel and the kind and parameters of heat treatment are discussed in connection with the special features of tool design and operating conditions.

  11. 49 CFR 179.400-12 - Postweld heat treatment.

    Science.gov (United States)

    2010-10-01

    ... 49 Transportation 2 2010-10-01 2010-10-01 false Postweld heat treatment. 179.400-12 Section 179... and 107A) § 179.400-12 Postweld heat treatment. (a) Postweld heat treatment of the inner tank is not... be attached before postweld heat treatment. Welds securing the following need not be postweld heat...

  12. Thermal contact resistance in carbon nanotube enhanced heat storage materials

    NARCIS (Netherlands)

    Zhang, H.; Nedea, S.V.; Rindt, C.C.M.; Smeulders, D.M.J.

    2015-01-01

    Solid-liquid phase change is one of the most favorable means of compact and economical heat storage in the built environment. In such storage systems, the vast available solar heat is stored as latent heat in the storage materials. Recent studies suggest using sugar alcohols as seasonal heat storage

  13. Polymers Advance Heat Management Materials for Vehicles

    Science.gov (United States)

    2013-01-01

    For 6 years prior to the retirement of the Space Shuttle Program, the shuttles carried an onboard repair kit with a tool for emergency use: two tubes of NOAX, or "good goo," as some people called it. NOAX flew on all 22 flights following the Columbia accident, and was designed to repair damage that occurred on the exterior of the shuttle. Bill McMahon, a structural materials engineer at Marshall Space Flight Center says NASA needed a solution for the widest range of possible damage to the shuttle s exterior thermal protection system. "NASA looked at several options in early 2004 and decided on a sealant. Ultimately, NOAX performed the best and was selected," he says. To prove NOAX would work effectively required hundreds of samples manufactured at Marshall and Johnson, and a concerted effort from various NASA field centers. Johnson Space Center provided programmatic leadership, testing, tools, and crew training; Glenn Research Center provided materials analysis; Langley Research Center provided test support and led an effort to perform large patch repairs; Ames Research Center provided additional testing; and Marshall provided further testing and the site of NOAX manufacturing. Although the sealant never had to be used in an emergency situation, it was tested by astronauts on samples of reinforced carbon-carbon (RCC) during two shuttle missions. (RCC is the thermal material on areas of the shuttle that experience the most heat, such as the nose cone and wing leading edges.) The material handled well on orbit, and tests showed the NOAX patch held up well on RCC.

  14. Evaluation of carbon diffusion in heat treatment of H13 tool steel under different atmospheric conditions

    Directory of Open Access Journals (Sweden)

    Maziar Ramezani

    2015-04-01

    Full Text Available Although the cost of the heat treatment process is only a minor portion of the total production cost, it is arguably the most important and crucial stage on the determination of material quality. In the study of the carbon diffusion in H13 steel during austenitization, a series of heat treatment experiments had been conducted under different atmospheric conditions and length of treatment. Four austenitization atmospheric conditions were studied, i.e., heat treatment without atmospheric control, heat treatment with stainless steel foil wrapping, pack carburization heat treatment and vacuum heat treatment. The results showed that stainless steel foil wrapping could restrict decarburization process, resulting in a constant hardness profile as vacuum heat treatment does. However, the tempering characteristic between these two heat treatment methods is different. Results from the gas nitrided samples showed that the thickness and the hardness of the nitrided layer is independent of the carbon content in H13 steel.

  15. Heat treatment effect on impact strength of 40Kh steel

    International Nuclear Information System (INIS)

    Golubev, V.K.; Novikov, S.A.; Sobolev, Yu.S.; Yukina, N.A.

    1984-01-01

    The paper presents results of studies on the effect of heat treatment on strength and pattern of 40Kh steel impact failure. Loading levels corresponding to macroscopic spalling microdamage initiation in the material are determined for three initial states. Metallographic study on the spalling failure pattern for 40Kh steel in different initial states and data on microhardness measurement are presented

  16. The effects of heat treatment on physical and technological ...

    African Journals Online (AJOL)

    STORAGESEVER

    2009-10-19

    Oct 19, 2009 ... surface of wood were used to evaluate the effect of heat treatment on the surface characteristics of ... Some of the products developed by thermal treat- .... boards were stored uncontrolled condition in an unheated room for .... These results can be explained with material loses in ...... Finland-state of the art.

  17. Effects of heat treatment on density, dimensional stability and color ...

    African Journals Online (AJOL)

    The purpose of this study was to evaluate the effect of heat treatment on some physical properties and color change of Pinus nigra wood which has high industrial use potential and large growing stocks in Turkey. Wood samples which comprised the material of the study were obtained from an industrial plant. Samples were ...

  18. Heat Transfer Analysis of Localized Heat-Treatment for Grade 91 Steel

    Science.gov (United States)

    Walker, Jacob D.

    Many of the projects utilizing Grade 91 steel are large in scale, therefore it is necessary to assemble on site. The assembly of the major pieces requires welding in the assembly; this drastically changes the superior mechanical properties of Grade 91 steel that it was specifically developed for. Therefore, because of the adverse effects of welding on the mechanical properties of Grade 91, it is necessary to do a localized post weld heat treatment. As with most metallic materials grade 91 steel requires a very specific heat treatment process. This process includes a specific temperature and duration at that temperature to achieve the heat treatment desired. Extensive research has been done to determine the proper temperatures and duration to provide the proper microstructure for the superior mechanical properties that are inherent to Grade 91 steel. The welded sections are typically large structures that require local heat treatments and cannot be placed in an oven. The locations of these structures vary from indoors in a controlled environment to outdoors with unpredictable environments. These environments can be controlled somewhat, however in large part the surrounding conditions are unchangeable. Therefore, there is a need to develop methods to accurately apply the surrounding conditions and geometries to a theoretical model in order to provide the proper requirements for the local heat treatment procedure. Within this requirement is the requirement to define unknowns used in the heat transfer equations so that accurate models can be produced and accurate results predicted. This study investigates experimentally and numerically the heat transfer and temperature fields of Grade 91 piping in a local heat treatment. The objective of this thesis research is to determine all of the needed heat transfer coefficients. The appropriate heat transfer coefficients are determined through the inverse heat conduction method utilizing a ceramic heat blanket. This will be done

  19. Lowcost automated control for steel heat treatments

    International Nuclear Information System (INIS)

    Zambaldi, Edimilson; Magalhães, Ricardo R.; Barbosa, Bruno H.G.; Silva, Sandro P. da; Ferreira, Danton D.

    2017-01-01

    Highlights: • Control the furnace temperature measured by thermocouple and adjusts it. • Activating the furnace resistors through Pulse Width Modulation. • Appling heat treatments to steels by a low-cost controller. - Abstract: The aim of this paper is to propose a low cost, automated furnace control system for the heat treatment of steel. We used an open source electronic prototyping platform to control the furnace temperature, thus reducing human interaction during the heat process. The platform can be adapted to non-controlled commercial furnaces, which are often used by small businesses. A Proportional-Integral-Derivative (PID) controller was implemented to regulate the furnace temperature based on a defined heat treatment cycle. The embedded system activates the furnace resistors through Pulse Width Modulation (PWM), allowing for control of electrical power supplied to the furnace. Hardening and tempering were performed on standard steel samples using a traditional method (visual inspection without temperature control) as well the embedded system with PID feedback control. The results show that the proposed system can reproduce an arbitrary heat treatment curve with accuracy and provide the desired final hardness as inferred through metallographic analysis. In addition, we observed a 6% saving in energy consumption using the proposed control system. Furthermore, the estimated cost to implement the system is 42% lower than a commercial controller model implemented in commercial furnaces.

  20. 49 CFR 179.220-11 - Postweld heat treatment.

    Science.gov (United States)

    2010-10-01

    ... 49 Transportation 2 2010-10-01 2010-10-01 false Postweld heat treatment. 179.220-11 Section 179... Postweld heat treatment. (a) Postweld heat treatment of the inner container is not a specification requirement. (b) Postweld heat treatment of the cylindrical portions of the outer shell to which the anchorage...

  1. 49 CFR 179.500-6 - Heat treatment.

    Science.gov (United States)

    2010-10-01

    ... 49 Transportation 2 2010-10-01 2010-10-01 false Heat treatment. 179.500-6 Section 179.500-6...-6 Heat treatment. (a) Each necked-down tank shall be uniformly heat treated. Heat treatment shall... treatment of alternate steels shall be approved. All scale shall be removed from outside of tank to an...

  2. Evaluation of carbon diffusion in heat treatment of H13 tool steel under different atmospheric conditions

    OpenAIRE

    Ramezani, Maziar; Pasang, Timotius; Chen, Zhan; Neitzert, Thomas; Au, Dominique

    2015-01-01

    Although the cost of the heat treatment process is only a minor portion of the total production cost, it is arguably the most important and crucial stage on the determination of material quality. In the study of the carbon diffusion in H13 steel during austenitization, a series of heat treatment experiments had been conducted under different atmospheric conditions and length of treatment. Four austenitization atmospheric conditions were studied, i.e., heat treatment without atmospheric contro...

  3. Heat transfer in composite materials disintegrating under high-rate one-sided heating

    Science.gov (United States)

    Isaev, K. B.

    1993-12-01

    A mathematical model of heat transfer in heat-protective materials is suggested with the proviso of a squarelaw temperature depence of the material density in the zone of thermal destruction of its binder. The influence of certain factors on the experimental temperature field and thermal conductivity of a glass-reinforced epoxy plastic material is shown.

  4. In situ heat treatment process utilizing a closed loop heating system

    Science.gov (United States)

    Vinegar, Harold J.; Nguyen, Scott Vinh

    2010-12-07

    Systems and methods for an in situ heat treatment process that utilizes a circulation system to heat one or more treatment areas are described herein. The circulation system may use a heated liquid heat transfer fluid that passes through piping in the formation to transfer heat to the formation. In some embodiments, the piping may be positioned in at least two of the wellbores.

  5. Heat Treatment and Properties of Iron and Steel

    National Research Council Canada - National Science Library

    Digges, Thomas

    1966-01-01

    .... Chemical compositions, heat treatments, and some properties and uses are presented for structural steels, tool steels, stainless and heat-resisting steels, precipitation-hardenable stainless steels...

  6. Investigation of material removal rate (MRR) and wire wear ratio (WWR) for alloy Ti6Al4 V exposed to heat treatment processing in WEDM and optimization of parameters using Grey relational analysis

    Energy Technology Data Exchange (ETDEWEB)

    Altug, Mehmet [Inonu Univ., Malatya (Turkey). Dept. of Machine and Metal Technologies

    2016-11-01

    The study examines the changes of the microstructural, mechanical and conductivity characteristics of the titanium alloy Ti6Al4 V as a result of heat treatment using wire electrical discharge machining, and their effect on machinability. By means of optical microscopy and scanning electron microscopy (SEM), analyses have been performed to determine various characteristics and additionally, microhardness and conductivity measurements have been conducted. Material removal rate (MRR) and wire wear ratio (WWR) values have been determined by using L18 Taguchi test design. The microstructures of the samples have been changed by thermal procedures. Results have been obtained by using the Grey relational analysis (GRA) optimization technique to solve the maximum MRR and minimum WWR values. The best (highest) MRR value is obtained from sample E which was water quenched in dual phase processing. The microstructure of this sample is composed of primary α and α' phases. The best (lowest) WWR value is obtained from sample A.

  7. Investigation of material removal rate (MRR) and wire wear ratio (WWR) for alloy Ti6Al4 V exposed to heat treatment processing in WEDM and optimization of parameters using Grey relational analysis

    International Nuclear Information System (INIS)

    Altug, Mehmet

    2016-01-01

    The study examines the changes of the microstructural, mechanical and conductivity characteristics of the titanium alloy Ti6Al4 V as a result of heat treatment using wire electrical discharge machining, and their effect on machinability. By means of optical microscopy and scanning electron microscopy (SEM), analyses have been performed to determine various characteristics and additionally, microhardness and conductivity measurements have been conducted. Material removal rate (MRR) and wire wear ratio (WWR) values have been determined by using L18 Taguchi test design. The microstructures of the samples have been changed by thermal procedures. Results have been obtained by using the Grey relational analysis (GRA) optimization technique to solve the maximum MRR and minimum WWR values. The best (highest) MRR value is obtained from sample E which was water quenched in dual phase processing. The microstructure of this sample is composed of primary α and α' phases. The best (lowest) WWR value is obtained from sample A.

  8. Phase Change Material (PCM) Heat Exchanger Development

    Data.gov (United States)

    National Aeronautics and Space Administration — The primary focus of the project is to provide future space vehicles a reliable form of long duration supplemental heat rejection (SHREDs). SHREDs allow a vehicle to...

  9. Heat transfer in Rockwool modelling and method of measurement. Modelling radiative heat transfer in fibrous materials

    Energy Technology Data Exchange (ETDEWEB)

    Dyrboel, Susanne

    1998-05-01

    Fibrous materials are some of the most widely used materials for thermal insulation. In this project the focus of interest has been on fibrous materials for building application. Interest in improving the thermal properties of insulation materials is increasing as legislation is being tightened to reduce the overall energy consumption. A knowledge of the individual heat transfer mechanisms - whereby heat is transferred within a particular material is an essential tool to improve continuously the thermal properties of the material. Heat is transferred in fibrous materials by four different transfer mechanisms: conduction through air, conduction through fibres, thermal radiation and convection. In a particular temperature range the conduction through air can be regarded as a constant, and conduction through fibres is an insignificant part of the total heat transfer. Radiation, however, constitutes 25-40% of the total heat transfer in light fibrous materials. In Denmark and a number of other countries convection in fibrous materials is considered as non-existent when calculating heat transmission as well as when designing building structures. Two heat transfer mechanisms have been the focus of the current project: radiation heat transfer and convection. The radiation analysis serves to develop a model that can be used in further work to gain a wider knowledge of the way in which the morphology of the fibrous material, i.e. fibre diameter distribution, fibre orientation distribution etc., influences the radiation heat transfer under different conditions. The convection investigation serves to examine whether considering convection as non-existent is a fair assumption to use in present and future building structures. The assumption applied in practically is that convection makes a notable difference only in very thick insulation, at external temperatures below -20 deg. C, and at very low densities. For lager thickness dimensions the resulting heat transfer through the

  10. Gas-solid heat exchange in a fibrous metallic material measured by a heat regenerator technique

    NARCIS (Netherlands)

    Golombok, M.; Jariwala, H.; Shirvill, C.

    1990-01-01

    The convective heat transfer properties of a porous metallic fibre material used in gas surface combustion burners are studied. The important parameter governing the heat transfer between hot gas and metal fibre—the heat transfer coefficient—is measured using a non-steady-state method based on

  11. Corrosion of heat exchanger materials under heat transfer conditions

    International Nuclear Information System (INIS)

    Tapping, R.L.; Lavoie, P.A.; Disney, D.J.

    1987-01-01

    Severe pitting has occurred in moderator heat exchangers tubed with Incoloy-800 in Pickering Nuclear Generating Station. The pitting originated on the cooling side (outside) of the tubes and perforation occurred in less than two years. It was known from corrosion testing at CRNL that Incoloy-800 was not susceptible to pitting in Lake Ontario water under isothermal conditions. Corrosion testing with heat transfer across the tube wall was carried out, and it was noted that severe pitting could occur under deposits formed on the tubes in silty Lake Ontario water. Subsequent testing, carried out in co-operation with Ontario Hydro Research Division, investigated the pitting resistance of other candidate tubing alloys: Incoloy-825, 904 L stainless steel, AL-6X, Inconel-625, 70:30 Cu:Ni, titanium, Sanicro-30 and Sanicro-28 1 . Of these, only titanium and Sanicro-28 have not suffered some degree of pitting attack in silt-containing Lake Ontario Water. In the absence of silt, and hence deposits, no pitting took place on any of the alloys tested

  12. The contact heat transfer between the heating plate and granular materials in rotary heat exchanger under overloaded condition

    Directory of Open Access Journals (Sweden)

    Luanfang Duan

    2018-03-01

    Full Text Available In the present work, the contact heat transfer between the granular materials and heating plates inside plate rotary heat exchanger (PRHE was investigated. The heat transfer coefficient is dominated by the contact heat transfer coefficient at hot wall surface of the heating plates and the heat penetration inside the solid bed. A plot scale PRHE with a diameter of Do = 273 mm and a length of L = 1000 mm has been established. Quartz sand with dp = 2 mm was employed as the experimental material. The operational parameters were in the range of ω = 1 – 8 rpm, and F = 15, 20, 25, 30%, and the effect of these parameters on the time-average contact heat transfer coefficient was analyzed. The time-average contact heat transfer coefficient increases with the increase of rotary speed, but decreases with the increase of the filling degree. The measured data of time-average heat transfer coefficients were compared with theoretical calculations from Schlünder’s model, a good agreement between the measurements and the model could be achieved, especially at a lower rotary speed and filling degree level. The maximum deviation between the calculated data and the experimental data is approximate 10%. Keywords: Rotary heat exchanger, Contact heat transfer, Granular material, Heating plate, Overloaded

  13. Heat treated 9 Cr-1 Mo steel material for high temperature application

    Science.gov (United States)

    Jablonski, Paul D.; Alman, David; Dogan, Omer; Holcomb, Gordon; Cowen, Christopher

    2012-08-21

    The invention relates to a composition and heat treatment for a high-temperature, titanium alloyed, 9 Cr-1 Mo steel exhibiting improved creep strength and oxidation resistance at service temperatures up to 650.degree. C. The novel combination of composition and heat treatment produces a heat treated material containing both large primary titanium carbides and small secondary titanium carbides. The primary titanium carbides contribute to creep strength while the secondary titanium carbides act to maintain a higher level of chromium in the finished steel for increased oxidation resistance, and strengthen the steel by impeding the movement of dislocations through the crystal structure. The heat treated material provides improved performance at comparable cost to commonly used high-temperature steels such as ASTM P91 and ASTM P92, and requires heat treatment consisting solely of austenization, rapid cooling, tempering, and final cooling, avoiding the need for any hot-working in the austenite temperature range.

  14. Effect of heavy ion irradiation and α+β phase heat treatment on oxide of Zr-2.5Nb pressure tube material

    Energy Technology Data Exchange (ETDEWEB)

    Choudhuri, Gargi, E-mail: gargi@barc.gov.in [Quality Assurance Division, BARC, Mumbai, 400085 (India); Mukherjee, P.; Gayathri, N. [Variable Energy Cyclotron Centre, Kolkata, 700064 (India); Kain, V.; Kiran Kumar, M.; Srivastava, D. [Material Science Division, BARC, Mumbai, 400085 (India); Basu, S. [Solid State Physics Division, BARC, Mumbai, 400085 (India); Mukherjee, D. [Quality Assurance Division, BARC, Mumbai, 400085 (India); Dey, G.K. [Material Science Division, BARC, Mumbai, 400085 (India)

    2017-06-15

    Effect of heavy-ion irradiation on the crystalline phase transformation of oxide of Zr-2.5Nb alloys has been studied. The steam-autoclaved oxide of pressure tube is irradiated with 306 KeV Ar{sup +9} ions at a dose of 3 × 10{sup 19} Ar{sup +9}/m{sup 2}. The damage profile has been estimated using “Stopping and Range of Ions in Matter” computer program. The variation of the crystal structure along the depth of the irradiated oxide have been characterized non-destructively by Grazing Incidence X-ray Diffraction technique and compared with unirradiated-oxide. The effect of different base metal microstructures on the characteristic of oxide has also been studied. Base metal microstructure as well as the cross-sectional oxide have been characterized using transmission electron microscope. Heavy ion irradiation can significantly alter the distribution of phases in the oxide of the alloy. The difference in chemical state of alloying element has also been found between unirradiated-oxide with that of irradiated-oxide using X-ray photo electron spectroscopy. Chemical state of Nb in steam autoclaved oxide is also altered when the base metal is α + β heat treated.

  15. Effects of Heat-treatments on the Mechanical Strength of Coated YSZ: An Experimental Assessment

    DEFF Research Database (Denmark)

    Toftegaard, Helmuth Langmaack; Sørensen, Bent F.; Linderoth, Søren

    2009-01-01

    The mechanical strength of thin, symmetric sandwich specimens consisting of a dense yttria-stabilized zirconia (YSZ) substrate coated with a porous NiO–YSZ layer at both major faces was investigated. Specimens were loaded in uniaxial tension to failure following heat treatments at various...... temperatures. In comparison with the YSZ material, the failure strength of coated specimens was found to increase for heat treatments at 1100°C, but decreased again with further increased heat-treatment temperatures....

  16. Metal-dusting resistance of uncoated and coated iron and nickel base materials against metal-dusting in heat treatment furnaces with carbonaceous atmospheres

    International Nuclear Information System (INIS)

    Kleingries, Mirko; Ackermann, Helen; Lucka, Klaus; Hoja, Timo; Mehner, Andeas; Zoch, Hans-Werner; Altena, Herwig

    2010-01-01

    Metal-Dusting is a well-known corrosion problem that occurs in carburizing atmospheres in industrial thermal processing plants. In literature almost no quantitative data on the metal dusting resistance of typical alloys employed in industrial furnaces are available. Therefore, a series of experiments with uncoated and sol gel ZrO 2 coated high temperature materials was conducted in order to quantify their metal dusting behaviour under conditions close to those in case hardening furnaces. The experimental results show a strong influence of the surface conditions on the alloys resistance and a noticeable enhancement of the resistance by sol gel coatings. (orig.)

  17. Fourier analysis of conductive heat transfer for glazed roofing materials

    Energy Technology Data Exchange (ETDEWEB)

    Roslan, Nurhana Lyana; Bahaman, Nurfaradila; Almanan, Raja Noorliyana Raja; Ismail, Razidah [Faculty of Computer and Mathematical Sciences, Universiti Teknologi MARA, 40450 Shah Alam, Selangor (Malaysia); Zakaria, Nor Zaini [Faculty of Applied Sciences, Universiti Teknologi MARA, 40450 Shah Alam, Selangor (Malaysia)

    2014-07-10

    For low-rise buildings, roof is the most exposed surface to solar radiation. The main mode of heat transfer from outdoor via the roof is conduction. The rate of heat transfer and the thermal impact is dependent on the thermophysical properties of roofing materials. Thus, it is important to analyze the heat distribution for the various types of roofing materials. The objectives of this paper are to obtain the Fourier series for the conductive heat transfer for two types of glazed roofing materials, namely polycarbonate and polyfilled, and also to determine the relationship between the ambient temperature and the conductive heat transfer for these materials. Ambient and surface temperature data were collected from an empirical field investigation in the campus of Universiti Teknologi MARA Shah Alam. The roofing materials were installed on free-standing structures in natural ventilation. Since the temperature data are generally periodic, Fourier series and numerical harmonic analysis are applied. Based on the 24-point harmonic analysis, the eleventh order harmonics is found to generate an adequate Fourier series expansion for both glazed roofing materials. In addition, there exists a linear relationship between the ambient temperature and the conductive heat transfer for both glazed roofing materials. Based on the gradient of the graphs, lower heat transfer is indicated through polyfilled. Thus polyfilled would have a lower thermal impact compared to polycarbonate.

  18. The technological raw material heating furnaces operation efficiency improving issue

    Science.gov (United States)

    Paramonov, A. M.

    2017-08-01

    The issue of fuel oil applying efficiency improving in the technological raw material heating furnaces by means of its combustion intensification is considered in the paper. The technical and economic optimization problem of the fuel oil heating before combustion is solved. The fuel oil heating optimal temperature defining method and algorithm analytically considering the correlation of thermal, operating parameters and discounted costs for the heating furnace were developed. The obtained optimization functionality provides the heating furnace appropriate thermal indices achievement at minimum discounted costs. The carried out research results prove the expediency of the proposed solutions using.

  19. Heat storage system utilizing phase change materials government rights

    Science.gov (United States)

    Salyer, Ival O.

    2000-09-12

    A thermal energy transport and storage system is provided which includes an evaporator containing a mixture of a first phase change material and a silica powder, and a condenser containing a second phase change material. The silica powder/PCM mixture absorbs heat energy from a source such as a solar collector such that the phase change material forms a vapor which is transported from the evaporator to the condenser, where the second phase change material melts and stores the heat energy, then releases the energy to an environmental space via a heat exchanger. The vapor is condensed to a liquid which is transported back to the evaporator. The system allows the repeated transfer of thermal energy using the heat of vaporization and condensation of the phase change material.

  20. Experimental investigation on heat transport in gravel-sand materials

    DEFF Research Database (Denmark)

    Maureschat, Gerald; Heller, Alfred

    1997-01-01

    in sand-gravel material, the storage media is to be water satured. In this case, handling of such material on site is rather complex. The conduction is highly dependent on the thermal properties of the storage media and so is the overall thermal performance of a storage applying such media. For sandy...... out in a small size experiment. The experiment consists of a highly insulated box filled with two kinds of sand material crossed by a plastic heat pipe. Heat transfer is measured under dry and water satured conditions in a cross-section.The conclusions are clear. To obtain necessary heat conduction...

  1. Preparation, heat treatment, and mechanical properties of the uranium-5 weight percent chromium eutectic alloy

    International Nuclear Information System (INIS)

    Townsend, A.B.

    1980-10-01

    The eutectic alloy of uranium-5 wt % chromium (U-5Cr) was prepared from high-purity materials and cast into 1-in.-thick ingots. This material was given several simple heat treatments, the mechanical properties of these heat-treated samples were determined; and the microstructure was examined. Some data on the melting point and transformation temperatures were obtained

  2. Novel magnetic heating probe for multimodal cancer treatment.

    Science.gov (United States)

    Kan-Dapaah, Kwabena; Rahbar, Nima; Soboyejo, Wole

    2015-05-01

    Multifunctional materials consisting of polymers and magnetic nanoparticles (MNPs) are highly sought after in the field of biomedical engineering. These materials offer new opportunities for the development of novel cancer treatment modalities that can increase the efficacy of cancer therapy. In this paper, a novel probe for multimodal cancer treatment is proposed and analyzed. The probe is essentially a cannula with two main parts: a distal heat generating tip made of a magnetic nanocomposite and a proximal insulated shaft. A description of the concept and functional operations of the probe is presented. In an effort to assess its feasibility, the authors evaluated the ability of probe tip (made of PMMA-Fe3O4 nanocomposite) to generate heat in biological tissue using alternating magnetic field (AMF) parameters (field strength and frequency) that are acceptable for human use. Heat generation by MNPs was determined using the linear response theory. The effects of Fe3O4 volume fraction on heat generation as well as treatment time on the thermal dose were studied. The finite element method model was tested for its validity using an analytical model. Lesions were revealed to have an ellipsoidal shape and their sizes were affected by treatment time. However, their shapes remained unchanged. The comparison with the analytical model showed reasonably a good agreement to within 2%. Furthermore, the authors' numerical predictions also showed reasonable agreement with the experimental results previously reported in the literature. The authors' predictions demonstrate the feasibility of their novel probe to achieve reasonable lesion sizes, during hyperthermic or ablative heating using AMF parameters (field strength and frequency) that are acceptable for human use.

  3. Saving energy resources during heat treatment - the most important problem of the branch

    Energy Technology Data Exchange (ETDEWEB)

    Zadernovskiy, V V; Firger, I V

    1980-01-01

    Natural gas fired thermal furnaces expend significantly less fuel than electric furnaces with an equal quality of metal heating. An important reserve in power reserve economy is the use of the forging heat in an article for heat treatment (TOB), where besides the power resources, metal is also saved as a result of the reduction in the volume of heating means and production spaces. From the experience in the progressive enterprises of the branch, in a number of cases it is possible to combine heating for plastic deformation with heating for primary or secondary heat treatment. Other measures are examined which save power resources in heat treatment: the use of thermal furnaces for aerodynamic heating, the use of local heat treatment, the reduction in the duration of the heat treatment processes, savings in the power carriers during heat treatment in furnaces with a roll out hearth. Fibrous refractory materials are being used more and more as fettling materials in the construction of thermal furnaces.

  4. Induction heat treatment of laser welds

    DEFF Research Database (Denmark)

    Bagger, Claus; Olsen, Flemming Ove; Sørensen, Joakim Ilsing

    2003-01-01

    of an induction coil. A number of systematic laboratory tests were then performed in order to study the effects of the coil on bead-on-plate laser welded samples. In these tests, important parameters such as coil current and distance between coil and sample were varied. Temperature measurements were made...... the laser beam as close as possible. After welding, the samples were quality assessed according to ISO 13.919-1 and tested for hardness. The metallurgical phases are analysed and briefly described. A comparison between purely laser welded samples and induction heat-treated laser welded samples is made......In this paper, a new approach based on induction heat-treatment of flat laser welded sheets is presented. With this new concept, the ductility of high strength steels GA260 with a thickness of 1.8 mm and CMn with a thickness of 2.13 mm is believed to be improved by prolonging the cooling time from...

  5. Microencapsulated Phase-Change Materials For Storage Of Heat

    Science.gov (United States)

    Colvin, David P.

    1989-01-01

    Report describes research on engineering issues related to storage and transport of heat in slurries containing phase-change materials in microscopic capsules. Specific goal of project to develop lightweight, compact, heat-management systems used safely in inhabited areas of spacecraft. Further development of obvious potential of technology expected to lead to commercialization and use in aircraft, electronic equipment, machinery, industrial processes, and other sytems in which requirements for management of heat compete with severe restrictions on weight or volume.

  6. Evaluation of material fracture energy by its heat content

    International Nuclear Information System (INIS)

    Frolov, G.A.; Pasichnyj, V.V.; Polezhaev, Yu.V.; Frolov, A.A.; Choba, A.V.

    1986-01-01

    Based on published and experimental data it is shown that there is a simple relationship between the heat of evaporation and heat content. This allows in some instances the evaluation of a rate of material fracture by its content. Experimental and theoretical data for quartz glass ceramics, and glass-reinforced plastic are presented

  7. Influence of Heat Treatment on Mercury Cavitation Resistance of Surface Hardened 316LN Stainless Steel

    Energy Technology Data Exchange (ETDEWEB)

    Pawel, Steven J [ORNL; Hsu, Julia [Massachusetts Institute of Technology (MIT)

    2010-11-01

    The cavitation-erosion resistance of carburized 316LN stainless steel was significantly degraded but not destroyed by heat treatment in the temperature range 500-800 C. The heat treatments caused rejection of some carbon from the carburized layer into an amorphous film that formed on each specimen surface. Further, the heat treatments encouraged carbide precipitation and reduced hardness within the carburized layer, but the overall change did not reduce surface hardness fully to the level of untreated material. Heat treatments as short as 10 min at 650 C substantially reduced cavitation-erosion resistance in mercury, while heat treatments at 500 and 800 C were found to be somewhat less detrimental. Overall, the results suggest that modest thermal excursions perhaps the result of a weld made at some distance to the carburized material or a brief stress relief treatment will not render the hardened layer completely ineffective but should be avoided to the greatest extent possible.

  8. Effect of phase change material on the heat transfer rate of different building materials

    Science.gov (United States)

    Hasan, Mushfiq; Alam, Shahnur; Ahmed, Dewan Hasan

    2017-12-01

    Phase change material (PCM) is widely known as latent heat storage. A comprehensive study is carried out to investigate the effect of PCM on heat transfer rate of building materials. Paraffin is used as PCM along with different conventional building materials to investigate the heat transfer rate from the heated region to the cold region. PCM is placed along with the three different types of building materials like plaster which is well know building material in urban areas and wood and straw which are commonly used in rural areas for roofing as well as wall panel material and investigated the heat transfer rate. An experimental setup was constructed with number of rectangular shape aluminum detachable casing (as cavity) and placed side by side. Series of rectangular cavity filled with convent ional building materials and PCM and these were placed in between two chambers filled with water at different temperature. Building materials and PCM were placed in different cavities with different combinations and investigated the heat transfer rate. The results show that using the PCM along with other building materials can be used to maintain lower temperature at the inner wall and chamber of the cold region. Moreover, the placement or orientation of the building materials and PCM make significant contribution to heat transfer rate from the heated zone to the cold zone.

  9. Heat transfer characteristics of building walls using phase change material

    Science.gov (United States)

    Irsyad, M.; Pasek, A. D.; Indartono, Y. S.; Pratomo, A. W.

    2017-03-01

    Minimizing energy consumption in air conditioning system can be done with reducing the cooling load in a room. Heat from solar radiation which passes through the wall increases the cooling load. Utilization of phase change material on walls is expected to decrease the heat rate by storing energy when the phase change process takes place. The stored energy is released when the ambient temperature is low. Temperature differences at noon and evening can be utilized as discharging and charging cycles. This study examines the characteristics of heat transfer in walls using phase change material (PCM) in the form of encapsulation and using the sleeve as well. Heat transfer of bricks containing encapsulated PCM, tested the storage and released the heat on the walls of the building models were evaluated in this study. Experiments of heat transfer on brick consist of time that is needed for heat transfer and thermal conductivity test as well. Experiments were conducted on a wall coated by PCM which was exposed on a day and night cycle to analyze the heat storage and heat release. PCM used in these experiments was coconut oil. The measured parameter is the temperature at some points in the brick, walls and ambient temperature as well. The results showed that the use of encapsulation on an empty brick can increase the time for thermal heat transfer. Thermal conductivity values of a brick containing encapsulated PCM was lower than hollow bricks, where each value was 1.3 W/m.K and 1.6 W/m.K. While the process of heat absorption takes place from 7:00 am to 06:00 pm, and the release of heat runs from 10:00 pm to 7:00 am. The use of this PCM layer can reduce the surface temperature of the walls of an average of 2°C and slows the heat into the room.

  10. Viscose liquid heat treatment using plate scraper heat exchanger

    Directory of Open Access Journals (Sweden)

    K. A. Rashkin

    2012-01-01

    Full Text Available The current work analyzes the use of different types of heat exchangers, depending on the technology of production. It is taken the detail analysis of the ways of applicability of various types of heat exchangers, depending on the viscosity of the processed product. It is posed the problem of the analytical determination of the required area of heat exchange with the use of differential equations of heat transfer in a moving liquid media, written in cylindrical coordinates, for symmetrical temperature distribution, without taking in account the energy dissipation.

  11. Improving the Material Response for Slow Heat of Energetic Materials

    Energy Technology Data Exchange (ETDEWEB)

    Nichols, A L

    2010-03-08

    The goal of modern high explosive slow heat cookoff modeling is to understand the level of mechanical violence. This requires understanding the coupled thermal-mechanical-chemical system that such an environment creates. Recent advances have improved our ability to predict the time to event, and we have been making progress on predicting the mechanical response. By adding surface tension to the product gas pores in the high explosive, we have been able to reduce the current model's tendency to overpressurize confinement vessels. We describe the model and demonstrate how it affects a LX-10 STEX experiment. Issues associated with current product gas equations of state are described and examined.

  12. Heat-resistant materials 2. Conference proceedings of the 2. international conference on heat-resistant materials

    International Nuclear Information System (INIS)

    Natesan, K.; Ganesan, P.; Lai, G.Y.

    1995-01-01

    The Second International Conference on Heat-Resistant Materials was held in Gatlinburg, Tennessee, September 11--14, 1995 and focused on materials performance in cross-cutting technologies where heat resistant materials play a large and sometimes life-and performance-limiting roles in process schemes. The scope of materials for heat-resistant applications included structural iron- and nickel-base alloys, intermetallics, and ceramics. The conference focused on materials development, performance of materials in simulated laboratory and actual service environments on mechanical and structural integrity of components, and state-of-the-art techniques for processing and evaluating materials performance. The three keynote talks described the history of heat-resistant materials, relationship between microstructure and mechanical behavior, and applications of these materials in process schemes. The technical sessions included alloy metallurgy and properties, environmental effects and properties, deformation behavior and properties, relation between corrosion and mechanical properties, coatings, intermetallics, ceramics, and materials for waste incineration. Seventy one papers have been processed separately for inclusion on the data base

  13. Nanoscale heat transfer in carbon nanotube - sugar alcohol composites as heat storage materials

    NARCIS (Netherlands)

    Zhang, H.; Rindt, C.C.M.; Smeulders, D.M.J.; Gaastra - Nedea, S.V.

    2016-01-01

    Nanoscale carbon structures such as graphene and carbon nanotubes (CNTs) can greatly improve the effective thermal conductivity of thermally sluggish heat storage materials, such as sugar alcohols (SAs). The specific improvement depends on the heat transfer rate across the carbon structure. Besides,

  14. Radiative heat transfer in 2D Dirac materials

    International Nuclear Information System (INIS)

    Rodriguez-López, Pablo; Tse, Wang-Kong; Dalvit, Diego A R

    2015-01-01

    We compute the radiative heat transfer between two sheets of 2D Dirac materials, including topological Chern insulators and graphene, within the framework of the local approximation for the optical response of these materials. In this approximation, which neglects spatial dispersion, we derive both numerically and analytically the short-distance asymptotic of the near-field heat transfer in these systems, and show that it scales as the inverse of the distance between the two sheets. Finally, we discuss the limitations to the validity of this scaling law imposed by spatial dispersion in 2D Dirac materials. (paper)

  15. Mortality of insect life stages during simulated heat treatment

    Science.gov (United States)

    . Heat treatment for insect disinfestation uses elevated air temperatures that are lethal to stored-product insects. Heat treatment has been demonstrated in our research to offer a reduced-risk alternative to fumigation or residual pesticide use in empty bins. Heat is also compatible with organic gr...

  16. Efficacy of heat treatment for disinfestation of concrete grain silos

    Science.gov (United States)

    Field experiments were conducted in 2007 and 2008 to evaluate heat treatment for disinfestations of empty concrete elevator silos. A Mobile Heat Treatment Unit was used to introduce heat into silos to attain target conditions of 50°C for at least 6 h. Ventilated plastic containers with a capacity of...

  17. Heat load material studies: Simulated tokamak disruptions

    International Nuclear Information System (INIS)

    Gahl, J.M.; McDonald, J.M.; Zakharov, A.; Tserevitinov, S.; Barabash, V.; Guseva, M.

    1991-01-01

    It is clear that an improved understanding of the effects of tokamak disruptions on plasma facing component materials is needed for the ITER program. very large energy fluxes are predicted to be deposited in ITER and could be very damaging to the machine. During 1991, Sandia National Laboratories and the University of New Mexico conducted cooperative tokamak disruption simulation experiments at several Soviet facilities. These facilities were located at the Efremov Institute in Leningrad, the Kurchatov Atomic Energy Institute (Troisk and Moscow) and the Institute for Physical Chemistry of the Soviet Adademy of Sciences in Moscow. Erosion of graphite from plasma stream impact is seen to be much less than that observed with laser or electron beams with similar energy fluxes. This, along with other data obtained, seem to suggest that the ''vapor shielding'' effect is a very important phenomenon in the study of graphite erosion during tokamak disruption

  18. Grain Refinement of Low Carbon Martensitic Steel by Heat Treatment

    Directory of Open Access Journals (Sweden)

    N. V. Kolebina

    2015-01-01

    Full Text Available The low-carbon steels have good corrosion and technological properties. Hot deformation is the main operation in manufacturing the parts from these steels. So one of the important properties of the material is a property of plasticity. The grain size significantly influences on the ductility properties of steel. The grain size of steel depends on the chemical composition of the crystallization process, heat treatment, and steel machining. There are plenty methods to have grain refinement. However, taking into account the large size of the blanks for the hydro turbine parts, the thermal cycling is an advanced method of the grain refinement adaptable to streamlined production. This work experimentally studies the heat treatment influence on the microstructure of the low-carbon 01X13N04 alloy steel and proposes the optimal regime of the heat treatment to provide a significantly reduced grain size. L.M. Kleiner, N.P. Melnikov and I.N. Bogachyova’s works focused both on the microstructure of these steels and on the influence of its parameters on the mechanical properties. The paper focuses mainly on defining an optimal regime of the heat treatment for grain refinement. The phase composition of steel and temperature of phase transformation were defined by the theoretical analysis. The dilatometric experiment was done to determine the precise temperature of the phase transformations. The analysis and comparison of the experimental data with theoretical data and earlier studies have shown that the initial sample has residual stress and chemical heterogeneity. The influence of the heat treatment on the grain size was studied in detail. It is found that at temperatures above 950 ° C there is a high grain growth. It is determined that the optimal number of cycles is two. The postincreasing number of cycles does not cause further reducing grain size because of the accumulative recrystallization process. Based on the results obtained, the thermal cycling

  19. Material Selection for Microchannel Heatsink: Conjugate Heat Transfer Simulation

    Science.gov (United States)

    Uday Kumar, A.; Javed, Arshad; Dubey, Satish K.

    2018-04-01

    Heat dissipation during the operation of electronic devices causes rise in temperature, which demands an effective thermal management for their performance, life and reliability. Single phase liquid cooling in microchannels is an effective and proven technology for electronics cooling. However, due to the ongoing trends of miniaturization and developments in the microelectronics technology, the future needs of heat flux dissipation rate are expected to rise to 1 kW/cm2. Air cooled systems are unable to meet this demand. Hence, liquid cooled heatsinks are preferred. This paper presents conjugate heat transfer simulation of single phase flow in microchannels with application to electronic cooling. The numerical model is simulated for different materials: copper, aluminium and silicon as solid and water as liquid coolant. The performances of microchannel heatsink are analysed for mass flow rate range of 20-40 ml/min. The investigation has been carried out on same size of electronic chip and heat flux in order to have comparative study of different materials. This paper is divided into two sections: fabrication techniques and numerical simulation for different materials. In the first part, a brief discussion of fabrication techniques of microchannel heatsink have been presented. The second section presents conjugate heat transfer simulation and parametric investigation for different material microchannel heatsink. The presented study and findings are useful for selection of materials for microchannel heatsink.

  20. THE HEAT TREATMENT ANALYSIS OF E110 CASE HARDENING STEEL

    Directory of Open Access Journals (Sweden)

    MAJID TOLOUEI-RAD

    2016-03-01

    Full Text Available This paper investigates mechanical and microstructural behaviour of E110 case hardening steel when subjected to different heat treatment processes including quenching, normalizing and tempering. After heat treatment samples were subjected to mechanical and metallographic analysis and the properties obtained from applying different processes were analysed. The heat treatment process had certain effects on the resultant properties and microstructures obtained for E110 steel which are described in details. Quenching produced a martensitic microstructure characterized by significant increase in material’s hardness and a significant decreased in its impact energy. Annealed specimens produced a coarse pearlitic microstructure with minimal variation in hardness and impact energy. For normalized samples, fine pearlitic microstructure was identified with a moderate increase in hardness and significant reduction in impact energy. Tempering had a significant effect on quenched specimens, with a substantial rise in material ductility and reduction of hardness with increasing tempering temperature. Furthermore, Results provide additional substantiation of temper embrittlement theory for low-carbon alloys, and indicate potential occurrence of temper embrittlement for fine pearlitic microstructures.

  1. Calculation of the major material parameters of heat carriers for cryogenic heat pipes

    International Nuclear Information System (INIS)

    Molt, W.

    1976-07-01

    In order to make predictions on the efficiency of cryogenic heat pipes, the material parameters of the heat carrier such as surface tension, viscosity, evaporation heat and density of the liquid should be known. The author therefore investigates suitable interpolation methods and equations which enable the calculation of the desired material parameter at a certain temperature from other known quantities or which require that 1 to 3 material parameters at different temperatures are known. The calculations are limited to the temperature between critical temperature and triple point, since this is the only temperature region in which the heat carrier is in its liquid phase. The applicability and exactness of the equations is tested using known experimental data on N 2 , O 2 , CH 4 and partly on CF 4 . (orig./TK) [de

  2. Materials for nuclear diffusion-bonded compact heat exchangers

    International Nuclear Information System (INIS)

    Li, Xiuqing; Smith, Tim; Kininmont, David; Dewson, Stephen John

    2009-01-01

    This paper discusses the characteristics of materials used in the manufacture of diffusion bonded compact heat exchangers. Heatric have successfully developed a wide range of alloys tailored to meet process and customer requirements. This paper will focus on two materials of interest to the nuclear industry: dual certified SS316/316L stainless steel and nickel-based alloy Inconel 617. Dual certified SS316/316L is the alloy used most widely in the manufacture of Heatric's compact heat exchangers. Its excellent mechanical and corrosion resistance properties make it a good choice for use with many heat transfer media, including water, carbon dioxide, liquid sodium, and helium. As part of Heatric's continuing product development programme, work has been done to investigate strengthening mechanisms of the alloy; this paper will focus in particular on the effects of nitrogen addition. Another area of Heatric's programme is Alloy 617. This alloy has recently been developed for diffusion bonded compact heat exchanger for high temperature nuclear applications, such as the intermediate heat exchanger (IHX) for the very high temperature nuclear reactors for production of electricity, hydrogen and process heat. This paper will focus on the effects of diffusion bonding process and cooling rate on the properties of alloy 617. This paper also compares the properties and discusses the applications of these two alloys to compact heat exchangers for various nuclear processes. (author)

  3. Nanomodified heat-accumulating materials controlled by a magnetic field

    Science.gov (United States)

    Shchegolkov, Alexander; Shchegolkov, Alexey; Dyachkova, Tatyana; Bodin, Nikolay; Semenov, Alexander

    2017-11-01

    The paper presents studies of nanomodified heat-accumulating materials controlled by a magnetic field. In order to obtain controlled heat-accumulating materials, synthetic motor oil CASTROL 0W30, ferromagnetic particles, CNTs and paraffin were used. Mechanically activated carbon nanotubes with ferromagnetic particles were used for the nanomodification of paraffin. Mechanoactivation ensured the production of ferromagnetic particles with an average particle size of 5 µm. Using an extrusion plant, a mixture of CNTs and ferromagnetic particles was introduced into the paraffin. Further, the nanomodified paraffin in a granular form was introduced into synthetic oil. To conduct experimental studies, a contactless method for measuring temperature was used. The thermal contact control with the help of the obtained nanomodified material is possible with a magnetic induction of 1250 mT, and a heat flux of about 74 kW/m2 is provided at the same time.

  4. Investigation of heat distribution during magnetic heating treatment using a polyurethane–ferrofluid phantom-model

    International Nuclear Information System (INIS)

    Henrich, F.; Rahn, H.; Odenbach, S.

    2014-01-01

    Magnetic heating treatment can be used as an adjuvant treatment for cancer therapy. In this therapy, magnetic nanoparticles are enriched inside the tumour and exposed to an alternating magnetic field. Due to magnetic losses the temperature in the tumour rises. The resulting temperature profile inside the tumour is useful for the therapeutic success. In this context heat transfer between tissue with nanoparticles and tissue without nanoparticles is a highly important feature which is actually not understood in detail. In order to investigate this, a phantom has been created which can be used to measure the temperature profile around a region enriched with magnetic nanoparticles. This phantom is composed of a material, which has similar thermal conductivity as human tissue. A tempered water bath surrounds the phantom to establish a constant surrounding temperature simulating the heat sink provided by the human body in a real therapeutic application. It has been found that even at a low concentration of magnetic nanoparticles around 13 mg/ml, sufficient heating of the enriched region can be achieved. Moreover it has been observed that the temperature drops rapidly in the material surrounding the enriched region. Corresponding numerical investigations provide a basis for future recalculations of the temperature inside the tumour using temperature data obtained in the surrounding tissue. - Highlights: • The temperature profile by magnetic hyperthermia was examined. • A model was built to get a deeper understanding of the temperature profile. • The temperature profile of the model inside magnetic fields was measured. • Based on the model a simulation of the temperature profile was performed. • The simulated temperature profile agreed well with the measured profile

  5. Dimensional Behavior of Matrix Graphite Compacts during Heat Treatments for HTGR Fuel Element Fabrication

    International Nuclear Information System (INIS)

    Lee, Young-Woo; Yeo, Seunghwan; Cho, Moon Sung

    2015-01-01

    The carbonization is a process step where the binder that is incorporated during the matrix graphite powder preparation step is evaporated and the residue of the binder is carbonized during the heat treatment at about 1073 K. This carbonization step is followed by the final high temperature heat treatment where the carbonized compacts are heat treated at 2073-2173 K in vacuum for a relatively short time (about 2 hrs). In order to develop a fuel compact fabrication technology, and for fuel matrix graphite to meet the required material properties, it is essential to investigate the relationship among the process parameters of the matrix graphite powder preparation, the fabrication parameters of fuel element green compact and the heat treatments conditions, which has a strong influence on the further steps and the material properties of fuel element. In this work, the dimensional changes of green compacts during the carbonization and final heat treatment are evaluated when compacts have different densities from different pressing conditions and different final heat treatment temperatures are employed, keeping other process parameters constant, such as the binder content, carbonization time, temperature and atmosphere (two hours ant 1073K and N2 atmosphere). In this work, the dimensional variations of green compacts during the carbonization and final heat treatment are evaluated when compacts have different densities from different pressing conditions and different final heat treatment temperatures are employed

  6. Energy density enhancement of chemical heat storage material for magnesium oxide/water chemical heat pump

    International Nuclear Information System (INIS)

    Myagmarjav, Odtsetseg; Zamengo, Massimiliano; Ryu, Junichi; Kato, Yukitaka

    2015-01-01

    A novel candidate chemical heat storage material having higher reaction performance and higher thermal conductivity used for magnesium oxide/water chemical heat pump was developed in this study. The material, called EML, was obtained by mixing pure Mg(OH)_2 with expanded graphite (EG) and lithium bromide (LiBr), which offer higher thermal conductivity and reactivity, respectively. With the aim to achieve a high energy density, the EML composite was compressed into figure of the EML tablet (ϕ7.1 mm × thickness 3.5 mm). The compression force did not degrade the reaction conversion, and furthermore it enabled us to achieve best heat storage and output performances. The EML tablet could store heat of 815.4 MJ m_t_a_b"−"3 at 300 °C within 120 min, which corresponded to almost 4.4 times higher the heat output of the EML composite, and therefore, the EML tablet is the solution which releases more heat in a shorter time. A relatively larger volumetric gross heat output was also recorded for the EML tablet, which was greater than one attained for the EML composite at certain temperatures. As a consequence, it is expected that the EML tablet could respond more quickly to sudden demand of heat from users. It was concluded that the EML tablet demonstrated superior performances. - Highlights: • A new chemical heat storage material, donated as EML, was developed. • EML composite made from pure Mg(OH)_2, expanded graphite and lithium bromide. • EML tablet was demonstrated by compressing the EML composite. • Compression force did not degrade the conversion in dehydration and hydration. • EML tablet demonstrated superior heat storage and output performances.

  7. Lauric and palmitic acids eutectic mixture as latent heat storage material for low temperature heating applications

    International Nuclear Information System (INIS)

    Tuncbilek, Kadir; Sari, Ahmet; Tarhan, Sefa; Erguenes, Gazanfer; Kaygusuz, Kamil

    2005-01-01

    Palmitic acid (PA, 59.8 deg. C) and lauric acid (LA, 42.6 deg. C) are phase change materials (PCM) having quite high melting temperatures which can limit their use in low temperature solar applications such as solar space heating and greenhouse heating. However, their melting temperatures can be tailored to appropriate value by preparing a eutectic mixture of the lauric and the palmitic acids. In the present study, the thermal analysis based on differential scanning calorimetry (DSC) technique shows that the mixture of 69.0 wt% LA and 31 wt% PA forms a eutectic mixture having melting temperature of 35.2 deg. C and the latent heat of fusion of 166.3 J g -1 . This study also considers the experimental determination of the thermal characteristics of the eutectic mixture during the heat charging and discharging processes. Radial and axial temperature distribution, heat transfer coefficient between the heat transfer fluid (HTF) pipe and the PCM, heat recovery rate and heat charging and discharging fractions were experimentally established employing a vertical concentric pipe-in-pipe energy storage system. The changes of these characteristics were evaluated with respect to the effect of inlet HTF temperature and mass flow rate. The DSC thermal analysis and the experimental results indicate that the LA-PA eutectic mixture can be a potential material for low temperature thermal energy storage applications in terms of its thermo-physical and thermal characteristics

  8. Methods for microwave heat treatment of manufactured components

    Science.gov (United States)

    Ripley, Edward B.

    2010-08-03

    An apparatus for heat treating manufactured components using microwave energy and microwave susceptor material. Heat treating medium such as eutectic salts may be employed. A fluidized bed introduces process gases which may include carburizing or nitriding gases. The process may be operated in a batch mode or continuous process mode. A microwave heating probe may be used to restart a frozen eutectic salt bath.

  9. 49 CFR 179.100-10 - Postweld heat treatment.

    Science.gov (United States)

    2010-10-01

    ... 49 Transportation 2 2010-10-01 2010-10-01 false Postweld heat treatment. 179.100-10 Section 179...-10 Postweld heat treatment. (a) After welding is complete, steel tanks and all attachments welded... treatment is prohibited. (c) Tank and welded attachments, fabricated from ASTM A 240/A 240M (IBR, see § 171...

  10. Water Based Phase Change Material Heat Exchanger Development

    Science.gov (United States)

    Hansen, Scott W.; Sheth, Ribik B.; Atwell, Matt; Cheek, Ann; Agarwal, Muskan; Hong, Steven; Patel, Aashini,; Nguyen, Lisa; Posada, Luciano

    2014-01-01

    In a cyclical heat load environment such as low Lunar orbit, a spacecraft’s radiators are not sized to reject the full heat load requirement. Traditionally, a supplemental heat rejection device (SHReD) such as an evaporator or sublimator is used to act as a “topper” to meet the additional heat rejection demands. Utilizing a Phase Change Material (PCM) heat exchanger (HX) as a SHReD provides an attractive alternative to evaporators and sublimators as PCM HXs do not use a consumable, thereby leading to reduced launch mass and volume requirements. Studies conducted in this paper investigate utilizing water’s high latent heat of formation as a PCM, as opposed to traditional waxes, and corresponding complications surrounding freezing water in an enclosed volume. Work highlighted in this study is primarily visual and includes understanding ice formation, freeze front propagation, and the solidification process of water/ice. Various test coupons were constructed of copper to emulate the interstitial pin configuration (to aid in conduction) of the proposed water PCM HX design. Construction of a prototypic HX was also completed in which a flexible bladder material and interstitial pin configurations were tested. Additionally, a microgravity flight was conducted where three copper test articles were frozen continuously during microgravity and 2-g periods and individual water droplets were frozen during microgravity.

  11. Study of heat treatment parameters for large-scale hydraulic steel gate track

    Directory of Open Access Journals (Sweden)

    Ping-zhou Cao

    2013-10-01

    Full Text Available In order to enhance external hardness and strength, a large-scale hydraulic gate track should go through heat treatment. The current design method of hydraulic gate wheels and tracks is based on Hertz contact linear elastic theory, and does not take into account the changes in mechanical properties of materials caused by heat treatment. In this study, the heat treatment parameters were designed and analyzed according to the bearing mechanisms of the wheel and track. The quenching process of the track was simulated by the ANSYS program, and the temperature variation, residual stress, and deformation were obtained and analyzed. The metallurgical structure field after heat treatment was predicted by the method based on time-temperature-transformation (TTT curves. The results show that the analysis method and designed track heat treatment process are feasible, and can provide a reference for practical projects.

  12. Heat Treatment of Cr- and Cr-V ledeburitic tool steels

    Directory of Open Access Journals (Sweden)

    Peter Jurči

    2014-11-01

    Full Text Available Cr- and Cr-V ledeburitic cold work tool steels belong to the most important tool materials for large series manufacturing. To enable high production stability, the tools must be heat treated before use. This overview paper brings a comprehensive study on the heat treatment of these materials, starting from the soft annealing and finishing with the tempering. Also, it describes the impact of any step of the heat treatment on the most important structural and mechanical characteristics, like the hardness, the toughness and the wear resistance. The widely used AIS D2- steel (conventionally manufactured and Vanadis 6 (PM are used as examples in most cases.

  13. Rapid charging of thermal energy storage materials through plasmonic heating.

    Science.gov (United States)

    Wang, Zhongyong; Tao, Peng; Liu, Yang; Xu, Hao; Ye, Qinxian; Hu, Hang; Song, Chengyi; Chen, Zhaoping; Shang, Wen; Deng, Tao

    2014-09-01

    Direct collection, conversion and storage of solar radiation as thermal energy are crucial to the efficient utilization of renewable solar energy and the reduction of global carbon footprint. This work reports a facile approach for rapid and efficient charging of thermal energy storage materials by the instant and intense photothermal effect of uniformly distributed plasmonic nanoparticles. Upon illumination with both green laser light and sunlight, the prepared plasmonic nanocomposites with volumetric ppm level of filler concentration demonstrated a faster heating rate, a higher heating temperature and a larger heating area than the conventional thermal diffusion based approach. With controlled dispersion, we further demonstrated that the light-to-heat conversion and thermal storage properties of the plasmonic nanocomposites can be fine-tuned by engineering the composition of the nanocomposites.

  14. A Liquid-Liquid Thermoelectric Heat Exchanger as a Heat Pump for Testing Phase Change Material Heat Exchangers

    Science.gov (United States)

    Sheth, Rubik B.; Makinen, Janice; Le, Hung V.

    2016-01-01

    The primary objective of the Phase Change HX payload on the International Space Station (ISS) is to test and demonstrate the viability and performance of Phase Change Material Heat Exchangers (PCM HX). The system was required to pump a working fluid through a PCM HX to promote the phase change material to freeze and thaw as expected on Orion's Multipurpose Crew Vehicle. Due to limitations on ISS's Internal Thermal Control System, a heat pump was needed on the Phase Change HX payload to help with reducing the working fluid's temperature to below 0degC (32degF). This paper will review the design and development of a TEC based liquid-liquid heat exchanger as a way to vary to fluid temperature for the freeze and thaw phase of the PCM HX. Specifically, the paper will review the design of custom coldplates and sizing for the required heat removal of the HX.

  15. Natural convection heat transfer from a heated horizontal cylinder with Microencapsulated Phase-Change-Material slurries

    International Nuclear Information System (INIS)

    Kubo, Shinji; Akino, Norio; Tanaka, Amane; Nagashima, Akira

    1998-01-01

    The present study investigates natural convection heat transfer from a heated cylinder cooled by a water slurry of Microencapsulated Phase Change Material (MCPCM). A normal paraffin hydrocarbon with carbon number of 18 and melting point of 27.9degC, is microencapsulated by Melamine resin into particles of which average diameter is 9.5 μm and specific weight is same as water. The slurry of the MCPCM and water is put into a rectangular enclosure with a heated horizontal cylinder. The heat transfer coefficients of the cylinder were evaluated. Changing the concentrations of PCM and temperature difference between cylinder surface and working fluid. Addition of MCPCM into water, the heat transfer is enhanced significantly comparison with pure water in cases with phase change and is reduced slightly in cases without phase change. (author)

  16. Ductile fracture behaviour of primary heat transport piping material ...

    Indian Academy of Sciences (India)

    R. Narasimhan (Krishtel eMaging) 1461 1996 Oct 15 13:05:22

    Abstract. Design of primary heat transport (PHT) piping of pressurised heavy water reactors (PHWR) has to ensure implementation of leak-before-break con- cepts. In order to be able to do so, the ductile fracture characteristics of PHT piping material have to be quantified. In this paper, the fracture resistance of SA333, Grade.

  17. Thermophysical and heat transfer properties of phase change material candidate for waste heat transportation system

    Science.gov (United States)

    Kaizawa, Akihide; Maruoka, Nobuhiro; Kawai, Atsushi; Kamano, Hiroomi; Jozuka, Tetsuji; Senda, Takeshi; Akiyama, Tomohiro

    2008-05-01

    A waste heat transportation system trans-heat (TH) system is quite attractive that uses the latent heat of a phase change material (PCM). The purpose of this paper is to study the thermophysical properties of various sugars and sodium acetate trihydrate (SAT) as PCMs for a practical TH system and the heat transfer property between PCM selected and heat transfer oil, by using differential scanning calorimetry (DSC), thermogravimetry-differential thermal analysis (TG-DTA) and a heat storage tube. As a result, erythritol, with a large latent heat of 344 kJ/kg at melting point of 117°C, high decomposition point of 160°C and excellent chemical stability under repeated phase change cycles was found to be the best PCM among them for the practical TH system. In the heat release experiments between liquid erythritol and flowing cold oil, we observed foaming phenomena of encapsulated oil, in which oil droplet was coated by solidification of PCM.

  18. Effects of heat treatment on the radiosensitivity of Salmonellae

    International Nuclear Information System (INIS)

    Choi, E.H.; Yang, J.S.; Lee, S.R.

    1978-01-01

    When the food poisoning bacteria Salmonella enteritidis and S. typhimurium were treated with radiation (cobalt-60 γ-rays) and heat (10 minutes at 45 0 C or 50 0 C), their sterilizing effect was revealed differently depending on the order of treatments. Post-irradiation heating showed a synergistic effect whereas pre-irradiation heating revealed the opposite effect and the effects differed slightly with heating temperature. (author)

  19. Effect of Carbon Nanofiber Heat Treatment on Physical Properties of Polymeric Nanocomposites—Part I

    Directory of Open Access Journals (Sweden)

    Khalid Lafdi

    2007-01-01

    Full Text Available The definition of a nanocomposite material has broadened significantly to encompass a large variety of systems made of dissimilar components and mixed at the nanometer scale. The properties of nanocomposite materials also depend on the morphology, crystallinity, and interfacial characteristics of the individual constituents. In the current work, vapor-grown carbon nanofibers were subjected to varying heat-treatment temperatures. The strength of adhesion between the nanofiber and an epoxy (thermoset matrix was characterized by the flexural strength and modulus. Heat treatment to 1800C∘ demonstrated maximum improvement in mechanical properties over that of the neat resin, while heat-treatment to higher temperatures demonstrated a slight decrease in mechanical properties likely due to the elimination of potential bonding sites caused by the elimination of the truncated edges of the graphene layers. Both the electrical and thermal properties of the resulting nanocomposites increased in conjunction with the increasing heat-treatment temperature.

  20. Continued treatment and utilization of separable material

    Energy Technology Data Exchange (ETDEWEB)

    Neumann, W.; Englmann, E.; Goettle, A.; Hruschka, H.; Resch, H.; Schramm, W.; Wiedmann, U.; Flohrschuetz, R.

    1980-04-01

    The separable material (material retained on trash rack, material collected in the sand, floating substances, fresh sludge) occurring in a biological mechanical sewage treatment plant are described with respect to quantity, provenance, and composition. The most common methods for subsequent treatment of this material are at first aimed at the reduction of volume (dehydration), then at processing it to obtain reusable products (fertilizer, compost, feeding stuff, raw material) or at converting it into a mass that can be deposited. The individual steps of the process and their specific requirement, with respect to temperature, oxygen, and conditioning agents are described in detail.

  1. Development of Latent Heat Storage Phase Change Material Containing Plaster

    Directory of Open Access Journals (Sweden)

    Diana BAJARE

    2016-05-01

    Full Text Available This paper reviews the development of latent heat storage Phase Change Material (PCM containing plaster as in passive application. Due to the phase change, these materials can store higher amounts of thermal energy than traditional building materials and can be used to add thermal inertia to lightweight constructions. It was shown that the use of PCMs have advantages stabilizing the room temperature variations during summer days, provided sufficient night ventilation is allowed. Another advantage of PCM usage is stabilized indoor temperature on the heating season. The goal of this study is to develop cement and lime based plaster containing microencapsulated PCM. The plaster is expected to be used for passive indoor applications and enhance the thermal properties of building envelope. The plaster was investigated under Scanning Electron Microscope and the mechanical, physical and thermal properties of created plaster samples were determined.

  2. Phase Change Material Heat Sink for an ISS Flight Experiment

    Science.gov (United States)

    Quinn, Gregory; Stieber, Jesse; Sheth, Rubik; Ahlstrom, Thomas

    2015-01-01

    A flight experiment is being constructed to utilize the persistent microgravity environment of the International Space Station (ISS) to prove out operation of a microgravity compatible phase change material (PCM) heat sink. A PCM heat sink can help to reduce the overall mass and volume of future exploration spacecraft thermal control systems (TCS). The program is characterizing a new PCM heat sink that incorporates a novel phase management approach to prevent high pressures and structural deformation that often occur with PCM heat sinks undergoing cyclic operation in microgravity. The PCM unit was made using brazed aluminum construction with paraffin wax as the fusible material. It is designed to be installed into a propylene glycol and water cooling loop, with scaling consistent with the conceptual designs for the Orion Multipurpose Crew Vehicle. This paper reports on the construction of the PCM heat sink and on initial ground test results conducted at UTC Aerospace Systems prior to delivery to NASA. The prototype will be tested later on the ground and in orbit via a self-contained experiment package developed by NASA Johnson Space Center to operate in an ISS EXPRESS rack.

  3. Corrosion of materials for heat exchangers and the countermeasures

    International Nuclear Information System (INIS)

    Kawamoto, Teruaki

    1978-01-01

    When the materials for heat exchangers are selected, the heat transfer performance, mechanical strength, workability, cost, corrosion resistance and so on are taken in consideration. Most of the failure of heat exchangers is due to corrosion, and the corrosion failure on cooling water side occurs frequently, to which attention is not paid much usually. The rate of occurrence of corrosion failure is overwhelmingly high in heating tubes, and the failure owing to cooling water exceeds that owing to process fluid. The material of heating tubes is mostly aluminum brass, and local failure such as pitting corrosion or stress corrosion cracking holds a majority. The cause of corrosion failure due to cooling water is mostly the poor water quality. The mechanism of corrosion of metals can be explained by the electrochemical reaction between the metals and solutions. As for the factors affecting corrosion, dissolved oxygen, pH, Cl - ions, temperature, flow velocity, and foreign matters are enumerated. Copper alloys are sensitive to the effect of polluted sea water. Erosion corrosion is caused by eddies and bubbles owing to high flow velocity, and impingement attack is caused by scratching foreign matters. The quality of fresh water affects corrosion more than sea water in case of copper alloys. The preliminary examination of water quality is essential. (Kako, I.)

  4. Effects of heat treatment on the mechanical properties of kenaf fiber

    Energy Technology Data Exchange (ETDEWEB)

    Carada, Paulo Teodoro D. L. [Master’s student in the Graduate School of Science and Engineering, Mechanical Engineering, Doshisha University, 1-3 Tatara Miyakodani, Kyotanabe City, Kyoto Prefecture, 610-0394 (Japan); Fujii, Toru; Okubo, Kazuya [Professor in the Faculty of Science and Engineering, Department of Mechanical and Systems Engineering, Doshisha University, 1-3 Tatara Miyakodani, Kyotanabe City, Kyoto Prefecture, 610-0394 (Japan)

    2016-05-18

    Natural fibers are utilized in various ways. One specific application of it, is in the field natural fiber composite (NFC). Considerable amount of researches are conducted in this field due to rising concerns in the harmful effects of synthetic materials to the environment. Additionally, these researches are done in order to overcome the drawbacks which limit the wide use of natural fiber. A way to improve NFC is to look into the reinforcing component (natural fiber). Treatments, which are classified as mechanical or chemical in nature, can be done in order to improve the performance of the natural fiber. The aim of this study is to assess the effects of heat treatment in the mechanical properties of kenaf fiber. In addition, the response of mechanical properties after exposure to high moisture environment of heat-treated kenaf fibers was observed. Heat treatment was done for one hour with the following heating temperatures: 140, 160, 180, and 200 °C. X-ray diffraction analysis was done to calculate the crystallinity index of kenaf fibers after heat treatment. The results showed that increase in tensile strength can be attained when kenaf fibers are heat treated at 140 °C. However, the tensile modulus showed inconsistency with respect to heat treatment temperature. The computed crystallinity index of the fiber matched the tensile strength observed in non-treated and heat-treated kenaf fibers. The results obtained in this study can be used for applications where heat treatment on kenaf fibers is needed.

  5. Experimental Investigation of Ice Phase Change Material Heat Exchangers

    Science.gov (United States)

    Leimkuehler, Thomas O.; Stephan, Ryan A.

    2012-01-01

    Phase change materials (PCM) may be useful for spacecraft thermal control systems that involve cyclical heat loads or cyclical thermal environments. Thermal energy can be stored in the PCM during peak heat loads or in adverse thermal environments. The stored thermal energy can then be released later during minimum heat loads or in more favorable thermal environments. This can result in a decreased turndown ratio for the radiator and a reduced system mass. The use of water as a PCM rather than the more traditional paraffin wax has the potential for significant mass reduction since the latent heat of formation of water is approximately 70% greater than that of wax. One of the potential drawbacks of using ice as a PCM is its potential to rupture its container as water expands upon freezing. In order to develop a space qualified ice PCM heat exchanger, failure mechanisms must first be understood. Therefore, a methodical experimental investigation has been undertaken to demonstrate and document specific failure mechanisms due to ice expansion in the PCM. A number of ice PCM heat exchangers were fabricated and tested. Additionally, methods for controlling void location in order to reduce the risk of damage due to ice expansion were investigated. This paper presents an overview of the results of this investigation from the past three years.

  6. Subscale Water Based Phase Change Material Heat Exchanger Development

    Science.gov (United States)

    Sheth, Rubik; Hansen, Scott

    2016-01-01

    Supplemental heat rejection devices are required in many spacecraft as the radiators are not sized to meet the full heat rejection demand. One means of obtaining additional heat rejection is through the use of phase change material heat exchangers (PCM HX's). PCM HX's utilize phase change to store energy in unfavorable thermal environments (melting) and reject the energy in favorable environments (freezing). Traditionally, wax has been used as a PCM on spacecraft. However, water is an attractive alternative because it is capable of storing about 40% more energy per unit mass due to its higher latent heat of fusion. The significant problem in using water as a PCM is its expansion while freezing, leading to structural integrity concerns when housed in an enclosed heat exchanger volume. Significant investigation and development has taken place over the past five years to understand and overcome the problems associated with water PCM HX's. This paper reports on the final efforts by Johnson Space Center's Thermal Systems Branch to develop a water based PCM HX. The test article developed and reported on is a subscale version of the full-scale water-based PCM HX's constructed by Mezzo Technologies. The subscale unit was designed by applying prior research on freeze front propagation and previous full-scale water PCM HX development. Design modifications to the subscale unit included use of urethane bladder, decreased aspect ratio, perforated protection sheet, and use of additional mid-plates. Testing of the subscale unit was successful and 150 cycles were completed without fail.

  7. Materials, Turbomachinery and Heat Exchangers for Supercritical CO2 Systems

    Energy Technology Data Exchange (ETDEWEB)

    Anderson, Mark; Nellis, Greg; Corradini, Michael

    2012-10-19

    The objective of this project is to produce the necessary data to evaluate the performance of the supercritical carbon dioxide cycle. The activities include a study of materials compatibility of various alloys at high temperatures, the heat transfer and pressure drop in compact heat exchanger units, and turbomachinery issues, primarily leakage rates through dynamic seals. This experimental work will serve as a test bed for model development and design calculations, and will help define further tests necessary to develop high-efficiency power conversion cycles for use on a variety of reactor designs, including the sodium fast reactor (SFR) and very high-temperature gas reactor (VHTR). The research will be broken into three separate tasks. The first task deals with the analysis of materials related to the high-temperature S-CO{sub 2} Brayton cycle. The most taxing materials issues with regard to the cycle are associated with the high temperatures in the reactor side heat exchanger and in the high-temperature turbine. The system could experience pressures as high as 20MPa and temperatures as high as 650°C. The second task deals with optimization of the heat exchangers required by the S-CO{sub 2} cycle; the S-CO{sub 2} flow passages in these heat exchangers are required whether the cycle is coupled with a VHTR or an SFR. At least three heat exchangers will be required: the pre-cooler before compression, the recuperator, and the heat exchanger that interfaces with the reactor coolant. Each of these heat exchangers is unique and must be optimized separately. The most challenging heat exchanger is likely the pre-cooler, as there is only about a 40°C temperature change but it operates close to the CO{sub 2} critical point, therefore inducing substantial changes in properties. The proposed research will focus on this most challenging component. The third task examines seal leakage through various dynamic seal designs under the conditions expected in the S-CO{sub 2} cycle

  8. Regularities of texture formation in alloys undergoing phase transformations during heat treatment and plastic working

    International Nuclear Information System (INIS)

    Ageev, N.V.; Babarehko, A.A.

    1983-01-01

    Peculiarities of texture formation in metals undergoing phase transformations in the temperature range of heat treatment and hot working are investigated theoretically and experimentally. A low-temperature phase after hot working is shown to inherite a high-temperature phase texture due to definite orientation conformity during phase transformation. Strengthened heat and thermomechanical treatments, as a rule, do not destroy material texture but change it

  9. Effect of heat treatment on structure and magnetic properties

    Indian Academy of Sciences (India)

    Fe46Co35Ni19/CNTs nanocomposites have been prepared by an easy two-step route including adsorption and heat treatment processes. We investigated the effect of heat treatment conditions on structure, morphology, nanoparticle sizes and magnetic properties of the Fe46Co35Ni19 alloy nanoparticles attached on the ...

  10. 7 CFR 58.236 - Pasteurization and heat treatment.

    Science.gov (United States)

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Pasteurization and heat treatment. 58.236 Section 58... Service 1 Operations and Operating Procedures § 58.236 Pasteurization and heat treatment. All milk and... is handled according to sanitary conditions approved by the Administrator. (a) Pasteurization. (1...

  11. Effect of heat treatment temperature on binder thermal conductivities

    International Nuclear Information System (INIS)

    Wagner, P.

    1975-12-01

    The effect of heat treatment on the thermal conductivities of a pitch and a polyfurfuryl alcohol binder residue was investigated. Graphites specially prepared with these two binders were used for the experiments. Measured thermal conductivities were treated in terms of a two-component system, and the binder thermal conductivities were calculated. Both binder residues showed increased thermal conductivity with increased heat treatment temperature

  12. Investigation of anodic oxide coatings on zirconium after heat treatment

    International Nuclear Information System (INIS)

    Sowa, Maciej; Dercz, Grzegorz; Suchanek, Katarzyna; Simka, Wojciech

    2015-01-01

    Highlights: • Oxide layers prepared via PEO of zirconium were subjected to heat treatment. • Surface characteristics were determined for the obtained oxide coatings. • Heat treatment led to the partial destruction of the anodic oxide layer. • Pitting corrosion resistance of zirconium was improved after the modification. - Abstract: Herein, results of heat treatment of zirconium anodised under plasma electrolytic oxidation (PEO) conditions at 500–800 °C are presented. The obtained oxide films were investigated by means of SEM, XRD and Raman spectroscopy. The corrosion resistance of the zirconium specimens was evaluated in Ringer's solution. A bilayer oxide coatings generated in the course of PEO of zirconium were not observed after the heat treatment. The resulting oxide layers contained a new sublayer located at the metal/oxide interface is suggested to originate from the thermal oxidation of zirconium. The corrosion resistance of the anodised metal was improved after the heat treatment

  13. Advanced materials for alternative fuel capable directly fired heat engines

    Energy Technology Data Exchange (ETDEWEB)

    Fairbanks, J.W.; Stringer, J. (eds.)

    1979-12-01

    The first conference on advanced materials for alternative fuel capable directly fired heat engines was held at the Maine Maritime Academy, Castine, Maine. It was sponsored by the US Department of Energy, (Assistant Secretary for Fossil Energy) and the Electric Power Research Institute, (Division of Fossil Fuel and Advanced Systems). Forty-four papers from the proceedings have been entered into EDB and ERA and one also into EAPA; three had been entered previously from other sources. The papers are concerned with US DOE research programs in this area, coal gasification, coal liquefaction, gas turbines, fluidized-bed combustion and the materials used in these processes or equipments. The materials papers involve alloys, ceramics, coatings, cladding, etc., and the fabrication and materials listing of such materials and studies involving corrosion, erosion, deposition, etc. (LTN)

  14. Method and equipment to utilize solar heat. [paraffin used as heat storage material

    Energy Technology Data Exchange (ETDEWEB)

    Poellein, H

    1976-09-16

    In this process, solar radiation is converted into heat by means of absorbers. The heat transferred to a liquid is led in forced circulation, first into a heat storage device and then into a water heater. The cooled-down liquid is rercirculated. The storage material used here is paraffin. A measuring and control device is provided to switch from periods with solar radiation to periods where only stored energy is consumed. This device consists of a photocell measuring the incoming sunlight and a temperarure sensor. The control system is put into operation by a combination of the two measured values. The heat accumulator consists of several elements connected in parallel. A control device makes sure that only one accumulator element at a time is part of the circuit. The absorbers, as usual, consists of the absorber plate proper and a cover plate.

  15. Divertor heat flux control and plasma-material interaction

    International Nuclear Information System (INIS)

    Kikuchi, Yusuke; Nagata, Masayoshi; Sawada, Keiji; Takamura, Shuichi; Ueda, Yoshio

    2014-01-01

    Development of reliable radiative-cooling divertors is essential in DEMO reactor because it uses low-activation materials with low heat removal and the plasma heat flux exhausted from the confined region is 5 times as large as in ITER. It is important to predict precisely the heat and particle flux toward the divertor plate by simulation. In this present article, theoretical and experimental data of the reflection, secondary emission and surface recombination coefficients of the divertor plate by ion bombardment are given and their effects on the power transmission coefficient are discussed. In addition, some topics such as the erosion process of the divertor plate by ELM and the plasma disruption, the thermal shielding due to the vapor layer on the divertor plate and the formation of fuzz structure on W by helium plasma irradiation, are described. (author)

  16. Computational simulation of laser heat processing of materials

    Science.gov (United States)

    Shankar, Vijaya; Gnanamuthu, Daniel

    1987-04-01

    A computational model simulating the laser heat treatment of AISI 4140 steel plates with a CW CO2 laser beam has been developed on the basis of the three-dimensional, time-dependent heat equation (subject to the appropriate boundary conditions). The solution method is based on Newton iteration applied to a triple-approximate factorized form of the equation. The method is implicit and time-accurate; the maintenance of time-accuracy in the numerical formulation is noted to be critical for the simulation of finite length workpieces with a finite laser beam dwell time.

  17. Improved process for heating finely divided carbonaceous materials

    Energy Technology Data Exchange (ETDEWEB)

    1956-08-01

    A process for heating finely divided carbonaceous particles by burning a proportion of the carbon consists of passing the carbonaceous material at a temperature above 800/sup 0/F into an upwardly disposed, slender, combustion zone, suspending the particles in an upwardly-moving gas containing free oxygen so that the suspension has a density from 0.1 to 5.0 lb/cu. ft., passing the suspension upwardly through the combustion zone at a velocity of from 5 to 100 ft./sec., and injecting at least one stream of a second gas containing free oxygen at a point in the combustion zone such that at least 50% of the oxygen in the first gas has been consumed by the time the suspension reaches this point. The total quantity of oxygen is chosen so that the finely divided carbonaceous material is heated to a temperature of not less than 1,050/sup 0/F.

  18. Preliminary observations of heat treatment to control Phytophthora ramorum in infected wood species: an extended abstract

    Science.gov (United States)

    K.M. Tubajika; R. Singh; Shelly J.R.

    2008-01-01

    Identification of appropriate phytosanitary treatments that can be used for certifying solid wood packing material movement from areas infested or threatened by actionable plant pests and pathogens into uninfested areas is mportant. Heat treatment has been used on commodities to control fungal diseases and insect infestations for many years. The restricted use of...

  19. Do bark beetles and wood borers infest lumber following heat treatment? The role of bark

    Science.gov (United States)

    Robert A. Haack; Toby R. Petrice; Pascal Nzokou

    2007-01-01

    Wood packing material (WPM) is an important pathway for the movement of bark- and wood-infesting insects (Haack 2006). New international standards for treating WPM, often referred to as "ISPM 15," were adopted in 2002 (FAO 2002). The two approved WPM treatments are heat treatment (56? C core temperature for 30 min) and fumigation with methyl bromide. These...

  20. Continued Water-Based Phase Change Material Heat Exchanger Development

    Science.gov (United States)

    Hansen, Scott W.; Sheth, Rubik B.; Poynot, Joe; Giglio, Tony; Ungar, Gene K.

    2015-01-01

    In a cyclical heat load environment such as low Lunar orbit, a spacecraft's radiators are not sized to meet the full heat rejection demands. Traditionally, a supplemental heat rejection device (SHReD) such as an evaporator or sublimator is used to act as a "topper" to meet the additional heat rejection demands. Utilizing a Phase Change Material (PCM) heat exchanger (HX) as a SHReD provides an attractive alternative to evaporators and sublimators as PCM HX's do not use a consumable, thereby leading to reduced launch mass and volume requirements. In continued pursuit of water PCM HX development two full-scale, Orion sized water-based PCM HX's were constructed by Mezzo Technologies. These HX's were designed by applying prior research on freeze front propagation to a full-scale design. Design options considered included bladder restraint and clamping mechanisms, bladder manufacturing, tube patterns, fill/drain methods, manifold dimensions, weight optimization, and midplate designs. Two units, Units A and B, were constructed and differed only in their midplate design. Both units failed multiple times during testing. This report highlights learning outcomes from these tests and are applied to a final sub-scale PCM HX which is slated to be tested on the ISS in early 2017.

  1. Heat-Assisted Machining for Material Removal Improvement

    Science.gov (United States)

    Mohd Hadzley, A. B.; Hafiz, S. Muhammad; Azahar, W.; Izamshah, R.; Mohd Shahir, K.; Abu, A.

    2015-09-01

    Heat assisted machining (HAM) is a process where an intense heat source is used to locally soften the workpiece material before machined by high speed cutting tool. In this paper, an HAM machine is developed by modification of small CNC machine with the addition of special jig to hold the heat sources in front of the machine spindle. Preliminary experiment to evaluate the capability of HAM machine to produce groove formation for slotting process was conducted. A block AISI D2 tool steel with100mm (width) × 100mm (length) × 20mm (height) size has been cut by plasma heating with different setting of arc current, feed rate and air pressure. Their effect has been analyzed based on distance of cut (DOC).Experimental results demonstrated the most significant factor that contributed to the DOC is arc current, followed by the feed rate and air pressure. HAM improves the slotting process of AISI D2 by increasing distance of cut due to initial cutting groove that formed during thermal melting and pressurized air from the heat source.

  2. Continued Water-Based Phase Change Material Heat Exchanger Development

    Science.gov (United States)

    Hansen, Scott; Poynot, Joe

    2014-01-01

    In a cyclical heat load environment such as low Lunar orbit, a spacecraft's radiators are not sized to reject the full heat load requirement. Traditionally, a supplemental heat rejection device (SHReD) such as an evaporator or sublimator is used to act as a "topper" to meet the additional heat rejection demands. Utilizing a Phase Change Material (PCM) heat exchanger (HX) as a SHReD provides an attractive alternative to evaporators and sublimators as PCM HXs do not use a consumable, thereby leading to reduced launch mass and volume requirements. In continued pursuit of water PCM HX development two full-scale, Orion sized water-based PCM HX's were constructed by Mezzo Technologies. These HX's were designed by applying prior research and experimentation to the full scale design. Design options considered included bladder restraint and clamping mechanisms, bladder manufacturing, tube patterns, fill/drain methods, manifold dimensions, weight optimization, and midplate designs. Design and construction of these HX's led to successful testing of both PCM HX's.

  3. Synchronized fusion development considering physics, materials and heat transfer

    Science.gov (United States)

    Wong, C. P. C.; Liu, Y.; Duan, X. R.; Xu, M.; Li, Q.; Feng, K. M.; Zheng, G. Y.; Li, Z. X.; Wang, X. Y.; Li, B.; Zhang, G. S.

    2017-12-01

    Significant achievements have been made in the last 60 years in the development of fusion energy with the tokamak configuration. Based on the accumulated knowledge, the world is embarking on the construction and operation of ITER (International Thermonuclear Experimental Reactor) with a production of 500 MWf fusion power and the demonstration of physics Q  =  10. ITER will demonstrate D-T burn physics for a duration of a few hundred seconds to prepare for the next long-burn or steady state nuclear testing tokamak operating at much higher neutron fluence. With the evolution into a steady state nuclear device, such as the China Fusion Engineering Test Reactor (CFETR), it is necessary to examine the boundary conditions imposed by the combined development of tokamak physics, fusion materials and fusion technology for a reactor. The development of ferritic steel alloys as the structural material suitable for use at high neutron fluence leads to the use of helium as the most likely reactor coolant. This points to the fundamental technology limitation on the removal of chamber wall maximum heat flux at around 1 MW m-2 and an average heat flux of 0.1 MW m-2 for the next test reactor. Future reactor performance will then depend on the control of spatial and temporal edge heat flux peaking in order to increase the average heat flux to the chamber wall. With these severe material and technological limitations, system studies were used to scope out a few robust steady state synchronized fusion reactor (SFR) designs. As an example, a low fusion power design at 131.6 MWf, which can satisfy steady state design requirements, would have a major radius of 5.5 m and minor radius of 1.6 m. Such a design with even more advanced structural materials like W f/W composite could allow higher performance and provide a net electrical production of 62 MWe. These can be incorporated into the CFETR program.

  4. New Nomenclatures for Heat Treatments of Additively Manufactured Titanium Alloys

    Science.gov (United States)

    Baker, Andrew H.; Collins, Peter C.; Williams, James C.

    2017-07-01

    The heat-treatment designations and microstructure nomenclatures for many structural metallic alloys were established for traditional metals processing, such as casting, hot rolling or forging. These terms do not necessarily apply for additively manufactured (i.e., three-dimensionally printed or "3D printed") metallic structures. The heat-treatment terminology for titanium alloys generally implies the heat-treatment temperatures and their sequence relative to a thermomechanical processing step (e.g., forging, rolling). These designations include: β-processing, α + β-processing, β-annealing, duplex annealing and mill annealing. Owing to the absence of a thermomechanical processing step, these traditional designations can pose a problem when titanium alloys are first produced via additive manufacturing, and then heat-treated. This communication proposes new nomenclatures for heat treatments of additively manufactured titanium alloys, and uses the distinct microstructural features to provide a correlation between traditional nomenclature and the proposed nomenclature.

  5. Evaluation of nickel-based materials for VHTR heat exchanger

    International Nuclear Information System (INIS)

    Burlet, H.; Gentzbittel, J.M.; Cabet, C.; Lamagnere, P.; Blat, M.; Renaud, D.; Dubiez-Le Goff, S.; Pierron, D.

    2008-01-01

    Two available conventional nickel-based alloys (617 and 230) have been selected as structural materials for the advanced gas-cooled reactors, especially for the heat exchanger. An extensive research programme has been launched in France within the framework of the ANTARES programme to evaluate the performances of these materials in VHTR service environment. The experimental work is focused on mechanical properties, thermal stability and corrosion resistance in the temperature range (700-1 000 deg C) over long time. Thus the experimental work includes creep and fatigue tests on as-received materials, short- and medium-term thermal exposure tests followed by tensile and impact toughness tests, short- and medium-term corrosion exposure tests under impure He environment. The status of the results obtained up to now is given in this paper. Additional tests such as long-term thermal ageing and long-term corrosion tests are required to conclude on the selection of the material. (author)

  6. Process for forming thin film, heat treatment process of thin film sheet, and heat treatment apparatus therefor

    International Nuclear Information System (INIS)

    Watanabe, S.

    1984-01-01

    The invention provides a process for forming a magnetic thin film on a base film, a heat treatment process of a thin film sheet consisting of the base film and the magnetic thin film, and an apparatus for performing heat treatment of the thin film sheet. Tension applied to the thin film sheet is substantially equal to that applied to the base film when the magnetic thin film is formed thereon. Then, the thin film sheet is treated with heat. The thin film sheet is heated with a given temperature gradient to a reactive temperature at which heat shrinkage occurs, while the tension is being applied thereto. Thereafter, the thin film sheet to which the tension is still applied is cooled with substantially the same temperature gradient as applied in heating. The heat treatment apparatus has a film driving unit including a supply reel, a take-up reel, a drive source and guide rollers; a heating unit including heating plates, heater blocks and a temperature controller for heating the sheet to the reactive temperature; and a heat insulating unit including a thermostat and another temperature controller for maintaining the sheet at the nonreactive temperature which is slightly lower than the reactive temperature

  7. A Study of Ballast Water Treatment Using Engine Waste Heat

    Science.gov (United States)

    Balaji, Rajoo; Yaakob, Omar; Koh, Kho King; Adnan, Faizul Amri bin; Ismail, Nasrudin bin; Ahmad, Badruzzaman bin; Ismail, Mohd Arif bin

    2018-05-01

    Heat treatment of ballast water using engine waste heat can be an advantageous option complementing any proven technology. A treatment system was envisaged based on the ballast system of an existing, operational crude carrier. It was found that the available waste heat could raise the temperatures by 25 °C and voyage time requirements were found to be considerable between 7 and 12 days to heat the high volumes of ballast water. Further, a heat recovery of 14-33% of input energies from exhaust gases was recorded while using a test rig arrangement representing a shipboard arrangement. With laboratory level tests at temperature ranges of around 55-75 °C, almost complete species mortalities for representative phytoplankton, zooplankton and bacteria were observed while the time for exposure varied from 15 to 60 s. Based on the heat availability analyses for harvesting heat from the engine exhaust gases(vessel and test rig), heat exchanger designs were developed and optimized using Lagrangian method applying Bell-Delaware approaches. Heat exchanger designs were developed to suit test rig engines also. Based on these designs, heat exchanger and other equipment were procured and erected. The species' mortalities were tested in this mini-scale arrangement resembling the shipboard arrangement. The mortalities realized were > 95% with heat from jacket fresh water and exhaust gases alone. The viability of the system was thus validated.

  8. Treatment of contaminated waste plastics material

    International Nuclear Information System (INIS)

    Sims, J.; Hitchcock, J.W.

    1984-01-01

    Radioactive contaminated plastics material is treated by reducing it to uniform-sized debris and extruding it from a heated extruder into a sealed container in monolithic block form or as an in-fill matrix for other contaminated waste articles to create a substantially void-free sealed mass for disposal. Density adjusting fillers may be included. Extrusion may alternatively take place into a clean sealable plastics tube. (author)

  9. Effect of heat treatment on carbon steel pipe welds

    International Nuclear Information System (INIS)

    Mohamad Harun.

    1987-01-01

    The heat treatment to improve the altered properties of carbon steel pipe welds is described. Pipe critical components in oil, gasification and nuclear reactor plants require adequate room temperature toughness and high strength at both room and moderately elevated temperatures. Microstructure and microhardness across the welds were changed markedly by the welding process and heat treatment. The presentation of hardness fluctuation in the welds can produce premature failure. A number of heat treatments are suggested to improve the properties of the welds. (author) 8 figs., 5 refs

  10. Enhancing heat capacity of colloidal suspension using nanoscale encapsulated phase-change materials for heat transfer.

    Science.gov (United States)

    Hong, Yan; Ding, Shujiang; Wu, Wei; Hu, Jianjun; Voevodin, Andrey A; Gschwender, Lois; Snyder, Ed; Chow, Louis; Su, Ming

    2010-06-01

    This paper describes a new method to enhance the heat-transfer property of a single-phase liquid by adding encapsulated phase-change nanoparticles (nano-PCMs), which absorb thermal energy during solid-liquid phase changes. Silica-encapsulated indium nanoparticles and polymer-encapsulated paraffin (wax) nanoparticles have been made using colloid method, and suspended into poly-alpha-olefin (PAO) and water for potential high- and low-temperature applications, respectively. The shells prevent leakage and agglomeration of molten phase-change materials, and enhance the dielectric properties of indium nanoparticles. The heat-transfer coefficients of PAO containing indium nanoparticles (30% by mass) and water containing paraffin nanoparticles (10% by mass) are 1.6 and 1.75 times higher than those of corresponding single-phase fluids. The structural integrity of encapsulation allows repeated use of such nanoparticles for many cycles in high heat generating devices.

  11. Phase Change Energy Storage Material Suitable for Solar Heating System

    Science.gov (United States)

    Li, Xiaohui; Li, Haihua; Zhang, Lihui; Liu, Zhenfa

    2018-01-01

    Differential scanning calorimetry (DSC) was used to investigate the thermal properties of palmitic acid, myristic acid, laurel acid and the binary composite of palmitic/laurel acid and palmitic/myristic acid. The results showed that the phase transition temperatures of the three monomers were between 46.9-65.9°C, and the latent heats were above 190 J/g, which could be used as solar energy storage material. When the mass ratio of Palmitic acid and myristic was 1:1, the eutectic mixture could be formed. The latent heat of the eutectic mixture was 186.6 J/g, the melting temperature and the solidification temperature was 50.6°C and 43.8°C respectively. The latent heat of phase change and the melting temperature had not obvious variations after 400 thermal cycles, which proved that the binary composite had good thermal stability and was suitable for solar floor radiant heating system.

  12. Preparation of sewage treatment material PVFM

    Directory of Open Access Journals (Sweden)

    Wenling YANG

    2018-04-01

    Full Text Available In order to study the optimal operating condition of the sewage treatment material PVFM(polyvinyl formal, the mechanical blowing method and the chemical foaming method are adopted. Single-factor experiments and orthogonal experiments are conducted to study the factors including the amount of raw materials, reaction time and reaction temperature influencing the preparation of the material PVFM. The material is characterized by SEM. The properties of the material are explored through the contrastive experiments of sewage treatment. The results show that when PVA mass concentration is 9% (50 mL, cellulose content is 0.4 g, sulfuric acid content is 6 mL, formaldehyde content is 6 mL, SDS content is 0.4 g, carbonate calcium content is 0.8 g, reaction temperature is 30 ℃, the dripping time of sulfuric acid is 9 minutes, the dripping time of formaldehyde is 4 minutes, and the curing time is 8 hours, the material has good physical and chemical property, and the results of the contrastive experiments of sewage treatment show that PVFM has good removal effects on both COD and NH4+-N in simulated sewage. The sewage treatment material PVFM with good properties can be obtained by the mechanical blowing method and the chemical foaming method.

  13. Online Adaptive Hyperthermia Treatment Planning During Locoregional Heating to Suppress Treatment-Limiting Hot Spots

    NARCIS (Netherlands)

    Kok, H. Petra; Korshuize-van Straten, Linda; Bakker, Akke; de Kroon-Oldenhof, Rianne; Geijsen, Elisabeth D.; Stalpers, Lukas J. A.; Crezee, Johannes

    2017-01-01

    Adequate tumor temperatures during hyperthermia are essential for good clinical response, but excessive heating of normal tissue should be avoided. This makes locoregional heating using phased array systems technically challenging. Online application of hyperthermia treatment planning could help to

  14. Effect of heat treatment of wood on the morphology, surface roughness and penetration of simulated and human blood.

    Science.gov (United States)

    Rekola, J; Lassila, L V J; Nganga, S; Ylä-Soininmäki, A; Fleming, G J P; Grenman, R; Aho, A J; Vallittu, P K

    2014-01-01

    Wood has been used as a model material for the development of novel fiber-reinforced composite bone substitute biomaterials. In previous studies heat treatment of wood was perceived to significantly increase the osteoconductivity of implanted wood material. The objective of this study was to examine some of the changing attributes of wood materials that may contribute to improved biological responses gained with heat treatment. Untreated and 140°C and 200°C heat-treated downy birch (Betula pubescens Ehrh.) were used as the wood materials. Surface roughness and the effect of pre-measurement grinding were measured with contact and non-contact profilometry. Liquid interaction was assessed with a dipping test using two manufactured liquids (simulated blood) as well as human blood. SEM was used to visualize possible heat treatment-induced changes in the hierarchical structure of wood. The surface roughness was observed to significantly decrease with heat treatment. Grinding methods had more influence on the surface contour and roughness than heat treatment. The penetration of the human blood in the 200°C heat-treated exceeded that in the untreated and 140°C heat-treated materials. SEM showed no significant change due to heat treatment in the dry-state morphology of the wood. The results of the liquid penetration test support previous findings in literature concerning the effects of heat treatment on the biological response to implanted wood. Heat-treatment has only a marginal effect on the surface contour of wood. The highly specialized liquid conveyance system of wood may serve as a biomimetic model for the further development of tailored fiber-composite materials.

  15. Hazardous properties and environmental effects of materials used in solar heating and cooling (SHAC) technologies: interim handbook

    Energy Technology Data Exchange (ETDEWEB)

    Searcy, J.Q.

    1978-12-01

    General background informaion related to SHAC systems, how a particular material was chosen for this handbook, and codes and standards are given. Materials are categorized according to their functional use in SHAC systems as follows: (1) heat transfer fluids and fluid treatment chemicals, (2) insulation materials, (3) seals and sealant materials, (4) glazing materials, (5) collector materials, and (6) storage media. The informaion is presented under: general properties, chemical composition, thermal degradation products, and thermoxidative products of some commercial materials; toxic properties and other potential health effects; fire hazard properties; and environmental effects of and disposal methods for SHAC materials. (MHR)

  16. Strength of heat-resistant materials. Vynoslivost' zharoprochnykh materialov

    Energy Technology Data Exchange (ETDEWEB)

    Akimov, L M

    1977-01-01

    A presentation is made of the research results of the effect that metallurgical, technological, construction, and exploitation factors have on the durability of heat-resistant alloys, tested for mechanical, heat, and corrosion effects on metal in standard cylindrical and specially contoured samples under conventional conditions and conditional approaching operational ones. The causes of changes in fatigue strength of alloys are explained by the use of fractographic and metallographic analyses of fractures and structure. The book is intended for engineering--technical personnel at research institutes, and plant mechanical and metal studies laboratories in machine-building factories. The book may also be used by undergraduate and graduate students at institutions of higher learning specializing in the field of material studies and mechanical testing of steels and alloys. 176 references, 79 figures, 12 tables.

  17. Removal of corrosion products of construction materials in heat carrier

    International Nuclear Information System (INIS)

    1975-01-01

    A review of reported data has been made on the removal of structural material corrosion products into the heat-carrying agent of power reactors. The corrosion rate, and at the same time, removal of corrosion products into the heat-carrying agent (water) decreases with time. Thus, for example, the corrosion rate of carbon steel in boiling water at 250 deg C and O 2 concentration of 0.1 mg/1 after 3000 hr is 0.083 g/m 2 . day; after 9000 hr the corrosion rate has been reduced 2.5 times. Under static conditions the transfer rate of corrosion products into water has been smaller than in the stream and also depends on time. The corrosion rate of carbon steel under nuclear plant operating conditions is almost an order higher over that of steel Kh18N10T

  18. Transient refractory material dissolution by a volumetrically-heated melt

    Energy Technology Data Exchange (ETDEWEB)

    Seiler, Jean Marie, E-mail: jean-marie.seiler@cea.fr [CEA, DEN, DTN, 17 Rue des Martyrs, 38054 Grenoble Cedex 9 (France); Ratel, Gilles [CEA, DEN, DTN, 17 Rue des Martyrs, 38054 Grenoble Cedex 9 (France); Combeau, Hervé [Institut Jean Lamour, UMR 7198, Lorraine University, Ecole des Mines de Nancy, Parc de Saurupt, 54042 Nancy Cedex (France); Gaus-Liu, Xiaoyang; Kretzschmar, Frank; Miassoedov, Alexei [Karlsruhe Institut of Technology, Hermann-von-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen (Germany)

    2014-12-15

    Highlights: • We describe a test investigating ceramic dissolution by a molten non-eutectic melt. • The evolution of the interface temperature between melt and refractory is measured. • A theoretical model describing dissolution kinetics is proposed. • When dissolution stops, interface temperature is the liquidus temperature of the melt. - Abstract: The present work addresses the question of corium–ceramic interaction in a core catcher during a core-melt accident in a nuclear power plant. It provides an original insight into transient aspects concerning dissolution of refractory material by a volumetrically heated pool. An experiment with simulant material (LIVECERAM) is presented. Test results clearly show that dissolution of solid refractory material can occur in a non-eutectic melt at a temperature which is lower than the melting temperature of the refractory material. During the dissolution transient, the interface temperature rises above the liquidus temperature, corresponding to the instantaneous average composition of the melt pool. With constant power dissipation in the melt and external cooling of the core-catcher, a final steady-state situation is reached. Dissolution stops when the heat flux (delivered by the melt to the refractory) can be removed by conduction through the residual thickness of the ceramic, with T{sub interface} = T{sub liquidus} (calculated for the average composition of the final liquid pool). The final steady state corresponds to a uniform pool composition and uniform interface temperature distribution. Convection in the pool is governed by natural thermal convection and the heat flux distribution is therefore similar to what would be obtained for a single component pool. An interpretation of the experiment with two model-based approaches (0D and 1D) is presented. The mass transfer kinetics between the interface and the bulk is controlled by a diffusion sublayer within the boundary layer. During the dissolution transient

  19. Influence of Heat Treatments on Carotenoid Content of Cherry Tomatoes

    OpenAIRE

    D'Evoli, Laura; Lombardi-Boccia, Ginevra; Lucarini, Massimo

    2013-01-01

    Tomatoes and tomato products are rich sources of carotenoids—principally lycopene, followed by β-carotene and lutein. The aim of this work was to study the effect of heat treatment on carotenoid content in cherry tomatoes. Raw and canned products were sampled and analysed; furthermore whole, skin and pulp fractions of cherry tomatoes were analysed when raw and home-processed, in order to better understand heat treatment effects. Lycopene content in canned tomatoes was two-fold higher than in ...

  20. Heat-treated stainless steel felt as scalable anode material for bioelectrochemical systems.

    Science.gov (United States)

    Guo, Kun; Soeriyadi, Alexander H; Feng, Huajun; Prévoteau, Antonin; Patil, Sunil A; Gooding, J Justin; Rabaey, Korneel

    2015-11-01

    This work reports a simple and scalable method to convert stainless steel (SS) felt into an effective anode for bioelectrochemical systems (BESs) by means of heat treatment. X-ray photoelectron spectroscopy and cyclic voltammetry elucidated that the heat treatment generated an iron oxide rich layer on the SS felt surface. The iron oxide layer dramatically enhanced the electroactive biofilm formation on SS felt surface in BESs. Consequently, the sustained current densities achieved on the treated electrodes (1 cm(2)) were around 1.5±0.13 mA/cm(2), which was seven times higher than the untreated electrodes (0.22±0.04 mA/cm(2)). To test the scalability of this material, the heat-treated SS felt was scaled up to 150 cm(2) and similar current density (1.5 mA/cm(2)) was achieved on the larger electrode. The low cost, straightforwardness of the treatment, high conductivity and high bioelectrocatalytic performance make heat-treated SS felt a scalable anodic material for BESs. Copyright © 2015 Elsevier Ltd. All rights reserved.

  1. The algorithms for control of heating massive material

    Directory of Open Access Journals (Sweden)

    Karol Kostúr

    2008-03-01

    Full Text Available In numerous technological processes a change on the output follows change on the input pending specific time. This time is called dead time and if this time is too large, it causes problems in the control. This contribution is aimed at analyzing the algorithms of discreet regulation of the systems with dead time. Verified were classical PID regulator and a regulator using Dead Beat method. The control was also tried with Dead interval method. The regulators were tested by simulation and in the electrical laboratory furnace. The task was to control the temperature inside the material heated by furnace power.

  2. Heat transfer in Rockwool modelling and method of measurement. The effect of natural convection on heat transfer in fibrous materials

    Energy Technology Data Exchange (ETDEWEB)

    Dyrboel, Susanne

    1998-05-01

    Fibrous materials are some of the most widely used materials for thermal insulation. In this project the focus of interest has been on fibrous materials for building application. Interest in improving the thermal properties of insulation materials is increasing as legislation is being tightened to reduce the overall energy consumption. A knowledge of the individual heat transfer mechanisms - whereby heat is transferred within a particular material is an essential tool to improve continuously the thermal properties of the material. Heat is transferred in fibrous materials by four different transfer mechanisms: conduction through air, conduction through fibres, thermal radiation and convection. In a particular temperature range the conduction through air can be regarded as a constant, and conduction through fibres is an insignificant part of the total heat transfer. Radiation, however, constitutes 25-40% of the total heat transfer in light fibrous materials. In Denmark and a number of other countries convection in fibrous materials is considered as non-existent when calculating heat transmission as well as when designing building structures. Two heat transfer mechanisms have been the focus of the current project: radiation heat transfer and convection. The radiation analysis serves to develop a model that can be used in further work to gain a wider knowledge of the way in which the morphology of the fibrous material, i.e. fibre diameter distribution, fibre orientation distribution etc., influences the radiation heat transfer under different conditions. The convection investigation serves to examine whether considering convection as non-existent is a fair assumption to use in present and future building structures. The assumption applied in practically is that convection makes a notable difference only in very thick insulation, at external temperatures below -20 deg. C, and at very low densities. For large thickness dimensions the resulting heat transfer through the

  3. Final Report, Materials for Industrial Heat Recovery Systems, Tasks 3 and 4 Materials for Heat Recovery in Recovery Boilers

    Energy Technology Data Exchange (ETDEWEB)

    Keiser, James R.; Kish, Joseph R.; Singh, Preet M.; Sarma, Gorti B.; Yuan, Jerry; Gorog, J. Peter; Frederick, Laurie A.; Jette, Francois R.; Meisner, Roberta A.; Singbeil, Douglas L.

    2007-12-31

    The DOE-funded project on materials for industrial heat recovery systems included four research tasks: materials for aluminum melting furnace recuperator tubes, materials and operational changes to prevent cracking and corrosion of the co-extruded tubes that form primary air ports in black liquor recovery boilers, the cause of and means to prevent corrosion of carbon steel tubes in the mid-furnace area of recovery boilers, and materials and operational changes to prevent corrosion and cracking of recovery boiler superheater tubes. Results from studies on the latter two topics are given in this report while separate reports on results for the first two tasks have already been published. Accelerated, localized corrosion has been observed in the mid-furnace area of kraft recovery boilers. This corrosion of the carbon steel waterwall tubes is typically observed in the vicinity of the upper level of air ports where the stainless clad co-extruded wall tubes used in the lower portion of the boiler are welded to the carbon steel tubes that extend from this transition point or “cut line” to the top of the boiler. Corrosion patterns generally vary from one boiler to another depending on boiler design and operating parameters, but the corrosion is almost always found within a few meters of the cut line and often much closer than that. This localized corrosion results in tube wall thinning that can reach the level where the integrity of the tube is at risk. Collection and analysis of gas samples from various areas near the waterwall surface showed reducing and sulfidizing gases were present in the areas where corrosion was accelerated. However, collection of samples from the same areas at intervals over a two year period showed the gaseous environment in the mid-furnace section can cycle between oxidizing and reducing conditions. These fluctuations are thought to be due to gas flow instabilities and they result in an unstable or a less protective scale on the carbon steel

  4. Heat treatment of transparent Yb:YAG and YAG ceramics and its influence on laser performance

    Science.gov (United States)

    Fujioka, Kana; Mochida, Tetsuo; Fujimoto, Yasushi; Tokita, Shigeki; Kawanaka, Junji; Maruyama, Momoko; Sugiyama, Akira; Miyanaga, Noriaki

    2018-05-01

    Composite transparent ceramic materials are promising for improving the performance of high-average-power lasers. A combination of room-temperature bonding via surface treatment by a fast atom beam and diffusion bonding via heating, which effectively controls the ion diffusion distance near the interface, makes the laser materials suitable for a variety of oscillator/amplifier. During the heat treatment of yttrium aluminum garnet (YAG) ceramics, the Si ions in the solid solution of the sintering aid incorporated within the grains were seen to segregate at the grain boundary, resulting in an increase of scattering sites. The number density and size of the scattering sites strongly depended on the post-heating temperature rather than the heating time. Specifically, heating at 1300 °C did not affect the transmittance of the YAG ceramic, whereas both the size and number of scattering sites substantially increased with a heat treatment at 1400 °C. The laser oscillation experiment using cryogenically-cooled Yb:YAG ceramics exhibited heating temperature dependence of the slope efficiency owing to the increasing scattering loss.

  5. Influence of Heat Treatment on Abrasive Wear Resistance of Silumin Matrix Composite Castings

    Directory of Open Access Journals (Sweden)

    Gawdzińska K.

    2016-03-01

    Full Text Available The authors attempted at examining the effect of heat treatment on abrasive wear resistance of metal composite castings. Metal matrix composites were made by infiltrating preforms created from unordered short fibers (graphite or silumin with liquid aluminium alloy AlSi12(b. Thus prepared composites were subject to solution heat treatment at a temperature of 520°C for four hours, then aging at a temperature of 220°C for four hours. Abrasion resistance of the material was tested before and after thermal treatment.

  6. Heat treatment of cathodic arc deposited amorphous hard carbon films

    Energy Technology Data Exchange (ETDEWEB)

    Anders, S.; Ager, J.W. III; Brown, I.G. [and others

    1997-02-01

    Amorphous hard carbon films of varying sp{sup 2}/sp{sup 3} fractions have been deposited on Si using filtered cathodic are deposition with pulsed biasing. The films were heat treated in air up to 550 C. Raman investigation and nanoindentation were performed to study the modification of the films caused by the heat treatment. It was found that films containing a high sp{sup 3} fraction sustain their hardness for temperatures at least up to 400 C, their structure for temperatures up to 500 C, and show a low thickness loss during heat treatment. Films containing at low sp{sup 3} fraction graphitize during the heat treatment, show changes in structure and hardness, and a considerable thickness loss.

  7. Heat treatment of processing sludge of ornamental rocks: application as pozzolan in cement matrices

    Directory of Open Access Journals (Sweden)

    J.G. Uliana

    Full Text Available The sector of ornamental rocks produces significant volume of waste during the sawing of the blocks and demand to find ways to recycle, given its environmental impact. Considering the possibilities of use of industrial by-products as mineral admixtures, aiming at sustainable development in the construction industry, this paper aims to study the performance of the processing sludge of ornamental rocks and grinding after heat treatment, based on their potential application as partial substitute for cement. The residue was characterized, cast and milled to produce glassy material. Was analyzed the mechanical performance and pozzolanic activity with partial replacement of cement by waste in natural condition and after heat treatment in mortars for comparison. The results were promising, so it was possible to verify that after heat treatment, the treated waste is presented as a material with pozzolanic characteristics.

  8. Radioactive Dry Process Material Treatment Technology Development

    Energy Technology Data Exchange (ETDEWEB)

    Park, J. J.; Hung, I. H.; Kim, K. K. (and others)

    2007-06-15

    The project 'Radioactive Dry Process Material Treatment Technology Development' aims to be normal operation for the experiments at DUPIC fuel development facility (DFDF) and safe operation of the facility through the technology developments such as remote operation, maintenance and pair of the facility, treatment of various high level process wastes and trapping of volatile process gases. DUPIC Fuel Development Facility (DFDF) can accommodate highly active nuclear materials, and now it is for fabrication of the oxide fuel by dry process characterizing the proliferation resistance. During the second stage from march 2005 to February 2007, we carried out technology development of the remote maintenance and the DFDF's safe operation, development of treatment technology for process off-gas, and development of treatment technology for PWR cladding hull and the results was described in this report.

  9. Modeling of heat transfer within porous multi-constituent materials

    International Nuclear Information System (INIS)

    Niezgoda, M.

    2012-01-01

    The CEA works a great deal with porous materials - carbon composites, ceramics - and aims to optimize their properties for specific uses. These materials can be composed of several constituents and generally has a complex structure with pore size of several tens of micrometers. It is used in large-scale systems that are bigger than its own characteristic scale in which they are considered as equivalent to a homogeneous medium for the simulation of its behavior in its using environment without taking into account its local morphology. We are especially interested in the effective thermal diffusivity of heterogeneous materials that we estimate as a function of temperature with the help of an inverse method by considering they are homogeneous. The identification of the diffusivity of porous and/or semi-transparent materials is made difficult because of the strong conducto-radiative coupling can quickly occur when the temperature increases. We have thus modeled the coupled conductive and radiative heat transfer as a function of the temperature within porous multi-constituent materials from their morphology discretized into a set of homogeneous voxels. We have developed a methodology that consists in starting from a 3D-microstructure of the studied materials obtained by tomography. The microstructures constitute the numerical support to this modeling that renders it possible, on the one hand, to simulate any kind of numerical thermal experiments, especially the flash method whose the results render it possible to estimate the thermal diffusivity, and on the other hand, to reproduce the thermal behavior of our materials in their using conditions. (author) [fr

  10. Modelling of heat treatment of soy

    NARCIS (Netherlands)

    Hout, van den R.

    1997-01-01


    Soybeans are used as raw material for human nutrition and animal feed because of their high nutritional value. Consumption of raw beans has negative effects on the growth and health of human beings and animals. These effects are caused by antinutritional. factors (ANFs). Trypsin

  11. Multifunctional materials for bone cancer treatment

    Directory of Open Access Journals (Sweden)

    Marques C

    2014-05-01

    Full Text Available Catarina Marques,1 José MF Ferreira,1 Ecaterina Andronescu,2 Denisa Ficai,2 Maria Sonmez,3 Anton Ficai21Department of Materials and Ceramics Engineering, Centre for Research in Ceramics and Composite Materials, University of Aveiro, Aveiro, Portugal; 2Faculty of Applied Chemistry and Material Science, University Politehnica of Bucharest, Bucharest, Romania; 3National Research and Development Institute for Textiles and Leather, Bucharest, RomaniaAbstract: The purpose of this review is to present the most recent findings in bone tissue engineering. Special attention is given to multifunctional materials based on collagen and collagen–hydroxyapatite composites used for skin and bone cancer treatments. The multifunctionality of these materials was obtained by adding to the base regenerative grafts proper components, such as ferrites (magnetite being the most important representative, cytostatics (cisplatin, carboplatin, vincristine, methotrexate, paclitaxel, doxorubicin, silver nanoparticles, antibiotics (anthracyclines, geldanamycin, and/or analgesics (ibuprofen, fentanyl. The suitability of complex systems for the intended applications was systematically analyzed. The developmental possibilities of multifunctional materials with regenerative and curative roles (antitumoral as well as pain management in the field of skin and bone cancer treatment are discussed. It is worth mentioning that better materials are likely to be developed by combining conventional and unconventional experimental strategies.Keywords: bone graft, cancer, collagen, magnetite, cytostatics, silver

  12. Vibration damping and heat transfer using material phase changes

    Science.gov (United States)

    Kloucek, Petr (Inventor); Reynolds, Daniel R. (Inventor)

    2009-01-01

    A method and apparatus wherein phase changes in a material can dampen vibrational energy, dampen noise and facilitate heat transfer. One embodiment includes a method for damping vibrational energy in a body. The method comprises attaching a material to the body, wherein the material comprises a substrate, a shape memory alloy layer, and a plurality of temperature change elements. The method further comprises sensing vibrations in the body. In addition, the method comprises indicating to at least a portion of the temperature change elements to provide a temperature change in the shape memory alloy layer, wherein the temperature change is sufficient to provide a phase change in at least a portion of the shape memory alloy layer, and further wherein the phase change consumes a sufficient amount of kinetic energy to dampen at least a portion of the vibrational energy in the body. In other embodiments, the shape memory alloy layer is a thin film. Additional embodiments include a sensor connected to the material.

  13. Vibration damping and heat transfer using material phase changes

    Science.gov (United States)

    Kloucek, Petr [Houston, TX; Reynolds, Daniel R [Oakland, CA

    2009-03-24

    A method and apparatus wherein phase changes in a material can dampen vibrational energy, dampen noise and facilitate heat transfer. One embodiment includes a method for damping vibrational energy in a body. The method comprises attaching a material to the body, wherein the material comprises a substrate, a shape memory alloy layer, and a plurality of temperature change elements. The method further comprises sensing vibrations in the body. In addition, the method comprises indicating to at least a portion of the temperature change elements to provide a temperature change in the shape memory alloy layer, wherein the temperature change is sufficient to provide a phase change in at least a portion of the shape memory alloy layer, and further wherein the phase change consumes a sufficient amount of kinetic energy to dampen at least a portion of the vibrational energy in the body. In other embodiments, the shape memory alloy layer is a thin film. Additional embodiments include a sensor connected to the material.

  14. Sliding seal materials for low heat rejection engines

    Science.gov (United States)

    Beaty, Kevin; Lankford, James; Vinyard, Shannon

    1989-01-01

    Sliding friction coefficients and wear rates of promising piston seal materials were measured under temperature, environmental, velocity, and loading conditions that are representative of the low heat rejection (LHR) diesel engine environment. These materials included carbides, oxides, and nitrides. In addition, silicon nitride and partially stablized zirconia disks (cylinder liners) were ion-implanted with TiNi, Ni, Co, and Cr, and subsequently run against carbide pins (piston rings), with the objective of producing reduced friction via solid lubrication at elevated temperature. Friction and wear measurements were obtained using pin-on-disk laboratory experiments and a unique engine friction test rig. Unmodified ceramic sliding couples were characterized at all temperatures by friction coefficients of 0.24 and above during the pin-on-disk tests. The coefficient at 800 C in an oxidizing environment was reduced to below 0.1, for certain material combination, by the ion-implantation of TiNi or Co. This beneficial effect was found to derive from the lubricious Ti, Ni, and Co oxides. Similar results were demonstrated on the engine friction test rig at lower temperatures. The structural integrity and feasibility of engine application with the most promising material combination were demonstrated during a 30-hour single-cylinder, direct-injection diesel engine test.

  15. Effect of heat moisture treatment and annealing on physicochemical ...

    African Journals Online (AJOL)

    Red sorghum starch was physically modified by annealing and heat moisture treatment. The swelling power and solubility increased with increasing temperature range (60-90°), while annealing and heatmoisture treatment decreased swelling power and solubility of starch. Solubility and swelling were pH dependent with ...

  16. Influence of heat treatment on the microstructure and mechanical properties of Alloy 718 base metal and weldments

    International Nuclear Information System (INIS)

    Mills, W.J.

    1979-06-01

    Effect of heat treatment on the metallurgical structure and tensile properties of three heats of Alloy 718 base metal and an Alloy 718 GTA weldment were characterized. Heat treatments employed were the conventional (ASTM A637) precipitation treatment and a modified precipitation treatment designed to improve the toughness of the weldments. The GTA weldments were characterized in the as-welded condition. Light microscopy, thin foil, and surface replica electron microscopy revealed that the microstructure of this superalloy was sensitive to heat treatment and heat-to-heat variations. The modified aging treatment resulted in a larger grain size and a more homogeneous microstructure than the conventional treatments. The morphology of the primary strengthening γ phase was found to be finer and more closely spaced in the conventionally treated condition. Room and elevated temperature tensile testing revealed that the strength of the conventionally treated alloy was generally superior to that of the modified material. The conventional aging treatment resulted in greater heat-to-heat variations in tensile properties. This behavior was correlated with variations in the microstructure resulting from the precipitation heat treatments. The precipitate morphology of the GTA weldments was sensitive to heat treatment. The Laves phase was present in the interdendritic regions of both heat-treated welds. The modified aging treatment reduced the amount of Laves phase present in the weld zone. Room and elevated temperature tensile properties of the precipitation hardened weldments were relatively insensitive to heat treatment, suggesting that reduction in Laves phase from the weld zone had essentially no effect on tensile properties. As-welded GTA weldments exhibited lower strength levels and higher ductility values than heat-treated welds

  17. Effect of heat treatment on strength and abrasive wear behaviour of ...

    Indian Academy of Sciences (India)

    Administrator

    Aluminum 6061 has been used as matrix material owing to its ... Mechanical properties such as microhardness, tensile strength, and abrasive wear tests have been ... heat treatment conditions, adopted Al6061–SiCp composites exhibited better microhardness and tensile ... corrosion resistance (Ramesh et al 2005).

  18. Heat treatment temperature influence on ASTM A890 GR 6A super duplex stainless steel microstructure

    International Nuclear Information System (INIS)

    Martins, Marcelo; Casteletti, Luiz Carlos

    2005-01-01

    Duplex and super duplex stainless steels are ferrous alloys with up to 26% chromium, 8% nickel, 5% molybdenum and 0.3% nitrogen, which are largely used in applications in media containing ions from the halogen family, mainly the chloride ion (Cl - ). The emergence of this material aimed at substituting Copper-Nickel alloys (Cupro-Nickel) that despite presenting good corrosion resistance, has mechanical properties quite inferior to steel properties. The metallurgy of duplex and super duplex stainless steel is complex due to high sensitiveness to sigma phase precipitation that becomes apparent, due to the temperatures they are exposed on cooling from solidification as well as from heat treatment processes. The objective of this study was to verify the influence of heat treating temperatures on the microstructure and hardness of ASTM A890/A890M Gr 6A super duplex stainless steel type. Microstructure control is of extreme importance for castings, as the chemical composition and cooling during solidification inevitably provide conditions for precipitation of sigma phase. Higher hardness in these materials is directly associated to high sigma phase concentration in the microstructure, precipitated in the ferrite/austenite interface. While heat treatment temperature during solution treatment increases, the sigma phase content in the microstructure decreases and consequently, the material hardness diminishes. When the sigma phase was completely dissolved by the heat treatment, the material hardness was influenced only due to ferrite and austenite contents in the microstructure

  19. Radiation treatment for sterilization of packaging materials

    International Nuclear Information System (INIS)

    Haji-Saeid, Mohammad; Sampa, Maria Helena O.; Chmielewski, Andrzej G.

    2007-01-01

    Treatment with gamma and electron radiation is becoming a common process for the sterilization of packages, mostly made of natural or synthetic plastics, used in the aseptic processing of foods and pharmaceuticals. The effect of irradiation on these materials is crucial for packaging engineering to understand the effects of these new treatments. Packaging material may be irradiated either prior to or after filling. The irradiation prior to filling is usually chosen for dairy products, processed food, beverages, pharmaceutical, and medical device industries in the United States, Europe, and Canada. Radiation effects on packaging material properties still need further investigation. This paper summarizes the work done by different groups and discusses recent developments in regulations and testing procedures in the field of packaging technology

  20. Seeking alternatives to probit 9 when developing treatments for wood packaging materials under ISPM No. 15

    Science.gov (United States)

    R.A. Haack; A. Uzunovic; K. Hoover; J.A. Cook

    2011-01-01

    ISPM No. 15 presents guidelines for treating wood packaging material used in international trade. There are currently two approved phytosanitary treatments: heat treatment and methyl bromide fumigation. New treatments are under development, and are needed given that methyl bromide is being phased out. Probit 9 efficacy (100% mortality of at least 93 613 test organisms...

  1. Effect of heat treatment operations on the Rm tensile strength of silumins

    Directory of Open Access Journals (Sweden)

    J. Pezda

    2010-10-01

    Full Text Available Owing to good technological properties, low weight and good corrosion resistance, aluminum-silicon alloys are widely used as a material for cast machinery components. State of macro- and microstructure of a castings manufactured from Al-Si alloys, which is determined by a shape and distribution of hardening phases, segregation of alloying constituents and impurities, as well as distribution of porosity, create conditions to obtainment of proper mechanical properties. These properties can be improved through modification of the alloy and performed heat treatment operations. The paper presents effect of modification and heat treatment process on the Rm tensile strength of a selected silumins (EN AB-AlSi9Cu3(Fe, EN AB-AlSi12CuNiMg, EN AB-AlSi17Cu1Ni1Mg. Investigated alloys were put to treatments of refining and modification, and next to heat treatment. Temperature range of the heat treatment operations was determined on base of curves from the ATD method. Obtained results illustrate registered curves of melting and solidification from the ATD method and strength tests. On base of performed initial tests one determined parameters of the heat treatment process (temperature and duration of solutionig and ageing treatments enabling obtainment of improved Rm tensile strength of the investigated alloys.

  2. A previously undescribed organic residue sheds light on heat treatment in the Middle Stone Age.

    Science.gov (United States)

    Schmidt, Patrick; Porraz, Guillaume; Bellot-Gurlet, Ludovic; February, Edmund; Ligouis, Bertrand; Paris, Céline; Texier, Pierre-Jean; Parkington, John E; Miller, Christopher E; Nickel, Klaus G; Conard, Nicholas J

    2015-08-01

    South Africa has in recent years gained increasing importance for our understanding of the evolution of 'modern human behaviour' during the Middle Stone Age (MSA). A key element in the suite of behaviours linked with modern humans is heat treatment of materials such as ochre for ritual purposes and stone prior to tool production. Until now, there has been no direct archaeological evidence for the exact procedure used in the heat treatment of silcrete. Through the analysis of heat-treated artefacts from the Howiesons Poort of Diepkloof Rock Shelter, we identified a hitherto unknown type of organic residue - a tempering-residue - that sheds light on the processes used for heat treatment in the MSA. This black film on the silcrete surface is an organic tar that contains microscopic fragments of charcoal and formed as a residue during the direct contact of the artefacts with hot embers of green wood. Our results suggest that heat treatment of silcrete was conducted directly using an open fire, similar to those likely used for cooking. These findings add to the discussion about the complexity of MSA behaviour and appear to contradict previous studies that had suggested that heat treatment of silcrete was a complex (i.e., requiring a large number of steps for its realization) and resource-consuming procedure. Copyright © 2015 Elsevier Ltd. All rights reserved.

  3. Effect of alkali and heat treatments for bioactivity of TiO{sub 2} nanotubes

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Seo young, E-mail: mast6269@nate.com [Dept. of Dental Biomaterials and Institute of Bio degradable material, Institute of Oral Bioscience and BK21 plus project, School of Dentistry, Chonbuk National University, Jeonju, 561-756 (Korea, Republic of); Kim, Yu kyoung, E-mail: yk0830@naver.com [Dept. of Dental Biomaterials and Institute of Bio degradable material, Institute of Oral Bioscience and BK21 plus project, School of Dentistry, Chonbuk National University, Jeonju, 561-756 (Korea, Republic of); Park, Il song, E-mail: ilsong@jbnu.ac.kr [Division of Advanced Materials Engineering, Research Center for Advanced Materials Development and Institute of Biodegradable Materials, Chonbuk National University, Jeonju 561-756 (Korea, Republic of); Jin, Guang chun, E-mail: jingc88@126.com [Oral Medical College, Beihua University, Jilin City 132013 (China); Bae, Tae sung, E-mail: bts@jbnu.ac.kr [Dept. of Dental Biomaterials and Institute of Bio degradable material, Institute of Oral Bioscience and BK21 plus project, School of Dentistry, Chonbuk National University, Jeonju, 561-756 (Korea, Republic of); Lee, Min ho, E-mail: mh@jbnu.ac.kr [Dept. of Dental Biomaterials and Institute of Bio degradable material, Institute of Oral Bioscience and BK21 plus project, School of Dentistry, Chonbuk National University, Jeonju, 561-756 (Korea, Republic of)

    2014-12-01

    Highlights: • TiO{sub 2} nanotubes formed via anodization were treated by alkali and heat. • The surface roughness was increased after alkali treatment (p < 0.05). • After alkali and heat treatment, the wettability was better than before treatment. • Alkali treated TiO{sub 2} nanotubes were shown higher HAp formation in SBF. • Heat treatment affected on the attachment of cells for alkali treated nanotubes. - Abstract: In this study, for improving the bioactivity of titanium used as an implant material, alkali and heat treatments were carried out after formation of the nanotubes via anodization. Nanotubes with uniform length, diameter, and thickness were formed by anodization. The alkali and heat-treated TiO{sub 2} nanotubes were covered with the complex network structure, and the Na compound was generated on the surface of the specimens. In addition, after 5 and 10 days of immersion in the SBF, the crystallized OCP and HAp phase was significantly increased on the surface of the alkali-treated TiO{sub 2} nanotubes (PNA) and alkali and heat-treated TiO{sub 2} nanotubes (PNAH) groups. Cell proliferation was decreased due to the formation of amorphous sodium titanate (Na{sub 2}TiO{sub 3}) layer on the surface of the PNA group. However, anatase and crystalline sodium titanate were formed on the surface of the PNAH group after heat treatment at 550 °C, and cell proliferation was improved. Thus, PNA group had higher HAp forming ability in the simulated body fluid. Additional heat treatment affected on enhancement of the bioactivity and the attachment of osteoblasts for PNA group.

  4. Heat transfer between relocated materials and the RPV lower head

    Energy Technology Data Exchange (ETDEWEB)

    Rempe, J.L.; Knudson, D.L. [Idaho National Engineering and Environmental Lab., Idaho Falls, ID (United States); Kohriyama, T. [INSS, Fukui (Japan)

    2001-07-01

    Questions about the coolability of a continuous mass of relocated corium were raised during the Three Mile Island Unit 2 (TMI-2) Vessel Investigation Project (VIP) Post-accident examinations indicate that nearly half of the material that relocated to the vessel lower head during the TMI-2 accident formed a cohesive or ''continuous'' layer. TMI-2 VIP results and other evidence suggest that conduction through this continuous layer of solidified corium materials was assisted by other cooling mechanisms. Because increased knowledge about in-vessel coolability of corium materials may assist reactor designers in demonstrating that their concepts are passively safe, there is international interest in this topic. However, data are needed to identify what cooling mechanism(s) occurred and to develop a validated model for predicting this cooling. Corium cooling models significantly impact predictions for subsequent accident progression, such as the estimated time and mode of vessel failure. Hence, improved cooling models will provide a much needed, missing component of severe accident analyses. This paper provides a critical review of research investigating the coolability of corium relocating to a water-filled lower head. Where possible, existing models and data for predicting cooling are quantitatively compared; and governing relationships are identified. Key phenomena that should be incorporated into models for predicting this heat transfer are discussed, and deficiencies in current models and available data for predicting cooling are noted. Recommendations for improving these models and for obtaining data to validate these models are also provided. (author)

  5. Heat transfer between relocated materials and the RPV lower head

    International Nuclear Information System (INIS)

    Rempe, J.L.; Knudson, D.L.; Kohriyama, T.

    2001-01-01

    Questions about the coolability of a continuous mass of relocated corium were raised during the Three Mile Island Unit 2 (TMI-2) Vessel Investigation Project (VIP) Post-accident examinations indicate that nearly half of the material that relocated to the vessel lower head during the TMI-2 accident formed a cohesive or ''continuous'' layer. TMI-2 VIP results and other evidence suggest that conduction through this continuous layer of solidified corium materials was assisted by other cooling mechanisms. Because increased knowledge about in-vessel coolability of corium materials may assist reactor designers in demonstrating that their concepts are passively safe, there is international interest in this topic. However, data are needed to identify what cooling mechanism(s) occurred and to develop a validated model for predicting this cooling. Corium cooling models significantly impact predictions for subsequent accident progression, such as the estimated time and mode of vessel failure. Hence, improved cooling models will provide a much needed, missing component of severe accident analyses. This paper provides a critical review of research investigating the coolability of corium relocating to a water-filled lower head. Where possible, existing models and data for predicting cooling are quantitatively compared; and governing relationships are identified. Key phenomena that should be incorporated into models for predicting this heat transfer are discussed, and deficiencies in current models and available data for predicting cooling are noted. Recommendations for improving these models and for obtaining data to validate these models are also provided. (author)

  6. Electron spin resonance and its application to heat treated carbonaceous materials

    International Nuclear Information System (INIS)

    Emmerich, Francisco Guilherme

    1993-01-01

    This work presents the basic characteristics of the electron spin resonance technique, also called paramagnetic resonance, being discussed its application to heat treated carbonaceous materials. In the low heat treatment temperature (HTT) range (below 700 deg C) the organic free radical are the predominant unpaired spin center, which play a key role in the process of carbonization and meso phase formation. At higher temperatures, it is possible to make correlations between the low H T T range and the high HTT range (above 130 deg C), where the predominant unpaired spin center are the free charge carriers (free electrons) of the graphite like crystallites of the material, which are formed by the carbonization process. (author)

  7. Influence of the chemical composition, heat and surface treatment in the biofouling of austenitic stainless steels

    International Nuclear Information System (INIS)

    Sarro, M. I.; Aleman, O.; Moreno, D. A.; Roso, M.; Ranninger, C.

    2004-01-01

    The main objective of this study was to analyse the biofouling processes in the kinds of stainless steels used normally in industry (UNS S30400, UNS S30403 and UNS S31600), with different surface treatments after grinding and polishing. The study was developed using two microscopy techniques. Scanning Electron Microscopy (SEM was used to evaluate the microorganisms distribution in the materials, and Epi fluorescence Microscopy was used to evaluate the viability of cells in the biofilm. The results revealed the influence of the material, heat treatment, surface treatment and roughness in the biofouling processes in the stainless steel assays. (Author) 33 refs

  8. Fast numerical upscaling of heat equation for fibrous materials

    KAUST Repository

    Iliev, Oleg; Lazarov, Raytcho; Willems, Joerg

    2010-01-01

    We are interested in numerical methods for computing the effective heat conductivities of fibrous insulation materials, such as glass or mineral wool, characterized by low solid volume fractions and high contrasts, i.e., high ratios between the thermal conductivities of the fibers and the surrounding air. We consider a fast numerical method for solving some auxiliary cell problems appearing in this upscaling procedure. The auxiliary problems are boundary value problems of the steady-state heat equation in a representative elementary volume occupied by fibers and air. We make a simplification by replacing these problems with appropriate boundary value problems in the domain occupied by the fibers only. Finally, the obtained problems are further simplified by taking advantage of the slender shape of the fibers and assuming that they form a network. A discretization on the graph defined by the fibers is presented and error estimates are provided. The resulting algorithm is discussed and the accuracy and the performance of the method are illusrated on a number of numerical experiments. © Springer-Verlag 2010.

  9. Promising materials for HTGR high temperature heat exchangers

    International Nuclear Information System (INIS)

    Kuznetsov, E.V.; Tokareva, T.B.; Ryabchenkov, A.V.; Novichkova, O.V.; Starostin, Yu.D.

    1989-01-01

    The service conditions for high-temperature heat-exchangers with helium coolant of HTGRs and requirements imposed on materials for their production are discussed. The choice of nickel-base alloys with solid-solution hardening for long-term service at high temperatures is grounded. Results of study on properties and structure of types Ni-25Cr-5W-5Mo and Ni-20Cr-20W alloy in the temperature range of 900 deg. - 1,000 deg. C are given. The ageing of Ni-25Cr-5W-5Mo alloy at 900 deg. - 950 deg. C results in decreased corrosion-mechanical properties and is caused by the change of structural metal stability. Alloy with 20% tungsten retains a high stability of both structure and properties after prolonged exposure in helium at above temperatures. The alloy has also increased resistance to delayed fracture and low-cycle fatigue at high temperatures. The developed alloy of type Ni-20Cr-20W with microalloying is recommended for production of tubes for HTGR high-temperature heat-exchangers with helium coolant. (author). 3 refs, 8 figs

  10. Fast numerical upscaling of heat equation for fibrous materials

    KAUST Repository

    Iliev, Oleg

    2010-08-01

    We are interested in numerical methods for computing the effective heat conductivities of fibrous insulation materials, such as glass or mineral wool, characterized by low solid volume fractions and high contrasts, i.e., high ratios between the thermal conductivities of the fibers and the surrounding air. We consider a fast numerical method for solving some auxiliary cell problems appearing in this upscaling procedure. The auxiliary problems are boundary value problems of the steady-state heat equation in a representative elementary volume occupied by fibers and air. We make a simplification by replacing these problems with appropriate boundary value problems in the domain occupied by the fibers only. Finally, the obtained problems are further simplified by taking advantage of the slender shape of the fibers and assuming that they form a network. A discretization on the graph defined by the fibers is presented and error estimates are provided. The resulting algorithm is discussed and the accuracy and the performance of the method are illusrated on a number of numerical experiments. © Springer-Verlag 2010.

  11. Photothermal heating in metal-embedded microtools for material transport

    DEFF Research Database (Denmark)

    Villangca, Mark Jayson; Palima, Darwin; Banas, Andrew Rafael

    2016-01-01

    Material transport is an important mechanism in microfluidics and drug delivery. The methods and solutions found in literature involve passively diffusing structures, microneedles and chemically fueled structures. In this work, we make use of optically actuated microtools with embedded metal layer...... as heating element for controlled loading and release. The new microtools take advantage of the photothermal-induced convection current to load and unload cargo. We also discuss some challenges encountered in realizing a self-contained polymerized microtool. Microfluidic mixing, fluid flow control...... and convection currents have been demonstrated both experimentally and numerically for static metal thin films or passively floating nanoparticles. Here we show an integration of aforementioned functionalities in an opticallyfabricated and actuated microtool. As proof of concept, we demonstrate loading...

  12. Application of newly developed heat resistant materials for USC boilers

    International Nuclear Information System (INIS)

    Sato, T.; Tamura, K.; Fukuda, Y.; Matsuda, J.

    2004-01-01

    This paper describes the research on the development and improvement of new high strength heat resistant steels such as SUPER304H (18Cr-9Ni-3Cu-Nb-N), NF709 (20Cr-25Ni-1.5Mo-Nb-Ti-N) and HR3C (25Cr-20Ni-Nb-N) as boiler tube, and NF616 (9Cr-0.5Mo-1.8W-Nb-V) and HCM12A (11Cr-0.4Mo-2W-Nb-V-Cu) as thick section pipe. The latest manufacturing techniques applied for these steels are introduced. In addition the high temperature strength of Alloy617 (52Ni-22Cr-13Co-9Mo-Ti-Al) that is one of the candidate materials for the next generation 700 □ USC boilers is described. (orig.)

  13. A Method to Make Classification of the Heat Treatment Processes Performed on Bronze Using Incomplete Knowledge

    Directory of Open Access Journals (Sweden)

    Kluska-Nawarecka S.

    2014-06-01

    Full Text Available The article describes the problem of selection of heat treatment parameters to obtain the required mechanical properties in heat- treated bronzes. A methodology for the construction of a classification model based on rough set theory is presented. A model of this type allows the construction of inference rules also in the case when our knowledge of the existing phenomena is incomplete, and this is situation commonly encountered when new materials enter the market. In the case of new test materials, such as the grade of bronze described in this article, we still lack full knowledge and the choice of heat treatment parameters is based on a fragmentary knowledge resulting from experimental studies. The measurement results can be useful in building of a model, this model, however, cannot be deterministic, but can only approximate the stochastic nature of phenomena. The use of rough set theory allows for efficient inference also in areas that are not yet fully explored.

  14. Irradiation in combination of heat treatment of mango puree

    International Nuclear Information System (INIS)

    Noomhorm, A.; Apintanapong, M.

    1996-01-01

    The effect of irradiation with heat combination treatment on the shelf life and quality of mango puree was studied. Thermal inactivation of polyphenol oxidase enzyme at 80 degree C and 15 min. was used as a measure of adequacy of pre-heat treatment. Irradiation of mango puree after heat treatment at dosage of 0, 2, 4, 6 and 8 kGy showed no change in mc, pH, acidity, and TSS but during storage, growth of microorganisms brought changes in these values. Irradiation in combination with low temperature (5 degree C) reduced discoloration and darkening rate during storage. Irradiation dose from 0 to 8 kGy resulted in log linear reductions in microorganism levels but at 6 and 8 kGy, there was no growth of microorganisms. Products irradiated at 8 kGy showed no microorganism growth at both temperatures

  15. A heat mathematical model of polymer composite cylinder during microwave treatment

    Directory of Open Access Journals (Sweden)

    S. V. Reznik

    2014-01-01

    Full Text Available Traditional technologies of producing epoxy based polymer composite materials (PCM require a long-term and energy consuming thermal processing. Microwave heating could be used as an alternative technology for heating work pieces made of PCM; this would allow to reduce treatment time and energy consumption significantly. A mathematical model of temperature distribution inside a cylindrical composite system during microwave treatment was investigated in this paper. The model includes a hollow PCM cylinder made of an epoxy binder and carbon fibers and a solid cylindrical mandrel. Theoretical and experimental results on the temperature state of the system were analyzed and discussed.

  16. PECULIARITIES OF GENERALIZATION OF SIMILAR PHENOMENA IN THE PROCESS OF FISH HEAT TREATMENT

    Directory of Open Access Journals (Sweden)

    V. A. Pokhol’chenko

    2015-01-01

    Full Text Available The theoretical presuppositions for the possibility of generalizing and similarity founding in dehydration and wet materials heating processes are studieded in this article. It is offered to carry out the given processes generalization by using dimensionless numbers of similarity. At the detailed analyzing of regularities of heat treatment processes of fish in different modes a significant amount of experienced material was successfully generalized on the basis of dimensionless simplex (similarity numbers. Using the dimensionless simplex allowed to detect a number of simple mathematical models for the studied phenomena. The generalized kinetic models of fish dehydration, the generalized dynamic models (changing moisture diffusion coefficients, the generalized kinetic models of fish heating (the temperature field changing in the products thickness, average volume and center were founded. These generalized mathematical models showed also relationship of dehydration and heating at the processes of fish semi-hot, hot smoking (drying and frying. The relationship of the results from the physical nature of the dehydration process, including a change in the binding energy of the moisture with the material to the extent of the process and the shrinkage impact on the rate of the product moisture removal is given in the article. The factors influencing the internal structure and properties of the raw material changing and retarding the dehydration processes are described there. There was a heating rate dependence of fish products on the chemical composition the geometric dimensions of the object of heating and on the coolant regime parameters. A unique opportunity is opened by using the generalized models, combined with empirically derived equations and the technique of engineering calculation of these processes, to design a rational modes of heat treatment of raw materials and to optimize the performance of thermal equipment.

  17. Study on Spheroidization and Related Heat Treatments of Medium Carbon Alloy Steels

    Directory of Open Access Journals (Sweden)

    Harisha S. R.

    2018-01-01

    Full Text Available The importance of medium carbon steels as engineering materials is reflected by the fact that out of the vast majority of engineering grade ferrous alloys available and used in the market today, a large proportion of them are from the family of medium carbon steels. Typically medium carbon steels have a carbon range of 0.25 to 0.65% by weight, and a manganese content ranging from 0.060 to 1.65% by weight. Medium carbon steels are more resistive to cutting, welding and forming as compared to low carbon steels. From the last two decades a number of research scholars reported the use of verity of heat treatments to tailor the properties of medium carbon steels. Spheroidizing is the novel industrial heat treatment employed to improve formability and machinability of medium/high carbon low alloy steels. This exclusive study covers procedure, the effects and possible outcomes of various heat treatments on medium carbon steels. In the present work, other related heat treatments like annealing and special treatments for property alterations which serve as pretreatments for spheroidizing are also reviewed. Medium carbon steels with property alterations by various heat treatment processes are finding increased responsiveness in transportation, aerospace, space, underwater along with other variegated fields. Improved tribological and mechanical properties consisting of impact resistance, stiffness, abrasion and strength are the main reasons for the increased attention of these steels in various industries. In the present scenario for the consolidation of important aspects of various heat treatments and effects on mechanical properties of medium carbons steel, a review of different research papers has been attempted. This review may be used as a guide to provide practical data for heat treatment industry, especially as a tool to enhance workability and tool life.

  18. Heat treatment of TI-6AL-4V produced by lasercusing

    Directory of Open Access Journals (Sweden)

    Becker, Thorsten

    2015-08-01

    Full Text Available LaserCUSING® is a selective laser melting (SLM process that is capable of manufacturing parts by melting powder with heat input from a laser beam. LaserCUSING demonstrates potential for producing the intricate geometries specifically required for biomedical implants and aerospace applications. One main limitation to this form of rapid prototyping is the lack of published studies on the material performance of the resulting material. Studies of the material’s performance are often complicated by dependence on several factors, including starting powder properties, laser parameters, and post-processing heat treatments. This study aims to investigate the mechanical properties of LaserCUSING-produced Ti-6Al-4V and its performance relative to the conventional wrought counterpart. A combination of conventional and LaserCUSING-tailored heat treatments is performed. The resulting microstructures are studied and linked to the properties obtained from hardness tests. The findings highlight that LaserCused Ti-6Al-4V is competitive with traditional materials, provided that optimal parameters are chosen and parts are subject to tailored post-processing. In the as-built condition, LaserCused Ti-6Al-4V displays superior strength and hardness as a result of a martensitic microstructure, and a poorer performance in ductility. However, the material performance can be improved using tailored heat treatments. Careful consideration must be given to suitable post-processing before application in critical components in the aerospace or biomedical industry can occur

  19. Characterization of the heat transfer properties of thermal interface materials

    Science.gov (United States)

    Fullem, Travis Z.

    Physicists have studied the thermal conductivity of solids for decades. As a result of these efforts, thermal conduction in crystalline solids is well understood; there are detailed theories describing thermal conduction due to electrons and phonons. Phonon scattering and transmission at solid/solid interfaces, particularly above cryogenic temperatures, is not well understood and more work is needed in this area. The desire to solve engineering problems which require good thermal contact between mating surfaces has provided enhanced motivation for furthering the state of the art on this topic. Effective thermal management is an important design consideration in microelectronic systems. A common technique for removing excess heat from an electronic device is to attach a heatsink to the device; it is desirable to minimize the thermal resistance between the device and the heatsink. This can be accomplished by placing a thermal interface material (TIM) between the two surfaces. Due to the ever-increasing power densities found in electronic components, there is a desire to design better TIMs, which necessitates the ability to characterize TIM bondlines and to better understand the physics of heat conduction through TIM bondlines. A micro Fourier apparatus which employs Pt thin film thermometers of our design has been built and is capable of precisely quantifying the thermal resistance of thermal interface materials. In the present work several types of commercially available TIMs have been studied using this apparatus, including: greases, filled epoxies, and thermally conductive pads. In the case of filled epoxies, bondlines of various thicknesses, ranging from thirty microns to several hundred microns, have been measured. The microstructure of these bondlines has been investigated using optical microscopy and acoustic microscopy. Measured values of thermal conductivity are considered in terms of microstructural features such as percolation networks and filler particle

  20. Using geothermal energy to heat a portion of a formation for an in situ heat treatment process

    Science.gov (United States)

    Pieterson, Roelof; Boyles, Joseph Michael; Diebold, Peter Ulrich

    2010-06-08

    Methods of using geothermal energy to treat subsurface formations are described herein. Methods for using geothermal energy to treat a subsurface treatment area containing or proximate to hydrocarbons may include producing geothermally heated fluid from at least one subsurface region. Heat from at least a portion of the geothermally heated fluid may be transferred to the subsurface treatment area to heat the subsurface treatment area. At least some hydrocarbon fluids may be produced from the formation.

  1. Experimental evaluation on natural convection heat transfer of microencapsulated phase change materials slurry in a rectangular heat storage tank

    International Nuclear Information System (INIS)

    Zhang Yanlai; Rao Zhonghao; Wang Shuangfeng; Zhang Zhao; Li Xiuping

    2012-01-01

    Highlights: ► It gives heat transfer characteristics in a rectangular heat storage tank as the basic unit for reservoir of thermal storage. ► Onset of natural convection gets easier for the MPCMS with a higher mass concentration. ► It enhances the heat transfer ability of natural convection for the MPCMS. ► Obtained the relationship between Ra and Nu of the MPCMS. - Abstract: The main purpose of this experiment is to evaluate natural convection heat transfer characteristics of microencapsulated PCM (phase change material) slurry (MPCMS) during phase change process in a rectangular heat storage tank heated from the bottom and cooled at the top. The microencapsulated PCM is several material compositions of n-paraffin waxes (mainly nonadecane) as the core materials, outside a layer of a melamine resin wrapped. In the present study, its slurry is used mixing with water. And the specific heat capacity with latent heat shows a peak value at the temperature of about T = 31 °C. We investigate the influences of the phase change process of the MPCMS on natural convection heat transfer. The experimental results indicate that phase change process of the MPCMS promote natural convection heat transfer. The local maximum heat transfer enhancement occurs at approximately T H = 34 °C corresponding to the heated plate temperature. With high mass concentration C m , the onset of natural convection gets easier for the MPCMS. The temperature gradient is larger near top plate and bottom plate of a rectangular heat storage tank. Heat transfer coefficient increases with the phase change of the PCM. And it summarizes that the phase change process of the PCM promote the occurrence of natural convection.

  2. Desensitization of stainless steels by laser surface heat-treatment

    Energy Technology Data Exchange (ETDEWEB)

    Nakao, Yoshikuni; Nishimoto, Kazutoshi

    1987-11-01

    Laser heating was applied for the desensitization heat-treatment of the surface layer in the sensitized HAZ of Type 304 stainless steel. The degree of sensitization was examined by EPR technique and the 10 % oxalic acid electrolytic etch test. The CO/sub 2/ laser with maximum power of 1.5 kW was used for heat-treatment. Time-Temperature-Desensitization diagram (TTDS diagram) for sensitized Type 304 stainless steels were developed by calculation assuming the chromium diffusion control for desensitization which might occur when the chromium depleted zone was healed up due to dissolution of chromium carbide and chromium diffusion from the matrix being heated at the solution annealing temperatures. TTDS diagrams calculated agree fairly well with ones determined by corrosion tests. Laser irradiation conditions (e.g., Laser power, beam diameter and traveling velocity) required for desensitization of sensitized Type 304 stainless steels were calculated using additivity rule from the TTDS diagram calculated and theoretical thermal curve of laser heating derived from the heat conduction theory. After laser beam irradiated under an optimum condition predicted by calculation, the sensitized HAZ of Type 304 stainless steel restored complete resistance to intergranular corrosion.

  3. Impact Toughness and Heat Treatment for Cast Aluminum

    Science.gov (United States)

    Lee, Jonathan A (Inventor)

    2016-01-01

    A method for transforming a cast component made of modified aluminum alloy by increasing the impact toughness coefficient using minimal heat and energy. The aluminum alloy is modified to contain 0.55%-0.60% magnesium, 0.10%-0.15% titanium or zirconium, less than 0.07% iron, a silicon-tomagnesium product ratio of 4.0, and less than 0.15% total impurities. The shortened heat treatment requires an initial heating at 1,000deg F. for up to I hour followed by a water quench and a second heating at 350deg F. to 390deg F. for up to I hour. An optional short bake paint cycle or powder coating process further increase.

  4. EFFECT OF HEAT TREATMENT ON SOYBEAN PROTEIN SOLUBILITY

    Directory of Open Access Journals (Sweden)

    RODICA CĂPRIŢĂ

    2007-05-01

    Full Text Available The use of soybean products in animal feeds is limited due to the presence of antinutritional factors (ANF. Proper heat processing is required to destroy ANF naturally present in raw soybeans and to remove solvent remaining from the oil extraction process. Over and under toasting of soybean causes lower nutritional value. Excessive heat treatment causes Maillard reaction which affects the availability of lysine in particular and produces changes to the chemical structure of proteins resulting in a decrease of the nutritive value. The objective of this study was to evaluate the effect of heating time on the protein solubility. The investigation of the heating time on protein solubility in soybean meal (SBM revealed a negative correlation (r = -0.9596. Since the urease index is suitable only for detecting under processed SBM, the protein solubility is an important index for monitoring SBM quality.

  5. Heat treatment effect on ductility of nickel-base alloys

    International Nuclear Information System (INIS)

    Burnakov, K.K.; Khasin, G.A.; Danilov, V.F.; Oshchepkov, B.V.; Listkova, A.I.

    1979-01-01

    Causes of low ductility of the KhN75MBTYu and KhN78T alloys were studied along with the heat treatment effects. Samples were tested at 20, 900, 1100, 1200 deg C. Large amount of inclusions was found in intercrystalline fractures of the above low-ductile alloys. The inclusions of two types took place: (α-Al 2 O 3 , FeO(Cr 2 O 3 xAl 2 O 3 )) dendrite-like ones and large-size laminated SiO 2 , FeO,(CrFe) 2 O 3 inclusions situated as separate colonies. Heat treatment of the alloys does not increase high-temperature impact strength and steel ductility. The heating above 1000 deg C leads to a partial dissolution and coagulation of film inclusions which results in an impact strength increase at room temperature

  6. Heat treatments and low temperature fracture toughness of a Ti-6A1-4V alloy

    International Nuclear Information System (INIS)

    Nagai, K.; Hiraga, K.; Ishikawa, K.; Ogata, T.

    1984-01-01

    Titanium alloy is one of the reliable structural materials for cryogenic use owing to its high strength, high specific strength and low thermal conductivity. Heat treatment is one method of controlling the normally poor fracture toughness of this alloy at ambient temperature. However, there have been few attempts to improve the low temperature fracture toughness by heat treatment. This study was conducted to elucidate the effects of heat treatments on the low temperature fracture toughness in a Ti-6A1-4V alloy. The effects of the heat treatments were as follows: the beta treatment was a very feasible method to improve the low temperature fracture properties; the alpha+beta treatment was favorable for the increment in the low temperature ductility but did not largely improve the fracture toughness; the double treatment yielded good ductility but was not useful for improving the fracture toughness

  7. Effect of Cold Drawing and Heat Treatment on the Microstructure of Invar36 Alloy Wire

    International Nuclear Information System (INIS)

    Han, Seung Youb; Jang, Seon Ah; Eun, Hee-Chul; Choi, Jung-Hoon; Lee, Ki Rak; Park, Hwan Seo; Ahn, Do-Hee; Kim, Soo Young; Kim, Jea Youl; Shin, Sang Yong

    2016-01-01

    In this study, the effect of cold drawing and heat treatment on the microstructure of Invar36 alloy wire was investigated. Invar36 alloy wire is used as a transmission line core material, and is required to have high strength. The diameter of the Invar36 alloy wire specimens were reduced from 16 mm to 4.3 mm after three cold drawing and two heat treatment processes, thereby increasing tensile strength. Specimens were taken after each of the cold drawing and heat treatment processes, and their microstructure and tensile properties were analyzed. The Invar36 alloy wire had a γ-(Fe, Ni) phase matrix before the cold drawing and heat treatment processes. After the cold drawing processes, {220} and {200} textures were mainly achieved. After the heat treatment processes, a {200} recrystallization γ-(Fe, Ni) phase was formed with fine carbides. The recrystallization γ-(Fe, Ni) phase grains had low dislocation density, so they probably accommodated a large amount of deformation during the cold drawing processes.

  8. Effect of Cold Drawing and Heat Treatment on the Microstructure of Invar36 Alloy Wire

    Energy Technology Data Exchange (ETDEWEB)

    Han, Seung Youb; Jang, Seon Ah; Eun, Hee-Chul; Choi, Jung-Hoon; Lee, Ki Rak; Park, Hwan Seo; Ahn, Do-Hee [Korea Atomic Energy Research Institute, Daejeon (Korea, Republic of); Kim, Soo Young; Kim, Jea Youl [RandD Center, KOS Ltd., Yangsan (Korea, Republic of); Shin, Sang Yong [University of Ulsan, Ulsan (Korea, Republic of)

    2016-10-15

    In this study, the effect of cold drawing and heat treatment on the microstructure of Invar36 alloy wire was investigated. Invar36 alloy wire is used as a transmission line core material, and is required to have high strength. The diameter of the Invar36 alloy wire specimens were reduced from 16 mm to 4.3 mm after three cold drawing and two heat treatment processes, thereby increasing tensile strength. Specimens were taken after each of the cold drawing and heat treatment processes, and their microstructure and tensile properties were analyzed. The Invar36 alloy wire had a γ-(Fe, Ni) phase matrix before the cold drawing and heat treatment processes. After the cold drawing processes, {220} and {200} textures were mainly achieved. After the heat treatment processes, a {200} recrystallization γ-(Fe, Ni) phase was formed with fine carbides. The recrystallization γ-(Fe, Ni) phase grains had low dislocation density, so they probably accommodated a large amount of deformation during the cold drawing processes.

  9. Effect of heat treatment on brewer's yeast fermentation activity

    OpenAIRE

    Kharandiuk, Tetiana; Kosiv, Ruslana; Palianytsia, Liubov; Berezovska, Natalia

    2015-01-01

    The influence of temperature treatment of brewer's yeast strain Saflager W-34/70 at temperatures of -17, 20, 25, 30, 35, 40 °C on their fermentative activity was studied. It was established that the freezing of yeast leads to a decrease of fermentation activity in directly proportional to the duration way. Fermentative activity of yeast samples can be increased by 20-24% by heat treatment at 35 °C during 15-30 minutes.

  10. Influence of heat treatment temperature on bonding and oxidation ...

    Indian Academy of Sciences (India)

    The effects of heat treatment temperature on the morphology, composition, chemical bonds, oxidation resistance and compressive strength of diamond particles coated with TiO2 films were characterized through scanning electron microscopy, Fourier transform infrared, Raman spectroscopy, X-ray diffraction analysis, X-ray ...

  11. Influence of heat treatment temperature on bonding and oxidation ...

    Indian Academy of Sciences (India)

    Administrator

    Diamond; TiO2 film; heat treatment temperature; anti-oxidation; mechanical properties. 1. Introduction. Due to its ..... figure 4a, which was due to the change of chemical envi- ronment of ... graphite, diamond, diamond-like carbon and carbon.10.

  12. The effects of heat treatment on physical and technological ...

    African Journals Online (AJOL)

    STORAGESEVER

    2009-10-19

    Oct 19, 2009 ... ween 450 and 660 m altitudes in Cide-Sehdagi (Gercek et al., 1998; Dogu ... changes continue as the temperature is increased in ... Heat treatment slows water uptake and wood cell wall absorbs ...... The Effect of Boiling Time.

  13. Application of microjet in heat treatment of aluminium bronzes

    Directory of Open Access Journals (Sweden)

    Z. Górny

    2011-04-01

    Full Text Available Mechanical properties of a CuAl10Fe4Ni4 bronze subjected to solution heat treatment and toughening were examined. In solution heattreatment, a microjet was used to raise the cooling rate. A slight increase of mechanical properties was observed.

  14. THE EFFECTS OF INTERCRITICAL HEAT TREATMENTS ON THE ...

    African Journals Online (AJOL)

    Effect of intercritical heat treatment on 0.14wt%C 0.56wt%Mn 0.13wt%Si struc- ... Table 1: Chemical composition of the steel used (wt. %) with its critical temperature (calculated). C. Mn. Si. Ni. S ... primary austenitic grain size hardening and.

  15. Effect of heat treatment on polyphenol oxidase and peroxidase ...

    African Journals Online (AJOL)

    Effect of heat treatment (55°C/20 min) on polyphenol oxidase (PPO) and peroxidase (POD) activities and total phenolic compounds was investigated in Algerian dates (Deglet Nour variety) at Tamar (fully ripe) stage and in dates stored for 5 months at ambient temperature and in cold storage (10°C). Results obtained ...

  16. Laser heat treatment of welds for various stainless steels

    Science.gov (United States)

    Dontu, O.; Ganatsios, S.; Alexandrescu, N.; Predescu, C.

    2008-03-01

    The paper presents a study concerning the post - weld heat treatment of a duplex stainless steel. Welded joint samples were surface - treated using the same laser source adopted during welding in order to counterbalance the excess of ferrite formed in the welding process.

  17. Temperature Dependence and Magnetic Properties of Injection Molding Tool Materials Used in Induction Heating

    DEFF Research Database (Denmark)

    Guerrier, Patrick; Nielsen, Kaspar Kirstein; Hattel, Jesper Henri

    2015-01-01

    To analyze the heating phase of an induction heated injection molding tool precisely, the temperature-dependent magnetic properties, B–H curves, and the hysteresis loss are necessary for the molding tool materials. Hence, injection molding tool steels, core materials among other materials have...

  18. Heat treatment giving a stable high temperature micro-structure in cast austenitic stainless steel

    Science.gov (United States)

    Anton, Donald L.; Lemkey, Franklin D.

    1988-01-01

    A novel micro-structure developed in a cast austenitic stainless steel alloy and a heat treatment thereof are disclosed. The alloy is based on a multicomponent Fe-Cr-Mn-Mo-Si-Nb-C system consisting of an austenitic iron solid solution (.gamma.) matrix reinforced by finely dispersed carbide phases and a heat treatment to produce the micro-structure. The heat treatment includes a prebraze heat treatment followed by a three stage braze cycle heat treatment.

  19. THE INFLUENCE OF PRE-HEAT TREATMENT ON WHITE CAST IRONS PLASTICITY

    Directory of Open Access Journals (Sweden)

    T. M. Myronova

    2013-11-01

    Full Text Available Purpose. The development of heat treatment modes of white cast irons for structure changes in their eutectic constituent, namely in disturbing the monolithic structure of ledeburite colonies cementite structure and eutectic net continuity. Also the mentioned heat treatment modes are targeted to the eutectic net shift for the most suitable position from the point of plastic deforming. Methodology. The hypoeutectic white cast irons with 2.92…3.35 % carbon content and additionally alloyed by 3.18 % vanadium have been used as the research materials. The mentioned alloys have been pre-heat treated and hot twist tested. Findings. The research results showed that the carbide net breaking by plastic deforming leads to cast irons mechanical properties increasing but has difficulties in implementation due to the white cast irons low plasticity. The influence of different pre-heat treatment modes on structure and plasticity of white hypoeutectic cast irons have been investigated. They include the isotherm soaking under the different temperatures as well as multiply soakings and thermo-cycling. The influence of eutectic level, as well as pre heat treatment modes on different composition white cast irons hot plasticity have been investigated. Originality. It was determined that the heat treatment, which leads to double α→γ recrystallization under 860 – 950 °С and reperlitization under 720-680 °С results in significant increase of plasticity, as well as in un-alloyed and alloyed by vanadium white cast irons. It takes place due to carbide matrix phase separation in ledeburite colonies by new phase boundaries forming especially due to carbide transformations under vanadium alloying. Practical value. The implementation of pre-heat treatment with phase recrystallization resulted in hypoeutectic white cast irons plasticity increasing. The obtained level of cast iron plasticity corresponds to the one of carbide class steels, which ensures the successful

  20. Influence of heat treatment on the machinability and corrosion behavior of AZ91 Mg alloy

    Directory of Open Access Journals (Sweden)

    Swetha Chowdary V

    2018-03-01

    Full Text Available In the present study, AZ91 Mg alloy was heat treated at 410 °C for 6, 12 and 24 h to investigate the influence of heat treatment on machinability and corrosion behavior. The effect of soaking time on the amount and distribution of Mg17Al12 (β – phase was analyzed under the optical microscope. Microhardness measurements demonstrated the increased hardness with increased heat treatment soaking time, which can be attributed to the solid solution strengthening. The influence of super saturated α-grains on reducing the cutting force (Fz with respect to increased cutting speed was observed as prominent. The corrosion behavior of the heat treated specimens was studied by conducting electrochemical tests. Surprisingly, corrosion rate of heat treated samples was observed as increased compared with the base material. From the results, it is evident that the machinability of AZ91 Mg alloy can be improved by producing super saturated α-grains through heat treatment but at the cost of losing corrosion resistance. Keywords: AZ91 Mg alloy, Solid solution, Turning, Corrosion, Machinability

  1. Reinforced concrete treatment as composite material

    International Nuclear Information System (INIS)

    Oller, S.; Onate, E.; Miguel, J.

    1995-01-01

    This paper presents the general mixing theory applied to the numerical simulation of multiphase composite material behaviour as reinforced concrete materials. This theory is based on the mixture of that composite basic substances and allows to evaluate the inter-dependence behaviour between the different compounding constitutive models. If it would be necessary to consider the initial anisotropy of each compound it could be done by mean of the mapped isotropic plastic formulation. The approach is a generalization of the classic isotropic plasticity theory to be applied to either ortho tropic or anisotropic materials such as reinforced concrete. The existence of a stress and strain real anisotropic spaces, and the respective fictitious isotropic spaces are assumed, where a mapped fictitious problem is solved. Those spaces are relating by means of two fourth order transformation tensors. Both formulation are joined establishing a powerful work tool for the treatment of bulk-fiber composite materials. The induced anisotropy behaviour is take into account by each compounding constitutive formulation. (author). 24 refs., 3 figs

  2. THE EFFECT OF HEAT TREATMENT ON THE DURABILITY OF BAMBOO Gigantochloa scortechinii

    Directory of Open Access Journals (Sweden)

    Norashikin Kamarudin

    2012-07-01

    Full Text Available Bamboo signifies as one of the fastest growing plants and it can be used for various products. In tropical countries such as Indonesia and Malaysia, bamboo is abundantly available at reasonable prices, therefore it is used for numerous purposes. However, as lignocellulosic material, bamboo is susceptible to fungal and insect attacks. Heat treatment is an option to improve bamboo's durability. The objective of this study was to improve the durability of bamboo using hot oil palm treatment. A Malaysian grown bamboo species, Buluh Semantan (Gigantochloa scortechinii, as a study material was soaked in hot oil palm for various temperatures and soaking time, before being inoculated with the basidiomycete Coriolus versicolor in an agar block test. The results demonstrated that the longer the heating time, the more improved the durability of bamboo. Altering the temperature in the palm oil treatment produced varying results. Bamboo blocks that heated in hot oil palm at 100°C for 60 minutes shows considerably less weight eduction that indicates less fungal attack. Overall, the higher the temperature, the better the durability of bamboo. Please indicates what the meaning of heat treatment in this experiment, it is not clear.

  3. A new paradigm for heat treatment of alloys

    Energy Technology Data Exchange (ETDEWEB)

    Ustinovshikov, Y., E-mail: ust@ftiudm.ru

    2014-11-25

    Highlights: • The sign of the ordering energy in alloys varies with the temperature. • Each temperature of heating leads to formation of its characteristic microstructure. • Quenching of alloys is a totally unnecessary and useless operation. - Abstract: The article considers the consequences in the field of heat treatment of alloys that could follow the introduction of the concept of phase transition ordering-phase separation into common use. By example of the Fe{sub 50}Cr{sub 50} alloy, industrial carbon tool steel and Ni{sub 88}Al{sub 12} alloy, it is shown that this transition occurs at a temperature, which is definite for each system, that the change of the sign of the chemical interaction between component atoms reverses the direction of diffusion fluxes in alloys, which affects changes in the type of microstructures. The discovery of this phase transition dramatically changes our understanding of the solid solution, changes the ideology of alloy heat treatment. It inevitably leads to the conclusion about the necessity of carrying out structural studies with the help of TEM in order to adjust the phase diagrams of the systems where this phase transition has been discovered. Conclusions have been made that quenching of alloys from the so-called region of the solid solution, which is usually performed before tempering (aging) is a completely unnecessary and useless operation, that the final structure of the alloy is formed during tempering (aging) no matter what the structure was before this heat treatment.

  4. Sour gas injection for use with in situ heat treatment

    Science.gov (United States)

    Fowler, Thomas David [Houston, TX

    2009-11-03

    Systems, methods, and heaters for treating a subsurface formation are described herein. At least one method for providing acidic gas to a subsurface formation is described herein. The method may include providing heat from one or more heaters to a portion of a subsurface formation; producing fluids that include one or more acidic gases from the formation using a heat treatment process. At least a portion of one of the acidic gases may be introduced into the formation, or into another formation, through one or more wellbores at a pressure below a lithostatic pressure of the formation in which the acidic gas is introduced.

  5. Physical aspects of thermotherapy: A study of heat transport with a view to treatment optimisation

    Science.gov (United States)

    Olsrud, Johan Karl Otto

    1998-12-01

    investigated as a method of non-invasive temperature monitoring, and an optically tissue-like phantom material, suitable for MRI, was developed. MRI thermometry in this material was shown to be an excellent method for characterization of laser applicators and for verification of numerical calculations. Finally, a water-cooled laser applicator for the treatment of benign prostatic hyperplasia, allowing anatomically correct heating, was developed and evaluated ex-vivo. An increased understanding of the physical aspects of thermotherapy, aided by the methods and results presented in this thesis, constitutes a significant contribution to the performance of safe and efficacious treatment.

  6. Numerical Heat Transfer Studies of a Latent Heat Storage System Containing Nano-Enhanced Phase Change Material

    Directory of Open Access Journals (Sweden)

    S F Hosseinizadeh

    2011-01-01

    Full Text Available The heat transfer enhancement in the latent heat thermal energy storage system through dispersion of nanoparticle is reported. The resulting nanoparticle-enhanced phase change materials (NEPCM exhibit enhanced thermal conductivity in comparison to the base material. The effects of nanoparticle volume fraction and some other parameters such as natural convection are studied in terms of solid fraction and the shape of the solid-liquid phase front. It has been found that higher nanoparticle volume fraction result in a larger solid fraction. The present results illustrate that the suspended nanoparticles substantially increase the heat transfer rate and also the nanofluid heat transfer rate increases with an increase in the nanoparticles volume fraction. The increase of the heat release rate of the NEPCM shows its great potential for diverse thermal energy storage application.

  7. Comparative study of heat transfer and wetting behaviour of conventional and bioquenchants for industrial heat treatment

    Energy Technology Data Exchange (ETDEWEB)

    Fernandes, Peter; Prabhu, K. Narayan [Department of Metallurgical and Materials Engineering, National Institute of Technology Karnataka, Surathkal, P.O. Srinivasnagar 575 025 Mangalore, Karnataka State (India)

    2008-02-15

    An investigation was conducted to study the suitability of vegetable oils as bioquenchants for industrial heat treatment. The study involved the assessment of the severity of quenching and wetting behaviour of conventional and vegetable oil quench media. Quench severities of sunflower, coconut and palm oils were found to be greater than mineral oil. The quench severity of aqueous media is greater than oil media although their wettability is poor as indicated by their higher contact angles. A dimensionless contact angle parameter defined in this work is found to be a better parameter to compare the wetting behaviour with heat transfer. (author)

  8. Effect of heat treatment on the characteristics of tool steel deposited by the directed energy deposition process

    Science.gov (United States)

    Park, Jun Seok; Lee, Min-Gyu; Cho, Yong-Jae; Sung, Ji Hyun; Jeong, Myeong-Sik; Lee, Sang-Kon; Choi, Yong-Jin; Kim, Da Hye

    2016-01-01

    The directed energy deposition process has been mainly applied to re-work and the restoration of damaged steel. Differences in material properties between the base and the newly deposited materials are unavoidable, which may affect the mechanical properties and durability of the part. We investigated the effect of heat treatment on the characteristics of tool steel deposited by the DED process. We prepared general tool steel materials of H13 and D2 that were deposited onto heat-treated substrates of H13 and D2, respectively, using a direct metal tooling process. The hardness and microstructure of the deposited steel before and after heat treatment were investigated. The hardness of the deposited H13 steel was higher than that of wrought H13 steel substrate, while that of the deposited D2 was lower than that of wrought D2. The evolution of the microstructures by deposition and heat treatment varied depending on the materials. In particular, the microstructure of the deposited D2 steel after heat treatment consisted of fine carbides in tempered martensite and it is expected that the deposited D2 steel will have isotropic properties and high hardness after heat treatment.

  9. Effect of Heat Treatment on the Surface Properties of Activated Carbons

    Directory of Open Access Journals (Sweden)

    Meriem Belhachemi

    2011-01-01

    Full Text Available This work reports the effect of heat treatment on the porosity and surface chemistry of two series of activated carbons prepared from a local agricultural biomass material, date pits, by physical activation with carbon dioxide and steam. Both series samples were oxidized with nitric acid and subsequently heat treated under N2 at 973 K in order to study the effect of these treatments in porosity and surface functional groups of activated carbons. When the activated carbons were heat treated after oxidation the surface area and the pore volume increase for both activated carbons prepared by CO2 and steam activations. However the amount of surface oxygen complexes decreases, the samples keep the most stable oxygen surface groups evolved as CO by temperature-programmed desorption experiments at high temperature. The results show that date pits can be used as precursors to produce activated carbons with a well developed porosity and tailored oxygen surface groups.

  10. Effects of heat treatment to the sound velocity and microstructural changes of ASTM A516 steels

    International Nuclear Information System (INIS)

    Norasiah Abdul Kasim; Azali Muhammad; Amry Amin Abas; Zaiton Selamat

    2010-01-01

    Full-text: The used of ultrasonic testing as a thickness measurement for structural components (pipeline and pressure vessel) is among the popular inspection tool widely use in the industrial power plant such as at petrochemical and nuclear power plant. Currently, there are cases where the thickness grows and the result will affect the reliability of the test. There are many factors that can affect the reliability of measurement. One of it is the material under test itself. In the Malaysian Nuclear Agency, initial efforts are underway to study the understanding on the effects of heat treatment to the sound velocity and microstructure changes of ASTM A516 steel. Few samples of thin square shaped prepared were heat treated under the following conditions: austenitization at 9800 degree Celsius - 2 hours, quenching; tempering at various temperature 4000, 5000, 6000 and 7000 degree Celsius. The results show that the microstructure changes and samples exhibit different sound velocity at different heat treatment. (author)

  11. Characterization by transmission electron microscopy of a JRQ steel subjected to different heat treatments

    International Nuclear Information System (INIS)

    Moreno G, N.

    2014-01-01

    In this work a study was conducted on the steel Astm A-533, Grade B, Class 1 of reference JRQ, for the purpose of carrying out a study by transmission electron microscopy on the size and distribution of precipitates in steel samples JRQ previously subjected to heat treatments. This because the reactor vessels of the nuclear power plant of Laguna Verde, are made of a steel Astm A-533 Grade B, Class 1. It is known that the neutron radiation causes damage primarily embrittlement in materials that are exposed to it. However, observable damage through mechanical tests result from microstructural defects and atomic, induced by the neutron radiation. In previous studies hardening by precipitation of a JRQ steel (provided by the IAEA) was induced by heat treatments, finding that the conditions of heat treatment that reproduce the hardness and stress mechanical properties of a steel Astm A-533, Grade B, Class 1 irradiated for 8 years to a fluence of 3.5 x 10 17 neutrons/cm 2 and to a temperature of 290 grades C are achieved with annealing treatments at 550 grades C. In the studied samples it was found that the more hardening phase both the heat treatments as the neutron radiation, is the bainite, being the ferrite practically unchanged. Which it gave the tone to believe that the ferrite is the phase that provides at level macro the mechanical properties in stress, since in the irradiated samples such properties remained unchanged with respect to the non-irradiated material, however changes were observed in material ductility, which may be attributable to the change of hardness in the bainite, which opens a possibility for modeling the micromechanical behavior of this material. (Author)

  12. Modeling and impacts of the latent heat of phase change and specific heat for phase change materials

    Science.gov (United States)

    Scoggin, J.; Khan, R. S.; Silva, H.; Gokirmak, A.

    2018-05-01

    We model the latent heats of crystallization and fusion in phase change materials with a unified latent heat of phase change, ensuring energy conservation by coupling the heat of phase change with amorphous and crystalline specific heats. We demonstrate the model with 2-D finite element simulations of Ge2Sb2Te5 and find that the heat of phase change increases local temperature up to 180 K in 300 nm × 300 nm structures during crystallization, significantly impacting grain distributions. We also show in electrothermal simulations of 45 nm confined and 10 nm mushroom cells that the higher amorphous specific heat predicted by this model increases nucleation probability at the end of reset operations. These nuclei can decrease set time, leading to variability, as demonstrated for the mushroom cell.

  13. Ploidy Manipulation of Zebrafish Embryos with Heat Shock 2 Treatment

    Science.gov (United States)

    Baars, Destiny L.; Pelegri, Francisco

    2016-01-01

    Manipulation of ploidy allows for useful transformations, such as diploids to tetraploids, or haploids to diploids. In the zebrafish Danio rerio, specifically the generation of homozygous gynogenetic diploids is useful in genetic analysis because it allows the direct production of homozygotes from a single heterozygous mother. This article describes a modified protocol for ploidy duplication based on a heat pulse during the first cell cycle, Heat Shock 2 (HS2). Through inhibition of centriole duplication, this method results in a precise cell division stall during the second cell cycle. The precise one-cycle division stall, coupled to unaffected DNA duplication, results in whole genome duplication. Protocols associated with this method include egg and sperm collection, UV treatment of sperm, in vitro fertilization and heat pulse to cause a one-cell cycle division delay and ploidy duplication. A modified version of this protocol could be applied to induce ploidy changes in other animal species. PMID:28060351

  14. Influence of Heat Treatments on Carotenoid Content of Cherry Tomatoes

    Directory of Open Access Journals (Sweden)

    Laura D'Evoli

    2013-07-01

    Full Text Available Tomatoes and tomato products are rich sources of carotenoids—principally lycopene, followed by β-carotene and lutein. The aim of this work was to study the effect of heat treatment on carotenoid content in cherry tomatoes. Raw and canned products were sampled and analysed; furthermore whole, skin and pulp fractions of cherry tomatoes were analysed when raw and home-processed, in order to better understand heat treatment effects. Lycopene content in canned tomatoes was two-fold higher than in raw tomatoes (11.60 mg/100 g versus 5.12 mg/100 g. Lutein and β-carotene were respectively 0.15 mg/100 g and 0.75 mg/100 g in canned tomatoes versus 0.11 mg/100 g and 1.00 mg/100 g in raw tomatoes. For home-processed tomatoes, β-carotene and lutein showed a content decrease in all thermally treated products. This decrease was more evident for β-carotene in the skin fraction (−17%, while for lutein it was greater in the pulp fraction (−25%. Lycopene presented a different pattern: after heat treatment its concentration increased both in the whole and in pulp fractions, while in the skin fraction it decreased dramatically (−36%. The analysis of the isomers formed during the thermal treatment suggests that lycopene is rather stable inside the tomato matrix.

  15. Influence of Heat Treatments on Carotenoid Content of Cherry Tomatoes.

    Science.gov (United States)

    D'Evoli, Laura; Lombardi-Boccia, Ginevra; Lucarini, Massimo

    2013-07-31

    Tomatoes and tomato products are rich sources of carotenoids-principally lycopene, followed by β-carotene and lutein. The aim of this work was to study the effect of heat treatment on carotenoid content in cherry tomatoes. Raw and canned products were sampled and analysed; furthermore whole, skin and pulp fractions of cherry tomatoes were analysed when raw and home-processed, in order to better understand heat treatment effects. Lycopene content in canned tomatoes was two-fold higher than in raw tomatoes (11.60 mg/100 g versus 5.12 mg/100 g). Lutein and β-carotene were respectively 0.15 mg/100 g and 0.75 mg/100 g in canned tomatoes versus 0.11 mg/100 g and 1.00 mg/100 g in raw tomatoes. For home-processed tomatoes, β-carotene and lutein showed a content decrease in all thermally treated products. This decrease was more evident for β-carotene in the skin fraction (-17%), while for lutein it was greater in the pulp fraction (-25%). Lycopene presented a different pattern: after heat treatment its concentration increased both in the whole and in pulp fractions, while in the skin fraction it decreased dramatically (-36%). The analysis of the isomers formed during the thermal treatment suggests that lycopene is rather stable inside the tomato matrix.

  16. Distributed Control of Heat Conduction in Thermal Inductive Materials with 2D Geometrical Isomorphism

    Directory of Open Access Journals (Sweden)

    Chia-Yu Chou

    2014-09-01

    Full Text Available In a previous study we provided analytical and experimental evidence that some materials are able to store entropy-flow, of which the heat-conduction behaves as standing waves in a bounded region small enough in practice. In this paper we continue to develop distributed control of heat conduction in these thermal-inductive materials. The control objective is to achieve subtle temperature distribution in space and simultaneously to suppress its transient overshoots in time. This technology concerns safe and accurate heating/cooling treatments in medical operations, polymer processing, and other prevailing modern day practices. Serving for distributed feedback, spatiotemporal H ∞ /μ control is developed by expansion of the conventional 1D-H ∞ /μ control to a 2D version. Therein 2D geometrical isomorphism is constructed with the Laplace-Galerkin transform, which extends the small-gain theorem into the mode-frequency domain, wherein 2D transfer-function controllers are synthesized with graphical methods. Finally, 2D digital-signal processing is programmed to implement 2D transfer-function controllers, possibly of spatial fraction-orders, into DSP-engine embedded microcontrollers.

  17. The effect of veneering and heat treatment on the flexural strength of Empress 2 ceramics.

    Science.gov (United States)

    Cattell, M J; Palumbo, R P; Knowles, J C; Clarke, R L; Samarawickrama, D Y D

    2002-05-01

    The aims of the study were to test and compare the biaxial flexural strength and reliability of Empress 2 ceramics after heat treatment and the addition of the veneering material and to characterise their microstructures. Forty disc specimens (2 x 14 mm) and forty disc specimens (1 x 14 mm) were produced by heat pressing in the EP 500 press furnace. Group 1 (2 x 14 mm Empress 2 core) was as heat pressed and group 2 (2 x 14 mm Empress 2 core) was subjected to the recommended firing cycles. Groups 3 and 4 (1 x 14 mm Empress 2 core) were veneered with the dentine material and heat-treated as per group 2. Groups 1, 2 and 3 were lapped to 800 grit silicon carbide paper on the compressive surface only and group 4 on both the compressive and tensile test surfaces. Twenty disc specimens per group were tested using the biaxial flexure test at a crosshead speed of 0.15 mm/min. Specimens were characterised using X-ray diffraction (XRD) and secondary electron imaging (SEM). Mean biaxial flexural strengths (MPa+/-SD) were group 1: 265.5+/-25.7; group 2: 251.3+/-30.2; group 3: 258.6+/-21.4 and group 4: 308.6+/-37.7. There was no statistical difference between groups 1, 2 and 3 (p>0.05), but differences for group 4 (pEmpress 2 core material and an amorphous glass and some evidence of a crystalline phase in the dentine material. CONCLUSIONS; Veneering or heat treatment of Empress 2 ceramics did not significantly affect the mean biaxial flexural strength (p>0.05) or reliability. Surface modification of the Empress 2 core material increased the mean biaxial flexural strength (p<0.05).

  18. Heat treatments of TiAl-Cr-V casting alloy

    International Nuclear Information System (INIS)

    Pu, Z.J.; Ma, J.L.; Wu, K.H.

    1995-01-01

    The need to investigate various kinds of fine microstructure based on casting TiAl alloy led to development of a multiple-stage heat treatment procedure. The first stage required the transformation of as-cast lamellar structure into near-gamma structure, followed by required transformation of near-gamma structure into various kinds of fine microstructure. The as-cast lamellar structure can be changed into near-gamma structure by annealing the alloy at 1,200 C for at least 50 hours. During the annealing process, two mechanisms are involved in transforming the lamellar structure into a near-gamma structure. One is the discontinuous coarsening (DC) process, and the other is the continuous coarsening (CC) process. With the near-gamma structure as an initial structure, the alloy being heat-treated in the γ + α and in the α fields can produce various kinds of microstructure with fine grain size. These microstructure significantly differ from the microstructure produced by heat-treating the deformed lamellar structure. Results of the investigation show that careful control of the time of the heat-treatment process in the single a field can produce a fine fully lamellar structure

  19. Residual stress and mechanical properties of SiC ceramic by heat treatment

    International Nuclear Information System (INIS)

    Yoon, H.K.; Kim, D.H.; Shin, B.C.

    2007-01-01

    Full text of publication follows: Silicon carbide is a compound of relatively low density, high hardness, elevated thermal stability and good thermal conductivity, resulting in good thermal shock resistance. Because of these properties, SiC materials are widely used as abrasives and refractories. In this study, SiC single and poly crystals was grown by the sublimation method using the SiC seed crystal and SiC powder as the source material. Mechanical properties of SiC single and poly crystals are carried out by using the nano-indentation method and small punch test after the heat treatment. As a result, mechanical properties of SiC poly crystal had over double than single. And SiC single and poly crystals were occurred residual stress, but residual stress was shown relaxant properties by the effect of heat treatment. (authors)

  20. Effect of Heat Treatment on Microstructure and Impact Toughness of Ti-6Al-4V Manufactured by Selective Laser Melting Process

    Directory of Open Access Journals (Sweden)

    Lee K.-A.

    2017-06-01

    Full Text Available This study manufactured Ti-6Al-4V alloy using one of the powder bed fusion 3D-printing processes, selective laser melting, and investigated the effect of heat treatment (650°C/3hrs on microstructure and impact toughness of the material. Initial microstructural observation identified prior-β grain along the building direction before and after heat treatment. In addition, the material formed a fully martensite structure before heat treatment, and after heat treatment, α and β phase were formed simultaneously. Charpy impact tests were conducted. The average impact energy measured as 6.0 J before heat treatment, and after heat treatment, the average impact energy increased by approximately 20% to 7.3 J. Fracture surface observation after the impact test showed that both alloys had brittle characteristics on macro levels, but showed ductile fracture characteristics and dimples at micro levels.

  1. Survey and evaluation of available thermal insulation materials for use on solar heating and cooling systems

    Energy Technology Data Exchange (ETDEWEB)

    1980-03-01

    This is the final report of a survey and evaluation of insulation materials for use with components of solar heating and cooling systems. The survey was performed by mailing questionnaires to manufacturers of insulation materials and by conducting an extensive literature search to obtain data on relevant properties of various types of insulation materials. The study evaluated insulation materials for active and passive solar heating and cooling systems and for multifunction applications. Primary and secondary considerations for selecting insulation materials for various components of solar heating and cooling systems are presented.

  2. Computerized property prediction and process planning in heat treatment of steels

    Energy Technology Data Exchange (ETDEWEB)

    Gergely, M. (Steel Advisory Centre for Industrial Technologies (SACIT), Budapest (Hungary)); Somogyi, S. (Steel Advisory Centre for Industrial Technologies (SACIT), Budapest (Hungary)); Kohlheb, R. (Steel Advisory Centre for Industrial Technologies (SACIT), Budapest (Hungary))

    1994-01-01

    Recent years have seen widespread interest in the establishment of prediction methods, based on phenomenological description and computer simulation of transformation processes during heat treatment, and in the introduction of software for technological planning. The steady development of this approach is aimed at meeting the requirement of metallurgists, design engineers dealing with material selection and dimensioning, and technologists planning heat treatment processes. Research in this field of computer simulation has been concentrated so far on two main areas of interest: . Modelling of transformation processes and the prediction of microstructures and/or properties, . Developing program packages to help solve concrete tasks such as material selection, on-line process control and monitoring, and the design of heat-treating operations. During the last two decades in the field of heat treatment, various mathematical models with different accuracy and complexity have been developed. In this paper, an attempt is made to outline some important results in computer simulation and computerized property prediction without aiming at completeness. The topic is restricted to quenched and tempered, and case-hardened steels. (orig.)

  3. Technologies and Materials for Recovering Waste Heat in Harsh Environments

    Energy Technology Data Exchange (ETDEWEB)

    Nimbalkar, Sachin U. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Thekdi, Arvind [E3M, Inc. North Potomac, MD (United States); Rogers, Benjamin M. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Kafka, Orion L. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Wenning, Thomas J. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

    2014-12-15

    A large amount (7,204 TBtu/year) of energy is used for process heating by the manufacturing sector in the United States (US). This energy is in the form of fuels mostly natural gas with some coal or other fuels and steam generated using fuels such as natural gas, coal, by-product fuels, and some others. Combustion of these fuels results in the release of heat, which is used for process heating, and in the generation of combustion products that are discharged from the heating system. All major US industries use heating equipment such as furnaces, ovens, heaters, kilns, and dryers. The hot exhaust gases from this equipment, after providing the necessary process heat, are discharged into the atmosphere through stacks. This report deals with identification of industries and industrial heating processes in which the exhaust gases are at high temperature (>1200 F), contain all of the types of reactive constituents described, and can be considered as harsh or contaminated. It also identifies specific issues related to WHR for each of these processes or waste heat streams.

  4. Research on application of carbon fiber heating material in clothing

    Science.gov (United States)

    Yang, Huanhong

    2017-08-01

    With the development of society, the way of keeping warm clothing is also developing. Carbon fiber has the advantages of high efficiency, safety, mobility and comfort. As a heating element, it has good application prospect. In this paper, the main technology, application issues and design method of carbon fiber heating garment are analyzed, and the key problems in industrialization are also put forward.

  5. The influence of distal-end heat treatment on deflection of nickel-titanium archwire

    Directory of Open Access Journals (Sweden)

    Marcelo Faria da Silva

    2016-02-01

    Full Text Available Objective: The aim of this in vitro study was to evaluate the deflection-force behavior of nickel-titanium (NiTi orthodontic wires adjacent to the portion submitted to heat treatment. Material and Methods: A total of 106 segments of NiTi wires (0.019 x 0.025-in and heat-activated NiTi wires (0.016 x 0.022-in from four commercial brands were tested. The segments were obtained from 80 archwires. For the experimental group, the distal portion of each segmented archwire was subjected to heat treatment (n = 40, while the other distal portion of the same archwire was used as a heating-free control group (n = 40. Deflection tests were performed in a temperature-controlled universal testing machine. Unpaired Student's t-tests were applied to determine if there were differences between the experimental and control groups for each commercial brand and size of wire. Statistical significance was set at p < 0.05. Results: There were no statistically significant differences between the tested groups with the same size and brand of wire. Conclusions: Heat treatment applied to the distal ends of rectangular NiTi archwires does not permanently change the elastic properties of the adjacent portions.

  6. The heat treatment of steel. A mathematical control problem

    Energy Technology Data Exchange (ETDEWEB)

    Hoemberg, Dietmar; Kern, Daniela

    2009-07-21

    The goal of this paper is to show how the heat treatment of steel can be modelled in terms of a mathematical optimal control problem. The approach is applied to laser surface hardening and the cooling of a steel slab including mechanical effects. Finally, it is shown how the results can be utilized in industrial practice by a coupling with machine-based control. (orig.)

  7. Deep heat muscle treatment: A mathematical model - I

    International Nuclear Information System (INIS)

    Ogulu, A.; Bestman, A.R.

    1992-03-01

    The flow of blood during deep heat muscle treatment is studied in this paper. We model the blood vessel as a long tube in circular section whose radius varied slowly. Under the Boussinesq approximation, we seek asymptotic series expansions for the velocity components, temperature and pressure about a small parameter, ε, characterizing the radius variation. The study reveals mathematically why physicians recommend a hot bath for cuts and physiotherapists use ice packs for bruises. (author). 5 refs, 3 figs

  8. Microwave heat treatment as a substitute for conventional treatment of palm oil fruits

    International Nuclear Information System (INIS)

    Mujahid H Al-Fayadh; Nor Azura Masabbir Ali

    1996-01-01

    Microwave energy has become a sound method of heat treatment because of its high penetration power, cleanliness and possible economic significance. In this research, microwave heat was used as a substitute for conventional blanching method of palm oil fruits. Microwave treatment at 2450 MHz and 800 watts gave very close color and frn,frying characteristics to oil of blanched fruits after one minute exposure time. However, five minutes of microwave heat gave severe husk oil discoloration after 49 hours of deep frying, compared to all oils extracted from fruits treated by either low, microwave exposure time or conventional steam treatment. Kernel oil, after five minutes of microwave treatment, was less discolored than both steam or microwave-treated fruits for one minute. More carotenes and discoloration compounds may be contributed to discoloration during microwave treatments. Oil chemical constants of both husk and kernel oils treated by microwave heat were close to those treated by conventional heat. Further research is needed to investigate detailed oil characteristics and evaluate the feasibility study for using microwave energy, as a substitute for conventional heat in palm oil industry

  9. Effect of Heat Treatment on the Microstructure and Properties of HVOF-Sprayed Co-Cr-W Coating

    Czech Academy of Sciences Publication Activity Database

    Houdková, Š.; Smazalová, E.; Pala, Zdeněk

    2016-01-01

    Roč. 25, č. 3 (2016), s. 546-557 ISSN 1059-9630 Institutional support: RVO:61389021 Keywords : ASTM * G-65ASTM * Co-Cr-W * heat treatment * HVOF * Stellite 6 * wear Subject RIV: JK - Corrosion ; Surface Treatment of Materials Impact factor: 1.488, year: 2016

  10. Simulations of Precipitate Microstructure Evolution during Heat Treatment

    Science.gov (United States)

    Wu, Kaisheng; Sterner, Gustaf; Chen, Qing; Jou, Herng-Jeng; Jeppsson, Johan; Bratberg, Johan; Engström, Anders; Mason, Paul

    Precipitation, a major solid state phase transformation during heat treatment processes, has for more than one century been intensively employed to improve the strength and toughness of various high performance alloys. Recently, sophisticated precipitation reaction models, in assistance with well-developed CALPHAD databases, provide an efficient and cost-effective way to tailor precipitate microstructures that maximize the strengthening effect via the optimization of alloy chemistries and heat treatment schedules. In this presentation, we focus on simulating precipitate microstructure evolution in Nickel-base superalloys under arbitrary heat treatment conditions. The newly-developed TC-PRISMA program has been used for these simulations, with models refined especially for non-isothermal conditions. The effect of different cooling profiles on the formation of multimodal microstructures has been thoroughly examined in order to understand the underlying thermodynamics and kinetics. Meanwhile, validations against several experimental results have been carried out. Practical issues that are critical to the accuracy and applicability of the current simulations, such as modifications that overcome mean-field approximations, compatibility between CALPHAD databases, selection of key parameters (particularly interfacial energy and nucleation site densities), etc., are also addressed.

  11. Heat treatment trials for ITER toroidal field coils

    International Nuclear Information System (INIS)

    Matsui, Kunihiro; Hemmi, Tsutomu; Koizumi, Norikiyo; Nakajima, Hideo; Kimura, Satoshi; Nakamoto, Kazunari

    2012-01-01

    Cable-in-conduit (CIC) conductors using Nb 3 Sn strands are used in ITER toroidal fields (TF) coils. Heat treatment generates thermal strain in CIC conductors because of the difference in thermal expansion between the Nb 3 Sn strands and the stainless-steel jacket. The elongation/shrinkage of the TF conductor may make it impossible to insert a wound TF conductor into the groove of a radial plate. In addition, it is expected that the deformation of the winding due to heat treatment-based release of the residual force in the jacket may also make it impossible to insert the winding in the groove, and that correcting the winding geometry to allow insertion of the winding may influence the superconducting performance of the TF conductor. The authors performed several trials using heat treatment as the part of activities in Phase II of TF coil procurement aiming to resolve the above-mentioned technical issues, and evaluated the elongations of 0.064, 0.074 and 0.072% for the straight and curved conductors and 1/3-scale double-pancake (DP) winding, respectively. It was confirmed that correction if the deformed winding did not influence the superconducting performance of the conductor. (author)

  12. Hybrid fuzzy logic control of laser surface heat treatments

    International Nuclear Information System (INIS)

    Perez, Jose Antonio; Ocana, Jose Luis; Molpeceres, Carlos

    2007-01-01

    This paper presents an advanced hybrid fuzzy logic control system for laser surface heat treatments, which allows to increase significantly the uniformity and final quality of the obtained product, reducing the rejection rate and increasing the productivity and efficiency of the treatment. Basically, the proposed hybrid control structure combines a fuzzy logic controller, with a pure integral action, both fully decoupled, improving the performances of the process with a reasonable design cost, since the system nonlinearities are fully compensated by the fuzzy component of the controller, while the integral action contributes to eliminate the steady-state error

  13. Effect of pre-cooling and heat treatment on antioxidant enzymes ...

    African Journals Online (AJOL)

    Effect of pre-cooling and heat treatment on antioxidant enzymes profile of mango and banana. ... In banana, pre-cooling treatment (8 ºC) and heat treatment followed by cooling reduced CAT activity in peel and pulp, whereas POX activity increased. Pre-cooling and heat treatments altered normal homeostasis of these fruits, ...

  14. Effect of grinding and heat treatment on the mechanical behavior of zirconia ceramic

    Directory of Open Access Journals (Sweden)

    Gabriela Freitas RAMOS

    2016-01-01

    Full Text Available Abstract The present study investigated the effect of grinding on roughness, flexural strength, and reliability of a zirconia ceramic before and after heat treatment. Seven groups were tested (n = 15: a control group (labeled CG, untreated, and six groups of samples ground with diamond discs, simulating diamond burs, with grits of 200 µm (G80; 160 µm (G120, and 25 µm (G600, either untreated or heat-treated at 1200°C for 2 h (labeled A. Yttria tetragonal zirconia polycrystal discs were manufactured, ground, and submitted to roughness and crystalline phase analyses before the biaxial flexural strength test. There was no correlation between roughness (Ra and Rz and flexural strength. The reliability of the materials was not affected by grinding or heat treatment, but the characteristic strength was higher after abrasion with diamond discs, irrespective of grit size. The X-ray diffraction data showed that grinding leads to a higher monoclinic (m phase content, whereas heat treatment produces reverse transformation, leading to a fraction of m-phase in ground samples similar to that observed in the control group. However, after heat treatment, only the G80A samples presented strength similar to that of the control group, while the other groups showed higher strength values. When zirconia pieces must be adjusted for clinical use, a smoother surface can be obtained by employing finer-grit diamond burs. Moreover, when the amount of monoclinic phase is related to the degradation of zirconia, the laboratory heat treatment of ground pieces is indicated for the reverse transformation of zirconia crystals.

  15. Impact of Heat Treatment on the Freezing Points of Cow and Goat Milk

    Directory of Open Access Journals (Sweden)

    Bohumíra Janštová

    2009-01-01

    Full Text Available The aim of this study was to monitor the impact of heat treatment variables on the freezing point of cow and goat milk. The freezing point (FP was established in 30 bulk tank samples of goat milk and in 30 bulk tank samples of cow milk which were subject to laboratory heat treatment at temperatures of 72 °C (A, 85 °C (B, 95 °C (C, with the same exposition times of 20 s. Freezing point measurements of raw and heat-treated milk were carried out in compliance with the Standard CTS 57 0538 by a thermistor cryoscope. The FP of raw cow milk increased with heat treatment from the initial values of -0.5252 ± 0.0114 °C (O by 0.0023 °C (A, 0.0034 °C (B and 0.0051°C (C. Changes in FP values of goat milk were detected, from its initial value of –0.5530 ± 0.0086 °C there was an increase in the FP depending on the mode of heat treatment due to pasteurization by an average of 0.0028 °C (A, 0.0036 °C (B and 0.0054 °C (C. The dynamics of the changes were similar both in goat and cow milk. Freezing point values in cow and goat milk differed (P ⪬ 0.01 when compared to the freezing point of untreated milk after the individual interventions as well as when compared between each other. An increase in the heat treatment temperature of cow and goat milk causes an increase in the freezing point (a shift towards zero. These results can be used in practice for checking the raw material in dairy industry.

  16. Heat transfer within hydrodissection fluids: An analysis of thermal conduction and convection using liquid and gel materials.

    Science.gov (United States)

    Johnson, Alexander; Brace, Christopher

    2015-01-01

    Interventional oncology procedures such as thermal ablation are becoming widely used for many tumours in the liver, kidney and lung. Thermal ablation refers to the focal destruction of tissue by generating cytotoxic temperatures in the treatment zone. Hydrodissection - separating tissues with fluids - protects healthy tissues adjacent to the ablation treatment zone to improve procedural safety, and facilitate more aggressive power application or applicator placement. However, fluids such as normal saline and 5% dextrose in water (D5W) can migrate into the peritoneum, reducing their protective efficacy. As an alternative, a thermo-gelable poloxamer 407 (P407) solution has been recently developed to facilitate hydrodissection procedures. We hypothesise that the P407 gel material does not provide convective heat dissipation from the ablation site, and therefore may alter the heat transfer dynamics compared to liquid materials during hydrodissection-assisted thermal ablation. The purpose of this study was to investigate the heat dissipation mechanics within D5W, liquid P407 and gel P407 hydrodissection barriers. Overall it was shown that the gel P407 dissipated heat primarily through conduction, whereas the liquid P407 and D5W dissipated heat through convection. Furthermore, the rate of temperature change within the gel P407 was greater than liquid P407 and D5W. Testing to evaluate the in vivo efficacy of the fluids with different modes of heat dissipation seems warranted for further study.

  17. Effect of prolonged isothermal heat treatment on the mechanical behavior of advanced NANOBAIN steel

    Science.gov (United States)

    Avishan, Behzad

    2017-09-01

    The microstructural evolution and consequent changes in strength and ductility of advanced NANOBAIN steel during prolonged isothermal heat-treatment stages were investigated. The microstructure and mechanical properties of nanostructured bainite were not expected to be influenced by extending the heat-treatment time beyond the optimum value because of the autotempering phenomenon and high tempering resistance. However, experimental results indicated that the microstructure was thermodynamically unstable and that prolonged austempering resulted in carbon depletion from high-carbon retained austenite and carbide precipitations. Therefore, austenite became thermally less stable and partially transformed into martensite during cooling to room temperature. Prolonged austempering did not lead to the typical tempering sequence of bainite, and the sizes of the microstructural constituents were independent of the extended heat-treatment times. This independence, in turn, resulted in almost constant ultimate tensile strength values. However, microstructural variations enhanced the yield strength and the hardness of the material at extended isothermal heat-treatment stages. Finally, although microstructural changes decreased the total elongation and impact toughness, considerable combinations of mechanical properties could still be achieved.

  18. Technical project of complex fast cycle heat treatment of hydrogenous coal preparation

    OpenAIRE

    Moiseev, V. A.; Andrienko, V. G.; Pileckij, V. G.; Urvancev, A. I.; Gvozdyakov, Dmitry Vasilievich; Gubin, Vladimir Evgenievich; Matveev, Aleksandr Sergeevich; Savostiyanova, Ludmila Viktorovna

    2015-01-01

    Problems of heat-treated milled hydrogenous coal preparation site creation in leading fast cycle heat treatment complex were considered. Conditions for effective use of electrostatic methods of heat-treated milled hydrogenous coal preparation were set. Technical project of heat treatment of milled hydrogenous coal preparation site was developed including coupling of working equipment complex on fast heat treatment and experimental samples of equipment being designed for manufacturing. It was ...

  19. A novel hyperthermia treatment for bone metastases using magnetic materials

    International Nuclear Information System (INIS)

    Matsumine, Akihiko; Asanuma, Kunihiro; Matsubara, Takao; Nakamura, Tomoki; Uchida, Atsumasa; Sudo, Akihiro; Takegami, Kenji

    2011-01-01

    Patients with bone metastases in the extremities sometimes require surgical intervention to prevent deterioration of quality of life due to a pathological fracture. The use of localized radiotherapy combined with surgical reinforcement has been a gold standard for the treatment of bone metastases. However, radiotherapy sometimes induces soft tissue damage, including muscle induration and joint contracture. Moreover, cancer cells are not always radiosensitive. Hyperthermia has been studied since the 1940s using an experimental animal model to treat various types of advanced cancer, and studies have now reached the stage of clinical application, especially in conjunction with radiotherapy or chemotherapy. Nevertheless, bone metastases have several special properties which discourage oncologists from developing hyperthermic therapeutic strategies. First, the bone is located deep in the body, and has low thermal conductivity due to the thickness of cortical bone and the highly vascularized medulla. To address these issues, we developed new hyperthermic strategies which generate heat using magnetic materials under an alternating electromagnetic field, and started clinical application of this treatment modality. The purpose of this review is to summarize the latest studies on hyperthermic treatment in the field of musculoskeletal tumors, and to introduce the treatment strategy employing our novel hyperthermia approach. (author)

  20. Coupled heat transfer in high temperature transporting system with semitransparent/opaque material

    International Nuclear Information System (INIS)

    Du Shenghua; Xia Xinjin

    2010-01-01

    The heat transfer model of the aerodynamic heating coupled with radiative cooling was developed. The thermal protect system includes the higher heat flux region with high temperature semitransparent material, the heat transporting channel and the lower heat flux region with metal. The control volume method was combined with the Monte Carlo method to calculate the coupled heat transfer of the transporting system, and the thermal equilibrium equation for the transporting channel was solved simultaneously. The effect of the aeroheating flux radio, the area ratio of radiative surfaces, the convective heat transfer coefficient of the heat transporting channel on the radiative surface temperature and the fluid temperature in the heat transporting channel were analyzed. The effect of radiation and conduction in the semitransparent material was discussed. The result shows that to increase the convective heat transfer coefficient in heat flux channel can enhance the heat transporting ability of the system, but the main parameter to effect on the temperature of the heat transporting system is the area ratio of radiative surfaces. (authors)

  1. Application of heat treatment and hot extrusion processes to improve mechanical properties of the AZ91 alloy

    Directory of Open Access Journals (Sweden)

    T. Reguła

    2010-04-01

    Full Text Available The main aim of this paper is to evaluate the effects of hot working (extrusion and hest treatment on room temperature mechanical properties of magnesium-based AZ91 alloy. The results were compared with as-cast condition. The examined material had been obtained by gravity casting to permanent moulds and subsequently subjected to heat treatment and/or processed by extrusion at 648 K. Microstructural and mechanical properties of properly prepared specimens were studied. Rm, Rp02 and A5 were determined from tensile tests. Brinell hardness tests were also conducted. The research has shown that hot working of AZ91 alloy provides high mechanical properties unattainable by cast material subjected to heat-treatment. The investigated alloy subjected to hot working and subsequently heat-treated has doubled its strength and considerably improved the elongation - compared with the as-cast material.

  2. Analysis of sweeping heat loads on divertor plate materials

    International Nuclear Information System (INIS)

    Hassanein, A.

    1991-01-01

    The heat flux on the divertor plate of a fusion reactor is probably one of the most limiting constraints on its lifetime. The current heat flux profile on the outer divertor plate of a device like ITER is highly peaked with narrow profile. The peak heat flux can be as high as 30--40 MW/m 2 with full width at half maximum (FWHM) is in the order of a few centimeters. Sweeping the separatrix along the divertor plate is one of the options proposed to reduce the thermomechanical effects of this highly peaked narrow profile distribution. The effectiveness of the sweeping process is investigated parametrically for various design values. The optimum sweeping parameters of a particular heat load will depend on the design of the divertor plate as well as on the profile of such a heat load. In general, moving a highly peaked heat load results in substantial reduction of the thermomechanical effects on the divertor plate. 3 refs., 8 figs

  3. Effect of Shortened Heat Treatment on the Hardness and Microstructure of 320.0 Aluminium Alloy

    Directory of Open Access Journals (Sweden)

    Pezda J.

    2014-06-01

    Full Text Available Improvement of Al-Si alloys properties in scope of classic method is connected with change of Si precipitations morphology through: using modification of the alloy, maintaining suitable temperature of overheating and pouring process, as well as perfection of heat treatment methods. Growing requirements of the market make it necessary to search after such procedures, which would quickly deliver positive results with simultaneous consideration of economic aspects. Presented in the paper shortened heat treatment with soaking of the alloy at temperature near temperature of solidus could be assumed as the method in the above mentioned understanding of the problem. Such treatment consists in soaking of the alloy to temperature of solutioning, keeping in such temperature, and next, quick quenching in water (20 °C followed by artificial ageing. Temperature ranges of solutioning and ageing treatments implemented in the adopted testing plan were based on analysis of recorded curves from the ATD method. Obtained results relate to dependencies and spatial diagrams describing effect of parameters of the solutioning and ageing treatments on HB hardness of the investigated alloy and change of its microstructure. Performed shortened heat treatment results in precipitation hardening of the investigated 320.0 alloy, what according to expectations produces increased hardness of the material.

  4. Effect of heat treatment upon the fatigue-crack growth behavior of Alloy 718 weldments

    International Nuclear Information System (INIS)

    Mills, W.J.; James, L.A.

    1981-05-01

    The microstructural features that influenced the room and elevated temperature fatigue-crack growth behavior of as-welded, conventional heat-treated, and modified heat-treated Alloy 718 GTA weldments were studied. Electron fractographic examination of fatigue fracture surfaces revealed that operative fatigue mechanisms were dependent on microstructure, temperatures and stress intensity factor. All specimens exhibited three basic fracture surface appearances at temperatures up to 538 degrees C: crystallographic faceting at low stress intensity range (ΔK) levels, striation, formation at intermediate values, and dimples coupled with striations in the highest (ΔK) regime. At 649 degrees C, the heat-treated welds exhibited extensive intergranular cracking. Laves and δ particles in the conventional heat-treated material nucleated microvoids ahead of the advancing crack front and caused on overall acceleration in crack growth rates at intermediate and high ΔK levels. The modified heat treatment removed many of these particles from the weld zone, thereby improving its fatigue resistance. The dramatically improved fatigue properties exhibited by the as-welded material was attributed to compressive residual stresses introduced by the welding process. 19 refs., 16 figs

  5. Effect of heat treatment on antimycotic activity of Sahara honey

    Directory of Open Access Journals (Sweden)

    Moussa Ahmed

    2014-11-01

    Full Text Available Objective: To evaluate the influence of the temperature on honey colour, polyphenol contents and antimycotic capacity and to evaluate the correlation between these parameters. Methods: Sahara honey were heated up to 25, 50, 75 and 100 °C for 15, 30 and 60 min, and their colour intensity, polyphenol contents and antimycotic capacity. The Folin-Ciocalteu test was used to determine the total polyphenol contents (TPC. The antimycotic activity was evaluated both by agar diffusion method and micro wells dilution method against the Candida albicans (C. albicans and Candida glabrata (C. glabrata. Results: Initial values for TPC in Sahara honey ranged from 0.55 to 1.14 mg of gallic acid per kg of honey, with the average value of 0.78 mg of gallic acid per kg of honey. The TPC values after heat-treatment were 0.54 to 1.54 with the average value of 1.49 mg. The minimal inhibitory concentrations before heat-treatment of Sahara honey against C. albicans and C. glabrata ranged from 3.06%-12.5% and 50% respectively. After heat-treatment the minimal inhibitory concentrations between 12.5% and 50% for C. albicans and C. glabrata, respectively. The diameters of inhibition zones of Sahara honey with 50% concentration varied from (12.67-15.00 mm by C. albicans to (14.33-15.67 mm by C. glabrata. The diameters of inhibition zones after heat-treatment at 25 and 50 °C for 15.30 and 60 min ranged from (2.00-18.67 mm by C. albicans to (8.00-16.67 mm by C. glabrata. Statistically significant relations between the TPC and the colour intensity of Sahara honey (r=0.99, P<0.05. Furthermore, the results showed that the TPC and colour is not correlated with the antimycotic capacity. Conclusions: To our knowledge this is the first report on the antimycotic capacity of Sahara honey.

  6. Survey of postirradiation heat treatment as a means to mitigate radiation embrittlement of reactor vessel steels

    International Nuclear Information System (INIS)

    Hawthorne, J.R.

    1979-01-01

    Nuclear-radiation service typically produces a progressive reduction in the notch ductility of low-alloy steels. The reduction is manifested by a decrease in Charpy-V (Csub(v)) upper-shelf energy level and by an elevation in temperature of the ductile-to-brittle transition. Post irradiation heat treatment (annealing) is being investigated as a method for the reversal of these detrimental radiation effects for reactor-vessel steels. This study was undertaken to analyze factors which could affect annealing response, report data available to qualify suspected influences on annealing, and summarize experimental results generated for many commercially produced reactor materials and companion materials produced in the laboratory

  7. Modeling heat and mass transfer in the heat treatment step of yerba maté processing

    Directory of Open Access Journals (Sweden)

    J. M. Peralta

    2007-03-01

    Full Text Available The aim of this research was to estimate the leaf and twig temperature and moisture content of yerba maté branches (Ilex paraguariensis Saint Hilaire during heat treatment, carried out in a rotary kiln dryer. These variables had to be estimated (modeling the heat and mass transfer due to the difficulty of experimental measurement in the dryer. For modeling, the equipment was divided into two zones: the flame or heat treatment zone and the drying zone. The model developed fit well with the experimental data when water loss took place only in leaves. In the first zone, leaf temperature increased until it reached 135°C and then it slowly decreased to 88°C at the exit, despite the gas temperature, which varied in this zone from 460°C to 120°C. Twig temperature increased in the two zones from its inlet temperature (25°C up to 75°C. A model error of about 3% was estimated based on theoretical and experimental data on leaf moisture content.

  8. Applicability of Solid Solution Heat Treatments to Aluminum Foams

    Directory of Open Access Journals (Sweden)

    Miguel Rodríguez-Pérez

    2012-12-01

    Full Text Available Present research work evaluates the influence of both density and size on the treatability of Aluminum-based (6000 series foam-parts subjected to a typical solid solution heat treatment (water quenching. The results are compared with those obtained for the bulk alloy, evaluating the fulfilment of cooling requirements. Density of the foams was modeled by tomography analysis and the thermal properties calculated, based on validated density-scaled models. With this basis, cooling velocity maps during water quenching were predicted by finite element modeling (FEM in which boundary conditions were obtained by solving the inverse heat conduction problem. Simulations under such conditions have been validated experimentally. Obtained results address incomplete matrix hardening for foam-parts bigger than 70 mm in diameter with a density below 650 kg/m3. An excellent agreement has been found in between the predicted cooling maps and final measured microhardness profiles.

  9. Advanced Thermoelectric Materials for Efficient Waste Heat Recovery in Process Industries

    Energy Technology Data Exchange (ETDEWEB)

    Adam Polcyn; Moe Khaleel

    2009-01-06

    The overall objective of the project was to integrate advanced thermoelectric materials into a power generation device that could convert waste heat from an industrial process to electricity with an efficiency approaching 20%. Advanced thermoelectric materials were developed with figure-of-merit ZT of 1.5 at 275 degrees C. These materials were not successfully integrated into a power generation device. However, waste heat recovery was demonstrated from an industrial process (the combustion exhaust gas stream of an oxyfuel-fired flat glass melting furnace) using a commercially available (5% efficiency) thermoelectric generator coupled to a heat pipe. It was concluded that significant improvements both in thermoelectric material figure-of-merit and in cost-effective methods for capturing heat would be required to make thermoelectric waste heat recovery viable for widespread industrial application.

  10. Complex use of waste in wastewater and circulating water treatment from oil in heat power stations

    Science.gov (United States)

    Nikolaeva, L. A.; Iskhakova, R. Ya.

    2017-06-01

    Sewage and circulating water from oil of thermal power plants (TPP) generated in fuel-oil shops during washing of electrical equipment and its running into the storm drainage system from the industrial site has been considered in the paper. It has been suggested to use the carbonate sludge of water treatment modified with hydrophobing emulsion as a sorption material for waste and circulating water treatment in thermal power plants. The carbonate sludge is waste accumulated in clarifiers at the stage of natural water pretreatment. General technical characteristics of the sludge, such as moisture, bulk density, total pore volume, ash, etc., have been determined. It has been found that the sludge without additional treatment is a hydrophilic material that has low adsorption capacity and wettability with nonpolar compounds. Therefore, the sludge is treated with organosilicon compounds to reduce the moisture capacity and increase its floatation. Several types of sorption materials based on the carbonate sludge subjected to surface and volume hydrophobization have been developed. During the volume treatment, the hydrophobing compound has been introduced into the material along with the plastifier. In case of the surface treatment, heat-treated granules have been soaked into hydrophobing emulsion. It has been shown that surface hydrophobization is most economically advantageous, because it reduces the consumption of water-repelling agent, wherein the total pore volume and sorption capacity during surface hydrophobization increase by 45 and 25% compared to that during volume hydrophobization. Based on the obtained results, the most effective sorption material has been chosen. To produce this material, it is necessary to sequentially carry out mixing of carbonate sludge with the binder, granulation, calcination, impregnation with a waterrepellent emulsion, and drying of the finished material. The suggested technology to produce the material and use it as a sorbent allows

  11. Effect of grain orientation and heat treatment on mechanical properties of pure W

    Energy Technology Data Exchange (ETDEWEB)

    Noto, Hiroyuki, E-mail: noto_hiroyuki@iae.kyoto-u.ac.jp [Graduate School of Energy Science, Kyoto University, Kyoto 611-0011 (Japan); Research Fellow of Japan Society for the Promotion of Science (Japan); Taniguchi, Shuichi [Graduate School of Energy Science, Kyoto University, Kyoto 611-0011 (Japan); Kurishita, Hiroaki; Matsuo, Satoru [International Research Center for Nuclear Materials Science, Institute for Materials Research, Tohoku University, Oarai, Ibaraki 311-1313 (Japan); Ukita, Takashi; Tokunaga, Kazutoshi [Institute for Applied Mechanics, Kyushu University, Kasuga, Fukuoka 816-8580 (Japan); Kimura, Akihiko [Institute of Advanced Energy, Kyoto University, Kyoto 611-0011 (Japan)

    2014-12-15

    The effect of grain orientation, heat-treatment temperature and test temperature on the mechanical properties of tungsten (W), which vary depending on plastic working and fabrication process, was investigated by mechanical testing of tensile or bending. Heavily worked W samples (1.5–2.0 mm in the final thickness) exhibit degradation of fracture strength due to recrystallization embrittlement after heat-treatment at 1240 °C (temperature of diffusion bonding between W and a candidate material of the Fe base support structure). On the other hand, W samples with lower thickness reduction rates do not suffer degradation of fracture strength after heating up to around 1300 °C, and show somewhat higher fracture strength by heat-treatment below 1300 °C than the samples in the as-received state. The observed behavior is a reflection of recovery of dislocations introduced by plastic working. High temperature tensile testing of ITER grade W with an anisotropic grain structure and S-TUN with an equiaxed grain structure revealed that both W grades exhibit plastic elongation at temperatures higher than 200 °C with essentially the same temperature dependence of yield strength, which is relatively insensitive to grain orientation in the structure at 200–1300 °C.

  12. Effect of grain orientation and heat treatment on mechanical properties of pure W

    International Nuclear Information System (INIS)

    Noto, Hiroyuki; Taniguchi, Shuichi; Kurishita, Hiroaki; Matsuo, Satoru; Ukita, Takashi; Tokunaga, Kazutoshi; Kimura, Akihiko

    2014-01-01

    The effect of grain orientation, heat-treatment temperature and test temperature on the mechanical properties of tungsten (W), which vary depending on plastic working and fabrication process, was investigated by mechanical testing of tensile or bending. Heavily worked W samples (1.5–2.0 mm in the final thickness) exhibit degradation of fracture strength due to recrystallization embrittlement after heat-treatment at 1240 °C (temperature of diffusion bonding between W and a candidate material of the Fe base support structure). On the other hand, W samples with lower thickness reduction rates do not suffer degradation of fracture strength after heating up to around 1300 °C, and show somewhat higher fracture strength by heat-treatment below 1300 °C than the samples in the as-received state. The observed behavior is a reflection of recovery of dislocations introduced by plastic working. High temperature tensile testing of ITER grade W with an anisotropic grain structure and S-TUN with an equiaxed grain structure revealed that both W grades exhibit plastic elongation at temperatures higher than 200 °C with essentially the same temperature dependence of yield strength, which is relatively insensitive to grain orientation in the structure at 200–1300 °C

  13. Effects of heat treatment on some physical properties of Douglas fir (Pseudotsuga menziesii) wood

    Science.gov (United States)

    Xianjun Li; Zhiyong Cai; Qunying Mou; Yiqiang Wu; Yuan Liu

    2011-01-01

    In this study the effect of heat treatment on some physical properties of Douglas fir (Pseudotsuga menziesii) was investigated. Wood specimens were subjected to heat treatment at 160, 180, 200 and 220°C for 1, 2, 3 and 4h. The results show that heat treatment resulted in a darkened color, decreased moisture performance and increased dimensional stability of...

  14. Influence of heat treatment on the high temperature oxidation mechanisms of an Fe-TiCN cermet

    OpenAIRE

    Alvaredo Olmos, Paula; Abajo Clemente, Carolina; Tsipas, Sophia Alexandra; Gordo Odériz, Elena

    2014-01-01

    In this study, the oxidation behaviour of an iron matrix cermet containing 50 % vol. Ti(C,N) was investigated before and after heat treatment by oxidation tests performed in static air at temperatures between 500 °C and 1000 °C. The oxidation mechanism for this type of composite materials was established and it was found that the heat treated material presents lower mass gain than the as-sintered material at the early stages of the oxidation, due to the volatilization of oxides. The oxidation...

  15. Study on the application of thickened welds without post weld heat treatment for containment vessels

    International Nuclear Information System (INIS)

    Takeuchi, T.; Fukaya, T.; Sato, M.; Takano, G.

    1978-01-01

    As material for containment vessels, SGV49 steel plates are mainly used. However, those used for this purpose are limited in thickness to smaller than 38 mm. This is because the present standard requires welds thicker than 38 mm to be subjected to post weld heat treatment but operation on the site is practically difficult. In the case of 3-loop containment vessels of pressurized water type reactors, use of 38 mm SGV49 brings an increase in their height and this is disadvantageous from a seismic viewpoint. Therefore, use of 45 mm-thick steel material has become necessary in order to increase design internal pressure and reduce the height of the vessels. To investigate the propriety of the use of 45 mm-thick SGV49 for this purpose without post weld heat treatment we investigated the basic performances of base metal and welded joints. We also conducted large-scale embrittlement fracture tests (CT test, deep notch test, wide plate tensile test and ESSO test) in order to examine whether welds not subjected to post weld heat treatment are safe against embrittlement fracture under the operating conditions of the vessels. The results proved that the welds of SGV49 steel plates are safe enough under the operating conditions. (author)

  16. Development of drying equipment for heat sensitive material : final report

    Energy Technology Data Exchange (ETDEWEB)

    Schoenau, G.J.; Sokhansanj, S. [Saskatchewan Univ., Saskatoon, SK (Canada)

    2003-07-01

    This paper described a project in which two types of prototype heat pump dryer systems were designed, constructed and field tested in 2000 to 2002. Performance testing was accomplished through a computer based simulation model for predicting dryer performance. The paper describes the procedures followed and the results obtained. The dryer is used for high value specialty crops such as ginseng, herbs and echinacea which require low temperature drying. The heat pump dryer operates under a closed loop and can dry these crops at low temperatures, independent of ambient conditions. The first prototype was a small fixed bed cabinet dryer suitable for small growers. The other was a full scale prototype moving bed cross flow system suitable for large scale commercial drying of sensitive agricultural crops. The heat pump system is faster and more energy efficient than conventional dryers. The average moisture content of ginseng roots was reduced by 10 per cent in 5 days using 190 kWh of energy. The heat pump dryer is 22 per cent more efficient than a conventional dryer due to its recirculating system. Drying time is reduced by 65 per cent. A computerized simulation validated experimental results. 30 refs., 10 tabs., 29 figs.

  17. Optimization of properties of parts in the heat treatment

    International Nuclear Information System (INIS)

    Shpis, Kh.I.

    1981-01-01

    Properties of parts of the improved steel depending considerably on the structure obtained after the tempering have been investigated. It is shown that in many cases properties of steel with the structure of the tempered lower bainite are no worse than the properties of steels with the structure of tempered martensite. At certain dimensions of parts and under certain conditions of cooling tempering degree is determined with calcination. Calcination of steel is evaluated by the dispersion bands of hardness obtained using the method of end quenching. Account of the calcination when steels are selected permits to optimize part properties during heat treatment [ru

  18. COMPUTERIZED HEAT-TREATMENT IN A ZIMBABWEAN FACTORY

    Directory of Open Access Journals (Sweden)

    M. Collier

    2012-01-01

    Full Text Available In the context of Zimbabwe's current economic problems, parts of the manufacturing industry are turning their attention to the possibility of utilising local design talent in upgrading their manufacturing plants. This paper describes a project undertaken by the National University of Science and Technology to convert the heat-treatment process in a major manufacturing plant from semi -manual to a computerized one. The system comprises microcontroller connection to the furnaces and sensors, and communicates with a central computer on which software for a windowed user-interface is hosted. Experimental results for the system are presented, and a strategy for other companies in the same predicament is proposed.

  19. Feasibility of using phase change materials to control the heat of hydration in massive concrete structures.

    Science.gov (United States)

    Choi, Won-Chang; Khil, Bae-Soo; Chae, Young-Seok; Liang, Qi-Bo; Yun, Hyun-Do

    2014-01-01

    This paper presents experimental results that can be applied to select a possible phase change material (PCM), such as a latent heat material (LHM), to control the hydration heat in mass concrete structures. Five experimental tests (microconduction, simplified adiabatic temperature rise, heat, and compressive strength tests) were conducted to select the most desirable LHM out of seven types of inorganic PCM used in cement mortar and to determine the most suitable mix design. The results of these experimental tests were used to assess the feasibility of using PCM to reduce hydration heat in mass concrete that was examined. The experimental results show that cement mortar containing barium- [Ba(OH)2 · 8H2O] based PCM has the lowest amount of total hydration heat of the cement pastes. The barium-based PCM provides good latent heat properties that help to prevent volume change and microcracks caused by thermal stress in mass concrete.

  20. Feasibility of Using Phase Change Materials to Control the Heat of Hydration in Massive Concrete Structures

    Directory of Open Access Journals (Sweden)

    Won-Chang Choi

    2014-01-01

    Full Text Available This paper presents experimental results that can be applied to select a possible phase change material (PCM, such as a latent heat material (LHM, to control the hydration heat in mass concrete structures. Five experimental tests (microconduction, simplified adiabatic temperature rise, heat, and compressive strength tests were conducted to select the most desirable LHM out of seven types of inorganic PCM used in cement mortar and to determine the most suitable mix design. The results of these experimental tests were used to assess the feasibility of using PCM to reduce hydration heat in mass concrete that was examined. The experimental results show that cement mortar containing barium- [Ba(OH2·8H2O] based PCM has the lowest amount of total hydration heat of the cement pastes. The barium-based PCM provides good latent heat properties that help to prevent volume change and microcracks caused by thermal stress in mass concrete.

  1. Microwave heating of electric cable insulated wires before their impregnation with a hydrophobic material

    Energy Technology Data Exchange (ETDEWEB)

    Niculae, D; Mihailescu, A [Romanian Electricity Authority (Romania); Indreias, I; Martin, D [Institute of Atomic Physics, Bucharest (Romania); Margaritescu, A [ICPE Electrostatica, Bucharest, (Romania); Zlatonovici, D

    1998-12-31

    Underground insulated telecommunication cables must be impregnated with a hydrophobic material in order to prevent water penetration damage. To do so, the cable wire bundle must be heated to a temperature of 60 to 90 degrees C to ensure proper fluidity of the hydrophobic material that must fill the free spaces between the copper wires of the telephone cable. This paper described the microwave heating method of the wires before their impregnation. A cylindrical applicator was designed to perform a telephone bundle heating test. 800 W of microwave power were used on a telephone cable made up of 800 wires of 0.4 mm in diameter. A uniform heating was obtained throughout the section. Microwave heating was also found to be 53 per cent more energy efficient than hot air heating. 4 refs., 4 figs.

  2. On the material properties of shell plate formed by line heating

    Directory of Open Access Journals (Sweden)

    Hyung Kyun Lim

    2017-01-01

    Full Text Available This paper is concerned with investigating the plastic material properties of steel plate formed by line heating method, and is aimed at implementing more rational design considering the accidental limit states such as collision or grounding. For the present study, line heating test for marine grade steel plate has been carried out with varying plate thickness and heating speed, and then microscopic examination and tensile test have been carried out. From the microscopic, it is found that the grain refined zones like ferrite and pearlite are formed all around the heat affected zone. From the tensile test results, it is seen that yield strength, tensile strength, fracture strain, hardening exponent and strength coefficient vary with plate thickness and heat input quantity. The formulae relating the material properties and heat input parameter should be, therefore, derived for the design purpose considering the accidental impact loading. This paper ends with describing the extension of the present study.

  3. Vanadium and heat treatments effect on elastic characteristics of niobium

    International Nuclear Information System (INIS)

    Vasil'eva, E.V.; Tret'yakov, V.I.; Prokoshkin, D.A.; Pustovalov, V.A.

    1975-01-01

    The effect of vanadium content and of heat treatment conditions on the elastic properties of niobium at temperatures of 20 to 800 deg C was studied. Nb-V alloys were produced by binary vacuum remelting. The Nb-V alloys have been then subjected to thermal treatment. The total degree of deformation amounts to about 95%. The specimens were tested with a view to determine their microhardness, specific electric resistance, elasticity limit and modulus of elasticity. The elastic limit of niobium rises when alloyed with vanadium. With the increase of vanadium content the elastic limit of the alloy becomes greater. Pre-crystallization annealing at 600 - 700 deg C considerably increases the elastic limit, which is explained by development of the thermally activated processes leading to a decrease of dislocation mobility and thereby to a strengthening of the alloy

  4. Beta dosimetry using pulsed laser heating of TLD materials

    International Nuclear Information System (INIS)

    Quam, W.

    1983-01-01

    Use of a pulsed CO 2 laser to heat the surface of hot-pressed LiF chips has been investigated. The thermoluminescent traps in the first 10 to 20 μm of depth may be read out with good efficiency, which will allow entrance dose and exit dose to be determined using a standard chip. These dose data can be used to calculate beta dose and gamma dose separately. Readout speed is estimated to be a few milliseconds per chip

  5. Hierarchical Cu precipitation in lamellated steel after multistage heat treatment

    Science.gov (United States)

    Liu, Qingdong; Gu, Jianfeng

    2017-09-01

    The hierarchical distribution of Cu-rich precipitates (CRPs) and related partitioning and segregation behaviours of solute atoms were investigated in a 1.54 Cu-3.51 Ni (wt.%) low-carbon high-strength low-alloy (HSLA) steel after multistage heat treatment by using the combination of electron backscatter diffraction (EBSD), transmission electron microscopy (TEM) and atom probe tomography (APT). Intercritical tempering at 725 °C of as-quenched lathlike martensitic structure leads to the coprecipitation of CRPs at the periphery of a carbide precipitate which is possibly in its paraequilibrium state due to distinct solute segregation at the interface. The alloyed carbide and CRPs provide constituent elements for each other and make the coprecipitation thermodynamically favourable. Meanwhile, austenite reversion occurs to form fresh secondary martensite (FSM) zone where is rich in Cu and pertinent Ni and Mn atoms, which gives rise to a different distributional morphology of CRPs with large size and high density. In addition, conventional tempering at 500 °C leads to the formation of nanoscale Cu-rich clusters in α-Fe matrix. As a consequence, three populations of CRPs are hierarchically formed around carbide precipitate, at FSM zone and in α-Fe matrix. The formation of different precipitated features can be turned by controlling diffusion pathways of related solute atoms and further to tailor mechanical properties via proper multistage heat treatments.

  6. Fast nanoscale heat-flux modulation with phase-change materials

    OpenAIRE

    Van Zwol , Pieter; Joulain , Karl; Ben-Abdallah , Philippe; Greffet , Jean-Jacques; Chevrier , Joël

    2011-01-01

    International audience; We introduce a new concept for electrically controlled heat flux modulation. A flux contrast larger than 10 dB is expected with switching time on the order of tens of nanoseconds. Heat flux modulation is based on the interplay between radiative heat transfer at the nanoscale and phase change materials. Such large contrasts are not obtainable in solids, or in far field. As such this opens up new horizons for temperature modulation and actuation at the nanoscale.

  7. Experiment of forced convection heat transfer using microencapsulated phase-change-material slurries

    International Nuclear Information System (INIS)

    Kubo, Shinji; Akino, Norio; Tanaka, Amane; Nagashima, Akira.

    1997-01-01

    The present study describes an experiment on forced convective heat transfer using a water slurry of Microencapsulated Phase-change-material. A normal paraffin hydrocarbon is microencapsulated by melamine resin, melting point of 28.1degC. The heat transfer coefficient and pressure drop in a circular tube were evaluated. The heat transfer coefficient using the slurry in case with and without phase change were compared to in case of using pure water. (author)

  8. Modernization and efficiency of heat treatment and heating up plants; Modernisierung und Effizienz von Thermoprozessanlagen

    Energy Technology Data Exchange (ETDEWEB)

    Wendt, Peter [LOI Thermprocess GmbH, Essen (Germany); Kuehn, Friedhelm [Ingenieurbuero fuer Waermebehandlung, Industrieoefen und Energieberatung, Muelheim (Germany)

    2010-10-15

    A goal of this contribution is to show, using examples of the thermal heat treatment industry and the thermal processing units used there (Beltype plants, routary hearth, walking hearth, walking beam, pusher type furnaces and gas carburizing plants as well as case hardening plants), which increases in efficiency within and outside of the actual thermal treatment process and the necessary thermal processing units for the order are available today. From the possibilities of the reduction of energy employment resulting from that, a high potential for the discharge of the environment can be derived. The economic effect concerning energy employment and saving possibilities will also be considered. Concluding, examples of case-hardening show which variants of a change of process present themselves partially in the future, in order to achieve substantial production increases and thus energy cost reductions. (orig.)

  9. Acoustoelastic evaluation of welding and heat treatment stress relieving of pressure vessel steel for Angra 3

    Energy Technology Data Exchange (ETDEWEB)

    Moraes, Bruno C. de, E-mail: bruno.cesar@nuclep.gov.br [Nuclebras Equipamentos Pesados S.A (NUCLEP), Itaguai, RJ (Brazil); Bittencourt, Marcelo de S.Q., E-mail: bruno.cesar@nuclep.gov.br, E-mail: bittenc@ien.gov.br [Instituto de Engenharia Nuclear (IEN/CNEN-RJ), Rio de Janeiro, RJ (Brazil)

    2015-07-01

    Currently the knowledge of non-destructive techniques allows to evaluate the stresses on components and mechanical structures, aiming at physical security, preservation of the environment and avoid financial losses associated with the construction and operation of industrial plants. The search for new techniques, especially applied in the nuclear industry to assess status more accurately, voltage safety and to ensure structural integrity, for example, core components of the primary circuit, such as the reactor pressure vessel and steam generator has become of great importance within the community of non-destructive testing .This paper aims to contribute to the non-destructive technique development in order to ensure the structural integrity of nuclear components. One acoustoelastic evaluation of steel 20 MnMoNi 55, used in pressure vessels of nuclear power plants were performed. The acoustic birefringence technique was use to evaluate the acoustoelastic behavior of the test material in the as received condition, after welding and after the stress relief heat treatment. The constant acoustoelastic material was obtained by an uniaxial loading test. It was found a slight anisotropy in the material as received. After welding, a marked variation of acoustic birefringence in the region near the weld bead was observed. The heat treatment indicated a new change of acoustic birefringence. Obtaining the acoustoelastic constant allowed the evaluation of stress in the different conditions of the weld and treated material. (author)

  10. Acoustoelastic evaluation of welding and heat treatment stress relieving of pressure vessel steel for Angra 3

    International Nuclear Information System (INIS)

    Moraes, Bruno C. de; Bittencourt, Marcelo de S.Q.

    2015-01-01

    Currently the knowledge of non-destructive techniques allows to evaluate the stresses on components and mechanical structures, aiming at physical security, preservation of the environment and avoid financial losses associated with the construction and operation of industrial plants. The search for new techniques, especially applied in the nuclear industry to assess status more accurately, voltage safety and to ensure structural integrity, for example, core components of the primary circuit, such as the reactor pressure vessel and steam generator has become of great importance within the community of non-destructive testing .This paper aims to contribute to the non-destructive technique development in order to ensure the structural integrity of nuclear components. One acoustoelastic evaluation of steel 20 MnMoNi 55, used in pressure vessels of nuclear power plants were performed. The acoustic birefringence technique was use to evaluate the acoustoelastic behavior of the test material in the as received condition, after welding and after the stress relief heat treatment. The constant acoustoelastic material was obtained by an uniaxial loading test. It was found a slight anisotropy in the material as received. After welding, a marked variation of acoustic birefringence in the region near the weld bead was observed. The heat treatment indicated a new change of acoustic birefringence. Obtaining the acoustoelastic constant allowed the evaluation of stress in the different conditions of the weld and treated material. (author)

  11. Heart rate variability during exertional heat stress: effects of heat production and treatment.

    Science.gov (United States)

    Flouris, Andreas D; Bravi, Andrea; Wright-Beatty, Heather E; Green, Geoffrey; Seely, Andrew J; Kenny, Glen P

    2014-04-01

    We assessed the efficacy of different treatments (i.e., treatment with ice water immersion vs. natural recovery) and the effect of exercise intensities (i.e., low vs. high) for restoring heart rate variability (HRV) indices during recovery from exertional heat stress (EHS). Nine healthy adults (26 ± 3 years, 174.2 ± 3.8 cm, 74.6 ± 4.3 kg, 17.9 ± 2.8 % body fat, 57 ± 2 mL·kg·(-1) min(-1) peak oxygen uptake) completed four EHS sessions incorporating either walking (4.0-4.5 km·h(-1), 2 % incline) or jogging (~7.0 km·h(-1), 2 % incline) on a treadmill in a hot-dry environment (40 °C, 20-30 % relative humidity) while wearing a non-permeable rain poncho for a slow or fast rate of rectal temperature (T re) increase, respectively. Upon reaching a T re of 39.5 °C, participants recovered until T re returned to 38 °C either passively or with whole-body immersion in 2 °C water. A comprehensive panel of 93 HRV measures were computed from the time, frequency, time-frequency, scale-invariant, entropy and non-linear domains. Exertional heat stress significantly affected 60/93 HRV measures analysed. Analyses during recovery demonstrated that there were no significant differences between HRV measures that had been influenced by EHS at the end of passive recovery vs. whole-body cooling treatment (p > 0.05). Nevertheless, the cooling treatment required statistically significantly less time to reduce T re (p whole-body immersion in 2 °C water results in faster cooling, there were no observed differences in restoration of autonomic heart rate modulation as measured by HRV indices with whole-body cold-water immersion compared to passive recovery in thermoneutral conditions.

  12. Advanced construction materials for thermo-chemical hydrogen production from VHTR process heat

    International Nuclear Information System (INIS)

    Kosmidou, Theodora; Haehner, Peter

    2009-01-01

    The (very) high temperature reactor concept ((V)HTR) is characterized by its potential for process heat applications. The production of hydrogen by means of thermo-chemical cycles is an appealing example, since it is more efficient than electrolysis due to the direct use of process heat. The sulfur-iodine cycle is one of the best studied processes for the production of hydrogen, and solar or nuclear energy can be used as a heating source for the high temperature reaction of this process. The chemical reactions involved in the cycle are: I 2 (l) + SO 2 (g) +2 H 2 O (l) → 2HI (l) + H 2 SO 4 (l) (70-120 deg. C); H 2 SO 4 (l) → H 2 O (l) + SO 2 (g) + 1/2 O 2 (g) (800-900 deg. C); 2HI (l) → I 2 (g) + H 2 (g) (300-450 deg. C) The high temperature decomposition of sulphuric acid, which is the most endothermic reaction, results in a very aggressive chemical environment which is why suitable materials for the decomposer heat exchanger have to be identified. The class of candidate materials for the decomposer is based on SiC. In the current study, SiC based materials were tested in order to determine the residual mechanical properties (flexural strength and bending modulus, interfacial strength of brazed joints), after exposure to an SO 2 rich environment, simulating the conditions in the hydrogen production plant. Brazed SiC specimens were tested after 20, 100, 500 and 1000 hrs exposure to SO 2 rich environment at 850 o C under atmospheric pressure. The gas composition in the corrosion rig was: 9.9 H 2 O, 12.25 SO 2 , 6.13 O 2 , balance N 2 (% mol). The characterization involved: weight change monitoring, SEM microstructural analysis and four-point bending tests after exposure. Most of the specimens gained weight due to the formation of a corrosion layer as observed in the SEM. The corrosion treatment also showed an effect on the mechanical properties. In the four-point bending tests performed at room temperature and at 850 deg. C, a decrease in bending modulus with

  13. Influence of Wind Speed on Heat Flow through Polypropylene Insulating Material

    Institute of Scientific and Technical Information of China (English)

    SUN Yu-chai; CHENG Zhong-hao; FENG Xun-wei

    2006-01-01

    The heat transfer properties of polypropylene insulation at different ambient temperature against wind were analysed.A theoretical model of the combined conductive, convective and radiative heat flow through fibrous insulating material was presented. Detail study was carried out by using the finite element method. The theoretical results are in accordance to the experimental results which were accomplished in an artificial climate chamber.

  14. INVESTIGATION OF HEAT CONDUCTION AND SPECIFIC ELECTRIC IMPEDANCE OF POROUS MATERIALS

    Directory of Open Access Journals (Sweden)

    E. S. Golubtsova

    2004-01-01

    Full Text Available In this article there was investigated the influence of porosity and temperature change on heat condition and electrical resistance of porous iron (PZh4M nickel and steel 14X17H2. There are received the adequate equations of regression, establishing connection between heat conduction and electrical resistance of the investigated materials with their porosity and temperature.

  15. Decay heat measurement on fusion reactor materials and validation of calculation code system

    Energy Technology Data Exchange (ETDEWEB)

    Maekawa, Fujio; Ikeda, Yujiro; Wada, Masayuki [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment

    1998-03-01

    Decay heat rates for 32 fusion reactor relevant materials irradiated with 14-MeV neutrons were measured for the cooling time period between 1 minute and 400 days. With using the experimental data base, validity of decay heat calculation systems for fusion reactors were investigated. (author)

  16. Coupled DQ-FE methods for two dimensional transient heat transfer analysis of functionally graded material

    Energy Technology Data Exchange (ETDEWEB)

    Golbahar Haghighi, M.R.; Eghtesad, M. [Department of Mechanical Engineering, School of Engineering, Shiraz University, Shiraz 71348-51154 (Iran, Islamic Republic of); Malekzadeh, P. [Department of Mechanical Engineering, School of Engineering, Persian Gulf University, Boushehr 75169-13798 (Iran, Islamic Republic of)], E-mail: malekzadeh@pgu.ac.ir

    2008-05-15

    In this paper, a mixed finite element (FE) and differential quadrature (DQ) method as a simple, accurate and computationally efficient numerical tool for two dimensional transient heat transfer analysis of functionally graded materials (FGMs) is developed. The method benefits from the high accuracy, fast convergence behavior and low computational efforts of the DQ in conjunction with the advantages of the FE method in general geometry, loading and systematic boundary treatment. Also, the boundary conditions at the top and bottom surfaces of the domain can be implemented more precisely and in strong form. The temporal derivatives are discretized using an incremental DQ method (IDQM), whose numerical stability is not sensitive to time step size. The effects of non-uniform convective-radiative conditions on the boundaries are investigated. The accuracy of the proposed method is demonstrated by comparing its results with those available in the literature. It is shown that using few grid points, highly accurate results can be obtained.

  17. Heat-processing method and facility for helium-containing metal material

    International Nuclear Information System (INIS)

    Kato, Takahiko; Kodama, Hideyo; Matsumoto, Toshimi; Aono, Yasuhisa; Nagata, Tetsuya; Hattori, Shigeo; Kaneda, Jun-ya; Ono, Shigeki.

    1996-01-01

    Electric current is supplied to an objective portion of a He-containing metal material to be applied with heat processing without causing melting, to decrease the He content of the portion. Subsequently, the defect portion of the tissues of the He-containing metal is modified by heating the portion with melting. Since electric current can be supplied to the metal material in a state where the metal material is heated and the temperature thereof is elevated, an effect of further reducing the He content can be obtained. Further, if the current supply and/or the heating relative to the metal material is performed in a vacuum or inert gas atmosphere, an effect of reducing the degradation of the surface of the objective portion to be supplied with electric current can be obtained. (T.M.)

  18. Experimental study on method for heat transfer enhancement using a porous material

    International Nuclear Information System (INIS)

    Shimura, Takuya; Takeda, Tetsuaki

    2011-01-01

    There are several methods for enhancement of heat transfer; for example, there are attaching various fins on the heat transfer surface, processing the surface roughly, and so on. When cooling high temperature circular or rectangular channels by forced convection of gas, there are several methods for enhancement of heat transfer such as attaching radial or spiral fins on the channel surface or inserting twisted tape in the channel. In the case of the gas heating type steam reformer, disk type fins are attached on the outside surface of the reformer tube, and the tube is inserted into the guide tube to increase an amount of heat transferred from the high temperature gas. However, it has to take into consideration the deterioration of the structure strength by attaching the fins on the tube surface with the design of the steam reformer. The objective of this study is to clarify performances of a method for heat transfer enhancement using porous material with high porosity. The experiment has been performed using an apparatus which simulated the passage structure of the steam reformer to obtain characteristics of heat transfer and pressure drop. From the results obtained in this experiment, the heat transfer rate by this method showed a good performance in the laminar flow region. It was also found that the method for heat transfer enhancement using porous material with high porosity is further improved under the high temperature condition as compared with the other methods for heat transfer enhancement. (author)

  19. Effects of the Solid Solution Heat Treatment on the Corrosion Resistance Property of SSC13 Cast Alloy

    Energy Technology Data Exchange (ETDEWEB)

    Kim, Kuk-Jin [Hi-Sten Co., Ltd., Gimhae (Korea, Republic of); Lim, Su Gun [Gyeongsang National University, Jinju (Korea, Republic of); Pak, S. J. [Gachon BioNano Research Institute, Gachon University, Sungnam (Korea, Republic of)

    2015-04-15

    Recently, Stainless steels have been increasingly selected as the fitting or the valve materials of water pipes as the human health issue is getting higher and higher. Therefore, the connectors attached at pipes to deliver water are exposed to more severe environments than the pipes because crevice or galvanic corrosion is apt to occur at the fittings or the valves. Effects of the solid solution annealing, cooling rate after this heat treatment, and passivation on the corrosion properties of the shell mold casted SSC13 (STS304 alloy equivalent) were studied. The heating and quenching treatment more or less reduced hardness but effectively improved corrosion resistance. It was explained by the reduction of delta ferrite contents. Independent of heat treatment, the chemical passivation treatment also lowered corrosion rate but the improvement of corrosion resistance depended on temperature and time for passivation treatment indicating that the optimum conditions for passivation treatment were the bath temperature of 34 .deg. C and operating time of 10 minutes. Therefore it is suggested that the corrosion resistance of SSC13 can be effectively improved with the heat treatment, where SSC13 is heated for 10 minutes at 1120 °C and quenched and passivation treatment, where SSC13 is passivated for at least 10 seconds at 34 °C nitric acid solution.

  20. Thermochemical Storage of Middle Temperature Wasted Heat by Functionalized C/Mg(OH2 Hybrid Materials

    Directory of Open Access Journals (Sweden)

    Emanuela Mastronardo

    2017-01-01

    Full Text Available For the thermochemical performance implementation of Mg(OH2 as a heat storage medium, several hybrid materials have been investigated. For this study, high-performance hybrid materials have been developed by exploiting the authors’ previous findings. Expanded graphite (EG/carbon nanotubes (CNTs-Mg(OH2 hybrid materials have been prepared through Mg(OH2 deposition-precipitation over functionalized, i.e., oxidized, or un-functionalized EG or CNTs. The heat storage performances of the carbon-based hybrid materials have been investigated through a laboratory-scale experimental simulation of the heat storage/release cycles, carried out by a thermogravimetric apparatus. This study offers a critical evaluation of the thermochemical performances of developed materials through their comparison in terms of heat storage and output capacities per mass and volume unit. It was demonstrated that both EG and CNTs improves the thermochemical performances of the storage medium in terms of reaction rate and conversion with respect to pure Mg(OH2. With functionalized EG/CNTs-Mg(OH2, (i the potential heat storage and output capacities per mass unit of Mg(OH2 have been completely exploited; and (ii higher heat storage and output capacities per volume unit were obtained. That means, for technological applications, as smaller volume at equal stored/released heat.

  1. Structural materials for high-heat flux applications

    International Nuclear Information System (INIS)

    Rybin, V.V.; Smith, D.L.

    1991-01-01

    The structural materials for the ITER, (International Thermonuclear Experimental Reactor) divertor must perform reliably under complex and diverse operating requirements. Only a limited number of materials offer a potential for meeting these requirements for the wide temperature range of interest. The candidate materials considered in the ITER design activity include copper, molybdenum, niobium alloys. Molybdenum alloys being considered include dilute alloys of the TZM type and the Mo-Re system. Niobium alloys under consideration include Nb-V-Zr and Nb-Zr systems. Copper alloys being considered include precipitation strengthened alloys of the Glidcop and MAGT type, alloys of Cu-Mo system and dispersion hardened bronzes. The projected operating conditions for the ITER divertor and the criteria for evaluating the candidate materials are reviewed. This paper summarizes the data base and presents recent experimental results on these candidate divertor structural alloys

  2. New method of processing heat treatment experiments with numerical simulation support

    Science.gov (United States)

    Kik, T.; Moravec, J.; Novakova, I.

    2017-08-01

    In this work, benefits of combining modern software for numerical simulations of welding processes with laboratory research was described. Proposed new method of processing heat treatment experiments leading to obtaining relevant input data for numerical simulations of heat treatment of large parts was presented. It is now possible, by using experiments on small tested samples, to simulate cooling conditions comparable with cooling of bigger parts. Results from this method of testing makes current boundary conditions during real cooling process more accurate, but also can be used for improvement of software databases and optimization of a computational models. The point is to precise the computation of temperature fields for large scale hardening parts based on new method of temperature dependence determination of the heat transfer coefficient into hardening media for the particular material, defined maximal thickness of processed part and cooling conditions. In the paper we will also present an example of the comparison standard and modified (according to newly suggested methodology) heat transfer coefficient data’s and theirs influence on the simulation results. It shows how even the small changes influence mainly on distribution of temperature, metallurgical phases, hardness and stresses distribution. By this experiment it is also possible to obtain not only input data and data enabling optimization of computational model but at the same time also verification data. The greatest advantage of described method is independence of used cooling media type.

  3. ADVANCED CERAMIC MATERIALS FOR DENTAL APPLICATIONS SINTERED BY MICROWAVE HEATING

    OpenAIRE

    Presenda Barrera, Álvaro

    2016-01-01

    [EN] Zirconia has become a widely utilized structural ceramic material with important applications in dentistry due to its superb mechanical properties, biocompatibility, aesthetic characteristics and durability. Zirconia needs to be stabilized in the t-phase to obtain improved mechanical properties such as hardness and fracture toughness. Fully dense yttria-stabilized tetragonal zirconia polycrystalline (Y-TZP) materials are normally consolidated through the energy-intensive processing of po...

  4. An experimental investigation of shell and tube latent heat storage for solar dryer using paraffin wax as heat storage material

    Directory of Open Access Journals (Sweden)

    Ashish Agarwal

    2016-03-01

    Full Text Available In the presented study the shell and tube type latent heat storage (LHS has been designed for solar dryer and paraffin wax is used as heat storage material. In the first part of the study, the thermal and heat transfer characteristics of the latent heat storage system have been evaluated during charging and discharging process using air as heat transfer fluid (HTF. In the last section of the study the effectiveness of the use of an LHS for drying of food product and also on the drying kinetics of a food product has been determined. A series of experiments were conducted to study the effects of flow rate and temperature of HTF on the charging and discharging process of LHS. The temperature distribution along the radial and longitudinal directions was obtained at different time during charging process to analyze the heat transfer phenomenon in the LHS. Thermal performance of the system is evaluated in terms of cumulative energy charged and discharged, during the charging and discharging process of LHS, respectively. Experimental results show that the LHS is suitable to supply the hot air for drying of food product during non-sunshine hours or when the intensity of solar energy is very low. Temperature gain of air in the range of 17 °C to 5 °C for approximately 10 hrs duration was achieved during discharging of LHS.

  5. One-step synthesis and effect of heat-treatment on the structure and electrochemical properties of LiNi0.5Mn1.5O4 cathode material for lithium-ion batteries

    International Nuclear Information System (INIS)

    Wen, Jian-Wu; Zhang, Da-Wei; Zang, Yong; Sun, Xin; Cheng, Bin; Ding, Chu-Xiong; Yu, Yan; Chen, Chun-Hua

    2014-01-01

    Highlights: • A one-step sol-gel route with resorcinol-formaldehyde resin is designed to synthesis LiNi 0.5 Mn 1.5 O 4 . • Fd-3 m phase delivers an excellent high rate performance and stable cycling retention. • A double “w”-shape R-V curve is a potential tool to indicate structure transition. - Abstract: Spinel LiNi 0.5 Mn 1.5 O 4 (Fd-3 m) powders are synthesized by a facile one-step sol-gel approach with a resorcinol formaldehyde (RF) resin as a chelating agent. The cross-linked metal-containing RF xerogel particles are sintered at different high temperatures from 750 to 950 °C to produce several micron-sized LiNi 0.5 Mn 1.5 O 4 powders. Electrochemical measurements suggest that the 850 °C-sintered (in air) sample (Fd-3 m phase) performs the best with a discharge capacity of 141 mAh g −1 at 0.1 C and 110 mAh g −1 at 10 C, and capacity-retention of 96.3% after 60 cycles at 0.25 C and 89% after 200 cycles at 1 C. For comparison, the LiNi 0.5 Mn 1.5 O 4 sample sintered at 850 °C in O 2 (P4 3 32 phase) presents limited rate performance (45 mAh g −1 at 10 C) and higher values in both AC impedance and DC-method derived resistance. A characteristic double “w”-shape curve of DC resistance against cell potential can be possibly considered as an indicator to probe the material structure transition during the charge/discharge process of the cell

  6. Development of whole energy absorption spectrometer for decay heat measurement on fusion reactor materials

    Energy Technology Data Exchange (ETDEWEB)

    Maekawa, Fujio; Ikeda, Yujiro [Japan Atomic Energy Research Inst., Tokai, Ibaraki (Japan). Tokai Research Establishment

    1997-03-01

    To measure decay heat on fusion reactor materials irradiated by D-T neutrons, a Whole Energy Absorption Spectrometer (WEAS) consisting of a pair of large BGO (bismuth-germanate) scintillators was developed. Feasibility of decay heat measurement with WEAS for various materials and for a wide range of half-lives (seconds - years) was demonstrated by experiments at FNS. Features of WEAS, such as high sensitivity, radioactivity identification, and reasonably low experimental uncertainty of {approx} 10 %, were found. (author)

  7. Mechanics/heat-transfer relation for particulate materials

    Energy Technology Data Exchange (ETDEWEB)

    Campbell, C.S.; Wang, D.G.; Rahman, K.

    1991-11-01

    The original goal of this study was to try and understand the relationship between the thermal and mechanical properties of particulate flows. Two situations were examined. The first is a study of the effects of simple shear flows, as a embryonic flow type on the apparent thermal conductivity and apparent viscosity of a dry granular flow. The second study involved fluidized beds. The original idea was to try and relate the heat transfer behavior of a fluidized bed to the particle pressure,'' the forces by only the particle phase of the two-phase mixture. (VC)

  8. Mechanics/heat-transfer relation for particulate materials. Final report

    Energy Technology Data Exchange (ETDEWEB)

    Campbell, C.S.; Wang, D.G.; Rahman, K.

    1991-11-01

    The original goal of this study was to try and understand the relationship between the thermal and mechanical properties of particulate flows. Two situations were examined. The first is a study of the effects of simple shear flows, as a embryonic flow type on the apparent thermal conductivity and apparent viscosity of a dry granular flow. The second study involved fluidized beds. The original idea was to try and relate the heat transfer behavior of a fluidized bed to the ``particle pressure,`` the forces by only the particle phase of the two-phase mixture. (VC)

  9. Heat treatment control of Bi-2212 coils: I. Unravelling the complex dependence of the critical current density of Bi-2212 wires on heat treatment

    Science.gov (United States)

    Shen, Tengming; Li, Pei; Ye, Liyang

    2018-01-01

    A robust and reliable heat treatment is crucial for developing superconducting magnets from several superconductors especially Bi-2212. An improper heat treatment may significantly reduce the critical current density Jc of a Bi-2212 superconducting coil, even to zero, since the Jc of Bi-2212 wires is sensitive to parameters of its heat treatment (partial melt processing). To provide an essential database for heat treating Bi-2212 coils, the dependence of Jc on heat treatment is studied systematically in 11 industrial Bi-2212 wires, revealing several common traits shared between these wires and outlier behaviors. The dependence of the Jc of Bi-2212 on heat treatment is rather complex, with many processing parameters affecting Jc, including the peak processing temperature Tp, the time at the peak temperature tp, the time in the melt tmelt, the rate at which Bi-2212 melt is initially cooled CR1, the rate at which the solidification of Bi-2212 melt occurs CR2, and the temperature Tq at which the cooling rate switches from CR1 to CR2. The role of these parameters is analyzed and clarified, in the perspective of heat treating a coil. Practical advices on heat treatment design are given. The ability of a Bi-2212 coil to follow the prescribed recipe decreases with increasing coil sizes. The size of a coil that can be properly heat treated is determined.

  10. Flexible and stable heat energy recovery from municipal wastewater treatment plants using a fixed-inverter hybrid heat pump system

    International Nuclear Information System (INIS)

    Chae, Kyu-Jung; Ren, Xianghao

    2016-01-01

    Highlights: • Specially designed fixed-inverter hybrid heat pump system was developed. • Hybrid operation performed better at part loads than single inverter operation. • The applied heat pump can work stably over a wide range of heat load variations. • Heat energy potential of treated effluent was better than influent. • The heat pump’s COP from the field test was 4.06 for heating and 3.64 for cooling. - Abstract: Among many options to improve energy self-sufficiency in sewage treatment plants, heat extraction using a heat pump holds great promise, since wastewater contains considerable amounts of thermal energy. The actual heat energy demand at municipal wastewater treatment plants (WWTPs) varies widely with time; however, the heat pumps typically installed in WWTPs are of the on/off controlled fixed-speed type, thus mostly run intermittently at severe part-load conditions with poor efficiency. To solve this mismatch, a specially designed, fixed-inverter hybrid heat pump system incorporating a fixed-speed compressor and an inverter-driven, variable-speed compressor was developed and tested in a real WWTP. In this hybrid configuration, to improve load response and energy efficiency, the base-heat load was covered by the fixed-speed compressor consuming relatively less energy than the variable-speed type at nominal power, and the remaining varying load was handled by the inverter compressor which exhibits a high load-match function while consuming relatively greater energy. The heat pump system developed reliably extracted heat from the treated effluent as a heat source for heating and cooling purposes throughout the year, and actively responded to the load changes with a high measured coefficient of performance (COP) of 4.06 for heating and 3.64 for cooling. Moreover, this hybrid operation yielded a performance up to 15.04% better on part loads than the single inverter operation, suggesting its effectiveness for improving annual energy saving when

  11. Gas injection to inhibit migration during an in situ heat treatment process

    Science.gov (United States)

    Kuhlman, Myron Ira; Vinegar; Harold J.; Baker, Ralph Sterman; Heron, Goren

    2010-11-30

    Methods of treating a subsurface formation are described herein. Methods for treating a subsurface treatment area in a formation may include introducing a fluid into the formation from a plurality of wells offset from a treatment area of an in situ heat treatment process to inhibit outward migration of formation fluid from the in situ heat treatment process.

  12. Enhanced heat transport in environmental systems using microencapsulated phase change materials

    Science.gov (United States)

    Colvin, D. P.; Mulligan, J. C.; Bryant, Y. G.

    1992-01-01

    A methodology for enhanced heat transport and storage that uses a new two-component fluid mixture consisting of a microencapsulated phase change material (microPCM) for enhanced latent heat transport is outlined. SBIR investigations for NASA, USAF, SDIO, and NSF since 1983 have demonstrated the ability of the two-component microPCM coolants to provide enhancements in heat transport up to 40 times over that of the carrier fluid alone, enhancements of 50 to 100 percent in the heat transfer coefficient, practically isothermal operation when the coolant flow is circulated in an optimal manner, and significant reductions in pump work.

  13. Effect of Stabilization Heat Treatment on Time-Dependent Polarization Losses in Sintered Nd-Fe-B Permanent Magnets

    Directory of Open Access Journals (Sweden)

    Tuominen S.

    2013-01-01

    Full Text Available Some companies in the motor and generator industry utilizing sintered NdFeB magnets have adopted pre-ageing heat treatment in order to improve the stability of the magnets. The parameters of this stabilization heat treatment are based mainly on assumptions rather than on any published research results. In this work, the effects of pre-ageing treatment on the time-dependent polarization losses of two different types of commercial sintered NdFeB magnets were studied. The material showing the squarer J(H curve did not benefit from the pre-ageing treatment, since it seems to be stable under a certain critical temperature. In contrast, a stabilizing effect was observed in the material showing rounder J(H curve. After the stabilization heat treatment, the polarization of the magnets was found to be at lower level, but unchanged over a certain period of time. The length of this period depends on the temperature and the duration of the pre-ageing treatment. In addition, our analysis reveals that the stabilization heat treatment performed in an open circuit condition does not stabilize the magnet uniformly.

  14. Chemistry and heat-treatment effects on mechanical and microstructural properties of heat-treated, beta-extruded Ti--6A1--6V--2Sn

    International Nuclear Information System (INIS)

    Ulitchny, M.G.; Rack, H.J.; Dawson, D.B.

    1979-04-01

    The mechanical behavior of beta-extruded Ti--6A1--6V--2Sn was examined after a variety of sub-transus heat treatments. The microstructural variations resulting from the range of heat treatments studied also were examined. A range of alloy chemistries, within commercial limits, was used to evaluate the effect of this variable on mechanical properties. The strength--toughness combinations obtained in beta-extruded Ti--6A1--6V--2Sn ranged from about 895 MPa and 82.5 MPa√m for duplex annealed material to 1200 MPa and 54.9 MPa√m for solution treated and peak aged material. Chemistry variations had less effect on mechanical properties than would have been the case with alpha--beta processing

  15. Thermal management of electronics using phase change material based pin fin heat sinks

    International Nuclear Information System (INIS)

    Baby, R; Balaji, C

    2012-01-01

    This paper reports the results of an experimental study carried out to explore the thermal characteristics of phase change material based heat sinks for electronic equipment cooling. The phase change material (PCM) used in this study is n – eicosane. All heat sinks used in the present study are made of aluminium with dimensions of 80 × 62 mm 2 base with a height of 25 mm. Pin fins acts as the thermal conductivity enhancer (TCE) to improve the distribution of heat more uniformly as the thermal conductivity of the PCM is very low. A total of three different pin fin heat sink geometries with 33, 72 and 120 pin fins filled with phase change materials giving rise to 4%, 9% and 15% volume fractions of the TCE respectively were experimentally investigated. Baseline comparisons are done with a heat sink filled with PCM, without any fin. Studies are conducted for heat sinks on which a uniform heat load is applied at the bottom for the finned and unfinned cases. The effect of pin fins of different volume fractions with power levels ranging from 4 to 8 W corresponding to a heat flux range of 1. 59 to 3.17 kW/m 2 , was explored in this paper. The volume fraction of the PCM (PCM volume / (Total volume – fin volume)) is also varied as 0. 3, 0.6 and 1 to determine the effect of PCM volume on the overall performance of the electronic equipment.

  16. Hemodialysis Catheter Heat Transfer for Biofilm Prevention and Treatment.

    Science.gov (United States)

    Richardson, Ian P; Sturtevant, Rachael; Heung, Michael; Solomon, Michael J; Younger, John G; VanEpps, J Scott

    2016-01-01

    Central line-associated bloodstream infections (CLABSIs) are not easily treated, and many catheters (e.g., hemodialysis catheters) are not easily replaced. Biofilms (the source of infection) on catheter surfaces are notoriously difficult to eradicate. We have recently demonstrated that modest elevations of temperature lead to increased staphylococcal susceptibility to vancomycin and significantly soften the biofilm matrix. In this study, using a combination of microbiological, computational, and experimental studies, we demonstrate the efficacy, feasibility, and safety of using heat as an adjuvant treatment for infected hemodialysis catheters. Specifically, we show that treating with heat in the presence of antibiotics led to additive killing of Staphylococcus epidermidis with similar trends seen for Staphylococcus aureus and Klebsiella pneumoniae. The magnitude of temperature elevation required is relatively modest (45-50°C) and similar to that used as an adjuvant to traditional cancer therapy. Using a custom-designed benchtop model of a hemodialysis catheter, positioned with tip in the human vena cava as well as computational fluid dynamic simulations, we demonstrate that these temperature elevations are likely achievable in situ with minimal increased in overall blood temperature.

  17. The effect of nitrogen gas flow rate on heat treatment of AISI SS-430: Study of microstructure and hardness

    Science.gov (United States)

    Sebayang, Perdamean; Darmawan, Bobby Aditya; Simbolon, Silviana; Alfirano, Sudiro, Toto; Aryanto, Didik

    2018-05-01

    The aim of this research was to obtain the austenite phase from ferritic stainless steel through sample heat treatment. The AISI 430 ferritic steel with the thickness of about 0.4 mm was used. The heat treatment was conducted in a tube furnace at elevated temperature of 1150, 1200, 1250 °C and nitrogen gas flow rate of 0.57 and 0.73 l/s. The samples were then rapidly quenched in water bath. An optical microscope, XRD, SEM-EDS and micro vickers hardness tester were used to characterize the sample before and after het treatment. The presence of anneal twins indicated the formation of austenite phase in the sample. Its fraction was varied from 10.89 wt% to 35.10 wt%. In addition, the heat treatment temperature strongly affected the sample hardness. The optimum hardness obtained was about 542.69 HV. According to the results, this material can be considered for biomedical applications.

  18. Calculation of α/γ equilibria in SA508 grade 3 steels for intercritical heat treatment

    International Nuclear Information System (INIS)

    Lee, B.J.; Kim, H.D.; Hong, J.H.

    1998-01-01

    An attempt has been made to suggest an optimum temperature for intercritical heat treatment of an SA508 grade 3 steel for nuclear pressure vessels, based on thermodynamic calculation of the α/γ phase equilibria. A thermodynamic database constructed for the Fe-Mn-Ni-Mo-Cr-Si-V-Al-C-N ten-component system and an empirical criterion that the amount of reformed austenite should be around 40 pct were used for thermodynamic calculation and derivation of the optimum heat-treatment temperature, respectively. The calculated optimum temperature, 720 C, was in good agreement with an experimentally determined temperature of 725 C obtained through an independent experimental investigation of the same steel. The agreement between the calculated and measured fraction of reformed austenite during the intercritical heat treatment was also confirmed. Based on the agreement between calculation and experiment, it could be concluded that thermodynamic calculations can be successfully applied to the materials and/or process design as an additive tool to the already established technology, and that the currently constructed thermodynamic database for steel systems shows an accuracy that makes such applications possible

  19. Effects of heat treatment conditions on microstructure and mechanical properties of AISI 420 steel

    Energy Technology Data Exchange (ETDEWEB)

    Scheuer, C.J.; Fraga, R.A.; Cardoso, R.P.; Brunatto, S.F. [Universidade Federal do Parana (UFPR), Curitiba, PR (Brazil). Departamento de Engenharia Mecanica. Grupo de Tecnologia de Fabricacao Assistida por Plasma e Metalurgia do Po

    2014-07-01

    The cycle control of heat treatments, on the quenching and tempering operation of AISI 420 stainless steel, is essential for improved material performance. The adequate choice of heat treatment parameters, can lead an optimization on its mechanical properties and corrosion resistance. Thus, this paper aims to investigate the effects of quenchants medium, and austenitizing and tempering temperatures, on the microstructure and mechanical properties of AISI 420 steel. Different heat treatments cycles were studied: 1) samples were austenitized at 1050°C and water, oil and air quenched; 2) samples were austenitized at range temperatures of 950-1050°C and oil quenched; and 3) as-quenched samples were tempering at range temperatures of 400-500°C. Treated samples were characterized by optical microscopy, X-ray diffractometry and hardness measurements. The samples hardness increases with increasing cooling rate (water > oil > air quenched). Water quenched samples presented crack after cooling to room temperature. Samples hardness also increases with austenitizing temperature increasing, and decreases with increasing tempering temperature. (author)

  20. Influence of heat treatment on corrosive resistance of concrete steels

    International Nuclear Information System (INIS)

    Woldan, A.; Suliga, I.; Kusinski, J.; Jazowy, R.

    1998-01-01

    The reinforcing bars are essential elements of ferro-concrete structures. During the building structure service the reinforcing bars should co-operate with surrounding concrete. Any bonding defects as well as corrosion induced strength reduction may result in construction failure. The reinforcing steel working environment is determined by concrete chemical and phase composition and surrounding environmental properties. The aggressive corrosive activity of the letter implies necessity of effective ways development to protect elements against corrosion. The effect of heat treatment, increased Si content in steel on corrosion resistance of reinforcing steel in concrete was studied in the current work. Corrosion tests and metallographic examinations proved a positive influence of hardening and Si enrichment on corrosion resistance of reinforcing bars in ferro-concrete structures. (author)

  1. Zr-2.5 Nb microstructure evolution during heat treatments

    International Nuclear Information System (INIS)

    Campitelli, Emiliano N.; Banchik, Abrahan D.; Versaci, Raul A.

    1999-01-01

    This work has the following two basic objectives: 1) To gain experience in the preparation of thin layers of zirconium alloys to be used as T.E.M specimens. To construct a double jet thinning prototype able to perform this task with appropriate finishing and reproducible results to be used in a future work (point 2). To become familiar with the relevant parameters of the thinning process and to apply this experience in the prototype. The layers must have sufficient area with good transmission and mechanical support, free of deformations and defects polishing. 2) To perform T.E.M. observations and metallographies to study the microstructural evolution during heat treatments of Zr-2.5 Nb alloy samples. These samples were obtained from a pressure tube similar to those used in Candu power plants, in the as-received condition. This alloy served, in this application, to replace Zircaloy-2, for better creep and corrosion resistance. (author)

  2. The Effect of Heat Treatment on Physical, Chemical and Structural Properties of Calcium Sulfate Based Scaffolds

    Directory of Open Access Journals (Sweden)

    Hakan OFLAZ

    2017-03-01

    Full Text Available 3D printed calcium sulfate (CS is a promising material for on custom bone substitutes. Since it dissolves easily in body fluids, manufactured samples require to being improved to reduce solubility.  The main aim of this study was reducing the dissolubility of CS based samples by using sintering and investigating the effect of heat treatment on their physical, chemical and structural properties. To observe the effect of heat treatment on samples, contact angles were measured, X-Ray diffraction analysis (XRD was performed, and scanning electron microscope (SEM micrographs were captured before and after the sintering process, and the results were compared. Furthermore, sintered and non-sintered samples were soaked in phosphate buffered saline (PBS to observe the impact of sintering on the solubility of the material. Also, three different pore sized scaffolds were manufactured to test the limits of the 3D printer for manufacturing of scaffolds with open pores. Sintering process results in a volume reduction and according to SEM results, CS grains were fused together after heat treatment. Although non-sintered CS sample starts to dissolve in high rate and nearly 1/3 of the sample was at the bottom of the glass in a matter of minutes, sintering creates more rigid structure and there were not visible dissolution in PBS at the end of a week. The contact angle of samples cannot be measured, so it can be concluded that 3D printed material showed a super-hydrophilic property. XRD diagram suggested that there is not any new phase created in the printing and sintering processes except related hydrates of CS. As a result of the 3D printing, 500 µm, 750 µm and 1000 µm pore sized scaffolds were manufactured, successfully. However, it was seen that 500 µm pores could not be open by using depowdering after the printing process.

  3. Effects of Heat Treatment on SiC-SiC Ceramic Matrix Composites

    Science.gov (United States)

    Knauf, Michael W.

    Residual stresses resulting from the manufacturing process found within a silicon carbide/silicon carbide (SiC/SiC) ceramic matrix composite were thoroughly investigated through the use of high-energy X-ray diffraction and Raman microspectroscopy. The material system studied was a Rolls-Royce composite produced with Hi-Nicalon fibers woven into a five harness satin weave, coated with boron nitride and silicon carbide interphases, and subsequently infiltrated with silicon carbide particles and a silicon matrix. Constituent stress states were measured before, during, and after heat treatments ranging from 900 °C to 1300 °C for varying times between one and sixty minutes. Stress determination methods developed through these analyses can be utilized in the development of ceramic matrix composites and other materials employing boron-doped silicon. X-ray diffraction experiments were performed at the Argonne National Laboratory Advanced Photon Source to investigate the evolution of constituent stresses through heat treatment, and determine how stress states are affected at high temperature through in situ measurements during heat treatments up to 1250 °C for 30 minutes. Silicon carbide particles in the as-received condition exhibited a nearly isotropic stress state with average tensile stresses of approximately 300 MPa. The silicon matrix exhibited a complimentary average compressive stress of approximately 300 MPa. Strong X-ray diffraction evidence is presented demonstrating solid state boron diffusion and increased boron solubility found in silicon throughout heat treatment. While the constituent stress states did evolve through the heat treatment cycles, including approaching nearly stress-free conditions at temperatures close to the manufacturing temperature, no permanent relaxation of stress was observed. Raman spectroscopy was utilized to investigate stresses found within silicon carbide particles embedded within the matrix and the silicon matrix as an alternate

  4. Online Adaptive Hyperthermia Treatment Planning During Locoregional Heating to Suppress Treatment-Limiting Hot Spots.

    Science.gov (United States)

    Kok, H Petra; Korshuize-van Straten, Linda; Bakker, Akke; de Kroon-Oldenhof, Rianne; Geijsen, Elisabeth D; Stalpers, Lukas J A; Crezee, Johannes

    2017-11-15

    Adequate tumor temperatures during hyperthermia are essential for good clinical response, but excessive heating of normal tissue should be avoided. This makes locoregional heating using phased array systems technically challenging. Online application of hyperthermia treatment planning could help to improve the heating quality. The aim of this study was to evaluate the clinical benefit of online treatment planning during treatment of pelvic tumors heated with the AMC-8 locoregional hyperthermia system. For online adaptive hyperthermia treatment planning, a graphical user interface was developed. Electric fields were calculated in a preprocessing step using our in-house-developed finite-difference-based treatment planning system. This allows instant calculation of the temperature distribution for user-selected phase-amplitude settings during treatment and projection onto the patient's computed tomographic scan for online visualization. Online treatment planning was used for 14 treatment sessions in 8 patients to reduce the patients' reports of hot spots while maintaining the same level of tumor heating. The predicted decrease in hot spot temperature should be at least 0.5°C, and the tumor temperature should decrease less than 0.2°C. These predictions were compared with clinical data: patient feedback about the hot spot and temperature measurements in the tumor region. In total, 17 hot spot reports occurred during the 14 sessions, and the alternative settings predicted the hot spot temperature to decrease by at least 0.5°C, which was confirmed by the disappearance of all 17 hot spot reports. At the same time, the average tumor temperature was predicted to change on average -0.01°C (range, -0.19°C to 0.34°C). The measured tumor temperature change was on average only -0.02°C (range, -0.26°C to 0.31°C). In only 2 cases the temperature decrease was slightly larger than 0.2°C, but at most it was 0.26°C. Online application of hyperthermia treatment planning is

  5. Electrodeposition of Copper/Carbonous Nanomaterial Composite Coatings for Heat-Dissipation Materials

    Directory of Open Access Journals (Sweden)

    Yasuki Goto

    2017-12-01

    Full Text Available Carbonous nanomaterials are promising additives for composite coatings for heat-dissipation materials because of their excellent thermal conductivity. Here, copper/carbonous nanomaterial composite coatings were prepared using nanodiamond (ND as the carbonous nanomaterial. The copper/ND composite coatings were electrically deposited onto copper substrates from a continuously stirred copper sulfate coating bath containing NDs. NDs were dispersed by ultrasonic treatment, and the initial bath pH was adjusted by adding sodium hydroxide solution or sulfuric acid solution before electrodeposition. The effects of various coating conditions—the initial ND concentration, initial bath pH, stirring speed, electrical current density, and the amount of electricity—on the ND content of the coatings were investigated. Furthermore, the surface of the NDs was modified by hydrothermal treatment to improve ND incorporation. A higher initial ND concentration and a higher stirring speed increased the ND content of the coatings, whereas a higher initial bath pH and a greater amount of electricity decreased it. The electrical current density showed a minimum ND content at approximately 5 A/dm2. Hydrothermal treatment, which introduced carboxyl groups onto the ND surface, improved the ND content of the coatings. A copper/ND composite coating with a maximum of 3.85 wt % ND was obtained.

  6. Thermal energy storage system using phase change materials: Constant heat source

    Directory of Open Access Journals (Sweden)

    Reddy Meenakshi R.

    2012-01-01

    Full Text Available The usage of phase change materials (PCM to store the heat in the form of latent heat is increased, because large quantity of thermal energy is stored in smaller volumes. In the present experimental investigation paraffin and stearic acid are employed as PCMs in thermal energy storage (TES system to store the heat as sensible and latent heat also. A constant heat source is used to supply heat transfer fluid (HTF at constant temperature to the TES system. In the TES system PCMs are stored in the form of spherical capsules of 38 mm diameter made of high density poly ethylene (HDPE. The results of the investigation are related to the charging time and recovery of stored energy from the TES system.

  7. Effect of heat treatment of whole cottonseed on in vitro, in situ and in ...

    African Journals Online (AJOL)

    Keywords: Amino acid flow, heat treatment, protein degradation, whole cononseed. * Author to whom ... heat-treated soybearu were compared with raw soybeans, it was found that ... et al., 1985; Faldet & Sarter, 1989) while milk fat percenrage.

  8. Structural steels for power generating equipment and heat and chemical heat treatments

    International Nuclear Information System (INIS)

    Astaf'ev, A.A.

    1979-01-01

    Development of structural steels for power generating equipment and for reactor engineering, in particular, is elucidated. Noted is utilization of the 15Kh2NMFA steels for the WWER-1000 reactor vessels, the 10GN2MFA steels for steam generators, pressurizers, vessels of the automatic emergency shut down and safety system; the 00Kh12N3DL steel for cast pump vessels and main locking bars. The recommendations on heat treatment of big forgings, for instance, ensuring the necessary complex of mechanical properties are given. Diffusion chromizing with subsequent nitriding of austenitic steels which increase durability of the components in BN reactors more than 4 times, is practised on a large scale

  9. POTENTIAL USE OF PHASE CHANGE MATERIALS IN GREENHOUSES HEATING: COMPARISON WITH A TRADITIONAL SYSTEM

    Directory of Open Access Journals (Sweden)

    Claudio Caprara

    2009-09-01

    Full Text Available In order to use solar radiation as thermal energy source, heat storage equipments result necessary in each application where continuous supply is required, because of the natural unsteady intensity of radiation during the day. Thermal solar collectors are especially suitable for low temperature applications, since their efficiency decreases when an high inlet temperature of fluid flowing through them is established. On the other hand, low temperatures and low temperature gaps, above all, make very difficult to use traditional sensible heat storing units (water tanks, because of the very large amounts of material required. In this work, a traditional sensible heat storage system is compared with a latent heat storing unit based on phase change materials (PCMs. As a case study, a 840 m3 greenhouse heating application was considered with an inside constant temperature of 18°C. It is thought to be heated by using single layer plate thermal solar collectors as energy source. Inlet temperature of the collectors fluid (HTF was fixed at 35°C (little higher than melting temperature of PCMs and a constant flux of 12 l/m2 hour was established as technical usual value. At these conditions, 215m2 solar panels exposed surface resulted necessary. The sensible heat storage system considered here is a traditional water tank storing unit equipped with two pipe coils, respectively for heat exchanges with HTF from collectors and water flux for greenhouse heating. Available DT for heat exchange is estimated as the difference of minimum HTF temperature (in outlet from the collectors and the required water temperature for greenhouse heating. The latent heat storing unit is instead a series of copper rectangular plate shells which a phase change material is filled in (Na2SO4⋅10H2O. Heat transfer fluids flow through thin channels between adjacent plates, so that a large heat exchange available surface is achieved. The developed computational model (Labview software

  10. Metallic materials for heat exchanger components and highly stressed internal of HTR reactors for nuclear process heat generation

    International Nuclear Information System (INIS)

    1982-01-01

    The programme was aimed at the development and improvement of materials for the high-temperature heat exchanger components of a process steam HTR. The materials must have high resistance to corrosion, i.e. carburisation and internal oxidation, and high long-term toughness over a wide range of temperatures. They must also meet the requirements set in the nuclear licensing procedure, i.e. resistance to cyclic stress and irradiation, non-destructive testing, etc. Initially, it was only intended to improve and qualify commercial alloys. Later on an alloy development programme was initiated in which new, non-commercial alloys were produced and modified for use in a nuclear process heat facility. Separate abstracts were prepared for 19 pays of this volume. (orig./IHOE) [de

  11. Endotoxin inactivation via steam-heat treatment in dilute simethicone emulsions used in biopharmaceutical processes.

    Science.gov (United States)

    Britt, Keith A; Galvin, Jeffrey; Gammell, Patrick; Nti-Gyabaah, Joseph; Boras, George; Kolwyck, David; Ramirez, José G; Presente, Esther; Naugle, Gregory

    2014-01-01

    Simethicone emulsion is used to regulate foaming in cell culture operations in biopharmaceutical processes. It is also a potential source of endotoxin contamination. The inactivation of endotoxins in dilute simethicone emulsions was assessed as a function of time at different steam temperatures using a Limulus amebocyte lysate kinetic chromogenic technique. Endotoxin inactivation from steam-heat treatment was fit to a four-parameter double exponential decay model, which indicated that endotoxin inactivation was biphasic, consisting of fast and slow regimes. In the fast regime, temperature-related effects were dominant. Transitioning into the slow regime, the observed temperature dependence diminished, and concentration-related effects became increasingly significant. The change in the Gibbs free energy moving through the transition state indicated that a large energy barrier must be overcome for endotoxin inactivation to occur. The corresponding Arrhenius pre-exponential factor was >10(12) s(-1) suggesting that endotoxins in aqueous solution exist as aggregates. The disorder associated with the endotoxin inactivation reaction pathway was assessed via the change in entropy moving through the transition state. This quantity was positive indicating that endotoxin inactivation may result from hydrolysis of individual endotoxin molecules, which perturbs the conformation of endotoxin aggregates, thereby modulating the biological activity observed. Steam-heat treatment decreased endotoxin levels by 1-2 logarithm (log) reduction (LRV), which may be practically relevant depending on incoming raw material endotoxin levels. Antifoam efficiency and cell culture performance were negligibly impacted following steam-heat treatment. The results from this study show that steam-heat treatment is a viable endotoxin control strategy that can be implemented to support large-scale biopharmaceutical manufacturing. © 2014 American Institute of Chemical Engineers.

  12. Enhancing the mechanical properties of electrospun polyester mats by heat treatment

    Directory of Open Access Journals (Sweden)

    M. Kancheva

    2015-01-01

    Full Text Available Microfibrous materials with a targeted design based on poly(L-lactic acid (PLA and poly(ε-caprolactone (PCL were prepared by electrospinning and by combining electrospinning and electrospraying. Several approaches were used: (i electrospinning of a common solution of the two polymers, (ii simultaneous electrospinning of two separate solutions of PLA and PCL, (iii electrospinning of PLA solution in conjunction with electrospraying of PCL solution, and (iv alternating layer-by-layer deposition by electrospinning of separate PLA and PCL solutions. The mats were heated at the melting temperature of PCL (60°", thus achieving melting of PCL fibers/particles and thermal sealing of the fibers. The mats subjected to thermal treatment were characterized by greater mean fiber diameters and reduced values of the water contact angle compared to the pristine mats. Heat treatment of the mats affected their thermal stability and led to an increase in the crystallinity degree of PLA incorporated in the mats, whereas that of PCL was reduced. All mats were characterized by enhanced mechanical properties after thermal treatment as compared to the non-treated fibrous materials.

  13. Heat transfer characteristics of liquid-gas Taylor flows incorporating microencapsulated phase change materials

    International Nuclear Information System (INIS)

    Howard, J A; Walsh, P A

    2014-01-01

    This paper presents an investigation on the heat transfer characteristics associated with liquid-gas Taylor flows in mini channels incorporating microencapsulated phase change materials (MPCM). Taylor flows have been shown to result in heat transfer enhancements due to the fluid recirculation experienced within liquid slugs which is attributable to the alternating liquid slug and gas bubble flow structure. Microencapsulated phase change materials (MPCM) also offer significant potential with increased thermal capacity due to the latent heat required to cause phase change. The primary aim of this work was to examine the overall heat transfer potential associated with combining these two novel liquid cooling technologies. By investigating the local heat transfer characteristics, the augmentation/degradation over single phase liquid cooling was quantified while examining the effects of dimensionless variables, including Reynolds number, liquid slug length and gas void fraction. An experimental test facility was developed which had a heated test section and allowed MPCM-air Taylor flows to be subjected to a constant heat flux boundary condition. Infrared thermography was used to record high resolution experimental wall temperature measurements and determine local heat transfer coefficients from the thermal entrance point. 30.2% mass particle concentration of the MPCM suspension fluid was examined as it provided the maximum latent heat for absorption. Results demonstrate a significant reduction in experimental wall temperatures associated with MPCM-air Taylor flows when compared with the Graetz solution for conventional single phase coolants. Total enhancement in the thermally developed region is observed to be a combination of the individual contributions due to recirculation within the liquid slugs and also absorption of latent heat. Overall, the study highlights the potential heat transfer enhancements that are attainable within heat exchange devices employing MPCM

  14. Study of secondary recrystallization in grain-oriented steel treated under dynamical heat treatment conditions

    Directory of Open Access Journals (Sweden)

    V. Stoyka

    2009-04-01

    Full Text Available The present study was made to investigate secondary recrystallization in grain-oriented steels annealed at short time temperature exposures with application of dynamical heating. The investigated GO steels for experiments were taken from one industrial line after final cold rolling reduction and subsequent box annealing. It was shown that application of short time heat treatment conditions could lead to complete abnormal grain growth in the investigated GO steel. The texture and microstructure obtained in the laboratory treated material is similar to that observed in the same GO steel taken after industrial final box-annealing. However, some “parasitic” grains were observed in the secondary recrystallized matrix of the laboratory treated GO steel. These “parasitic” grains possess the unwanted from magnetic properties point of view {111} orientation components.

  15. Effect of heat treatment on the structural and optical properties of tellurite glasses doped erbium

    Energy Technology Data Exchange (ETDEWEB)

    Jlassi, I., E-mail: ifa.jlassi@fst.rnu.tn [Laboratoire de Physico-Chimie des Materiaux Mineraux et leurs Applications, Centre National de Recherches en Sciences des Materiaux, B.P. 95 Hammam-Lif 2050 (Tunisia); Elhouichet, H. [Laboratoire de Physico-Chimie des Materiaux Mineraux et leurs Applications, Centre National de Recherches en Sciences des Materiaux, B.P. 95 Hammam-Lif 2050 (Tunisia); Departement de Physique, Faculte des Sciences de Tunis, Campus ElManar 2092 (Tunisia); Hraiech, S.; Ferid, M. [Laboratoire de Physico-Chimie des Materiaux Mineraux et leurs Applications, Centre National de Recherches en Sciences des Materiaux, B.P. 95 Hammam-Lif 2050 (Tunisia)

    2012-03-15

    The 75TeO{sub 2}-20ZnO-4Na{sub 2}CO{sub 3}-1Er{sub 2}O{sub 3} (in molar ratio) glass system was prepared by the conventional melt-quenching method. As such, the samples prepared were investigated by differential scanning calorimetry (DSC), X-ray diffractrometry (XRD), Raman spectroscopy and infrared luminescence. DSC analyses were carried out on our glass at different heating rates between 5 and 20 Degree-Sign C/min. The result of the annealing temperature on the spectroscopic properties of Er{sup 3+} in tellurite glasses was discussed. The activation energy, for surface crystallization, was determined graphically from a Kissinger-type plot and had a value about 897.2 kJ/mol. Crystalline phases for both {alpha}-TeO{sub 2}, {gamma}-TeO{sub 2} and Zn{sub 2}Te{sub 3}O{sub 8} system were determined by the XRD method and were confirmed by Raman spectroscopy characterizations after heat treatment. The effect of heat treatment on absorption spectra and luminescence properties in the tellurite glass was also investigated. With heat treatment, the ultraviolet absorption edge presented a redshift. As a result, the Judd-Ofelt (J-O) intensity parameters ({Omega}{sub 2}, {Omega}{sub 4}, {Omega}{sub 6}) were determined. The spontaneous emission probabilities of some relevant transitions, the branching ratio and the radiative lifetimes of several excited states of Er{sup 3+} were predicted using intensity J-O parameters. The near infrared emission that corresponds to Er{sup 3+}: {sup 4}I{sub 13/2}{yields}{sup 4}I{sub 15/2} can be significantly enhanced after heat treatment. Notably, it is found that the luminescence lifetime in the present system is much longer than that in most other glasses and glass ceramics. A comparative study on luminescence performance suggests that the obtained glass ceramic is a promising material for Er{sup 3+} doped fiber amplifiers. - Highlights: Black-Right-Pointing-Pointer Tellurite glasses were prepared by conventional melt-quenching method. Black

  16. Insulation and Heat Treatment of Bi-2212 Wire for Wind-and-React Coils

    Energy Technology Data Exchange (ETDEWEB)

    Peter K. F. Hwang

    2007-10-22

    Higher Field Magnets demand higher field materials such as Bi-2212 round superconducting wire. The Bi-2212 wire manufacture process depends on the coil fabrication method and wire insulation material. Considering the wind-and-react method, the coil must unifirmly heated to the melt temperature and uniformly cooled to the solidification temperature. During heat treat cycle for tightly wound coils, the leakage melt from conductor can chemically react with insulation on the conductor and creat short turns in the coils. In this research project, conductor, insulation, and coils are made to systemically study the suitable insulation materials, coil fabrication method, and heat treatment cycles. In this phase I study, 800 meters Bi-2212 wire with 3 different insulation materials have been produced. Best insulation material has been identified after testing six small coils for insulation integrity and critical current at 4.2 K. Four larger coils (2" dia) have been also made with Bi-2212 wrapped with best insulation and with different heattreatment cycle. These coils were tested for Ic in a 6T background field and at 4.2 K. The test result shows that Ic from 4 coils are very close to short samples (1 meter) result. It demonstrates that HTS coils can be made with Bi-2212 wire with best insulation consistently. Better wire insulation, improving coil winding technique, and wire manufacture process can be used for a wide range of high field magnet application including acclerators such as Muon Collider, fusion energy research, NMR spectroscopy, MRI, and other industrial magnets.

  17. Insulation and Heat Treatment of Bi-2212 Wires for Wind-and-React Coils

    International Nuclear Information System (INIS)

    Hwang, Peter K.F.

    2007-01-01

    Higher Field Magnets demand higher field materials such as Bi-2212 round superconducting wire. The Bi-2212 wire manufacture process depends on the coil fabrication method and wire insulation material. Considering the wind-and-react method, the coil must unifirmly heated to the melt temperature and uniformly cooled to the solidification temperature. During heat treat cycle for tightly wound coils, the leakage melt from conductor can chemically react with insulation on the conductor and creat short turns in the coils. In this research project, conductor, insulation, and coils are made to systemically study the suitable insulation materials, coil fabrication method, and heat treatment cycles. In this phase I study, 800 meters Bi-2212 wire with 3 different insulation materials have been produced. Best insulation material has been identified after testing six small coils for insulation integrity and critical current at 4.2 K. Four larger coils (2-inch dia) have been also made with Bi-2212 wrapped with best insulation and with different heattreatment cycle. These coils were tested for Ic in a 6T background field and at 4.2 K. The test result shows that Ic from 4 coils are very close to short samples (1 meter) result. It demonstrates that HTS coils can be made with Bi-2212 wire with best insulation consistently. Better wire insulation, improving coil winding technique, and wire manufacture process can be used for a wide range of high field magnet application including acclerators such as Muon Collider, fusion energy research, NMR spectroscopy, MRI, and other industrial magnets.

  18. Evaluation of heat sink materials for thermal management of lithium batteries

    Science.gov (United States)

    Dimpault-Darcy, E. C.; Miller, K.

    Aluminum, neopentyl glycol (NPG), and resins FT and KT are evaluated theoretically and experimentally as heat sink materials for lithium battery packs. The thermal performances of the two resins are compared in a thermal vacuum experiment. As solutions to the sublimation property were not immediately apparent, a theoretical comparison of the thermal performance of NPG versus KT, Al, and no material, is presented.

  19. Evaluation of heat sink materials for thermal management of lithium batteries

    Science.gov (United States)

    Dimpault-Darcy, E. C.; Miller, K.

    1988-01-01

    Aluminum, neopentyl glycol (NPG), and resins FT and KT are evaluated theoretically and experimentally as heat sink materials for lithium battery packs. The thermal performances of the two resins are compared in a thermal vacuum experiment. As solutions to the sublimation property were not immediately apparent, a theoretical comparison of the thermal performance of NPG versus KT, Al, and no material, is presented.

  20. Method of treating organic material. [addition of formate, heating under pressure, and distilling the mass

    Energy Technology Data Exchange (ETDEWEB)

    Bergstrom, H O.V.; Cederquist, K N

    1932-02-08

    A method is given of treating organic material such as wood, peat, shale, etc. It is characterized by the addition of formate to the material, before, during, or after heating it under pressure with alkalis, earth alkalis, et cetera, and by the mass thus produced undergoing dry distillation. The patent has three more claims.

  1. Certification of materials for steam generator condensor and regeneration heat exchanger for nuclear plant

    International Nuclear Information System (INIS)

    Stevanovicj, M.V.; Jovashevicj, V.J.; Jovashevicj, V.D.J.; Spasicj, Zh.Lj.

    1977-01-01

    In the construction of a nuclear power plant almost all known materials are used. The choice depends on working conditions. In this work standard specifications of contemporary materials that take part in larger quantities in the following components of the secondary circuit of PWR-type nuclear power plant are proposed: steam generator with moisture separator, condensor and regenerative heat eXchanger

  2. Direct waste heat recovery via thermoelectric materials - chosen issues of the thermodynamic description

    International Nuclear Information System (INIS)

    Kolasiński, Piotr; Kolasińska, Ewa

    2016-01-01

    The effective waste heat recovery is one of the present-day challenges in the industry and power engineering. The energy systems dedicated for waste heat conversion into electricity are usually characterized by low efficiency and are complicated in the design. The possibility of waste heat recovery via thermoelectric materials may be an interesting alternative to the currently used technologies. In particular, due to their material characteristics, conducting polymers may be competitive when compared with the power machinery and equipment. These materials can be used in a wide range of the geometries e.g. the bulk products, thin films, pristine form or composites and the others. In this article, the authors present selected issues related to the mathematical and thermodynamic description of the heat transfer processes in the thermoelectric materials dedicated for the waste heat recovery. The link of these models with electrical properties of the material and a material solution based on a conducting polymer have also been presented in this paper. (paper)

  3. Influence of technical parameters of disk-shaped reactor on productivity of heat treatment of crushed wood

    Science.gov (United States)

    Safin, R. R.; Khasanshin, R. R.; Mukhametzyanov, S. R.

    2018-03-01

    The existing installations for heat treatment of the crushed wood are analyzed. The technology of heat treatment of the crushed wood in the devices of disk-shaped type is offered. The results of modeling for the purpose of determination of interrelation of the key design and technological parameters of the disk-shaped device are presented. It is established that the major factors, affecting duration of stay of the material in a device, are the speed of rotation of the mixer, the number of mixers and the number of rakes on the mixer.

  4. Influence of temperature of the short-period heat treatment on mechanical properties of the NiTi alloy

    Directory of Open Access Journals (Sweden)

    Jaroslav Čapek

    2014-01-01

    Full Text Available The equiatomic alloy of nickel and titanium, known as nitinol, possesses unique properties such as superelasticity, pseudoplasticity, shape memory, while maintaining good corrosion resistance and sufficient biocompatibility. Therefore it is used for production of various devices including surgery implants. Heat treatment of nickel-rich NiTi alloys can result in precipitation of nickel-rich phases, which strongly influence tensile and fatigue behaviour of the material.In this work we have studied influence of short-period heat treatment on tensile behaviour and fatigue life of the NiTi (50.9 at. % Ni wire intended for fabrication of surgery stents.

  5. The development of heat exchangers with advanced thermomechanical materials

    International Nuclear Information System (INIS)

    Capra, Marcello

    1997-07-01

    Current metallurgical limitations necessarily impose a number of restrictions on the efficiency of power plant and combustion systems. These limitations include both temperature and corrosion resistance. If significant improvements can be made in these areas, then not only will it be possible to obtain higher system efficiencies, but it will also be possible to further exploit new technologies. Consequently, there is appreciable interest in the development of ceramic tubes for heat exchangers. Such tubes would offer the potential of operation at much higher temperatures combined with a much improved resistance to chemical attack. They are unlikely to be suitable for high pressure operation, at least in the foreseeable future, and hence their use would be limited generally to gas to gas exchangers. In spite of the limitations on details and specific technological solutions imposed by industrial property conditions, this report provides an overview on the development of these components, which is in charge of all the major international industrial companies of the field, in consideration of the relevant benefits coming from their large industrialization. After an analysis of the industrial situation of the product, in terms both of possible applications and economical impacts on the market, an overview of major on-going R and D programmes is carried out. At present, these programmes are mostly within the general frame of the study of advanced thermomechanical components and the related manufacturing technologies development

  6. Analysis of the building system of four mills and their suitability for heat treatment pest disinfestation

    Directory of Open Access Journals (Sweden)

    Loredana Strano

    2013-09-01

    Full Text Available The last century researchers at Kansas State University demonstrated the validity of the heat treatment as a method of pest control in more than 20 mills. However factors such as the high capital investment required to heat large buildings, inadequate control of high temperatures and the risk of damage to parts of the plants or the construction materials have prevented the large-scale adoption of this technique as a viable alternative to fumigants. Today the combination of the industrialization of the food industry, the technological and structural modernization of plants and developments in heat disinfection technologies have resulted in interesting results being obtained for the use of this system in primary and secondary production processing plants, both experimentally and in practice. However, the scientific literature highlights some of the factors that limit the efficiency of the treatment. This is related to aspects of the buildings and the plants and the environment of the buildings. The structure of the buildings appear to have an enormous impact on energy consumption, because this depends on the amount of heating time and the methods that have to be used when establishing a heat treatment regime. These factors are important if the fumigation temperatures are to be reached in the shortest possible time and can affect the choice of the technique used with current fumigants, especially when this is combined with the amount and cost of the energy consumed. The aim of this work is to analyse four Sicilians mills that intend to use the heat system for fumigation and pest control in order to identify those aspects of the buildings, plant and their environment which are “critical elements” and may discourage the use of this technology. Particular attention was paid to the type of construction materials and their thermal conductivity (roof, floors and walls, the number and volume of the buildings and the distance between them, the

  7. Heat transport in low-dimensional materials: A review and perspective

    Directory of Open Access Journals (Sweden)

    Zhiping Xu

    2016-05-01

    Full Text Available Heat transport is a key energetic process in materials and devices. The reduced sample size, low dimension of the problem and the rich spectrum of material imperfections introduce fruitful phenomena at nanoscale. In this review, we summarize recent progresses in the understanding of heat transport process in low-dimensional materials, with focus on the roles of defects, disorder, interfaces, and the quantum-mechanical effect. New physics uncovered from computational simulations, experimental studies, and predictable models will be reviewed, followed by a perspective on open challenges.

  8. Size limitations for microwave cavity to simulate heating of blanket material in fusion reactor

    International Nuclear Information System (INIS)

    Wolf, D.

    1987-01-01

    The power profile in the blanket material of a nuclear fusion reactor can be simulated by using microwaves at 200 MHz. Using these microwaves, ceramic breeder materials can be thermally tested to determine their acceptability as blanket materials without entering a nuclear fusion environment. A resonating cavity design is employed which can achieve uniform cross sectional heating in the plane transverse to the neutron flux. As the sample size increases in height and width, higher order modes, above the dominant mode, are propagated and destroy the approximation to the heating produced in a fusion reactor. The limits at which these modes develop are determined in the paper

  9. Specification of steam generator, condenser and regenerative heat exchanger materials for nuclear applications

    International Nuclear Information System (INIS)

    Jovasevic, J.V.; Stefanovic, V.M.; Spasic, Z.LJ.

    1977-01-01

    The basic standards specifications of materials for nuclear applications are selected. Seamless Ni-Cr-Fe alloy Tubes (Inconel-600) for steam generators, condensers and other heat exchangers can be employed instead of austenitic stainless steal or copper alloys tubes; supplementary requirements for these materials are given. Specifications of Ni-Cr-Fe alloy plate, sheet and strip for steam generator lower sub-assembly, U-bend seamless copper-alloy tubes for heat exchanger and condensers are also presented. At the end, steam generator channel head material is proposed in the specification for carbon-steel castings suitable for welding

  10. Recovery of palladium, cesium, and selenium from heavy metal alkali borosilicate glass by combination of heat treatment and leaching processes

    Energy Technology Data Exchange (ETDEWEB)

    Xu, Zhanglian; Okada, Takashi, E-mail: t-okada@u-fukui.ac.jp; Nishimura, Fumihiro; Yonezawa, Susumu

    2017-06-05

    Highlights: • A separation technique of both noble and less noble metal from glass is studied. • Via reductive heat treatment, 80% of palladium is extracted in liquid bismuth. • Sodium–potassium-rich materials with cesium and selenium are phase separated. • From the materials, over 80% of cesium and selenium are extracted in water. - Abstract: Reductive heat-treatment and leaching process were applied to a simulated lead or bismuth soda-potash-borosilicate glass with palladium, cesium, and selenium to separate these elements. In the reductive heat treatment, palladium is extracted in liquid heavy metal phase generated by the reduction of the heavy metal oxides, whereas cesium and selenium are concentrated in phase separated Na–K-rich materials on the glass surface. From the materials, cesium and selenium can be extracted in water, and the selenium extraction was higher in the treatment of the bismuth containing glass. The chemical forms of palladium in the glass affected the extraction efficiencies of cesium and selenium. Among the examined conditions, in the bismuth glass treatment, the cesium and selenium extraction efficiencies in water were over 80%, and that of palladium in liquid bismuth was over 80%.

  11. Local total and radiative heat-transfer coefficients during the heat treatment of a workpiece in a fluidised bed

    International Nuclear Information System (INIS)

    Gao, W.M.; Kong, L.X.; Hodgson, P.D.

    2006-01-01

    The heat-transfer coefficients around a workpiece immersed in an electrically heated heat treatment fluidised bed were studied. A suspension probe designed to simulate a workpiece of complex geometry was developed to measure local total and radiative heat-transfer coefficients at a high bed temperature. The probe consisted of an energy-storage region separated by insulation from the fluidised bed, except for the measuring surface, and a multi-thermocouple measurement system. Experiments in the fluidised bed were performed for a fluidising medium of 120-mesh alumina, a wide temperature range of 110-1050 deg. C and a fluidising number range of 1.18-4.24. It was found that the workpiece surface temperature has a more significant effect on heat transfer than the bed temperature. The total heat-transfer coefficient at the upper surface of the workpiece sharply decreased at the start of heating, and then steadily increased as heating progressed, while a sharp decrease became a rapid increase and then a slow increase for the radiative heat-transfer coefficient. A great difference in the heat-transfer coefficients around the workpiece was observed

  12. Shearographic System for Dynamic Analysis of Materials under Heat Stress

    Directory of Open Access Journals (Sweden)

    Nelson A. Correa-Rojas

    2013-11-01

    Full Text Available Shearography is a tool for monitoring and inspecting of structural flaws and imperfections in different types of industrial, automotive and aeronautics applications. It is based on digital correlation of two speckle patterns in two states of interest: with and without load. The technique has the special quality of being very robust against environmental disturbances. We present a shearographic system to analyze the dynamic behavior of the strain that suffers a material in response to changes in temperature throughout the thermal load process.

  13. Experimental study on heat storage system using phase-change material in a diesel engine

    International Nuclear Information System (INIS)

    Park, Sangki; Woo, Seungchul; Shon, Jungwook; Lee, Kihyung

    2017-01-01

    Engines usually use only about 25% of the total fuel energy for power, and the rest is discarded to the cooling water and exhaust gas. Therefore, a technique for utilizing external waste heat is required to improve fuel efficiency in terms of total energy consumption. In this study, a heat storage system was built using a phase-change material in order to recover about 30% of the thermal energy wasted through engine cooling. The components of the heat storage system were divided into phase-change material, a heat exchanger, and a heat-insulating container. For each component, a phase-change material that is suitable for use in vehicles was selected based on the safety, thermal properties, and durability. As a result, a stearic acid of a fatty acid series with natural extracts was determined to be appropriate. In order to measure the reduction in engine fuel consumption, a thermal storage system designed for the actual engine was applied to realize a quick warm-up by releasing stored heat energy directly on the coolant during a cold start. This technique added about 95 calories of heat storage device warm-up time compared to the non-added state, which was reduced by about 18.1% to about 27.1%. - Highlights: • The diesel engine used phase-change material with heat storage system. • The thermal storage system designed for the actual engine. • A stearic acid of a fatty acid series was determined to be appropriate. • Applied heat storage system was reduced by about 18.1%–27.1%.

  14. The effects of heat treatment and environment on corrosion fatigue

    International Nuclear Information System (INIS)

    Ballinger, R.G.; Hwang, I.S.; Elliott, C.K.

    1993-05-01

    Alloy X-750 is a nickel-base alloy used extensively in Light Water Reactor (LWR) nuclear power systems due to its excellent corrosion resistance and high temperature strength. In spite of alloy X-750's exceptional high temperature properties, it has been found to be susceptible to environmentally assisted fatigue and stress corrosion cracking in relatively low temperature aqueous environments such as those that exist in LWR systems. In order to develop a better understanding of the role that microstructure plays in the fatigue behavior of alloy X-750, three thermal treatments were studied. The treatments used were as hot worked + : (1) 24 h at 885 degree C + 20 h at 704 degree C (AH), (2) lh at 982 degree C + 20 h at 704 degree C (BH), and (3) 1 h at 1093 degree C + 20 h at 704 degree C (HTH). Fatigue crack growth tests were conducted at frequencies of 0.1 and 10 Hz in the following aqueous environments: (1) high purity, air saturated water (8 ppM O 2 ) at 93 degree C and 288 degree C, (2) high purity, deoxygenated water (5 ppb O 2 ) at 93 degree C, and (3) simulated BWR water chemistry with hydrogen additions at 288 degree C. Crack growth rate data was collected at constant values of stress intensity factor range (ΔK). The results show that crack growth rates and morphology are a function of ΔK, frequency, thermal treatment and environment. Frequency effects were most significant for the AH material. Crack growth rates generally decrease, for a given value of ΔK, in the BH and HTH materials with the HTH material showing the lowest growth rate

  15. Microstructure evolution during spray rolling and heat treatment of 2124 Al

    Energy Technology Data Exchange (ETDEWEB)

    McHugh, K.M. [Industrial Technology Department, Idaho National Laboratory, Idaho Falls, ID 83415-2050 (United States)], E-mail: kevin.mchugh@inl.gov; Lin, Y.; Zhou, Y.; Johnson, S.B.; Delplanque, J.-P.; Lavernia, E.J. [Department of Chemical Engineering and Materials Science, University of California, Davis, CA 95616 (United States)

    2008-03-25

    Spray rolling is a strip-casting technology that combines elements of spray forming and twin-roll casting. It consists of atomizing molten metal with a high velocity inert gas, quenching the resultant droplets in flight, and directing the spray between mill rolls. In-flight convection heat transfer from atomized droplets and conduction heat transfer at the rolls rapidly remove the metal's latent heat. Hot deformation of the semi-solid material in the rolls results in fully consolidated, rapidly-solidified strip. Spray rolling operates at a higher solidification rate than conventional twin-roll casting and is able to process a broader range of alloys at high production rates. A laboratory-scale strip caster was constructed and used to evaluate the interplay of processing parameters and strip quality for strips up to 200 mm wide and 1.6-6.4 mm thick. This paper examines microstructure evolution during spray rolling and explores how gas-to-metal mass flow ratio influences the microstructure and mechanical properties of spray-rolled 2124 Al. The influences of solution heat treatment and cold rolling on grain structure and constituent particle spheroidization are also examined.

  16. Bedding material affects mechanical thresholds, heat thresholds and texture preference

    Science.gov (United States)

    Moehring, Francie; O’Hara, Crystal L.; Stucky, Cheryl L.

    2015-01-01

    It has long been known that the bedding type animals are housed on can affect breeding behavior and cage environment. Yet little is known about its effects on evoked behavior responses or non-reflexive behaviors. C57BL/6 mice were housed for two weeks on one of five bedding types: Aspen Sani Chips® (standard bedding for our institute), ALPHA-Dri®, Cellu-Dri™, Pure-o’Cel™ or TEK-Fresh. Mice housed on Aspen exhibited the lowest (most sensitive) mechanical thresholds while those on TEK-Fresh exhibited 3-fold higher thresholds. While bedding type had no effect on responses to punctate or dynamic light touch stimuli, TEK-Fresh housed animals exhibited greater responsiveness in a noxious needle assay, than those housed on the other bedding types. Heat sensitivity was also affected by bedding as animals housed on Aspen exhibited the shortest (most sensitive) latencies to withdrawal whereas those housed on TEK-Fresh had the longest (least sensitive) latencies to response. Slight differences between bedding types were also seen in a moderate cold temperature preference assay. A modified tactile conditioned place preference chamber assay revealed that animals preferred TEK-Fresh to Aspen bedding. Bedding type had no effect in a non-reflexive wheel running assay. In both acute (two day) and chronic (5 week) inflammation induced by injection of Complete Freund’s Adjuvant in the hindpaw, mechanical thresholds were reduced in all groups regardless of bedding type, but TEK-Fresh and Pure-o’Cel™ groups exhibited a greater dynamic range between controls and inflamed cohorts than Aspen housed mice. PMID:26456764

  17. Indirect Versus Direct Heating of Sheet Materials: Superplastic Forming and Diffusion Bonding Using Lasers

    Science.gov (United States)

    Jocelyn, Alan; Kar, Aravinda; Fanourakis, Alexander; Flower, Terence; Ackerman, Mike; Keevil, Allen; Way, Jerome

    2010-06-01

    Many from within manufacturing industry consider superplastic forming (SPF) to be ‘high tech’, but it is often criticized as too complicated, expensive, slow and, in general, an unstable process when compared to other methods of manipulating sheet materials. Perhaps, the fundamental cause of this negative perception of SPF, and also of diffusion bonding (DB), is the fact that the current process of SPF/DB relies on indirect sources of heating to produce the conditions necessary for the material to be formed. Thus, heat is usually derived from the electrically heated platens of hydraulic presses, to a lesser extent from within furnaces and, sometimes, from heaters imbedded in ceramic moulds. Recent evaluations of these isothermal methods suggest they are slow, thermally inefficient and inappropriate for the process. In contrast, direct heating of only the material to be formed by modern, electrically efficient, lasers could transform SPF/DB into the first choice of designers in aerospace, automotive, marine, medical, architecture and leisure industries. Furthermore, ‘variable temperature’ direct heating which, in theory, is possible with a laser beam(s) may provide a means to control material thickness distribution, a goal of enormous importance as fuel efficient, lightweight structures for transportation systems are universally sought. This paper compares, and contrasts, the two systems and suggests how a change to laser heating might be achieved.

  18. Influence of lactic acid and post-treatment recovery time on the heat resistance of Listeria monocytogenes.

    Science.gov (United States)

    Omori, Yasuo; Miake, Kiyotaka; Nakamura, Hiromi; Kage-Nakadai, Eriko; Nishikawa, Yoshikazu

    2017-09-18

    The aim of this study was to evaluate the effect of lactic acid (LA) with and without organic material at various post-treatment recovery times on the heat resistance of Listeria monocytogenes (Lm). LA decreased Lm numbers; however, the effect was remarkably attenuated by the presence of organic matter. Five strains of Lm were treated with LA and the listericidal effects were compared. The effect of LA varied depending on the strain, with ≥3.0% (w/w) LA required to kill the Lm strains in a short time. The heat resistance of Lm treated with LA was examined with respect to the time interval between the acid treatment and the subsequent manufacturing step. The heat resistance of Lm was shown to significantly increase during the post-treatment period. Heat tolerance (D value) increased up to 3.4-fold compared with the non-treated control bacteria. RNA sequencing and RT-PCR analyses suggested that several stress chaperones, proteins controlled by RecA and associated with high-temperature survival, were involved in the mechanism of enhanced heat resistance. These results are applicable to manufacturers when LA and heat treatment methods are utilized for the effective control of Lm in foods. Copyright © 2017 The Authors. Published by Elsevier B.V. All rights reserved.

  19. Material and fabrication considerations for the CANDU-PHWR heat transport system

    International Nuclear Information System (INIS)

    Filipovic, A.; Price, E.G.; Barber, D.; Nickerson, J.

    1987-03-01

    CANDU PHWR nuclear systems have used carbon steel material for over 25 years. The accumulated operating experience of over 200 reactor years has proven this unique AECL approach to be both technically and economically attractive. This paper discusses design, material and fabrication considerations for out-reactor heat transport system major components. The contribution of this unique choice of materials and equipment to the outstanding CANDU performance is briefly covered

  20. Determination of Specific Heat Capacity on Composite Shape-Stabilized Phase Change Materials and Asphalt Mixtures by Heat Exchange System.

    Science.gov (United States)

    Ma, Biao; Zhou, Xue-Yan; Liu, Jiang; You, Zhanping; Wei, Kun; Huang, Xiao-Feng

    2016-05-19

    Previous research has shown that composite shape-stabilized phase change material (CPCM) has a remarkable capacity for thermal storage and stabilization, and it can be directly applied to highway construction without leakage. However, recent studies on temperature changing behaviors of CPCM and asphalt mixture cannot intuitively reflect the thermoregulation mechanism and efficiency of CPCM on asphalt mixture. The objective of this paper is to determine the specific heat capacity of CPCM and asphalt mixtures mixed with CPCM using the heat exchange system and the data acquisition system. Studies have shown that the temperature-rise curve of 5 °C CPCM has an obvious temperature plateau, while an asphalt mixture mixed with 5 °C CPCM does not; with increasing temperature, the specific heat capacities of both 5 °C CPCM and asphalt mixture first increase and then decrease, while the variation rate of 5 °C CPCM is larger than that of the asphalt mixture, and the maximum specific heat capacity of 5 °C CPCM appears around the initial phase change temperature. It is concluded that the temperature intervals of 5 °C CPCM are -18 °C-7 °C, 7 °C-25 °C and 25 °C-44 °C, respectively, and that of the asphalt mixture are -18 °C~10 °C, -10 °C~5 °C and 5 °C~28 °C. A low dosage of 5 °C CPCM has little influence on the specific heat capacity of asphalt mixture. Finally, the functions of specific heat capacities and temperature for CPCM and asphalt mixture mixed with CPCM were recommended by the sectional regression method.

  1. Optimization of the heat and mechanical treatment of the Al-Zn-Mg-Li alloy

    Directory of Open Access Journals (Sweden)

    M. Stegliński

    2010-07-01

    Full Text Available In terms of high strength in relation to mass the alloys of aluminium – lithium find more and more use mainly in aircraft industry like inspacecraft. At present intensive investigations are carried out in aim of use of Al – Li in automotive industry in particular to components subject to fatigue wear. It could contribute to replace transmission’s elements made from traditional materials by aluminium - lithium alloys. However low resistance to wear due to forming of thin Al2O3 layer which is reproducing in friction contact disqualifies using aluminium alloys in friction contact. From this point of view first stage of investigation was to enhance hardness properties of the substrate by applying thermo-mechanical treatment.In this article the results of heat treatment of Al-Zn-Mg-Li alloy were presented. During investigations optimum parameters (timetemperature of the solution heat treatment were elaborated. Micro hardness on the cross-section were investigated. Phase, chemicalcomposition and morphology were determined. It was found that hardness after thermo-mechanical treatment of Al-Zn-Mg-Li is about20% higher than for AlCu4Mg1 (7075 –T6 alloy.

  2. Copper matrix composites as heat sink materials for water-cooled divertor target

    Directory of Open Access Journals (Sweden)

    Jeong-Ha You

    2015-12-01

    Full Text Available According to the recent high heat flux (HHF qualification tests of ITER divertor target mock-ups and the preliminary design studies of DEMO divertor target, the performance of CuCrZr alloy, the baseline heat sink material for DEMO divertor, seems to only marginally cover the envisaged operation regime. The structural integrity of the CuCrZr heat sink was shown to be affected by plastic fatigue at 20 MW/m². The relatively high neutron irradiation dose expected for the DEMO divertor target is another serious concern, as it would cause significant embrittlement below 250 °C or irradiation creep above 350 °C. Hence, an advanced design concept of the divertor target needs to be devised for DEMO in order to enhance the HHF performance so that the structural design criteria are fulfilled for full operation scenarios including slow transients. The biggest potential lies in copper-matrix composite materials for the heat sink. In this article, three promising Cu-matrix composite materials are reviewed in terms of thermal, mechanical and HHF performance as structural heat sink materials. The considered candidates are W particle-reinforced, W wire-reinforced and SiC fiber-reinforced Cu matrix composites. The comprehensive results of recent studies on fabrication technology, design concepts, materials properties and the HHF performance of mock-ups are presented. Limitations and challenges are discussed.

  3. Material Research on Salt Hydrates for Seasonal Heat Storage Application in a Residential Environment

    Energy Technology Data Exchange (ETDEWEB)

    Ferchaud, C.J.; Zondag, H.A.; De Boer, R. [ECN Biomass and Energy Efficiency, Petten (Netherlands)

    2013-09-15

    Water vapor sorption in salt hydrates is a promising method to realize seasonal solar heat storage in the residential sector. Several materials already showed promising performance for this application. However, the stability of these materials needs to be improved for long-term (30 year) application in seasonal solar heat storages. The purpose of this article is to identify the influence of the material properties of the salt hydrates on the performance and the reaction kinetics of the sorption process. The experimental investigation presented in this article shows that the two salt hydrates Li2SO4.H2O and CuSO4.5H2O can store and release heat under the operating conditions of a seasonal solar heat storage in a fully reversible way. However, these two materials show differences in terms of energy density and reaction kinetics. Li2SO4.H2O can release heat with an energy density of around 0.80 GJ/m{sup 3} within 4 hours of rehydration at 25C, while CuSO4.5H2O needs around 130 hours at the same temperature to be fully rehydrated and reaches an energy density of 1.85 GJ/m{sup 3}. Since the two salts are dehydrated and hydrated under the same conditions, this difference in behavior is directly related to the intrinsic properties of the materials.

  4. Treatment and storage of contaminated materials

    International Nuclear Information System (INIS)

    Cerre, P.; Pomarola, J.

    1959-01-01

    The ultimate disposal of radioactive wastes sets an important problem which has been partly solved. France has temporarily adopted the following method: 1) Volume reduction, 2) Fixation of the activity in non leakable solids standing all temporarily or ultimate kinds of storing. According to those two basic principles the authors have presented: - a decontamination plant allowing maximum recovery of materials, - the plans of an installation devised for carrying out radioactive waste volume reduction and conditioning. Both of them are being built at Saclay. (author) [fr

  5. Apparatus for dynamic measurement of gases released from materials heated under programmed temperature-time control

    International Nuclear Information System (INIS)

    Early, J.W.; Abernathey, R.M.

    1982-04-01

    This apparatus, a prototype of one being constructed for hotcell examination of irradiated nuclear materials, measures dynamic release rates and integrated volumes of individual gases from materials heated under controlled temperature-time programs. It consists of an inductively heated vacuum furnace connected to a quadrupole mass spectrometer. A computerized control system with data acquisition provides scanning rates down to 1s and on-line tabular and graphic displays. Heating rates are up to 1300 0 C/min to a maximum temperature of 2000 0 C. The measurement range is about 10 -6 to 10 -2 torr-liter/s for H 2 , CH 4 , H 2 O, N 2 , and CO and 10 -8 to 10 -2 torr-liter/s for He, Kr, and Xe. Applications are described for measurements of Kr and Xe in mixed oxide fuel, various gases in UO 2 pellets, and He in 238 PuO 2 power and heat sources

  6. Fusion surface material melting, ablation, and ejection under high heat loading

    International Nuclear Information System (INIS)

    Holliday, M.R.; Doster, J.M.; Gilligan, J.G.

    1986-01-01

    Limiters, divertor plates, and sections of the first wall are exposed to intense heat loads during normal operation and plasma disruptions. This results in severe thermal stresses as well as erosion of the surface material. Large surface areas of compact high-field tokamaks are expected to be exposed to these high heat loads. The need for a fast and accurate computational model describing the heat transfer and phase change process has arisen as a part of the larger model of the plasma-edge region. The authors report on a solution scheme that has been developed that minimizes computational time for this time-dependent, one-dimensional, moving boundary problem. This research makes use of the heat balance integral technique, which is at least an order of magnitude faster than previous finite difference techniques. In addition, we report on the effect of molten material ejection (by external forces) on the total surface erosion rate

  7. Simultaneous Heat and Mass Transfer Model for Convective Drying of Building Material

    Science.gov (United States)

    Upadhyay, Ashwani; Chandramohan, V. P.

    2018-04-01

    A mathematical model of simultaneous heat and moisture transfer is developed for convective drying of building material. A rectangular brick is considered for sample object. Finite-difference method with semi-implicit scheme is used for solving the transient governing heat and mass transfer equation. Convective boundary condition is used, as the product is exposed in hot air. The heat and mass transfer equations are coupled through diffusion coefficient which is assumed as the function of temperature of the product. Set of algebraic equations are generated through space and time discretization. The discretized algebraic equations are solved by Gauss-Siedel method via iteration. Grid and time independent studies are performed for finding the optimum number of nodal points and time steps respectively. A MATLAB computer code is developed to solve the heat and mass transfer equations simultaneously. Transient heat and mass transfer simulations are performed to find the temperature and moisture distribution inside the brick.

  8. Heat exchanger tubing materials for CANDU nuclear generating stations

    International Nuclear Information System (INIS)

    Taylor, G.F.

    1977-07-01

    The performance of steam generator tubing (nickel-chromium-iron alloy in NPD and nickel-copper alloy in Douglas Point and Pickering generating stations) has been outstanding and no corrosion-induced failures have occurred. The primary coolant will be allowed to boil in the 600 MW (electrical) CANDU-PHW reactors. An iron-nickel-chromium alloy has been selected for the steam generator tubing because it will result in lower radiation fields than the alloys used before. It is also more resistant than nickel-chromium-iron alloy to stress corrosion cracking in the high purity water of the primary circuit, an unlikely but conceivable hazard associated with higher operating temperatures. Austenitic alloy and ferritic-austenitic stainless steel tubing have been selected for the moderator coolers in CANDU reactors being designed and under construction. These materials will reduce the radiation fields around the moderator circuit while retaining the good resistance to corrosion in service water that has characterized the copper-nickel alloys now in use. Brass and bronze tubes in feedwater heaters and condensers have given satisfactory service but do, however, complicate corrosion control in the steam cycle and, to reduce the transport of corrosion products from the feedtrain to the steam generator, stainless steel is preferred for feedwater heaters and stainlss steel or titanium for condensers. (author)

  9. Manufacturing of tailored tubes with a process integrated heat treatment

    Science.gov (United States)

    Hordych, Illia; Boiarkin, Viacheslav; Rodman, Dmytro; Nürnberger, Florian

    2017-10-01

    The usage of work-pieces with tailored properties allows for reducing costs and materials. One example are tailored tubes that can be used as end parts e.g. in the automotive industry or in domestic applications as well as semi-finished products for subsequent controlled deformation processes. An innovative technology to manufacture tubes is roll forming with a subsequent inductive heating and adapted quenching to obtain tailored properties in the longitudinal direction. This processing offers a great potential for the production of tubes with a wide range of properties, although this novel approach still requires a suited process design. Based on experimental data, a process simulation is being developed. The simulation shall be suitable for a virtual design of the tubes and allows for gaining a deeper understanding of the required processing. The model proposed shall predict microstructural and mechanical tube properties by considering process parameters, different geometries, batch-related influences etc. A validation is carried out using experimental data of tubes manufactured from various steel grades.

  10. 5. International conference on materials science and condensed matter physics and symposium 'Electrical methods of materials treatment'. Abstracts

    International Nuclear Information System (INIS)

    2010-09-01

    This book includes abstracts of the communications presented at the 5th International Conference on Materials Science and Condensed-Matter Physics and at the Symposium dedicated to the 100th anniversary of academician Boris Lazarenko, the prominent scientist and inventor, the first director of the Institute of Applied Physics of the Academy of Sciences of Moldova. The abstracts presented in the book cover a vast range of subjects, such as: advanced materials and fabrication processes; methods of crystal growth, post-growth technological processes, doping and implantation, fabrication of solid state structures; defect engineering, engineering of molecular assembly; methods of nanostructures and nano materials fabrication and characterization; quantum wells and superlattices; nano composite, nanowires and nano dots; fullerenes and nano tubes, molecular materials, meso- and nano electronics; methods of material and structure characterization; structure and mechanical characterization; optical, electrical, magnetic and superconductor properties, transport processes, nonlinear phenomena, size and interface effects; advances in condensed matter theory; theory of low dimensional systems; modelling of materials and structure properties; development of theoretical methods of solid-state characterization; phase transition; advanced quantum physics for nano systems; device modelling and simulation, device structures and elements; micro- and optoelectronics; photonics; microsensors and micro electro-mechanical systems; microsystems; degradation and reliability, solid-state device design; theory and advanced technologies of electro-physico-chemical and combined methods of materials machining and treatment, including modification of surfaces; theory and advanced technologies of using electric fields, currents and discharges so as to intensify heat mass-transfer, to raise the efficiency of treatment of materials, of biological preparations and foodstuff; modern equipment for

  11. Transient cooling of electronics using phase change material (PCM)-based heat sinks

    International Nuclear Information System (INIS)

    Kandasamy, Ravi; Wang Xiangqi; Mujumdar, Arun S.

    2008-01-01

    Use of a phase change material (PCM)-based heat sink in transient thermal management of plastic quad flat package (QFP) electronic devices was investigated experimentally and numerically. Results show that increased power inputs enhance the melting rate as well as the thermal performance of the PCM-based heat sinks until the PCM is fully melted. A three-dimensional computational fluid dynamics model was proposed to simulate the problem and demonstrated good agreement with experimental data. Results indicate the potential for PCM-based heat sinks for use in intermittent-use devices

  12. Effect of standard heat treatment on the microstructure and mechanical properties of hot isostatically pressed superalloy inconel 718

    International Nuclear Information System (INIS)

    Rao, G. Appa; Kumar, Mahendra; Srinivas, M.; Sarma, D.S.

    2003-01-01

    Ni-Fe base superalloy, Inconel 718, was processed through powder metallurgy (P/M) hot isostatic pressing (HIP) route. In order to balance the strength and ductility, the HIPed material was given the standard heat treatment, viz. solution treatment at 980 deg. C for 1 h/water quenched (WQ) to room temperature and a two-step ageing treatment consisting of 720 deg. C for 8 h/furnace cooling (FC) at 55 deg. C h -1 to 620 deg. C and holding at 620 deg. C for 8 h before air cooling (AC) to room temperature. Optical microscopy and scanning electron microscopy (SEM) studies on the heat treated alloy have shown a homogeneous microstructure with fine grain size (25 μm) along with the presence of prior particle boundary (PPB) networks. Transmission electron microscopy (TEM) on the heat treated material has revealed the presence of oxides, MC carbides and δ-precipitates at the grain boundaries and a uniform precipitation of fine γ'' and γ' strengthening phases in the matrix. Tensile and stress rupture tests were performed on the heat treated material. While the yield strength (YS) and ultimate tensile strength (UTS) of the HIPed and heat treated alloy at room temperature and 650 deg. C were comparable to those of conventionally processed wrought IN 718, its ductility was lower. The stress rupture life of the HIPed alloy improved marginally due to heat treatment and met the minimum specification requirement of life hours but the rupture ductility was found to be inferior to that of the wrought material. The fractography of the failed samples has revealed the transgranular ductile mode of fracture in the as-solution treated alloy, while intergranular mode of failure with the decohesion of PPBs occurred more predominantly in the aged condition. This change of fracture mode with ageing treatment shows the ductility dependence on the relative strength of the matrix and PPBs. The TEM studies on the deformed alloy have revealed that the brittle oxides and carbides at the prior

  13. Melting of a phase change material in a horizontal annulus with discrete heat sources

    Directory of Open Access Journals (Sweden)

    Mirzaei Hooshyar

    2015-01-01

    Full Text Available Phase change materials have found many industrial applications such as cooling of electronic devices and thermal energy storage. This paper investigates numerically the melting process of a phase change material in a two-dimensional horizontal annulus with different arrangements of two discrete heat sources. The sources are positioned on the inner cylinder of the annulus and assumed as constant-temperature boundary conditions. The remaining portion of the inner cylinder wall as well as the outer cylinder wall is considered to be insulated. The emphasis is mainly on the effects of the arrangement of the heat source pair on the fluid flow and heat transfer features. The governing equations are solved on a non-uniform O type mesh using a pressure-based finite volume method with an enthalpy porosity technique to trace the solid and liquid interface. The results are obtained at Ra=104 and presented in terms of streamlines, isotherms, melting phase front, liquid fraction and dimensionless heat flux. It is observed that, depending on the arrangement of heat sources, the liquid fraction increases both linearly and non-linearly with time but will slow down at the end of the melting process. It can also be concluded that proper arrangement of discrete heat sources has the great potential in improving the energy storage system. For instance, the arrangement C3 where the heat sources are located on the bottom part of the inner cylinder wall can expedite the melting process as compared to the other arrangements.

  14. Selection of engineering materials for heat exchangers (An expert system approach)

    International Nuclear Information System (INIS)

    Ahmed, K.; Abou-Ali, M.; Bassuni, M.

    1997-01-01

    The materials selection as a part of the design process of the heat exchangers is one of the most important steps in the whole industry. The clear recognition of the service requirements of the different types of the heat exchangers is very important to select the adequate and economic materials to meet such requirements. of course the manufacturer should ensure that failure does not occur in service specially it is one of the main and fetal component of the nuclear reactor, pressurized water type (PWR). It is necessary to know the possible mechanisms of failure. Also the achievement of the materials selection using the expert system approach in the process sequence of heat exchanger manufacturing is introduced. Different parameters and requirements controlling each process and the linkage between these parameters and the final product will be shown. 2 figs., 3 tabs

  15. Nanostructured Thermoelectric Oxide Materials for Effective Power Generation from Waste Heat

    DEFF Research Database (Denmark)

    Van Nong, Ngo; Pryds, Nini

    A large amount of thermal energy that emitted from many industrial processes is available as waste heat. It is difficult to reclaim this heat due to the dispersed nature and relative smallness of its sources. Thermoelectric conversion can offer a very promising method to overcome these difficulties...... by converting heat directly into electricity. However, the requirements for this task place in the materials are not easily satisfied by the conventional thermoelectric materials. Not only they must possess a high thermoelectric performance, they should also be stable at high temperatures and be composed...... of nontoxic and low-cost elements, and must be able to be processed and shaped cheaply. Oxides are among the strongest candidate materials for this purpose, and recently they have been intensively investigated and developed [1-5]. In this report, the development progress of two state-of-the-art p-type Ca3Co4O...

  16. Effect of heat-treatment on toughness and strength properties of C-Mn steel

    International Nuclear Information System (INIS)

    Mohd bin Harun; Goh Kian Seong; Jasmin binti Baba

    1991-01-01

    The strength and toughness of the heat-treated and tempered C-Mn are studied. Two types of heat-treatment have been carried out with the specimens in an argon gas. The variation in the fracture surfaces of the heat-treated and tempered specimens with impact test temperature is discussed also

  17. Effect of heat treatment of toughness and strength properties of C-Mn steel

    International Nuclear Information System (INIS)

    Mohamad bin Harun; Goh Kian Seong; Yasmin binti Baba

    1989-01-01

    The strength and toughness of the heat-treated and tempered C-Mn are studied. Two type of heat-treatments have been carried out with the specimens in an argon gas. The variation in the fracture surfaces of the heat-treated and tempered specimens with impact test temperatures also is discussed. (author)

  18. Structure and strength of carbide-steel cermet and their changes during heat treatment

    International Nuclear Information System (INIS)

    Dariel, M.P.; Frage, N.R.; Kaputkina, L.M.; Kaputkin, D.M.; Sverdlova, N.R.

    2004-01-01

    Both homogeneous and 'graded' materials were produced by pressing and sintering of titanium carbide TiC x (0.7 x takes place during the joining. If the titanium carbide is carbon deficient that the carbon goes from the steel binder to TiC x , and this redistribution intensity with the x decreases. So-named graded cermets were produced on controlled distribution of TiC x with different x. An additional flow of carbon from C-rich to C-poor TiC x layers was obtained in these cermets. These changes both in the steel and TiC x compositions result in changes in such processes as austenitization, carbide dissolution and precipitation, and martensitic transformation. Both general strength of the material and the gradient of properties in graded cermets can be increased using kinetic factors of element redistribution and structure changes resulted from the heat treatment. (author)

  19. Calculation and Designing of Up-to-Date Gas-Flame Plants for Metal Heating and Heat Treatment

    Directory of Open Access Journals (Sweden)

    V. I. Тimoshpolsky

    2008-01-01

    Full Text Available An analysis of development trends in the CIS machine-building industry and current status of the heating and heat treatment furnaces of main machine-building enterprises of the Republic of Belarus as of the 1st quarter of 2008 is given in the paper.The paper presents the most efficient engineering solutions from technological and economic point of view that concern calculation and designing of up-to-date gas-flame plants which are to be applied for modernization of the current heating and heat treatment furnaces of the machine-building enterprises in the Republic of Belarus.A thermo-technical calculation of main indices of the up-to-date gas-flame plant has been carried out in the paper.

  20. Microstructural evolution of aluminide coatings on Eurofer during heat treatments

    International Nuclear Information System (INIS)

    Bhanumurthy, K.; Krauss, W.; Konys, J.

    2011-01-01

    Development of ceramic coatings are essential for the realization of Demo fusion reactor beyond ITER. These functional coatings have to be stable at high temperatures, provide insulating coatings to reduce MHD effects and also act as corrosion barriers to reduce tritium permeation. Some of important development of high temperature coatings are CVD process, powder slurry coatings, hot-dip aluminization and plasma detonation jet processes. Recently Galvono-Al (ECA) process is being used for depositing Al from organic electrolyte, where Al is existing as an toluol-based Al(C x H y ) complex. The deposit is performed under Ar cover gas at 100 deg C with a deposit rate of 10-12 μm/hr. This process is suitable for coating large and complex shaped assemblies and is a well established industrial process for coating Al for wide range of applications including automobile industry. In order to study the effect of high temperature on these coatings, few Al coated on Eurofer specimens were obtained from M/s. Rasant-Alcotec, Germany. The thickness of these coating is around 20 μm. The objective of the presents studies is to subject these coatings to standard heat treatment schedule of Eurofer and study the evolution of microchemistry and microstructure

  1. Do encapsulated heat storage materials really retain their original thermal properties?

    Science.gov (United States)

    Chaiyasat, Preeyaporn; Noppalit, Sayrung; Okubo, Masayoshi; Chaiyasat, Amorn

    2015-01-14

    The encapsulation of Rubitherm®27 (RT27), which is one of the most common commercially supplied heat storage materials, by polystyrene (PS), polydivinyl benzene (PDVB) and polymethyl methacrylate (PMMA) was carried out using conventional radical microsuspension polymerization. The products were purified to remove free RT27 and free polymer particles without RT27. In the cases of PS and PDVB microcapsules, the latent heats of melting and crystallization for RT27 ( and , J/g-RT27) were clearly decreased by the encapsulation. On the other hand, those of the PMMA microcapsules were the same as pure RT27. A supercooling phenomenon was observed not only for PS and PDVB but also for the PMMA microcapsules. These results indicate that the thermal properties of the heat storage materials encapsulated depend on the type of polymer shells, i.e., encapsulation by polymer shell changes the thermal properties of RT27. This is quite different from the idea of other groups in the world, in which they discussed the thermal properties based on the ΔHm and ΔHc values expressed in J/g-capsule, assuming that the thermal properties of the heat storage materials are not changed by the encapsulation. Hereafter, this report should raise an alarm concerning the "wrong" common knowledge behind developing the encapsulation technology of heat storage materials.

  2. Thermal effects on transducer material for heat assisted magnetic recording application

    Energy Technology Data Exchange (ETDEWEB)

    Ji, Rong, E-mail: Ji-Rong@dsi.a-star.edu.sg; Xu, Baoxi; Cen, Zhanhong; Ying, Ji Feng; Toh, Yeow Teck [Data Storage Institute, Agency for Science, Technology and Research (A-STAR), 5 Engineering Drive 1, Singapore 117608 (Singapore)

    2015-05-07

    Heat Assisted Magnetic Recording (HAMR) is a promising technology for next generation hard disk drives with significantly increased data recording capacities. In HAMR, an optical near-field transducer (NFT) is used to concentrate laser energy on a magnetic recording medium to fulfill the heat assist function. The key components of a NFT are transducer material, cladding material, and adhesion material between the cladding and the transducer materials. Since transducer materials and cladding materials have been widely reported, this paper focuses on the adhesion materials between the Au transducer and the Al{sub 2}O{sub 3} cladding material. A comparative study for two kinds of adhesion material, Ta and Cr, has been conducted. We found that Ta provides better thermal stability to the whole transducer than Cr. This is because after thermal annealing, chromium forms oxide material at interfaces and chromium atoms diffuse remarkably into the Au layer and react with Au to form Au alloy. This study also provides insights on the selection of adhesion material for HAMR transducer.

  3. Heat transfer characteristics of coconut oil as phase change material to room cooling application

    Science.gov (United States)

    Irsyad, M.; Harmen

    2017-03-01

    Thermal comfort in a room is one of human needs in the workplace and dwellings, so that the use of air conditioning system in tropical countries is inevitable. This equipment has an impact on the increase of energy consumption. One method of minimizing the energy use is by using the phase change material (PCM) as thermal energy storage. This material utilizes the temperature difference between day and night for the storage and release of thermal energy. PCM development on application as a material for air cooling inlet, partitioning and interior needs to be supported by the study of heat transfer characteristics when PCM absorbs heat from ambient temperature. This study was conducted to determine the heat transfer characteristics on coconut oil as a phase change material. There are three models of experiments performed in this research. Firstly, an experiment was conducted to analyze the time that was needed by material to phase change by varying the temperature. The second experiment analyzed the heat transfer characteristics of air to PCM naturally convection. The third experiment analyzed the forced convection heat transfer on the surface of the PCM container by varying the air velocity. The data of experimental showed that, increasing ambient air temperature resulted in shorter time for phase change. At temperatures of 30°C, the time for phase change of PCM with the thickness of 8 cm was 1700 min, and it was stable at temperatures of 27°C. Increasing air temperature accelerated the phase change in the material. While for the forced convection heat transfer, PCM could reduce the air temperature in the range of 30 to 35°C at about 1 to 2°C, with a velocity of 1-3 m/s.

  4. Effects of Microencapsulated Phase Change Material (MPCM) on Critical Heat Flux in Pool Boiling

    International Nuclear Information System (INIS)

    Park, Sung Dae; Kim, Seong Man; Kang, Sarah; Lee, Seung Won; Seo, Han; Bang, In Cheol

    2011-01-01

    Thermal power is limited by critical heat flux (CHF) in the nuclear power plant. And the in-vessel retention by external reactor vessel cooling (IVR-ERVC) is applied in some nuclear power plants; AP600, AP1000, Loviisa and APR1400. The heat removal capacity of IVR-ERVC is also restricted by CHF. So, it is essential to get CHF margin to improve an economics and a safety of the plant. There are some typical approaches to enhance CHF: vibrating the heater or fluid, coating with porous media on the heater surface, applying an electric field. The recent study related to the CHF is focus on using the nanofluid. In this paper, the new approach was investigated by using the microencapsulated phase change material (MPCM). MPCM is the particles whose diameter is from 0.1μm to 1000μm. The MPCM consists of the core material and the shell material. The core material can be solid, liquid, gas or even the mixture. The solid paraffin is the best candidate as the core material due to its stable chemical and thermal properties. And the shell material is generally synthesized polymer of about several micrometers in thickness. The most interesting feature of the MPCM is that the latent heat associated with the solid-liquid phase change is related to the heat transfer. When the MPCM is dispersed into the carrier fluid, a kind of suspension named as microencapsulated phase change slurry (MPCS) is formed. The study on the MPCS was conducted in field of both the heat transfer fluids and energy storage media. It is inspired by the fact that the latent heat can serve distribution to the additional CHF margin. The purpose of this work is to confirm whether or not the CHF is enhanced

  5. Pitch-based carbon foam heat sink with phase change material

    Science.gov (United States)

    Klett, James W.; Burchell, Timothy D.

    2004-08-24

    A process for producing a carbon foam heat sink is disclosed which obviates the need for conventional oxidative stabilization. The process employs mesophase or isotropic pitch and a simplified process using a single mold. The foam has a relatively uniform distribution of pore sizes and a highly aligned graphic structure in the struts. The foam material can be made into a composite which is useful in high temperature sandwich panels for both thermal and structural applications. The foam is encased and filled with a phase change material to provide a very efficient heat sink device.

  6. Heat applied chitosan treatment on hardwood chips to improve physical and mechanical properties of particleboard

    Directory of Open Access Journals (Sweden)

    Mehmet Altay Basturk

    2012-11-01

    Full Text Available High-heat treatment after surface application of chitosan was used in an effort to improve physical and mechanical performances of particleboard. Particleboard is mainly used in the furniture industry and also used as a home decoration material; however, it has a poor dimensional stability. In this work, hardwood chips were obtained from a commercial plant; half of the chips were used for the control panels without chitosan treatment, and the other half were treated with chitosan acetate solutions (2% wt. Those chitosan-treated particles were also exposed to extra high-heat (140oC treatment for 90 minutes to convert chitosan acetate back to chitin. Liquid phenol-formaldehyde resin was sprayed onto dry particles at a level of 6 and 7% (wt based upon oven-dry weight. The mat was pressed (200oC for 11 minutes to form 19 mm thickness and a target of 0.63 g cm-3 density panels. Thickness swelling, linear expansion, and water gain of the treated panels were reduced over untreated panels during a 24-hour water-soak test. In addition, chitosan-treated panels showed better internal bond strength than control panels. Static bending test results showed a negative effect for the chitosan treated particleboard.

  7. Heat treatment versus properties studies associated with the Inconel 718 PBF acoustic filters

    International Nuclear Information System (INIS)

    Smolik, G.R.; Reuter, W.G.

    1975-01-01

    PBF acoustic filter Unit No. 1 cracked when heat treatment was attempted. The effects of prior thermal cycling, solution anneal temperature, and cooling rate from solution anneals were investigated. The investigations concerned influences of the above variables upon both 1400 0 F stress rupture solution-annealed properties and room temperature age-hardened properties. 1400 0 F stress rupture properties were of interest to assist the prevention of cracking during heat treatments. Room temperature age-hardened properties were needed to ensure that design requirement would be provided. Prior thermal cycling was investigated to determine if extra thermal cycles would be detrimental to the repaired filter. Slow furnace cools were considered as a means of reducing thermal stresses. Effects of solution annealing at 2000 and 1900 0 F were also determined. Test results showed that slow cooling rates would not only reduce thermal stresses but also improve 1400 0 F ductility. A modified aging treatment was established which provided the required 145 ksi room temperature yield strength for the slowly cooled material. Prior cooling did not degrade final age-hardened room temperature tensile or impact properties

  8. Analytical description of the effects of melting practice and heat treatment on the creep properties of a 2 1/4 Cr-1 Mo steel

    International Nuclear Information System (INIS)

    Booker, M.K.

    1977-01-01

    2 1 / 4 Cr-1 Mo steel is used worldwide as an elevated-temperature structural material, particularly in steam generation systems. Since this material is often used at service temperatures up to 600 0 C, successful design requires a consideration of its creep properties. Unfortunately, the development of an analytical description of the creep behavior of 2 1 / 4 Cr-1 Mo steel is complicated by two phenomena. First, the creep strength of this material is quite sensitive to heat treatment. Second, this material tends to exhibit nonclassical creep under some conditions. In addition, especially in nuclear applications, the material used may be air-melted, vacuum-arc remelted (VAR), or electroslag remelted (ESR). Available creep data from air-melted, VAR, and ESR material have been analyzed. Heat treatments included both annealed and isothermally annealed, with and without a subsequent ''postweld'' heat treatment. It has been found that the elevated-temperature ultimate tensile strength (UTS) is a useful indicator of creep strength for a given heat of material regardless of melting practice or heat treatment. Meanwhile, the nonclassical creep behavior has been attributed to a change in creep mechanism which has been mathematically modeled

  9. Influence of heat treatment on microstructure and properties of bainitic cast steel used for frogs in railway crossovers

    Directory of Open Access Journals (Sweden)

    E. Tasak

    2010-01-01

    Full Text Available This work deals with influence of heat treatment on microstructure and properties of sample cast assigned as a material used for frogs in railway crossover. Materials used in railway industry for frogs (manganese cast steel and forged pearlitic steel do not fulfil strict conditions of exploitation of railway. One of the solutions is using cast steel with bainitic or bainite-martensite microstructure, what allows to gain high resistance properties (Rm = 1400 MPa, Rp0,2 = 900 MPa, hardness to 400 HBW. The cooling rates of rail type UIC60 shows that it is possible to reach the bainitic microstructure in cast of frog. The microstructure of lower banite should have an advantageous influence on cracking resistance. In order to set the parameters of heat treatment, the critical temperatures were determined by dilatometric methods determined. This heat treatment consisted of normalizing that prepared it to the farther process of resistance welding. Moreover, the CCT diagram of proposed bainitic cast steel was prepared. The exams were done that can be used to evaluate the influence of heat treatment on microstructure and properties of the sample cast.

  10. Processing and refinement of steel microstructure images for assisting in computerized heat treatment of plain carbon steel

    Science.gov (United States)

    Gupta, Shubhank; Panda, Aditi; Naskar, Ruchira; Mishra, Dinesh Kumar; Pal, Snehanshu

    2017-11-01

    Steels are alloys of iron and carbon, widely used in construction and other applications. The evolution of steel microstructure through various heat treatment processes is an important factor in controlling properties and performance of steel. Extensive experimentations have been performed to enhance the properties of steel by customizing heat treatment processes. However, experimental analyses are always associated with high resource requirements in terms of cost and time. As an alternative solution, we propose an image processing-based technique for refinement of raw plain carbon steel microstructure images, into a digital form, usable in experiments related to heat treatment processes of steel in diverse applications. The proposed work follows the conventional steps practiced by materials engineers in manual refinement of steel images; and it appropriately utilizes basic image processing techniques (including filtering, segmentation, opening, and clustering) to automate the whole process. The proposed refinement of steel microstructure images is aimed to enable computer-aided simulations of heat treatment of plain carbon steel, in a timely and cost-efficient manner; hence it is beneficial for the materials and metallurgy industry. Our experimental results prove the efficiency and effectiveness of the proposed technique.

  11. Heat treatment device for extending the life of a pressure vessel, particularly a reactor pressure vessel

    International Nuclear Information System (INIS)

    Krauss, P.; Mueller, E.; Poerner, H.; Weber, R.

    1979-01-01

    A support body in the form of an insulating cylinder is tightly sealed by connected surfaces at its outer circumference to the inner wall of the pressure vessel. It forms an annular heating space. The heat treatment or tempering of the pressure vessel takes place with the reactor space empty and screened from the outside by ceiling bolts. Heating gas or an induction winding can be used as the means of heating. (DG) [de

  12. Transient modelling of heat loading of phase change material for energy storage

    Directory of Open Access Journals (Sweden)

    Asyraf W.M.

    2017-01-01

    Full Text Available As the development of solar energy is getting advance from time to time, the concentration solar technology also get the similar attention from the researchers all around the globe. This technology concentrate a large amount of energy into main spot. To collect all the available energy harvest from the solar panel, a thermal energy storage is required to convert the heat energy to one of the purpose such as electrical energy. With the idea of energy storage application that can be narrow down to commercial application such as cooking stove. Using latent heat type energy storage seem to be appropriate with the usage of phase change material (PCM that can release and absorb heat energy at nearly constant temperature by changing its state. Sodium nitrate (NaNO3 and potassium nitrate (KNO3 was selected to use as PCM in this project. This paper focus on the heat loading process and the melting process of the PCM in the energy storage using a computer simulation. The model of the energy storage was created as solid three dimensional modelling using computer aided software and the geometry size of it depend on how much it can apply to boil 1 kg of water in cooking application. The materials used in the tank, heat exchanger and the heat transfer fluid are stainless steel, copper and XCELTHERM MK1, respectively. The analysis was performed using a commercial simulation software in a transient state. The simulation run on different value of velocity but kept controlled under laminar state only, then the relationship of velocity and heat distribution was studied and the melting process of the PCM also has been analyzed. On the effect of heat transfer fluid velocity, the higher the velocity resulted in higher the rate of heat transfer. The comparison between the melting percentages of the PCMs under test conditions show that NaNO3 melts quite faster than KNO3.

  13. Integral analysis of debris material and heat transport in reactor vessel lower plenum

    International Nuclear Information System (INIS)

    Suh, K.Y.; Henry, R.E.

    1994-01-01

    An integral, fast-running, two-region model has been developed to characterize the debris material and heat transport in the reactor lower plenum under severe accident conditions. The debris bed is segregated into the oxidic pool and an overlying metallic layer. Debris crusts can develop on three surfaces: the top of the molten pool, the RPV wall, and the internal structures. To account for the decay heat generation, the crust temperature profile is assumed to be parabolic. The oxidic debris pool is homogeneously mixed and has the same material composition, and hence the same thermophysical properties, as the crusts, while the metallic constituents are assumed to rise to the top of the debris pool. Steady-state relationships are used to describe the heat transfer rates, with the assessment of solid or liquid state, and the liquid superheat in the pool being based on the average debris temperature. Natural convection heat transfer from the molten debris pool to the upper, lower and embedded crusts is calculated based on the pool Rayleigh number with the conduction heat transfer from the crusts being determined by the crust temperature profile. The downward heat flux is transferred to the lowest part of the RPV lower head through a crust-to-RPV contact resistance. The sideward heat flux is transferred to the upper regions of the RPV lower head as well as to the internal structures. The upward heat flux goes to the metal layer, water, or available heat sink structures above. Quenching due to water ingression is modeled separately from the energy transfer through the crust. The RPV wall temperature distribution and the primary system pressure are utilized to estimate challenges to the RPV integrity. ((orig.))

  14. Effect of heat treatment on the microstructure and properties of Ni based soft magnetic alloy.

    Science.gov (United States)

    Li, Chunhong; Ruan, Hui; Chen, Dengming; Li, Kejian; Guo, Donglin; Shao, Bin

    2018-04-20

    A Ni-based alloy was heat treated by changing the temperature and ambient atmosphere of the heat treatment. Morphology, crystal structure, and physical performance of the Ni-based alloy were characterized via SEM, XRD, TEM, and PPMS. Results show that due to the heat treatment process, the grain growth of the Ni-based alloy and the removal of impurities and defects are promoted. Both the orientation and stress caused by rolling are reduced. The permeability and saturation magnetization of the alloy are improved. The hysteresis loss and coercivity are decreased. Higher heat treatment temperature leads to increased improvement of permeability and saturation magnetization. Heat treatment in hydrogen is more conducive to the removal of impurities. At the same temperature, the magnetic performance of the heat-treated alloy in hydrogen is better than that of an alloy with heat treatment in vacuum. The Ni-based alloy shows an excellent magnetic performance on 1,373 K heat treatment in hydrogen atmosphere. In this process, the µ m , B s , P u , and H c of the obtained alloy are 427 mHm -1 , 509 mT, 0.866 Jm -3 , and 0.514 Am -1 , respectively. At the same time, the resistivity of alloy decreases and its thermal conductivity increases in response to heat treatment. © 2018 Wiley Periodicals, Inc.

  15. Comparing the Structure and Mechanical Properties of Welds on Ductile Cast Iron (700 MPa under Different Heat Treatment Conditions

    Directory of Open Access Journals (Sweden)

    Ronny M. Gouveia

    2018-01-01

    Full Text Available The weldability of ductile iron, as widely known, is relatively poor, essentially due to its typical carbon equivalent value. The present study was developed surrounding the heat treatability of welded joints made with a high strength ductile cast iron detaining an ultimate tensile strength of 700 MPa, and aims to determine which heat treatment procedures promote the best results, in terms of microstructure and mechanical properties. These types of alloys are suitable for the automotive industry, as they allow engineers to reduce the thickness of parts while maintaining mechanical strength, decreasing the global weight of vehicles and providing a path for more sustainable development. The results allow us to conclude that heat treatment methodology has a large impact on the mechanical properties of welded joints created from the study material. However, the thermal cycles suffered during welding promote the formation of ledeburite areas near the weld joint. This situation could possibly be dealt through the implementation of post-welding heat treatments (PWHT with specific parameters. In contrast to a ductile cast iron tested in a previous work, the bull-eye ductile cast iron with 700 MPa ultimate tensile strength presented better results during the post-welding heat treatment than during preheating.

  16. Nuclear safety inspection in treatment process for SG heat exchange tubes deficiency of unit 1, TNPS

    International Nuclear Information System (INIS)

    Zhang Chunming; Song Chenxiu; Zhao Pengyu; Hou Wei

    2006-01-01

    This paper describes treatment process for SG heat exchange tubes deficiency of Unit 1, TNPS, nuclear safety inspection of Northern Regional Office during treatment process for deficiency and further inspection after deficiency had been treated. (authors)

  17. The local heat treatment equipment and technology of the pipelines welded joints

    International Nuclear Information System (INIS)

    Korol'kov, P.M.

    1998-01-01

    The principal methods and equipment for local treatment of the pipe-lines weld joints in different industry branches is described. Recommendations about heat treatment equipment and technology application are given

  18. Study of critical dependence of stable phases in Nitinol on heat treatment using electrical resistivity probe

    International Nuclear Information System (INIS)

    Uchil, J.; Mohanchandra, K.P.; Kumara, K.G.; Mahesh, K.K.

    1998-01-01

    Phase transformations in 40% cold-worked Nitinol as a function of heat treatment have been studied using electrical resistivity variation with temperature. The stabilisation of austenitic, rhombohedral and martensitic phases is shown to critically depend on the temperatures of heat treatment by the analysis of temperature dependence of electrical resistivity in heating and cooling parts of the cycle. Characteristic values of electrical resistivity of the stable phases are determined. The R-phase has been found to form continuously with increasing heat-treatment temperature starting from room temperature and to suddenly disappear beyond heat-treatment at 683 K. The observed presence or absence of R-phase is confirmed by heat capacity measurements as a function of temperature. (orig.)

  19. Prediction of heat treatment in food processing machinery

    DEFF Research Database (Denmark)

    Karlson, Torben; Friis, Alan; Szabo, Peter

    1997-01-01

    The velocity and temperature fields of a shear thinning fluid in a co-rotating disc scraped surface heat exchanger (CDHE) are calculated using the finite element method. By tracking and timingparticles through the heat exchanger residence time and thermal time distributions are computed. The resi...

  20. Characterization of Machine Variability and Progressive Heat Treatment in Selective Laser Melting of Inconel 718

    Science.gov (United States)

    Prater, Tracie; Tilson, Will; Jones, Zack

    2015-01-01

    The absence of an economy of scale in spaceflight hardware makes additive manufacturing an immensely attractive option for propulsion components. As additive manufacturing techniques are increasingly adopted by government and industry to produce propulsion hardware in human-rated systems, significant development efforts are needed to establish these methods as reliable alternatives to conventional subtractive manufacturing. One of the critical challenges facing powder bed fusion techniques in this application is variability between machines used to perform builds. Even with implementation of robust process controls, it is possible for two machines operating at identical parameters with equivalent base materials to produce specimens with slightly different material properties. The machine variability study presented here evaluates 60 specimens of identical geometry built using the same parameters. 30 samples were produced on machine 1 (M1) and the other 30 samples were built on machine 2 (M2). Each of the 30-sample sets were further subdivided into three subsets (with 10 specimens in each subset) to assess the effect of progressive heat treatment on machine variability. The three categories for post-processing were: stress relief, stress relief followed by hot isostatic press (HIP), and stress relief followed by HIP followed by heat treatment per AMS 5664. Each specimen (a round, smooth tensile) was mechanically tested per ASTM E8. Two formal statistical techniques, hypothesis testing for equivalency of means and one-way analysis of variance (ANOVA), were applied to characterize the impact of machine variability and heat treatment on six material properties: tensile stress, yield stress, modulus of elasticity, fracture elongation, and reduction of area. This work represents the type of development effort that is critical as NASA, academia, and the industrial base work collaboratively to establish a path to certification for additively manufactured parts. For future

  1. Effect of Heat Treatment on Machining Properties of the AlSi9Cu3(Fe Alloy

    Directory of Open Access Journals (Sweden)

    Wieroński P.

    2016-09-01

    Full Text Available Automation of machining operations, being result of mass volume production of components, imposes more restrictive requirements concerning mechanical properties of starting materials, inclusive of machinability mainly. In stage of preparation of material, the machinability is influenced by such factors as chemical composition, structure, mechanical properties, plastic working and heat treatment, as well as a factors present during machining operations, as machining type, cutting parameters, material and geometry of cutting tools, stiffness of the system: workpiece – machine tool – fixture and cutting tool.

  2. MXene Ti3C2: An Effective 2D Light-to-Heat Conversion Material

    KAUST Repository

    Li, Renyuan

    2017-03-25

    MXene, a new series of 2D material, has been steadily advancing its applications to a variety of fields, such as catalysis, supercapacitor, molecular separation, electromagnetic wave interference shielding. This work reports a carefully designed aqueous droplet light heating system along with a thorough mathematical procedure, which combined leads to a precise determination of internal light-to-heat conversion efficiency of a variety of nanomaterials. The internal light-to-heat conversion efficiency of MXene, more specifically Ti3C2, was measured to be 100%, indicating a perfect energy conversion. Furthermore, a self-floating MXene thin membrane was prepared by simple vacuum filtration and the membrane, in the presence of a rationally chosen heat barrier, produced a light-to-water-evaporation efficiency of 84% under one sun irradiation, which is among the state of art energy efficiency for similar photothermal evaporation system. The outstanding internal light-to-heat conversion efficiency and great light-to-water evaporation efficiency reported in this work suggest that MXene is a very promising light-to-heat conversion material and thus deserves more research attention toward practical applications.

  3. Advanced Materials Development Program: Ceramic Technology for Advanced Heat Engines program plan, 1983--1993

    Energy Technology Data Exchange (ETDEWEB)

    1990-07-01

    The purpose of the Ceramic Technology for Advanced Heat Engines (CTAHE) Project is the development of an industrial technology base capable of providing reliable and cost-effective high temperature ceramic components for application in advanced heat engines. There is a deliberate emphasis on industrial'' in the purpose statement. The project is intended to support the US ceramic and engine industries by providing the needed ceramic materials technology. The heat engine programs have goals of component development and proof-of-concept. The CTAHE Project is aimed at developing generic basic ceramic technology and does not involve specific engine designs and components. The materials research and development efforts in the CTAHE Project are focused on the needs and general requirements of the advanced gas turbine and low heat rejection diesel engines. The CTAHE Project supports the DOE Office of Transportation Systems' heat engine programs, Advanced Turbine Technology Applications (ATTAP) and Heavy Duty Transport (HDT) by providing the basic technology required for development of reliable and cost-effective ceramic components. The heat engine programs provide the iterative component design, fabrication, and test development logic. 103 refs., 18 figs., 11 tabs.

  4. Preparation and characterization of a novel polymeric based solid-solid phase change heat storage material

    International Nuclear Information System (INIS)

    Xi Peng; Gu Xiaohua; Cheng Bowen; Wang Yufei

    2009-01-01

    Here we reported a two-step procedure for preparing a novel polymeric based solid-solid phase change heat storage material. Firstly, a copolymer monomer containing a polyethylene glycol monomethyl ether (MPEG) phase change unit and a vinyl unit was synthesized via the modification of hydrogen group of MPEG. Secondly, by copolymerization of the copolymer monomer and phenyl ethylene, a novel polymeric based solid-solid phase change heat storage material was prepared. The composition, structure and properties of the novel polymeric based solid-solid phase change material were characterized by IR, 1 H NMR, DSC, WAXD, and POM, respectively. The results show that the novel polymeric based solid-solid phase change material possesses of excellent crystal properties and high phase change enthalpy.

  5. QUALITY IMPROVEMENT OF SECONDARY SILUMINS BY USING REFINING-MODIFYING, HEAT AND LASER TREATMENTS

    Directory of Open Access Journals (Sweden)

    I. P. Volchok

    2014-10-01

    Full Text Available Purpose. As a rule secondary silumins are characterized by lower quality than their primary analogues. During manufacture of alloys a large quantity of intermetallides, first of all on the basis of iron, in their structure is ignored. To achieve the optimum level of properties it is necessary to search for ways to adapt refining-modifying, heat and laser treatments to peculiarities of the structure of secondary Al-Si alloys. Methodology. The research was carried out by using standard methods of metallographic analysis, determination of foundry, mechanical and service properties of alloys according to rotatable plans of multifactor experiments. Findings. It was established, that refiningmodifying treatment is a required procedure during manufacture of secondary silumins as it permits to effectively influence the iron-containing phases' segregations by changing their morphology, size and distribution and to increase the effectiveness of further treatment in solid state. It was found that standard modes of heat treatment are not optimal for secondary silumins. Laser treatment has shown high effectiveness in increasing of strength, wear resistance, corrosion and cavitation resistance of secondary Al-Si alloys, and the increased iron content contributed to additional solid solution hardening. Originality. It was established, that after refining-modifying treatment the phase Al5SiFe, which crystallizes in the shape of long stretched plates transformed into phase Al15(FeMn3Si2 in skeletal or polyhedral shape. The relationship between iron content in secondary silumins and holding time during heat treatment that ensures optimum of mechanical properties was obtained. It was proved that the presence of ironcontaining intermetallides Al5SiFe results in the decrease of hardened layer's depth during laser treatment. It was established, that with increasing of iron concentration the corrosion rate of secondary silumins in 3 % NaCl + 0.1 % H2O2 and 10 % HCl

  6. A novel laboratory scale method for studying heat treatment of cake flour

    OpenAIRE

    Chesterton, AKS; Wilson, David Ian; Sadd, PI; Moggridge, Geoffrey Dillwyn

    2014-01-01

    A lab-scale method for replicating the time–temperature history experienced by cake flours undergoing heat treatment was developed based on a packed bed configuration. The performance of heat-treated flours was compared with untreated and commercially heat-treated flour by test baking a high ratio cake formulation. Both cake volume and AACC shape measures were optimal after 15 min treatment at 130 °C, though their values varied between harvests. Separate oscillatory rheometry tests of cake ba...

  7. Heat Treatment of Gas-Atomized Powders for Cold Spray Deposition

    Science.gov (United States)

    Story, William A.; Brewer, Luke N.

    2018-02-01

    This communication demonstrates the efficacy of heat treatment on the improved deposition characteristics of aluminum alloy powders. A novel furnace was constructed for solutionizing of feedstock powders in an inert atmosphere while avoiding sintering. This furnace design achieved sufficiently high cooling rates to limit re-precipitation during powder cooling. Microscopy showed homogenization of the powder particle microstructures after heat treatment. Cold spray deposition efficiency with heat-treated powders substantially increased for the alloys AA2024, AA6061, and AA7075.

  8. Heat stroke during long-term clozapine treatment: should we be concerned about hot weather?

    OpenAIRE

    Hoffmann, Maurício Scopel; Oliveira, Lucas Mendes; Lobato, Maria Inês Rodrigues; Belmonte-de-Abreu, Paulo

    2016-01-01

    Objective To describe the case of a patient with schizophrenia on clozapine treatment who had an episode of heat stroke. Case description During a heat wave in January and February 2014, a patient with schizophrenia who was on treatment with clozapine was initially referred for differential diagnose between systemic infection and neuroleptic malignant syndrome, but was finally diagnosed with heat stroke and treated with control of body temperature and hydration. Comments This report aims to...

  9. Effect of heat treatment duration on phase separation of sodium borosilicate glass, containing copper

    International Nuclear Information System (INIS)

    Shejnina, T.G.; Gutner, S.Kh.; Anan'in, N.I.

    1989-01-01

    The effect of heat treatment duration on phase separation of sodium borosilicate (SBS) glass, containing copper is studied. It is stated that phase separation close to equilibrium one is attained under 12 hours of heat treatment of SBS glass containing copper

  10. Industrial heat treatment of R-HPDC A356 automotive brake callipers

    CSIR Research Space (South Africa)

    Chauke, L

    2012-10-01

    Full Text Available Heat treatment of rheo-high pressure die cast (R-HPDC) A356 brake callipers has produced good mechanical properties on the laboratory scale. An industrial heat treatment is required to evaluate the applicability and conformance of the R-HPDC A356...

  11. Relaxation of residual stress in MMC after combined plastic deformation and heat treatment

    International Nuclear Information System (INIS)

    Bruno, G.; Ceretti, M.; Girardin, E.; Giuliani, A.; Manescu, A.

    2004-01-01

    Neutron Diffraction shows that plastic pre-deformation and heat treatments have opposite effects on the residual stress in Al-SiC p composites. The thermal micro residual stress is relaxed or even reversed by pre-strains above 0.2%, but restored by heat treatments. The sense of relaxation changes above 400 deg. C (the mixing temperature)

  12. Influence of heat treatment on magnesium alloys meant to automotive industry

    NARCIS (Netherlands)

    Popescu, G.; Moldovan, P.; Bojin, D.; Sillekens, W.H.

    2009-01-01

    The paper presents a study concerning the heat treatment realized on magnesium alloys, from AZ80 and ZK60 class. These alloys are destined to replace the conventional ferrous and aluminum alloys in automotive industry. It was realized the heat treatment, T5 - artificially aging, and it were

  13. Effect of heat treatment and impurity concentration on some mechanical properties V-15Cr-5Ti alloy

    International Nuclear Information System (INIS)

    Loomis, B.A.; Kestel, B.J.; Diercks, D.R.

    1986-03-01

    The effects of heat treatment and O, N, C, Si, and S impurity level on the yield strength, ductility, and fracture mode for specimens from four different heats of the V-15Cr-5Ti alloy are presented. The heat treatments for the alloy consisted of annealing as-rolled material for one hour at either 950, 1050, 1125, or 1200 0 C. The total oxygen, nitrogen, and carbon impurity concentration ranged from 400 to 1200 wppm. The Si concentration ranged from 300 to 1050 wppm, and the S concentration ranged from 440 to 1100 wppm. The yield strength and ductility for the alloy, regardless of impurity concentration, exhibited minimum and maximum values, respectively, for the 1125 0 C anneal. The primary mode of failure for the tensile specimens was transgranular fracture

  14. Simultaneous Contact Sensing and Characterizing of Mechanical and Dynamic Heat Transfer Properties of Porous Polymeric Materials

    Directory of Open Access Journals (Sweden)

    Bao-guo Yao

    2017-10-01

    Full Text Available Porous polymeric materials, such as textile fabrics, are elastic and widely used in our daily life for garment and household products. The mechanical and dynamic heat transfer properties of porous polymeric materials, which describe the sensations during the contact process between porous polymeric materials and parts of the human body, such as the hand, primarily influence comfort sensations and aesthetic qualities of clothing. A multi-sensory measurement system and a new method were proposed to simultaneously sense the contact and characterize the mechanical and dynamic heat transfer properties of porous polymeric materials, such as textile fabrics in one instrument, with consideration of the interactions between different aspects of contact feels. The multi-sensory measurement system was developed for simulating the dynamic contact and psychological judgment processes during human hand contact with porous polymeric materials, and measuring the surface smoothness, compression resilience, bending and twisting, and dynamic heat transfer signals simultaneously. The contact sensing principle and the evaluation methods were presented. Twelve typical sample materials with different structural parameters were measured. The results of the experiments and the interpretation of the test results were described. An analysis of the variance and a capacity study were investigated to determine the significance of differences among the test materials and to assess the gage repeatability and reproducibility. A correlation analysis was conducted by comparing the test results of this measurement system with the results of Kawabata Evaluation System (KES in separate instruments. This multi-sensory measurement system provides a new method for simultaneous contact sensing and characterizing of mechanical and dynamic heat transfer properties of porous polymeric materials.

  15. X-Ray Micro-Tomography Applied to Nasa's Materials Research: Heat Shields, Parachutes and Asteroids

    Science.gov (United States)

    Panerai, Francesco; Borner, Arnaud; Ferguson, Joseph C.; Mansour, Nagi N.; Stern, Eric C.; Barnard, Harold S.; Macdowell, Alastair A.; Parkinson, Dilworth Y.

    2017-01-01

    X-ray micro-tomography is used to support the research on materials carried out at NASA Ames Research Center. The technique is applied to a variety of applications, including the ability to characterize heat shield materials for planetary entry, to study the Earth- impacting asteroids, and to improve broadcloths of spacecraft parachutes. From micro-tomography images, relevant morphological and transport properties are determined and validated against experimental data.

  16. Natural convection heat transfer enhancement using Microencapsulated Phase-Change-Material slurries

    International Nuclear Information System (INIS)

    Kubo, Shinji; Akino, Norio; Tanaka, Amane; Nakano, Fumihiko; Nagashima, Akira.

    1997-01-01

    The present study investigates natural convection heat transfer from a heated cylinder cooled by a water slurry of Microencapsulated Phase Change Material (MCPCM). A normal paraffin hydrocarbon with carbon number of 18 and melting point of 27.9degC, is microencapsulated by Melamine resin into particles of which average diameter is 9.5μm and specific weight is same as water. The slurry of the MCPCM and water is put into a test apparatus, which is a rectangular enclosure with a heated horizontal cylinder. As the concentrations of PCM in the slurry are changed in 1,3 and 5%, the heat transfer coefficients of the cylinder are larger than that of water as working fluid, by 3,20 and 35% enhancements respectively. (author)

  17. Phase separation of cesium from lead borosilicate glass by heat treatment under a reducing atmosphere

    Energy Technology Data Exchange (ETDEWEB)

    Xu, Zhanglian; Okada, Takashi, E-mail: t-okada@u-fukui.ac.jp; Nishimura, Fumihiro; Yonezawa, Susumu

    2016-11-05

    Highlights: • Cesium was phase separated from lead borosilicate glass under a reductive atmosphere. • The phase separation occurred on the glass surface that was in contact with the gas. • The leachability of cesium was enhanced by the phase separation. • The degree of such enhancement varied depending on the heat treatment conditions. - Abstract: A phase-separation technique for removing sodium from glass using a heat-treatment method under a reducing atmosphere was previously developed for sodium recovery from waste glass. In this study, this technique was applied to cesium-containing lead borosilicate glass to concentrate the cesium in phase-separated sodium-rich materials for efficient cesium extraction. The theoretical phase-separation temperature of the sodium-rich phase was simulated by thermodynamic equilibrium calculations and was predicted to occur below 700 °C for lead borosilicate glass. Experimentally, a simulated lead borosilicate glass was melted at 1000 °C and subsequently annealed below 700 °C under a CO-containing reducing atmosphere. The phase separation of cesium was found to occur with sodium enrichment on the glass surface that was in contact with the gas phase, promoting cesium extraction from the treated glass using water. The cesium extraction efficiency was affected by the surface area of the treated glass that was in contact with water, and under the examined conditions, the cesium extraction efficiency was up to 66%. Phase separation using reductive heat treatment, combined with a water leaching technique, is suggested to be effective for extracting cesium incorporated in borosilicate glass waste.

  18. Reducing Pumping Power in Hydronic Heating and Cooling Systems with Microencapsulated Phase Change Material Slurries

    Science.gov (United States)

    Karas, Kristoffer Jason

    Phase change materials (PCMs) are being used increasingly in a variety of thermal transfer and thermal storage applications. This thesis presents the results of a laboratory study into the feasibility of improving the performance of hydronic heating and cooling systems by adding microcapsules filled with a PCM to the water used as heat transport media in these systems. Microencapsulated PCMs (MPCMs) increase the heat carrying capacity of heat transport liquids by absorbing or releasing heat at a constant temperature through a change of phase. Three sequences of tests and their results are presented: 1) Thermal cycling tests conducted to determine the melting temperatures and extent of supercooling associated with the MPCMs tested. 2) Hydronic performance tests in which MPCM slurries were pumped through a fin-and-tube, air-to-liquid heat exchanger and their thermal transfer performance compared against that of ordinary water. 3) Mechanical stability tests in which MPCM slurries were pumped in a continuous loop in order to gauge the extent of rupture due to pumping. It is shown that slurries consisting of water and MPCMs ˜ 14-24 mum in diameter improve thermal performance and offer the potential for power savings in the form of reduced pumping requirements. In addition, it is shown that while slurries of MPCMs 2-5 mum in diameter appear to exhibit better mechanical stability than slurries of larger diameter MPCMs, the smaller MPCMs appear to reduce the thermal performance of air-to-liquid heat exchangers.

  19. Enhancing ultra-high CPV passive cooling using least-material finned heat sinks

    Energy Technology Data Exchange (ETDEWEB)

    Micheli, Leonardo, E-mail: lm409@exeter.ac.uk; Mallick, Tapas K., E-mail: T.K.Mallick@exeter.ac.uk [Environment and Sustainability Institute, University of Exeter, Penryn, Cornwall TR10 9FE (United Kingdom); Fernandez, Eduardo F., E-mail: E.Fernandez-Fernandez2@exeter.ac.uk [Environment and Sustainability Institute, University of Exeter, Penryn, Cornwall TR10 9FE (United Kingdom); Centre of Advanced Studies in Energy and Environment, University of Jaen, Jaen 23071 (Spain); Almonacid, Florencia, E-mail: facruz@ujaen.es [Centre of Advanced Studies in Energy and Environment, University of Jaen, Jaen 23071 (Spain); Reddy, K. S., E-mail: ksreddy@iitm.ac.in [Department of Mechanical Engineering, Indian Institute of Technology Madras, Chennai, 600036 (India)

    2015-09-28

    Ultra-high concentrating photovoltaic (CPV) systems aim to increase the cost-competiveness of CPV by increasing the concentrations over 2000 suns. In this work, the design of a heat sink for ultra-high concentrating photovoltaic (CPV) applications is presented. For the first time, the least-material approach, widely used in electronics to maximize the thermal dissipation while minimizing the weight of the heat sink, has been applied in CPV. This method has the potential to further decrease the cost of this technology and to keep the multijunction cell within the operative temperature range. The designing procedure is described in the paper and the results of a thermal simulation are shown to prove the reliability of the solution. A prediction of the costs is also reported: a cost of 0.151$/W{sub p} is expected for a passive least-material heat sink developed for 4000x applications.

  20. High heat load experiments for first wall materials by high power ion beams

    Energy Technology Data Exchange (ETDEWEB)

    Kuroda, Tsutomu; Kaneko, Osamu; Sakurai, Keiichi; Oka, Yoshihide; Shibui, Masanao; Ohmori, Junji

    1985-09-01

    Preliminary results are presented with some analytical calculations for thermal shock fractures of first-wall material candidates under plasma disruption heating conditions. A 120 keV - 90 A ion source has been used as an energy source to heat large specimens with heat fluxes of about 9 kW/cm/sup 2/ for pulse length of about 57 msec. Materials examined here are graphite (POCO), SiC, AlN, TiC-coated graphite, and sus 304. The SiC and AlN specimens were completely broken by only one thermal shock. The web-like surface cracks with a depth of about 0.6 mm were created in the tungsten specimen during five shots. No apparent destructive changes were observed in the graphite specimen.

  1. Heat treatment evaluation of steel ASTM A-131 grade A by X-Ray diffraction

    Energy Technology Data Exchange (ETDEWEB)

    Ferreira Junior, Francisco; Feio, Luciana Gaspar; Costa, Ednelson Silva; Rodrigues, Lino Alberto Soares; Braga, Eduardo Magalhaes, E-mail: juniorferrer93@gmail.com [Universidade Federal do Pará (UFPA), Belém, PA (Brazil)

    2016-07-01

    Full text: This study evaluates the residual stress of naval steel ASTM A-131 grade A before and after heat treatment. Residual stresses were determined by the technique of X-ray diffraction (XRD). Before heat treatment the residual stress measurements were made at 36 (thirty six) points distributed in a specimen with dimensions of 400 mm long, 200 mm wide and 95 mm thick, then the plate under analysis was brought to the oven for the implementation of heat treatment. To check the performance of the heat treatment, the plate was again subjected to XRD measurements of the same points previously measured in order to compare the residual stresses. As result, there was a reduction of residual stresses with the application of heat treatment. References: [1] COLPAERT, H. Metalografia dos Produtos Siderurgicos Comuns. 4 Edição. Editora Blucher. Saõ Paulo, SP, 2008. [2] HILL, R. Princípios de Metalurgia Física, 1992. (author)

  2. Effect of heat treatment on the temperature dependence of the fracture behavior of X-750 alloy

    Energy Technology Data Exchange (ETDEWEB)

    Marsh, C.; Depinoy, S. [University of South Carolina (United States); Kaoumi, D. [North Carolina State University (United States)

    2016-11-20

    X-750 is a nickel-chromium based super alloy of usefulness in a wide variety of applications such as gas turbines, rocket engines, nuclear reactors, pressure vessels, tooling, and aircraft structures. Its good mechanical properties are due to the strengthening from precipitation of γ′ particles upon prior ageing heat treatment. In this work, the effect of such heat treatment on the fracture mechanisms of X-750 was studied at various temperatures by comparing it with a non-aged, solution annealed X-750. Tensile tests were conducted from room temperatures up to 900 °C; fracture surfaces were analyzed by means of SEM observations. In addition, the microstructure of both aged and solution annealed materials were studied using SEM and TEM, both on as received and on tested specimens. In terms of mechanical properties, as expected, the yield strength and the ultimate tensile strength of the aged material were better than for the solution-annealed one, and only slightly decreased with increasing temperature when tested between room temperatures and 650 °C. In this range of temperature, the fracture surface of aged material evolves from purely intergranular to purely transgranular due to the thermal activation of dislocation mobility that relieves the stress at the grain boundaries, while the rupture of the solution annealed material is due to the coalescence of voids induced by decohesion at the MC carbides/matrix interface. At higher temperatures, precipitation of γ’ particles upon testing of the solution-annealed material leads to a temperature-dependent increase in both yield strength and ultimate tensile strength, which nevertheless remain below the aged material ones with the exception of the higher temperatures. At the same time, an overall decrease of the aged material mechanical properties is observed. Minimum ductility was observed at 750 °C for both solution annealed and aged specimen, due to the oxidation of grain boundaries leading to an

  3. Microstructure and hardness studies of Inconel 718 manufactured by selective laser melting before and after solution heat treatment

    Energy Technology Data Exchange (ETDEWEB)

    Tucho, Wakshum M., E-mail: wakshum.m.tucho@uis.no [Department of Mechanical and Structural Engineering and Materials Science, University of Stavanger, N-4036 Stavanger (Norway); Cuvillier, Priscille [Department of Mechanical and Structural Engineering and Materials Science, University of Stavanger, N-4036 Stavanger (Norway); Sjolyst-Kverneland, Atle [Roxar/Emerson Process Management, POB 112, 4065 Stavanger (Norway); Hansen, Vidar [Department of Mechanical and Structural Engineering and Materials Science, University of Stavanger, N-4036 Stavanger (Norway)

    2017-03-24

    The microstructure of Additive Manufactured (AM) Inconel 718 in general and Selective Laser Melting (SLM), in particular is different from the material produced by conventional methods due to the rapid solidification process associated with the former. As a result, the widely adapted standard solution heat treatment temperature (<1100 °C) for conventional material is found to be not high enough for materials fabricated with SLM method in order to dissolve Laves and other microsegregated phases for releasing the ageing constituents (Nb, Ti, Al) sufficiently into the alloy matrix. In this study, sample of Inconel 718 fabricated with SLM method were solution heat-treated to 1100 °C or 1250 °C at different hold times to investigate the dissolution of macro- and micro-segregated precipitates. Investigations of microstructure and segregation in as-printed and solution heat-treated states have been studied using Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM) and Optical Microscopy (OM). Measurement of material hardness was performed with Vickers hardness tests. The microstructure of the as-printed parts exhibit non-columnar grains, but contain well-shaped columnar/cellular sub-grains. The intergranular boundaries are decorated with high density of dislocations and segregated particles. Tremendous stress relief and grain coarsening were observed with solution heat treatment. In particular, at 1250 °C annealing, the sub-grains, including precipitates and dislocation networks along the sub-grain boundaries, were entirely dissolved. However, the 1100/1250 °C solution heat treatment scheme could not dissolve microsegregated precipitates and carbides completely. Details of the analysis on microstructure, dissolution of precipitates and hardness are presented.

  4. Microstructure and hardness studies of Inconel 718 manufactured by selective laser melting before and after solution heat treatment

    International Nuclear Information System (INIS)

    Tucho, Wakshum M.; Cuvillier, Priscille; Sjolyst-Kverneland, Atle; Hansen, Vidar

    2017-01-01

    The microstructure of Additive Manufactured (AM) Inconel 718 in general and Selective Laser Melting (SLM), in particular is different from the material produced by conventional methods due to the rapid solidification process associated with the former. As a result, the widely adapted standard solution heat treatment temperature (<1100 °C) for conventional material is found to be not high enough for materials fabricated with SLM method in order to dissolve Laves and other microsegregated phases for releasing the ageing constituents (Nb, Ti, Al) sufficiently into the alloy matrix. In this study, sample of Inconel 718 fabricated with SLM method were solution heat-treated to 1100 °C or 1250 °C at different hold times to investigate the dissolution of macro- and micro-segregated precipitates. Investigations of microstructure and segregation in as-printed and solution heat-treated states have been studied using Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM) and Optical Microscopy (OM). Measurement of material hardness was performed with Vickers hardness tests. The microstructure of the as-printed parts exhibit non-columnar grains, but contain well-shaped columnar/cellular sub-grains. The intergranular boundaries are decorated with high density of dislocations and segregated particles. Tremendous stress relief and grain coarsening were observed with solution heat treatment. In particular, at 1250 °C annealing, the sub-grains, including precipitates and dislocation networks along the sub-grain boundaries, were entirely dissolved. However, the 1100/1250 °C solution heat treatment scheme could not dissolve microsegregated precipitates and carbides completely. Details of the analysis on microstructure, dissolution of precipitates and hardness are presented.

  5. An artificial compressibility CBS method for modelling heat transfer and fluid flow in heterogeneous porous materials

    CSIR Research Space (South Africa)

    Malan, AG

    2011-08-01

    Full Text Available to modelling both forced convection as well as heat transfer and fluid flow through heterogeneous saturated porous materials via an edge-based finite volume discretization scheme. A volume-averaged set of local thermal disequilibrium governing equations...

  6. Latent heat storage by silica-coated polymer beads containing organic phase change materials

    Czech Academy of Sciences Publication Activity Database

    Feczkó, T.; Trif, L.; Horák, Daniel

    2016-01-01

    Roč. 132, July (2016), s. 405-414 ISSN 0038-092X R&D Projects: GA MŠk(CZ) LH14318 Institutional support: RVO:61389013 Keywords : latent heat storage * phase change materials * porous beads by suspension polymerization Subject RIV: CD - Macromolecular Chemistry Impact factor: 4.018, year: 2016

  7. Evaluation of procedures for estimation of the isosteric heat of adsorption in microporous materials

    NARCIS (Netherlands)

    Krishna, R.

    2014-01-01

    The major objective of this communication is to evaluate procedures for estn. of the isosteric heat of adsorption, Qst, in microporous materials such as zeolites, metal org. frameworks (MOFs)​, and zeolitic imidazolate frameworks (ZIFs)​. For this purpose we have carefully analyzed published exptl.

  8. Evaporation equipment with electron beam heating for the evaporation of metals and other conducting materials

    International Nuclear Information System (INIS)

    Mueller, P.

    1977-01-01

    Equipment for the evaporation of metals and other conducting materials by electron beam heating is to be improved by surrou nding the evaporation equipment with a grid, which has a negative voltage compared to the cathode. This achieves the state where the cathode is hit and damaged less by the ions formed, so that its life period is prolonged. (UWI) [de

  9. Customer Overview of Pulsed Laser Heating for Evaluation of Gun Bore Materials

    Science.gov (United States)

    2015-05-01

    properties of the gun bore materials. Ideally, well validated interior ballistics modeling has been carried out (typically with NOVA) to provide time...03002, February 2003. 5. J. Warrender, C. Mulligan, and J. Underwood , “Analysis of thermo-mechanical cracking in refractory coatings using variable pulse duration laser pulse heating,” Wear 263 1540 (2007).

  10. Fractional-Order Identification and Control of Heating Processes with Non-Continuous Materials

    Directory of Open Access Journals (Sweden)

    Riccardo Caponetto

    2016-11-01

    Full Text Available The paper presents a fractional order model of a heating process and a comparison of fractional and standard PI controllers in its closed loop system. Preliminarily, an enhanced fractional order model for the heating process on non-continuous materials has been identified through a fitting algorithm on experimental data. Experimentation has been carried out on a finite length beam filled with three non-continuous materials (air, styrofoam, metal buckshots in order to identify a model in the frequency domain and to obtain a relationship between the fractional order of the heating process and the different materials’ properties. A comparison between the experimental model and the theoretical one has been performed, proving a significant enhancement of the fitting performances. Moreover the obtained modelling results confirm the fractional nature of the heating processes when diffusion occurs in non-continuous composite materials, and they show how the model’s fractional order can be used as a characteristic parameter for non-continuous materials with different composition and structure. Finally, three different kinds of controllers have been applied and compared in order to keep constant the beam temperature constant at a fixed length.

  11. Some aspects of using Be as high heat flux protective armour material

    International Nuclear Information System (INIS)

    Gervash, A.; Mazul, I.; Yablokov, N.; Linke, J.

    2000-01-01

    The beryllium as plasma facing armour material must protect the actively cooled copper alloy heat sink of the First Wall and Divertor components from sputtering erosion, disruption and VDE transients and withstand the number of cycles under expected heat and neutron fluxes. The presented paper discusses some topical questions and presents recent results obtained in Russia in the frame of such consideration. In real operation beryllium as plasma facing component will be subjected to sequence of normal (cyclic heat fluxes) and off-normal (disruption, VDE) heat loads. Aiming to investigate the results of mentioned events the experiments with the number of Russian Be grades (DShG-200, TGP-56, TShG-56, TR-30, Condensed Be) as well as S-65C (ITER reference grade) at simulated disruption loads (∝5 MJ/m 2 ) and subsequent thermal cycling (∝5 MW/m 2 , 1000 cycles) were carried out. Experiments have revealed no macroscopic damage of the tested grades, although significant differences in crack formation and propagation were observed. The main statistics of performed experiments is presented and discussed. One of the main requirements to use Be as a candidate for plasma facing component is providing a reliable joint between Be and Cu-alloy heat sink structure. The unique Russian fast brazing process of joining beryllium to Cu-alloy that allows to survive high heat fluxes ≥10 MW/m 2 during thousand heating/cooling cycles without serious damaging in the armour material and its joint was described in previous works. The main goal of experiments presented in this paper was to study the high heat flux durability limit for joints as function of the pulse duration (i.e. investigation of creep/fatigue interaction). Authors present a description of the testing procedure and discuss the first results of mentioned experiments. (orig.)

  12. Microstructural characterisation of vacuum sintered T42 powder metallurgy high-speed steel after heat treatments

    International Nuclear Information System (INIS)

    Trabadelo, V.; Gimenez, S.; Iturriza, I.

    2009-01-01

    High-speed steel powders (T42 grade) have been uniaxially cold-pressed and vacuum sintered to full density. Subsequently, the material was heat treated following an austenitising + quenching + multitempering route or alternatively austenitising + isothermal annealing. The isothermal annealing route was designed in order to attain a hardness value of ∼50 Rockwell C (HRC) (adequate for structural applications) while the multitempering parameters were selected to obtain this value and also the maximum hardening of the material (∼66 HRC). Microstructural characterisation has been carried out by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The microstructure consists of a ferrous (martensitic or ferritic) matrix with a distribution of second phase particles corresponding to nanometric and submicrometric secondary carbides precipitated during heat treatment together with primary carbides. The identification of those secondary precipitates (mainly M 3 C, M 6 C and M 23 C 6 carbides) has allowed understanding the microstructural evolution of T42 high-speed steel under different processing conditions

  13. Detrimental Cr-rich Phases Precipitation on SAF 2205 Duplex Stainless Steels Welds After Heat Treatment

    Directory of Open Access Journals (Sweden)

    Argelia Fabiola Miranda Pérez

    Full Text Available Abstract The austeno-ferritic Stainless Steels are commonly employed in various applications requiring structural performances with enhanced corrosion resistance. Their characteristics can be worsened if the material is exposed to thermal cycles, since the high-temperature decomposition of ferrite causes the formation of detrimental secondary phases. The Submerged Arc Welding (SAW process is currently adopted for joining DSS owing to its relatively simple execution, cost savings, and using molten slag and granular flux from protecting the seam of atmospheric gases. However, since it produces high contents of δ-ferrite in the heat affected zone and low content of γ-austenite in the weld, high-Ni filler materials must be employed, to avoid excessive ferritization of the joint. The present work is aimed to study the effect of 3 and 6 hours isothermal heat treatments at 850°C and 900°C in a SAF 2205 DSS welded joint in terms of phases precipitation. The results showed the presence of σ-phase at any time-temperature combination, precipitating at the δ/γ interphases and often accompanied by the presence of χ-phase. However, certain differences in secondary phases amounts were revealed among the different zones constituting the joint, ascribable both to peculiar elements partitioning and to the different morphology pertaining to each microstructure.

  14. Heat Treatment of a Casting Element of a Through Clamp to Suspension of Electric Cables on Line Post Insulators

    Directory of Open Access Journals (Sweden)

    Pezda J.

    2016-09-01

    Full Text Available Heat treatment of a casting elements poured from silumins belongs to technological processes aimed mainly at change of their mechanical properties in solid state, inducing predetermined structural changes, which are based on precipitation processes (structural strengthening of the material, being a derivative of temperature and duration of solutioning and ageing operations. The subject-matter of this paper is the issue concerning implementation of a heat treatment process, basing on selection of dispersion hardening parameters to assure improvement of technological quality in terms of mechanical properties of a clamping element of energy network suspension, poured from hypoeutectic silumin of the LM25 brand; performed on the basis of experimental research program with use of the ATD method, serving to determination of temperature range of solutioning and ageing treatments. The heat treatment performed in laboratory conditions on a component of energy network suspension has enabled increase of the tensile strength Rm and the hardness HB with about 60-70% comparing to the casting without the heat treatment, when the casting was solutioned at temperature 520 °C for 1 hour and aged at temperature 165 °C during 3 hours.

  15. Effect of heat treatment on polyphenol oxidase and peroxidase ...

    African Journals Online (AJOL)

    GREGO

    2006-12-18

    Dec 18, 2006 ... enzymes in plant and its resistance to heat has been reported by a ... sintered glass funnel and washed with cold acetone under low vacuum ... Peroxidase activity was determined by measuring the colour deve- lopment at ...

  16. Development of advanced high heat flux and plasma-facing materials

    Science.gov (United States)

    Linsmeier, Ch.; Rieth, M.; Aktaa, J.; Chikada, T.; Hoffmann, A.; Hoffmann, J.; Houben, A.; Kurishita, H.; Jin, X.; Li, M.; Litnovsky, A.; Matsuo, S.; von Müller, A.; Nikolic, V.; Palacios, T.; Pippan, R.; Qu, D.; Reiser, J.; Riesch, J.; Shikama, T.; Stieglitz, R.; Weber, T.; Wurster, S.; You, J.-H.; Zhou, Z.

    2017-09-01

    Plasma-facing materials and components in a fusion reactor are the interface between the plasma and the material part. The operational conditions in this environment are probably the most challenging parameters for any material: high power loads and large particle and neutron fluxes are simultaneously impinging at their surfaces. To realize fusion in a tokamak or stellarator reactor, given the proven geometries and technological solutions, requires an improvement of the thermo-mechanical capabilities of currently available materials. In its first part this article describes the requirements and needs for new, advanced materials for the plasma-facing components. Starting points are capabilities and limitations of tungsten-based alloys and structurally stabilized materials. Furthermore, material requirements from the fusion-specific loading scenarios of a divertor in a water-cooled configuration are described, defining directions for the material development. Finally, safety requirements for a fusion reactor with its specific accident scenarios and their potential environmental impact lead to the definition of inherently passive materials, avoiding release of radioactive material through intrinsic material properties. The second part of this article demonstrates current material development lines answering the fusion-specific requirements for high heat flux materials. New composite materials, in particular fiber-reinforced and laminated structures, as well as mechanically alloyed tungsten materials, allow the extension of the thermo-mechanical operation space towards regions of extreme steady-state and transient loads. Self-passivating tungsten alloys, demonstrating favorable tungsten-like plasma-wall interaction behavior under normal operation conditions, are an intrinsic solution to otherwise catastrophic consequences of loss-of-coolant and air ingress events in a fusion reactor. Permeation barrier layers avoid the escape of tritium into structural and cooling

  17. Ploidy Manipulation of Zebrafish Embryos with Heat Shock 2 Treatment

    OpenAIRE

    Baars, Destiny L.; Takle, Kendra A.; Heier, Jonathon; Pelegri, Francisco

    2016-01-01

    Manipulation of ploidy allows for useful transformations, such as diploids to tetraploids, or haploids to diploids. In the zebrafish Danio rerio, specifically the generation of homozygous gynogenetic diploids is useful in genetic analysis because it allows the direct production of homozygotes from a single heterozygous mother. This article describes a modified protocol for ploidy duplication based on a heat pulse during the first cell cycle, Heat Shock 2 (HS2). Through inhibition of centriole...

  18. Interactions between goethite particles subjected to heat treatment

    DEFF Research Database (Denmark)

    Madsen, Daniel Esmarch; Hansen, Mikkel Fougt; Koch, C.B.

    2008-01-01

    We have studied the effect of heating on the magnetic properties of particles of nanocrystalline goethite by use of Mossbauer spectroscopy. Heating at 150 degrees C for 24 h leads to a change in the quadrupole shift in the low-temperature spectra, indicating a rotation of the sublattice...... magnetization directions. Fitting of quantiles, derived from the asymmetrically broadened spectra between 80 and 300 K, to the superferromagnetism model indicates that this change is due to a stronger magnetic coupling between the particles....

  19. Behaviour of candidate materials for fusion applications under high surface heat loads

    International Nuclear Information System (INIS)

    Bolt, H.; Nickel, H.; Kuroda, T.; Miyahara, A.

    1988-07-01

    High heat fluxes to in-vessel components of nuclear fusion devices (tokamaks) during normal operation and abnormal operation conditions are one of the governing issues in the selection of a plasma facing material and the design of first wall components. Their failure under high heat loads during service can severely influence the further operability of the entire fusion device. In order to determine the response of candidate materials to high heat fluxes an experimental program was carried out using the 10 MW Neutral Beam Injection Test Stand of the Institute for Plasma Physics of Nagoya University. Metal samples, 13 different fine grain graphites, carbon - carbon composites, and pyrolytic carbon samples were subjected to heat loads between 16 and 117 MW/m 2 and pulse durations of 50 to 950 ms. Afterwards the resulting structural changes as well as threshold values for the occurance of material damage were determined. The main damage observed on carbon materials was cracking in the case of graphites and pyrolytic carbon and erosion in the case of graphites and carbon - carbon composites. Processes leading to such damage were discussed and described in form of models. Parallel to these laboratory experiments numerical analyses of the response of graphite materials to high heat fluxes were carried out. The results are in general agreement with the experimentally determined values. In order to verify the results from experiments and numerical analyses, graphite test limiters were exposed to about 900 discharges in the JIPP T-IIU tokamak. These proof tests fully confirmed the results obtained. (orig.) [de

  20. Heat Treatment Optimization and Properties Correlation for H11-Type Hot-Work Tool Steel

    Science.gov (United States)

    Podgornik, B.; Puš, G.; Žužek, B.; Leskovšek, V.; Godec, M.

    2018-02-01

    The aim of this research was to determine the effect of vacuum-heat-treatment process parameters on the material properties and their correlations for low-Si-content AISI H11-type hot-work tool steel using a single Circumferentially Notched and fatigue Pre-cracked Tensile Bar (CNPTB) test specimen. The work was also focused on the potential of the proposed approach for designing advanced tempering diagrams and optimizing the vacuum heat treatment and design of forming tools. The results show that the CNPTB specimen allows a simultaneous determination and correlation of multiple properties for hot-work tool steels, with the compression and bending strength both increasing with hardness, and the strain-hardening exponent and bending strain increasing with the fracture toughness. On the other hand, the best machinability and surface quality of the hardened hot-work tool steel are obtained for hardness values between 46 and 50 HRC and a fracture toughness below 60 MPa√m.

  1. Study on the elastic behavior of Ti-13Nb-13Zr subjected to different heat treatments

    International Nuclear Information System (INIS)

    Florencio, O.; Chaves, J.M.; Silva Junior, P.S.; Schneider, S.G.

    2010-01-01

    Study of elastic behavior of Ti-13Nb-13Zr alloy was realized through measures of anelastic relaxation (internal friction and frequency) as a function of temperature, obtained by mechanical spectroscopy using flexural vibration of the fundamental mode of the two samples, β-ST WQ heat-treated to 1170K for 30min and water quenched and β-ST WQ +670 K/3h with subsequent aging treatment at 670K for 3h. Spectra of anelastic relaxation not showed the presence of relaxation processes due to interstitial and substitutional solutes in the alloy, the dynamic elastic modulus of alloys at room temperature was 64GPa and 87GPa, respectively. After a further heat treatment at 1170K for 30 minutes, for to reduce internal stresses of the material was observed an increase in elastic modulus, with values of 87GPa and 110GPa respectively, this increment was associated with the variation of the proportions of phases α and β present in the samples, as was revealed by XRD and SEM results. (author)

  2. Optimizing Heat Treatment Process of Fe-13Cr-3Mo-3Ni Martensitic Stainless of Steel

    Science.gov (United States)

    Anwar, M. S.; Prifiharni, S.; Mabruri, E.

    2017-05-01

    The Fe-13Cr-3Mo-3Ni stainless steels are modified into martensitic stainless steels for steam turbine blades application. The working temperature of steam turbine was around 600 - 700 °C. The improvement properties of turbine blade material is necessary to maintain steam turbine work. The previous research revealed that it has corrosion resistance of Fe-13Cr-3Mo-3Ni which is better than 13Cr stainless steels in the chloride environment. In this work, the effect of heat treatment on microstructure and hardness of Fe-13Cr-3Mo-3Ni stainless steels has been studied. The steel was prepared by induction melting followed by hot forging. The steels were austenitized at 1000, 1050, and 1100 °C for 1 hour and were tempered at 600, 650, and 700 °C for 1 hour. The steels were then subjected to metallographic observation and hardness test of Rockwell C. The optimal heat treatment of Fe-13Cr-3Mo-3Ni was carried out austenitized in 1050 °C and tempered in 600 - 700 °C.

  3. Effect of Heat treatment on Hardness and Corrosion Resistance of Super Cast Iron

    Energy Technology Data Exchange (ETDEWEB)

    Lee, Roun; Kim, Young Sik [Andong National University, Andong (Korea, Republic of)

    2014-07-15

    In fossil-fuel-fired power plants, a variety of pollutants are produced from the combustion of conventional fuels such as coal, oil and gas. Major component of such pollution are ash and corrosive chemicals, which also destroy pumps and piping; by causing erosion/corrosion, pitting, and wear. In order to over come such damage, materials with high hardness and high corrosion resistance are needed. In this work, we melted super-cast-iron with excellent corrosion resistance and high hardness. To elucidate the effect of heat treatment, microstructural analysis, hardness measurement, and corrosion tests were performed. Test results revealed that the super-cast-iron had several tens better corrosion resistance than 316 L stainless steel, and it also had a high surface hardness (> HRC45). High hardness, in spite of its low carbon content (0.74%C), could resulted from a hardening heat treatment to precipitate sufficient Cr{sub 7}C{sub 3} and Cr{sub 2}3C{sub 6}. Also, it was concluded that the excellent corrosion resistance of the super-cast-iron was due to the increase of the relative chromium content by minimizing the carbon content, and by the enhancement of passive film by the addition of Cr, Mo, Cu, and W.

  4. Analysis of residual stress relief mechanisms in post-weld heat treatment

    International Nuclear Information System (INIS)

    Dong, Pingsha; Song, Shaopin; Zhang, Jinmiao

    2014-01-01

    This paper presents a recent study on weld residual stress relief mechanisms associated with furnace-based uniform post-weld heat treatment (PWHT). Both finite element and analytical methods are used to quantitatively examine how plastic deformation and creep relaxation contribute to residual stress relief process at different stages of PWHT process. The key contribution of this work to an improved understanding of furnace based uniform PWHT can be summarized as follows: (1)Plastic deformation induced stress relief during PWHT can be analytically expressed by the change in material elastic deformation capacity (or elastic deformation limit) measured in terms of material yield strength to Young's modulus ratio, which has a rather limited role in overall residual stress relief during furnace based uniform PWHT. (2)The most dominant stress relief mechanism is creep strain induced stress relaxation, as expected. However, a rapid creep strain development accompanied by a rapid residual stress reduction during heating stage before reaching PWHT temperature is shown to contribute to most of the stress relief seen in overall PWHT process, suggesting PWHT hold time can be significantly reduced as far as residual stress relief is concerned. (3)A simple engineering scheme for estimating residual stress reduction is proposed based on this study by relating material type, PWHT temperature, and component wall thickness. - Highlights: • The paper clarified effects of plastic deformation and creep relaxation on weld residual stress relief during uniform PWHT. • Creep strain development is far more important than plastic strain, mostly completed even before hold time starts. • Plastic strain development is insignificant and be analytically described by a material elastic deformation capacity parameter. • An engineering estimation scheme is proposed for determining residual stress reduction resulted from furnace based PWHT

  5. Effect of heat treatment on microstructure and mechanical properties of PIP-SiC/SiC composites

    Energy Technology Data Exchange (ETDEWEB)

    Zhao, Shuang, E-mail: zhsh6007@126.com [Key Laboratory of Advanced Ceramic Fibres and Composites, College of Aerospace and Materials Engineering, National University of Defense Technology, Changsha 410073 (China); School of Mechanical, Aerospace, and Civil Engineering, University of Manchester, Manchester M13 9PL (United Kingdom); Zhou, Xingui; Yu, Jinshan [Key Laboratory of Advanced Ceramic Fibres and Composites, College of Aerospace and Materials Engineering, National University of Defense Technology, Changsha 410073 (China); Mummery, Paul [School of Mechanical, Aerospace, and Civil Engineering, University of Manchester, Manchester M13 9PL (United Kingdom)

    2013-01-01

    Continuous SiC fibre reinforced SiC matrix composites (SiC/SiC) have been studied as materials for heat resistant and nuclear applications. Thermal stability is one of the key issues for SiC/SiC composites. In this study, 3D SiC/SiC composites are fabricated via the polymer impregnation and pyrolysis (PIP) process, and then heat treated at 1400 Degree-Sign C, 1600 Degree-Sign C and 1800 Degree-Sign C in an inert atmosphere for 1 h, respectively. The effect of heat treatment on microstructure and mechanical properties of the composites is investigated. The results indicate that the mechanical properties of the SiC/SiC composites are significantly improved after heat treatment at 1400 Degree-Sign C mainly because the mechanical properties of the matrix are greatly improved due to crystallisation. With the increasing of heat treatment temperature, the properties of the composites are conversely decreased because of severe damage of the fibres and the matrix.

  6. Dependence of radon emanation of red mud bauxite processing wastes on heat treatment

    International Nuclear Information System (INIS)

    Jobbagy, V.; Somlai, J.; Kovacs, J.; Szeiler, G.; Kovacs, T.

    2009-01-01

    Natural radioactivity content, radon emanation and some other physical characteristics of red mud were investigated, so that to identify the possibilities of the safe utilization of such material as a building material additive. Based on the radionuclide concentration, red mud is not permitted to be used directly as a building material, however, mixing of a maximum 20% red mud and 80% clay meets the requirements. The main aim of this work was to determine the dependence of the emanation factor of red mud firing temperature and some other parameters. The relevant experimental procedure was carried out in two different ways: without any additional material, and by adding a known amount of sawdust (5-35 wt%) then firing the sample at a given temperature (100-1000 deg. C). The average emanation factor of the untreated dry red mud was estimated to 20%, which decreased to about 5% at a certain heat treatment. Even lower values were found using semi-reductive atmosphere. It has been concluded that all emanation measurements results correlate well to the firing temperature, the specific surface and the pore volume.

  7. Experimental screening of carbon-base materials for impact members in isotopic heat sources

    International Nuclear Information System (INIS)

    Bansal, G.K.; Duckworth, W.H.

    1976-11-01

    Fourteen C/C composites and three reentry-grade bulk graphites were evaluated experimentally to determine their applicability for impact member use in radioisotope heat sources. The composites included the following generic types: (1) 2-D cloth lay-ups; (2) 2-D and 3-D felts; (3) 3-D weaves; (4) 3-D pierced fabrics; (5) 7-D weave; and (6) coarse polar weave. Also included was the 2-D randomly wound, resin-impregnated C/C material presently used as the impact member in the MHW RTG and commonly designated ''GIS'' (an acronym for graphite impact shell). The various materials were evaluated as energy absorbing materials. None of the materials in these tests performed appreciably better than the GIS impact member material now used in the MHW heat source, HITCO Pyro Carb 814. Two cloth lay-up composites, HITCO's Pyro Carb 903 and Carborundum's Carbitex 700, were somewhat superior in performance, while the bulk graphites and felt-base composites ranked least effective as energy absorbers. All experimental data and other factors considered to date suggest that Pyro Carb 903 is the best prospect for a bifunctional heat shield and impact member. Its high density (1.80 g/cm 3 ) indicates potentially good ablation resistance to accompany its indicated good performance as an energy absorber

  8. Assessment of weld heat-affected zones in a reactor vessel material

    International Nuclear Information System (INIS)

    Marston, T.U.; Server, W.

    1978-01-01

    The mechanical properties of weld heat-affected zones (HAZ's) associated with the heavy section, nuclear quality weldments are evaluated and found to be superior to those of the parent base material. The nil ductility transition temperature (NDTT), Charpy impact and static and dynamic fracture toughness properties of a HAZ associated with a submerged arc weld and one associated with a manual metal arc weld are directly compared with those of the parent base material. It is concluded that the stigma normally associated with HAZ is not justified for this grade and quality of material and weld procedure

  9. A small-plane heat source method for measuring the thermal conductivities of anisotropic materials

    Science.gov (United States)

    Cheng, Liang; Yue, Kai; Wang, Jun; Zhang, Xinxin

    2017-07-01

    A new small-plane heat source method was proposed in this study to simultaneously measure the in-plane and cross-plane thermal conductivities of anisotropic insulating materials. In this method the size of the heat source element is smaller than the sample size and the boundary condition is thermal insulation due to no heat flux at the edge of the sample during the experiment. A three-dimensional model in a rectangular coordinate system was established to exactly describe the heat transfer process of the measurement system. Using the Laplace transform, variable separation, and Laplace inverse transform methods, the analytical solution of the temperature rise of the sample was derived. The temperature rises calculated by the analytical solution agree well with the results of numerical calculation. The result of the sensitivity analysis shows that the sensitivity coefficients of the estimated thermal conductivities are high and uncorrelated to each other. At room temperature and in a high-temperature environment, experimental measurements of anisotropic silica aerogel were carried out using the traditional one-dimensional plane heat source method and the proposed method, respectively. The results demonstrate that the measurement method developed in this study is effective and feasible for simultaneously obtaining the in-plane and cross-plane thermal conductivities of the anisotropic materials.

  10. Gas Furnace with Pulsed Feeding of the Heating Agent for Volume Precision Heat Treatment of CCM Rolls

    Science.gov (United States)

    Moroz, V. I.; Egorova, V. M.; Gusev, S. V.

    2001-05-01

    A standard chamber batch furnace of the Severstal' plant has been modified for precision heat treatment of CCM rolls. The certification tests of a charge of rolls from steel 24KhM1F have shown the technical and economical advantages of the new design.

  11. Review of thermo-physical properties, wetting and heat transfer characteristics of nanofluids and their applicability in industrial quench heat treatment.

    Science.gov (United States)

    Ramesh, Gopalan; Prabhu, Narayan Kotekar

    2011-04-14

    The success of quenching process during industrial heat treatment mainly depends on the heat transfer characteristics of the quenching medium. In the case of quenching, the scope for redesigning the system or operational parameters for enhancing the heat transfer is very much limited and the emphasis should be on designing quench media with enhanced heat transfer characteristics. Recent studies on nanofluids have shown that these fluids offer improved wetting and heat transfer characteristics. Further water-based nanofluids are environment friendly as compared to mineral oil quench media. These potential advantages have led to the development of nanofluid-based quench media for heat treatment practices. In this article, thermo-physical properties, wetting and boiling heat transfer characteristics of nanofluids are reviewed and discussed. The unique thermal and heat transfer characteristics of nanofluids would be extremely useful for exploiting them as quench media for industrial heat treatment.

  12. Review of thermo-physical properties, wetting and heat transfer characteristics of nanofluids and their applicability in industrial quench heat treatment

    Directory of Open Access Journals (Sweden)

    Ramesh Gopalan

    2011-01-01

    Full Text Available Abstract The success of quenching process during industrial heat treatment mainly depends on the heat transfer characteristics of the quenching medium. In the case of quenching, the scope for redesigning the system or operational parameters for enhancing the heat transfer is very much limited and the emphasis should be on designing quench media with enhanced heat transfer characteristics. Recent studies on nanofluids have shown that these fluids offer improved wetting and heat transfer characteristics. Further water-based nanofluids are environment friendly as compared to mineral oil quench media. These potential advantages have led to the development of nanofluid-based quench media for heat treatment practices. In this article, thermo-physical properties, wetting and boiling heat transfer characteristics of nanofluids are reviewed and discussed. The unique thermal and heat transfer characteristics of nanofluids would be extremely useful for exploiting them as quench media for industrial heat treatment.

  13. Development, Testing, and Failure Mechanisms of a Replicative Ice Phase Change Material Heat Exchanger

    Science.gov (United States)

    Leimkuehler, Thomas O.; Hansen, Scott; Stephan, Ryan A.

    2010-01-01

    Phase change materials (PCM) may be useful for thermal control systems that involve cyclical heat loads or cyclical thermal environments such as Low Earth Orbit (LEO) and Low Lunar Orbit (LLO). Thermal energy can be stored in the PCM during peak heat loads or in adverse thermal environments. The stored thermal energy can then be released later during minimum heat loads or in more favorable thermal environments. One advantage that PCM's have over evaporators in this scenario is that they do not use a consumable. Wax PCM units have been baselined for the Orion thermal control system and also provide risk mitigation for the Altair Lander. However, the use of water as a PCM has the potential for significant mass reduction since the latent heat of formation of water is approximately 70% greater than that of wax. One of the potential drawbacks of using ice as a PCM is its potential to rupture its container as water expands upon freezing. In order to develop a space qualified ice PCM heat exchanger, failure mechanisms must first be understood. Therefore, a methodical experimental investigation has been undertaken to demonstrate and document specific failure mechanisms due to ice expansion in the PCM. An ice PCM heat exchanger that replicates the thermal energy storage capacity of an existing wax PCM unit was fabricated and tested. Additionally, methods for controlling void location in order to reduce the risk of damage due to ice expansion are investigated. This paper presents the results to date of this investigation. Nomenclature

  14. Testing and Failure Mechanisms of Ice Phase Change Material Heat Exchangers

    Science.gov (United States)

    Leimkuehler, Thomas O.; Stephan, Ryan A.; Hawkins-Reynolds, Ebony

    2011-01-01

    Phase change materials (PCM) may be useful for thermal control systems that involve cyclical heat loads or cyclical thermal environments such as specific spacecraft orientations in Low Earth Orbit (LEO) and low beta angle Low Lunar Orbit (LLO). Thermal energy can be stored in the PCM during peak heat loads or in adverse thermal environments. The stored thermal energy can then be released later during minimum heat loads or in more favorable thermal environments. One advantage that PCM s have over evaporators in this scenario is that they do not use a consumable. The use of water as a PCM rather than the more traditional paraffin wax has the potential for significant mass reduction since the latent heat of formation of water is approximately 70% greater than that of wax. One of the potential drawbacks of using ice as a PCM is its potential to rupture its container as water expands upon freezing. In order to develop a space qualified ice PCM heat exchanger, failure mechanisms must first be understood. Therefore, a methodical experimental investigation has been undertaken to demonstrate and document specific failure mechanisms due to ice expansion in the PCM. A number of ice PCM heat exchangers were fabricated and tested. Additionally, methods for controlling void location in order to reduce the risk of damage due to ice expansion were investigated. This paper presents the results of testing that occurred from March through September of 2010 and builds on testing that occurred during the previous year.

  15. Performance analysis of phase-change material storage unit for both heating and cooling of buildings

    Science.gov (United States)

    Waqas, Adeel; Ali, Majid; Ud Din, Zia

    2017-04-01

    Utilisation of solar energy and the night ambient (cool) temperatures are the passive ways of heating and cooling of buildings. Intermittent and time-dependent nature of these sources makes thermal energy storage vital for efficient and continuous operation of these heating and cooling techniques. Latent heat thermal energy storage by phase-change materials (PCMs) is preferred over other storage techniques due to its high-energy storage density and isothermal storage process. The current study was aimed to evaluate the performance of the air-based PCM storage unit utilising solar energy and cool ambient night temperatures for comfort heating and cooling of a building in dry-cold and dry-hot climates. The performance of the studied PCM storage unit was maximised when the melting point of the PCM was ∼29°C in summer and 21°C during winter season. The appropriate melting point was ∼27.5°C for all-the-year-round performance. At lower melting points than 27.5°C, declination in the cooling capacity of the storage unit was more profound as compared to the improvement in the heating capacity. Also, it was concluded that the melting point of the PCM that provided maximum cooling during summer season could be used for winter heating also but not vice versa.

  16. Theoretical model of an evacuated tube heat pipe solar collector integrated with phase change material

    International Nuclear Information System (INIS)

    Naghavi, M.S.; Ong, K.S.; Badruddin, I.A.; Mehrali, M.; Silakhori, M.; Metselaar, H.S.C.

    2015-01-01

    The purpose of this paper is to model theoretically a solar hot water system consisting of an array of ETHPSC (evacuated tube heat pipe solar collectors) connected to a common manifold filled with phase change material and acting as a LHTES (latent heat thermal energy storage) tank. Solar energy incident on the ETHPSC is collected and stored in the LHTES tank. The stored heat is then transferred to the domestic hot water supply via a finned heat exchanger pipe placed inside the tank. A combination of mathematical algorithms is used to model a complete process of the heat absorption, storage and release modes of the proposed system. The results show that for a large range of flow rates, the thermal performance of the ETHPSC-LHTES system is higher than that of a similar system without latent heat storage. Furthermore, the analysis shows that the efficiency of the introduced system is less sensitive to the draw off water flowrate than a conventional system. Analysis indicates that this system could be applicable as a complementary part to conventional ETHPSC systems to be able to produce hot water at night time or at times with weak radiation. - Highlights: • The ETHPSC is integrated with PCM at manifold side for night hot water demands. • The thermal performance of the ETHPSC-PCM is often higher than the baseline model. • The efficiency of the proposed model is stable for different flow rates. • Using PCM as thermal storage increases reliability on the performance of the system.

  17. Influence of inductive heating on microstructure and material properties in roll forming processes

    Science.gov (United States)

    Guk, Anna; Kunke, Andreas; Kräusel, Verena; Landgrebe, Dirk

    2017-10-01

    The increasing demand for sheet metal parts and profiles with enhanced mechanical properties by using high and ultra-high-strength (UHS) steels for the automotive industry must be covered by increasing flexibility of tools and machines. This can be achieved by applying innovative technologies such as roll forming with integrated inductive heating. This process is similar to indirect press hardening and can be used for the production of hardened profiles and profiles with graded properties in longitudinal and traverse direction. The advantage is that the production of hardened components takes place in a continuous process and the integration of heating and quenching units in the profiling system increases flexibility, accompanied by shortening of the entire process chain and minimizing the springback risk. The features of the mentioned process consists of the combination of inhomogeneous strain distribution over the stripe width by roll forming and inhomogeneity of microstructure by accelerated inductive heating to austenitizing temperature. Therefore, these two features have a direct influence on the mechanical properties of the material during forming and hardening. The aim of this work is the investigation of the influence of heating rates on microstructure evolution and mechanical properties to determine the process window. The results showed that heating rate should be set at 110 K/s for economic integration of inductive heating into the roll forming process.

  18. Investigations into the influence of the tup velocity and the heat treatment on the dynamic fracture toughness of Inconel 625

    International Nuclear Information System (INIS)

    Krompholz, K.; Tipping, P.; Ullrich, G.

    1983-09-01

    Experiments were performed with an instrumented impact machine using different drop heights, on the nickel base alloy Inconel 625 in the as received state and after heat treatment for about 1000 h at 923 K. The absorbed impact energy can be obtained either by the direct dial reading, by the integration of the load versus load point displacement diagram or by the integration of the load versus time diagram, knowing the initial impact velocity of the tup. In all cases the agreement was excellent. It is shown that, (i) the dynamic fracture toughness is dependent on the tup velocity and as a consequence on the total energy of the hammer at the different drop heights; (ii) the embrittlement during heat treatment is not combined with a decrease in the fracture toughness although a strong decrease in the absorbed impact energy is observed; (iii) defining a dynamic stress from the velocity dependence of the fracture toughness, the stress is higher for the embrittled material - a tendency verified by tensile tests; (iv) the dynamic fracture toughness can be correlated with the absorbed impact energy up to the load maximum for the heat treated material while the as received material exhibits no such dependency. The change in the tup velocity during the impact process is only small for this type of material. (Auth.)

  19. Dynamical Treatment of Virialization Heating in Galaxy Formation

    Science.gov (United States)

    Wang, Peng; Abel, Tom

    2008-01-01

    In a hierarchical picture of galaxy formation virialization continually transforms gravitational potential energy into kinetic energies of the baryonic and dark matter. For the gaseous component the kinetic, turbulent energy is transformed eventually into internal thermal energy through shocks and viscous dissipation. Traditionally this virialization and shock heating has been assumed to occur instantaneously, allowing an estimate of the gas temperature to be derived from the virial temperature defined from the embedding dark matter halo velocity dispersion. As the mass grows the virial temperature of a halo grows. Mass accretion hence can be translated into a heating term. We derive this heating rate from the extended Press Schechter formalism and demonstrate its usefulness in semianalytical models of galaxy formation. Our method explicitly conserves energy, unlike the previous impulsive heating assumptions. Our formalism can trivially be applied in all current semianalytical models as the heating term can be computed directly from the underlying merger trees. Our analytic results for the first cooling halos and the transition from cold to hot accretion are in agreement with numerical simulations.

  20. ANALYSIS OF THERMAL PROPERTIES AND HEAT LOSS IN CONSTRUCTION AND ISOTHERMAL MATERIALS OF MULTILAYER BUILDING WALLS

    Directory of Open Access Journals (Sweden)

    Arkadiusz Urzędowski

    2017-06-01

    Full Text Available The article discusses the impact of vertical partition, technology on thermal insulation of the building, and the resulting savings and residents thermal comfort. The study is carried out as an analysis of three selected design solutions including such materials as: aerated concrete elements, polystyrene, ceramic elements, concrete, mineral plaster. Simulation results of heat transfer in a multi-layered wall, are subjected to detailed analysis by means of thermal visual methods. The study of existing structures, helped to identify the local point of heat loss by means of infrared technology leading to determination of U-value reduction by 36% in maximum for the described 3 types of structure.

  1. Specific heats of lunar surface materials from 90 to 350 degrees Kelvin

    Science.gov (United States)

    Robie, R.A.; Hemingway, B.S.; Wilson, W.H.

    1970-01-01

    The specific heats of lunar samples 10057 and 10084 returned by the Apollo 11 mission have been measured between 90 and 350 degrees Kelvin by use of an adiabatic calorimeter. The samples are representative of type A vesicular basalt-like rocks and of finely divided lunar soil. The specific heat of these materials changes smoothly from about 0.06 calorie per gram per degree at 90 degrees Kelvin to about 0.2 calorie per gram per degree at 350 degrees Kelvin. The thermal parameter ??=(k??C)-1/2 for the lunar surface will accordingly vary by a factor of about 2 between lunar noon and midnight.

  2. Experimental and analytical investigations of granular materials: Shear flow and convective heat transfer

    Science.gov (United States)

    Ahn, Hojin

    1989-12-01

    Granular materials flowing down an inclined chute were studied experimentally and analytically. Characteristics of convective heat transfer to granular flows were also investigated experimentally and numerically. Experiments on continuous, steady flows of granular materials in an inclined chute were conducted with the objectives of understanding the characteristics of chute flows and of acquiring information on the rheological behavior of granular material flow. Existing constitutive equations and governing equations were used to solve for fully developed chute flows of granular materials, and thus the boundary value problem was formulated with two parameters (the coefficient of restitution between particles, and the chute inclination) and three boundary values at the chute base wall (the values of solid fraction, granular temperature, and mean velocity at the wall). The boundary value problem was numerically solved by the shooting method. These analytical results were also compared with the present experimental values and with the computer simulations by other investigators in their literature. Experiments on heat transfer to granular flows over a flat heating plate were conducted with three sizes of glass beads, polystyrene beads, and mustard seeds. A modification on the existing model for the convective heat transfer was made using the effective Nusselt number and the effective Peclet number, which include the effects of solid fraction variations. The slightly modified model could describe the heat transfer characteristics of both fast and slow flows (supercritical and subcritical). A numerical analysis of the transfer to granular flows was also performed. The results were compared with the present experimental data, and reasonable agreement was found in the comparison.

  3. Division of Development and Technology Plasma/Materials Interaction and High Heat Flux Materials and Components Task Groups: Report on the joint meeting, July 9, 1986

    International Nuclear Information System (INIS)

    Watson, R.D.

    1986-09-01

    This paper contains a collection of viewgraphs from a joint meeting of the Division of Development and Technology Plasma/Materials Interaction and High Heat Flux Materials and Components Task Groups. A list of contributing topics is: PPPL update, ATF update, Los Alamos RFP program update, status of DIII-D, PMI graphite studies at ORNL, PMI studies for low atomic number materials, high heat flux materials issues, high heat flux testing program, particle confinement in tokamaks, helium self pumping, self-regenerating coatings technical planning activity and international collaboration update

  4. Steam reforming as an alternative technique for treatment of oil sludge containing naturally occurring radioactive material

    International Nuclear Information System (INIS)

    Norasalwa Zakaria; Muhd Noor Muhd Yunus; Mohd Khairi Muhd Said; Mohamad Azman Che Mat Isa; Mohd Puad Abu

    2004-01-01

    Steam reforming treatment system is an innovative technology that holds a potential to treat mixed waste containing radioactive material. The system is utilizing the thermal heat of the superheated steam at 500 degree C to produce combustible gases and integrates it with ash melting at 1400 degree C for final destruction. In this system, liquids are evaporated, organics are converted into a hydrogen-rich gas, chlorinated compounds are converted in hydrochloric acid, and reactive chemicals in the waste containing radionuclide and heavy metals are converted into the stable product through ash melting dioxins and furans are not formed, but instead are destroyed in the reducing environment of the system. No secondary pollutants are produced from the system that requires subsequent treatment. The system is divided into three development stages, and currently the project is progressing at development stage 1. This project is an entailment of a concentrated effort to solve oil sludge containing radioactive material treatment issue. (Author)

  5. Improvement of high temperature fatigue lifetime in AZ91 magnesium alloy by heat treatment

    Energy Technology Data Exchange (ETDEWEB)

    Mokhtarishirazabad, Mehdi [School of Metallurgy and Materials Engineering, Iran University of Science and Technology, Tehran (Iran, Islamic Republic of); Azadi, Mohammad, E-mail: m_azadi@ip-co.com [Fatigue and Wear Workgroup, Irankhodro Powertrain Company (IPCO), Tehran (Iran, Islamic Republic of); Hossein Farrahi, Gholam [School of Mechanical Engineering, Sharif University of Technology, Tehran (Iran, Islamic Republic of); Winter, Gerhard; Eichlseder, Wilfred [Chair of Mechanical Engineering, University of Leoben, Leoben (Austria)

    2013-12-20

    In the present paper, an improvement in high temperature fatigue properties of the AZ91 magnesium alloy with rare earth elements has been obtained by a typical heat treatment, denoted by T6. For this objective, out-of-phase thermo-mechanical fatigue, room temperature and high temperature low cycle fatigue tests are performed to compare lifetimes. Several rare earth elements are initially added to the AZ91 alloy during a gravity casting process in permanent molds. Also, the type of the heat treatment is examined. Results of specimens with only the solution (the T4 heat treatment) and the solution with the ageing process (the T6 heat treatment) are compared under isothermal fatigue loadings. Microstructural investigations are carried out, before and after fatigue experiments to demonstrate the heat treatment effect. Results showed that both low cycle fatigue and thermo-mechanical fatigue of the alloy at high temperatures increases tremendously after the T6 heat treatment. This behavior attributes to the variation of the ductility, which was a result of microstructural changes during the heat treatment and the varying temperature in fatigue tests.

  6. Improvement of high temperature fatigue lifetime in AZ91 magnesium alloy by heat treatment

    International Nuclear Information System (INIS)

    Mokhtarishirazabad, Mehdi; Azadi, Mohammad; Hossein Farrahi, Gholam; Winter, Gerhard; Eichlseder, Wilfred

    2013-01-01

    In the present paper, an improvement in high temperature fatigue properties of the AZ91 magnesium alloy with rare earth elements has been obtained by a typical heat treatment, denoted by T6. For this objective, out-of-phase thermo-mechanical fatigue, room temperature and high temperature low cycle fatigue tests are performed to compare lifetimes. Several rare earth elements are initially added to the AZ91 alloy during a gravity casting process in permanent molds. Also, the type of the heat treatment is examined. Results of specimens with only the solution (the T4 heat treatment) and the solution with the ageing process (the T6 heat treatment) are compared under isothermal fatigue loadings. Microstructural investigations are carried out, before and after fatigue experiments to demonstrate the heat treatment effect. Results showed that both low cycle fatigue and thermo-mechanical fatigue of the alloy at high temperatures increases tremendously after the T6 heat treatment. This behavior attributes to the variation of the ductility, which was a result of microstructural changes during the heat treatment and the varying temperature in fatigue tests

  7. The Effect of Heat Treatment on the Crystallography and Mineral Magnetism of Pyrrhotite

    Science.gov (United States)

    Hobart, K.; Feinberg, J. M.; Jones, D. S.

    2017-12-01

    Pyrrhotite (Fe1-xS, 0 ≤ x ≤ 0.125) is the second most common sulfide mineral after pyrite in the Earth's crust, and its properties are of interest to a wide variety of scientific disciplines, including electrical engineering, physical chemistry, planetary geology and meteoritics, and economic geology. The physical properties of pyrrhotite are highly dependent on slight variations in composition and the ordering of iron vacancies, resulting in a number of possible phases between the endmember compositions of FeS and Fe7S8­­. A common complication in studies on pyrrhotite is that different phases are frequently intergrown, making it difficult to isolate a natural single phase. This has led many researchers to rely on synthesis techniques, which produce a specific structure by using precise iron/sulfur ratios, heating protocols, and controlled cooling. One of the most common synthesis treatments used to create 4C pyrrhotite is an extended heating and annealing process, which is believed to allow the reordering of vacancies to a more thermodynamically stable, ordered state with elevated saturation magnetization. The process was first studied in detail by Schwarz and Vaughan (1972) who produced synthetic pyrrhotite at varying Fe/S ratios with annealing at either 700, 300, or 144°C. The most common method for producing 4C pyrrhotite is heating at 500°C for 24 hours under a vacuum followed by annealing at 250°C for 50 hours. While this technique has been broadly applied in diverse disciplines, there is debate about whether it produces ferrimagnetic, monoclinic 4C pyrrhotite or a different metastable disordered phase. We examined this process using a combination of rock magnetic, X-ray diffraction, and electron imaging techniques to study the effect of heating and annealing on a natural sample of pyrrhotite. Due to the lack of a Besnus transition in the annealed material, our data suggest that the increased magnetization we found following annealing, rather than

  8. Using a quasi-heat-pulse method to determine heat and moisture transfer properties for porous orthotropic wood products or cellular solid materials

    Science.gov (United States)

    M. A. Dietenberger

    2006-01-01

    Understanding heat and moisture transfer in a wood specimen as used in the K-tester has led to an unconventional numerical solution arid intriguing protocol to deriving the transfer properties. Laplace transform solutions of Luikov’s differential equations are derived for one-dimensional heat and moisture transfer in porous hygroscopic orthotropic materials and for a...

  9. Numerical simulation of the cladding of a ferritic block with a stainless steel. Study of post-weld heat treatment

    International Nuclear Information System (INIS)

    Dupas, P.; Carayol, R.

    1994-06-01

    This report presents the calculation results of post-weld heat treatment, using the SYSWELD finite element program. Starting from the metallurgical and mechanical states obtained after welding, we performed a numerical heat treatment over the clad block. The principle is to relieve residual stresses by transforming elastic energy into plastic or viscoplastic energy. Increasing the temperature may lead to this result by decreasing yield stress, by creep or by changes of material properties due to structural transformations. Another way of relieving stresses is the transformation plasticity, but we don't use it in our simulation. Some experimental results lead us to believe we should have stresses from 200 to 300 MPa in the weld metal and from - 100 to 100 MPa in the HAZ, whatever are the stresses before heat treatment. Moreover, transverse and longitudinal stresses should have similar values and profile in depth. As in welding simulation, heat treatment calculations are two dimensional. They can be split in a thermo-metallurgical calculation followed by a mechanical one. The following parameters are studied : metallurgy, plastic and viscoplastic behaviour, plane strain or generalized plane strain model. The creep model used in SYSWELD has been more particularly studied. We also study the possibility to simplify calculations by simulating only the cooling, starting from no stresses at 610 deg C, which is a usual method in crack assessment. (authors). 23 refs., 52 figs., 3 annexes

  10. Modeling Precipitation Kinetics During Heat Treatment with Calphad-Based Tools

    Science.gov (United States)

    Chen, Qing; Wu, Kaisheng; Sterner, Gustaf; Mason, Paul

    2014-12-01

    Sophisticated precipitation reaction models combined with well-developed CALPHAD databases provide an efficient way to tailor precipitate microstructures that maximize strengthening via the optimization of alloy chemistries and heat treatment schedules. The success of the CALPHAD approach relies on the capability to provide fundamental phase equilibrium and phase transformation information in materials of industrial relevance taking into consideration composition and temperature variation. The newly developed TC-PRISMA program is described. The effect of growth modes, alloy chemistries, and cooling profiles on the formation of multimodal microstructures has been examined in order to understand the underlying thermodynamics and kinetics. Practical issues that are critical to the accuracy and applicability of the current simulations, such as modifications that overcome mean field approximations, compatibility between CALPHAD databases, and selections of key parameters (particularly interfacial energy and nucleation site densities), are also addressed.

  11. Effect of Heat Treatment on Microstructure and Hardness of Grade 91 Steel

    Directory of Open Access Journals (Sweden)

    Triratna Shrestha

    2015-01-01

    Full Text Available Grade 91 steel (modified 9Cr-1Mo steel is considered a prospective material for the Next Generation Nuclear Power Plant for application in reactor pressure vessels at temperatures of up to 650 °C. In this study, heat treatment of Grade 91 steel was performed by normalizing and tempering the steel at various temperatures for different periods of time. Optical microscopy, scanning and transmission electron microscopy in conjunction with microhardness profiles and calorimetric plots were used to understand the microstructural evolution including precipitate structures and were correlated with mechanical behavior of the steel. Thermo-Calc™ calculations were used to support the experimental work. Furthermore, carbon isopleth and temperature dependencies of the volume fraction of different precipitates were constructed.

  12. Influence of composition, heat treatment and neutron irradiation on the electrical conductivity of copper alloys

    DEFF Research Database (Denmark)

    Eldrup, Morten Mostgaard; Singh, B.N.

    1998-01-01

    The electrical conductivity of three different types of copper alloys, viz. CuNiBe, CuCrZr and Cu-Al(2)O(3) as well as of pure copper are reported. The alloys have undergone different pre-irradiation heat treatments and have been fission-neutron irradiated up to 0.3 dpa. In some cases post......-irradiation annealing has been carried out. The results are discussed with reference to equivalent Transmission Electron Microscopy results on the microstructure of the materials. The CuNiBe has the lowest conductivity (less than or equal to 55% of that of pure Cu), and Cu-Al(2)O(3) the highest (75-90% of pure Cu). (C...

  13. Influence of composition, heat treatment and neutron irradiation on the electrical conductivity of copper alloys

    Science.gov (United States)

    Eldrup, M.; Singh, B. N.

    1998-10-01

    The electrical conductivity of three different types of copper alloys, viz. CuNiBe, CuCrZr and Cu-Al 2O 3 as well as of pure copper are reported. The alloys have undergone different pre-irradiation heat treatments and have been fission-neutron irradiated up to 0.3 dpa. In some cases post-irradiation annealing has been carried out. The results are discussed with reference to equivalent Transmission Electron Microscopy results on the microstructure of the materials. The CuNiBe has the lowest conductivity (⩽55% of that of pure Cu), and Cu-Al 2O 3 the highest (75-90% of pure Cu).

  14. Gemstone enhancement. Heat, irradiation, impregnation, dyeing, and other treatments which alter the appearance of gemstones, and the detection of such treatments

    Energy Technology Data Exchange (ETDEWEB)

    Nassau, K.

    1984-01-01

    One of the important tasks of the gemologist is to identify treatments which may have been used to modify the colour or appearance of the gemstones being examined. The book is written for gemologists, to explain the details of possible treatment techniques. An historical account of treatments is given in chapter 2, general accounts of heat treatments in chapter 3, irradiations in chapter 4 and miscellaneous techniques (including impregnation and dyeing) in chapter 5. Chapter 6 is a brief discussion of the identification techniques used to reveal treatments. In chapter 7 the various gemstone materials are considered alphabetically, by groups. The irradiation treatments considered in chapter 4 start by summarising and explaining the rays and particles used for the irradiation of gemstones. The major colour changes that occur on irradiation are tabulated. Colour centres are explained. Colour-centre-like colour changes are mentioned. Finally, radioactive gemstones are considered.

  15. Evaluation of materials for heat exchanging components in advanced helium-cooled reactors

    International Nuclear Information System (INIS)

    Schubert, F.

    1984-01-01

    The qualification of metallic materials for advanced HTR applications is based on creep behaviour, fatigue properties, structural stability and corrosion resistance. A brief state of the art is provided for the materials for heat exchanging components. The experimental results are treated with respect to the importance for the design, the characteristic of time-depend materials behaviour are evaluated. Of specific interest are the possible effects of helium on the mechanical properties. Helium, which serves as primary coolant, contains traces of reactive impurities such as hydrogen, methane, carbon monoxide and water vapor. The evaluation of the HTR materials program serves as basis for structural design rules of components with operation temperatures above 800 deg C. The materials mechanical topics are discussed. Alloy improvement and the progress in development of new alloys are reviewed. (author)

  16. Evaluation of dry heat treatment of soft wheat flour for the production of high ratio cakes.

    Science.gov (United States)

    Keppler, S; Bakalis, S; Leadley, C E; Sahi, S S; Fryer, P J

    2018-05-01

    An accurate method to heat treat flour samples has been used to quantify the effects of heat treatment on flour functionality. A variety of analytical methods has been used such as oscillatory rheology, rheomixer, solvent retention capacity tests, and Rapid Visco Analysis (RVA) in water and in aqueous solutions of sucrose, lactic acid, and sodium carbonate. This work supports the hypothesis that heat treatment facilitates the swelling of starch granules at elevated temperature. Results furthermore indicated improved swelling ability and increased interactions of flour polymers (in particular arabinoxylans) of heat treated flour at ambient conditions. The significant denaturation of the proteins was indicated by a lack of gluten network formation after severe heat treatments as shown by rheomixer traces. Results of these analyses were used to develop a possible cake flour specification. A method was developed using response surfaces of heat treated flour samples in the RVA using i) water and ii) 50% sucrose solution. This can uniquely characterise the heat treatment a flour sample has received and to establish a cake flour specification. This approach might be useful for the characterisation of processed samples, rather than by baking cakes. Hence, it may no longer be needed to bake a cake after flour heat treatment to assess the suitability of the flour for high ratio cake production, but 2 types of RVA tests suffice. Copyright © 2018 The Authors. Published by Elsevier Ltd.. All rights reserved.

  17. Effect of heat treatment upon the fatigue-crack growth behavior of Alloy 718 weldments

    International Nuclear Information System (INIS)

    James, L.A.; Mills, W.J.

    1981-05-01

    Gas-tungsten-arc weldments in Alloy 718 were studied in fatigue-crack growth test conducted at five temperatures over the range 24--649 degree C. In general, crack growth rates increased with increasing temperature, and weldments given the ''conventional'' post-weld heat-treatment generally exhibited crack growth rates that were higher than for weldments given the ''modified'' (INEL) heat-treatment. Limited testing in the as-welded condition revealed crack growth rates significantly lower than observed for the heat-treated cases, and this was attributed to residual stresses. Three different heats of filler wire were utilized, and no heat-to-heat variations were noted. 23 refs., 9 figs., 6 tabs

  18. The heat storage material based on paraffin-modified multilayer carbon nanotubes with Nickel-zinc ferrite

    Science.gov (United States)

    Shchegolkov, A.; Shchegolkov, A.; Dyachkova, T.; Semenov, A.

    2018-02-01

    The paper presents an investigation of magnetically controlled heat-storage material based on paraffin, modified with multilayer carbon nanotubes with nickel-zinc ferrite. The technology of obtaining nanomodified material capable of interacting with magnetic field is presented. The study of the heat-exchange processes of charge/discharge with the help of magnetic field are carried out.

  19. Optimisation of the T6 heat treatment of rheocast alloy A356

    CSIR Research Space (South Africa)

    Moller, H

    2007-11-01

    Full Text Available popular solution heat treatment employed for SSM processed A356 is 6 hours at 540oC (i.e. similar to that used for permanent mould cast A356)6,7,9. Only limited work has been performed on the optimisation of the solution heat treatment of SSM processed... was not adequately studied by either Dewhirst8 or Rosso and Actis Grande5. The optimum artificial aging heat treatment proposed in both papers5,8 is 180oC for 4 hours. This was also confirmed in this work, but importantly, this applies only when natural aging...

  20. Experimental Investigation on the Specific Heat of Carbonized Phenolic Resin-Based Ablative Materials

    Science.gov (United States)

    Zhao, Te; Ye, Hong; Zhang, Lisong; Cai, Qilin

    2017-10-01

    As typical phenolic resin-based ablative materials, the high silica/phenolic and carbon/phenolic composites are widely used in aerospace field. The specific heat of the carbonized ablators after ablation is an important thermophysical parameter in the process of heat transfer, but it is rarely reported. In this investigation, the carbonized samples of the high silica/phenolic and carbon/phenolic were obtained through carbonization experiments, and the specific heat of the carbonized samples was determined by a 3D DSC from 150 °C to 970 °C. Structural and compositional characterizations were performed to determine the mass fractions of the fiber and the carbonized product of phenolic which are the two constituents of the carbonized samples, while the specific heat of each constituent was also measured by 3D DSC. The masses of the carbonized samples were reduced when heated to a high temperature in the specific heat measurements, due to the thermal degradation of the carbonized product of phenolic resin in the carbonized samples. The raw experimental specific heat of the two carbonized samples and the carbonized product of phenolic resin was modified according to the quality changes of the carbonized samples presented by TGA results. Based on the mass fraction and the specific heat of each constituent, a weighted average method was adopted to obtain the calculated results of the carbonized samples. Due to the unconsolidated property of the fiber samples which impacts the reliability of the DSC measurement, there is a certain deviation between the experimental and calculated results of the carbonized samples. Considering the similarity of composition and structure, the data of quartz glass and graphite were used to substitute the specific heat of the high silica fiber and carbon fiber, respectively, resulting in better agreements with the experimental ones. Furthermore, the accurate specific heat of the high silica fiber and carbon fiber bundles was obtained by